# Electronic Supplementary Material (ESI) for Chemical Communications # This journal is © The Royal Society of Chemistry 2013 ####################################################################### # # Cambridge Crystallographic Data Centre # CCDC # ####################################################################### # # This CIF contains data from an original supplementary publication # deposited with the CCDC, and may include chemical, crystal, # experimental, refinement, atomic coordinates, # anisotropic displacement parameters and molecular geometry data, # as required by the journal to which it was submitted. # # This CIF is provided on the understanding that it is used for bona # fide research purposes only. It may contain copyright material # of the CCDC or of third parties, and may not be copied or further # disseminated in any form, whether machine-readable or not, # except for the purpose of generating routine backup copies # on your local computer system. # # For further information on the CCDC, data deposition and # data retrieval see: # www.ccdc.cam.ac.uk # # Bona fide researchers may freely download Mercury and enCIFer # from this site to visualise CIF-encoded structures and # to carry out CIF format checking respectively. # data_enterobactin _audit_creation_method SHELXL-2012 #----------------------------------------------------------------------------# # CHEMICAL INFORMATION # #----------------------------------------------------------------------------# _chemical_name_systematic ; ? ; _chemical_name_common 'Complex between enterobactin and silicon' _chemical_melting_point ? _chemical_formula_moiety 'C32 H28 N3 Na2 O18 Si' _chemical_formula_sum 'C32 H28 N3 Na2 O18 Si' _chemical_formula_weight 816.64 _chemical_compound_source 'Isolated natural product' loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Na Na 0.1353 0.1239 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.2541 0.3302 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 4 _space_group_name_H-M_alt 'P 21' _space_group_name_Hall 'P 2yb' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' #----------------------------------------------------------------------------# # UNIT CELL INFORMATION # #----------------------------------------------------------------------------# _cell_length_a 11.2372(18) _cell_length_b 9.8524(15) _cell_length_c 15.840(3) _cell_angle_alpha 90 _cell_angle_beta 106.713(8) _cell_angle_gamma 90 _cell_volume 1679.6(5) _cell_formula_units_Z 2 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 9834 _cell_measurement_theta_min 4.1075 _cell_measurement_theta_max 75.1 #----------------------------------------------------------------------------# # CRYSTAL INFORMATION # #----------------------------------------------------------------------------# _exptl_crystal_description cube _exptl_crystal_colour colorless _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.6148 _exptl_crystal_F_000 842 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.24 _exptl_crystal_size_mid 0.21 _exptl_crystal_size_min 0.18 #----------------------------------------------------------------------------# # ABSORPTION CORRECTION # #----------------------------------------------------------------------------# _exptl_absorpt_coefficient_mu 1.683 _exptl_absorpt_correction_type empirical _exptl_absorpt_correction_T_min 0.6709 _exptl_absorpt_correction_T_max 0.7533 _exptl_absorpt_process_details ; SADABS version 2008/2, multi-scan. (G. M. Sheldrick, 2008) ; #----------------------------------------------------------------------------# # COMPUTER PROGRAMS USED # #----------------------------------------------------------------------------# _computing_data_collection 'Apex2 v2009.11-0 (Bruker AXS, 2009)' _computing_cell_refinement 'SAINT V7.61A (Bruker AXS, 2008)' _computing_data_reduction 'SAINT V7.61A (Bruker AXS, 2008)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 2008)' _computing_structure_refinement 'SHELXL-12 (Sheldrick, 2012)' _computing_publication_material 'enCIFer 1.4, CCDC, 2011' _exptl_special_details ; ? ; _diffrn_measurement_device_type 'Bruker SMART 6000 Diffractometer' _diffrn_detector_area_resol_mean 5.6020 _diffrn_radiation_wavelength 1.54178 _diffrn_radiation_type CuK\a _diffrn_source ? _diffrn_measurement_method ? _diffrn_ambient_temperature 100(2) _diffrn_reflns_number 33667 _diffrn_reflns_av_unetI/netI 0.0212 _diffrn_reflns_av_R_equivalents 0.0324 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_l_min -19 _diffrn_reflns_limit_l_max 19 _diffrn_orient_matrix_UB_11 2.2650883e-02 _diffrn_orient_matrix_UB_12 9.8435007e-02 _diffrn_orient_matrix_UB_13 4.8580267e-03 _diffrn_orient_matrix_UB_21 -2.3300067e-02 _diffrn_orient_matrix_UB_22 6.7767682e-03 _diffrn_orient_matrix_UB_23 -6.5723985e-02 _diffrn_orient_matrix_UB_31 -8.7047696e-02 _diffrn_orient_matrix_UB_32 2.3800062e-02 _diffrn_orient_matrix_UB_33 -1.3783025e-03 _diffrn_reflns_theta_min 2.913 _diffrn_reflns_theta_max 70.331 _diffrn_reflns_theta_full 67.679 _diffrn_measured_fraction_theta_max 0.987 _diffrn_measured_fraction_theta_full 0.995 _diffrn_reflns_Laue_measured_fraction_max 0.987 _diffrn_reflns_Laue_measured_fraction_full 0.995 _diffrn_reflns_point_group_measured_fraction_max 0.961 _diffrn_reflns_point_group_measured_fraction_full 0.976 _reflns_number_total 6167 _reflns_number_gt 5913 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.832 _reflns_Friedel_fraction_max 0.931 _reflns_Friedel_fraction_full 0.954 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _refine_special_details ; The following restraints were used for the disordered solvent: ISOR 0.01 O2M_2 C2M_2 SIMU 0.01 O2M_2 C2M_2 SIMU 0.01 O1M_2 C1M_2 DELU 0.01 O1M_2 C1M_2 ISOR 0.01 O1M_2 O3M_3 ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details ; w=1/[\s^2^(Fo^2^)+(0.0504P)^2^+0.4447P] where P=(Fo^2^+2Fc^2^)/3 ; _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_abs_structure_details ; Flack x determined using 2609 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons and Flack (2004), Acta Cryst. A60, s61). ; _refine_ls_abs_structure_Flack 0.018(8) _chemical_absolute_configuration ad _refine_ls_number_reflns 6168 _refine_ls_number_parameters 547 _refine_ls_number_restraints 58 _refine_ls_R_factor_all 0.0310 _refine_ls_R_factor_gt 0.0293 _refine_ls_wR_factor_ref 0.0782 _refine_ls_wR_factor_gt 0.0768 _refine_ls_goodness_of_fit_ref 1.038 _refine_ls_restrained_S_all 1.077 _refine_ls_shift/su_max 0.003 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Si1 Si 0.04270(7) 0.42002(8) 0.26995(5) 0.02024(15) Uani 1 1 d . . . . . Na1 Na 0.40019(10) 0.06217(12) 0.20918(7) 0.0277(3) Uani 1 1 d . . . . . Na2 Na 0.23005(10) 0.17705(11) 0.35466(7) 0.0236(2) Uani 1 1 d . . . . . O1 O -0.44684(19) 0.8897(2) 0.24672(14) 0.0303(5) Uani 1 1 d . . . . . N1 N -0.2163(2) 0.6575(2) 0.37138(15) 0.0214(5) Uani 1 1 d . . . . . H1N H -0.1816 0.6263 0.3321 0.026 Uiso 1 1 calc R U . . . C1 C -0.2785(2) 0.7862(3) 0.35580(17) 0.0224(5) Uani 1 1 d . . . . . H1 H -0.3270 0.7939 0.3995 0.027 Uiso 1 1 calc R U . . . O2 O -0.10573(17) 0.89517(19) 0.31734(12) 0.0228(4) Uani 1 1 d . . . . . C2 C -0.3719(2) 0.7995(3) 0.26478(18) 0.0230(5) Uani 1 1 d . . . . . O3 O -0.25747(18) 0.6191(2) 0.50127(12) 0.0238(4) Uani 1 1 d . . . . . C3 C -0.1871(3) 0.9039(3) 0.37399(18) 0.0237(5) Uani 1 1 d . . . . . H3A H -0.2333 0.9908 0.3632 0.028 Uiso 1 1 calc R U . . . H3B H -0.1367 0.9019 0.4365 0.028 Uiso 1 1 calc R U . . . O4 O -0.03776(17) 0.50288(19) 0.33710(12) 0.0195(4) Uani 1 1 d . . . . . C4 C -0.2090(2) 0.5824(3) 0.44378(16) 0.0196(5) Uani 1 1 d . . . . . O5 O 0.01352(17) 0.26277(19) 0.31685(12) 0.0217(4) Uani 1 1 d . . . . . C5 C -0.1463(2) 0.4495(3) 0.44644(17) 0.0206(5) Uani 1 1 d . . . . . C6 C -0.1664(3) 0.3479(3) 0.50318(18) 0.0249(6) Uani 1 1 d . . . . . H6 H -0.2124 0.3686 0.5433 0.030 Uiso 1 1 calc R U . . . C7 C -0.1201(3) 0.2189(3) 0.50133(19) 0.0271(6) Uani 1 1 d . . . . . H7 H -0.1310 0.1526 0.5420 0.032 Uiso 1 1 calc R U . . . C8 C -0.0568(2) 0.1847(3) 0.43949(18) 0.0235(5) Uani 1 1 d . . . . . H8 H -0.0265 0.0952 0.4372 0.028 Uiso 1 1 calc R U . . . C9 C -0.0395(2) 0.2824(3) 0.38268(17) 0.0207(5) Uani 1 1 d . . . . . C10 C -0.0757(2) 0.4162(3) 0.39007(16) 0.0194(5) Uani 1 1 d . . . . . O11A O -0.3744(10) 0.9256(13) 0.0405(12) 0.057(5) Uani 0.276(15) 1 d . . P A 1 O11B O -0.3517(3) 0.8991(3) -0.0108(3) 0.0327(15) Uani 0.724(15) 1 d . . P A 2 N11 N -0.2952(2) 0.5645(3) 0.07098(16) 0.0292(5) Uani 1 1 d . . . . . H11N H -0.2500 0.5482 0.1254 0.035 Uiso 1 1 calc R U . . . C11 C -0.3760(3) 0.6823(3) 0.0532(2) 0.0324(7) Uani 1 1 d . . . . . H11 H -0.4392 0.6662 -0.0049 0.039 Uiso 1 1 calc R U . . . O12 O -0.3589(2) 0.7034(2) 0.20907(13) 0.0308(5) Uani 1 1 d . . . . . C12 C -0.3076(3) 0.8131(4) 0.0441(2) 0.0377(7) Uani 1 1 d . . . . . O13 O -0.3592(2) 0.4890(3) -0.06934(14) 0.0409(6) Uani 1 1 d . . . . . C13 C -0.4470(3) 0.7005(3) 0.1209(2) 0.0344(7) Uani 1 1 d . . . . . H13A H -0.4947 0.7864 0.1096 0.041 Uiso 1 1 calc R U . . . H13B H -0.5063 0.6247 0.1164 0.041 Uiso 1 1 calc R U . . . O14 O -0.09717(18) 0.43760(19) 0.18179(12) 0.0227(4) Uani 1 1 d . . . . . C14 C -0.2877(3) 0.4793(3) 0.00602(19) 0.0289(6) Uani 1 1 d . . . . . O15 O 0.10115(19) 0.3202(2) 0.19571(13) 0.0276(4) Uani 1 1 d . . . . . C15 C -0.1859(3) 0.3771(3) 0.02736(19) 0.0285(6) Uani 1 1 d . . . . . C16 C -0.1717(3) 0.2901(3) -0.0404(2) 0.0351(7) Uani 1 1 d . . . . . H16 H -0.2346 0.2881 -0.0953 0.042 Uiso 1 1 calc R U . . . C17 C -0.0691(4) 0.2090(3) -0.0283(2) 0.0381(8) Uani 1 1 d . . . . . H17 H -0.0636 0.1483 -0.0737 0.046 Uiso 1 1 calc R U . . . C18 C 0.0275(3) 0.2147(3) 0.0503(2) 0.0331(7) Uani 1 1 d . . . . . H18 H 0.1006 0.1620 0.0575 0.040 Uiso 1 1 calc R U . . . C19 C 0.0150(3) 0.2980(3) 0.11717(19) 0.0272(6) Uani 1 1 d . . . . . C20 C -0.0949(3) 0.3722(3) 0.10807(18) 0.0243(6) Uani 1 1 d . . . . . O21 O -0.2169(2) 1.0547(2) 0.22702(15) 0.0342(5) Uani 1 1 d . . . . . N21 N 0.0490(2) 0.8542(2) 0.22189(15) 0.0221(5) Uani 1 1 d . . . . . H21N H 0.0222 0.7698 0.2177 0.027 Uiso 1 1 calc R U . . . C21 C -0.0413(3) 0.9612(3) 0.19122(18) 0.0226(6) Uani 1 1 d . . . . . H21 H 0.0049 1.0486 0.1942 0.027 Uiso 1 1 calc R U . . . O22 O -0.1916(2) 0.8171(2) 0.09583(14) 0.0307(5) Uani 1 1 d . . . . . C22 C -0.1313(2) 0.9767(3) 0.24722(18) 0.0228(6) Uani 1 1 d . . . . . O23 O 0.21803(18) 0.9916(2) 0.25836(13) 0.0248(4) Uani 1 1 d . . . . . C23 C -0.1201(3) 0.9407(3) 0.09643(19) 0.0278(6) Uani 1 1 d . . . . . H23A H -0.1763 1.0191 0.0764 0.033 Uiso 1 1 calc R U . . . H23B H -0.0665 0.9310 0.0569 0.033 Uiso 1 1 calc R U . . . O24 O 0.08612(17) 0.58498(19) 0.24128(12) 0.0218(4) Uani 1 1 d . . . . . C24 C 0.1708(3) 0.8762(3) 0.25624(17) 0.0213(5) Uani 1 1 d . . . . . O25 O 0.19488(17) 0.4104(2) 0.34660(13) 0.0251(4) Uani 1 1 d . . . . . C25 C 0.2467(3) 0.7566(3) 0.29684(18) 0.0225(5) Uani 1 1 d . . . . . C26 C 0.3684(3) 0.7781(3) 0.3517(2) 0.0279(6) Uani 1 1 d . . . . . H26 H 0.4047 0.8657 0.3546 0.033 Uiso 1 1 calc R U . . . C27 C 0.4355(3) 0.6735(3) 0.4012(2) 0.0324(7) Uani 1 1 d . . . . . H27 H 0.5191 0.6888 0.4351 0.039 Uiso 1 1 calc R U . . . C28 C 0.3823(3) 0.5451(3) 0.4021(2) 0.0309(6) Uani 1 1 d . . . . . H28 H 0.4276 0.4744 0.4381 0.037 Uiso 1 1 calc R U . . . C29 C 0.2626(3) 0.5237(3) 0.34942(19) 0.0244(6) Uani 1 1 d . . . . . C30 C 0.1976(2) 0.6259(3) 0.29281(18) 0.0213(5) Uani 1 1 d . . . . . O1M_2 O 0.5631(4) 0.1876(5) 0.1767(3) 0.0365(10) Uani 0.5 1 d . U P B 1 C1M_2 C 0.6159(8) 0.3150(10) 0.1799(9) 0.060(3) Uani 0.5 1 d . U P B 1 H21M_2 H 0.6250 0.3378 0.1219 0.090 Uiso 0.5 1 calc R U P B 1 H22M_2 H 0.6977 0.3152 0.2237 0.090 Uiso 0.5 1 calc R U P B 1 H23M_2 H 0.5623 0.3822 0.1964 0.090 Uiso 0.5 1 calc R U P B 1 O2M_2 O 0.5916(5) 0.2049(6) 0.2567(4) 0.0509(13) Uani 0.5 1 d . U P B 2 C2M_2 C 0.6216(9) 0.3328(10) 0.2334(7) 0.052(2) Uani 0.5 1 d . U P B 2 H24M_2 H 0.5815 0.3477 0.1704 0.078 Uiso 0.5 1 calc R U P B 2 H25M_2 H 0.7119 0.3402 0.2454 0.078 Uiso 0.5 1 calc R U P B 2 H26M_2 H 0.5925 0.4013 0.2677 0.078 Uiso 0.5 1 calc R U P B 2 O3M_3 O 0.4412(3) 0.1888(4) 0.3536(3) 0.0853(12) Uani 1 1 d . U . C -1 C3M_3 C 0.5585(8) 0.2116(10) 0.3881(6) 0.082(2) Uani 0.6666 1 d . U P C -1 H31M_3 H 0.5695 0.2907 0.4271 0.122 Uiso 0.6666 1 calc R U P C -1 H32M_3 H 0.5974 0.2292 0.3412 0.122 Uiso 0.6666 1 calc R U P C -1 H33M_3 H 0.5974 0.1320 0.4221 0.122 Uiso 0.6666 1 calc R U P C -1 O4M_4 O 0.3280(3) 0.2926(4) 0.1814(2) 0.0631(8) Uani 1 1 d D U . . . H4M_4 H 0.2572 0.2801 0.1880 0.15(3) Uiso 1 1 calc R . . . . C4M_4 C 0.3453(14) 0.4333(6) 0.1686(14) 0.087(5) Uani 0.3333 1 d D U P . . H41M_4 H 0.3621 0.4808 0.2252 0.131 Uiso 0.3333 1 calc R U P . . H42M_4 H 0.2700 0.4706 0.1273 0.131 Uiso 0.3333 1 calc R U P . . H43M_4 H 0.4157 0.4455 0.1445 0.131 Uiso 0.3333 1 calc R U P . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Si1 0.0245(3) 0.0144(3) 0.0238(3) 0.0010(3) 0.0102(3) 0.0023(3) Na1 0.0277(6) 0.0275(6) 0.0291(5) -0.0010(5) 0.0100(4) 0.0025(5) Na2 0.0294(6) 0.0180(5) 0.0243(5) 0.0005(4) 0.0090(4) 0.0032(4) O1 0.0284(11) 0.0265(11) 0.0363(11) 0.0064(8) 0.0099(8) 0.0082(8) N1 0.0257(12) 0.0192(11) 0.0222(11) 0.0008(9) 0.0113(9) 0.0031(9) C1 0.0232(13) 0.0214(13) 0.0255(13) 0.0005(11) 0.0113(10) 0.0034(10) O2 0.0235(9) 0.0208(10) 0.0263(9) 0.0026(7) 0.0108(7) 0.0024(7) C2 0.0213(13) 0.0204(13) 0.0292(14) 0.0043(11) 0.0100(10) -0.0004(11) O3 0.0231(10) 0.0285(10) 0.0211(9) -0.0005(7) 0.0085(7) 0.0022(7) C3 0.0254(13) 0.0228(13) 0.0253(13) -0.0002(11) 0.0109(10) 0.0027(11) O4 0.0237(9) 0.0157(8) 0.0213(9) 0.0025(7) 0.0099(7) 0.0020(7) C4 0.0160(12) 0.0236(13) 0.0187(12) -0.0020(10) 0.0041(9) -0.0022(10) O5 0.0259(10) 0.0167(9) 0.0241(9) -0.0001(7) 0.0098(7) 0.0002(7) C5 0.0200(13) 0.0212(13) 0.0183(12) -0.0002(10) 0.0017(9) -0.0016(10) C6 0.0251(14) 0.0301(15) 0.0203(12) 0.0031(11) 0.0075(10) -0.0009(11) C7 0.0281(14) 0.0260(14) 0.0267(14) 0.0078(11) 0.0074(11) -0.0018(11) C8 0.0212(13) 0.0196(12) 0.0273(13) 0.0036(11) 0.0031(10) -0.0003(10) C9 0.0190(12) 0.0204(13) 0.0213(12) 0.0001(10) 0.0038(9) -0.0016(10) C10 0.0200(12) 0.0186(12) 0.0179(11) 0.0031(11) 0.0029(9) -0.0022(10) O11A 0.045(6) 0.048(6) 0.074(12) 0.004(7) 0.012(5) 0.000(5) O11B 0.0405(19) 0.0237(17) 0.028(2) 0.0069(13) 0.0007(14) 0.0043(13) N11 0.0364(14) 0.0246(13) 0.0221(11) 0.0006(10) 0.0012(10) -0.0001(11) C11 0.0347(16) 0.0276(15) 0.0274(14) 0.0007(13) -0.0028(12) 0.0000(13) O12 0.0303(11) 0.0288(11) 0.0278(10) -0.0040(8) -0.0007(8) 0.0072(8) C12 0.0393(17) 0.0276(16) 0.0389(17) 0.0034(14) -0.0004(14) -0.0012(14) O13 0.0519(14) 0.0418(13) 0.0237(11) -0.0008(10) 0.0024(10) -0.0060(11) C13 0.0289(15) 0.0306(16) 0.0349(16) -0.0008(13) -0.0049(12) 0.0022(12) O14 0.0312(10) 0.0188(9) 0.0198(9) -0.0021(7) 0.0101(7) 0.0006(8) C14 0.0392(17) 0.0254(15) 0.0212(13) -0.0002(11) 0.0072(12) -0.0126(12) O15 0.0359(11) 0.0199(9) 0.0320(10) -0.0013(8) 0.0179(8) 0.0029(8) C15 0.0429(17) 0.0205(14) 0.0245(13) -0.0003(11) 0.0132(12) -0.0085(12) C16 0.057(2) 0.0271(16) 0.0262(14) -0.0052(13) 0.0198(13) -0.0128(14) C17 0.067(2) 0.0255(16) 0.0321(16) -0.0056(12) 0.0306(16) -0.0096(14) C18 0.052(2) 0.0182(14) 0.0401(17) -0.0024(12) 0.0313(15) -0.0036(12) C19 0.0433(17) 0.0160(13) 0.0292(14) 0.0023(11) 0.0211(12) -0.0023(12) C20 0.0387(16) 0.0155(12) 0.0230(13) -0.0016(10) 0.0158(12) -0.0061(11) O21 0.0292(11) 0.0361(12) 0.0408(12) 0.0131(10) 0.0156(9) 0.0118(9) N21 0.0252(12) 0.0142(10) 0.0291(12) 0.0021(9) 0.0114(9) 0.0004(9) C21 0.0256(14) 0.0162(12) 0.0284(14) 0.0035(10) 0.0116(11) 0.0015(10) O22 0.0353(11) 0.0207(10) 0.0312(10) 0.0038(8) 0.0017(8) -0.0015(8) C22 0.0220(14) 0.0205(13) 0.0257(14) 0.0005(11) 0.0064(11) -0.0006(10) O23 0.0295(11) 0.0175(9) 0.0307(10) -0.0013(8) 0.0141(8) -0.0027(8) C23 0.0356(16) 0.0194(13) 0.0294(14) 0.0049(11) 0.0111(12) 0.0010(11) O24 0.0252(10) 0.0169(9) 0.0247(9) 0.0015(7) 0.0096(7) 0.0018(7) C24 0.0275(14) 0.0199(13) 0.0211(12) -0.0009(10) 0.0140(10) 0.0017(11) O25 0.0243(9) 0.0162(9) 0.0356(10) 0.0043(8) 0.0099(8) 0.0030(8) C25 0.0246(14) 0.0203(13) 0.0270(13) 0.0015(11) 0.0145(11) 0.0015(11) C26 0.0236(14) 0.0244(14) 0.0394(16) 0.0053(12) 0.0150(12) -0.0015(11) C27 0.0190(14) 0.0337(16) 0.0438(17) 0.0073(14) 0.0078(12) -0.0004(12) C28 0.0246(15) 0.0266(15) 0.0422(17) 0.0102(13) 0.0107(12) 0.0041(11) C29 0.0250(15) 0.0189(13) 0.0328(14) 0.0026(11) 0.0137(11) 0.0019(11) C30 0.0214(13) 0.0214(13) 0.0250(13) 0.0009(10) 0.0128(10) 0.0034(10) O1M_2 0.024(2) 0.033(2) 0.057(3) 0.013(2) 0.0181(19) 0.0068(18) C1M_2 0.040(4) 0.047(5) 0.098(8) 0.035(6) 0.027(5) 0.006(4) O2M_2 0.042(3) 0.045(3) 0.069(4) 0.010(3) 0.021(2) 0.007(2) C2M_2 0.046(4) 0.051(5) 0.061(5) 0.008(4) 0.019(4) -0.019(4) O3M_3 0.0462(17) 0.093(2) 0.131(3) -0.073(2) 0.0487(18) -0.0305(16) C3M_3 0.066(5) 0.089(6) 0.084(5) -0.027(5) 0.014(4) 0.006(4) O4M_4 0.0424(16) 0.084(2) 0.0668(18) 0.0162(17) 0.0220(13) 0.0103(15) C4M_4 0.037(7) 0.097(10) 0.129(13) -0.003(11) 0.026(8) -0.006(8) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Si1 O4 1.7800(19) . ? Si1 O14 1.786(2) . ? Si1 O5 1.789(2) . ? Si1 O25 1.792(2) . ? Si1 O24 1.793(2) . ? Si1 O15 1.796(2) . ? Si1 Na2 3.2153(13) . ? Na1 O13 2.247(3) 2_545 ? Na1 O1 2.368(2) 1_645 ? Na1 O1M_2 2.384(4) . ? Na1 O4M_4 2.408(4) . ? Na1 O23 2.490(2) 1_545 ? Na1 O2M_2 2.498(6) . ? Na1 O3M_3 2.529(4) . ? Na1 Na2 3.5751(16) . ? Na2 O3 2.286(2) 2_546 ? Na2 O25 2.330(2) . ? Na2 O23 2.359(2) 1_545 ? Na2 O3M_3 2.381(3) . ? Na2 O5 2.481(2) . ? Na2 O15 2.886(2) . ? O1 C2 1.201(3) . ? O1 Na1 2.368(2) 1_465 ? N1 C4 1.347(3) . ? N1 C1 1.434(3) . ? C1 C3 1.521(4) . ? C1 C2 1.525(4) . ? O2 C22 1.334(3) . ? O2 C3 1.456(3) . ? C2 O12 1.331(4) . ? O3 C4 1.242(3) . ? O3 Na2 2.286(2) 2_556 ? O4 C10 1.349(3) . ? C4 C5 1.482(4) . ? O5 C9 1.356(3) . ? C5 C10 1.394(4) . ? C5 C6 1.406(4) . ? C6 C7 1.377(4) . ? C7 C8 1.407(4) . ? C8 C9 1.369(4) . ? C9 C10 1.394(4) . ? O11A C12 1.330(14) . ? O11B C12 1.214(5) . ? N11 C14 1.349(4) . ? N11 C11 1.451(4) . ? C11 C13 1.520(5) . ? C11 C12 1.528(5) . ? O12 C13 1.462(3) . ? C12 O22 1.325(4) . ? O13 C14 1.236(4) . ? O13 Na1 2.247(3) 2 ? O14 C20 1.340(3) . ? C14 C15 1.489(5) . ? O15 C19 1.356(4) . ? C15 C20 1.389(4) . ? C15 C16 1.418(4) . ? C16 C17 1.370(5) . ? C17 C18 1.398(5) . ? C18 C19 1.379(4) . ? C19 C20 1.407(4) . ? O21 C22 1.200(4) . ? N21 C24 1.338(4) . ? N21 C21 1.447(3) . ? C21 C23 1.521(4) . ? C21 C22 1.532(4) . ? O22 C23 1.458(4) . ? O23 C24 1.251(3) . ? O23 Na2 2.359(2) 1_565 ? O23 Na1 2.490(2) 1_565 ? O24 C30 1.345(3) . ? C24 C25 1.488(4) . ? O25 C29 1.345(3) . ? C25 C30 1.396(4) . ? C25 C26 1.409(4) . ? C26 C27 1.380(4) . ? C27 C28 1.402(5) . ? C28 C29 1.380(4) . ? C29 C30 1.405(4) . ? O1M_2 C1M_2 1.382(11) . ? O2M_2 C2M_2 1.382(11) . ? O3M_3 C3M_3 1.292(9) . ? O4M_4 C4M_4 1.4230(15) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O4 Si1 O14 86.48(9) . . ? O4 Si1 O5 87.92(9) . . ? O14 Si1 O5 100.57(9) . . ? O4 Si1 O25 99.73(9) . . ? O14 Si1 O25 171.34(10) . . ? O5 Si1 O25 85.77(9) . . ? O4 Si1 O24 87.57(9) . . ? O14 Si1 O24 87.50(9) . . ? O5 Si1 O24 170.49(10) . . ? O25 Si1 O24 86.75(9) . . ? O4 Si1 O15 170.62(10) . . ? O14 Si1 O15 86.93(9) . . ? O5 Si1 O15 86.72(9) . . ? O25 Si1 O15 87.56(10) . . ? O24 Si1 O15 98.81(9) . . ? O4 Si1 Na2 118.44(7) . . ? O14 Si1 Na2 136.23(7) . . ? O5 Si1 Na2 50.07(7) . . ? O25 Si1 Na2 45.21(7) . . ? O24 Si1 Na2 125.98(7) . . ? O15 Si1 Na2 63.05(7) . . ? O13 Na1 O1 86.89(9) 2_545 1_645 ? O13 Na1 O1M_2 84.63(15) 2_545 . ? O1 Na1 O1M_2 83.06(12) 1_645 . ? O13 Na1 O4M_4 99.17(11) 2_545 . ? O1 Na1 O4M_4 154.74(10) 1_645 . ? O1M_2 Na1 O4M_4 73.22(13) . . ? O13 Na1 O23 105.36(10) 2_545 1_545 ? O1 Na1 O23 108.89(8) 1_645 1_545 ? O1M_2 Na1 O23 164.51(14) . 1_545 ? O4M_4 Na1 O23 93.22(9) . 1_545 ? O13 Na1 O2M_2 113.10(16) 2_545 . ? O1 Na1 O2M_2 80.10(14) 1_645 . ? O4M_4 Na1 O2M_2 74.95(15) . . ? O23 Na1 O2M_2 141.00(15) 1_545 . ? O13 Na1 O3M_3 169.13(14) 2_545 . ? O1 Na1 O3M_3 101.33(12) 1_645 . ? O1M_2 Na1 O3M_3 89.28(16) . . ? O4M_4 Na1 O3M_3 70.39(15) . . ? O23 Na1 O3M_3 78.89(9) 1_545 . ? O13 Na1 Na2 137.79(8) 2_545 . ? O1 Na1 Na2 123.33(7) 1_645 . ? O1M_2 Na1 Na2 124.12(13) . . ? O4M_4 Na1 Na2 66.72(8) . . ? O23 Na1 Na2 41.10(5) 1_545 . ? O2M_2 Na1 Na2 101.61(14) . . ? O3M_3 Na1 Na2 41.67(7) . . ? O3 Na2 O25 105.85(8) 2_546 . ? O3 Na2 O23 114.73(8) 2_546 1_545 ? O25 Na2 O23 138.73(9) . 1_545 ? O3 Na2 O3M_3 99.84(13) 2_546 . ? O25 Na2 O3M_3 96.04(12) . . ? O23 Na2 O3M_3 84.54(10) 1_545 . ? O3 Na2 O5 99.63(7) 2_546 . ? O25 Na2 O5 60.77(6) . . ? O23 Na2 O5 103.75(8) 1_545 . ? O3M_3 Na2 O5 153.14(14) . . ? O3 Na2 O15 151.98(8) 2_546 . ? O25 Na2 O15 55.62(7) . . ? O23 Na2 O15 83.88(7) 1_545 . ? O3M_3 Na2 O15 102.77(14) . . ? O5 Na2 O15 53.96(6) . . ? O3 Na2 Si1 119.12(6) 2_546 . ? O25 Na2 Si1 33.09(5) . . ? O23 Na2 Si1 113.45(6) 1_545 . ? O3M_3 Na2 Si1 119.67(13) . . ? O5 Na2 Si1 33.57(5) . . ? O15 Na2 Si1 33.69(4) . . ? O3 Na2 Na1 128.39(7) 2_546 . ? O25 Na2 Na1 113.00(6) . . ? O23 Na2 Na1 43.93(5) 1_545 . ? O3M_3 Na2 Na1 44.91(8) . . ? O5 Na2 Na1 128.41(6) . . ? O15 Na2 Na1 79.61(5) . . ? Si1 Na2 Na1 111.96(4) . . ? C2 O1 Na1 178.1(2) . 1_465 ? C4 N1 C1 122.6(2) . . ? N1 C1 C3 111.9(2) . . ? N1 C1 C2 114.0(2) . . ? C3 C1 C2 110.9(2) . . ? C22 O2 C3 117.0(2) . . ? O1 C2 O12 124.9(3) . . ? O1 C2 C1 122.2(3) . . ? O12 C2 C1 112.9(2) . . ? C4 O3 Na2 147.50(17) . 2_556 ? O2 C3 C1 110.3(2) . . ? C10 O4 Si1 112.74(16) . . ? O3 C4 N1 122.1(2) . . ? O3 C4 C5 122.8(2) . . ? N1 C4 C5 114.9(2) . . ? C9 O5 Si1 111.70(16) . . ? C9 O5 Na2 118.72(15) . . ? Si1 O5 Na2 96.37(8) . . ? C10 C5 C6 117.8(2) . . ? C10 C5 C4 122.9(2) . . ? C6 C5 C4 119.0(2) . . ? C7 C6 C5 120.9(3) . . ? C6 C7 C8 120.4(3) . . ? C9 C8 C7 119.0(3) . . ? O5 C9 C8 125.6(3) . . ? O5 C9 C10 113.7(2) . . ? C8 C9 C10 120.6(2) . . ? O4 C10 C5 126.1(2) . . ? O4 C10 C9 113.3(2) . . ? C5 C10 C9 120.7(2) . . ? C14 N11 C11 121.5(2) . . ? N11 C11 C13 112.6(3) . . ? N11 C11 C12 112.9(3) . . ? C13 C11 C12 110.3(3) . . ? C2 O12 C13 118.3(2) . . ? O11B C12 O22 123.3(3) . . ? O22 C12 O11A 116.4(6) . . ? O11B C12 C11 122.9(3) . . ? O22 C12 C11 113.5(3) . . ? O11A C12 C11 114.4(6) . . ? C14 O13 Na1 150.3(2) . 2 ? O12 C13 C11 109.1(2) . . ? C20 O14 Si1 113.71(18) . . ? O13 C14 N11 121.5(3) . . ? O13 C14 C15 121.0(3) . . ? N11 C14 C15 117.4(3) . . ? C19 O15 Si1 112.95(18) . . ? C19 O15 Na2 140.20(17) . . ? Si1 O15 Na2 83.26(8) . . ? C20 C15 C16 117.6(3) . . ? C20 C15 C14 123.1(3) . . ? C16 C15 C14 118.9(3) . . ? C17 C16 C15 121.3(3) . . ? C16 C17 C18 120.5(3) . . ? C19 C18 C17 118.9(3) . . ? O15 C19 C18 126.7(3) . . ? O15 C19 C20 112.6(2) . . ? C18 C19 C20 120.7(3) . . ? O14 C20 C15 126.3(3) . . ? O14 C20 C19 113.3(3) . . ? C15 C20 C19 120.3(3) . . ? C24 N21 C21 123.7(2) . . ? N21 C21 C23 112.8(2) . . ? N21 C21 C22 113.2(2) . . ? C23 C21 C22 106.9(2) . . ? C12 O22 C23 118.1(2) . . ? O21 C22 O2 124.9(3) . . ? O21 C22 C21 121.4(2) . . ? O2 C22 C21 113.7(2) . . ? C24 O23 Na2 131.76(17) . 1_565 ? C24 O23 Na1 128.78(17) . 1_565 ? Na2 O23 Na1 94.97(8) 1_565 1_565 ? O22 C23 C21 106.3(2) . . ? C30 O24 Si1 113.07(17) . . ? O23 C24 N21 122.4(2) . . ? O23 C24 C25 121.5(3) . . ? N21 C24 C25 116.1(2) . . ? C29 O25 Si1 113.54(17) . . ? C29 O25 Na2 137.04(16) . . ? Si1 O25 Na2 101.70(10) . . ? C30 C25 C26 117.9(3) . . ? C30 C25 C24 122.8(2) . . ? C26 C25 C24 118.8(2) . . ? C27 C26 C25 120.9(3) . . ? C26 C27 C28 121.0(3) . . ? C29 C28 C27 118.4(3) . . ? O25 C29 C28 126.2(3) . . ? O25 C29 C30 112.8(2) . . ? C28 C29 C30 121.0(3) . . ? O24 C30 C25 126.3(2) . . ? O24 C30 C29 113.3(2) . . ? C25 C30 C29 120.4(3) . . ? C1M_2 O1M_2 Na1 144.1(5) . . ? C2M_2 O2M_2 Na1 133.4(6) . . ? C3M_3 O3M_3 Na2 154.5(5) . . ? C3M_3 O3M_3 Na1 111.5(4) . . ? Na2 O3M_3 Na1 93.41(12) . . ? C4M_4 O4M_4 Na1 153.1(6) . . ? _refine_diff_density_max 0.338 _refine_diff_density_min -0.246 _refine_diff_density_rms 0.050 _iucr_refine_instructions_details ; REM TITL solve in P2(1) CELL 1.54178 11.2372 9.8524 15.8396 90.0000 106.7134 90.0000 ZERR 4.00 0.0018 0.0015 0.0025 0.0000 0.0084 0.0000 LATT -1 SYMM -X, 0.5+Y, -Z SFAC C H N O Na Si UNIT 64 56 6 36 4 2 TEMP -173.000 L.S. 10 PLAN 10 FMAP ACTA LIST 6 WGHT 0.050400 0.444700 FVAR 0.61183 0.27564 SI1 6 0.042704 0.420019 0.269949 11.00000 0.02453 0.01435 = 0.02384 0.00102 0.01017 0.00232 NA1 5 0.400187 0.062169 0.209176 11.00000 0.02774 0.02747 = 0.02912 -0.00100 0.01005 0.00254 NA2 5 0.230050 0.177045 0.354665 11.00000 0.02944 0.01797 = 0.02429 0.00047 0.00904 0.00322 O1 4 -0.446841 0.889724 0.246716 11.00000 0.02842 0.02653 = 0.03629 0.00637 0.00988 0.00815 N1 3 -0.216350 0.657503 0.371378 11.00000 0.02569 0.01917 = 0.02219 0.00077 0.01132 0.00310 AFIX 43 H1N 2 -0.181622 0.626325 0.332056 11.00000 -1.20000 AFIX 0 C1 1 -0.278470 0.786200 0.355803 11.00000 0.02318 0.02141 = 0.02546 0.00054 0.01129 0.00337 AFIX 13 H1 2 -0.327015 0.793936 0.399514 11.00000 -1.20000 AFIX 0 O2 4 -0.105730 0.895170 0.317336 11.00000 0.02353 0.02081 = 0.02629 0.00263 0.01075 0.00242 C2 1 -0.371878 0.799480 0.264782 11.00000 0.02127 0.02039 = 0.02916 0.00431 0.00998 -0.00041 O3 4 -0.257467 0.619120 0.501267 11.00000 0.02308 0.02847 = 0.02106 -0.00053 0.00851 0.00219 C3 1 -0.187107 0.903914 0.373992 11.00000 0.02538 0.02284 = 0.02525 -0.00017 0.01091 0.00267 AFIX 23 H3A 2 -0.233257 0.990806 0.363192 11.00000 -1.20000 H3B 2 -0.136673 0.901885 0.436536 11.00000 -1.20000 AFIX 0 O4 4 -0.037756 0.502875 0.337100 11.00000 0.02371 0.01571 = 0.02128 0.00246 0.00992 0.00196 C4 1 -0.209020 0.582419 0.443780 11.00000 0.01597 0.02361 = 0.01874 -0.00195 0.00406 -0.00216 O5 4 0.013520 0.262765 0.316845 11.00000 0.02589 0.01671 = 0.02410 -0.00013 0.00980 0.00024 C5 1 -0.146322 0.449496 0.446439 11.00000 0.01998 0.02123 = 0.01827 -0.00025 0.00168 -0.00157 C6 1 -0.166353 0.347910 0.503176 11.00000 0.02508 0.03007 = 0.02030 0.00313 0.00753 -0.00093 AFIX 43 H6 2 -0.212395 0.368562 0.543315 11.00000 -1.20000 AFIX 0 C7 1 -0.120124 0.218911 0.501328 11.00000 0.02811 0.02602 = 0.02671 0.00780 0.00738 -0.00182 AFIX 43 H7 2 -0.131016 0.152621 0.542027 11.00000 -1.20000 AFIX 0 C8 1 -0.056826 0.184700 0.439486 11.00000 0.02124 0.01963 = 0.02731 0.00364 0.00313 -0.00032 AFIX 43 H8 2 -0.026549 0.095157 0.437188 11.00000 -1.20000 AFIX 0 C9 1 -0.039520 0.282373 0.382679 11.00000 0.01903 0.02040 = 0.02132 0.00006 0.00384 -0.00156 C10 1 -0.075652 0.416162 0.390073 11.00000 0.02002 0.01864 = 0.01791 0.00305 0.00286 -0.00219 PART 1 O11A 4 -0.374370 0.925591 0.040489 21.00000 0.04515 0.04766 = 0.07412 0.00390 0.01172 -0.00042 PART 2 O11B 4 -0.351729 0.899067 -0.010842 -21.00000 0.04047 0.02375 = 0.02803 0.00689 0.00067 0.00433 PART 0 N11 3 -0.295202 0.564474 0.070981 11.00000 0.03641 0.02463 = 0.02206 0.00056 0.00119 -0.00009 AFIX 43 H11N 2 -0.250044 0.548168 0.125385 11.00000 -1.20000 AFIX 0 C11 1 -0.376035 0.682345 0.053211 11.00000 0.03469 0.02762 = 0.02744 0.00074 -0.00275 0.00004 AFIX 13 H11 2 -0.439181 0.666240 -0.004888 11.00000 -1.20000 AFIX 0 O12 4 -0.358865 0.703383 0.209066 11.00000 0.03028 0.02875 = 0.02782 -0.00396 -0.00067 0.00725 C12 1 -0.307574 0.813095 0.044144 11.00000 0.03925 0.02760 = 0.03891 0.00344 -0.00042 -0.00116 O13 4 -0.359185 0.489042 -0.069344 11.00000 0.05192 0.04184 = 0.02369 -0.00076 0.00235 -0.00598 C13 1 -0.447016 0.700532 0.120894 11.00000 0.02892 0.03058 = 0.03486 -0.00082 -0.00487 0.00219 AFIX 23 H13A 2 -0.494744 0.786393 0.109562 11.00000 -1.20000 H13B 2 -0.506296 0.624686 0.116445 11.00000 -1.20000 AFIX 0 O14 4 -0.097172 0.437601 0.181790 11.00000 0.03124 0.01881 = 0.01979 -0.00208 0.01006 0.00058 C14 1 -0.287699 0.479326 0.006016 11.00000 0.03916 0.02537 = 0.02120 -0.00016 0.00716 -0.01258 O15 4 0.101147 0.320197 0.195710 11.00000 0.03590 0.01989 = 0.03200 -0.00125 0.01788 0.00286 C15 1 -0.185870 0.377059 0.027362 11.00000 0.04287 0.02049 = 0.02445 -0.00029 0.01318 -0.00854 C16 1 -0.171720 0.290120 -0.040417 11.00000 0.05684 0.02708 = 0.02621 -0.00521 0.01978 -0.01283 AFIX 43 H16 2 -0.234598 0.288083 -0.095320 11.00000 -1.20000 AFIX 0 C17 1 -0.069133 0.208961 -0.028303 11.00000 0.06685 0.02546 = 0.03213 -0.00564 0.03062 -0.00957 AFIX 43 H17 2 -0.063628 0.148322 -0.073661 11.00000 -1.20000 AFIX 0 C18 1 0.027500 0.214717 0.050307 11.00000 0.05235 0.01820 = 0.04008 -0.00243 0.03127 -0.00358 AFIX 43 H18 2 0.100568 0.162049 0.057525 11.00000 -1.20000 AFIX 0 C19 1 0.015044 0.298047 0.117172 11.00000 0.04329 0.01596 = 0.02917 0.00227 0.02110 -0.00232 C20 1 -0.094945 0.372247 0.108069 11.00000 0.03870 0.01546 = 0.02300 -0.00165 0.01582 -0.00610 O21 4 -0.216884 1.054704 0.227016 11.00000 0.02917 0.03614 = 0.04076 0.01311 0.01564 0.01182 N21 3 0.048957 0.854157 0.221885 11.00000 0.02519 0.01417 = 0.02913 0.00210 0.01138 0.00035 AFIX 43 H21N 2 0.022215 0.769775 0.217694 11.00000 -1.20000 AFIX 0 C21 1 -0.041348 0.961162 0.191222 11.00000 0.02565 0.01617 = 0.02839 0.00353 0.01159 0.00146 AFIX 13 H21 2 0.004887 1.048582 0.194166 11.00000 -1.20000 AFIX 0 O22 4 -0.191638 0.817060 0.095831 11.00000 0.03533 0.02068 = 0.03118 0.00381 0.00167 -0.00154 C22 1 -0.131287 0.976744 0.247224 11.00000 0.02197 0.02052 = 0.02572 0.00054 0.00639 -0.00056 O23 4 0.218027 0.991569 0.258359 11.00000 0.02950 0.01745 = 0.03072 -0.00131 0.01408 -0.00274 C23 1 -0.120109 0.940718 0.096430 11.00000 0.03556 0.01940 = 0.02944 0.00490 0.01112 0.00104 AFIX 23 H23A 2 -0.176305 1.019063 0.076377 11.00000 -1.20000 H23B 2 -0.066531 0.931049 0.056913 11.00000 -1.20000 AFIX 0 O24 4 0.086116 0.584979 0.241276 11.00000 0.02520 0.01691 = 0.02471 0.00153 0.00959 0.00178 C24 1 0.170787 0.876240 0.256242 11.00000 0.02746 0.01987 = 0.02114 -0.00086 0.01404 0.00170 O25 4 0.194879 0.410436 0.346599 11.00000 0.02430 0.01616 = 0.03556 0.00430 0.00989 0.00301 C25 1 0.246671 0.756650 0.296843 11.00000 0.02463 0.02030 = 0.02699 0.00154 0.01452 0.00147 C26 1 0.368359 0.778100 0.351660 11.00000 0.02358 0.02438 = 0.03939 0.00530 0.01500 -0.00145 AFIX 43 H26 2 0.404659 0.865697 0.354591 11.00000 -1.20000 AFIX 0 C27 1 0.435531 0.673522 0.401161 11.00000 0.01899 0.03373 = 0.04378 0.00733 0.00784 -0.00036 AFIX 43 H27 2 0.519050 0.688843 0.435112 11.00000 -1.20000 AFIX 0 C28 1 0.382299 0.545057 0.402060 11.00000 0.02461 0.02660 = 0.04216 0.01016 0.01068 0.00412 AFIX 43 H28 2 0.427567 0.474351 0.438070 11.00000 -1.20000 AFIX 0 C29 1 0.262620 0.523732 0.349417 11.00000 0.02496 0.01886 = 0.03275 0.00258 0.01368 0.00188 C30 1 0.197557 0.625913 0.292811 11.00000 0.02139 0.02139 = 0.02503 0.00088 0.01279 0.00343 RESI 2 MEOH ISOR 0.01 O2M_2 C2M_2 SIMU 0.01 O2M_2 C2M_2 SIMU 0.01 O1M_2 C1M_2 DELU 0.01 O1M_2 C1M_2 ISOR 0.01 O1M_2 O3M_3 PART 1 O1M 4 0.563106 0.187629 0.176747 10.50000 0.02367 0.03300 = 0.05685 0.01272 0.01814 0.00680 C1M 1 0.615865 0.314974 0.179940 10.50000 0.03986 0.04737 = 0.09793 0.03544 0.02670 0.00633 AFIX 137 H21M 2 0.624990 0.337789 0.121900 10.50000 -1.50000 H22M 2 0.697729 0.315197 0.223733 10.50000 -1.50000 H23M 2 0.562280 0.382214 0.196449 10.50000 -1.50000 AFIX 0 PART 2 O2M 4 0.591634 0.204858 0.256745 10.50000 0.04175 0.04519 = 0.06921 0.00963 0.02132 0.00656 C2M 1 0.621558 0.332816 0.233380 10.50000 0.04602 0.05050 = 0.06080 0.00803 0.01881 -0.01928 AFIX 137 H24M 2 0.581540 0.347721 0.170419 10.50000 -1.50000 H25M 2 0.711878 0.340162 0.245414 10.50000 -1.50000 H26M 2 0.592471 0.401278 0.267744 10.50000 -1.50000 AFIX 0 PART 0 RESI 3 MEOH PART -1 ISOR 0.005 O3M_3 SIMU 0.005 O3M_3 C3M_3 O3M 4 0.441250 0.188809 0.353572 11.00000 0.04615 0.09315 = 0.13125 -0.07316 0.04868 -0.03046 C3M 1 0.558470 0.211562 0.388075 10.66660 0.06647 0.08935 = 0.08384 -0.02683 0.01377 0.00594 AFIX 137 H31M 2 0.569503 0.290680 0.427067 10.66660 -1.50000 H32M 2 0.597417 0.229216 0.341184 10.66660 -1.50000 H33M 2 0.597385 0.132046 0.422139 10.66660 -1.50000 AFIX 0 PART 0 RESI 4 MEOH ISOR 0.01 O4M_4 SIMU 0.01 O4M_4 C4M_4 DELU 0.01 O4M_4 C4M_4 DFIX 1.423 0.001 C4M_4 O4M_4 O4M 4 0.327954 0.292572 0.181402 11.00000 0.04239 0.08400 = 0.06685 0.01617 0.02205 0.01029 AFIX 143 H4M 2 0.257222 0.280099 0.188004 11.00000 0.14646 AFIX 0 C4M 1 0.345266 0.433336 0.168604 10.33330 0.03662 0.09707 = 0.12906 -0.00325 0.02623 -0.00588 AFIX 137 H41M 2 0.362092 0.480824 0.225185 10.33330 -1.50000 H42M 2 0.269951 0.470644 0.127341 10.33330 -1.50000 H43M 2 0.415676 0.445480 0.144471 10.33330 -1.50000 AFIX 0 HKLF 4 REM solve in P2(1) REM R1 = 0.0293 for 5914 Fo > 4sig(Fo) and 0.0310 for all 6168 data REM 547 parameters refined using 58 restraints END WGHT 0.0504 0.4447 REM Highest difference peak 0.338, deepest hole -0.246, 1-sigma level 0.050 Q1 1 0.4706 0.1558 0.3853 11.00000 0.05 0.34 Q2 1 0.4398 0.2204 0.3165 11.00000 0.05 0.33 Q3 1 -0.0379 0.4227 0.2207 11.00000 0.05 0.27 Q4 1 0.1315 0.4179 0.3066 11.00000 0.05 0.26 Q5 1 0.0865 0.5136 0.2477 11.00000 0.05 0.22 Q6 1 0.0122 0.3403 0.2990 11.00000 0.05 0.21 Q7 1 0.2217 0.8052 0.2714 11.00000 0.05 0.21 Q8 1 0.0228 0.4753 0.3185 11.00000 0.05 0.20 Q9 1 0.6285 0.1419 0.1878 11.00000 0.05 0.20 Q10 1 -0.3308 0.7880 0.3088 11.00000 0.05 0.20 ; _shelx_res_checksum 81998 _shelx_hkl_file ; 1 0 0 4364.69 177.40 1 1 0 0 5017.26 202.29 3 1 0 0 4528.87 189.75 8 1 0 0 4738.61 181.76 10 1 0 0 4554.03 162.09 12 1 0 0 4455.82 159.28 14 1 0 0 4618.72 188.85 20 1 0 0 4884.51 201.04 21 -1 0 0 4666.02 162.95 12 -1 0 0 4634.82 160.19 14 -1 0 0 4793.88 189.37 20 -1 0 0 4964.82 201.26 21 -1 0 0 4636.41 181.15 10 -1 0 0 4189.59 176.94 1 -1 0 0 4435.24 199.23 3 -1 0 0 4398.70 189.73 8 -2 0 0 96.6671 5.7219 12 -2 0 0 99.1798 4.8860 14 -2 0 0 101.120 5.841 20 2 0 0 97.4808 5.8598 21 -2 0 0 96.6062 5.8880 21 2 0 0 96.2819 6.3986 20 -2 0 0 93.4912 6.3447 10 -2 0 0 93.9652 6.5367 8 -2 0 0 94.9535 5.6777 1 -3 0 0 90.6679 6.6774 21 -3 0 0 96.8491 5.7250 14 -3 0 0 111.098 6.795 1 3 0 0 100.157 6.096 3 -3 0 0 104.795 6.408 12 3 0 0 93.3211 6.5873 21 -3 0 0 103.602 8.035 8 -3 0 0 105.823 7.662 10 4 0 0 191.205 10.251 8 4 0 0 188.921 9.755 20 -4 0 0 191.780 8.625 14 -4 0 0 175.156 9.667 12 -4 0 0 182.759 9.762 21 -4 0 0 196.688 9.797 1 -4 0 0 195.239 10.753 10 -4 0 0 188.742 9.476 21 4 0 0 180.413 10.001 3 -5 0 0 1811.82 62.85 14 5 0 0 2026.49 102.73 3 5 0 0 1790.44 89.51 8 5 0 0 1878.66 79.73 20 -5 0 0 1960.40 69.79 1 -5 0 0 1873.52 63.78 12 -5 0 0 1867.86 70.93 10 -6 0 0 515.087 16.764 13 -6 0 0 524.826 17.700 11 6 0 0 504.728 23.439 8 6 0 0 518.073 24.273 3 -6 0 0 537.735 19.557 14 -6 0 0 519.831 22.264 1 6 0 0 540.236 22.623 10 -6 0 0 527.325 21.280 12 -7 0 0 521.816 21.920 1 -7 0 0 486.026 20.970 12 -7 0 0 483.065 17.755 9 7 0 0 428.950 22.441 8 7 0 0 492.841 23.698 3 -7 0 0 496.833 16.552 11 -7 0 0 471.298 17.952 4 -7 0 0 486.873 15.734 13 7 0 0 500.538 21.992 10 -7 0 0 467.322 16.981 2 -8 0 0 58.5822 7.4504 1 -8 0 0 62.8032 4.1342 4 -8 0 0 56.8536 3.8570 2 -8 0 0 57.3805 3.2931 7 -8 0 0 56.8623 4.4442 9 8 0 0 76.5833 8.0767 8 -8 0 0 70.5073 4.0182 6 -8 0 0 66.6168 4.1289 19 8 0 0 70.5089 6.6122 12 8 0 0 74.4766 7.6955 10 -8 0 0 59.3471 4.5072 13 -8 0 0 63.0635 4.8144 11 -9 0 0 8.09257 1.99964 19 -9 0 0 10.6486 2.3607 6 -9 0 0 10.6397 3.1052 13 -9 0 0 11.4959 1.9777 7 -9 0 0 7.49546 3.30743 11 -9 0 0 13.8939 2.5835 4 -9 0 0 8.91526 2.18355 2 -9 0 0 7.65082 2.77197 9 -10 0 0 5.43930 2.00435 7 -10 0 0 7.98995 2.03601 19 -10 0 0 8.17595 2.44244 6 -10 0 0 2.00252 2.17622 2 -10 0 0 3.94349 2.80302 9 -10 0 0 4.02498 3.43841 11 -10 0 0 7.27987 3.11414 13 -11 0 0 2.54763 2.92039 13 -11 0 0 6.81749 2.08018 2 -11 0 0 7.82354 2.43141 6 -11 0 0 6.70259 1.90525 7 -11 0 0 8.03681 2.64116 9 -11 0 0 3.81572 1.83231 19 -11 0 0 9.50814 3.46769 11 -12 0 0 205.084 7.585 13 -12 0 0 209.598 8.140 11 0 -1 0 -0.9190 1.6335 20 0 -1 0 0.35345 0.93594 8 0 -1 0 -0.4019 1.0525 10 0 -1 0 -0.3492 0.8814 3 0 -1 0 -0.0402 1.2224 12 0 -1 0 -0.0505 1.1401 1 0 -1 0 -1.1730 1.9573 21 0 -1 0 0.15501 1.09291 14 0 1 0 0.17507 2.10853 21 0 1 0 -1.0488 1.1891 14 0 1 0 0.69725 1.79227 20 0 1 0 0.70504 0.86716 8 0 1 0 -0.3213 1.1894 12 0 1 0 -0.1099 1.0476 1 0 1 0 1.05405 0.94453 3 -1 -1 0 1352.33 74.62 21 1 -1 0 1299.35 53.05 12 1 -1 0 1345.86 59.94 1 1 -1 0 1302.83 57.34 10 1 -1 0 1388.48 59.00 3 -1 -1 0 1294.62 54.65 12 -1 -1 0 1253.90 63.20 8 1 -1 0 1369.90 56.44 8 1 -1 0 1334.32 64.54 21 -1 -1 0 1416.84 60.73 1 -1 -1 0 1395.65 60.86 10 1 -1 0 1378.23 56.97 8 1 1 0 1294.90 71.78 21 1 1 0 1238.54 64.29 3 -1 1 0 1383.82 66.88 20 -1 1 0 1369.14 59.63 3 1 1 0 1296.94 62.28 20 -1 1 0 1315.76 64.16 21 -1 1 0 1275.04 50.35 12 1 1 0 1326.98 54.34 8 -1 1 0 1310.24 53.99 14 -2 -1 0 2247.05 107.94 21 -2 -1 0 2084.96 95.34 1 2 -1 0 2045.21 84.57 12 -2 -1 0 2187.82 99.72 8 2 -1 0 2151.63 99.75 21 2 -1 0 2105.31 94.62 10 -2 -1 0 2099.99 97.24 10 -2 -1 0 2043.76 74.78 14 2 -1 0 2122.62 97.13 8 -2 -1 0 2286.17 91.50 12 2 -1 0 2094.71 97.58 3 -2 1 0 2194.05 97.70 1 2 1 0 2160.31 118.16 21 -2 1 0 2202.39 90.11 14 -2 1 0 2191.85 102.41 21 2 1 0 2198.74 100.23 20 2 1 0 2211.23 75.29 14 2 1 0 2171.49 108.59 3 -2 1 0 2177.79 102.40 3 -2 1 0 2098.09 105.64 20 -3 -1 0 1077.43 41.76 10 -3 -1 0 1178.82 47.78 21 -3 -1 0 1174.32 48.37 12 3 -1 0 1098.88 60.17 8 3 -1 0 1123.35 51.65 3 3 -1 0 1102.20 55.58 10 -3 -1 0 1098.84 39.95 14 -3 -1 0 985.982 40.712 1 -3 1 0 1104.96 46.59 14 3 1 0 1101.51 56.54 3 -3 1 0 1116.65 37.52 12 -3 1 0 1127.13 44.39 20 3 1 0 1130.85 51.15 20 3 1 0 1070.93 37.58 14 -3 1 0 1006.68 49.30 1 3 1 0 1158.08 47.69 21 -4 -1 0 44.9059 4.9641 1 -4 -1 0 36.2660 5.0897 10 -4 -1 0 38.4079 5.1229 21 4 -1 0 35.2733 4.4942 8 4 -1 0 42.9103 4.3315 3 4 -1 0 41.6434 4.2373 10 -4 -1 0 48.3127 5.3530 12 -4 -1 0 43.8012 3.6814 14 -4 1 0 32.4920 4.4464 14 4 1 0 32.6653 4.5349 20 4 1 0 36.8956 5.1630 21 -4 1 0 38.0423 4.7189 20 -4 1 0 43.3801 5.2586 1 4 1 0 47.1063 5.4662 3 -4 1 0 39.9167 5.1956 12 -5 -1 0 11.3458 4.0879 1 5 -1 0 9.60798 3.19681 8 -5 -1 0 13.0628 2.4218 14 -5 -1 0 14.8957 3.8349 21 5 -1 0 8.67582 2.79810 3 -5 -1 0 16.1798 4.8954 12 -5 -1 0 10.3098 4.6736 10 5 -1 0 7.18516 3.43390 10 -5 1 0 11.7928 4.1777 14 5 1 0 11.6116 4.2315 21 -5 1 0 11.9288 4.1408 1 5 1 0 7.43035 2.86935 20 5 1 0 6.12375 3.86669 3 5 1 0 7.81111 3.71184 8 -5 1 0 12.2121 3.7882 20 -6 -1 0 32.7228 2.8030 2 -6 -1 0 37.1189 3.4695 13 6 -1 0 30.5282 4.3431 3 -6 -1 0 32.1991 3.0039 4 -6 -1 0 32.0787 5.9912 10 -6 -1 0 36.4145 3.4917 11 6 -1 0 38.7783 4.9558 8 6 -1 0 36.3997 4.8637 12 -6 -1 0 32.0308 3.3176 9 -6 -1 0 33.9843 5.7631 12 -6 -1 0 36.6929 5.3551 1 6 -1 0 38.2697 5.0591 10 6 1 0 26.2926 5.0745 3 -6 1 0 25.9865 4.7852 1 -6 1 0 28.4956 2.5447 13 -6 1 0 31.5255 4.6767 14 6 1 0 30.7561 5.2217 8 -7 -1 0 107.325 5.401 11 -7 -1 0 110.338 4.902 2 -7 -1 0 124.644 8.809 1 -7 -1 0 109.031 5.542 9 -7 -1 0 108.688 5.244 13 -7 -1 0 105.775 9.311 12 7 -1 0 121.689 8.952 8 -7 -1 0 114.426 5.485 4 7 -1 0 125.290 9.034 10 7 -1 0 113.754 8.016 12 7 -1 0 113.005 8.475 3 -7 1 0 107.328 5.111 13 -7 1 0 111.676 5.343 9 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0 862.573 33.660 1 -6 -2 0 835.282 31.366 12 -6 -2 0 818.620 29.790 9 6 -2 0 857.967 33.494 10 -6 -2 0 797.777 26.194 13 6 -2 0 838.759 30.480 12 -6 -2 0 824.598 28.704 2 6 -2 0 870.688 33.144 1 -6 -2 0 858.676 35.098 10 -6 -2 0 822.264 30.392 4 6 2 0 816.634 35.589 8 -6 2 0 818.823 28.677 2 -6 2 0 840.189 30.933 14 6 2 0 840.973 37.441 3 -6 2 0 814.461 26.202 13 -7 -2 0 34.7933 6.8895 10 7 -2 0 49.4088 5.9925 12 -7 -2 0 35.7816 3.5348 4 -7 -2 0 33.3751 3.8084 11 7 -2 0 63.5968 6.5991 10 -7 -2 0 34.7414 6.4107 12 7 -2 0 35.7407 5.3335 1 -7 -2 0 43.2934 6.1055 1 -7 -2 0 35.0463 3.9585 9 -7 -2 0 37.9271 3.5357 13 -7 -2 0 38.4467 3.3111 2 -7 2 0 51.2227 4.1129 11 -7 2 0 42.0196 3.8547 13 7 2 0 36.6935 6.3105 3 7 2 0 39.6280 6.1845 8 -7 2 0 36.3637 3.2508 2 -7 2 0 33.3866 5.7871 14 -8 -2 0 92.6434 4.0561 7 -8 -2 0 104.109 5.046 16 -8 -2 0 96.7107 4.7840 2 -8 -2 0 97.5936 4.8974 19 -8 -2 0 94.1939 5.2996 4 -8 -2 0 88.2934 5.5348 9 -8 -2 0 96.2527 5.2181 6 -8 -2 0 87.4016 5.3436 11 -8 -2 0 93.2152 5.1177 13 -8 2 0 92.6926 4.2284 7 -8 2 0 97.4767 5.6331 11 -8 2 0 96.8439 5.0825 19 -8 2 0 89.2945 4.7817 2 -8 2 0 89.2526 4.7640 18 -9 -2 0 143.653 6.932 11 -9 -2 0 141.278 6.248 19 -9 -2 0 141.472 6.566 13 -9 -2 0 132.048 6.726 6 -9 -2 0 134.141 6.971 4 -9 -2 0 140.776 5.270 7 -9 -2 0 136.675 7.086 9 -9 -2 0 139.982 6.222 2 -9 2 0 135.952 5.481 7 -9 2 0 143.544 7.171 11 -9 2 0 134.452 6.276 2 -9 2 0 146.722 6.057 18 -9 2 0 142.552 6.300 13 -9 2 0 149.289 6.469 19 -10 -2 0 24.9290 3.3140 4 -10 -2 0 30.1391 2.7610 7 -10 -2 0 26.3366 3.0754 6 -10 -2 0 27.8076 3.1919 2 -10 -2 0 25.9526 3.4433 13 -10 -2 0 28.0646 3.5305 9 -10 -2 0 25.9135 3.7456 11 -10 -2 0 31.7998 3.4554 19 -10 2 0 25.5653 2.7259 2 -10 2 0 23.1175 3.3362 13 -10 2 0 22.9238 3.7279 11 -10 2 0 29.5809 3.2367 18 -10 2 0 29.2945 3.3169 19 -10 2 0 27.0143 2.4208 7 -11 -2 0 96.2097 4.6370 2 -11 -2 0 104.671 5.499 13 -11 -2 0 95.0369 5.4562 6 -11 -2 0 94.5357 5.8206 11 -11 -2 0 91.3887 5.5898 9 -11 -2 0 93.7117 5.4417 4 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68.9030 9.3260 21 -2 -3 0 75.7647 6.7902 10 2 -3 0 74.9935 5.6125 1 -2 -3 0 79.5965 6.6582 12 -2 -3 0 84.8818 6.5925 1 2 3 0 78.1960 6.4820 3 2 3 0 84.4049 8.2931 20 -2 3 0 77.2798 8.3738 21 2 3 0 68.0124 9.8131 21 -2 3 0 73.8498 6.9322 14 -2 3 0 79.3217 9.7332 20 -3 -3 0 333.656 15.231 1 3 -3 0 325.100 14.707 8 3 -3 0 361.385 18.099 21 3 -3 0 385.204 14.682 12 -3 -3 0 373.246 20.485 21 -3 -3 0 353.234 17.299 8 3 -3 0 375.927 15.375 10 3 -3 0 359.653 15.423 1 -3 -3 0 382.782 15.065 12 -3 -3 0 381.523 16.538 10 3 3 0 344.004 20.533 21 -3 3 0 359.353 18.504 20 3 3 0 334.385 17.002 20 -3 3 0 362.724 18.440 21 -3 3 0 366.230 14.947 14 3 3 0 346.822 17.268 3 4 -3 0 427.565 16.711 12 4 -3 0 447.773 17.856 1 -4 -3 0 433.269 17.759 1 -4 -3 0 416.064 18.994 10 4 -3 0 369.332 17.794 10 4 -3 0 405.668 17.132 8 -4 3 0 410.939 17.333 14 4 3 0 432.685 20.231 3 -4 3 0 422.215 20.577 20 4 3 0 403.581 18.820 8 4 3 0 391.304 19.159 20 5 -3 0 139.118 8.495 1 5 -3 0 131.533 8.651 12 5 -3 0 130.634 8.711 10 -5 -3 0 129.288 5.479 2 -5 -3 0 131.618 9.256 12 -5 -3 0 130.281 5.277 13 -5 -3 0 131.346 5.863 4 -5 -3 0 123.606 5.604 11 -5 -3 0 138.914 8.512 1 -5 -3 0 127.084 5.958 9 -5 -3 0 135.700 10.073 10 -5 3 0 131.988 10.501 20 5 3 0 128.543 9.307 8 -5 3 0 131.203 9.015 14 5 3 0 136.367 9.873 3 -6 -3 0 170.821 6.733 13 -6 -3 0 187.375 12.494 10 -6 -3 0 173.287 7.537 4 -6 -3 0 170.058 7.594 9 -6 -3 0 171.352 7.194 2 -6 -3 0 177.638 11.326 12 6 -3 0 177.232 10.002 12 6 -3 0 177.791 10.333 1 -6 -3 0 161.562 10.721 1 6 -3 0 207.906 10.763 10 -6 -3 0 169.238 7.174 11 -6 3 0 201.990 12.219 20 6 3 0 191.094 11.821 8 6 3 0 193.111 12.355 3 -6 3 0 199.403 11.050 14 -6 3 0 175.797 6.991 2 -7 -3 0 50.9509 3.9408 13 -7 -3 0 42.6818 4.1423 11 -7 -3 0 56.7822 7.5874 12 -7 -3 0 53.7577 3.9866 6 -7 -3 0 50.7674 4.0511 4 -7 -3 0 58.4691 7.3710 1 -7 -3 0 52.9770 3.6263 2 -7 -3 0 50.4572 4.3924 9 -7 -3 0 41.2763 7.6614 10 7 -3 0 54.6297 6.6365 12 7 -3 0 54.8093 6.5986 1 -7 3 0 49.5773 3.9563 19 7 3 0 55.8054 7.7989 3 -7 3 0 49.1371 3.5284 2 7 3 0 55.6562 7.3468 8 -7 3 0 52.8583 6.9642 14 -7 3 0 46.2075 4.2037 13 -8 -3 0 134.980 6.310 11 -8 -3 0 123.661 6.023 19 -8 -3 0 126.650 5.068 7 -8 -3 0 127.017 6.650 9 -8 -3 0 126.356 6.347 6 -8 -3 0 129.560 5.771 2 -8 -3 0 128.320 6.045 16 -8 -3 0 133.261 6.685 4 -8 -3 0 125.239 6.090 13 -8 3 0 129.614 5.032 15 -8 3 0 122.522 5.173 7 -8 3 0 136.993 6.149 19 -8 3 0 131.491 5.833 18 -8 3 0 130.804 6.054 13 -8 3 0 124.554 5.877 2 -9 -3 0 229.198 9.873 6 -9 -3 0 233.991 9.423 16 -9 -3 0 233.068 9.029 2 -9 -3 0 228.041 9.432 11 -9 -3 0 230.304 9.973 4 -9 -3 0 229.329 7.828 7 -9 -3 0 231.668 8.984 13 -9 -3 0 229.244 9.168 19 -9 -3 0 219.322 9.899 9 -9 3 0 225.008 8.760 13 -9 3 0 239.349 9.332 19 -9 3 0 239.217 9.065 2 -9 3 0 234.747 7.930 7 -9 3 0 239.941 8.756 18 -10 -3 0 61.0295 4.9497 13 -10 -3 0 51.3936 5.0463 9 -10 -3 0 57.1368 5.1589 11 -10 -3 0 57.9578 4.9150 4 -10 -3 0 55.7048 4.3170 16 -10 -3 0 64.5692 4.0780 2 -10 -3 0 60.7989 3.2721 7 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1 4 0 137.731 8.546 3 -1 4 0 142.212 7.056 3 -1 4 0 158.882 12.746 21 2 -4 0 923.674 34.785 10 -2 -4 0 993.098 35.642 1 2 -4 0 885.901 42.608 21 -2 -4 0 870.893 44.175 21 -2 -4 0 933.603 32.790 12 -2 -4 0 979.442 36.048 10 2 -4 0 915.785 32.194 12 2 -4 0 965.305 35.553 1 -2 -4 0 924.856 30.611 14 -2 4 0 806.378 42.578 21 2 4 0 907.251 39.479 20 -2 4 0 928.959 33.104 14 2 4 0 907.296 44.312 21 2 4 0 943.758 39.379 3 -2 4 0 958.401 40.631 20 2 4 0 941.443 36.820 8 3 -4 0 1913.63 65.68 12 -3 -4 0 1763.47 85.94 1 3 -4 0 1993.98 72.16 10 -3 -4 0 1865.20 66.24 12 -3 -4 0 2036.62 73.67 10 3 -4 0 2005.12 96.48 1 -3 4 0 2053.88 87.64 14 3 4 0 2028.67 79.33 20 3 4 0 1941.74 88.26 8 -3 4 0 1986.69 80.31 20 3 4 0 2017.30 81.14 3 -4 -4 0 64.1653 7.5849 10 -4 -4 0 71.3732 6.7686 1 -4 -4 0 65.4148 3.7372 2 -4 -4 0 65.6199 3.8277 13 4 -4 0 65.7809 6.6680 1 4 -4 0 71.3049 7.5907 12 -4 -4 0 65.7057 7.2856 12 -4 4 0 80.8570 9.4883 20 4 4 0 64.5380 7.5283 3 4 4 0 73.5863 7.0421 8 -4 4 0 80.4459 6.9888 14 4 4 0 86.1916 9.2094 20 5 -4 0 13.0685 4.3525 1 -5 -4 0 14.5321 2.2273 13 -5 -4 0 16.0763 4.4836 1 -5 -4 0 14.3271 2.0046 2 -5 -4 0 18.7062 5.2043 10 -5 -4 0 17.6630 2.2824 9 -5 -4 0 16.8298 2.2864 4 5 -4 0 9.93741 4.88919 12 -5 -4 0 17.2684 5.2126 12 -5 -4 0 14.4170 2.3285 11 -5 4 0 16.9945 5.0680 14 5 4 0 23.4997 5.2966 3 -5 4 0 18.2807 6.2732 20 5 4 0 14.5026 4.4616 8 -5 4 0 15.0408 1.9223 2 -5 4 0 11.4319 2.4241 13 -6 -4 0 151.547 11.932 10 -6 -4 0 166.289 6.353 13 6 -4 0 162.797 10.391 1 6 -4 0 162.352 10.980 12 -6 -4 0 159.341 10.671 1 -6 -4 0 157.445 6.947 11 -6 -4 0 160.699 6.591 2 -6 -4 0 162.735 7.185 9 -6 -4 0 154.098 10.779 12 -6 -4 0 160.387 7.067 4 6 4 0 171.672 11.435 8 -6 4 0 157.594 10.745 14 6 4 0 180.058 12.384 3 -6 4 0 158.770 6.473 2 -6 4 0 139.584 12.040 20 -6 4 0 145.712 6.461 13 -7 -4 0 122.681 6.530 9 -7 -4 0 126.268 5.120 7 -7 -4 0 129.902 6.433 4 -7 -4 0 132.450 6.401 11 -7 -4 0 133.191 5.870 13 -7 -4 0 133.095 5.904 2 -7 -4 0 141.205 5.917 19 -7 -4 0 129.628 6.328 6 -7 -4 0 141.491 6.233 16 -7 4 0 121.593 5.719 2 -7 4 0 119.868 6.114 13 -7 4 0 120.945 5.026 5 -7 4 0 136.450 5.785 18 -7 4 0 121.076 4.972 7 -7 4 0 133.649 6.097 19 -7 4 0 130.865 5.055 15 -8 -4 0 317.609 12.096 19 -8 -4 0 327.935 12.394 16 -8 -4 0 324.153 11.261 13 -8 -4 0 318.469 12.868 4 -8 -4 0 313.033 12.768 6 -8 -4 0 312.769 11.845 2 -8 -4 0 312.175 10.382 7 -8 -4 0 314.099 12.659 9 -8 -4 0 309.688 11.773 11 -8 4 0 332.830 10.247 15 -8 4 0 339.892 12.260 19 -8 4 0 324.599 11.409 18 -8 4 0 313.191 11.860 2 -8 4 0 294.803 11.118 13 -8 4 0 306.815 10.377 7 -9 -4 0 126.640 5.856 2 -9 -4 0 128.105 6.505 6 -9 -4 0 124.534 6.545 11 -9 -4 0 129.984 6.682 4 -9 -4 0 130.078 5.055 7 -9 -4 0 121.141 6.246 13 -9 -4 0 124.336 6.281 16 -9 -4 0 125.927 6.729 9 -9 4 0 120.528 5.889 13 -9 4 0 130.368 5.031 15 -9 4 0 127.776 5.673 18 -9 4 0 127.927 5.870 2 -9 4 0 128.545 6.073 19 -9 4 0 125.694 5.139 7 -10 -4 0 335.611 12.218 2 -10 -4 0 332.764 11.577 13 -10 -4 0 322.722 12.324 11 -10 -4 0 329.640 13.043 9 -10 -4 0 315.863 12.698 16 -10 -4 0 327.351 13.237 6 -10 -4 0 331.704 13.197 4 -10 4 0 338.590 10.640 7 -10 4 0 338.281 11.602 18 -10 4 0 344.453 12.108 2 -10 4 0 322.364 12.455 19 -11 -4 0 57.1045 4.4615 13 -11 -4 0 58.3608 3.4644 2 -11 -4 0 57.7263 4.3636 6 -11 -4 0 55.2635 4.4378 4 -11 -4 0 63.1590 4.6153 11 -11 -4 0 55.4974 4.4998 9 -11 4 0 64.2706 3.1149 7 -11 4 0 66.8166 3.3514 18 -11 4 0 65.2782 3.5667 19 -12 -4 0 37.0644 3.1348 6 0 -5 0 -0.3864 3.5830 1 0 -5 0 -5.8312 3.8118 12 0 -5 0 -1.6013 5.8894 21 0 -5 0 -0.2698 2.9621 10 0 5 0 0.87579 3.33345 14 0 5 0 -0.2214 6.2165 20 0 5 0 3.29409 6.34949 21 1 -5 0 241.125 11.456 12 -1 -5 0 244.108 9.515 14 -1 -5 0 235.516 11.881 1 -1 -5 0 237.487 11.990 10 -1 -5 0 265.487 11.749 12 1 -5 0 220.575 11.995 1 1 5 0 230.276 12.345 3 -1 5 0 248.359 11.587 14 -1 5 0 254.383 16.022 20 1 5 0 224.032 17.743 21 1 5 0 233.951 15.344 20 2 -5 0 35.0104 4.7959 1 2 -5 0 30.6263 5.0011 12 -2 -5 0 37.8806 5.3182 12 -2 -5 0 33.2975 5.1744 1 -2 -5 0 32.8430 4.9186 10 2 5 0 30.7311 4.7684 3 2 5 0 30.5198 3.6846 8 2 5 0 29.4664 7.0050 20 -2 5 0 30.6326 5.0785 14 -2 5 0 27.9572 7.6703 20 -3 -5 0 473.001 21.766 10 3 -5 0 496.171 21.149 1 -3 -5 0 529.926 20.305 12 -3 -5 0 478.351 21.263 1 -3 -5 0 476.792 17.378 2 -3 -5 0 498.311 15.972 13 3 -5 0 493.995 19.380 12 -3 5 0 487.349 20.445 14 3 5 0 489.903 24.220 20 3 5 0 531.669 23.665 3 -3 5 0 483.944 17.298 2 -3 5 0 491.596 25.376 20 3 5 0 524.310 21.886 8 4 -5 0 73.5052 6.8600 1 -4 -5 0 75.1177 4.3042 11 -4 -5 0 81.3255 7.8966 12 -4 -5 0 71.7958 3.9676 2 -4 -5 0 72.2236 4.5222 4 -4 -5 0 66.2315 7.0159 1 -4 -5 0 79.6225 4.3393 9 -4 -5 0 71.0712 4.0761 13 -4 -5 0 71.0775 8.1072 10 -4 5 0 92.8064 3.8748 13 -4 5 0 84.3665 10.4139 20 4 5 0 91.6407 8.2812 3 4 5 0 87.8731 7.5944 8 -4 5 0 84.9316 7.4822 14 -4 5 0 80.1663 4.0269 2 5 -5 0 7.08098 5.08923 12 -5 -5 0 19.9143 2.4055 9 5 -5 0 17.7574 4.8590 1 -5 -5 0 14.0222 5.3626 12 -5 -5 0 16.0502 2.5624 11 -5 -5 0 23.7303 5.8491 10 -5 -5 0 18.3551 2.4321 13 -5 -5 0 17.9256 2.1931 2 -5 -5 0 17.8076 5.0324 1 -5 -5 0 20.9846 2.6297 4 5 5 0 16.7721 5.2592 3 -5 5 0 10.1820 5.0444 14 -5 5 0 13.7569 1.9630 2 -5 5 0 11.3298 6.5417 20 -5 5 0 19.0971 2.3344 13 5 5 0 19.4164 4.7726 8 -6 -5 0 569.357 27.348 10 -6 -5 0 608.872 21.254 9 -6 -5 0 561.350 17.942 7 -6 -5 0 599.383 20.974 19 -6 -5 0 587.514 20.403 2 6 -5 0 591.262 25.674 1 -6 -5 0 589.055 18.706 13 -6 -5 0 592.844 19.776 11 -6 -5 0 580.947 21.244 16 -6 -5 0 568.518 21.599 4 -6 -5 0 581.086 25.960 1 -6 -5 0 579.851 21.885 6 -6 5 0 531.153 29.039 20 -6 5 0 591.362 19.433 18 6 5 0 582.754 28.845 3 -6 5 0 580.836 17.687 15 -6 5 0 567.395 20.260 2 -6 5 0 552.202 17.854 7 -6 5 0 562.556 18.556 13 -6 5 0 568.361 18.754 5 6 5 0 589.795 26.961 8 -6 5 0 553.747 17.928 17 -6 5 0 580.481 20.941 19 -7 -5 0 478.987 19.052 6 -7 -5 0 497.008 18.184 19 -7 -5 0 495.837 16.515 13 -7 -5 0 482.975 15.548 7 -7 -5 0 483.327 18.515 16 -7 -5 0 510.945 17.899 2 -7 -5 0 505.407 17.345 11 -7 -5 0 494.432 18.595 9 -7 -5 0 490.668 18.948 4 -7 5 0 490.949 17.630 2 -7 5 0 514.293 16.952 18 -7 5 0 485.178 15.569 7 -7 5 0 491.509 15.337 15 -7 5 0 515.242 18.264 19 -7 5 0 502.049 16.284 5 -8 -5 0 496.924 18.468 9 -8 -5 0 483.750 15.365 7 -8 -5 0 496.227 18.348 16 -8 -5 0 485.039 17.205 11 -8 -5 0 491.633 17.667 2 -8 -5 0 478.618 18.914 6 -8 -5 0 502.090 18.784 4 -8 -5 0 414.824 16.210 13 -8 -5 0 491.408 17.988 19 -8 5 0 490.349 17.493 2 -8 5 0 485.746 15.379 7 -8 5 0 498.458 16.042 5 -8 5 0 497.912 16.762 18 -8 5 0 515.500 15.273 15 -8 5 0 516.833 18.108 19 -9 -5 0 123.207 4.768 7 -9 -5 0 123.105 6.287 6 -9 -5 0 118.663 6.508 9 -9 -5 0 134.220 6.697 4 -9 -5 0 113.050 5.944 13 -9 -5 0 127.840 5.608 2 -9 -5 0 120.647 6.213 16 -9 -5 0 113.484 6.158 11 -9 5 0 122.267 5.510 2 -9 5 0 112.037 5.418 18 -9 5 0 113.852 4.723 15 -9 5 0 116.684 4.879 7 -9 5 0 116.698 4.577 5 -9 5 0 104.759 5.710 19 -10 -5 0 11.7564 2.9471 13 -10 -5 0 14.6801 2.4963 16 -10 -5 0 16.7153 2.9808 9 -10 -5 0 14.2924 2.2539 2 -10 -5 0 13.7897 3.2215 11 -10 -5 0 17.7059 3.0371 4 -10 -5 0 10.7642 2.6846 6 -10 5 0 14.5293 2.0606 2 -10 5 0 15.3176 2.1586 18 -10 5 0 17.1681 2.2308 19 -10 5 0 16.8015 1.9191 15 -10 5 0 14.0722 2.0143 7 -11 -5 0 28.5362 2.9631 11 -11 -5 0 19.2246 2.4679 6 -11 -5 0 24.1469 2.7011 9 -11 -5 0 21.6507 2.7079 13 -11 5 0 18.5276 1.8512 18 -11 5 0 21.3976 2.1878 7 -11 5 0 21.2845 2.6229 19 11 5 0 18.5200 2.6404 16 0 -6 0 100.715 4.481 2 0 -6 0 95.8103 4.4581 13 0 -6 0 102.274 6.015 14 0 -6 0 97.1318 7.6203 12 0 -6 0 118.974 8.264 1 0 6 0 80.7956 10.6783 20 1 -6 0 532.612 19.249 2 1 -6 0 533.279 17.571 13 1 -6 0 544.301 21.431 12 -1 -6 0 542.111 19.298 2 -1 -6 0 530.441 21.681 12 -1 -6 0 543.804 17.637 13 1 -6 0 567.280 23.575 1 -1 -6 0 567.797 23.730 1 -1 6 0 581.815 28.490 20 1 6 0 548.252 27.763 20 -1 6 0 587.017 22.037 14 -2 -6 0 325.516 15.277 1 2 -6 0 287.838 10.281 13 2 -6 0 315.782 15.153 1 -2 -6 0 321.460 14.975 12 -2 -6 0 319.659 11.249 2 -2 -6 0 313.088 10.393 13 2 -6 0 306.677 13.971 12 2 6 0 279.628 18.552 20 -2 6 0 276.105 18.916 20 -2 6 0 306.967 14.460 14 -3 -6 0 97.2856 8.6342 12 -3 -6 0 91.8693 8.0367 1 -3 -6 0 104.175 4.568 13 3 -6 0 96.1856 8.0500 12 3 -6 0 88.5968 7.6610 1 -3 -6 0 100.971 4.514 2 -3 6 0 98.7925 4.4697 2 -3 6 0 105.776 8.505 14 3 6 0 102.602 11.786 20 -3 6 0 101.500 11.906 20 -4 -6 0 104.370 4.844 13 -4 -6 0 108.903 8.796 1 -4 -6 0 99.6241 5.3153 4 -4 -6 0 98.1386 4.8155 2 4 -6 0 95.3016 8.1776 1 -4 -6 0 103.284 5.318 16 -4 -6 0 100.779 9.027 12 -4 6 0 104.943 4.989 19 -4 6 0 99.1886 4.7059 2 -4 6 0 98.2144 8.8573 14 -4 6 0 99.5309 4.0737 15 -4 6 0 105.027 4.328 5 -4 6 0 99.2780 4.2754 7 4 6 0 126.571 9.359 3 -4 6 0 100.917 12.084 20 -4 6 0 101.333 4.748 18 -5 -6 0 117.360 5.857 16 -5 -6 0 114.919 5.438 13 -5 -6 0 113.901 5.970 4 -5 -6 0 114.000 5.547 11 -5 -6 0 116.592 4.662 7 -5 -6 0 106.193 5.509 19 -5 -6 0 117.761 5.536 2 -5 6 0 117.261 4.725 5 -5 6 0 114.119 5.236 18 -5 6 0 111.904 4.600 15 -5 6 0 113.901 4.505 7 -5 6 0 114.795 5.316 2 -5 6 0 114.384 5.527 19 -5 6 0 105.757 5.053 17 -6 -6 0 133.069 6.765 4 -6 -6 0 135.212 6.429 9 -6 -6 0 137.375 6.385 6 -6 -6 0 126.277 5.191 7 -6 -6 0 134.521 6.014 2 -6 -6 0 123.246 6.039 19 -6 -6 0 128.362 6.044 13 -6 -6 0 135.149 6.414 11 -6 -6 0 134.506 6.476 16 -6 6 0 130.970 6.165 19 -6 6 0 128.563 5.258 5 -6 6 0 128.041 5.142 15 -6 6 0 130.933 5.427 17 -6 6 0 130.914 5.860 18 -6 6 0 124.340 5.174 7 -6 6 0 135.138 5.778 2 -7 -6 0 1.80774 2.92808 4 -7 -6 0 4.72776 2.16540 7 -7 -6 0 1.30208 2.60828 9 -7 -6 0 0.74339 2.87521 11 -7 -6 0 1.87818 2.90434 13 -7 -6 0 1.41447 1.95993 19 -7 -6 0 -0.0160 2.4698 6 -7 -6 0 5.19168 2.47976 2 -7 -6 0 2.32210 2.58012 16 -7 6 0 2.17882 2.17520 19 -7 6 0 1.16966 2.05306 15 -7 6 0 3.49587 2.32551 18 -7 6 0 3.37848 2.14392 2 -7 6 0 2.90730 1.67194 5 -7 6 0 2.56476 2.11179 7 -8 -6 0 49.6301 4.0480 2 -8 -6 0 51.2468 4.8285 11 -8 -6 0 50.1213 3.4525 7 -8 -6 0 47.3129 3.8503 19 -8 -6 0 54.0746 4.7996 4 -8 -6 0 45.3079 4.4588 13 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-0.8685 1.9252 2 0 -7 0 -1.4779 4.4905 12 0 -7 0 -0.7907 2.1846 13 0 7 0 9.24726 7.63979 20 0 7 0 0.09119 1.65881 7 0 7 0 0.30067 1.71040 19 -1 -7 0 310.262 10.638 13 -1 -7 0 304.382 15.972 1 1 -7 0 300.740 10.605 13 1 -7 0 345.387 16.467 1 -1 -7 0 310.568 11.576 2 1 -7 0 301.723 14.800 12 1 -7 0 308.575 11.555 2 -1 -7 0 313.096 15.251 12 -1 -7 0 311.635 10.186 7 -1 7 0 327.859 10.606 17 -1 7 0 304.410 10.100 7 -1 7 0 331.134 11.775 19 -1 7 0 310.399 20.731 20 1 7 0 302.927 20.107 20 2 -7 0 283.281 11.236 2 -2 -7 0 294.105 9.903 7 -2 -7 0 312.994 11.663 19 -2 -7 0 310.050 15.697 12 2 -7 0 288.570 15.686 1 -2 -7 0 282.888 15.695 1 -2 -7 0 303.495 10.450 13 -2 -7 0 301.223 11.301 2 -2 7 0 304.476 9.789 7 -2 7 0 303.485 20.420 20 2 7 0 290.861 19.576 20 -2 7 0 325.172 11.535 19 -2 7 0 318.171 10.676 18 -2 7 0 301.661 10.270 5 -2 7 0 327.621 10.299 17 2 7 0 301.343 12.100 16 -3 -7 0 5.49970 2.07988 19 -3 -7 0 5.82178 2.10280 7 -3 -7 0 6.90290 5.32547 12 -3 -7 0 5.81546 2.15563 2 -3 -7 0 8.96214 2.48410 13 3 -7 0 7.94337 2.26019 2 -3 7 0 8.53204 2.73757 17 -3 7 0 8.69211 1.88901 19 -3 7 0 7.13144 2.06436 18 -3 7 0 6.51098 1.61471 5 -3 7 0 8.91045 1.79704 15 -3 7 0 8.29453 1.81891 7 -4 -7 0 102.774 5.652 16 -4 -7 0 107.538 5.352 13 -4 -7 0 106.789 5.524 19 -4 -7 0 94.5842 4.4556 7 -4 -7 0 108.063 5.345 2 -4 7 0 109.043 4.405 15 -4 7 0 114.390 5.296 17 -4 7 0 102.699 4.396 7 -4 7 0 109.224 4.573 5 -4 7 0 114.205 5.371 19 -4 7 0 110.752 5.080 18 -5 -7 0 98.4624 5.2338 13 -5 -7 0 94.1863 5.5897 4 -5 -7 0 100.787 4.615 7 -5 -7 0 100.103 5.135 2 -5 -7 0 107.396 5.608 16 -5 -7 0 101.364 5.287 19 -5 7 0 95.1273 4.9276 17 -5 7 0 96.0063 4.4534 7 -5 7 0 99.4041 4.4514 5 -5 7 0 100.685 5.263 19 -5 7 0 97.8075 4.3509 15 -5 7 0 100.340 4.967 18 -5 7 0 101.829 5.066 2 -6 -7 0 167.106 7.429 2 -6 -7 0 160.896 7.855 4 -6 -7 0 165.854 6.456 7 -6 -7 0 177.439 7.822 16 -6 -7 0 171.949 7.318 11 -6 -7 0 165.615 7.403 19 -6 -7 0 174.708 7.170 13 -6 7 0 185.507 6.750 17 -6 7 0 182.007 7.596 19 -6 7 0 182.208 7.092 18 -6 7 0 174.038 6.370 7 -6 7 0 174.408 6.581 5 -6 7 0 177.621 6.341 15 -6 7 0 171.350 7.176 2 -7 -7 0 131.190 6.686 4 -7 -7 0 132.309 6.402 11 -7 -7 0 138.175 6.100 19 -7 -7 0 133.779 6.319 2 -7 -7 0 136.988 6.660 6 -7 -7 0 133.586 6.321 13 -7 -7 0 149.594 6.654 16 -7 -7 0 131.474 5.250 7 -7 7 0 132.949 5.357 5 -7 7 0 128.664 5.879 18 -7 7 0 133.381 5.598 17 -7 7 0 133.370 6.285 19 -7 7 0 132.054 5.353 7 -7 7 0 133.370 5.293 15 -7 7 0 128.201 5.881 2 -8 -7 0 38.0140 4.1119 13 -8 -7 0 40.3224 4.1268 11 -8 -7 0 40.0110 3.6024 2 -8 -7 0 38.5999 3.0363 7 -8 -7 0 32.0294 3.4195 4 -8 -7 0 36.6939 4.0705 6 -8 7 0 33.6428 3.6168 19 -8 7 0 34.9667 2.6861 5 -8 7 0 34.9528 3.0180 15 -8 7 0 33.2221 3.4620 18 -8 7 0 38.9780 3.2061 2 -8 7 0 37.9200 3.1288 7 -9 -7 0 6.81808 2.32782 6 -9 -7 0 4.76966 1.97038 2 -9 -7 0 15.4309 2.6962 11 -9 -7 0 5.12570 2.63303 13 -9 7 0 5.70233 1.78375 7 -9 7 0 4.06492 1.74572 15 -9 7 0 5.39169 1.34044 5 -9 7 0 4.01397 1.88840 18 9 7 0 5.44431 2.89036 4 -9 7 0 4.51698 1.89064 19 9 7 0 10.4682 2.9414 16 -10 -7 0 3.82478 1.79939 6 -10 7 0 4.89676 1.37010 7 10 7 0 8.46475 2.40507 16 -10 7 0 3.79107 1.50450 18 -10 7 0 5.82706 1.54369 19 -10 7 0 3.90121 1.37896 15 0 -8 0 853.641 29.383 2 0 -8 0 826.725 26.693 13 0 8 0 855.587 26.129 17 0 8 0 838.742 30.114 19 -1 -8 0 20.3955 2.6277 2 -1 -8 0 12.3492 2.4122 7 -1 -8 0 5.56388 2.25778 19 1 -8 0 14.9322 2.4486 2 -1 -8 0 6.47688 2.44222 13 -1 8 0 6.34433 2.79740 17 -1 8 0 8.83829 2.10204 19 -1 8 0 9.00964 2.17925 18 -1 8 0 11.0916 1.6393 5 1 8 0 4.78777 2.71202 17 -1 8 0 9.91269 1.97074 7 -2 -8 0 48.4057 3.4050 7 -2 -8 0 45.3405 4.1223 19 -2 -8 0 51.4057 3.8711 13 2 -8 0 50.4139 3.9448 2 -2 -8 0 46.2421 3.7487 2 -2 8 0 49.1307 3.0662 5 2 8 0 43.4691 3.7942 16 -2 8 0 54.0412 4.4456 17 -2 8 0 47.1194 3.2448 7 -2 8 0 49.5826 3.8597 18 -2 8 0 50.7055 3.9007 19 2 8 0 45.1093 4.3658 17 3 -8 0 52.5584 4.1094 2 -3 -8 0 52.9673 4.4138 13 -3 -8 0 54.5720 3.6544 7 -3 -8 0 50.2383 4.0354 2 -3 -8 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24.5067 5.0723 8 -5 -1 -3 21.0378 2.5944 9 -5 -1 -3 21.3919 2.1109 2 5 -1 3 23.7649 4.5038 3 5 -1 3 27.3778 4.5652 12 5 -1 3 24.6437 5.2093 10 -5 -1 -3 26.0919 5.8965 12 -5 -1 -3 22.2705 2.5640 13 -5 1 -3 21.5662 2.0874 2 -5 1 -3 21.5708 2.5519 13 -5 1 -3 23.6484 5.1401 1 5 1 3 24.4014 5.1431 3 -5 1 -3 22.3314 2.9566 11 5 1 3 23.9871 4.7054 10 5 1 3 24.7981 5.1186 8 -5 1 -3 26.2404 5.1606 14 -6 -1 -3 62.1196 4.1660 13 6 -1 3 59.8308 6.7299 12 6 -1 3 89.0814 8.4391 8 -6 -1 -3 65.0282 3.7273 2 6 -1 3 68.7957 7.7148 10 -6 -1 -3 76.7124 7.4872 1 -6 -1 -3 60.2722 4.6356 11 -6 -1 -3 54.8438 7.6965 12 -6 -1 -3 57.4934 4.7110 9 -6 -1 -3 60.8590 4.3500 4 -6 1 -3 60.1590 4.6373 9 -6 1 -3 64.3237 3.7828 2 6 1 3 66.8416 7.7144 8 -6 1 -3 56.8763 4.3755 13 -6 1 -3 62.7197 7.2655 14 -6 1 -3 59.2894 4.6618 11 6 1 3 84.2346 8.2328 3 -6 1 -3 68.4187 7.6225 1 6 1 3 72.9174 7.8329 10 -7 -1 -3 28.6710 2.5587 18 -7 -1 -3 23.5106 2.9318 4 -7 -1 -3 26.5511 2.6103 19 7 -1 3 38.0289 5.9866 10 -7 -1 -3 25.2397 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-3 3.88405 1.29613 7 -12 1 -3 3.37438 1.26573 19 -13 -2 3 90.2833 4.3546 6 -12 -2 3 4.59895 2.38931 9 -12 -2 3 10.5827 2.4549 13 -12 -2 3 3.04034 2.18743 6 -12 -2 3 4.62804 2.39143 4 -12 -2 3 8.18881 2.79548 11 -11 -2 3 56.5771 4.1295 6 -11 -2 3 63.1267 3.9041 16 -11 -2 3 52.3998 5.0435 11 -11 -2 3 57.7236 4.6257 9 -11 -2 3 64.4305 4.6386 13 -11 -2 3 61.3207 4.6031 4 -10 -2 3 7.05283 2.41347 6 -10 -2 3 6.58717 2.74539 9 -10 -2 3 10.3813 2.2261 16 -10 -2 3 7.00987 2.81567 13 -10 -2 3 10.3504 3.2133 11 -10 -2 3 8.52985 2.81183 4 -9 -2 3 152.675 6.741 16 -9 -2 3 154.930 6.596 13 -9 -2 3 153.215 7.006 11 -9 -2 3 141.259 7.109 9 -9 -2 3 146.077 7.110 4 -9 -2 3 147.081 6.959 6 -8 -2 3 172.785 7.022 16 -8 -2 3 160.590 7.214 4 -8 -2 3 164.261 7.223 11 -8 -2 3 146.842 11.167 12 -8 -2 3 163.815 7.350 9 -8 -2 3 166.726 6.611 13 -8 -2 3 159.592 7.153 6 -8 -2 3 165.500 12.722 10 8 2 -3 145.236 11.372 8 8 2 -3 149.063 11.993 3 -7 -2 3 105.660 5.351 9 7 -2 -3 93.6090 6.4165 14 -7 -2 3 109.774 5.161 11 -7 -2 3 95.9572 4.7691 13 -7 -2 3 99.0903 9.4899 10 -7 -2 3 103.606 5.212 4 7 -2 -3 112.803 7.839 3 -7 -2 3 101.078 8.544 12 7 -2 -3 100.143 8.430 20 -7 -2 3 109.385 10.475 8 -7 -2 3 105.314 7.740 1 7 2 -3 106.466 9.198 3 -6 -2 3 44.1364 3.1302 13 6 -2 -3 49.7922 4.4805 10 6 -2 -3 50.8755 4.6906 12 -6 -2 3 38.1535 6.3570 8 6 -2 -3 32.4256 4.2144 1 -6 -2 3 41.7458 3.5410 11 -6 -2 3 34.3902 3.5596 9 -6 -2 3 48.2353 6.6026 10 -6 -2 3 33.5007 3.3301 4 -6 -2 3 47.3885 6.0719 12 -6 -2 3 35.4415 4.9080 1 6 -2 -3 40.9497 4.3894 14 -6 2 3 33.8348 5.5886 3 6 2 -3 51.5085 6.7329 20 6 2 -3 34.5937 5.4368 3 -6 2 3 42.6200 7.0277 20 -5 -2 3 305.742 13.435 1 -5 -2 3 309.039 13.408 12 -5 -2 3 284.271 15.935 8 5 -2 -3 278.489 12.436 1 5 -2 -3 297.569 12.792 10 -5 -2 3 292.372 16.393 3 5 -2 -3 297.706 12.281 14 -5 -2 3 297.370 15.013 10 5 -2 -3 288.321 11.710 12 -5 2 3 296.899 14.257 8 5 2 -3 290.571 15.897 20 -5 2 3 283.617 16.001 20 -5 2 3 307.629 15.523 3 -4 -2 3 260.174 13.986 3 4 -2 -3 216.869 10.103 1 4 -2 -3 241.272 10.276 14 -4 -2 3 237.393 10.574 1 -4 -2 3 229.543 13.489 8 -4 -2 3 228.344 11.029 12 4 -2 -3 240.714 9.277 12 -4 -2 3 243.978 13.770 21 -4 -2 3 208.460 12.186 10 -4 2 3 229.315 12.583 3 -4 2 3 231.931 11.640 8 -4 2 3 242.014 14.063 20 4 2 -3 248.876 14.929 21 4 2 -3 239.520 13.585 20 -3 -2 3 51.4799 5.0403 12 -3 -2 3 40.2477 5.5231 3 -3 -2 3 38.6790 4.9847 10 3 -2 -3 41.5848 4.3758 14 -3 -2 3 36.8959 4.4423 1 -3 -2 3 43.4057 2.8768 14 -3 -2 3 48.3571 6.9305 21 -3 -2 3 41.2100 5.4911 8 3 -2 -3 31.0997 3.1838 1 3 -2 -3 46.8475 6.3679 21 3 -2 -3 43.2141 3.4727 12 3 2 -3 53.2585 6.8991 21 -3 2 3 40.7087 5.3130 8 -3 2 3 44.3974 6.3863 20 -3 2 3 52.5836 5.6579 21 3 2 -3 54.9095 6.3098 20 3 2 -3 43.7536 3.5876 14 -3 2 3 35.3558 4.9001 3 2 -2 -3 1966.07 79.59 1 -2 -2 3 1634.50 79.17 21 2 -2 -3 1782.29 62.67 12 -2 -2 3 1865.84 89.31 10 -2 -2 3 1885.32 94.65 3 2 -2 -3 1914.76 82.69 14 -2 -2 3 1851.46 87.96 12 2 -2 -3 1849.84 62.85 12 2 -2 -3 1956.12 79.09 21 -2 -2 3 1872.85 83.81 8 -2 -2 3 1920.28 83.44 1 -2 2 3 1871.46 81.53 8 2 2 -3 1911.79 98.98 21 -2 2 3 1797.42 91.30 21 2 2 -3 1861.42 71.90 14 -2 2 3 1746.99 85.68 20 2 2 -3 2084.79 93.02 20 -2 2 3 1805.35 83.56 3 -1 -2 3 504.427 18.401 12 1 -2 -3 496.387 24.742 21 -1 -2 3 507.288 19.531 1 1 -2 -3 506.419 18.169 14 1 -2 -3 501.187 16.966 12 -1 -2 3 515.054 22.177 3 -1 -2 3 516.087 21.432 8 -1 -2 3 482.314 20.603 10 -1 -2 3 495.715 24.608 21 1 -2 -3 518.518 19.427 1 1 2 -3 542.394 22.777 20 -1 2 3 490.104 22.434 3 -1 2 3 500.159 16.963 12 1 2 -3 501.854 24.850 21 -1 2 3 526.825 20.690 8 -1 2 3 539.498 22.748 20 -1 2 3 557.270 24.964 21 1 2 -3 498.350 18.135 14 0 -2 -3 157.770 8.251 1 0 -2 -3 190.807 12.915 21 0 -2 3 189.010 12.016 21 0 -2 -3 174.082 7.404 12 0 -2 -3 182.210 7.927 14 0 -2 3 184.060 8.755 12 0 -2 3 187.250 9.760 10 0 -2 3 163.545 8.459 1 0 -2 3 174.670 9.036 3 0 -2 3 180.819 9.610 8 0 2 3 203.178 12.879 21 0 2 3 198.886 10.656 20 0 2 -3 194.221 8.911 14 0 2 -3 187.767 12.531 21 0 2 3 159.293 10.685 3 0 2 -3 187.394 11.313 20 0 2 3 174.327 7.824 10 0 2 3 175.691 9.408 8 1 -2 3 9.24251 3.58652 8 -1 -2 -3 14.6938 6.0616 21 -1 -2 -3 16.7827 3.0640 1 1 -2 3 13.1338 2.5132 3 1 -2 3 9.24325 3.89311 12 1 -2 3 14.9176 5.3144 21 1 -2 3 12.6582 4.1121 10 -1 -2 -3 15.7401 3.3400 14 1 -2 3 14.7467 3.2284 1 -1 -2 -3 9.31004 3.36468 12 1 2 3 10.4789 3.3241 8 -1 2 -3 16.1792 4.9887 20 -1 2 -3 15.6704 2.2576 3 1 2 3 8.54491 4.23911 3 1 2 3 17.5258 3.6461 20 -1 2 -3 13.1359 4.0662 14 1 2 3 13.3425 2.7392 10 1 2 3 15.8530 6.1229 21 -1 2 -3 14.2580 5.6241 21 2 -2 3 416.941 17.346 3 2 -2 3 414.816 18.176 8 -2 -2 -3 414.269 16.810 1 -2 -2 -3 439.047 15.025 14 2 -2 3 402.632 16.674 1 -2 -2 -3 422.455 15.625 12 -2 -2 -3 406.026 22.180 21 -2 -2 -3 374.844 16.618 20 2 -2 3 401.063 15.616 12 2 -2 3 402.571 20.682 21 2 -2 3 401.809 17.629 10 2 2 3 378.856 19.033 3 2 2 3 382.072 16.604 10 -2 2 -3 407.392 18.753 20 -2 2 -3 397.887 16.318 14 -2 2 -3 408.748 21.273 21 2 2 3 390.714 21.961 21 2 2 3 390.582 17.696 8 3 -2 3 161.349 10.401 8 3 -2 3 160.723 9.398 1 3 -2 3 160.948 10.872 10 -3 -2 -3 176.919 9.575 12 -3 -2 -3 171.013 9.582 1 3 -2 3 170.173 9.325 3 -3 -2 -3 178.093 7.981 14 -3 -2 -3 168.218 13.556 21 3 -2 3 165.614 9.539 12 3 2 3 169.804 10.361 8 3 2 3 160.331 10.895 3 -3 2 -3 172.944 9.467 14 -3 2 -3 182.657 12.683 21 3 2 3 168.356 9.496 10 -3 2 -3 184.599 10.921 20 3 2 3 166.391 13.731 21 -3 2 -3 190.953 12.860 21 4 -2 3 122.045 8.488 12 4 -2 3 113.223 9.315 10 4 -2 3 134.869 7.976 3 4 -2 3 126.329 9.083 8 -4 -2 -3 116.637 8.710 12 -4 -2 -3 128.819 8.626 1 4 -2 3 120.223 8.125 1 -4 2 -3 114.585 8.672 14 -4 2 -3 103.189 7.832 20 4 2 3 105.489 8.840 8 4 2 3 112.990 8.285 10 4 2 3 111.963 8.996 3 -5 -2 -3 172.756 6.866 2 5 -2 3 175.858 10.239 1 5 -2 3 189.810 11.367 8 5 -2 3 188.360 11.209 10 -5 -2 -3 175.539 7.393 4 5 -2 3 175.018 10.105 12 -5 -2 -3 161.453 7.530 9 -5 -2 -3 185.318 10.891 1 -5 -2 -3 193.559 11.046 12 -5 -2 -3 174.841 7.020 11 -5 -2 -3 180.974 6.646 13 -5 2 -3 166.801 10.740 14 5 2 3 163.195 11.658 3 -5 2 -3 163.869 7.166 11 -5 2 -3 164.395 6.929 13 5 2 3 169.455 10.496 10 -5 2 -3 155.061 6.834 2 5 2 3 175.259 11.214 8 6 -2 3 245.732 13.545 1 -6 -2 -3 260.214 9.305 13 6 -2 3 262.335 13.146 12 -6 -2 -3 242.805 9.679 11 -6 -2 -3 262.572 10.522 9 -6 -2 -3 254.410 10.509 4 -6 -2 -3 269.778 14.348 1 -6 -2 -3 260.194 14.316 12 -6 -2 -3 253.900 9.700 2 6 -2 3 278.468 15.043 8 6 -2 3 271.502 14.712 10 -6 2 -3 254.666 9.716 2 6 2 3 266.791 14.460 10 -6 2 -3 252.447 10.302 9 6 2 3 255.335 14.946 8 -6 2 -3 238.854 13.500 14 -6 2 -3 258.297 9.266 13 -6 2 -3 263.721 9.977 11 6 2 3 277.368 15.827 3 -7 -2 -3 106.124 6.139 9 -7 -2 -3 111.989 5.769 6 -7 -2 -3 101.036 6.168 11 7 -2 3 125.259 10.452 10 -7 -2 -3 109.045 5.458 19 -7 -2 -3 107.741 4.464 7 -7 -2 -3 107.722 5.783 4 -7 -2 -3 106.929 5.398 13 -7 -2 -3 110.288 5.172 2 -7 2 -3 108.133 5.661 19 -7 2 -3 103.670 5.157 2 -7 2 -3 100.965 6.036 11 -7 2 -3 104.056 5.491 13 -7 2 -3 102.416 4.523 7 -7 2 -3 106.287 5.470 18 -8 -2 -3 29.0565 2.9357 2 -8 -2 -3 29.3180 3.7220 9 -8 -2 -3 32.1956 3.5583 4 -8 -2 -3 26.5355 3.2777 6 -8 -2 -3 40.1373 3.9430 19 -8 -2 -3 25.0298 3.4880 13 -8 -2 -3 34.3811 3.9777 11 -8 -2 -3 29.5471 2.8737 7 -8 2 -3 28.1800 2.4826 7 -8 2 -3 33.2958 4.0956 11 -8 2 -3 34.6407 2.8567 18 -8 2 -3 23.7280 2.9033 2 -8 2 -3 35.3719 4.1799 19 -8 2 -3 34.3070 3.6817 13 -9 -2 -3 7.20529 3.71843 11 -9 -2 -3 16.0242 2.4525 19 -9 -2 -3 11.7506 2.2414 7 -9 -2 -3 14.2636 3.4450 9 -9 -2 -3 11.1099 3.3887 13 -9 -2 -3 15.7264 2.5480 2 -9 -2 -3 12.5989 3.0959 6 -9 -2 -3 17.0160 3.2303 4 -9 2 -3 13.7633 2.3262 7 -9 2 -3 15.0620 3.7240 11 -9 2 -3 11.0811 2.4276 18 -9 2 -3 14.7176 3.4144 13 -9 2 -3 16.7036 2.6326 2 -9 2 -3 14.2252 2.4057 19 -10 -2 -3 16.7212 2.8481 6 -10 -2 -3 10.1701 3.7846 11 -10 -2 -3 18.5117 3.3770 9 -10 -2 -3 14.3314 3.2341 13 -10 -2 -3 17.2842 2.4914 2 -10 -2 -3 14.8379 2.1409 7 -10 -2 -3 12.8134 2.1894 19 -10 2 -3 12.4056 2.1318 7 -10 2 -3 11.2770 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34.4971 6.4293 8 6 -3 -3 34.1407 4.7323 14 -6 3 3 30.6903 6.6364 20 6 3 -3 35.8044 5.7331 3 6 3 -3 30.1866 6.3392 20 5 -3 -3 29.7061 3.9951 1 -5 -3 3 24.9497 5.5364 8 -5 -3 3 26.7740 5.4438 10 -5 -3 3 30.3945 4.4178 1 -5 -3 3 27.5989 5.2973 12 5 -3 -3 28.1717 3.9197 12 5 -3 -3 29.5978 4.1902 14 -5 3 3 26.7840 4.3630 3 -5 3 3 34.0779 6.8096 20 5 3 -3 37.3434 6.4555 20 5 3 -3 25.9107 5.0538 3 -4 -3 3 1130.24 39.77 12 4 -3 -3 1131.65 39.30 14 4 -3 -3 1119.56 42.36 1 -4 -3 3 1184.56 46.77 8 4 -3 -3 1125.43 38.05 12 -4 -3 3 1158.14 44.44 10 -4 -3 3 1132.75 42.73 1 4 3 -3 1111.02 47.54 20 4 3 -3 1135.98 48.11 3 -4 3 3 1165.49 47.66 3 -4 3 3 1093.19 48.10 20 -3 -3 3 1677.03 83.19 10 3 -3 -3 1703.90 67.41 14 -3 -3 3 1711.59 67.27 8 -3 -3 3 1541.74 70.61 3 3 -3 -3 1776.16 58.33 12 -3 -3 3 1707.51 74.81 21 -3 -3 3 1756.71 57.69 12 -3 -3 3 1666.57 70.83 1 3 -3 -3 1714.28 69.38 1 3 -3 -3 1717.07 73.24 21 -3 3 3 1676.20 64.88 8 -3 3 3 1658.17 78.13 3 3 3 -3 1768.54 75.41 21 -3 3 3 1645.64 69.48 20 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621.946 27.186 10 -5 -3 -3 605.931 25.016 12 -5 3 -3 611.920 21.669 2 5 3 3 653.140 29.658 3 5 3 3 643.669 28.188 8 -5 3 -3 612.712 25.144 14 -5 3 -3 612.763 20.958 11 -5 3 -3 619.537 19.878 13 5 3 3 599.564 26.379 10 -6 -3 -3 24.9408 2.2310 7 -6 -3 -3 17.9164 2.9588 4 6 -3 3 22.3268 5.7959 12 6 -3 3 16.6111 6.2976 10 -6 -3 -3 24.1271 5.5766 1 -6 -3 -3 19.4057 2.6603 6 6 -3 3 22.2955 5.2712 1 -6 -3 -3 24.1195 6.4106 12 -6 -3 -3 17.7065 2.6201 13 -6 -3 -3 19.3042 2.3620 2 -6 -3 -3 21.6354 2.3440 19 -6 -3 -3 14.2703 2.9457 11 -6 -3 -3 18.6537 2.9901 9 -6 3 -3 22.1031 5.6562 14 -6 3 -3 20.7002 2.4669 2 -6 3 -3 20.4853 2.5073 18 -6 3 -3 21.3318 2.3232 19 -6 3 -3 17.4572 2.9157 13 -6 3 -3 20.8172 3.2301 11 6 3 3 30.3279 5.6065 8 6 3 3 27.1517 5.8434 3 -6 3 -3 20.2576 2.1056 7 6 3 3 20.1966 4.8074 10 -7 -3 -3 240.461 10.201 6 -7 -3 -3 239.641 8.242 7 -7 -3 -3 243.240 9.112 13 -7 -3 -3 238.183 10.212 9 -7 -3 -3 216.823 9.677 16 -7 -3 -3 243.270 10.335 4 -7 -3 -3 242.051 9.489 11 -7 -3 -3 235.781 9.330 2 -7 -3 -3 267.305 9.778 19 -7 3 -3 237.236 8.068 15 -7 3 -3 250.067 9.729 19 -7 3 -3 251.901 9.255 13 -7 3 -3 239.099 9.360 2 -7 3 -3 227.549 9.694 11 -7 3 -3 243.066 9.053 18 -7 3 -3 225.169 8.135 7 -8 -3 -3 346.886 13.034 4 -8 -3 -3 307.105 12.051 11 -8 -3 -3 317.300 11.386 13 -8 -3 -3 325.229 10.465 7 -8 -3 -3 323.172 13.068 6 -8 -3 -3 322.251 12.994 9 -8 -3 -3 306.930 12.300 19 -8 -3 -3 343.383 11.993 2 -8 3 -3 295.949 11.939 11 -8 3 -3 307.436 11.403 13 -8 3 -3 314.253 11.517 18 -8 3 -3 310.654 10.426 7 -8 3 -3 338.217 11.977 2 -8 3 -3 307.525 12.321 19 -8 3 -3 311.848 10.261 15 -9 -3 -3 26.0939 3.5726 13 -9 -3 -3 22.4083 2.4093 7 -9 -3 -3 21.3681 2.7628 2 -9 -3 -3 27.4143 3.4597 4 -9 -3 -3 24.9520 3.3707 6 -9 -3 -3 25.5953 2.6107 19 -9 -3 -3 19.5687 3.8947 11 -9 -3 -3 23.0760 3.6486 9 -9 3 -3 22.8263 2.7555 2 -9 3 -3 21.9672 2.6488 18 -9 3 -3 22.4232 3.3882 13 -9 3 -3 22.1440 2.4356 7 -9 3 -3 22.2593 2.6584 19 -10 -3 -3 63.7206 5.6035 11 -10 -3 -3 72.4730 4.9919 6 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22.370 3 -7 4 3 409.962 15.312 19 -7 4 3 417.009 14.272 18 -7 4 3 415.085 12.978 15 -6 -4 3 423.711 15.748 2 -6 -4 3 454.840 14.603 13 -6 -4 3 438.638 21.881 10 -6 -4 3 461.248 23.346 8 -6 -4 3 463.610 15.559 11 6 -4 -3 443.831 19.326 1 -6 -4 3 451.440 20.026 1 6 -4 -3 433.112 18.395 14 -6 -4 3 435.635 19.453 12 -6 -4 3 436.767 16.786 4 -6 -4 3 468.086 16.613 9 6 4 -3 441.556 22.749 3 -6 4 3 427.249 23.514 20 -5 -4 3 684.277 22.986 11 5 -4 -3 700.064 27.292 1 5 -4 -3 681.596 25.773 14 -5 -4 3 680.677 29.674 10 -5 -4 3 649.620 25.128 4 -5 -4 3 663.255 27.640 1 -5 -4 3 704.854 21.783 13 -5 -4 3 711.019 24.750 9 -5 -4 3 660.211 23.709 2 -5 -4 3 701.382 26.627 12 -5 -4 3 716.630 31.431 8 5 4 -3 703.436 31.590 20 5 4 -3 709.205 31.581 3 -5 4 3 639.934 32.085 20 4 -4 -3 1001.30 38.04 1 4 -4 -3 1005.55 35.31 14 -4 -4 3 1000.20 31.15 13 -4 -4 3 1008.94 41.96 8 -4 -4 3 982.321 36.032 12 -4 -4 3 992.087 40.021 10 -4 -4 3 987.747 38.340 1 -4 4 3 1025.71 43.82 20 4 4 -3 934.744 42.846 3 4 4 -3 1029.91 43.28 20 -3 -4 3 1302.44 53.00 8 3 -4 -3 1272.73 45.15 14 3 -4 -3 1327.33 43.86 12 3 -4 -3 1293.64 49.03 1 -3 -4 3 1281.08 50.71 10 -3 -4 3 1320.26 45.65 12 -3 -4 3 1361.82 49.48 1 3 4 -3 1345.40 55.18 20 -3 4 3 1350.54 55.67 20 3 4 -3 1316.12 54.95 3 -3 4 3 1296.11 54.46 3 2 -4 -3 835.122 28.425 14 -2 -4 3 784.479 33.117 8 -2 -4 3 807.577 28.861 12 2 -4 -3 804.530 38.245 21 2 -4 -3 820.719 30.741 1 2 -4 -3 811.276 27.291 12 -2 -4 3 770.323 38.905 21 -2 -4 3 798.033 32.084 10 -2 -4 3 810.930 31.107 1 -2 4 3 812.583 35.495 20 -2 4 3 770.693 34.072 3 2 4 -3 824.043 39.761 21 2 4 -3 784.583 33.842 3 2 4 -3 756.151 27.412 14 2 4 -3 796.349 35.517 20 -1 -4 3 627.442 24.551 1 -1 -4 3 632.110 26.067 8 1 -4 -3 588.858 22.247 14 -1 -4 3 619.613 23.262 12 1 -4 -3 603.316 31.503 21 1 -4 -3 579.407 21.677 12 1 -4 -3 662.627 24.668 1 -1 -4 3 636.087 25.616 10 -1 -4 3 524.293 30.397 21 1 4 -3 637.537 32.329 21 -1 4 3 648.601 28.664 20 -1 4 3 637.120 31.734 21 -1 4 3 629.636 27.564 3 1 4 -3 633.133 22.475 14 1 4 -3 659.938 29.110 20 1 4 -3 611.986 26.142 3 0 -4 3 1096.26 41.28 1 0 -4 -3 1103.22 41.19 1 0 -4 3 1035.62 50.45 21 0 -4 -3 1014.61 50.86 21 0 -4 -3 1094.21 37.00 12 0 -4 3 1117.64 43.01 8 0 -4 3 1033.31 41.80 10 0 -4 -3 1063.58 37.08 14 0 -4 3 1128.30 38.08 12 0 4 3 1133.67 45.96 20 0 4 3 1119.79 42.84 8 0 4 -3 1068.74 37.95 14 0 4 3 1025.57 50.87 21 0 4 -3 1159.31 47.01 20 0 4 -3 1101.06 51.08 21 0 4 3 1142.58 46.90 3 -1 -4 -3 150.412 8.560 12 1 -4 3 170.316 8.807 8 -1 -4 -3 137.460 12.676 21 1 -4 3 170.122 9.499 1 1 -4 3 161.049 9.696 12 -1 -4 -3 184.989 9.333 1 -1 -4 -3 158.696 7.458 14 1 -4 3 153.684 13.098 21 1 -4 3 184.535 10.234 10 1 4 3 160.775 8.976 8 1 4 3 161.225 11.640 20 1 4 3 172.001 11.473 3 -1 4 -3 168.104 9.638 14 -1 4 -3 166.545 12.675 20 -1 4 -3 150.276 13.601 21 1 4 3 154.063 14.662 21 -2 -4 -3 64.8590 6.6430 1 2 -4 3 75.8806 7.8750 10 2 -4 3 83.5872 7.9093 12 2 -4 3 75.6516 7.0518 1 -2 -4 -3 74.4267 7.3333 10 -2 -4 -3 66.3003 6.8188 12 -2 -4 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2 -10 -4 -3 1.64007 2.81591 13 -10 -4 -3 2.94926 2.53735 6 -10 -4 -3 7.01113 3.29524 11 -10 4 -3 1.03740 1.87723 19 10 4 3 3.60472 3.17098 4 -10 4 -3 1.64064 1.96287 2 -10 4 -3 2.53585 2.42920 13 -10 4 -3 0.67395 1.85107 7 -10 4 -3 2.94684 1.88822 18 -11 -4 -3 14.4857 1.5819 19 -11 -4 -3 11.7968 2.0572 6 -11 -4 -3 7.73025 2.26322 9 -11 -4 -3 12.7403 1.4815 7 -11 4 -3 11.9243 1.6114 7 -11 4 -3 14.3493 1.7745 19 -11 4 -3 11.6694 1.5818 18 -12 -5 3 3.37638 1.80021 6 -11 -5 3 4.26543 2.15273 16 -11 -5 3 4.12524 2.48989 13 -11 -5 3 4.87857 2.44257 4 -11 -5 3 -0.6550 2.1311 6 -11 -5 3 4.62910 2.71458 11 -11 -5 3 4.91696 2.43038 9 -10 -5 3 38.8540 3.4509 13 -10 -5 3 35.1107 3.6930 6 -10 -5 3 37.2050 3.9708 16 -10 -5 3 32.5563 3.3880 9 -10 -5 3 37.4942 4.2162 4 -10 -5 3 38.8539 3.7028 11 -10 5 3 39.0182 3.2178 18 -10 5 3 42.0728 2.5455 5 -10 5 3 43.3363 2.9421 15 -9 -5 3 61.6465 4.9851 11 -9 -5 3 63.0949 4.7113 13 -9 -5 3 62.0972 4.8923 9 -9 -5 3 61.1878 4.4847 16 -9 -5 3 61.3222 3.8905 2 -9 -5 3 57.7244 4.5078 6 -9 -5 3 59.4248 4.8332 4 -9 5 3 71.5510 4.0734 19 -9 5 3 68.3048 4.0349 18 -9 5 3 72.4343 3.4731 15 -9 5 3 62.7622 3.2915 5 -8 -5 3 6.80568 2.83034 4 -8 -5 3 9.44662 2.35282 2 -8 -5 3 10.0268 3.1713 11 -8 -5 3 8.07378 2.41922 16 -8 -5 3 9.21722 2.74890 9 -8 -5 3 9.18122 2.42930 6 -8 -5 3 5.52361 2.92891 13 -8 5 3 7.94603 2.02691 15 -8 5 3 12.2355 2.0215 7 -8 5 3 8.72684 2.21793 18 -8 5 3 13.0599 1.7330 5 -8 5 3 11.4274 2.0895 19 -8 5 3 11.5075 2.4103 17 -7 -5 3 11.6170 2.5632 4 -7 -5 3 12.5602 2.3427 2 -7 -5 3 12.3401 2.5755 9 -7 -5 3 11.0936 2.3427 16 -7 -5 3 14.9736 2.3463 6 -7 -5 3 12.1066 2.7349 13 -7 -5 3 14.7721 2.8797 11 -7 5 3 13.7443 2.0628 19 -7 5 3 12.3064 2.3594 17 -7 5 3 13.9926 1.7393 5 -7 5 3 11.8460 2.1947 18 -7 5 3 11.3386 2.0348 15 -7 5 3 13.2144 1.9115 7 -6 -5 3 128.240 10.306 12 -6 -5 3 148.832 6.742 11 -6 -5 3 153.600 6.130 2 -6 -5 3 146.050 6.761 9 -6 -5 3 145.437 9.982 1 -6 -5 3 156.745 6.526 16 -6 -5 3 140.972 11.706 10 6 -5 -3 137.299 9.295 14 -6 -5 3 161.358 6.391 13 -6 -5 3 145.390 6.597 4 -6 -5 3 154.209 6.600 6 -6 5 3 128.329 13.165 20 -6 5 3 139.216 5.250 7 -6 5 3 144.103 5.659 17 6 5 -3 156.204 11.449 3 -6 5 3 145.089 5.324 15 -6 5 3 143.982 6.276 19 -6 5 3 149.384 5.630 5 -6 5 3 142.977 6.018 18 5 -5 -3 123.447 8.371 1 -5 -5 3 129.875 5.973 9 -5 -5 3 142.546 9.761 12 -5 -5 3 137.004 10.696 10 5 -5 -3 134.125 8.478 14 -5 -5 3 123.630 5.904 4 -5 -5 3 140.616 5.593 13 -5 -5 3 135.435 5.811 11 -5 -5 3 124.832 5.519 2 -5 -5 3 137.448 11.542 8 -5 -5 3 122.775 8.958 1 -5 5 3 116.661 5.197 2 -5 5 3 149.133 13.159 20 5 5 -3 116.003 9.845 3 5 5 -3 122.363 11.767 20 -4 -5 3 41.0872 3.4762 13 -4 -5 3 46.7916 3.6457 9 -4 -5 3 52.8028 3.4026 4 -4 -5 3 41.7360 6.2001 12 -4 -5 3 44.0563 6.6298 8 -4 -5 3 47.7395 6.7652 10 -4 -5 3 48.0300 5.7038 1 -4 -5 3 44.3661 3.0458 2 4 -5 -3 45.4596 5.7958 1 -4 -5 3 51.2300 3.7810 11 4 -5 -3 47.3454 5.4841 14 4 5 -3 47.0060 6.0802 3 -4 5 3 40.4124 8.1604 20 -4 5 3 44.5586 2.8137 2 4 5 -3 43.4547 7.8661 20 3 -5 -3 249.310 11.948 1 -3 -5 3 236.980 13.216 10 -3 -5 3 232.511 8.248 13 -3 -5 3 226.610 8.659 2 -3 -5 3 246.436 12.107 1 3 -5 -3 234.571 11.132 14 -3 -5 3 215.175 11.971 12 -3 -5 3 231.173 8.613 11 -3 -5 3 235.399 13.506 8 -3 5 3 233.147 15.716 20 3 5 -3 227.612 12.660 3 3 5 -3 226.767 15.362 20 -2 -5 3 1324.45 45.94 12 -2 -5 3 1330.89 50.82 10 2 -5 -3 1325.44 45.26 14 -2 -5 3 1328.46 52.37 8 -2 -5 3 1338.85 40.68 13 2 -5 -3 1221.38 49.27 1 -2 -5 3 1221.67 49.53 1 -2 5 3 1357.53 55.98 20 2 5 -3 1297.88 54.25 3 2 5 -3 1328.34 56.04 20 -1 -5 3 2120.71 89.97 1 -1 -5 3 2033.48 75.24 10 1 -5 -3 1970.09 66.58 12 -1 -5 3 2015.09 68.04 12 1 -5 -3 2046.59 67.31 14 1 -5 -3 1988.37 74.09 1 1 5 -3 2014.97 67.33 14 -1 5 3 1982.72 82.26 3 -1 5 3 1843.49 81.69 20 1 5 -3 2039.34 82.76 20 0 -5 3 424.113 18.057 12 0 -5 -3 446.226 18.987 1 0 -5 3 415.847 19.019 1 0 -5 3 438.954 19.523 10 0 -5 -3 420.363 16.612 14 0 -5 -3 434.655 16.950 12 0 5 3 453.626 21.971 3 0 5 -3 452.327 23.153 20 0 5 3 470.573 22.581 20 0 5 -3 457.500 17.966 14 -1 -5 -3 529.478 19.709 12 1 -5 3 504.047 21.479 1 -1 -5 -3 476.823 17.684 2 1 -5 3 516.210 21.896 10 1 -5 3 488.839 20.252 12 -1 -5 -3 498.055 21.388 1 -1 -5 -3 519.186 18.543 14 1 -5 3 471.254 16.281 13 1 5 3 537.888 24.701 20 -1 5 -3 517.311 25.823 20 -1 5 -3 487.796 17.683 2 1 5 3 546.974 24.636 3 -1 5 -3 529.429 20.527 14 2 -5 3 116.118 8.100 1 2 -5 3 107.408 5.291 13 -2 -5 -3 117.185 8.348 1 -2 -5 -3 114.800 4.874 2 -2 -5 -3 116.115 8.116 12 2 -5 3 113.696 8.874 10 2 -5 3 116.621 8.526 12 2 5 3 102.167 10.202 20 -2 5 -3 104.671 4.895 2 -2 5 -3 102.451 8.544 14 2 5 3 131.345 10.484 3 -2 5 -3 100.402 11.771 20 3 -5 3 38.2013 6.3977 12 -3 -5 -3 43.8316 3.1669 2 -3 -5 -3 39.7153 5.9075 12 3 -5 3 41.5280 5.8843 1 -3 -5 -3 48.2305 5.9496 1 3 -5 3 30.5884 5.7510 10 -3 -5 -3 42.8913 3.6348 4 -3 -5 -3 34.6928 3.1478 13 -3 5 -3 36.3387 3.6219 13 -3 5 -3 43.1487 2.8879 2 -3 5 -3 36.7043 8.4508 20 3 5 3 41.8547 6.6008 3 -3 5 -3 46.0261 6.6190 14 -4 -5 -3 35.8462 6.1471 12 4 -5 3 34.2454 6.0705 1 -4 -5 -3 36.3915 3.2800 2 -4 -5 -3 34.6955 3.1355 13 -4 -5 -3 34.5529 4.0828 4 -4 -5 -3 44.7908 3.9635 9 -4 -5 -3 32.1161 5.8526 1 4 -5 3 24.3606 6.5100 12 4 5 3 59.3952 6.4268 8 -4 5 -3 34.5893 2.8981 13 4 5 3 42.0522 6.6540 3 -4 5 -3 25.2073 7.2821 20 -4 5 -3 31.4828 6.3971 14 -4 5 -3 35.6220 3.2627 2 5 -5 3 64.7027 8.6813 12 -5 -5 -3 78.5249 5.0114 16 -5 -5 -3 92.8389 5.2415 6 -5 -5 -3 85.0285 5.1800 9 -5 -5 -3 86.7946 4.3670 7 -5 -5 -3 80.1860 4.3697 13 -5 -5 -3 88.4761 5.4113 4 -5 -5 -3 85.4395 4.8465 11 -5 -5 -3 99.3854 9.5105 12 -5 -5 -3 79.8654 4.4943 2 -5 -5 -3 81.3180 4.8160 19 -5 5 -3 79.2056 4.5958 18 -5 5 -3 75.3386 4.1161 15 -5 5 -3 77.2334 3.9339 5 -5 5 -3 73.3597 4.8909 13 5 5 3 101.421 9.619 3 -5 5 -3 73.7146 4.7781 19 -5 5 -3 76.1626 4.5173 2 -5 5 -3 76.6053 3.8808 7 -6 -5 -3 261.704 9.825 19 -6 -5 -3 246.668 9.520 11 -6 -5 -3 259.429 10.353 4 -6 -5 -3 242.756 8.342 7 -6 -5 -3 233.006 9.998 16 -6 -5 -3 248.504 9.737 2 -6 -5 -3 246.324 10.184 9 -6 -5 -3 252.050 9.044 13 -6 -5 -3 249.564 10.445 6 -6 5 -3 237.061 9.087 13 -6 5 -3 239.433 9.849 19 -6 5 -3 233.192 8.505 5 -6 5 -3 246.294 8.317 15 -6 5 -3 223.560 9.152 18 -6 5 -3 238.818 9.511 2 -6 5 -3 232.824 8.372 7 -7 -5 -3 35.6100 3.4800 7 -7 -5 -3 31.8809 3.6436 9 -7 -5 -3 53.0242 4.6907 4 -7 -5 -3 31.3748 3.7714 11 -7 -5 -3 32.5631 3.5210 6 -7 -5 -3 38.3121 3.8516 2 -7 -5 -3 30.2187 3.4525 13 -7 -5 -3 34.9757 3.8727 19 -7 5 -3 37.6964 3.8739 18 -7 5 -3 35.0432 3.4523 15 -7 5 -3 37.8005 2.7576 5 -7 5 -3 35.9820 4.2386 19 -7 5 -3 31.5895 2.7770 7 -7 5 -3 32.3362 3.5304 13 -7 5 -3 37.4474 3.9939 2 -8 -5 -3 32.7219 3.6683 9 -8 -5 -3 32.0010 3.5181 6 -8 -5 -3 34.1279 3.4684 13 -8 -5 -3 39.3152 3.8535 11 -8 -5 -3 35.3796 3.8665 19 -8 -5 -3 33.5649 3.7989 2 -8 -5 -3 34.8866 3.3429 7 -8 5 -3 34.2441 3.7337 2 -8 5 -3 32.9628 3.3558 13 8 5 3 37.8914 3.7555 16 -8 5 -3 37.3745 3.2735 15 -8 5 -3 35.7333 3.4275 7 -8 5 -3 33.4789 3.6936 18 -8 5 -3 38.5655 3.9211 19 -9 -5 -3 17.0635 3.1242 13 -9 -5 -3 13.2246 2.3752 2 -9 -5 -3 18.4786 2.2145 7 -9 -5 -3 17.9537 3.1977 9 -9 -5 -3 13.2432 2.8759 6 -9 -5 -3 14.6804 2.3016 19 -9 -5 -3 21.3520 3.4532 11 9 5 3 17.4278 3.1015 16 9 5 3 14.5508 3.6588 4 -9 5 -3 18.1504 2.1058 15 -9 5 -3 11.4442 2.2262 18 -9 5 -3 14.4300 2.3397 19 -9 5 -3 15.0124 2.3240 2 -9 5 -3 17.3915 2.2054 7 -9 5 -3 21.0018 2.6567 13 -10 -5 -3 104.605 4.579 2 -10 -5 -3 97.5707 5.1550 6 -10 -5 -3 98.5208 4.6412 19 -10 -5 -3 111.954 5.509 11 -10 -5 -3 104.315 4.007 7 -10 -5 -3 102.100 5.324 9 -10 -5 -3 101.810 4.961 13 -10 5 -3 96.1182 3.7939 15 -10 5 -3 101.111 4.115 7 -10 5 -3 92.1481 4.7247 19 -10 5 -3 94.3877 4.3553 18 10 5 3 100.681 5.860 4 -10 5 -3 102.061 4.482 2 -11 -5 -3 106.726 4.579 6 -11 5 -3 99.8338 3.6386 7 -11 5 -3 97.4782 4.3536 19 -11 -6 3 72.6385 4.0226 13 -11 -6 3 68.9688 3.8726 16 -11 -6 3 74.2320 4.2102 11 -11 -6 3 72.4153 3.9802 9 -11 -6 3 58.9216 4.1018 4 -11 -6 3 61.8634 3.8930 6 -11 6 3 70.7485 3.1644 18 -11 6 3 69.4977 2.8472 15 -10 -6 3 19.7987 2.5262 6 -10 -6 3 19.6148 2.8966 13 -10 -6 3 20.4966 2.6564 16 -10 -6 3 22.1989 3.1218 11 -10 -6 3 22.7014 2.8768 4 -10 -6 3 22.2441 2.7896 9 -10 6 3 24.6811 2.1210 5 -10 6 3 21.3445 2.1116 18 -10 6 3 25.0969 2.5030 15 -9 -6 3 82.9190 5.2512 16 -9 -6 3 94.9922 5.5035 4 -9 -6 3 89.2348 5.1104 6 -9 -6 3 93.0163 5.3491 11 -9 -6 3 90.8856 5.1127 13 -9 -6 3 90.5898 5.3548 9 -9 6 3 93.3030 3.9964 15 -9 6 3 93.7903 3.9821 5 -9 6 3 87.5611 4.5510 19 -9 6 3 89.3132 4.2351 17 -9 6 3 89.3565 3.8585 7 -9 6 3 92.8520 4.6091 18 -8 -6 3 133.389 6.338 13 -8 -6 3 128.615 6.507 16 -8 -6 3 130.116 6.773 11 -8 -6 3 140.371 6.445 6 -8 -6 3 131.621 6.595 9 -8 -6 3 139.133 6.148 2 -8 -6 3 134.287 6.662 4 -8 6 3 130.207 5.496 17 -8 6 3 129.371 6.020 19 -8 6 3 134.351 5.046 7 -8 6 3 133.541 5.846 18 -8 6 3 139.479 5.314 5 -8 6 3 127.913 5.171 15 -7 -6 3 5.14631 2.65146 4 -7 -6 3 6.75383 2.27653 6 -7 -6 3 4.17399 2.22060 2 -7 -6 3 4.98174 2.90027 11 -7 -6 3 1.89547 2.41254 16 -7 -6 3 3.65322 2.85532 13 -7 -6 3 5.90913 2.47972 9 -7 6 3 3.40252 2.43410 17 -7 6 3 4.66171 1.94135 7 -7 6 3 4.37028 1.99990 19 -7 6 3 1.91040 2.01552 15 -7 6 3 5.46904 1.65707 5 -7 6 3 2.80579 2.18032 18 -6 -6 3 58.9616 3.9204 2 -6 -6 3 55.6544 4.6339 11 -6 -6 3 50.6166 4.3709 16 -6 -6 3 60.6423 4.3145 13 -6 -6 3 58.0584 4.2857 4 -6 -6 3 66.7704 4.0137 6 -6 -6 3 57.8286 4.2848 9 -6 6 3 60.2081 3.4487 5 -6 6 3 53.0118 3.1440 7 -6 6 3 56.6005 3.9195 19 -6 6 3 56.4044 4.0754 17 -6 6 3 56.5139 3.4742 15 -6 6 3 50.0336 3.9269 18 -6 6 3 62.8250 3.4919 2 -5 -6 3 27.9907 2.8742 13 -5 -6 3 24.5347 2.5195 2 -5 -6 3 23.0551 5.3280 1 -5 -6 3 27.0954 2.7860 4 -5 -6 3 27.9916 6.2992 10 -5 -6 3 26.5517 2.8856 11 -5 -6 3 31.9776 3.5057 16 -5 6 3 27.1985 2.6316 17 -5 6 3 26.5046 2.5142 7 -5 6 3 26.5504 3.0687 19 -5 6 3 27.6423 2.8439 15 -5 6 3 29.6479 3.2919 18 -5 6 3 27.1676 2.6300 5 -4 -6 3 287.448 9.701 13 4 -6 -3 275.032 13.459 14 4 -6 -3 287.296 13.967 1 -4 -6 3 261.882 14.428 12 -4 -6 3 282.876 10.264 2 4 -6 -3 264.725 10.111 2 -4 -6 3 278.934 10.162 11 -4 -6 3 266.380 14.281 1 -4 -6 3 281.533 15.757 10 -4 6 3 255.106 18.439 20 -4 6 3 281.210 9.844 18 -4 6 3 280.168 8.888 15 -4 6 3 283.457 9.366 17 -4 6 3 265.229 9.374 5 4 6 -3 269.262 18.421 20 3 -6 -3 231.755 11.460 14 -3 -6 3 221.657 8.602 2 3 -6 -3 217.883 8.512 2 3 -6 -3 238.337 12.300 1 -3 -6 3 224.702 8.574 11 -3 -6 3 229.195 12.797 12 -3 -6 3 225.997 8.234 13 -3 -6 3 228.633 12.641 1 -3 -6 3 231.283 13.524 10 -3 6 3 227.612 16.538 20 3 6 -3 235.367 16.789 20 -2 -6 3 142.284 10.132 10 2 -6 -3 143.592 5.972 2 2 -6 -3 155.509 8.695 14 -2 -6 3 138.938 9.944 12 -2 -6 3 147.850 9.417 1 -2 -6 3 149.930 6.081 2 -2 -6 3 144.739 6.178 11 2 -6 -3 149.177 9.465 1 -2 -6 3 149.500 5.990 13 -2 6 3 146.348 13.287 20 2 6 -3 140.295 13.418 20 1 -6 -3 225.096 12.158 1 1 -6 -3 232.180 10.802 14 1 -6 -3 224.432 8.623 2 -1 -6 3 241.028 8.442 13 -1 -6 3 228.788 8.703 2 -1 -6 3 232.732 12.404 1 -1 -6 3 228.411 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4 533.801 23.582 8 -5 -2 -4 494.037 16.965 11 5 -2 4 509.978 20.406 12 -5 -2 -4 525.729 22.265 1 -5 2 -4 477.361 17.413 2 5 2 4 499.970 24.656 3 -5 2 -4 473.533 18.057 9 -5 2 -4 484.166 20.876 14 5 2 4 501.097 23.568 8 -5 2 -4 478.303 16.967 11 -5 2 -4 504.616 16.165 13 5 2 4 503.243 22.307 10 6 -2 4 33.6637 6.9872 10 -6 -2 -4 30.6754 3.0341 6 -6 -2 -4 27.6223 2.3300 7 -6 -2 -4 28.6088 5.7845 1 -6 -2 -4 34.3290 3.8172 19 -6 -2 -4 29.2598 3.0826 4 6 -2 4 30.9890 5.4301 1 -6 -2 -4 29.2527 3.4208 11 6 -2 4 30.1649 6.5684 8 -6 -2 -4 30.0671 2.9406 13 -6 -2 -4 20.8735 6.6625 12 -6 -2 -4 27.7523 3.2064 2 6 -2 4 30.1474 5.9463 12 -6 -2 -4 30.9222 3.3071 9 -6 2 -4 30.6115 3.2631 2 6 2 4 39.8454 5.9022 10 -6 2 -4 38.1204 3.2611 13 -6 2 -4 32.8546 3.4838 11 6 2 4 42.1212 6.4922 8 -6 2 -4 37.8108 3.7355 19 -6 2 -4 32.2301 2.7920 7 -6 2 -4 32.3205 6.3310 14 6 2 4 57.3804 7.8506 3 -6 2 -4 35.0706 3.0669 9 -6 2 -4 33.2084 3.8148 18 -7 -2 -4 23.6442 3.6806 11 -7 -2 -4 25.4597 3.3701 13 -7 -2 -4 29.5009 2.8297 18 -7 -2 -4 26.8070 2.7889 2 -7 -2 -4 30.5742 3.1287 7 -7 -2 -4 31.0965 2.8238 19 -7 -2 -4 26.8695 3.3328 6 -7 -2 -4 35.5428 4.2809 4 -7 -2 -4 27.5898 3.6328 9 -7 2 -4 33.5799 3.5269 13 -7 2 -4 32.5956 2.7923 19 -7 2 -4 37.3506 4.2583 18 -7 2 -4 35.2094 3.0403 15 -7 2 -4 34.6872 3.5650 2 -7 2 -4 31.9924 3.3057 9 -7 2 -4 38.5191 4.0794 11 -7 2 -4 32.8101 3.1097 7 -8 -2 -4 314.542 12.996 9 -8 -2 -4 324.110 11.518 13 -8 -2 -4 320.876 12.216 11 -8 -2 -4 320.644 13.123 6 -8 -2 -4 324.375 12.329 19 -8 -2 -4 305.927 10.445 7 -8 -2 -4 319.636 12.769 4 -8 -2 -4 327.254 12.011 2 -8 -2 -4 319.773 11.374 18 -8 2 -4 315.682 11.928 2 -8 2 -4 315.940 12.206 11 -8 2 -4 321.790 11.567 18 -8 2 -4 316.979 12.405 19 -8 2 -4 315.579 10.445 7 -8 2 -4 317.321 11.533 13 -9 -2 -4 83.5040 6.0175 9 -9 -2 -4 79.7077 4.9744 19 -9 -2 -4 84.2094 4.2324 7 -9 -2 -4 79.5571 5.4864 13 -9 -2 -4 89.0704 5.6537 6 -9 -2 -4 72.9932 6.1805 11 -9 -2 -4 92.4310 4.7127 2 -9 2 -4 85.7858 4.2334 7 9 2 4 99.2239 6.1802 4 -9 2 -4 78.1974 5.8292 11 -9 2 -4 86.2798 5.5422 13 -9 2 -4 79.5582 4.7478 18 -9 2 -4 86.1029 4.8538 2 -9 2 -4 76.7898 4.8529 19 -10 -2 -4 107.016 5.520 6 -10 -2 -4 102.380 4.291 7 -10 -2 -4 98.8915 5.7678 9 -10 -2 -4 101.789 5.115 19 -10 -2 -4 90.6168 5.5385 13 -10 -2 -4 94.5371 5.9253 11 -10 -2 -4 99.8329 4.9083 2 -10 2 -4 99.8028 4.6338 18 -10 2 -4 100.182 5.442 13 10 2 4 92.8251 6.0060 4 -10 2 -4 102.688 5.575 11 -10 2 -4 92.0953 4.8781 19 -10 2 -4 102.691 4.338 7 -10 2 -4 99.5080 4.9424 2 -11 -2 -4 34.9037 3.3378 11 -11 -2 -4 39.0933 3.8204 13 -11 -2 -4 40.6257 3.2875 6 -11 -2 -4 35.0646 2.7590 19 -11 -2 -4 36.7046 2.5167 7 -11 -2 -4 39.7334 2.8775 2 -11 2 -4 38.9330 2.8517 2 -11 2 -4 39.8457 2.5694 7 -11 2 -4 32.4046 2.8160 13 -11 2 -4 33.6817 2.4787 18 -11 2 -4 37.3963 2.8942 19 -13 -3 4 49.0729 3.1269 6 -12 -3 4 27.2005 3.2588 6 -12 -3 4 39.9144 3.9374 11 -12 -3 4 30.8235 3.0378 16 -12 -3 4 34.2835 3.5224 4 -12 -3 4 32.1247 3.5312 9 -11 -3 4 8.50034 2.15770 16 -11 -3 4 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4 584.847 24.319 10 -2 3 -4 592.208 27.857 20 -2 3 -4 640.384 23.843 14 2 3 4 625.046 26.328 8 2 3 4 597.060 28.307 3 3 -3 4 203.248 11.964 8 -3 -3 -4 185.759 10.598 12 -3 -3 -4 194.159 10.699 1 3 -3 4 207.862 10.801 1 3 -3 4 203.206 12.446 10 3 -3 4 179.190 10.917 12 3 3 4 198.848 12.733 3 -3 3 -4 179.035 12.336 20 3 3 4 186.767 10.314 10 -3 3 -4 192.882 11.246 14 3 3 4 187.730 11.595 8 4 -3 4 445.243 19.647 1 4 -3 4 469.623 18.968 12 -4 -3 -4 446.806 15.296 11 4 -3 4 443.347 20.959 8 -4 -3 -4 453.628 16.555 9 -4 -3 -4 436.908 16.774 4 -4 -3 -4 458.295 14.480 13 -4 -3 -4 442.980 15.803 2 4 -3 4 454.396 20.901 10 -4 -3 -4 472.798 18.942 12 -4 -3 -4 408.890 19.885 1 4 3 4 456.018 22.571 3 4 3 4 436.883 21.193 8 -4 3 -4 418.607 19.298 14 -4 3 -4 447.121 14.583 13 -4 3 -4 444.828 15.286 11 4 3 4 443.229 19.799 10 -4 3 -4 441.259 15.792 2 -5 -3 -4 490.886 18.372 4 -5 -3 -4 479.768 15.809 13 -5 -3 -4 482.873 17.221 2 5 -3 4 496.076 21.843 1 5 -3 4 484.467 22.918 10 -5 -3 -4 495.942 22.238 1 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364.097 15.919 14 -6 -4 4 370.333 13.710 9 -6 -4 4 334.166 13.780 4 -6 -4 4 393.835 20.414 8 -6 -4 4 342.053 18.699 10 -6 -4 4 359.028 16.764 1 -6 -4 4 350.462 16.920 12 6 4 -4 364.009 20.155 20 6 4 -4 344.365 19.204 3 -6 4 4 362.988 20.658 20 -5 -4 4 27.9824 5.7343 10 -5 -4 4 23.2065 2.5679 13 -5 -4 4 24.3650 2.3402 4 -5 -4 4 26.0196 2.4856 9 -5 -4 4 24.0673 5.7762 8 -5 -4 4 30.1363 4.5513 1 5 -4 -4 25.4577 4.6752 14 5 -4 -4 23.7448 4.1267 1 -5 -4 4 24.3497 2.7129 11 -5 -4 4 22.2208 5.3026 12 5 4 -4 22.4352 6.6628 20 5 4 -4 29.2762 5.2694 3 -5 4 4 26.0843 6.9188 20 -4 -4 4 455.449 15.067 13 -4 -4 4 492.460 22.647 8 -4 -4 4 470.439 19.273 12 -4 -4 4 455.455 19.600 1 -4 -4 4 482.478 21.566 10 4 -4 -4 472.870 19.217 1 4 -4 -4 451.681 18.461 14 -4 -4 4 461.034 16.041 11 -4 4 4 483.792 24.075 20 4 4 -4 447.644 22.048 3 4 4 -4 471.964 23.669 20 -3 -4 4 2791.79 129.94 8 3 -4 -4 2846.56 106.85 14 -3 -4 4 2926.19 120.85 1 -3 -4 4 2709.42 105.07 10 3 -4 -4 2695.62 115.17 1 -3 -4 4 2706.39 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14 0 -2 5 125.605 7.649 12 0 -2 -5 112.303 11.828 21 0 -2 5 120.289 6.682 1 0 -2 5 116.392 10.744 21 0 -2 5 107.997 7.817 3 0 -2 -5 114.072 6.094 12 0 -2 5 123.946 8.977 10 0 -2 -5 116.116 6.495 1 0 2 5 117.456 8.936 8 0 2 -5 108.236 7.938 14 0 2 5 117.487 7.525 10 0 2 -5 110.690 9.399 20 0 2 -5 111.441 11.759 21 0 2 5 110.383 8.507 20 0 2 5 116.359 9.571 3 0 2 5 114.415 11.864 21 -1 -2 -5 46.6080 4.9309 14 1 -2 5 41.3709 5.2625 12 1 -2 5 39.0114 7.7151 21 1 -2 5 38.7392 4.6273 3 1 -2 5 35.6678 4.2275 1 1 -2 5 43.2304 5.8949 8 -1 -2 -5 32.6715 8.2341 21 -1 -2 -5 41.4790 4.9436 1 -1 -2 -5 41.3100 4.5131 12 1 -2 5 50.0786 6.1348 10 1 2 5 35.6491 4.2529 10 1 2 5 36.8880 8.4093 21 1 2 5 35.5464 6.8104 3 -1 2 -5 41.2536 5.5757 14 1 2 5 34.9749 5.7641 8 -1 2 -5 40.6291 6.1593 20 -1 2 -5 48.3681 8.5475 21 2 -2 5 676.572 28.419 10 -2 -2 -5 672.472 27.055 1 2 -2 5 685.856 25.259 12 -2 -2 -5 740.151 24.913 14 2 -2 5 656.668 29.277 8 2 -2 5 692.542 29.421 3 -2 -2 -5 671.900 24.805 12 2 -2 5 672.181 26.866 1 2 2 5 676.546 31.285 3 -2 2 -5 667.264 29.284 20 -2 2 -5 690.783 25.923 14 2 2 5 670.947 27.200 10 -2 2 -5 691.430 34.541 21 2 2 5 692.938 29.424 8 3 -2 5 747.498 30.764 10 -3 -2 -5 778.580 29.727 1 -3 -2 -5 726.114 27.423 12 3 -2 5 723.680 27.161 12 3 -2 5 714.787 31.798 8 -3 -2 -5 732.493 26.500 14 3 -2 5 724.587 29.184 1 -3 2 -5 739.732 28.106 14 3 2 5 715.794 33.480 3 3 2 5 712.532 31.576 8 3 2 5 767.323 29.886 10 -4 -2 -5 79.4563 4.6554 4 4 -2 5 91.0823 7.7960 12 -4 -2 -5 77.9915 5.3546 9 -4 -2 -5 79.3920 4.2223 13 4 -2 5 90.0309 9.5863 10 4 -2 5 78.2584 9.9976 8 -4 -2 -5 85.8955 7.6889 1 -4 -2 -5 82.5088 8.7637 12 -4 -2 -5 85.1526 5.0373 11 -4 -2 -5 76.6742 4.1893 2 4 -2 5 78.2058 7.1459 1 -4 2 -5 79.3774 3.9644 2 4 2 5 78.9305 8.9272 3 4 2 5 97.5564 8.7268 8 -4 2 -5 91.6770 4.6375 13 4 2 5 87.2305 7.6464 10 -4 2 -5 83.8018 8.0982 14 -4 2 -5 90.1511 5.4187 11 -5 -2 -5 626.564 21.952 2 5 -2 5 621.688 28.370 10 -5 -2 -5 657.756 21.338 11 5 -2 5 643.263 24.994 12 5 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20 -6 3 5 319.245 17.539 3 6 3 -5 325.295 18.900 20 6 3 -5 310.502 17.455 3 -5 -3 5 233.949 9.763 4 -5 -3 5 243.844 8.455 13 -5 -3 5 235.706 11.285 1 -5 -3 5 238.262 14.950 8 -5 -3 5 250.293 9.150 11 -5 -3 5 248.775 12.268 12 -5 -3 5 243.210 9.781 9 5 -3 -5 252.326 11.538 14 -5 -3 5 255.035 14.025 10 -5 -3 5 244.790 15.155 3 5 3 -5 264.847 16.013 20 -5 3 5 257.828 15.663 20 -5 3 5 251.053 14.174 3 4 -3 -5 1013.64 37.57 1 -4 -3 5 985.677 44.166 3 -4 -3 5 1031.00 42.62 8 -4 -3 5 1008.08 35.97 12 -4 -3 5 969.994 40.329 10 4 -3 -5 1000.29 35.57 14 -4 -3 5 1034.17 38.05 1 4 3 -5 964.564 43.788 20 -4 3 5 1027.78 43.99 20 -4 3 5 1059.11 43.97 3 3 -3 -5 104.086 7.171 14 -3 -3 5 95.1906 8.5877 3 3 -3 -5 103.743 6.289 1 -3 -3 5 104.333 9.683 8 -3 -3 5 108.685 7.949 12 -3 -3 5 100.481 8.748 10 -3 -3 5 94.1938 6.3534 1 -3 3 5 109.444 9.377 3 -3 3 5 107.982 6.992 8 3 3 -5 117.406 11.214 20 -3 3 5 133.452 10.707 20 3 3 -5 109.484 6.705 14 2 -3 -5 797.237 27.924 14 -2 -3 5 791.960 31.696 10 -2 -3 5 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217.912 11.201 12 -3 -3 -5 194.269 7.740 2 3 -3 5 206.587 11.211 1 -3 3 -5 202.955 12.561 20 3 3 5 196.679 13.039 3 -3 3 -5 196.141 7.836 11 -3 3 -5 194.832 7.745 2 3 3 5 200.054 12.240 8 -3 3 -5 209.172 7.518 13 3 3 5 198.253 11.005 10 -3 3 -5 207.546 11.771 14 4 -3 5 184.791 13.457 8 4 -3 5 235.178 12.280 1 -4 -3 -5 239.071 8.990 4 -4 -3 -5 231.972 12.626 12 4 -3 5 212.817 13.824 10 -4 -3 -5 205.877 7.777 13 -4 -3 -5 217.164 8.429 2 -4 -3 -5 227.381 9.273 9 -4 -3 -5 213.546 8.423 11 -4 -3 -5 236.935 12.731 1 4 -3 5 211.483 12.617 12 -4 3 -5 225.221 8.061 13 -4 3 -5 219.983 8.584 11 4 3 5 239.432 14.684 3 4 3 5 207.434 13.150 8 -4 3 -5 196.602 12.459 14 4 3 5 211.847 12.069 10 -4 3 -5 214.306 8.383 2 -5 -3 -5 92.4536 4.8418 2 5 -3 5 91.9077 8.3285 1 -5 -3 -5 92.5717 4.3155 7 -5 -3 -5 95.6286 8.8206 1 5 -3 5 75.2665 9.3280 10 -5 -3 -5 82.0861 9.3025 12 -5 -3 -5 89.9514 5.8498 9 -5 -3 -5 93.2837 5.8579 6 -5 -3 -5 103.919 5.333 4 -5 -3 -5 91.8081 5.2009 11 -5 -3 -5 91.1842 4.8270 13 -5 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