# Electronic Supplementary Material (ESI) for ChemComm.
# This journal is © The Royal Society of Chemistry 2014

#######################################################################
#
#                 Cambridge Crystallographic Data Centre
#                                CCDC 
# 
#######################################################################
# 
#  This CIF contains data from an original supplementary publication
#  deposited with the CCDC, and may include chemical, crystal,
#  experimental, refinement, atomic coordinates,
#  anisotropic displacement parameters and molecular geometry data,
#  as required by the journal to which it was submitted.
#
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#  fide research purposes only. It may contain copyright material
#  of the CCDC or of third parties, and may not be copied or further
#  disseminated in any form, whether machine-readable or not,
#  except for the purpose of generating routine backup copies
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#  data retrieval see:
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#  from this site to visualise CIF-encoded structures and 
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data_c:\sir97\manuel\547cr\547crs

_audit_creation_method           SHELXL-97
_chemical_name_systematic        
; 
 ? 
;
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C35 H76 Cl N13 O9 P4 Ru2'
_chemical_formula_weight         1184.55

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_symmetry_cell_setting           Triclinic
_symmetry_space_group_name_H-M   P-1

loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   14.5313(7)
_cell_length_b                   17.5256(8)
_cell_length_c                   18.3097(9)
_cell_angle_alpha                66.9270(10)
_cell_angle_beta                 73.1200(10)
_cell_angle_gamma                76.5130(10)
_cell_volume                     4067.1(3)
_cell_formula_units_Z            1
_cell_measurement_temperature    100(2)
_cell_measurement_reflns_used    9734
_cell_measurement_theta_min      4.722
_cell_measurement_theta_max      49.958

_exptl_crystal_description       prismatic
_exptl_crystal_colour            yellow
_exptl_crystal_size_max          0.200
_exptl_crystal_size_mid          0.170
_exptl_crystal_size_min          0.150
_exptl_crystal_density_meas      ?
_exptl_crystal_density_diffrn    1.429
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             1788
_exptl_absorpt_coefficient_mu    0.781
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_correction_T_min  0.855
_exptl_absorpt_correction_T_max  0.889
_exptl_absorpt_process_details   ?

_exptl_special_details           
; 
 ? 
;

_diffrn_ambient_temperature      100(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_monochromator  graphite
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_detector_area_resol_mean ?
_diffrn_standards_number         ?
_diffrn_standards_interval_count ?
_diffrn_standards_interval_time  ?
_diffrn_standards_decay_%        ?
_diffrn_reflns_number            21874
_diffrn_reflns_av_R_equivalents  0.0248
_diffrn_reflns_av_sigmaI/netI    0.0467
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_h_max       16
_diffrn_reflns_limit_k_min       -20
_diffrn_reflns_limit_k_max       20
_diffrn_reflns_limit_l_min       -21
_diffrn_reflns_limit_l_max       14
_diffrn_reflns_theta_min         1.24
_diffrn_reflns_theta_max         25.04
_reflns_number_total             14015
_reflns_number_gt                12264
_reflns_threshold_expression     >2sigma(I)

_computing_data_collection       'Bruker APEX'
_computing_cell_refinement       'Bruker APEX'
_computing_data_reduction        'Bruker SHELXTL'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'

_refine_special_details          
; 
 Refinement of F² against ALL reflections.  The weighted R-factor wR and 
 goodness of fit S are based on F², conventional R-factors R are based 
 on F, with F set to zero for negative F². The threshold expression of 
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is 
 not relevant to the choice of reflections for refinement.  R-factors based 
 on F² are statistically about twice as large as those based on F, and R- 
 factors based on ALL data will be even larger. 
;

_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'calc w=1/[σ²(Fo²)+(0.1020P)²+16.9505P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       ?
_refine_ls_number_reflns         14015
_refine_ls_number_parameters     940
_refine_ls_number_restraints     3
_refine_ls_R_factor_all          0.0640
_refine_ls_R_factor_gt           0.0569
_refine_ls_wR_factor_ref         0.1767
_refine_ls_wR_factor_gt          0.1679
_refine_ls_goodness_of_fit_ref   1.062
_refine_ls_restrained_S_all      1.062
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ru1 Ru 0.09522(3) -0.03884(2) 0.61253(3) 0.01873(13) Uani 1 1 d . . .
Ru2 Ru 0.50502(3) 0.62844(2) 0.53445(2) 0.01549(12) Uani 1 1 d . . .
Ru3 Ru 0.16769(3) 0.55235(3) -0.05883(2) 0.02139(13) Uani 1 1 d . . .
Cl1 Cl 0.3566(4) 0.8051(3) 0.8495(4) 0.0495(15) Uiso 0.372(5) 1 d P A 1
Cl2 Cl 0.3856(7) 0.8203(6) 0.8039(7) 0.042(2) Uiso 0.175(2) 1 d P A 1
Cl3 Cl 0.4432(6) 0.9184(5) 0.1929(5) 0.0387(19) Uiso 0.213(3) 1 d P A 2
Cl4 Cl 0.4141(11) 0.8897(9) 0.2827(9) 0.039(3) Uiso 0.1132(18) 1 d P A 2
Cl5 Cl 0.3922(9) 0.9619(8) 0.2114(8) 0.039(3) Uiso 0.127(2) 1 d P A 2
Cl6 Cl 0.9512(4) 0.4925(3) 0.5287(3) 0.0675(12) Uani 0.50 1 d P . .
P1A P -0.00086(10) 0.07204(9) 0.64130(9) 0.0227(3) Uani 1 1 d . . .
P2A P 0.20952(10) 0.03652(8) 0.51819(8) 0.0201(3) Uani 1 1 d . . .
P1B P 0.63703(9) 0.65385(8) 0.43032(8) 0.0184(3) Uani 1 1 d . . .
P2B P 0.58453(9) 0.53295(8) 0.62886(8) 0.0172(3) Uani 1 1 d . . .
P1C P 0.20000(11) 0.44397(9) 0.05257(8) 0.0241(3) Uani 1 1 d . . .
P2C P 0.11635(10) 0.64522(9) 0.00694(8) 0.0235(3) Uani 1 1 d . . .
N1P N 0.0218(4) -0.0089(3) 0.5240(3) 0.0206(10) Uani 0.453(9) 1 d P . .
C1P C 0.0218(4) -0.0089(3) 0.5240(3) 0.0206(10) Uani 0.547(9) 1 d P . .
N2P N 0.4999(3) 0.5293(3) 0.5068(3) 0.0175(13) Uani 0.36(7) 1 d P . .
C2P C 0.4999(3) 0.5293(3) 0.5068(3) 0.0175(13) Uani 0.64(7) 1 d P . .
N3P N 0.0360(4) 0.5140(3) -0.0146(3) 0.0270(14) Uani 0.77(8) 1 d P . .
C3P C 0.0360(4) 0.5140(3) -0.0146(3) 0.0270(14) Uani 0.23(8) 1 d P . .
N11A N -0.0998(4) 0.2329(3) 0.5922(4) 0.0396(13) Uani 1 1 d . . .
N12A N -0.1865(5) 0.1301(4) 0.7107(6) 0.080(3) Uani 1 1 d . . .
N13A N -0.0537(5) 0.1839(4) 0.7230(4) 0.0502(16) Uani 1 1 d . . .
N21A N 0.2783(3) 0.1472(3) 0.3639(3) 0.0267(10) Uani 1 1 d . . .
N22A N 0.3419(4) 0.1468(3) 0.4753(3) 0.0301(11) Uani 1 1 d . . .
N23A N 0.3981(4) 0.0296(3) 0.4233(3) 0.0387(13) Uani 1 1 d . . .
N11B N 0.8062(4) 0.6048(3) 0.3330(4) 0.0452(15) Uani 1 1 d . . .
N12B N 0.6993(4) 0.7243(5) 0.2629(3) 0.058(2) Uani 1 1 d . . .
N13B N 0.7924(5) 0.7409(4) 0.3449(4) 0.057(2) Uani 1 1 d . . .
N21B N 0.6961(3) 0.3808(3) 0.6902(3) 0.0282(11) Uani 1 1 d . . .
N22B N 0.6885(4) 0.4884(3) 0.7478(3) 0.0322(11) Uani 1 1 d . . .
N23B N 0.5482(4) 0.4149(3) 0.7857(3) 0.0376(13) Uani 1 1 d . . .
N11C N 0.1422(4) 0.3503(3) 0.2154(3) 0.0333(12) Uani 1 1 d . . .
N12C N 0.2204(4) 0.2704(3) 0.1234(3) 0.0350(12) Uani 1 1 d . . .
N13C N 0.3186(4) 0.3443(3) 0.1578(3) 0.0396(13) Uani 1 1 d . . .
N21C N -0.0193(4) 0.7101(3) 0.1169(3) 0.0304(11) Uani 1 1 d . . .
N22C N 0.1525(4) 0.7228(4) 0.1002(4) 0.0410(14) Uani 1 1 d . . .
N23C N 0.0640(5) 0.8123(3) -0.0068(4) 0.0524(18) Uani 1 1 d . . .
C11A C -0.1271(5) 0.0549(5) 0.6954(7) 0.068(3) Uani 1 1 d . . .
H11A H -0.1570 0.0383 0.6627 0.081 Uiso 1 1 calc R . .
H11B H -0.1268 0.0083 0.7481 0.081 Uiso 1 1 calc R . .
C12A C 0.0247(5) 0.1162(4) 0.7091(4) 0.0428(17) Uani 1 1 d . . .
H12A H 0.0302 0.0713 0.7619 0.051 Uiso 1 1 calc R . .
H12B H 0.0873 0.1389 0.6841 0.051 Uiso 1 1 calc R . .
C13A C -0.0277(6) 0.1720(4) 0.5607(4) 0.0417(17) Uani 1 1 d . . .
H13A H 0.0332 0.1967 0.5313 0.050 Uiso 1 1 calc R . .
H13B H -0.0523 0.1610 0.5212 0.050 Uiso 1 1 calc R . .
C14A C -0.1918(5) 0.2008(5) 0.6350(7) 0.063(3) Uani 1 1 d . . .
H14A H -0.2144 0.1832 0.5987 0.076 Uiso 1 1 calc R . .
H14B H -0.2405 0.2465 0.6475 0.076 Uiso 1 1 calc R . .
C15A C -0.1461(7) 0.1538(5) 0.7622(5) 0.068(3) Uani 1 1 d . . .
H15A H -0.1927 0.1979 0.7795 0.082 Uiso 1 1 calc R . .
H15B H -0.1387 0.1046 0.8118 0.082 Uiso 1 1 calc R . .
C16A C -0.0625(5) 0.2517(4) 0.6490(4) 0.0379(15) Uani 1 1 d . . .
H16A H 0.0021 0.2701 0.6210 0.045 Uiso 1 1 calc R . .
H16B H -0.1062 0.2992 0.6625 0.045 Uiso 1 1 calc R . .
C21A C 0.3238(4) -0.0243(3) 0.4836(4) 0.0331(14) Uani 1 1 d . . .
H21A H 0.3510 -0.0616 0.5314 0.040 Uiso 1 1 calc R . .
H21B H 0.3100 -0.0600 0.4586 0.040 Uiso 1 1 calc R . .
C22A C 0.1906(4) 0.1093(3) 0.4166(3) 0.0245(12) Uani 1 1 d . . .
H22A H 0.1710 0.0785 0.3895 0.029 Uiso 1 1 calc R . .
H22B H 0.1370 0.1543 0.4236 0.029 Uiso 1 1 calc R . .
C23A C 0.2626(4) 0.1076(4) 0.5418(4) 0.0283(12) Uani 1 1 d . . .
H23A H 0.2109 0.1522 0.5532 0.034 Uiso 1 1 calc R . .
H23B H 0.2878 0.0758 0.5917 0.034 Uiso 1 1 calc R . .
C24A C 0.4196(5) 0.0843(4) 0.4578(4) 0.0365(15) Uani 1 1 d . . .
H24A H 0.4408 0.0487 0.5089 0.044 Uiso 1 1 calc R . .
H24B H 0.4750 0.1130 0.4194 0.044 Uiso 1 1 calc R . .
C25A C 0.3589(5) 0.0839(4) 0.3498(4) 0.0377(15) Uani 1 1 d . . .
H25A H 0.4120 0.1121 0.3067 0.045 Uiso 1 1 calc R . .
H25B H 0.3373 0.0480 0.3293 0.045 Uiso 1 1 calc R . .
C26A C 0.3072(4) 0.1969(4) 0.4008(4) 0.0308(13) Uani 1 1 d . . .
H26A H 0.3591 0.2290 0.3604 0.037 Uiso 1 1 calc R . .
H26B H 0.2508 0.2377 0.4133 0.037 Uiso 1 1 calc R . .
C31A C 0.0744(5) -0.1737(3) 0.6671(4) 0.0325(14) Uani 1 1 d . . .
H31A H 0.0376 -0.1972 0.6480 0.039 Uiso 1 1 calc R . .
C32A C 0.0378(5) -0.1376(4) 0.7288(4) 0.0351(14) Uani 1 1 d . . .
H32A H -0.0274 -0.1331 0.7588 0.042 Uiso 1 1 calc R . .
C33A C 0.1171(5) -0.1093(4) 0.7372(4) 0.0364(15) Uani 1 1 d . . .
H33A H 0.1137 -0.0817 0.7736 0.044 Uiso 1 1 calc R . .
C34A C 0.2003(5) -0.1287(4) 0.6834(4) 0.0355(15) Uani 1 1 d . . .
H34A H 0.2635 -0.1172 0.6770 0.043 Uiso 1 1 calc R . .
C35A C 0.1745(5) -0.1690(3) 0.6392(4) 0.0335(14) Uani 1 1 d . . .
H35A H 0.2173 -0.1889 0.5984 0.040 Uiso 1 1 calc R . .
C11B C 0.6112(5) 0.7065(6) 0.3286(4) 0.060(2) Uani 1 1 d . . .
H11C H 0.5758 0.6709 0.3186 0.072 Uiso 1 1 calc R . .
H11D H 0.5682 0.7598 0.3268 0.072 Uiso 1 1 calc R . .
C12B C 0.7165(6) 0.7253(6) 0.4209(5) 0.060(3) Uani 1 1 d . . .
H12C H 0.6771 0.7791 0.4225 0.072 Uiso 1 1 calc R . .
H12D H 0.7478 0.7014 0.4679 0.072 Uiso 1 1 calc R . .
C13B C 0.7305(5) 0.5716(4) 0.4070(5) 0.055(2) Uani 1 1 d . . .
H13C H 0.7615 0.5407 0.4538 0.066 Uiso 1 1 calc R . .
H13D H 0.6996 0.5315 0.3991 0.066 Uiso 1 1 calc R . .
C14B C 0.7644(5) 0.6477(6) 0.2613(4) 0.052(2) Uani 1 1 d . . .
H14C H 0.8178 0.6614 0.2123 0.063 Uiso 1 1 calc R . .
H14D H 0.7283 0.6090 0.2567 0.063 Uiso 1 1 calc R . .
C15B C 0.7521(7) 0.7777(5) 0.2737(5) 0.066(3) Uani 1 1 d . . .
H15C H 0.8056 0.7941 0.2252 0.079 Uiso 1 1 calc R . .
H15D H 0.7081 0.8293 0.2767 0.079 Uiso 1 1 calc R . .
C16B C 0.8542(5) 0.6642(6) 0.3419(4) 0.051(2) Uani 1 1 d . . .
H16C H 0.8789 0.6370 0.3924 0.061 Uiso 1 1 calc R . .
H16D H 0.9108 0.6781 0.2956 0.061 Uiso 1 1 calc R . .
C21B C 0.4994(4) 0.4783(4) 0.7216(4) 0.0324(14) Uani 1 1 d . . .
H21C H 0.4552 0.5201 0.7439 0.039 Uiso 1 1 calc R . .
H21D H 0.4594 0.4502 0.7069 0.039 Uiso 1 1 calc R . .
C22B C 0.6655(4) 0.4392(4) 0.6153(3) 0.0282(12) Uani 1 1 d . . .
H22C H 0.6317 0.4096 0.5967 0.034 Uiso 1 1 calc R . .
H22D H 0.7239 0.4568 0.5722 0.034 Uiso 1 1 calc R . .
C23B C 0.6576(5) 0.5609(4) 0.6795(4) 0.0298(13) Uani 1 1 d . . .
H23C H 0.7159 0.5832 0.6392 0.036 Uiso 1 1 calc R . .
H23D H 0.6190 0.6056 0.7004 0.036 Uiso 1 1 calc R . .
C24B C 0.6066(5) 0.4553(4) 0.8102(4) 0.0381(16) Uani 1 1 d . . .
H24C H 0.5642 0.5014 0.8269 0.046 Uiso 1 1 calc R . .
H24D H 0.6304 0.4138 0.8583 0.046 Uiso 1 1 calc R . .
C25B C 0.6131(4) 0.3496(4) 0.7554(4) 0.0355(14) Uani 1 1 d . . .
H25C H 0.6374 0.3044 0.8013 0.043 Uiso 1 1 calc R . .
H25D H 0.5751 0.3252 0.7352 0.043 Uiso 1 1 calc R . .
C26B C 0.7487(4) 0.4217(4) 0.7190(4) 0.0305(13) Uani 1 1 d . . .
H26C H 0.7772 0.3788 0.7638 0.037 Uiso 1 1 calc R . .
H26D H 0.8029 0.4456 0.6740 0.037 Uiso 1 1 calc R . .
C31B C 0.3476(4) 0.6816(3) 0.5379(4) 0.0244(12) Uani 1 1 d . . .
H31B H 0.3040 0.6583 0.5252 0.029 Uiso 1 1 calc R . .
C32B C 0.4053(4) 0.7435(3) 0.4817(4) 0.0290(13) Uani 1 1 d . . .
H32B H 0.4076 0.7691 0.4250 0.035 Uiso 1 1 calc R . .
C33B C 0.4595(4) 0.7604(3) 0.5255(4) 0.0328(14) Uani 1 1 d . . .
H33B H 0.5046 0.7996 0.5030 0.039 Uiso 1 1 calc R . .
C34B C 0.4351(4) 0.7093(4) 0.6083(4) 0.0304(13) Uani 1 1 d . . .
H34B H 0.4605 0.7081 0.6511 0.036 Uiso 1 1 calc R . .
C35B C 0.3652(4) 0.6599(4) 0.6158(3) 0.0268(12) Uani 1 1 d . . .
H35B H 0.3358 0.6196 0.6645 0.032 Uiso 1 1 calc R . .
C11C C 0.2023(5) 0.3399(4) 0.0490(4) 0.0311(13) Uani 1 1 d . . .
H11E H 0.1394 0.3372 0.0400 0.037 Uiso 1 1 calc R . .
H11F H 0.2536 0.3327 0.0020 0.037 Uiso 1 1 calc R . .
C12C C 0.3135(5) 0.4228(4) 0.0861(4) 0.0361(15) Uani 1 1 d . . .
H12E H 0.3690 0.4182 0.0407 0.043 Uiso 1 1 calc R . .
H12F H 0.3190 0.4703 0.1003 0.043 Uiso 1 1 calc R . .
C13C C 0.1147(5) 0.4288(4) 0.1531(3) 0.0307(13) Uani 1 1 d . . .
H13E H 0.1128 0.4760 0.1706 0.037 Uiso 1 1 calc R . .
H13F H 0.0487 0.4295 0.1476 0.037 Uiso 1 1 calc R . .
C14C C 0.1451(5) 0.2766(4) 0.1941(4) 0.0365(15) Uani 1 1 d . . .
H14E H 0.1550 0.2254 0.2415 0.044 Uiso 1 1 calc R . .
H14F H 0.0813 0.2784 0.1837 0.044 Uiso 1 1 calc R . .
C15C C 0.3148(5) 0.2718(4) 0.1382(4) 0.0410(16) Uani 1 1 d . . .
H15E H 0.3296 0.2202 0.1837 0.049 Uiso 1 1 calc R . .
H15F H 0.3661 0.2711 0.0891 0.049 Uiso 1 1 calc R . .
C16C C 0.2384(5) 0.3486(4) 0.2273(4) 0.0395(15) Uani 1 1 d . . .
H16E H 0.2501 0.2996 0.2760 0.047 Uiso 1 1 calc R . .
H16F H 0.2384 0.3995 0.2384 0.047 Uiso 1 1 calc R . .
C21C C 0.0953(5) 0.7565(4) -0.0557(4) 0.0412(16) Uani 1 1 d . . .
H21E H 0.1558 0.7726 -0.0965 0.049 Uiso 1 1 calc R . .
H21F H 0.0448 0.7645 -0.0856 0.049 Uiso 1 1 calc R . .
C22C C 0.0011(4) 0.6419(4) 0.0844(3) 0.0240(11) Uani 1 1 d . . .
H22E H -0.0528 0.6456 0.0598 0.029 Uiso 1 1 calc R . .
H22F H 0.0040 0.5876 0.1297 0.029 Uiso 1 1 calc R . .
C23C C 0.1941(4) 0.6567(4) 0.0650(4) 0.0338(14) Uani 1 1 d . . .
H23E H 0.2047 0.6028 0.1095 0.041 Uiso 1 1 calc R . .
H23F H 0.2581 0.6694 0.0285 0.041 Uiso 1 1 calc R . .
C24C C 0.1393(6) 0.8025(5) 0.0386(5) 0.0497(19) Uani 1 1 d . . .
H24E H 0.2021 0.8127 -0.0010 0.060 Uiso 1 1 calc R . .
H24F H 0.1212 0.8460 0.0640 0.060 Uiso 1 1 calc R . .
C25C C -0.0283(5) 0.7915(4) 0.0536(4) 0.0435(17) Uani 1 1 d . . .
H25E H -0.0527 0.8348 0.0792 0.052 Uiso 1 1 calc R . .
H25F H -0.0771 0.7931 0.0246 0.052 Uiso 1 1 calc R . .
C26C C 0.0579(4) 0.7059(4) 0.1561(4) 0.0341(14) Uani 1 1 d . . .
H26E H 0.0368 0.7468 0.1847 0.041 Uiso 1 1 calc R . .
H26F H 0.0661 0.6494 0.1977 0.041 Uiso 1 1 calc R . .
C31C C 0.1860(5) 0.5524(5) -0.1851(4) 0.0410(16) Uani 1 1 d . . .
H31C H 0.1395 0.5362 -0.2016 0.049 Uiso 1 1 calc R . .
C32C C 0.2622(5) 0.4996(4) -0.1526(4) 0.0426(17) Uani 1 1 d . . .
H32C H 0.2769 0.4413 -0.1433 0.051 Uiso 1 1 calc R . .
C33C C 0.3146(5) 0.5469(6) -0.1356(4) 0.050(2) Uani 1 1 d . . .
H33C H 0.3701 0.5261 -0.1124 0.059 Uiso 1 1 calc R . .
C34C C 0.2694(6) 0.6304(5) -0.1594(4) 0.052(2) Uani 1 1 d . . .
H34C H 0.2896 0.6763 -0.1558 0.063 Uiso 1 1 calc R . .
C35C C 0.1884(5) 0.6339(4) -0.1898(4) 0.0440(18) Uani 1 1 d . . .
H35C H 0.1441 0.6823 -0.2095 0.053 Uiso 1 1 calc R . .
O1W O 0.0286(5) 0.3066(3) 0.3757(3) 0.0622(16) Uani 1 1 d . . .
O2W O 0.0037(5) 0.9784(4) 0.9019(4) 0.0781(19) Uani 1 1 d . . .
O3W O 0.4246(4) 0.3198(4) 0.9255(4) 0.083(2) Uani 1 1 d . . .
O4W O 0.8303(5) 0.9562(4) 0.1277(4) 0.0708(17) Uani 1 1 d . . .
O5W O 0.5397(5) 0.9241(4) 0.3449(4) 0.089(3) Uani 1 1 d . . .
O6W O 0.8718(5) 0.3849(5) 0.4673(4) 0.0605(18) Uiso 0.80 1 d P . .
O7W O 0.0003(6) 0.5130(4) 0.2926(4) 0.068(2) Uani 0.80 1 d P . .
O8W O 0.7003(11) -0.0019(7) 0.2513(8) 0.054(3) Uani 0.60 1 d P . .
O9W O 0.6840(16) 0.0377(11) 0.2390(14) 0.054(5) Uani 0.40 1 d P . .
O10W O 0.4873(9) 0.2932(9) 0.2323(8) 0.062(3) Uani 0.59 1 d P . .
O11W O 0.4892(12) 0.3391(9) 0.1989(10) 0.043(4) Uani 0.41 1 d P . .
O12W O 0.3502(10) 0.2013(11) 0.8923(8) 0.062(4) Uani 0.47 1 d P . .
O13W O 0.311(2) 0.242(2) 0.9008(13) 0.064(7) Uani 0.28 1 d P . .
O14W O 0.8687(6) 0.6655(7) 0.5421(6) 0.058(2) Uani 0.60 1 d P . .
O15W O 0.8787(9) 0.5930(10) 0.5704(10) 0.060(4) Uani 0.40 1 d P . .
O16W O 0.7761(12) 0.8483(11) 0.9584(10) 0.063(4) Uiso 0.35 1 d P . .
O17W O 0.8475(14) 0.8715(12) 0.8744(12) 0.061(5) Uiso 0.30 1 d P . .
O18W O 0.5762(9) 0.0344(8) 0.0720(7) 0.068(3) Uani 0.50 1 d P . .
O19W O 0.4255(9) 0.7504(7) 0.9910(7) 0.061(3) Uiso 0.50 1 d P . .
O20W O 0.8126(10) 1.0019(8) 0.9666(9) 0.053(5) Uani 0.40 1 d P . .
O21W O 0.7723(7) 0.9690(7) 0.9815(6) 0.054(2) Uani 0.60 1 d P . .
O22W O 0.4422(12) 0.5813(10) 0.9711(10) 0.055(4) Uiso 0.33 1 d P . .
O23W O 0.344(2) 0.857(2) 0.070(2) 0.055(8) Uiso 0.17 1 d P . .


_geom_special_details            
; 
 All esds (except the esd in the dihedral angle between two l.s. planes) 
 are estimated using the full covariance matrix.  The cell esds are taken 
 into account individually in the estimation of esds in distances, angles 
 and torsion angles; correlations between esds in cell parameters are only 
 used when they are defined by crystal symmetry.  An approximate (isotropic) 
 treatment of cell esds is used for estimating esds involving l.s. planes. 
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ru1 N1P 2.029(5) . ?
Ru1 C33A 2.206(6) . ?
Ru1 C34A 2.219(6) . ?
Ru1 C32A 2.231(6) . ?
Ru1 C31A 2.233(5) . ?
Ru1 C35A 2.235(6) . ?
Ru1 P2A 2.2485(14) . ?
Ru1 P1A 2.2612(14) . ?
Ru2 N2P 2.013(5) . ?
Ru2 C33B 2.206(5) . ?
Ru2 C34B 2.214(5) . ?
Ru2 C35B 2.239(5) . ?
Ru2 C32B 2.240(5) . ?
Ru2 C31B 2.252(5) . ?
Ru2 P2B 2.2615(14) . ?
Ru2 P1B 2.2631(13) . ?
Ru3 N3P 2.011(5) . ?
Ru3 C33C 2.194(6) . ?
Ru3 C34C 2.199(6) . ?
Ru3 C32C 2.230(6) . ?
Ru3 C35C 2.231(6) . ?
Ru3 C31C 2.249(6) . ?
Ru3 P1C 2.2566(15) . ?
Ru3 P2C 2.2591(15) . ?
Cl1 Cl2 0.787(10) . ?
Cl3 Cl5 1.019(14) . ?
Cl3 Cl4 1.478(16) . ?
Cl4 Cl5 1.472(19) . ?
Cl6 Cl6 1.510(10) 2_766 ?
Cl6 O15W 2.125(14) . ?
P1A C13A 1.840(6) . ?
P1A C11A 1.846(7) . ?
P1A C12A 1.852(6) . ?
P2A C21A 1.841(6) . ?
P2A C23A 1.843(6) . ?
P2A C22A 1.854(5) . ?
P1B C12B 1.822(6) . ?
P1B C13B 1.827(7) . ?
P1B C11B 1.833(7) . ?
P2B C21B 1.841(6) . ?
P2B C22B 1.843(5) . ?
P2B C23B 1.844(5) . ?
P1C C12C 1.832(6) . ?
P1C C11C 1.843(6) . ?
P1C C13C 1.854(6) . ?
P2C C21C 1.840(6) . ?
P2C C23C 1.849(6) . ?
P2C C22C 1.850(5) . ?
N1P C1P 1.135(10) 2_556 ?
N1P N1P 1.135(10) 2_556 ?
N2P C2P 1.148(9) 2_666 ?
N2P N2P 1.148(9) 2_666 ?
N3P C3P 1.153(10) 2_565 ?
N3P N3P 1.153(10) 2_565 ?
N11A C14A 1.454(10) . ?
N11A C16A 1.472(8) . ?
N11A C13A 1.476(8) . ?
N12A C14A 1.461(13) . ?
N12A C15A 1.466(13) . ?
N12A C11A 1.475(9) . ?
N13A C16A 1.426(9) . ?
N13A C15A 1.438(11) . ?
N13A C12A 1.485(8) . ?
N21A C25A 1.454(8) . ?
N21A C22A 1.475(7) . ?
N21A C26A 1.478(8) . ?
N22A C24A 1.437(8) . ?
N22A C26A 1.462(8) . ?
N22A C23A 1.477(7) . ?
N23A C24A 1.465(9) . ?
N23A C25A 1.494(9) . ?
N23A C21A 1.497(8) . ?
N11B C14B 1.460(10) . ?
N11B C16B 1.461(10) . ?
N11B C13B 1.483(8) . ?
N12B C15B 1.440(12) . ?
N12B C14B 1.456(11) . ?
N12B C11B 1.476(8) . ?
N13B C15B 1.436(12) . ?
N13B C16B 1.444(11) . ?
N13B C12B 1.476(8) . ?
N21B C25B 1.462(8) . ?
N21B C26B 1.470(8) . ?
N21B C22B 1.472(7) . ?
N22B C24B 1.439(9) . ?
N22B C26B 1.466(8) . ?
N22B C23B 1.481(7) . ?
N23B C24B 1.473(9) . ?
N23B C25B 1.483(9) . ?
N23B C21B 1.487(7) . ?
N11C C13C 1.460(7) . ?
N11C C16C 1.468(8) . ?
N11C C14C 1.476(8) . ?
N12C C14C 1.456(9) . ?
N12C C11C 1.472(7) . ?
N12C C15C 1.481(9) . ?
N13C C15C 1.464(9) . ?
N13C C16C 1.470(9) . ?
N13C C12C 1.488(7) . ?
N21C C25C 1.449(8) . ?
N21C C22C 1.471(7) . ?
N21C C26C 1.473(8) . ?
N22C C24C 1.423(10) . ?
N22C C23C 1.468(8) . ?
N22C C26C 1.470(8) . ?
N23C C25C 1.485(9) . ?
N23C C21C 1.486(8) . ?
N23C C24C 1.498(11) . ?
C31A C35A 1.406(9) . ?
C31A C32A 1.419(9) . ?
C32A C33A 1.424(9) . ?
C33A C34A 1.389(10) . ?
C34A C35A 1.427(9) . ?
C31B C32B 1.408(8) . ?
C31B C35B 1.409(8) . ?
C32B C33B 1.418(9) . ?
C33B C34B 1.413(9) . ?
C34B C35B 1.428(9) . ?
C31C C32C 1.381(10) . ?
C31C C35C 1.405(10) . ?
C32C C33C 1.413(11) . ?
C33C C34C 1.407(11) . ?
C34C C35C 1.421(11) . ?
O8W O9W 0.648(14) . ?
O10W O11W 0.798(15) . ?
O12W O13W 0.85(3) . ?
O14W O15W 1.161(16) . ?
O16W O17W 1.55(3) . ?
O20W O21W 0.832(12) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N1P Ru1 C33A 151.8(2) . . ?
N1P Ru1 C34A 148.4(2) . . ?
C33A Ru1 C34A 36.6(3) . . ?
N1P Ru1 C32A 114.4(2) . . ?
C33A Ru1 C32A 37.4(2) . . ?
C34A Ru1 C32A 61.8(2) . . ?
N1P Ru1 C31A 95.7(2) . . ?
C33A Ru1 C31A 62.0(2) . . ?
C34A Ru1 C31A 61.8(2) . . ?
C32A Ru1 C31A 37.1(2) . . ?
N1P Ru1 C35A 111.4(2) . . ?
C33A Ru1 C35A 61.8(2) . . ?
C34A Ru1 C35A 37.4(2) . . ?
C32A Ru1 C35A 61.7(2) . . ?
C31A Ru1 C35A 36.7(2) . . ?
N1P Ru1 P2A 88.05(14) . . ?
C33A Ru1 P2A 119.82(18) . . ?
C34A Ru1 P2A 93.75(17) . . ?
C32A Ru1 P2A 155.30(18) . . ?
C31A Ru1 P2A 135.95(18) . . ?
C35A Ru1 P2A 101.66(17) . . ?
N1P Ru1 P1A 85.39(14) . . ?
C33A Ru1 P1A 95.62(18) . . ?
C34A Ru1 P1A 125.80(19) . . ?
C32A Ru1 P1A 97.04(17) . . ?
C31A Ru1 P1A 129.21(18) . . ?
C35A Ru1 P1A 156.62(17) . . ?
P2A Ru1 P1A 94.83(5) . . ?
N2P Ru2 C33B 151.6(2) . . ?
N2P Ru2 C34B 147.7(2) . . ?
C33B Ru2 C34B 37.3(2) . . ?
N2P Ru2 C35B 110.8(2) . . ?
C33B Ru2 C35B 62.0(2) . . ?
C34B Ru2 C35B 37.4(2) . . ?
N2P Ru2 C32B 114.4(2) . . ?
C33B Ru2 C32B 37.2(2) . . ?
C34B Ru2 C32B 62.2(2) . . ?
C35B Ru2 C32B 61.6(2) . . ?
N2P Ru2 C31B 95.86(19) . . ?
C33B Ru2 C31B 61.4(2) . . ?
C34B Ru2 C31B 61.7(2) . . ?
C35B Ru2 C31B 36.6(2) . . ?
C32B Ru2 C31B 36.5(2) . . ?
N2P Ru2 P2B 84.27(14) . . ?
C33B Ru2 P2B 123.44(18) . . ?
C34B Ru2 P2B 94.75(16) . . ?
C35B Ru2 P2B 99.98(15) . . ?
C32B Ru2 P2B 156.88(16) . . ?
C31B Ru2 P2B 133.21(15) . . ?
N2P Ru2 P1B 87.06(13) . . ?
C33B Ru2 P1B 95.10(17) . . ?
C34B Ru2 P1B 125.01(17) . . ?
C35B Ru2 P1B 156.68(15) . . ?
C32B Ru2 P1B 97.94(16) . . ?
C31B Ru2 P1B 130.30(15) . . ?
P2B Ru2 P1B 96.49(5) . . ?
N3P Ru3 C33C 150.2(3) . . ?
N3P Ru3 C34C 149.0(3) . . ?
C33C Ru3 C34C 37.4(3) . . ?
N3P Ru3 C32C 113.2(2) . . ?
C33C Ru3 C32C 37.3(3) . . ?
C34C Ru3 C32C 61.7(3) . . ?
N3P Ru3 C35C 111.9(3) . . ?
C33C Ru3 C35C 62.3(3) . . ?
C34C Ru3 C35C 37.4(3) . . ?
C32C Ru3 C35C 61.1(2) . . ?
N3P Ru3 C31C 95.9(2) . . ?
C33C Ru3 C31C 61.4(3) . . ?
C34C Ru3 C31C 61.4(3) . . ?
C32C Ru3 C31C 35.9(3) . . ?
C35C Ru3 C31C 36.6(3) . . ?
N3P Ru3 P1C 81.88(14) . . ?
C33C Ru3 P1C 96.9(2) . . ?
C34C Ru3 P1C 128.3(3) . . ?
C32C Ru3 P1C 97.92(18) . . ?
C35C Ru3 P1C 157.83(18) . . ?
C31C Ru3 P1C 128.3(2) . . ?
N3P Ru3 P2C 89.31(15) . . ?
C33C Ru3 P2C 120.4(2) . . ?
C34C Ru3 P2C 94.46(19) . . ?
C32C Ru3 P2C 155.79(19) . . ?
C35C Ru3 P2C 103.19(19) . . ?
C31C Ru3 P2C 137.76(19) . . ?
P1C Ru3 P2C 93.94(5) . . ?
Cl5 Cl3 Cl4 69.5(10) . . ?
Cl5 Cl4 Cl3 40.4(7) . . ?
Cl3 Cl5 Cl4 70.1(10) . . ?
Cl6 Cl6 O15W 114.4(5) 2_766 . ?
C13A P1A C11A 97.9(4) . . ?
C13A P1A C12A 97.3(3) . . ?
C11A P1A C12A 97.4(4) . . ?
C13A P1A Ru1 121.9(2) . . ?
C11A P1A Ru1 115.2(2) . . ?
C12A P1A Ru1 121.9(2) . . ?
C21A P2A C23A 97.7(3) . . ?
C21A P2A C22A 97.8(3) . . ?
C23A P2A C22A 97.1(3) . . ?
C21A P2A Ru1 115.76(19) . . ?
C23A P2A Ru1 120.48(19) . . ?
C22A P2A Ru1 122.92(18) . . ?
C12B P1B C13B 98.2(4) . . ?
C12B P1B C11B 96.9(4) . . ?
C13B P1B C11B 97.1(4) . . ?
C12B P1B Ru2 120.3(2) . . ?
C13B P1B Ru2 123.6(2) . . ?
C11B P1B Ru2 115.3(2) . . ?
C21B P2B C22B 97.2(3) . . ?
C21B P2B C23B 97.1(3) . . ?
C22B P2B C23B 97.8(3) . . ?
C21B P2B Ru2 111.40(19) . . ?
C22B P2B Ru2 124.07(18) . . ?
C23B P2B Ru2 123.41(19) . . ?
C12C P1C C11C 97.9(3) . . ?
C12C P1C C13C 98.2(3) . . ?
C11C P1C C13C 97.1(3) . . ?
C12C P1C Ru3 123.3(2) . . ?
C11C P1C Ru3 114.64(19) . . ?
C13C P1C Ru3 120.6(2) . . ?
C21C P2C C23C 97.1(3) . . ?
C21C P2C C22C 97.5(3) . . ?
C23C P2C C22C 97.6(3) . . ?
C21C P2C Ru3 117.1(2) . . ?
C23C P2C Ru3 120.1(2) . . ?
C22C P2C Ru3 122.11(19) . . ?
C1P N1P N1P 0.0(5) 2_556 2_556 ?
C1P N1P Ru1 177.7(6) 2_556 . ?
N1P N1P Ru1 177.7(6) 2_556 . ?
C2P N2P N2P 0.0(5) 2_666 2_666 ?
C2P N2P Ru2 176.8(6) 2_666 . ?
N2P N2P Ru2 176.8(6) 2_666 . ?
C3P N3P N3P 0.0(5) 2_565 2_565 ?
C3P N3P Ru3 174.4(6) 2_565 . ?
N3P N3P Ru3 174.4(6) 2_565 . ?
C14A N11A C16A 108.4(6) . . ?
C14A N11A C13A 111.8(5) . . ?
C16A N11A C13A 109.4(5) . . ?
C14A N12A C15A 109.1(6) . . ?
C14A N12A C11A 111.7(8) . . ?
C15A N12A C11A 110.1(8) . . ?
C16A N13A C15A 109.1(6) . . ?
C16A N13A C12A 111.8(6) . . ?
C15A N13A C12A 112.0(6) . . ?
C25A N21A C22A 111.5(4) . . ?
C25A N21A C26A 109.2(5) . . ?
C22A N21A C26A 110.6(4) . . ?
C24A N22A C26A 108.3(5) . . ?
C24A N22A C23A 110.8(5) . . ?
C26A N22A C23A 111.0(4) . . ?
C24A N23A C25A 107.8(5) . . ?
C24A N23A C21A 110.6(5) . . ?
C25A N23A C21A 109.3(5) . . ?
C14B N11B C16B 108.1(6) . . ?
C14B N11B C13B 111.1(6) . . ?
C16B N11B C13B 111.0(6) . . ?
C15B N12B C14B 107.7(6) . . ?
C15B N12B C11B 111.0(7) . . ?
C14B N12B C11B 111.4(7) . . ?
C15B N13B C16B 108.6(6) . . ?
C15B N13B C12B 112.2(7) . . ?
C16B N13B C12B 110.8(7) . . ?
C25B N21B C26B 108.5(5) . . ?
C25B N21B C22B 111.7(5) . . ?
C26B N21B C22B 110.8(5) . . ?
C24B N22B C26B 109.1(5) . . ?
C24B N22B C23B 111.7(5) . . ?
C26B N22B C23B 110.9(5) . . ?
C24B N23B C25B 108.6(5) . . ?
C24B N23B C21B 110.1(5) . . ?
C25B N23B C21B 110.6(5) . . ?
C13C N11C C16C 110.6(5) . . ?
C13C N11C C14C 112.3(5) . . ?
C16C N11C C14C 108.0(5) . . ?
C14C N12C C11C 111.0(5) . . ?
C14C N12C C15C 108.0(5) . . ?
C11C N12C C15C 110.3(5) . . ?
C15C N13C C16C 108.6(5) . . ?
C15C N13C C12C 110.9(5) . . ?
C16C N13C C12C 111.2(5) . . ?
C25C N21C C22C 111.5(5) . . ?
C25C N21C C26C 108.6(5) . . ?
C22C N21C C26C 111.0(5) . . ?
C24C N22C C23C 111.4(5) . . ?
C24C N22C C26C 108.3(6) . . ?
C23C N22C C26C 110.9(5) . . ?
C25C N23C C21C 110.6(6) . . ?
C25C N23C C24C 108.1(6) . . ?
C21C N23C C24C 110.5(6) . . ?
N12A C11A P1A 112.5(5) . . ?
N13A C12A P1A 110.9(5) . . ?
N11A C13A P1A 113.1(5) . . ?
N11A C14A N12A 113.7(6) . . ?
N13A C15A N12A 114.0(6) . . ?
N13A C16A N11A 115.0(5) . . ?
N23A C21A P2A 113.0(4) . . ?
N21A C22A P2A 112.6(4) . . ?
N22A C23A P2A 113.2(4) . . ?
N22A C24A N23A 116.6(5) . . ?
N21A C25A N23A 114.3(5) . . ?
N22A C26A N21A 114.1(5) . . ?
C35A C31A C32A 108.3(6) . . ?
C35A C31A Ru1 71.8(3) . . ?
C32A C31A Ru1 71.4(3) . . ?
C31A C32A C33A 107.1(6) . . ?
C31A C32A Ru1 71.5(3) . . ?
C33A C32A Ru1 70.3(3) . . ?
C34A C33A C32A 108.7(6) . . ?
C34A C33A Ru1 72.2(3) . . ?
C32A C33A Ru1 72.2(3) . . ?
C33A C34A C35A 108.2(6) . . ?
C33A C34A Ru1 71.2(3) . . ?
C35A C34A Ru1 71.9(3) . . ?
C31A C35A C34A 107.7(6) . . ?
C31A C35A Ru1 71.6(3) . . ?
C34A C35A Ru1 70.7(3) . . ?
N12B C11B P1B 113.3(5) . . ?
N13B C12B P1B 112.5(5) . . ?
N11B C13B P1B 112.7(5) . . ?
N12B C14B N11B 114.0(6) . . ?
N13B C15B N12B 114.8(6) . . ?
N13B C16B N11B 114.0(6) . . ?
N23B C21B P2B 113.5(4) . . ?
N21B C22B P2B 113.1(4) . . ?
N22B C23B P2B 112.2(4) . . ?
N22B C24B N23B 114.5(5) . . ?
N21B C25B N23B 113.6(5) . . ?
N22B C26B N21B 114.1(5) . . ?
C32B C31B C35B 109.0(5) . . ?
C32B C31B Ru2 71.3(3) . . ?
C35B C31B Ru2 71.2(3) . . ?
C31B C32B C33B 107.4(5) . . ?
C31B C32B Ru2 72.2(3) . . ?
C33B C32B Ru2 70.1(3) . . ?
C34B C33B C32B 108.6(5) . . ?
C34B C33B Ru2 71.7(3) . . ?
C32B C33B Ru2 72.7(3) . . ?
C33B C34B C35B 107.4(5) . . ?
C33B C34B Ru2 71.1(3) . . ?
C35B C34B Ru2 72.3(3) . . ?
C31B C35B C34B 107.6(5) . . ?
C31B C35B Ru2 72.2(3) . . ?
C34B C35B Ru2 70.3(3) . . ?
N12C C11C P1C 113.6(4) . . ?
N13C C12C P1C 112.1(4) . . ?
N11C C13C P1C 112.5(4) . . ?
N12C C14C N11C 114.5(5) . . ?
N13C C15C N12C 114.5(5) . . ?
N11C C16C N13C 114.2(5) . . ?
N23C C21C P2C 112.8(4) . . ?
N21C C22C P2C 112.7(4) . . ?
N22C C23C P2C 113.2(5) . . ?
N22C C24C N23C 114.9(6) . . ?
N21C C25C N23C 113.8(5) . . ?
N22C C26C N21C 114.7(5) . . ?
C32C C31C C35C 109.0(7) . . ?
C32C C31C Ru3 71.3(4) . . ?
C35C C31C Ru3 71.0(4) . . ?
C31C C32C C33C 108.6(6) . . ?
C31C C32C Ru3 72.8(4) . . ?
C33C C32C Ru3 70.0(4) . . ?
C34C C33C C32C 107.3(6) . . ?
C34C C33C Ru3 71.5(4) . . ?
C32C C33C Ru3 72.8(4) . . ?
C33C C34C C35C 108.1(6) . . ?
C33C C34C Ru3 71.1(4) . . ?
C35C C34C Ru3 72.5(4) . . ?
C31C C35C C34C 107.0(6) . . ?
C31C C35C Ru3 72.4(3) . . ?
C34C C35C Ru3 70.1(4) . . ?
O14W O15W Cl6 136.0(13) . . ?

_diffrn_measured_fraction_theta_max 0.974
_diffrn_reflns_theta_full        25.04
_diffrn_measured_fraction_theta_full 0.974
_refine_diff_density_max         2.841
_refine_diff_density_min         -0.849
_refine_diff_density_rms         0.176
_database_code_depnum_ccdc_archive 'CCDC 1000027'
