Figure 2 Lambda = 1.5418 A 2theta Intensity 5 146 5.05 133 5.1 134 5.15 152 5.2 133 5.25 133 5.3 138 5.35 132 5.4 142 5.45 146 5.5 157 5.55 147 5.6 151 5.65 138 5.7 157 5.75 155 5.8 140 5.85 131 5.9 147 5.95 156 6 155 6.05 149 6.1 158 6.15 167 6.2 142 6.25 141 6.3 146 6.35 161 6.4 158 6.45 159 6.5 169 6.55 140 6.6 163 6.65 125 6.7 142 6.75 138 6.8 148 6.85 173 6.9 147 6.95 166 7 162 7.05 163 7.1 151 7.15 202 7.2 173 7.25 178 7.3 165 7.35 185 7.4 171 7.45 177 7.5 203 7.55 200 7.6 185 7.65 183 7.7 199 7.75 161 7.8 213 7.85 217 7.9 196 7.95 174 8 192 8.05 186 8.1 220 8.15 198 8.2 186 8.25 213 8.3 189 8.35 188 8.4 194 8.45 189 8.5 181 8.55 183 8.6 198 8.65 223 8.7 210 8.75 218 8.8 253 8.85 212 8.9 214 8.95 207 9 225 9.05 216 9.1 210 9.15 211 9.2 211 9.25 213 9.3 253 9.35 208 9.4 193 9.45 234 9.5 199 9.55 209 9.6 187 9.65 192 9.7 204 9.75 217 9.8 174 9.85 183 9.9 187 9.95 200 10 154 10.05 176 10.1 166 10.15 186 10.2 163 10.25 177 10.3 178 10.35 168 10.4 181 10.45 167 10.5 151 10.55 164 10.6 164 10.65 173 10.7 178 10.75 171 10.8 154 10.85 165 10.9 174 10.95 159 11 182 11.05 179 11.1 159 11.15 176 11.2 170 11.25 189 11.3 190 11.35 207 11.4 189 11.45 188 11.5 190 11.55 184 11.6 177 11.65 193 11.7 196 11.75 212 11.8 189 11.85 210 11.9 213 11.95 208 12 181 12.05 198 12.1 193 12.15 178 12.2 192 12.25 178 12.3 225 12.35 187 12.4 181 12.45 218 12.5 180 12.55 183 12.6 183 12.65 190 12.7 163 12.75 174 12.8 166 12.85 176 12.9 178 12.95 157 13 147 13.05 176 13.1 147 13.15 171 13.2 151 13.25 152 13.3 143 13.35 159 13.4 138 13.45 160 13.5 149 13.55 161 13.6 112 13.65 129 13.7 139 13.75 137 13.8 134 13.85 141 13.9 123 13.95 127 14 98 14.05 157 14.1 121 14.15 149 14.2 131 14.25 144 14.3 129 14.35 139 14.4 133 14.45 126 14.5 127 14.55 128 14.6 121 14.65 119 14.7 120 14.75 107 14.8 109 14.85 107 14.9 99 14.95 118 15 109 15.05 113 15.1 106 15.15 115 15.2 108 15.25 125 15.3 107 15.35 105 15.4 101 15.45 118 15.5 105 15.55 108 15.6 114 15.65 113 15.7 126 15.75 91 15.8 103 15.85 96 15.9 93 15.95 101 16 112 16.05 111 16.1 89 16.15 103 16.2 113 16.25 92 16.3 126 16.35 106 16.4 96 16.45 115 16.5 97 16.55 100 16.6 116 16.65 103 16.7 115 16.75 88 16.8 104 16.85 121 16.9 108 16.95 102 17 117 17.05 126 17.1 124 17.15 127 17.2 92 17.25 100 17.3 101 17.35 119 17.4 131 17.45 133 17.5 124 17.55 116 17.6 108 17.65 132 17.7 93 17.75 123 17.8 109 17.85 119 17.9 122 17.95 141 18 117 18.05 124 18.1 139 18.15 134 18.2 121 18.25 120 18.3 114 18.35 115 18.4 110 18.45 122 18.5 110 18.55 119 18.6 112 18.65 131 18.7 105 18.75 111 18.8 104 18.85 104 18.9 133 18.95 118 19 116 19.05 121 19.1 95 19.15 113 19.2 136 19.25 134 19.3 128 19.35 120 19.4 108 19.45 138 19.5 125 19.55 133 19.6 132 19.65 158 19.7 135 19.75 133 19.8 147 19.85 148 19.9 143 19.95 144 20 159 20.05 165 20.1 146 20.15 158 20.2 179 20.25 204 20.3 204 20.35 223 20.4 197 20.45 246 20.5 242 20.55 261 20.6 263 20.65 296 20.7 353 20.75 350 20.8 410 20.85 458 20.9 478 20.95 570 21 669 21.05 779 21.1 917 21.15 1000 21.2 1081 21.25 1075 21.3 1120 21.35 973 21.4 940 21.45 895 21.5 828 21.55 762 21.6 723 21.65 661 21.7 569 21.75 520 21.8 463 21.85 458 21.9 420 21.95 352 22 338 22.05 344 22.1 306 22.15 273 22.2 255 22.25 237 22.3 211 22.35 197 22.4 222 22.45 204 22.5 181 22.55 177 22.6 137 22.65 154 22.7 146 22.75 150 22.8 155 22.85 134 22.9 108 22.95 113 23 108 23.05 108 23.1 110 23.15 97 23.2 101 23.25 97 23.3 103 23.35 70 23.4 100 23.45 91 23.5 73 23.55 80 23.6 75 23.65 93 23.7 86 23.75 81 23.8 74 23.85 83 23.9 90 23.95 85 24 68 24.05 74 24.1 86 24.15 74 24.2 90 24.25 50 24.3 62 24.35 67 24.4 62 24.45 42 24.5 59 24.55 58 24.6 50 24.65 54 24.7 54 24.75 66 24.8 50 24.85 50 24.9 56 24.95 54 25 64 25.05 59 25.1 42 25.15 45 25.2 58 25.25 47 25.3 54 25.35 54 25.4 47 25.45 43 25.5 52 25.55 52 25.6 42 25.65 38 25.7 45 25.75 34 25.8 47 25.85 51 25.9 49 25.95 49 26 51 26.05 40 26.1 62 26.15 38 26.2 48 26.25 46 26.3 37 26.35 52 26.4 35 26.45 45 26.5 47 26.55 52 26.6 48 26.65 45 26.7 43 26.75 50 26.8 44 26.85 38 26.9 53 26.95 38 27 42 27.05 39 27.1 49 27.15 44 27.2 37 27.25 37 27.3 49 27.35 54 27.4 38 27.45 50 27.5 50 27.55 47 27.6 43 27.65 52 27.7 43 27.75 43 27.8 39 27.85 47 27.9 39 27.95 42 28 45 28.05 59 28.1 44 28.15 59 28.2 47 28.25 60 28.3 50 28.35 51 28.4 65 28.45 67 28.5 74 28.55 76 28.6 79 28.65 122 28.7 231 28.75 259 28.8 233 28.85 161 28.9 115 28.95 97 29 85 29.05 75 29.1 64 29.15 78 29.2 65 29.25 64 29.3 60 29.35 65 29.4 86 29.45 78 29.5 81 29.55 83 29.6 99 29.65 107 29.7 91 29.75 89 29.8 83 29.85 88 29.9 67 29.95 59 30 62 30.05 76 30.1 60 30.15 70 30.2 65 30.25 65 30.3 52 30.35 50 30.4 53 30.45 48 30.5 45 30.55 60 30.6 39 30.65 50 30.7 39 30.75 63 30.8 53 30.85 43 30.9 52 30.95 49 31 42 31.05 38 31.1 61 31.15 56 31.2 60 31.25 48 31.3 57 31.35 42 31.4 54 31.45 53 31.5 58 31.55 50 31.6 50 31.65 53 31.7 58 31.75 64 31.8 68 31.85 78 31.9 60 31.95 74 32 79 32.05 58 32.1 65 32.15 55 32.2 51 32.25 49 32.3 43 32.35 42 32.4 38 32.45 47 32.5 38 32.55 40 32.6 44 32.65 39 32.7 45 32.75 45 32.8 53 32.85 40 32.9 48 32.95 46 33 39 33.05 46 33.1 40 33.15 38 33.2 38 33.25 39 33.3 43 33.35 45 33.4 40 33.45 46 33.5 35 33.55 45 33.6 53 33.65 51 33.7 51 33.75 44 33.8 47 33.85 57 33.9 54 33.95 42 34 51 34.05 50 34.1 50 34.15 45 34.2 59 34.25 54 34.3 65 34.35 73 34.4 56 34.45 66 34.5 66 34.55 53 34.6 59 34.65 88 34.7 88 34.75 88 34.8 76 34.85 79 34.9 76 34.95 89 35 82 35.05 77 35.1 85 35.15 75 35.2 90 35.25 60 35.3 83 35.35 90 35.4 87 35.45 78 35.5 85 35.55 95 35.6 98 35.65 103 35.7 72 35.75 76 35.8 85 35.85 81 35.9 76 35.95 72 36 60 36.05 80 36.1 83 36.15 64 36.2 73 36.25 65 36.3 55 36.35 63 36.4 56 36.45 70 36.5 52 36.55 76 36.6 67 36.65 49 36.7 56 36.75 48 36.8 48 36.85 59 36.9 41 36.95 63 37 57 37.05 45 37.1 53 37.15 58 37.2 49 37.25 43 37.3 49 37.35 53 37.4 55 37.45 60 37.5 49 37.55 36 37.6 46 37.65 40 37.7 39 37.75 46 37.8 42 37.85 38 37.9 39 37.95 42 38 41 38.05 34 38.1 32 38.15 38 38.2 30 38.25 32 38.3 38 38.35 44 38.4 52 38.45 33 38.5 55 38.55 34 38.6 57 38.65 52 38.7 37 38.75 37 38.8 35 38.85 33 38.9 35 38.95 42 39 39 39.05 38 39.1 43 39.15 35 39.2 33 39.25 35 39.3 40 39.35 37 39.4 43 39.45 34 39.5 43 39.55 38 39.6 37 39.65 43 39.7 34 39.75 40 39.8 37 39.85 50 39.9 38 39.95 38 40 37 40.05 43 40.1 46 40.15 42 40.2 36 40.25 36 40.3 39 40.35 49 40.4 51 40.45 46 40.5 41 40.55 33 40.6 56 40.65 43 40.7 44 40.75 54 40.8 47 40.85 39 40.9 45 40.95 45 41 47 41.05 65 41.1 46 41.15 53 41.2 50 41.25 51 41.3 41 41.35 44 41.4 54 41.45 59 41.5 84 41.55 71 41.6 59 41.65 70 41.7 82 41.75 66 41.8 65 41.85 83 41.9 78 41.95 73 42 73 42.05 68 42.1 62 42.15 67 42.2 70 42.25 59 42.3 60 42.35 53 42.4 67 42.45 44 42.5 70 42.55 55 42.6 58 42.65 49 42.7 49 42.75 59 42.8 58 42.85 46 42.9 60 42.95 65 43 81 43.05 77 43.1 96 43.15 103 43.2 91 43.25 87 43.3 62 43.35 69 43.4 57 43.45 66 43.5 66 43.55 59 43.6 48 43.65 35 43.7 55 43.75 52 43.8 37 43.85 30 43.9 41 43.95 45 44 41 44.05 35 44.1 34 44.15 39 44.2 36 44.25 36 44.3 38 44.35 32 44.4 36 44.45 29 44.5 34 44.55 42 44.6 34 44.65 43 44.7 21 44.75 40 44.8 41 44.85 38 44.9 30 44.95 37 45 37 45.05 48 45.1 43 45.15 52 45.2 44 45.25 36 45.3 45 45.35 36 45.4 46 45.45 47 45.5 44 45.55 31 45.6 47 45.65 48 45.7 29 45.75 36 45.8 30 45.85 41 45.9 34 45.95 30 46 32 46.05 24 46.1 38 46.15 49 46.2 52 46.25 40 46.3 53 46.35 43 46.4 39 46.45 41 46.5 29 46.55 37 46.6 29 46.65 27 46.7 28 46.75 22 46.8 33 46.85 30 46.9 16 46.95 24 47 32 47.05 35 47.1 19 47.15 32 47.2 19 47.25 22 47.3 25 47.35 28 47.4 37 47.45 34 47.5 26 47.55 18 47.6 30 47.65 30 47.7 25 47.75 30 47.8 23 47.85 31 47.9 39 47.95 26 48 25 48.05 25 48.1 16 48.15 21 48.2 34 48.25 19 48.3 21 48.35 38 48.4 32 48.45 20 48.5 27 48.55 28 48.6 25 48.65 28 48.7 35 48.75 29 48.8 26 48.85 26 48.9 18 48.95 23 49 27 49.05 26 49.1 34 49.15 31 49.2 32 49.25 30 49.3 27 49.35 38 49.4 31 49.45 33 49.5 29 49.55 38 49.6 30 49.65 32 49.7 22 49.75 32 49.8 27 49.85 38 49.9 42 49.95 29 50 25 50.05 28 50.1 35 50.15 29 50.2 20 50.25 40 50.3 31 50.35 40 50.4 30 50.45 40 50.5 35 50.55 38 50.6 31 50.65 42 50.7 35 50.75 24 50.8 41 50.85 26 50.9 31 50.95 40 51 28 51.05 35 51.1 30 51.15 29 51.2 22 51.25 38 51.3 27 51.35 17 51.4 27 51.45 38 51.5 27 51.55 33 51.6 29 51.65 30 51.7 30 51.75 20 51.8 18 51.85 36 51.9 29 51.95 28 52 34 52.05 25 52.1 35 52.15 29 52.2 29 52.25 25 52.3 24 52.35 21 52.4 28 52.45 26 52.5 27 52.55 20 52.6 29 52.65 25 52.7 26 52.75 31 52.8 36 52.85 36 52.9 30 52.95 25 53 21 53.05 25 53.1 23 53.15 31 53.2 34 53.25 39 53.3 31 53.35 37 53.4 37 53.45 33 53.5 33 53.55 20 53.6 31 53.65 30 53.7 28 53.75 37 53.8 49 53.85 31 53.9 27 53.95 38 54 39 54.05 39 54.1 32 54.15 54 54.2 37 54.25 38 54.3 32 54.35 62 54.4 44 54.45 34 54.5 42 54.55 49 54.6 53 54.65 40 54.7 52 54.75 40 54.8 54 54.85 54 54.9 60 54.95 53 55 42 55.05 45 55.1 53 55.15 46 55.2 36 55.25 54 55.3 39 55.35 49 55.4 56 55.45 53 55.5 46 55.55 37 55.6 39 55.65 50 55.7 43 55.75 59 55.8 43 55.85 49 55.9 44 55.95 37 56 45 56.05 51 56.1 39 56.15 53 56.2 35 56.25 45 56.3 51 56.35 45 56.4 36 56.45 44 56.5 50 56.55 36 56.6 45 56.65 33 56.7 32 56.75 45 56.8 28 56.85 47 56.9 34 56.95 38 57 32 57.05 39 57.1 51 57.15 28 57.2 36 57.25 26 57.3 37 57.35 30 57.4 25 57.45 26 57.5 35 57.55 37 57.6 27 57.65 25 57.7 28 57.75 30 57.8 30 57.85 27 57.9 29 57.95 35 58 30 58.05 25 58.1 24 58.15 35 58.2 22 58.25 27 58.3 37 58.35 31 58.4 29 58.45 21 58.5 29 58.55 26 58.6 30 58.65 30 58.7 23 58.75 30 58.8 26 58.85 32 58.9 17 58.95 28 59 24 59.05 14 59.1 21 59.15 27 59.2 21 59.25 20 59.3 34 59.35 29 59.4 25 59.45 26 59.5 37 59.55 46 59.6 56 59.65 41 59.7 39 59.75 38 59.8 34 59.85 33 59.9 31 59.95 28 60 40 60.05 28 60.1 33 60.15 27 60.2 33 60.25 34 60.3 23 60.35 27 60.4 24 60.45 25 60.5 23 60.55 29 60.6 30 60.65 23 60.7 19 60.75 22 60.8 24 60.85 25 60.9 20 60.95 21 61 21 61.05 27 61.1 28 61.15 32 61.2 19 61.25 28 61.3 19 61.35 24 61.4 24 61.45 21 61.5 14 61.55 37 61.6 27 61.65 20 61.7 28 61.75 21 61.8 20 61.85 36 61.9 21 61.95 23 62 23 62.05 28 62.1 30 62.15 25 62.2 17 62.25 27 62.3 24 62.35 18 62.4 20 62.45 30 62.5 27 62.55 28 62.6 37 62.65 28 62.7 23 62.75 24 62.8 26 62.85 27 62.9 19 62.95 35 63 31 63.05 28 63.1 27 63.15 18 63.2 24 63.25 24 63.3 26 63.35 30 63.4 33 63.45 34 63.5 30 63.55 31 63.6 32 63.65 38 63.7 39 63.75 35 63.8 31 63.85 36 63.9 27 63.95 33 64 22 64.05 35 64.1 25 64.15 26 64.2 29 64.25 26 64.3 24 64.35 24 64.4 22 64.45 31 64.5 20 64.55 21 64.6 28 64.65 20 64.7 26 64.75 25 64.8 29 64.85 32 64.9 31 64.95 25 65 32 65.05 26 65.1 37 65.15 22 65.2 26 65.25 28 65.3 23 65.35 39 65.4 24 65.45 26 65.5 22 65.55 15 65.6 28 65.65 32 65.7 30 65.75 24 65.8 19 65.85 33 65.9 39 65.95 25 66 31 66.05 22 66.1 25 66.15 24 66.2 28 66.25 32 66.3 28 66.35 29 66.4 34 66.45 27 66.5 27 66.55 27 66.6 27 66.65 21 66.7 27 66.75 26 66.8 25 66.85 26 66.9 28 66.95 29 67 31 67.05 23 67.1 24 67.15 27 67.2 24 67.25 31 67.3 26 67.35 18 67.4 35 67.45 26 67.5 29 67.55 30 67.6 41 67.65 26 67.7 41 67.75 25 67.8 28 67.85 26 67.9 26 67.95 29 68 27 68.05 25 68.1 26 68.15 25 68.2 22 68.25 28 68.3 20 68.35 35 68.4 26 68.45 19 68.5 22 68.55 21 68.6 20 68.65 30 68.7 25 68.75 20 68.8 27 68.85 26 68.9 30 68.95 20 69 18 69.05 28 69.1 16 69.15 24 69.2 16 69.25 18 69.3 34 69.35 27 69.4 21 69.45 32 69.5 25 69.55 14 69.6 20 69.65 28 69.7 19 69.75 19 69.8 30 69.85 33 69.9 29 69.95 30 70 24 70.05 18 70.1 21 70.15 26 70.2 24 70.25 31 70.3 20 70.35 21 70.4 19 70.45 17 70.5 16 70.55 23 70.6 17 70.65 24 70.7 14 70.75 22 70.8 33 70.85 30 70.9 26 70.95 25 71 17 71.05 24 71.1 21 71.15 20 71.2 25 71.25 27 71.3 20 71.35 20 71.4 18 71.45 21 71.5 23 71.55 24 71.6 27 71.65 24 71.7 25 71.75 21 71.8 18 71.85 28 71.9 23 71.95 15 72 18 72.05 28 72.1 16 72.15 30 72.2 25 72.25 29 72.3 24 72.35 21 72.4 20 72.45 16 72.5 27 72.55 25 72.6 31 72.65 28 72.7 15 72.75 34 72.8 24 72.85 15 72.9 19 72.95 22 73 22 73.05 27 73.1 33 73.15 19 73.2 26 73.25 25 73.3 18 73.35 25 73.4 21 73.45 19 73.5 28 73.55 22 73.6 29 73.65 28 73.7 22 73.75 25 73.8 27 73.85 22 73.9 25 73.95 19 74 26 74.05 27 74.1 22 74.15 18 74.2 25 74.25 17 74.3 22 74.35 20 74.4 27 74.45 28 74.5 24 74.55 19 74.6 25 74.65 21 74.7 18 74.75 19 74.8 26 74.85 25 74.9 17 74.95 20 75 26