# Electronic Supplementary Material (ESI) for Chemical Communications # This journal is © The Royal Society of Chemistry 2013 ####################################################################### # # Cambridge Crystallographic Data Centre # CCDC # ####################################################################### # # This CIF contains data from an original supplementary publication # deposited with the CCDC, and may include chemical, crystal, # experimental, refinement, atomic coordinates, # anisotropic displacement parameters and molecular geometry data, # as required by the journal to which it was submitted. # # This CIF is provided on the understanding that it is used for bona # fide research purposes only. It may contain copyright material # of the CCDC or of third parties, and may not be copied or further # disseminated in any form, whether machine-readable or not, # except for the purpose of generating routine backup copies # on your local computer system. # # For further information on the CCDC, data deposition and # data retrieval see: # www.ccdc.cam.ac.uk # # Bona fide researchers may freely download Mercury and enCIFer # from this site to visualise CIF-encoded structures and # to carry out CIF format checking respectively. # data_sad_a _audit_creation_method SHELXL-2013 _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C28 H38 Cl2 N2 Si' _chemical_formula_sum 'C28 H38 Cl2 N2 Si' _chemical_formula_weight 501.59 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 9.431(2) _cell_length_b 9.553(2) _cell_length_c 17.281(3) _cell_angle_alpha 89.69(2) _cell_angle_beta 85.15(3) _cell_angle_gamma 63.15(2) _cell_volume 1383.3(2) _cell_formula_units_Z 2 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 9001 _cell_measurement_theta_min 2.52 _cell_measurement_theta_max 26.375 _exptl_crystal_description plate _exptl_crystal_colour colourless _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.204 _exptl_crystal_F_000 536 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.1 _exptl_crystal_size_mid 0.1 _exptl_crystal_size_min 0.05 _exptl_absorpt_coefficient_mu 0.297 _shelx_estimated_absorpt_T_min ? _shelx_estimated_absorpt_T_max ? _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.7110 _exptl_absorpt_correction_T_max 0.7454 _exptl_absorpt_process_details SADABS-2012/1 _exptl_special_details ; ? ; _diffrn_ambient_temperature 100(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source 'INCOATEC Mo Microsource' _diffrn_measurement_device_type 'Smart APEX II Ultra' _diffrn_measurement_method 'omega scans' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 21444 _diffrn_reflns_av_unetI/netI 0.0212 _diffrn_reflns_av_R_equivalents 0.0232 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_l_min -20 _diffrn_reflns_limit_l_max 20 _diffrn_reflns_theta_min 1.183 _diffrn_reflns_theta_max 25.350 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measured_fraction_theta_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.999 _diffrn_reflns_point_group_measured_fraction_full 0.999 _reflns_number_total 5061 _reflns_number_gt 4509 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection ? _computing_cell_refinement 'SAINT V8.30C' _computing_data_reduction 'SAINT V8.30C' _computing_structure_solution 'SHELXS-2012 (Sheldrick, 2012)' _computing_structure_refinement 'SHELXL-2013 (Sheldrick, 2013)' _computing_molecular_graphics 'XP Version 5.1' _computing_publication_material 'XSHELL in SHELXTL-97' _refine_special_details ; ? ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0319P)^2^+1.1636P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens mixed _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 5061 _refine_ls_number_parameters 310 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0400 _refine_ls_R_factor_gt 0.0345 _refine_ls_wR_factor_ref 0.0860 _refine_ls_wR_factor_gt 0.0819 _refine_ls_goodness_of_fit_ref 1.053 _refine_ls_restrained_S_all 1.053 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cl1 Cl 1.25722(5) -0.14342(5) 0.25874(3) 0.02312(12) Uani 1 1 d . . . . . Si1 Si 1.02905(5) 0.03192(5) 0.29354(3) 0.01528(12) Uani 1 1 d . . . . . N1 N 0.68305(16) -0.01531(16) 0.17858(8) 0.0142(3) Uani 1 1 d . . . . . C1 C 0.89878(19) 0.0259(2) 0.22658(10) 0.0160(3) Uani 1 1 d . . . . . H1 H 0.9356 0.0263 0.1737 0.019 Uiso 1 1 calc R U . . . Cl2 Cl 1.06518(6) 0.23139(5) 0.29175(3) 0.02892(13) Uani 1 1 d . . . . . H2 H 1.003(2) 0.016(2) 0.3708(11) 0.019(5) Uiso 1 1 d . . . . . N2 N 0.65203(16) 0.04637(16) 0.30207(8) 0.0137(3) Uani 1 1 d . . . . . C2 C 0.75455(19) 0.02069(18) 0.23646(9) 0.0133(3) Uani 1 1 d . . . . . C3 C 0.5401(2) -0.0131(2) 0.20894(10) 0.0173(4) Uani 1 1 d . . . . . H3 H 0.4693 -0.0344 0.1808 0.021 Uiso 1 1 calc R U . . . C4 C 0.52111(19) 0.0243(2) 0.28479(10) 0.0170(4) Uani 1 1 d . . . . . H4 H 0.4345 0.0342 0.3205 0.020 Uiso 1 1 calc R U . . . C1A C 0.7564(2) -0.0662(2) 0.10073(9) 0.0154(3) Uani 1 1 d . . . . . C2A C 0.8789(2) -0.2200(2) 0.08861(10) 0.0183(4) Uani 1 1 d . . . . . C1B C 0.67661(19) 0.09031(19) 0.37727(9) 0.0140(3) Uani 1 1 d . . . . . C3A C 0.9485(2) -0.2666(2) 0.01296(11) 0.0237(4) Uani 1 1 d . . . . . H3A H 1.0327 -0.3696 0.0027 0.028 Uiso 1 1 calc R U . . . C2B C 0.64475(19) 0.24742(19) 0.39066(10) 0.0154(3) Uani 1 1 d . . . . . C4A C 0.8973(2) -0.1655(2) -0.04754(11) 0.0266(4) Uani 1 1 d . . . . . H4A H 0.9462 -0.1998 -0.0988 0.032 Uiso 1 1 calc R U . . . C3B C 0.6772(2) 0.2860(2) 0.46253(10) 0.0197(4) Uani 1 1 d . . . . . H3B H 0.6592 0.3904 0.4733 0.024 Uiso 1 1 calc R U . . . C5A C 0.7751(2) -0.0145(2) -0.03399(11) 0.0240(4) Uani 1 1 d . . . . . H5A H 0.7411 0.0536 -0.0761 0.029 Uiso 1 1 calc R U . . . C4B C 0.7353(2) 0.1745(2) 0.51846(10) 0.0214(4) Uani 1 1 d . . . . . H4B H 0.7568 0.2033 0.5670 0.026 Uiso 1 1 calc R U . . . C6A C 0.7014(2) 0.0387(2) 0.04078(10) 0.0177(4) Uani 1 1 d . . . . . C5B C 0.7622(2) 0.0216(2) 0.50434(10) 0.0202(4) Uani 1 1 d . . . . . H5B H 0.8006 -0.0530 0.5436 0.024 Uiso 1 1 calc R U . . . C7A C 0.5696(2) 0.2057(2) 0.05741(10) 0.0205(4) Uani 1 1 d . . . . . H7A H 0.4977 0.2027 0.1027 0.025 Uiso 1 1 calc R U . . . C6B C 0.73382(19) -0.0245(2) 0.43303(10) 0.0160(3) Uani 1 1 d . . . . . C8A C 0.4677(2) 0.2715(2) -0.01044(12) 0.0282(4) Uani 1 1 d . . . . . H8AA H 0.3801 0.3753 0.0048 0.042 Uiso 1 1 calc R U . . . H8AB H 0.4238 0.2007 -0.0245 0.042 Uiso 1 1 calc R U . . . H8AC H 0.5338 0.2808 -0.0551 0.042 Uiso 1 1 calc R U . . . C7B C 0.7706(2) -0.1954(2) 0.41665(10) 0.0189(4) Uani 1 1 d . . . . . H7B H 0.7067 -0.1968 0.3736 0.023 Uiso 1 1 calc R U . . . C9A C 0.6399(3) 0.3135(2) 0.08113(13) 0.0329(5) Uani 1 1 d . . . . . H9AA H 0.7033 0.2699 0.1252 0.049 Uiso 1 1 calc R U . . . H9AB H 0.5532 0.4179 0.0961 0.049 Uiso 1 1 calc R U . . . H9AC H 0.7082 0.3219 0.0373 0.049 Uiso 1 1 calc R U . . . C8B C 0.9469(2) -0.2949(2) 0.38921(13) 0.0318(5) Uani 1 1 d . . . . . H8BA H 1.0126 -0.2962 0.4305 0.048 Uiso 1 1 calc R U . . . H8BB H 0.9749 -0.2498 0.3428 0.048 Uiso 1 1 calc R U . . . H8BC H 0.9664 -0.4023 0.3767 0.048 Uiso 1 1 calc R U . . . C10A C 0.9276(2) -0.3338(2) 0.15457(10) 0.0227(4) Uani 1 1 d . . . . . H10A H 0.9039 -0.2702 0.2040 0.027 Uiso 1 1 calc R U . . . C9B C 0.7229(2) -0.2676(2) 0.48686(12) 0.0283(4) Uani 1 1 d . . . . . H9BA H 0.6103 -0.2019 0.5045 0.042 Uiso 1 1 calc R U . . . H9BB H 0.7890 -0.2743 0.5289 0.042 Uiso 1 1 calc R U . . . H9BC H 0.7390 -0.3731 0.4723 0.042 Uiso 1 1 calc R U . . . C11A C 0.8263(2) -0.4218(2) 0.16065(12) 0.0275(4) Uani 1 1 d . . . . . H11A H 0.7135 -0.3465 0.1710 0.041 Uiso 1 1 calc R U . . . H11B H 0.8586 -0.4950 0.2031 0.041 Uiso 1 1 calc R U . . . H11C H 0.8420 -0.4804 0.1117 0.041 Uiso 1 1 calc R U . . . C10B C 0.5729(2) 0.3702(2) 0.33012(10) 0.0193(4) Uani 1 1 d . . . . . H10B H 0.6201 0.3188 0.2777 0.023 Uiso 1 1 calc R U . . . C12A C 1.1060(2) -0.4489(2) 0.14736(13) 0.0324(5) Uani 1 1 d . . . . . H12A H 1.1328 -0.5086 0.1948 0.049 Uiso 1 1 calc R U . . . H12B H 1.1685 -0.3904 0.1401 0.049 Uiso 1 1 calc R U . . . H12C H 1.1307 -0.5213 0.1026 0.049 Uiso 1 1 calc R U . . . C12B C 0.6086(2) 0.5103(2) 0.33827(11) 0.0231(4) Uani 1 1 d . . . . . H12D H 0.7239 0.4726 0.3387 0.035 Uiso 1 1 calc R U . . . H12E H 0.5541 0.5693 0.3870 0.035 Uiso 1 1 calc R U . . . H12F H 0.5705 0.5788 0.2944 0.035 Uiso 1 1 calc R U . . . C11B C 0.3915(2) 0.4284(2) 0.33374(12) 0.0267(4) Uani 1 1 d . . . . . H11D H 0.3424 0.4776 0.3851 0.040 Uiso 1 1 calc R U . . . H11E H 0.3692 0.3394 0.3248 0.040 Uiso 1 1 calc R U . . . H11F H 0.3473 0.5054 0.2937 0.040 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cl1 0.0133(2) 0.0218(2) 0.0308(3) 0.00267(18) -0.00344(17) -0.00475(17) Si1 0.0127(2) 0.0169(2) 0.0170(2) 0.00209(18) -0.00438(18) -0.00686(19) N1 0.0137(7) 0.0172(7) 0.0117(7) -0.0015(6) -0.0017(5) -0.0069(6) C1 0.0157(8) 0.0207(9) 0.0119(8) 0.0015(7) -0.0016(6) -0.0086(7) Cl2 0.0269(2) 0.0199(2) 0.0454(3) 0.0056(2) -0.0141(2) -0.01354(19) N2 0.0123(7) 0.0170(7) 0.0119(7) -0.0002(5) -0.0015(5) -0.0065(6) C2 0.0140(8) 0.0113(8) 0.0131(8) 0.0010(6) -0.0031(6) -0.0041(6) C3 0.0142(8) 0.0208(9) 0.0188(9) 0.0013(7) -0.0041(7) -0.0093(7) C4 0.0116(8) 0.0220(9) 0.0184(9) -0.0003(7) -0.0012(6) -0.0085(7) C1A 0.0168(8) 0.0199(9) 0.0116(8) -0.0018(7) -0.0014(6) -0.0102(7) C2A 0.0197(9) 0.0192(9) 0.0169(9) -0.0006(7) -0.0032(7) -0.0093(7) C1B 0.0116(8) 0.0184(8) 0.0112(8) -0.0035(6) 0.0010(6) -0.0063(7) C3A 0.0249(10) 0.0209(9) 0.0207(9) -0.0041(7) 0.0005(7) -0.0067(8) C2B 0.0134(8) 0.0166(8) 0.0139(8) -0.0005(7) 0.0003(6) -0.0049(7) C4A 0.0334(11) 0.0289(10) 0.0147(9) -0.0035(8) 0.0046(8) -0.0127(9) C3B 0.0222(9) 0.0169(9) 0.0190(9) -0.0032(7) -0.0015(7) -0.0081(7) C5A 0.0312(10) 0.0261(10) 0.0160(9) 0.0050(7) -0.0031(8) -0.0141(8) C4B 0.0250(9) 0.0253(10) 0.0145(9) -0.0016(7) -0.0048(7) -0.0114(8) C6A 0.0197(9) 0.0195(9) 0.0167(9) 0.0012(7) -0.0038(7) -0.0111(7) C5B 0.0228(9) 0.0209(9) 0.0162(9) 0.0039(7) -0.0048(7) -0.0090(8) C7A 0.0222(9) 0.0197(9) 0.0191(9) 0.0030(7) -0.0040(7) -0.0088(8) C6B 0.0135(8) 0.0190(9) 0.0156(9) -0.0001(7) -0.0004(6) -0.0074(7) C8A 0.0269(10) 0.0261(10) 0.0300(11) 0.0065(8) -0.0114(8) -0.0092(8) C7B 0.0216(9) 0.0174(9) 0.0185(9) 0.0014(7) -0.0040(7) -0.0092(7) C9A 0.0363(11) 0.0210(10) 0.0417(12) 0.0018(9) -0.0146(10) -0.0114(9) C8B 0.0284(11) 0.0199(10) 0.0430(13) -0.0034(9) 0.0086(9) -0.0092(8) C10A 0.0274(10) 0.0173(9) 0.0165(9) -0.0016(7) -0.0036(7) -0.0038(8) C9B 0.0361(11) 0.0242(10) 0.0287(11) 0.0008(8) 0.0023(9) -0.0181(9) C11A 0.0256(10) 0.0246(10) 0.0246(10) 0.0071(8) 0.0016(8) -0.0056(8) C10B 0.0217(9) 0.0167(9) 0.0150(9) 0.0003(7) -0.0019(7) -0.0048(7) C12A 0.0273(11) 0.0275(11) 0.0397(12) 0.0075(9) -0.0136(9) -0.0083(9) C12B 0.0207(9) 0.0197(9) 0.0254(10) 0.0050(7) -0.0012(7) -0.0062(7) C11B 0.0239(10) 0.0219(10) 0.0338(11) 0.0068(8) -0.0123(8) -0.0083(8) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cl1 Si1 2.0820(6) . ? Si1 C1 1.7768(17) . ? Si1 Cl2 2.0815(7) . ? Si1 H2 1.358(19) . ? N1 C2 1.379(2) . ? N1 C3 1.396(2) . ? N1 C1A 1.439(2) . ? C1 C2 1.380(2) . ? C1 H1 0.9500 . ? N2 C2 1.373(2) . ? N2 C4 1.398(2) . ? N2 C1B 1.436(2) . ? C3 C4 1.336(2) . ? C3 H3 0.9500 . ? C4 H4 0.9500 . ? C1A C6A 1.399(2) . ? C1A C2A 1.402(2) . ? C2A C3A 1.391(3) . ? C2A C10A 1.522(2) . ? C1B C6B 1.402(2) . ? C1B C2B 1.408(2) . ? C3A C4A 1.383(3) . ? C3A H3A 0.9500 . ? C2B C3B 1.394(2) . ? C2B C10B 1.523(2) . ? C4A C5A 1.385(3) . ? C4A H4A 0.9500 . ? C3B C4B 1.386(3) . ? C3B H3B 0.9500 . ? C5A C6A 1.396(3) . ? C5A H5A 0.9500 . ? C4B C5B 1.384(3) . ? C4B H4B 0.9500 . ? C6A C7A 1.526(2) . ? C5B C6B 1.397(2) . ? C5B H5B 0.9500 . ? C7A C8A 1.526(2) . ? C7A C9A 1.528(3) . ? C7A H7A 1.0000 . ? C6B C7B 1.530(2) . ? C8A H8AA 0.9800 . ? C8A H8AB 0.9800 . ? C8A H8AC 0.9800 . ? C7B C9B 1.526(3) . ? C7B C8B 1.529(3) . ? C7B H7B 1.0000 . ? C9A H9AA 0.9800 . ? C9A H9AB 0.9800 . ? C9A H9AC 0.9800 . ? C8B H8BA 0.9800 . ? C8B H8BB 0.9800 . ? C8B H8BC 0.9800 . ? C10A C11A 1.529(3) . ? C10A C12A 1.533(3) . ? C10A H10A 1.0000 . ? C9B H9BA 0.9800 . ? C9B H9BB 0.9800 . ? C9B H9BC 0.9800 . ? C11A H11A 0.9800 . ? C11A H11B 0.9800 . ? C11A H11C 0.9800 . ? C10B C12B 1.530(2) . ? C10B C11B 1.537(2) . ? C10B H10B 1.0000 . ? C12A H12A 0.9800 . ? C12A H12B 0.9800 . ? C12A H12C 0.9800 . ? C12B H12D 0.9800 . ? C12B H12E 0.9800 . ? C12B H12F 0.9800 . ? C11B H11D 0.9800 . ? C11B H11E 0.9800 . ? C11B H11F 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C1 Si1 Cl2 115.66(6) . . ? C1 Si1 Cl1 107.55(6) . . ? Cl2 Si1 Cl1 101.65(3) . . ? C1 Si1 H2 121.3(8) . . ? Cl2 Si1 H2 102.2(8) . . ? Cl1 Si1 H2 106.5(8) . . ? C2 N1 C3 110.15(13) . . ? C2 N1 C1A 124.03(14) . . ? C3 N1 C1A 125.41(13) . . ? C2 C1 Si1 132.47(13) . . ? C2 C1 H1 113.8 . . ? Si1 C1 H1 113.8 . . ? C2 N2 C4 110.20(13) . . ? C2 N2 C1B 124.44(13) . . ? C4 N2 C1B 125.36(14) . . ? N2 C2 N1 104.61(13) . . ? N2 C2 C1 130.23(15) . . ? N1 C2 C1 125.15(15) . . ? C4 C3 N1 107.52(14) . . ? C4 C3 H3 126.2 . . ? N1 C3 H3 126.2 . . ? C3 C4 N2 107.50(15) . . ? C3 C4 H4 126.2 . . ? N2 C4 H4 126.2 . . ? C6A C1A C2A 123.13(15) . . ? C6A C1A N1 118.78(15) . . ? C2A C1A N1 118.08(15) . . ? C3A C2A C1A 117.16(16) . . ? C3A C2A C10A 121.33(16) . . ? C1A C2A C10A 121.43(15) . . ? C6B C1B C2B 123.15(15) . . ? C6B C1B N2 119.02(14) . . ? C2B C1B N2 117.82(14) . . ? C4A C3A C2A 121.08(17) . . ? C4A C3A H3A 119.5 . . ? C2A C3A H3A 119.5 . . ? C3B C2B C1B 117.01(15) . . ? C3B C2B C10B 121.76(15) . . ? C1B C2B C10B 121.20(15) . . ? C3A C4A C5A 120.53(17) . . ? C3A C4A H4A 119.7 . . ? C5A C4A H4A 119.7 . . ? C4B C3B C2B 121.04(16) . . ? C4B C3B H3B 119.5 . . ? C2B C3B H3B 119.5 . . ? C4A C5A C6A 120.82(17) . . ? C4A C5A H5A 119.6 . . ? C6A C5A H5A 119.6 . . ? C5B C4B C3B 120.71(16) . . ? C5B C4B H4B 119.6 . . ? C3B C4B H4B 119.6 . . ? C5A C6A C1A 117.27(16) . . ? C5A C6A C7A 121.73(16) . . ? C1A C6A C7A 120.98(15) . . ? C4B C5B C6B 120.84(16) . . ? C4B C5B H5B 119.6 . . ? C6B C5B H5B 119.6 . . ? C6A C7A C8A 112.89(15) . . ? C6A C7A C9A 110.44(15) . . ? C8A C7A C9A 110.92(16) . . ? C6A C7A H7A 107.4 . . ? C8A C7A H7A 107.4 . . ? C9A C7A H7A 107.4 . . ? C5B C6B C1B 117.23(15) . . ? C5B C6B C7B 120.50(15) . . ? C1B C6B C7B 122.23(15) . . ? C7A C8A H8AA 109.5 . . ? C7A C8A H8AB 109.5 . . ? H8AA C8A H8AB 109.5 . . ? C7A C8A H8AC 109.5 . . ? H8AA C8A H8AC 109.5 . . ? H8AB C8A H8AC 109.5 . . ? C9B C7B C8B 110.25(15) . . ? C9B C7B C6B 112.33(15) . . ? C8B C7B C6B 111.02(14) . . ? C9B C7B H7B 107.7 . . ? C8B C7B H7B 107.7 . . ? C6B C7B H7B 107.7 . . ? C7A C9A H9AA 109.5 . . ? C7A C9A H9AB 109.5 . . ? H9AA C9A H9AB 109.5 . . ? C7A C9A H9AC 109.5 . . ? H9AA C9A H9AC 109.5 . . ? H9AB C9A H9AC 109.5 . . ? C7B C8B H8BA 109.5 . . ? C7B C8B H8BB 109.5 . . ? H8BA C8B H8BB 109.5 . . ? C7B C8B H8BC 109.5 . . ? H8BA C8B H8BC 109.5 . . ? H8BB C8B H8BC 109.5 . . ? C2A C10A C11A 110.00(15) . . ? C2A C10A C12A 113.33(16) . . ? C11A C10A C12A 110.86(16) . . ? C2A C10A H10A 107.5 . . ? C11A C10A H10A 107.5 . . ? C12A C10A H10A 107.5 . . ? C7B C9B H9BA 109.5 . . ? C7B C9B H9BB 109.5 . . ? H9BA C9B H9BB 109.5 . . ? C7B C9B H9BC 109.5 . . ? H9BA C9B H9BC 109.5 . . ? H9BB C9B H9BC 109.5 . . ? C10A C11A H11A 109.5 . . ? C10A C11A H11B 109.5 . . ? H11A C11A H11B 109.5 . . ? C10A C11A H11C 109.5 . . ? H11A C11A H11C 109.5 . . ? H11B C11A H11C 109.5 . . ? C2B C10B C12B 113.23(14) . . ? C2B C10B C11B 110.36(15) . . ? C12B C10B C11B 109.62(14) . . ? C2B C10B H10B 107.8 . . ? C12B C10B H10B 107.8 . . ? C11B C10B H10B 107.8 . . ? C10A C12A H12A 109.5 . . ? C10A C12A H12B 109.5 . . ? H12A C12A H12B 109.5 . . ? C10A C12A H12C 109.5 . . ? H12A C12A H12C 109.5 . . ? H12B C12A H12C 109.5 . . ? C10B C12B H12D 109.5 . . ? C10B C12B H12E 109.5 . . ? H12D C12B H12E 109.5 . . ? C10B C12B H12F 109.5 . . ? H12D C12B H12F 109.5 . . ? H12E C12B H12F 109.5 . . ? C10B C11B H11D 109.5 . . ? C10B C11B H11E 109.5 . . ? H11D C11B H11E 109.5 . . ? C10B C11B H11F 109.5 . . ? H11D C11B H11F 109.5 . . ? H11E C11B H11F 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Cl2 Si1 C1 C2 -117.84(16) . . . . ? Cl1 Si1 C1 C2 129.41(16) . . . . ? C4 N2 C2 N1 0.78(17) . . . . ? C1B N2 C2 N1 -178.91(14) . . . . ? C4 N2 C2 C1 -178.53(17) . . . . ? C1B N2 C2 C1 1.8(3) . . . . ? C3 N1 C2 N2 -0.64(17) . . . . ? C1A N1 C2 N2 -173.66(14) . . . . ? C3 N1 C2 C1 178.73(16) . . . . ? C1A N1 C2 C1 5.7(3) . . . . ? Si1 C1 C2 N2 13.1(3) . . . . ? Si1 C1 C2 N1 -166.12(13) . . . . ? C2 N1 C3 C4 0.25(19) . . . . ? C1A N1 C3 C4 173.16(15) . . . . ? N1 C3 C4 N2 0.24(19) . . . . ? C2 N2 C4 C3 -0.66(19) . . . . ? C1B N2 C4 C3 179.04(15) . . . . ? C2 N1 C1A C6A -106.45(18) . . . . ? C3 N1 C1A C6A 81.6(2) . . . . ? C2 N1 C1A C2A 74.3(2) . . . . ? C3 N1 C1A C2A -97.7(2) . . . . ? C6A C1A C2A C3A 1.0(3) . . . . ? N1 C1A C2A C3A -179.80(15) . . . . ? C6A C1A C2A C10A -175.87(16) . . . . ? N1 C1A C2A C10A 3.4(2) . . . . ? C2 N2 C1B C6B -101.65(19) . . . . ? C4 N2 C1B C6B 78.7(2) . . . . ? C2 N2 C1B C2B 77.0(2) . . . . ? C4 N2 C1B C2B -102.60(19) . . . . ? C1A C2A C3A C4A -0.7(3) . . . . ? C10A C2A C3A C4A 176.16(17) . . . . ? C6B C1B C2B C3B 1.9(2) . . . . ? N2 C1B C2B C3B -176.74(14) . . . . ? C6B C1B C2B C10B -176.12(15) . . . . ? N2 C1B C2B C10B 5.2(2) . . . . ? C2A C3A C4A C5A 0.2(3) . . . . ? C1B C2B C3B C4B -1.2(2) . . . . ? C10B C2B C3B C4B 176.79(16) . . . . ? C3A C4A C5A C6A 0.0(3) . . . . ? C2B C3B C4B C5B -0.1(3) . . . . ? C4A C5A C6A C1A 0.2(3) . . . . ? C4A C5A C6A C7A 178.43(17) . . . . ? C2A C1A C6A C5A -0.7(3) . . . . ? N1 C1A C6A C5A -179.97(15) . . . . ? C2A C1A C6A C7A -178.96(16) . . . . ? N1 C1A C6A C7A 1.8(2) . . . . ? C3B C4B C5B C6B 0.9(3) . . . . ? C5A C6A C7A C8A 31.9(2) . . . . ? C1A C6A C7A C8A -149.91(17) . . . . ? C5A C6A C7A C9A -92.9(2) . . . . ? C1A C6A C7A C9A 85.3(2) . . . . ? C4B C5B C6B C1B -0.3(3) . . . . ? C4B C5B C6B C7B 177.42(16) . . . . ? C2B C1B C6B C5B -1.2(2) . . . . ? N2 C1B C6B C5B 177.47(15) . . . . ? C2B C1B C6B C7B -178.83(15) . . . . ? N2 C1B C6B C7B -0.2(2) . . . . ? C5B C6B C7B C9B 40.7(2) . . . . ? C1B C6B C7B C9B -141.66(17) . . . . ? C5B C6B C7B C8B -83.2(2) . . . . ? C1B C6B C7B C8B 94.38(19) . . . . ? C3A C2A C10A C11A -88.4(2) . . . . ? C1A C2A C10A C11A 88.3(2) . . . . ? C3A C2A C10A C12A 36.3(2) . . . . ? C1A C2A C10A C12A -146.96(17) . . . . ? C3B C2B C10B C12B 25.6(2) . . . . ? C1B C2B C10B C12B -156.51(15) . . . . ? C3B C2B C10B C11B -97.76(19) . . . . ? C1B C2B C10B C11B 80.18(19) . . . . ? _refine_diff_density_max 0.328 _refine_diff_density_min -0.232 _refine_diff_density_rms 0.048 _shelxl_version_number 2013-4 _shelx_res_file ; REM Solution 1 R1 0.120 Rweak 0.006, Alpha = 0.1163 in P-1 REM Formula: C28 N2 Si Cl2 TITL sad in P-1 CELL 0.71073 9.4313 9.5533 17.2813 89.689 85.151 63.154 ZERR 2.0 0.0009 0.0009 0.0016 0.002 0.002 0.002 LATT 1 SFAC C H N SI CL UNIT 56 76 4 2 4 TEMP -173.000 shel 999 0.83 L.S. 10 LIST 4 bond $H acta conf FMAP 2 PLAN 20 WGHT 0.031900 1.163600 FVAR 0.61206 CL1 5 1.257218 -0.143422 0.258743 11.00000 0.01326 0.02184 = 0.03085 0.00267 -0.00344 -0.00475 SI1 4 1.029049 0.031917 0.293538 11.00000 0.01268 0.01690 = 0.01699 0.00209 -0.00438 -0.00686 N1 3 0.683054 -0.015307 0.178584 11.00000 0.01371 0.01724 = 0.01171 -0.00146 -0.00168 -0.00690 C1 1 0.898777 0.025873 0.226581 11.00000 0.01569 0.02074 = 0.01190 0.00153 -0.00158 -0.00862 AFIX 43 H1 2 0.935577 0.026293 0.173723 11.00000 -1.20000 AFIX 0 CL2 5 1.065175 0.231391 0.291753 11.00000 0.02688 0.01988 = 0.04537 0.00559 -0.01411 -0.01354 H2 2 1.002616 0.016151 0.370819 11.00000 0.01940 N2 3 0.652034 0.046367 0.302074 11.00000 0.01230 0.01697 = 0.01186 -0.00016 -0.00154 -0.00651 C2 1 0.754547 0.020688 0.236458 11.00000 0.01398 0.01129 = 0.01314 0.00096 -0.00306 -0.00415 C3 1 0.540137 -0.013108 0.208945 11.00000 0.01416 0.02084 = 0.01883 0.00129 -0.00411 -0.00932 AFIX 43 H3 2 0.469290 -0.034365 0.180818 11.00000 -1.20000 AFIX 0 C4 1 0.521113 0.024348 0.284791 11.00000 0.01159 0.02205 = 0.01840 -0.00033 -0.00115 -0.00850 AFIX 43 H4 2 0.434469 0.034217 0.320460 11.00000 -1.20000 AFIX 0 C1A 1 0.756377 -0.066158 0.100731 11.00000 0.01684 0.01988 = 0.01160 -0.00183 -0.00142 -0.01020 C2A 1 0.878904 -0.219957 0.088613 11.00000 0.01971 0.01915 = 0.01687 -0.00060 -0.00322 -0.00926 C1B 1 0.676612 0.090309 0.377273 11.00000 0.01157 0.01835 = 0.01124 -0.00349 0.00099 -0.00630 C3A 1 0.948550 -0.266612 0.012959 11.00000 0.02493 0.02093 = 0.02066 -0.00407 0.00047 -0.00672 AFIX 43 H3A 2 1.032694 -0.369628 0.002690 11.00000 -1.20000 AFIX 0 C2B 1 0.644750 0.247424 0.390657 11.00000 0.01336 0.01657 = 0.01392 -0.00050 0.00031 -0.00491 C4A 1 0.897274 -0.165452 -0.047544 11.00000 0.03336 0.02886 = 0.01466 -0.00355 0.00463 -0.01273 AFIX 43 H4A 2 0.946217 -0.199769 -0.098800 11.00000 -1.20000 AFIX 0 C3B 1 0.677208 0.286017 0.462530 11.00000 0.02221 0.01694 = 0.01899 -0.00320 -0.00155 -0.00807 AFIX 43 H3B 2 0.659242 0.390424 0.473340 11.00000 -1.20000 AFIX 0 C5A 1 0.775127 -0.014505 -0.033994 11.00000 0.03123 0.02610 = 0.01601 0.00501 -0.00313 -0.01406 AFIX 43 H5A 2 0.741129 0.053641 -0.076124 11.00000 -1.20000 AFIX 0 C4B 1 0.735271 0.174477 0.518458 11.00000 0.02497 0.02529 = 0.01447 -0.00157 -0.00477 -0.01141 AFIX 43 H4B 2 0.756790 0.203275 0.567007 11.00000 -1.20000 AFIX 0 C6A 1 0.701399 0.038693 0.040783 11.00000 0.01971 0.01946 = 0.01675 0.00120 -0.00379 -0.01109 C5B 1 0.762241 0.021579 0.504337 11.00000 0.02284 0.02093 = 0.01624 0.00391 -0.00477 -0.00903 AFIX 43 H5B 2 0.800566 -0.052972 0.543621 11.00000 -1.20000 AFIX 0 C7A 1 0.569551 0.205735 0.057413 11.00000 0.02215 0.01970 = 0.01913 0.00298 -0.00395 -0.00879 AFIX 13 H7A 2 0.497676 0.202702 0.102674 11.00000 -1.20000 AFIX 0 C6B 1 0.733815 -0.024531 0.433029 11.00000 0.01349 0.01899 = 0.01557 -0.00013 -0.00038 -0.00743 C8A 1 0.467696 0.271522 -0.010442 11.00000 0.02689 0.02609 = 0.03004 0.00646 -0.01142 -0.00924 AFIX 137 H8AA 2 0.380132 0.375275 0.004774 11.00000 -1.50000 H8AB 2 0.423785 0.200710 -0.024542 11.00000 -1.50000 H8AC 2 0.533777 0.280819 -0.055123 11.00000 -1.50000 AFIX 0 C7B 1 0.770575 -0.195359 0.416652 11.00000 0.02155 0.01741 = 0.01852 0.00138 -0.00403 -0.00918 AFIX 13 H7B 2 0.706709 -0.196757 0.373587 11.00000 -1.20000 AFIX 0 C9A 1 0.639853 0.313515 0.081126 11.00000 0.03626 0.02101 = 0.04172 0.00177 -0.01455 -0.01145 AFIX 137 H9AA 2 0.703254 0.269857 0.125217 11.00000 -1.50000 H9AB 2 0.553178 0.417891 0.096114 11.00000 -1.50000 H9AC 2 0.708216 0.321923 0.037256 11.00000 -1.50000 AFIX 0 C8B 1 0.946942 -0.294863 0.389212 11.00000 0.02841 0.01988 = 0.04296 -0.00343 0.00865 -0.00921 AFIX 137 H8BA 2 1.012553 -0.296231 0.430538 11.00000 -1.50000 H8BB 2 0.974922 -0.249789 0.342840 11.00000 -1.50000 H8BC 2 0.966371 -0.402333 0.376676 11.00000 -1.50000 AFIX 0 REM ##### C10A 1 0.927632 -0.333791 0.154570 11.00000 0.02741 0.01730 = 0.01654 -0.00160 -0.00360 -0.00377 AFIX 13 H10A 2 0.903898 -0.270195 0.204021 11.00000 -1.20000 AFIX 0 C9B 1 0.722948 -0.267639 0.486864 11.00000 0.03606 0.02417 = 0.02871 0.00085 0.00229 -0.01806 AFIX 137 H9BA 2 0.610304 -0.201880 0.504455 11.00000 -1.50000 H9BB 2 0.788956 -0.274323 0.528938 11.00000 -1.50000 H9BC 2 0.739005 -0.373122 0.472280 11.00000 -1.50000 AFIX 0 C11A 1 0.826330 -0.421822 0.160646 11.00000 0.02565 0.02464 = 0.02465 0.00713 0.00158 -0.00559 AFIX 137 H11A 2 0.713469 -0.346459 0.171000 11.00000 -1.50000 H11B 2 0.858604 -0.494974 0.203140 11.00000 -1.50000 H11C 2 0.842001 -0.480442 0.111692 11.00000 -1.50000 AFIX 0 C10B 1 0.572897 0.370224 0.330119 11.00000 0.02170 0.01669 = 0.01497 0.00034 -0.00190 -0.00480 AFIX 13 H10B 2 0.620139 0.318802 0.277679 11.00000 -1.20000 AFIX 0 C12A 1 1.106004 -0.448927 0.147363 11.00000 0.02727 0.02755 = 0.03970 0.00749 -0.01355 -0.00832 AFIX 137 H12A 2 1.132782 -0.508641 0.194778 11.00000 -1.50000 H12B 2 1.168523 -0.390410 0.140088 11.00000 -1.50000 H12C 2 1.130733 -0.521330 0.102617 11.00000 -1.50000 AFIX 0 C12B 1 0.608552 0.510306 0.338267 11.00000 0.02067 0.01975 = 0.02538 0.00501 -0.00123 -0.00623 AFIX 137 H12D 2 0.723891 0.472553 0.338688 11.00000 -1.50000 H12E 2 0.554062 0.569335 0.386957 11.00000 -1.50000 H12F 2 0.570543 0.578766 0.294375 11.00000 -1.50000 AFIX 0 C11B 1 0.391483 0.428418 0.333745 11.00000 0.02386 0.02190 = 0.03380 0.00681 -0.01228 -0.00830 AFIX 137 H11D 2 0.342362 0.477593 0.385066 11.00000 -1.50000 H11E 2 0.369183 0.339367 0.324801 11.00000 -1.50000 H11F 2 0.347263 0.505391 0.293678 11.00000 -1.50000 REM ##### REM ##### AFIX 0 HKLF 4 REM sad in P-1 REM R1 = 0.0345 for 4509 Fo > 4sig(Fo) and 0.0400 for all 5061 data REM 310 parameters refined using 0 restraints END WGHT 0.0319 1.1636 REM Highest difference peak 0.328, deepest hole -0.232, 1-sigma level 0.048 Q1 1 1.1192 0.2043 0.2272 11.00000 0.05 0.33 Q2 1 0.9588 0.0066 0.2651 11.00000 0.05 0.32 Q3 1 0.7440 -0.1021 0.4266 11.00000 0.05 0.30 Q4 1 0.5971 0.3166 0.3644 11.00000 0.05 0.30 Q5 1 1.0696 0.1258 0.2941 11.00000 0.05 0.30 Q6 1 0.6323 0.1101 0.0522 11.00000 0.05 0.26 Q7 1 0.6584 0.0739 0.3395 11.00000 0.05 0.26 Q8 1 0.7143 -0.0423 0.1349 11.00000 0.05 0.26 Q9 1 0.9960 0.0927 0.3871 11.00000 0.05 0.25 Q10 1 0.7201 0.0173 0.2758 11.00000 0.05 0.25 Q11 1 0.6766 0.0359 0.4072 11.00000 0.05 0.24 Q12 1 0.5864 0.4393 0.3438 11.00000 0.05 0.23 Q13 1 0.7456 -0.2172 0.4497 11.00000 0.05 0.23 Q14 1 0.9134 -0.2766 0.1225 11.00000 0.05 0.23 Q15 1 0.7195 0.0040 0.2060 11.00000 0.05 0.23 Q16 1 0.6344 0.2769 0.4271 11.00000 0.05 0.23 Q17 1 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1.40 1 7 0 3.20 1.50 1 7 0 3.90 1.30 -2 -7 0 73.99 6.10 -2 -7 0 68.69 5.30 -2 -7 0 73.89 3.50 -2 -7 0 73.89 3.50 2 7 0 75.19 4.10 2 7 0 66.19 4.20 2 7 0 82.39 4.90 -3 -7 0 0.00 0.90 -3 -7 0 -1.20 1.40 -3 -7 0 -0.80 1.10 -3 -7 0 0.00 0.90 3 7 0 1.10 1.20 3 7 0 -0.30 0.80 3 7 0 -0.70 1.00 3 7 0 0.30 1.20 3 7 0 -0.30 0.80 -4 -7 0 367.76 11.40 -4 -7 0 344.67 12.00 -4 -7 0 341.67 11.80 4 7 0 351.76 10.30 4 7 0 353.46 7.40 4 7 0 344.37 10.90 4 7 0 353.46 7.40 -5 -7 0 9.50 2.20 -5 -7 0 4.00 1.90 -5 -7 0 6.40 2.20 5 7 0 1.90 1.80 5 7 0 6.70 1.30 5 7 0 6.70 1.30 -6 -7 0 50.19 3.50 -6 -7 0 45.40 5.20 -6 -7 0 50.69 4.10 6 7 0 39.00 4.70 6 7 0 46.40 2.80 6 7 0 46.40 2.80 -7 -7 0 15.00 3.30 7 7 0 8.50 1.70 7 7 0 8.50 1.70 7 7 0 13.80 3.10 -8 -7 0 3.30 2.10 8 7 0 6.90 1.70 8 7 0 6.90 1.70 8 7 0 7.60 2.60 -9 -7 0 32.40 5.00 9 7 0 28.30 3.10 9 7 0 28.30 3.10 9 7 0 30.90 4.90 -10 -7 0 196.88 12.20 -10 -7 0 204.18 10.80 10 7 0 205.58 7.10 10 7 0 205.58 7.10 10 7 0 195.98 10.40 -11 -7 0 -0.20 2.30 -11 -7 0 -2.30 2.50 11 7 0 -4.10 1.20 11 7 0 -4.10 1.20 11 7 0 -2.70 1.60 4 -8 0 3.30 2.30 4 -8 0 3.80 3.00 4 -8 0 3.30 2.30 -4 8 0 7.00 3.00 -4 8 0 2.90 2.30 3 -8 0 52.19 5.00 3 -8 0 36.20 6.40 3 -8 0 52.19 5.00 -3 8 0 35.60 5.50 -3 8 0 37.60 4.90 2 -8 0 2.70 1.70 2 -8 0 2.70 1.70 2 -8 0 1.60 2.60 -2 8 0 2.80 2.10 -2 8 0 -0.30 1.80 1 -8 0 57.49 4.20 1 -8 0 57.49 4.20 1 -8 0 63.99 7.50 -1 8 0 71.99 5.90 -1 8 0 66.09 5.10 0 -8 0 38.60 5.60 0 -8 0 41.00 3.80 0 -8 0 41.00 3.80 0 8 0 48.40 4.30 0 8 0 45.50 5.30 -1 -8 0 60.79 3.80 -1 -8 0 59.69 5.90 -1 -8 0 60.79 3.80 1 8 0 55.69 4.90 1 8 0 57.19 4.30 -2 -8 0 15.50 2.50 -2 -8 0 15.50 2.50 -2 -8 0 17.70 4.40 -2 -8 0 23.70 4.10 2 8 0 20.60 2.80 2 8 0 19.50 2.90 2 8 0 12.70 3.00 -3 -8 0 32.70 3.00 -3 -8 0 33.20 5.10 -3 -8 0 32.30 4.70 -3 -8 0 32.70 3.00 3 8 0 29.20 3.70 3 8 0 30.90 3.70 3 8 0 34.50 3.30 -4 -8 0 146.79 7.30 -4 -8 0 136.29 5.40 -4 -8 0 154.88 8.40 -4 -8 0 136.29 5.40 4 8 0 156.38 6.80 4 8 0 153.28 4.80 4 8 0 153.28 4.80 4 8 0 159.78 7.20 -5 -8 0 4.60 2.40 -5 -8 0 2.70 1.80 -5 -8 0 6.00 2.60 5 8 0 4.80 1.30 5 8 0 5.20 1.90 5 8 0 5.40 2.10 5 8 0 4.80 1.30 -6 -8 0 76.69 4.90 -6 -8 0 76.09 6.00 -6 -8 0 70.39 5.50 6 8 0 76.79 3.60 6 8 0 81.29 5.90 6 8 0 76.79 3.60 -7 -8 0 259.87 11.10 7 8 0 262.47 6.90 7 8 0 262.47 6.90 7 8 0 246.18 10.70 -8 -8 0 100.29 7.30 8 8 0 105.59 7.20 8 8 0 111.19 4.60 8 8 0 111.19 4.60 -9 -8 0 29.80 5.10 9 8 0 27.20 3.20 9 8 0 32.50 5.30 9 8 0 27.20 3.20 -10 -8 0 190.68 10.50 -10 -8 0 174.68 11.80 10 8 0 185.88 10.20 10 8 0 181.18 6.70 10 8 0 181.18 6.70 -11 -8 0 87.39 9.00 -11 -8 0 95.69 7.90 11 8 0 91.49 7.60 11 8 0 70.99 4.80 11 8 0 70.99 4.80 2 -9 0 11.90 2.90 2 -9 0 14.70 4.80 2 -9 0 11.90 2.90 -2 9 0 15.50 4.10 -2 9 0 11.80 3.00 1 -9 0 2.20 3.20 1 -9 0 1.50 1.80 1 -9 0 1.50 1.80 -1 9 0 1.30 2.20 -1 9 0 1.20 1.80 0 -9 0 5.00 3.30 0 -9 0 6.00 3.70 0 -9 0 5.50 2.00 0 -9 0 5.50 2.00 0 9 0 6.10 2.20 0 9 0 6.80 2.70 -1 -9 0 117.79 5.40 -1 -9 0 132.59 10.10 -1 -9 0 117.79 5.40 -1 -9 0 129.49 9.00 1 9 0 115.49 7.40 1 9 0 122.39 6.70 -2 -9 0 28.00 5.60 -2 -9 0 27.70 3.20 -2 -9 0 26.20 4.80 -2 -9 0 27.70 3.20 2 9 0 26.30 3.50 2 9 0 30.70 4.20 -3 -9 0 241.28 12.30 -3 -9 0 242.98 7.40 -3 -9 0 242.98 7.40 -3 -9 0 243.58 11.20 3 9 0 246.88 9.40 3 9 0 239.08 8.80 3 9 0 242.28 9.90 -4 -9 0 244.18 10.70 -4 -9 0 231.08 11.40 -4 -9 0 232.28 7.20 -4 -9 0 232.28 7.20 4 9 0 231.28 9.20 4 9 0 231.68 9.00 -5 -9 0 6.00 2.50 -5 -9 0 2.60 1.70 -5 -9 0 2.60 2.30 -5 -9 0 3.30 2.60 -5 -9 0 2.60 1.70 5 9 0 3.60 1.20 5 9 0 3.60 1.20 5 9 0 1.70 1.70 5 9 0 6.10 2.40 -6 -9 0 98.89 7.00 -6 -9 0 92.39 6.60 -6 -9 0 102.09 7.00 6 9 0 97.79 6.70 6 9 0 90.49 4.00 6 9 0 90.49 4.00 -7 -9 0 574.84 18.30 7 9 0 551.64 17.60 7 9 0 565.04 11.40 7 9 0 565.04 11.40 -8 -9 0 154.48 8.90 8 9 0 148.59 5.50 8 9 0 161.38 9.00 8 9 0 148.59 5.50 -9 -9 0 15.80 3.80 9 9 0 18.50 2.70 9 9 0 24.00 4.60 9 9 0 18.50 2.70 -10 -9 0 7.10 4.10 -10 -9 0 16.00 4.10 10 9 0 18.80 2.80 10 9 0 18.80 2.80 10 9 0 16.90 4.30 1 -10 0 15.80 5.20 1 -10 0 13.80 4.80 -1 10 0 16.60 3.60 -1 10 0 14.00 4.10 0 -10 0 23.80 5.60 0 -10 0 42.50 7.50 0 10 0 39.70 5.00 0 10 0 27.60 4.90 -1 -10 0 47.10 7.90 -1 -10 0 41.00 6.30 1 10 0 50.29 4.90 1 10 0 48.60 6.20 -2 -10 0 13.60 4.70 -2 -10 0 7.90 2.10 -2 -10 0 13.90 4.00 -2 -10 0 7.90 2.10 2 10 0 15.90 3.20 2 10 0 13.70 3.20 -3 -10 0 213.78 7.70 -3 -10 0 205.28 11.10 -3 -10 0 200.78 12.10 -3 -10 0 213.78 7.70 3 10 0 211.18 9.90 3 10 0 200.08 9.00 -4 -10 0 119.09 6.20 -4 -10 0 119.09 6.20 -4 -10 0 120.39 8.40 -4 -10 0 131.49 9.40 4 10 0 125.79 7.00 4 10 0 130.09 6.90 -5 -10 0 3.40 2.50 -5 -10 0 -1.10 2.20 -5 -10 0 0.80 2.00 5 10 0 0.10 1.70 5 10 0 4.10 2.30 -6 -10 0 -1.10 2.30 -6 -10 0 2.50 2.20 6 10 0 4.90 2.40 -7 -10 0 121.49 8.30 7 10 0 118.69 7.70 -8 -10 0 132.39 8.60 8 10 0 104.29 7.70 -9 -10 0 117.19 8.50 9 10 0 122.29 8.70 -10 -10 0 3.60 2.80 -10 -10 0 5.00 3.70 10 10 0 5.10 3.30 -1 -11 0 53.89 8.90 -1 -11 0 37.70 6.60 1 11 0 37.00 5.70 1 11 0 41.20 5.30 -2 -11 0 -0.70 3.30 -2 -11 0 4.50 3.10 2 11 0 0.90 2.40 2 11 0 2.60 2.00 -3 -11 0 5.70 3.80 -3 -11 0 0.70 2.40 3 11 0 5.70 2.50 3 11 0 2.10 2.50 -4 -11 0 0.20 3.00 -4 -11 0 3.40 2.60 4 11 0 2.30 2.00 -5 -11 0 6.50 3.20 -5 -11 0 5.70 3.70 -5 -11 0 3.80 2.80 -5 -11 0 -0.20 2.30 5 11 0 3.60 2.10 5 11 0 1.50 2.00 -6 -11 0 -0.60 2.50 -6 -11 0 -1.00 2.30 6 11 0 1.80 2.20 6 11 0 0.70 1.90 -7 -11 0 0.60 2.70 7 11 0 0.20 1.90 -8 -11 0 39.80 6.00 -8 -11 0 40.30 7.10 8 11 0 33.80 5.40 8 11 -1 3.30 2.90 -8 -11 1 9.80 3.70 7 11 -1 24.50 4.40 -7 -11 1 31.90 5.90 6 11 -1 10.80 3.10 6 11 -1 12.50 3.20 -6 -11 1 10.80 3.70 -6 -11 1 6.20 3.90 5 11 -1 47.60 5.00 5 11 -1 44.20 5.30 -5 -11 1 61.59 8.30 -5 -11 1 55.59 6.90 -5 -11 1 48.60 6.80 4 11 -1 6.90 2.70 -4 -11 1 6.60 3.80 -4 -11 1 5.20 3.00 3 11 -1 1.90 1.90 -3 -11 1 0.50 2.70 -3 -11 1 1.70 2.20 2 11 -1 26.00 4.90 2 11 -1 21.00 4.00 -2 -11 1 23.30 6.10 -2 -11 1 22.20 5.10 1 11 -1 18.70 4.40 1 11 -1 22.70 4.20 -1 -11 1 14.40 5.60 -1 -11 1 18.50 5.30 10 10 -1 14.10 4.50 -10 -10 1 21.00 4.80 9 10 -1 54.39 7.10 -9 -10 1 69.09 8.30 8 10 -1 -2.00 1.80 -8 -10 1 2.00 2.50 7 10 -1 17.90 3.90 -7 -10 1 14.90 4.00 6 10 -1 4.30 2.40 6 10 -1 8.60 3.00 -6 -10 1 8.70 3.40 -6 -10 1 6.30 3.00 5 10 -1 2.00 2.00 5 10 -1 0.50 1.80 -5 -10 1 0.90 2.80 -5 -10 1 -1.40 1.90 -5 -10 1 1.20 1.90 4 10 -1 5.50 2.30 4 10 -1 -0.40 1.70 -4 -10 1 5.00 3.00 -4 -10 1 6.00 3.30 3 10 -1 76.19 5.70 -3 -10 1 85.39 8.10 -3 -10 1 79.79 7.20 2 10 -1 28.00 4.10 2 10 -1 29.20 4.70 -2 -10 1 27.40 5.90 -2 -10 1 25.10 5.00 1 10 -1 -0.10 1.90 1 10 -1 -0.30 1.60 -1 -10 1 2.20 2.60 -1 -10 1 8.00 4.00 0 10 -1 33.80 4.80 0 10 -1 42.60 6.10 0 -10 1 35.30 6.30 0 -10 1 43.60 8.30 -1 10 -1 65.19 6.60 -1 10 -1 60.59 5.70 1 -10 1 60.49 9.70 1 -10 1 67.59 8.90 10 9 -1 26.10 4.90 -10 -9 1 28.60 5.60 9 9 -1 19.00 4.20 -9 -9 1 19.10 4.40 8 9 -1 6.90 1.70 8 9 -1 3.90 2.70 8 9 -1 6.90 1.70 -8 -9 1 5.30 2.90 7 9 -1 12.20 1.90 7 9 -1 12.20 1.90 7 9 -1 8.90 2.90 -7 -9 1 5.80 2.90 6 9 -1 29.90 2.70 6 9 -1 29.90 2.70 6 9 -1 37.10 5.00 -6 -9 1 26.30 4.60 -6 -9 1 36.30 5.00 -6 -9 1 30.20 4.80 5 9 -1 15.90 2.00 5 9 -1 14.50 3.10 5 9 -1 19.10 3.40 5 9 -1 15.90 2.00 -5 -9 1 18.20 3.60 -5 -9 1 20.80 2.90 -5 -9 1 20.80 2.90 -5 -9 1 14.60 3.80 -5 -9 1 22.70 4.40 4 9 -1 91.89 5.70 4 9 -1 94.49 5.80 -4 -9 1 72.79 4.70 -4 -9 1 92.29 6.70 -4 -9 1 72.79 4.70 -4 -9 1 88.79 7.30 3 9 -1 36.90 4.40 3 9 -1 43.50 5.10 3 9 -1 37.60 3.80 -3 -9 1 42.80 3.60 -3 -9 1 55.59 7.40 -3 -9 1 42.80 3.60 -3 -9 1 43.70 5.70 2 9 -1 179.08 8.70 2 9 -1 162.78 7.80 -2 -9 1 183.78 6.30 -2 -9 1 188.78 11.40 -2 -9 1 183.78 6.30 -2 -9 1 173.28 9.80 1 9 -1 101.89 7.00 1 9 -1 94.09 6.00 -1 -9 1 91.49 4.70 -1 -9 1 92.59 8.90 -1 -9 1 78.69 7.20 -1 -9 1 91.49 4.70 0 9 -1 83.89 5.90 0 9 -1 76.79 6.60 0 -9 1 84.79 7.80 0 -9 1 79.99 4.70 0 -9 1 79.99 4.70 0 -9 1 68.19 8.70 -1 9 -1 65.89 6.20 -1 9 -1 64.09 5.60 1 -9 1 58.19 8.00 1 -9 1 75.99 4.80 1 -9 1 75.39 9.90 1 -9 1 75.99 4.80 -2 9 -1 32.60 4.80 -2 9 -1 28.40 5.00 2 -9 1 24.20 3.50 2 -9 1 24.20 3.50 2 -9 1 25.70 5.90 2 -9 1 28.40 6.60 11 8 -1 119.99 5.80 11 8 -1 119.99 5.80 11 8 -1 119.09 8.70 -11 -8 1 118.29 10.30 -11 -8 1 114.79 8.90 10 8 -1 11.30 3.50 10 8 -1 14.90 2.60 10 8 -1 14.90 2.60 -10 -8 1 14.90 4.00 9 8 -1 85.39 6.90 9 8 -1 92.19 4.50 9 8 -1 92.19 4.50 -9 -8 1 90.69 7.20 8 8 -1 200.08 6.20 8 8 -1 200.08 6.20 8 8 -1 198.88 10.00 -8 -8 1 207.38 10.40 7 8 -1 -0.30 1.00 7 8 -1 -0.30 1.00 7 8 -1 0.00 1.70 -7 -8 1 -0.50 1.70 6 8 -1 210.18 5.70 6 8 -1 210.18 5.70 6 8 -1 199.08 9.00 -6 -8 1 191.98 9.60 -6 -8 1 204.98 9.30 -6 -8 1 205.98 8.10 5 8 -1 127.09 6.40 5 8 -1 128.39 4.30 5 8 -1 130.19 6.90 5 8 -1 128.39 4.30 -5 -8 1 119.19 7.40 -5 -8 1 127.49 7.50 -5 -8 1 126.59 6.70 4 8 -1 153.38 4.70 4 8 -1 159.18 7.00 4 8 -1 153.38 4.70 4 8 -1 153.48 7.20 -4 -8 1 153.88 8.70 -4 -8 1 160.38 5.50 -4 -8 1 160.38 5.50 -4 -8 1 158.28 7.50 3 8 -1 47.00 3.90 3 8 -1 48.00 4.30 3 8 -1 50.89 4.10 -3 -8 1 48.00 3.10 -3 -8 1 48.00 3.10 -3 -8 1 49.50 6.10 -3 -8 1 49.20 4.90 2 8 -1 230.38 8.60 2 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3 -0.30 1.10 3 7 -3 49.70 3.90 3 7 -3 41.70 3.60 -3 -7 3 48.40 5.70 -3 -7 3 47.40 2.60 -3 -7 3 43.00 4.10 -3 -7 3 47.40 2.60 2 7 -3 98.49 5.40 2 7 -3 103.09 5.10 -2 -7 3 116.99 6.90 -2 -7 3 105.49 3.70 -2 -7 3 100.29 7.30 -2 -7 3 105.59 3.70 1 7 -3 0.20 1.30 1 7 -3 3.00 1.40 1 7 -3 -1.30 1.30 -1 -7 3 0.50 0.90 -1 -7 3 -2.10 1.60 -1 -7 3 0.70 1.70 -1 -7 3 0.50 0.90 0 7 -3 243.98 7.40 0 7 -3 248.88 9.70 0 7 -3 240.28 9.10 0 -7 3 230.78 11.80 0 -7 3 241.48 10.90 0 -7 3 242.38 6.50 0 -7 3 242.38 6.50 -1 7 -3 10.90 2.80 -1 7 -3 15.30 3.00 1 -7 3 12.20 2.30 1 -7 3 12.20 2.30 1 -7 3 8.90 3.60 1 -7 3 7.60 3.10 -2 7 -3 -0.90 1.60 -2 7 -3 -0.60 1.40 2 -7 3 5.70 3.40 2 -7 3 0.00 1.30 2 -7 3 0.00 1.30 2 -7 3 -1.40 2.40 -3 7 -3 293.47 11.90 -3 7 -3 279.77 11.20 3 -7 3 282.67 8.60 3 -7 3 272.67 14.60 3 -7 3 295.17 13.60 3 -7 3 282.67 8.60 -4 7 -3 3.20 2.40 -4 7 -3 0.40 1.70 4 -7 3 3.00 1.80 4 -7 3 -1.30 2.50 4 -7 3 -2.20 2.50 4 -7 3 3.00 1.80 -5 7 -3 1.80 2.30 -5 7 -3 -1.10 1.90 5 -7 3 -0.60 1.90 5 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4.00 1 6 -3 6.80 2.00 1 6 -3 9.40 1.80 1 6 -3 8.00 1.90 -1 -6 3 5.60 2.20 -1 -6 3 10.00 1.40 -1 -6 3 10.00 1.40 -1 -6 3 12.40 3.10 0 6 -3 963.30 21.80 0 6 -3 994.80 22.80 0 6 -3 979.50 20.30 0 -6 3 994.30 15.70 0 -6 3 994.30 15.70 0 -6 3 1086.79 25.00 0 -6 3 941.31 25.80 -1 6 -3 172.58 7.60 -1 6 -3 173.98 7.20 -1 6 -3 167.58 5.30 1 -6 3 179.48 9.00 1 -6 3 169.98 9.70 1 -6 3 169.88 5.30 1 -6 3 169.88 5.30 -2 6 -3 110.29 6.20 -2 6 -3 119.19 6.60 2 -6 3 114.39 7.60 2 -6 3 108.49 4.80 2 -6 3 108.49 4.80 2 -6 3 114.59 8.60 -3 6 -3 446.46 14.40 -3 6 -3 477.05 14.40 3 -6 3 477.25 11.00 3 -6 3 477.25 11.00 3 -6 3 483.15 18.30 3 -6 3 455.05 16.40 -4 6 -3 37.90 5.00 -4 6 -3 31.30 4.50 4 -6 3 36.60 6.30 4 -6 3 43.00 6.20 4 -6 3 28.70 3.40 4 -6 3 28.70 3.40 -5 6 -3 190.28 9.50 -5 6 -3 176.68 9.20 5 -6 3 178.78 10.60 5 -6 3 170.68 11.70 5 -6 3 167.38 7.00 5 -6 3 167.38 7.00 -6 6 -3 176.48 9.60 -6 6 -3 179.28 9.70 6 -6 3 180.18 12.40 6 -6 3 190.08 8.00 6 -6 3 177.08 10.90 6 -6 3 190.08 8.00 11 5 -3 23.30 3.40 11 5 -3 26.80 4.70 11 5 -3 23.30 3.40 -11 -5 3 11.80 3.70 10 5 -3 14.00 2.60 10 5 -3 14.00 2.60 10 5 -3 12.30 3.20 -10 -5 3 18.80 4.50 9 5 -3 36.50 3.60 9 5 -3 36.50 3.60 9 5 -3 28.50 4.50 -9 -5 3 38.00 5.40 8 5 -3 502.85 10.70 8 5 -3 502.85 10.70 8 5 -3 502.05 15.50 -8 -5 3 491.05 16.00 7 5 -3 -1.90 0.90 7 5 -3 -0.80 1.30 7 5 -3 -1.90 0.90 -7 -5 3 1.10 1.10 -7 -5 3 -0.80 1.40 6 5 -3 15.60 1.80 6 5 -3 11.50 2.50 6 5 -3 15.60 1.80 -6 -5 3 12.60 2.30 -6 -5 3 9.60 2.60 5 5 -3 141.09 6.60 5 5 -3 168.98 4.10 5 5 -3 168.98 4.10 -5 -5 3 159.18 6.50 -5 -5 3 150.48 7.20 4 5 -3 258.17 5.00 4 5 -3 258.17 5.00 4 5 -3 247.68 8.00 4 5 -3 253.57 8.50 -4 -5 3 250.37 8.70 -4 -5 3 242.78 9.00 3 5 -3 692.63 16.10 3 5 -3 728.13 10.50 3 5 -3 728.13 10.50 3 5 -3 725.83 16.80 -3 -5 3 733.43 18.00 2 5 -3 85.59 4.20 2 5 -3 80.49 4.10 -2 -5 3 90.09 2.70 -2 -5 3 96.09 5.00 -2 -5 3 81.49 5.30 -2 -5 3 90.09 2.70 1 5 -3 7.00 1.70 1 5 -3 6.40 1.50 -1 -5 3 9.80 2.40 -1 -5 3 5.30 1.00 -1 -5 3 5.30 1.00 -1 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55.69 5.10 11 4 -3 55.69 5.10 -11 -4 3 78.39 7.50 -11 -4 3 68.09 8.10 10 4 -3 41.00 4.40 10 4 -3 41.00 4.40 10 4 -3 37.80 5.30 -10 -4 3 30.80 5.50 9 4 -3 37.20 3.70 9 4 -3 37.20 3.70 9 4 -3 26.70 4.10 -9 -4 3 29.00 4.80 8 4 -3 445.96 14.00 8 4 -3 436.76 10.00 8 4 -3 436.76 10.00 -8 -4 3 455.85 14.90 7 4 -3 883.21 15.30 7 4 -3 883.21 15.30 7 4 -3 918.71 22.10 -7 -4 3 927.71 19.20 -7 -4 3 899.61 22.50 6 4 -3 35.20 4.00 6 4 -3 36.70 2.30 6 4 -3 36.70 2.30 -6 -4 3 38.30 2.80 -6 -4 3 29.90 3.80 5 4 -3 31.00 2.00 5 4 -3 28.70 3.50 5 4 -3 31.00 2.00 -5 -4 3 25.30 3.20 -5 -4 3 26.50 2.50 4 4 -3 151.78 3.60 4 4 -3 151.78 3.60 4 4 -3 155.08 6.20 -4 -4 3 160.38 6.80 -4 -4 3 151.08 5.90 3 4 -3 174.58 3.50 3 4 -3 185.78 6.40 3 4 -3 174.58 3.50 3 4 -3 173.78 5.90 -3 -4 3 175.08 6.70 -3 -4 3 176.48 7.00 2 4 -3 3.80 0.60 2 4 -3 6.10 1.40 2 4 -3 3.80 0.60 2 4 -3 4.80 1.40 -2 -4 3 6.50 2.00 -2 -4 3 6.90 1.70 1 4 -3 856.41 17.50 1 4 -3 848.32 17.60 -1 -4 3 869.11 18.90 -1 -4 3 842.42 11.90 -1 -4 3 842.42 11.90 -1 -4 3 828.12 20.00 0 4 -3 1.50 1.10 0 4 -3 2.10 1.00 0 4 -3 0.70 0.90 0 -4 3 2.40 1.80 0 -4 3 1.10 0.70 0 -4 3 1.10 0.70 0 -4 3 4.50 1.80 -1 4 -3 25.60 1.80 -1 4 -3 27.70 2.70 -1 4 -3 26.30 2.90 1 -4 3 22.90 3.70 1 -4 3 29.50 3.50 1 -4 3 24.90 1.80 1 -4 3 24.90 1.80 -2 4 -3 519.75 10.70 -2 4 -3 488.95 13.00 -2 4 -3 516.45 13.30 2 -4 3 522.45 14.80 2 -4 3 516.65 9.60 2 -4 3 516.65 9.60 2 -4 3 501.95 15.70 -3 4 -3 266.57 6.30 -3 4 -3 267.37 9.10 -3 4 -3 294.07 9.40 3 -4 3 257.67 10.20 3 -4 3 270.87 7.00 3 -4 3 270.87 7.00 -4 4 -3 35.50 4.00 -4 4 -3 30.20 3.90 4 -4 3 37.10 4.90 4 -4 3 30.20 3.00 4 -4 3 30.20 3.00 -5 4 -3 0.20 1.50 -5 4 -3 3.30 1.90 5 -4 3 1.20 1.40 5 -4 3 1.20 1.40 5 -4 3 0.50 2.00 -6 4 -3 267.57 11.00 -6 4 -3 267.37 10.30 6 -4 3 273.07 8.70 6 -4 3 273.07 8.70 6 -4 3 271.67 12.80 6 -4 3 248.08 11.40 -7 4 -3 9.30 2.90 -7 4 -3 10.50 3.30 7 -4 3 23.70 5.00 7 -4 3 16.70 4.00 7 -4 3 11.90 2.70 7 -4 3 11.90 2.70 -8 4 -3 -0.70 2.10 8 -4 3 0.30 1.80 8 -4 3 0.30 1.80 11 3 -3 280.07 9.90 11 3 -3 280.07 9.90 -11 -3 3 275.27 13.40 10 3 -3 59.59 5.10 10 3 -3 59.59 5.10 10 3 -3 72.49 5.80 -10 -3 3 68.69 6.80 9 3 -3 21.70 3.70 9 3 -3 28.80 3.40 9 3 -3 28.80 3.40 -9 -3 3 28.70 4.60 8 3 -3 252.97 7.50 8 3 -3 244.28 9.50 8 3 -3 252.97 7.50 -8 -3 3 232.28 10.20 7 3 -3 10.30 2.00 7 3 -3 10.30 2.00 7 3 -3 7.50 2.10 -7 -3 3 9.10 1.80 -7 -3 3 10.30 2.80 6 3 -3 65.59 3.20 6 3 -3 65.59 3.20 6 3 -3 70.29 4.40 -6 -3 3 64.29 4.70 -6 -3 3 67.49 3.50 5 3 -3 225.78 5.40 5 3 -3 225.78 5.40 5 3 -3 229.88 7.90 -5 -3 3 230.98 6.90 4 3 -3 28.80 1.70 4 3 -3 24.50 2.80 4 3 -3 28.80 1.70 -4 -3 3 26.30 3.00 -4 -3 3 27.90 2.40 3 3 -3 162.18 3.30 3 3 -3 170.48 5.80 3 3 -3 162.18 3.30 -3 -3 3 163.28 5.80 -3 -3 3 168.58 6.20 2 3 -3 210.08 3.40 2 3 -3 210.08 3.40 2 3 -3 218.88 6.40 -2 -3 3 208.58 3.40 -2 -3 3 208.58 3.40 -2 -3 3 215.08 7.00 1 3 -3 1889.11 34.50 1 3 -3 1888.01 33.70 -1 -3 3 1881.21 23.10 -1 -3 3 1881.21 23.10 -1 -3 3 1843.62 23.40 -1 -3 3 1843.62 23.40 -1 -3 3 1849.11 34.40 0 3 -3 4.20 1.00 0 3 -3 4.00 1.10 0 -3 3 5.10 1.60 0 -3 3 4.50 0.70 0 -3 3 4.50 0.70 0 -3 3 5.30 1.70 -1 3 -3 72.99 2.90 -1 3 -3 70.19 3.50 1 -3 3 81.09 4.60 1 -3 3 76.19 2.60 1 -3 3 76.19 2.60 -2 3 -3 57.99 3.40 -2 3 -3 58.79 2.40 -2 3 -3 54.09 3.40 2 -3 3 49.90 3.90 2 -3 3 56.09 2.60 2 -3 3 58.59 4.60 2 -3 3 56.09 2.60 -3 3 -3 14.00 1.30 -3 3 -3 11.40 2.00 -3 3 -3 9.50 1.90 3 -3 3 14.00 1.80 3 -3 3 14.00 1.80 3 -3 3 13.30 2.50 -4 3 -3 94.19 4.90 -4 3 -3 92.69 5.20 -4 3 -3 90.99 3.30 4 -3 3 88.59 4.00 4 -3 3 99.99 6.00 4 -3 3 88.59 4.00 -5 3 -3 142.99 6.30 -5 3 -3 141.49 6.90 5 -3 3 136.59 5.40 5 -3 3 151.88 7.70 5 -3 3 136.59 5.40 -6 3 -3 50.49 4.80 -6 3 -3 56.99 4.50 6 -3 3 54.39 4.00 6 -3 3 54.39 4.00 6 -3 3 48.90 4.90 -7 3 -3 8.80 2.40 -7 3 -3 5.40 2.50 7 -3 3 3.70 2.00 7 -3 3 7.40 2.30 7 -3 3 7.10 3.20 7 -3 3 7.40 2.30 -8 3 -3 46.00 6.10 8 -3 3 32.20 4.10 8 -3 3 32.20 4.10 10 2 -3 -2.60 1.80 10 2 -3 -2.60 1.80 -10 -2 3 2.40 2.80 9 2 -3 3.70 2.20 9 2 -3 2.80 1.90 9 2 -3 2.80 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7 -4 0.60 1.70 7 7 -4 -0.50 0.80 -7 -7 4 0.30 1.60 -7 -7 4 0.50 1.90 6 7 -4 67.49 2.80 6 7 -4 67.49 2.80 6 7 -4 63.59 5.20 -6 -7 4 76.79 5.80 -6 -7 4 81.19 6.30 5 7 -4 -0.20 0.60 5 7 -4 -0.20 0.60 5 7 -4 0.40 1.50 5 7 -4 -0.80 1.70 -5 -7 4 3.20 2.10 -5 -7 4 -1.50 1.30 4 7 -4 490.25 8.30 4 7 -4 500.55 14.30 4 7 -4 490.35 8.30 4 7 -4 469.95 13.50 -4 -7 4 495.25 15.60 3 7 -4 12.30 2.50 3 7 -4 11.90 2.50 -3 -7 4 17.20 1.80 -3 -7 4 17.20 1.80 -3 -7 4 18.60 3.30 -3 -7 4 17.80 3.60 2 7 -4 674.63 17.00 2 7 -4 676.53 16.70 -2 -7 4 684.33 11.30 -2 -7 4 682.93 20.50 -2 -7 4 684.43 11.30 -2 -7 4 681.23 18.80 1 7 -4 277.27 9.70 1 7 -4 282.07 8.80 -1 -7 4 285.37 6.50 -1 -7 4 285.37 6.50 -1 -7 4 292.27 12.80 -1 -7 4 294.47 11.70 0 7 -4 962.90 22.50 0 7 -4 920.51 20.30 0 -7 4 957.30 25.40 0 -7 4 984.70 15.90 0 -7 4 984.60 15.90 0 -7 4 969.70 27.00 -1 7 -4 670.23 18.50 -1 7 -4 663.43 17.80 1 -7 4 630.64 20.10 1 -7 4 669.93 12.60 1 -7 4 648.34 21.90 1 -7 4 669.93 12.60 -2 7 -4 -1.10 1.60 -2 7 -4 0.80 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397.76 11.90 4 6 -4 402.76 6.80 4 6 -4 396.46 11.40 4 6 -4 402.76 6.80 -4 -6 4 397.06 13.20 -4 -6 4 384.66 12.60 3 6 -4 0.30 0.50 3 6 -4 0.30 0.50 3 6 -4 1.00 1.30 3 6 -4 2.70 1.40 -3 -6 4 2.00 1.70 -3 -6 4 -0.40 0.60 -3 -6 4 -0.40 0.60 2 6 -4 18.20 2.60 2 6 -4 14.10 2.30 -2 -6 4 16.20 2.90 -2 -6 4 25.00 4.00 -2 -6 4 21.30 1.60 -2 -6 4 21.30 1.60 1 6 -4 2.10 1.10 1 6 -4 -0.70 1.10 -1 -6 4 2.20 0.80 -1 -6 4 2.20 0.80 -1 -6 4 0.30 1.80 -1 -6 4 -0.20 1.50 0 6 -4 1270.77 27.00 0 6 -4 1293.67 25.80 0 -6 4 1320.47 31.60 0 -6 4 1269.77 19.00 0 -6 4 1287.47 29.80 0 -6 4 1269.77 19.00 -1 6 -4 49.60 4.00 -1 6 -4 53.39 4.40 -1 6 -4 54.79 3.00 1 -6 4 51.89 2.90 1 -6 4 42.50 5.20 1 -6 4 51.89 2.90 1 -6 4 40.10 5.80 -2 6 -4 127.09 6.70 -2 6 -4 113.69 6.50 2 -6 4 135.99 9.10 2 -6 4 124.79 4.80 2 -6 4 124.79 4.80 2 -6 4 118.39 7.90 -3 6 -4 195.28 8.80 -3 6 -4 171.58 8.20 3 -6 4 184.18 6.40 3 -6 4 184.18 6.40 3 -6 4 171.78 9.80 3 -6 4 188.58 11.20 -4 6 -4 238.68 10.20 -4 6 -4 248.78 10.50 4 -6 4 223.08 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111.29 4.40 -5 3 -4 79.69 4.80 -5 3 -4 75.99 5.20 5 -3 4 73.49 5.50 5 -3 4 72.49 6.20 5 -3 4 77.79 4.10 5 -3 4 77.79 4.10 -6 3 -4 278.87 9.70 -6 3 -4 269.57 10.60 6 -3 4 263.97 8.20 6 -3 4 272.57 12.00 6 -3 4 263.97 8.20 6 -3 4 265.77 10.70 -7 3 -4 11.10 2.70 -7 3 -4 9.30 3.00 7 -3 4 14.40 3.30 7 -3 4 10.40 2.50 7 -3 4 10.40 2.50 7 -3 4 16.40 4.10 -8 3 -4 6.50 2.90 8 -3 4 -2.50 1.50 8 -3 4 -2.50 1.50 10 2 -4 11.40 2.80 10 2 -4 11.40 2.80 -10 -2 4 21.00 4.70 9 2 -4 558.54 16.00 9 2 -4 563.34 13.20 9 2 -4 563.34 13.20 -9 -2 4 540.85 17.80 8 2 -4 155.78 6.00 8 2 -4 148.69 7.00 8 2 -4 155.78 6.00 -8 -2 4 148.49 8.10 7 2 -4 281.27 9.50 7 2 -4 288.47 7.70 7 2 -4 288.47 7.70 -7 -2 4 272.37 8.60 -7 -2 4 269.77 10.50 6 2 -4 2.40 1.20 6 2 -4 2.40 1.20 6 2 -4 2.10 1.40 -6 -2 4 1.20 1.50 -6 -2 4 2.50 1.30 5 2 -4 358.86 7.60 5 2 -4 358.86 7.60 5 2 -4 349.77 10.10 -5 -2 4 355.86 10.80 -5 -2 4 365.86 9.70 4 2 -4 56.19 2.40 4 2 -4 58.59 3.50 4 2 -4 56.19 2.40 -4 -2 4 51.49 3.70 -4 -2 4 55.99 3.30 3 2 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6 720.73 9.70 -3 -4 6 713.53 17.80 2 4 -6 1575.74 30.10 2 4 -6 1541.45 31.10 -2 -4 6 1542.95 32.60 1 4 -6 42.00 3.00 1 4 -6 44.40 3.10 -1 -4 6 49.80 4.30 0 4 -6 13.70 2.00 0 4 -6 14.80 2.10 0 -4 6 15.70 1.00 0 -4 6 19.80 3.40 0 -4 6 15.70 1.00 -1 4 -6 0.30 1.00 -1 4 -6 2.80 1.20 1 -4 6 4.10 0.90 1 -4 6 4.10 0.90 1 -4 6 4.30 2.10 -2 4 -6 2.00 1.30 -2 4 -6 0.00 0.90 2 -4 6 -0.20 1.70 2 -4 6 0.90 0.80 2 -4 6 0.90 0.80 -3 4 -6 775.42 17.00 -3 4 -6 790.92 19.20 3 -4 6 797.92 22.10 3 -4 6 799.42 13.60 3 -4 6 786.82 20.80 3 -4 6 799.32 13.60 -4 4 -6 525.05 15.20 4 -4 6 548.45 17.80 4 -4 6 534.75 11.10 4 -4 6 534.75 11.10 4 -4 6 525.35 16.50 -5 4 -6 1.70 2.00 5 -4 6 2.00 2.60 5 -4 6 3.90 1.80 5 -4 6 3.90 1.80 -6 4 -6 2.20 2.20 6 -4 6 5.90 2.20 6 -4 6 4.30 3.00 6 -4 6 5.90 2.20 -7 4 -6 18.20 3.70 7 -4 6 25.30 3.60 7 -4 6 25.30 3.60 10 3 -6 86.59 5.50 10 3 -6 86.59 5.50 -10 -3 6 91.29 7.50 9 3 -6 -0.40 1.60 9 3 -6 -0.40 1.60 9 3 -6 2.80 2.10 -9 -3 6 4.70 2.40 8 3 -6 231.88 9.60 8 3 -6 256.27 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4.30 -2 -7 9 41.60 6.00 1 7 -9 0.30 1.50 1 7 -9 7.90 2.40 -1 -7 9 0.50 2.30 0 7 -9 1.90 1.60 0 7 -9 7.30 2.50 0 -7 9 13.20 4.30 -1 7 -9 25.40 4.00 1 -7 9 29.10 5.80 -2 7 -9 1.00 2.00 2 -7 9 -0.30 2.90 -3 7 -9 8.10 3.20 3 -7 9 15.30 4.80 -4 7 -9 78.09 6.80 4 -7 9 66.09 8.90 10 6 -9 -1.40 1.60 -10 -6 9 -0.50 2.70 9 6 -9 2.70 2.40 -9 -6 9 3.90 3.00 8 6 -9 25.30 4.40 -8 -6 9 17.80 4.30 -8 -6 9 22.50 3.90 7 6 -9 5.10 2.50 -7 -6 9 1.40 2.30 -7 -6 9 3.50 2.30 6 6 -9 14.40 3.30 -6 -6 9 14.20 3.30 -6 -6 9 18.80 3.90 5 6 -9 51.49 4.90 -5 -6 9 58.09 5.40 -5 -6 9 50.49 5.90 4 6 -9 27.00 3.70 4 6 -9 27.90 3.90 -4 -6 9 35.70 5.20 -4 -6 9 38.20 5.40 3 6 -9 33.00 4.10 3 6 -9 39.20 3.80 -3 -6 9 36.80 5.20 2 6 -9 142.99 7.10 2 6 -9 142.49 6.80 -2 -6 9 152.68 8.70 1 6 -9 54.59 4.40 1 6 -9 58.29 4.40 -1 -6 9 69.69 6.30 0 6 -9 6.60 2.30 0 6 -9 5.70 2.00 0 -6 9 11.50 3.70 -1 6 -9 270.87 10.10 -1 6 -9 256.17 9.10 1 -6 9 257.67 12.50 -2 6 -9 227.88 9.70 2 -6 9 248.38 12.60 -3 6 -9 71.09 5.70 3 -6 9 87.49 8.20 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40.90 6.10 9 4 -9 23.00 4.20 -9 -4 9 29.20 4.90 8 4 -9 0.90 1.40 8 4 -9 -1.30 1.60 8 4 -9 0.90 1.40 -8 -4 9 3.30 2.30 -8 -4 9 2.70 2.20 7 4 -9 37.10 3.00 7 4 -9 37.80 4.80 7 4 -9 37.10 3.00 -7 -4 9 41.40 5.50 -7 -4 9 33.30 4.40 6 4 -9 126.69 4.10 6 4 -9 126.69 4.10 6 4 -9 111.39 6.70 -6 -4 9 113.49 7.00 -6 -4 9 122.89 6.80 5 4 -9 511.35 15.00 5 4 -9 514.65 8.80 5 4 -9 514.65 8.80 -5 -4 9 530.55 15.40 -5 -4 9 506.35 15.30 4 4 -9 1.40 0.60 4 4 -9 0.20 1.30 4 4 -9 1.40 0.60 -4 -4 9 -0.20 1.30 -4 -4 9 0.30 1.40 3 4 -9 20.50 2.70 3 4 -9 17.00 2.80 -3 -4 9 18.40 3.30 -3 -4 9 21.70 3.80 2 4 -9 615.14 14.80 2 4 -9 592.54 15.70 -2 -4 9 603.24 17.20 1 4 -9 108.39 5.10 1 4 -9 111.29 5.60 -1 -4 9 126.39 7.20 0 4 -9 -0.20 1.30 0 4 -9 -0.20 1.00 0 -4 9 -1.00 1.50 -1 4 -9 11.20 2.30 -1 4 -9 8.70 2.00 1 -4 9 12.80 1.10 1 -4 9 8.60 2.80 1 -4 9 12.80 1.10 -2 4 -9 184.18 7.20 -2 4 -9 190.08 7.60 2 -4 9 181.38 4.50 2 -4 9 193.78 9.60 2 -4 9 181.38 4.50 -3 4 -9 162.18 6.70 -3 4 -9 176.48 7.70 3 -4 9 167.48 4.90 3 -4 9 188.58 9.70 3 -4 9 167.48 4.90 -4 4 -9 98.49 5.10 -4 4 -9 107.79 6.40 4 -4 9 91.49 7.30 4 -4 9 92.09 4.30 4 -4 9 92.09 4.30 -5 4 -9 1.30 1.90 5 -4 9 2.30 1.50 5 -4 9 4.00 2.80 5 -4 9 2.30 1.50 -6 4 -9 54.79 5.50 6 -4 9 51.99 4.40 6 -4 9 51.99 4.40 6 -4 9 51.79 6.80 -7 4 -9 45.60 5.80 7 -4 9 47.00 4.60 7 -4 9 47.00 4.60 10 3 -9 6.00 2.50 10 3 -9 6.00 2.50 -10 -3 9 6.00 3.10 9 3 -9 23.40 4.10 9 3 -9 24.40 3.30 9 3 -9 24.40 3.30 -9 -3 9 18.40 4.00 8 3 -9 105.79 5.00 8 3 -9 107.09 6.90 8 3 -9 105.79 5.00 -8 -3 9 118.39 6.70 -8 -3 9 106.69 7.30 7 3 -9 117.99 6.80 7 3 -9 120.49 4.90 7 3 -9 120.49 4.90 -7 -3 9 114.49 6.70 -7 -3 9 107.09 6.90 6 3 -9 145.59 4.90 6 3 -9 145.59 4.90 6 3 -9 153.08 7.50 -6 -3 9 158.28 7.60 -6 -3 9 153.48 7.80 5 3 -9 635.94 11.00 5 3 -9 635.94 11.00 5 3 -9 649.74 17.10 -5 -3 9 654.93 17.40 -5 -3 9 631.64 17.20 4 3 -9 218.48 8.40 4 3 -9 202.28 4.60 4 3 -9 202.28 4.60 -4 -3 9 234.48 9.00 -4 -3 9 205.38 8.40 3 3 -9 82.29 4.30 3 3 -9 73.39 2.10 3 3 -9 73.39 2.10 3 3 -9 70.29 4.50 -3 -3 9 74.69 4.80 -3 -3 9 73.19 5.10 2 3 -9 142.29 6.30 2 3 -9 147.29 5.60 -2 -3 9 153.38 7.30 1 3 -9 454.25 12.70 1 3 -9 476.55 11.60 -1 -3 9 466.05 14.00 0 3 -9 13.90 2.50 0 3 -9 11.80 1.90 0 3 -9 11.50 0.80 0 3 -9 11.50 0.80 0 -3 9 12.50 0.70 0 -3 9 12.50 0.70 0 -3 9 11.90 2.70 -1 3 -9 117.49 5.20 -1 3 -9 121.29 5.60 1 -3 9 119.99 2.80 1 -3 9 119.99 2.80 1 -3 9 120.59 6.70 -2 3 -9 31.00 3.00 -2 3 -9 29.50 2.90 2 -3 9 27.70 4.10 2 -3 9 26.80 1.70 2 -3 9 26.80 1.70 -3 3 -9 272.67 9.30 -3 3 -9 262.87 8.90 3 -3 9 274.37 11.00 3 -3 9 276.97 6.20 3 -3 9 276.97 6.20 -4 3 -9 217.98 8.10 -4 3 -9 224.68 8.90 4 -3 9 223.18 10.10 4 -3 9 229.28 6.10 4 -3 9 229.18 6.10 -5 3 -9 47.00 3.80 -5 3 -9 47.30 4.50 5 -3 9 51.09 5.90 5 -3 9 41.80 3.40 5 -3 9 41.80 3.40 -6 3 -9 216.68 9.60 6 -3 9 190.18 6.70 6 -3 9 190.18 6.70 6 -3 9 204.38 10.30 -7 3 -9 114.19 7.60 7 -3 9 107.29 5.60 7 -3 9 107.29 5.60 -8 3 -9 0.20 2.00 8 -3 9 4.80 2.30 8 -3 9 4.80 2.30 9 2 -9 28.20 3.70 9 2 -9 28.20 3.70 -9 -2 9 37.00 5.60 8 2 -9 107.19 5.40 8 2 -9 107.19 5.40 8 2 -9 105.69 6.50 -8 -2 9 112.79 7.30 -8 -2 9 103.29 6.60 7 2 -9 3.40 1.80 7 2 -9 1.90 1.90 7 2 -9 3.40 1.80 -7 -2 9 5.00 2.40 -7 -2 9 2.10 1.90 6 2 -9 142.99 5.20 6 2 -9 142.99 5.20 6 2 -9 138.29 6.90 -6 -2 9 139.09 7.20 -6 -2 9 139.79 7.10 5 2 -9 43.20 3.90 5 2 -9 41.90 2.70 5 2 -9 41.90 2.70 -5 -2 9 46.50 4.20 -5 -2 9 41.80 4.00 4 2 -9 105.39 3.60 4 2 -9 105.39 3.60 4 2 -9 113.29 5.60 -4 -2 9 106.49 5.60 3 2 -9 39.60 2.00 3 2 -9 41.60 3.40 3 2 -9 39.60 2.00 -3 -2 9 41.70 3.80 -3 -2 9 39.40 3.40 2 2 -9 7.50 0.90 2 2 -9 7.50 0.90 2 2 -9 6.50 1.50 2 2 -9 10.20 2.10 -2 -2 9 6.40 1.90 -2 -2 9 10.70 2.20 1 2 -9 82.69 4.60 1 2 -9 79.89 3.60 1 2 -9 70.69 1.80 1 2 -9 70.69 1.80 1 2 -9 72.49 2.00 1 2 -9 72.49 2.00 0 2 -9 43.70 3.40 0 2 -9 49.00 2.90 0 -2 9 48.00 1.50 0 -2 9 45.50 4.10 0 -2 9 48.00 1.50 -1 2 -9 91.39 4.10 -1 2 -9 93.09 4.80 1 -2 9 82.49 2.30 1 -2 9 82.49 2.30 1 -2 9 79.99 5.20 -2 2 -9 4.90 1.60 -2 2 -9 4.50 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