# Electronic Supplementary Material (ESI) for CrystEngComm
# This journal is © The Royal Society of Chemistry 2012


data_global
_journal_name_full               CrystEngComm
_journal_coden_cambridge         1350
_journal_year                    ?
_journal_volume                  ?
_journal_page_first              ?
_publ_contact_author_name        'Karla Fejfarova'
_publ_contact_author_email       fejfarov@fzu.cz
loop_
_publ_author_name
'I. Matulkova'
'J. Cihelka'
'M. Pojarova'
'K. Fejfarova'
'M. Dusek'
'P. Vanek'
;
J.Kroupa
;
'R. Krupkova'
'J. Fabry'
'I. Nemec'

data_I
_database_code_depnum_ccdc_archive 'CCDC 831896'
#TrackingRef '6000_web_deposit_cif_file_0_KarlaFejfarova_1309265877.dat_h2seo4_1_precislovany.cif'

#=======================================================================

# 5. CHEMICAL DATA

_chemical_name_systematic        
; ?
;
_chemical_name_common            ?
_chemical_formula_moiety         '2(C2 H6 N5), O4 Se, 2(H2 O)'
_chemical_formula_structural     ?
_chemical_formula_analytical     ?
_chemical_formula_iupac          ?
_chemical_formula_sum            'C4 H16 N10 O6 Se1'
_chemical_formula_weight         379.2
_chemical_melting_point          ?
_chemical_compound_source        ?
_chemical_absolute_configuration .

#=======================================================================

# 6. CRYSTAL DATA

_symmetry_cell_setting           triclinic
_symmetry_space_group_name_H-M   'P -1'
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_Int_Tables_number      2
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 x,y,z
2 -x,-y,-z
_cell_length_a                   6.16030(10)
_cell_length_b                   6.3726(2)
_cell_length_c                   17.9756(5)
_cell_angle_alpha                97.743(2)
_cell_angle_beta                 99.269(2)
_cell_angle_gamma                96.969(2)
_cell_volume                     682.69(3)
_cell_formula_units_Z            2

_cell_measurement_reflns_used    10452
_cell_measurement_theta_min      5.0438
_cell_measurement_theta_max      66.8427
_cell_measurement_temperature    120
_cell_special_details            
; ?
;

_exptl_crystal_density_diffrn    1.8441
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             384

_exptl_absorpt_coefficient_mu    4.226
_exptl_crystal_description       prism
_exptl_crystal_size_max          0.1995
_exptl_crystal_size_mid          0.1537
_exptl_crystal_size_min          0.1139
_exptl_crystal_colour            colorless
_exptl_absorpt_correction_T_min  0.575
_exptl_absorpt_correction_T_max  0.724
_exptl_absorpt_correction_type   analytical
_exptl_absorpt_process_details   
;
CrysAlisPro, Oxford Diffraction (2009)
Analytical numeric absorption correction using a multifaceted crystal
model.
;

#=======================================================================

# 7. EXPERIMENTAL DATA

_exptl_special_details           ?

_diffrn_ambient_temperature      120
_diffrn_radiation_type           'Cu K\a'
_diffrn_radiation_source         'X-ray tube'
_diffrn_radiation_wavelength     1.54184
_diffrn_measurement_device       'four-cycle diffractometer'
_diffrn_radiation_monochromator  mirror
_diffrn_measurement_device_type  
'Goniometer Xcalibur, detector: Atlas (Gemini ultra Cu)'
_diffrn_detector_area_resol_mean 10.3784
_diffrn_measurement_method       
'Rotation method data acquisition using \w scans'
_diffrn_reflns_number            10277
_diffrn_reflns_theta_min         5.05
_diffrn_reflns_theta_max         66.99
_diffrn_reflns_theta_full        66.38
_diffrn_measured_fraction_theta_max 0.97
_diffrn_measured_fraction_theta_full 0.98
_diffrn_reflns_av_R_equivalents  0.0219
_diffrn_reflns_av_sigmaI/netI    0.0042
_diffrn_reflns_limit_h_min       -7
_diffrn_reflns_limit_h_max       7
_diffrn_reflns_limit_k_min       -7
_diffrn_reflns_limit_k_max       7
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_limit_l_max       21
_diffrn_reflns_reduction_process 
;
Integration of the CCD images was done by program Crysalis RED
(Oxford diffraction, 2009). The same program was used for indexing of the
crystal shape and absorption correction.
;

#=======================================================================

# 8. REFINEMENT DATA

_refine_special_details          
;
The refinement was carried out against all reflections. The conventional
R-factor is always based on F. The goodness of fit as well as the weighted
R-factor are based on F and F^2^ for refinement carried out on F and F^2^,
respectively. The threshold expression is used only for calculating
R-factors etc. and it is not relevant to the choice of reflections for
refinement.

The program used for refinement, Jana2006, uses the weighting scheme
based on the experimental expectations, see _refine_ls_weighting_details,
that does not force S to be one. Therefore the values of S are usually larger
than the ones from the SHELX program.
;

_reflns_number_total             2365
_reflns_number_gt                2342
_reflns_threshold_expression     I>3\s(I)

_refine_ls_structure_factor_coef Fsqd
_refine_ls_R_factor_gt           0.0221
_refine_ls_wR_factor_gt          0.0763
_refine_ls_R_factor_all          0.0223
_refine_ls_wR_factor_ref         0.0765
_refine_ls_goodness_of_fit_ref   1.86
_refine_ls_goodness_of_fit_gt    1.87
_refine_ls_restrained_S_gt       ?
_refine_ls_restrained_S_all      ?
_refine_ls_number_reflns         2365
_refine_ls_number_parameters     239
_refine_ls_number_restraints     16
_refine_ls_number_constraints    16
_refine_ls_weighting_scheme      sigma
_refine_ls_weighting_details     w=1/(\s^2^(I)+0.0016I^2^)
_refine_ls_hydrogen_treatment    refxyz
_refine_ls_shift/su_max          0.0072
_refine_ls_shift/su_mean         0.0005
_refine_diff_density_max         0.31
_refine_diff_density_min         -0.32
_refine_ls_extinction_method     
'B-C type 1 Lorentzian isotropic (Becker & Coppens, 1974)'
_refine_ls_extinction_coef       290(90)
_refine_ls_abs_structure_details ?
_refine_ls_abs_structure_Flack   ?
_refine_ls_abs_structure_Rogers  ?

loop_
_atom_type_symbol
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C 0.0181 0.0091 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1'
H 0.0000 0.0000 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1'
N 0.0311 0.0180 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1'
O 0.0492 0.0322 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1'
Se -0.7943 1.1372 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1'

_computing_data_collection       'Crysalis CCD (Oxford diffraction, 2009)'
_computing_cell_refinement       'Crysalis RED (Oxford diffraction, 2009)'
_computing_data_reduction        'Crysalis RED'
_computing_structure_solution    'SIR2002 (Burla et al., 2003)'
_computing_structure_refinement  
"Jana2006 (Pet\<r\'i\<cek, Du\<sek & Palatinus, 2006)"
_computing_molecular_graphics    'Diamond (Brandenburg & Putz, 2005)'
_computing_publication_material  Jana2006

#=======================================================================

# 9. ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_adp_type
_atom_site_U_iso_or_equiv
_atom_site_symmetry_multiplicity
_atom_site_occupancy
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Se1 Se 0.75754(2) 0.13844(2) 0.727875(8) Uani 0.01216(10) 2 1 d . . .
O1 O 0.5568(2) 0.2868(2) 0.72635(7) Uani 0.0180(4) 2 1 d . . .
O2 O 0.66770(19) -0.08958(20) 0.67102(7) Uani 0.0182(4) 2 1 d . . .
O3 O 0.9744(2) 0.2662(2) 0.70289(7) Uani 0.0202(4) 2 1 d . . .
O4 O 0.82874(19) 0.08771(19) 0.81489(7) Uani 0.0160(4) 2 1 d . . .
O1W O 0.1141(2) 0.6733(2) 0.78612(8) Uani 0.0225(4) 2 1 d . . .
O2W O 0.5882(2) 0.6775(2) 0.81634(8) Uani 0.0224(4) 2 1 d . . .
N2 N 0.8468(2) 0.2421(2) 0.49921(8) Uani 0.0142(4) 2 1 d . . .
N1 N 1.0390(2) 0.2719(2) 0.55607(8) Uani 0.0130(4) 2 1 d . . .
N4 N 1.1552(2) 0.2432(2) 0.44940(8) Uani 0.0127(4) 2 1 d . . .
N6 N 1.4290(2) 0.3011(3) 0.56341(9) Uani 0.0194(5) 2 1 d . . .
N7 N 0.8093(3) 0.1943(3) 0.36485(9) Uani 0.0214(5) 2 1 d . . .
N9 N 0.3425(2) 0.2390(2) 0.98524(8) Uani 0.0134(4) 2 1 d . . .
N8 N 0.5321(2) 0.2679(2) 1.04324(8) Uani 0.0134(4) 2 1 d . . .
N11 N 0.6558(2) 0.2385(2) 0.93816(8) Uani 0.0138(4) 2 1 d . . .
N13 N 0.9239(2) 0.2981(3) 1.05367(9) Uani 0.0190(5) 2 1 d . . .
N14 N 0.3126(2) 0.1762(3) 0.85076(9) Uani 0.0223(5) 2 1 d . . .
C5 C 1.2207(3) 0.2714(3) 0.52593(10) Uani 0.0140(5) 2 1 d . . .
C3 C 0.9258(3) 0.2251(3) 0.43597(10) Uani 0.0135(5) 2 1 d . . .
C12 C 0.7171(3) 0.2687(2) 1.01485(10) Uani 0.0133(5) 2 1 d . . .
C10 C 0.4262(3) 0.2182(3) 0.92260(10) Uani 0.0142(5) 2 1 d . . .
H1W H 0.079(4) 0.551(2) 0.7632(13) Uiso 0.027 2 1 d . . .
H2W H 0.2471(18) 0.686(4) 0.7846(14) Uiso 0.027 2 1 d . . .
H3W H 0.626(4) 0.572(3) 0.7935(13) Uiso 0.0269 2 1 d . . .
H4W H 0.679(3) 0.773(3) 0.8089(14) Uiso 0.0269 2 1 d . . .
H1A H 1.027(3) 0.279(3) 0.6034(6) Uiso 0.0155 2 1 d . . .
H4A H 1.237(3) 0.210(3) 0.4156(10) Uiso 0.0153 2 1 d . . .
H6A H 1.537(3) 0.273(3) 0.5398(12) Uiso 0.0233 2 1 d . . .
H6B H 1.461(4) 0.304(4) 0.6125(6) Uiso 0.0233 2 1 d . . .
H7A H 0.6675(17) 0.158(4) 0.3557(14) Uiso 0.0256 2 1 d . . .
H7B H 0.884(4) 0.202(4) 0.3278(10) Uiso 0.0256 2 1 d . . .
H8A H 0.509(3) 0.291(3) 1.0898(7) Uiso 0.016 2 1 d . . .
H11A H 0.740(3) 0.211(3) 0.9046(10) Uiso 0.0166 2 1 d . . .
H13A H 1.037(3) 0.286(3) 1.0310(12) Uiso 0.0228 2 1 d . . .
H13B H 0.943(4) 0.296(4) 1.1027(6) Uiso 0.0228 2 1 d . . .
H14A H 0.380(4) 0.207(4) 0.8138(10) Uiso 0.0268 2 1 d . . .
H14B H 0.1693(16) 0.145(4) 0.8429(14) Uiso 0.0268 2 1 d . . .

loop_
_atom_site_aniso_label
_atom_site_aniso_type_symbol
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
Se1 Se 0.00983(17) 0.01650(17) 0.00965(16) 0.00230(10) 0.00138(10) 0.00040(10)
O1 O 0.0169(6) 0.0223(6) 0.0158(6) 0.0086(5) 0.0011(5) 0.0030(5)
O2 O 0.0139(6) 0.0211(6) 0.0165(6) 0.0017(5) 0.0010(5) -0.0052(5)
O3 O 0.0165(6) 0.0288(7) 0.0140(6) -0.0031(5) 0.0056(5) 0.0009(5)
O4 O 0.0135(6) 0.0230(6) 0.0117(6) 0.0053(5) 0.0009(4) 0.0028(5)
O1W O 0.0223(7) 0.0244(7) 0.0197(7) 0.0027(5) 0.0029(5) 0.0011(5)
O2W O 0.0295(7) 0.0194(7) 0.0200(7) 0.0004(6) 0.0129(6) 0.0016(5)
N2 N 0.0110(7) 0.0161(7) 0.0144(7) 0.0030(5) 0.0000(5) 0.0008(5)
N1 N 0.0116(7) 0.0183(7) 0.0091(7) 0.0039(5) 0.0013(5) 0.0018(5)
N4 N 0.0112(7) 0.0160(7) 0.0118(7) 0.0038(5) 0.0035(5) 0.0015(5)
N6 N 0.0136(7) 0.0315(8) 0.0130(7) 0.0049(6) 0.0012(6) 0.0028(6)
N7 N 0.0128(7) 0.0341(9) 0.0149(8) 0.0012(6) -0.0008(6) 0.0018(6)
N9 N 0.0106(7) 0.0163(7) 0.0130(7) 0.0028(5) 0.0004(5) 0.0019(5)
N8 N 0.0109(7) 0.0181(7) 0.0108(7) 0.0035(5) 0.0011(5) 0.0009(6)
N11 N 0.0104(7) 0.0179(7) 0.0141(7) 0.0032(5) 0.0046(5) 0.0020(5)
N13 N 0.0131(7) 0.0295(8) 0.0143(8) 0.0032(6) 0.0017(6) 0.0036(6)
N14 N 0.0121(7) 0.0403(9) 0.0130(8) 0.0006(6) 0.0010(6) 0.0027(7)
C5 C 0.0149(8) 0.0118(8) 0.0160(9) 0.0053(6) 0.0027(6) 0.0026(6)
C3 C 0.0125(8) 0.0116(8) 0.0165(9) 0.0031(6) 0.0025(6) 0.0013(6)
C12 C 0.0147(8) 0.0110(8) 0.0144(8) 0.0033(6) 0.0028(6) 0.0012(6)
C10 C 0.0120(8) 0.0126(8) 0.0180(9) 0.0026(6) 0.0015(6) 0.0029(7)

#=======================================================================

# 10. MOLECULAR GEOMETRY

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_1
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Se1 O1 . . 1.6442(13) ?
Se1 O2 . . 1.6386(11) ?
Se1 O3 . . 1.6360(13) ?
Se1 O4 . . 1.6410(12) ?
O1W H1W . . 0.819(14) ?
O1W H2W . . 0.819(12) ?
O2W H3W . . 0.82(2) ?
O2W H4W . . 0.81(2) ?
N2 N1 . . 1.4095(18) ?
N2 C3 . . 1.303(2) ?
N1 C5 . . 1.319(2) ?
N1 H1A . . 0.861(13) ?
N4 C5 . . 1.351(2) ?
N4 C3 . . 1.383(2) ?
N4 H4A . . 0.869(19) ?
N6 C5 . . 1.329(2) ?
N6 H6A . . 0.87(2) ?
N6 H6B . . 0.870(11) ?
N7 C3 . . 1.338(2) ?
N7 H7A . . 0.859(10) ?
N7 H7B . . 0.87(2) ?
N9 N8 . . 1.4104(18) ?
N9 C10 . . 1.310(2) ?
N8 C12 . . 1.321(2) ?
N8 H8A . . 0.869(14) ?
N11 C12 . . 1.350(2) ?
N11 C10 . . 1.383(2) ?
N11 H11A . . 0.871(19) ?
N13 C12 . . 1.329(2) ?
N13 H13A . . 0.867(19) ?
N13 H13B . . 0.871(11) ?
N14 C10 . . 1.341(2) ?
N14 H14A . . 0.87(2) ?
N14 H14B . . 0.865(10) ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_2
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
O1 Se1 O2 . . . 109.45(6) ?
O1 Se1 O3 . . . 110.11(7) ?
O1 Se1 O4 . . . 108.96(6) ?
O2 Se1 O3 . . . 111.18(6) ?
O2 Se1 O4 . . . 108.26(6) ?
O3 Se1 O4 . . . 108.83(6) ?
H1W O1W H2W . . . 98(2) ?
H3W O2W H4W . . . 101(2) ?
N1 N2 C3 . . . 103.25(13) ?
N2 N1 C5 . . . 111.42(14) ?
N2 N1 H1A . . . 119.9(14) ?
C5 N1 H1A . . . 128.5(14) ?
C5 N4 C3 . . . 106.49(15) ?
C5 N4 H4A . . . 126.1(11) ?
C3 N4 H4A . . . 125.7(10) ?
C5 N6 H6A . . . 120.6(12) ?
C5 N6 H6B . . . 122.3(15) ?
H6A N6 H6B . . . 114(2) ?
C3 N7 H7A . . . 121.4(17) ?
C3 N7 H7B . . . 117.3(12) ?
H7A N7 H7B . . . 121(2) ?
N8 N9 C10 . . . 103.04(13) ?
N9 N8 C12 . . . 111.74(14) ?
N9 N8 H8A . . . 116.1(14) ?
C12 N8 H8A . . . 131.9(13) ?
C12 N11 C10 . . . 106.89(15) ?
C12 N11 H11A . . . 126.7(11) ?
C10 N11 H11A . . . 125.4(11) ?
C12 N13 H13A . . . 121.8(12) ?
C12 N13 H13B . . . 118.3(15) ?
H13A N13 H13B . . . 118(2) ?
C10 N14 H14A . . . 119.0(12) ?
C10 N14 H14B . . . 119.4(17) ?
H14A N14 H14B . . . 120(2) ?
N1 C5 N4 . . . 106.89(14) ?
N1 C5 N6 . . . 126.80(16) ?
N4 C5 N6 . . . 126.27(17) ?
N2 C3 N4 . . . 111.95(14) ?
N2 C3 N7 . . . 126.94(16) ?
N4 C3 N7 . . . 121.11(16) ?
N8 C12 N11 . . . 106.59(14) ?
N8 C12 N13 . . . 127.09(16) ?
N11 C12 N13 . . . 126.31(17) ?
N9 C10 N11 . . . 111.70(14) ?
N9 C10 N14 . . . 126.73(15) ?
N11 C10 N14 . . . 121.54(17) ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion
_geom_torsion_publ_flag
? ? ? ? ? ? ? ? ? ?

loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_site_symmetry_D
_geom_hbond_site_symmetry_H
_geom_hbond_site_symmetry_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_publ_flag
O1W H1W O3 . . 1_455 0.819(14) 1.960(14) 2.7765(17) 175(2) ?
O1W H2W O2W . . . 0.819(12) 2.097(12) 2.8797(19) 160(3) ?
O2W H3W O1 . . . 0.82(2) 2.001(17) 2.7478(17) 152(2) ?
O2W H4W O4 . . 1_565 0.81(2) 2.087(19) 2.8496(17) 156(2) ?
N1 H1A O3 . . . 0.861(13) 1.879(13) 2.736(2) 173.4(19) ?
N4 H4A O2 . . 2_756 0.869(19) 1.855(18) 2.699(2) 163.1(15) ?
N6 H6A N2 . . 1_655 0.87(2) 2.174(19) 3.028(2) 168.9(16) ?
N6 H6B O1 . . 1_655 0.870(11) 2.058(12) 2.925(2) 174(2) ?
N7 H7A O2 . . 2_656 0.859(10) 2.022(10) 2.8799(19) 176(2) ?
N7 H7B O1W . . 2_666 0.87(2) 2.29(2) 3.038(2) 143(2) ?
N8 H8A O2W . . 2_667 0.869(14) 1.872(15) 2.733(2) 171.0(19) ?
N11 H11A O4 . . . 0.871(19) 1.888(19) 2.721(2) 159.4(16) ?
N13 H13A N9 . . 1_655 0.867(19) 2.210(19) 3.072(2) 173(2) ?
N13 H13B O1W . . 2_667 0.871(11) 2.073(13) 2.910(2) 161(2) ?
N14 H14A O1 . . . 0.87(2) 2.13(2) 3.002(2) 177.8(18) ?
N14 H14B O4 . . 1_455 0.865(10) 2.052(10) 2.9144(18) 174(3) ?

#=======================================================================

# Attachment '6001_web_deposit_cif_file_1_KarlaFejfarova_1309265877.DAT_H2SO4_1_precislovany.cif'

#=======================================================================
data_II
_database_code_depnum_ccdc_archive 'CCDC 831897'
#TrackingRef '6001_web_deposit_cif_file_1_KarlaFejfarova_1309265877.DAT_H2SO4_1_precislovany.cif'

#=======================================================================

# 5. CHEMICAL DATA

_chemical_name_systematic        
; ?
;
_chemical_name_common            ?
_chemical_formula_moiety         '2(C2 H6 N5), O4 S, 2(H2 O)'
_chemical_formula_structural     ?
_chemical_formula_analytical     ?
_chemical_formula_iupac          ?
_chemical_formula_sum            'C4 H16 N10 O6 S1'
_chemical_formula_weight         332.3
_chemical_melting_point          ?
_chemical_compound_source        ?
_chemical_absolute_configuration .

#=======================================================================

# 6. CRYSTAL DATA

_symmetry_cell_setting           triclinic
_symmetry_space_group_name_H-M   'P -1'
_symmetry_space_group_name_Hall  '-P 1'
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 x,y,z
2 -x,-y,-z
_cell_length_a                   6.1197(2)
_cell_length_b                   6.3410(2)
_cell_length_c                   17.7076(6)
_cell_angle_alpha                99.528(3)
_cell_angle_beta                 98.220(3)
_cell_angle_gamma                96.967(3)
_cell_volume                     663.26(4)
_cell_formula_units_Z            2

_cell_measurement_reflns_used    5717
_cell_measurement_theta_min      5.1301
_cell_measurement_theta_max      62.3790
_cell_measurement_temperature    120
_cell_special_details            
; ?
;

_exptl_crystal_density_diffrn    1.6633
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             348

_exptl_absorpt_coefficient_mu    2.672
_exptl_crystal_description       prism
_exptl_crystal_size_max          0.1435
_exptl_crystal_size_mid          0.0793
_exptl_crystal_size_min          0.0291
_exptl_crystal_colour            colorless
_exptl_absorpt_correction_T_min  0.769
_exptl_absorpt_correction_T_max  0.932
_exptl_absorpt_correction_type   analytical
_exptl_absorpt_process_details   
;
CrysAlisPro, Oxford Diffraction Ltd.,
Version 1.171.33.51 (release 27-10-2009 CrysAlis171 .NET)
Analytical numeric absorption correction using a multifaceted crystal
model based on expressions derived by R.C. Clark & J.S. Reid.
;

#=======================================================================

# 7. EXPERIMENTAL DATA

_exptl_special_details           ?

_diffrn_ambient_temperature      120
_diffrn_radiation_type           'Cu K\a'
_diffrn_radiation_source         'X-ray tube'
_diffrn_radiation_wavelength     1.54184
_diffrn_measurement_device       'four-cycle diffractometer'
_diffrn_radiation_monochromator  mirror
_diffrn_measurement_device_type  
'Goniometer Xcalibur, detector: Atlas (Gemini ultra Cu)'
_diffrn_detector_area_resol_mean 10.3784
_diffrn_measurement_method       
'Rotation method data acquisition using \w scans'
_diffrn_reflns_number            7382
_diffrn_reflns_theta_min         5.13
_diffrn_reflns_theta_max         62.38
_diffrn_reflns_theta_full        61.65
_diffrn_measured_fraction_theta_max 0.96
_diffrn_measured_fraction_theta_full 0.98
_diffrn_reflns_av_R_equivalents  0.0222
_diffrn_reflns_av_sigmaI/netI    0.0101
_diffrn_reflns_limit_h_min       -7
_diffrn_reflns_limit_h_max       6
_diffrn_reflns_limit_k_min       -7
_diffrn_reflns_limit_k_max       6
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_limit_l_max       19
_diffrn_reflns_reduction_process 
;
Integration of the CCD images was done by program Crysalis RED
(Oxford diffraction, 2008). The same program was used for indexing of the
crystal shape and absorption correction.
;

#=======================================================================

# 8. REFINEMENT DATA

_refine_special_details          
;
The refinement was carried out against all reflections. The conventional
R-factor is always based on F. The goodness of fit as well as the weighted
R-factor are based on F and F^2^ for refinement carried out on F and F^2^,
respectively. The threshold expression is used only for calculating
R-factors etc. and it is not relevant to the choice of reflections for
refinement.

The program used for refinement, Jana2006, uses the weighting scheme
based on the experimental expectations, see _refine_ls_weighting_details,
that does not force S to be one. Therefore the values of S are usually larger
than the ones from the SHELX program.
;

_reflns_number_total             2042
_reflns_number_gt                1826
_reflns_threshold_expression     I>3\s(I)

_refine_ls_structure_factor_coef Fsqd
_refine_ls_R_factor_gt           0.0270
_refine_ls_wR_factor_gt          0.0824
_refine_ls_R_factor_all          0.0315
_refine_ls_wR_factor_ref         0.0848
_refine_ls_goodness_of_fit_ref   1.74
_refine_ls_goodness_of_fit_gt    1.80
_refine_ls_restrained_S_gt       ?
_refine_ls_restrained_S_all      ?
_refine_ls_number_reflns         2042
_refine_ls_number_parameters     238
_refine_ls_number_restraints     0
_refine_ls_number_constraints    16
_refine_ls_weighting_scheme      sigma
_refine_ls_weighting_details     w=1/(\s^2^(I)+0.0016I^2^)
_refine_ls_hydrogen_treatment    refxyz
_refine_ls_shift/su_max          0.0089
_refine_ls_shift/su_mean         0.0008
_refine_diff_density_max         0.22
_refine_diff_density_min         -0.27
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       ?
_refine_ls_abs_structure_details ?
_refine_ls_abs_structure_Flack   ?
_refine_ls_abs_structure_Rogers  ?

loop_
_atom_type_symbol
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C 0.018 0.009 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1'
H 0.000 0.000 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1'
N 0.031 0.018 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1'
O 0.049 0.032 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1'
S 0.333 0.557 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1'

_computing_data_collection       'Crysalis CCD (Oxford diffraction, 2009)'
_computing_cell_refinement       'Crysalis RED (Oxford diffraction, 2009)'
_computing_data_reduction        'Crysalis RED'
_computing_structure_solution    'SIR2002 (Burla et al., 2003)'
_computing_structure_refinement  
"Jana2006 (Pet\<r\'i\<cek, Du\<sek & Palatinus, 2006)"
_computing_molecular_graphics    'Diamond (Brandenburg & Putz, 2005)'
_computing_publication_material  Jana2006

#=======================================================================

# 9. ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_adp_type
_atom_site_U_iso_or_equiv
_atom_site_symmetry_multiplicity
_atom_site_occupancy
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
S1 S 0.47226(7) 0.58860(7) 0.22718(2) Uani 0.01371(16) 2 1 d . . .
O2 O 0.2527(2) 0.4524(2) 0.20318(7) Uani 0.0202(4) 2 1 d . . .
O1 O 0.6513(2) 0.45215(20) 0.22722(7) Uani 0.0183(4) 2 1 d . . .
O3 O 0.5042(2) 0.7412(2) 0.17390(7) Uani 0.0190(4) 2 1 d . . .
O4 O 0.48444(19) 0.71283(20) 0.30648(7) Uani 0.0170(4) 2 1 d . . .
O1W O 0.1780(2) 0.1228(2) 0.28591(8) Uani 0.0229(5) 2 1 d . . .
O2W O 0.7276(2) 0.1332(2) 0.31290(8) Uani 0.0223(5) 2 1 d . . .
N2 N 0.1535(2) 0.2581(2) -0.00161(8) Uani 0.0147(5) 2 1 d . . .
N1 N 0.0191(2) 0.2850(2) 0.05669(9) Uani 0.0142(5) 2 1 d . . .
N4 N -0.2071(2) 0.2079(2) -0.05148(9) Uani 0.0137(5) 2 1 d . . .
N6 N -0.3659(3) 0.2659(3) 0.06442(10) Uani 0.0196(5) 2 1 d . . .
N7 N 0.0529(3) 0.1753(3) -0.13804(10) Uani 0.0214(6) 2 1 d . . .
N9 N -0.1450(2) 0.2536(2) 0.51721(8) Uani 0.0144(5) 2 1 d . . .
N8 N -0.0137(2) 0.2251(2) 0.45839(9) Uani 0.0145(5) 2 1 d . . .
N11 N 0.2170(2) 0.3016(2) 0.56505(9) Uani 0.0141(5) 2 1 d . . .
N13 N 0.3697(3) 0.2453(3) 0.44769(10) Uani 0.0189(5) 2 1 d . . .
N14 N -0.0378(3) 0.3293(3) 0.65364(10) Uani 0.0230(6) 2 1 d . . .
C5 C -0.1952(3) 0.2567(3) 0.02652(10) Uani 0.0145(6) 2 1 d . . .
C3 C 0.0084(3) 0.2140(3) -0.06580(10) Uani 0.0135(5) 2 1 d . . .
C12 C 0.2023(3) 0.2544(3) 0.48682(10) Uani 0.0142(6) 2 1 d . . .
C10 C 0.0022(3) 0.2963(3) 0.58088(10) Uani 0.0142(6) 2 1 d . . .
H1W H 0.193(4) 0.223(4) 0.2579(13) Uiso 0.0275 2 1 d . . .
H2W H 0.038(4) 0.114(4) 0.2864(13) Uiso 0.0275 2 1 d . . .
H3W H 0.681(4) 0.208(4) 0.2853(13) Uiso 0.0268 2 1 d . . .
H4W H 0.623(4) 0.028(4) 0.3014(13) Uiso 0.0268 2 1 d . . .
H1A H 0.078(3) 0.329(3) 0.1035(13) Uiso 0.017 2 1 d . . .
H4A H -0.319(3) 0.212(3) -0.0873(12) Uiso 0.0164 2 1 d . . .
H6B H -0.342(3) 0.320(3) 0.1164(14) Uiso 0.0236 2 1 d . . .
H6A H -0.494(4) 0.261(3) 0.0416(13) Uiso 0.0236 2 1 d . . .
H7B H 0.194(4) 0.199(3) -0.1441(13) Uiso 0.0257 2 1 d . . .
H7A H -0.054(4) 0.137(4) -0.1781(13) Uiso 0.0257 2 1 d . . .
H8A H -0.080(3) 0.205(3) 0.4102(13) Uiso 0.0174 2 1 d . . .
H11A H 0.331(4) 0.310(3) 0.6004(12) Uiso 0.017 2 1 d . . .
H13B H 0.341(3) 0.197(3) 0.3961(14) Uiso 0.0227 2 1 d . . .
H13A H 0.499(4) 0.250(3) 0.4663(13) Uiso 0.0227 2 1 d . . .
H14B H -0.173(4) 0.316(4) 0.6624(13) Uiso 0.0276 2 1 d . . .
H14A H 0.069(4) 0.390(4) 0.6950(14) Uiso 0.0276 2 1 d . . .

loop_
_atom_site_aniso_label
_atom_site_aniso_type_symbol
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
S1 S 0.0125(3) 0.0176(3) 0.0103(3) 0.00085(17) 0.00080(17) 0.00256(18)
O2 O 0.0152(7) 0.0271(7) 0.0146(7) -0.0047(5) -0.0007(5) 0.0023(5)
O1 O 0.0188(7) 0.0211(7) 0.0153(7) 0.0054(5) 0.0023(5) 0.0029(5)
O3 O 0.0177(7) 0.0253(7) 0.0158(6) 0.0032(5) 0.0025(5) 0.0094(5)
O4 O 0.0156(7) 0.0214(7) 0.0129(6) 0.0031(5) 0.0012(5) 0.0012(5)
O1W O 0.0220(8) 0.0250(8) 0.0217(7) 0.0017(6) 0.0030(6) 0.0061(6)
O2W O 0.0224(8) 0.0194(8) 0.0216(8) -0.0020(6) -0.0056(6) 0.0055(6)
N2 N 0.0144(8) 0.0156(8) 0.0143(8) 0.0026(6) 0.0040(6) 0.0021(6)
N1 N 0.0142(8) 0.0169(8) 0.0099(8) 0.0014(6) 0.0003(6) 0.0006(6)
N4 N 0.0123(8) 0.0167(8) 0.0114(8) 0.0024(6) -0.0005(6) 0.0027(6)
N6 N 0.0150(8) 0.0292(9) 0.0142(9) 0.0042(7) 0.0023(7) 0.0018(7)
N7 N 0.0154(9) 0.0345(10) 0.0136(8) 0.0020(7) 0.0033(7) 0.0027(7)
N9 N 0.0130(8) 0.0159(8) 0.0143(8) 0.0018(6) 0.0031(6) 0.0024(6)
N8 N 0.0129(8) 0.0186(8) 0.0106(8) 0.0013(6) 0.0001(6) 0.0013(6)
N11 N 0.0118(8) 0.0182(8) 0.0116(8) 0.0018(6) -0.0009(6) 0.0030(6)
N13 N 0.0121(8) 0.0298(9) 0.0139(8) 0.0020(7) 0.0019(7) 0.0023(7)
N14 N 0.0131(8) 0.0395(10) 0.0149(9) 0.0010(7) 0.0035(7) 0.0014(7)
C5 C 0.0167(10) 0.0110(9) 0.0158(9) 0.0022(7) 0.0018(7) 0.0028(7)
C3 C 0.0145(9) 0.0105(8) 0.0154(9) 0.0018(7) 0.0018(7) 0.0031(7)
C12 C 0.0155(10) 0.0109(9) 0.0157(9) 0.0010(7) 0.0008(7) 0.0033(7)
C10 C 0.0140(9) 0.0113(9) 0.0173(10) 0.0008(7) 0.0033(7) 0.0030(7)

#=======================================================================

# 10. MOLECULAR GEOMETRY

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_1
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
S1 O2 . . 1.4718(12) yes
S1 O1 . . 1.4763(14) yes
S1 O3 . . 1.4744(14) yes
S1 O4 . . 1.4789(12) yes
O1W H1W . . 0.87(3) yes
O1W H2W . . 0.85(3) yes
O2W H3W . . 0.78(3) yes
O2W H4W . . 0.84(2) yes
N2 N1 . . 1.410(2) yes
N2 C3 . . 1.305(2) yes
N1 C5 . . 1.322(2) yes
N1 H1A . . 0.84(2) yes
N4 C5 . . 1.354(2) yes
N4 C3 . . 1.375(2) yes
N4 H4A . . 0.87(2) yes
N6 C5 . . 1.322(3) yes
N6 H6B . . 0.91(2) yes
N6 H6A . . 0.82(2) yes
N7 C3 . . 1.335(3) yes
N7 H7B . . 0.88(3) yes
N7 H7A . . 0.87(2) yes
N9 N8 . . 1.405(2) yes
N9 C10 . . 1.306(2) yes
N8 C12 . . 1.325(2) yes
N8 H8A . . 0.87(2) yes
N11 C12 . . 1.355(2) yes
N11 C10 . . 1.381(2) yes
N11 H11A . . 0.86(2) yes
N13 C12 . . 1.318(3) yes
N13 H13B . . 0.90(2) yes
N13 H13A . . 0.81(2) yes
N14 C10 . . 1.333(3) yes
N14 H14B . . 0.86(3) yes
N14 H14A . . 0.90(2) yes

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_2
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
O2 S1 O1 . . . 110.07(7) yes
O2 S1 O3 . . . 110.38(7) yes
O2 S1 O4 . . . 109.06(7) yes
O1 S1 O3 . . . 109.28(8) yes
O1 S1 O4 . . . 109.11(7) yes
O3 S1 O4 . . . 108.91(7) yes
H1W O1W H2W . . . 99(2) yes
H3W O2W H4W . . . 100(2) yes
N1 N2 C3 . . . 103.31(14) yes
N2 N1 C5 . . . 111.44(14) yes
N2 N1 H1A . . . 120.3(15) yes
C5 N1 H1A . . . 127.8(15) yes
C5 N4 C3 . . . 107.04(14) yes
C5 N4 H4A . . . 128.0(15) yes
C3 N4 H4A . . . 122.4(15) yes
C5 N6 H6B . . . 119.9(13) yes
C5 N6 H6A . . . 121.5(17) yes
H6B N6 H6A . . . 116(2) yes
C3 N7 H7B . . . 117.6(14) yes
C3 N7 H7A . . . 121.2(17) yes
H7B N7 H7A . . . 121(2) yes
N8 N9 C10 . . . 103.27(14) yes
N9 N8 C12 . . . 112.12(14) yes
N9 N8 H8A . . . 118.3(14) yes
C12 N8 H8A . . . 129.2(14) yes
C12 N11 C10 . . . 107.36(14) yes
C12 N11 H11A . . . 129.0(15) yes
C10 N11 H11A . . . 122.6(16) yes
C12 N13 H13B . . . 119.4(14) yes
C12 N13 H13A . . . 125.5(17) yes
H13B N13 H13A . . . 113(2) yes
C10 N14 H14B . . . 120.0(15) yes
C10 N14 H14A . . . 123.0(16) yes
H14B N14 H14A . . . 116(2) yes
N1 C5 N4 . . . 106.40(16) yes
N1 C5 N6 . . . 127.29(16) yes
N4 C5 N6 . . . 126.28(15) yes
N2 C3 N4 . . . 111.79(16) yes
N2 C3 N7 . . . 126.65(17) yes
N4 C3 N7 . . . 121.56(15) yes
N8 C12 N11 . . . 105.73(16) yes
N8 C12 N13 . . . 127.55(16) yes
N11 C12 N13 . . . 126.70(15) yes
N9 C10 N11 . . . 111.50(16) yes
N9 C10 N14 . . . 127.11(17) yes
N11 C10 N14 . . . 121.38(15) yes

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion
_geom_torsion_publ_flag
? ? ? ? ? ? ? ? ? ?

loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_site_symmetry_D
_geom_hbond_site_symmetry_H
_geom_hbond_site_symmetry_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_publ_flag
? ? ? ? ? ? ? ? ? ? ?

#=======================================================================

# 11. STRUCTURE-FACTOR LIST

loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
1 0 0 378.76 308.74 2.55 o
2 0 0 703.39 663.34 8.43 o
3 0 0 216.76 199.14 2.49 o
4 0 0 1634.15 1687.55 6.42 o
5 0 0 164.51 159.26 3.19 o
6 0 0 839.06 830.44 7.69 o
-6 1 0 32.86 28.13 2.37 o
-5 1 0 13.91 10.62 1.79 o
-4 1 0 129.45 117.05 2.22 o
-3 1 0 0.80 1.81 0.90 <
-2 1 0 0.88 2.32 0.82 <
-1 1 0 1204.19 1195.80 2.79 o
0 1 0 1593.76 1662.73 3.63 o
1 1 0 1356.49 1332.14 4.66 o
2 1 0 1422.49 1410.87 5.27 o
3 1 0 83.17 78.95 1.47 o
4 1 0 169.28 172.70 2.35 o
5 1 0 162.37 155.86 2.68 o
6 1 0 249.78 260.08 4.15 o
-6 2 0 554.36 561.06 6.49 o
-5 2 0 445.31 434.33 5.32 o
-4 2 0 399.37 406.88 3.69 o
-3 2 0 1451.60 1461.38 4.35 o
-2 2 0 722.63 818.24 3.50 o
-1 2 0 2012.23 2023.94 8.73 o
0 2 0 14506.58 15122.69 55.23 o
1 2 0 1209.60 1161.32 3.42 o
2 2 0 337.60 378.78 2.69 o
3 2 0 476.35 488.77 3.70 o
4 2 0 6.02 10.05 1.39 o
5 2 0 473.33 517.36 5.91 o
6 2 0 193.77 159.93 3.21 o
-6 3 0 120.75 141.69 2.99 o
-5 3 0 68.24 70.27 2.50 o
-4 3 0 15.34 15.88 1.32 o
-3 3 0 320.63 330.91 2.87 o
-2 3 0 1707.98 1729.88 5.22 o
-1 3 0 58.66 56.46 1.62 o
0 3 0 72.42 70.22 1.76 o
1 3 0 19.37 22.78 0.95 o
2 3 0 28.92 31.03 1.29 o
3 3 0 16.41 15.08 1.53 o
4 3 0 1.54 2.11 1.51 <
5 3 0 53.47 46.41 2.37 o
-6 4 0 94.51 99.88 4.46 o
-5 4 0 224.48 237.90 4.91 o
-4 4 0 201.84 194.53 3.68 o
-3 4 0 0.59 0.55 1.06 <
-2 4 0 12.32 11.01 1.00 o
-1 4 0 210.35 236.77 2.50 o
0 4 0 1156.12 1214.31 6.22 o
1 4 0 0.74 2.30 0.94 <
2 4 0 22.96 20.34 1.36 o
3 4 0 2.16 2.11 1.40 <
4 4 0 44.79 38.32 2.02 o
5 4 0 160.30 132.00 3.77 o
-5 5 0 0.34 0.60 2.09 <
-4 5 0 46.94 42.61 2.17 o
-3 5 0 163.41 158.65 3.15 o
-2 5 0 150.89 156.09 2.87 o
-1 5 0 75.14 84.83 1.95 o
0 5 0 10.96 9.27 1.18 o
1 5 0 78.72 79.47 1.99 o
2 5 0 91.07 91.05 2.52 o
3 5 0 21.42 16.96 1.49 o
4 5 0 1.58 -2.23 2.16 <
-4 6 0 32.03 39.85 2.33 o
-3 6 0 527.88 553.84 6.10 o
-2 6 0 316.25 334.09 4.69 o
-1 6 0 84.24 96.06 3.05 o
0 6 0 760.30 743.10 6.95 o
1 6 0 293.98 331.12 3.30 o
2 6 0 6.67 10.84 2.25 o
-2 7 0 13.93 19.99 2.41 o
-1 7 0 79.99 103.37 3.85 o
0 -7 1 5.04 8.40 2.63 o
1 -7 1 115.77 130.31 4.22 o
2 -7 1 31.67 38.88 2.76 o
-2 -6 1 118.10 115.97 2.97 o
-1 -6 1 1.82 3.10 1.68 <
0 -6 1 206.33 205.70 3.29 o
1 -6 1 19.73 20.91 3.71 o
2 -6 1 30.17 26.93 2.08 o
3 -6 1 12.65 9.76 1.82 o
4 -6 1 59.03 74.34 2.67 o
-4 -5 1 29.97 30.80 2.17 o
-3 -5 1 49.88 46.62 1.68 o
-2 -5 1 587.61 589.13 6.36 o
-1 -5 1 350.50 371.13 3.57 o
0 -5 1 95.51 101.13 1.90 o
1 -5 1 7.83 6.93 1.59 o
2 -5 1 77.45 75.11 2.13 o
3 -5 1 208.58 190.14 3.50 o
4 -5 1 46.60 48.15 2.21 o
5 -5 1 16.84 15.05 2.47 o
-5 -4 1 0.46 -0.12 1.84 <
-4 -4 1 153.53 139.36 3.06 o
-3 -4 1 480.86 503.15 4.67 o
-2 -4 1 72.41 72.71 1.74 o
-1 -4 1 0.52 0.54 0.94 <
0 -4 1 0.67 1.46 1.12 <
1 -4 1 9.13 8.36 1.01 o
2 -4 1 93.30 81.04 1.56 o
3 -4 1 1.22 1.85 1.23 <
4 -4 1 46.24 51.93 2.49 o
5 -4 1 18.16 15.34 2.25 o
6 -4 1 0.67 8.19 4.23 <
-5 -3 1 15.17 17.28 1.82 o
-4 -3 1 95.51 96.40 2.51 o
-3 -3 1 777.28 791.77 5.43 o
-2 -3 1 66.20 73.92 1.37 o
-1 -3 1 296.27 328.43 1.92 o
0 -3 1 17.16 27.09 1.10 o
1 -3 1 227.69 214.15 2.67 o
2 -3 1 1029.74 976.78 4.03 o
3 -3 1 481.37 511.27 4.07 o
4 -3 1 468.55 489.69 3.77 o
5 -3 1 88.14 102.43 2.46 o
6 -3 1 207.48 228.30 4.38 o
-6 -2 1 6.91 9.06 1.58 o
-5 -2 1 0.66 0.44 1.69 <
-4 -2 1 131.55 139.19 2.61 o
-3 -2 1 639.08 643.62 4.79 o
-2 -2 1 473.64 489.21 3.24 o
-1 -2 1 325.12 300.65 1.78 o
0 -2 1 1976.76 1993.57 5.85 o
1 -2 1 393.67 385.97 2.82 o
2 -2 1 7.44 5.17 0.64 o
3 -2 1 252.91 252.25 1.95 o
4 -2 1 665.75 686.84 4.07 o
5 -2 1 255.90 275.82 5.47 o
6 -2 1 102.25 102.07 3.24 o
-6 -1 1 265.82 251.93 4.24 o
-5 -1 1 261.73 260.21 3.84 o
-4 -1 1 1217.36 1298.64 7.05 o
-3 -1 1 18.47 17.94 1.08 o
-2 -1 1 5623.67 6015.15 10.64 o
-1 -1 1 2212.68 2167.80 4.55 o
0 -1 1 1030.94 1089.53 3.02 o
1 -1 1 11.28 25.55 0.78 o
2 -1 1 506.71 507.92 3.95 o
3 -1 1 1908.91 1950.90 5.71 o
4 -1 1 68.25 51.08 1.74 o
5 -1 1 1980.71 2004.56 10.41 o
6 -1 1 1064.54 1131.38 9.23 o
-6 0 1 71.75 70.09 2.88 o
-5 0 1 163.74 152.47 3.84 o
-4 0 1 606.65 609.44 3.93 o
-3 0 1 1.78 1.45 0.90 <
-2 0 1 525.24 534.16 4.01 o
-1 0 1 1.02 1.16 0.82 <
1 0 1 98.50 98.52 1.59 o
2 0 1 128.19 134.58 1.97 o
3 0 1 108.46 95.57 1.55 o
4 0 1 629.56 589.69 5.09 o
5 0 1 287.49 279.66 4.07 o
6 0 1 140.51 135.98 3.56 o
-7 1 1 44.23 36.35 2.56 o
-6 1 1 30.47 41.18 2.50 o
-5 1 1 607.99 580.41 5.11 o
-4 1 1 1970.19 2037.95 7.69 o
-3 1 1 8.06 7.44 0.94 o
-2 1 1 9295.88 9377.41 17.52 o
-1 1 1 1220.84 1147.75 4.37 o
0 1 1 603.58 644.03 2.66 o
1 1 1 963.84 865.87 4.39 o
2 1 1 645.60 787.86 4.12 o
3 1 1 1671.39 1737.97 5.17 o
4 1 1 7.42 7.59 1.12 o
5 1 1 95.19 88.88 2.51 o
6 1 1 70.31 73.95 2.54 o
-6 2 1 252.28 248.56 4.46 o
-5 2 1 412.14 432.06 5.30 o
-4 2 1 324.54 319.03 3.33 o
-3 2 1 470.91 487.92 2.74 o
-2 2 1 354.01 329.36 1.87 o
-1 2 1 504.75 493.77 3.47 o
0 2 1 1352.27 1310.62 4.73 o
1 2 1 48.87 41.98 0.92 o
2 2 1 223.16 244.41 2.19 o
3 2 1 939.84 956.54 7.79 o
4 2 1 140.09 143.39 2.99 o
5 2 1 30.73 26.98 2.52 o
6 2 1 20.53 19.01 1.70 o
-6 3 1 183.37 185.89 3.37 o
-5 3 1 4.69 4.96 1.57 o
-4 3 1 11.06 16.47 1.35 o
-3 3 1 23.91 22.29 1.27 o
-2 3 1 8.44 10.54 0.88 o
-1 3 1 1.30 1.59 0.82 <
0 3 1 960.59 1159.17 5.79 o
1 3 1 854.27 940.27 4.33 o
2 3 1 1383.84 1378.08 6.11 o
3 3 1 6.10 4.64 1.40 o
4 3 1 180.05 168.32 2.79 o
5 3 1 131.43 134.43 3.33 o
-6 4 1 1.77 -2.95 3.86 <
-5 4 1 9.73 6.79 2.28 <
-4 4 1 41.69 41.19 2.22 o
-3 4 1 8.09 7.79 1.21 o
-2 4 1 347.76 329.86 3.17 o
-1 4 1 0.66 2.16 1.06 <
0 4 1 118.83 123.82 2.31 o
1 4 1 42.22 44.72 1.39 o
2 4 1 269.55 266.07 3.21 o
3 4 1 181.01 174.73 3.43 o
4 4 1 20.26 20.67 1.67 o
-5 5 1 0.91 0.56 1.98 <
-4 5 1 91.95 85.02 3.15 o
-3 5 1 447.20 429.31 6.01 o
-2 5 1 17.49 17.72 1.44 o
-1 5 1 82.56 91.86 2.00 o
0 5 1 126.29 129.37 2.39 o
1 5 1 13.59 12.30 1.27 o
2 5 1 17.24 17.82 1.64 o
3 5 1 385.66 369.67 4.16 o
-4 6 1 6.33 3.07 2.27 <
-3 6 1 16.49 14.66 1.73 o
-2 6 1 66.49 66.34 1.78 o
-1 6 1 0.08 -2.72 2.07 <
0 6 1 50.69 52.51 2.19 o
1 6 1 57.53 57.98 1.89 o
2 6 1 125.80 113.91 2.30 o
0 -7 2 16.38 17.61 2.42 o
1 -7 2 29.57 29.19 2.95 o
2 -7 2 1.72 -4.13 2.38 <
-3 -6 2 207.35 201.38 4.67 o
-2 -6 2 13.03 12.03 2.32 o
-1 -6 2 256.39 254.59 4.27 o
0 -6 2 368.42 349.91 5.21 o
1 -6 2 1002.58 1085.60 12.53 o
2 -6 2 104.82 106.05 3.05 o
3 -6 2 45.20 43.29 2.22 o
4 -6 2 16.61 11.81 2.18 o
-4 -5 2 35.56 35.27 2.32 o
-3 -5 2 11.17 11.71 1.90 o
-2 -5 2 254.23 257.14 3.30 o
-1 -5 2 134.17 136.86 2.34 o
0 -5 2 4.79 4.66 1.25 o
1 -5 2 125.14 130.35 2.41 o
2 -5 2 475.17 476.38 4.08 o
3 -5 2 158.93 153.70 2.67 o
4 -5 2 10.34 11.90 2.30 o
5 -5 2 0.93 -0.31 2.28 <
-5 -4 2 253.98 251.36 4.14 o
-4 -4 2 169.42 161.72 3.18 o
-3 -4 2 13.14 14.23 1.38 o
-2 -4 2 66.85 67.02 1.91 o
-1 -4 2 283.19 293.93 3.33 o
0 -4 2 6555.47 6727.19 13.68 o
1 -4 2 1596.09 1657.44 5.36 o
2 -4 2 293.94 294.68 2.45 o
3 -4 2 203.75 208.42 2.77 o
4 -4 2 198.18 205.02 4.60 o
5 -4 2 458.50 456.08 6.34 o
6 -4 2 490.19 520.18 9.23 o
-5 -3 2 10.70 11.17 1.72 o
-4 -3 2 0.42 2.68 1.51 <
-3 -3 2 18.94 19.46 1.39 o
-2 -3 2 10.68 11.46 1.02 o
-1 -3 2 1.92 0.40 0.77 <
0 -3 2 143.13 159.68 1.98 o
1 -3 2 113.79 111.32 1.68 o
2 -3 2 1607.14 1652.60 4.44 o
3 -3 2 225.99 221.07 2.49 o
4 -3 2 38.84 44.85 1.65 o
5 -3 2 96.16 105.19 2.52 o
6 -3 2 243.80 261.89 3.86 o
-6 -2 2 173.70 148.53 3.25 o
-5 -2 2 447.63 504.13 6.15 o
-4 -2 2 529.37 515.61 4.99 o
-3 -2 2 50.09 44.46 1.36 o
-2 -2 2 261.80 315.04 2.64 o
-1 -2 2 967.32 1070.46 3.58 o
0 -2 2 25324.52 25549.68 70.88 o
1 -2 2 6409.52 6986.05 10.39 o
2 -2 2 541.54 629.73 2.90 o
3 -2 2 1992.48 1998.13 6.05 o
4 -2 2 34.89 30.75 1.42 o
5 -2 2 1140.93 1151.73 8.39 o
6 -2 2 114.50 104.74 2.88 o
-6 -1 2 105.09 111.29 3.08 o
-5 -1 2 323.60 327.52 4.27 o
-4 -1 2 138.40 135.51 2.66 o
-3 -1 2 15.92 10.41 0.96 o
-2 -1 2 788.85 738.46 4.57 o
-1 -1 2 1062.36 1057.02 3.87 o
0 -1 2 514.47 549.64 2.41 o
1 -1 2 404.39 399.48 2.19 o
2 -1 2 53.55 49.61 1.38 o
3 -1 2 81.21 91.27 1.38 o
4 -1 2 11.64 9.04 1.31 o
5 -1 2 93.69 97.73 2.62 o
6 -1 2 2.57 3.52 2.04 <
-6 0 2 24.02 32.78 2.41 o
-5 0 2 2196.66 2287.83 8.88 o
-4 0 2 683.12 690.35 5.16 o
-3 0 2 114.59 139.47 1.64 o
-2 0 2 255.30 236.16 2.01 o
-1 0 2 7268.21 7195.87 27.11 o
0 0 2 93.07 61.35 1.36 o
1 0 2 6353.01 6352.41 29.25 o
2 0 2 427.00 453.00 2.43 o
3 0 2 1888.05 1928.41 5.30 o
4 0 2 204.90 188.83 2.85 o
5 0 2 553.66 595.61 6.95 o
6 0 2 134.97 124.51 3.15 o
-7 1 2 13.87 13.94 1.48 o
-6 1 2 0.03 0.59 2.29 <
-5 1 2 98.58 100.14 3.03 o
-4 1 2 437.94 420.51 3.69 o
-3 1 2 8.51 4.87 0.85 o
-2 1 2 77.80 85.38 1.09 o
-1 1 2 1700.76 1622.08 6.41 o
0 1 2 1477.40 1493.57 4.45 o
1 1 2 1548.51 1491.58 3.84 o
2 1 2 1607.65 1581.82 5.48 o
3 1 2 239.42 236.23 2.23 o
4 1 2 47.60 47.70 1.60 o
5 1 2 332.26 340.61 5.49 o
6 1 2 54.91 59.72 2.26 o
-6 2 2 106.45 96.22 2.99 o
-5 2 2 295.02 318.88 4.62 o
-4 2 2 777.40 786.70 4.52 o
-3 2 2 56.14 50.23 1.13 o
-2 2 2 2.35 11.71 0.84 o
-1 2 2 1.83 1.81 0.61 <
0 2 2 1220.91 1364.03 6.17 o
1 2 2 40.86 30.92 0.81 o
2 2 2 494.71 567.98 3.67 o
3 2 2 162.54 159.15 3.66 o
4 2 2 34.39 38.59 1.79 o
5 2 2 63.52 51.21 2.65 o
6 2 2 118.73 106.66 3.77 o
-6 3 2 31.04 35.50 2.37 o
-5 3 2 22.38 23.69 1.70 o
-4 3 2 22.63 24.93 1.98 o
-3 3 2 238.31 232.67 2.75 o
-2 3 2 792.61 791.34 3.03 o
-1 3 2 8.70 8.57 0.75 o
0 3 2 433.12 452.36 2.65 o
1 3 2 37.69 40.68 1.07 o
2 3 2 70.41 78.16 1.84 o
3 3 2 191.14 191.35 3.42 o
4 3 2 8.43 6.68 1.53 o
5 3 2 0.64 -1.47 1.70 <
-6 4 2 300.23 359.08 7.49 o
-5 4 2 170.40 162.56 4.15 o
-4 4 2 74.05 67.67 2.61 o
-3 4 2 764.39 746.16 5.84 o
-2 4 2 37.29 37.08 1.50 o
-1 4 2 0.68 0.90 0.98 <
0 4 2 247.58 260.75 2.88 o
1 4 2 4.09 2.08 0.98 <
2 4 2 1474.07 1521.22 8.66 o
3 4 2 2.18 4.95 1.41 o
4 4 2 114.59 114.83 2.34 o
-5 5 2 2.06 0.94 2.02 <
-4 5 2 88.97 93.71 3.37 o
-3 5 2 191.73 184.00 2.87 o
-2 5 2 27.53 25.20 1.57 o
-1 5 2 48.69 50.81 1.77 o
0 5 2 77.05 78.98 1.90 o
1 5 2 36.39 35.84 1.44 o
2 5 2 32.72 32.85 1.65 o
3 5 2 27.92 22.98 1.62 o
-4 6 2 176.04 171.85 4.65 o
-3 6 2 6.52 8.54 1.73 o
-2 6 2 321.40 323.90 4.84 o
-1 6 2 153.31 176.59 3.83 o
0 6 2 119.81 134.19 3.40 o
1 6 2 131.80 130.51 2.55 o
2 6 2 392.02 382.15 4.18 o
0 -7 3 224.21 254.42 5.23 o
1 -7 3 157.07 162.21 4.64 o
2 -7 3 149.40 160.04 4.33 o
-3 -6 3 12.07 12.50 2.32 o
-2 -6 3 0.31 -3.03 2.10 <
-1 -6 3 90.36 87.82 2.94 o
0 -6 3 277.31 299.88 4.94 o
1 -6 3 59.08 58.58 3.96 o
2 -6 3 0.81 1.86 1.72 <
3 -6 3 105.99 111.50 2.99 o
4 -6 3 162.19 170.88 4.63 o
-4 -5 3 144.04 152.92 3.58 o
-3 -5 3 363.33 360.09 4.68 o
-2 -5 3 12.18 8.56 1.83 o
-1 -5 3 39.35 37.11 1.86 o
0 -5 3 16.78 15.75 2.17 o
1 -5 3 91.70 87.31 2.75 o
2 -5 3 5.58 7.12 1.30 o
3 -5 3 271.39 272.00 3.37 o
4 -5 3 75.25 71.27 3.11 o
5 -5 3 210.91 226.16 4.20 o
-5 -4 3 11.70 12.11 2.04 o
-4 -4 3 316.51 296.58 4.75 o
-3 -4 3 470.70 480.82 3.73 o
-2 -4 3 75.18 75.74 1.97 o
-1 -4 3 25.81 28.41 1.55 o
0 -4 3 85.37 90.08 2.03 o
1 -4 3 7.28 6.00 1.04 o
2 -4 3 6.59 7.85 1.01 o
3 -4 3 18.75 16.59 1.27 o
4 -4 3 0.20 2.21 1.84 <
5 -4 3 9.47 4.80 2.27 <
-5 -3 3 39.89 40.53 2.15 o
-4 -3 3 907.41 938.61 6.12 o
-3 -3 3 75.88 63.03 1.57 o
-2 -3 3 3064.86 3199.41 10.77 o
-1 -3 3 53.11 52.06 1.18 o
0 -3 3 0.99 1.34 0.79 <
1 -3 3 540.90 558.35 2.76 o
2 -3 3 93.00 106.35 1.33 o
3 -3 3 181.32 179.32 2.03 o
4 -3 3 0.11 2.34 1.35 <
5 -3 3 63.64 58.57 2.12 o
6 -3 3 70.89 71.54 2.34 o
-6 -2 3 39.03 45.93 2.23 o
-5 -2 3 9.24 9.25 1.79 o
-4 -2 3 31.56 30.23 2.04 o
-3 -2 3 550.86 538.85 3.25 o
-2 -2 3 521.68 536.80 4.02 o
-1 -2 3 345.19 311.28 1.85 o
0 -2 3 1953.54 1950.70 6.94 o
1 -2 3 77.46 74.47 1.01 o
2 -2 3 40.71 51.40 1.11 o
3 -2 3 290.64 284.56 2.22 o
4 -2 3 601.68 591.46 3.77 o
5 -2 3 81.38 77.53 2.18 o
6 -2 3 62.44 56.00 2.32 o
-6 -1 3 44.43 46.11 2.10 o
-5 -1 3 250.76 231.55 3.23 o
-4 -1 3 26.96 36.49 1.84 o
-3 -1 3 569.54 586.73 3.60 o
-2 -1 3 59.84 69.50 1.28 o
-1 -1 3 1304.22 1332.45 3.71 o
0 -1 3 885.80 854.35 4.17 o
1 -1 3 9214.09 8937.39 9.27 o
2 -1 3 1017.60 887.64 5.80 o
3 -1 3 131.94 157.19 1.74 o
4 -1 3 130.40 133.57 2.21 o
5 -1 3 1566.65 1594.07 8.39 o
6 -1 3 8.18 11.88 2.17 o
-6 0 3 77.74 73.11 3.05 o
-5 0 3 103.54 102.73 2.67 o
-4 0 3 229.39 215.57 3.46 o
-3 0 3 0.66 1.35 0.90 <
-2 0 3 720.99 739.48 3.62 o
-1 0 3 118.03 126.42 1.33 o
0 0 3 16.12 16.64 0.98 o
1 0 3 1047.45 1049.17 5.45 o
2 0 3 15.45 12.58 0.96 o
3 0 3 20.96 16.40 0.92 o
4 0 3 395.64 381.09 3.83 o
5 0 3 519.54 506.55 5.42 o
6 0 3 36.68 39.48 2.20 o
-7 1 3 56.49 63.90 2.20 o
-6 1 3 821.22 899.35 11.56 o
-5 1 3 52.27 51.97 2.03 o
-4 1 3 16.09 11.54 1.21 o
-3 1 3 12.67 17.02 0.90 o
-2 1 3 2901.29 2927.46 6.82 o
-1 1 3 15.71 19.57 1.07 o
0 1 3 698.44 774.12 3.55 o
1 1 3 1566.00 1592.82 4.76 o
2 1 3 3023.11 3150.77 7.03 o
3 1 3 160.82 159.80 1.68 o
4 1 3 520.46 514.90 4.35 o
5 1 3 12.19 10.49 1.60 o
6 1 3 273.10 272.72 3.70 o
-6 2 3 321.42 340.60 6.86 o
-5 2 3 269.96 275.98 4.25 o
-4 2 3 74.87 73.47 1.58 o
-3 2 3 353.12 360.79 2.30 o
-2 2 3 937.40 890.62 4.13 o
-1 2 3 115.50 105.11 1.51 o
0 2 3 245.06 199.55 2.59 o
1 2 3 33.47 28.78 0.91 o
2 2 3 284.00 302.97 2.23 o
3 2 3 321.91 339.23 3.43 o
4 2 3 2.22 2.78 1.73 <
5 2 3 6.66 6.74 1.76 o
6 2 3 35.64 26.63 2.37 o
-6 3 3 67.45 79.22 4.78 o
-5 3 3 224.97 212.99 3.49 o
-4 3 3 358.46 375.39 4.61 o
-3 3 3 1598.26 1625.89 7.99 o
-2 3 3 56.31 46.96 1.23 o
-1 3 3 33.80 28.27 0.96 o
0 3 3 432.94 468.67 3.14 o
1 3 3 164.26 160.55 1.54 o
2 3 3 0.85 1.05 1.18 <
3 3 3 266.36 293.60 3.52 o
4 3 3 20.07 22.03 1.67 o
5 3 3 0.88 2.46 2.25 <
-5 4 3 27.67 20.41 2.19 o
-4 4 3 0.37 -1.68 1.86 <
-3 4 3 259.53 270.05 4.28 o
-2 4 3 591.00 565.71 4.99 o
-1 4 3 0.89 1.36 1.16 <
0 4 3 183.10 192.16 2.58 o
1 4 3 221.11 222.43 2.59 o
2 4 3 157.60 151.62 2.63 o
3 4 3 147.32 150.09 3.20 o
4 4 3 48.53 48.37 1.72 o
-5 5 3 69.54 71.35 2.73 o
-4 5 3 27.71 20.60 2.41 o
-3 5 3 8.64 6.41 1.36 o
-2 5 3 122.62 122.28 2.45 o
-1 5 3 124.26 121.87 2.03 o
0 5 3 621.75 670.73 4.22 o
1 5 3 0.39 0.43 1.18 <
2 5 3 541.44 572.01 4.87 o
3 5 3 45.05 40.77 2.45 o
-4 6 3 1.14 -0.15 1.91 <
-3 6 3 10.48 2.85 2.36 <
-2 6 3 20.33 18.24 1.98 o
-1 6 3 7.37 9.11 1.95 o
0 6 3 9.41 6.98 1.96 o
1 6 3 55.99 55.45 2.39 o
2 6 3 232.65 232.68 4.68 o
0 -7 4 3.73 -3.15 2.39 <
1 -7 4 1.85 -1.98 2.39 <
2 -7 4 0.76 -6.40 2.33 <
-3 -6 4 48.02 42.91 2.79 o
-2 -6 4 3.95 4.95 2.21 <
-1 -6 4 27.93 22.32 2.16 o
0 -6 4 1751.13 1722.26 11.15 o
1 -6 4 726.58 750.95 10.34 o
2 -6 4 75.83 78.10 2.63 o
3 -6 4 1.06 -1.74 1.68 <
4 -6 4 8.95 2.62 1.96 <
-4 -5 4 93.95 97.90 3.10 o
-3 -5 4 159.36 156.71 4.26 o
-2 -5 4 409.01 423.13 6.20 o
-1 -5 4 158.40 167.25 3.07 o
0 -5 4 0.57 0.89 1.50 <
1 -5 4 251.04 229.01 5.43 o
2 -5 4 779.86 801.12 6.07 o
3 -5 4 86.55 81.48 2.31 o
4 -5 4 14.55 13.41 2.14 o
5 -5 4 0.25 2.69 2.17 <
-5 -4 4 865.90 903.50 7.61 o
-4 -4 4 1.43 0.97 2.37 <
-3 -4 4 7.66 6.76 1.54 o
-2 -4 4 542.82 580.26 4.60 o
-1 -4 4 492.98 531.92 3.82 o
0 -4 4 1092.02 1147.18 5.36 o
1 -4 4 2459.59 2566.82 7.06 o
2 -4 4 686.32 695.66 5.26 o
3 -4 4 956.43 954.51 5.21 o
4 -4 4 45.37 40.80 2.00 o
5 -4 4 308.11 296.35 5.31 o
-6 -3 4 39.69 35.92 2.45 o
-5 -3 4 60.58 48.26 2.08 o
-4 -3 4 22.36 23.67 1.92 o
-3 -3 4 91.32 88.43 1.66 o
-2 -3 4 0.09 0.83 1.11 <
-1 -3 4 1.14 2.66 0.80 o
0 -3 4 7.88 11.61 0.96 o
1 -3 4 215.14 198.55 1.49 o
2 -3 4 884.36 884.70 3.51 o
3 -3 4 220.27 219.86 1.90 o
4 -3 4 31.83 32.43 1.41 o
5 -3 4 384.89 404.76 5.15 o
6 -3 4 64.60 66.90 2.24 o
-6 -2 4 9.53 16.10 2.00 o
-5 -2 4 1287.34 1395.05 10.23 o
-4 -2 4 493.97 480.25 4.98 o
-3 -2 4 646.97 705.24 5.05 o
-2 -2 4 81.59 79.58 1.81 o
-1 -2 4 617.59 704.40 4.05 o
0 -2 4 8.26 9.22 0.67 o
1 -2 4 108.16 126.44 1.45 o
2 -2 4 41.78 42.29 0.91 o
3 -2 4 246.36 245.89 2.38 o
4 -2 4 189.87 199.83 2.42 o
5 -2 4 35.08 35.27 1.74 o
6 -2 4 455.21 464.32 5.82 o
-6 -1 4 91.29 88.57 2.47 o
-5 -1 4 307.40 308.73 4.30 o
-4 -1 4 182.74 179.72 3.02 o
-3 -1 4 2.56 5.33 1.13 o
-2 -1 4 185.94 174.49 2.24 o
-1 -1 4 646.39 631.78 3.74 o
0 -1 4 5.50 6.22 1.25 o
1 -1 4 388.90 374.25 2.68 o
2 -1 4 381.14 386.51 2.58 o
3 -1 4 200.86 214.15 2.06 o
4 -1 4 74.28 73.71 1.87 o
5 -1 4 45.18 42.37 1.75 o
6 -1 4 63.77 57.08 2.04 o
-6 0 4 685.32 671.77 7.22 o
-5 0 4 23.91 19.07 1.87 o
-4 0 4 9.45 13.11 1.84 o
-3 0 4 1225.47 1279.84 7.30 o
-2 0 4 174.62 124.42 1.63 o
-1 0 4 1260.05 1191.45 4.07 o
0 0 4 4693.61 4816.24 10.36 o
1 0 4 101.95 93.19 1.38 o
2 0 4 2368.98 2584.27 8.08 o
3 0 4 1392.88 1409.86 4.70 o
4 0 4 1.46 3.58 1.21 <
5 0 4 0.42 3.63 1.58 <
6 0 4 2.50 -1.82 2.01 <
-7 1 4 8.68 9.73 1.50 o
-6 1 4 19.79 23.43 2.75 o
-5 1 4 137.32 135.70 2.48 o
-4 1 4 492.84 476.86 3.95 o
-3 1 4 30.08 25.71 0.95 o
-2 1 4 122.91 132.94 1.62 o
-1 1 4 1245.74 1182.69 4.93 o
0 1 4 2249.51 2290.52 4.84 o
1 1 4 506.71 452.14 2.97 o
2 1 4 230.15 186.65 2.05 o
3 1 4 465.73 465.43 3.11 o
4 1 4 0.69 -0.91 1.33 <
5 1 4 173.35 174.92 3.17 o
6 1 4 30.37 36.79 1.81 o
-6 2 4 16.64 17.86 2.40 o
-5 2 4 903.97 915.75 9.03 o
-4 2 4 34.36 36.71 1.26 o
-3 2 4 779.72 860.91 4.15 o
-2 2 4 140.16 125.60 1.48 o
-1 2 4 345.29 322.95 2.31 o
0 2 4 48.11 68.79 1.36 o
1 2 4 529.78 498.73 2.65 o
2 2 4 3257.46 3485.62 7.47 o
3 2 4 2.25 2.39 1.23 <
4 2 4 409.12 411.43 4.81 o
5 2 4 246.43 230.76 4.46 o
-6 3 4 4.12 5.37 3.89 <
-5 3 4 25.05 19.19 2.08 o
-4 3 4 4.45 4.58 1.43 o
-3 3 4 156.11 151.34 2.46 o
-2 3 4 64.93 64.76 1.51 o
-1 3 4 46.71 47.53 1.05 o
0 3 4 239.21 222.68 1.83 o
1 3 4 1.45 2.34 0.79 <
2 3 4 228.19 242.57 2.76 o
3 3 4 232.91 231.05 3.18 o
4 3 4 213.23 219.14 3.40 o
5 3 4 54.52 44.54 3.03 o
-5 4 4 101.57 122.03 3.28 o
-4 4 4 82.80 80.01 3.24 o
-3 4 4 37.69 39.83 1.61 o
-2 4 4 26.29 26.16 1.23 o
-1 4 4 0.24 0.80 1.37 <
0 4 4 28.93 25.36 1.40 o
1 4 4 6.33 6.36 1.14 o
2 4 4 14.60 13.27 1.41 o
3 4 4 304.54 330.57 4.58 o
4 4 4 131.19 141.74 2.80 o
-5 5 4 29.03 27.91 2.15 o
-4 5 4 273.48 306.77 6.18 o
-3 5 4 29.64 30.20 1.94 o
-2 5 4 11.87 10.99 1.38 o
-1 5 4 87.73 91.36 1.91 o
0 5 4 214.28 210.05 2.38 o
1 5 4 15.41 14.52 1.29 o
2 5 4 4.13 3.21 1.50 <
3 5 4 123.99 116.80 2.64 o
-4 6 4 3.13 6.83 1.97 o
-3 6 4 468.89 472.93 6.05 o
-2 6 4 110.26 125.18 2.89 o
-1 6 4 379.04 363.66 5.34 o
0 6 4 84.14 87.18 2.81 o
1 6 4 66.49 79.32 2.61 o
0 -7 5 16.20 17.21 2.31 o
1 -7 5 14.10 4.71 2.54 <
2 -7 5 132.80 129.69 3.81 o
-3 -6 5 1.06 -0.01 2.24 <
-2 -6 5 67.34 63.02 2.77 o
-1 -6 5 176.65 183.89 3.80 o
0 -6 5 304.96 320.00 4.12 o
1 -6 5 110.11 112.77 3.32 o
2 -6 5 102.61 101.65 2.92 o
3 -6 5 220.44 217.45 4.00 o
4 -6 5 139.53 149.32 4.24 o
-4 -5 5 29.68 29.06 2.29 o
-3 -5 5 44.59 42.93 2.89 o
-2 -5 5 92.83 92.91 2.75 o
-1 -5 5 300.39 312.24 3.94 o
0 -5 5 368.05 372.75 4.32 o
1 -5 5 998.33 1006.78 7.75 o
2 -5 5 105.75 106.16 2.59 o
3 -5 5 13.63 10.61 1.48 o
4 -5 5 72.89 70.75 2.78 o
5 -5 5 237.08 236.89 4.22 o
-5 -4 5 34.01 35.53 2.27 o
-4 -4 5 215.48 206.58 3.88 o
-3 -4 5 393.14 404.89 5.08 o
-2 -4 5 27.40 24.91 1.82 o
-1 -4 5 35.48 37.13 1.69 o
0 -4 5 281.36 307.33 2.76 o
1 -4 5 40.88 40.52 1.40 o
2 -4 5 122.15 123.41 2.24 o
3 -4 5 7.42 6.72 1.35 o
4 -4 5 6.88 5.27 1.60 o
5 -4 5 18.81 16.68 2.35 o
-6 -3 5 360.47 364.05 5.89 o
-5 -3 5 3.27 1.64 1.87 <
-4 -3 5 193.95 190.06 3.94 o
-3 -3 5 729.89 760.73 6.41 o
-2 -3 5 1594.05 1610.04 6.73 o
-1 -3 5 765.87 802.34 3.60 o
0 -3 5 529.32 518.26 3.09 o
1 -3 5 2031.50 2113.12 5.20 o
2 -3 5 359.32 326.15 2.28 o
3 -3 5 419.97 442.10 2.67 o
4 -3 5 0.23 0.10 1.19 <
5 -3 5 508.09 491.03 5.50 o
6 -3 5 111.03 123.09 2.63 o
-6 -2 5 49.98 54.08 2.03 o
-5 -2 5 23.54 19.79 2.01 o
-4 -2 5 25.58 22.78 1.93 o
-3 -2 5 305.26 302.72 3.49 o
-2 -2 5 846.95 800.74 4.86 o
-1 -2 5 475.76 462.38 2.95 o
0 -2 5 1256.09 1164.44 5.12 o
1 -2 5 198.58 196.56 1.73 o
2 -2 5 21.45 23.36 0.85 o
3 -2 5 93.19 88.81 1.60 o
4 -2 5 308.42 294.33 2.68 o
5 -2 5 125.99 126.87 2.83 o
6 -2 5 7.04 6.83 1.90 o
-6 -1 5 405.14 401.79 5.54 o
-5 -1 5 30.14 31.03 2.15 o
-4 -1 5 160.26 176.14 2.95 o
-3 -1 5 570.51 588.10 4.18 o
-2 -1 5 2464.31 2645.28 6.83 o
-1 -1 5 363.24 293.33 2.39 o
0 -1 5 107.29 106.58 1.64 o
1 -1 5 210.57 168.74 1.87 o
2 -1 5 734.35 864.02 2.80 o
3 -1 5 692.66 732.81 3.31 o
4 -1 5 422.55 399.02 3.97 o
5 -1 5 91.51 93.32 2.18 o
6 -1 5 184.48 207.50 3.99 o
-6 0 5 87.36 89.47 2.58 o
-5 0 5 9.70 9.54 1.79 o
-4 0 5 33.65 29.68 1.72 o
-3 0 5 6.95 5.98 1.19 o
-2 0 5 159.38 145.67 2.11 o
-1 0 5 175.51 172.43 2.27 o
0 0 5 3.38 2.72 1.13 <
1 0 5 1100.96 1092.30 6.42 o
2 0 5 2.82 6.33 0.68 o
3 0 5 89.19 84.75 1.58 o
4 0 5 332.78 324.72 3.62 o
5 0 5 165.38 158.50 3.98 o
6 0 5 120.14 144.31 3.33 o
-6 1 5 14.96 21.60 2.97 o
-5 1 5 262.32 268.83 3.90 o
-4 1 5 24.76 26.52 1.45 o
-3 1 5 704.20 763.43 3.13 o
-2 1 5 337.11 364.54 2.46 o
-1 1 5 1413.28 1535.13 8.85 o
0 1 5 7414.26 7764.31 10.75 o
1 1 5 639.90 684.37 3.02 o
2 1 5 145.09 163.97 1.71 o
3 1 5 64.88 84.86 1.85 o
4 1 5 301.66 299.23 3.55 o
5 1 5 69.85 84.49 2.94 o
6 1 5 109.16 90.13 3.39 o
-6 2 5 155.88 166.58 3.69 o
-5 2 5 193.26 210.91 3.64 o
-4 2 5 0.54 0.61 1.06 <
-3 2 5 527.32 511.12 3.11 o
-2 2 5 627.36 597.21 3.09 o
-1 2 5 146.29 160.44 1.51 o
0 2 5 379.51 450.42 2.33 o
1 2 5 54.10 50.17 1.09 o
2 2 5 21.60 20.97 1.10 o
3 2 5 192.19 200.66 3.50 o
4 2 5 9.99 7.23 2.46 <
5 2 5 102.99 95.91 3.08 o
-6 3 5 119.33 144.22 5.39 o
-5 3 5 1.11 2.55 2.16 <
-4 3 5 729.16 708.56 5.27 o
-3 3 5 387.00 371.94 3.37 o
-2 3 5 170.91 181.52 2.15 o
-1 3 5 942.07 930.63 3.92 o
0 3 5 964.69 1015.07 4.22 o
1 3 5 81.82 93.22 1.69 o
2 3 5 723.45 763.74 4.82 o
3 3 5 90.15 100.82 2.43 o
4 3 5 8.00 8.73 1.95 o
5 3 5 2.39 2.29 2.05 <
-5 4 5 2.41 2.96 1.93 <
-4 4 5 154.02 141.62 3.42 o
-3 4 5 419.14 416.49 5.06 o
-2 4 5 710.14 720.15 4.15 o
-1 4 5 138.16 135.88 1.90 o
0 4 5 18.21 20.89 1.25 o
1 4 5 230.68 239.35 3.00 o
2 4 5 508.01 539.03 5.85 o
3 4 5 1.20 2.94 2.10 <
4 4 5 49.01 51.84 2.44 o
-5 5 5 112.97 110.18 2.85 o
-4 5 5 15.87 15.03 2.03 o
-3 5 5 189.14 183.69 3.71 o
-2 5 5 227.12 222.00 3.30 o
-1 5 5 10.19 8.08 1.67 o
0 5 5 0.47 0.73 1.42 <
1 5 5 251.61 252.55 3.99 o
2 5 5 17.22 15.73 1.68 o
3 5 5 378.28 380.63 4.88 o
-3 6 5 16.34 12.31 2.21 o
-2 6 5 1.64 -0.64 2.13 <
-1 6 5 0.29 0.95 2.21 <
0 6 5 0.19 1.60 1.98 <
1 6 5 111.86 115.71 2.91 o
0 -7 6 99.82 103.11 3.66 o
1 -7 6 10.42 8.42 2.29 o
2 -7 6 0.07 0.65 2.14 <
-3 -6 6 33.03 25.84 2.47 o
-2 -6 6 24.76 24.63 2.97 o
-1 -6 6 3.09 3.06 1.88 <
0 -6 6 248.19 240.78 6.26 o
1 -6 6 131.06 130.55 3.68 o
2 -6 6 17.25 15.87 1.91 o
3 -6 6 20.99 21.98 1.83 o
4 -6 6 97.66 98.75 3.49 o
-4 -5 6 210.41 211.48 4.01 o
-3 -5 6 298.08 287.32 5.15 o
-2 -5 6 310.19 319.35 4.43 o
-1 -5 6 98.92 97.61 2.24 o
0 -5 6 2.57 1.29 1.61 <
1 -5 6 308.43 313.98 4.68 o
2 -5 6 642.77 647.86 5.72 o
3 -5 6 12.51 11.75 1.54 o
4 -5 6 0.20 -0.45 1.87 <
5 -5 6 28.77 23.43 2.24 o
-5 -4 6 19.33 15.49 2.10 o
-4 -4 6 152.26 167.78 3.52 o
-3 -4 6 1881.01 1933.95 10.60 o
-2 -4 6 783.69 812.55 5.63 o
-1 -4 6 201.77 203.13 2.97 o
0 -4 6 566.36 615.38 3.58 o
1 -4 6 317.75 308.11 3.48 o
2 -4 6 63.38 60.22 1.80 o
3 -4 6 1655.26 1671.51 5.98 o
4 -4 6 260.32 247.43 3.62 o
5 -4 6 161.87 172.97 4.04 o
-5 -3 6 30.62 27.23 2.10 o
-4 -3 6 84.95 84.19 3.00 o
-3 -3 6 260.04 263.76 4.06 o
-2 -3 6 2.22 1.69 1.23 <
-1 -3 6 7.05 6.52 0.99 o
0 -3 6 200.07 189.70 1.79 o
1 -3 6 127.95 121.92 1.63 o
2 -3 6 144.84 141.96 1.62 o
3 -3 6 509.07 522.20 2.98 o
4 -3 6 112.07 112.03 1.95 o
5 -3 6 420.15 434.07 4.41 o
6 -3 6 59.88 59.87 2.62 o
-6 -2 6 609.86 624.11 4.93 o
-5 -2 6 0.43 0.04 1.74 <
-4 -2 6 298.59 303.26 4.14 o
-3 -2 6 847.78 893.21 5.76 o
-2 -2 6 0.05 1.20 0.94 <
-1 -2 6 448.64 513.14 3.07 o
0 -2 6 2064.92 2461.41 6.29 o
1 -2 6 230.34 213.57 2.06 o
2 -2 6 1886.14 1973.91 5.81 o
3 -2 6 658.94 688.30 4.00 o
4 -2 6 222.61 223.95 2.55 o
5 -2 6 23.15 24.92 1.96 o
6 -2 6 103.76 108.66 2.87 o
-6 -1 6 77.91 73.72 2.34 o
-5 -1 6 232.94 213.89 4.29 o
-4 -1 6 283.72 280.68 3.76 o
-3 -1 6 7.50 5.41 1.06 o
-2 -1 6 12.26 10.56 0.82 o
-1 -1 6 311.34 324.79 2.65 o
0 -1 6 67.47 85.77 2.62 o
1 -1 6 153.09 150.15 1.70 o
2 -1 6 19.34 17.11 0.78 o
3 -1 6 6.88 6.81 0.94 o
4 -1 6 376.24 374.32 3.56 o
5 -1 6 8.06 7.01 1.71 o
6 -1 6 93.31 97.68 2.75 o
-6 0 6 79.90 67.02 2.96 o
-5 0 6 602.83 605.95 7.10 o
-4 0 6 58.68 53.26 1.99 o
-3 0 6 1465.84 1656.34 8.71 o
-2 0 6 1.29 1.50 0.72 <
-1 0 6 215.59 180.34 2.05 o
0 0 6 0.38 15.60 1.43 o
1 0 6 103.53 97.56 1.60 o
2 0 6 288.18 325.30 2.13 o
3 0 6 199.53 212.83 2.62 o
4 0 6 42.22 41.80 2.08 o
5 0 6 1564.50 1643.84 11.39 o
6 0 6 0.26 -0.11 1.57 <
-6 1 6 95.84 85.55 2.90 o
-5 1 6 240.29 244.89 3.83 o
-4 1 6 306.96 301.83 3.94 o
-3 1 6 75.98 78.43 1.53 o
-2 1 6 112.02 117.45 1.49 o
-1 1 6 654.62 596.90 3.42 o
0 1 6 928.10 841.10 4.59 o
1 1 6 76.14 65.64 1.08 o
2 1 6 329.07 308.47 2.21 o
3 1 6 31.07 27.90 1.42 o
4 1 6 21.64 26.42 1.91 o
5 1 6 114.98 105.93 2.60 o
-6 2 6 22.70 25.94 2.34 o
-5 2 6 481.38 474.52 6.02 o
-4 2 6 41.47 35.01 1.43 o
-3 2 6 1658.60 1723.40 5.24 o
-2 2 6 831.39 800.70 4.47 o
-1 2 6 767.33 779.64 3.16 o
0 2 6 2.36 -0.09 0.81 <
1 2 6 411.62 401.16 2.48 o
2 2 6 1010.15 1002.88 4.21 o
3 2 6 823.32 856.97 8.08 o
4 2 6 36.73 27.91 2.74 o
5 2 6 538.20 545.74 6.08 o
-6 3 6 44.89 48.75 3.66 o
-5 3 6 80.07 80.17 2.42 o
-4 3 6 10.31 7.86 1.54 o
-3 3 6 221.66 225.55 2.79 o
-2 3 6 102.97 98.77 1.93 o
-1 3 6 298.72 293.59 2.31 o
0 3 6 139.06 147.19 1.78 o
1 3 6 62.01 61.24 1.40 o
2 3 6 377.64 380.54 3.04 o
3 3 6 1034.78 1106.17 9.73 o
4 3 6 30.18 30.68 2.55 o
-5 4 6 299.45 349.24 6.34 o
-4 4 6 55.25 47.53 2.23 o
-3 4 6 831.83 862.50 7.16 o
-2 4 6 0.42 0.51 1.19 <
-1 4 6 362.92 370.74 3.39 o
0 4 6 28.59 27.00 1.57 o
1 4 6 185.44 190.38 2.79 o
2 4 6 278.82 273.54 3.73 o
3 4 6 28.78 35.65 2.56 o
4 4 6 175.08 165.95 3.45 o
-5 5 6 131.73 120.48 3.62 o
-4 5 6 155.70 161.00 3.43 o
-3 5 6 241.91 232.74 4.54 o
-2 5 6 4.02 4.86 1.59 o
-1 5 6 528.83 494.51 5.42 o
0 5 6 221.02 224.43 3.06 o
1 5 6 15.06 15.26 2.26 o
2 5 6 59.61 60.45 2.72 o
3 5 6 33.70 37.61 2.00 o
-3 6 6 56.38 49.35 2.52 o
-2 6 6 457.81 457.65 5.87 o
-1 6 6 9.21 10.15 2.24 o
0 6 6 220.17 231.63 4.10 o
1 6 6 241.33 249.41 4.98 o
0 -7 7 40.08 41.50 2.75 o
1 -7 7 178.78 175.92 4.61 o
-3 -6 7 6.98 5.15 2.20 <
-2 -6 7 193.74 199.76 5.10 o
-1 -6 7 162.18 172.51 3.46 o
0 -6 7 128.77 126.94 4.90 o
1 -6 7 222.10 234.97 6.36 o
2 -6 7 212.49 201.78 3.79 o
3 -6 7 158.90 158.90 2.75 o
4 -6 7 56.70 60.50 2.79 o
-4 -5 7 78.04 76.34 2.69 o
-3 -5 7 15.60 11.76 2.34 o
-2 -5 7 61.07 60.07 2.37 o
-1 -5 7 245.45 256.21 3.81 o
0 -5 7 304.33 322.43 4.12 o
1 -5 7 217.93 231.16 4.21 o
2 -5 7 264.59 254.09 3.31 o
3 -5 7 1290.64 1328.78 8.48 o
4 -5 7 179.22 171.76 3.88 o
-5 -4 7 16.33 16.95 1.98 o
-4 -4 7 90.45 87.71 2.81 o
-3 -4 7 116.25 115.70 2.77 o
-2 -4 7 21.53 18.82 1.63 o
-1 -4 7 18.65 21.32 1.34 o
0 -4 7 197.29 210.12 2.58 o
1 -4 7 187.72 176.19 2.86 o
2 -4 7 252.04 250.40 2.81 o
3 -4 7 84.39 74.92 1.64 o
4 -4 7 0.27 -0.45 1.66 <
5 -4 7 16.66 18.44 2.27 o
-5 -3 7 476.88 483.05 6.18 o
-4 -3 7 710.63 783.81 9.03 o
-3 -3 7 1162.42 1197.85 7.83 o
-2 -3 7 0.55 0.51 1.26 <
-1 -3 7 551.24 599.94 3.45 o
0 -3 7 145.52 167.33 2.07 o
1 -3 7 1594.38 1581.66 5.51 o
2 -3 7 38.86 38.69 1.12 o
3 -3 7 460.84 459.36 3.07 o
4 -3 7 44.05 38.05 1.63 o
5 -3 7 52.34 49.58 2.00 o
-6 -2 7 65.54 67.02 1.77 o
-5 -2 7 140.26 143.54 3.07 o
-4 -2 7 29.44 29.64 2.05 o
-3 -2 7 328.30 326.82 3.69 o
-2 -2 7 662.41 661.23 3.45 o
-1 -2 7 447.81 444.01 2.89 o
0 -2 7 385.65 390.72 2.73 o
1 -2 7 628.98 632.19 3.05 o
2 -2 7 110.16 114.01 1.33 o
3 -2 7 365.36 358.75 2.86 o
4 -2 7 161.32 150.39 2.11 o
5 -2 7 6.33 3.30 1.62 <
6 -2 7 1.02 2.29 2.10 <
-6 -1 7 21.52 18.21 1.73 o
-5 -1 7 199.25 203.97 3.65 o
-4 -1 7 78.89 74.44 2.37 o
-3 -1 7 187.64 203.02 1.88 o
-2 -1 7 24.22 25.80 0.85 o
-1 -1 7 2299.15 2309.05 6.61 o
0 -1 7 2923.26 3045.57 15.37 o
1 -1 7 1873.97 2122.31 4.54 o
2 -1 7 1.65 1.91 0.64 <
3 -1 7 545.33 596.23 3.24 o
4 -1 7 130.67 127.67 2.35 o
5 -1 7 22.19 26.18 2.05 o
6 -1 7 78.55 68.36 2.96 o
-6 0 7 41.55 39.77 1.99 o
-5 0 7 19.46 19.23 2.44 o
-4 0 7 21.22 21.08 1.75 o
-3 0 7 41.04 43.46 1.37 o
-2 0 7 51.20 45.83 1.13 o
-1 0 7 682.04 721.66 3.49 o
0 0 7 199.51 210.58 2.42 o
1 0 7 87.98 67.56 1.08 o
2 0 7 216.79 209.65 2.00 o
3 0 7 128.15 131.18 2.54 o
4 0 7 133.73 130.43 3.44 o
5 0 7 116.22 111.81 3.51 o
-6 1 7 29.29 27.45 2.23 o
-5 1 7 422.27 442.33 5.05 o
-4 1 7 139.79 138.08 2.16 o
-3 1 7 13.53 14.20 1.13 o
-2 1 7 423.62 422.22 2.46 o
-1 1 7 0.28 2.05 0.62 o
0 1 7 1173.80 1198.25 4.60 o
1 1 7 1390.78 1525.83 4.63 o
2 1 7 7.20 12.41 0.83 o
3 1 7 1648.32 1714.03 7.45 o
4 1 7 350.16 345.50 3.11 o
5 1 7 102.01 105.71 2.99 o
-6 2 7 86.78 91.22 2.95 o
-5 2 7 10.23 9.93 1.81 o
-4 2 7 3.80 4.95 1.15 o
-3 2 7 221.52 216.31 2.17 o
-2 2 7 287.53 258.32 2.07 o
-1 2 7 154.85 158.85 1.68 o
0 2 7 536.77 584.21 3.76 o
1 2 7 144.21 154.18 1.85 o
2 2 7 15.01 13.02 1.16 o
3 2 7 161.01 162.46 2.85 o
4 2 7 87.92 76.28 3.18 o
5 2 7 186.06 180.34 3.57 o
-6 3 7 50.33 47.06 3.69 o
-5 3 7 1099.06 1110.75 6.94 o
-4 3 7 93.64 94.73 2.34 o
-3 3 7 906.36 905.43 4.81 o
-2 3 7 366.77 357.53 3.39 o
-1 3 7 1.47 1.04 0.96 <
0 3 7 83.82 70.66 1.45 o
1 3 7 330.69 359.09 2.90 o
2 3 7 65.62 63.04 1.59 o
3 3 7 100.70 104.34 3.60 o
4 3 7 24.83 27.02 2.42 o
-5 4 7 271.46 258.06 4.67 o
-4 4 7 189.38 194.27 3.45 o
-3 4 7 696.63 680.02 5.14 o
-2 4 7 634.32 641.06 4.32 o
-1 4 7 98.34 100.49 1.98 o
0 4 7 30.15 30.28 1.65 o
1 4 7 788.52 817.89 5.40 o
2 4 7 305.53 318.40 4.68 o
3 4 7 16.82 19.51 2.18 o
-4 5 7 217.43 192.85 4.25 o
-3 5 7 107.24 107.15 2.93 o
-2 5 7 128.28 128.93 3.06 o
-1 5 7 80.75 76.61 2.42 o
0 5 7 354.83 363.28 4.19 o
1 5 7 0.96 0.63 1.85 <
2 5 7 0.44 -0.18 1.87 <
-2 6 7 5.66 8.53 2.03 o
-1 6 7 14.51 15.91 1.82 o
0 6 7 139.18 142.58 4.08 o
1 -7 8 2.49 -0.24 2.38 <
-3 -6 8 326.35 321.43 5.76 o
-2 -6 8 10.57 3.47 2.35 <
-1 -6 8 35.35 36.15 2.08 o
0 -6 8 0.03 -2.39 2.55 <
1 -6 8 148.47 144.75 5.28 o
2 -6 8 229.38 211.84 3.21 o
3 -6 8 124.95 114.26 2.15 o
-4 -5 8 289.31 302.76 4.45 o
-3 -5 8 310.03 309.32 5.01 o
-2 -5 8 94.99 86.02 3.20 o
-1 -5 8 27.72 24.26 1.75 o
0 -5 8 29.22 32.85 1.97 o
1 -5 8 105.27 113.47 3.34 o
2 -5 8 104.23 104.08 2.37 o
3 -5 8 23.93 22.99 1.88 o
4 -5 8 16.53 18.10 1.93 o
-5 -4 8 278.51 290.46 4.26 o
-4 -4 8 55.96 51.64 2.43 o
-3 -4 8 81.99 78.24 2.83 o
-2 -4 8 1258.86 1317.38 10.01 o
-1 -4 8 335.38 327.64 5.04 o
0 -4 8 101.99 101.08 1.99 o
1 -4 8 1373.94 1368.77 7.60 o
2 -4 8 1342.44 1364.92 6.97 o
3 -4 8 7.14 7.82 1.20 o
4 -4 8 564.74 579.81 5.76 o
5 -4 8 38.26 38.18 2.39 o
-5 -3 8 0.40 -0.53 1.69 <
-4 -3 8 110.28 114.15 3.20 o
-3 -3 8 238.52 244.10 3.40 o
-2 -3 8 71.85 66.00 1.93 o
-1 -3 8 147.73 149.26 1.96 o
0 -3 8 393.76 397.30 2.95 o
1 -3 8 176.05 162.54 2.28 o
2 -3 8 197.98 198.19 1.85 o
3 -3 8 228.45 221.66 2.31 o
4 -3 8 517.67 527.29 3.96 o
5 -3 8 38.35 38.89 1.76 o
-6 -2 8 268.40 242.91 3.10 o
-5 -2 8 145.18 158.04 3.23 o
-4 -2 8 19.39 17.85 1.53 o
-3 -2 8 738.72 768.35 5.44 o
-2 -2 8 73.25 89.79 1.42 o
-1 -2 8 426.36 448.03 2.69 o
0 -2 8 827.53 849.47 4.13 o
1 -2 8 42.32 47.49 1.27 o
2 -2 8 6.03 4.03 0.81 o
3 -2 8 79.22 86.15 1.70 o
4 -2 8 12.42 13.92 1.48 o
5 -2 8 1070.64 1073.00 7.36 o
-6 -1 8 87.61 77.95 2.91 o
-5 -1 8 184.79 188.90 3.51 o
-4 -1 8 276.66 273.56 3.81 o
-3 -1 8 132.59 136.14 1.85 o
-2 -1 8 0.06 -0.81 1.04 <
-1 -1 8 176.10 187.64 1.66 o
0 -1 8 111.83 119.13 2.57 o
1 -1 8 147.30 140.97 1.66 o
2 -1 8 71.66 68.20 1.15 o
3 -1 8 208.12 207.20 2.12 o
4 -1 8 74.45 79.63 2.71 o
5 -1 8 177.50 184.76 4.19 o
-6 0 8 23.58 32.99 1.88 o
-5 0 8 704.42 741.38 7.98 o
-4 0 8 352.28 353.96 4.27 o
-3 0 8 715.41 766.70 4.50 o
-2 0 8 118.75 150.08 1.98 o
-1 0 8 33.65 31.50 1.10 o
0 0 8 2227.88 2467.48 7.55 o
1 0 8 347.91 363.96 2.49 o
2 0 8 5.14 5.27 0.88 o
3 0 8 79.61 81.08 2.23 o
4 0 8 781.77 780.55 6.58 o
5 0 8 25.47 33.45 1.76 o
-6 1 8 153.35 157.95 3.69 o
-5 1 8 323.75 354.44 5.57 o
-4 1 8 41.63 38.93 1.58 o
-3 1 8 164.51 176.14 2.68 o
-2 1 8 189.24 194.84 1.63 o
-1 1 8 582.04 536.89 2.56 o
0 1 8 15.26 9.53 0.89 o
1 1 8 123.82 133.94 1.54 o
2 1 8 67.43 61.94 1.30 o
3 1 8 282.82 276.62 2.67 o
4 1 8 191.75 177.23 2.37 o
5 1 8 13.86 9.91 1.65 o
-6 2 8 378.16 352.11 4.80 o
-5 2 8 4.62 1.27 1.42 <
-4 2 8 1006.50 1045.40 5.86 o
-3 2 8 34.09 43.22 1.39 o
-2 2 8 2924.74 2916.63 7.37 o
-1 2 8 41.63 50.29 1.21 o
0 2 8 1200.38 1311.00 5.34 o
1 2 8 2141.06 2219.78 6.51 o
2 2 8 1347.54 1346.57 5.25 o
3 2 8 36.28 34.80 1.85 o
4 2 8 330.62 320.49 5.18 o
5 2 8 0.93 1.90 2.29 <
-5 3 8 22.11 20.30 1.79 o
-4 3 8 22.79 23.11 1.80 o
-3 3 8 92.18 84.67 1.85 o
-2 3 8 1279.33 1269.98 5.56 o
-1 3 8 0.79 1.51 1.05 <
0 3 8 396.91 404.16 2.98 o
1 3 8 745.52 766.15 4.27 o
2 3 8 804.68 832.26 4.54 o
3 3 8 198.58 202.72 4.47 o
4 3 8 413.12 432.01 5.76 o
-5 4 8 2.57 13.38 2.78 o
-4 4 8 0.03 2.08 1.78 <
-3 4 8 87.02 86.88 2.04 o
-2 4 8 748.24 770.82 4.48 o
-1 4 8 218.45 230.41 2.76 o
0 4 8 138.96 137.58 2.36 o
1 4 8 24.32 23.70 1.63 o
2 4 8 71.30 71.02 2.16 o
3 4 8 687.13 701.39 6.84 o
-4 5 8 75.63 70.60 2.40 o
-3 5 8 5.62 3.58 2.29 <
-2 5 8 153.30 143.00 3.46 o
-1 5 8 126.95 127.80 3.19 o
0 5 8 316.51 317.00 4.51 o
1 5 8 5.87 2.96 1.89 <
2 5 8 10.08 7.78 1.93 o
-1 6 8 221.43 216.17 4.86 o
0 6 8 30.31 26.40 2.13 o
-2 -6 9 173.06 161.66 3.21 o
-1 -6 9 76.08 73.25 1.96 o
0 -6 9 25.41 19.14 2.51 o
1 -6 9 318.64 320.05 5.02 o
2 -6 9 166.29 161.54 2.84 o
3 -6 9 176.94 173.38 2.40 o
-4 -5 9 22.83 18.74 1.88 o
-3 -5 9 3.50 1.34 2.29 <
-2 -5 9 177.18 181.63 4.25 o
-1 -5 9 332.08 326.94 4.14 o
0 -5 9 406.32 414.27 4.68 o
1 -5 9 0.47 1.59 1.54 <
2 -5 9 667.76 674.65 5.92 o
3 -5 9 60.86 56.48 1.92 o
4 -5 9 258.90 254.11 4.37 o
-4 -4 9 0.08 0.42 1.50 <
-3 -4 9 13.53 16.19 1.76 o
-2 -4 9 0.01 1.00 1.63 <
-1 -4 9 2.87 0.14 1.40 <
0 -4 9 8.55 9.82 1.29 o
1 -4 9 107.60 107.56 2.70 o
2 -4 9 736.60 745.85 5.41 o
3 -4 9 0.46 -0.20 1.37 <
4 -4 9 38.54 42.05 1.82 o
-5 -3 9 1.74 1.25 1.74 <
-4 -3 9 795.17 847.13 5.99 o
-3 -3 9 95.06 99.61 2.45 o
-2 -3 9 77.14 84.25 2.09 o
-1 -3 9 1885.71 1949.27 8.80 o
0 -3 9 552.19 600.98 3.43 o
1 -3 9 228.81 239.05 2.59 o
2 -3 9 16.99 18.30 1.18 o
3 -3 9 285.01 296.17 2.66 o
4 -3 9 73.67 80.88 1.87 o
5 -3 9 39.76 39.11 1.82 o
-6 -2 9 83.71 81.25 2.59 o
-5 -2 9 70.07 69.31 2.15 o
-4 -2 9 137.76 140.48 2.54 o
-3 -2 9 134.53 131.28 1.92 o
-2 -2 9 625.63 620.56 3.73 o
-1 -2 9 808.58 833.00 3.74 o
0 -2 9 214.61 216.19 2.19 o
1 -2 9 74.34 73.17 1.19 o
2 -2 9 23.88 20.50 0.99 o
3 -2 9 3.30 4.69 1.00 o
4 -2 9 63.67 65.21 2.05 o
5 -2 9 0.03 -1.95 1.69 <
-6 -1 9 18.76 18.89 1.60 o
-5 -1 9 663.29 645.45 6.65 o
-4 -1 9 169.84 171.92 2.63 o
-3 -1 9 1.01 1.02 1.11 <
-2 -1 9 2.37 4.94 0.91 o
-1 -1 9 2.49 0.44 0.86 <
0 -1 9 998.19 954.26 4.57 o
1 -1 9 64.51 73.68 1.27 o
2 -1 9 193.40 206.13 2.11 o
3 -1 9 154.15 160.31 2.80 o
4 -1 9 4.77 3.32 1.75 <
5 -1 9 21.14 19.50 1.82 o
-6 0 9 15.31 13.85 1.68 o
-5 0 9 180.81 186.90 4.45 o
-4 0 9 1.57 2.15 1.63 <
-3 0 9 16.95 17.49 1.35 o
-2 0 9 4.78 5.27 0.89 o
-1 0 9 240.55 222.73 1.92 o
0 0 9 257.75 253.76 2.22 o
1 0 9 542.76 534.59 3.56 o
2 0 9 73.70 64.25 1.63 o
3 0 9 3.29 2.55 1.77 <
4 0 9 39.91 34.16 1.77 o
5 0 9 65.85 65.07 2.65 o
-6 1 9 174.65 178.40 3.82 o
-5 1 9 442.18 430.59 5.06 o
-4 1 9 533.65 539.03 4.58 o
-3 1 9 0.67 -0.43 1.36 <
-2 1 9 606.07 633.80 2.93 o
-1 1 9 1520.80 1609.07 4.72 o
0 1 9 1417.17 1501.98 6.16 o
1 1 9 3.00 1.31 0.89 <
2 1 9 106.37 105.83 1.79 o
3 1 9 742.99 777.89 4.74 o
4 1 9 252.16 258.45 3.08 o
5 1 9 79.08 83.13 2.79 o
-6 2 9 0.58 8.43 2.28 o
-5 2 9 88.91 86.47 2.21 o
-4 2 9 89.93 81.28 2.12 o
-3 2 9 201.21 182.13 2.39 o
-2 2 9 67.80 58.55 1.29 o
-1 2 9 692.43 712.11 3.87 o
0 2 9 1003.45 1068.57 5.09 o
1 2 9 19.17 20.86 1.29 o
2 2 9 88.41 90.02 1.73 o
3 2 9 426.81 417.50 4.91 o
4 2 9 130.05 131.38 3.76 o
-5 3 9 298.78 269.02 5.18 o
-4 3 9 1651.09 1667.85 7.83 o
-3 3 9 507.26 510.88 4.07 o
-2 3 9 232.61 244.76 2.74 o
-1 3 9 153.19 137.72 2.06 o
0 3 9 770.66 817.20 4.33 o
1 3 9 225.50 253.65 2.68 o
2 3 9 64.05 69.05 1.69 o
3 3 9 76.22 88.48 3.12 o
4 3 9 40.64 39.67 2.14 o
-5 4 9 1.33 2.06 1.95 <
-4 4 9 802.81 778.48 8.11 o
-3 4 9 497.54 496.85 5.88 o
-2 4 9 293.69 303.96 3.22 o
-1 4 9 236.69 234.98 3.10 o
0 4 9 480.78 509.47 4.04 o
1 4 9 92.48 88.94 2.15 o
2 4 9 48.00 44.18 2.56 o
3 4 9 11.59 8.32 1.80 o
-4 5 9 85.04 83.09 2.72 o
-3 5 9 34.19 26.74 2.40 o
-2 5 9 184.65 189.16 4.44 o
-1 5 9 78.25 76.55 3.34 o
0 5 9 1.62 1.79 1.75 <
1 5 9 285.66 302.32 5.09 o
-2 -6 10 203.83 187.83 4.74 o
-1 -6 10 13.19 5.59 1.74 o
0 -6 10 0.18 -2.17 2.38 <
1 -6 10 0.06 1.30 1.82 <
2 -6 10 4.63 4.42 1.51 <
3 -6 10 144.08 130.48 3.84 o
-4 -5 10 249.17 276.78 5.48 o
-3 -5 10 109.89 101.53 2.81 o
-2 -5 10 35.04 31.47 2.27 o
-1 -5 10 14.76 14.20 1.46 o
0 -5 10 39.02 38.78 2.18 o
1 -5 10 16.07 19.67 1.69 o
2 -5 10 4.27 4.40 1.50 <
3 -5 10 17.68 12.71 1.75 o
4 -5 10 8.06 7.93 2.01 o
-4 -4 10 18.44 18.60 1.59 o
-3 -4 10 1308.07 1369.01 6.68 o
-2 -4 10 45.18 47.12 2.56 o
-1 -4 10 78.89 79.66 2.52 o
0 -4 10 99.58 88.14 2.17 o
1 -4 10 266.78 276.45 3.91 o
2 -4 10 307.91 309.28 3.40 o
3 -4 10 296.16 325.82 3.50 o
4 -4 10 0.72 1.89 1.55 <
-5 -3 10 31.21 32.46 1.98 o
-4 -3 10 66.65 62.28 2.16 o
-3 -3 10 681.06 689.72 4.72 o
-2 -3 10 36.56 30.67 1.32 o
-1 -3 10 312.85 323.30 3.01 o
0 -3 10 183.96 182.15 2.16 o
1 -3 10 39.08 35.24 1.51 o
2 -3 10 88.51 88.49 1.76 o
3 -3 10 602.27 629.74 4.08 o
4 -3 10 132.88 134.60 2.20 o
5 -3 10 192.99 190.20 3.50 o
-6 -2 10 19.27 26.71 3.16 o
-5 -2 10 417.85 421.47 4.93 o
-4 -2 10 511.78 532.52 4.06 o
-3 -2 10 111.72 132.24 2.16 o
-2 -2 10 940.75 958.81 4.78 o
-1 -2 10 194.19 231.45 2.23 o
0 -2 10 1271.94 1323.78 6.17 o
1 -2 10 264.79 243.56 2.02 o
2 -2 10 0.93 1.60 0.90 <
3 -2 10 243.95 258.86 2.50 o
4 -2 10 724.05 726.96 6.48 o
5 -2 10 30.62 38.35 1.89 o
-6 -1 10 52.25 58.42 2.03 o
-5 -1 10 237.00 249.61 4.93 o
-4 -1 10 27.26 26.90 1.55 o
-3 -1 10 1.43 1.15 1.21 <
-2 -1 10 603.33 621.11 3.68 o
-1 -1 10 315.96 336.47 2.38 o
0 -1 10 201.93 216.79 2.54 o
1 -1 10 45.02 46.68 1.31 o
2 -1 10 11.23 10.69 1.17 o
3 -1 10 2.15 1.36 1.42 <
4 -1 10 611.20 622.23 6.05 o
5 -1 10 7.82 7.46 1.76 o
-6 0 10 264.03 249.81 4.29 o
-5 0 10 3.69 4.41 1.78 <
-4 0 10 34.62 44.94 2.20 o
-3 0 10 112.02 133.62 2.34 o
-2 0 10 2130.50 2262.16 7.51 o
-1 0 10 1653.95 1839.77 5.46 o
0 0 10 51.34 63.80 1.44 o
1 0 10 156.36 139.08 2.17 o
2 0 10 4.91 3.97 1.10 o
3 0 10 1245.77 1214.69 9.61 o
4 0 10 0.64 3.85 1.74 <
5 0 10 554.89 568.93 5.91 o
-6 1 10 322.35 336.34 4.75 o
-5 1 10 78.50 90.36 2.78 o
-4 1 10 54.83 55.37 1.97 o
-3 1 10 38.96 35.68 1.62 o
-2 1 10 467.74 467.11 3.53 o
-1 1 10 26.55 37.03 1.28 o
0 1 10 221.29 217.11 2.42 o
1 1 10 0.18 1.17 1.30 <
2 1 10 42.97 36.95 1.57 o
3 1 10 50.87 45.01 1.56 o
4 1 10 10.22 10.33 1.37 o
-6 2 10 66.68 69.98 2.33 o
-5 2 10 390.13 409.93 4.03 o
-4 2 10 936.85 1016.93 6.83 o
-3 2 10 417.05 426.64 3.51 o
-2 2 10 53.21 61.83 1.30 o
-1 2 10 773.09 831.66 4.35 o
0 2 10 2.88 1.82 1.13 <
1 2 10 276.43 271.81 3.08 o
2 2 10 762.79 772.34 4.97 o
3 2 10 825.98 836.47 6.94 o
4 2 10 112.59 99.96 2.96 o
-5 3 10 54.22 51.84 2.63 o
-4 3 10 114.29 110.95 3.10 o
-3 3 10 468.37 463.71 3.90 o
-2 3 10 221.29 221.86 2.32 o
-1 3 10 64.44 68.56 1.82 o
0 3 10 49.82 54.81 1.45 o
1 3 10 350.69 359.14 3.18 o
2 3 10 690.64 693.02 4.38 o
3 3 10 843.24 833.87 7.45 o
-5 4 10 3.79 2.88 1.94 <
-4 4 10 128.42 124.26 3.53 o
-3 4 10 42.75 45.25 2.42 o
-2 4 10 124.43 118.85 2.47 o
-1 4 10 0.34 0.69 1.33 <
0 4 10 4.49 3.28 1.47 <
1 4 10 264.45 270.11 4.18 o
2 4 10 27.61 27.34 2.24 o
-4 5 10 85.95 72.15 2.81 o
-3 5 10 4.71 2.78 1.88 <
-2 5 10 6.04 3.87 1.67 <
-1 5 10 88.24 87.37 2.56 o
0 5 10 150.27 158.67 3.54 o
1 5 10 207.64 213.65 4.77 o
-2 -6 11 144.45 135.06 3.96 o
-1 -6 11 42.60 38.63 1.81 o
0 -6 11 5.35 0.64 2.42 <
1 -6 11 161.26 161.14 3.62 o
2 -6 11 298.98 280.65 3.42 o
-3 -5 11 47.01 48.79 3.59 o
-2 -5 11 17.83 17.42 3.30 o
-1 -5 11 8.20 8.82 1.85 o
0 -5 11 108.56 104.12 3.68 o
1 -5 11 424.79 424.79 4.29 o
2 -5 11 87.66 86.51 2.58 o
3 -5 11 351.97 366.82 5.36 o
4 -5 11 5.91 9.92 2.02 o
-4 -4 11 0.07 2.58 2.23 <
-3 -4 11 15.75 15.15 2.24 o
-2 -4 11 0.44 -2.69 2.23 <
-1 -4 11 0.13 0.36 1.64 <
0 -4 11 29.02 25.79 1.75 o
1 -4 11 388.25 390.16 5.65 o
2 -4 11 317.02 313.46 3.45 o
3 -4 11 52.88 52.16 1.97 o
4 -4 11 45.38 45.64 1.82 o
-5 -3 11 523.02 533.18 6.45 o
-4 -3 11 261.66 260.15 4.16 o
-3 -3 11 0.87 -0.02 1.50 <
-2 -3 11 84.21 79.26 2.08 o
-1 -3 11 44.06 46.01 1.64 o
0 -3 11 95.90 84.37 1.77 o
1 -3 11 4.75 9.42 1.19 o
2 -3 11 277.74 271.54 2.81 o
3 -3 11 118.28 122.39 2.63 o
4 -3 11 43.48 47.98 1.83 o
-5 -2 11 365.59 362.19 4.54 o
-4 -2 11 6.58 5.29 1.43 o
-3 -2 11 62.16 65.93 1.60 o
-2 -2 11 199.26 201.29 2.29 o
-1 -2 11 171.29 159.84 2.60 o
0 -2 11 26.31 22.88 1.54 o
1 -2 11 366.95 381.86 3.02 o
2 -2 11 1.48 1.76 1.17 <
3 -2 11 111.89 112.05 2.24 o
4 -2 11 1.95 3.40 1.80 <
5 -2 11 16.96 23.07 2.05 o
-6 -1 11 480.63 542.92 4.79 o
-5 -1 11 92.77 75.07 3.08 o
-4 -1 11 1638.44 1701.56 8.96 o
-3 -1 11 4.99 6.59 1.18 o
-2 -1 11 346.89 342.57 2.71 o
-1 -1 11 882.06 888.83 5.99 o
0 -1 11 1381.59 1411.93 9.06 o
1 -1 11 668.94 745.61 4.95 o
2 -1 11 8.03 6.56 1.23 o
3 -1 11 395.47 418.85 4.35 o
4 -1 11 17.37 17.34 1.83 o
5 -1 11 23.99 22.20 1.85 o
-6 0 11 38.45 41.13 2.24 o
-5 0 11 18.91 24.66 2.04 o
-4 0 11 695.80 718.67 6.41 o
-3 0 11 8.43 7.25 1.41 o
-2 0 11 46.89 46.01 1.66 o
-1 0 11 852.91 879.82 4.08 o
0 0 11 962.98 1008.15 4.81 o
1 0 11 0.86 2.00 1.19 <
2 0 11 133.22 137.07 2.40 o
3 0 11 82.09 78.19 2.67 o
4 0 11 46.63 42.80 2.14 o
5 0 11 59.72 73.49 2.84 o
-6 1 11 8.29 8.77 1.97 o
-5 1 11 662.23 648.13 6.04 o
-4 1 11 1029.45 1033.60 6.46 o
-3 1 11 3.36 5.01 1.42 o
-2 1 11 408.88 409.07 3.11 o
-1 1 11 343.42 365.24 3.69 o
0 1 11 0.66 2.76 1.21 <
1 1 11 1847.79 1988.10 9.93 o
2 1 11 484.95 496.08 4.91 o
3 1 11 96.67 93.58 2.69 o
4 1 11 3.57 7.38 1.65 o
-5 2 11 33.82 30.17 1.62 o
-4 2 11 209.64 201.49 3.22 o
-3 2 11 201.71 190.97 2.73 o
-2 2 11 0.02 -0.36 0.90 <
-1 2 11 329.31 338.58 3.31 o
0 2 11 93.33 91.55 2.11 o
1 2 11 185.79 191.66 2.78 o
2 2 11 222.87 213.94 3.23 o
3 2 11 308.51 317.05 4.38 o
4 2 11 4.39 3.58 3.56 <
-5 3 11 209.84 208.79 3.99 o
-4 3 11 7.12 5.10 2.19 <
-3 3 11 1.49 1.02 1.80 <
-2 3 11 268.01 277.63 2.53 o
-1 3 11 55.80 55.42 1.77 o
0 3 11 0.87 0.18 1.17 <
1 3 11 20.69 20.98 1.47 o
2 3 11 8.36 11.38 1.50 o
3 3 11 0.75 1.98 2.11 <
-4 4 11 185.79 201.58 4.17 o
-3 4 11 4.48 3.64 1.85 <
-2 4 11 213.71 208.71 3.52 o
-1 4 11 196.92 191.12 2.73 o
0 4 11 154.34 149.93 2.64 o
1 4 11 77.81 74.65 2.14 o
2 4 11 14.95 11.31 2.08 o
-3 5 11 725.05 685.51 7.73 o
-2 5 11 4.07 6.00 1.69 o
-1 5 11 79.87 79.47 2.36 o
0 5 11 34.00 36.10 1.88 o
-1 -6 12 19.28 13.77 3.70 o
0 -6 12 195.73 184.19 3.49 o
1 -6 12 5.24 4.61 2.25 <
2 -6 12 3.72 -0.34 2.02 <
-3 -5 12 172.94 179.71 3.83 o
-2 -5 12 33.04 24.92 2.55 o
-1 -5 12 84.64 85.01 2.51 o
0 -5 12 2.14 -3.31 2.18 <
1 -5 12 8.26 3.67 1.59 <
2 -5 12 7.91 6.46 1.47 o
3 -5 12 17.29 16.88 1.51 o
-4 -4 12 199.77 217.91 3.99 o
-3 -4 12 15.72 15.55 2.52 o
-2 -4 12 798.57 830.87 11.68 o
-1 -4 12 276.51 271.87 5.30 o
0 -4 12 225.90 237.27 3.91 o
1 -4 12 45.28 48.82 1.86 o
2 -4 12 27.70 27.45 1.56 o
3 -4 12 369.79 368.89 4.38 o
4 -4 12 312.84 310.05 7.28 o
-5 -3 12 1.30 2.16 2.40 <
-4 -3 12 100.55 92.75 3.50 o
-3 -3 12 243.59 251.93 3.02 o
-2 -3 12 597.70 622.40 7.44 o
-1 -3 12 4.28 5.47 1.32 o
0 -3 12 548.74 544.81 4.25 o
1 -3 12 9.44 9.25 1.21 o
2 -3 12 1.03 0.55 1.16 <
3 -3 12 22.74 22.04 1.38 o
4 -3 12 528.61 540.44 6.21 o
-5 -2 12 163.15 172.30 3.15 o
-4 -2 12 587.57 586.81 4.89 o
-3 -2 12 213.32 209.54 2.47 o
-2 -2 12 147.39 165.46 2.19 o
-1 -2 12 1786.60 1857.69 8.19 o
0 -2 12 130.65 121.87 2.49 o
1 -2 12 99.71 92.58 1.84 o
2 -2 12 263.77 275.97 3.25 o
3 -2 12 917.78 969.95 7.58 o
4 -2 12 1.18 -0.66 1.78 <
-6 -1 12 23.18 20.61 1.98 o
-5 -1 12 1.26 0.53 1.63 <
-4 -1 12 12.31 10.75 1.37 o
-3 -1 12 71.61 69.90 1.77 o
-2 -1 12 30.86 27.73 1.23 o
-1 -1 12 202.83 207.04 3.98 o
0 -1 12 53.47 53.89 1.75 o
1 -1 12 170.41 164.00 2.19 o
2 -1 12 106.88 103.87 2.11 o
3 -1 12 525.08 545.03 5.68 o
4 -1 12 14.05 17.99 1.74 o
-6 0 12 257.82 286.42 4.25 o
-5 0 12 197.55 199.94 3.00 o
-4 0 12 624.24 644.50 6.17 o
-3 0 12 1.16 1.55 1.33 <
-2 0 12 68.11 77.75 2.02 o
-1 0 12 18.83 13.89 1.37 o
0 0 12 180.20 183.22 2.75 o
1 0 12 0.40 3.37 1.35 <
2 0 12 275.08 272.82 3.36 o
3 0 12 14.76 12.97 1.85 o
4 0 12 886.74 912.53 6.64 o
-6 1 12 381.15 442.27 6.46 o
-5 1 12 137.49 140.98 3.09 o
-4 1 12 272.64 278.24 3.61 o
-3 1 12 269.06 263.19 3.38 o
-2 1 12 47.95 40.86 1.60 o
-1 1 12 3.24 4.89 1.30 o
0 1 12 61.58 57.69 1.78 o
1 1 12 31.39 36.62 2.17 o
2 1 12 281.20 261.47 3.83 o
3 1 12 228.80 235.83 3.82 o
4 1 12 309.86 297.71 4.68 o
-5 2 12 143.69 156.01 3.03 o
-4 2 12 7.13 7.41 1.56 o
-3 2 12 479.31 501.34 4.13 o
-2 2 12 406.88 416.59 4.86 o
-1 2 12 121.39 123.48 2.37 o
0 2 12 11.83 12.47 1.76 o
1 2 12 875.87 925.02 5.89 o
2 2 12 0.33 1.05 1.72 <
3 2 12 43.70 46.53 2.63 o
-5 3 12 22.13 20.45 1.94 o
-4 3 12 1.12 0.42 2.01 <
-3 3 12 379.42 386.28 4.93 o
-2 3 12 571.00 585.80 3.75 o
-1 3 12 0.57 1.12 1.27 <
0 3 12 31.49 32.87 1.42 o
1 3 12 1173.10 1243.96 5.97 o
2 3 12 21.09 20.23 1.85 o
-4 4 12 198.89 194.87 4.78 o
-3 4 12 56.15 51.80 2.23 o
-2 4 12 35.71 30.47 1.90 o
-1 4 12 3.70 3.76 1.29 <
0 4 12 400.57 440.52 4.77 o
1 4 12 71.12 73.95 2.66 o
0 -6 13 6.86 7.52 2.01 o
1 -6 13 370.46 352.26 6.31 o
-3 -5 13 0.34 3.62 2.15 <
-2 -5 13 42.80 45.32 2.62 o
-1 -5 13 10.08 8.41 1.62 o
0 -5 13 21.62 21.39 2.43 o
1 -5 13 52.07 50.37 2.82 o
2 -5 13 163.89 168.61 4.01 o
3 -5 13 179.51 176.41 3.54 o
-4 -4 13 281.22 287.50 5.81 o
-3 -4 13 3.81 2.66 2.30 <
-2 -4 13 0.56 -0.14 2.31 <
-1 -4 13 15.46 12.00 1.87 o
0 -4 13 130.04 124.92 3.13 o
1 -4 13 1.69 -0.18 1.76 <
2 -4 13 276.14 287.45 3.05 o
3 -4 13 145.10 135.39 3.16 o
-4 -3 13 481.52 507.34 6.10 o
-3 -3 13 273.18 268.68 3.10 o
-2 -3 13 241.14 220.16 4.62 o
-1 -3 13 0.23 0.34 1.36 <
0 -3 13 19.94 23.82 1.65 o
1 -3 13 2062.56 2151.30 8.55 o
2 -3 13 321.20 314.07 3.49 o
3 -3 13 6.91 8.00 1.53 o
4 -3 13 60.74 65.59 2.43 o
-5 -2 13 32.05 33.86 1.82 o
-4 -2 13 228.64 227.02 3.72 o
-3 -2 13 12.88 8.94 1.25 o
-2 -2 13 1.95 2.59 1.18 <
-1 -2 13 34.07 30.81 1.89 o
0 -2 13 25.19 28.21 1.64 o
1 -2 13 131.03 127.21 2.61 o
2 -2 13 16.12 12.75 1.63 o
3 -2 13 128.99 135.92 2.69 o
4 -2 13 25.08 25.75 2.08 o
-5 -1 13 725.06 713.51 7.02 o
-4 -1 13 107.40 102.86 2.09 o
-3 -1 13 36.18 35.54 1.55 o
-2 -1 13 1358.26 1389.93 7.11 o
-1 -1 13 760.42 735.68 7.54 o
0 -1 13 194.23 174.97 2.68 o
1 -1 13 632.08 637.57 4.51 o
2 -1 13 75.65 73.52 2.62 o
3 -1 13 16.98 17.91 2.02 o
4 -1 13 112.86 102.69 2.55 o
-5 0 13 375.24 380.58 4.48 o
-4 0 13 90.92 103.97 2.91 o
-3 0 13 6.65 5.46 1.45 o
-2 0 13 546.70 538.55 4.54 o
-1 0 13 1069.67 1060.71 7.04 o
0 0 13 586.68 562.18 5.35 o
1 0 13 418.98 417.28 4.72 o
2 0 13 285.33 277.21 3.45 o
3 0 13 74.96 71.12 2.48 o
4 0 13 8.35 7.85 1.75 o
-5 1 13 7.11 11.22 1.64 o
-4 1 13 9.98 7.13 1.48 o
-3 1 13 477.27 506.28 5.17 o
-2 1 13 55.31 53.84 1.70 o
-1 1 13 56.32 64.24 2.17 o
0 1 13 6.63 6.04 1.59 o
1 1 13 276.92 270.94 3.75 o
2 1 13 128.78 134.12 2.94 o
3 1 13 161.81 162.98 2.77 o
-5 2 13 13.42 11.36 1.48 o
-4 2 13 59.99 56.87 1.98 o
-3 2 13 67.15 68.57 2.19 o
-2 2 13 186.97 173.84 4.13 o
-1 2 13 106.06 123.12 2.64 o
0 2 13 1.10 0.35 1.72 <
1 2 13 32.01 28.76 1.96 o
2 2 13 59.01 58.10 2.48 o
3 2 13 356.75 363.15 5.24 o
-4 3 13 0.28 0.24 1.90 <
-3 3 13 780.88 802.55 8.02 o
-2 3 13 217.36 218.44 3.14 o
-1 3 13 19.32 15.19 1.73 o
0 3 13 126.20 136.61 2.59 o
1 3 13 5.36 9.40 1.85 o
2 3 13 358.39 378.54 5.50 o
-4 4 13 58.41 52.37 2.63 o
-3 4 13 194.56 188.02 3.68 o
-2 4 13 111.38 115.34 3.05 o
-1 4 13 278.22 280.82 3.58 o
0 4 13 20.28 20.55 1.50 o
-3 -5 14 70.25 69.50 3.17 o
-2 -5 14 22.28 22.35 2.25 o
-1 -5 14 1.99 1.78 1.66 <
0 -5 14 33.73 37.85 2.11 o
1 -5 14 59.70 53.30 2.77 o
2 -5 14 109.87 104.97 2.60 o
-4 -4 14 246.43 259.07 5.32 o
-3 -4 14 19.30 16.92 2.30 o
-2 -4 14 97.57 96.79 3.55 o
-1 -4 14 63.01 63.73 2.50 o
0 -4 14 23.56 16.44 1.62 o
1 -4 14 54.23 57.68 3.18 o
2 -4 14 5.92 6.50 1.79 o
3 -4 14 2.47 -2.94 1.93 <
-4 -3 14 107.42 106.59 3.10 o
-3 -3 14 99.10 100.54 3.59 o
-2 -3 14 80.57 81.85 2.89 o
-1 -3 14 101.80 100.70 2.30 o
0 -3 14 117.80 126.45 2.35 o
1 -3 14 22.69 25.01 1.90 o
2 -3 14 45.26 44.35 1.81 o
3 -3 14 146.83 152.22 3.03 o
4 -3 14 40.16 40.56 2.24 o
-5 -2 14 143.18 154.74 2.69 o
-4 -2 14 74.26 75.27 2.02 o
-3 -2 14 834.28 845.17 4.67 o
-2 -2 14 718.64 759.55 5.61 o
-1 -2 14 949.14 982.37 5.76 o
0 -2 14 457.69 462.78 4.60 o
1 -2 14 535.61 560.08 4.00 o
2 -2 14 41.78 42.33 1.92 o
3 -2 14 101.59 102.74 2.67 o
4 -2 14 972.22 1047.74 7.95 o
-5 -1 14 27.25 28.03 1.93 o
-4 -1 14 4.81 5.04 1.36 o
-3 -1 14 241.70 260.60 3.46 o
-2 -1 14 624.14 641.68 5.98 o
-1 -1 14 317.34 320.56 5.41 o
0 -1 14 88.65 86.52 2.22 o
1 -1 14 1246.65 1285.16 7.25 o
2 -1 14 7.32 6.65 1.80 o
3 -1 14 76.00 81.59 3.20 o
4 -1 14 690.13 754.91 6.71 o
-5 0 14 138.40 152.64 2.93 o
-4 0 14 15.76 16.06 1.78 o
-3 0 14 352.22 350.42 3.95 o
-2 0 14 328.92 346.84 5.20 o
-1 0 14 68.71 75.85 2.50 o
0 0 14 495.97 483.20 6.33 o
1 0 14 718.76 722.41 7.23 o
2 0 14 282.43 286.71 3.10 o
3 0 14 261.94 282.12 3.42 o
-5 1 14 117.88 128.24 2.66 o
-4 1 14 71.20 62.94 2.05 o
-3 1 14 661.71 680.77 5.86 o
-2 1 14 732.66 749.71 5.48 o
-1 1 14 14.74 13.53 1.60 o
0 1 14 90.44 90.38 2.43 o
1 1 14 665.00 702.04 6.16 o
2 1 14 49.70 51.08 1.95 o
3 1 14 3.87 2.29 1.60 <
-4 2 14 298.46 299.05 4.92 o
-3 2 14 71.78 66.06 3.10 o
-2 2 14 201.34 220.56 3.75 o
-1 2 14 56.36 53.56 2.15 o
0 2 14 326.84 325.59 3.62 o
1 2 14 107.08 119.88 2.78 o
2 2 14 301.63 297.76 4.12 o
-4 3 14 87.09 90.80 2.78 o
-3 3 14 168.09 172.82 3.95 o
-2 3 14 23.41 17.18 1.76 o
-1 3 14 1.76 2.76 1.59 <
0 3 14 132.19 134.69 3.22 o
1 3 14 13.75 13.50 1.82 o
-3 4 14 144.12 136.31 3.63 o
-2 4 14 477.48 515.54 5.53 o
-1 4 14 9.89 14.30 2.14 o
0 4 14 0.73 3.98 3.43 <
-2 -5 15 240.91 257.42 4.14 o
-1 -5 15 11.58 8.04 1.70 o
0 -5 15 10.34 4.67 2.17 <
1 -5 15 376.53 403.33 5.72 o
2 -5 15 12.01 13.45 2.66 o
-3 -4 15 39.07 35.37 2.47 o
-2 -4 15 75.14 76.11 3.24 o
-1 -4 15 29.44 26.42 2.01 o
0 -4 15 54.30 50.63 2.07 o
1 -4 15 122.51 112.45 3.72 o
2 -4 15 66.51 69.18 2.40 o
-4 -3 15 332.39 340.58 6.29 o
-3 -3 15 510.27 551.52 6.61 o
-2 -3 15 59.53 64.45 2.60 o
-1 -3 15 34.59 34.84 1.74 o
0 -3 15 89.42 86.10 2.22 o
1 -3 15 416.49 436.49 4.06 o
2 -3 15 281.70 277.98 3.78 o
3 -3 15 337.09 360.39 4.12 o
-4 -2 15 0.17 -0.71 1.50 <
-3 -2 15 283.02 281.76 4.02 o
-2 -2 15 143.80 145.50 2.82 o
-1 -2 15 4.24 5.79 1.67 o
0 -2 15 0.37 -0.18 1.62 <
1 -2 15 72.31 62.85 2.40 o
2 -2 15 46.94 45.85 2.17 o
3 -2 15 501.32 514.15 6.20 o
-5 -1 15 296.39 312.05 4.43 o
-4 -1 15 69.44 67.70 1.89 o
-3 -1 15 1090.68 1141.86 9.69 o
-2 -1 15 13.34 12.79 2.58 o
-1 -1 15 376.88 374.46 6.09 o
0 -1 15 1.16 -1.80 1.56 <
1 -1 15 374.00 358.35 4.64 o
2 -1 15 5.47 9.24 1.78 o
3 -1 15 200.21 222.07 4.24 o
-5 0 15 302.95 319.49 4.64 o
-4 0 15 182.64 194.47 3.39 o
-3 0 15 517.33 509.04 4.60 o
-2 0 15 3.39 2.22 1.92 <
-1 0 15 1311.91 1363.16 10.78 o
0 0 15 70.20 73.56 2.57 o
1 0 15 513.62 494.92 4.62 o
2 0 15 84.13 86.26 2.14 o
3 0 15 490.62 472.28 5.45 o
-5 1 15 28.18 36.42 2.18 o
-4 1 15 11.85 14.38 1.43 o
-3 1 15 179.57 171.60 3.97 o
-2 1 15 958.15 962.93 8.99 o
-1 1 15 10.22 9.63 1.92 o
0 1 15 407.88 416.61 6.32 o
1 1 15 30.97 38.19 2.11 o
2 1 15 505.54 510.61 3.88 o
3 1 15 94.87 115.88 4.43 o
-4 2 15 38.11 36.69 2.24 o
-3 2 15 65.17 50.64 2.73 o
-2 2 15 280.52 284.01 4.00 o
-1 2 15 79.55 71.12 2.65 o
0 2 15 228.65 221.74 3.88 o
1 2 15 42.36 32.00 2.15 o
2 2 15 402.69 412.49 4.44 o
-4 3 15 5.04 8.84 2.00 o
-3 3 15 48.28 47.63 2.42 o
-2 3 15 182.70 162.30 3.26 o
-1 3 15 71.52 81.39 2.39 o
0 3 15 39.49 32.63 2.36 o
1 3 15 381.68 405.70 5.12 o
-1 -5 16 15.19 14.99 2.45 o
0 -5 16 12.44 12.79 1.91 o
1 -5 16 355.31 361.53 4.77 o
-3 -4 16 130.28 135.16 4.38 o
-2 -4 16 41.99 45.11 2.63 o
-1 -4 16 0.92 4.17 1.49 <
0 -4 16 84.33 83.45 3.12 o
1 -4 16 24.55 26.41 1.99 o
2 -4 16 668.84 688.54 6.63 o
-4 -3 16 16.88 21.59 2.73 o
-3 -3 16 222.03 235.97 4.30 o
-2 -3 16 328.90 346.38 4.53 o
-1 -3 16 2.26 3.24 1.41 <
0 -3 16 10.27 9.82 1.55 o
1 -3 16 215.96 223.69 3.15 o
2 -3 16 294.98 283.19 3.68 o
3 -3 16 3.60 1.17 2.25 <
-4 -2 16 267.38 268.91 5.50 o
-3 -2 16 39.54 36.51 2.65 o
-2 -2 16 7.46 11.37 1.63 o
-1 -2 16 1440.05 1486.48 9.25 o
0 -2 16 1203.23 1224.04 9.58 o
1 -2 16 108.13 103.67 2.31 o
2 -2 16 547.32 564.70 6.46 o
3 -2 16 232.76 261.89 4.18 o
-4 -1 16 85.07 85.10 2.28 o
-3 -1 16 39.97 34.07 2.61 o
-2 -1 16 25.69 23.97 2.76 o
-1 -1 16 924.03 904.97 8.98 o
0 -1 16 860.49 852.61 6.01 o
1 -1 16 43.28 50.39 1.91 o
2 -1 16 527.31 547.36 5.37 o
3 -1 16 79.26 87.89 2.68 o
-5 0 16 18.41 14.24 2.06 o
-4 0 16 81.37 105.54 2.69 o
-3 0 16 7.77 6.02 1.78 o
-2 0 16 463.44 463.77 6.48 o
-1 0 16 5.25 5.09 2.26 <
0 0 16 17.60 15.67 1.93 o
1 0 16 77.72 68.28 2.14 o
2 0 16 15.43 8.45 1.97 o
3 0 16 153.05 165.08 3.24 o
-4 1 16 100.35 97.10 2.94 o
-3 1 16 415.21 393.84 4.56 o
-2 1 16 11.31 7.48 2.13 o
-1 1 16 1.02 0.93 1.85 <
0 1 16 75.48 65.24 3.10 o
1 1 16 16.27 16.68 1.58 o
2 1 16 35.23 28.22 1.92 o
-4 2 16 157.27 136.02 3.10 o
-3 2 16 67.18 67.54 2.66 o
-2 2 16 193.02 183.60 3.77 o
-1 2 16 13.61 8.03 2.05 o
0 2 16 30.15 30.57 2.08 o
1 2 16 0.68 6.38 1.80 o
-3 3 16 42.71 42.63 2.53 o
-2 3 16 130.59 125.42 2.86 o
-1 3 16 24.02 22.73 1.67 o
0 3 16 16.62 19.51 2.02 o
-2 -4 17 64.25 67.42 3.37 o
-1 -4 17 228.22 224.47 4.01 o
0 -4 17 11.05 13.31 2.06 o
1 -4 17 131.58 148.30 3.45 o
-3 -3 17 8.58 12.38 2.54 o
-2 -3 17 733.61 736.83 7.17 o
-1 -3 17 0.40 -2.53 1.47 <
0 -3 17 382.11 396.43 4.58 o
1 -3 17 28.05 26.29 1.99 o
2 -3 17 364.45 339.92 4.29 o
-4 -2 17 0.08 0.83 2.80 <
-3 -2 17 1.55 -1.67 2.00 <
-2 -2 17 376.25 360.40 5.55 o
-1 -2 17 91.54 86.68 2.73 o
0 -2 17 298.36 292.65 3.67 o
1 -2 17 15.59 10.30 1.99 o
2 -2 17 337.30 317.18 4.59 o
-4 -1 17 12.71 9.47 2.37 o
-3 -1 17 3.79 6.25 1.94 o
-2 -1 17 887.02 914.36 8.75 o
-1 -1 17 20.40 19.21 2.44 o
0 -1 17 170.54 176.46 3.53 o
1 -1 17 12.95 9.85 1.51 o
2 -1 17 132.51 130.21 3.22 o
-4 0 17 88.73 88.13 2.93 o
-3 0 17 58.60 60.15 2.81 o
-2 0 17 613.33 586.95 7.04 o
-1 0 17 106.60 105.11 3.62 o
0 0 17 455.81 452.88 4.36 o
1 0 17 22.09 20.85 1.51 o
2 0 17 420.75 443.29 5.30 o
-4 1 17 77.44 72.22 2.55 o
-3 1 17 56.83 46.52 1.89 o
-2 1 17 7.97 4.42 2.01 <
-1 1 17 57.30 53.20 2.12 o
0 1 17 1.36 -0.53 1.58 <
1 1 17 669.21 675.17 4.75 o
-3 2 17 76.61 76.17 3.34 o
-2 2 17 5.79 -0.71 1.81 <
-1 2 17 0.89 -0.15 2.10 <
0 2 17 1.88 3.22 1.95 <
1 2 17 363.11 355.46 6.11 o
-1 -4 18 404.03 361.60 5.74 o
0 -4 18 56.22 65.01 3.18 o
1 -4 18 363.44 332.15 5.77 o
-3 -3 18 86.12 90.66 3.68 o
-2 -3 18 8.57 10.29 2.08 o
-1 -3 18 250.58 228.00 3.86 o
0 -3 18 88.09 81.29 1.86 o
1 -3 18 14.02 11.77 1.70 o
-3 -2 18 58.14 65.92 2.48 o
-2 -2 18 552.13 546.98 6.33 o
-1 -2 18 76.34 78.02 3.13 o
0 -2 18 31.67 33.04 1.90 o
1 -2 18 24.11 19.53 1.96 o
2 -2 18 11.96 11.13 1.71 o
-3 -1 18 1.29 2.26 1.88 <
-2 -1 18 438.13 438.21 5.91 o
-1 -1 18 171.17 172.75 4.18 o
0 -1 18 84.71 82.98 2.60 o
1 -1 18 185.82 173.98 2.53 o
2 -1 18 92.90 98.80 3.50 o
-3 0 18 15.16 17.18 1.92 o
-2 0 18 23.83 31.62 2.38 o
-1 0 18 238.06 217.62 4.32 o
0 0 18 262.46 250.59 3.67 o
1 0 18 50.01 61.38 1.73 o
-3 1 18 74.00 84.45 2.62 o
-2 1 18 7.17 2.31 2.04 <
-1 1 18 193.54 200.78 3.85 o
0 1 18 103.28 102.14 2.06 o
1 1 18 23.36 19.32 3.06 o
-2 2 18 4.72 4.94 2.05 <
-1 2 18 8.64 6.23 1.70 o
-2 -3 19 56.06 54.44 3.00 o
-1 -3 19 186.53 171.23 3.13 o
0 -3 19 22.13 21.28 1.68 o
-3 -2 19 25.49 27.24 2.65 o
-2 -2 19 13.83 9.31 2.04 o
-1 -2 19 9.09 7.78 1.48 o
0 -2 19 6.56 4.25 1.40 o
1 -2 19 286.20 273.21 3.91 o
-3 -1 19 0.63 -1.95 2.69 <
-2 -1 19 21.52 22.33 2.11 o
-1 -1 19 23.69 21.34 1.81 o
0 -1 19 16.28 19.50 1.55 o
1 -1 19 176.50 178.28 4.34 o
-2 0 19 0.38 -0.10 2.02 <
-1 0 19 22.55 25.09 1.86 o
0 0 19 3.20 2.09 1.62 <
-2 1 19 132.74 131.62 3.89 o
-1 1 19 24.55 21.52 2.59 o
0 1 19 56.90 60.61 3.07 o
-1 -2 20 193.76 180.28 4.55 o
-2 -1 20 125.39 139.52 4.01 o
-1 -1 20 289.59 306.43 5.77 o
0 -1 20 207.00 214.25 4.59 o
-1 0 20 70.59 74.66 3.24 o

# Attachment '6002_web_deposit_cif_file_2_KarlaFejfarova_1309265877.dat_hcl_precislovany.cif'

#=============================================================================

data_dat_hcl
_database_code_depnum_ccdc_archive 'CCDC 831898'
#TrackingRef '6002_web_deposit_cif_file_2_KarlaFejfarova_1309265877.dat_hcl_precislovany.cif'

_symmetry_space_group_name_hall  '-P 2yn'
#Added by publCIF

_audit_update_record             
;
2010-04-28 # Formatted by publCIF
;

_audit_creation_method           SHELXL-97
_chemical_name_systematic        
;
?
;
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         '2(C2 H6 N5), H2 O, 2 (Cl)'
_chemical_formula_sum            'C4 H14 Cl2 N10 O'
_chemical_formula_weight         289.15

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_H-M   P2(1)/n

loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'

_cell_length_a                   6.07010(10)
_cell_length_b                   24.6727(6)
_cell_length_c                   8.1489(2)
_cell_angle_alpha                90.00
_cell_angle_beta                 93.766(2)
_cell_angle_gamma                90.00
_cell_volume                     1217.79(5)
_cell_formula_units_Z            4
_cell_measurement_temperature    120(2)
_cell_measurement_reflns_used    4734
_cell_measurement_theta_min      3.5799
_cell_measurement_theta_max      62.2718

_exptl_crystal_description       plate
_exptl_crystal_colour            colourless
_exptl_crystal_size_max          0.4934
_exptl_crystal_size_mid          0.2033
_exptl_crystal_size_min          0.1466
_exptl_crystal_density_meas      ?
_exptl_crystal_density_diffrn    1.577
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             600
_exptl_absorpt_coefficient_mu    4.888
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_correction_T_min  0.40266
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_process_details   
;
CrysAlisPro, Oxford Diffraction Ltd.,
Version 1.171.33.55
;
_exptl_special_details           
;
?
;

_diffrn_ambient_temperature      120(2)
_diffrn_radiation_wavelength     1.54178
_diffrn_radiation_type           CuK\a
_diffrn_radiation_source         'Enhance Ultra (Cu) X-ray Source'
_diffrn_radiation_monochromator  mirror
_diffrn_measurement_device_type  'Xcalibur, Atlas, Gemini ultra'
_diffrn_measurement_method       
;
Rotation method data acquisition using \w scans
;
_diffrn_detector_area_resol_mean 10.3784
_diffrn_standards_number         ?
_diffrn_standards_interval_count ?
_diffrn_standards_interval_time  ?
_diffrn_standards_decay_%        ?
_diffrn_reflns_number            5297
_diffrn_reflns_av_R_equivalents  0.0189
_diffrn_reflns_av_sigmaI/netI    0.0141
_diffrn_reflns_limit_h_min       -6
_diffrn_reflns_limit_h_max       6
_diffrn_reflns_limit_k_min       -28
_diffrn_reflns_limit_k_max       26
_diffrn_reflns_limit_l_min       -9
_diffrn_reflns_limit_l_max       8
_diffrn_reflns_theta_min         3.58
_diffrn_reflns_theta_max         62.36
_reflns_number_total             1907
_reflns_number_gt                1850
_reflns_threshold_expression     >2sigma(I)

_computing_data_collection       'Crysalis CCD (Oxford Diffraction, 2007)'
_computing_cell_refinement       'Crysalis RED (Oxford Diffraction, 2007)'
_computing_data_reduction        'Crysalis RED (Oxford Diffraction, 2007)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_molecular_graphics    ?
_computing_publication_material  'publCIF (MacMahon, 2008)'

_refine_special_details          
;
Refinement of F^2^ against ALL reflections. The weighted R-factor wR and
goodness of fit S are based on F^2^, conventional R-factors R are based
on F, with F set to zero for negative F^2^. The threshold expression of
F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is
not relevant to the choice of reflections for refinement. R-factors based
on F^2^ are statistically about twice as large as those based on F, and R-
factors based on ALL data will be even larger.
Hydrogen atoms were located from the maps of electron density and left
unrestrained.
;

_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'calc w=1/[\s^2^(Fo^2^)+(0.0503P)^2^+0.6633P] where P=(Fo^2^+2Fc^2^)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       ?
_refine_ls_number_reflns         1907
_refine_ls_number_parameters     154
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0298
_refine_ls_R_factor_gt           0.0290
_refine_ls_wR_factor_ref         0.0771
_refine_ls_wR_factor_gt          0.0764
_refine_ls_goodness_of_fit_ref   1.038
_refine_ls_restrained_S_all      1.038
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
O1W O 0.80397(18) 0.37926(4) 0.84901(14) 0.0171(3) Uani 1 1 d . . .
H1W H 0.7733 0.3680 0.7663 0.019 Uiso 1 1 d . . .
H2W H 0.6817 0.3876 0.8766 0.034 Uiso 1 1 d . . .
Cl1 Cl 0.23710(6) 0.662406(15) 0.51395(5) 0.01539(15) Uani 1 1 d . . .
Cl2 Cl 0.15283(6) 0.902642(15) 0.50311(5) 0.01811(15) Uani 1 1 d . . .
C10 C 0.6642(3) 0.73486(6) 0.30720(19) 0.0134(4) Uani 1 1 d . . .
C12 C 0.3837(3) 0.79050(6) 0.28188(19) 0.0134(3) Uani 1 1 d . . .
N11 N 0.4687(2) 0.74511(5) 0.21884(16) 0.0125(3) Uani 1 1 d . . .
H11A H 0.4206 0.7309 0.1393 0.013 Uiso 1 1 d . . .
N9 N 0.7029(2) 0.77098(6) 0.42381(17) 0.0147(3) Uani 1 1 d . . .
H8A H 0.5132 0.8317 0.4638 0.014 Uiso 1 1 d . . .
N8 N 0.5220(2) 0.80602(5) 0.40393(16) 0.0147(3) Uani 1 1 d . . .
N14 N 0.7963(2) 0.69324(6) 0.27497(18) 0.0229(4) Uani 1 1 d . . .
H14A H 0.7502 0.6684 0.2077 0.025 Uiso 1 1 d . . .
H14B H 0.9042 0.6874 0.3409 0.023 Uiso 1 1 d . . .
N13 N 0.1989(2) 0.81509(6) 0.22553(18) 0.0202(3) Uani 1 1 d . . .
H13A H 0.1085 0.7966 0.1616 0.031 Uiso 1 1 d . . .
H13B H 0.1525 0.8389 0.2844 0.025 Uiso 1 1 d . . .
C3 C 0.7846(3) 0.54442(6) 0.5864(2) 0.0141(4) Uani 1 1 d . . .
C5 C 1.0684(3) 0.52223(6) 0.75227(19) 0.0145(4) Uani 1 1 d . . .
N4 N 0.9851(2) 0.56281(5) 0.65596(16) 0.0150(3) Uani 1 1 d . . .
H4A H 1.0575 0.5915 0.6226 0.027 Uiso 1 1 d . . .
N1 N 0.9224(2) 0.48247(5) 0.74134(17) 0.0161(3) Uani 1 1 d . . .
H1A H 0.9278 0.4542 0.7899 0.028 Uiso 1 1 d . . .
N2 N 0.7390(2) 0.49596(6) 0.63671(17) 0.0162(3) Uani 1 1 d . . .
N6 N 1.2579(2) 0.52232(6) 0.84162(19) 0.0225(4) Uani 1 1 d . . .
H6A H 1.3485 0.5496 0.8453 0.034 Uiso 1 1 d . . .
H6B H 1.3006 0.4928 0.8823 0.029 Uiso 1 1 d . . .
N7 N 0.6627(2) 0.57376(6) 0.47266(18) 0.0202(3) Uani 1 1 d . . .
H7B H 0.5396 0.5578 0.4471 0.029 Uiso 1 1 d . . .
H7A H 0.6572 0.6077 0.4885 0.029 Uiso 1 1 d . . .

loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_23
_atom_site_aniso_U_13
_atom_site_aniso_U_12
O1W 0.0180(6) 0.0158(6) 0.0169(6) -0.0002(5) -0.0029(5) 0.0004(5)
Cl1 0.0143(2) 0.0137(2) 0.0176(2) 0.00018(14) -0.00285(16) -0.00019(14)
Cl2 0.0182(3) 0.0158(2) 0.0199(2) 0.00037(15) -0.00227(17) 0.00356(15)
C10 0.0143(8) 0.0120(8) 0.0135(8) 0.0016(7) -0.0033(6) -0.0013(6)
C12 0.0146(8) 0.0128(8) 0.0125(8) 0.0021(6) -0.0010(6) 0.0005(7)
N11 0.0141(7) 0.0110(7) 0.0116(6) -0.0010(5) -0.0056(5) -0.0010(5)
N9 0.0153(7) 0.0123(7) 0.0158(7) 0.0001(6) -0.0048(6) 0.0045(5)
N8 0.0165(7) 0.0120(7) 0.0150(7) -0.0037(6) -0.0037(5) 0.0035(5)
N14 0.0229(8) 0.0202(8) 0.0238(8) -0.0099(6) -0.0132(6) 0.0097(6)
N13 0.0167(8) 0.0224(8) 0.0204(8) -0.0059(6) -0.0068(6) 0.0061(6)
C3 0.0141(8) 0.0121(8) 0.0159(8) -0.0038(6) -0.0003(6) 0.0008(6)
C5 0.0161(9) 0.0115(8) 0.0159(8) -0.0020(6) 0.0015(7) 0.0013(7)
N4 0.0159(7) 0.0110(7) 0.0180(7) 0.0002(5) 0.0001(6) -0.0015(5)
N1 0.0163(7) 0.0103(7) 0.0211(7) 0.0034(6) -0.0044(6) -0.0011(6)
N2 0.0136(7) 0.0132(7) 0.0211(7) 0.0010(6) -0.0040(6) -0.0007(6)
N6 0.0204(8) 0.0145(7) 0.0310(8) 0.0039(6) -0.0110(6) -0.0023(6)
N7 0.0201(8) 0.0125(7) 0.0269(8) 0.0013(6) -0.0066(6) 0.0003(6)

_geom_special_details            
;
All esds (except the esd in the dihedral angle between two l.s. planes)
are estimated using the full covariance matrix. The cell esds are taken
into account individually in the estimation of esds in distances, angles
and torsion angles; correlations between esds in cell parameters are only
used when they are defined by crystal symmetry. An approximate (isotropic)
treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
O1W H1W 0.7414 . ?
O1W H2W 0.8159 . ?
C10 N9 1.313(2) . ?
C10 N14 1.339(2) . ?
C10 N11 1.371(2) . ?
C12 N8 1.315(2) . ?
C12 N13 1.330(2) . ?
C12 N11 1.348(2) . ?
N11 H11A 0.7770 . ?
N9 N8 1.3986(19) . ?
N8 H8A 0.8036 . ?
N14 H14A 0.8577 . ?
N14 H14B 0.8320 . ?
N13 H13A 0.8621 . ?
N13 H13B 0.8192 . ?
C3 N2 1.300(2) . ?
C3 N7 1.356(2) . ?
C3 N4 1.385(2) . ?
C5 N6 1.320(2) . ?
C5 N1 1.321(2) . ?
C5 N4 1.350(2) . ?
N4 H4A 0.8863 . ?
N1 N2 1.3972(19) . ?
N1 H1A 0.8021 . ?
N6 H6A 0.8680 . ?
N6 H6B 0.8352 . ?
N7 H7B 0.8574 . ?
N7 H7A 0.8476 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
H1W O1W H2W 99.6 . . ?
N9 C10 N14 125.56(14) . . ?
N9 C10 N11 111.25(14) . . ?
N14 C10 N11 123.19(14) . . ?
N8 C12 N13 127.58(15) . . ?
N8 C12 N11 106.80(13) . . ?
N13 C12 N11 125.58(15) . . ?
C12 N11 C10 107.01(13) . . ?
C12 N11 H11A 124.1 . . ?
C10 N11 H11A 128.3 . . ?
C10 N9 N8 103.54(13) . . ?
C12 N8 N9 111.39(13) . . ?
C12 N8 H8A 128.6 . . ?
N9 N8 H8A 120.0 . . ?
C10 N14 H14A 120.0 . . ?
C10 N14 H14B 117.6 . . ?
H14A N14 H14B 119.9 . . ?
C12 N13 H13A 117.1 . . ?
C12 N13 H13B 116.0 . . ?
H13A N13 H13B 120.2 . . ?
N2 C3 N7 126.06(15) . . ?
N2 C3 N4 111.82(14) . . ?
N7 C3 N4 122.02(15) . . ?
N6 C5 N1 126.49(15) . . ?
N6 C5 N4 126.81(15) . . ?
N1 C5 N4 106.70(14) . . ?
C5 N4 C3 106.31(13) . . ?
C5 N4 H4A 126.6 . . ?
C3 N4 H4A 125.3 . . ?
C5 N1 N2 111.61(13) . . ?
C5 N1 H1A 127.4 . . ?
N2 N1 H1A 120.9 . . ?
C3 N2 N1 103.55(13) . . ?
C5 N6 H6A 123.2 . . ?
C5 N6 H6B 117.0 . . ?
H6A N6 H6B 118.8 . . ?
C3 N7 H7B 110.4 . . ?
C3 N7 H7A 116.6 . . ?
H7B N7 H7A 116.6 . . ?

_diffrn_measured_fraction_theta_max 0.987
_diffrn_reflns_theta_full        62.36
_diffrn_measured_fraction_theta_full 0.987
_refine_diff_density_max         0.233
_refine_diff_density_min         -0.316
_refine_diff_density_rms         0.074

# Attachment '6003_web_deposit_cif_file_3_KarlaFejfarova_1309265877.dat_hclo4_precislovany.cif'

data_dat_hclo4
_database_code_depnum_ccdc_archive 'CCDC 831899'
#TrackingRef '6003_web_deposit_cif_file_3_KarlaFejfarova_1309265877.dat_hclo4_precislovany.cif'

_audit_creation_method           SHELXL-97
_chemical_name_systematic        
;
?
;
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C4 H12 Cl2 N10 O8'
_chemical_formula_weight         399.14

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_symmetry_cell_setting           ?
_symmetry_space_group_name_H-M   ?

loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   5.3075(2)
_cell_length_b                   7.5977(4)
_cell_length_c                   9.1610(5)
_cell_angle_alpha                74.424(5)
_cell_angle_beta                 84.547(4)
_cell_angle_gamma                83.648(4)
_cell_volume                     352.84(3)
_cell_formula_units_Z            2
_cell_measurement_temperature    150(2)
_cell_measurement_reflns_used    ?
_cell_measurement_theta_min      ?
_cell_measurement_theta_max      ?

_exptl_crystal_description       ?
_exptl_crystal_colour            ?
_exptl_crystal_size_max          ?
_exptl_crystal_size_mid          ?
_exptl_crystal_size_min          ?
_exptl_crystal_density_meas      ?
_exptl_crystal_density_diffrn    1.878
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             204
_exptl_absorpt_coefficient_mu    4.821
_exptl_absorpt_correction_type   ?
_exptl_absorpt_correction_T_min  ?
_exptl_absorpt_correction_T_max  ?
_exptl_absorpt_process_details   ?

_exptl_special_details           
;
?
;

_diffrn_ambient_temperature      150(2)
_diffrn_radiation_wavelength     1.54178
_diffrn_radiation_type           CuK\a
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_monochromator  graphite
_diffrn_measurement_device_type  ?
_diffrn_measurement_method       ?
_diffrn_detector_area_resol_mean ?
_diffrn_standards_number         ?
_diffrn_standards_interval_count ?
_diffrn_standards_interval_time  ?
_diffrn_standards_decay_%        ?
_diffrn_reflns_number            3565
_diffrn_reflns_av_R_equivalents  0.0186
_diffrn_reflns_av_sigmaI/netI    0.0124
_diffrn_reflns_limit_h_min       -6
_diffrn_reflns_limit_h_max       6
_diffrn_reflns_limit_k_min       -8
_diffrn_reflns_limit_k_max       8
_diffrn_reflns_limit_l_min       -10
_diffrn_reflns_limit_l_max       10
_diffrn_reflns_theta_min         5.02
_diffrn_reflns_theta_max         62.32
_reflns_number_total             1098
_reflns_number_gt                1066
_reflns_threshold_expression     >2sigma(I)

_computing_data_collection       ?
_computing_cell_refinement       ?
_computing_data_reduction        ?
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_molecular_graphics    ?
_computing_publication_material  ?

_refine_special_details          
;
Refinement of F^2^ against ALL reflections. The weighted R-factor wR and
goodness of fit S are based on F^2^, conventional R-factors R are based
on F, with F set to zero for negative F^2^. The threshold expression of
F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is
not relevant to the choice of reflections for refinement. R-factors based
on F^2^ are statistically about twice as large as those based on F, and R-
factors based on ALL data will be even larger.
;

_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'calc w=1/[\s^2^(Fo^2^)+(0.0415P)^2^+0.3835P] where P=(Fo^2^+2Fc^2^)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    mixed
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       ?
_refine_ls_number_reflns         1098
_refine_ls_number_parameters     133
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0284
_refine_ls_R_factor_gt           0.0278
_refine_ls_wR_factor_ref         0.0745
_refine_ls_wR_factor_gt          0.0741
_refine_ls_goodness_of_fit_ref   1.064
_refine_ls_restrained_S_all      1.064
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
H4A H 0.050(5) 0.647(3) 0.705(3) 0.013(6) Uiso 1 1 d . . .
H7A H -0.240(5) 0.805(4) 0.500(3) 0.018(7) Uiso 1 1 d . . .
H7B H -0.399(5) 0.702(4) 0.456(3) 0.021(7) Uiso 1 1 d . . .
H6B H 0.164(5) 0.241(4) 0.962(3) 0.016(7) Uiso 1 1 d . . .
H1A H -0.198(5) 0.199(4) 0.811(3) 0.016(6) Uiso 1 1 d . . .
H6A H 0.256(5) 0.413(4) 0.925(3) 0.026(7) Uiso 1 1 d . . .
Cl1 Cl 0.37443(9) 0.86992(6) 0.80873(5) 0.01262(19) Uani 1 1 d . . .
O2 O 0.2325(3) 0.8889(2) 0.67761(17) 0.0211(4) Uani 1 1 d . . .
O1 O 0.4335(3) 0.67735(19) 0.87821(17) 0.0176(4) Uani 1 1 d . . .
O3 O 0.2215(3) 0.9519(2) 0.91557(17) 0.0239(4) Uani 1 1 d . . .
O4 O 0.6042(3) 0.9584(2) 0.76280(18) 0.0233(4) Uani 1 1 d . . .
N4 N -0.0292(3) 0.5647(2) 0.70799(19) 0.0124(4) Uani 1 1 d . . .
N1 N -0.1717(3) 0.3020(3) 0.77107(19) 0.0141(4) Uani 1 1 d . . .
N2 N -0.3075(3) 0.4037(2) 0.64795(19) 0.0149(4) Uani 1 1 d . . .
C5 C -0.0052(4) 0.3976(3) 0.8064(2) 0.0125(5) Uani 1 1 d . . .
C3 C -0.2145(4) 0.5631(3) 0.6137(2) 0.0125(4) Uani 1 1 d . . .
N7 N -0.2770(4) 0.7063(3) 0.4966(2) 0.0160(4) Uani 1 1 d . . .
N6 N 0.1516(4) 0.3444(3) 0.9171(2) 0.0172(4) Uani 1 1 d . . .

loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_23
_atom_site_aniso_U_13
_atom_site_aniso_U_12
Cl1 0.0162(3) 0.0097(3) 0.0127(3) -0.00408(19) 0.00205(19) -0.00409(19)
O2 0.0284(9) 0.0175(8) 0.0171(8) 0.0001(6) -0.0076(7) -0.0070(6)
O1 0.0214(8) 0.0101(7) 0.0208(8) -0.0030(6) -0.0024(6) -0.0014(6)
O3 0.0346(9) 0.0144(8) 0.0218(9) -0.0080(6) 0.0105(7) -0.0012(7)
O4 0.0235(8) 0.0214(8) 0.0273(9) -0.0079(7) 0.0041(7) -0.0134(7)
N4 0.0157(9) 0.0093(9) 0.0140(9) -0.0046(7) 0.0005(7) -0.0056(7)
N1 0.0207(10) 0.0090(9) 0.0120(9) 0.0002(7) -0.0013(7) -0.0057(7)
N2 0.0193(9) 0.0141(9) 0.0112(9) -0.0016(7) -0.0014(7) -0.0042(7)
C5 0.0148(11) 0.0123(10) 0.0112(10) -0.0054(8) 0.0037(8) -0.0023(8)
C3 0.0145(10) 0.0143(11) 0.0100(10) -0.0064(8) 0.0025(8) -0.0021(8)
N7 0.0211(11) 0.0106(10) 0.0169(10) -0.0023(8) -0.0045(8) -0.0041(8)
N6 0.0226(10) 0.0117(10) 0.0172(10) -0.0009(8) -0.0047(8) -0.0060(8)

_geom_special_details            
;
All esds (except the esd in the dihedral angle between two l.s. planes)
are estimated using the full covariance matrix. The cell esds are taken
into account individually in the estimation of esds in distances, angles
and torsion angles; correlations between esds in cell parameters are only
used when they are defined by crystal symmetry. An approximate (isotropic)
treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Cl1 O4 1.4309(16) . ?
Cl1 O3 1.4385(15) . ?
Cl1 O1 1.4424(15) . ?
Cl1 O2 1.4444(16) . ?
N4 C5 1.346(3) . ?
N4 C3 1.373(3) . ?
N1 C5 1.317(3) . ?
N1 N2 1.397(2) . ?
N2 C3 1.307(3) . ?
C5 N6 1.323(3) . ?
C3 N7 1.344(3) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O4 Cl1 O3 110.11(9) . . ?
O4 Cl1 O1 109.87(9) . . ?
O3 Cl1 O1 109.35(9) . . ?
O4 Cl1 O2 109.65(9) . . ?
O3 Cl1 O2 109.09(10) . . ?
O1 Cl1 O2 108.75(9) . . ?
C5 N4 C3 107.40(17) . . ?
C5 N1 N2 112.11(17) . . ?
C3 N2 N1 103.18(17) . . ?
N1 C5 N6 127.91(19) . . ?
N1 C5 N4 105.96(18) . . ?
N6 C5 N4 126.12(19) . . ?
N2 C3 N7 125.7(2) . . ?
N2 C3 N4 111.35(18) . . ?
N7 C3 N4 122.84(19) . . ?

_diffrn_measured_fraction_theta_max 0.979
_diffrn_reflns_theta_full        62.32
_diffrn_measured_fraction_theta_full 0.979
_refine_diff_density_max         0.305
_refine_diff_density_min         -0.380
_refine_diff_density_rms         0.055

# Attachment '6004_web_deposit_cif_file_4_KarlaFejfarova_1309265877.dat_hpo3_precislovany.cif'

#==============================================================================

data_dat_hpo3
_database_code_depnum_ccdc_archive 'CCDC 831900'
#TrackingRef '6004_web_deposit_cif_file_4_KarlaFejfarova_1309265877.dat_hpo3_precislovany.cif'

_cell_special_details            ?
#Added by publCIF

_symmetry_space_group_name_hall  '-P 2ybc'
#Added by publCIF

_audit_update_record             
;
2010-04-26 # Formatted by publCIF
;

_audit_creation_method           SHELXL-97
_chemical_name_systematic        
;
?
;
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         'C2 H6 N5, H2 O3 P '
_chemical_formula_sum            'C2 H8 N5 O3 P'
_chemical_formula_weight         181.10

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_H-M   P2(1)/c

loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'

_cell_length_a                   8.16880(10)
_cell_length_b                   11.4624(2)
_cell_length_c                   7.74230(10)
_cell_angle_alpha                90.00
_cell_angle_beta                 96.1060(10)
_cell_angle_gamma                90.00
_cell_volume                     720.830(18)
_cell_formula_units_Z            4
_cell_measurement_temperature    120(2)
_cell_measurement_reflns_used    7111
_cell_measurement_theta_min      3.8532
_cell_measurement_theta_max      62.4539

_exptl_crystal_description       plate
_exptl_crystal_colour            colourless
_exptl_crystal_size_max          0.3956
_exptl_crystal_size_mid          0.2358
_exptl_crystal_size_min          0.1328
_exptl_crystal_density_meas      ?
_exptl_crystal_density_diffrn    1.669
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             376
_exptl_absorpt_coefficient_mu    3.242

_exptl_absorpt_correction_T_min  0.08792
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
CrysAlisPro, Oxford Diffraction Ltd.,
Version 1.171.33.55
;

_exptl_special_details           
;
?
;

_diffrn_ambient_temperature      120(2)
_diffrn_radiation_wavelength     1.54184
_diffrn_radiation_type           CuK\a
_diffrn_radiation_source         'Enhance Ultra (Cu) X-ray Source'
_diffrn_radiation_monochromator  mirror
_diffrn_measurement_device_type  'Xcalibur, Atlas, Gemini ultra'
_diffrn_measurement_method       'Rotation method data acquisition using \w'
_diffrn_detector_area_resol_mean 10.3784
_diffrn_standards_number         ?
_diffrn_standards_interval_count ?
_diffrn_standards_interval_time  ?
_diffrn_standards_decay_%        ?
_diffrn_reflns_number            8465
_diffrn_reflns_av_R_equivalents  0.0339
_diffrn_reflns_av_sigmaI/netI    0.0145
_diffrn_reflns_limit_h_min       -9
_diffrn_reflns_limit_h_max       9
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_l_min       -8
_diffrn_reflns_limit_l_max       8
_diffrn_reflns_theta_min         5.45
_diffrn_reflns_theta_max         62.55
_reflns_number_total             1137
_reflns_number_gt                1106
_reflns_threshold_expression     >2sigma(I)

_computing_data_collection       'Crysalis CCD (Oxford Diffraction, 2007)'
_computing_cell_refinement       'Crysalis RED (Oxford Diffraction, 2007)'
_computing_data_reduction        'Crysalis RED (Oxford Diffraction, 2007)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_molecular_graphics    ?
_computing_publication_material  'publCIF (MacMahon, 2008)'

_refine_special_details          
;
Refinement of F^2^ against ALL reflections. The weighted R-factor wR and
goodness of fit S are based on F^2^, conventional R-factors R are based
on F, with F set to zero for negative F^2^. The threshold expression of
F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is
not relevant to the choice of reflections for refinement. R-factors based
on F^2^ are statistically about twice as large as those based on F, and R-
factors based on ALL data will be even larger. The hydrogen atoms could be
localized from the
difference Fourier map. Despite of that, all hydrogen atoms, except H1A, H1
and H2, were constrained
to ideal positions. The N---H distances were not restrained.
;

_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'calc w=1/[\s^2^(Fo^2^)+(0.0423P)^2^+1.0464P] where P=(Fo^2^+2Fc^2^)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     SHELXL
_refine_ls_extinction_coef       0.0078(6)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^
_refine_ls_number_reflns         1137
_refine_ls_number_parameters     101
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0286
_refine_ls_R_factor_gt           0.0281
_refine_ls_wR_factor_ref         0.0718
_refine_ls_wR_factor_gt          0.0714
_refine_ls_goodness_of_fit_ref   0.883
_refine_ls_restrained_S_all      0.883
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
H1A H 0.6143 0.4398 0.8607 0.050 Uiso 1 1 d . . .
H2 H 1.0267 0.3442 0.8127 0.050 Uiso 1 1 d . . .
H1 H 0.9447 0.3855 1.1682 0.050 Uiso 1 1 d . . .
H7A H 0.1509 0.5573 0.4657 0.050 Uiso 1 1 d . . .
H7B H 0.1569 0.4295 0.5061 0.050 Uiso 1 1 d . . .
C3 C 0.3370(2) 0.50518(15) 0.6202(2) 0.0142(4) Uani 1 1 d . . .
C5 C 0.5332(2) 0.59276(15) 0.7862(2) 0.0148(4) Uani 1 1 d . . .
N7 N 0.20705(19) 0.49184(13) 0.4983(2) 0.0194(4) Uani 1 1 d . . .
N4 N 0.40276(18) 0.61269(13) 0.66740(19) 0.0141(3) Uani 1 1 d . . .
H4A H 0.3676 0.6795 0.6288 0.022 Uiso 1 1 calc . . .
N6 N 0.6302(2) 0.67309(14) 0.8648(2) 0.0225(4) Uani 1 1 d . . .
H6B H 0.7101 0.6529 0.9403 0.033 Uiso 1 1 calc . . .
H6A H 0.6136 0.7456 0.8406 0.030 Uiso 1 1 calc . . .
N1 N 0.54253(18) 0.47840(13) 0.8089(2) 0.0162(3) Uani 1 1 d . . .
N2 N 0.41924(18) 0.42067(13) 0.70266(19) 0.0159(4) Uani 1 1 d . . .
O1 O 0.75288(15) 0.31457(10) 0.95478(17) 0.0185(3) Uani 1 1 d . . .
O2 O 1.04899(15) 0.37061(11) 0.91808(16) 0.0184(3) Uani 1 1 d . . .
O3 O 0.99092(15) 0.19540(11) 1.09951(16) 0.0174(3) Uani 1 1 d . . .
P1 P 0.92732(5) 0.31383(4) 1.03886(6) 0.01345(19) Uani 1 1 d . . .

loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_23
_atom_site_aniso_U_13
_atom_site_aniso_U_12
C3 0.0135(9) 0.0127(9) 0.0166(9) -0.0006(7) 0.0033(7) -0.0011(7)
C5 0.0130(9) 0.0124(9) 0.0191(9) 0.0008(7) 0.0019(7) 0.0009(7)
N7 0.0182(8) 0.0138(8) 0.0246(8) 0.0012(6) -0.0053(6) -0.0025(6)
N4 0.0134(7) 0.0089(7) 0.0196(8) 0.0019(6) -0.0004(6) 0.0010(6)
N6 0.0192(8) 0.0129(8) 0.0323(10) 0.0023(7) -0.0110(7) -0.0002(6)
N1 0.0134(8) 0.0120(8) 0.0219(8) 0.0012(6) -0.0038(6) 0.0011(6)
N2 0.0142(8) 0.0128(8) 0.0201(8) -0.0001(6) -0.0017(6) -0.0009(6)
O1 0.0151(7) 0.0120(6) 0.0269(7) 0.0002(5) -0.0042(5) 0.0007(5)
O2 0.0185(7) 0.0197(7) 0.0160(6) -0.0005(5) -0.0029(5) -0.0046(5)
O3 0.0186(7) 0.0147(7) 0.0180(7) 0.0003(5) -0.0023(5) 0.0030(5)
P1 0.0129(3) 0.0115(3) 0.0151(3) -0.00099(16) -0.00243(18) 0.00075(16)

_geom_special_details            
;
All esds (except the esd in the dihedral angle between two l.s. planes)
are estimated using the full covariance matrix. The cell esds are taken
into account individually in the estimation of esds in distances, angles
and torsion angles; correlations between esds in cell parameters are only
used when they are defined by crystal symmetry. An approximate (isotropic)
treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C3 N2 1.306(2) . ?
C3 N7 1.352(2) . ?
C3 N4 1.378(2) . ?
C5 N6 1.321(2) . ?
C5 N1 1.324(2) . ?
C5 N4 1.351(2) . ?
N7 H7A 0.9011 . ?
N7 H7B 0.8296 . ?
N4 H4A 0.8600 . ?
N6 H6B 0.8600 . ?
N6 H6A 0.8600 . ?
N1 N2 1.397(2) . ?
N1 H1A 0.8069 . ?
O1 P1 1.5023(13) . ?
O2 P1 1.5759(13) . ?
O2 H2 0.8714 . ?
O3 P1 1.5104(13) . ?
P1 H1 1.2918 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N2 C3 N7 125.61(16) . . ?
N2 C3 N4 111.58(15) . . ?
N7 C3 N4 122.76(16) . . ?
N6 C5 N1 127.28(17) . . ?
N6 C5 N4 125.97(16) . . ?
N1 C5 N4 106.75(15) . . ?
C3 N7 H7A 116.1 . . ?
C3 N7 H7B 113.8 . . ?
H7A N7 H7B 119.8 . . ?
C5 N4 C3 106.63(14) . . ?
C5 N4 H4A 126.7 . . ?
C3 N4 H4A 126.7 . . ?
C5 N6 H6B 120.0 . . ?
C5 N6 H6A 120.0 . . ?
H6B N6 H6A 120.0 . . ?
C5 N1 N2 111.28(15) . . ?
C5 N1 H1A 129.7 . . ?
N2 N1 H1A 118.2 . . ?
C3 N2 N1 103.75(14) . . ?
P1 O2 H2 109.3 . . ?
O1 P1 O3 114.76(7) . . ?
O1 P1 O2 111.69(7) . . ?
O3 P1 O2 109.75(7) . . ?
O1 P1 H1 110.7 . . ?
O3 P1 H1 109.0 . . ?
O2 P1 H1 100.0 . . ?

_diffrn_measured_fraction_theta_max 0.994
_diffrn_reflns_theta_full        62.55
_diffrn_measured_fraction_theta_full 0.994
_refine_diff_density_max         0.358
_refine_diff_density_min         -0.352
_refine_diff_density_rms         0.066

# Attachment '6005_web_deposit_cif_file_5_KarlaFejfarova_1309265877.dat_no3_1_precislovany.cif'

data_dat_no3_1
_database_code_depnum_ccdc_archive 'CCDC 831901'
#TrackingRef '6005_web_deposit_cif_file_5_KarlaFejfarova_1309265877.dat_no3_1_precislovany.cif'

_audit_creation_method           SHELXL-97
_chemical_name_systematic        
;
?
;
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C8 H24 N44 O12'
_chemical_formula_weight         648.51

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_H-M   P21/c

loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'

_cell_length_a                   9.51950(10)
_cell_length_b                   9.10000(10)
_cell_length_c                   7.41270(10)
_cell_angle_alpha                90.00
_cell_angle_beta                 95.9880(10)
_cell_angle_gamma                90.00
_cell_volume                     638.640(13)
_cell_formula_units_Z            4
_cell_measurement_temperature    120(2)
_cell_measurement_reflns_used    4542
_cell_measurement_theta_min      4.6668
_cell_measurement_theta_max      62.3029

_exptl_crystal_description       yellowish
_exptl_crystal_colour            plate
_exptl_crystal_size_max          0.4260
_exptl_crystal_size_mid          0.2800
_exptl_crystal_size_min          0.1837
_exptl_crystal_density_meas      ?
_exptl_crystal_density_diffrn    1.686
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             336
_exptl_absorpt_coefficient_mu    1.336
_exptl_absorpt_correction_type   multiscan
_exptl_absorpt_correction_T_min  0.18263
_exptl_absorpt_correction_T_max  1.0000
_exptl_absorpt_process_details   ?

_exptl_special_details           
;
CrysAlisPro, Oxford Diffraction Ltd.,
Version 1.171.33.55 (release 05-01-2010 CrysAlis171 .NET)
(compiled Jan 5 2010,16:28:46)
Empirical absorption correction using spherical harmonics,
implemented in SCALE3 ABSPACK scaling algorithm.
;

_diffrn_ambient_temperature      150(2)
_diffrn_radiation_wavelength     1.54178
_diffrn_radiation_type           CuK\a
_diffrn_radiation_source         'Enhance Ultra (Cu) X-ray Source'
_diffrn_radiation_monochromator  minor
_diffrn_measurement_device_type  'Xcalibur, Atlas, Gemini ultra'
_diffrn_measurement_method       ?
_diffrn_detector_area_resol_mean 10.3784
_diffrn_standards_number         ?
_diffrn_standards_interval_count ?
_diffrn_standards_interval_time  ?
_diffrn_standards_decay_%        ?
_diffrn_reflns_number            4685
_diffrn_reflns_av_R_equivalents  0.0293
_diffrn_reflns_av_sigmaI/netI    0.0156
_diffrn_reflns_limit_h_min       -10
_diffrn_reflns_limit_h_max       10
_diffrn_reflns_limit_k_min       -10
_diffrn_reflns_limit_k_max       10
_diffrn_reflns_limit_l_min       -8
_diffrn_reflns_limit_l_max       8
_diffrn_reflns_theta_min         4.67
_diffrn_reflns_theta_max         62.39
_reflns_number_total             1011
_reflns_number_gt                969
_reflns_threshold_expression     >2sigma(I)

_computing_data_collection       
;
CrysAlisPro, Oxford Diffraction Ltd.,
Version 1.171.33.55 (release 05-01-2010 CrysAlis171 .NET)
(compiled Jan 5 2010,16:28:46)
;
_computing_cell_refinement       
;
CrysAlisPro, Oxford Diffraction Ltd.,
Version 1.171.33.55 (release 05-01-2010 CrysAlis171 .NET)
(compiled Jan 5 2010,16:28:46)
;

_computing_data_reduction        
;
CrysAlisPro, Oxford Diffraction Ltd.,
Version 1.171.33.55 (release 05-01-2010 CrysAlis171 .NET)
(compiled Jan 5 2010,16:28:46)
;
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_molecular_graphics    ?
_computing_publication_material  ?

_refine_special_details          
;
Refinement of F^2^ against ALL reflections. The weighted R-factor wR and
goodness of fit S are based on F^2^, conventional R-factors R are based
on F, with F set to zero for negative F^2^. The threshold expression of
F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is
not relevant to the choice of reflections for refinement. R-factors based
on F^2^ are statistically about twice as large as those based on F, and R-
factors based on ALL data will be even larger.
;

_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'calc w=1/[\s^2^(Fo^2^)+(0.0457P)^2^+0.2247P] where P=(Fo^2^+2Fc^2^)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    mixed
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       ?
_refine_ls_number_reflns         1011
_refine_ls_number_parameters     124
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0293
_refine_ls_R_factor_gt           0.0281
_refine_ls_wR_factor_ref         0.0781
_refine_ls_wR_factor_gt          0.0769
_refine_ls_goodness_of_fit_ref   1.117
_refine_ls_restrained_S_all      1.117
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
H6B H -0.4594(19) 0.567(2) -0.674(3) 0.027(4) Uiso 1 1 d . . .
H7A H 0.0158(19) 0.779(2) -0.219(2) 0.030(5) Uiso 1 1 d . . .
H4A H -0.2238(19) 0.797(2) -0.419(2) 0.032(5) Uiso 1 1 d . . .
H6A H -0.4357(19) 0.726(2) -0.619(2) 0.034(5) Uiso 1 1 d . . .
H7B H 0.072(2) 0.630(2) -0.166(3) 0.034(5) Uiso 1 1 d . . .
H1A H -0.2756(18) 0.381(2) -0.501(2) 0.024(4) Uiso 1 1 d . . .
O3 O 0.40473(10) 0.45275(10) 0.14206(12) 0.0173(3) Uani 1 1 d . . .
O1 O 0.34633(10) 0.67973(10) 0.08810(13) 0.0222(3) Uani 1 1 d . . .
O2 O 0.24683(10) 0.50557(10) -0.08069(13) 0.0215(3) Uani 1 1 d . . .
N3 N 0.33251(11) 0.54713(12) 0.05009(15) 0.0148(3) Uani 1 1 d . . .
N7 N -0.00002(13) 0.68362(15) -0.20986(18) 0.0248(3) Uani 1 1 d . . .
N6 N -0.41749(12) 0.63063(15) -0.60247(17) 0.0195(3) Uani 1 1 d . . .
N4 N -0.21116(12) 0.69707(13) -0.41309(14) 0.0155(3) Uani 1 1 d . . .
N2 N -0.11677(12) 0.47805(13) -0.34852(15) 0.0177(3) Uani 1 1 d . . .
C3 C -0.10232(13) 0.61917(15) -0.32006(18) 0.0156(3) Uani 1 1 d . . .
N1 N -0.24065(12) 0.46764(13) -0.46782(15) 0.0162(3) Uani 1 1 d . . .
C5 C -0.29748(13) 0.59812(14) -0.50344(17) 0.0143(3) Uani 1 1 d . . .

loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_23
_atom_site_aniso_U_13
_atom_site_aniso_U_12
O3 0.0179(5) 0.0123(5) 0.0207(5) 0.0027(4) -0.0024(4) 0.0032(4)
O1 0.0257(6) 0.0103(5) 0.0294(5) -0.0003(4) -0.0035(4) 0.0001(4)
O2 0.0204(5) 0.0179(5) 0.0241(6) -0.0019(4) -0.0082(4) 0.0003(4)
N3 0.0135(6) 0.0121(6) 0.0186(6) 0.0011(4) 0.0013(5) -0.0003(4)
N7 0.0198(7) 0.0126(7) 0.0391(8) -0.0005(6) -0.0106(6) 0.0008(5)
N6 0.0200(7) 0.0124(7) 0.0246(7) -0.0008(5) -0.0049(5) -0.0002(5)
N4 0.0147(6) 0.0102(6) 0.0211(6) -0.0001(5) 0.0001(5) -0.0006(4)
N2 0.0140(6) 0.0149(7) 0.0233(6) -0.0015(5) -0.0024(5) -0.0001(4)
C3 0.0139(7) 0.0123(7) 0.0207(7) 0.0003(5) 0.0018(5) 0.0000(5)
N1 0.0154(6) 0.0116(6) 0.0211(6) -0.0017(5) -0.0016(5) -0.0006(5)
C5 0.0148(7) 0.0124(7) 0.0158(6) 0.0000(5) 0.0025(5) -0.0012(5)

_geom_special_details            
;
All esds (except the esd in the dihedral angle between two l.s. planes)
are estimated using the full covariance matrix. The cell esds are taken
into account individually in the estimation of esds in distances, angles
and torsion angles; correlations between esds in cell parameters are only
used when they are defined by crystal symmetry. An approximate (isotropic)
treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
O3 N3 1.2559(14) . ?
O1 N3 1.2430(15) . ?
O2 N3 1.2583(14) . ?
N7 C3 1.3392(18) . ?
N6 C5 1.3254(18) . ?
N4 C5 1.3489(17) . ?
N4 C3 1.3793(17) . ?
N2 C3 1.3064(19) . ?
N2 N1 1.4015(16) . ?
N1 C5 1.3200(18) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O1 N3 O3 120.12(11) . . ?
O1 N3 O2 120.75(11) . . ?
O3 N3 O2 119.13(11) . . ?
C5 N4 C3 106.98(12) . . ?
C3 N2 N1 103.64(11) . . ?
N2 C3 N7 125.92(13) . . ?
N2 C3 N4 111.32(12) . . ?
N7 C3 N4 122.71(13) . . ?
C5 N1 N2 111.45(11) . . ?
N1 C5 N6 128.54(13) . . ?
N1 C5 N4 106.58(12) . . ?
N6 C5 N4 124.84(13) . . ?

_diffrn_measured_fraction_theta_max 0.992
_diffrn_reflns_theta_full        62.39
_diffrn_measured_fraction_theta_full 0.992
_refine_diff_density_max         0.177
_refine_diff_density_min         -0.219
_refine_diff_density_rms         0.046

# Attachment '6006_web_deposit_cif_file_6_KarlaFejfarova_1309265877.dat-h3po4_1_precislovany.cif'

#=======================================================================
data_III
_database_code_depnum_ccdc_archive 'CCDC 831902'
#TrackingRef '6006_web_deposit_cif_file_6_KarlaFejfarova_1309265877.dat-h3po4_1_precislovany.cif'

#=======================================================================

# 5. CHEMICAL DATA

_chemical_name_systematic        
; ?
;
_chemical_name_common            ?
_chemical_formula_moiety         'C2 H6 N5, H2 O4 P '
_chemical_formula_structural     ?
_chemical_formula_analytical     ?
_chemical_formula_iupac          ?
_chemical_formula_sum            'C2 H8 N5 O4 P1'
_chemical_formula_weight         197.1
_chemical_melting_point          ?
_chemical_compound_source        ?
_chemical_absolute_configuration ad

#=======================================================================

# 6. CRYSTAL DATA

_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_H-M   'F d d 2'
_symmetry_space_group_name_Hall  'F 2 -2d'
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 x,y,z
2 -x,-y,z
3 x+1/4,-y+1/4,z+1/4
4 -x+1/4,y+1/4,z+1/4
5 x,y+1/2,z+1/2
6 -x,-y+1/2,z+1/2
7 x+1/4,-y+3/4,z+3/4
8 -x+1/4,y+3/4,z+3/4
9 x+1/2,y,z+1/2
10 -x+1/2,-y,z+1/2
11 x+3/4,-y+1/4,z+3/4
12 -x+3/4,y+1/4,z+3/4
13 x+1/2,y+1/2,z
14 -x+1/2,-y+1/2,z
15 x+3/4,-y+3/4,z+1/4
16 -x+3/4,y+3/4,z+1/4
_cell_length_a                   13.3492(4)
_cell_length_b                   37.1096(12)
_cell_length_c                   6.0702(2)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_volume                     3007.08(17)
_cell_formula_units_Z            16

_cell_measurement_reflns_used    7644
_cell_measurement_theta_min      4.7671
_cell_measurement_theta_max      66.6468
_cell_measurement_temperature    120
_cell_special_details            
; ?
;

_exptl_crystal_density_diffrn    1.7408
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             1632

_exptl_absorpt_coefficient_mu    3.270
_exptl_crystal_description       'irregular shape'
_exptl_crystal_size_max          0.3851
_exptl_crystal_size_mid          0.2734
_exptl_crystal_size_min          0.1800
_exptl_crystal_colour            colorless
_exptl_absorpt_correction_T_min  0.485
_exptl_absorpt_correction_T_max  0.686
_exptl_absorpt_correction_type   analytical
_exptl_absorpt_process_details   
;
CrysAlisPro, Oxford Diffraction Ltd.,
Version 1.171.33.51 (release 27-10-2009 CrysAlis171 .NET)
Analytical numeric absorption correction using a multifaceted crystal
model based on expressions derived by R.C. Clark & J.S. Reid.
;

#=======================================================================

# 7. EXPERIMENTAL DATA

_exptl_special_details           ?

_diffrn_ambient_temperature      120
_diffrn_radiation_type           'Cu K\a'
_diffrn_radiation_source         'X-ray tube'
_diffrn_radiation_wavelength     1.54184
_diffrn_radiation_monochromator  mirror
_diffrn_measurement_device       'four-cycle diffractometer'
_diffrn_measurement_device_type  
'Goniometer Xcalibur, detector: Atlas (Gemini ultra Cu)'
_diffrn_detector_area_resol_mean 10.3784
_diffrn_measurement_method       
'Rotation method data acquisition using \w scans'
_diffrn_reflns_number            8122
_diffrn_reflns_theta_min         7.05
_diffrn_reflns_theta_max         66.79
_diffrn_reflns_theta_full        66.79
_diffrn_measured_fraction_theta_max 0.99
_diffrn_measured_fraction_theta_full 0.99
_diffrn_reflns_av_R_equivalents  0.0247
_diffrn_reflns_av_sigmaI/netI    0.0055
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_k_min       -42
_diffrn_reflns_limit_k_max       44
_diffrn_reflns_limit_l_min       -7
_diffrn_reflns_limit_l_max       6
_diffrn_reflns_reduction_process 
;
Integration of the CCD images was done by program Crysalis RED
(Oxford diffraction, 2008). The same program was used for indexing of the
crystal shape and absorption correction.
;
#=======================================================================

# 8. REFINEMENT DATA

_refine_special_details          
;
The refinement was carried out against all reflections. The conventional
R-factor is always based on F. The goodness of fit as well as the weighted
R-factor are based on F and F^2^ for refinement carried out on F and F^2^,
respectively. The threshold expression is used only for calculating
R-factors etc. and it is not relevant to the choice of reflections for
refinement.

The program used for refinement, Jana2006, uses the weighting scheme
based on the experimental expectations, see _refine_ls_weighting_details,
that does not force S to be one. Therefore the values of S are usually larger
than the ones from the SHELX program.
;

_reflns_number_total             1295
_reflns_number_gt                1290
_reflns_threshold_expression     I>3\s(I)

_refine_ls_structure_factor_coef Fsqd
_refine_ls_R_factor_gt           0.0189
_refine_ls_wR_factor_gt          0.0615
_refine_ls_R_factor_all          0.0190
_refine_ls_wR_factor_ref         0.0617
_refine_ls_goodness_of_fit_ref   1.52
_refine_ls_goodness_of_fit_gt    1.52
_refine_ls_restrained_S_gt       ?
_refine_ls_restrained_S_all      ?
_refine_ls_number_reflns         1295
_refine_ls_number_parameters     133
_refine_ls_number_restraints     8
_refine_ls_number_constraints    9
_refine_ls_weighting_scheme      sigma
_refine_ls_weighting_details     w=1/(\s^2^(I)+0.0016I^2^)
_refine_ls_hydrogen_treatment    refxyz
_refine_ls_shift/su_max          0.0100
_refine_ls_shift/su_mean         0.0013
_refine_diff_density_max         0.09
_refine_diff_density_min         -0.11
_refine_ls_extinction_method     
'B-C type 1 Lorentzian isotropic (Becker & Coppens, 1974)'
_refine_ls_extinction_coef       1900(200)
_refine_ls_abs_structure_details 'Flack (1983)'
_refine_ls_abs_structure_Flack   0.034(16)
_refine_ls_abs_structure_Rogers  ?

loop_
_atom_type_symbol
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C 0.018 0.009 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1'
H 0.000 0.000 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1'
N 0.031 0.018 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1'
O 0.049 0.032 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1'
P 0.296 0.433 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1'

_computing_data_collection       'Crysalis CCD (Oxford diffraction, 2009)'
_computing_cell_refinement       'Crysalis RED (Oxford diffraction, 2009)'
_computing_data_reduction        'Crysalis RED'
_computing_structure_solution    'SIR2002 (Burla et al., 2003)'
_computing_structure_refinement  
"Jana2006 (Pet\<r\'i\<cek, Du\<sek & Palatinus, 2006)"
_computing_molecular_graphics    'Diamond (Brandenburg & Putz, 2005)'
_computing_publication_material  Jana2006

#=======================================================================

# 9. ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_adp_type
_atom_site_U_iso_or_equiv
_atom_site_symmetry_multiplicity
_atom_site_occupancy
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
P1 P 0.10815(3) 0.229170(8) 0.33533 Uani 0.01068(13) 16 1 d . . .
O1 O 0.10097(8) 0.23298(3) 0.0797(2) Uani 0.0170(4) 16 1 d . . .
O2 O 0.12943(9) 0.26783(3) 0.4298(2) Uani 0.0167(3) 16 1 d . . .
O3 O 0.01071(8) 0.21727(3) 0.43643(19) Uani 0.0149(3) 16 1 d . . .
O4 O 0.19550(7) 0.20384(3) 0.37417(19) Uani 0.0130(3) 16 1 d . . .
N4 N 0.21523(10) 0.14230(4) 1.1209(2) Uani 0.0137(4) 16 1 d . . .
N2 N 0.22888(10) 0.12095(4) 0.7812(2) Uani 0.0158(4) 16 1 d . . .
N1 N 0.22293(10) 0.09308(3) 0.9377(2) Uani 0.0147(4) 16 1 d . . .
N7 N 0.23167(11) 0.18427(4) 0.8286(3) Uani 0.0200(4) 16 1 d . . .
N6 N 0.20645(10) 0.08810(4) 1.3276(2) Uani 0.0185(4) 16 1 d . . .
C3 C 0.22433(12) 0.15011(4) 0.8992(3) Uani 0.0149(4) 16 1 d . . .
C5 C 0.21481(11) 0.10610(4) 1.1402(3) Uani 0.0132(4) 16 1 d . . .
H4A H 0.2088(15) 0.1581(5) 1.224(3) Uiso 0.0164 16 1 d . . .
H1A H 0.2356(15) 0.0709(3) 0.897(3) Uiso 0.0176 16 1 d . . .
H7B H 0.2185(15) 0.1867(6) 0.6881(17) Uiso 0.024 16 1 d . . .
H7A H 0.2035(15) 0.2015(4) 0.905(3) Uiso 0.024 16 1 d . . .
H6B H 0.1976(14) 0.0649(3) 1.312(4) Uiso 0.0222 16 1 d . . .
H6A H 0.2082(16) 0.1008(5) 1.450(2) Uiso 0.0222 16 1 d . . .
H1 H 0.0651(13) 0.2496(4) 0.034(3) Uiso 0.0203 16 1 d . . .
H2 H 0.1861(9) 0.2760(5) 0.411(3) Uiso 0.02 16 1 d . . .

loop_
_atom_site_aniso_label
_atom_site_aniso_type_symbol
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
P1 P 0.0141(2) 0.0078(2) 0.0102(2) 0.00037(12) 0.00078(14) -0.00024(15)
O1 O 0.0220(6) 0.0168(6) 0.0121(6) 0.0080(4) 0.0000(5) 0.0015(5)
O2 O 0.0162(5) 0.0092(6) 0.0246(6) -0.0012(4) 0.0039(5) -0.0052(5)
O3 O 0.0161(5) 0.0115(5) 0.0172(6) -0.0005(4) 0.0030(4) -0.0013(5)
O4 O 0.0155(5) 0.0105(5) 0.0131(5) 0.0015(4) -0.0006(4) 0.0000(4)
N4 N 0.0191(6) 0.0135(7) 0.0085(7) 0.0018(5) 0.0007(5) -0.0020(5)
N2 N 0.0248(7) 0.0130(7) 0.0098(7) 0.0012(5) 0.0006(5) 0.0017(5)
N1 N 0.0261(7) 0.0060(6) 0.0119(6) 0.0018(5) -0.0015(6) -0.0011(5)
N7 N 0.0347(7) 0.0134(6) 0.0119(6) 0.0046(5) 0.0031(7) 0.0005(6)
N6 N 0.0306(7) 0.0124(7) 0.0126(7) -0.0007(5) 0.0000(7) -0.0014(6)
C3 C 0.0166(7) 0.0159(7) 0.0124(8) 0.0019(5) 0.0004(6) 0.0001(6)
C5 C 0.0140(7) 0.0109(7) 0.0148(8) 0.0012(5) -0.0021(5) 0.0002(6)

#=======================================================================

# 10. MOLECULAR GEOMETRY

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_1
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
P1 O1 . . 1.5610(13) yes
P1 O2 . . 1.5710(11) yes
P1 O3 . . 1.5045(11) yes
P1 O4 . . 1.5160(11) yes
O1 H1 . . 0.827(17) yes
O2 H2 . . 0.823(13) yes
N4 C3 . . 1.382(2) yes
N4 C5 . . 1.348(2) yes
N4 H4A . . 0.864(16) yes
N2 N1 . . 1.4065(19) yes
N2 C3 . . 1.299(2) yes
N1 C5 . . 1.326(2) yes
N1 H1A . . 0.873(13) yes
N7 C3 . . 1.342(2) yes
N7 H7B . . 0.875(11) yes
N7 H7A . . 0.877(18) yes
N6 C5 . . 1.324(2) yes
N6 H6B . . 0.875(11) yes
N6 H6A . . 0.882(16) yes

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_2
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
O1 P1 O2 . . . 106.92(7) yes
O1 P1 O3 . . . 112.27(6) yes
O1 P1 O4 . . . 104.95(6) yes
O2 P1 O3 . . . 105.99(6) yes
O2 P1 O4 . . . 111.74(6) yes
O3 P1 O4 . . . 114.81(6) yes
P1 O1 H1 . . . 115.8(13) yes
P1 O2 H2 . . . 116.9(13) yes
C3 N4 C5 . . . 107.12(14) yes
C3 N4 H4A . . . 125.0(11) yes
C5 N4 H4A . . . 127.9(11) yes
N1 N2 C3 . . . 103.74(13) yes
N2 N1 C5 . . . 111.28(12) yes
N2 N1 H1A . . . 119.5(13) yes
C5 N1 H1A . . . 128.2(13) yes
C3 N7 H7B . . . 113.1(15) yes
C3 N7 H7A . . . 119.3(12) yes
H7B N7 H7A . . . 111.0(19) yes
C5 N6 H6B . . . 114.5(16) yes
C5 N6 H6A . . . 117.1(12) yes
H6B N6 H6A . . . 128.4(19) yes
N4 C3 N2 . . . 111.48(14) yes
N4 C3 N7 . . . 121.07(15) yes
N2 C3 N7 . . . 127.38(16) yes
N4 C5 N1 . . . 106.38(14) yes
N4 C5 N6 . . . 125.31(15) yes
N1 C5 N6 . . . 128.30(14) yes

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion
_geom_torsion_publ_flag
? ? ? ? ? ? ? ? ? ?

loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_site_symmetry_D
_geom_hbond_site_symmetry_H
_geom_hbond_site_symmetry_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_publ_flag
? ? ? ? ? ? ? ? ? ? ?

#=======================================================================

# 11. STRUCTURE-FACTOR LIST

loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
1 1 -7 924.00 983.73 15.73 o
3 1 -7 3963.52 3729.64 39.70 o
1 3 -7 363.10 469.50 12.96 o
3 3 -7 1441.19 1508.31 25.32 o
1 5 -7 1951.61 1875.92 21.08 o
3 5 -7 3904.30 4093.07 57.90 o
1 7 -7 2785.67 2699.14 24.37 o
3 7 -7 1881.37 1899.47 39.45 o
1 9 -7 3805.38 3929.58 28.54 o
2 0 -6 1546.22 1627.80 36.18 o
6 0 -6 1968.14 1915.99 22.92 o
0 2 -6 848.92 915.25 19.64 o
2 2 -6 954.46 947.82 16.35 o
4 2 -6 1881.23 1920.37 18.00 o
6 2 -6 3059.25 2865.44 25.92 o
2 4 -6 6855.43 6390.42 39.80 o
4 4 -6 2041.70 1899.39 18.00 o
6 4 -6 4136.65 4024.34 30.79 o
8 4 -6 1382.44 1409.95 33.69 o
0 6 -6 2675.01 2494.47 42.75 o
2 6 -6 6136.51 6175.69 32.72 o
4 6 -6 1514.67 1521.63 16.03 o
6 6 -6 3642.42 3512.06 28.66 o
2 8 -6 5093.88 4882.87 29.10 o
4 8 -6 161.23 153.09 6.01 o
6 8 -6 117.09 108.75 6.80 o
8 8 -6 3311.39 3142.34 50.48 o
0 10 -6 1177.79 1106.04 17.83 o
2 10 -6 4272.74 4275.34 30.72 o
4 10 -6 1312.25 1177.30 16.32 o
6 10 -6 9171.84 8829.00 42.99 o
8 10 -6 917.03 899.25 26.86 o
2 12 -6 332.83 281.22 8.18 o
4 12 -6 1893.72 1738.31 26.93 o
6 12 -6 497.65 525.20 12.17 o
0 14 -6 1333.11 1279.56 24.84 o
2 14 -6 5938.58 5813.02 29.70 o
4 14 -6 3987.53 3961.08 33.16 o
6 14 -6 4807.64 4597.29 37.73 o
2 16 -6 656.36 719.32 12.71 o
4 16 -6 709.23 758.34 18.21 o
6 16 -6 612.06 616.84 13.72 o
0 18 -6 586.39 570.72 26.85 o
2 18 -6 3174.56 3020.10 26.16 o
4 18 -6 3066.65 2980.75 32.44 o
6 18 -6 1041.29 1104.88 29.27 o
2 20 -6 361.00 379.92 9.54 o
4 20 -6 802.78 761.22 20.01 o
0 22 -6 7284.23 7199.81 60.37 o
2 22 -6 178.20 177.56 7.98 o
4 22 -6 1064.53 1047.33 28.50 o
2 24 -6 600.03 576.86 21.37 o
1 1 -5 5803.95 5942.24 33.19 o
3 1 -5 275.10 335.33 10.11 o
5 1 -5 1092.74 1123.80 12.99 o
7 1 -5 8830.32 8875.32 46.56 o
9 1 -5 4479.18 4323.23 37.18 o
11 1 -5 3621.90 3875.07 39.34 o
1 3 -5 3543.60 3462.55 25.71 o
3 3 -5 16756.57 16800.90 58.50 o
5 3 -5 569.77 596.60 10.43 o
7 3 -5 1845.84 1745.94 21.46 o
9 3 -5 2246.16 2079.52 23.44 o
11 3 -5 75.96 123.65 9.15 o
1 5 -5 451.34 449.04 10.37 o
3 5 -5 933.02 888.59 14.49 o
5 5 -5 13617.16 13829.79 48.98 o
7 5 -5 3051.76 3061.12 27.45 o
9 5 -5 332.72 310.74 10.04 o
1 7 -5 5538.50 5781.45 29.96 o
3 7 -5 9986.92 9875.11 42.77 o
5 7 -5 13480.83 13359.87 57.11 o
7 7 -5 837.99 789.88 16.39 o
9 7 -5 491.74 494.67 13.44 o
1 9 -5 366.84 327.17 10.41 o
3 9 -5 8357.69 8410.18 40.12 o
5 9 -5 4821.34 4708.93 34.57 o
7 9 -5 4010.60 3831.28 38.51 o
9 9 -5 7643.32 7536.66 46.71 o
1 11 -5 13354.98 13077.09 46.80 o
3 11 -5 409.53 411.39 10.13 o
5 11 -5 6527.79 6331.31 39.51 o
7 11 -5 645.54 683.22 17.08 o
9 11 -5 1223.64 1224.98 22.87 o
1 13 -5 3285.47 3008.36 24.97 o
3 13 -5 5843.05 5982.52 34.47 o
5 13 -5 3658.61 3480.57 32.90 o
7 13 -5 3686.93 3694.35 35.63 o
9 13 -5 9080.50 9543.71 59.16 o
1 15 -5 10715.13 10645.90 49.41 o
3 15 -5 6830.67 6703.70 38.21 o
5 15 -5 7754.18 7734.78 42.95 o
7 15 -5 888.68 836.31 15.67 o
9 15 -5 3706.52 3730.69 35.52 o
1 17 -5 3837.64 3484.14 32.11 o
3 17 -5 127.72 132.57 7.50 o
5 17 -5 9759.83 9926.86 52.88 o
7 17 -5 6778.60 6869.27 40.69 o
9 17 -5 154.90 130.02 8.95 o
1 19 -5 5081.59 4866.43 41.37 o
3 19 -5 9895.96 9569.30 55.56 o
5 19 -5 2483.64 2344.34 25.82 o
7 19 -5 4794.58 4671.25 32.28 o
9 19 -5 1878.70 1825.26 36.10 o
1 21 -5 4097.58 4047.72 42.28 o
3 21 -5 2601.55 2445.47 28.32 o
5 21 -5 709.88 622.06 13.13 o
7 21 -5 4828.15 4385.45 37.96 o
1 23 -5 2761.68 2515.18 32.71 o
3 23 -5 1434.46 1354.39 23.90 o
5 23 -5 202.37 199.51 8.99 o
7 23 -5 1380.26 1312.03 24.58 o
1 25 -5 1928.13 1885.07 27.28 o
3 25 -5 6036.61 5691.40 44.05 o
5 25 -5 1080.92 1040.79 17.88 o
1 27 -5 93.36 106.96 8.00 o
3 27 -5 1828.64 1809.18 23.65 o
5 27 -5 3597.52 3368.75 28.63 o
1 29 -5 2270.72 2066.72 20.97 o
3 29 -5 1022.98 1066.57 18.41 o
1 31 -5 1647.08 1643.31 25.77 o
0 0 -4 64604.24 66523.94 178.40 o
4 0 -4 12745.33 12483.97 63.12 o
8 0 -4 112.81 127.26 10.64 o
12 0 -4 4343.71 4623.26 69.41 o
2 2 -4 1488.32 1501.87 14.39 o
4 2 -4 6213.86 6529.54 32.66 o
6 2 -4 21252.50 20624.58 69.70 o
8 2 -4 7197.43 7394.48 40.55 o
10 2 -4 8616.59 8613.10 50.32 o
12 2 -4 309.74 359.81 14.80 o
0 4 -4 5104.25 4814.69 32.64 o
2 4 -4 11457.03 11315.83 41.91 o
4 4 -4 19135.25 19326.13 53.44 o
6 4 -4 4570.10 4406.60 31.02 o
8 4 -4 1970.36 2087.08 22.29 o
10 4 -4 1573.22 1638.25 21.00 o
12 4 -4 392.16 405.63 12.98 o
2 6 -4 3327.65 3254.99 20.78 o
4 6 -4 385.49 429.93 8.99 o
6 6 -4 3035.45 3023.49 25.07 o
8 6 -4 7647.56 7978.96 46.24 o
10 6 -4 7826.09 8300.83 50.05 o
12 6 -4 3651.38 3658.25 35.68 o
0 8 -4 1357.19 1269.11 20.33 o
2 8 -4 27605.45 27481.78 59.63 o
4 8 -4 5694.52 5706.30 29.00 o
6 8 -4 14640.32 14786.49 51.11 o
8 8 -4 1119.43 1177.61 16.94 o
10 8 -4 634.91 701.99 15.87 o
12 8 -4 517.09 550.10 14.56 o
2 10 -4 2732.14 2598.28 19.36 o
4 10 -4 3549.78 3619.12 25.34 o
6 10 -4 1955.11 2099.10 20.19 o
8 10 -4 9652.51 9995.21 51.07 o
10 10 -4 1906.20 2065.14 22.57 o
12 10 -4 4959.57 5160.91 67.23 o
0 12 -4 531.30 560.46 12.54 o
2 12 -4 31265.18 30705.46 69.58 o
4 12 -4 150.64 174.67 8.62 o
6 12 -4 19781.79 21122.69 70.57 o
8 12 -4 1627.12 1555.40 20.96 o
10 12 -4 2589.41 2635.25 25.01 o
12 12 -4 210.91 227.48 14.76 o
2 14 -4 2246.36 2334.06 20.20 o
4 14 -4 6043.76 6256.60 34.25 o
6 14 -4 523.24 484.26 12.87 o
8 14 -4 5752.84 5732.23 35.48 o
10 14 -4 1063.72 980.13 15.29 o
0 16 -4 13165.38 12726.62 75.01 o
2 16 -4 21405.13 21254.79 61.17 o
4 16 -4 18265.54 18956.26 55.64 o
6 16 -4 20747.23 21320.25 75.42 o
8 16 -4 1661.68 1676.70 21.57 o
10 16 -4 3787.39 3889.80 33.49 o
2 18 -4 4359.51 4145.15 30.00 o
4 18 -4 8316.50 8258.41 39.40 o
6 18 -4 6123.66 6340.10 37.73 o
8 18 -4 10437.47 11033.35 51.85 o
10 18 -4 624.36 604.35 11.18 o
0 20 -4 16140.00 16313.45 87.84 o
2 20 -4 14124.73 14203.85 61.19 o
4 20 -4 11117.29 11175.34 49.55 o
6 20 -4 1826.60 1832.60 20.60 o
8 20 -4 3612.53 3655.98 26.48 o
10 20 -4 3328.83 3266.09 22.98 o
2 22 -4 151.74 188.31 11.29 o
4 22 -4 4617.96 4937.92 33.18 o
6 22 -4 7789.31 7860.90 40.29 o
8 22 -4 5181.01 5188.87 30.07 o
10 22 -4 6517.33 6083.64 69.08 o
0 24 -4 17804.95 17862.33 126.77 o
2 24 -4 1046.53 1029.19 22.02 o
4 24 -4 5661.23 5750.89 38.40 o
6 24 -4 179.24 181.72 7.24 o
8 24 -4 6113.25 5952.76 29.91 o
2 26 -4 1041.11 1038.41 21.50 o
4 26 -4 349.60 326.21 10.22 o
6 26 -4 5857.07 5756.51 34.56 o
8 26 -4 2521.78 2378.40 21.49 o
0 28 -4 10749.41 10770.71 93.06 o
2 28 -4 1986.07 2097.87 28.31 o
4 28 -4 8994.56 9091.45 48.72 o
6 28 -4 991.40 983.30 14.05 o
8 28 -4 1167.39 1119.99 22.24 o
2 30 -4 7448.80 7818.90 46.35 o
4 30 -4 3970.47 3937.35 30.16 o
6 30 -4 200.83 228.63 10.15 o
0 32 -4 10874.02 11434.71 83.36 o
2 32 -4 4976.46 5111.59 34.66 o
4 32 -4 242.13 232.61 8.88 o
6 32 -4 7403.68 8089.39 82.66 o
2 34 -4 410.48 450.79 11.09 o
4 34 -4 1395.59 1327.28 20.44 o
0 36 -4 18.89 43.05 11.84 o
2 36 -4 12976.01 12763.34 96.21 o
1 1 -3 11454.29 12051.11 42.97 o
3 1 -3 16561.03 16295.62 56.51 o
5 1 -3 2572.70 2601.88 19.02 o
7 1 -3 1476.37 1464.39 16.10 o
9 1 -3 2564.53 2534.65 23.02 o
11 1 -3 8218.75 8263.89 46.72 o
13 1 -3 1915.21 1983.40 26.25 o
1 3 -3 11756.86 11789.81 41.25 o
3 3 -3 10512.89 10279.95 45.24 o
5 3 -3 11945.48 11960.93 42.87 o
7 3 -3 12121.89 11902.04 41.78 o
9 3 -3 2737.39 2633.62 23.34 o
11 3 -3 5714.18 6075.50 44.77 o
13 3 -3 2219.10 2482.13 29.07 o
1 5 -3 34557.34 36595.09 71.93 o
3 5 -3 2045.19 2240.46 18.65 o
5 5 -3 5050.59 5178.08 25.57 o
7 5 -3 6201.10 6058.31 32.18 o
9 5 -3 511.24 508.34 12.36 o
11 5 -3 1713.14 1722.16 21.94 o
13 5 -3 2857.99 3084.88 28.05 o
1 7 -3 17047.08 17188.84 54.01 o
3 7 -3 34111.78 33968.64 77.59 o
5 7 -3 280.20 290.82 6.82 o
7 7 -3 2620.81 2563.57 21.58 o
9 7 -3 9910.59 10036.01 52.56 o
11 7 -3 6227.57 6556.00 41.42 o
13 7 -3 2810.35 2942.64 30.50 o
1 9 -3 133.01 120.09 5.02 o
3 9 -3 6634.09 6816.00 32.81 o
5 9 -3 9963.53 9750.54 33.74 o
7 9 -3 3575.33 3347.69 26.37 o
9 9 -3 7585.03 7445.57 40.12 o
11 9 -3 2213.66 2210.98 22.11 o
13 9 -3 4500.88 4543.47 36.24 o
1 11 -3 1184.76 1416.45 11.83 o
3 11 -3 11417.79 11472.51 40.46 o
5 11 -3 28665.24 28772.89 60.66 o
7 11 -3 6512.88 6551.99 38.27 o
9 11 -3 3977.77 4181.86 30.62 o
11 11 -3 1767.09 1867.12 21.90 o
13 11 -3 1758.96 1809.14 22.80 o
1 13 -3 18332.22 18747.42 45.25 o
3 13 -3 7374.16 7637.36 34.34 o
5 13 -3 2547.50 2323.36 19.56 o
7 13 -3 1713.97 1874.31 20.13 o
9 13 -3 7660.08 8025.32 42.21 o
11 13 -3 3768.37 3879.32 30.58 o
13 13 -3 1149.46 1272.44 45.48 o
1 15 -3 19945.94 20959.46 47.25 o
3 15 -3 7529.80 8032.08 34.23 o
5 15 -3 4586.26 4587.56 32.00 o
7 15 -3 4524.67 4525.55 31.00 o
9 15 -3 6432.34 6684.63 38.42 o
11 15 -3 338.41 379.43 11.69 o
13 15 -3 1880.78 1819.36 35.77 o
1 17 -3 3408.61 3249.00 20.10 o
3 17 -3 1842.46 1763.88 17.32 o
5 17 -3 17080.86 17453.90 62.15 o
7 17 -3 16477.66 16896.07 59.01 o
9 17 -3 2965.65 2935.42 28.04 o
11 17 -3 112.06 136.84 8.31 o
1 19 -3 479.87 536.18 9.05 o
3 19 -3 8039.27 8162.59 41.99 o
5 19 -3 8532.29 8768.19 45.38 o
7 19 -3 1443.31 1407.83 18.66 o
9 19 -3 283.93 305.77 9.93 o
11 19 -3 1109.60 1138.53 20.18 o
1 21 -3 8390.01 8089.15 37.58 o
3 21 -3 4727.96 4571.87 32.41 o
5 21 -3 2074.33 1977.91 21.08 o
7 21 -3 8849.43 8977.34 44.51 o
9 21 -3 3064.95 3166.10 27.49 o
11 21 -3 6891.18 7063.90 45.43 o
1 23 -3 409.01 358.84 11.01 o
3 23 -3 21636.80 21604.05 76.96 o
5 23 -3 1766.67 1787.78 19.03 o
7 23 -3 1583.57 1610.76 19.32 o
9 23 -3 329.86 351.72 12.59 o
11 23 -3 1916.62 1914.39 19.99 o
1 25 -3 2748.59 2518.01 24.09 o
3 25 -3 9957.39 10347.14 54.71 o
5 25 -3 1814.24 1815.83 20.30 o
7 25 -3 8430.32 8241.63 43.34 o
9 25 -3 445.49 521.24 14.54 o
11 25 -3 917.44 887.98 15.84 o
1 27 -3 3212.83 3206.86 27.36 o
3 27 -3 3652.88 3720.42 28.83 o
5 27 -3 12274.44 12558.47 51.56 o
7 27 -3 9397.31 9296.97 51.46 o
9 27 -3 1974.78 2035.13 22.07 o
1 29 -3 7210.02 7191.52 39.92 o
3 29 -3 1080.36 1025.70 14.57 o
5 29 -3 30.97 47.70 7.13 o
7 29 -3 6873.57 7199.16 49.27 o
9 29 -3 2813.13 2894.96 27.02 o
1 31 -3 12102.08 11848.34 56.66 o
3 31 -3 3873.14 4027.36 28.50 o
5 31 -3 3277.73 3304.51 34.55 o
7 31 -3 988.40 1007.15 17.99 o
9 31 -3 2111.68 2069.00 23.05 o
1 33 -3 603.62 600.74 13.53 o
3 33 -3 956.02 903.39 19.88 o
5 33 -3 3267.09 3503.93 38.82 o
7 33 -3 894.22 866.31 15.16 o
1 35 -3 5381.87 5934.34 46.15 o
3 35 -3 6072.52 6181.86 59.52 o
5 35 -3 3412.77 3315.48 40.91 o
7 35 -3 684.74 758.95 17.47 o
1 37 -3 5100.23 5303.05 50.59 o
3 37 -3 745.42 802.04 20.03 o
5 37 -3 1010.92 960.47 20.09 o
1 39 -3 4261.25 4126.48 43.45 o
3 39 -3 1142.34 1073.58 29.79 o
2 0 -2 40423.91 41358.50 123.68 o
6 0 -2 7358.00 7413.78 47.78 o
10 0 -2 7041.83 7057.64 50.41 o
14 0 -2 3591.61 3899.44 81.57 o
0 2 -2 67649.53 66026.27 519.89 o
2 2 -2 7516.62 7080.83 40.26 o
4 2 -2 2449.81 1864.35 30.29 o
6 2 -2 5896.81 5878.23 33.50 o
8 2 -2 8796.08 8861.01 34.47 o
10 2 -2 1755.04 1792.31 18.59 o
12 2 -2 1594.13 1629.10 18.51 o
14 2 -2 333.04 351.72 16.42 o
2 4 -2 2157.65 2053.70 22.35 o
4 4 -2 321.29 357.17 12.32 o
6 4 -2 3675.05 3764.14 22.60 o
8 4 -2 1906.56 1722.17 16.68 o
10 4 -2 6854.84 6821.06 40.09 o
12 4 -2 2441.78 2504.20 25.39 o
14 4 -2 1940.92 2142.64 26.36 o
0 6 -2 27341.00 26731.20 75.34 o
2 6 -2 12147.25 11616.79 53.63 o
4 6 -2 4587.76 4198.77 33.52 o
6 6 -2 12715.14 13606.83 38.16 o
8 6 -2 3376.53 3359.37 23.51 o
10 6 -2 1086.65 1115.67 15.75 o
12 6 -2 2435.98 2608.65 26.15 o
14 6 -2 1228.94 1245.28 20.20 o
2 8 -2 19109.38 21057.38 75.06 o
4 8 -2 4898.16 5286.34 28.30 o
6 8 -2 224.01 249.10 6.53 o
8 8 -2 5794.34 5596.31 29.11 o
10 8 -2 1032.22 1130.58 16.04 o
12 8 -2 7793.36 7763.21 44.10 o
14 8 -2 1590.23 1664.75 24.03 o
0 10 -2 29241.22 31841.09 157.09 o
2 10 -2 6140.07 6257.18 43.79 o
4 10 -2 11629.68 11357.94 43.02 o
6 10 -2 10737.05 10988.84 36.75 o
8 10 -2 3460.05 3367.56 23.20 o
10 10 -2 2061.34 2158.75 21.67 o
12 10 -2 226.33 237.09 10.28 o
14 10 -2 271.30 291.98 10.81 o
2 12 -2 13112.42 14520.22 48.88 o
4 12 -2 8321.14 7961.81 44.88 o
6 12 -2 8325.25 8232.75 32.92 o
8 12 -2 49.00 77.42 7.65 o
10 12 -2 1830.67 1767.25 19.27 o
12 12 -2 4806.55 5185.33 45.53 o
14 12 -2 553.82 498.93 15.08 o
0 14 -2 17008.86 17830.89 67.63 o
2 14 -2 3887.33 3752.58 24.77 o
4 14 -2 9230.84 9353.06 39.07 o
6 14 -2 10614.83 10564.06 40.96 o
8 14 -2 807.71 747.28 12.43 o
10 14 -2 2091.05 2151.03 20.71 o
12 14 -2 304.62 311.31 12.81 o
14 14 -2 3286.78 3201.18 34.48 o
2 16 -2 4630.40 4761.16 27.32 o
4 16 -2 8355.41 8423.82 34.24 o
6 16 -2 456.38 508.02 10.26 o
8 16 -2 906.13 1024.72 14.97 o
10 16 -2 5436.78 5372.62 37.78 o
12 16 -2 456.36 441.52 14.54 o
14 16 -2 1241.47 1153.26 29.13 o
0 18 -2 1976.50 1815.20 17.97 o
2 18 -2 8527.55 8823.76 33.97 o
4 18 -2 7821.64 7315.98 33.33 o
6 18 -2 2519.53 2359.01 21.03 o
8 18 -2 8268.11 8171.18 43.15 o
10 18 -2 7222.50 7268.73 49.46 o
12 18 -2 273.70 275.60 11.62 o
2 20 -2 8428.44 9125.79 36.51 o
4 20 -2 371.85 399.24 8.97 o
6 20 -2 6995.47 6902.48 36.14 o
8 20 -2 3025.10 3011.75 32.44 o
10 20 -2 1480.64 1543.29 23.50 o
12 20 -2 818.66 847.65 17.56 o
0 22 -2 13873.17 12979.52 51.91 o
2 22 -2 2014.93 2207.73 19.42 o
4 22 -2 5533.10 5340.40 28.92 o
6 22 -2 1878.60 2027.85 22.22 o
8 22 -2 10938.32 10349.38 58.50 o
10 22 -2 950.26 858.08 17.57 o
12 22 -2 986.58 929.67 16.94 o
2 24 -2 6480.91 6589.98 32.28 o
4 24 -2 897.00 920.41 13.04 o
6 24 -2 3162.59 3153.30 30.92 o
8 24 -2 43.58 54.26 7.81 o
10 24 -2 1279.81 1283.47 19.98 o
12 24 -2 159.81 149.62 9.50 o
0 26 -2 10884.04 10574.94 62.69 o
2 26 -2 270.04 235.48 8.20 o
4 26 -2 9840.36 9170.70 46.61 o
6 26 -2 13388.59 13617.03 59.28 o
8 26 -2 6122.00 5862.15 37.97 o
10 26 -2 120.83 111.12 7.24 o
12 26 -2 1534.86 1481.13 23.10 o
2 28 -2 10611.12 10651.00 40.58 o
4 28 -2 1542.69 1476.32 18.81 o
6 28 -2 2023.71 2012.56 23.40 o
8 28 -2 4449.01 4564.00 32.09 o
10 28 -2 4956.16 5051.12 33.39 o
0 30 -2 334.24 380.65 16.20 o
2 30 -2 7902.48 8208.74 39.52 o
4 30 -2 14538.55 14512.09 55.86 o
6 30 -2 964.47 1013.63 18.58 o
8 30 -2 43.81 55.57 6.23 o
10 30 -2 6348.15 5897.33 49.28 o
2 32 -2 3637.27 3650.86 31.52 o
4 32 -2 5932.29 6028.07 33.49 o
6 32 -2 1102.10 1058.55 18.30 o
8 32 -2 31.82 46.19 6.89 o
10 32 -2 711.98 666.26 22.88 o
0 34 -2 7400.20 6844.26 74.79 o
2 34 -2 3602.37 3723.79 37.34 o
4 34 -2 1185.30 1134.89 16.91 o
6 34 -2 11014.94 10605.38 46.03 o
8 34 -2 375.15 362.75 11.42 o
2 36 -2 7193.79 6815.92 42.48 o
4 36 -2 1506.85 1460.06 21.79 o
6 36 -2 471.09 425.27 11.20 o
8 36 -2 7130.57 6603.30 68.72 o
0 38 -2 2716.38 2562.06 42.05 o
2 38 -2 5467.30 5312.83 40.38 o
4 38 -2 1324.44 1330.93 20.18 o
2 40 -2 566.03 630.35 17.67 o
4 40 -2 13.83 23.71 11.40 <
1 1 -1 18510.13 18426.09 36.13 o
3 1 -1 69889.41 68630.43 322.39 o
5 1 -1 11589.78 11131.07 47.40 o
7 1 -1 4391.04 4517.34 25.18 o
9 1 -1 1422.99 1421.13 13.87 o
11 1 -1 26351.80 27364.73 67.15 o
13 1 -1 2377.64 2302.90 27.38 o
15 1 -1 3303.49 3222.85 27.23 o
1 3 -1 23710.43 24162.36 50.27 o
3 3 -1 11143.42 10178.14 41.56 o
5 3 -1 2192.58 1835.44 20.45 o
7 3 -1 30834.38 30213.50 75.76 o
9 3 -1 910.83 941.16 13.08 o
11 3 -1 11727.99 11954.51 44.84 o
13 3 -1 1020.84 1000.08 16.02 o
15 3 -1 3597.63 3738.60 33.89 o
1 5 -1 54266.86 54027.52 314.98 o
3 5 -1 13802.26 12689.80 37.12 o
5 5 -1 17496.73 17684.28 59.44 o
7 5 -1 18941.89 19534.46 63.51 o
9 5 -1 6469.03 6392.89 30.62 o
11 5 -1 4594.12 4779.29 29.47 o
13 5 -1 3532.27 3654.00 28.82 o
15 5 -1 1760.28 1694.08 22.99 o
1 7 -1 48534.22 47742.77 146.89 o
3 7 -1 2172.03 1987.93 17.70 o
5 7 -1 17304.27 18792.60 63.51 o
7 7 -1 3915.75 4047.80 23.82 o
9 7 -1 3453.48 3504.80 23.22 o
11 7 -1 3433.79 3460.44 24.20 o
13 7 -1 1601.53 1661.41 26.30 o
15 7 -1 1964.13 1918.18 28.88 o
1 9 -1 6230.45 5666.02 29.56 o
3 9 -1 25344.21 25819.77 71.23 o
5 9 -1 9189.31 9530.96 49.37 o
7 9 -1 5261.97 5411.99 29.97 o
9 9 -1 18352.74 18375.22 48.32 o
11 9 -1 6357.44 6524.96 35.33 o
13 9 -1 2274.88 2403.85 30.91 o
15 9 -1 462.04 489.58 14.89 o
1 11 -1 20530.13 20150.53 58.72 o
3 11 -1 5843.35 6450.33 35.28 o
5 11 -1 6899.37 7245.34 36.28 o
7 11 -1 5661.19 6007.52 28.30 o
9 11 -1 6213.69 6296.97 29.19 o
11 11 -1 1121.51 1087.34 20.73 o
13 11 -1 386.35 380.46 13.48 o
15 11 -1 3061.26 3241.73 34.70 o
1 13 -1 2339.29 2145.17 17.05 o
3 13 -1 9074.69 9777.20 40.90 o
5 13 -1 7874.78 8182.19 40.61 o
7 13 -1 760.10 696.06 10.74 o
9 13 -1 9493.27 9552.68 44.48 o
11 13 -1 1998.79 1932.06 26.86 o
13 13 -1 1562.96 1543.34 24.93 o
15 13 -1 2244.31 2291.14 28.23 o
1 15 -1 39277.70 41777.17 97.59 o
3 15 -1 3623.18 3461.50 18.26 o
5 15 -1 12479.21 12473.36 41.62 o
7 15 -1 1242.91 1249.58 15.14 o
9 15 -1 6917.76 6768.52 41.35 o
11 15 -1 2800.95 2635.73 28.16 o
13 15 -1 136.58 176.36 9.65 o
1 17 -1 920.54 909.30 10.87 o
3 17 -1 7101.63 7340.17 27.09 o
5 17 -1 21044.13 22079.41 51.10 o
7 17 -1 1535.33 1459.65 20.30 o
9 17 -1 532.47 531.24 12.98 o
11 17 -1 6740.91 6463.92 38.08 o
13 17 -1 3568.45 3688.48 35.31 o
1 19 -1 10261.65 9865.24 32.37 o
3 19 -1 16883.06 17795.87 44.60 o
5 19 -1 7613.08 7266.74 28.23 o
7 19 -1 14092.43 13972.67 52.36 o
9 19 -1 3466.62 3695.74 27.37 o
11 19 -1 269.92 250.85 9.12 o
13 19 -1 2828.39 2910.57 29.80 o
1 21 -1 3729.55 3795.44 20.63 o
3 21 -1 10145.15 9614.37 33.23 o
5 21 -1 7624.11 7670.20 31.20 o
7 21 -1 11751.56 11728.25 47.73 o
9 21 -1 3528.24 3677.91 29.62 o
11 21 -1 1992.00 1983.47 22.53 o
13 21 -1 110.93 117.11 8.07 o
1 23 -1 18038.96 18909.10 47.44 o
3 23 -1 19146.45 18859.80 50.55 o
5 23 -1 5755.75 6029.25 29.53 o
7 23 -1 11168.48 10593.58 49.70 o
9 23 -1 3503.43 3344.53 30.13 o
11 23 -1 3713.85 3701.68 28.99 o
13 23 -1 786.44 880.39 19.24 o
1 25 -1 16.20 29.26 5.90 o
3 25 -1 26177.97 26333.07 67.29 o
5 25 -1 1742.37 1591.32 16.86 o
7 25 -1 2107.98 1926.37 23.45 o
9 25 -1 3066.58 3014.91 28.02 o
11 25 -1 5024.24 4804.05 33.34 o
1 27 -1 3799.05 3446.46 25.51 o
3 27 -1 5712.02 5596.26 32.82 o
5 27 -1 9393.21 9628.82 40.43 o
7 27 -1 11980.68 12208.39 50.57 o
9 27 -1 263.55 268.26 9.30 o
11 27 -1 1925.00 1898.56 20.03 o
1 29 -1 7776.24 7831.84 36.90 o
3 29 -1 4115.69 3978.35 28.36 o
5 29 -1 9945.26 9789.31 43.17 o
7 29 -1 7397.99 7636.25 39.41 o
9 29 -1 1216.20 1089.10 15.88 o
11 29 -1 2545.81 2486.90 32.03 o
1 31 -1 14521.79 14110.04 56.80 o
3 31 -1 269.52 293.03 8.86 o
5 31 -1 2542.30 2526.13 22.32 o
7 31 -1 4375.62 4142.20 26.26 o
9 31 -1 617.42 608.39 12.25 o
11 31 -1 1691.41 1506.31 32.62 o
1 33 -1 10724.41 10532.54 59.12 o
3 33 -1 2068.98 1921.41 18.56 o
5 33 -1 2282.08 2541.07 25.30 o
7 33 -1 4260.41 4159.87 32.51 o
9 33 -1 8385.31 8081.72 50.16 o
1 35 -1 3832.10 3784.97 35.50 o
3 35 -1 7700.11 7469.00 39.60 o
5 35 -1 3159.18 3074.68 29.00 o
7 35 -1 1364.30 1367.01 20.39 o
9 35 -1 5110.32 5074.71 60.32 o
1 37 -1 1262.29 1225.64 19.98 o
3 37 -1 382.79 392.17 13.22 o
5 37 -1 6379.71 6191.05 42.44 o
7 37 -1 76.46 100.57 7.13 o
1 39 -1 742.29 789.19 15.15 o
3 39 -1 2457.80 2581.68 28.10 o
5 39 -1 4764.45 4537.67 43.31 o
1 41 -1 256.91 306.19 8.20 o
3 41 -1 2962.62 2738.40 29.40 o
1 43 -1 8715.46 8815.96 58.22 o
4 0 0 34003.12 36095.89 120.66 o
8 0 0 26642.87 29878.67 90.26 o
12 0 0 17031.31 17427.62 109.76 o
2 2 0 7421.17 7371.35 21.40 o
4 2 0 92928.38 95399.48 371.88 o
6 2 0 3997.17 3483.33 25.11 o
8 2 0 76407.05 79444.95 82.03 o
10 2 0 27445.26 27510.28 59.70 o
12 2 0 1685.02 1714.48 22.69 o
14 2 0 6294.85 6648.74 47.62 o
2 4 0 19507.95 19427.82 52.53 o
4 4 0 134079.34 134919.89 567.22 o
6 4 0 254.87 329.81 7.45 o
8 4 0 19087.51 20418.09 43.73 o
10 4 0 820.33 727.57 10.02 o
12 4 0 821.25 700.83 15.34 o
14 4 0 604.55 544.60 14.58 o
2 6 0 3876.89 4011.34 19.78 o
4 6 0 26816.71 25159.73 56.76 o
6 6 0 3362.88 3083.77 21.22 o
8 6 0 150.03 233.90 6.51 o
10 6 0 15970.96 16671.87 49.09 o
12 6 0 30981.01 31980.09 92.57 o
14 6 0 1916.86 1847.14 25.57 o
0 8 0 43376.10 42816.49 122.76 o
2 8 0 55940.99 55030.31 248.65 o
4 8 0 26176.92 25964.68 68.96 o
6 8 0 3596.43 4300.19 26.00 o
8 8 0 12727.23 13655.66 43.54 o
10 8 0 2409.78 2432.42 21.19 o
12 8 0 1787.67 1817.38 21.06 o
14 8 0 160.07 183.00 9.54 o
2 10 0 29354.22 31007.84 72.92 o
4 10 0 21936.03 20897.19 61.79 o
6 10 0 6105.64 6067.11 33.22 o
8 10 0 13340.81 13333.00 48.62 o
10 10 0 967.95 847.64 12.05 o
12 10 0 17438.66 18176.95 82.71 o
14 10 0 1573.85 1747.69 23.17 o
0 12 0 1179.75 2037.84 33.86 o
2 12 0 12538.85 11557.18 42.04 o
4 12 0 7300.54 8463.52 44.74 o
6 12 0 18533.94 18303.82 53.09 o
8 12 0 49.55 72.81 9.87 o
10 12 0 93.21 109.15 6.12 o
12 12 0 675.89 787.60 14.42 o
14 12 0 1411.04 1265.18 20.57 o
2 14 0 5942.65 6467.60 35.36 o
4 14 0 13326.63 12932.56 42.66 o
6 14 0 7420.92 7166.00 29.06 o
8 14 0 22945.07 23715.78 63.10 o
10 14 0 7659.45 7347.67 36.99 o
12 14 0 10329.97 10411.74 52.37 o
14 14 0 7.15 15.68 9.08 <
0 16 0 57393.48 58458.91 330.40 o
2 16 0 2230.41 1870.96 19.34 o
4 16 0 35.23 34.98 4.89 o
6 16 0 23553.38 23551.12 54.61 o
8 16 0 1883.64 1606.79 17.93 o
10 16 0 135.54 127.06 9.69 o
12 16 0 1617.53 1533.65 24.59 o
14 16 0 2635.32 2536.81 35.23 o
2 18 0 36847.00 40029.61 76.75 o
4 18 0 33233.12 33902.61 70.42 o
6 18 0 184.23 216.63 6.82 o
8 18 0 2841.50 2843.30 18.75 o
10 18 0 3184.44 3047.13 27.36 o
12 18 0 4167.15 4347.41 31.99 o
14 18 0 3166.94 3172.42 36.80 o
0 20 0 9880.63 9250.62 42.81 o
2 20 0 7535.19 7491.90 27.63 o
4 20 0 30473.25 30500.89 52.25 o
6 20 0 6.57 17.72 5.68 o
8 20 0 25433.15 24795.49 57.28 o
10 20 0 695.97 729.49 15.06 o
12 20 0 945.46 901.29 16.26 o
14 20 0 319.89 311.47 11.71 o
2 22 0 1.79 31.10 4.28 o
4 22 0 1342.58 1514.98 12.46 o
6 22 0 13793.63 14112.20 40.85 o
8 22 0 14342.44 15702.11 46.96 o
10 22 0 7441.89 7460.42 49.13 o
12 22 0 1.57 14.89 6.67 <
0 24 0 51737.80 53363.39 130.00 o
2 24 0 8.97 44.11 5.42 o
4 24 0 23211.75 21465.23 48.99 o
6 24 0 689.40 741.59 10.96 o
8 24 0 17890.23 18193.69 56.03 o
10 24 0 2184.15 1988.50 23.68 o
12 24 0 2467.40 2321.24 24.45 o
2 26 0 77.60 135.77 5.94 o
4 26 0 1540.31 1360.92 15.81 o
6 26 0 15157.86 15885.22 52.59 o
8 26 0 158.67 164.75 7.41 o
10 26 0 2657.15 2820.59 28.01 o
12 26 0 378.68 384.30 10.22 o
0 28 0 25273.67 24332.73 109.38 o
2 28 0 1195.75 1257.32 15.47 o
4 28 0 36196.48 36296.78 78.56 o
6 28 0 1276.07 1084.71 17.26 o
8 28 0 4190.47 3976.34 26.57 o
10 28 0 3618.05 3586.77 29.69 o
12 28 0 1585.72 1615.68 33.81 o
2 30 0 1031.45 1212.41 15.29 o
4 30 0 2457.98 2563.52 25.23 o
6 30 0 1587.11 1600.41 18.92 o
8 30 0 2934.80 2915.62 24.61 o
10 30 0 4585.70 4463.34 39.54 o
0 32 0 4832.59 4514.94 50.33 o
2 32 0 2384.47 2398.26 23.48 o
4 32 0 28101.32 28229.30 84.60 o
6 32 0 13857.22 14506.25 66.32 o
8 32 0 78.34 95.00 6.78 o
10 32 0 775.05 796.42 20.08 o
2 34 0 10404.68 10850.50 53.18 o
4 34 0 2290.88 2237.75 24.47 o
6 34 0 3054.09 3341.44 31.19 o
8 34 0 3729.27 3834.74 32.16 o
10 34 0 2342.30 2326.72 39.87 o
0 36 0 5395.97 5307.27 52.93 o
2 36 0 14671.91 15412.34 77.87 o
4 36 0 206.07 209.90 8.35 o
6 36 0 20.58 20.44 6.40 o
8 36 0 1062.58 1007.27 22.55 o
2 38 0 1037.28 1141.09 18.87 o
4 38 0 486.51 480.84 13.92 o
6 38 0 196.90 186.44 8.44 o
8 38 0 9849.57 9757.66 82.84 o
0 40 0 283.26 348.97 16.03 o
2 40 0 4546.07 4363.95 40.98 o
4 40 0 1247.30 1272.66 19.43 o
6 40 0 3056.62 3192.67 35.19 o
2 42 0 8.12 35.99 8.14 o
4 42 0 35.67 67.00 7.76 o
0 44 0 8952.58 7671.41 73.83 o
1 1 1 17640.72 16357.11 122.18 o
3 1 1 70062.73 68231.32 568.90 o
5 1 1 11630.19 11593.43 50.87 o
7 1 1 3802.37 3858.24 32.67 o
9 1 1 1330.95 1337.51 19.65 o
11 1 1 25675.78 25894.38 69.91 o
13 1 1 2198.68 2145.12 28.19 o
15 1 1 3694.97 3665.47 41.45 o
1 3 1 24768.95 24038.15 100.81 o
3 3 1 9909.13 9238.29 42.15 o
5 3 1 2223.26 1924.69 20.41 o
7 3 1 29884.39 30128.23 99.45 o
9 3 1 838.58 894.52 12.01 o
11 3 1 12841.29 12566.16 52.77 o
13 3 1 997.77 940.83 19.52 o
15 3 1 3140.82 3153.82 38.25 o
1 5 1 54014.42 53140.74 260.30 o
3 5 1 12315.42 11617.12 48.52 o
5 5 1 16398.99 17307.24 68.94 o
7 5 1 18673.71 19850.44 62.36 o
9 5 1 6452.55 6328.86 30.71 o
11 5 1 4523.65 4598.18 32.11 o
13 5 1 3201.51 3295.50 39.58 o
15 5 1 1545.64 1419.13 25.60 o
1 7 1 48377.42 48116.00 333.90 o
3 7 1 2101.28 1956.26 14.58 o
5 7 1 16484.46 18606.53 51.45 o
7 7 1 4133.17 4391.34 23.36 o
9 7 1 3782.16 3783.04 22.71 o
11 7 1 3409.77 3396.84 30.52 o
13 7 1 1605.92 1689.26 28.54 o
15 7 1 1946.57 1911.99 23.58 o
1 9 1 6304.43 5621.53 41.76 o
3 9 1 24313.21 25366.87 49.73 o
5 9 1 8000.15 8537.12 34.67 o
7 9 1 5146.05 5374.71 26.76 o
9 9 1 17386.52 17438.72 48.92 o
11 9 1 6018.48 6112.12 37.58 o
13 9 1 2195.28 2306.26 29.05 o
15 9 1 502.99 509.82 12.43 o
1 11 1 19817.41 18676.26 54.29 o
3 11 1 5486.32 6156.65 31.53 o
5 11 1 5815.53 6104.35 40.02 o
7 11 1 5673.52 6339.18 32.36 o
9 11 1 6361.19 6481.68 30.71 o
11 11 1 1248.87 1168.82 17.04 o
13 11 1 224.47 212.86 10.59 o
15 11 1 2999.72 3101.48 34.73 o
1 13 1 2065.29 1852.34 19.16 o
3 13 1 8445.03 9195.14 42.06 o
5 13 1 7041.34 7375.35 33.13 o
7 13 1 806.64 763.14 11.99 o
9 13 1 8932.18 9225.94 41.93 o
11 13 1 2041.79 2098.41 21.76 o
13 13 1 1366.58 1335.30 21.80 o
1 15 1 37159.77 38591.42 78.07 o
3 15 1 3584.01 3389.39 24.97 o
5 15 1 12564.92 12895.12 41.59 o
7 15 1 1042.32 1145.17 13.10 o
9 15 1 6352.69 6375.35 31.10 o
11 15 1 2916.68 2820.12 29.75 o
13 15 1 222.33 206.72 9.65 o
1 17 1 1002.32 958.08 12.79 o
3 17 1 8008.29 8235.38 32.35 o
5 17 1 19748.21 20720.82 52.90 o
7 17 1 1206.19 1264.26 13.26 o
9 17 1 803.86 800.57 11.99 o
11 17 1 6567.34 6549.12 44.30 o
13 17 1 3272.40 3241.29 36.48 o
1 19 1 10092.65 9699.54 35.33 o
3 19 1 15700.93 16480.29 44.11 o
5 19 1 7161.44 6791.44 30.34 o
7 19 1 14009.51 14238.21 44.11 o
9 19 1 3032.82 3214.63 24.87 o
11 19 1 275.94 254.55 9.63 o
13 19 1 2640.14 2734.35 31.88 o
1 21 1 3888.02 3995.02 22.62 o
3 21 1 9687.41 9060.90 32.57 o
5 21 1 7812.95 7891.45 34.22 o
7 21 1 12032.43 12431.69 43.49 o
9 21 1 3241.11 3487.42 24.97 o
11 21 1 2162.42 2114.47 27.39 o
13 21 1 110.43 117.13 8.25 o
1 23 1 16974.72 17972.86 46.51 o
3 23 1 19798.65 19732.53 47.35 o
5 23 1 5951.09 6324.76 32.03 o
7 23 1 10577.73 10374.17 44.04 o
9 23 1 3365.79 3301.40 26.85 o
11 23 1 3441.36 3327.03 32.56 o
1 25 1 70.60 84.81 5.15 o
3 25 1 25708.94 26395.51 60.07 o
5 25 1 1875.03 1723.02 21.41 o
7 25 1 2494.19 2426.15 21.01 o
9 25 1 2907.67 2918.91 25.33 o
11 25 1 4877.86 4811.08 44.12 o
1 27 1 4167.91 3845.63 23.75 o
3 27 1 5806.75 5741.23 31.79 o
5 27 1 9553.48 10139.98 46.64 o
7 27 1 11379.23 12202.76 46.26 o
9 27 1 236.74 232.81 8.75 o
11 27 1 2032.72 1997.69 26.78 o
1 29 1 7573.35 7790.30 36.60 o
3 29 1 3452.66 3481.88 25.65 o
5 29 1 9757.55 9740.93 46.00 o
7 29 1 7718.09 8325.49 46.41 o
9 29 1 1466.78 1446.52 21.55 o
11 29 1 2271.40 2410.46 34.56 o
1 31 1 15164.25 15122.93 56.29 o
3 31 1 133.75 156.60 6.86 o
5 31 1 2183.46 2224.11 24.45 o
7 31 1 4281.06 4361.58 33.98 o
9 31 1 752.39 818.05 15.08 o
11 31 1 1521.28 1415.77 33.09 o
1 33 1 9863.91 9773.91 44.26 o
3 33 1 2248.03 2129.71 22.76 o
5 33 1 2255.85 2547.58 27.71 o
7 33 1 3939.60 4125.09 31.30 o
9 33 1 8278.87 8193.56 51.23 o
1 35 1 3263.28 3223.42 25.17 o
3 35 1 7893.23 7690.53 49.61 o
5 35 1 3840.71 3772.74 33.81 o
7 35 1 1420.24 1519.31 19.98 o
9 35 1 4649.92 4641.69 61.18 o
1 37 1 1204.71 1205.48 17.88 o
3 37 1 280.30 314.17 12.15 o
5 37 1 5964.55 5747.77 38.34 o
7 37 1 89.90 101.87 7.81 o
1 39 1 698.05 710.38 13.09 o
3 39 1 2431.73 2609.64 28.98 o
5 39 1 4380.88 4587.15 42.27 o
7 39 1 1253.70 1271.75 31.06 o
1 41 1 282.29 350.11 10.59 o
3 41 1 2690.46 2625.67 26.21 o
5 41 1 216.11 236.80 10.74 o
3 43 1 410.58 359.23 17.17 o
2 0 2 40722.10 40211.21 186.68 o
6 0 2 6491.28 6530.11 57.43 o
10 0 2 7448.68 7311.12 56.39 o
14 0 2 3408.30 3154.84 59.39 o
0 2 2 70435.71 66148.28 356.98 o
2 2 2 7447.94 6907.69 23.64 o
4 2 2 2811.26 2339.61 18.52 o
6 2 2 5782.59 5776.84 38.10 o
8 2 2 9444.55 9565.74 39.20 o
10 2 2 1751.76 1801.51 18.88 o
12 2 2 1654.19 1578.01 25.40 o
14 2 2 324.33 274.60 13.90 o
2 4 2 2210.02 1974.93 11.26 o
4 4 2 347.80 412.45 7.76 o
6 4 2 3120.60 3213.04 25.80 o
8 4 2 1762.47 1585.10 16.88 o
10 4 2 7274.62 7209.80 34.71 o
12 4 2 2756.01 2657.16 32.07 o
14 4 2 1627.41 1591.09 30.07 o
0 6 2 29404.61 27701.70 72.72 o
2 6 2 12214.65 11519.91 28.54 o
4 6 2 4709.72 4420.96 20.05 o
6 6 2 11469.36 12525.27 42.72 o
8 6 2 3873.99 3900.33 28.13 o
10 6 2 1157.54 1178.72 16.17 o
12 6 2 2474.42 2538.01 27.84 o
14 6 2 1214.84 1175.75 25.48 o
2 8 2 19267.42 20194.42 37.77 o
4 8 2 4802.78 5219.45 25.14 o
6 8 2 149.36 163.02 6.91 o
8 8 2 5849.60 5626.25 34.32 o
10 8 2 840.23 929.85 12.91 o
12 8 2 8259.07 7945.62 46.98 o
14 8 2 1646.98 1664.49 29.39 o
0 10 2 28953.76 29527.54 108.55 o
2 10 2 4597.29 4367.65 22.40 o
4 10 2 11958.60 11509.37 40.19 o
6 10 2 10400.51 10741.35 43.91 o
8 10 2 3543.71 3556.27 24.18 o
10 10 2 1685.69 1719.18 16.88 o
12 10 2 240.26 262.63 10.39 o
14 10 2 250.20 241.84 11.51 o
2 12 2 13065.38 13884.64 38.03 o
4 12 2 8599.81 8043.78 36.45 o
6 12 2 8332.71 8357.14 36.92 o
8 12 2 115.28 123.23 6.21 o
10 12 2 1850.88 1752.94 17.12 o
12 12 2 4905.18 5095.86 44.42 o
14 12 2 558.18 466.13 11.93 o
0 14 2 17634.78 17893.28 76.34 o
2 14 2 2876.48 2747.67 18.85 o
4 14 2 8799.57 8894.60 34.37 o
6 14 2 9245.34 9353.09 37.96 o
8 14 2 910.40 868.49 13.28 o
10 14 2 2343.36 2405.71 20.64 o
12 14 2 302.68 290.15 9.58 o
14 14 2 3219.56 3104.43 46.49 o
2 16 2 4501.92 4592.54 26.99 o
4 16 2 8774.93 8841.57 33.77 o
6 16 2 427.86 466.07 9.95 o
8 16 2 687.34 776.97 14.18 o
10 16 2 5584.05 5468.68 33.08 o
12 16 2 608.75 576.21 12.52 o
0 18 2 2302.14 2131.01 25.74 o
2 18 2 7223.28 7520.91 33.25 o
4 18 2 7986.97 7364.04 32.45 o
6 18 2 2955.23 2837.01 23.17 o
8 18 2 8628.34 8767.83 46.92 o
10 18 2 6784.48 7080.33 37.32 o
12 18 2 215.96 233.65 7.92 o
2 20 2 8826.57 9610.62 37.13 o
4 20 2 307.93 348.83 8.29 o
6 20 2 6508.87 6614.78 34.50 o
8 20 2 3318.36 3388.70 30.33 o
10 20 2 1577.65 1650.19 22.36 o
12 20 2 609.74 556.63 12.54 o
0 22 2 15054.21 14222.57 61.51 o
2 22 2 1856.94 2056.40 18.52 o
4 22 2 5632.55 5431.27 29.35 o
6 22 2 1799.42 1989.30 19.12 o
8 22 2 11513.66 11428.45 55.04 o
10 22 2 895.41 812.35 18.67 o
12 22 2 1043.15 974.61 34.53 o
2 24 2 6474.78 6755.13 36.62 o
4 24 2 892.15 940.01 14.00 o
6 24 2 3366.95 3499.78 25.26 o
8 24 2 44.55 52.83 6.91 o
10 24 2 786.24 783.46 15.32 o
0 26 2 10540.88 10367.98 56.19 o
2 26 2 214.84 226.94 7.85 o
4 26 2 11226.01 10764.37 44.66 o
6 26 2 13514.64 14086.57 51.84 o
8 26 2 6243.26 6182.13 44.30 o
10 26 2 150.84 136.77 8.68 o
2 28 2 10348.03 10504.91 43.52 o
4 28 2 1685.47 1708.86 17.74 o
6 28 2 2246.29 2392.42 25.81 o
8 28 2 4325.82 4644.73 32.25 o
10 28 2 4953.63 5145.67 38.67 o
0 30 2 643.93 680.32 16.15 o
2 30 2 7929.04 8247.30 38.72 o
4 30 2 15138.38 15656.25 50.49 o
6 30 2 640.61 673.33 13.11 o
8 30 2 31.99 49.94 6.67 o
10 30 2 6489.34 6188.94 43.41 o
2 32 2 3674.37 3770.28 26.08 o
4 32 2 6003.60 6264.97 36.04 o
6 32 2 1117.19 1124.38 17.59 o
8 32 2 1.19 21.27 7.46 <
10 32 2 547.42 585.16 21.42 o
0 34 2 7557.44 7116.41 45.66 o
2 34 2 3067.12 3211.62 25.11 o
4 34 2 1344.20 1324.55 18.64 o
6 34 2 11301.73 11230.07 54.05 o
8 34 2 352.85 358.15 11.14 o
2 36 2 7194.82 6946.02 44.00 o
4 36 2 1276.50 1218.38 21.38 o
6 36 2 464.18 427.33 10.61 o
8 36 2 7599.48 7318.26 69.04 o
0 38 2 2805.90 2635.68 32.34 o
2 38 2 5363.65 5342.36 40.74 o
4 38 2 1192.80 1295.90 19.85 o
6 38 2 1346.85 1367.78 23.33 o
2 40 2 518.88 588.85 18.72 o
4 40 2 16.40 30.38 11.54 <
1 1 3 12553.56 12285.35 32.33 o
3 1 3 17250.42 16651.81 47.22 o
5 1 3 2658.52 2672.44 17.13 o
7 1 3 1554.00 1602.43 15.77 o
9 1 3 2448.39 2420.87 23.39 o
11 1 3 9036.05 8807.48 61.13 o
13 1 3 2071.68 1857.73 21.13 o
1 3 3 12553.78 12004.00 28.42 o
3 3 3 11265.13 10736.96 30.59 o
5 3 3 11961.85 12111.16 34.41 o
7 3 3 12864.47 12742.22 40.79 o
9 3 3 3054.28 2934.04 25.92 o
11 3 3 5708.81 5877.58 43.07 o
13 3 3 2065.93 2093.20 26.56 o
1 5 3 35655.07 36674.51 53.21 o
3 5 3 2359.90 2494.52 14.11 o
5 5 3 4415.63 4579.66 21.72 o
7 5 3 6596.69 6547.59 31.88 o
9 5 3 479.95 483.31 11.22 o
11 5 3 1979.94 1979.21 25.75 o
13 5 3 3113.20 3049.13 31.19 o
1 7 3 17760.08 17153.23 41.15 o
3 7 3 34822.48 33406.24 51.30 o
5 7 3 262.45 263.54 5.94 o
7 7 3 2395.24 2354.42 21.73 o
9 7 3 9833.86 9906.07 46.19 o
11 7 3 6618.58 6738.75 46.33 o
13 7 3 2846.73 2771.57 29.51 o
1 9 3 84.94 61.87 3.53 o
3 9 3 6688.66 6769.73 27.75 o
5 9 3 9292.01 9165.07 34.37 o
7 9 3 3904.25 3661.18 30.47 o
9 9 3 8520.08 8252.37 42.83 o
11 9 3 2492.08 2452.92 28.25 o
13 9 3 4095.92 4037.65 34.22 o
1 11 3 1666.43 1917.88 14.58 o
3 11 3 11421.21 11215.24 38.81 o
5 11 3 28550.67 28600.95 62.29 o
7 11 3 6556.65 6510.09 41.43 o
9 11 3 4363.98 4535.33 30.28 o
11 11 3 1833.69 1897.73 24.57 o
13 11 3 1597.05 1539.86 20.54 o
1 13 3 18528.10 18793.71 46.84 o
3 13 3 6847.64 7069.17 30.56 o
5 13 3 3028.03 2781.71 19.84 o
7 13 3 1640.42 1827.46 19.91 o
9 13 3 7442.69 7769.83 44.53 o
11 13 3 4045.79 3954.18 31.84 o
13 13 3 1283.77 1213.79 33.56 o
1 15 3 20416.37 21231.26 51.96 o
3 15 3 7114.35 7614.39 35.70 o
5 15 3 5014.88 4970.07 27.12 o
7 15 3 4307.61 4341.03 30.85 o
9 15 3 6164.81 6176.36 42.75 o
11 15 3 452.36 466.56 13.88 o
13 15 3 2011.26 1974.71 39.58 o
1 17 3 3153.21 2916.89 22.55 o
3 17 3 1971.42 1936.67 19.36 o
5 17 3 17371.04 17395.38 51.55 o
7 17 3 16725.11 17279.95 66.10 o
9 17 3 3244.54 3087.28 28.91 o
11 17 3 54.06 87.75 8.20 o
1 19 3 339.20 399.60 8.99 o
3 19 3 8083.62 8176.91 39.85 o
5 19 3 8773.85 9017.98 40.00 o
7 19 3 1739.49 1703.32 24.39 o
9 19 3 371.54 375.29 11.31 o
11 19 3 1201.75 1233.44 22.22 o
1 21 3 8523.28 8393.60 38.10 o
3 21 3 5081.80 4925.69 32.12 o
5 21 3 2366.74 2333.04 21.34 o
7 21 3 9449.10 9574.49 49.88 o
9 21 3 2917.53 2998.27 28.37 o
11 21 3 6907.91 6812.91 42.34 o
1 23 3 260.42 253.46 8.09 o
3 23 3 22691.00 23083.64 65.43 o
5 23 3 1797.74 1836.43 18.48 o
7 23 3 1312.88 1288.14 17.72 o
9 23 3 285.17 316.16 9.89 o
11 23 3 2265.31 2221.46 22.78 o
1 25 3 3252.66 3096.45 26.55 o
3 25 3 10559.93 11003.83 46.01 o
5 25 3 1740.54 1698.18 17.80 o
7 25 3 8539.98 8519.19 42.29 o
9 25 3 428.63 467.58 14.08 o
1 27 3 3106.83 3155.72 26.84 o
3 27 3 3559.41 3588.91 28.81 o
5 27 3 12475.73 13076.66 48.88 o
7 27 3 10419.50 10595.56 46.40 o
9 27 3 2215.45 2192.94 23.71 o
1 29 3 7558.55 7721.24 46.20 o
3 29 3 1189.59 1162.40 18.86 o
5 29 3 91.99 86.17 6.27 o
7 29 3 7278.66 7560.67 40.97 o
9 29 3 2659.72 2656.92 29.23 o
1 31 3 12368.48 12274.17 56.15 o
3 31 3 3823.19 4085.07 29.07 o
5 31 3 3653.22 3943.07 33.97 o
7 31 3 1044.70 1041.06 14.53 o
1 33 3 869.41 828.93 14.92 o
3 33 3 1081.50 1018.15 17.97 o
5 33 3 3030.23 3395.54 33.53 o
7 33 3 921.09 910.29 23.56 o
1 35 3 5084.86 5494.71 42.71 o
3 35 3 6299.48 6316.14 44.69 o
5 35 3 3400.20 3420.91 36.25 o
1 37 3 4666.15 5115.55 56.68 o
3 37 3 873.57 828.88 28.38 o
0 0 4 67599.25 66931.80 277.14 o
4 0 4 11742.19 11470.45 58.66 o
8 0 4 136.66 153.55 10.37 o
12 0 4 4603.93 4436.86 63.04 o
2 2 4 1437.24 1468.59 14.79 o
4 2 4 6088.02 6543.61 31.48 o
6 2 4 20789.68 20587.60 58.30 o
8 2 4 7444.50 7847.90 40.26 o
10 2 4 9017.41 8998.56 63.05 o
12 2 4 261.84 262.14 8.84 o
0 4 4 5154.67 4780.53 36.96 o
2 4 4 11591.64 11274.43 43.07 o
4 4 4 19677.67 19785.97 59.32 o
6 4 4 4169.79 4171.84 26.94 o
8 4 4 2276.37 2361.86 24.51 o
10 4 4 1556.55 1561.25 23.24 o
12 4 4 312.94 306.66 9.47 o
2 6 4 3383.05 3278.82 21.96 o
4 6 4 391.14 446.24 10.09 o
6 6 4 2905.27 2912.20 24.76 o
8 6 4 7334.04 7663.53 48.58 o
10 6 4 7781.44 7944.25 49.88 o
12 6 4 4016.22 3890.45 34.55 o
0 8 4 1299.76 1202.40 22.26 o
2 8 4 27348.50 26994.73 62.62 o
4 8 4 5855.77 5939.48 33.17 o
6 8 4 14165.82 14352.77 64.38 o
8 8 4 1192.60 1235.94 22.87 o
10 8 4 489.63 543.62 14.78 o
12 8 4 568.13 556.98 13.72 o
2 10 4 2712.32 2584.58 19.01 o
4 10 4 3507.22 3608.08 26.65 o
6 10 4 2058.09 2185.34 26.84 o
8 10 4 9545.30 9793.62 55.05 o
10 10 4 1781.01 1807.41 25.51 o
12 10 4 5302.30 5229.08 38.22 o
0 12 4 535.40 570.04 13.15 o
2 12 4 30643.47 30598.08 59.63 o
4 12 4 155.98 166.09 6.58 o
6 12 4 19211.78 19975.50 72.61 o
8 12 4 1646.70 1604.40 23.26 o
10 12 4 2697.31 2746.37 30.33 o
12 12 4 212.78 217.31 10.00 o
2 14 4 2228.93 2312.60 18.56 o
4 14 4 6014.12 6228.93 30.85 o
6 14 4 510.46 462.56 12.54 o
8 14 4 6198.30 6044.27 43.75 o
10 14 4 1124.31 1063.49 18.30 o
12 14 4 9688.86 9998.99 83.23 o
0 16 4 14340.94 14067.53 72.61 o
2 16 4 20391.59 20237.52 54.46 o
4 16 4 17569.26 17959.85 56.19 o
6 16 4 21047.80 21132.57 71.53 o
8 16 4 1876.65 1968.62 28.55 o
10 16 4 3564.74 3692.13 35.68 o
2 18 4 4510.06 4352.16 26.19 o
4 18 4 8798.81 8710.40 40.01 o
6 18 4 5920.65 5975.81 42.06 o
8 18 4 9743.73 10236.71 61.60 o
10 18 4 624.11 591.52 14.80 o
0 20 4 14531.82 15429.36 80.37 o
2 20 4 13901.36 13821.78 49.55 o
4 20 4 12283.19 12276.23 47.39 o
6 20 4 1714.80 1667.18 22.80 o
8 20 4 3824.48 3759.17 34.17 o
10 20 4 3322.48 3390.54 31.01 o
2 22 4 190.35 205.30 7.81 o
4 22 4 4470.14 4757.35 30.47 o
6 22 4 7925.12 8014.90 46.60 o
8 22 4 5438.21 5372.60 43.59 o
10 22 4 6221.15 6099.83 71.13 o
0 24 4 19265.32 18711.51 124.96 o
2 24 4 1050.61 1004.05 15.60 o
4 24 4 5068.34 5215.01 31.24 o
6 24 4 179.45 187.71 8.66 o
8 24 4 6426.20 6391.12 53.30 o
10 24 4 1063.65 928.88 26.77 o
2 26 4 1079.59 1086.99 15.89 o
4 26 4 305.45 317.89 10.44 o
6 26 4 5854.77 5957.69 36.53 o
8 26 4 2679.14 2654.19 32.67 o
0 28 4 9887.20 10459.54 123.44 o
2 28 4 1794.94 1950.60 22.90 o
4 28 4 9892.20 10390.13 49.81 o
6 28 4 1174.19 1237.72 23.58 o
8 28 4 1172.76 1097.15 30.10 o
2 30 4 7369.44 8079.42 48.18 o
4 30 4 4234.05 4440.42 38.52 o
6 30 4 241.23 263.88 13.75 o
2 32 4 4838.57 5270.32 48.00 o
4 32 4 229.73 183.51 10.20 o
6 32 4 7266.09 6848.47 70.82 o
2 34 4 386.91 460.79 17.39 o
1 1 5 5895.22 5831.53 50.33 o
3 1 5 494.91 610.11 12.67 o
5 1 5 964.56 1030.82 15.12 o
7 1 5 7846.39 8174.58 43.93 o
9 1 5 4443.42 4424.04 36.20 o
11 1 5 3857.28 3836.08 58.41 o
1 3 5 3145.11 3026.27 36.77 o
3 3 5 16189.54 16292.95 59.65 o
5 3 5 691.02 699.97 12.32 o
7 3 5 1834.81 1745.80 21.22 o
9 3 5 2214.54 2152.27 30.45 o
11 3 5 12.35 28.31 8.05 o
1 5 5 361.84 373.37 12.91 o
3 5 5 707.81 655.05 11.90 o
5 5 5 13646.19 14299.93 51.90 o
7 5 5 3393.34 3573.55 29.67 o
9 5 5 399.13 410.10 12.63 o
11 5 5 1682.18 1735.37 26.78 o
1 7 5 5992.14 6281.37 38.11 o
3 7 5 9156.52 9329.13 39.43 o
5 7 5 12547.51 12825.31 61.64 o
7 7 5 917.24 913.35 17.01 o
9 7 5 337.44 370.35 10.74 o
11 7 5 1764.56 1820.55 26.78 o
1 9 5 279.37 302.74 8.22 o
3 9 5 8787.42 9141.06 39.08 o
5 9 5 4458.63 4602.68 37.35 o
7 9 5 3832.77 3799.39 34.30 o
9 9 5 7567.45 7240.12 54.06 o
11 9 5 268.67 279.12 10.72 o
1 11 5 12931.43 13157.38 48.27 o
3 11 5 330.00 368.09 10.28 o
5 11 5 6236.35 6459.26 40.80 o
7 11 5 621.00 633.35 14.60 o
9 11 5 1085.39 1119.93 21.69 o
1 13 5 2886.01 2830.05 22.86 o
3 13 5 5555.04 5858.13 36.25 o
5 13 5 4030.91 3922.76 35.62 o
7 13 5 3740.48 3731.23 32.99 o
9 13 5 8540.40 9397.87 71.86 o
1 15 5 9782.61 10312.24 49.61 o
3 15 5 7264.90 7426.30 40.46 o
5 15 5 8010.75 8189.85 57.07 o
7 15 5 796.19 747.81 15.52 o
9 15 5 3685.76 3747.66 32.83 o
1 17 5 3817.80 3752.72 30.18 o
3 17 5 217.54 232.77 9.23 o
5 17 5 9147.19 9232.04 52.32 o
7 17 5 6193.07 6305.48 45.31 o
9 17 5 220.35 194.94 10.94 o
1 19 5 5663.73 5779.85 36.81 o
3 19 5 9254.70 9362.66 54.27 o
5 19 5 2234.49 2140.25 25.26 o
7 19 5 5329.78 5337.68 37.02 o
9 19 5 1794.23 1953.06 39.98 o
1 21 5 3574.34 3693.31 31.64 o
3 21 5 2272.37 2242.22 22.59 o
5 21 5 850.92 790.93 15.87 o
7 21 5 5098.46 4772.85 37.23 o
1 23 5 2555.03 2354.51 27.31 o
3 23 5 1514.20 1517.08 19.87 o
5 23 5 232.51 224.81 9.85 o
7 23 5 1536.45 1386.11 34.49 o
1 25 5 1601.46 1686.84 25.34 o
3 25 5 6289.72 6257.65 46.09 o
5 25 5 1194.15 1216.38 19.02 o
7 25 5 1559.79 1512.01 35.06 o
1 27 5 175.88 171.97 14.12 o
3 27 5 1569.35 1624.77 32.20 o
1 29 5 2265.81 2306.29 37.25 o
2 0 6 1663.12 1745.52 39.90 o
6 0 6 1775.34 1844.70 33.20 o
0 2 6 1181.23 1349.26 24.36 o
2 2 6 865.05 954.90 21.37 o
4 2 6 1854.73 2084.02 28.97 o
6 2 6 3260.35 3172.92 27.67 o
8 2 6 1472.62 1355.22 24.68 o
2 4 6 6603.18 6593.64 47.31 o
4 4 6 1898.00 1876.99 24.90 o
6 4 6 4420.84 4502.65 30.61 o
8 4 6 1580.95 1503.70 25.64 o
0 6 6 2136.98 2164.61 35.55 o
2 6 6 6674.95 7092.96 48.36 o
4 6 6 1781.20 1977.42 28.80 o
6 6 6 3133.13 3179.11 25.57 o
8 6 6 110.07 89.78 8.49 o
2 8 6 5190.70 5303.79 41.31 o
4 8 6 143.94 125.06 9.34 o
6 8 6 98.05 109.37 7.87 o
8 8 6 3151.02 3036.31 48.30 o
0 10 6 1224.71 1134.79 25.44 o
2 10 6 4383.02 4705.77 34.78 o
4 10 6 1194.83 1218.48 22.08 o
6 10 6 9532.74 9525.03 46.72 o
2 12 6 335.97 333.30 11.23 o
4 12 6 1804.13 1801.01 25.69 o
6 12 6 492.06 557.87 11.90 o
0 14 6 1443.77 1478.51 27.40 o
2 14 6 5941.52 6372.26 42.37 o
4 14 6 3922.49 4281.08 45.16 o
6 14 6 5108.00 4860.15 62.74 o
2 16 6 628.17 750.99 15.06 o
4 16 6 882.43 1067.24 22.31 o
6 16 6 738.77 666.87 23.58 o
0 18 6 392.02 509.56 27.54 o
2 18 6 3215.47 3447.13 38.21 o
4 18 6 3181.54 3469.30 46.45 o