Figure 5b Lambda = 1.5418 A 2theta Intensity 5 162 5.05 162 5.1 162 5.15 150 5.2 163 5.25 129 5.3 151 5.35 174 5.4 154 5.45 152 5.5 158 5.55 154 5.6 154 5.65 140 5.7 147 5.75 136 5.8 138 5.85 147 5.9 139 5.95 141 6 137 6.05 126 6.1 112 6.15 128 6.2 129 6.25 119 6.3 140 6.35 107 6.4 123 6.45 113 6.5 98 6.55 106 6.6 105 6.65 98 6.7 104 6.75 92 6.8 103 6.85 110 6.9 108 6.95 112 7 121 7.05 103 7.1 93 7.15 98 7.2 119 7.25 107 7.3 116 7.35 120 7.4 111 7.45 110 7.5 123 7.55 141 7.6 112 7.65 109 7.7 129 7.75 135 7.8 150 7.85 119 7.9 125 7.95 113 8 139 8.05 119 8.1 126 8.15 128 8.2 147 8.25 126 8.3 109 8.35 134 8.4 116 8.45 127 8.5 138 8.55 153 8.6 146 8.65 143 8.7 188 8.75 163 8.8 141 8.85 153 8.9 137 8.95 158 9 146 9.05 161 9.1 153 9.15 137 9.2 146 9.25 145 9.3 160 9.35 153 9.4 157 9.45 136 9.5 136 9.55 139 9.6 113 9.65 127 9.7 130 9.75 127 9.8 146 9.85 121 9.9 124 9.95 107 10 127 10.05 124 10.1 113 10.15 138 10.2 116 10.25 131 10.3 117 10.35 152 10.4 110 10.45 129 10.5 124 10.55 137 10.6 125 10.65 116 10.7 116 10.75 107 10.8 121 10.85 111 10.9 115 10.95 136 11 150 11.05 141 11.1 155 11.15 142 11.2 138 11.25 178 11.3 155 11.35 162 11.4 159 11.45 156 11.5 155 11.55 139 11.6 161 11.65 164 11.7 186 11.75 188 11.8 153 11.85 186 11.9 171 11.95 170 12 137 12.05 156 12.1 153 12.15 160 12.2 171 12.25 160 12.3 185 12.35 192 12.4 177 12.45 152 12.5 168 12.55 154 12.6 153 12.65 158 12.7 133 12.75 148 12.8 149 12.85 140 12.9 152 12.95 147 13 148 13.05 136 13.1 136 13.15 124 13.2 147 13.25 122 13.3 129 13.35 123 13.4 127 13.45 112 13.5 128 13.55 112 13.6 127 13.65 129 13.7 115 13.75 126 13.8 126 13.85 117 13.9 135 13.95 121 14 123 14.05 130 14.1 129 14.15 114 14.2 124 14.25 119 14.3 141 14.35 120 14.4 120 14.45 114 14.5 121 14.55 101 14.6 121 14.65 136 14.7 151 14.75 133 14.8 132 14.85 144 14.9 147 14.95 142 15 166 15.05 148 15.1 172 15.15 162 15.2 151 15.25 168 15.3 153 15.35 140 15.4 184 15.45 180 15.5 175 15.55 132 15.6 134 15.65 147 15.7 145 15.75 161 15.8 149 15.85 134 15.9 152 15.95 133 16 146 16.05 134 16.1 116 16.15 131 16.2 121 16.25 122 16.3 132 16.35 123 16.4 129 16.45 127 16.5 119 16.55 125 16.6 119 16.65 123 16.7 138 16.75 115 16.8 116 16.85 108 16.9 98 16.95 128 17 124 17.05 105 17.1 93 17.15 101 17.2 99 17.25 97 17.3 115 17.35 94 17.4 117 17.45 77 17.5 106 17.55 92 17.6 97 17.65 91 17.7 95 17.75 73 17.8 91 17.85 103 17.9 88 17.95 96 18 91 18.05 98 18.1 92 18.15 94 18.2 79 18.25 121 18.3 108 18.35 111 18.4 97 18.45 100 18.5 111 18.55 100 18.6 120 18.65 89 18.7 101 18.75 96 18.8 99 18.85 88 18.9 107 18.95 92 19 89 19.05 125 19.1 96 19.15 113 19.2 96 19.25 118 19.3 118 19.35 96 19.4 127 19.45 127 19.5 118 19.55 129 19.6 109 19.65 119 19.7 139 19.75 117 19.8 116 19.85 106 19.9 111 19.95 98 20 98 20.05 93 20.1 93 20.15 95 20.2 104 20.25 100 20.3 87 20.35 103 20.4 94 20.45 73 20.5 90 20.55 91 20.6 91 20.65 101 20.7 104 20.75 108 20.8 92 20.85 71 20.9 73 20.95 82 21 88 21.05 92 21.1 75 21.15 80 21.2 94 21.25 62 21.3 66 21.35 78 21.4 58 21.45 72 21.5 74 21.55 82 21.6 74 21.65 68 21.7 80 21.75 72 21.8 73 21.85 84 21.9 75 21.95 80 22 66 22.05 81 22.1 83 22.15 57 22.2 59 22.25 76 22.3 79 22.35 62 22.4 77 22.45 84 22.5 80 22.55 81 22.6 76 22.65 61 22.7 87 22.75 67 22.8 78 22.85 76 22.9 75 22.95 87 23 91 23.05 87 23.1 91 23.15 72 23.2 81 23.25 85 23.3 77 23.35 92 23.4 92 23.45 100 23.5 90 23.55 98 23.6 94 23.65 103 23.7 122 23.75 108 23.8 90 23.85 107 23.9 116 23.95 114 24 103 24.05 130 24.1 113 24.15 134 24.2 106 24.25 98 24.3 110 24.35 98 24.4 78 24.45 100 24.5 83 24.55 76 24.6 82 24.65 77 24.7 89 24.75 78 24.8 76 24.85 81 24.9 72 24.95 82 25 79 25.05 88 25.1 76 25.15 89 25.2 82 25.25 82 25.3 73 25.35 86 25.4 67 25.45 79 25.5 80 25.55 70 25.6 91 25.65 89 25.7 87 25.75 79 25.8 89 25.85 85 25.9 92 25.95 88 26 90 26.05 118 26.1 94 26.15 127 26.2 140 26.25 119 26.3 133 26.35 105 26.4 132 26.45 128 26.5 147 26.55 143 26.6 143 26.65 145 26.7 138 26.75 121 26.8 155 26.85 133 26.9 136 26.95 144 27 111 27.05 131 27.1 146 27.15 97 27.2 106 27.25 96 27.3 96 27.35 103 27.4 86 27.45 87 27.5 103 27.55 87 27.6 91 27.65 86 27.7 74 27.75 85 27.8 78 27.85 84 27.9 86 27.95 66 28 84 28.05 74 28.1 77 28.15 89 28.2 92 28.25 83 28.3 89 28.35 81 28.4 98 28.45 108 28.5 101 28.55 97 28.6 100 28.65 105 28.7 77 28.75 88 28.8 100 28.85 91 28.9 95 28.95 90 29 75 29.05 73 29.1 79 29.15 73 29.2 71 29.25 71 29.3 91 29.35 76 29.4 77 29.45 76 29.5 80 29.55 94 29.6 90 29.65 87 29.7 71 29.75 76 29.8 79 29.85 94 29.9 104 29.95 118 30 144 30.05 162 30.1 227 30.15 327 30.2 434 30.25 518 30.3 467 30.35 410 30.4 290 30.45 256 30.5 207 30.55 165 30.6 149 30.65 111 30.7 122 30.75 112 30.8 89 30.85 90 30.9 77 30.95 77 31 68 31.05 79 31.1 91 31.15 62 31.2 71 31.25 78 31.3 72 31.35 80 31.4 71 31.45 91 31.5 76 31.55 78 31.6 80 31.65 77 31.7 65 31.75 80 31.8 70 31.85 89 31.9 88 31.95 76 32 76 32.05 81 32.1 69 32.15 84 32.2 82 32.25 71 32.3 68 32.35 78 32.4 82 32.45 93 32.5 71 32.55 71 32.6 73 32.65 73 32.7 84 32.75 68 32.8 66 32.85 77 32.9 88 32.95 67 33 58 33.05 77 33.1 88 33.15 84 33.2 65 33.25 80 33.3 80 33.35 74 33.4 74 33.45 78 33.5 78 33.55 89 33.6 70 33.65 72 33.7 80 33.75 58 33.8 62 33.85 63 33.9 68 33.95 63 34 70 34.05 71 34.1 71 34.15 67 34.2 83 34.25 78 34.3 52 34.35 62 34.4 54 34.45 60 34.5 67 34.55 56 34.6 63 34.65 68 34.7 48 34.75 55 34.8 55 34.85 47 34.9 62 34.95 47 35 60 35.05 46 35.1 52 35.15 43 35.2 42 35.25 46 35.3 61 35.35 50 35.4 42 35.45 54 35.5 46 35.55 53 35.6 45 35.65 41 35.7 37 35.75 44 35.8 43 35.85 43 35.9 40 35.95 41 36 46 36.05 38 36.1 55 36.15 39 36.2 50 36.25 46 36.3 58 36.35 45 36.4 37 36.45 46 36.5 44 36.55 53 36.6 40 36.65 49 36.7 55 36.75 47 36.8 48 36.85 34 36.9 45 36.95 45 37 52 37.05 66 37.1 53 37.15 51 37.2 61 37.25 79 37.3 76 37.35 109 37.4 87 37.45 76 37.5 78 37.55 53 37.6 45 37.65 46 37.7 51 37.75 39 37.8 41 37.85 44 37.9 37 37.95 36 38 40 38.05 44 38.1 31 38.15 41 38.2 38 38.25 46 38.3 37 38.35 28 38.4 43 38.45 42 38.5 44 38.55 34 38.6 44 38.65 56 38.7 37 38.75 37 38.8 34 38.85 33 38.9 48 38.95 43 39 37 39.05 50 39.1 44 39.15 58 39.2 47 39.25 48 39.3 46 39.35 40 39.4 37 39.45 49 39.5 42 39.55 51 39.6 58 39.65 44 39.7 49 39.75 46 39.8 57 39.85 37 39.9 53 39.95 53 40 51 40.05 45 40.1 44 40.15 69 40.2 56 40.25 50 40.3 46 40.35 55 40.4 46 40.45 57 40.5 43 40.55 42 40.6 49 40.65 50 40.7 36 40.75 44 40.8 65 40.85 55 40.9 41 40.95 52 41 43 41.05 61 41.1 38 41.15 33 41.2 42 41.25 42 41.3 56 41.35 43 41.4 39 41.45 31 41.5 45 41.55 42 41.6 41 41.65 35 41.7 43 41.75 44 41.8 41 41.85 40 41.9 37 41.95 33 42 40 42.05 50 42.1 54 42.15 41 42.2 55 42.25 45 42.3 38 42.35 42 42.4 50 42.45 47 42.5 38 42.55 41 42.6 46 42.65 51 42.7 32 42.75 38 42.8 38 42.85 32 42.9 33 42.95 50 43 28 43.05 54 43.1 47 43.15 34 43.2 40 43.25 45 43.3 46 43.35 41 43.4 34 43.45 36 43.5 44 43.55 33 43.6 44 43.65 34 43.7 44 43.75 32 43.8 45 43.85 47 43.9 43 43.95 41 44 40 44.05 46 44.1 42 44.15 44 44.2 39 44.25 39 44.3 34 44.35 37 44.4 37 44.45 31 44.5 36 44.55 50 44.6 28 44.65 43 44.7 48 44.75 29 44.8 41 44.85 42 44.9 26 44.95 40 45 34 45.05 44 45.1 45 45.15 40 45.2 35 45.25 36 45.3 29 45.35 30 45.4 31 45.45 21 45.5 33 45.55 34 45.6 30 45.65 43 45.7 27 45.75 30 45.8 36 45.85 40 45.9 44 45.95 39 46 31 46.05 39 46.1 46 46.15 44 46.2 47 46.25 49 46.3 49 46.35 46 46.4 47 46.45 39 46.5 48 46.55 47 46.6 42 46.65 36 46.7 36 46.75 47 46.8 35 46.85 47 46.9 36 46.95 40 47 46 47.05 32 47.1 45 47.15 47 47.2 42 47.25 62 47.3 49 47.35 47 47.4 48 47.45 58 47.5 54 47.55 65 47.6 55 47.65 55 47.7 63 47.75 63 47.8 73 47.85 52 47.9 63 47.95 64 48 63 48.05 60 48.1 63 48.15 58 48.2 62 48.25 59 48.3 54 48.35 67 48.4 71 48.45 73 48.5 76 48.55 57 48.6 84 48.65 72 48.7 88 48.75 82 48.8 96 48.85 88 48.9 99 48.95 89 49 98 49.05 82 49.1 93 49.15 65 49.2 86 49.25 70 49.3 62 49.35 71 49.4 63 49.45 65 49.5 67 49.55 58 49.6 52 49.65 54 49.7 50 49.75 53 49.8 46 49.85 55 49.9 53 49.95 54 50 43 50.05 48 50.1 49 50.15 37 50.2 39 50.25 56 50.3 46 50.35 63 50.4 52 50.45 52 50.5 56 50.55 34 50.6 42 50.65 36 50.7 40 50.75 32 50.8 43 50.85 33 50.9 44 50.95 49 51 39 51.05 41 51.1 36 51.15 56 51.2 42 51.25 53 51.3 46 51.35 38 51.4 41 51.45 40 51.5 53 51.55 40 51.6 36 51.65 57 51.7 49 51.75 45 51.8 46 51.85 38 51.9 48 51.95 52 52 35 52.05 46 52.1 32 52.15 39 52.2 39 52.25 38 52.3 39 52.35 49 52.4 35 52.45 41 52.5 48 52.55 37 52.6 38 52.65 41 52.7 37 52.75 41 52.8 38 52.85 35 52.9 45 52.95 38 53 33 53.05 37 53.1 41 53.15 31 53.2 41 53.25 45 53.3 39 53.35 29 53.4 42 53.45 39 53.5 34 53.55 41 53.6 38 53.65 30 53.7 44 53.75 37 53.8 39 53.85 33 53.9 52 53.95 45 54 44 54.05 50 54.1 38 54.15 51 54.2 30 54.25 41 54.3 40 54.35 37 54.4 43 54.45 40 54.5 36 54.55 29 54.6 36 54.65 35 54.7 33 54.75 47 54.8 42 54.85 38 54.9 43 54.95 41 55 52 55.05 38 55.1 44 55.15 47 55.2 50 55.25 44 55.3 37 55.35 62 55.4 53 55.45 47 55.5 47 55.55 56 55.6 41 55.65 48 55.7 49 55.75 47 55.8 38 55.85 51 55.9 32 55.95 51 56 55 56.05 40 56.1 67 56.15 53 56.2 40 56.25 48 56.3 54 56.35 46 56.4 48 56.45 47 56.5 35 56.55 38 56.6 36 56.65 38 56.7 50 56.75 34 56.8 35 56.85 40 56.9 45 56.95 40 57 33 57.05 39 57.1 25 57.15 32 57.2 30 57.25 39 57.3 38 57.35 34 57.4 53 57.45 41 57.5 31 57.55 44 57.6 31 57.65 36 57.7 39 57.75 25 57.8 39 57.85 37 57.9 31 57.95 20 58 29 58.05 24 58.1 42 58.15 35 58.2 32 58.25 26 58.3 27 58.35 24 58.4 37 58.45 35 58.5 35 58.55 34 58.6 24 58.65 20 58.7 22 58.75 34 58.8 24 58.85 24 58.9 27 58.95 29 59 35 59.05 31 59.1 35 59.15 40 59.2 27 59.25 37 59.3 30 59.35 26 59.4 27 59.45 33 59.5 31 59.55 46 59.6 30 59.65 35 59.7 42 59.75 40 59.8 42 59.85 41 59.9 38 59.95 31 60 30 60.05 24 60.1 47 60.15 36 60.2 40 60.25 29 60.3 28 60.35 29 60.4 29 60.45 34 60.5 32 60.55 36 60.6 30 60.65 27 60.7 29 60.75 40 60.8 45 60.85 40 60.9 37 60.95 44 61 43 61.05 46 61.1 35 61.15 30 61.2 28 61.25 33 61.3 33 61.35 28 61.4 35 61.45 30 61.5 31 61.55 25 61.6 25 61.65 28 61.7 31 61.75 33 61.8 37 61.85 30 61.9 22 61.95 36 62 28 62.05 32 62.1 26 62.15 37 62.2 34 62.25 31 62.3 45 62.35 37 62.4 26 62.45 35 62.5 31 62.55 30 62.6 35 62.65 30 62.7 31 62.75 49 62.8 37 62.85 37 62.9 47 62.95 58 63 62 63.05 66 63.1 67 63.15 66 63.2 67 63.25 60 63.3 43 63.35 48 63.4 42 63.45 48 63.5 48 63.55 43 63.6 38 63.65 36 63.7 42 63.75 36 63.8 36 63.85 30 63.9 39 63.95 22 64 37 64.05 32 64.1 23 64.15 22 64.2 21 64.25 23 64.3 36 64.35 9 64.4 26 64.45 32 64.5 33 64.55 27 64.6 26 64.65 35 64.7 41 64.75 40 64.8 17 64.85 33 64.9 36 64.95 28 65 23 65.05 41 65.1 34 65.15 34 65.2 20 65.25 19 65.3 26 65.35 37 65.4 31 65.45 24 65.5 37 65.55 34 65.6 27 65.65 36 65.7 39 65.75 29 65.8 38 65.85 34 65.9 32 65.95 34 66 32 66.05 37 66.1 35 66.15 31 66.2 30 66.25 40 66.3 25 66.35 31 66.4 30 66.45 28 66.5 32 66.55 38 66.6 31 66.65 32 66.7 23 66.75 41 66.8 24 66.85 29 66.9 41 66.95 27 67 20 67.05 25 67.1 41 67.15 33 67.2 15 67.25 43 67.3 34 67.35 31 67.4 43 67.45 30 67.5 27 67.55 35 67.6 37 67.65 23 67.7 36 67.75 33 67.8 26 67.85 35 67.9 35 67.95 41 68 25 68.05 35 68.1 31 68.15 24 68.2 20 68.25 20 68.3 33 68.35 22 68.4 30 68.45 29 68.5 33 68.55 28 68.6 24 68.65 26 68.7 27 68.75 28 68.8 26 68.85 28 68.9 35 68.95 33 69 23 69.05 23 69.1 26 69.15 28 69.2 33 69.25 33 69.3 47 69.35 26 69.4 28 69.45 32 69.5 39 69.55 31 69.6 32 69.65 39 69.7 32 69.75 50 69.8 34 69.85 29 69.9 30 69.95 40 70 22 70.05 37 70.1 31 70.15 32 70.2 26 70.25 33 70.3 27 70.35 26 70.4 33 70.45 37 70.5 37 70.55 24 70.6 24 70.65 25 70.7 25 70.75 37 70.8 29 70.85 27 70.9 29 70.95 28 71 28 71.05 28 71.1 26 71.15 30 71.2 33 71.25 34 71.3 41 71.35 34 71.4 46 71.45 29 71.5 29 71.55 32 71.6 34 71.65 35 71.7 44 71.75 41 71.8 32 71.85 33 71.9 39 71.95 36 72 35 72.05 24 72.1 38 72.15 43 72.2 40 72.25 40 72.3 36 72.35 30 72.4 45 72.45 37 72.5 26 72.55 38 72.6 22 72.65 23 72.7 30 72.75 39 72.8 38 72.85 21 72.9 37 72.95 34 73 33 73.05 28 73.1 18 73.15 24 73.2 26 73.25 26 73.3 38 73.35 35 73.4 27 73.45 31 73.5 29 73.55 35 73.6 31 73.65 31 73.7 22 73.75 23 73.8 23 73.85 31 73.9 27 73.95 32 74 32 74.05 26 74.1 23 74.15 31 74.2 23 74.25 36 74.3 27 74.35 31 74.4 22 74.45 32 74.5 23 74.55 32 74.6 32 74.65 30 74.7 29 74.75 15 74.8 33 74.85 17 74.9 24 74.95 26 75 0