Figure 5e Lambda = 1.5418 A 2theta Intensity 5 130 5.05 130 5.1 150 5.15 151 5.2 136 5.25 134 5.3 134 5.35 136 5.4 142 5.45 141 5.5 135 5.55 134 5.6 126 5.65 139 5.7 154 5.75 133 5.8 148 5.85 128 5.9 133 5.95 165 6 140 6.05 152 6.1 133 6.15 156 6.2 140 6.25 166 6.3 170 6.35 167 6.4 148 6.45 154 6.5 139 6.55 148 6.6 138 6.65 130 6.7 149 6.75 157 6.8 165 6.85 156 6.9 148 6.95 161 7 176 7.05 155 7.1 159 7.15 169 7.2 167 7.25 195 7.3 196 7.35 184 7.4 171 7.45 165 7.5 158 7.55 181 7.6 174 7.65 185 7.7 165 7.75 204 7.8 185 7.85 172 7.9 178 7.95 190 8 181 8.05 185 8.1 176 8.15 206 8.2 180 8.25 162 8.3 197 8.35 183 8.4 175 8.45 181 8.5 206 8.55 204 8.6 169 8.65 193 8.7 199 8.75 199 8.8 217 8.85 207 8.9 176 8.95 192 9 215 9.05 212 9.1 184 9.15 196 9.2 208 9.25 221 9.3 216 9.35 189 9.4 191 9.45 198 9.5 183 9.55 187 9.6 185 9.65 199 9.7 180 9.75 146 9.8 163 9.85 174 9.9 175 9.95 159 10 148 10.05 148 10.1 152 10.15 152 10.2 122 10.25 120 10.3 138 10.35 155 10.4 149 10.45 130 10.5 144 10.55 120 10.6 134 10.65 129 10.7 139 10.75 126 10.8 135 10.85 135 10.9 119 10.95 149 11 169 11.05 140 11.1 147 11.15 131 11.2 124 11.25 127 11.3 152 11.35 119 11.4 127 11.45 139 11.5 134 11.55 141 11.6 131 11.65 128 11.7 154 11.75 118 11.8 123 11.85 135 11.9 130 11.95 139 12 143 12.05 147 12.1 143 12.15 164 12.2 122 12.25 132 12.3 161 12.35 136 12.4 122 12.45 125 12.5 129 12.55 156 12.6 116 12.65 154 12.7 136 12.75 125 12.8 138 12.85 150 12.9 125 12.95 125 13 142 13.05 161 13.1 135 13.15 134 13.2 151 13.25 139 13.3 118 13.35 124 13.4 134 13.45 122 13.5 148 13.55 152 13.6 144 13.65 135 13.7 146 13.75 166 13.8 139 13.85 147 13.9 144 13.95 131 14 122 14.05 126 14.1 145 14.15 125 14.2 139 14.25 130 14.3 147 14.35 124 14.4 134 14.45 124 14.5 126 14.55 133 14.6 132 14.65 140 14.7 143 14.75 129 14.8 134 14.85 164 14.9 179 14.95 212 15 246 15.05 196 15.1 222 15.15 277 15.2 353 15.25 464 15.3 594 15.35 836 15.4 1065 15.45 1063 15.5 733 15.55 450 15.6 277 15.65 257 15.7 198 15.75 168 15.8 154 15.85 130 15.9 144 15.95 119 16 133 16.05 133 16.1 141 16.15 113 16.2 130 16.25 112 16.3 101 16.35 91 16.4 117 16.45 106 16.5 95 16.55 111 16.6 108 16.65 101 16.7 106 16.75 102 16.8 127 16.85 123 16.9 100 16.95 128 17 115 17.05 123 17.1 101 17.15 103 17.2 96 17.25 104 17.3 100 17.35 113 17.4 102 17.45 106 17.5 109 17.55 102 17.6 124 17.65 98 17.7 99 17.75 78 17.8 96 17.85 82 17.9 102 17.95 91 18 108 18.05 86 18.1 110 18.15 108 18.2 100 18.25 133 18.3 142 18.35 158 18.4 118 18.45 98 18.5 99 18.55 89 18.6 102 18.65 130 18.7 123 18.75 99 18.8 109 18.85 106 18.9 94 18.95 95 19 120 19.05 107 19.1 105 19.15 129 19.2 140 19.25 177 19.3 224 19.35 275 19.4 357 19.45 448 19.5 509 19.55 445 19.6 299 19.65 230 19.7 150 19.75 146 19.8 132 19.85 113 19.9 108 19.95 118 20 101 20.05 97 20.1 105 20.15 81 20.2 92 20.25 94 20.3 95 20.35 110 20.4 93 20.45 99 20.5 93 20.55 99 20.6 78 20.65 101 20.7 93 20.75 84 20.8 92 20.85 93 20.9 92 20.95 93 21 96 21.05 94 21.1 81 21.15 89 21.2 91 21.25 96 21.3 108 21.35 78 21.4 101 21.45 115 21.5 97 21.55 142 21.6 155 21.65 129 21.7 102 21.75 106 21.8 104 21.85 106 21.9 84 21.95 80 22 102 22.05 112 22.1 89 22.15 80 22.2 71 22.25 84 22.3 70 22.35 102 22.4 87 22.45 76 22.5 101 22.55 89 22.6 73 22.65 94 22.7 84 22.75 78 22.8 91 22.85 73 22.9 75 22.95 92 23 81 23.05 90 23.1 85 23.15 88 23.2 98 23.25 92 23.3 75 23.35 102 23.4 81 23.45 75 23.5 96 23.55 93 23.6 81 23.65 98 23.7 99 23.75 117 23.8 113 23.85 130 23.9 139 23.95 191 24 270 24.05 342 24.1 418 24.15 342 24.2 220 24.25 145 24.3 155 24.35 105 24.4 112 24.45 90 24.5 94 24.55 91 24.6 86 24.65 93 24.7 85 24.75 69 24.8 90 24.85 75 24.9 97 24.95 76 25 70 25.05 87 25.1 95 25.15 84 25.2 95 25.25 86 25.3 81 25.35 92 25.4 80 25.45 74 25.5 94 25.55 65 25.6 82 25.65 92 25.7 82 25.75 61 25.8 73 25.85 78 25.9 69 25.95 89 26 89 26.05 98 26.1 96 26.15 64 26.2 78 26.25 66 26.3 73 26.35 76 26.4 87 26.45 99 26.5 100 26.55 100 26.6 91 26.65 116 26.7 114 26.75 154 26.8 225 26.85 332 26.9 446 26.95 504 27 419 27.05 312 27.1 182 27.15 143 27.2 119 27.25 93 27.3 91 27.35 97 27.4 92 27.45 74 27.5 74 27.55 108 27.6 78 27.65 95 27.7 84 27.75 87 27.8 79 27.85 74 27.9 94 27.95 98 28 80 28.05 92 28.1 96 28.15 95 28.2 92 28.25 99 28.3 116 28.35 140 28.4 129 28.45 195 28.5 223 28.55 264 28.6 263 28.65 188 28.7 155 28.75 137 28.8 90 28.85 90 28.9 105 28.95 89 29 84 29.05 67 29.1 88 29.15 85 29.2 72 29.25 104 29.3 83 29.35 76 29.4 66 29.45 91 29.5 80 29.55 86 29.6 70 29.65 93 29.7 99 29.75 86 29.8 83 29.85 124 29.9 113 29.95 126 30 135 30.05 173 30.1 216 30.15 353 30.2 514 30.25 679 30.3 713 30.35 459 30.4 302 30.45 145 30.5 118 30.55 99 30.6 117 30.65 107 30.7 94 30.75 80 30.8 90 30.85 82 30.9 89 30.95 74 31 91 31.05 75 31.1 79 31.15 69 31.2 62 31.25 94 31.3 80 31.35 78 31.4 67 31.45 83 31.5 79 31.55 83 31.6 95 31.65 86 31.7 106 31.75 110 31.8 134 31.85 157 31.9 206 31.95 187 32 149 32.05 117 32.1 89 32.15 93 32.2 77 32.25 76 32.3 93 32.35 77 32.4 73 32.45 78 32.5 69 32.55 74 32.6 71 32.65 79 32.7 87 32.75 83 32.8 88 32.85 54 32.9 85 32.95 64 33 67 33.05 81 33.1 88 33.15 98 33.2 103 33.25 104 33.3 100 33.35 110 33.4 157 33.45 178 33.5 208 33.55 245 33.6 213 33.65 177 33.7 127 33.75 116 33.8 94 33.85 90 33.9 110 33.95 90 34 110 34.05 103 34.1 128 34.15 157 34.2 158 34.25 122 34.3 109 34.35 104 34.4 83 34.45 68 34.5 77 34.55 75 34.6 69 34.65 69 34.7 98 34.75 90 34.8 108 34.85 115 34.9 104 34.95 96 35 84 35.05 105 35.1 79 35.15 81 35.2 79 35.25 89 35.3 74 35.35 72 35.4 67 35.45 81 35.5 66 35.55 59 35.6 67 35.65 77 35.7 73 35.75 71 35.8 79 35.85 61 35.9 88 35.95 58 36 67 36.05 56 36.1 72 36.15 78 36.2 66 36.25 76 36.3 82 36.35 81 36.4 96 36.45 86 36.5 87 36.55 113 36.6 95 36.65 86 36.7 73 36.75 82 36.8 73 36.85 73 36.9 65 36.95 76 37 73 37.05 65 37.1 79 37.15 91 37.2 114 37.25 144 37.3 122 37.35 93 37.4 100 37.45 80 37.5 70 37.55 78 37.6 62 37.65 81 37.7 67 37.75 68 37.8 56 37.85 54 37.9 62 37.95 91 38 82 38.05 66 38.1 75 38.15 58 38.2 76 38.25 60 38.3 63 38.35 75 38.4 72 38.45 59 38.5 75 38.55 69 38.6 67 38.65 66 38.7 74 38.75 59 38.8 91 38.85 65 38.9 62 38.95 77 39 53 39.05 67 39.1 64 39.15 79 39.2 74 39.25 81 39.3 70 39.35 69 39.4 68 39.45 82 39.5 73 39.55 74 39.6 93 39.65 104 39.7 90 39.75 113 39.8 110 39.85 82 39.9 91 39.95 75 40 78 40.05 72 40.1 81 40.15 88 40.2 122 40.25 112 40.3 105 40.35 93 40.4 79 40.45 81 40.5 84 40.55 78 40.6 93 40.65 83 40.7 85 40.75 73 40.8 98 40.85 80 40.9 85 40.95 66 41 74 41.05 68 41.1 71 41.15 73 41.2 72 41.25 49 41.3 63 41.35 63 41.4 85 41.45 63 41.5 53 41.55 69 41.6 58 41.65 57 41.7 50 41.75 59 41.8 69 41.85 64 41.9 73 41.95 57 42 72 42.05 64 42.1 60 42.15 85 42.2 78 42.25 82 42.3 84 42.35 104 42.4 87 42.45 82 42.5 67 42.55 64 42.6 72 42.65 60 42.7 73 42.75 55 42.8 73 42.85 61 42.9 61 42.95 70 43 72 43.05 60 43.1 59 43.15 56 43.2 50 43.25 69 43.3 50 43.35 70 43.4 63 43.45 54 43.5 57 43.55 68 43.6 69 43.65 58 43.7 61 43.75 59 43.8 64 43.85 69 43.9 78 43.95 93 44 99 44.05 113 44.1 116 44.15 107 44.2 94 44.25 73 44.3 80 44.35 79 44.4 59 44.45 63 44.5 61 44.55 63 44.6 78 44.65 60 44.7 72 44.75 63 44.8 63 44.85 69 44.9 60 44.95 82 45 57 45.05 62 45.1 63 45.15 55 45.2 53 45.25 69 45.3 56 45.35 60 45.4 48 45.45 58 45.5 65 45.55 65 45.6 50 45.65 47 45.7 76 45.75 52 45.8 65 45.85 54 45.9 60 45.95 66 46 76 46.05 80 46.1 73 46.15 79 46.2 73 46.25 77 46.3 75 46.35 64 46.4 68 46.45 74 46.5 63 46.55 60 46.6 47 46.65 50 46.7 51 46.75 61 46.8 49 46.85 67 46.9 67 46.95 70 47 64 47.05 63 47.1 48 47.15 47 47.2 68 47.25 65 47.3 76 47.35 78 47.4 62 47.45 67 47.5 86 47.55 99 47.6 113 47.65 150 47.7 128 47.75 103 47.8 105 47.85 92 47.9 71 47.95 64 48 66 48.05 70 48.1 73 48.15 63 48.2 67 48.25 67 48.3 68 48.35 63 48.4 76 48.45 50 48.5 78 48.55 68 48.6 74 48.65 92 48.7 101 48.75 109 48.8 112 48.85 121 48.9 171 48.95 151 49 175 49.05 187 49.1 151 49.15 141 49.2 126 49.25 116 49.3 108 49.35 120 49.4 93 49.45 109 49.5 125 49.55 124 49.6 116 49.65 99 49.7 97 49.75 82 49.8 79 49.85 68 49.9 78 49.95 63 50 58 50.05 68 50.1 67 50.15 75 50.2 77 50.25 86 50.3 70 50.35 61 50.4 67 50.45 82 50.5 81 50.55 54 50.6 69 50.65 62 50.7 59 50.75 67 50.8 80 50.85 70 50.9 58 50.95 65 51 56 51.05 64 51.1 54 51.15 74 51.2 75 51.25 70 51.3 88 51.35 93 51.4 97 51.45 113 51.5 142 51.55 154 51.6 123 51.65 140 51.7 137 51.75 121 51.8 83 51.85 103 51.9 62 51.95 87 52 74 52.05 62 52.1 70 52.15 50 52.2 68 52.25 60 52.3 68 52.35 97 52.4 77 52.45 70 52.5 56 52.55 68 52.6 59 52.65 78 52.7 68 52.75 60 52.8 60 52.85 72 52.9 56 52.95 65 53 79 53.05 76 53.1 68 53.15 72 53.2 78 53.25 89 53.3 72 53.35 55 53.4 65 53.45 61 53.5 57 53.55 57 53.6 70 53.65 61 53.7 60 53.75 62 53.8 64 53.85 77 53.9 77 53.95 87 54 79 54.05 79 54.1 95 54.15 72 54.2 79 54.25 59 54.3 88 54.35 71 54.4 74 54.45 83 54.5 60 54.55 64 54.6 65 54.65 50 54.7 67 54.75 67 54.8 53 54.85 46 54.9 63 54.95 60 55 59 55.05 64 55.1 67 55.15 68 55.2 74 55.25 76 55.3 62 55.35 69 55.4 69 55.45 93 55.5 92 55.55 92 55.6 108 55.65 111 55.7 98 55.75 105 55.8 86 55.85 91 55.9 76 55.95 82 56 85 56.05 118 56.1 109 56.15 90 56.2 81 56.25 74 56.3 77 56.35 72 56.4 79 56.45 75 56.5 67 56.55 65 56.6 67 56.65 69 56.7 72 56.75 94 56.8 108 56.85 93 56.9 94 56.95 102 57 86 57.05 86 57.1 74 57.15 75 57.2 69 57.25 54 57.3 64 57.35 92 57.4 82 57.45 67 57.5 66 57.55 65 57.6 55 57.65 63 57.7 71 57.75 61 57.8 72 57.85 48 57.9 61 57.95 64 58 58 58.05 60 58.1 65 58.15 64 58.2 60 58.25 62 58.3 61 58.35 51 58.4 65 58.45 60 58.5 58 58.55 58 58.6 49 58.65 54 58.7 49 58.75 49 58.8 58 58.85 53 58.9 68 58.95 70 59 58 59.05 70 59.1 70 59.15 69 59.2 78 59.25 58 59.3 73 59.35 62 59.4 69 59.45 66 59.5 52 59.55 65 59.6 59 59.65 72 59.7 65 59.75 70 59.8 79 59.85 92 59.9 63 59.95 75 60 46 60.05 76 60.1 58 60.15 58 60.2 66 60.25 70 60.3 63 60.35 64 60.4 52 60.45 59 60.5 62 60.55 57 60.6 58 60.65 57 60.7 61 60.75 74 60.8 68 60.85 75 60.9 65 60.95 81 61 74 61.05 64 61.1 59 61.15 60 61.2 61 61.25 63 61.3 50 61.35 76 61.4 68 61.45 65 61.5 57 61.55 58 61.6 73 61.65 61 61.7 77 61.75 74 61.8 93 61.85 73 61.9 65 61.95 59 62 74 62.05 74 62.1 80 62.15 84 62.2 83 62.25 99 62.3 97 62.35 58 62.4 73 62.45 61 62.5 58 62.55 67 62.6 71 62.65 62 62.7 73 62.75 62 62.8 75 62.85 63 62.9 78 62.95 84 63 84 63.05 101 63.1 111 63.15 87 63.2 103 63.25 85 63.3 123 63.35 80 63.4 92 63.45 62 63.5 73 63.55 85 63.6 56 63.65 57 63.7 52 63.75 51 63.8 61 63.85 64 63.9 51 63.95 60 64 56 64.05 58 64.1 59 64.15 80 64.2 49 64.25 47 64.3 46 64.35 50 64.4 56 64.45 48 64.5 53 64.55 54 64.6 69 64.65 60 64.7 60 64.75 52 64.8 54 64.85 43 64.9 54 64.95 74 65 61 65.05 51 65.1 55 65.15 57 65.2 83 65.25 80 65.3 77 65.35 91 65.4 83 65.45 78 65.5 72 65.55 71 65.6 81 65.65 76 65.7 60 65.75 67 65.8 76 65.85 64 65.9 63 65.95 55 66 64 66.05 59 66.1 68 66.15 60 66.2 65 66.25 71 66.3 55 66.35 64 66.4 58 66.45 67 66.5 58 66.55 67 66.6 57 66.65 56 66.7 51 66.75 78 66.8 53 66.85 73 66.9 56 66.95 55 67 71 67.05 67 67.1 54 67.15 48 67.2 53 67.25 57 67.3 53 67.35 60 67.4 51 67.45 54 67.5 75 67.55 96 67.6 85 67.65 77 67.7 71 67.75 74 67.8 71 67.85 72 67.9 61 67.95 73 68 73 68.05 72 68.1 58 68.15 56 68.2 48 68.25 60 68.3 51 68.35 47 68.4 48 68.45 70 68.5 56 68.55 55 68.6 62 68.65 51 68.7 53 68.75 49 68.8 80 68.85 68 68.9 52 68.95 55 69 65 69.05 60 69.1 66 69.15 60 69.2 59 69.25 59 69.3 64 69.35 68 69.4 82 69.45 86 69.5 70 69.55 67 69.6 84 69.65 75 69.7 71 69.75 76 69.8 61 69.85 65 69.9 64 69.95 66 70 54 70.05 62 70.1 60 70.15 51 70.2 60 70.25 48 70.3 67 70.35 65 70.4 58 70.45 67 70.5 56 70.55 66 70.6 66 70.65 69 70.7 59 70.75 53 70.8 52 70.85 60 70.9 79 70.95 67 71 61 71.05 71 71.1 58 71.15 65 71.2 51 71.25 70 71.3 68 71.35 61 71.4 72 71.45 84 71.5 69 71.55 65 71.6 63 71.65 63 71.7 57 71.75 94 71.8 77 71.85 71 71.9 73 71.95 84 72 73 72.05 77 72.1 83 72.15 73 72.2 72 72.25 89 72.3 69 72.35 72 72.4 62 72.45 62 72.5 60 72.55 77 72.6 65 72.65 54 72.7 68 72.75 60 72.8 52 72.85 68 72.9 61 72.95 51 73 48 73.05 53 73.1 66 73.15 51 73.2 67 73.25 48 73.3 52 73.35 64 73.4 67 73.45 56 73.5 54 73.55 80 73.6 61 73.65 82 73.7 68 73.75 94 73.8 74 73.85 95 73.9 91 73.95 78 74 78 74.05 87 74.1 75 74.15 67 74.2 67 74.25 69 74.3 55 74.35 67 74.4 57 74.45 51 74.5 61 74.55 58 74.6 65 74.65 49 74.7 59 74.75 48 74.8 59 74.85 50 74.9 60 74.95 47 75 0