Figure 5d Lambda = 1.5418 A 2theta Intensity 5 97 5.05 94 5.1 97 5.15 113 5.2 93 5.25 101 5.3 132 5.35 101 5.4 105 5.45 102 5.5 79 5.55 106 5.6 118 5.65 106 5.7 105 5.75 123 5.8 133 5.85 116 5.9 108 5.95 112 6 104 6.05 79 6.1 108 6.15 116 6.2 101 6.25 124 6.3 90 6.35 122 6.4 117 6.45 113 6.5 101 6.55 98 6.6 128 6.65 88 6.7 125 6.75 129 6.8 111 6.85 108 6.9 97 6.95 102 7 95 7.05 113 7.1 113 7.15 107 7.2 110 7.25 109 7.3 108 7.35 116 7.4 124 7.45 94 7.5 107 7.55 111 7.6 112 7.65 112 7.7 100 7.75 121 7.8 123 7.85 118 7.9 107 7.95 102 8 112 8.05 108 8.1 85 8.15 127 8.2 116 8.25 123 8.3 101 8.35 110 8.4 110 8.45 115 8.5 106 8.55 117 8.6 130 8.65 115 8.7 123 8.75 113 8.8 114 8.85 118 8.9 123 8.95 116 9 123 9.05 112 9.1 118 9.15 122 9.2 126 9.25 117 9.3 152 9.35 146 9.4 106 9.45 103 9.5 112 9.55 114 9.6 118 9.65 116 9.7 127 9.75 116 9.8 103 9.85 107 9.9 114 9.95 88 10 138 10.05 111 10.1 95 10.15 127 10.2 106 10.25 103 10.3 116 10.35 106 10.4 122 10.45 92 10.5 105 10.55 100 10.6 106 10.65 115 10.7 115 10.75 107 10.8 112 10.85 103 10.9 96 10.95 113 11 97 11.05 105 11.1 92 11.15 108 11.2 104 11.25 112 11.3 111 11.35 95 11.4 122 11.45 120 11.5 99 11.55 120 11.6 112 11.65 127 11.7 136 11.75 184 11.8 206 11.85 245 11.9 156 11.95 139 12 131 12.05 121 12.1 160 12.15 129 12.2 138 12.25 161 12.3 204 12.35 213 12.4 219 12.45 207 12.5 191 12.55 185 12.6 215 12.65 209 12.7 176 12.75 144 12.8 162 12.85 147 12.9 170 12.95 180 13 173 13.05 200 13.1 225 13.15 205 13.2 173 13.25 154 13.3 186 13.35 185 13.4 199 13.45 237 13.5 263 13.55 203 13.6 158 13.65 148 13.7 127 13.75 146 13.8 158 13.85 205 13.9 176 13.95 182 14 135 14.05 122 14.1 137 14.15 130 14.2 163 14.25 172 14.3 163 14.35 137 14.4 139 14.45 117 14.5 164 14.55 156 14.6 158 14.65 136 14.7 170 14.75 161 14.8 180 14.85 167 14.9 177 14.95 191 15 206 15.05 156 15.1 174 15.15 186 15.2 184 15.25 158 15.3 180 15.35 166 15.4 144 15.45 174 15.5 164 15.55 150 15.6 165 15.65 168 15.7 182 15.75 158 15.8 183 15.85 156 15.9 142 15.95 134 16 161 16.05 140 16.1 126 16.15 130 16.2 151 16.25 146 16.3 135 16.35 108 16.4 100 16.45 85 16.5 85 16.55 80 16.6 107 16.65 90 16.7 89 16.75 97 16.8 97 16.85 73 16.9 109 16.95 99 17 88 17.05 91 17.1 85 17.15 82 17.2 77 17.25 85 17.3 84 17.35 80 17.4 85 17.45 68 17.5 88 17.55 93 17.6 95 17.65 81 17.7 89 17.75 81 17.8 75 17.85 97 17.9 85 17.95 106 18 76 18.05 104 18.1 83 18.15 76 18.2 78 18.25 100 18.3 107 18.35 130 18.4 140 18.45 112 18.5 102 18.55 80 18.6 95 18.65 96 18.7 104 18.75 98 18.8 99 18.85 104 18.9 102 18.95 104 19 120 19.05 101 19.1 125 19.15 116 19.2 104 19.25 119 19.3 117 19.35 120 19.4 110 19.45 133 19.5 130 19.55 137 19.6 137 19.65 134 19.7 135 19.75 135 19.8 103 19.85 117 19.9 120 19.95 134 20 96 20.05 98 20.1 83 20.15 104 20.2 88 20.25 97 20.3 86 20.35 93 20.4 99 20.45 98 20.5 85 20.55 96 20.6 93 20.65 84 20.7 88 20.75 82 20.8 84 20.85 91 20.9 87 20.95 81 21 122 21.05 112 21.1 110 21.15 75 21.2 83 21.25 90 21.3 89 21.35 94 21.4 80 21.45 72 21.5 81 21.55 85 21.6 88 21.65 79 21.7 77 21.75 86 21.8 89 21.85 100 21.9 140 21.95 113 22 121 22.05 127 22.1 144 22.15 155 22.2 185 22.25 157 22.3 93 22.35 87 22.4 72 22.45 78 22.5 80 22.55 69 22.6 60 22.65 75 22.7 79 22.75 66 22.8 88 22.85 82 22.9 85 22.95 65 23 76 23.05 99 23.1 57 23.15 59 23.2 79 23.25 86 23.3 96 23.35 83 23.4 79 23.45 87 23.5 88 23.55 93 23.6 92 23.65 108 23.7 97 23.75 88 23.8 106 23.85 135 23.9 125 23.95 110 24 112 24.05 131 24.1 112 24.15 114 24.2 120 24.25 148 24.3 140 24.35 113 24.4 119 24.45 121 24.5 97 24.55 110 24.6 110 24.65 111 24.7 146 24.75 154 24.8 137 24.85 85 24.9 73 24.95 72 25 81 25.05 66 25.1 64 25.15 63 25.2 76 25.25 79 25.3 81 25.35 72 25.4 76 25.45 69 25.5 67 25.55 64 25.6 70 25.65 66 25.7 73 25.75 62 25.8 79 25.85 78 25.9 63 25.95 73 26 65 26.05 71 26.1 63 26.15 79 26.2 99 26.25 120 26.3 148 26.35 131 26.4 131 26.45 119 26.5 113 26.55 121 26.6 104 26.65 130 26.7 114 26.75 119 26.8 151 26.85 147 26.9 128 26.95 166 27 153 27.05 121 27.1 119 27.15 123 27.2 134 27.25 151 27.3 125 27.35 105 27.4 104 27.45 86 27.5 97 27.55 85 27.6 88 27.65 87 27.7 102 27.75 101 27.8 118 27.85 107 27.9 121 27.95 111 28 140 28.05 170 28.1 135 28.15 113 28.2 88 28.25 83 28.3 89 28.35 98 28.4 100 28.45 101 28.5 106 28.55 104 28.6 101 28.65 99 28.7 83 28.75 87 28.8 119 28.85 76 28.9 84 28.95 77 29 85 29.05 82 29.1 48 29.15 70 29.2 63 29.25 72 29.3 57 29.35 76 29.4 69 29.45 79 29.5 71 29.55 59 29.6 51 29.65 73 29.7 63 29.75 75 29.8 77 29.85 87 29.9 93 29.95 92 30 107 30.05 132 30.1 163 30.15 218 30.2 294 30.25 525 30.3 578 30.35 555 30.4 405 30.45 259 30.5 174 30.55 136 30.6 121 30.65 102 30.7 87 30.75 69 30.8 76 30.85 75 30.9 87 30.95 88 31 90 31.05 97 31.1 111 31.15 98 31.2 100 31.25 86 31.3 83 31.35 101 31.4 110 31.45 115 31.5 121 31.55 104 31.6 85 31.65 85 31.7 78 31.75 92 31.8 117 31.85 117 31.9 106 31.95 102 32 95 32.05 84 32.1 84 32.15 65 32.2 70 32.25 82 32.3 73 32.35 80 32.4 64 32.45 56 32.5 60 32.55 58 32.6 38 32.65 67 32.7 59 32.75 68 32.8 56 32.85 76 32.9 73 32.95 54 33 71 33.05 74 33.1 70 33.15 47 33.2 73 33.25 59 33.3 61 33.35 72 33.4 58 33.45 72 33.5 82 33.55 80 33.6 73 33.65 82 33.7 69 33.75 69 33.8 77 33.85 73 33.9 83 33.95 86 34 60 34.05 88 34.1 73 34.15 72 34.2 91 34.25 60 34.3 68 34.35 82 34.4 77 34.45 57 34.5 85 34.55 69 34.6 59 34.65 60 34.7 58 34.75 48 34.8 65 34.85 60 34.9 49 34.95 59 35 48 35.05 54 35.1 36 35.15 45 35.2 42 35.25 37 35.3 54 35.35 56 35.4 50 35.45 55 35.5 49 35.55 44 35.6 46 35.65 38 35.7 49 35.75 60 35.8 49 35.85 47 35.9 46 35.95 32 36 58 36.05 68 36.1 63 36.15 50 36.2 57 36.25 62 36.3 42 36.35 29 36.4 61 36.45 44 36.5 49 36.55 49 36.6 37 36.65 48 36.7 44 36.75 56 36.8 59 36.85 48 36.9 44 36.95 49 37 54 37.05 50 37.1 58 37.15 63 37.2 72 37.25 88 37.3 99 37.35 98 37.4 86 37.45 79 37.5 73 37.55 55 37.6 42 37.65 43 37.7 48 37.75 48 37.8 43 37.85 44 37.9 33 37.95 42 38 36 38.05 35 38.1 61 38.15 57 38.2 72 38.25 81 38.3 66 38.35 65 38.4 44 38.45 34 38.5 44 38.55 41 38.6 52 38.65 50 38.7 39 38.75 33 38.8 37 38.85 28 38.9 37 38.95 47 39 36 39.05 47 39.1 35 39.15 39 39.2 41 39.25 33 39.3 50 39.35 57 39.4 45 39.45 41 39.5 44 39.55 39 39.6 32 39.65 44 39.7 54 39.75 35 39.8 38 39.85 49 39.9 49 39.95 59 40 47 40.05 53 40.1 58 40.15 57 40.2 64 40.25 53 40.3 47 40.35 49 40.4 64 40.45 61 40.5 56 40.55 69 40.6 73 40.65 64 40.7 40 40.75 42 40.8 40 40.85 51 40.9 44 40.95 51 41 43 41.05 45 41.1 48 41.15 40 41.2 50 41.25 31 41.3 52 41.35 31 41.4 43 41.45 60 41.5 59 41.55 56 41.6 55 41.65 41 41.7 40 41.75 33 41.8 28 41.85 40 41.9 39 41.95 36 42 36 42.05 36 42.1 41 42.15 44 42.2 38 42.25 50 42.3 26 42.35 46 42.4 43 42.45 53 42.5 44 42.55 45 42.6 52 42.65 49 42.7 37 42.75 27 42.8 43 42.85 43 42.9 50 42.95 66 43 75 43.05 61 43.1 74 43.15 58 43.2 48 43.25 45 43.3 37 43.35 44 43.4 43 43.45 33 43.5 37 43.55 33 43.6 47 43.65 39 43.7 42 43.75 44 43.8 42 43.85 37 43.9 40 43.95 51 44 57 44.05 35 44.1 55 44.15 43 44.2 56 44.25 51 44.3 49 44.35 68 44.4 76 44.45 101 44.5 80 44.55 76 44.6 78 44.65 58 44.7 52 44.75 46 44.8 58 44.85 39 44.9 46 44.95 48 45 38 45.05 41 45.1 52 45.15 38 45.2 54 45.25 39 45.3 35 45.35 43 45.4 27 45.45 44 45.5 46 45.55 39 45.6 44 45.65 38 45.7 41 45.75 39 45.8 43 45.85 33 45.9 34 45.95 48 46 26 46.05 31 46.1 42 46.15 37 46.2 55 46.25 46 46.3 62 46.35 40 46.4 41 46.45 43 46.5 37 46.55 33 46.6 38 46.65 51 46.7 35 46.75 36 46.8 26 46.85 39 46.9 47 46.95 37 47 26 47.05 39 47.1 43 47.15 49 47.2 64 47.25 50 47.3 56 47.35 46 47.4 56 47.45 63 47.5 52 47.55 63 47.6 67 47.65 67 47.7 72 47.75 70 47.8 61 47.85 64 47.9 47 47.95 58 48 62 48.05 47 48.1 45 48.15 47 48.2 38 48.25 47 48.3 47 48.35 41 48.4 42 48.45 53 48.5 45 48.55 51 48.6 48 48.65 68 48.7 72 48.75 80 48.8 80 48.85 93 48.9 104 48.95 113 49 102 49.05 97 49.1 87 49.15 70 49.2 77 49.25 84 49.3 86 49.35 63 49.4 73 49.45 65 49.5 63 49.55 63 49.6 49 49.65 51 49.7 57 49.75 56 49.8 57 49.85 52 49.9 48 49.95 51 50 61 50.05 50 50.1 51 50.15 40 50.2 42 50.25 44 50.3 38 50.35 38 50.4 32 50.45 51 50.5 42 50.55 41 50.6 50 50.65 39 50.7 33 50.75 51 50.8 48 50.85 35 50.9 33 50.95 46 51 31 51.05 40 51.1 45 51.15 49 51.2 47 51.25 44 51.3 46 51.35 46 51.4 35 51.45 46 51.5 43 51.55 39 51.6 42 51.65 40 51.7 46 51.75 45 51.8 49 51.85 52 51.9 44 51.95 38 52 49 52.05 25 52.1 41 52.15 30 52.2 39 52.25 39 52.3 39 52.35 40 52.4 32 52.45 38 52.5 41 52.55 28 52.6 35 52.65 31 52.7 35 52.75 36 52.8 25 52.85 35 52.9 37 52.95 44 53 45 53.05 50 53.1 36 53.15 32 53.2 38 53.25 35 53.3 40 53.35 32 53.4 38 53.45 37 53.5 56 53.55 32 53.6 29 53.65 39 53.7 34 53.75 28 53.8 38 53.85 29 53.9 40 53.95 33 54 34 54.05 37 54.1 40 54.15 40 54.2 53 54.25 55 54.3 34 54.35 40 54.4 42 54.45 44 54.5 36 54.55 32 54.6 36 54.65 47 54.7 34 54.75 27 54.8 43 54.85 26 54.9 34 54.95 32 55 39 55.05 40 55.1 44 55.15 45 55.2 43 55.25 38 55.3 46 55.35 47 55.4 57 55.45 59 55.5 47 55.55 40 55.6 61 55.65 48 55.7 62 55.75 53 55.8 47 55.85 65 55.9 47 55.95 57 56 48 56.05 57 56.1 51 56.15 58 56.2 61 56.25 51 56.3 47 56.35 45 56.4 57 56.45 40 56.5 35 56.55 45 56.6 37 56.65 37 56.7 33 56.75 50 56.8 35 56.85 34 56.9 36 56.95 37 57 46 57.05 35 57.1 37 57.15 33 57.2 45 57.25 28 57.3 44 57.35 49 57.4 44 57.45 46 57.5 43 57.55 56 57.6 49 57.65 51 57.7 45 57.75 31 57.8 32 57.85 34 57.9 36 57.95 37 58 50 58.05 36 58.1 30 58.15 39 58.2 33 58.25 37 58.3 43 58.35 32 58.4 23 58.45 22 58.5 24 58.55 25 58.6 27 58.65 34 58.7 25 58.75 33 58.8 35 58.85 30 58.9 25 58.95 34 59 32 59.05 32 59.1 31 59.15 33 59.2 33 59.25 44 59.3 32 59.35 33 59.4 34 59.45 37 59.5 39 59.55 35 59.6 28 59.65 38 59.7 32 59.75 44 59.8 42 59.85 38 59.9 38 59.95 33 60 48 60.05 44 60.1 36 60.15 35 60.2 38 60.25 42 60.3 33 60.35 34 60.4 36 60.45 30 60.5 34 60.55 25 60.6 23 60.65 33 60.7 30 60.75 33 60.8 37 60.85 50 60.9 49 60.95 48 61 32 61.05 39 61.1 32 61.15 38 61.2 32 61.25 32 61.3 36 61.35 35 61.4 29 61.45 27 61.5 34 61.55 32 61.6 25 61.65 40 61.7 29 61.75 21 61.8 33 61.85 32 61.9 30 61.95 37 62 29 62.05 36 62.1 34 62.15 45 62.2 34 62.25 38 62.3 39 62.35 25 62.4 33 62.45 44 62.5 44 62.55 28 62.6 34 62.65 33 62.7 28 62.75 31 62.8 45 62.85 57 62.9 46 62.95 52 63 48 63.05 58 63.1 74 63.15 75 63.2 50 63.25 67 63.3 63 63.35 58 63.4 54 63.45 55 63.5 47 63.55 43 63.6 51 63.65 32 63.7 32 63.75 39 63.8 26 63.85 25 63.9 29 63.95 32 64 21 64.05 34 64.1 28 64.15 38 64.2 25 64.25 41 64.3 35 64.35 32 64.4 36 64.45 39 64.5 27 64.55 46 64.6 48 64.65 58 64.7 92 64.75 109 64.8 91 64.85 88 64.9 86 64.95 78 65 55 65.05 44 65.1 51 65.15 45 65.2 48 65.25 49 65.3 38 65.35 42 65.4 38 65.45 30 65.5 34 65.55 43 65.6 23 65.65 35 65.7 30 65.75 37 65.8 32 65.85 24 65.9 36 65.95 35 66 22 66.05 29 66.1 22 66.15 34 66.2 25 66.25 26 66.3 29 66.35 35 66.4 32 66.45 35 66.5 36 66.55 25 66.6 21 66.65 23 66.7 31 66.75 31 66.8 39 66.85 29 66.9 28 66.95 29 67 36 67.05 21 67.1 23 67.15 38 67.2 23 67.25 42 67.3 34 67.35 26 67.4 29 67.45 30 67.5 28 67.55 40 67.6 43 67.65 29 67.7 29 67.75 31 67.8 29 67.85 40 67.9 36 67.95 34 68 31 68.05 44 68.1 40 68.15 38 68.2 40 68.25 33 68.3 36 68.35 22 68.4 41 68.45 29 68.5 33 68.55 27 68.6 16 68.65 29 68.7 24 68.75 23 68.8 32 68.85 21 68.9 19 68.95 26 69 14 69.05 20 69.1 24 69.15 31 69.2 23 69.25 27 69.3 25 69.35 25 69.4 41 69.45 33 69.5 35 69.55 33 69.6 43 69.65 42 69.7 37 69.75 40 69.8 36 69.85 28 69.9 30 69.95 36 70 32 70.05 33 70.1 35 70.15 33 70.2 34 70.25 25 70.3 24 70.35 31 70.4 20 70.45 35 70.5 25 70.55 22 70.6 38 70.65 33 70.7 27 70.75 40 70.8 27 70.85 39 70.9 29 70.95 35 71 36 71.05 24 71.1 25 71.15 33 71.2 32 71.25 31 71.3 29 71.35 45 71.4 37 71.45 31 71.5 29 71.55 51 71.6 35 71.65 36 71.7 37 71.75 38 71.8 45 71.85 36 71.9 40 71.95 26 72 33 72.05 32 72.1 25 72.15 44 72.2 44 72.25 48 72.3 32 72.35 26 72.4 27 72.45 39 72.5 39 72.55 39 72.6 36 72.65 31 72.7 40 72.75 36 72.8 39 72.85 34 72.9 32 72.95 23 73 34 73.05 25 73.1 30 73.15 27 73.2 31 73.25 42 73.3 38 73.35 45 73.4 25 73.45 36 73.5 34 73.55 43 73.6 39 73.65 33 73.7 31 73.75 25 73.8 40 73.85 31 73.9 32 73.95 31 74 31 74.05 38 74.1 22 74.15 35 74.2 29 74.25 23 74.3 37 74.35 39 74.4 21 74.45 20 74.5 31 74.55 25 74.6 27 74.65 23 74.7 28 74.75 24 74.8 18 74.85 28 74.9 32 74.95 28 75 32