Figure 1b Lambda = 1.5418 A 2theta Intensity 5 241 5.05 277 5.1 272 5.15 311 5.2 300 5.25 250 5.3 264 5.35 321 5.4 278 5.45 298 5.5 263 5.55 251 5.6 266 5.65 273 5.7 260 5.75 250 5.8 262 5.85 261 5.9 245 5.95 246 6 283 6.05 265 6.1 230 6.15 241 6.2 223 6.25 222 6.3 240 6.35 236 6.4 214 6.45 217 6.5 227 6.55 236 6.6 224 6.65 220 6.7 217 6.75 199 6.8 211 6.85 197 6.9 228 6.95 212 7 193 7.05 188 7.1 185 7.15 222 7.2 201 7.25 217 7.3 207 7.35 213 7.4 210 7.45 209 7.5 188 7.55 196 7.6 209 7.65 189 7.7 184 7.75 179 7.8 192 7.85 204 7.9 200 7.95 207 8 189 8.05 184 8.1 206 8.15 189 8.2 194 8.25 206 8.3 198 8.35 187 8.4 197 8.45 157 8.5 199 8.55 197 8.6 187 8.65 171 8.7 203 8.75 180 8.8 185 8.85 190 8.9 187 8.95 163 9 200 9.05 195 9.1 187 9.15 210 9.2 214 9.25 224 9.3 198 9.35 228 9.4 207 9.45 188 9.5 173 9.55 203 9.6 203 9.65 187 9.7 170 9.75 161 9.8 157 9.85 167 9.9 179 9.95 187 10 178 10.05 148 10.1 161 10.15 147 10.2 173 10.25 172 10.3 166 10.35 148 10.4 153 10.45 185 10.5 192 10.55 167 10.6 185 10.65 194 10.7 214 10.75 219 10.8 245 10.85 256 10.9 198 10.95 198 11 172 11.05 199 11.1 180 11.15 191 11.2 227 11.25 213 11.3 280 11.35 301 11.4 376 11.45 483 11.5 646 11.55 890 11.6 1184 11.65 1670 11.7 2239 11.75 3105 11.8 4625 11.85 7282 11.9 11629 11.95 17100 12 18491 12.05 10351 12.1 2966 12.15 1633 12.2 1232 12.25 956 12.3 724 12.35 558 12.4 498 12.45 434 12.5 353 12.55 358 12.6 354 12.65 346 12.7 340 12.75 312 12.8 326 12.85 323 12.9 305 12.95 323 13 281 13.05 273 13.1 238 13.15 246 13.2 267 13.25 226 13.3 224 13.35 239 13.4 225 13.45 222 13.5 231 13.55 193 13.6 214 13.65 220 13.7 179 13.75 182 13.8 180 13.85 171 13.9 193 13.95 182 14 146 14.05 181 14.1 176 14.15 172 14.2 152 14.25 152 14.3 153 14.35 148 14.4 135 14.45 139 14.5 113 14.55 113 14.6 124 14.65 120 14.7 124 14.75 119 14.8 115 14.85 124 14.9 139 14.95 116 15 117 15.05 137 15.1 112 15.15 115 15.2 122 15.25 93 15.3 105 15.35 87 15.4 123 15.45 96 15.5 99 15.55 115 15.6 90 15.65 93 15.7 113 15.75 84 15.8 97 15.85 93 15.9 91 15.95 96 16 104 16.05 88 16.1 102 16.15 93 16.2 74 16.25 103 16.3 76 16.35 81 16.4 72 16.45 96 16.5 99 16.55 83 16.6 73 16.65 81 16.7 86 16.75 90 16.8 87 16.85 81 16.9 84 16.95 92 17 83 17.05 81 17.1 88 17.15 90 17.2 91 17.25 77 17.3 78 17.35 58 17.4 86 17.45 79 17.5 66 17.55 69 17.6 65 17.65 78 17.7 64 17.75 83 17.8 68 17.85 69 17.9 88 17.95 75 18 74 18.05 70 18.1 72 18.15 54 18.2 72 18.25 83 18.3 85 18.35 80 18.4 79 18.45 122 18.5 150 18.55 164 18.6 225 18.65 248 18.7 236 18.75 163 18.8 111 18.85 75 18.9 88 18.95 72 19 68 19.05 73 19.1 77 19.15 71 19.2 73 19.25 69 19.3 65 19.35 64 19.4 73 19.45 66 19.5 61 19.55 65 19.6 64 19.65 46 19.7 68 19.75 70 19.8 53 19.85 77 19.9 91 19.95 81 20 76 20.05 67 20.1 68 20.15 60 20.2 78 20.25 81 20.3 88 20.35 77 20.4 88 20.45 65 20.5 69 20.55 71 20.6 69 20.65 76 20.7 67 20.75 75 20.8 62 20.85 61 20.9 70 20.95 71 21 93 21.05 76 21.1 83 21.15 64 21.2 84 21.25 92 21.3 78 21.35 85 21.4 79 21.45 80 21.5 83 21.55 85 21.6 99 21.65 92 21.7 80 21.75 105 21.8 79 21.85 80 21.9 66 21.95 85 22 75 22.05 81 22.1 82 22.15 68 22.2 85 22.25 79 22.3 54 22.35 78 22.4 71 22.45 70 22.5 71 22.55 72 22.6 61 22.65 63 22.7 64 22.75 75 22.8 73 22.85 64 22.9 68 22.95 48 23 49 23.05 64 23.1 73 23.15 57 23.2 84 23.25 90 23.3 80 23.35 94 23.4 82 23.45 88 23.5 91 23.55 114 23.6 96 23.65 110 23.7 135 23.75 151 23.8 188 23.85 268 23.9 400 23.95 616 24 1151 24.05 2233 24.1 3138 24.15 2353 24.2 1088 24.25 431 24.3 275 24.35 190 24.4 156 24.45 111 24.5 125 24.55 86 24.6 95 24.65 67 24.7 76 24.75 72 24.8 78 24.85 58 24.9 57 24.95 70 25 62 25.05 69 25.1 70 25.15 66 25.2 65 25.25 50 25.3 64 25.35 54 25.4 68 25.45 59 25.5 57 25.55 49 25.6 56 25.65 68 25.7 62 25.75 50 25.8 66 25.85 62 25.9 54 25.95 51 26 51 26.05 54 26.1 54 26.15 58 26.2 53 26.25 55 26.3 57 26.35 56 26.4 51 26.45 50 26.5 61 26.55 60 26.6 55 26.65 49 26.7 44 26.75 57 26.8 45 26.85 53 26.9 51 26.95 49 27 43 27.05 50 27.1 49 27.15 47 27.2 40 27.25 57 27.3 43 27.35 48 27.4 50 27.45 51 27.5 42 27.55 51 27.6 48 27.65 47 27.7 50 27.75 56 27.8 65 27.85 69 27.9 87 27.95 102 28 155 28.05 187 28.1 217 28.15 198 28.2 141 28.25 98 28.3 93 28.35 57 28.4 64 28.45 54 28.5 55 28.55 56 28.6 68 28.65 86 28.7 137 28.75 147 28.8 120 28.85 95 28.9 58 28.95 56 29 53 29.05 52 29.1 47 29.15 37 29.2 51 29.25 46 29.3 36 29.35 48 29.4 45 29.45 45 29.5 54 29.55 42 29.6 46 29.65 43 29.7 31 29.75 37 29.8 35 29.85 44 29.9 51 29.95 48 30 41 30.05 40 30.1 37 30.15 46 30.2 42 30.25 32 30.3 36 30.35 31 30.4 36 30.45 51 30.5 42 30.55 39 30.6 39 30.65 22 30.7 38 30.75 40 30.8 44 30.85 38 30.9 48 30.95 46 31 50 31.05 51 31.1 59 31.15 71 31.2 102 31.25 88 31.3 70 31.35 64 31.4 51 31.45 51 31.5 45 31.55 52 31.6 47 31.65 62 31.7 51 31.75 32 31.8 45 31.85 32 31.9 46 31.95 26 32 56 32.05 47 32.1 37 32.15 32 32.2 34 32.25 40 32.3 31 32.35 44 32.4 25 32.45 33 32.5 43 32.55 34 32.6 26 32.65 23 32.7 27 32.75 38 32.8 27 32.85 38 32.9 39 32.95 41 33 35 33.05 44 33.1 35 33.15 29 33.2 39 33.25 39 33.3 44 33.35 35 33.4 24 33.45 28 33.5 22 33.55 40 33.6 36 33.65 34 33.7 34 33.75 34 33.8 35 33.85 42 33.9 23 33.95 32 34 35 34.05 39 34.1 24 34.15 45 34.2 25 34.25 36 34.3 41 34.35 43 34.4 37 34.45 42 34.5 27 34.55 57 34.6 38 34.65 24 34.7 22 34.75 22 34.8 30 34.85 30 34.9 35 34.95 34 35 18 35.05 19 35.1 33 35.15 46 35.2 30 35.25 32 35.3 32 35.35 33 35.4 40 35.45 37 35.5 31 35.55 33 35.6 37 35.65 28 35.7 50 35.75 32 35.8 31 35.85 41 35.9 29 35.95 19 36 48 36.05 37 36.1 38 36.15 42 36.2 36 36.25 51 36.3 50 36.35 69 36.4 131 36.45 182 36.5 255 36.55 195 36.6 149 36.65 101 36.7 60 36.75 48 36.8 32 36.85 43 36.9 50 36.95 41 37 44 37.05 45 37.1 27 37.15 33 37.2 38 37.25 35 37.3 34 37.35 44 37.4 48 37.45 36 37.5 43 37.55 35 37.6 50 37.65 42 37.7 53 37.75 84 37.8 94 37.85 92 37.9 83 37.95 75 38 83 38.05 71 38.1 59 38.15 49 38.2 43 38.25 44 38.3 27 38.35 42 38.4 42 38.45 37 38.5 31 38.55 58 38.6 38 38.65 47 38.7 41 38.75 50 38.8 36 38.85 43 38.9 47 38.95 61 39 75 39.05 79 39.1 92 39.15 127 39.2 198 39.25 299 39.3 480 39.35 565 39.4 503 39.45 406 39.5 336 39.55 200 39.6 114 39.65 103 39.7 75 39.75 65 39.8 56 39.85 57 39.9 55 39.95 39 40 33 40.05 39 40.1 37 40.15 36 40.2 39 40.25 40 40.3 40 40.35 41 40.4 33 40.45 42 40.5 39 40.55 38 40.6 40 40.65 45 40.7 52 40.75 35 40.8 43 40.85 53 40.9 51 40.95 42 41 34 41.05 37 41.1 27 41.15 45 41.2 22 41.25 34 41.3 33 41.35 36 41.4 39 41.45 34 41.5 27 41.55 25 41.6 34 41.65 27 41.7 38 41.75 41 41.8 26 41.85 29 41.9 42 41.95 35 42 34 42.05 42 42.1 38 42.15 28 42.2 33 42.25 31 42.3 40 42.35 36 42.4 28 42.45 27 42.5 44 42.55 37 42.6 33 42.65 42 42.7 26 42.75 37 42.8 33 42.85 30 42.9 28 42.95 34 43 32 43.05 31 43.1 30 43.15 30 43.2 34 43.25 28 43.3 25 43.35 27 43.4 37 43.45 34 43.5 31 43.55 28 43.6 23 43.65 33 43.7 27 43.75 32 43.8 28 43.85 21 43.9 34 43.95 29 44 32 44.05 36 44.1 25 44.15 22 44.2 30 44.25 37 44.3 29 44.35 37 44.4 24 44.45 35 44.5 30 44.55 25 44.6 31 44.65 25 44.7 28 44.75 22 44.8 37 44.85 21 44.9 16 44.95 29 45 25 45.05 38 45.1 26 45.15 23 45.2 26 45.25 23 45.3 26 45.35 27 45.4 32 45.45 30 45.5 37 45.55 43 45.6 30 45.65 29 45.7 33 45.75 29 45.8 24 45.85 27 45.9 31 45.95 27 46 22 46.05 29 46.1 23 46.15 35 46.2 25 46.25 48 46.3 32 46.35 30 46.4 23 46.45 26 46.5 29 46.55 18 46.6 30 46.65 28 46.7 26 46.75 25 46.8 41 46.85 21 46.9 17 46.95 23 47 25 47.05 25 47.1 21 47.15 27 47.2 36 47.25 25 47.3 24 47.35 26 47.4 27 47.45 23 47.5 21 47.55 22 47.6 26 47.65 25 47.7 24 47.75 33 47.8 25 47.85 29 47.9 28 47.95 41 48 35 48.05 40 48.1 28 48.15 53 48.2 41 48.25 43 48.3 39 48.35 37 48.4 29 48.45 26 48.5 33 48.55 24 48.6 36 48.65 33 48.7 28 48.75 25 48.8 29 48.85 20 48.9 34 48.95 32 49 28 49.05 38 49.1 54 49.15 53 49.2 77 49.25 124 49.3 218 49.35 241 49.4 173 49.45 173 49.5 114 49.55 79 49.6 58 49.65 44 49.7 44 49.75 32 49.8 33 49.85 34 49.9 36 49.95 18 50 24 50.05 35 50.1 28 50.15 30 50.2 26 50.25 24 50.3 35 50.35 27 50.4 34 50.45 45 50.5 47 50.55 37 50.6 57 50.65 54 50.7 35 50.75 39 50.8 25 50.85 23 50.9 39 50.95 31 51 25 51.05 31 51.1 23 51.15 23 51.2 25 51.25 33 51.3 31 51.35 39 51.4 43 51.45 38 51.5 74 51.55 58 51.6 82 51.65 80 51.7 75 51.75 68 51.8 33 51.85 35 51.9 43 51.95 32 52 24 52.05 34 52.1 28 52.15 26 52.2 22 52.25 37 52.3 25 52.35 29 52.4 18 52.45 25 52.5 27 52.55 19 52.6 15 52.65 34 52.7 31 52.75 27 52.8 18 52.85 22 52.9 27 52.95 19 53 23 53.05 22 53.1 28 53.15 25 53.2 20 53.25 27 53.3 32 53.35 30 53.4 37 53.45 32 53.5 38 53.55 46 53.6 77 53.65 82 53.7 112 53.75 128 53.8 176 53.85 175 53.9 152 53.95 145 54 141 54.05 69 54.1 78 54.15 70 54.2 37 54.25 45 54.3 43 54.35 34 54.4 33 54.45 36 54.5 30 54.55 37 54.6 27 54.65 31 54.7 15 54.75 25 54.8 31 54.85 29 54.9 27 54.95 26 55 41 55.05 23 55.1 30 55.15 21 55.2 22 55.25 22 55.3 19 55.35 19 55.4 37 55.45 21 55.5 21 55.55 26 55.6 28 55.65 32 55.7 26 55.75 26 55.8 30 55.85 21 55.9 25 55.95 25 56 29 56.05 34 56.1 28 56.15 28 56.2 32 56.25 28 56.3 19 56.35 24 56.4 27 56.45 23 56.5 21 56.55 23 56.6 17 56.65 19 56.7 13 56.75 21 56.8 19 56.85 14 56.9 20 56.95 15 57 26 57.05 22 57.1 23 57.15 20 57.2 23 57.25 23 57.3 23 57.35 22 57.4 17 57.45 17 57.5 19 57.55 18 57.6 18 57.65 21 57.7 21 57.75 25 57.8 31 57.85 25 57.9 24 57.95 28 58 33 58.05 35 58.1 36 58.15 42 58.2 49 58.25 46 58.3 37 58.35 37 58.4 42 58.45 36 58.5 32 58.55 18 58.6 29 58.65 24 58.7 20 58.75 12 58.8 26 58.85 21 58.9 29 58.95 21 59 22 59.05 25 59.1 19 59.15 19 59.2 20 59.25 19 59.3 22 59.35 27 59.4 35 59.45 33 59.5 39 59.55 24 59.6 32 59.65 29 59.7 25 59.75 36 59.8 28 59.85 29 59.9 27 59.95 22 60 31 60.05 49 60.1 35 60.15 45 60.2 52 60.25 55 60.3 41 60.35 31 60.4 45 60.45 31 60.5 29 60.55 34 60.6 24 60.65 26 60.7 20 60.75 28 60.8 26 60.85 22 60.9 34 60.95 38 61 23 61.05 26 61.1 32 61.15 13 61.2 21 61.25 21 61.3 19 61.35 23 61.4 17 61.45 13 61.5 17 61.55 16 61.6 20 61.65 20 61.7 19 61.75 23 61.8 21 61.85 15 61.9 17 61.95 10 62 14 62.05 12 62.1 24 62.15 32 62.2 29 62.25 13 62.3 24 62.35 24 62.4 17 62.45 26 62.5 15 62.55 27 62.6 20 62.65 27 62.7 18 62.75 28 62.8 40 62.85 57 62.9 54 62.95 42 63 41 63.05 40 63.1 30 63.15 23 63.2 28 63.25 22 63.3 17 63.35 28 63.4 16 63.45 26 63.5 19 63.55 24 63.6 30 63.65 22 63.7 22 63.75 23 63.8 21 63.85 11 63.9 21 63.95 17 64 17 64.05 19 64.1 19 64.15 22 64.2 18 64.25 20 64.3 24 64.35 21 64.4 20 64.45 18 64.5 24 64.55 18 64.6 21 64.65 19 64.7 29 64.75 25 64.8 22 64.85 30 64.9 20 64.95 28 65 35 65.05 22 65.1 29 65.15 31 65.2 18 65.25 18 65.3 22 65.35 21 65.4 22 65.45 20 65.5 21 65.55 17 65.6 16 65.65 22 65.7 17 65.75 20 65.8 18 65.85 22 65.9 23 65.95 25 66 29 66.05 34 66.1 23 66.15 26 66.2 38 66.25 26 66.3 17 66.35 34 66.4 29 66.45 34 66.5 31 66.55 36 66.6 45 66.65 39 66.7 48 66.75 62 66.8 60 66.85 53 66.9 49 66.95 40 67 40 67.05 33 67.1 27 67.15 31 67.2 23 67.25 18 67.3 25 67.35 22 67.4 38 67.45 29 67.5 25 67.55 30 67.6 19 67.65 26 67.7 26 67.75 22 67.8 24 67.85 26 67.9 27 67.95 23 68 27 68.05 23 68.1 23 68.15 23 68.2 26 68.25 13 68.3 18 68.35 27 68.4 25 68.45 13 68.5 11 68.55 16 68.6 17 68.65 18 68.7 27 68.75 31 68.8 10 68.85 26 68.9 24 68.95 24 69 19 69.05 27 69.1 18 69.15 17 69.2 10 69.25 30 69.3 22 69.35 27 69.4 13 69.45 27 69.5 28 69.55 27 69.6 37 69.65 26 69.7 40 69.75 40 69.8 48 69.85 48 69.9 56 69.95 52 70 46 70.05 40 70.1 55 70.15 31 70.2 31 70.25 24 70.3 26 70.35 24 70.4 33 70.45 21 70.5 19 70.55 24 70.6 26 70.65 19 70.7 19 70.75 18 70.8 18 70.85 19 70.9 20 70.95 16 71 15 71.05 14 71.1 11 71.15 16 71.2 15 71.25 18 71.3 19 71.35 23 71.4 12 71.45 16 71.5 20 71.55 10 71.6 20 71.65 19 71.7 17 71.75 24 71.8 23 71.85 19 71.9 18 71.95 14 72 26 72.05 22 72.1 18 72.15 19 72.2 33 72.25 30 72.3 34 72.35 29 72.4 29 72.45 29 72.5 34 72.55 29 72.6 37 72.65 32 72.7 21 72.75 37 72.8 22 72.85 28 72.9 19 72.95 22 73 19 73.05 19 73.1 16 73.15 22 73.2 18 73.25 15 73.3 19 73.35 20 73.4 20 73.45 17 73.5 24 73.55 22 73.6 19 73.65 16 73.7 18 73.75 23 73.8 20 73.85 17 73.9 22 73.95 12 74 15 74.05 15 74.1 13 74.15 12 74.2 17 74.25 12 74.3 13 74.35 19 74.4 15 74.45 11 74.5 15 74.55 21 74.6 14 74.65 15 74.7 18 74.75 18 74.8 21 74.85 12 74.9 18 74.95 16 75 24