# Electronic Supplementary Material (ESI) for CrystEngComm # This journal is © The Royal Society of Chemistry 2013 ####################################################################### # # Cambridge Crystallographic Data Centre # CCDC # ####################################################################### # # This CIF contains data from an original supplementary publication # deposited with the CCDC, and may include chemical, crystal, # experimental, refinement, atomic coordinates, # anisotropic displacement parameters and molecular geometry data, # as required by the journal to which it was submitted. # # This CIF is provided on the understanding that it is used for bona # fide research purposes only. It may contain copyright material # of the CCDC or of third parties, and may not be copied or further # disseminated in any form, whether machine-readable or not, # except for the purpose of generating routine backup copies # on your local computer system. # # For further information on the CCDC, data deposition and # data retrieval see: # www.ccdc.cam.ac.uk # # Bona fide researchers may freely download Mercury and enCIFer # from this site to visualise CIF-encoded structures and # to carry out CIF format checking respectively. # data_1 _exptl_special_details ; The crystal was placed in the cold stream of an Oxford Cryosystems open-flow nitrogen cryostat (Cosier & Glazer, 1986) with a nominal stability of 0.1K. Cosier, J. & Glazer, A.M., 1986. J. Appl. Cryst. 105-107. ; _refine_special_details ; ? ; #--------------------------------------------------------------- # _oxford_ data items, April 2010: # There is some uncertainty about the correct way of forming local data # names, e.g. # _atom_site_special_shape_oxford # or # _oxford_atom_site_special_shape # see: # http://www.iucr.org/resources/cif/spec/version1.1/semantics#namespace # A reserved prefix, e.g. foo, must be used in the following way # " If the data file contains items defined in a DDL1 dictionary, the # local data names assigned under the reserved prefix must contain it as # their first component, e.g. _foo_atom_site_my_item. " # However, this seems to say the opposite: # http://www.iucr.org/__data/iucr/cif/standard/cifstd8.html # According to advice from the IUCr, CRYSTALS is correct #--------------------------------------------------------------- # End of 'script/refcif.dat' #end of refcif _cell_length_a 7.5755(4) _cell_length_b 7.3774(4) _cell_length_c 12.0168(6) _cell_angle_alpha 90 _cell_angle_beta 102.173(3) _cell_angle_gamma 90 _cell_volume 656.49(6) _symmetry_cell_setting monoclinic _symmetry_space_group_name_H-M 'C 1 2/c 1 ' _symmetry_space_group_name_Hall ? loop_ _symmetry_equiv_pos_as_xyz x,y,z -x,-y,-z x+1/2,y+1/2,z -x+1/2,-y+1/2,-z -x,y,-z+1/2 x,-y,z+1/2 -x+1/2,y+1/2,-z+1/2 x+1/2,-y+1/2,z+1/2 loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_Cromer_Mann_a1 _atom_type_scat_Cromer_Mann_b1 _atom_type_scat_Cromer_Mann_a2 _atom_type_scat_Cromer_Mann_b2 _atom_type_scat_Cromer_Mann_a3 _atom_type_scat_Cromer_Mann_b3 _atom_type_scat_Cromer_Mann_a4 _atom_type_scat_Cromer_Mann_b4 _atom_type_scat_Cromer_Mann_c _atom_type_scat_source C 0.0033 0.0016 2.3100 20.8439 1.0200 10.2075 1.5886 0.5687 0.8650 51.6512 0.2156 'International Tables Vol C 4.2.6.8 and 6.1.1.4' H 0.0000 0.0000 0.4930 10.5109 0.3229 26.1257 0.1402 3.1424 0.0408 57.7998 0.0030 'International Tables Vol C 4.2.6.8 and 6.1.1.4' O 0.0106 0.0060 3.0485 13.2771 2.2868 5.7011 1.5463 0.3239 0.8670 32.9089 0.2508 'International Tables Vol C 4.2.6.8 and 6.1.1.4' Br -0.2901 2.4595 17.1789 2.1723 5.2358 16.5796 5.6377 0.2609 3.9851 41.4328 2.9557 'International Tables Vol C 4.2.6.8 and 6.1.1.4' Cd -0.8075 1.2024 19.2214 0.5946 17.6444 6.9089 4.4610 24.7008 1.6029 87.4825 5.0694 'International Tables Vol C 4.2.6.8 and 6.1.1.4' _cell_formula_units_Z 4 # Given Formula = C3 H6 Br1 O1 # Dc = 2.79 Fooo = 408.00 Mu = 122.72 M = 137.98 # Found Formula = C1.50 H3 Br1 O0.50 # Dc = 2.20 FOOO = 408.00 Mu = 122.29 M = 108.94 _chemical_formula_sum 'C3 D6 Br2 O1' _chemical_formula_moiety 'C3 D6 Br2 O1' _chemical_compound_source ? _chemical_formula_weight 223.92 _cell_measurement_reflns_used 0 _cell_measurement_theta_min 0 _cell_measurement_theta_max 0 _cell_measurement_temperature 110 _exptl_crystal_description block _exptl_crystal_colour orange _exptl_crystal_size_min 0.130 _exptl_crystal_size_mid 0.170 _exptl_crystal_size_max 0.370 _exptl_crystal_density_diffrn 2.266 _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' # Non-dispersive F(000): _exptl_crystal_F_000 408 _exptl_absorpt_coefficient_mu 12.229 # Sheldrick geometric approximatio 0.13 0.21 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS 2007/2 (Sheldrick, G.M., 2007)' _exptl_absorpt_correction_T_min 0.1251 _exptl_absorpt_correction_T_max 0.2040 _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_source 'Bruker-Nonius FR591 rotating anode' _diffrn_radiation_monochromator '10cm confocal mirrors' _diffrn_measurement_device_type 'Bruker-Nonius APEX II CCD camera on \k-goniostat' _diffrn_measurement_method '\f & \w scans' _diffrn_detector_area_resol_mean '4096x4096pixels / 62x62mm' # If a reference occurs more than once, delete the author # and date from subsequent references. _computing_data_collection 'USER DEFINED DATA COLLECTION' _computing_cell_refinement 'USER DEFINED CELL REFINEMENT' _computing_data_reduction 'USER DEFINED DATA REDUCTION' _computing_structure_solution 'SHELXS 86 (Sheldrick, 1986)' _computing_structure_refinement 'CRYSTALS (Betteridge et al., 2003)' _computing_publication_material 'CRYSTALS (Betteridge et al., 2003)' _computing_molecular_graphics 'CAMERON (Watkin et al., 1996)' _diffrn_standards_number 0 _diffrn_standards_decay_% ? _diffrn_ambient_temperature 110 _diffrn_reflns_number 3227 _reflns_number_total 748 _diffrn_reflns_av_R_equivalents 0.054 # Number of reflections without Friedels Law is 0 # Number of reflections with Friedels Law is 748 # Theoretical number of reflections is about 1512 _diffrn_reflns_theta_min 3.469 _diffrn_reflns_theta_max 27.522 _diffrn_measured_fraction_theta_max 0.993 _diffrn_reflns_theta_full 26.972 _diffrn_measured_fraction_theta_full 0.996 _diffrn_reflns_limit_h_min -8 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_k_min -9 _diffrn_reflns_limit_k_max 9 _diffrn_reflns_limit_l_min -15 _diffrn_reflns_limit_l_max 14 _reflns_limit_h_min -9 _reflns_limit_h_max 9 _reflns_limit_k_min 0 _reflns_limit_k_max 9 _reflns_limit_l_min 0 _reflns_limit_l_max 15 _oxford_diffrn_Wilson_B_factor 1.67 _oxford_diffrn_Wilson_scale 5.18 _atom_sites_solution_primary direct #heavy,direct,difmap,geom # _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens difmap _refine_diff_density_min -1.32 _refine_diff_density_max 0.55 # The current dictionary definitions do not cover the # situation where the reflections used for refinement were # selected by a user-defined sigma threshold # The values actually used during refinement _oxford_reflns_threshold_expression_ref I>3.0\s(I) _refine_ls_number_reflns 668 _refine_ls_number_restraints 12 _refine_ls_number_parameters 39 _oxford_refine_ls_R_factor_ref 0.0301 _refine_ls_wR_factor_ref 0.0726 _refine_ls_goodness_of_fit_ref 1.0035 _refine_ls_shift/su_max 0.0009737 _refine_ls_shift/su_mean 0.0000947 # The values computed with all filters except I/sigma _oxford_reflns_number_all 748 _refine_ls_R_factor_all 0.0353 _refine_ls_wR_factor_all 0.0788 # The values computed with a 2 sigma cutoff - a la SHELX _reflns_threshold_expression I>2.0\s(I) _reflns_number_gt 681 _refine_ls_R_factor_gt 0.0309 _refine_ls_wR_factor_gt 0.0743 # choose from: rm (reference molecule of known chirality), # ad (anomolous dispersion - Flack), rmad (rm and ad), # syn (from synthesis), unk (unknown) or . (not applicable). _chemical_absolute_configuration . _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_hydrogen_treatment mixed #undef, noref, refall, # refxyz, refU, constr or mixed _refine_ls_weighting_scheme calc _refine_ls_weighting_details ; Method, part 1, Chebychev polynomial, (Watkin, 1994, Prince, 1982) [weight] = 1.0/[A~0~*T~0~(x)+A~1~*T~1~(x) ... +A~n-1~]*T~n-1~(x)] where A~i~ are the Chebychev coefficients listed below and x= Fcalc/Fmax Method = Robust Weighting (Prince, 1982) W = [weight] * [1-(deltaF/6*sigmaF)^2^]^2^ A~i~ are: 40.9 43.4 30.5 ; # Uequiv = arithmetic mean of Ui i.e. Ueqiv = (U1+U2+U3)/3 # Replace last . with number of unfound hydrogen atoms attached to an atom. # ..._refinement_flags_... # . no refinement constraints S special position constraint on site # G rigid group refinement of site R riding atom # D distance or angle restraint on site T thermal displacement constraints # U Uiso or Uij restraint (rigid bond) P partial occupancy constraint loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_occupancy _atom_site_adp_type _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group _atom_site_attached_hydrogens Br1 Br 0.32651(5) 0.65801(6) 0.57237(3) 0.0207 1.0000 Uani . . . . . . O1 O 0.5000 0.4442(6) 0.7500 0.0242 1.0000 Uani S T . . . . C1 C 0.5000 0.2775(8) 0.7500 0.0172 1.0000 Uani DS T . . . . C2 C 0.3740(7) 0.1730(6) 0.6607(4) 0.0249 1.0000 Uani D . . . . . D1 D 0.321(9) 0.089(11) 0.694(5) 0.067(14) 1.0000 Uiso D . . . . . D2 D 0.288(10) 0.260(10) 0.614(6) 0.067(14) 1.0000 Uiso D . . . . . D3 D 0.442(9) 0.106(10) 0.613(6) 0.067(14) 1.0000 Uiso D . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Br1 0.0215(3) 0.0183(3) 0.0204(3) -0.00006(15) 0.00055(18) 0.00264(15) O1 0.030(2) 0.019(2) 0.0201(19) 0.0000 -0.0043(17) 0.0000 C1 0.016(3) 0.019(3) 0.016(3) 0.0000 0.002(2) 0.0000 C2 0.034(3) 0.016(2) 0.020(2) 0.0002(16) -0.0039(18) -0.0063(19) _refine_ls_extinction_method None _oxford_refine_ls_scale 0.4431(10) loop_ _geom_bond_atom_site_label_1 _geom_bond_site_symmetry_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Br1 . Br1 4_566 2.3153(8) yes O1 . C1 . 1.230(8) yes C1 . C2 5_656 1.491(5) yes C1 . C2 . 1.491(5) yes C2 . D1 . 0.88(9) no C2 . D2 . 1.00(8) no C2 . D3 . 0.98(8) no loop_ _geom_angle_atom_site_label_1 _geom_angle_site_symmetry_1 _geom_angle_atom_site_label_2 _geom_angle_site_symmetry_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C2 5_656 C1 . O1 . 121.1(3) yes C2 5_656 C1 . C2 . 117.8(5) yes O1 . C1 . C2 . 121.1(3) yes C1 . C2 . D1 . 109(4) no C1 . C2 . D2 . 108(3) no D1 . C2 . D2 . 113(4) no C1 . C2 . D3 . 110(4) no D1 . C2 . D3 . 105(4) no D2 . C2 . D3 . 111(4) no _iucr_refine_instruction_details_constraints ; # # Punched on 16/07/13 at 01:54:51 # #LIST 12 BLOCK CONT SCALE CONT BR ( 1 ,X'S,U'S) UNTIL C ( 2 ) CONT D ( 1 ,X'S,U[ISO]) UNTIL D ( 3 ) EQUIV D(1,U[ISO]) UNTIL D(3) END ; _iucr_refine_instruction_details_restraints ; # # Punched on 16/07/13 at 01:54:51 # #LIST 16 NO REM HREST START (DO NOT REMOVE THIS LINE) REM NO H NO #H U MULT DIST REM C-H REM >4 1.5 .96 DISORDER REM 1 1 1.2 .93 C C-H (ACETYLENE) REM 1 2 1.2 .93 C-C(H)-C REM 1 3 1.2 .98 (C)3-C-H REM 2 1 1.2 .93 C=C-H(2) REM 2 2 1.2 .97 (C)2-C-(H)2 REM 3 1 1.5 .96 C-C-(H)3 REM N-H REM >4 1.5 .89 DISORDER REM 1 1 1.2 .86 N-N/H REM 1 2 1.2 .86 (C)2-N-H REM 1 3 1.2 .89 (C)3-N-H REM 2 1 1.2 .86 C-N-(H)2 REM 2 2 1.2 .89 (C)2-N-(H)2 REM 3 1 1.2 .89 C-H-(H)3 REM O-H REM 1 1 1.5 .82 O-H REM REM DIST ESD = 0.02 REM VIB ESD = 0.002 REM ANGLE ESD = 2.0 REM 3 H ON SP 3 ANGLE 109.54, 6.0 = CONT C(1) TO C ( 2) TO D(1) CONT C(1) TO C ( 2) TO D(2) CONT C(1) TO C ( 2) TO D(3) ANGLE 0.0, 6.0 = MEAN D(1) TO C ( 2) TO D(2) CONT D(1) TO C ( 2) TO D(3) CONT D(2) TO C ( 2) TO D(3) REM HREST END (DO NOT REMOVE THIS LINE) END ; # start Validation Reply Form _vrf_PLAT431_I ; PROBLEM: Short Inter HL..A Contact Br1 .. O1 . 2.76 Ang. RESPONSE:This is a short O...Br halogen bond which is discussed in paper ; # end Validation Reply Form _database_code_depnum_ccdc_archive 'CCDC 950040' ####################################################################### # # Cambridge Crystallographic Data Centre # CCDC # ####################################################################### # # This CIF contains data from an original supplementary publication # deposited with the CCDC, and may include chemical, crystal, # experimental, refinement, atomic coordinates, # anisotropic displacement parameters and molecular geometry data, # as required by the journal to which it was submitted. # # This CIF is provided on the understanding that it is used for bona # fide research purposes only. It may contain copyright material # of the CCDC or of third parties, and may not be copied or further # disseminated in any form, whether machine-readable or not, # except for the purpose of generating routine backup copies # on your local computer system. # # For further information on the CCDC, data deposition and # data retrieval see: # www.ccdc.cam.ac.uk # # Bona fide researchers may freely download Mercury and enCIFer # from this site to visualise CIF-encoded structures and # to carry out CIF format checking respectively. # data_1 _exptl_special_details ; The crystal was placed in the cold stream of an Oxford Cryosystems open-flow nitrogen cryostat (Cosier & Glazer, 1986) with a nominal stability of 0.1K. Cosier, J. & Glazer, A.M., 1986. J. Appl. Cryst. 105-107. ; _refine_special_details ; ? ; #--------------------------------------------------------------- # _oxford_ data items, April 2010: # There is some uncertainty about the correct way of forming local data # names, e.g. # _atom_site_special_shape_oxford # or # _oxford_atom_site_special_shape # see: # http://www.iucr.org/resources/cif/spec/version1.1/semantics#namespace # A reserved prefix, e.g. foo, must be used in the following way # " If the data file contains items defined in a DDL1 dictionary, the # local data names assigned under the reserved prefix must contain it as # their first component, e.g. _foo_atom_site_my_item. " # However, this seems to say the opposite: # http://www.iucr.org/__data/iucr/cif/standard/cifstd8.html # According to advice from the IUCr, CRYSTALS is correct #--------------------------------------------------------------- # End of 'script/refcif.dat' #end of refcif _cell_length_a 7.6349(5) _cell_length_b 7.4263(6) _cell_length_c 12.1724(8) _cell_angle_alpha 90 _cell_angle_beta 102.788(4) _cell_angle_gamma 90 _cell_volume 673.04(8) _symmetry_cell_setting Monoclinic _symmetry_space_group_name_H-M 'C 1 2/c 1 ' _symmetry_space_group_name_Hall ? loop_ _symmetry_equiv_pos_as_xyz x,y,z -x,-y,-z x+1/2,y+1/2,z -x+1/2,-y+1/2,-z -x,y,-z+1/2 x,-y,z+1/2 -x+1/2,y+1/2,-z+1/2 x+1/2,-y+1/2,z+1/2 loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_Cromer_Mann_a1 _atom_type_scat_Cromer_Mann_b1 _atom_type_scat_Cromer_Mann_a2 _atom_type_scat_Cromer_Mann_b2 _atom_type_scat_Cromer_Mann_a3 _atom_type_scat_Cromer_Mann_b3 _atom_type_scat_Cromer_Mann_a4 _atom_type_scat_Cromer_Mann_b4 _atom_type_scat_Cromer_Mann_c _atom_type_scat_source C 0.0033 0.0016 2.3100 20.8439 1.0200 10.2075 1.5886 0.5687 0.8650 51.6512 0.2156 'International Tables Vol C 4.2.6.8 and 6.1.1.4' H 0.0000 0.0000 0.4930 10.5109 0.3229 26.1257 0.1402 3.1424 0.0408 57.7998 0.0030 'International Tables Vol C 4.2.6.8 and 6.1.1.4' O 0.0106 0.0060 3.0485 13.2771 2.2868 5.7011 1.5463 0.3239 0.8670 32.9089 0.2508 'International Tables Vol C 4.2.6.8 and 6.1.1.4' Br -0.2901 2.4595 17.1789 2.1723 5.2358 16.5796 5.6377 0.2609 3.9851 41.4328 2.9557 'International Tables Vol C 4.2.6.8 and 6.1.1.4' Cd -0.8075 1.2024 19.2214 0.5946 17.6444 6.9089 4.4610 24.7008 1.6029 87.4825 5.0694 'International Tables Vol C 4.2.6.8 and 6.1.1.4' _cell_formula_units_Z 4 # Given Formula = C3 H6 Br1 O1 # Dc = 2.72 Fooo = 408.00 Mu = 119.70 M = 137.98 # Found Formula = C1.50 H3 Br1 O0.50 # Dc = 2.15 FOOO = 408.00 Mu = 119.28 M = 108.94 _chemical_formula_sum 'C3 D6 Br2 O1' _chemical_formula_moiety 'C3 D6 Br2 O1' _chemical_compound_source ? _chemical_formula_weight 223.92 _cell_measurement_reflns_used 0 _cell_measurement_theta_min 0 _cell_measurement_theta_max 0 _cell_measurement_temperature 200 _exptl_crystal_description block _exptl_crystal_colour orange _exptl_crystal_size_min 0.130 _exptl_crystal_size_mid 0.170 _exptl_crystal_size_max 0.370 _exptl_crystal_density_diffrn 2.150 _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' # Non-dispersive F(000): _exptl_crystal_F_000 408 _exptl_absorpt_coefficient_mu 11.928 # Sheldrick geometric approximatio 0.13 0.21 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS 2007/2 (Sheldrick, G.M., 2007)' _exptl_absorpt_correction_T_min 0.1316 _exptl_absorpt_correction_T_max 0.2121 _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_source 'Bruker-Nonius FR591 rotating anode' _diffrn_radiation_monochromator '10cm confocal mirrors' _diffrn_measurement_device_type 'Bruker-Nonius APEX II CCD camera on \k-goniostat' _diffrn_measurement_method '\f & \w scans' _diffrn_detector_area_resol_mean '4096x4096pixels / 62x62mm' # If a reference occurs more than once, delete the author # and date from subsequent references. _computing_data_collection 'USER DEFINED DATA COLLECTION' _computing_cell_refinement 'USER DEFINED CELL REFINEMENT' _computing_data_reduction 'USER DEFINED DATA REDUCTION' _computing_structure_solution 'SHELXS 86 (Sheldrick, 1986)' _computing_structure_refinement 'CRYSTALS (Betteridge et al., 2003)' _computing_publication_material 'CRYSTALS (Betteridge et al., 2003)' _computing_molecular_graphics 'CAMERON (Watkin et al., 1996)' _diffrn_standards_number 0 _diffrn_standards_decay_% ? _diffrn_ambient_temperature 200 _diffrn_reflns_number 2261 _reflns_number_total 720 _diffrn_reflns_av_R_equivalents 0.057 # Number of reflections without Friedels Law is 0 # Number of reflections with Friedels Law is 720 # Theoretical number of reflections is about 1533 _diffrn_reflns_theta_min 3.433 _diffrn_reflns_theta_max 27.412 _diffrn_measured_fraction_theta_max 0.941 _diffrn_reflns_theta_full 27.412 _diffrn_measured_fraction_theta_full 0.941 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_k_min -9 _diffrn_reflns_limit_k_max 9 _diffrn_reflns_limit_l_min -14 _diffrn_reflns_limit_l_max 15 _reflns_limit_h_min -9 _reflns_limit_h_max 9 _reflns_limit_k_min 0 _reflns_limit_k_max 9 _reflns_limit_l_min 0 _reflns_limit_l_max 15 _oxford_diffrn_Wilson_B_factor 3.06 _oxford_diffrn_Wilson_scale 3.18 _atom_sites_solution_primary Direct #heavy,direct,difmap,geom # _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens difmap _refine_diff_density_min -0.91 _refine_diff_density_max 0.83 # The current dictionary definitions do not cover the # situation where the reflections used for refinement were # selected by a user-defined sigma threshold # The values actually used during refinement _oxford_reflns_threshold_expression_ref I>3.0\s(I) _refine_ls_number_reflns 626 _refine_ls_number_restraints 6 _refine_ls_number_parameters 39 _oxford_refine_ls_R_factor_ref 0.0545 _refine_ls_wR_factor_ref 0.1374 _refine_ls_goodness_of_fit_ref 1.0975 _refine_ls_shift/su_max 0.0001846 _refine_ls_shift/su_mean 0.0000122 # The values computed from all data _oxford_reflns_number_all 720 _refine_ls_R_factor_all 0.0623 _refine_ls_wR_factor_all 0.1507 # The values computed with a 2 sigma cutoff - a la SHELX _reflns_threshold_expression I>2.0\s(I) _reflns_number_gt 649 _refine_ls_R_factor_gt 0.0562 _refine_ls_wR_factor_gt 0.1391 # choose from: rm (reference molecule of known chirality), # ad (anomolous dispersion - Flack), rmad (rm and ad), # syn (from synthesis), unk (unknown) or . (not applicable). _chemical_absolute_configuration . _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_hydrogen_treatment mixed # none, undef, noref, refall, # refxyz, refU, constr or mixed _refine_ls_weighting_scheme calc _refine_ls_weighting_details ; Method, part 1, Chebychev polynomial, (Watkin, 1994, Prince, 1982) [weight] = 1.0/[A~0~*T~0~(x)+A~1~*T~1~(x) ... +A~n-1~]*T~n-1~(x)] where A~i~ are the Chebychev coefficients listed below and x= Fcalc/Fmax Method = Robust Weighting (Prince, 1982) W = [weight] * [1-(deltaF/6*sigmaF)^2^]^2^ A~i~ are: 87.1 99.2 65.4 ; # Uequiv = arithmetic mean of Ui i.e. Ueqiv = (U1+U2+U3)/3 # Replace last . with number of unfound hydrogen atoms attached to an atom. # ..._refinement_flags_... # . no refinement constraints S special position constraint on site # G rigid group refinement of site R riding atom # D distance or angle restraint on site T thermal displacement constraints # U Uiso or Uij restraint (rigid bond) P partial occupancy constraint loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_occupancy _atom_site_adp_type _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group _atom_site_attached_hydrogens Br1 Br 0.67415(9) 0.65852(11) 0.42841(5) 0.0394 1.0000 Uani . . . . . . O1 O 0.5000 0.4457(13) 0.2500 0.0476 1.0000 Uani S T . . . . C1 C 0.5000 0.2847(16) 0.2500 0.0302 1.0000 Uani DS T . . . . C2 C 0.3714(13) 0.1766(12) 0.1624(7) 0.0458 1.0000 Uani D . . . . . D1 D 0.424(12) 0.121(16) 0.121(8) 0.09(2) 1.0000 Uiso D . . . . . D2 D 0.275(16) 0.277(17) 0.112(9) 0.09(2) 1.0000 Uiso D . . . . . D3 D 0.308(15) 0.106(18) 0.190(7) 0.09(2) 1.0000 Uiso D . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Br1 0.0450(6) 0.0328(6) 0.0370(5) 0.0003(2) 0.0020(4) -0.0057(2) O1 0.058(5) 0.034(5) 0.038(4) 0.0000 -0.016(3) 0.0000 C1 0.023(4) 0.041(7) 0.024(4) 0.0000 0.002(3) 0.0000 C2 0.067(5) 0.026(4) 0.038(4) -0.007(3) -0.002(4) -0.011(4) _refine_ls_extinction_method None _oxford_refine_ls_scale 0.574(3) loop_ _geom_bond_atom_site_label_1 _geom_bond_site_symmetry_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Br1 . Br1 4_666 2.3090(13) yes O1 . C1 . 1.196(14) yes C1 . C2 5_655 1.510(10) yes C1 . C2 . 1.510(10) yes C2 . D1 . 0.83(14) no C2 . D2 . 1.13(15) no C2 . D3 . 0.83(16) no loop_ _geom_angle_atom_site_label_1 _geom_angle_site_symmetry_1 _geom_angle_atom_site_label_2 _geom_angle_site_symmetry_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C2 5_655 C1 . O1 . 122.1(5) yes C2 5_655 C1 . C2 . 115.8(10) yes O1 . C1 . C2 . 122.1(5) yes C1 . C2 . D1 . 112(5) no C1 . C2 . D2 . 106(4) no D1 . C2 . D2 . 110(5) no C1 . C2 . D3 . 113(5) no D1 . C2 . D3 . 109(5) no D2 . C2 . D3 . 106(5) no _iucr_refine_instruction_details_constraints ; # # Punched on 19/07/12 at 10:39:02 # #LIST 12 BLOCK CONT SCALE CONT BR ( 1 ,X'S,U'S) UNTIL C ( 2 ) CONT D ( 1 ,X'S,U[ISO]) UNTIL D ( 3 ) EQUIV D(1,U[ISO]) D(2,U[ISO]) d(3,U[ISO]) END ; _iucr_refine_instruction_details_restraints ; # # Punched on 19/07/12 at 10:39:02 # #LIST 16 REM HREST START (DO NOT REMOVE THIS LINE) REM NO H NO #H U MULT DIST REM C-H REM >4 1.5 .96 DISORDER REM 1 1 1.2 .93 C C-H (ACETYLENE) REM 1 2 1.2 .93 C-C(H)-C REM 1 3 1.2 .98 (C)3-C-H REM 2 1 1.2 .93 C=C-H(2) REM 2 2 1.2 .97 (C)2-C-(H)2 REM 3 1 1.5 .96 C-C-(H)3 REM N-H REM >4 1.5 .89 DISORDER REM 1 1 1.2 .86 N-N/H REM 1 2 1.2 .86 (C)2-N-H REM 1 3 1.2 .89 (C)3-N-H REM 2 1 1.2 .86 C-N-(H)2 REM 2 2 1.2 .89 (C)2-N-(H)2 REM 3 1 1.2 .89 C-H-(H)3 REM O-H REM 1 1 1.5 .82 O-H REM REM DIST ESD = 0.02 REM VIB ESD = 0.002 REM ANGLE ESD = 2.0 REM 3 H ON SP 3 ANGLE 109.54, 6.0 = CONT C(1) TO C ( 2) TO D(1) CONT C(1) TO C ( 2) TO D(2) CONT C(1) TO C ( 2) TO D(3) ANGLE 0.0, 6.0 = MEAN D(1) TO C ( 2) TO D(2) CONT D(1) TO C ( 2) TO D3) CONT D(2) TO C ( 2) TO D(3) REM HREST END (DO NOT REMOVE THIS LINE) END ; # start Validation Reply Form _vrf_PLAT431_I ; PROBLEM: Short Inter HL..A Contact Br1 .. O1 . 2.78 Ang. RESPONSE: This is a short O...Br halogen bond which is discussed in the paper. ; # end Validation Reply Form _database_code_depnum_ccdc_archive 'CCDC 950041' ####################################################################### # # Cambridge Crystallographic Data Centre # CCDC # ####################################################################### # # This CIF contains data from an original supplementary publication # deposited with the CCDC, and may include chemical, crystal, # experimental, refinement, atomic coordinates, # anisotropic displacement parameters and molecular geometry data, # as required by the journal to which it was submitted. # # This CIF is provided on the understanding that it is used for bona # fide research purposes only. It may contain copyright material # of the CCDC or of third parties, and may not be copied or further # disseminated in any form, whether machine-readable or not, # except for the purpose of generating routine backup copies # on your local computer system. # # For further information on the CCDC, data deposition and # data retrieval see: # www.ccdc.cam.ac.uk # # Bona fide researchers may freely download Mercury and enCIFer # from this site to visualise CIF-encoded structures and # to carry out CIF format checking respectively. # data_BR2-ACETONE-CIF_phase_1 _pd_block_id 2013-04-15T10:09|BR2-ACETONE-CIF_phase1|rhj|| # Histograms for phase 1 loop_ _pd_block_diffractogram_id 2013-04-15T10:09|BR2-ACETONE-CIF_H_01|rhj|hrpd 2013-04-15T10:09|BR2-ACETONE-CIF_H_02|rhj|hrpd #============================================================================== # 7. CHEMICAL, STRUCTURAL AND CRYSTAL DATA _pd_char_particle_morphology ? _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_formula_moiety 'C3 D6 Br2 O1' _chemical_formula_structural ? _chemical_formula_analytical ? _chemical_melting_point ? _chemical_compound_source ? # for minerals and # natural products _symmetry_space_group_name_Hall ? _exptl_crystal_F_000 ? _exptl_crystal_density_diffrn 2.260 _exptl_crystal_density_meas 'not measured' _exptl_crystal_density_method 'not measured' _cell_measurement_temperature 110 _cell_special_details ; ? ; _geom_special_details ? # The following item identifies the program(s) used (if appropriate). _computing_structure_solution ? #============================================================================== # 8. REFINEMENT DATA # Use the next field to give any special details about the fitting of the # powder pattern. _pd_proc_ls_special_details ; ? ; # The next three items are given as text. _pd_proc_ls_profile_function ? _pd_proc_ls_background_function ? _pd_proc_ls_pref_orient_corr ; ? ; _pd_proc_ls_prof_R_factor 0.0148 _pd_proc_ls_prof_wR_factor 0.0160 _pd_proc_ls_prof_wR_expected 0.0061 _refine_ls_R_I_factor ? _refine_ls_R_Fsqd_factor 0.17965 _refine_ls_R_factor_all ? _refine_special_details ; ? ; _refine_ls_matrix_type ? _refine_ls_weighting_scheme ? # options are 'sigma' (based on measured su's) # or 'calc' (calculated weights) _refine_ls_weighting_details ? _refine_ls_hydrogen_treatment ? _refine_ls_extinction_method ? _refine_ls_extinction_coef ? _refine_ls_number_restraints ? _refine_ls_number_constraints ? # The following item is the same as CHI, the square root of 'CHI squared' _refine_ls_goodness_of_fit_all 3.53 _refine_ls_restrained_S_all ? _refine_ls_shift/su_max ? _refine_ls_shift/su_mean ? # The following four items apply to angular dispersive measurements. # 2theta minimum, maximum and increment (in degrees) are for the # intensities used in the refinement. _pd_proc_2theta_range_min ? _pd_proc_2theta_range_max ? _pd_proc_2theta_range_inc ? _pd_proc_wavelength ? # Each refinement must be accompanied by a listing of the powder data # in CIF format. Each listing should be sent as a separate file consisting # of one data block containing a single powder profile. The value of # _pd_block_diffractogram_id is used to associate each refinement with # its corresponding powder profile, since it must match the value # of _pd_block_id in the file containing the powder data. A template # for supplying powder data in CIF format is available by ftp at # ftp://ftp.iucr.org/pub/rietdataform.cif and an example is given # at ftp://ftp.iucr.org/pub/rietdataxmpl.cif. # Give appropriate details in the next two text fields. _pd_proc_info_excluded_regions ? _pd_proc_info_data_reduction ? # The following items are used to identify the programs used. _computing_data_collection ? _computing_cell_refinement ? _computing_data_reduction ? _computing_structure_refinement ? _computing_molecular_graphics ? _computing_publication_material ? #============================================================================== # 9. Phase information from GSAS _pd_phase_name avbr2 _cell_length_a 7.58233(11) _cell_length_b 7.37528(9) _cell_length_c 12.04151(16) _cell_angle_alpha 90.0 _cell_angle_beta 102.2629(6) _cell_angle_gamma 90.0 _cell_volume 658.019(22) _diffrn_ambient_temperature 110 _diffrn_measurement_device_type 'ISIS HRPD ' _diffrn_radiation_type neutron _pd_instr_location 'ISIS spallation source, England' _pd_meas_scan_method tof _symmetry_cell_setting monoclinic _symmetry_space_group_name_H-M C2/c loop_ _symmetry_equiv_pos_site_id _symmetry_equiv_pos_as_xyz 1 +x,+y,+z 2 -x,+y,-z+1/2 -1 -x,-y,-z -2 +x,-y,+z+1/2 101 +x+1/2,+y+1/2,+z 102 -x+1/2,+y+1/2,-z+1/2 -101 -x+1/2,-y+1/2,-z -102 +x+1/2,-y+1/2,+z+1/2 # ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_occupancy _atom_site_thermal_displace_type _atom_site_U_iso_or_equiv _atom_site_symmetry_multiplicity Br BR1 0.32738(23) 0.65805(20) 0.57249(13) 1.0 Uani 0.0334 8 O O1 0.5 0.44557(34) 0.75 1.0 Uani 0.03264 4 C C1 0.5 0.27882(31) 0.75 1.0 Uani 0.02338 4 C C2 0.3731(4) 0.17252(33) 0.66021(19) 1.0 Uani 0.0411 8 D D1 0.2954(5) 0.0852(5) 0.69368(19) 1.0 Uani 0.1032 8 D D2 0.2890(5) 0.2567(4) 0.60612(24) 1.0 Uani 0.12665 8 D D3 0.4461(4) 0.0949(4) 0.61192(23) 1.0 Uani 0.10051 8 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_22 _atom_site_aniso_U_23 _atom_site_aniso_U_33 BR1 0.0446(15) 0.0044(8) -0.0102(9) 0.0141(10) -0.0007(7) 0.0333(12) O1 0.0605(20) 0.0 -0.0132(14) 0.0164(17) 0.0 0.0117(15) C1 0.0126(16) 0.0 -0.0099(10) 0.0313(16) 0.0 0.0203(14) C2 0.0538(16) -0.0169(11) -0.0149(12) 0.0332(13) -0.0083(10) 0.0259(13) D1 0.1469(28) -0.0931(21) 0.0135(18) 0.1104(24) -0.0125(15) 0.0491(16) D2 0.1664(32) -0.0039(20) -0.1027(22) 0.0585(18) -0.0010(14) 0.0969(23) D3 0.0778(22) -0.0141(16) 0.0120(16) 0.1307(26) -0.0949(21) 0.0904(22) loop_ _atom_type_symbol _atom_type_number_in_cell Br 8.0 O 4.0 C 12.0 D 24.0 # If you change Z, be sure to change all 3 of the following _chemical_formula_sum 'C3 Br2 D6 O' _chemical_formula_weight 223.92 _cell_formula_units_Z 4 _exptl_crystal_colour orange _refine_ls_number_parameters 103 _diffrn_radiation_probe neutron # MOLECULAR GEOMETRY loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_1 _geom_bond_site_symmetry_2 _geom_bond_publ_flag BR1 BR1 2.3224(28) . -101_566 N BR1 O1 2.7476(19) . 1_555 N O1 BR1 2.7476(19) . 1_555 N O1 BR1 2.7476(19) . 2_656 N O1 C1 1.2298(28) . 1_555 N O1 C2 2.3891(29) . 1_555 N O1 C2 2.3891(29) . 2_656 N O1 D1 2.6798(33) . 101_555 N O1 D1 2.6798(33) . 102_556 N O1 D2 2.5150(27) . 1_555 N O1 D2 2.5150(27) . 2_656 N C1 O1 1.2298(28) . 1_555 N C1 C2 1.5057(23) . 1_555 N C1 C2 1.5057(23) . 2_656 N C1 D1 2.1118(31) . 1_555 N C1 D1 2.1118(31) . 2_656 N C1 D2 2.1002(22) . 1_555 N C1 D2 2.1002(22) . 2_656 N C1 D3 2.1172(26) . 1_555 N C1 D3 2.1172(26) . 2_656 N C2 O1 2.3891(29) . 1_555 N C2 C1 1.5057(23) . 1_555 N C2 D1 1.0128(26) . 1_555 N C2 D2 1.0197(27) . 1_555 N C2 D3 1.0529(28) . 1_555 N D1 O1 2.6798(33) . 101_445 N D1 C1 2.1118(31) . 1_555 N D1 C2 1.0128(26) . 1_555 N D1 D2 1.641(4) . 1_555 N D1 D3 1.661(4) . 1_555 N D2 O1 2.5150(27) . 1_555 N D2 C1 2.1002(22) . 1_555 N D2 C2 1.0197(27) . 1_555 N D2 D1 1.641(4) . 1_555 N D2 D3 1.677(4) . 1_555 N D3 C1 2.1172(26) . 1_555 N D3 C2 1.0529(28) . 1_555 N D3 D1 1.661(4) . 1_555 N D3 D2 1.677(4) . 1_555 N loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_2 _geom_angle_site_symmetry_3 _geom_angle_publ_flag BR1 BR1 O1 177.41(13) -101_566 . 1_555 N BR1 O1 BR1 110.45(10) 1_555 . 2_656 N BR1 O1 C1 124.77(5) 1_555 . 1_555 N BR1 O1 C1 124.77(5) 2_656 . 1_555 N O1 C1 C2 121.38(13) 1_555 . 1_555 N O1 C1 C2 121.38(13) 1_555 . 2_656 N C2 C1 C2 117.24(26) 1_555 . 2_656 N C1 C2 D1 112.49(26) 1_555 . 1_555 N C1 C2 D2 111.07(28) 1_555 . 1_555 N C1 C2 D3 110.44(26) 1_555 . 1_555 N D1 C2 D2 107.6(4) 1_555 . 1_555 N D1 C2 D3 107.02(34) 1_555 . 1_555 N D2 C2 D3 107.99(33) 1_555 . 1_555 N C2 D1 D2 36.33(22) 1_555 . 1_555 N C2 D1 D3 37.31(20) 1_555 . 1_555 N D2 D1 D3 61.05(18) 1_555 . 1_555 N C2 D2 D1 36.04(23) 1_555 . 1_555 N C2 D2 D3 36.67(19) 1_555 . 1_555 N D1 D2 D3 60.07(18) 1_555 . 1_555 N C2 D3 D1 35.67(18) 1_555 . 1_555 N C2 D3 D2 35.34(18) 1_555 . 1_555 N D1 D3 D2 58.88(21) 1_555 . 1_555 N #============================================================================== # 9. INSTRUMENT CHARACTERIZATION _exptl_special_details ; ? ; # if regions of the data are excluded, the reason(s) are supplied here: _pd_calibration_special_details # description of the method used # to calibrate the instrument ; ? ; # The following item is used for angular dispersive measurements only. _diffrn_radiation_monochromator ? # The following items are used to define the size of the instrument. # Not all distances are appropriate for all instrument types. _pd_instr_dist_src/mono ? _pd_instr_dist_mono/spec ? _pd_instr_dist_src/spec ? _pd_instr_dist_spec/anal ? _pd_instr_dist_anal/detc ? _pd_instr_dist_spec/detc ? # 10. Specimen size and mounting information # The next three fields give the specimen dimensions in mm. The equatorial # plane contains the incident and diffracted beam. _pd_spec_size_axial ? # perpendicular to # equatorial plane _pd_spec_size_equat ? # parallel to # scattering vector # in transmission _pd_spec_size_thick ? # parallel to # scattering vector # in reflection _pd_spec_mounting # This field should be # used to give details of the # container. ; ? ; _pd_spec_mount_mode ? # options are 'reflection' # or 'transmission' _pd_spec_shape ? # options are 'cylinder' # 'flat_sheet' or 'irregular' _pd_proc_ls_peak_cutoff 10.76(24) _exptl_absorpt_correction_T_min 0.58953 _exptl_absorpt_correction_T_max 0.86101 # Extinction correction _gsas_exptl_extinct_corr_T_min 0.75531 _gsas_exptl_extinct_corr_T_max 1.00000 _pd_proc_info_datetime 2013-04-15T10:09:50 _pd_calc_method 'Rietveld Refinement' _pd_meas_2theta_fixed 168.33 #---- raw/calc data loop ----- loop_ _pd_meas_time_of_flight _pd_proc_d_spacing _pd_meas_intensity_total _pd_proc_ls_weight _pd_proc_intensity_bkg_calc _pd_calc_intensity_total 31370.1 . 1.73(5) . . . 31379.6 . 1.80(6) . . . 31389.0 . 1.75(5) . . . 31398.4 . 1.76(5) . . . 31407.8 . 1.71(5) . . . 31417.2 . 1.75(5) . . . 31426.7 . 1.79(5) . . . 31436.1 . 1.78(5) . . . 31445.5 . 1.79(5) . . . 31454.9 . 1.76(5) . . . 31464.4 . 1.82(5) . . . 31473.8 . 1.78(5) . . . 31483.3 . 1.73(5) . . . 31492.7 . 1.75(5) . . . 31502.2 . 1.81(5) . . . 31511.6 . 1.79(5) . . . 31521.1 . 1.80(5) . . . 31530.5 . 1.81(5) . . . 31540.0 . 1.89(5) . . . 31549.4 . 1.87(5) . . . 31558.9 . 1.84(5) . . . 31568.4 . 1.76(5) . . . 31577.8 . 1.87(5) . . . 31587.3 . 1.82(5) . . . 31596.8 . 1.92(5) . . . 31606.3 . 1.89(5) . . . 31615.8 . 1.84(5) . . . 31625.2 . 1.80(5) . . . 31634.7 . 1.75(4) . . . 31644.2 . 1.79(4) . . . 31653.7 . 1.89(5) . . . 31663.2 . 1.88(5) . . . 31672.7 . 1.93(5) . . . 31682.2 . 1.98(5) . . . 31691.7 . 2.02(5) . . . 31701.2 . 1.98(5) . . . 31710.7 . 2.05(5) . . . 31720.2 . 1.90(4) . . . 31729.8 . 1.94(4) . . . 31739.3 . 1.93(4) . . . 31748.8 . 1.92(4) . . . 31758.3 . 1.85(4) . . . 31767.9 . 1.83(4) . . . 31777.4 . 1.91(4) . . . 31786.9 . 1.96(4) . . . 31796.5 . 1.90(4) . . . 31806.0 . 1.83(4) . . . 31815.5 . 1.91(4) . . . 31825.1 . 1.86(4) . . . 31834.6 . 1.89(4) . . . 31844.2 . 1.92(4) . . . 31853.7 . 1.86(4) . . . 31863.3 . 1.86(4) . . . 31872.8 . 1.90(4) . . . 31882.4 . 1.91(4) . . . 31892.0 . 1.88(4) . . . 31901.5 . 1.97(4) . . . 31911.1 . 1.92(4) . . . 31920.7 . 1.94(4) . . . 31930.3 . 1.93(4) . . . 31939.8 . 1.88(4) . . . 31949.4 . 1.98(4) . . . 31959.0 . 1.91(4) . . . 31968.6 . 1.93(4) . . . 31978.2 . 1.97(4) . . . 31987.8 . 2.02(4) . . . 31997.4 0.66261 1.89(4) 0.0 1.812 . 32007.0 0.66281 2.01(4) 685. 1.813 1.932 32016.6 0.66301 1.99(4) 691. 1.815 1.912 32026.2 0.66321 2.02(4) 690. 1.816 1.891 32035.8 0.66341 1.94(4) 721. 1.817 1.872 32045.4 0.66361 1.92(4) 742. 1.819 1.860 32055.0 0.66381 1.91(4) 764. 1.820 1.859 32064.6 0.66401 1.93(4) 766. 1.821 1.867 32074.2 0.66420 1.89(4) 786. 1.823 1.877 32083.9 0.66440 1.90(4) 794. 1.824 1.881 32093.5 0.66460 1.94(4) 780. 1.825 1.883 32103.1 0.66480 1.94(4) 790. 1.827 1.885 32112.8 0.66500 1.92(4) 804. 1.828 1.886 32122.4 0.66520 1.94(4) 785. 1.829 1.885 32132.0 0.66540 1.893(35) 815. 1.8306 1.8825 32141.7 0.66560 1.893(35) 829. 1.8318 1.8807 32151.3 0.66580 1.944(35) 824. 1.8331 1.8800 32160.9 0.66600 1.885(34) 850. 1.8343 1.8783 32170.6 0.66620 1.863(34) 864. 1.8356 1.8736 32180.3 0.66640 1.898(34) 850. 1.8368 1.8690 32189.9 0.66660 1.966(34) 841. 1.8380 1.8694 32199.6 0.66680 1.924(34) 870. 1.8392 1.8772 32209.2 0.66700 1.950(34) 870. 1.8404 1.8925 32218.9 0.66720 1.943(34) 872. 1.8416 1.9141 32228.5 0.66740 1.949(34) 876. 1.8428 1.9360 32238.2 0.66760 1.886(33) 909. 1.8440 1.9443 32247.9 0.66780 1.916(34) 883. 1.8451 1.9326 32257.6 0.66800 1.907(33) 911. 1.8463 1.9109 32267.2 0.66820 1.929(33) 920. 1.8474 1.8922 32276.9 0.66840 1.864(32) 953. 1.8486 1.8814 32286.6 0.66860 1.905(33) 937. 1.8497 1.8786 32296.3 0.66880 1.921(33) 921. 1.8508 1.8817 32306.0 0.66901 1.867(32) 985. 1.8519 1.8871 32315.7 0.66921 1.882(32) 975. 1.8530 1.8916 32325.4 0.66941 1.920(32) 963. 1.8541 1.8971 32335.1 0.66961 1.883(32) 998. 1.8552 1.9043 32344.8 0.66981 1.929(32) 961. 1.8563 1.9103 32354.5 0.67001 1.909(32) 1001. 1.8574 1.9126 32364.2 0.67021 1.895(32) 1002. 1.8585 1.9101 32373.9 0.67041 1.869(31) 1042. 1.8595 1.9023 32383.6 0.67061 1.892(31) 1012. 1.8606 1.8928 32393.3 0.67081 1.856(31) 1054. 1.8616 1.8850 32403.0 0.67102 1.841(30) 1095. 1.8627 1.8797 32412.7 0.67122 1.863(31) 1068. 1.8637 1.8772 32422.5 0.67142 1.881(31) 1053. 1.8647 1.8778 32432.2 0.67162 1.905(31) 1040. 1.8657 1.8822 32441.9 0.67182 1.913(31) 1052. 1.8667 1.8905 32451.7 0.67202 1.910(31) 1066. 1.8677 1.9001 32461.4 0.67222 1.925(31) 1065. 1.8687 1.9051 32471.1 0.67243 1.860(30) 1105. 1.8697 1.9026 32480.9 0.67263 1.919(30) 1078. 1.8707 1.8959 32490.6 0.67283 1.901(30) 1085. 1.8717 1.8899 32500.4 0.67303 1.872(30) 1137. 1.8727 1.8878 32510.1 0.67323 1.882(30) 1124. 1.8736 1.8902 32519.9 0.67344 1.867(29) 1165. 1.8746 1.8965 32529.6 0.67364 1.897(30) 1138. 1.8755 1.9037 32539.4 0.67384 1.895(30) 1144. 1.8765 1.9078 32549.1 0.67404 1.877(29) 1164. 1.8774 1.9089 32558.9 0.67424 1.916(30) 1148. 1.8784 1.9101 32568.7 0.67445 1.852(29) 1198. 1.8793 1.9119 32578.4 0.67465 1.887(29) 1183. 1.8802 1.9110 32588.2 0.67485 1.884(29) 1181. 1.8811 1.9069 32598.0 0.67505 1.884(29) 1199. 1.8820 1.9026 32607.8 0.67526 1.873(29) 1220. 1.8830 1.9001 32617.6 0.67546 1.888(29) 1206. 1.8839 1.8996 32627.3 0.67566 1.934(29) 1188. 1.8847 1.9007 32637.1 0.67586 1.853(28) 1263. 1.8856 1.9026 32646.9 0.67607 1.848(28) 1277. 1.8865 1.9040 32656.7 0.67627 1.880(28) 1243. 1.8874 1.9046 32666.5 0.67647 1.872(28) 1263. 1.8883 1.9057 32676.3 0.67668 1.879(28) 1267. 1.8891 1.9090 32686.1 0.67688 1.895(28) 1264. 1.8900 1.9151 32695.9 0.67708 1.932(29) 1226. 1.8909 1.9245 32705.7 0.67729 1.933(28) 1269. 1.8917 1.9404 32715.5 0.67749 1.959(28) 1243. 1.8926 1.9708 32725.4 0.67769 1.988(29) 1213. 1.8934 2.0140 32735.2 0.67790 1.935(28) 1255. 1.8942 2.0462 32745.0 0.67810 1.933(28) 1262. 1.8951 2.0441 32754.8 0.67830 1.930(28) 1285. 1.8959 2.0168 32764.7 0.67851 1.884(27) 1344. 1.8967 1.9866 32774.5 0.67871 1.943(28) 1293. 1.8976 1.9671 32784.3 0.67891 1.919(27) 1323. 1.8984 1.9621 32794.1 0.67912 1.931(27) 1328. 1.8992 1.9670 32804.0 0.67932 1.953(28) 1310. 1.9000 1.9713 32813.8 0.67952 1.985(28) 1259. 1.9008 1.9703 32823.7 0.67973 1.940(27) 1324. 1.9016 1.9733 32833.5 0.67993 1.943(27) 1338. 1.9024 1.9988 32843.4 0.68014 1.986(28) 1319. 1.9032 2.0573 32853.2 0.68034 2.052(28) 1281. 1.9040 2.1304 32863.1 0.68055 2.039(28) 1310. 1.9047 2.1755 32872.9 0.68075 2.037(28) 1311. 1.9055 2.1686 32882.8 0.68095 2.034(28) 1290. 1.9063 2.1231 32892.7 0.68116 1.967(27) 1393. 1.9071 2.0679 32902.5 0.68136 1.978(27) 1349. 1.9078 2.0197 32912.4 0.68157 1.967(27) 1358. 1.9086 1.9829 32922.3 0.68177 1.980(27) 1352. 1.9094 1.9581 32932.1 0.68198 1.942(27) 1410. 1.9101 1.9446 32942.0 0.68218 1.908(26) 1443. 1.9109 1.9419 32951.9 0.68239 1.960(27) 1388. 1.9116 1.9495 32961.8 0.68259 1.932(26) 1441. 1.9124 1.9634 32971.7 0.68279 1.941(27) 1417. 1.9131 1.9739 32981.6 0.68300 1.929(26) 1460. 1.9138 1.9720 32991.5 0.68320 1.931(26) 1460. 1.9146 1.9605 33001.4 0.68341 1.926(26) 1474. 1.9153 1.9482 33011.3 0.68361 1.877(26) 1535. 1.9160 1.9410 33021.2 0.68382 1.908(26) 1520. 1.9168 1.9400 33031.1 0.68403 1.922(26) 1507. 1.9175 1.9435 33041.0 0.68423 1.954(26) 1490. 1.9182 1.9484 33050.9 0.68444 1.910(25) 1539. 1.9189 1.9544 33060.8 0.68464 1.973(26) 1458. 1.9196 1.9639 33070.7 0.68485 2.016(26) 1443. 1.9203 1.9742 33080.7 0.68505 1.916(25) 1577. 1.9210 1.9785 33090.6 0.68526 1.979(26) 1505. 1.9218 1.9766 33100.5 0.68546 1.976(26) 1505. 1.9225 1.9733 33110.4 0.68567 1.960(25) 1568. 1.9232 1.9706 33120.4 0.68587 1.960(25) 1540. 1.9239 1.9684 33130.3 0.68608 1.975(25) 1545. 1.9245 1.9714 33140.2 0.68629 1.962(25) 1565. 1.9252 1.9877 33150.2 0.68649 2.003(26) 1513. 1.9259 2.0170 33160.1 0.68670 1.998(25) 1546. 1.9266 2.0429 33170.1 0.68690 1.991(25) 1559. 1.9273 2.0459 33180.0 0.68711 1.924(25) 1604. 1.9280 2.0284 33190.0 0.68732 1.981(25) 1575. 1.9287 2.0048 33199.9 0.68752 1.914(25) 1623. 1.9293 1.9861 33209.9 0.68773 1.959(25) 1589. 1.9300 1.9790 33219.9 0.68794 1.942(25) 1629. 1.9307 1.9879 33229.8 0.68814 2.010(25) 1587. 1.9314 2.0083 33239.8 0.68835 2.035(25) 1563. 1.9320 2.0241 33249.8 0.68856 2.059(26) 1534. 1.9327 2.0224 33259.8 0.68876 2.023(25) 1566. 1.9334 2.0086 33269.7 0.68897 2.013(25) 1601. 1.9340 1.9929 33279.7 0.68918 1.987(25) 1617. 1.9347 1.9789 33289.7 0.68938 1.999(25) 1602. 1.9354 1.9678 33299.7 0.68959 1.956(24) 1668. 1.9360 1.9618 33309.7 0.68980 1.953(24) 1691. 1.9367 1.9635 33319.7 0.69000 1.919(24) 1728. 1.9373 1.9728 33329.7 0.69021 1.972(24) 1697. 1.9380 1.9833 33339.7 0.69042 1.978(24) 1697. 1.9386 1.9850 33349.7 0.69062 1.971(24) 1707. 1.9393 1.9770 33359.7 0.69083 1.975(24) 1676. 1.9399 1.9665 33369.7 0.69104 1.964(24) 1698. 1.9406 1.9583 33379.7 0.69125 1.915(24) 1745. 1.9412 1.9536 33389.7 0.69145 1.973(24) 1693. 1.9419 1.9526 33399.7 0.69166 1.968(24) 1702. 1.9425 1.9565 33409.7 0.69187 1.944(24) 1757. 1.9432 1.9664 33419.8 0.69208 1.960(24) 1757. 1.9438 1.9800 33429.8 0.69228 1.984(24) 1721. 1.9444 1.9912 33439.8 0.69249 1.969(24) 1771. 1.9451 1.9994 33449.8 0.69270 1.986(24) 1769. 1.9457 2.0111 33459.9 0.69291 1.996(24) 1746. 1.9463 2.0255 33469.9 0.69312 1.981(24) 1765. 1.9470 2.0344 33480.0 0.69332 2.032(24) 1703. 1.9476 2.0395 33490.0 0.69353 2.042(24) 1699. 1.9482 2.0491 33500.0 0.69374 2.039(24) 1726. 1.9489 2.0573 33510.1 0.69395 2.028(24) 1746. 1.9495 2.0498 33520.2 0.69416 1.991(24) 1774. 1.9501 2.0293 33530.2 0.69436 2.003(24) 1784. 1.9508 2.0081 33540.3 0.69457 1.993(24) 1807. 1.9514 1.9932 33550.3 0.69478 1.987(23) 1817. 1.9520 1.9875 33560.4 0.69499 1.998(23) 1842. 1.9526 1.9916 33570.5 0.69520 2.025(24) 1788. 1.9533 2.0035 33580.5 0.69541 2.003(23) 1826. 1.9539 2.0178 33590.6 0.69562 1.998(23) 1876. 1.9545 2.0276 33600.7 0.69582 1.997(23) 1839. 1.9551 2.0265 33610.8 0.69603 2.013(23) 1823. 1.9558 2.0162 33620.8 0.69624 2.047(23) 1812. 1.9564 2.0061 33630.9 0.69645 2.009(23) 1856. 1.9570 2.0018 33641.0 0.69666 2.032(23) 1833. 1.9576 2.0030 33651.1 0.69687 2.034(23) 1826. 1.9583 2.0079 33661.2 0.69708 2.022(23) 1836. 1.9589 2.0149 33671.3 0.69729 2.057(23) 1816. 1.9595 2.0213 33681.4 0.69750 2.019(23) 1869. 1.9601 2.0281 33691.5 0.69771 2.086(24) 1794. 1.9607 2.0436 33701.6 0.69792 2.123(24) 1769. 1.9614 2.0722 33711.7 0.69812 2.106(24) 1795. 1.9620 2.1075 33721.8 0.69833 2.120(24) 1788. 1.9626 2.1365 33732.0 0.69854 2.134(24) 1792. 1.9632 2.1571 33742.1 0.69875 2.174(24) 1771. 1.9638 2.1817 33752.2 0.69896 2.145(24) 1787. 1.9644 2.1988 33762.3 0.69917 2.158(24) 1751. 1.9651 2.1820 33772.5 0.69938 2.107(23) 1836. 1.9657 2.1412 33782.6 0.69959 2.106(23) 1826. 1.9663 2.1039 33792.7 0.69980 2.085(23) 1871. 1.9669 2.0779 33802.9 0.70001 2.080(23) 1883. 1.9675 2.0553 33813.0 0.70022 2.071(23) 1894. 1.9682 2.0348 33823.1 0.70043 2.062(23) 1907. 1.9688 2.0243 33833.3 0.70064 2.053(23) 1950. 1.9694 2.0306 33843.4 0.70085 2.077(23) 1938. 1.9700 2.0516 33853.6 0.70106 2.143(23) 1842. 1.9706 2.0717 33863.8 0.70127 2.097(23) 1890. 1.9712 2.0711 33873.9 0.70148 2.045(23) 1967. 1.9719 2.0517 33884.1 0.70169 2.052(23) 1961. 1.9725 2.0293 33894.2 0.70191 2.022(22) 2004. 1.9731 2.0130 33904.4 0.70212 2.051(22) 1982. 1.9737 2.0036 33914.6 0.70233 2.060(23) 1967. 1.9743 1.9989 33924.8 0.70254 2.048(22) 1987. 1.9750 1.9973 33934.9 0.70275 2.044(22) 2019. 1.9756 1.9989 33945.1 0.70296 2.080(22) 1978. 1.9762 2.0057 33955.3 0.70317 2.063(22) 1988. 1.9768 2.0188 33965.5 0.70338 2.077(22) 1988. 1.9774 2.0376 33975.7 0.70359 2.108(23) 1952. 1.9781 2.0634 33985.9 0.70380 2.137(23) 1941. 1.9787 2.0972 33996.1 0.70401 2.114(23) 1967. 1.9793 2.1289 34006.3 0.70423 2.118(22) 1996. 1.9799 2.1528 34016.5 0.70444 2.161(23) 1962. 1.9806 2.1836 34026.7 0.70465 2.200(23) 1906. 1.9812 2.2236 34036.9 0.70486 2.162(23) 1949. 1.9818 2.2525 34047.1 0.70507 2.185(23) 1952. 1.9824 2.2616 34057.3 0.70528 2.182(23) 1934. 1.9831 2.2482 34067.5 0.70549 2.203(23) 1925. 1.9837 2.2101 34077.7 0.70571 2.162(22) 1987. 1.9843 2.1560 34088.0 0.70592 2.145(23) 1960. 1.9849 2.1037 34098.2 0.70613 2.096(22) 2037. 1.9856 2.0653 34108.4 0.70634 2.107(22) 2059. 1.9862 2.0436 34118.7 0.70655 2.067(22) 2117. 1.9868 2.0371 34128.9 0.70677 2.082(22) 2090. 1.9875 2.0417 34139.1 0.70698 2.122(22) 2059. 1.9881 2.0493 34149.4 0.70719 2.108(22) 2091. 1.9887 2.0522 34159.6 0.70740 2.085(22) 2101. 1.9893 2.0483 34169.9 0.70761 2.111(22) 2050. 1.9900 2.0384 34180.1 0.70783 2.078(22) 2088. 1.9906 2.0269 34190.4 0.70804 2.054(21) 2167. 1.9913 2.0170 34200.6 0.70825 2.068(22) 2131. 1.9919 2.0098 34210.9 0.70846 2.027(21) 2208. 1.9925 2.0052 34221.1 0.70868 2.049(21) 2211. 1.9932 2.0027 34231.4 0.70889 2.036(21) 2204. 1.9938 2.0021 34241.7 0.70910 2.028(21) 2242. 1.9944 2.0027 34252.0 0.70931 2.053(21) 2215. 1.9951 2.0046 34262.2 0.70953 2.062(21) 2198. 1.9957 2.0079 34272.5 0.70974 2.067(21) 2187. 1.9964 2.0137 34282.8 0.70995 2.070(21) 2189. 1.9970 2.0246 34293.1 0.71017 2.117(22) 2143. 1.9977 2.0434 34303.4 0.71038 2.080(21) 2213. 1.9983 2.0690 34313.7 0.71059 2.096(21) 2185. 1.9990 2.0910 34323.9 0.71081 2.130(22) 2139. 1.9996 2.0972 34334.2 0.71102 2.100(21) 2203. 2.0002 2.0917 34344.5 0.71123 2.136(22) 2154. 2.0009 2.0871 34354.8 0.71145 2.099(21) 2201. 2.0016 2.0860 34365.2 0.71166 2.101(21) 2219. 2.0022 2.0824 34375.5 0.71187 2.101(21) 2230. 2.0029 2.0727 34385.8 0.71209 2.082(21) 2246. 2.0035 2.0603 34396.1 0.71230 2.094(21) 2224. 2.0042 2.0504 34406.4 0.71251 2.121(21) 2206. 2.0048 2.0448 34416.7 0.71273 2.094(21) 2242. 2.0055 2.0436 34427.1 0.71294 2.090(21) 2284. 2.0061 2.0481 34437.4 0.71316 2.123(21) 2244. 2.0068 2.0621 34447.7 0.71337 2.112(21) 2276. 2.0075 2.0883 34458.1 0.71358 2.157(21) 2236. 2.0081 2.1220 34468.4 0.71380 2.188(21) 2180. 2.0088 2.1509 34478.7 0.71401 2.173(21) 2211. 2.0095 2.1695 34489.1 0.71423 2.212(21) 2182. 2.0101 2.1832 34499.4 0.71444 2.229(22) 2156. 2.0108 2.1958 34509.8 0.71466 2.246(22) 2139. 2.0115 2.1957 34520.1 0.71487 2.201(21) 2207. 2.0121 2.1809 34530.5 0.71508 2.205(21) 2236. 2.0128 2.1688 34540.8 0.71530 2.202(21) 2230. 2.0135 2.1670 34551.2 0.71551 2.228(21) 2189. 2.0142 2.1679 34561.6 0.71573 2.186(21) 2262. 2.0148 2.1700 34571.9 0.71594 2.197(21) 2273. 2.0155 2.1804 34582.3 0.71616 2.224(21) 2231. 2.0162 2.1900 34592.7 0.71637 2.235(21) 2266. 2.0169 2.1838 34603.1 0.71659 2.194(21) 2302. 2.0176 2.1653 34613.4 0.71680 2.208(21) 2287. 2.0183 2.1445 34623.8 0.71702 2.182(21) 2317. 2.0189 2.1257 34634.2 0.71723 2.177(21) 2328. 2.0196 2.1073 34644.6 0.71745 2.139(20) 2405. 2.0203 2.0912 34655.0 0.71766 2.121(20) 2427. 2.0210 2.0826 34665.4 0.71788 2.123(20) 2432. 2.0217 2.0796 34675.8 0.71809 2.117(20) 2433. 2.0224 2.0753 34686.2 0.71831 2.086(20) 2480. 2.0231 2.0698 34696.6 0.71853 2.157(21) 2379. 2.0238 2.0712 34707.0 0.71874 2.147(20) 2426. 2.0245 2.0875 34717.4 0.71896 2.150(20) 2430. 2.0252 2.1189 34727.8 0.71917 2.155(20) 2417. 2.0259 2.1506 34738.3 0.71939 2.151(20) 2443. 2.0266 2.1644 34748.7 0.71960 2.148(20) 2461. 2.0273 2.1620 34759.1 0.71982 2.149(20) 2458. 2.0280 2.1535 34769.5 0.72004 2.157(20) 2435. 2.0287 2.1398 34780.0 0.72025 2.156(20) 2462. 2.0294 2.1210 34790.4 0.72047 2.166(20) 2470. 2.0301 2.1064 34800.8 0.72068 2.145(20) 2520. 2.0308 2.1102 34811.3 0.72090 2.215(20) 2418. 2.0315 2.1427 34821.7 0.72112 2.260(21) 2363. 2.0323 2.1998 34832.2 0.72133 2.314(21) 2307. 2.0330 2.2541 34842.6 0.72155 2.274(21) 2374. 2.0337 2.2773 34853.1 0.72177 2.239(20) 2411. 2.0344 2.2625 34863.5 0.72198 2.226(20) 2472. 2.0351 2.2232 34874.0 0.72220 2.173(20) 2518. 2.0359 2.1784 34884.4 0.72242 2.168(20) 2536. 2.0366 2.1394 34894.9 0.72263 2.147(20) 2558. 2.0373 2.1090 34905.4 0.72285 2.100(19) 2641. 2.0380 2.0874 34915.8 0.72307 2.132(20) 2578. 2.0388 2.0749 34926.3 0.72328 2.143(20) 2572. 2.0395 2.0720 34936.8 0.72350 2.124(19) 2645. 2.0402 2.0773 34947.3 0.72372 2.144(20) 2620. 2.0410 2.0858 34957.8 0.72394 2.129(19) 2648. 2.0417 2.0893 34968.2 0.72415 2.102(19) 2698. 2.0424 2.0856 34978.7 0.72437 2.109(19) 2681. 2.0432 2.0805 34989.2 0.72459 2.117(19) 2679. 2.0439 2.0785 34999.7 0.72480 2.127(19) 2676. 2.0447 2.0816 35010.2 0.72502 2.124(19) 2657. 2.0454 2.0912 35020.7 0.72524 2.124(19) 2711. 2.0462 2.1081 35031.2 0.72546 2.109(19) 2729. 2.0469 2.1269 35041.7 0.72567 2.154(19) 2680. 2.0477 2.1369 35052.3 0.72589 2.139(19) 2690. 2.0484 2.1329 35062.8 0.72611 2.111(19) 2734. 2.0492 2.1255 35073.3 0.72633 2.154(19) 2715. 2.0499 2.1303 35084. 0.72655 2.173(19) 2659. 2.0507 2.1581 35094. 0.72676 2.218(19) 2641. 2.0514 2.2105 35105. 0.72698 2.259(20) 2597. 2.0522 2.2693 35115. 0.72720 2.215(19) 2646. 2.0529 2.2970 35126. 0.72742 2.245(20) 2590. 2.0537 2.2741 35136. 0.72764 2.224(19) 2641. 2.0545 2.2224 35147. 0.72786 2.142(19) 2792. 2.0552 2.1745 35158. 0.72807 2.143(19) 2782. 2.0560 2.1458 35168. 0.72829 2.179(19) 2741. 2.0568 2.1397 35179. 0.72851 2.177(19) 2746. 2.0576 2.1540 35189. 0.72873 2.194(19) 2723. 2.0583 2.1772 35200. 0.72895 2.150(19) 2774. 2.0591 2.1874 35210. 0.72917 2.151(19) 2792. 2.0599 2.1755 35221. 0.72939 2.162(19) 2783. 2.0607 2.1553 35231. 0.72960 2.140(19) 2807. 2.0614 2.1426 35242. 0.72982 2.149(19) 2813. 2.0622 2.1413 35253. 0.73004 2.141(19) 2850. 2.0630 2.1443 35263. 0.73026 2.133(19) 2889. 2.0638 2.1440 35274. 0.73048 2.144(19) 2862. 2.0646 2.1420 35284. 0.73070 2.160(19) 2868. 2.0654 2.1460 35295. 0.73092 2.188(19) 2819. 2.0662 2.1616 35306. 0.73114 2.205(19) 2773. 2.0670 2.1824 35316. 0.73136 2.212(19) 2771. 2.0678 2.1954 35327. 0.73158 2.190(19) 2835. 2.0686 2.2007 35337. 0.73180 2.197(19) 2838. 2.0694 2.2037 35348. 0.73202 2.196(19) 2855. 2.0702 2.1994 35359. 0.73224 2.154(19) 2906. 2.0710 2.1797 35369. 0.73246 2.162(19) 2909. 2.0718 2.1522 35380. 0.73268 2.148(18) 2936. 2.0726 2.1279 35390. 0.73290 2.106(18) 3013. 2.0734 2.1103 35401. 0.73312 2.112(18) 2998. 2.0742 2.0987 35412. 0.73334 2.110(18) 3036. 2.0750 2.0915 35422. 0.73356 2.113(18) 3021. 2.0758 2.0877 35433. 0.73378 2.117(18) 3005. 2.0766 2.0872 35443. 0.73400 2.119(18) 3001. 2.0774 2.0906 35454. 0.73422 2.108(18) 3053. 2.0782 2.0970 35465. 0.73444 2.121(18) 3050. 2.0791 2.1032 35475. 0.73466 2.118(18) 3029. 2.0799 2.1058 35486. 0.73488 2.156(18) 2955. 2.0807 2.1072 35497. 0.73510 2.142(18) 3016. 2.0815 2.1115 35507. 0.73532 2.124(18) 3070. 2.0824 2.1208 35518. 0.73554 2.112(18) 3102. 2.0832 2.1364 35529. 0.73576 2.203(18) 2966. 2.0840 2.1600 35539. 0.73598 2.183(18) 3007. 2.0848 2.1848 35550. 0.73620 2.163(18) 3034. 2.0857 2.1936 35561. 0.73642 2.191(18) 2983. 2.0865 2.1809 35571. 0.73664 2.128(18) 3111. 2.0874 2.1617 35582. 0.73686 2.146(18) 3095. 2.0882 2.1537 35593. 0.73709 2.172(18) 3039. 2.0890 2.1644 35603. 0.73731 2.185(18) 3037. 2.0899 2.1874 35614. 0.73753 2.181(18) 3072. 2.0907 2.2067 35625. 0.73775 2.206(18) 3049. 2.0916 2.2167 35635. 0.73797 2.238(18) 2974. 2.0924 2.2252 35646. 0.73819 2.205(18) 3039. 2.0933 2.2300 35657. 0.73841 2.174(18) 3108. 2.0941 2.2223 35667. 0.73864 2.203(18) 3056. 2.0950 2.2069 35678. 0.73886 2.183(18) 3126. 2.0958 2.1951 35689. 0.73908 2.226(18) 3015. 2.0967 2.1963 35700. 0.73930 2.215(18) 3079. 2.0975 2.2113 35710. 0.73952 2.239(18) 3017. 2.0984 2.2267 35721. 0.73974 2.198(18) 3084. 2.0992 2.2291 35732. 0.73997 2.177(18) 3131. 2.1001 2.2198 35742. 0.74019 2.181(18) 3159. 2.1010 2.2025 35753. 0.74041 2.179(18) 3161. 2.1018 2.1804 35764. 0.74063 2.162(18) 3147. 2.1027 2.1601 35775. 0.74085 2.123(18) 3263. 2.1036 2.1460 35785. 0.74108 2.113(17) 3287. 2.1044 2.1391 35796. 0.74130 2.126(17) 3270. 2.1053 2.1410 35807. 0.74152 2.125(17) 3283. 2.1062 2.1531 35818. 0.74174 2.153(18) 3227. 2.1070 2.1700 35828. 0.74197 2.173(18) 3232. 2.1079 2.1792 35839. 0.74219 2.152(17) 3274. 2.1088 2.1739 35850. 0.74241 2.129(17) 3328. 2.1097 2.1617 35861. 0.74264 2.110(17) 3375. 2.1106 2.1530 35871. 0.74286 2.158(18) 3259. 2.1114 2.1536 35882. 0.74308 2.155(17) 3308. 2.1123 2.1634 35893. 0.74330 2.171(18) 3246. 2.1132 2.1770 35904. 0.74353 2.183(18) 3251. 2.1141 2.1907 35914. 0.74375 2.178(17) 3301. 2.1150 2.2068 35925. 0.74397 2.160(17) 3344. 2.1159 2.2240 35936. 0.74420 2.219(18) 3214. 2.1168 2.2365 35947. 0.74442 2.224(18) 3233. 2.1176 2.2488 35957. 0.74464 2.215(17) 3281. 2.1185 2.2639 35968. 0.74487 2.196(17) 3297. 2.1194 2.2657 35979. 0.74509 2.169(17) 3360. 2.1203 2.2460 35990. 0.74531 2.158(17) 3358. 2.1212 2.2211 36001. 0.74554 2.166(17) 3356. 2.1221 2.2061 36011. 0.74576 2.155(17) 3408. 2.1230 2.2002 36022. 0.74599 2.174(17) 3341. 2.1239 2.1958 36033. 0.74621 2.151(17) 3438. 2.1248 2.1889 36044. 0.74643 2.134(17) 3461. 2.1257 2.1819 36055. 0.74666 2.150(17) 3414. 2.1267 2.1793 36065. 0.74688 2.185(17) 3387. 2.1276 2.1851 36076. 0.74711 2.165(17) 3451. 2.1285 2.2034 36087. 0.74733 2.205(17) 3353. 2.1294 2.2295 36098. 0.74755 2.182(17) 3389. 2.1303 2.2442 36109. 0.74778 2.199(17) 3372. 2.1312 2.2362 36120. 0.74800 2.168(17) 3458. 2.1321 2.2159 36130. 0.74823 2.153(17) 3496. 2.1330 2.1949 36141. 0.74845 2.154(17) 3488. 2.1340 2.1782 36152. 0.74868 2.170(17) 3449. 2.1349 2.1659 36163. 0.74890 2.144(17) 3529. 2.1358 2.1576 36174. 0.74913 2.167(17) 3482. 2.1367 2.1534 36185. 0.74935 2.168(17) 3460. 2.1376 2.1540 36196. 0.74957 2.131(17) 3577. 2.1386 2.1591 36206. 0.74980 2.159(17) 3562. 2.1395 2.1658 36217. 0.75002 2.177(17) 3500. 2.1404 2.1701 36228. 0.75025 2.151(17) 3584. 2.1414 2.1716 36239. 0.75047 2.169(17) 3564. 2.1423 2.1723 36250. 0.75070 2.161(17) 3577. 2.1432 2.1729 36261. 0.75093 2.186(17) 3524. 2.1441 2.1731 36272. 0.75115 2.157(17) 3578. 2.1451 2.1713 36282. 0.75138 2.126(17) 3659. 2.1460 2.1670 36293. 0.75160 2.134(16) 3678. 2.1470 2.1622 36304. 0.75183 2.140(17) 3664. 2.1479 2.1588 36315. 0.75205 2.117(16) 3705. 2.1488 2.1572 36326. 0.75228 2.138(16) 3683. 2.1498 2.1574 36337. 0.75250 2.136(16) 3685. 2.1507 2.1591 36348. 0.75273 2.124(16) 3716. 2.1517 2.1633 36359. 0.75296 2.175(17) 3642. 2.1526 2.1716 36370. 0.75318 2.162(17) 3654. 2.1535 2.1840 36381. 0.75341 2.178(17) 3653. 2.1545 2.1981 36391. 0.75363 2.207(17) 3594. 2.1554 2.2117 36402. 0.75386 2.219(17) 3586. 2.1564 2.2224 36413. 0.75409 2.218(17) 3597. 2.1573 2.2264 36424. 0.75431 2.201(17) 3617. 2.1583 2.2225 36435. 0.75454 2.200(17) 3654. 2.1592 2.2130 36446. 0.75477 2.188(17) 3641. 2.1602 2.2037 36457. 0.75499 2.219(17) 3642. 2.1611 2.1987 36468. 0.75522 2.216(17) 3649. 2.1621 2.1974 36479. 0.75544 2.206(17) 3656. 2.1631 2.1956 36490. 0.75567 2.180(16) 3688. 2.1640 2.1919 36501. 0.75590 2.170(16) 3746. 2.1650 2.1887 36512. 0.75613 2.205(17) 3646. 2.1659 2.1893 36523. 0.75635 2.207(17) 3642. 2.1669 2.1944 36534. 0.75658 2.204(16) 3713. 2.1679 2.2015 36545. 0.75681 2.160(16) 3806. 2.1688 2.2065 36556. 0.75703 2.193(16) 3727. 2.1698 2.2099 36567. 0.75726 2.199(16) 3727. 2.1707 2.2163 36578. 0.75749 2.240(17) 3659. 2.1717 2.2289 36588. 0.75771 2.233(16) 3685. 2.1727 2.2498 36599. 0.75794 2.280(17) 3608. 2.1736 2.2823 36610. 0.75817 2.268(17) 3640. 2.1746 2.3212 36621. 0.75840 2.305(17) 3572. 2.1756 2.3457 36632. 0.75862 2.294(17) 3598. 2.1766 2.3388 36643. 0.75885 2.266(17) 3671. 2.1775 2.3090 36654. 0.75908 2.239(16) 3728. 2.1785 2.2774 36665. 0.75931 2.256(16) 3733. 2.1795 2.2541 36676. 0.75954 2.251(16) 3724. 2.1804 2.2376 36687. 0.75976 2.243(16) 3739. 2.1814 2.2239 36698. 0.75999 2.260(16) 3710. 2.1824 2.2123 36709. 0.76022 2.250(16) 3715. 2.1834 2.2038 36720. 0.76045 2.216(16) 3814. 2.1844 2.1982 36731. 0.76068 2.195(16) 3842. 2.1853 2.1950 36742. 0.76090 2.197(16) 3866. 2.1863 2.1933 36753. 0.76113 2.189(16) 3889. 2.1873 2.1926 36765. 0.76136 2.182(16) 3913. 2.1883 2.1926 36776. 0.76159 2.165(16) 3909. 2.1893 2.1932 36787. 0.76182 2.186(16) 3878. 2.1902 2.1942 36798. 0.76205 2.203(16) 3854. 2.1912 2.1956 36809. 0.76228 2.192(16) 3929. 2.1922 2.1977 36820. 0.76250 2.181(16) 3936. 2.1932 2.2025 36831. 0.76273 2.190(16) 3948. 2.1942 2.2149 36842. 0.76296 2.201(16) 3944. 2.1952 2.2425 36853. 0.76319 2.264(16) 3795. 2.1962 2.2873 36864. 0.76342 2.273(16) 3820. 2.1971 2.3357 36875. 0.76365 2.271(16) 3808. 2.1981 2.3674 36886. 0.76388 2.324(16) 3720. 2.1991 2.3760 36897. 0.76411 2.330(16) 3747. 2.2001 2.3719 36908. 0.76434 2.330(16) 3715. 2.2011 2.3648 36919. 0.76457 2.296(16) 3754. 2.2021 2.3482 36930. 0.76480 2.286(16) 3841. 2.2031 2.3194 36941. 0.76502 2.277(16) 3838. 2.2041 2.2884 36952. 0.76525 2.296(16) 3813. 2.2051 2.2652 36964. 0.76548 2.243(16) 3938. 2.2061 2.2564 36975. 0.76571 2.276(16) 3870. 2.2071 2.2674 36986. 0.76594 2.315(16) 3793. 2.2081 2.3004 36997. 0.76617 2.323(16) 3787. 2.2091 2.3433 37008. 0.76640 2.315(16) 3855. 2.2101 2.3717 37019. 0.76663 2.321(16) 3858. 2.2110 2.3740 37030. 0.76686 2.323(16) 3840. 2.2120 2.3630 37041. 0.76709 2.358(16) 3747. 2.2130 2.3551 37052. 0.76732 2.350(16) 3764. 2.2140 2.3461 37063. 0.76755 2.307(16) 3881. 2.2150 2.3254 37075. 0.76778 2.316(16) 3886. 2.2160 2.2978 37086. 0.76801 2.304(16) 3868. 2.2170 2.2737 37097. 0.76825 2.254(16) 3995. 2.2180 2.2578 37108. 0.76848 2.225(16) 4073. 2.2190 2.2493 37119. 0.76871 2.242(16) 4023. 2.2200 2.2461 37130. 0.76894 2.259(16) 4012. 2.2210 2.2459 37141. 0.76917 2.271(16) 3967. 2.2221 2.2469 37153. 0.76940 2.269(16) 3985. 2.2231 2.2475 37164. 0.76963 2.263(16) 4006. 2.2241 2.2466 37175. 0.76986 2.262(16) 3999. 2.2251 2.2440 37186. 0.77009 2.272(16) 3997. 2.2261 2.2409 37197. 0.77032 2.254(16) 4060. 2.2271 2.2383 37208. 0.77055 2.246(16) 4096. 2.2281 2.2366 37219. 0.77078 2.235(16) 4093. 2.2291 2.2353 37231. 0.77102 2.232(16) 4115. 2.2301 2.2347 37242. 0.77125 2.222(15) 4163. 2.2311 2.2346 37253. 0.77148 2.228(16) 4099. 2.2321 2.2351 37264. 0.77171 2.224(16) 4140. 2.2331 2.2362 37275. 0.77194 2.231(15) 4178. 2.2341 2.2388 37286. 0.77217 2.237(16) 4155. 2.2351 2.2449 37298. 0.77241 2.246(16) 4109. 2.2361 2.2564 37309. 0.77264 2.270(16) 4064. 2.2371 2.2726 37320. 0.77287 2.277(16) 4071. 2.2381 2.2887 37331. 0.77310 2.257(16) 4111. 2.2392 2.3018 37342. 0.77333 2.245(15) 4180. 2.2402 2.3111 37354. 0.77356 2.257(16) 4139. 2.2412 2.3123 37365. 0.77380 2.272(16) 4097. 2.2422 2.3034 37376. 0.77403 2.257(16) 4157. 2.2432 2.2894 37387. 0.77426 2.237(15) 4220. 2.2442 2.2766 37398. 0.77449 2.251(15) 4203. 2.2452 2.2678 37410. 0.77473 2.258(15) 4173. 2.2462 2.2633 37421. 0.77496 2.279(16) 4134. 2.2472 2.2644 37432. 0.77519 2.299(16) 4108. 2.2482 2.2741 37443. 0.77542 2.294(15) 4165. 2.2493 2.2940 37455. 0.77566 2.325(16) 4098. 2.2503 2.3178 37466. 0.77589 2.358(16) 4009. 2.2513 2.3342 37477. 0.77612 2.333(16) 4105. 2.2523 2.3419 37488. 0.77636 2.346(16) 4062. 2.2533 2.3456 37500. 0.77659 2.329(16) 4141. 2.2543 2.3418 37511. 0.77682 2.314(16) 4142. 2.2553 2.3282 37522. 0.77705 2.300(15) 4170. 2.2563 2.3119 37533. 0.77729 2.294(15) 4195. 2.2573 2.3004 37545. 0.77752 2.304(15) 4176. 2.2583 2.2954 37556. 0.77775 2.288(15) 4239. 2.2594 2.2934 37567. 0.77799 2.288(15) 4220. 2.2604 2.2906 37578. 0.77822 2.323(16) 4142. 2.2614 2.2870 37590. 0.77845 2.315(15) 4180. 2.2624 2.2858 37601. 0.77869 2.308(15) 4248. 2.2634 2.2925 37612. 0.77892 2.298(15) 4271. 2.2644 2.3159 37624. 0.77916 2.347(15) 4191. 2.2654 2.3616 37635. 0.77939 2.387(16) 4095. 2.2664 2.4213 37646. 0.77962 2.384(16) 4145. 2.2674 2.4748 37657. 0.77986 2.435(16) 4045. 2.2685 2.5079 37669. 0.78009 2.489(16) 3958. 2.2695 2.5159 37680. 0.78032 2.494(16) 3961. 2.2705 2.5019 37691. 0.78056 2.457(16) 4008. 2.2715 2.4725 37703. 0.78079 2.426(16) 4085. 2.2725 2.4418 37714. 0.78103 2.399(16) 4153. 2.2735 2.4149 37725. 0.78126 2.376(15) 4203. 2.2745 2.3865 37737. 0.78150 2.365(15) 4249. 2.2755 2.3571 37748. 0.78173 2.341(15) 4302. 2.2765 2.3324 37759. 0.78197 2.302(15) 4409. 2.2775 2.3148 37771. 0.78220 2.298(15) 4437. 2.2786 2.3035 37782. 0.78243 2.279(15) 4475. 2.2796 2.2967 37793. 0.78267 2.331(15) 4312. 2.2806 2.2931 37805. 0.78290 2.302(15) 4424. 2.2816 2.2916 37816. 0.78314 2.294(15) 4440. 2.2826 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3.1386 3.1895 68364. 1.41595 3.230(18) 3128. 3.1388 3.1873 68384. 1.41637 3.206(18) 3133. 3.1391 3.1801 68405. 1.41680 3.206(18) 3141. 3.1393 3.1712 68425. 1.41722 3.183(18) 3167. 3.1395 3.1669 68446. 1.41765 3.195(18) 3161. 3.1398 3.1720 68466. 1.41807 3.204(18) 3154. 3.1400 3.1857 68487. 1.41850 3.187(18) 3163. 3.1402 3.1975 68507. 1.41892 3.217(18) 3124. 3.1405 3.1963 68528. 1.41935 3.198(18) 3155. 3.1407 3.1849 68548. 1.41978 3.172(18) 3187. 3.1409 3.1717 68569. 1.42020 3.172(18) 3161. 3.1412 3.1614 68590. 1.42063 3.158(18) 3206. 3.1414 3.1549 68610. 1.42105 3.169(18) 3176. 3.1417 3.1509 68631. 1.42148 3.171(18) 3181. 3.1419 3.1485 68651. 1.42191 3.150(18) 3208. 3.1421 3.1472 68672. 1.42233 3.162(18) 3163. 3.1424 3.1466 68692. 1.42276 3.165(18) 3173. 3.1426 3.1459 68713. 1.42319 3.158(18) 3166. 3.1429 3.1463 68734. 1.42361 3.166(18) 3157. 3.1432 3.1475 68754. 1.42404 3.159(18) 3180. 3.1434 3.1520 68775. 1.42447 3.180(18) 3145. 3.1437 3.1678 68796. 1.42490 3.223(18) 3091. 3.1439 3.2085 68816. 1.42532 3.246(18) 3059. 3.1442 3.2754 68837. 1.42575 3.298(18) 3001. 3.1445 3.3349 68857. 1.42618 3.319(18) 2957. 3.1447 3.3437 68878. 1.42661 3.304(18) 2988. 3.1450 3.3067 68899. 1.42703 3.271(18) 3010. 3.1453 3.2591 68919. 1.42746 3.237(18) 3027. 3.1455 3.2241 68940. 1.42789 3.212(18) 3046. 3.1458 3.2078 68961. 1.42832 3.180(18) 3071. 3.1461 3.2050 68982. 1.42875 3.182(18) 3073. 3.1463 3.2041 69002. 1.42918 3.192(18) 3080. 3.1466 3.1964 69023. 1.42961 3.216(18) 3025. 3.1469 3.1848 69044. 1.43003 3.191(18) 3052. 3.1472 3.1753 69064. 1.43046 3.196(18) 3021. 3.1475 3.1700 69085. 1.43089 3.207(18) 3005. 3.1477 3.1667 69106. 1.43132 3.199(18) 3008. 3.1480 3.1631 69127. 1.43175 3.189(18) 3015. 3.1483 3.1610 69147. 1.43218 3.159(18) 3055. 3.1486 3.1582 69168. 1.43261 3.188(18) 2997. 3.1489 3.1564 69189. 1.43304 3.176(18) 3013. 3.1492 3.1556 69210. 1.43347 3.216(18) 2941. 3.1495 3.1555 69230. 1.43390 3.231(19) 2916. 3.1498 3.1565 69251. 1.43433 3.345(19) 2785. 3.1501 3.1609 69272. 1.43476 3.433(19) 2693. 3.1504 3.1749 69293. 1.43519 3.459(19) 2692. 3.1507 3.2054 69313. 1.43562 3.522(19) 2643. 3.1510 3.2457 69334. 1.43605 3.518(19) 2676. 3.1513 3.2706 69355. 1.43648 3.457(19) 2728. 3.1516 3.2637 69376. 1.43692 3.402(19) 2787. 3.1519 3.2380 69397. 1.43735 3.325(19) 2853. 3.1522 3.2123 69417. 1.43778 3.225(18) 2963. 3.1525 3.1941 69438. 1.43821 3.200(18) 2983. 3.1528 3.1830 69459. 1.43864 3.167(18) 3008. 3.1531 3.1770 69480. 1.43907 3.169(18) 3019. 3.1534 3.1744 69501. 1.43950 3.163(18) 3032. 3.1538 3.1744 69522. 1.43994 3.151(18) 3026. 3.1541 3.1767 69542. 1.44037 3.167(18) 3023. 3.1544 3.1816 69563. 1.44080 3.202(18) 2975. 3.1547 3.1930 69584. 1.44123 3.256(18) 2944. 3.1550 3.2322 69605. 1.44167 3.445(19) 2794. 3.1554 3.3768 69626. 1.44210 3.844(20) 2526. 3.1557 3.7764 69647. 1.44253 4.573(22) 2071. 3.1560 4.4925 69668. 1.44296 5.339(24) 1675. 3.1564 5.2185 69689. 1.44340 5.667(26) 1532. 3.1567 5.4265 69710. 1.44383 5.219(24) 1713. 3.1570 5.0644 69730. 1.44426 4.562(22) 2028. 3.1574 4.5056 69751. 1.44470 4.020(21) 2355. 3.1577 4.0341 69772. 1.44513 3.685(20) 2598. 3.1580 3.7197 69793. 1.44556 3.455(19) 2791. 3.1584 3.5379 69814. 1.44600 3.367(19) 2868. 3.1587 3.4534 69835. 1.44643 3.320(19) 2922. 3.1591 3.4228 69856. 1.44687 3.279(18) 2960. 3.1594 3.3942 69877. 1.44730 3.247(18) 2989. 3.1598 3.3460 69898. 1.44773 3.229(18) 3013. 3.1601 3.2925 69919. 1.44817 3.204(18) 3050. 3.1605 3.2496 69940. 1.44860 3.185(18) 3066. 3.1608 3.2206 69961. 1.44904 3.202(18) 3055. 3.1612 3.2027 69982. 1.44947 3.195(18) 3061. 3.1615 3.1930 70003. 1.44991 3.188(18) 3065. 3.1619 3.1919 70024. 1.45034 3.176(18) 3089. 3.1622 3.2044 70045. 1.45078 3.213(18) 3045. 3.1626 3.2344 70066. 1.45121 3.226(18) 3050. 3.1630 3.2767 70087. 1.45165 3.277(18) 3013. 3.1633 3.3272 70108. 1.45208 3.344(18) 2936. 3.1637 3.3994 70129. 1.45252 3.490(19) 2785. 3.1641 3.4873 70150. 1.45296 3.593(19) 2711. 3.1644 3.5327 70171. 1.45339 3.553(19) 2736. 3.1648 3.5030 70192. 1.45383 3.489(19) 2786. 3.1652 3.4320 70213. 1.45426 3.430(19) 2842. 3.1655 3.3626 70234. 1.45470 3.319(18) 2949. 3.1659 3.3035 70255. 1.45514 3.269(18) 2994. 3.1663 3.2576 70276. 1.45557 3.243(18) 3002. 3.1667 3.2255 70297. 1.45601 3.230(18) 3027. 3.1671 3.2047 70319. 1.45645 3.214(18) 3031. 3.1674 3.1918 70340. 1.45688 3.175(18) 3085. 3.1678 3.1839 70361. 1.45732 3.191(18) 3053. 3.1682 3.1791 70382. 1.45776 3.204(18) 3010. 3.1686 3.1761 70403. 1.45820 3.168(18) 3065. 3.1690 3.1744 70424. 1.45863 3.180(18) 3056. 3.1694 3.1735 70445. 1.45907 3.178(18) 3044. 3.1698 3.1731 70466. 1.45951 3.175(18) 3038. 3.1701 3.1731 70487. 1.45995 3.183(18) 3026. 3.1705 3.1732 70509. 1.46038 3.201(18) 2995. 3.1709 3.1735 70530. 1.46082 3.191(18) 3012. 3.1713 3.1739 70551. 1.46126 3.172(18) 3045. 3.1717 3.1747 70572. 1.46170 3.171(18) 3019. 3.1721 3.1754 70593. 1.46214 3.165(18) 3021. 3.1725 3.1763 70614. 1.46258 3.163(18) 3026. 3.1729 3.1775 70636. 1.46302 3.180(18) 2982. 3.1733 3.1797 70657. 1.46345 3.167(18) 3014. 3.1738 3.1859 70678. 1.46389 3.229(18) 2934. 3.1742 3.2077 70699. 1.46433 3.272(19) 2907. 3.1746 3.2681 70720. 1.46477 3.410(19) 2781. 3.1750 3.3774 70742. 1.46521 3.554(19) 2632. 3.1754 3.4910 70763. 1.46565 3.696(20) 2474. 3.1758 3.5273 70784. 1.46609 3.677(20) 2484. 3.1762 3.4752 70805. 1.46653 3.530(20) 2630. 3.1766 3.3909 70827. 1.46697 3.418(19) 2728. 3.1771 3.3181 70848. 1.46741 3.343(19) 2780. 3.1775 3.2676 70869. 1.46785 3.233(19) 2883. 3.1779 3.2362 70890. 1.46829 3.219(19) 2901. 3.1783 3.2162 70912. 1.46873 3.193(18) 2942. 3.1788 3.2046 70933. 1.46917 3.184(18) 2950. 3.1792 3.1976 70954. 1.46961 3.229(19) 2876. 3.1796 3.1939 70975. 1.47006 3.240(19) 2885. 3.1800 3.1927 70997. 1.47050 3.213(19) 2910. 3.1805 3.1953 71018. 1.47094 3.243(19) 2904. 3.1809 3.2088 71039. 1.47138 3.228(19) 2910. 3.1813 3.2474 71061. 1.47182 3.282(19) 2860. 3.1818 3.3172 71082. 1.47226 3.359(19) 2775. 3.1822 3.3889 71103. 1.47270 3.434(19) 2702. 3.1826 3.4121 71125. 1.47315 3.386(19) 2758. 3.1831 3.3846 71146. 1.47359 3.334(19) 2817. 3.1835 3.3501 71167. 1.47403 3.313(19) 2828. 3.1840 3.3400 71189. 1.47447 3.286(19) 2867. 3.1844 3.3461 71210. 1.47492 3.290(19) 2840. 3.1848 3.3391 71231. 1.47536 3.247(19) 2910. 3.1853 3.3116 71253. 1.47580 3.278(19) 2890. 3.1857 3.2792 71274. 1.47624 3.238(18) 2932. 3.1862 3.2552 71296. 1.47669 3.215(18) 2963. 3.1866 3.2446 71317. 1.47713 3.337(19) 2822. 3.1871 3.2587 71338. 1.47757 3.420(19) 2786. 3.1875 3.3420 71360. 1.47802 3.697(20) 2549. 3.1880 3.5823 71381. 1.47846 4.078(21) 2284. 3.1885 4.0188 71403. 1.47890 4.505(22) 2014. 3.1889 4.4972 71424. 1.47935 4.794(23) 1850. 3.1894 4.7404 71445. 1.47979 4.695(23) 1899. 3.1898 4.6643 71467. 1.48023 4.380(22) 2066. 3.1903 4.3713 71488. 1.48068 4.047(21) 2280. 3.1908 4.0239 71510. 1.48112 3.699(20) 2548. 3.1912 3.7353 71531. 1.48157 3.504(19) 2704. 3.1917 3.5358 71553. 1.48201 3.398(19) 2802. 3.1922 3.4098 71574. 1.48246 3.316(19) 2861. 3.1926 3.3353 71596. 1.48290 3.287(19) 2900. 3.1931 3.3008 71617. 1.48335 3.291(19) 2878. 3.1936 3.3040 71639. 1.48379 3.323(19) 2850. 3.1940 3.3345 71660. 1.48424 3.346(19) 2805. 3.1945 3.3591 71682. 1.48468 3.413(19) 2718. 3.1950 3.3494 71703. 1.48513 3.361(19) 2780. 3.1955 3.3142 71725. 1.48557 3.308(19) 2838. 3.1959 3.2769 71746. 1.48602 3.276(19) 2863. 3.1964 3.2491 71768. 1.48646 3.249(19) 2885. 3.1969 3.2311 71789. 1.48691 3.207(19) 2914. 3.1974 3.2200 71811. 1.48736 3.218(19) 2906. 3.1978 3.2133 71832. 1.48780 3.196(18) 2926. 3.1983 3.2093 71854. 1.48825 3.238(19) 2855. 3.1988 3.2069 71875. 1.48870 3.221(19) 2875. 3.1993 3.2056 71897. 1.48914 3.172(18) 2923. 3.1998 3.2049 71918. 1.48959 3.209(19) 2856. 3.2003 3.2047 71940. 1.49004 3.211(19) 2861. 3.2008 3.2057 71962. 1.49048 3.212(19) 2853. 3.2013 3.2061 71983. 1.49093 3.210(19) 2843. 3.2017 3.2057 72005. 1.49138 3.211(19) 2835. 3.2022 3.2068 72026. 1.49183 3.211(19) 2835. 3.2027 3.2091 72048. 1.49227 3.245(19) 2786. 3.2032 3.2182 72070. 1.49272 3.255(19) 2777. 3.2037 3.2441 72091. 1.49317 3.299(19) 2726. 3.2042 3.2944 72113. 1.49362 3.335(19) 2678. 3.2047 3.3526 72134. 1.49407 3.356(19) 2651. 3.2052 3.3785 72156. 1.49451 3.333(19) 2677. 3.2057 3.3582 72178. 1.49496 3.363(20) 2619. 3.2062 3.3172 72199. 1.49541 3.329(19) 2653. 3.2067 3.2802 72221. 1.49586 3.274(19) 2701. 3.2072 3.2549 72243. 1.49631 3.266(19) 2703. 3.2077 3.2393 72264. 1.49676 3.269(19) 2671. 3.2082 3.2304 72286. 1.49721 3.267(19) 2682. 3.2087 3.2257 72308. 1.49766 3.230(19) 2716. 3.2092 3.2237 72329. 1.49811 3.291(19) 2657. 3.2098 3.2237 72351. 1.49855 3.278(19) 2652. 3.2103 3.2256 72373. 1.49900 3.293(19) 2639. 3.2108 3.2309 72395. 1.49945 3.291(19) 2664. 3.2113 3.2507 72416. 1.49990 3.383(20) 2598. 3.2118 3.3197 72438. 1.50035 3.566(20) 2460. 3.2123 3.5144 72460. 1.50080 3.827(21) 2262. 3.2128 3.8729 72481. 1.50125 4.119(22) 2051. 3.2133 4.2510 72503. 1.50171 4.282(23) 1923. 3.2139 4.3765 72525. 1.50216 4.157(22) 2002. 3.2144 4.2017 72547. 1.50261 3.912(21) 2177. 3.2149 3.9148 72569. 1.50306 3.709(21) 2306. 3.2154 3.6711 72590. 1.50351 3.546(20) 2420. 3.2159 3.5055 72612. 1.50396 3.396(20) 2570. 3.2165 3.4034 72634. 1.50441 3.353(20) 2608. 3.2170 3.3425 72656. 1.50486 3.337(20) 2600. 3.2175 3.3074 72677. 1.50531 3.300(19) 2641. 3.2180 3.2884 72699. 1.50577 3.286(19) 2667. 3.2186 3.2797 72721. 1.50622 3.266(19) 2681. 3.2191 3.2780 72743. 1.50667 3.265(19) 2684. 3.2196 3.2815 72765. 1.50712 3.285(19) 2674. 3.2201 3.2884 72787. 1.50757 3.311(19) 2650. 3.2207 3.2988 72808. 1.50803 3.320(19) 2637. 3.2212 3.3137 72830. 1.50848 3.338(19) 2633. 3.2217 3.3427 72852. 1.50893 3.437(20) 2589. 3.2223 3.4222 72874. 1.50938 3.621(20) 2482. 3.2228 3.6395 72896. 1.50984 4.044(21) 2213. 3.2233 4.0627 72918. 1.51029 4.550(23) 1900. 3.2239 4.5616 72939. 1.51074 4.892(24) 1725. 3.2244 4.8045 72961. 1.51120 4.812(24) 1756. 3.2249 4.6796 72983. 1.51165 4.493(23) 1913. 3.2255 4.4385 73005. 1.51210 4.300(22) 2029. 3.2260 4.3493 73027. 1.51256 4.356(22) 1997. 3.2265 4.4675 73049. 1.51301 4.583(23) 1887. 3.2271 4.6850 73071. 1.51346 4.970(24) 1748. 3.2276 5.0051 73093. 1.51392 5.609(26) 1510. 3.2282 5.5413 73115. 1.51437 6.279(28) 1280. 3.2287 6.0543 73137. 1.51483 6.380(29) 1225. 3.2292 6.0444 73159. 1.51528 5.646(26) 1437. 3.2298 5.5022 73181. 1.51574 4.866(24) 1727. 3.2303 4.8231 73203. 1.51619 4.271(22) 2014. 3.2309 4.2868 73224. 1.51665 3.934(21) 2216. 3.2314 3.9571 73246. 1.51710 3.799(21) 2300. 3.2320 3.8167 73268. 1.51756 3.828(21) 2293. 3.2325 3.8208 73290. 1.51801 3.918(21) 2186. 3.2331 3.8732 73312. 1.51847 4.030(22) 2104. 3.2336 3.8838 73334. 1.51892 4.008(22) 2145. 3.2342 3.8967 73356. 1.51938 3.968(21) 2188. 3.2347 3.9938 73378. 1.51983 4.052(22) 2118. 3.2353 4.1276 73400. 1.52029 4.075(22) 2105. 3.2358 4.1774 73422. 1.52075 4.017(22) 2146. 3.2364 4.1435 73444. 1.52120 3.978(22) 2146. 3.2369 4.0663 73466. 1.52166 3.913(22) 2163. 3.2375 3.9278 73489. 1.52212 3.729(21) 2281. 3.2380 3.7465 73511. 1.52257 3.566(20) 2407. 3.2386 3.5794 73533. 1.52303 3.442(20) 2496. 3.2391 3.4578 73555. 1.52349 3.398(20) 2518. 3.2397 3.3812 73577. 1.52394 3.326(20) 2566. 3.2402 3.3331 73599. 1.52440 3.294(20) 2597. 3.2408 3.3038 73621. 1.52486 3.273(20) 2600. 3.2413 3.2861 73643. 1.52532 3.286(20) 2586. 3.2419 3.2757 73665. 1.52577 3.260(20) 2586. 3.2425 3.2698 73687. 1.52623 3.241(20) 2611. 3.2430 3.2670 73709. 1.52669 3.246(20) 2583. 3.2436 3.2665 73731. 1.52715 3.274(20) 2559. 3.2441 3.2694 73754. 1.52761 3.329(20) 2517. 3.2447 3.2834 73776. 1.52806 3.357(20) 2490. 3.2452 3.3356 73798. 1.52852 3.477(20) 2397. 3.2458 3.4733 73820. 1.52898 3.680(21) 2245. 3.2464 3.7044 73842. 1.52944 3.859(22) 2122. 3.2469 3.9143 73864. 1.52990 3.881(22) 2089. 3.2475 3.9511 73886. 1.53036 3.745(21) 2182. 3.2480 3.8225 73909. 1.53082 3.602(21) 2289. 3.2486 3.6491 73931. 1.53128 3.459(20) 2388. 3.2492 3.5112 73953. 1.53174 3.368(20) 2455. 3.2497 3.4227 73975. 1.53220 3.360(20) 2466. 3.2503 3.3765 73997. 1.53266 3.407(20) 2435. 3.2509 3.3789 74019. 1.53312 3.568(21) 2342. 3.2514 3.4929 74042. 1.53358 3.965(22) 2094. 3.2520 3.8457 74064. 1.53404 4.559(24) 1761. 3.2526 4.4735 74086. 1.53450 5.168(26) 1479. 3.2531 5.0833 74108. 1.53496 5.249(26) 1436. 3.2537 5.2214 74131. 1.53542 4.829(25) 1606. 3.2543 4.8740 74153. 1.53588 4.315(23) 1851. 3.2548 4.3763 74175. 1.53634 3.899(22) 2091. 3.2554 3.9679 74197. 1.53680 3.611(21) 2287. 3.2560 3.6964 74220. 1.53726 3.446(20) 2411. 3.2565 3.5287 74242. 1.53772 3.376(20) 2462. 3.2571 3.4269 74264. 1.53818 3.351(20) 2457. 3.2577 3.3650 74286. 1.53865 3.279(20) 2531. 3.2582 3.3274 74309. 1.53911 3.284(20) 2525. 3.2588 3.3044 74331. 1.53957 3.271(20) 2545. 3.2594 3.2902 74353. 1.54003 3.271(20) 2554. 3.2599 3.2828 74376. 1.54049 3.254(20) 2579. 3.2605 3.2775 74398. 1.54096 3.257(20) 2567. 3.2611 3.2743 74420. 1.54142 3.247(20) 2574. 3.2616 3.2718 74443. 1.54188 3.233(20) 2600. 3.2622 3.2714 74465. 1.54234 3.245(20) 2575. 3.2628 3.2709 74487. 1.54281 3.257(20) 2580. 3.2634 3.2709 74510. 1.54327 3.228(20) 2606. 3.2639 3.2711 74532. 1.54373 3.264(20) 2565. 3.2645 3.2715 74554. 1.54419 3.254(20) 2582. 3.2651 3.2720 74577. 1.54466 3.260(20) 2567. 3.2656 3.2728 74599. 1.54512 3.285(20) 2533. 3.2662 3.2736 74621. 1.54559 3.302(20) 2516. 3.2668 3.2747 74644. 1.54605 3.256(20) 2546. 3.2674 3.2759 74666. 1.54651 3.252(20) 2560. 3.2679 3.2755 74689. 1.54698 3.292(20) 2511. 3.2685 3.2775 74711. 1.54744 3.260(20) 2553. 3.2691 3.2798 74733. 1.54791 3.262(20) 2553. 3.2696 3.2828 74756. 1.54837 3.305(20) 2503. 3.2702 3.2868 74778. 1.54883 3.289(20) 2519. 3.2708 3.2929 74801. 1.54930 3.246(20) 2586. 3.2714 3.3071 74823. 1.54976 3.324(20) 2491. 3.2719 3.3568 74846. 1.55023 3.467(20) 2388. 3.2725 3.5177 74868. 1.55069 3.776(21) 2179. 3.2731 3.8827 74890. 1.55116 4.273(23) 1869. 3.2736 4.3990 74913. 1.55162 4.698(25) 1646. 3.2742 4.7731 74935. 1.55209 4.790(25) 1613. 3.2748 4.8080 74958. 1.55256 4.724(24) 1671. 3.2754 4.6852 74980. 1.55302 4.719(25) 1656. 3.2759 4.5926 75003. 1.55349 4.689(25) 1637. 3.2765 4.4667 75025. 1.55395 4.405(24) 1762. 3.2771 4.2240 75048. 1.55442 4.090(23) 1908. 3.2777 3.9377 75070. 1.55489 3.771(22) 2090. 3.2782 3.7017 75093. 1.55535 3.591(21) 2202. 3.2788 3.5423 75115. 1.55582 3.455(21) 2293. 3.2794 3.4433 75138. 1.55629 3.407(21) 2307. 3.2799 3.3833 75160. 1.55675 3.372(21) 2321. 3.2805 3.3469 75183. 1.55722 3.278(20) 2408. 3.2811 3.3249 75206. 1.55769 3.360(21) 2313. 3.2817 3.3116 75228. 1.55816 3.311(21) 2364. 3.2822 3.3036 75251. 1.55862 3.287(21) 2376. 3.2828 3.2989 75273. 1.55909 3.318(21) 2330. 3.2834 3.2962 75296. 1.55956 3.304(21) 2361. 3.2840 3.2951 75318. 1.56003 3.307(21) 2344. 3.2845 3.2960 75341. 1.56049 3.318(21) 2320. 3.2851 3.3029 75364. 1.56096 3.304(21) 2342. 3.2857 3.3271 75386. 1.56143 3.362(21) 2297. 3.2862 3.3817 75409. 1.56190 3.449(21) 2211. 3.2868 3.4565 75432. 1.56237 3.437(21) 2222. 3.2874 3.5044 75454. 1.56284 3.443(21) 2214. 3.2879 3.4918 75477. 1.56331 3.440(21) 2209. 3.2885 3.4408 75499. 1.56378 3.392(21) 2245. 3.2891 3.3901 75522. 1.56424 3.346(21) 2281. 3.2897 3.3531 75545. 1.56471 3.336(21) 2296. 3.2902 3.3299 75567. 1.56518 3.320(21) 2295. 3.2908 3.3153 75590. 1.56565 3.286(21) 2335. 3.2914 3.3073 75613. 1.56612 3.308(21) 2323. 3.2919 3.3028 75635. 1.56659 3.317(21) 2306. 3.2925 3.3003 75658. 1.56706 3.312(21) 2316. 3.2931 3.2991 75681. 1.56753 3.270(21) 2359. 3.2936 3.2986 75704. 1.56800 3.299(21) 2323. 3.2942 3.2987 75726. 1.56847 3.290(21) 2331. 3.2948 3.2991 75749. 1.56894 3.325(21) 2296. 3.2954 3.2997 75772. 1.56942 3.307(21) 2316. 3.2959 3.3005 75794. 1.56989 3.296(21) 2327. 3.2965 3.3015 75817. 1.57036 3.316(21) 2313. 3.2971 3.3027 75840. 1.57083 3.306(21) 2319. 3.2976 3.3041 75863. 1.57130 3.357(21) 2290. 3.2982 3.3058 75885. 1.57177 3.345(21) 2299. 3.2988 3.3079 75908. 1.57224 3.341(21) 2314. 3.2993 3.3106 75931. 1.57272 3.345(21) 2319. 3.2999 3.3144 75954. 1.57319 3.321(21) 2351. 3.3004 3.3211 75977. 1.57366 3.412(21) 2270. 3.3010 3.3403 75999. 1.57413 3.495(21) 2218. 3.3016 3.4082 76022. 1.57460 3.706(22) 2101. 3.3021 3.6060 76045. 1.57508 4.037(23) 1919. 3.3027 3.9978 76068. 1.57555 4.457(24) 1693. 3.3033 4.4738 76091. 1.57602 4.676(25) 1589. 3.3038 4.7319 76113. 1.57649 4.668(25) 1584. 3.3044 4.6124 76136. 1.57697 4.352(24) 1728. 3.3050 4.2753 76159. 1.57744 3.982(23) 1913. 3.3055 3.9399 76182. 1.57791 3.757(22) 2036. 3.3061 3.6985 76205. 1.57839 3.567(21) 2167. 3.3066 3.5464 76228. 1.57886 3.484(21) 2215. 3.3072 3.4545 76250. 1.57933 3.410(21) 2278. 3.3078 3.3993 76273. 1.57981 3.374(21) 2281. 3.3083 3.3661 76296. 1.58028 3.357(21) 2287. 3.3089 3.3462 76319. 1.58076 3.319(21) 2323. 3.3094 3.3342 76342. 1.58123 3.334(21) 2308. 3.3100 3.3269 76365. 1.58171 3.314(21) 2306. 3.3106 3.3225 76388. 1.58218 3.337(21) 2280. 3.3111 3.3199 76411. 1.58265 3.358(21) 2247. 3.3117 3.3184 76434. 1.58313 3.312(21) 2297. 3.3122 3.3175 76457. 1.58360 3.333(21) 2276. 3.3128 3.3171 76480. 1.58408 3.328(21) 2269. 3.3133 3.3169 76502. 1.58456 3.345(21) 2242. 3.3139 3.3170 76525. 1.58503 3.314(21) 2270. 3.3144 3.3171 76548. 1.58551 3.329(21) 2246. 3.3150 3.3175 76571. 1.58598 3.319(21) 2255. 3.3155 3.3180 76594. 1.58646 3.319(21) 2250. 3.3161 3.3184 76617. 1.58693 3.285(21) 2278. 3.3167 3.3188 76640. 1.58741 3.308(21) 2235. 3.3172 3.3186 76663. 1.58789 3.384(21) 2176. 3.3178 3.3183 76686. 1.58836 3.345(21) 2210. 3.3183 3.3189 76709. 1.58884 3.340(21) 2190. 3.3189 3.3195 76732. 1.58932 3.327(21) 2206. 3.3194 3.3201 76755. 1.58979 3.284(21) 2228. 3.3200 3.3207 76778. 1.59027 3.331(21) 2190. 3.3205 3.3214 76801. 1.59075 3.335(21) 2170. 3.3211 3.3220 76824. 1.59122 3.298(21) 2201. 3.3216 3.3227 76847. 1.59170 3.349(22) 2161. 3.3221 3.3252 76871. 1.59218 3.333(22) 2154. 3.3227 3.3261 76894. 1.59266 3.333(22) 2150. 3.3232 3.3270 76917. 1.59314 3.363(22) 2130. 3.3238 3.3280 76940. 1.59361 3.364(22) 2122. 3.3243 3.3292 76963. 1.59409 3.387(22) 2102. 3.3249 3.3322 76986. 1.59457 3.328(22) 2162. 3.3254 3.3339 77009. 1.59505 3.340(22) 2152. 3.3260 3.3361 77032. 1.59553 3.367(22) 2112. 3.3265 3.3400 77055. 1.59601 3.390(22) 2111. 3.3270 3.3507 77078. 1.59648 3.405(22) 2096. 3.3276 3.3827 77101. 1.59696 3.478(22) 2054. 3.3281 3.4580 77125. 1.59744 3.574(22) 1996. 3.3287 3.5828 77148. 1.59792 3.666(23) 1934. 3.3292 3.7154 77171. 1.59840 3.701(23) 1904. 3.3297 3.7861 77194. 1.59888 3.657(23) 1939. 3.3303 3.7563 77217. 1.59936 3.610(23) 1964. 3.3308 3.6597 77240. 1.59984 3.517(22) 2047. 3.3313 3.5578 77263. 1.60032 3.440(22) 2095. 3.3319 3.4835 77287. 1.60080 3.395(22) 2130. 3.3324 3.4389 77310. 1.60128 3.388(22) 2133. 3.3329 3.4177 77333. 1.60176 3.395(22) 2144. 3.3335 3.4193 77356. 1.60224 3.445(22) 2139. 3.3340 3.4763 77379. 1.60272 3.678(22) 1992. 3.3345 3.6955 77403. 1.60320 4.251(24) 1719. 3.3351 4.2264 77426. 1.60369 5.122(27) 1365. 3.3356 5.0201 77449. 1.60417 5.799(29) 1151. 3.3361 5.6332 77472. 1.60465 5.755(29) 1177. 3.3367 5.6878 77496. 1.60513 5.405(28) 1304. 3.3372 5.4776 77519. 1.60561 5.352(27) 1343. 3.3377 5.5062 77542. 1.60609 5.605(28) 1242. 3.3382 5.7951 77565. 1.60657 5.749(29) 1179. 3.3388 5.8609 77589. 1.60706 5.394(28) 1274. 3.3393 5.4535 77612. 1.60754 4.780(26) 1484. 3.3398 4.8326 77635. 1.60802 4.217(24) 1722. 3.3403 4.2938 77658. 1.60850 3.847(23) 1901. 3.3409 3.9282 77682. 1.60899 3.627(22) 2016. 3.3414 3.7029 77705. 1.60947 3.469(22) 2127. 3.3419 3.5675 77728. 1.60995 3.432(22) 2145. 3.3424 3.4863 77752. 1.61044 3.385(22) 2147. 3.3430 3.4376 77775. 1.61092 3.391(22) 2156. 3.3435 3.4093 77798. 1.61140 3.384(22) 2150. 3.3440 3.3950 77822. 1.61189 3.327(21) 2213. 3.3445 3.3985 77845. 1.61237 3.427(22) 2130. 3.3450 3.4410 77868. 1.61285 3.538(22) 2058. 3.3455 3.5515 77892. 1.61334 3.713(23) 1927. 3.3461 3.7137 77915. 1.61382 3.850(23) 1825. 3.3466 3.8278 77939. 1.61431 3.838(23) 1825. 3.3471 3.8091 77962. 1.61479 3.720(23) 1898. 3.3476 3.6991 77985. 1.61527 3.555(22) 1999. 3.3481 3.5805 78009. 1.61576 3.471(22) 2046. 3.3486 3.4934 78032. 1.61624 3.419(22) 2065. 3.3491 3.4363 78055. 1.61673 3.365(22) 2107. 3.3496 3.4036 78079. 1.61721 3.341(22) 2115. 3.3502 3.3842 78102. 1.61770 3.306(22) 2136. 3.3507 3.3727 78126. 1.61818 3.298(22) 2154. 3.3512 3.3638 78149. 1.61867 3.307(22) 2134. 3.3517 3.3600 78173. 1.61916 3.319(22) 2112. 3.3522 3.3581 78196. 1.61964 3.300(22) 2119. 3.3527 3.3569 78220. 1.62013 3.329(22) 2088. 3.3532 3.3564 78243. 1.62061 3.309(22) 2107. 3.3537 3.3562 78267. 1.62110 3.318(22) 2089. 3.3542 3.3563 78290. 1.62159 3.346(22) 2056. 3.3547 3.3565 78313. 1.62207 3.335(22) 2074. 3.3552 3.3568 78337. 1.62256 3.318(22) 2074. 3.3557 3.3572 78360. 1.62305 3.275(22) 2107. 3.3562 3.3576 78384. 1.62353 3.282(22) 2099. 3.3567 3.3580 78407. 1.62402 3.304(22) 2074. 3.3572 3.3585 78431. 1.62451 3.325(22) 2056. 3.3577 3.3590 78455. 1.62500 3.318(22) 2059. 3.3582 3.3596 78478. 1.62548 3.316(22) 2064. 3.3587 3.3601 78502. 1.62597 3.320(22) 2078. 3.3592 3.3603 78525. 1.62646 3.310(22) 2080. 3.3597 3.3610 78549. 1.62695 3.335(22) 2042. 3.3602 3.3617 78572. 1.62743 3.301(22) 2077. 3.3607 3.3626 78596. 1.62792 3.259(22) 2099. 3.3612 3.3635 78619. 1.62841 3.298(22) 2078. 3.3616 3.3648 78643. 1.62890 3.303(22) 2074. 3.3621 3.3669 78667. 1.62939 3.345(22) 2047. 3.3626 3.3728 78690. 1.62988 3.371(22) 2045. 3.3631 3.3931 78714. 1.63037 3.428(22) 2025. 3.3636 3.4470 78737. 1.63086 3.592(23) 1910. 3.3641 3.5407 78761. 1.63135 3.712(23) 1834. 3.3646 3.6317 78785. 1.63183 3.769(24) 1799. 3.3651 3.6530 78808. 1.63232 3.696(23) 1847. 3.3655 3.6017 78832. 1.63281 3.519(23) 1964. 3.3660 3.5276 78856. 1.63330 3.434(22) 2021. 3.3665 3.4672 78879. 1.63379 3.379(22) 2064. 3.3670 3.4279 78903. 1.63428 3.330(22) 2095. 3.3675 3.4042 78927. 1.63477 3.331(22) 2082. 3.3680 3.3904 78950. 1.63527 3.322(22) 2091. 3.3684 3.3824 78974. 1.63576 3.272(22) 2151. 3.3689 3.3777 78998. 1.63625 3.313(22) 2102. 3.3694 3.3752 79021. 1.63674 3.291(22) 2143. 3.3699 3.3738 79045. 1.63723 3.291(22) 2131. 3.3703 3.3731 79069. 1.63772 3.320(22) 2108. 3.3708 3.3729 79093. 1.63821 3.320(22) 2100. 3.3713 3.3730 79116. 1.63870 3.332(22) 2103. 3.3718 3.3735 79140. 1.63920 3.317(22) 2123. 3.3722 3.3747 79164. 1.63969 3.302(22) 2133. 3.3727 3.3773 79187. 1.64018 3.307(22) 2125. 3.3732 3.3808 79211. 1.64067 3.352(22) 2090. 3.3737 3.3833 79235. 1.64116 3.337(22) 2095. 3.3741 3.3833 79259. 1.64166 3.318(22) 2119. 3.3746 3.3816 79283. 1.64215 3.305(22) 2112. 3.3751 3.3798 79306. 1.64264 3.330(22) 2091. 3.3755 3.3787 79330. 1.64313 3.282(22) 2115. 3.3760 3.3781 79354. 1.64363 3.274(22) 2129. 3.3765 3.3780 79378. 1.64412 3.304(22) 2106. 3.3769 3.3786 79402. 1.64461 3.309(22) 2114. 3.3774 3.3786 79425. 1.64511 3.317(22) 2091. 3.3779 3.3791 79449. 1.64560 3.337(22) 2058. 3.3783 3.3796 79473. 1.64609 3.296(22) 2088. 3.3788 3.3802 79497. 1.64659 3.284(22) 2085. 3.3792 3.3808 79521. 1.64708 3.291(22) 2079. 3.3797 3.3815 79545. 1.64758 3.269(22) 2097. 3.3802 3.3824 79568. 1.64807 3.322(22) 2049. 3.3806 3.3836 79592. 1.64857 3.266(22) 2084. 3.3811 3.3864 79616. 1.64906 3.307(22) 2052. 3.3815 3.3952 79640. 1.64956 3.351(22) 2038. 3.3820 3.4176 79664. 1.65005 3.434(23) 1948. 3.3824 3.4549 79688. 1.65055 3.481(23) 1879. 3.3829 3.4897 79712. 1.65104 3.461(23) 1887. 3.3834 3.4965 79736. 1.65154 3.507(23) 1871. 3.3838 3.4762 79760. 1.65203 3.458(23) 1914. 3.3843 3.4484 79784. 1.65253 3.453(23) 1907. 3.3847 3.4267 79807. 1.65302 3.434(23) 1854. 3.3852 3.4139 79831. 1.65352 3.405(23) 1828. 3.3856 3.4091 79855. 1.65402 3.427(23) 1812. 3.3861 3.4148 79879. 1.65451 3.446(24) 1776. 3.3865 3.4431 79903. 1.65501 3.533(24) 1686. 3.3870 3.5214 79927. 1.65550 3.670(25) 1586. 3.3874 3.6750 79951. 1.65600 3.883(26) 1443. 3.3879 3.8638 79975. 1.65650 4.039(27) 1339. 3.3883 3.9654 79999. 1.65700 3.919(27) 1390. 3.3888 3.9103 80023. 1.65749 3.746(26) 1456. 3.3892 3.7691 80047. 1.65799 3.644(26) 1504. 3.3896 3.6335 80071. 1.65849 3.488(25) 1586. 3.3901 3.5389 80095. 1.65898 3.405(25) 1631. 3.3905 3.4810 80119. 1.65948 3.359(25) 1649. 3.3910 3.4470 80143. 1.65998 3.364(25) 1641. 3.3914 3.4273 80167. 1.66048 3.356(25) 1641. 3.3919 3.4159 80191. 1.66098 3.348(25) 1659. 3.3923 3.4095 80215. 1.66148 3.343(25) 1656. 3.3927 3.4061 80239. 1.66197 3.301(24) 1693. 3.3932 3.4045 80264. 1.66247 3.372(25) 1636. 3.3936 3.4045 80288. 1.66297 3.369(25) 1648. 3.3941 3.4050 80312. 1.66347 3.350(25) 1657. 3.3945 3.4062 80336. 1.66397 3.358(25) 1664. 3.3949 3.4079 80360. 1.66447 3.380(25) 1638. 3.3954 3.4107 80384. 1.66497 3.371(24) 1668. 3.3958 3.4148 80408. 1.66547 3.377(25) 1659. 3.3962 3.4221 80432. 1.66597 3.385(24) 1673. 3.3967 3.4432 80456. 1.66647 3.466(25) 1640. 3.3971 3.5203 80481. 1.66697 3.712(26) 1526. 3.3975 3.7529 80505. 1.66747 4.117(27) 1386. 3.3980 4.2285 80529. 1.66797 4.863(30) 1140. 3.3984 4.8211 80553. 1.66847 5.388(32) 995. 3.3988 5.1487 80577. 1.66897 5.269(31) 1028. 3.3993 5.0037 80601. 1.66947 4.805(30) 1147. 3.3997 4.5832 80626. 1.66997 4.270(28) 1296. 3.4001 4.1648 80650. 1.67047 3.907(26) 1437. 3.4006 3.8664 80674. 1.67097 3.644(25) 1559. 3.4010 3.6815 80698. 1.67147 3.533(25) 1591. 3.4014 3.5736 80722. 1.67198 3.470(25) 1611. 3.4018 3.5104 80747. 1.67248 3.456(25) 1604. 3.4023 3.4752 80771. 1.67298 3.418(25) 1657. 3.4027 3.4613 80795. 1.67348 3.423(25) 1655. 3.4031 3.4790 80819. 1.67398 3.498(25) 1603. 3.4036 3.5554 80843. 1.67449 3.731(26) 1506. 3.4040 3.6990 80868. 1.67499 3.852(26) 1442. 3.4044 3.8431 80892. 1.67549 3.920(27) 1396. 3.4048 3.8786 80916. 1.67599 3.838(26) 1443. 3.4053 3.7973 80941. 1.67650 3.693(26) 1503. 3.4057 3.6816 80965. 1.67700 3.614(26) 1518. 3.4061 3.5982 80989. 1.67750 3.542(25) 1567. 3.4065 3.5740 81013. 1.67801 3.550(25) 1594. 3.4069 3.6032 81038. 1.67851 3.574(25) 1598. 3.4074 3.6454 81062. 1.67901 3.653(25) 1570. 3.4078 3.6494 81086. 1.67952 3.652(25) 1595. 3.4082 3.6090 81111. 1.68002 3.574(25) 1658. 3.4086 3.5538 81135. 1.68053 3.555(24) 1700. 3.4090 3.5089 81159. 1.68103 3.529(24) 1721. 3.4095 3.4830 81184. 1.68153 3.508(24) 1730. 3.4099 3.4816 81208. 1.68204 3.653(25) 1647. 3.4103 3.5426 81232. 1.68254 3.784(25) 1597. 3.4107 3.7409 81257. 1.68305 4.084(26) 1467. 3.4111 4.1161 81281. 1.68355 4.613(29) 1231. 3.4116 4.5166 81306. 1.68406 4.906(30) 1122. 3.4120 4.6495 81330. 1.68456 4.737(29) 1172. 3.4124 4.4574 81354. 1.68507 4.439(28) 1273. 3.4128 4.1443 81379. 1.68557 4.117(27) 1399. 3.4132 3.8909 81403. 1.68608 3.883(26) 1495. 3.4136 3.7588 81428. 1.68659 3.840(26) 1529. 3.4141 3.7414 81452. 1.68709 3.922(26) 1474. 3.4145 3.7989 81476. 1.68760 3.964(26) 1441. 3.4149 3.8972 81501. 1.68811 4.060(27) 1399. 3.4153 4.0569 81525. 1.68861 4.170(27) 1356. 3.4157 4.2595 81550. 1.68912 4.214(27) 1327. 3.4161 4.3491 81574. 1.68963 4.130(27) 1360. 3.4166 4.2288 81599. 1.69013 3.926(26) 1450. 3.4170 3.9986 81623. 1.69064 3.753(25) 1539. 3.4174 3.7871 81648. 1.69115 3.656(25) 1585. 3.4178 3.6419 81672. 1.69165 3.608(25) 1606. 3.4182 3.5535 81697. 1.69216 3.553(25) 1637. 3.4186 3.5018 81721. 1.69267 3.511(25) 1658. 3.4190 3.4721 81746. 1.69318 3.497(24) 1674. 3.4195 3.4571 81770. 1.69369 3.529(25) 1657. 3.4199 3.4567 81795. 1.69419 3.497(24) 1676. 3.4203 3.4765 81819. 1.69470 3.509(24) 1679. 3.4207 3.5150 81844. 1.69521 3.523(25) 1665. 3.4211 3.5496 81868. 1.69572 3.588(25) 1619. 3.4215 3.5519 81893. 1.69623 3.516(24) 1672. 3.4219 3.5253 81918. 1.69674 3.517(24) 1669. 3.4223 3.4910 81942. 1.69725 3.495(24) 1688. 3.4228 3.4654 81967. 1.69776 3.486(24) 1691. 3.4232 3.4492 81991. 1.69826 3.479(24) 1718. 3.4236 3.4397 82016. 1.69877 3.449(24) 1721. 3.4240 3.4343 82040. 1.69928 3.453(24) 1731. 3.4244 3.4312 82065. 1.69979 3.455(24) 1725. 3.4248 3.4295 82090. 1.70030 3.429(24) 1742. 3.4252 3.4284 82114. 1.70081 3.479(24) 1716. 3.4256 3.4280 82139. 1.70132 3.451(24) 1735. 3.4261 3.4279 82164. 1.70183 3.444(24) 1755. 3.4265 3.4272 82188. 1.70235 3.451(24) 1739. 3.4269 3.4275 82213. 1.70286 3.444(24) 1751. 3.4273 3.4282 82238. 1.70337 3.431(24) 1756. 3.4277 3.4286 82262. 1.70388 3.436(24) 1765. 3.4281 3.4290 82287. 1.70439 3.418(24) 1765. 3.4285 3.4294 82312. 1.70490 3.445(24) 1734. 3.4289 3.4298 82336. 1.70541 3.443(24) 1748. 3.4294 3.4303 82361. 1.70592 3.435(24) 1741. 3.4298 3.4308 82386. 1.70644 3.437(24) 1742. 3.4302 3.4312 82410. 1.70695 3.437(24) 1745. 3.4306 3.4317 82435. 1.70746 3.438(24) 1726. 3.4310 3.4323 82460. 1.70797 3.463(24) 1718. 3.4314 3.4328 82485. 1.70849 3.420(24) 1729. 3.4318 3.4333 82509. 1.70900 3.434(24) 1728. 3.4322 3.4339 82534. 1.70951 3.422(24) 1726. 3.4327 3.4346 82559. 1.71002 3.419(24) 1721. 3.4331 3.4354 82584. 1.71054 3.434(24) 1703. 3.4335 3.4363 82608. 1.71105 3.410(24) 1725. 3.4339 3.4374 82633. 1.71156 3.424(24) 1693. 3.4343 3.4387 82658. 1.71208 3.475(25) 1658. 3.4347 3.4406 82683. 1.71259 3.492(25) 1649. 3.4351 3.4441 82708. 1.71310 3.507(25) 1638. 3.4356 3.4553 82732. 1.71362 3.493(25) 1647. 3.4360 3.4946 82757. 1.71413 3.629(25) 1556. 3.4364 3.5981 82782. 1.71465 3.722(26) 1524. 3.4368 3.7736 82807. 1.71516 3.831(26) 1457. 3.4372 3.9376 82832. 1.71568 3.917(27) 1400. 3.4376 3.9678 82857. 1.71619 3.853(27) 1422. 3.4381 3.8656 82881. 1.71671 3.687(26) 1510. 3.4385 3.7258 82906. 1.71722 3.634(26) 1535. 3.4389 3.6146 82931. 1.71774 3.529(25) 1588. 3.4393 3.5434 82956. 1.71825 3.498(25) 1597. 3.4397 3.5015 82981. 1.71877 3.516(25) 1584. 3.4401 3.4777 83006. 1.71928 3.472(25) 1611. 3.4406 3.4637 83031. 1.71980 3.518(25) 1576. 3.4410 3.4558 83056. 1.72032 3.490(25) 1589. 3.4414 3.4512 83081. 1.72083 3.471(25) 1612. 3.4418 3.4487 83105. 1.72135 3.536(25) 1563. 3.4422 3.4473 83130. 1.72186 3.484(25) 1590. 3.4427 3.4466 83155. 1.72238 3.484(25) 1603. 3.4431 3.4464 83180. 1.72290 3.439(25) 1623. 3.4435 3.4464 83205. 1.72341 3.451(25) 1619. 3.4439 3.4466 83230. 1.72393 3.412(25) 1650. 3.4444 3.4469 83255. 1.72445 3.432(25) 1637. 3.4448 3.4473 83280. 1.72497 3.435(25) 1635. 3.4452 3.4478 83305. 1.72548 3.411(25) 1648. 3.4456 3.4484 83330. 1.72600 3.468(25) 1602. 3.4461 3.4490 83355. 1.72652 3.429(25) 1649. 3.4465 3.4498 83380. 1.72704 3.430(25) 1651. 3.4469 3.4507 83405. 1.72756 3.455(25) 1636. 3.4473 3.4519 83430. 1.72807 3.457(25) 1629. 3.4478 3.4535 83455. 1.72859 3.414(25) 1660. 3.4482 3.4556 83480. 1.72911 3.517(25) 1605. 3.4486 3.4630 83505. 1.72963 3.503(25) 1617. 3.4491 3.4896 83530. 1.73015 3.552(25) 1612. 3.4495 3.5674 83555. 1.73067 3.738(26) 1522. 3.4499 3.7213 83580. 1.73119 3.971(27) 1396. 3.4503 3.8994 83606. 1.73171 4.046(27) 1351. 3.4508 3.9776 83631. 1.73223 4.000(27) 1387. 3.4512 3.9098 83656. 1.73275 3.785(26) 1481. 3.4516 3.7750 83681. 1.73327 3.686(26) 1533. 3.4521 3.6543 83706. 1.73379 3.585(25) 1587. 3.4525 3.5734 83731. 1.73431 3.509(25) 1612. 3.4530 3.5253 83756. 1.73483 3.482(25) 1628. 3.4534 3.4977 83781. 1.73535 3.465(25) 1626. 3.4538 3.4820 83806. 1.73587 3.459(25) 1627. 3.4543 3.4733 83832. 1.73639 3.447(25) 1640. 3.4547 3.4686 83857. 1.73691 3.448(25) 1642. 3.4551 3.4663 83882. 1.73743 3.447(25) 1646. 3.4556 3.4655 83907. 1.73795 3.447(25) 1632. 3.4560 3.4669 83932. 1.73847 3.489(25) 1601. 3.4565 3.4680 83957. 1.73900 3.451(25) 1628. 3.4569 3.4700 83983. 1.73952 3.478(25) 1598. 3.4574 3.4735 84008. 1.74004 3.455(25) 1611. 3.4578 3.4817 84033. 1.74056 3.511(25) 1568. 3.4582 3.5076 84058. 1.74108 3.575(25) 1541. 3.4587 3.5842 84083. 1.74161 3.658(26) 1511. 3.4591 3.7610 84109. 1.74213 3.842(27) 1416. 3.4596 4.0603 84134. 1.74265 4.121(28) 1295. 3.4600 4.4083 84159. 1.74318 4.366(29) 1201. 3.4605 4.6314 84184. 1.74370 4.518(30) 1131. 3.4609 4.5772 84210. 1.74422 4.365(29) 1175. 3.4614 4.3134 84235. 1.74474 4.066(28) 1285. 3.4619 4.0201 84260. 1.74527 3.833(27) 1371. 3.4623 3.8017 84285. 1.74579 3.686(26) 1425. 3.4628 3.6660 84311. 1.74632 3.609(26) 1450. 3.4632 3.5873 84336. 1.74684 3.543(26) 1476. 3.4637 3.5427 84361. 1.74736 3.564(26) 1445. 3.4641 3.5182 84387. 1.74789 3.542(26) 1450. 3.4646 3.5056 84412. 1.74841 3.531(26) 1469. 3.4651 3.5010 84437. 1.74894 3.570(26) 1434. 3.4655 3.5037 84463. 1.74946 3.616(26) 1428. 3.4660 3.5254 84488. 1.74999 3.717(27) 1389. 3.4665 3.6163 84513. 1.75051 4.068(28) 1256. 3.4669 3.8845 84539. 1.75104 4.595(30) 1084. 3.4674 4.3993 84564. 1.75156 5.207(33) 903. 3.4679 4.9733 84589. 1.75209 5.427(34) 848. 3.4683 5.1955 84615. 1.75261 5.070(33) 929. 3.4688 4.9454 84640. 1.75314 4.555(31) 1070. 3.4693 4.4962 84665. 1.75367 4.101(29) 1216. 3.4697 4.1054 84691. 1.75419 3.869(28) 1304. 3.4702 3.8469 84716. 1.75472 3.688(27) 1373. 3.4707 3.6938 84742. 1.75525 3.631(27) 1399. 3.4712 3.6055 84767. 1.75577 3.611(27) 1415. 3.4716 3.5554 84793. 1.75630 3.546(26) 1449. 3.4721 3.5263 84818. 1.75683 3.545(26) 1443. 3.4726 3.5121 84843. 1.75735 3.540(26) 1452. 3.4731 3.5147 84869. 1.75788 3.587(26) 1435. 3.4736 3.5410 84894. 1.75841 3.660(27) 1416. 3.4741 3.6109 84920. 1.75894 3.785(27) 1362. 3.4745 3.7137 84945. 1.75946 3.906(28) 1301. 3.4750 3.7876 84971. 1.75999 3.934(28) 1295. 3.4755 3.7835 84996. 1.76052 3.806(27) 1360. 3.4760 3.7443 85022. 1.76105 3.811(27) 1364. 3.4765 3.7529 85047. 1.76158 3.843(27) 1352. 3.4770 3.8421 85073. 1.76210 3.887(27) 1326. 3.4775 3.9444 85098. 1.76263 3.992(28) 1279. 3.4780 3.9514 85124. 1.76316 3.880(27) 1338. 3.4785 3.8569 85149. 1.76369 3.804(27) 1367. 3.4790 3.7355 85175. 1.76422 3.689(27) 1411. 3.4795 3.6407 85200. 1.76475 3.641(26) 1433. 3.4800 3.5797 85226. 1.76528 3.581(26) 1461. 3.4805 3.5464 85252. 1.76581 3.575(26) 1457. 3.4810 3.5288 85277. 1.76634 3.587(26) 1453. 3.4815 3.5207 85303. 1.76687 3.557(26) 1466. 3.4820 3.5187 85328. 1.76740 3.583(26) 1458. 3.4825 3.5215 85354. 1.76793 3.542(26) 1474. 3.4830 3.5292 85380. 1.76846 3.525(26) 1484. 3.4836 3.5486 85405. 1.76899 3.676(27) 1405. 3.4841 3.6175 85431. 1.76952 3.841(27) 1375. 3.4846 3.8710 85456. 1.77005 4.447(29) 1179. 3.4851 4.5617 85482. 1.77058 5.590(34) 889. 3.4856 5.7773 85508. 1.77111 6.84(4) 665. 3.486 6.977 85533. 1.77165 7.30(4) 599. 3.487 7.270 85559. 1.77218 6.48(4) 705. 3.487 6.582 85585. 1.77271 5.351(33) 898. 3.4877 5.5760 85610. 1.77324 4.541(30) 1087. 3.4882 4.7572 85636. 1.77377 4.073(29) 1222. 3.4888 4.2322 85662. 1.77431 3.805(28) 1322. 3.4893 3.9245 85687. 1.77484 3.706(27) 1354. 3.4898 3.7482 85713. 1.77537 3.600(27) 1380. 3.4904 3.6467 85739. 1.77590 3.601(27) 1370. 3.4909 3.5883 85765. 1.77644 3.554(27) 1388. 3.4914 3.5543 85790. 1.77697 3.563(27) 1384. 3.4920 3.5343 85816. 1.77750 3.518(27) 1401. 3.4925 3.5223 85842. 1.77804 3.513(27) 1397. 3.4931 3.5150 85868. 1.77857 3.513(27) 1392. 3.4936 3.5104 85893. 1.77910 3.487(27) 1397. 3.4942 3.5076 85919. 1.77964 3.510(27) 1380. 3.4947 3.5057 85945. 1.78017 3.530(27) 1372. 3.4953 3.5046 85971. 1.78070 3.529(27) 1366. 3.4958 3.5038 85996. 1.78124 3.494(27) 1386. 3.4964 3.5034 86022. 1.78177 3.544(27) 1351. 3.4969 3.5031 86048. 1.78231 3.535(27) 1360. 3.4975 3.5030 86074. 1.78284 3.519(27) 1360. 3.4980 3.5030 86100. 1.78338 3.541(27) 1350. 3.4986 3.5031 86125. 1.78391 3.548(27) 1352. 3.4992 3.5033 86151. 1.78445 3.526(27) 1362. 3.4997 3.4997 86177. 1.78498 3.491(27) 1385. 3.5003 3.5003 86203. 1.78552 3.511(27) 1381. 3.5009 3.5009 86229. 1.78606 3.492(27) 1383. 3.5014 3.5014 86255. 1.78659 3.477(27) 1379. 3.5020 3.5020 86281. 1.78713 3.545(27) 1354. 3.5026 3.5026 86307. 1.78766 3.524(27) 1365. 3.5032 3.5032 86332. 1.78820 3.509(27) 1385. 3.5037 3.5037 86358. 1.78874 3.500(27) 1383. 3.5043 3.5043 86384. 1.78927 3.540(27) 1370. 3.5049 3.5049 86410. 1.78981 3.542(27) 1371. 3.5055 3.5055 86436. 1.79035 3.479(27) 1404. 3.5061 3.5061 86462. 1.79088 3.549(27) 1374. 3.5067 3.5067 86488. 1.79142 3.526(27) 1387. 3.5073 3.5073 86514. 1.79196 3.572(27) 1367. 3.5079 3.5079 86540. 1.79250 3.524(27) 1390. 3.5085 3.5085 86566. 1.79303 3.538(27) 1386. 3.5091 3.5091 86592. 1.79357 3.514(27) 1403. 3.5096 3.5097 86618. 1.79411 3.524(27) 1403. 3.5103 3.5103 86644. 1.79465 3.548(27) 1390. 3.5109 3.5109 86670. 1.79519 3.570(27) 1368. 3.5115 3.5115 86696. 1.79573 3.497(27) 1423. 3.5121 3.5121 86722. 1.79627 3.507(27) 1409. 3.5127 3.5127 86748. 1.79680 3.542(27) 1400. 3.5133 3.5133 86774. 1.79734 3.545(27) 1400. 3.5139 3.5139 86800. 1.79788 3.500(27) 1421. 3.5145 3.5145 86826. 1.79842 3.543(27) 1395. 3.5151 3.5151 86852. 1.79896 3.508(27) 1419. 3.5158 3.5158 86878. 1.79950 3.523(27) 1402. 3.5164 3.5164 86904. 1.80004 3.553(27) 1395. 3.5170 3.5170 86930. 1.80058 3.519(27) 1402. 3.5176 3.5176 86956. 1.80112 3.500(27) 1402. 3.5183 3.5183 86982. 1.80166 3.526(27) 1387. 3.5189 3.5189 87008. 1.80220 3.511(27) 1389. 3.5195 3.5195 87034. 1.80274 3.537(27) 1372. 3.5202 3.5202 87061. 1.80328 3.521(27) 1376. 3.5208 3.5208 87087. 1.80383 3.529(27) 1365. 3.5214 3.5214 87113. 1.80437 3.489(27) 1385. 3.5221 3.5221 87139. 1.80491 3.521(27) 1359. 3.5227 3.5227 87165. 1.80545 3.555(27) 1331. 3.5234 3.5234 87191. 1.80599 3.499(27) 1353. 3.5240 3.5240 87217. 1.80653 3.514(27) 1335. 3.5247 3.5247 87244. 1.80708 3.530(27) 1341. 3.5253 3.5253 87270. 1.80762 3.515(27) 1344. 3.5260 3.5261 87296. 1.80816 3.545(28) 1321. 3.5266 3.5268 87322. 1.80870 3.530(28) 1314. 3.5273 3.5275 87348. 1.80925 3.552(28) 1297. 3.5280 3.5316 87374. 1.80979 3.567(28) 1281. 3.5286 3.5326 87401. 1.81033 3.576(28) 1269. 3.5293 3.5336 87427. 1.81087 3.538(28) 1288. 3.5300 3.5346 87453. 1.81142 3.578(28) 1263. 3.5306 3.5357 87479. 1.81196 3.540(28) 1271. 3.5313 3.5369 87506. 1.81251 3.506(28) 1306. 3.5320 3.5382 87532. 1.81305 3.518(28) 1285. 3.5327 3.5395 87558. 1.81359 3.552(28) 1270. 3.5333 3.5410 87584. 1.81414 3.545(28) 1266. 3.5340 3.5426 87611. 1.81468 3.578(28) 1260. 3.5347 3.5444 87637. 1.81523 3.515(28) 1282. 3.5354 3.5465 87663. 1.81577 3.535(28) 1278. 3.5361 3.5488 87690. 1.81632 3.531(28) 1273. 3.5368 3.5516 87716. 1.81686 3.502(28) 1298. 3.5375 3.5549 87742. 1.81741 3.545(28) 1273. 3.5382 3.5591 87768. 1.81795 3.539(28) 1278. 3.5389 3.5643 87795. 1.81850 3.541(28) 1283. 3.5396 3.5714 87821. 1.81904 3.561(28) 1275. 3.5403 3.5824 87847. 1.81959 3.667(29) 1227. 3.5410 3.6046 87874. 1.82013 3.664(28) 1243. 3.5417 3.6635 87900. 1.82068 3.872(29) 1176. 3.5424 3.8357 87927. 1.82123 4.306(31) 1061. 3.5431 4.3067 87953. 1.82177 5.214(34) 854. 3.5438 5.3133 87979. 1.82232 6.63(4) 614. 3.545 6.753 88006. 1.82287 7.88(5) 474. 3.545 7.817 88032. 1.82341 7.62(4) 496. 3.546 7.697 88059. 1.82396 6.39(4) 639. 3.547 6.686 88085. 1.82451 5.261(35) 825. 3.5474 5.5606 88111. 1.82506 4.491(32) 1005. 3.5482 4.7376 88138. 1.82560 4.082(30) 1121. 3.5489 4.2357 88164. 1.82615 3.818(29) 1200. 3.5496 3.9487 88191. 1.82670 3.756(29) 1210. 3.5504 3.7866 88217. 1.82725 3.659(28) 1269. 3.5511 3.6947 88244. 1.82780 3.632(28) 1278. 3.5519 3.6421 88270. 1.82834 3.640(28) 1261. 3.5526 3.6117 88297. 1.82889 3.562(28) 1313. 3.5534 3.5939 88323. 1.82944 3.598(28) 1286. 3.5541 3.5833 88350. 1.82999 3.584(28) 1293. 3.5549 3.5770 88376. 1.83054 3.574(28) 1299. 3.5556 3.5730 88403. 1.83109 3.662(28) 1244. 3.5564 3.5706 88429. 1.83164 3.638(28) 1261. 3.5571 3.5690 88456. 1.83219 3.619(28) 1266. 3.5579 3.5681 88482. 1.83274 3.611(28) 1266. 3.5586 3.5676 88509. 1.83329 3.588(28) 1267. 3.5594 3.5673 88535. 1.83384 3.583(28) 1268. 3.5602 3.5673 88562. 1.83439 3.614(28) 1242. 3.5610 3.5674 88588. 1.83494 3.688(29) 1211. 3.5617 3.5676 88615. 1.83549 3.609(28) 1246. 3.5625 3.5679 88642. 1.83604 3.617(28) 1238. 3.5633 3.5682 88668. 1.83659 3.537(28) 1261. 3.5641 3.5687 88695. 1.83714 3.532(28) 1268. 3.5648 3.5655 88721. 1.83769 3.586(29) 1228. 3.5656 3.5664 88748. 1.83824 3.588(29) 1223. 3.5664 3.5673 88775. 1.83880 3.555(28) 1233. 3.5672 3.5684 88801. 1.83935 3.607(29) 1201. 3.5680 3.5695 88828. 1.83990 3.626(29) 1187. 3.5688 3.5706 88855. 1.84045 3.649(29) 1168. 3.5696 3.5721 88881. 1.84100 3.602(29) 1196. 3.5704 3.5744 88908. 1.84156 3.589(29) 1190. 3.5712 3.5806 88935. 1.84211 3.581(29) 1191. 3.5720 3.6002 88961. 1.84266 3.609(29) 1170. 3.5728 3.6467 88988. 1.84321 3.626(29) 1168. 3.5736 3.7172 89015. 1.84377 3.631(29) 1168. 3.5744 3.7749 89041. 1.84432 3.698(30) 1129. 3.5752 3.7745 89068. 1.84487 3.661(30) 1143. 3.5760 3.7292 89095. 1.84543 3.667(30) 1138. 3.5769 3.6765 89121. 1.84598 3.623(30) 1146. 3.5777 3.6378 89148. 1.84654 3.601(29) 1157. 3.5785 3.6146 89175. 1.84709 3.601(29) 1167. 3.5793 3.6020 89202. 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3.870 3.870 97601. 2.02165 3.96(4) 719. 3.870 3.871 97630. 2.02226 3.95(4) 718. 3.871 3.872 97659. 2.02287 3.97(4) 696. 3.872 3.872 97689. 2.02347 3.94(4) 707. 3.873 3.878 97718. 2.02408 3.96(4) 690. 3.874 3.885 97747. 2.02469 3.84(4) 720. 3.874 3.887 97777. 2.02530 3.83(4) 717. 3.875 3.889 97806. 2.02590 3.80(4) 719. 3.876 3.891 97835. 2.02651 3.86(4) 696. 3.877 3.894 97865. 2.02712 3.80(4) 709. 3.878 3.896 97894. 2.02773 3.83(4) 698. 3.878 3.899 97923. 2.02834 3.94(4) 664. 3.879 3.902 97953. 2.02894 4.04(4) 632. 3.880 3.908 97982. 2.02955 4.16(4) 608. 3.881 3.912 98012. 2.03016 4.16(4) 610. 3.881 3.917 98041. 2.03077 4.10(4) 623. 3.882 3.923 98070. 2.03138 4.04(4) 637. 3.883 3.932 98100. 2.03199 4.08(4) 624. 3.884 3.944 98129. 2.03260 4.04(4) 632. 3.884 3.970 98159. 2.03321 4.12(4) 614. 3.885 4.029 98188. 2.03382 4.19(4) 600. 3.886 4.135 98218. 2.03443 4.37(4) 565. 3.887 4.258 98247. 2.03504 4.42(4) 552. 3.887 4.337 98277. 2.03565 4.49(4) 548. 3.888 4.393 98306. 2.03626 4.75(4) 526. 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399. 4.012 4.013 114659. 2.37506 3.99(5) 410. 4.011 4.012 114693. 2.37578 4.02(5) 402. 4.010 4.011 114728. 2.37649 4.04(5) 395. 4.009 4.010 114762. 2.37720 4.01(5) 397. 4.008 4.009 114797. 2.37792 4.05(5) 390. 4.007 4.008 114831. 2.37863 4.02(5) 394. 4.006 4.007 114866. 2.37934 3.96(5) 399. 4.004 4.006 114900. 2.38006 3.98(5) 399. 4.003 4.005 114934. 2.38077 4.01(5) 388. 4.002 4.004 114969. 2.38148 4.05(5) 383. 4.001 4.003 115003. 2.38220 3.96(5) 402. 4.000 4.002 115038. 2.38291 3.97(5) 401. 3.999 4.001 115072. 2.38363 4.02(5) 394. 3.997 4.000 115107. 2.38434 4.00(5) 399. 3.996 4.000 115141. 2.38506 4.00(5) 402. 3.995 4.000 115176. 2.38578 4.01(5) 404. 3.994 4.000 115211. 2.38649 3.96(5) 418. 3.992 4.001 115245. 2.38721 3.98(5) 414. 3.991 4.005 115280. 2.38792 4.03(5) 414. 3.990 4.024 115314. 2.38864 4.02(5) 420. 3.989 4.089 115349. 2.38936 4.04(5) 419. 3.987 4.246 115384. 2.39007 4.19(5) 403. 3.986 4.487 115418. 2.39079 4.35(5) 383. 3.985 4.680 115453. 2.39151 4.51(5) 364. 3.983 4.677 115487. 2.39223 4.39(5) 380. 3.982 4.504 115522. 2.39294 4.23(5) 405. 3.981 4.299 115557. 2.39366 4.11(5) 421. 3.979 4.150 115591. 2.39438 4.06(5) 429. 3.978 4.065 115626. 2.39510 4.03(5) 434. 3.977 4.022 115661. 2.39582 3.98(5) 440. 3.975 4.014 115695. 2.39654 4.01(5) 434. 3.974 4.004 115730. 2.39726 3.97(5) 444. 3.972 3.999 115765. 2.39797 3.94(5) 445. 3.971 3.996 115800. 2.39869 3.93(5) 444. 3.970 3.995 115834. 2.39941 3.93(5) 440. 3.968 3.994 115869. 2.40013 3.96(5) 434. 3.967 3.995 115904. 2.40085 3.94(5) 436. 3.966 3.996 115939. 2.40157 3.90(5) 437. 3.964 3.997 115973. 2.40230 3.94(5) 429. 3.963 3.999 116008. 2.40302 3.94(5) 425. 3.961 4.003 116043. 2.40374 3.94(5) 423. 3.960 4.007 116078. 2.40446 3.99(5) 412. 3.958 4.012 116113. 2.40518 3.95(5) 413. 3.957 4.019 116147. 2.40590 3.99(5) 407. 3.956 4.029 116182. 2.40662 3.94(5) 412. 3.954 4.042 116217. 2.40735 3.99(5) 400. 3.953 4.059 116252. 2.40807 4.01(5) 392. 3.951 4.085 116287. 2.40879 4.03(5) 389. 3.950 4.123 116322. 2.40951 4.12(5) 377. 3.948 4.200 116357. 2.41024 4.53(5) 335.0 3.947 4.446 116392. 2.41096 5.58(6) 258.6 3.945 5.347 116426. 2.41168 7.90(8) 157.0 3.944 7.958 116461. 2.41241 12.67(12) 73.2 3.942 13.073 116496. 2.41313 18.50(16) 38.2 3.941 19.159 116531. 2.41385 21.27(18) 29.93 3.940 22.058 116566. 2.41458 18.34(16) 38.6 3.938 19.706 116601. 2.41530 13.05(12) 68.9 3.937 14.616 116636. 2.41603 8.78(9) 130.2 3.935 10.007 116671. 2.41675 6.37(7) 211.5 3.934 7.082 116706. 2.41748 5.06(6) 290.7 3.932 5.534 116741. 2.41820 4.48(5) 342.9 3.931 4.770 116776. 2.41893 4.28(5) 361. 3.929 4.396 116811. 2.41966 4.13(5) 386. 3.928 4.207 116846. 2.42038 4.06(5) 395. 3.926 4.108 116881. 2.42111 4.00(5) 403. 3.925 4.052 116916. 2.42183 3.96(5) 412. 3.923 4.019 116952. 2.42256 3.93(5) 419. 3.922 3.998 116987. 2.42329 3.93(5) 418. 3.921 3.983 117022. 2.42402 3.96(5) 414. 3.919 3.971 117057. 2.42474 3.93(5) 419. 3.918 3.962 117092. 2.42547 3.97(5) 416. 3.916 3.955 117127. 2.42620 3.96(5) 422. 3.915 3.949 117162. 2.42693 3.91(5) 427. 3.913 3.944 117197. 2.42765 3.87(5) 434. 3.912 3.939 117232. 2.42838 4.00(5) 412. 3.911 3.935 117268. 2.42911 3.92(5) 423. 3.909 3.931 117303. 2.42984 3.94(5) 418. 3.908 3.928 117338. 2.43057 3.97(5) 415. 3.906 3.906 117373. 2.43130 3.93(5) 420. 3.905 3.905 117408. 2.43203 3.96(5) 408. 3.904 3.904 117444. 2.43276 3.95(5) 405. 3.902 3.902 117479. 2.43349 3.97(5) 397. 3.901 3.901 117514. 2.43422 3.92(5) 398. 3.899 3.899 117549. 2.43495 3.95(5) 395. 3.898 3.898 117585. 2.43568 3.92(5) 388. 3.897 3.897 117620. 2.43641 3.93(5) 387. 3.895 3.895 117655. 2.43714 4.03(5) 371. 3.894 3.894 117691. 2.43787 3.93(5) 381. 3.893 3.893 117726. 2.43860 3.98(5) 370. 3.892 3.892 117761. 2.43934 4.07(5) 353. 3.890 3.890 117796. 2.44007 3.98(5) 362. 3.889 3.889 117832. 2.44080 4.00(5) 356. 3.888 3.888 117867. 2.44153 4.02(5) 352. 3.886 3.886 117903. 2.44226 3.99(5) 357. 3.885 3.885 117938. 2.44300 4.02(5) 347.5 3.884 3.884 117973. 2.44373 4.00(5) 349.9 3.883 3.883 118009. 2.44446 4.06(5) 341.8 3.882 3.882 118044. 2.44520 4.04(5) 346.8 3.880 3.880 118079. 2.44593 4.03(5) 346.6 3.879 3.879 118115. 2.44667 4.00(5) 351. 3.878 3.878 118150. 2.44740 4.02(5) 354. 3.877 3.877 118186. 2.44813 4.00(5) 356. 3.876 3.876 118221. 2.44887 3.98(5) 359. 3.875 3.875 118257. 2.44960 3.99(5) 358. 3.874 3.874 118292. 2.45034 3.98(5) 364. 3.873 3.873 118328. 2.45107 4.11(5) 347.5 3.871 3.871 118363. 2.45181 4.04(5) 361. 3.870 3.870 118399. 2.45254 3.99(5) 371. 3.869 3.869 118434. 2.45328 4.09(5) 356. 3.868 3.868 118470. 2.45402 4.00(5) 372. 3.867 3.867 118505. 2.45475 4.01(5) 373. 3.866 3.866 118541. 2.45549 4.10(5) 360. 3.865 3.865 118576. 2.45623 4.04(5) 372. 3.865 3.879 118612. 2.45696 4.05(5) 371. 3.864 3.879 118648. 2.45770 3.94(5) 385. 3.863 3.879 118683. 2.45844 3.98(5) 385. 3.862 3.880 118719. 2.45918 4.02(5) 377. 3.861 3.881 118754. 2.45991 4.10(5) 363. 3.860 3.882 118790. 2.46065 4.02(5) 375. 3.859 3.884 118826. 2.46139 4.03(5) 372. 3.859 3.886 118861. 2.46213 3.98(5) 375. 3.858 3.888 118897. 2.46287 3.96(5) 377. 3.857 3.891 118933. 2.46361 3.98(5) 370. 3.856 3.895 118968. 2.46435 4.01(5) 367. 3.856 3.901 119004. 2.46509 3.97(5) 365. 3.855 3.907 119040. 2.46582 4.00(5) 358. 3.854 3.916 119075. 2.46656 4.04(5) 351. 3.854 3.927 119111. 2.46730 4.02(5) 352. 3.853 3.942 119147. 2.46804 4.03(5) 347.7 3.852 3.963 119183. 2.46879 4.06(5) 341.0 3.852 3.992 119218. 2.46953 4.24(6) 318.6 3.851 4.043 119254. 2.47027 4.51(6) 293.5 3.851 4.178 119290. 2.47101 4.98(6) 261.6 3.850 4.669 119326. 2.47175 6.49(7) 180.9 3.850 6.272 119361. 2.47249 9.40(10) 103.2 3.849 9.995 119397. 2.47323 14.19(14) 51.5 3.849 15.521 119433. 2.47398 18.79(18) 31.21 3.848 19.824 119469. 2.47472 18.95(18) 30.30 3.848 19.587 119505. 2.47546 15.39(15) 42.8 3.848 15.565 119541. 2.47620 10.96(12) 74.4 3.847 10.912 119576. 2.47695 7.87(9) 125.0 3.847 7.583 119612. 2.47769 5.96(7) 190.0 3.847 5.727 119648. 2.47843 5.00(6) 237.8 3.846 4.805 119684. 2.47918 4.50(6) 273.4 3.846 4.361 119720. 2.47992 4.22(6) 303.2 3.846 4.144 119756. 2.48066 4.05(6) 319.1 3.846 4.034 119792. 2.48141 4.11(6) 311.4 3.845 3.974 119828. 2.48215 4.08(6) 308.0 3.845 3.940 119864. 2.48290 3.99(6) 318.9 3.845 3.919 119900. 2.48364 3.98(6) 319.8 3.845 3.905 119936. 2.48439 3.99(6) 314.4 3.845 3.895 119972. 2.48513 4.04(6) 308.0 3.845 3.888 120008. 2.48588 3.95(6) 320.0 3.845 3.882 120044. 2.48663 3.97(6) 318.2 3.845 3.877 120080. 2.48737 3.85(5) 332.9 3.845 3.874 120116. 2.48812 3.86(5) 333.6 3.845 3.870 120152. 2.48887 3.91(6) 327.0 3.845 3.868 120188. 2.48961 3.89(6) 329.3 3.845 3.866 120224. 2.49036 3.94(6) 322.4 3.845 3.864 120260. 2.49111 3.90(6) 328.7 3.845 3.862 120296. 2.49185 3.83(5) 336.5 3.845 3.845 120332. 2.49260 3.78(5) 335.0 3.845 3.845 120368. 2.49335 3.78(5) 339.5 3.845 3.845 120404. 2.49410 3.90(6) 322.8 3.845 3.845 120440. 2.49485 3.86(6) 324.1 3.846 3.845 120477. 2.49559 3.85(6) 323.0 3.846 3.846 120513. 2.49634 3.89(6) 317.5 3.846 3.846 120549. 2.49709 3.92(6) 309.0 3.846 3.846 120585. 2.49784 3.93(6) 303.7 3.846 3.846 120621. 2.49859 3.83(6) 309.6 3.846 3.846 120657. 2.49934 3.83(6) 308.9 3.847 3.847 120694. 2.50009 3.82(6) 308.6 3.847 3.847 120730. 2.50084 3.83(6) 298.4 3.847 3.847 120766. 2.50159 3.88(6) 294.5 3.847 3.847 120802. 2.50234 3.82(6) 296.8 3.848 3.848 120838. 2.50309 3.86(6) 289.5 3.848 3.848 120875. 2.50384 3.83(6) 294.2 3.848 3.848 120911. 2.50460 3.76(6) 295.7 3.848 3.848 120947. 2.50535 3.83(6) 285.0 3.849 3.849 120984. 2.50610 3.81(6) 289.7 3.849 3.849 121020. 2.50685 3.82(6) 284.7 3.849 3.849 121056. 2.50760 3.76(6) 290.2 3.849 3.849 121092. 2.50836 3.85(6) 281.2 3.850 3.850 121129. 2.50911 3.83(6) 285.5 3.850 3.850 121165. 2.50986 3.80(6) 286.6 3.850 3.850 121201. 2.51061 3.85(6) 281.6 3.850 3.850 121238. 2.51137 3.81(6) 289.7 3.851 3.851 121274. 2.51212 3.80(6) 291.4 3.851 3.851 121311. 2.51287 3.70(6) 302.5 3.851 3.851 121347. 2.51363 3.75(6) 298.2 3.851 3.851 121383. 2.51438 3.80(6) 295.7 3.851 3.855 121420. 2.51514 3.74(6) 303.5 3.851 3.855 121456. 2.51589 3.62(6) 312.0 3.851 3.856 121493. 2.51665 3.70(6) 311.3 3.851 3.856 121529. 2.51740 3.72(6) 313.3 3.852 3.856 121566. 2.51816 3.75(6) 314.5 3.852 3.857 121602. 2.51891 3.70(5) 330.7 3.851 3.857 121638. 2.51967 3.79(6) 326.8 3.851 3.858 121675. 2.52043 3.85(6) 322.2 3.851 3.859 121711. 2.52118 3.77(6) 329.5 3.851 3.859 121748. 2.52194 3.82(6) 322.4 3.851 3.860 121785. 2.52269 3.74(5) 335.2 3.851 3.861 121821. 2.52345 3.74(6) 328.8 3.850 3.863 121858. 2.52421 3.71(5) 334.7 3.850 3.864 121894. 2.52497 3.73(5) 337.7 3.850 3.866 121931. 2.52572 3.69(5) 334.3 3.849 3.869 121967. 2.52648 3.68(5) 333.7 3.849 3.873 122004. 2.52724 3.80(6) 314.2 3.848 3.878 122041. 2.52800 3.72(6) 320.2 3.847 3.885 122077. 2.52876 3.79(6) 312.2 3.847 3.898 122114. 2.52952 3.85(6) 306.1 3.846 3.934 122150. 2.53027 4.09(6) 284.2 3.845 4.063 122187. 2.53103 4.52(6) 249.7 3.844 4.488 122224. 2.53179 5.35(7) 195.3 3.843 5.482 122260. 2.53255 6.50(8) 145.7 3.842 6.975 122297. 2.53331 7.67(10) 110.4 3.840 8.168 122334. 2.53407 7.89(10) 103.3 3.839 8.142 122370. 2.53483 7.07(9) 120.5 3.837 7.063 122407. 2.53559 5.94(8) 153.8 3.836 5.784 122444. 2.53636 4.91(7) 200.3 3.834 4.859 122481. 2.53712 4.37(7) 231.6 3.832 4.343 122517. 2.53788 4.04(6) 254.1 3.830 4.088 122554. 2.53864 3.90(6) 264.4 3.828 3.965 122591. 2.53940 3.84(6) 268.6 3.826 3.905 122628. 2.54016 3.75(6) 272.1 3.824 3.874 122664. 2.54093 3.80(6) 265.2 3.821 3.855 122701. 2.54169 3.68(6) 279.8 3.818 3.844 122738. 2.54245 3.71(6) 277.6 3.816 3.836 122775. 2.54321 3.67(6) 276.8 3.813 3.829 122812. 2.54398 3.80(6) 265.6 3.809 3.823 122849. 2.54474 3.79(6) 262.3 3.806 3.818 122885. 2.54550 3.71(6) 272.9 3.802 3.813 122922. 2.54627 3.70(6) 276.9 3.799 3.808 122959. 2.54703 3.77(6) 267.5 3.795 3.803 122996. 2.54779 3.84(6) 261.2 3.791 3.798 123033. 2.54856 3.74(6) 273.6 3.786 3.792 123070. 2.54932 3.75(6) 274.7 3.782 3.787 123107. 2.55009 3.65(6) 277.2 3.777 3.782 123144. 2.55085 3.71(6) 276.9 3.772 3.776 123181. 2.55162 3.72(6) 274.8 3.766 3.766 123218. 2.55239 3.77(6) 267.2 3.761 3.761 123255. 2.55315 3.83(6) 260.6 3.755 3.755 123292. 2.55392 3.75(6) 265.2 3.749 3.749 123328. 2.55468 3.81(6) 258.6 3.743 3.743 123365. 2.55545 3.76(6) 265.9 3.736 3.736 123402. 2.55622 3.86(6) 251.9 3.729 3.729 123440. 2.55698 3.80(6) 253.0 3.722 3.722 123477. 2.55775 3.78(6) 255.3 3.714 3.714 123514. 2.55852 3.91(6) 237.2 3.707 3.707 123551. 2.55929 3.88(6) 239.3 3.698 3.698 123588. 2.56005 3.79(6) 245.7 3.690 3.690 123625. 2.56082 3.74(6) 243.7 3.681 3.681 123662. 2.56159 3.82(7) 233.3 3.672 3.672 123699. 2.56236 3.85(7) 228.5 3.662 3.662 123736. 2.56313 3.87(7) 222.3 3.652 3.652 123773. 2.56390 3.84(7) 219.7 3.642 3.642 123810. 2.56467 3.89(7) 214.3 3.631 3.631 123847. 2.56544 3.90(7) 209.2 3.619 3.619 123885. . 3.82(7) . . . 123922. . 3.84(7) . . . 123959. . 3.88(7) . . . 123996. . 3.95(7) . . . 124033. . 3.81(7) . . . 124071. . 3.81(7) . . . 124108. . 3.80(7) . . . 124145. . 3.74(7) . . . 124182. . 3.75(7) . . . 124220. . 3.82(7) . . . 124257. . 3.84(7) . . . 124294. . 3.87(7) . . . 124331. . 3.90(7) . . . 124369. . 3.86(7) . . . 124406. . 3.90(7) . . . 124443. . 3.83(7) . . . 124481. . 3.89(7) . . . 124518. . 3.84(7) . . . 124555. . 3.77(7) . . . 124593. . 3.89(7) . . . 124630. . 3.74(7) . . . 124667. . 3.77(7) . . . 124705. . 3.86(7) . . . 124742. . 3.92(7) . . . 124780. . 3.96(7) . . . 124817. . 4.26(8) . . . 124855. . 4.58(8) . . . 124892. . 4.89(8) . . . 124929. . 4.67(8) . . . 124967. . 4.33(8) . . . 125005. . -0.001240(22) . . . _pd_meas_number_of_points 4610 _pd_proc_number_of_points 4610 loop_ _refln_index_h _refln_index_k _refln_index_l _pd_refln_phase_id _refln_observed_status _refln_F_squared_meas _refln_F_squared_calc _refln_phase_calc _refln_d_spacing _gsas_i100_meas 2 2 -2 1 o 23.513 30.219 0.00 2.53348 21.33 2 2 1 1 o 144.048 141.998 180.00 2.47411 100.00 1 1 4 1 o 154.400 171.335 0.00 2.41368 95.42 3 1 -1 1 o 3.169 5.347 0.00 2.39094 2.48 3 1 -2 1 o 7.403 8.679 180.00 2.34417 5.36 2 2 -3 1 o 1.587 1.561 0.00 2.34297 1.16 3 1 0 1 o 2.719 2.564 0.00 2.34195 1.99 1 3 0 1 o 0.252 0.489 0.00 2.33334 0.18 1 3 -1 1 o 0.000 0.000 0.00 2.31855 0.00 0 2 4 1 o 18.196 15.656 0.00 2.29963 12.16 1 1 -5 1 o 0.427 0.175 0.00 2.27744 0.28 2 2 2 1 o 1.456 1.453 180.00 2.26584 0.95 1 3 1 1 o 19.832 16.797 180.00 2.26011 12.44 1 3 -2 1 o 0.661 0.867 180.00 2.22048 0.40 3 1 -3 1 o 0.000 0.254 180.00 2.21689 0.00 3 1 1 1 o 0.000 0.000 0.00 2.21315 0.00 1 1 0 2 o 0.006 0.006 180.00 2.13870 15.53 1 3 2 1 o 5.238 3.337 180.00 2.12091 2.69 2 2 -4 1 o 7.165 4.437 180.00 2.11772 3.65 2 0 4 1 o 45.829 37.230 0.00 2.09703 10.70 1 3 -3 1 o 1.687 0.733 180.00 2.06699 0.79 3 1 -4 1 o 20.285 25.396 0.00 2.04374 8.81 3 1 2 1 o 95.708 94.904 180.00 2.03934 37.62 2 2 3 1 o 79.173 78.213 0.00 2.03854 31.72 1 1 5 1 o 5.139 3.385 0.00 2.03479 2.27 0 2 5 1 o 10.419 15.599 180.00 1.98381 4.13 0 0 6 1 o 27.815 33.605 180.00 1.96113 5.16 1 3 3 1 o 2.908 4.545 180.00 1.94886 1.10 1 1 -6 1 o 12.951 13.386 180.00 1.93393 4.70 2 0 -6 1 o 19.272 14.232 180.00 1.90900 3.33 2 2 -5 1 o 28.729 26.940 0.00 1.89580 9.54 1 3 -4 1 o 21.158 20.538 0.00 1.89069 7.01 4 0 -2 1 o 4.436 1.997 180.00 1.88525 0.75 3 1 -5 1 o 39.229 36.174 0.00 1.85760 11.98 3 1 3 1 o 0.106 0.073 0.00 1.85319 0.03 4 0 0 1 o 3.490 2.277 0.00 1.85233 0.55 0 4 0 1 o 5.400 6.210 180.00 1.84382 0.83 2 2 4 1 o 69.135 72.058 180.00 1.82290 18.97 0 4 1 1 o 2.881 2.847 180.00 1.82159 0.85 1 3 4 1 o 66.134 69.297 180.00 1.77131 16.46 3 3 -1 1 o 8.725 7.620 0.00 1.76226 2.28 0 4 2 1 o 6.854 5.184 180.00 1.75944 1.79 1 1 6 1 o 35.969 31.002 180.00 1.75185 8.96 4 0 -4 1 o 29.657 32.082 0.00 1.74329 3.63 3 3 -2 1 o 1.033 1.119 0.00 1.74328 0.26 3 3 0 1 o 4.776 5.905 0.00 1.74237 1.20 0 2 6 1 o 10.136 9.539 0.00 1.73150 2.48 1 3 -5 1 o 10.567 10.045 0.00 1.71531 2.50 2 2 -6 1 o 3.605 2.434 180.00 1.69531 0.82 3 3 -3 1 o 15.949 16.154 0.00 1.68899 3.54 3 3 1 1 o 5.797 5.143 0.00 1.68733 1.30 4 2 -1 1 o 30.075 24.588 0.00 1.68378 6.54 3 1 -6 1 o 0.707 0.614 180.00 1.67924 0.16 4 2 -2 1 o 3.759 3.676 180.00 1.67861 0.83 3 1 4 1 o 8.511 8.496 0.00 1.67517 1.85 1 1 -7 1 o 0.780 0.784 0.00 1.67508 0.17 0 4 3 1 o 9.453 9.141 180.00 1.66864 2.02 4 0 2 1 o 56.826 56.431 180.00 1.66825 5.79 2 4 -1 1 o 8.760 11.566 0.00 1.65638 1.82 4 2 0 1 o 0.495 0.593 0.00 1.65525 0.10 2 4 0 1 o 0.085 2.325 0.00 1.65068 0.02 4 2 -3 1 o 0.000 0.192 0.00 1.64063 0.00 2 2 5 1 o 1.496 6.247 180.00 1.63150 0.30 2 4 -2 1 o 0.000 0.003 0.00 1.62994 0.00 2 4 1 1 o 7.600 10.676 0.00 1.61379 1.44 3 3 -4 1 o 0.038 0.051 180.00 1.60854 0.01 3 3 2 1 o 45.397 49.137 0.00 1.60639 8.14 1 3 5 1 o 54.480 54.197 0.00 1.60417 9.68 2 0 6 1 o 11.320 12.847 180.00 1.59854 1.03 4 2 1 1 o 4.552 4.635 180.00 1.59781 0.83 4 2 -4 1 o 21.271 19.525 180.00 1.57605 3.66 2 4 -3 1 o 17.347 15.657 180.00 1.57568 2.99 0 4 4 1 o 4.662 5.263 0.00 1.56230 0.79 1 3 -6 1 o 21.765 19.124 0.00 1.55334 3.55 2 4 2 1 o 36.540 37.512 180.00 1.55158 5.84 1 1 7 1 o 51.491 52.875 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1 o 77.350 73.672 0.00 1.44312 9.26 4 0 4 1 o 25.302 7.204 0.00 1.43597 1.56 4 2 3 1 o 0.882 0.268 0.00 1.43083 0.11 1 5 1 1 o 1.745 1.252 0.00 1.42870 0.21 5 1 -4 1 o 6.683 6.431 0.00 1.42583 0.80 1 5 -2 1 o 2.420 1.696 180.00 1.41853 0.29 2 4 -5 1 o 1.650 0.977 180.00 1.41585 0.19 3 3 -6 1 o 26.177 21.275 180.00 1.41181 3.00 3 3 4 1 o 1.804 1.434 0.00 1.40939 0.21 1 3 -7 1 o 6.348 4.997 180.00 1.40934 0.73 5 1 1 1 o 2.613 0.831 0.00 1.40670 0.30 4 2 -6 1 o 13.984 14.224 0.00 1.40296 1.58 1 5 2 1 o 1.647 1.588 0.00 1.39150 0.18 2 4 4 1 o 16.649 17.456 0.00 1.38469 1.78 3 1 -8 1 o 1.630 1.224 0.00 1.37669 0.17 1 5 -3 1 o 0.213 0.174 180.00 1.37594 0.02 3 1 6 1 o 29.568 27.757 0.00 1.37356 3.05 2 2 -8 1 o 4.701 4.733 0.00 1.37273 0.49 5 1 -5 1 o 0.044 0.061 180.00 1.37035 0.00 0 2 8 1 o 0.000 0.117 0.00 1.36618 0.00 1 1 8 1 o 0.000 0.095 180.00 1.36359 0.00 5 1 2 1 o 0.616 6.642 180.00 1.34670 0.06 0 4 6 1 o 0.295 1.053 180.00 1.34334 0.03 1 5 3 1 o 2.482 4.234 0.00 1.33937 0.24 4 2 4 1 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1.442 180.00 0.70088 0.01 10 4 -4 1 o 0.011 0.007 0.00 0.70077 0.00 6 0 -16 1 o 1.540 1.051 0.00 0.70066 0.01 9 3 5 1 o 0.598 0.450 0.00 0.70001 0.00 1 1 -17 1 o 0.174 0.134 180.00 0.69996 0.00 4 6 11 1 o 11.462 9.100 0.00 0.69987 0.09 10 2 -9 1 o 0.174 0.138 0.00 0.69987 0.00 2 10 -5 1 o 0.108 0.095 180.00 0.69961 0.00 7 7 4 1 o 3.550 3.578 180.00 0.69922 0.03 9 5 -8 1 o 0.581 0.608 0.00 0.69903 0.00 6 0 12 1 o 69.269 72.610 0.00 0.69901 0.28 10 4 -2 1 o 1.124 1.189 180.00 0.69892 0.01 1 9 -9 1 o 0.299 0.317 0.00 0.69869 0.00 0 8 11 1 o 23.280 23.335 180.00 0.69834 0.19 9 5 2 1 o 5.573 5.250 180.00 0.69815 0.05 10 4 -5 1 o 0.017 0.015 180.00 0.69798 0.00 4 2 14 1 o 6.943 5.963 0.00 0.69784 0.06 10 0 -10 1 o 1.858 1.475 180.00 0.69732 0.01 5 5 11 1 o 9.215 7.252 0.00 0.69726 0.07 5 9 -6 1 o 0.072 0.055 180.00 0.69701 0.00 4 4 13 1 o 1.974 1.456 180.00 0.69681 0.02 2 4 -16 1 o 2.990 2.192 0.00 0.69673 0.02 6 8 -8 1 o 0.002 0.002 0.00 0.69661 0.00 8 6 -9 1 o 2.075 1.547 0.00 0.69642 0.02 6 8 4 1 o 0.072 0.067 180.00 0.69592 0.00 2 10 4 1 o 11.060 11.051 180.00 0.69575 0.09 2 2 -17 1 o 4.480 4.572 0.00 0.69538 0.04 2 8 10 1 o 2.356 2.326 0.00 0.69519 0.02 7 7 -9 1 o 0.144 0.142 0.00 0.69481 0.00 10 4 -1 1 o 1.332 1.486 180.00 0.69434 0.01 1 7 -13 1 o 0.429 0.517 0.00 0.69399 0.00 0 6 14 1 o 12.643 15.407 0.00 0.69380 0.10 2 0 16 1 o 5.421 6.619 0.00 0.69375 0.02 5 3 -16 1 o 0.226 0.293 180.00 0.69337 0.00 2 6 13 1 o 9.533 13.754 180.00 0.69305 0.07 5 9 3 1 o 0.075 0.112 180.00 0.69294 0.00 10 4 -6 1 o 0.809 1.242 180.00 0.69282 0.01 4 8 8 1 o 0.525 0.832 180.00 0.69235 0.00 8 4 7 1 o 4.268 6.675 180.00 0.69226 0.03 7 5 8 1 o 0.783 1.190 0.00 0.69217 0.01 3 7 -13 1 o 0.076 0.094 0.00 0.69083 0.00 4 6 -14 1 o 0.006 0.008 0.00 0.69072 0.00 0 10 6 1 o 6.339 9.201 0.00 0.69033 0.05 8 6 4 1 o 0.450 0.704 180.00 0.69021 0.00 3 7 11 1 o 0.092 0.148 0.00 0.69015 0.00 5 7 -12 1 o 0.538 0.554 180.00 0.68943 0.00 10 2 3 1 o 2.493 2.148 0.00 0.68904 0.02 3 9 -9 1 o 1.623 1.389 180.00 0.68900 0.01 8 2 -14 1 o 0.574 0.500 0.00 0.68855 0.00 3 9 7 1 o 4.704 4.108 180.00 0.68855 0.04 6 2 -16 1 o 0.087 0.083 180.00 0.68835 0.00 1 3 16 1 o 16.120 15.449 180.00 0.68833 0.12 2 10 -6 1 o 0.003 0.004 0.00 0.68797 0.00 10 4 0 1 o 0.397 0.865 0.00 0.68750 0.00 4 10 -1 1 o 1.622 3.917 180.00 0.68719 0.01 4 10 -2 1 o 0.168 0.342 180.00 0.68684 0.00 6 2 12 1 o 10.911 21.175 180.00 0.68678 0.08 9 5 -9 1 o 1.185 1.497 0.00 0.68593 0.01 4 2 -17 1 o 0.001 0.001 180.00 0.68665 0.00 7 3 10 1 o 2.263 3.828 0.00 0.68659 0.02 11 1 -3 1 o 3.044 3.719 180.00 0.68572 0.02 4 4 -16 1 o 0.281 0.416 180.00 0.68636 0.00 4 8 -11 1 o 0.002 0.003 180.00 0.68558 0.00 5 9 -7 1 o 0.265 0.320 180.00 0.68553 0.00 11 1 -4 1 o 0.009 0.012 0.00 0.68621 0.00 10 4 -7 1 o 0.659 0.795 0.00 0.68542 0.00 7 5 -13 1 o 1.216 1.469 0.00 0.68529 0.01 4 10 0 1 o 0.136 0.165 0.00 0.68521 0.00 10 2 -10 1 o 0.421 0.508 0.00 0.68517 0.00 9 5 3 1 o 7.704 9.169 0.00 0.68493 0.06 10 0 4 1 o 0.326 0.389 0.00 0.68487 0.00 11 1 -5 1 o 0.658 1.059 0.00 0.68438 0.00 1 9 9 1 o 0.997 2.180 0.00 0.68419 0.01 4 10 -3 1 o 0.490 1.151 180.00 0.68416 0.00 6 4 -15 1 o 0.059 0.141 0.00 0.68415 0.00 2 4 15 1 o 0.012 0.120 180.00 0.68387 0.00 2 10 5 1 o 0.000 0.052 180.00 0.68350 0.00 0 4 16 1 o 0.162 1.007 0.00 0.68309 0.00 11 1 -2 1 o 0.000 0.000 0.00 0.68292 0.00 9 1 -13 1 o 0.207 0.739 0.00 0.68289 0.00 7 7 5 1 o 2.420 8.366 0.00 0.68287 0.02 6 4 11 1 o 1.078 2.913 0.00 0.68272 0.01 5 1 -17 1 o 0.644 1.325 0.00 0.68248 0.00 2 2 16 1 o 0.038 0.050 0.00 0.68179 0.00 6 8 -9 1 o 0.223 0.326 0.00 0.68132 0.00 9 1 7 1 o 3.510 5.307 0.00 0.68125 0.03 9 3 -12 1 o 0.020 0.030 0.00 0.68125 0.00 4 10 1 1 o 0.054 0.092 180.00 0.68095 0.00 5 9 4 1 o 9.092 15.840 0.00 0.68081 0.07 6 6 -13 1 o 0.254 0.449 0.00 0.68071 0.00 5 3 13 1 o 3.687 6.510 0.00 0.68071 0.03 6 8 5 1 o 10.872 19.379 0.00 0.68056 0.08 7 1 11 1 o 13.511 24.186 0.00 0.68041 0.10 8 6 -10 1 o 0.742 1.329 0.00 0.68040 0.01 5 7 9 1 o 0.720 1.289 180.00 0.68034 0.01 0 2 17 1 o 0.747 1.336 180.00 0.68028 0.01 11 1 -6 1 o 0.063 0.112 180.00 0.68027 0.00 9 3 6 1 o 0.189 0.304 0.00 0.67978 0.00 6 6 9 1 o 3.209 4.827 180.00 0.67952 0.02 4 10 -4 1 o 5.396 8.621 180.00 0.67924 0.04 3 3 -17 1 o 0.009 0.016 0.00 0.67913 0.00 7 3 -15 1 o 0.097 0.249 0.00 0.67861 0.00 10 4 1 1 o 0.172 0.454 0.00 0.67859 0.00 2 8 -12 1 o 0.446 1.297 180.00 0.67845 0.00 3 3 15 1 o 0.454 1.371 180.00 0.67826 0.00 8 4 -13 1 o 0.019 0.058 0.00 0.67825 0.00 7 7 -10 1 o 0.727 2.086 0.00 0.67813 0.01 5 5 -15 1 o 0.307 0.877 180.00 0.67812 0.00 8 2 9 1 o 0.213 0.569 0.00 0.67804 0.00 1 5 15 1 o 12.235 28.999 0.00 0.67791 0.09 11 1 -1 1 o 0.752 1.746 0.00 0.67789 0.01 1 9 -10 1 o 1.987 3.508 180.00 0.67715 0.01 1 3 -17 1 o 0.000 0.130 0.00 0.67603 0.00 10 4 -8 1 o 0.000 1.040 0.00 0.67602 0.00 0 10 7 1 o 0.009 0.138 180.00 0.67538 0.00 2 10 -7 1 o 0.014 0.262 180.00 0.67467 0.00 4 10 2 1 o 0.342 4.371 0.00 0.67455 0.00 4 2 0 2 o 0.000 0.001 180.00 0.67632 0.01 11 1 -7 1 o 0.372 1.286 180.00 0.67402 0.00 1 7 13 1 o 0.145 0.429 0.00 0.67374 0.00 8 6 5 1 o 1.500 4.421 180.00 0.67373 0.01 10 2 4 1 o 0.172 0.460 180.00 0.67335 0.00 1 1 17 1 o 0.018 0.039 180.00 0.67317 0.00 5 9 -8 1 o 2.353 2.388 0.00 0.67239 0.02 4 10 -5 1 o 1.623 1.472 0.00 0.67222 0.01 2 6 -15 1 o 5.428 4.616 180.00 0.67213 0.04 7 1 -16 1 o 0.266 0.213 0.00 0.67204 0.00 0 8 12 1 o 0.975 0.738 180.00 0.67167 0.01 9 5 -10 1 o 0.337 0.390 180.00 0.67134 0.00 11 1 0 1 o 0.328 1.121 0.00 0.67078 0.00 9 5 4 1 o 3.434 5.855 0.00 0.67025 0.02 4 6 12 1 o 1.106 1.564 180.00 0.67007 0.01 4 8 9 1 o 1.814 2.215 0.00 0.66988 0.01 3 9 -10 1 o 0.235 0.271 0.00 0.66978 0.00 2 10 6 1 o 3.928 4.370 180.00 0.66969 0.03 5 1 14 1 o 0.054 0.058 180.00 0.66958 0.00 2 8 11 1 o 1.494 1.599 180.00 0.66957 0.01 3 9 8 1 o 0.008 0.008 180.00 0.66931 0.00 10 2 -11 1 o 0.034 0.033 180.00 0.66919 0.00 8 4 8 1 o 6.379 5.736 0.00 0.66905 0.04 2 0 -18 1 o 1.735 1.342 180.00 0.66852 0.01 3 5 -16 1 o 0.321 0.254 0.00 0.66836 0.00 10 4 2 1 o 0.486 0.455 180.00 0.66785 0.00 1 11 0 1 o 4.999 4.758 180.00 0.66775 0.03 3 5 14 1 o 3.849 3.578 180.00 0.66759 0.03 7 5 9 1 o 13.845 12.571 180.00 0.66754 0.09 1 11 -1 1 o 2.468 2.049 0.00 0.66740 0.02 5 9 5 1 o 0.071 0.046 0.00 0.66713 0.00 5 5 12 1 o 7.293 4.374 0.00 0.66706 0.05 1 5 -16 1 o 3.356 1.710 0.00 0.66684 0.02 4 10 3 1 o 3.878 2.161 0.00 0.66617 0.03 1 11 1 1 o 8.210 4.868 0.00 0.66596 0.06 11 1 -8 1 o 0.064 0.039 0.00 0.66579 0.00 7 7 6 1 o 7.048 4.348 0.00 0.66548 0.05 3 1 -18 1 o 1.560 0.948 180.00 0.66529 0.01 5 7 -13 1 o 1.644 0.982 0.00 0.66518 0.01 1 11 -2 1 o 13.065 7.545 0.00 0.66492 0.09 10 4 -9 1 o 0.050 0.028 180.00 0.66487 0.00 6 8 -10 1 o 0.646 0.371 0.00 0.66486 0.00 3 1 16 1 o 3.409 1.945 0.00 0.66443 0.02 1 7 -14 1 o 15.961 8.837 0.00 0.66425 0.11 6 8 6 1 o 1.139 0.591 180.00 0.66405 0.01 11 3 -4 1 o 0.280 0.128 180.00 0.66362 0.00 8 6 -11 1 o 0.418 0.188 180.00 0.66332 0.00 4 10 -6 1 o 0.100 0.045 180.00 0.66330 0.00 11 3 -3 1 o 0.870 0.397 0.00 0.66318 0.01 4 4 14 1 o 13.903 6.383 180.00 0.66313 0.09 4 8 -12 1 o 0.295 0.136 180.00 0.66311 0.00 3 7 -14 1 o 3.645 1.746 0.00 0.66289 0.02 10 0 -12 1 o 0.792 0.389 0.00 0.66272 0.00 _reflns_number_total 1166 _reflns_limit_h_min 0 _reflns_limit_h_max 11 _reflns_limit_k_min 0 _reflns_limit_k_max 11 _reflns_limit_l_min -18 _reflns_limit_l_max 17 _reflns_d_resolution_high 0.663 _reflns_d_resolution_low 2.533 _database_code_depnum_ccdc_archive 'CCDC 951695'