# Electronic Supplementary Material (ESI) for Chemical Communications # This journal is © The Royal Society of Chemistry 2013 ####################################################################### # # Cambridge Crystallographic Data Centre # CCDC # ####################################################################### # # This CIF contains data from an original supplementary publication # deposited with the CCDC, and may include chemical, crystal, # experimental, refinement, atomic coordinates, # anisotropic displacement parameters and molecular geometry data, # as required by the journal to which it was submitted. # # This CIF is provided on the understanding that it is used for bona # fide research purposes only. It may contain copyright material # of the CCDC or of third parties, and may not be copied or further # disseminated in any form, whether machine-readable or not, # except for the purpose of generating routine backup copies # on your local computer system. # # For further information on the CCDC, data deposition and # data retrieval see: # www.ccdc.cam.ac.uk # # Bona fide researchers may freely download Mercury and enCIFer # from this site to visualise CIF-encoded structures and # to carry out CIF format checking respectively. # ####################################################################### data_squweeze _database_code_depnum_ccdc_archive 'CCDC 903979' #TrackingRef '14748_web_deposit_cif_file_0_YujiKikukawa_1350469596.121017_Ag6.cif' _audit_creation_date 2012-02-08T19:42:25-00:00 _audit_creation_method 'WinGX routine CIF_UPDATE' #------------------ CHEMICAL INFORMATION ------------------------------------# _chemical_formula_moiety 'C128 Ag6 N8 O72 Si2 W20' _chemical_formula_sum 'C128 Ag6 N8 O72 Si2 W20' _chemical_formula_weight 7181.76 #------------------ UNIT CELL INFORMATION -----------------------------------# _symmetry_cell_setting monoclinic _symmetry_space_group_name_H-M 'P 1 21/n 1' loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 22.3265(2) _cell_length_b 18.8039(3) _cell_length_c 27.4531(4) _cell_angle_alpha 90 _cell_angle_beta 94.39 _cell_angle_gamma 90 _cell_volume 11491.7(3) _cell_formula_units_Z 2 _cell_measurement_temperature 153 _cell_measurement_reflns_used 0 _cell_measurement_theta_min 0 _cell_measurement_theta_max 0 #------------------ CRYSTAL INFORMATION -------------------------------------# _exptl_crystal_description prism _exptl_crystal_colour yellow _exptl_crystal_size_max 0.2 _exptl_crystal_size_mid 0.2 _exptl_crystal_size_min 0.2 _exptl_crystal_density_diffrn 2.076 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 6380 _exptl_absorpt_coefficient_mu 10.532 _exptl_absorpt_correction_type none #------------------ DATA COLLECTION INFORMATION -----------------------------# _diffrn_radiation_wavelength 0.71069 _diffrn_radiation_type MoK\a _diffrn_radiation_probe x-ray _diffrn_reflns_number 31494 _diffrn_ambient_temperature 153 _diffrn_reflns_av_R_equivalents 0 _diffrn_reflns_limit_h_min 0 _diffrn_reflns_limit_h_max 30 _diffrn_reflns_limit_k_min 0 _diffrn_reflns_limit_k_max 25 _diffrn_reflns_limit_l_min -38 _diffrn_reflns_limit_l_max 37 _diffrn_reflns_theta_min 1.13 _diffrn_reflns_theta_max 29.55 _diffrn_reflns_theta_full 29.55 _diffrn_measured_fraction_theta_max 0.98 _diffrn_measured_fraction_theta_full 0.98 _reflns_number_total 31494 _reflns_number_gt 20010 _reflns_threshold_expression >2sigma(I) #------------------ COMPUTER PROGRAMS USED ----------------------------------# _computing_structure_solution 'SHELXS-86 (Sheldrick, 1986)' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_molecular_graphics 'Ortep-3 for Windows (Farrugia, 1997)' _computing_publication_material 'WinGX publication routines (Farrugia, 1999)' #------------------ REFINEMENT INFORMATION ----------------------------------# _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.1480P)^2^+82.5972P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_hydrogen_treatment none _refine_ls_extinction_method none _refine_ls_number_reflns 31494 _refine_ls_number_parameters 729 _refine_ls_number_restraints 112 _refine_ls_R_factor_gt 0.0864 _refine_ls_wR_factor_ref 0.2753 _refine_ls_goodness_of_fit_ref 1.107 _refine_ls_restrained_S_all 1.105 _refine_ls_shift/su_max 0.001 _refine_diff_density_max 5.832 _refine_diff_density_min -5.156 #------------------ ATOMIC TYPES, COORDINATES AND THERMAL PARAMETERS --------# loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.006 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' W W -0.849 6.8722 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_group _atom_site_disorder_assembly W1 W 0.03907(3) 1.11070(3) 0.16241(2) 0.05654(16) Uani 1 d . . . W2 W -0.10554(3) 1.07033(4) 0.14605(2) 0.06028(17) Uani 1 d . . . W3 W 0.09758(3) 0.82253(3) 0.10921(2) 0.05420(16) Uani 1 d . . . W4 W -0.04741(3) 0.78451(3) 0.09415(2) 0.05913(17) Uani 1 d . . . W5 W 0.14950(3) 0.96746(4) 0.19329(2) 0.05702(17) Uani 1 d . . . W6 W -0.15717(3) 0.88537(4) 0.16148(3) 0.0682(2) Uani 1 d . . . W7 W 0.06046(3) 1.00264(5) 0.28136(2) 0.0718(2) Uani 1 d . . . W8 W -0.10072(3) 0.95139(4) 0.26651(2) 0.06127(17) Uani 1 d . . . W9 W 0.09499(3) 0.83366(4) 0.25401(3) 0.0694(2) Uani 1 d . . . W10 W -0.06613(3) 0.78538(4) 0.23305(3) 0.06630(19) Uani 1 d . . . Ag1 Ag 0.00064(5) 0.97179(6) 0.06596(4) 0.0497(2) Uani 1 d . . . Ag2 Ag 0.04759(5) 1.08681(6) 0.02028(4) 0.0553(3) Uani 1 d . . . Ag3 Ag -0.07362(5) 1.05555(6) 0.00784(4) 0.0553(3) Uani 1 d . . . Si1 Si -0.00382(15) 0.92907(18) 0.17182(13) 0.0415(7) Uani 1 d . . . O1 O 0.0385(4) 1.1231(5) 0.0992(3) 0.052(2) Uiso 1 d . . . O2 O -0.1005(5) 1.0849(5) 0.0832(4) 0.057(2) Uiso 1 d . . . O3 O 0.0922(5) 0.8588(5) 0.0503(4) 0.056(2) Uiso 1 d . . . O4 O -0.0478(5) 0.8251(6) 0.0364(4) 0.061(3) Uiso 1 d . . . O5 O -0.0168(4) 1.0078(5) 0.1493(3) 0.051(2) Uiso 1 d . . . O6 O 0.0096(4) 0.8780(5) 0.1259(3) 0.0449(19) Uiso 1 d . . . O7 O 0.0710(6) 1.1872(7) 0.1850(5) 0.081(3) Uiso 1 d . . . O8 O -0.1675(6) 1.1197(7) 0.1583(5) 0.082(3) Uiso 1 d . . . O9 O 0.1580(6) 0.7657(6) 0.1074(4) 0.071(3) Uiso 1 d . . . O10 O -0.0836(6) 0.7063(7) 0.0808(5) 0.083(4) Uiso 1 d . . . O11 O -0.0446(6) 1.1366(7) 0.1694(4) 0.073(3) Uiso 1 d . . . O12 O 0.0337(5) 0.7529(6) 0.0995(4) 0.060(2) Uiso 1 d . . . O13 O 0.1061(5) 1.0444(6) 0.1648(4) 0.060(2) Uiso 1 d . . . O14 O -0.1402(5) 0.9769(6) 0.1386(4) 0.063(3) Uiso 1 d . . . O15 O 0.1327(5) 0.9075(5) 0.1399(4) 0.056(2) Uiso 1 d . . . O16 O -0.1151(5) 0.8434(6) 0.1140(4) 0.063(3) Uiso 1 d . . . O17 O 0.2225(6) 0.9910(7) 0.1884(5) 0.079(3) Uiso 1 d . . . O18 O -0.2292(7) 0.8710(8) 0.1391(5) 0.088(4) Uiso 1 d . . . O19 O 0.0535(4) 0.9293(5) 0.2119(3) 0.049(2) Uiso 1 d . . . O20 O -0.0604(4) 0.8989(5) 0.1994(3) 0.049(2) Uiso 1 d . . . O21 O 0.0321(5) 1.0717(6) 0.2366(4) 0.062(3) Uiso 1 d . . . O22 O -0.0933(5) 1.0377(6) 0.2241(4) 0.060(2) Uiso 1 d . . . O23 O 0.0853(5) 0.7913(6) 0.1865(4) 0.067(3) Uiso 1 d . . . O24 O -0.0381(5) 0.7577(6) 0.1720(4) 0.065(3) Uiso 1 d . . . O25 O 0.1381(5) 1.0101(6) 0.2567(4) 0.065(3) Uiso 1 d . . . O26 O -0.1682(6) 0.9313(7) 0.2254(5) 0.080(3) Uiso 1 d . . . O27 O 0.1624(5) 0.8809(5) 0.2321(4) 0.059(2) Uiso 1 d . . . O28 O -0.1435(6) 0.8017(6) 0.2004(4) 0.071(3) Uiso 1 d . . . O29 O -0.0188(5) 0.9715(5) 0.2889(4) 0.059(2) Uiso 1 d . . . O30 O 0.0146(5) 0.8011(6) 0.2572(4) 0.061(2) Uiso 1 d . . . O31 O 0.0858(5) 0.9022(6) 0.3004(4) 0.068(3) Uiso 1 d . . . O32 O -0.0908(5) 0.8555(6) 0.2834(4) 0.065(3) Uiso 1 d . . . O33 O 0.0750(6) 1.0481(7) 0.3360(5) 0.077(3) Uiso 1 d . . . O34 O -0.1361(6) 0.9858(7) 0.3156(5) 0.081(3) Uiso 1 d . . . O35 O 0.1311(7) 0.7666(8) 0.2891(5) 0.090(4) Uiso 1 d . . . O36 O -0.0777(7) 0.7063(7) 0.2614(5) 0.087(4) Uiso 1 d . . . N101 N 0.2719(9) 0.6878(10) 0.2068(7) 0.098(5) Uiso 1 d D . . C101 C 0.321(3) 0.659(3) 0.165(2) 0.096(5) Uiso 0.49(2) d P . . C102 C 0.288(3) 0.659(3) 0.112(2) 0.096(5) Uiso 0.49(2) d P . . C103 C 0.346(2) 0.632(3) 0.0766(18) 0.096(5) Uiso 0.49(2) d P . . C104 C 0.320(2) 0.612(3) 0.0287(18) 0.096(5) Uiso 0.49(2) d P . . C151 C 0.300(2) 0.640(3) 0.1732(19) 0.096(5) Uiso 0.51(2) d P . . C152 C 0.268(2) 0.642(3) 0.1212(19) 0.096(5) Uiso 0.51(2) d P . . C153 C 0.298(2) 0.592(3) 0.0893(17) 0.096(5) Uiso 0.51(2) d P . . C154 C 0.278(2) 0.594(2) 0.0406(18) 0.096(5) Uiso 0.51(2) d P . . C105 C 0.305(2) 0.680(3) 0.2572(19) 0.110(6) Uiso 0.593(19) d P . . C106 C 0.285(2) 0.725(2) 0.2976(15) 0.110(6) Uiso 0.593(19) d PD . . C107 C 0.280(2) 0.679(2) 0.3433(13) 0.110(6) Uiso 0.593(19) d PD . . C108 C 0.254(2) 0.716(2) 0.3874(15) 0.110(6) Uiso 0.593(19) d PD . . C155 C 0.287(3) 0.649(4) 0.263(3) 0.110(6) Uiso 0.407(19) d P . . C156 C 0.267(3) 0.675(4) 0.298(2) 0.110(6) Uiso 0.407(19) d PD . . C157 C 0.216(3) 0.642(3) 0.3250(19) 0.110(6) Uiso 0.407(19) d PD . . C158 C 0.219(3) 0.664(4) 0.3796(19) 0.110(6) Uiso 0.407(19) d PD . . C109 C 0.2056(16) 0.6725(18) 0.2009(13) 0.137(10) Uiso 1 d D . . C110 C 0.214(4) 0.591(2) 0.204(4) 0.196(15) Uiso 0.54(3) d PD . . C111 C 0.151(4) 0.584(5) 0.223(4) 0.196(15) Uiso 0.54(3) d PD . . C112 C 0.109(4) 0.520(5) 0.231(3) 0.196(15) Uiso 0.54(3) d PD . . C160 C 0.177(4) 0.601(3) 0.213(5) 0.196(15) Uiso 0.46(3) d PD . . C161 C 0.107(4) 0.598(6) 0.211(4) 0.196(15) Uiso 0.46(3) d PD . . C162 C 0.056(5) 0.554(6) 0.231(4) 0.196(15) Uiso 0.46(3) d PD . . C113 C 0.277(4) 0.764(2) 0.194(6) 0.148(9) Uiso 0.52(3) d PD . . C114 C 0.329(3) 0.809(4) 0.178(3) 0.148(9) Uiso 0.52(3) d PD . . C115 C 0.343(3) 0.878(3) 0.150(3) 0.148(9) Uiso 0.52(3) d PD . . C116 C 0.400(3) 0.924(4) 0.156(3) 0.148(9) Uiso 0.52(3) d PD . . C163 C 0.276(4) 0.765(2) 0.199(6) 0.148(9) Uiso 0.48(3) d PD . . C164 C 0.343(4) 0.787(3) 0.208(3) 0.148(9) Uiso 0.48(3) d PD . . C165 C 0.346(4) 0.859(4) 0.181(2) 0.148(9) Uiso 0.48(3) d PD . . C166 C 0.328(4) 0.862(4) 0.126(2) 0.148(9) Uiso 0.48(3) d PD . . N201 N -0.2892(15) 0.6745(17) 0.2038(13) 0.090(7) Uiso 0.60(3) d PD . . N251 N -0.272(2) 0.669(2) 0.224(2) 0.090(7) Uiso 0.40(3) d PD . . C201 C -0.262(3) 0.629(4) 0.244(2) 0.138(8) Uiso 0.47(2) d PD . . C202 C -0.196(3) 0.613(3) 0.257(3) 0.138(8) Uiso 0.47(2) d PD . . C203 C -0.177(3) 0.537(3) 0.272(3) 0.138(8) Uiso 0.47(2) d PD . . C204 C -0.120(3) 0.538(4) 0.242(3) 0.138(8) Uiso 0.47(2) d PD . . C251 C -0.259(3) 0.600(3) 0.246(3) 0.138(8) Uiso 0.53(2) d PD . . C252 C -0.192(3) 0.592(4) 0.2387(19) 0.138(8) Uiso 0.53(2) d PD . . C253 C -0.185(2) 0.568(4) 0.292(2) 0.138(8) Uiso 0.53(2) d PD . . C254 C -0.120(2) 0.543(3) 0.306(2) 0.138(8) Uiso 0.53(2) d PD . . C205 C -0.245(3) 0.673(3) 0.167(3) 0.125(7) Uiso 0.48(3) d PD . . C206 C -0.255(3) 0.602(3) 0.139(2) 0.125(7) Uiso 0.48(3) d PD . . C207 C -0.204(3) 0.597(4) 0.104(2) 0.125(7) Uiso 0.48(3) d PD . . C208 C -0.235(3) 0.518(4) 0.057(3) 0.125(7) Uiso 0.48(3) d P . . C255 C -0.269(3) 0.663(3) 0.155(2) 0.125(7) Uiso 0.52(3) d PD . . C256 C -0.273(3) 0.593(3) 0.125(2) 0.125(7) Uiso 0.52(3) d PD . . C257 C -0.240(3) 0.611(4) 0.079(2) 0.125(7) Uiso 0.52(3) d PD . . C258 C -0.230(3) 0.564(4) 0.066(2) 0.125(7) Uiso 0.52(3) d P . . C209 C -0.270(3) 0.746(3) 0.224(2) 0.138(8) Uiso 0.62(2) d P . . C210 C -0.295(3) 0.781(3) 0.276(2) 0.138(8) Uiso 0.62(2) d P . . C211 C -0.242(3) 0.802(3) 0.314(2) 0.138(8) Uiso 0.62(2) d PD . . C212 C -0.268(3) 0.876(2) 0.322(2) 0.138(8) Uiso 0.62(2) d PD . . C259 C -0.234(3) 0.716(4) 0.252(3) 0.138(8) Uiso 0.53(2) d P . . C260 C -0.258(5) 0.761(6) 0.251(4) 0.138(8) Uiso 0.38(2) d P . . C261 C -0.256(4) 0.837(5) 0.298(3) 0.138(8) Uiso 0.38(2) d PD . . C262 C -0.301(4) 0.882(5) 0.266(3) 0.138(8) Uiso 0.38(2) d PD . . C213 C -0.3540(16) 0.665(3) 0.207(2) 0.154(9) Uiso 0.75(3) d PD . . C214 C -0.393(2) 0.715(3) 0.174(2) 0.154(9) Uiso 0.75(3) d PD . . C215 C -0.459(2) 0.690(3) 0.1748(19) 0.154(9) Uiso 0.75(3) d PD . . C216 C -0.498(2) 0.745(3) 0.1450(18) 0.154(9) Uiso 0.75(3) d PD . . C263 C -0.337(3) 0.652(8) 0.219(7) 0.154(9) Uiso 0.25(3) d PD . . C264 C -0.369(8) 0.709(7) 0.187(7) 0.154(9) Uiso 0.25(3) d PD . . C265 C -0.404(6) 0.776(6) 0.168(6) 0.154(9) Uiso 0.25(3) d PD . . C266 C -0.459(6) 0.731(9) 0.178(6) 0.154(9) Uiso 0.25(3) d PD . . N301 N 0.0611(16) 0.688(2) -0.0647(15) 0.087(7) Uiso 0.50(4) d PD . . N351 N 0.0748(18) 0.691(2) -0.0529(15) 0.087(7) Uiso 0.50(4) d PD . . C301 C 0.106(2) 0.746(3) -0.062(3) 0.128(7) Uiso 0.47(2) d PD . . C302 C 0.171(2) 0.722(3) -0.070(3) 0.128(7) Uiso 0.47(2) d PD . . C303 C 0.217(2) 0.782(3) -0.058(3) 0.128(7) Uiso 0.47(2) d PD . . C304 C 0.282(2) 0.810(4) -0.056(3) 0.128(7) Uiso 0.47(2) d PD . . C351 C 0.112(2) 0.754(3) -0.039(2) 0.128(7) Uiso 0.53(2) d PD . . C352 C 0.180(2) 0.752(3) -0.051(2) 0.128(7) Uiso 0.53(2) d PD . . C353 C 0.216(2) 0.796(3) -0.011(2) 0.128(7) Uiso 0.53(2) d PD . . C354 C 0.284(2) 0.788(3) -0.014(2) 0.128(7) Uiso 0.53(2) d PD . . C305 C 0.0048(14) 0.7161(17) -0.0471(12) 0.109(5) Uiso 0.810(17) d PD . . C306 C -0.0451(13) 0.6608(17) -0.0445(13) 0.109(5) Uiso 0.810(17) d PD . . C307 C -0.1060(12) 0.6994(15) -0.0450(12) 0.109(5) Uiso 0.810(17) d PD . . C308 C -0.1565(14) 0.6463(17) -0.0357(12) 0.109(5) Uiso 0.810(17) d PD . . C355 C 0.048(4) 0.650(7) -0.015(4) 0.109(5) Uiso 0.190(17) d PD . . C356 C -0.020(4) 0.633(8) -0.014(5) 0.109(5) Uiso 0.190(17) d PD . . C357 C -0.084(4) 0.605(7) -0.007(5) 0.109(5) Uiso 0.190(17) d PD . . C358 C -0.149(4) 0.577(7) -0.017(5) 0.109(5) Uiso 0.190(17) d PD . . C309 C 0.082(4) 0.625(3) -0.0370(18) 0.109(5) Uiso 0.46(2) d PD . . C311 C 0.100(3) 0.555(3) 0.034(2) 0.109(5) Uiso 0.46(2) d PD . . C310 C 0.077(3) 0.631(3) 0.0186(19) 0.109(5) Uiso 0.46(2) d PD . . C312 C 0.108(3) 0.534(3) 0.093(2) 0.109(5) Uiso 0.46(2) d P . . C359 C 0.090(4) 0.623(2) -0.0287(17) 0.109(5) Uiso 0.54(2) d PD . . C360 C 0.107(3) 0.644(2) 0.0244(16) 0.109(5) Uiso 0.54(2) d PD . . C361 C 0.107(2) 0.585(3) 0.0628(18) 0.109(5) Uiso 0.54(2) d PD . . C362 C 0.073(3) 0.541(3) 0.059(2) 0.109(5) Uiso 0.54(2) d P . . C313 C 0.066(3) 0.640(3) -0.1070(18) 0.131(7) Uiso 0.55(2) d PD . . C314 C 0.030(3) 0.683(3) -0.149(2) 0.131(7) Uiso 0.55(2) d P . . C315 C 0.056(3) 0.666(4) -0.199(3) 0.131(7) Uiso 0.55(2) d P . . C316 C -0.014(3) 0.651(4) -0.222(2) 0.131(7) Uiso 0.55(2) d P . . C363 C 0.070(4) 0.701(4) -0.120(3) 0.131(7) Uiso 0.45(2) d P . . C364 C 0.015(4) 0.651(4) -0.136(3) 0.131(7) Uiso 0.45(2) d P . . C365 C 0.028(4) 0.648(4) -0.200(3) 0.131(7) Uiso 0.45(2) d P . . C366 C -0.035(3) 0.599(4) -0.220(3) 0.131(7) Uiso 0.45(2) d P . . C401 C -0.004(3) 0.697(4) 0.458(3) 0.200(13) Uiso 0.68(3) d PD . . C402 C 0.038(3) 0.653(4) 0.493(3) 0.200(13) Uiso 0.68(3) d PD . . C403 C -0.002(3) 0.615(4) 0.528(3) 0.200(13) Uiso 0.68(3) d PD . . C404 C 0.042(3) 0.644(4) 0.569(3) 0.200(13) Uiso 0.68(3) d PD . . C451 C -0.016(7) 0.704(8) 0.453(5) 0.200(13) Uiso 0.32(3) d PD . . C452 C -0.028(7) 0.623(8) 0.450(5) 0.200(13) Uiso 0.32(3) d PD . . C453 C -0.019(8) 0.584(7) 0.500(5) 0.200(13) Uiso 0.32(3) d PD . . C454 C -0.037(8) 0.639(8) 0.538(5) 0.200(13) Uiso 0.32(3) d PD . . C405 C -0.006(4) 0.783(4) 0.383(3) 0.213(15) Uiso 0.61(3) d PD . . C406 C -0.040(4) 0.854(4) 0.387(3) 0.213(15) Uiso 0.61(3) d PD . . C407 C -0.103(4) 0.835(5) 0.402(4) 0.213(15) Uiso 0.61(3) d PD . . C408 C -0.149(4) 0.874(4) 0.432(3) 0.213(15) Uiso 0.61(3) d PD . . C455 C -0.016(5) 0.712(7) 0.376(4) 0.213(15) Uiso 0.39(3) d PD . . C456 C -0.063(6) 0.765(7) 0.393(5) 0.213(15) Uiso 0.39(3) d PD . . C457 C -0.109(6) 0.816(8) 0.414(5) 0.213(15) Uiso 0.39(3) d PD . . C458 C -0.168(6) 0.826(7) 0.381(5) 0.213(15) Uiso 0.39(3) d PD . . C409 C 0.047(5) 0.687(7) 0.380(5) 0.206(15) Uiso 0.49(3) d PD . . C410 C -0.006(5) 0.636(6) 0.368(4) 0.206(15) Uiso 0.49(3) d PD . . C411 C 0.035(4) 0.590(6) 0.338(4) 0.206(15) Uiso 0.49(3) d PD . . C412 C 0.100(4) 0.595(6) 0.361(4) 0.206(15) Uiso 0.49(3) d PD . . C459 C 0.065(4) 0.690(7) 0.389(4) 0.206(15) Uiso 0.51(3) d PD . . C460 C 0.039(4) 0.638(5) 0.350(4) 0.206(15) Uiso 0.51(3) d PD . . C461 C -0.014(4) 0.587(5) 0.338(4) 0.206(15) Uiso 0.51(3) d PD . . C462 C 0.021(5) 0.543(5) 0.302(4) 0.206(15) Uiso 0.51(3) d PD . . C413 C -0.006(4) 0.790(4) 0.443(4) 0.193(13) Uiso 0.43(3) d PD . . C414 C 0.026(4) 0.834(6) 0.406(3) 0.193(13) Uiso 0.43(3) d PD . . C415 C 0.093(4) 0.840(7) 0.423(4) 0.193(13) Uiso 0.43(3) d PD . . C416 C 0.149(4) 0.888(6) 0.431(5) 0.193(13) Uiso 0.43(3) d PD . . C463 C 0.078(4) 0.793(4) 0.439(3) 0.193(13) Uiso 0.57(3) d PD . . C464 C 0.107(4) 0.846(5) 0.405(3) 0.193(13) Uiso 0.57(3) d PD . . C465 C 0.164(4) 0.858(5) 0.439(3) 0.193(13) Uiso 0.57(3) d PD . . C466 C 0.192(4) 0.915(4) 0.407(3) 0.193(13) Uiso 0.57(3) d PD . . N401 N 0.025(2) 0.733(3) 0.4180(19) 0.237(19) Uiso 1 d D . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 W1 0.0666(4) 0.0534(3) 0.0508(3) -0.0120(2) 0.0123(3) -0.0119(3) W2 0.0513(3) 0.0708(4) 0.0614(4) -0.0060(3) 0.0210(3) 0.0176(3) W3 0.0551(3) 0.0581(3) 0.0499(3) -0.0024(2) 0.0073(2) 0.0138(3) W4 0.0722(4) 0.0497(3) 0.0547(3) -0.0058(2) -0.0003(3) -0.0167(3) W5 0.0370(3) 0.0826(4) 0.0519(3) -0.0032(3) 0.0057(2) -0.0124(3) W6 0.0384(3) 0.1006(5) 0.0661(4) 0.0026(3) 0.0086(3) -0.0199(3) W7 0.0604(4) 0.1053(6) 0.0510(3) -0.0240(3) 0.0136(3) -0.0299(4) W8 0.0455(3) 0.0848(4) 0.0559(3) -0.0023(3) 0.0196(3) -0.0005(3) W9 0.0544(4) 0.0885(5) 0.0644(4) 0.0218(3) -0.0020(3) -0.0047(3) W10 0.0623(4) 0.0648(4) 0.0726(4) 0.0022(3) 0.0109(3) -0.0222(3) Ag1 0.0480(5) 0.0559(6) 0.0460(5) -0.0026(4) 0.0078(4) 0.0045(4) Ag2 0.0579(6) 0.0590(6) 0.0494(5) -0.0045(5) 0.0067(5) -0.0043(5) Ag3 0.0493(6) 0.0636(6) 0.0543(6) 0.0003(5) 0.0116(5) 0.0122(5) Si1 0.0371(16) 0.0437(17) 0.0446(17) -0.0058(14) 0.0089(13) -0.0043(13) #------------------ MOLECULAR GEOMETRY --------------------------------------# _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag W1 O7 1.701(14) . ? W1 O1 1.750(10) . ? W1 O13 1.944(11) . ? W1 O11 1.954(13) . ? W1 O21 2.182(11) . ? W1 O5 2.316(9) . ? W2 O8 1.720(14) . ? W2 O2 1.760(10) . ? W2 O11 1.919(13) . ? W2 O14 1.924(11) . ? W2 O22 2.226(11) . ? W2 O5 2.301(10) . ? W3 O9 1.724(12) . ? W3 O3 1.751(10) . ? W3 O12 1.940(11) . ? W3 O15 1.944(10) . ? W3 O23 2.238(11) . ? W3 O6 2.301(9) . ? W4 O10 1.705(14) . ? W4 O4 1.759(11) . ? W4 O12 1.901(11) . ? W4 O16 1.982(11) . ? W4 O24 2.191(11) . ? W4 O6 2.302(9) . ? W5 O17 1.704(14) . ? W5 O15 1.864(10) . ? W5 O13 1.879(11) . ? W5 O25 1.950(11) . ? W5 O27 1.955(10) . ? W5 O19 2.353(10) . ? W6 O18 1.699(15) . ? W6 O16 1.843(11) . ? W6 O14 1.881(11) . ? W6 O28 1.913(12) . ? W6 O26 1.989(13) . ? W6 O20 2.339(9) . ? W7 O33 1.735(13) . ? W7 O21 1.865(11) . ? W7 O29 1.890(11) . ? W7 O25 1.915(12) . ? W7 O31 2.029(12) . ? W7 O19 2.348(9) . ? W8 O34 1.738(14) . ? W8 O26 1.851(14) . ? W8 O32 1.871(11) . ? W8 O29 1.922(11) . ? W8 O22 2.011(11) . ? W8 O20 2.331(9) . ? W9 O35 1.746(15) . ? W9 O31 1.834(12) . ? W9 O27 1.886(11) . ? W9 O30 1.904(11) . ? W9 O23 2.014(11) . ? W9 O19 2.294(9) . ? W10 O36 1.707(14) . ? W10 O30 1.896(11) . ? W10 O24 1.905(11) . ? W10 O28 1.909(12) . ? W10 O32 2.018(11) . ? W10 O20 2.333(9) . ? Ag1 O6 2.411(9) . ? Ag1 O5 2.446(9) . ? Ag1 Ag3 2.7146(15) . ? Ag1 Ag3 2.7441(15) 3_575 ? Ag1 Ag2 2.7478(16) . ? Ag1 Ag2 2.7547(15) 3_575 ? Ag1 Si1 3.024(4) . ? Ag2 O4 2.272(11) 3_575 ? Ag2 O1 2.295(10) . ? Ag2 Ag1 2.7547(15) 3_575 ? Ag2 Ag3 2.7647(17) . ? Ag2 Ag3 2.8579(16) 3_575 ? Ag3 O2 2.265(10) . ? Ag3 O3 2.283(10) 3_575 ? Ag3 Ag1 2.7441(15) 3_575 ? Ag3 Ag2 2.8579(16) 3_575 ? Si1 O5 1.621(10) . ? Si1 O19 1.623(10) . ? Si1 O20 1.624(10) . ? Si1 O6 1.630(9) . ? O3 Ag3 2.283(10) 3_575 ? O4 Ag2 2.272(11) 3_575 ? N101 C151 1.46(5) . ? N101 C163 1.48(2) . ? N101 C113 1.482(19) . ? N101 C109 1.50(4) . ? N101 C105 1.53(5) . ? N101 C155 1.73(8) . ? N101 C101 1.74(6) . ? C101 C151 0.64(6) . ? C101 C102 1.57(8) . ? C101 C152 1.65(8) . ? C102 C152 0.64(6) . ? C102 C153 1.43(7) . ? C102 C151 1.72(7) . ? C102 C103 1.76(7) . ? C103 C153 1.39(7) . ? C103 C104 1.44(7) . ? C103 C154 1.90(7) . ? C104 C154 1.09(6) . ? C104 C153 1.81(7) . ? C151 C152 1.55(7) . ? C152 C153 1.47(7) . ? C153 C154 1.38(6) . ? C105 C155 0.74(7) . ? C105 C156 1.46(8) . ? C105 C106 1.48(6) . ? C106 C156 1.01(7) . ? C106 C107 1.528(19) . ? C106 C155 1.71(9) . ? C107 C156 1.26(7) . ? C107 C108 1.545(19) . ? C107 C157 1.64(8) . ? C107 C158 1.77(8) . ? C108 C158 1.26(7) . ? C155 C156 1.20(9) . ? C156 C157 1.54(2) . ? C157 C158 1.55(2) . ? C109 C160 1.54(2) . ? C109 C110 1.54(2) . ? C110 C160 0.90(12) . ? C110 C111 1.54(2) . ? C111 C160 0.73(10) . ? C111 C161 1.04(13) . ? C111 C112 1.55(2) . ? C112 C162 1.36(12) . ? C112 C161 1.58(14) . ? C160 C161 1.55(2) . ? C161 C162 1.55(2) . ? C113 C114 1.54(2) . ? C113 C164 1.56(15) . ? C114 C164 0.96(8) . ? C114 C165 1.00(8) . ? C114 C115 1.54(2) . ? C114 C163 1.59(13) . ? C114 C166 1.73(10) . ? C115 C166 0.78(8) . ? C115 C165 0.93(8) . ? C115 C116 1.54(2) . ? C116 C165 1.87(10) . ? C163 C164 1.54(2) . ? C164 C165 1.54(2) . ? C165 C166 1.54(2) . ? N201 N251 0.65(5) . ? N201 C263 1.25(10) . ? N201 C205 1.46(8) . ? N201 C213 1.469(19) . ? N201 C201 1.48(2) . ? N201 C255 1.47(7) . ? N201 C209 1.51(7) . ? N201 C259 1.91(8) . ? N201 C251 1.92(6) . ? N201 C264 1.93(15) . ? N251 C201 0.94(6) . ? N251 C259 1.42(8) . ? N251 C251 1.46(2) . ? N251 C209 1.46(8) . ? N251 C263 1.47(2) . ? N251 C205 1.71(9) . ? N251 C213 1.85(7) . ? N251 C260 1.90(12) . ? N251 C255 1.91(9) . ? C201 C251 0.56(8) . ? C201 C202 1.54(2) . ? C201 C252 1.74(11) . ? C201 C263 1.80(9) . ? C201 C259 1.76(11) . ? C202 C252 0.65(9) . ? C202 C253 1.30(9) . ? C202 C251 1.44(11) . ? C202 C203 1.54(2) . ? C203 C253 0.83(8) . ? C203 C252 1.40(9) . ? C203 C254 1.52(10) . ? C203 C204 1.55(2) . ? C204 C254 1.75(9) . ? C204 C252 1.89(9) . ? C251 C252 1.53(2) . ? C252 C253 1.54(2) . ? C253 C254 1.55(2) . ? C205 C255 0.65(9) . ? C205 C206 1.55(2) . ? C205 C256 1.97(8) . ? C206 C256 0.56(9) . ? C206 C255 1.27(9) . ? C206 C207 1.56(2) . ? C206 C257 1.73(9) . ? C207 C257 1.06(8) . ? C207 C258 1.32(9) . ? C207 C256 1.69(9) . ? C208 C258 0.89(8) . ? C208 C257 1.85(9) . ? C255 C256 1.54(2) . ? C256 C257 1.55(2) . ? C256 C258 2.03(9) . ? C257 C258 0.99(8) . ? C209 C260 0.82(10) . ? C209 C259 1.22(9) . ? C209 C210 1.70(9) . ? C210 C260 1.17(11) . ? C210 C261 1.48(11) . ? C210 C211 1.58(8) . ? C210 C262 1.92(10) . ? C210 C259 1.97(9) . ? C211 C261 0.84(8) . ? C211 C212 1.54(2) . ? C211 C260 1.90(12) . ? C212 C261 1.03(10) . ? C212 C262 1.65(10) . ? C259 C260 1.00(11) . ? C260 C261 1.93(15) . ? C261 C262 1.53(2) . ? C213 C263 0.54(11) . ? C213 C264 1.04(12) . ? C213 C214 1.545(19) . ? C214 C264 0.63(15) . ? C214 C265 1.17(12) . ? C214 C215 1.54(2) . ? C214 C266 1.50(16) . ? C215 C266 0.77(16) . ? C215 C216 1.53(2) . ? C215 C265 2.05(14) . ? C215 C264 2.03(19) . ? C216 C266 1.23(16) . ? C263 C264 1.54(2) . ? C264 C265 1.54(2) . ? C265 C266 1.54(2) . ? N301 C309 1.469(19) . ? N301 C305 1.475(19) . ? N301 C301 1.48(2) . ? N301 C313 1.481(19) . ? N301 C363 1.56(8) . ? N301 C355 1.61(8) . ? N301 C359 1.68(7) . ? N301 C351 1.79(6) . ? N351 C301 1.29(7) . ? N351 C309 1.32(8) . ? N351 C359 1.475(19) . ? N351 C355 1.48(2) . ? N351 C351 1.482(19) . ? N351 C305 1.65(6) . ? N351 C313 1.76(6) . ? N351 C363 1.84(8) . ? C301 C351 0.65(9) . ? C301 C302 1.56(2) . ? C301 C352 1.65(8) . ? C301 C363 1.91(10) . ? C302 C352 0.78(7) . ? C302 C303 1.55(2) . ? C302 C351 1.71(9) . ? C303 C352 1.03(7) . ? C303 C353 1.30(8) . ? C303 C304 1.54(2) . ? C303 C354 1.85(8) . ? C304 C354 1.23(8) . ? C304 C353 2.01(8) . ? C351 C352 1.56(2) . ? C352 C353 1.55(2) . ? C353 C354 1.53(2) . ? C305 C306 1.53(4) . ? C305 C355 1.77(11) . ? C305 C356 1.90(13) . ? C306 C356 1.09(14) . ? C306 C307 1.541(19) . ? C306 C357 1.75(12) . ? C307 C308 1.542(18) . ? C308 C358 1.41(14) . ? C308 C357 1.91(13) . ? C355 C309 1.11(14) . ? C355 C310 1.14(10) . ? C355 C359 1.17(13) . ? C355 C356 1.55(2) . ? C355 C360 1.64(11) . ? C356 C357 1.55(2) . ? C357 C358 1.54(2) . ? C309 C310 1.54(2) . ? C309 C360 1.78(9) . ? C309 C313 1.95(7) . ? C311 C361 0.98(7) . ? C311 C362 0.98(7) . ? C311 C310 1.55(2) . ? C311 C312 1.67(9) . ? C311 C360 1.70(8) . ? C310 C360 0.72(7) . ? C310 C359 1.36(9) . ? C310 C361 1.59(7) . ? C310 C362 2.03(7) . ? C312 C362 1.18(7) . ? C312 C361 1.27(7) . ? C359 C360 1.532(19) . ? C360 C361 1.529(19) . ? C361 C362 1.13(7) . ? C313 C363 1.21(8) . ? C313 C364 1.34(9) . ? C313 C314 1.58(9) . ? C314 C364 0.81(8) . ? C314 C363 1.21(8) . ? C314 C315 1.57(9) . ? C314 C365 1.54(10) . ? C315 C365 0.72(9) . ? C315 C316 1.67(9) . ? C315 C364 2.06(10) . ? C316 C365 1.08(9) . ? C316 C366 1.08(8) . ? C363 C364 1.60(11) . ? C364 C365 1.81(11) . ? C365 C366 1.73(11) . ? C401 N401 1.48(2) . ? C401 C452 1.5(2) . ? C401 C402 1.54(2) . ? C401 C413 1.79(11) . ? C402 C403 1.53(2) . ? C402 C453 1.83(18) . ? C402 C452 1.89(16) . ? C402 C451 1.9(2) . ? C402 C404 2.09(10) . ? C403 C454 0.96(15) . ? C403 C453 1.02(15) . ? C403 C404 1.54(2) . ? C404 C454 1.90(19) . ? C451 N401 1.47(2) . ? C451 C452 1.54(2) . ? C451 C413 1.66(16) . ? C451 C455 2.10(18) . ? C452 C453 1.54(2) . ? C453 C454 1.54(2) . ? C405 C456 1.36(15) . ? C405 C455 1.36(14) . ? C405 C414 1.33(13) . ? C405 N401 1.48(2) . ? C405 C413 1.66(12) . ? C405 C406 1.55(2) . ? C406 C407 1.54(2) . ? C406 C414 1.57(11) . ? C406 C456 1.76(17) . ? C406 C457 1.90(18) . ? C406 C413 2.05(14) . ? C407 C457 0.5(2) . ? C407 C458 1.51(17) . ? C407 C408 1.54(2) . ? C407 C456 1.61(15) . ? C408 C457 1.51(15) . ? C408 C458 1.68(15) . ? C455 N401 1.47(2) . ? C455 C410 1.48(15) . ? C455 C409 1.49(14) . ? C455 C456 1.54(2) . ? C455 C459 1.87(14) . ? C455 C460 2.03(15) . ? C456 C457 1.54(2) . ? C456 C413 1.88(17) . ? C457 C458 1.54(2) . ? C409 C460 1.23(12) . ? C409 N401 1.47(2) . ? C409 C410 1.54(2) . ? C410 C460 1.16(14) . ? C410 C461 1.23(13) . ? C410 C411 1.54(2) . ? C410 C459 1.94(18) . ? C411 C460 0.96(13) . ? C411 C461 1.11(12) . ? C411 C462 1.35(13) . ? C411 C412 1.53(2) . ? C412 C460 1.61(15) . ? C459 N401 1.47(2) . ? C459 C460 1.54(2) . ? C460 C461 1.54(2) . ? C461 C462 1.55(2) . ? C413 N401 1.48(2) . ? C413 C414 1.54(2) . ? C413 C463 1.88(12) . ? C414 C415 1.54(2) . ? C414 C463 1.62(12) . ? C414 C464 1.82(14) . ? C415 C463 1.06(12) . ? C415 C416 1.54(2) . ? C415 C465 1.65(13) . ? C416 C465 0.68(15) . ? C416 C466 1.31(13) . ? C416 C464 1.40(14) . ? C463 C464 1.54(2) . ? C463 N401 1.71(9) . ? C464 C465 1.54(2) . ? C465 C466 1.54(2) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O7 W1 O1 102.8(6) . . ? O7 W1 O13 103.3(6) . . ? O1 W1 O13 93.7(5) . . ? O7 W1 O11 97.4(6) . . ? O1 W1 O11 97.4(5) . . ? O13 W1 O11 153.6(5) . . ? O7 W1 O21 90.1(5) . . ? O1 W1 O21 167.1(4) . . ? O13 W1 O21 82.1(4) . . ? O11 W1 O21 81.7(5) . . ? O7 W1 O5 165.6(5) . . ? O1 W1 O5 89.7(4) . . ? O13 W1 O5 82.7(4) . . ? O11 W1 O5 73.5(4) . . ? O21 W1 O5 77.7(4) . . ? O8 W2 O2 102.7(6) . . ? O8 W2 O11 98.3(6) . . ? O2 W2 O11 97.4(5) . . ? O8 W2 O14 101.0(6) . . ? O2 W2 O14 95.3(5) . . ? O11 W2 O14 153.8(5) . . ? O8 W2 O22 90.1(5) . . ? O2 W2 O22 167.1(4) . . ? O11 W2 O22 80.0(5) . . ? O14 W2 O22 82.5(4) . . ? O8 W2 O5 166.3(5) . . ? O2 W2 O5 89.9(4) . . ? O11 W2 O5 74.5(4) . . ? O14 W2 O5 82.8(4) . . ? O22 W2 O5 77.2(4) . . ? O9 W3 O3 102.3(5) . . ? O9 W3 O12 98.4(5) . . ? O3 W3 O12 98.0(5) . . ? O9 W3 O15 103.4(5) . . ? O3 W3 O15 94.4(4) . . ? O12 W3 O15 152.0(4) . . ? O9 W3 O23 91.0(5) . . ? O3 W3 O23 166.7(4) . . ? O12 W3 O23 79.1(4) . . ? O15 W3 O23 83.1(4) . . ? O9 W3 O6 165.4(5) . . ? O3 W3 O6 90.5(4) . . ? O12 W3 O6 72.7(4) . . ? O15 W3 O6 82.2(4) . . ? O23 W3 O6 76.2(4) . . ? O10 W4 O4 102.2(6) . . ? O10 W4 O12 100.3(6) . . ? O4 W4 O12 98.4(5) . . ? O10 W4 O16 100.5(6) . . ? O4 W4 O16 93.1(5) . . ? O12 W4 O16 153.5(4) . . ? O10 W4 O24 91.1(5) . . ? O4 W4 O24 166.6(5) . . ? O12 W4 O24 80.5(4) . . ? O16 W4 O24 83.0(4) . . ? O10 W4 O6 168.3(5) . . ? O4 W4 O6 88.6(4) . . ? O12 W4 O6 73.4(4) . . ? O16 W4 O6 83.1(4) . . ? O24 W4 O6 78.3(4) . . ? O17 W5 O15 103.4(5) . . ? O17 W5 O13 103.5(6) . . ? O15 W5 O13 94.1(5) . . ? O17 W5 O25 98.8(6) . . ? O15 W5 O25 156.7(5) . . ? O13 W5 O25 87.5(5) . . ? O17 W5 O27 99.0(5) . . ? O15 W5 O27 86.4(4) . . ? O13 W5 O27 156.7(5) . . ? O25 W5 O27 83.1(5) . . ? O17 W5 O19 171.4(5) . . ? O15 W5 O19 81.7(4) . . ? O13 W5 O19 82.9(4) . . ? O25 W5 O19 75.4(4) . . ? O27 W5 O19 74.1(4) . . ? O18 W6 O16 101.3(6) . . ? O18 W6 O14 103.6(6) . . ? O16 W6 O14 91.6(5) . . ? O18 W6 O28 100.2(6) . . ? O16 W6 O28 88.6(5) . . ? O14 W6 O28 155.7(5) . . ? O18 W6 O26 102.1(6) . . ? O16 W6 O26 156.3(5) . . ? O14 W6 O26 86.5(5) . . ? O28 W6 O26 83.7(5) . . ? O18 W6 O20 174.1(5) . . ? O16 W6 O20 81.8(4) . . ? O14 W6 O20 81.1(4) . . ? O28 W6 O20 74.8(4) . . ? O26 W6 O20 74.5(5) . . ? O33 W7 O21 104.9(5) . . ? O33 W7 O29 100.0(6) . . ? O21 W7 O29 90.8(5) . . ? O33 W7 O25 98.9(6) . . ? O21 W7 O25 89.3(5) . . ? O29 W7 O25 160.4(5) . . ? O33 W7 O31 101.9(5) . . ? O21 W7 O31 153.1(5) . . ? O29 W7 O31 85.9(5) . . ? O25 W7 O31 85.2(5) . . ? O33 W7 O19 170.9(5) . . ? O21 W7 O19 82.9(4) . . ? O29 W7 O19 84.4(4) . . ? O25 W7 O19 76.1(4) . . ? O31 W7 O19 70.3(4) . . ? O34 W8 O26 98.7(6) . . ? O34 W8 O32 102.6(6) . . ? O26 W8 O32 91.7(5) . . ? O34 W8 O29 99.0(6) . . ? O26 W8 O29 161.0(5) . . ? O32 W8 O29 91.1(5) . . ? O34 W8 O22 102.2(5) . . ? O26 W8 O22 84.9(5) . . ? O32 W8 O22 155.2(5) . . ? O29 W8 O22 84.7(4) . . ? O34 W8 O20 175.1(5) . . ? O26 W8 O20 77.1(5) . . ? O32 W8 O20 75.1(4) . . ? O29 W8 O20 85.4(4) . . ? O22 W8 O20 80.2(4) . . ? O35 W9 O31 101.3(6) . . ? O35 W9 O27 99.8(6) . . ? O31 W9 O27 91.5(5) . . ? O35 W9 O30 98.0(6) . . ? O31 W9 O30 92.2(5) . . ? O27 W9 O30 160.8(4) . . ? O35 W9 O23 103.6(6) . . ? O31 W9 O23 155.1(5) . . ? O27 W9 O23 85.7(5) . . ? O30 W9 O23 83.1(5) . . ? O35 W9 O19 174.5(5) . . ? O31 W9 O19 74.8(4) . . ? O27 W9 O19 76.8(4) . . ? O30 W9 O19 86.0(4) . . ? O23 W9 O19 80.5(4) . . ? O36 W10 O30 98.6(6) . . ? O36 W10 O24 103.6(6) . . ? O30 W10 O24 89.0(5) . . ? O36 W10 O28 101.0(6) . . ? O30 W10 O28 160.3(5) . . ? O24 W10 O28 88.7(5) . . ? O36 W10 O32 101.4(6) . . ? O30 W10 O32 87.7(5) . . ? O24 W10 O32 155.0(5) . . ? O28 W10 O32 86.1(5) . . ? O36 W10 O20 172.8(6) . . ? O30 W10 O20 85.2(4) . . ? O24 W10 O20 82.5(4) . . ? O28 W10 O20 75.0(4) . . ? O32 W10 O20 72.5(4) . . ? O6 Ag1 O5 64.8(3) . . ? O6 Ag1 Ag3 147.2(2) . . ? O5 Ag1 Ag3 104.8(2) . . ? O6 Ag1 Ag3 110.1(2) . 3_575 ? O5 Ag1 Ag3 152.7(2) . 3_575 ? Ag3 Ag1 Ag3 92.59(4) . 3_575 ? O6 Ag1 Ag2 150.8(2) . . ? O5 Ag1 Ag2 107.6(2) . . ? Ag3 Ag1 Ag2 60.81(4) . . ? Ag3 Ag1 Ag2 62.72(4) 3_575 . ? O6 Ag1 Ag2 107.5(2) . 3_575 ? O5 Ag1 Ag2 146.6(2) . 3_575 ? Ag3 Ag1 Ag2 63.00(4) . 3_575 ? Ag3 Ag1 Ag2 60.37(4) 3_575 3_575 ? Ag2 Ag1 Ag2 93.45(4) . 3_575 ? O6 Ag1 Si1 32.5(2) . . ? O5 Ag1 Si1 32.3(2) . . ? Ag3 Ag1 Si1 130.95(8) . . ? Ag3 Ag1 Si1 136.46(8) 3_575 . ? Ag2 Ag1 Si1 133.59(8) . . ? Ag2 Ag1 Si1 132.86(8) 3_575 . ? O4 Ag2 O1 115.8(4) 3_575 . ? O4 Ag2 Ag1 155.1(3) 3_575 . ? O1 Ag2 Ag1 74.8(2) . . ? O4 Ag2 Ag1 74.0(3) 3_575 3_575 ? O1 Ag2 Ag1 150.8(3) . 3_575 ? Ag1 Ag2 Ag1 86.55(4) . 3_575 ? O4 Ag2 Ag3 97.1(3) 3_575 . ? O1 Ag2 Ag3 91.3(3) . . ? Ag1 Ag2 Ag3 59.00(4) . . ? Ag1 Ag2 Ag3 59.63(4) 3_575 . ? O4 Ag2 Ag3 119.1(3) 3_575 3_575 ? O1 Ag2 Ag3 124.6(2) . 3_575 ? Ag1 Ag2 Ag3 58.58(4) . 3_575 ? Ag1 Ag2 Ag3 57.81(4) 3_575 3_575 ? Ag3 Ag2 Ag3 89.13(4) . 3_575 ? O2 Ag3 O3 114.8(4) . 3_575 ? O2 Ag3 Ag1 78.3(3) . . ? O3 Ag3 Ag1 152.9(3) 3_575 . ? O2 Ag3 Ag1 159.0(3) . 3_575 ? O3 Ag3 Ag1 72.7(3) 3_575 3_575 ? Ag1 Ag3 Ag1 87.41(4) . 3_575 ? O2 Ag3 Ag2 99.2(3) . . ? O3 Ag3 Ag2 93.5(3) 3_575 . ? Ag1 Ag3 Ag2 60.19(4) . . ? Ag1 Ag3 Ag2 60.01(4) 3_575 . ? O2 Ag3 Ag2 123.2(3) . 3_575 ? O3 Ag3 Ag2 120.1(3) 3_575 3_575 ? Ag1 Ag3 Ag2 59.19(4) . 3_575 ? Ag1 Ag3 Ag2 58.70(4) 3_575 3_575 ? Ag2 Ag3 Ag2 90.87(4) . 3_575 ? O5 Si1 O19 111.4(5) . . ? O5 Si1 O20 112.0(5) . . ? O19 Si1 O20 106.7(5) . . ? O5 Si1 O6 106.3(5) . . ? O19 Si1 O6 110.1(5) . . ? O20 Si1 O6 110.5(5) . . ? O5 Si1 Ag1 53.8(3) . . ? O19 Si1 Ag1 124.6(4) . . ? O20 Si1 Ag1 128.7(4) . . ? O6 Si1 Ag1 52.6(3) . . ? W1 O1 Ag2 154.5(5) . . ? W2 O2 Ag3 154.0(6) . . ? W3 O3 Ag3 156.4(6) . 3_575 ? W4 O4 Ag2 159.0(6) . 3_575 ? Si1 O5 W2 127.6(5) . . ? Si1 O5 W1 128.7(5) . . ? W2 O5 W1 91.8(3) . . ? Si1 O5 Ag1 93.9(4) . . ? W2 O5 Ag1 107.6(4) . . ? W1 O5 Ag1 104.7(4) . . ? Si1 O6 W3 129.2(5) . . ? Si1 O6 W4 127.9(5) . . ? W3 O6 W4 91.9(3) . . ? Si1 O6 Ag1 94.9(4) . . ? W3 O6 Ag1 102.9(3) . . ? W4 O6 Ag1 106.6(3) . . ? W2 O11 W1 117.7(6) . . ? W4 O12 W3 119.0(5) . . ? W5 O13 W1 151.5(6) . . ? W6 O14 W2 152.8(6) . . ? W5 O15 W3 152.6(6) . . ? W6 O16 W4 151.0(6) . . ? Si1 O19 W9 127.3(5) . . ? Si1 O19 W7 123.5(5) . . ? W9 O19 W7 93.0(3) . . ? Si1 O19 W5 122.5(5) . . ? W9 O19 W5 90.5(3) . . ? W7 O19 W5 89.6(3) . . ? Si1 O20 W8 125.5(5) . . ? Si1 O20 W10 124.9(5) . . ? W8 O20 W10 92.2(3) . . ? Si1 O20 W6 123.8(5) . . ? W8 O20 W6 89.9(3) . . ? W10 O20 W6 90.0(3) . . ? W7 O21 W1 143.5(6) . . ? W8 O22 W2 140.4(5) . . ? W9 O23 W3 139.2(6) . . ? W10 O24 W4 141.5(6) . . ? W7 O25 W5 118.0(6) . . ? W8 O26 W6 118.5(7) . . ? W9 O27 W5 118.5(5) . . ? W10 O28 W6 119.7(6) . . ? W7 O29 W8 154.4(6) . . ? W10 O30 W9 155.2(6) . . ? W9 O31 W7 121.2(6) . . ? W8 O32 W10 119.5(6) . . ? C151 N101 C163 118(7) . . ? C151 N101 C113 113(6) . . ? C163 N101 C113 6(10) . . ? C151 N101 C109 106(3) . . ? C163 N101 C109 105(4) . . ? C113 N101 C109 104(4) . . ? C151 N101 C105 108(3) . . ? C163 N101 C105 101(6) . . ? C113 N101 C105 106(6) . . ? C109 N101 C105 119(3) . . ? C151 N101 C155 104(3) . . ? C163 N101 C155 123(7) . . ? C113 N101 C155 128(7) . . ? C109 N101 C155 98(3) . . ? C105 N101 C155 25(3) . . ? C151 N101 C101 21(2) . . ? C163 N101 C101 99(6) . . ? C113 N101 C101 94(5) . . ? C109 N101 C101 122(3) . . ? C105 N101 C101 107(3) . . ? C155 N101 C101 112(3) . . ? C151 C101 C102 92(9) . . ? C151 C101 C152 70(8) . . ? C102 C101 C152 23(2) . . ? C151 C101 N101 54(8) . . ? C102 C101 N101 110(4) . . ? C152 C101 N101 95(3) . . ? C152 C102 C153 81(8) . . ? C152 C102 C101 86(9) . . ? C153 C102 C101 109(4) . . ? C152 C102 C151 64(8) . . ? C153 C102 C151 103(4) . . ? C101 C102 C151 22(2) . . ? C152 C102 C103 131(10) . . ? C153 C102 C103 50(3) . . ? C101 C102 C103 102(4) . . ? C151 C102 C103 115(4) . . ? C153 C103 C104 80(4) . . ? C153 C103 C102 53(3) . . ? C104 C103 C102 108(4) . . ? C153 C103 C154 46(3) . . ? C104 C103 C154 35(3) . . ? C102 C103 C154 78(3) . . ? C154 C104 C103 97(5) . . ? C154 C104 C153 49(4) . . ? C103 C104 C153 49(3) . . ? C101 C151 N101 105(9) . . ? C101 C151 C152 87(8) . . ? N101 C151 C152 113(4) . . ? C101 C151 C102 66(8) . . ? N101 C151 C102 117(4) . . ? C152 C151 C102 22(2) . . ? C102 C152 C153 74(8) . . ? C102 C152 C151 95(9) . . ? C153 C152 C151 110(4) . . ? C102 C152 C101 72(8) . . ? C153 C152 C101 103(4) . . ? C151 C152 C101 23(2) . . ? C154 C153 C103 87(4) . . ? C154 C153 C102 111(4) . . ? C103 C153 C102 77(4) . . ? C154 C153 C152 116(4) . . ? C103 C153 C152 102(4) . . ? C102 C153 C152 25(3) . . ? C154 C153 C104 37(3) . . ? C103 C153 C104 52(3) . . ? C102 C153 C104 106(4) . . ? C152 C153 C104 126(4) . . ? C104 C154 C153 94(5) . . ? C104 C154 C103 49(4) . . ? C153 C154 C103 47(3) . . ? C155 C105 C156 55(8) . . ? C155 C105 C106 95(9) . . ? C156 C105 C106 40(3) . . ? C155 C105 N101 93(8) . . ? C156 C105 N101 116(4) . . ? C106 C105 N101 118(4) . . ? C156 C106 C105 69(5) . . ? C156 C106 C107 55(4) . . ? C105 C106 C107 110(4) . . ? C156 C106 C155 43(5) . . ? C105 C106 C155 26(3) . . ? C107 C106 C155 90(4) . . ? C156 C107 C106 41(3) . . ? C156 C107 C108 137(5) . . ? C106 C107 C108 117(4) . . ? C156 C107 C157 63(3) . . ? C106 C107 C157 96(3) . . ? C108 C107 C157 93(3) . . ? C156 C107 C158 115(4) . . ? C106 C107 C158 131(4) . . ? C108 C107 C158 44(3) . . ? C157 C107 C158 54(2) . . ? C158 C108 C107 78(4) . . ? C105 C155 C156 95(9) . . ? C105 C155 C106 60(7) . . ? C156 C155 C106 35(4) . . ? C105 C155 N101 62(7) . . ? C156 C155 N101 119(6) . . ? C106 C155 N101 97(4) . . ? C106 C156 C155 102(7) . . ? C106 C156 C107 84(5) . . ? C155 C156 C107 138(7) . . ? C106 C156 C105 71(5) . . ? C155 C156 C105 30(4) . . ? C107 C156 C105 131(6) . . ? C106 C156 C157 133(7) . . ? C155 C156 C157 124(7) . . ? C107 C156 C157 71(4) . . ? C105 C156 C157 153(6) . . ? C156 C157 C158 112(5) . . ? C156 C157 C107 47(3) . . ? C158 C157 C107 68(4) . . ? C108 C158 C157 110(5) . . ? C108 C158 C107 58(3) . . ? C157 C158 C107 59(3) . . ? N101 C109 C160 125(5) . . ? N101 C109 C110 94(4) . . ? C160 C109 C110 34(5) . . ? C160 C110 C111 17(5) . . ? C160 C110 C109 73(3) . . ? C111 C110 C109 90(5) . . ? C160 C111 C161 121(10) . . ? C160 C111 C110 21(8) . . ? C161 C111 C110 136(10) . . ? C160 C111 C112 153(10) . . ? C161 C111 C112 72(8) . . ? C110 C111 C112 133(8) . . ? C162 C112 C111 99(7) . . ? C162 C112 C161 63(5) . . ? C111 C112 C161 39(5) . . ? C111 C160 C110 142(10) . . ? C111 C160 C109 145(10) . . ? C110 C160 C109 73(3) . . ? C111 C160 C161 35(10) . . ? C110 C160 C161 156(10) . . ? C109 C160 C161 117(7) . . ? C111 C161 C160 24(6) . . ? C111 C161 C162 117(10) . . ? C160 C161 C162 140(9) . . ? C111 C161 C112 69(7) . . ? C160 C161 C112 91(6) . . ? C162 C161 C112 52(6) . . ? C112 C162 C161 65(7) . . ? N101 C113 C114 133(6) . . ? N101 C113 C164 107(6) . . ? C114 C113 C164 36(3) . . ? C164 C114 C165 104(8) . . ? C164 C114 C115 138(9) . . ? C165 C114 C115 35(4) . . ? C164 C114 C113 73(9) . . ? C165 C114 C113 141(10) . . ? C115 C114 C113 142(6) . . ? C164 C114 C163 70(6) . . ? C165 C114 C163 138(10) . . ? C115 C114 C163 143(7) . . ? C113 C114 C163 5(10) . . ? C164 C114 C166 161(9) . . ? C165 C114 C166 62(5) . . ? C115 C114 C166 27(3) . . ? C113 C114 C166 126(7) . . ? C163 C114 C166 129(7) . . ? C166 C115 C165 129(10) . . ? C166 C115 C116 128(10) . . ? C165 C115 C116 96(8) . . ? C166 C115 C114 90(8) . . ? C165 C115 C114 39(5) . . ? C116 C115 C114 127(6) . . ? C115 C116 C165 30(3) . . ? N101 C163 C164 108(5) . . ? N101 C163 C114 129(8) . . ? C164 C163 C114 36(4) . . ? C114 C164 C163 75(9) . . ? C114 C164 C165 39(5) . . ? C163 C164 C165 104(6) . . ? C114 C164 C113 71(8) . . ? C163 C164 C113 5(10) . . ? C165 C164 C113 102(6) . . ? C115 C165 C114 106(8) . . ? C115 C165 C166 23(5) . . ? C114 C165 C166 83(7) . . ? C115 C165 C164 141(8) . . ? C114 C165 C164 37(5) . . ? C166 C165 C164 119(7) . . ? C115 C165 C116 55(5) . . ? C114 C165 C116 145(8) . . ? C166 C165 C116 76(5) . . ? C164 C165 C116 143(6) . . ? C115 C166 C165 28(6) . . ? C115 C166 C114 63(6) . . ? C165 C166 C114 35(4) . . ? N251 N201 C263 96(9) . . ? N251 N201 C205 101(7) . . ? C263 N201 C205 150(10) . . ? N251 N201 C213 116(7) . . ? C263 N201 C213 21(6) . . ? C205 N201 C213 140(5) . . ? N251 N201 C201 27(6) . . ? C263 N201 C201 82(6) . . ? C205 N201 C201 104(5) . . ? C213 N201 C201 103(4) . . ? N251 N201 C255 124(7) . . ? C263 N201 C255 126(10) . . ? C205 N201 C255 26(3) . . ? C213 N201 C255 115(4) . . ? C201 N201 C255 117(5) . . ? N251 N201 C209 73(6) . . ? C263 N201 C209 114(10) . . ? C205 N201 C209 94(4) . . ? C213 N201 C209 110(4) . . ? C201 N201 C209 99(5) . . ? C255 N201 C209 111(4) . . ? N251 N201 C259 35(6) . . ? C263 N201 C259 115(9) . . ? C205 N201 C259 93(4) . . ? C213 N201 C259 126(4) . . ? C201 N201 C259 61(4) . . ? C255 N201 C259 118(4) . . ? C209 N201 C259 40(3) . . ? N251 N201 C251 38(5) . . ? C263 N201 C251 79(6) . . ? C205 N201 C251 100(4) . . ? C213 N201 C251 100(3) . . ? C201 N201 C251 12(5) . . ? C255 N201 C251 109(4) . . ? C209 N201 C251 111(4) . . ? C259 N201 C251 72(3) . . ? N251 N201 C264 136(9) . . ? C263 N201 C264 53(5) . . ? C205 N201 C264 120(6) . . ? C213 N201 C264 32(5) . . ? C201 N201 C264 134(6) . . ? C255 N201 C264 100(6) . . ? C209 N201 C264 91(6) . . ? C259 N201 C264 125(6) . . ? C251 N201 C264 132(6) . . ? N201 N251 C201 135(10) . . ? N201 N251 C259 130(7) . . ? C201 N251 C259 95(8) . . ? N201 N251 C251 126(8) . . ? C201 N251 C251 10(7) . . ? C259 N251 C251 103(5) . . ? N201 N251 C209 82(6) . . ? C201 N251 C209 143(9) . . ? C259 N251 C209 50(4) . . ? C251 N251 C209 152(6) . . ? N201 N251 C263 58(8) . . ? C201 N251 C263 94(7) . . ? C259 N251 C263 136(10) . . ? C251 N251 C263 91(6) . . ? C209 N251 C263 105(7) . . ? N201 N251 C205 57(6) . . ? C201 N251 C205 118(7) . . ? C259 N251 C205 103(5) . . ? C251 N251 C205 110(5) . . ? C209 N251 C205 86(4) . . ? C263 N251 C205 111(9) . . ? N201 N251 C213 46(5) . . ? C201 N251 C213 107(7) . . ? C259 N251 C213 134(5) . . ? C251 N251 C213 104(4) . . ? C209 N251 C213 94(4) . . ? C263 N251 C213 14(5) . . ? C205 N251 C213 101(4) . . ? N201 N251 C260 105(7) . . ? C201 N251 C260 119(8) . . ? C259 N251 C260 31(4) . . ? C251 N251 C260 129(6) . . ? C209 N251 C260 24(4) . . ? C263 N251 C260 111(9) . . ? C205 N251 C260 105(5) . . ? C213 N251 C260 105(5) . . ? N201 N251 C255 40(6) . . ? C201 N251 C255 120(7) . . ? C259 N251 C255 121(5) . . ? C251 N251 C255 110(4) . . ? C209 N251 C255 93(4) . . ? C263 N251 C255 91(8) . . ? C205 N251 C255 20(3) . . ? C213 N251 C255 82(4) . . ? C260 N251 C255 115(4) . . ? C251 C201 N251 153(10) . . ? C251 C201 N201 136(10) . . ? N251 C201 N201 18(4) . . ? C251 C201 C202 69(10) . . ? N251 C201 C202 118(8) . . ? N201 C201 C202 128(6) . . ? C251 C201 C252 59(10) . . ? N251 C201 C252 117(8) . . ? N201 C201 C252 120(5) . . ? C202 C201 C252 22(4) . . ? C251 C201 C263 114(10) . . ? N251 C201 C263 55(5) . . ? N201 C201 C263 44(4) . . ? C202 C201 C263 172(7) . . ? C252 C201 C263 153(9) . . ? C251 C201 C259 148(10) . . ? N251 C201 C259 53(6) . . ? N201 C201 C259 71(4) . . ? C202 C201 C259 80(5) . . ? C252 C201 C259 94(5) . . ? C263 C201 C259 98(6) . . ? C252 C202 C253 98(8) . . ? C252 C202 C251 85(10) . . ? C253 C202 C251 99(6) . . ? C252 C202 C201 96(10) . . ? C253 C202 C201 115(6) . . ? C251 C202 C201 21(3) . . ? C252 C202 C203 66(8) . . ? C253 C202 C203 33(4) . . ? C251 C202 C203 98(5) . . ? C201 C202 C203 119(5) . . ? C253 C203 C252 83(6) . . ? C253 C203 C254 76(6) . . ? C252 C203 C254 120(6) . . ? C253 C203 C202 58(6) . . ? C252 C203 C202 25(4) . . ? C254 C203 C202 107(6) . . ? C253 C203 C204 125(9) . . ? C252 C203 C204 79(5) . . ? C254 C203 C204 69(5) . . ? C202 C203 C204 94(5) . . ? C203 C204 C254 54(4) . . ? C203 C204 C252 47(4) . . ? C254 C204 C252 88(4) . . ? C201 C251 C202 89(10) . . ? C201 C251 N251 17(10) . . ? C202 C251 N251 96(5) . . ? C201 C251 C252 102(10) . . ? C202 C251 C252 25(4) . . ? N251 C251 C252 102(5) . . ? C201 C251 N201 32(10) . . ? C202 C251 N201 107(4) . . ? N251 C251 N201 16(3) . . ? C252 C251 N201 107(4) . . ? C202 C252 C203 89(8) . . ? C202 C252 C251 70(10) . . ? C203 C252 C251 100(5) . . ? C202 C252 C253 57(7) . . ? C203 C252 C253 32(3) . . ? C251 C252 C253 86(4) . . ? C202 C252 C201 62(9) . . ? C203 C252 C201 115(5) . . ? C251 C252 C201 18(3) . . ? C253 C252 C201 94(4) . . ? C202 C252 C204 116(10) . . ? C203 C252 C204 54(3) . . ? C251 C252 C204 151(5) . . ? C253 C252 C204 76(4) . . ? C201 C252 C204 169(5) . . ? C203 C253 C202 90(6) . . ? C203 C253 C252 65(6) . . ? C202 C253 C252 25(4) . . ? C203 C253 C254 72(7) . . ? C202 C253 C254 120(6) . . ? C252 C253 C254 110(5) . . ? C203 C254 C253 31(3) . . ? C203 C254 C204 56(3) . . ? C253 C254 C204 81(4) . . ? C255 C205 N201 78(10) . . ? C255 C205 C206 53(8) . . ? N201 C205 C206 106(5) . . ? C255 C205 N251 98(10) . . ? N201 C205 N251 22(2) . . ? C206 C205 N251 111(5) . . ? C255 C205 C256 41(7) . . ? N201 C205 C256 102(4) . . ? C206 C205 C256 12(4) . . ? N251 C205 C256 112(4) . . ? C256 C206 C255 109(10) . . ? C256 C206 C205 132(10) . . ? C255 C206 C205 24(4) . . ? C256 C206 C207 94(10) . . ? C255 C206 C207 119(6) . . ? C205 C206 C207 107(5) . . ? C256 C206 C257 63(9) . . ? C255 C206 C257 108(6) . . ? C205 C206 C257 112(5) . . ? C207 C206 C257 37(3) . . ? C257 C207 C258 47(5) . . ? C257 C207 C206 80(6) . . ? C258 C207 C206 103(5) . . ? C257 C207 C256 64(4) . . ? C258 C207 C256 84(5) . . ? C206 C207 C256 19(3) . . ? C258 C208 C257 11(6) . . ? C205 C255 C206 103(10) . . ? C205 C255 N201 76(10) . . ? C206 C255 N201 123(6) . . ? C205 C255 C256 123(10) . . ? C206 C255 C256 20(4) . . ? N201 C255 C256 127(5) . . ? C205 C255 N251 62(10) . . ? C206 C255 N251 114(6) . . ? N201 C255 N251 16(2) . . ? C256 C255 N251 124(5) . . ? C206 C256 C255 51(10) . . ? C206 C256 C257 98(10) . . ? C255 C256 C257 104(5) . . ? C206 C256 C207 67(9) . . ? C255 C256 C207 98(5) . . ? C257 C256 C207 38(3) . . ? C206 C256 C205 36(9) . . ? C255 C256 C205 16(3) . . ? C257 C256 C205 100(4) . . ? C207 C256 C205 85(4) . . ? C206 C256 C258 106(10) . . ? C255 C256 C258 130(5) . . ? C257 C256 C258 28(3) . . ? C207 C256 C258 40(3) . . ? C205 C256 C258 122(4) . . ? C258 C257 C207 80(7) . . ? C258 C257 C256 104(6) . . ? C207 C257 C256 78(6) . . ? C258 C257 C206 109(7) . . ? C207 C257 C206 63(4) . . ? C256 C257 C206 19(3) . . ? C258 C257 C208 10(5) . . ? C207 C257 C208 85(6) . . ? C256 C257 C208 96(4) . . ? C206 C257 C208 104(4) . . ? C208 C258 C257 159(10) . . ? C208 C258 C207 135(10) . . ? C257 C258 C207 52(6) . . ? C208 C258 C256 115(8) . . ? C257 C258 C256 48(4) . . ? C207 C258 C256 56(4) . . ? C260 C209 C259 55(9) . . ? C260 C209 N251 110(10) . . ? C259 C209 N251 63(5) . . ? C260 C209 N201 134(10) . . ? C259 C209 N201 88(6) . . ? N251 C209 N201 25(2) . . ? C260 C209 C210 38(10) . . ? C259 C209 C210 83(6) . . ? N251 C209 C210 111(5) . . ? N201 C209 C210 123(5) . . ? C260 C210 C261 92(8) . . ? C260 C210 C211 86(7) . . ? C261 C210 C211 32(3) . . ? C260 C210 C209 26(6) . . ? C261 C210 C209 113(6) . . ? C211 C210 C209 112(5) . . ? C260 C210 C262 106(8) . . ? C261 C210 C262 52(3) . . ? C211 C210 C262 83(4) . . ? C209 C210 C262 106(5) . . ? C260 C210 C259 23(6) . . ? C261 C210 C259 100(5) . . ? C211 C210 C259 82(4) . . ? C209 C210 C259 38(3) . . ? C262 C210 C259 127(5) . . ? C261 C211 C212 39(7) . . ? C261 C211 C210 68(9) . . ? C212 C211 C210 92(4) . . ? C261 C211 C260 79(9) . . ? C212 C211 C260 117(6) . . ? C210 C211 C260 38(4) . . ? C261 C212 C211 31(5) . . ? C261 C212 C262 65(5) . . ? C211 C212 C262 94(5) . . ? C260 C259 C209 42(7) . . ? C260 C259 N251 103(9) . . ? C209 C259 N251 67(5) . . ? C260 C259 C201 127(9) . . ? C209 C259 C201 98(6) . . ? N251 C259 C201 32(3) . . ? C260 C259 N201 91(8) . . ? C209 C259 N201 52(4) . . ? N251 C259 N201 15(2) . . ? C201 C259 N201 47(2) . . ? C260 C259 C210 27(7) . . ? C209 C259 C210 59(5) . . ? N251 C259 C210 100(5) . . ? C201 C259 C210 112(5) . . ? N201 C259 C210 93(4) . . ? C209 C260 C259 83(10) . . ? C209 C260 C210 116(10) . . ? C259 C260 C210 130(10) . . ? C209 C260 N251 46(9) . . ? C259 C260 N251 47(7) . . ? C210 C260 N251 114(8) . . ? C209 C260 C211 172(10) . . ? C259 C260 C211 104(10) . . ? C210 C260 C211 56(6) . . ? N251 C260 C211 137(7) . . ? C209 C260 C261 148(10) . . ? C259 C260 C261 128(10) . . ? C210 C260 C261 50(6) . . ? N251 C260 C261 159(7) . . ? C211 C260 C261 25(3) . . ? C211 C261 C212 110(10) . . ? C211 C261 C210 81(10) . . ? C212 C261 C210 126(10) . . ? C211 C261 C262 159(10) . . ? C212 C261 C262 77(7) . . ? C210 C261 C262 79(6) . . ? C211 C261 C260 76(9) . . ? C212 C261 C260 163(10) . . ? C210 C261 C260 37(4) . . ? C262 C261 C260 92(7) . . ? C261 C262 C212 38(4) . . ? C261 C262 C210 49(5) . . ? C212 C262 C210 78(4) . . ? C263 C213 C264 151(10) . . ? C263 C213 N201 56(10) . . ? C264 C213 N201 99(10) . . ? C263 C213 C214 169(10) . . ? C264 C213 C214 17(10) . . ? N201 C213 C214 114(4) . . ? C263 C213 N251 40(10) . . ? C264 C213 N251 113(10) . . ? N201 C213 N251 19(2) . . ? C214 C213 N251 129(4) . . ? C264 C214 C265 114(10) . . ? C264 C214 C215 134(10) . . ? C265 C214 C215 97(8) . . ? C264 C214 C213 29(10) . . ? C265 C214 C213 140(9) . . ? C215 C214 C213 108(3) . . ? C264 C214 C266 141(10) . . ? C265 C214 C266 69(6) . . ? C215 C214 C266 29(6) . . ? C213 C214 C266 126(8) . . ? C266 C215 C216 53(10) . . ? C266 C215 C214 73(10) . . ? C216 C215 C214 107(4) . . ? C266 C215 C265 40(10) . . ? C216 C215 C265 75(5) . . ? C214 C215 C265 35(4) . . ? C266 C215 C264 79(10) . . ? C216 C215 C264 119(5) . . ? C214 C215 C264 13(5) . . ? C265 C215 C264 44(3) . . ? C266 C216 C215 30(7) . . ? C213 C263 N201 102(10) . . ? C213 C263 N251 126(10) . . ? N201 C263 N251 26(2) . . ? C213 C263 C264 19(10) . . ? N201 C263 C264 87(10) . . ? N251 C263 C264 108(10) . . ? C213 C263 C201 157(10) . . ? N201 C263 C201 54(3) . . ? N251 C263 C201 32(3) . . ? C264 C263 C201 140(9) . . ? C214 C264 C213 134(10) . . ? C214 C264 C263 143(10) . . ? C213 C264 C263 10(6) . . ? C214 C264 C265 44(10) . . ? C213 C264 C265 164(10) . . ? C263 C264 C265 164(10) . . ? C214 C264 N201 159(10) . . ? C213 C264 N201 49(7) . . ? C263 C264 N201 40(5) . . ? C265 C264 N201 141(10) . . ? C214 C264 C215 33(10) . . ? C213 C264 C215 104(10) . . ? C263 C264 C215 113(9) . . ? C265 C264 C215 68(7) . . ? N201 C264 C215 150(8) . . ? C214 C265 C266 66(9) . . ? C214 C265 C264 22(8) . . ? C266 C265 C264 83(10) . . ? C214 C265 C215 48(5) . . ? C266 C265 C215 19(7) . . ? C264 C265 C215 67(8) . . ? C215 C266 C216 98(10) . . ? C215 C266 C265 122(10) . . ? C216 C266 C265 107(10) . . ? C215 C266 C214 78(10) . . ? C216 C266 C214 128(10) . . ? C265 C266 C214 45(6) . . ? C309 N301 C305 111(5) . . ? C309 N301 C301 113(5) . . ? C305 N301 C301 108(3) . . ? C309 N301 C313 83(4) . . ? C305 N301 C313 126(4) . . ? C301 N301 C313 114(4) . . ? C309 N301 C363 125(4) . . ? C305 N301 C363 116(4) . . ? C301 N301 C363 78(4) . . ? C313 N301 C363 47(3) . . ? C309 N301 C355 42(6) . . ? C305 N301 C355 70(5) . . ? C301 N301 C355 118(6) . . ? C313 N301 C355 115(6) . . ? C363 N301 C355 161(6) . . ? C309 N301 C359 7(5) . . ? C305 N301 C359 112(4) . . ? C301 N301 C359 107(4) . . ? C313 N301 C359 88(4) . . ? C363 N301 C359 128(4) . . ? C355 N301 C359 42(5) . . ? C309 N301 C351 101(4) . . ? C305 N301 C351 100(3) . . ? C301 N301 C351 20(3) . . ? C313 N301 C351 130(4) . . ? C363 N301 C351 98(4) . . ? C355 N301 C351 98(5) . . ? C359 N301 C351 94(3) . . ? C301 N351 C309 141(6) . . ? C301 N351 C359 133(5) . . ? C309 N351 C359 10(5) . . ? C301 N351 C355 146(7) . . ? C309 N351 C355 46(6) . . ? C359 N351 C355 47(6) . . ? C301 N351 C351 26(4) . . ? C309 N351 C351 128(5) . . ? C359 N351 C351 118(5) . . ? C355 N351 C351 120(6) . . ? C301 N351 C305 109(4) . . ? C309 N351 C305 109(5) . . ? C359 N351 C305 113(4) . . ? C355 N351 C305 69(5) . . ? C351 N351 C305 106(3) . . ? C301 N351 C313 108(4) . . ? C309 N351 C313 77(4) . . ? C359 N351 C313 85(3) . . ? C355 N351 C313 107(6) . . ? C351 N351 C313 132(4) . . ? C305 N351 C313 101(3) . . ? C301 N351 C363 73(4) . . ? C309 N351 C363 115(4) . . ? C359 N351 C363 122(4) . . ? C355 N351 C363 141(6) . . ? C351 N351 C363 99(4) . . ? C305 N351 C363 95(3) . . ? C313 N351 C363 39(3) . . ? C351 C301 N351 94(8) . . ? C351 C301 N301 108(8) . . ? N351 C301 N301 16(3) . . ? C351 C301 C302 93(9) . . ? N351 C301 C302 108(5) . . ? N301 C301 C302 114(4) . . ? C351 C301 C352 70(7) . . ? N351 C301 C352 124(5) . . ? N301 C301 C352 136(5) . . ? C302 C301 C352 28(3) . . ? C351 C301 C363 161(8) . . ? N351 C301 C363 67(4) . . ? N301 C301 C363 53(3) . . ? C302 C301 C363 95(4) . . ? C352 C301 C363 122(5) . . ? C352 C302 C303 36(5) . . ? C352 C302 C301 83(7) . . ? C303 C302 C301 111(4) . . ? C352 C302 C351 65(6) . . ? C303 C302 C351 99(4) . . ? C301 C302 C351 22(3) . . ? C352 C303 C353 83(5) . . ? C352 C303 C304 162(8) . . ? C353 C303 C304 90(5) . . ? C352 C303 C302 27(4) . . ? C353 C303 C302 107(5) . . ? C304 C303 C302 149(6) . . ? C352 C303 C354 123(7) . . ? C353 C303 C354 55(3) . . ? C304 C303 C354 41(3) . . ? C302 C303 C354 132(5) . . ? C354 C304 C303 83(5) . . ? C354 C304 C353 49(3) . . ? C303 C304 C353 40(3) . . ? C301 C351 N351 60(6) . . ? C301 C351 C352 87(8) . . ? N351 C351 C352 118(4) . . ? C301 C351 C302 65(8) . . ? N351 C351 C302 92(4) . . ? C352 C351 C302 27(2) . . ? C301 C351 N301 52(5) . . ? N351 C351 N301 11(3) . . ? C352 C351 N301 120(4) . . ? C302 C351 N301 93(3) . . ? C302 C352 C303 117(8) . . ? C302 C352 C353 160(9) . . ? C303 C352 C353 56(5) . . ? C302 C352 C351 88(7) . . ? C303 C352 C351 145(7) . . ? C353 C352 C351 108(4) . . ? C302 C352 C301 69(5) . . ? C303 C352 C301 144(8) . . ? C353 C352 C301 129(5) . . ? C351 C352 C301 23(3) . . ? C303 C353 C354 81(5) . . ? C303 C353 C352 41(3) . . ? C354 C353 C352 112(4) . . ? C303 C353 C304 50(3) . . ? C354 C353 C304 38(3) . . ? C352 C353 C304 90(4) . . ? C304 C354 C353 93(5) . . ? C304 C354 C303 56(3) . . ? C353 C354 C303 44(3) . . ? N301 C305 C306 115(3) . . ? N301 C305 N351 14(2) . . ? C306 C305 N351 121(3) . . ? N301 C305 C355 58(4) . . ? C306 C305 C355 82(3) . . ? N351 C305 C355 51(2) . . ? N301 C305 C356 99(4) . . ? C306 C305 C356 35(3) . . ? N351 C305 C356 97(4) . . ? C355 C305 C356 50(3) . . ? C356 C306 C305 92(6) . . ? C356 C306 C307 129(7) . . ? C305 C306 C307 109(2) . . ? C356 C306 C357 61(5) . . ? C305 C306 C357 147(5) . . ? C307 C306 C357 79(5) . . ? C306 C307 C308 110(3) . . ? C358 C308 C307 126(4) . . ? C358 C308 C357 53(4) . . ? C307 C308 C357 74(4) . . ? C309 C355 C310 86(9) . . ? C309 C355 C359 14(5) . . ? C310 C355 C359 72(7) . . ? C309 C355 N351 59(5) . . ? C310 C355 N351 119(7) . . ? C359 C355 N351 67(3) . . ? C309 C355 C356 129(10) . . ? C310 C355 C356 116(7) . . ? C359 C355 C356 138(10) . . ? N351 C355 C356 124(8) . . ? C309 C355 N301 62(4) . . ? C310 C355 N301 134(7) . . ? C359 C355 N301 73(4) . . ? N351 C355 N301 15(2) . . ? C356 C355 N301 110(8) . . ? C309 C355 C360 78(7) . . ? C310 C355 C360 22(4) . . ? C359 C355 C360 63(5) . . ? N351 C355 C360 98(5) . . ? C356 C355 C360 137(7) . . ? N301 C355 C360 113(5) . . ? C309 C355 C305 112(6) . . ? C310 C355 C305 151(10) . . ? C359 C355 C305 124(4) . . ? N351 C355 C305 60(4) . . ? C356 C355 C305 70(7) . . ? N301 C355 C305 51(3) . . ? C360 C355 C305 138(8) . . ? C306 C356 C357 81(8) . . ? C306 C356 C355 110(10) . . ? C357 C356 C355 169(10) . . ? C306 C356 C305 53(6) . . ? C357 C356 C305 131(10) . . ? C355 C356 C305 61(6) . . ? C358 C357 C356 162(10) . . ? C358 C357 C306 127(10) . . ? C356 C357 C306 38(6) . . ? C358 C357 C308 47(6) . . ? C356 C357 C308 124(10) . . ? C306 C357 C308 88(6) . . ? C308 C358 C357 81(8) . . ? C355 C309 N351 74(5) . . ? C355 C309 N301 76(6) . . ? N351 C309 N301 17(3) . . ? C355 C309 C310 48(5) . . ? N351 C309 C310 104(4) . . ? N301 C309 C310 114(5) . . ? C355 C309 C360 65(6) . . ? N351 C309 C360 98(4) . . ? N301 C309 C360 113(4) . . ? C310 C309 C360 24(3) . . ? C355 C309 C313 114(7) . . ? N351 C309 C313 62(3) . . ? N301 C309 C313 48.9(19) . . ? C310 C309 C313 161(5) . . ? C360 C309 C313 158(5) . . ? C361 C311 C362 70(6) . . ? C361 C311 C310 74(5) . . ? C362 C311 C310 104(6) . . ? C361 C311 C312 49(4) . . ? C362 C311 C312 44(5) . . ? C310 C311 C312 120(5) . . ? C361 C311 C360 63(4) . . ? C362 C311 C360 117(6) . . ? C310 C311 C360 25(3) . . ? C312 C311 C360 112(4) . . ? C360 C310 C355 123(9) . . ? C360 C310 C359 89(8) . . ? C355 C310 C359 55(6) . . ? C360 C310 C309 97(8) . . ? C355 C310 C309 46(7) . . ? C359 C310 C309 9(6) . . ? C360 C310 C311 89(7) . . ? C355 C310 C311 131(9) . . ? C359 C310 C311 94(5) . . ? C309 C310 C311 99(4) . . ? C360 C310 C361 72(6) . . ? C355 C310 C361 164(8) . . ? C359 C310 C361 124(5) . . ? C309 C310 C361 132(4) . . ? C311 C310 C361 36(3) . . ? C360 C310 C362 105(6) . . ? C355 C310 C362 130(7) . . ? C359 C310 C362 117(4) . . ? C309 C310 C362 120(4) . . ? C311 C310 C362 28(3) . . ? C361 C310 C362 34(3) . . ? C362 C312 C361 54(4) . . ? C362 C312 C311 35(4) . . ? C361 C312 C311 36(3) . . ? C355 C359 C310 53(6) . . ? C355 C359 N351 67(3) . . ? C310 C359 N351 106(4) . . ? C355 C359 C360 74(7) . . ? C310 C359 C360 28(3) . . ? N351 C359 C360 104(4) . . ? C355 C359 N301 66(4) . . ? C310 C359 N301 112(4) . . ? N351 C359 N301 14(2) . . ? C360 C359 N301 115(4) . . ? C310 C360 C361 81(6) . . ? C310 C360 C359 63(7) . . ? C361 C360 C359 117(4) . . ? C310 C360 C355 36(6) . . ? C361 C360 C355 117(4) . . ? C359 C360 C355 43(5) . . ? C310 C360 C311 66(6) . . ? C361 C360 C311 35(3) . . ? C359 C360 C311 82(3) . . ? C355 C360 C311 94(5) . . ? C310 C360 C309 60(6) . . ? C361 C360 C309 119(4) . . ? C359 C360 C309 5(4) . . ? C355 C360 C309 38(5) . . ? C311 C360 C309 85(4) . . ? C311 C361 C362 55(5) . . ? C311 C361 C312 95(6) . . ? C362 C361 C312 59(4) . . ? C311 C361 C360 82(5) . . ? C362 C361 C360 121(5) . . ? C312 C361 C360 177(6) . . ? C311 C361 C310 70(4) . . ? C362 C361 C310 95(5) . . ? C312 C361 C310 153(6) . . ? C360 C361 C310 27(3) . . ? C311 C362 C361 55(5) . . ? C311 C362 C312 101(7) . . ? C361 C362 C312 67(5) . . ? C311 C362 C310 48(4) . . ? C361 C362 C310 51(4) . . ? C312 C362 C310 118(5) . . ? C363 C313 C364 78(6) . . ? C363 C313 N301 70(4) . . ? C364 C313 N301 106(5) . . ? C363 C313 C314 49(5) . . ? C364 C313 C314 31(4) . . ? N301 C313 C314 102(4) . . ? C363 C313 N351 74(4) . . ? C364 C313 N351 117(5) . . ? N301 C313 N351 11(2) . . ? C314 C313 N351 111(4) . . ? C363 C313 C309 114(5) . . ? C364 C313 C309 133(6) . . ? N301 C313 C309 48.3(19) . . ? C314 C313 C309 148(4) . . ? N351 C313 C309 41(3) . . ? C364 C314 C363 103(10) . . ? C364 C314 C313 58(8) . . ? C363 C314 C313 49(5) . . ? C364 C314 C315 116(10) . . ? C363 C314 C315 110(7) . . ? C313 C314 C315 110(5) . . ? C364 C314 C365 96(10) . . ? C363 C314 C365 134(8) . . ? C313 C314 C365 115(5) . . ? C315 C314 C365 27(4) . . ? C365 C315 C314 74(10) . . ? C365 C315 C316 27(9) . . ? C314 C315 C316 87(5) . . ? C365 C315 C364 60(10) . . ? C314 C315 C364 21(3) . . ? C316 C315 C364 79(4) . . ? C365 C316 C366 106(9) . . ? C365 C316 C315 17(6) . . ? C366 C316 C315 122(8) . . ? C314 C363 C313 81(7) . . ? C314 C363 C364 30(4) . . ? C313 C363 C364 55(5) . . ? C314 C363 N301 117(7) . . ? C313 C363 N301 63(4) . . ? C364 C363 N301 91(5) . . ? C314 C363 N351 128(7) . . ? C313 C363 N351 67(4) . . ? C364 C363 N351 101(5) . . ? N301 C363 N351 11(2) . . ? C314 C363 C301 156(7) . . ? C313 C363 C301 103(5) . . ? C364 C363 C301 139(6) . . ? N301 C363 C301 49(3) . . ? N351 C363 C301 40(3) . . ? C314 C364 C313 91(10) . . ? C314 C364 C363 48(8) . . ? C313 C364 C363 48(4) . . ? C314 C364 C365 58(8) . . ? C313 C364 C365 112(6) . . ? C363 C364 C365 96(6) . . ? C314 C364 C315 43(8) . . ? C313 C364 C315 96(5) . . ? C363 C364 C315 76(5) . . ? C365 C364 C315 20(3) . . ? C315 C365 C316 136(10) . . ? C315 C365 C314 79(10) . . ? C316 C365 C314 117(9) . . ? C315 C365 C366 162(10) . . ? C316 C365 C366 37(5) . . ? C314 C365 C366 119(6) . . ? C315 C365 C364 100(10) . . ? C316 C365 C364 110(8) . . ? C314 C365 C364 26(3) . . ? C366 C365 C364 98(5) . . ? C316 C366 C365 37(5) . . ? N401 C401 C452 119(9) . . ? N401 C401 C402 115(6) . . ? C452 C401 C402 77(7) . . ? N401 C401 C413 53(3) . . ? C452 C401 C413 151(8) . . ? C402 C401 C413 132(7) . . ? C403 C402 C401 107(6) . . ? C403 C402 C453 34(5) . . ? C401 C402 C453 93(7) . . ? C403 C402 C452 78(6) . . ? C401 C402 C452 50(7) . . ? C453 C402 C452 49(3) . . ? C403 C402 C451 104(6) . . ? C401 C402 C451 3(3) . . ? C453 C402 C451 90(6) . . ? C452 C402 C451 49(4) . . ? C403 C402 C404 47(3) . . ? C401 C402 C404 130(6) . . ? C453 C402 C404 80(6) . . ? C452 C402 C404 125(6) . . ? C451 C402 C404 128(6) . . ? C454 C403 C453 103(10) . . ? C454 C403 C402 120(10) . . ? C453 C403 C402 89(10) . . ? C454 C403 C404 96(10) . . ? C453 C403 C404 160(10) . . ? C402 C403 C404 86(5) . . ? C403 C404 C454 30(5) . . ? C403 C404 C402 47(3) . . ? C454 C404 C402 66(6) . . ? N401 C451 C452 116(10) . . ? N401 C451 C413 56(4) . . ? C452 C451 C413 169(10) . . ? N401 C451 C402 100(9) . . ? C452 C451 C402 67(9) . . ? C413 C451 C402 120(10) . . ? N401 C451 C455 44(5) . . ? C452 C451 C455 93(10) . . ? C413 C451 C455 76(6) . . ? C402 C451 C455 126(8) . . ? C401 C452 C451 12(9) . . ? C401 C452 C453 107(10) . . ? C451 C452 C453 115(10) . . ? C401 C452 C402 53(5) . . ? C451 C452 C402 64(10) . . ? C453 C452 C402 63(9) . . ? C403 C453 C454 37(8) . . ? C403 C453 C452 115(10) . . ? C454 C453 C452 106(10) . . ? C403 C453 C402 57(8) . . ? C454 C453 C402 80(10) . . ? C452 C453 C402 68(8) . . ? C403 C454 C453 40(8) . . ? C403 C454 C404 54(9) . . ? C453 C454 C404 94(10) . . ? C456 C405 C455 69(6) . . ? C456 C405 C414 125(10) . . ? C455 C405 C414 149(7) . . ? C456 C405 N401 97(8) . . ? C455 C405 N401 62(3) . . ? C414 C405 N401 87(6) . . ? C456 C405 C413 76(8) . . ? C455 C405 C413 102(6) . . ? C414 C405 C413 61(4) . . ? N401 C405 C413 56(3) . . ? C456 C405 C406 74(8) . . ? C455 C405 C406 142(9) . . ? C414 C405 C406 65(6) . . ? N401 C405 C406 135(8) . . ? C413 C405 C406 80(6) . . ? C407 C406 C405 106(7) . . ? C407 C406 C414 136(8) . . ? C405 C406 C414 51(5) . . ? C407 C406 C456 58(6) . . ? C405 C406 C456 48(6) . . ? C414 C406 C456 91(7) . . ? C407 C406 C457 12(6) . . ? C405 C406 C457 97(7) . . ? C414 C406 C457 124(7) . . ? C456 C406 C457 50(4) . . ? C407 C406 C413 88(6) . . ? C405 C406 C413 52(5) . . ? C414 C406 C413 48(3) . . ? C456 C406 C413 58(5) . . ? C457 C406 C413 76(5) . . ? C457 C407 C458 84(10) . . ? C457 C407 C408 77(10) . . ? C458 C407 C408 67(7) . . ? C457 C407 C406 128(10) . . ? C458 C407 C406 142(10) . . ? C408 C407 C406 133(8) . . ? C457 C407 C456 73(10) . . ? C458 C407 C456 112(9) . . ? C408 C407 C456 150(9) . . ? C406 C407 C456 68(7) . . ? C407 C408 C457 19(8) . . ? C407 C408 C458 56(7) . . ? C457 C408 C458 57(4) . . ? C405 C455 N401 63(3) . . ? C405 C455 C410 161(10) . . ? N401 C455 C410 106(8) . . ? C405 C455 C409 99(9) . . ? N401 C455 C409 60(3) . . ? C410 C455 C409 63(5) . . ? C405 C455 C456 55(7) . . ? N401 C455 C456 90(8) . . ? C410 C455 C456 143(10) . . ? C409 C455 C456 148(8) . . ? C405 C455 C459 92(7) . . ? N401 C455 C459 50(4) . . ? C410 C455 C459 70(8) . . ? C409 C455 C459 9(3) . . ? C456 C455 C459 139(8) . . ? C405 C455 C460 128(10) . . ? N401 C455 C460 95(6) . . ? C410 C455 C460 34(6) . . ? C409 C455 C460 37(5) . . ? C456 C455 C460 174(8) . . ? C459 C455 C460 46(3) . . ? C405 C455 C451 87(6) . . ? N401 C455 C451 44(5) . . ? C410 C455 C451 95(9) . . ? C409 C455 C451 89(8) . . ? C456 C455 C451 73(8) . . ? C459 C455 C451 82(7) . . ? C460 C455 C451 110(8) . . ? C405 C456 C455 55(7) . . ? C405 C456 C457 126(10) . . ? C455 C456 C457 175(10) . . ? C405 C456 C407 112(10) . . ? C455 C456 C407 166(10) . . ? C457 C456 C407 18(8) . . ? C405 C456 C406 58(6) . . ? C455 C456 C406 112(10) . . ? C457 C456 C406 70(9) . . ? C407 C456 C406 54(5) . . ? C405 C456 C413 59(7) . . ? C455 C456 C413 86(7) . . ? C457 C456 C413 90(8) . . ? C407 C456 C413 92(8) . . ? C406 C456 C413 69(7) . . ? C407 C457 C458 77(10) . . ? C407 C457 C456 88(10) . . ? C458 C457 C456 114(10) . . ? C407 C457 C408 84(10) . . ? C458 C457 C408 67(7) . . ? C456 C457 C408 172(10) . . ? C407 C457 C406 40(10) . . ? C458 C457 C406 114(10) . . ? C456 C457 C406 60(8) . . ? C408 C457 C406 112(9) . . ? C407 C458 C457 19(8) . . ? C407 C458 C408 57(5) . . ? C457 C458 C408 56(7) . . ? C460 C409 N401 150(10) . . ? C460 C409 C455 96(9) . . ? N401 C409 C455 60(3) . . ? C460 C409 C410 48(7) . . ? N401 C409 C410 103(8) . . ? C455 C409 C410 58(7) . . ? C460 C410 C461 80(7) . . ? C460 C410 C455 100(10) . . ? C461 C410 C455 143(10) . . ? C460 C410 C411 39(6) . . ? C461 C410 C411 45(6) . . ? C455 C410 C411 137(10) . . ? C460 C410 C409 52(6) . . ? C461 C410 C409 132(9) . . ? C455 C410 C409 59(7) . . ? C411 C410 C409 89(7) . . ? C460 C410 C459 52(7) . . ? C461 C410 C459 132(8) . . ? C455 C410 C459 65(7) . . ? C411 C410 C459 87(7) . . ? C409 C410 C459 8(10) . . ? C460 C411 C461 96(9) . . ? C460 C411 C462 150(10) . . ? C461 C411 C462 77(7) . . ? C460 C411 C412 76(10) . . ? C461 C411 C412 156(10) . . ? C462 C411 C412 121(10) . . ? C460 C411 C410 49(8) . . ? C461 C411 C410 52(7) . . ? C462 C411 C410 129(9) . . ? C412 C411 C410 110(9) . . ? C411 C412 C460 36(5) . . ? N401 C459 C460 120(8) . . ? N401 C459 C455 50(4) . . ? C460 C459 C455 72(6) . . ? N401 C459 C410 86(6) . . ? C460 C459 C410 36(6) . . ? C455 C459 C410 45(5) . . ? C411 C460 C410 93(10) . . ? C411 C460 C409 157(10) . . ? C410 C460 C409 80(7) . . ? C411 C460 C461 46(7) . . ? C410 C460 C461 52(7) . . ? C409 C460 C461 132(10) . . ? C411 C460 C459 148(10) . . ? C410 C460 C459 91(10) . . ? C409 C460 C459 15(8) . . ? C461 C460 C459 142(10) . . ? C411 C460 C412 68(8) . . ? C410 C460 C412 130(10) . . ? C409 C460 C412 100(10) . . ? C461 C460 C412 111(8) . . ? C459 C460 C412 85(7) . . ? C411 C460 C455 137(10) . . ? C410 C460 C455 46(8) . . ? C409 C460 C455 47(6) . . ? C461 C460 C455 91(7) . . ? C459 C460 C455 62(6) . . ? C412 C460 C455 144(7) . . ? C411 C461 C410 82(7) . . ? C411 C461 C460 39(7) . . ? C410 C461 C460 48(7) . . ? C411 C461 C462 58(7) . . ? C410 C461 C462 140(9) . . ? C460 C461 C462 93(8) . . ? C411 C462 C461 44(6) . . ? N401 C413 C405 56(3) . . ? N401 C413 C414 80(6) . . ? C405 C413 C414 49(5) . . ? N401 C413 C451 56(4) . . ? C405 C413 C451 95(7) . . ? C414 C413 C451 135(7) . . ? N401 C413 C456 78(6) . . ? C405 C413 C456 45(5) . . ? C414 C413 C456 88(7) . . ? C451 C413 C456 77(9) . . ? N401 C413 C463 60(4) . . ? C405 C413 C463 83(5) . . ? C414 C413 C463 55(4) . . ? C451 C413 C463 101(7) . . ? C456 C413 C463 126(6) . . ? N401 C413 C406 104(5) . . ? C405 C413 C406 48(3) . . ? C414 C413 C406 49(5) . . ? C451 C413 C406 130(9) . . ? C456 C413 C406 53(6) . . ? C463 C413 C406 104(5) . . ? N401 C413 C401 53(3) . . ? C405 C413 C401 98(5) . . ? C414 C413 C401 133(6) . . ? C451 C413 C401 10(8) . . ? C456 C413 C401 86(6) . . ? C463 C413 C401 93(5) . . ? C406 C413 C401 138(6) . . ? C405 C414 C415 132(10) . . ? C405 C414 C413 70(7) . . ? C415 C414 C413 109(3) . . ? C405 C414 C406 64(4) . . ? C415 C414 C406 162(10) . . ? C413 C414 C406 83(7) . . ? C405 C414 C463 105(8) . . ? C415 C414 C463 39(5) . . ? C413 C414 C463 73(5) . . ? C406 C414 C463 156(8) . . ? C405 C414 C464 126(10) . . ? C415 C414 C464 19(5) . . ? C413 C414 C464 125(6) . . ? C406 C414 C464 152(7) . . ? C463 C414 C464 53(4) . . ? C463 C415 C414 75(7) . . ? C463 C415 C416 135(10) . . ? C414 C415 C416 147(10) . . ? C463 C415 C465 113(10) . . ? C414 C415 C465 172(10) . . ? C416 C415 C465 24(6) . . ? C465 C416 C466 95(10) . . ? C465 C416 C464 89(10) . . ? C466 C416 C464 115(10) . . ? C465 C416 C415 87(10) . . ? C466 C416 C415 139(10) . . ? C464 C416 C415 23(6) . . ? C415 C463 C464 16(10) . . ? C415 C463 C414 66(6) . . ? C464 C463 C414 70(6) . . ? C415 C463 N401 130(10) . . ? C464 C463 N401 122(6) . . ? C414 C463 N401 71(6) . . ? C415 C463 C413 114(9) . . ? C464 C463 C413 122(7) . . ? C414 C463 C413 52(3) . . ? N401 C463 C413 48(3) . . ? C416 C464 C463 110(8) . . ? C416 C464 C465 26(6) . . ? C463 C464 C465 95(6) . . ? C416 C464 C414 133(9) . . ? C463 C464 C414 57(5) . . ? C465 C464 C414 142(7) . . ? C416 C465 C466 58(10) . . ? C416 C465 C464 65(10) . . ? C466 C465 C464 96(6) . . ? C416 C465 C415 69(10) . . ? C466 C465 C415 114(8) . . ? C464 C465 C415 22(5) . . ? C416 C466 C465 26(7) . . ? C459 N401 C409 18(7) . . ? C459 N401 C455 79(7) . . ? C409 N401 C455 61(6) . . ? C459 N401 C451 126(10) . . ? C409 N401 C451 120(9) . . ? C455 N401 C451 91(10) . . ? C459 N401 C413 166(8) . . ? C409 N401 C413 162(9) . . ? C455 N401 C413 106(7) . . ? C451 N401 C413 68(7) . . ? C459 N401 C405 106(8) . . ? C409 N401 C405 94(8) . . ? C455 N401 C405 55(6) . . ? C451 N401 C405 111(9) . . ? C413 N401 C405 68(6) . . ? C459 N401 C401 118(8) . . ? C409 N401 C401 117(8) . . ? C455 N401 C401 100(8) . . ? C451 N401 C401 13(9) . . ? C413 N401 C401 74(5) . . ? C405 N401 C401 124(6) . . ? C459 N401 C463 96(6) . . ? C409 N401 C463 112(7) . . ? C455 N401 C463 145(8) . . ? C451 N401 C463 118(9) . . ? C413 N401 C463 72(5) . . ? C405 N401 C463 94(6) . . ? C401 N401 C463 112(5) . . ? loop_ _platon_squeeze_void_nr _platon_squeeze_void_average_x _platon_squeeze_void_average_y _platon_squeeze_void_average_z _platon_squeeze_void_volume _platon_squeeze_void_count_electrons _platon_squeeze_void_content 1 0.500 0.500 0.000 889 255 ' ' 2 1.000 0.000 0.500 889 255 ' ' 3 0.519 0.114 0.299 8 6 ' ' 4 0.493 0.118 0.363 9 6 ' ' 5 0.639 0.151 0.653 18 7 ' ' 6 0.139 0.348 0.153 18 7 ' ' 7 -0.004 0.382 0.857 11 8 ' ' 8 0.021 0.385 0.792 6 4 ' ' 9 0.004 0.617 0.143 10 8 ' ' 10 0.979 0.614 0.208 6 4 ' ' 11 0.861 0.651 0.847 18 7 ' ' 12 0.361 0.848 0.347 18 7 ' ' 13 0.504 0.882 0.643 10 8 ' ' 14 0.479 0.885 0.708 6 4 ' ' _platon_squeeze_details ; ;