# Electronic Supplementary Material (ESI) for CrystEngComm.
# This journal is © The Royal Society of Chemistry 2020

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
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data_Cs2UO2Ga2O5
_database_code_depnum_ccdc_archive 'CCDC 1984888'
loop_
_audit_author_name
_audit_author_address
'Christian Juillerat'
;University of South Carolina
United States of America
;
_audit_update_record             
;
2020-02-18 deposited with the CCDC.	2020-04-07 downloaded from the CCDC.
;
_audit_creation_date             2019-04-17
_audit_creation_method           
;
Olex2 1.2
(compiled May 18 2018 14:05:52 for OlexSys, GUI svn.r5506)
;
_shelx_SHELXL_version_number     2016/6
_chemical_name_common            ?
_chemical_name_systematic        Cs2UO2Ga2O5
_chemical_formula_moiety         '0.13(Cs5.88 Ga16 O56 U8), 0.16(Cs8)'
_chemical_formula_sum            'Cs2 Ga2 O7 U'
_chemical_formula_weight         755.62
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Cs Cs -0.3680 2.1192 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ga Ga 0.2307 1.6083 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
U U -9.6767 9.6646 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      tetragonal
_space_group_IT_number           141
_space_group_name_H-M_alt        'I 41/a m d'
_space_group_name_Hall           '-I 4bd 2'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, -y, z+1/2'
'-y+1/4, x+3/4, z+1/4'
'y+1/4, -x+1/4, z+3/4'
'-x+1/2, y, -z+1/2'
'x, -y, -z'
'y+1/4, x+3/4, -z+1/4'
'-y+1/4, -x+1/4, -z+3/4'
'x+1/2, y+1/2, z+1/2'
'-x+1, -y+1/2, z+1'
'-y+3/4, x+5/4, z+3/4'
'y+3/4, -x+3/4, z+5/4'
'-x+1, y+1/2, -z+1'
'x+1/2, -y+1/2, -z+1/2'
'y+3/4, x+5/4, -z+3/4'
'-y+3/4, -x+3/4, -z+5/4'
'-x, -y, -z'
'x-1/2, y, -z-1/2'
'y-1/4, -x-3/4, -z-1/4'
'-y-1/4, x-1/4, -z-3/4'
'x-1/2, -y, z-1/2'
'-x, y, z'
'-y-1/4, -x-3/4, z-1/4'
'y-1/4, x-1/4, z-3/4'
'-x+1/2, -y+1/2, -z+1/2'
'x, y+1/2, -z'
'y+1/4, -x-1/4, -z+1/4'
'-y+1/4, x+1/4, -z-1/4'
'x, -y+1/2, z'
'-x+1/2, y+1/2, z+1/2'
'-y+1/4, -x-1/4, z+1/4'
'y+1/4, x+1/4, z-1/4'

_cell_length_a                   7.41690(10)
_cell_length_b                   7.41690(10)
_cell_length_c                   31.9700(7)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_volume                     1758.68(6)
_cell_formula_units_Z            8
_cell_measurement_reflns_used    9671
_cell_measurement_temperature    302(2)
_cell_measurement_theta_max      36.34
_cell_measurement_theta_min      2.82
_shelx_estimated_absorpt_T_max   0.562
_shelx_estimated_absorpt_T_min   0.245
_exptl_absorpt_coefficient_mu    32.620
_exptl_absorpt_correction_T_max  0.1661
_exptl_absorpt_correction_T_min  0.0997
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
SADABS-2016/2 (Bruker,2016) was used for absorption correction.
wR2(int) was 0.0911 before and 0.0520 after correction.
The Ratio of minimum to maximum transmission is 0.6002.
The λ/2 correction factor is Not present.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            'clear yellow'
_exptl_crystal_colour_lustre     clear
_exptl_crystal_colour_primary    yellow
_exptl_crystal_density_diffrn    5.708
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       shard
_exptl_crystal_F_000             2561
_exptl_crystal_preparation       Luminescent
_exptl_crystal_size_max          0.06
_exptl_crystal_size_mid          0.04
_exptl_crystal_size_min          0.02
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0352
_diffrn_reflns_av_unetI/netI     0.0088
_diffrn_reflns_Laue_measured_fraction_full 0.996
_diffrn_reflns_Laue_measured_fraction_max 0.998
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       11
_diffrn_reflns_limit_k_min       -12
_diffrn_reflns_limit_l_max       53
_diffrn_reflns_limit_l_min       -53
_diffrn_reflns_number            61580
_diffrn_reflns_point_group_measured_fraction_full 0.996
_diffrn_reflns_point_group_measured_fraction_max 0.998
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         36.353
_diffrn_reflns_theta_min         2.548
_diffrn_ambient_temperature      302.0
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_diffrn_standards_number         0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                1184
_reflns_number_total             1204
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       ?
_computing_data_collection       ?
_computing_data_reduction        ?
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    'ShelXT (Sheldrick, 2015)'
_refine_diff_density_max         1.481
_refine_diff_density_min         -1.450
_refine_diff_density_rms         0.213
_refine_ls_extinction_coef       0.00022(3)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     'SHELXL-2016/6 (Sheldrick 2016)'
_refine_ls_goodness_of_fit_ref   1.326
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     73
_refine_ls_number_reflns         1204
_refine_ls_number_restraints     6
_refine_ls_R_factor_all          0.0214
_refine_ls_R_factor_gt           0.0210
_refine_ls_restrained_S_all      1.340
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0062P)²+32.4069P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0498
_refine_ls_wR_factor_ref         0.0499
_refine_special_details          ?
_olex2_refinement_description    
;
1. Uiso/Uaniso restraints and constraints
Uanis(Cs2) \\sim Ueq: with sigma of 0.006 and sigma for terminal atoms of 0.01
2. Others
 Fixed Sof: Cs1(0.3169) Cs2(0.065) Cs3(0.02227) Cs4(0.026) Cs5(0.02042)
 Cs6(0.025) Cs7(0.025)
;
_atom_sites_solution_hydrogens   .
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
U1 U 0.000000 0.250000 0.24030(2) 0.01109(6) Uani 1 4 d S T P . .
Cs1 Cs 0.500000 0.4951(4) 0.44168(8) 0.0441(5) Uani 0.6338 2 d S T P . .
Cs2 Cs 0.500000 0.4576(19) 0.4412(2) 0.037(2) Uani 0.13 2 d S TU P . .
Cs3 Cs 0.500000 0.378(3) 0.4397(5) 0.047(4) Uani 0.0445 2 d S T P . .
Cs4 Cs 0.500000 0.2856(17) 0.4396(3) 0.038(4) Uani 0.052 2 d S T P . .
Cs5 Cs 0.500000 0.829(3) 0.4166(7) 0.053(6) Uani 0.0408 2 d S T P . .
Cs6 Cs 0.500000 0.750000 0.4126(4) 0.042(3) Uani 0.1 4 d S T P . .
Cs7 Cs 0.500000 0.567(2) 0.4278(5) 0.042(3) Uani 0.05 2 d S T P . .
Ga2 Ga 0.25922(7) 0.250000 0.34698(2) 0.01454(10) Uani 1 2 d S T P . .
O1 O 0.000000 0.4992(6) 0.23971(13) 0.0235(8) Uani 1 2 d S T P . .
O2 O 0.2049(5) 0.250000 0.29054(11) 0.0215(8) Uani 1 2 d S T P . .
O3 O 0.2042(5) 0.4542(5) 0.375000 0.0321(10) Uani 1 2 d S T P . .
O4 O 0.500000 0.250000 0.33555(19) 0.0359(19) Uani 1 4 d S T P . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
U1 U1 3.75994(9) 25_455 ?
U1 U1 3.75994(9) 25 ?
U1 Cs4 4.341(5) 19_576 ?
U1 Ga2 3.3129(5) 18_556 ?
U1 Ga2 3.3129(5) 25 ?
U1 O1 1.849(4) . ?
U1 O1 1.849(4) 10_454 ?
U1 O2 2.401(4) 18_556 ?
U1 O2 2.401(4) 25 ?
U1 O2 2.211(4) . ?
U1 O2 2.211(4) 10_454 ?
U1 O4 2.425(6) 25 ?
Cs1 Cs3 2.77(2) 10_554 ?
Cs1 Cs3 0.87(2) . ?
Cs1 Cs4 2.083(13) 10_554 ?
Cs1 Cs4 1.555(13) . ?
Cs1 Cs5 2.60(2) . ?
Cs1 Cs5 1.53(2) 10_564 ?
Cs1 Cs6 2.106(7) . ?
Cs1 Cs7 0.693(18) . ?
Cs1 O1 3.064(4) 3_655 ?
Cs1 O1 3.064(4) 12_454 ?
Cs1 O3 3.074(4) 28_656 ?
Cs1 O3 3.074(4) . ?
Cs2 Cs2 3.08(3) 10_554 ?
Cs2 Cs3 2.49(3) 10_554 ?
Cs2 Cs3 0.595(18) . ?
Cs2 Cs4 1.804(19) 10_554 ?
Cs2 Cs4 1.277(19) . ?
Cs2 Cs5 1.77(3) 10_564 ?
Cs2 Cs5 2.86(3) . ?
Cs2 Cs6 2.354(15) . ?
Cs2 Cs7 0.92(2) . ?
Cs2 O1 3.251(10) 3_655 ?
Cs2 O3 3.049(6) 28_656 ?
Cs2 O3 3.049(6) . ?
Cs3 Cs3 1.89(4) 10_554 ?
Cs3 Cs4 0.68(2) . ?
Cs3 Cs4 1.21(3) 10_554 ?
Cs3 Cs5 2.30(3) 10_564 ?
Cs3 Cs6 2.89(2) . ?
Cs3 Cs7 1.45(3) . ?
Cs3 O3 3.068(13) 28_656 ?
Cs3 O3 3.068(13) . ?
Cs4 Cs4 0.53(3) 10_554 ?
Cs4 Cs5 2.95(3) 10_564 ?
Cs4 Cs7 2.64(2) 10_554 ?
Cs4 Cs7 2.12(2) . ?
Cs4 O1 2.939(8) 19_566 ?
Cs4 O1 2.939(8) 28_656 ?
Cs5 Cs5 2.78(4) 28_656 ?
Cs5 Cs5 2.78(4) 19_576 ?
Cs5 Cs5 1.17(4) 10_564 ?
Cs5 Cs6 2.599(18) 19_576 ?
Cs5 Cs6 0.60(2) . ?
Cs5 Cs7 1.97(3) . ?
Cs5 Cs7 0.85(2) 10_564 ?
Cs6 Cs6 2.41(3) 19_576 ?
Cs6 Cs7 1.442(18) 10_564 ?
Cs6 Cs7 1.442(18) . ?
Cs7 Cs7 2.71(3) 10_564 ?
Cs7 O1 3.036(10) 3_655 ?
Cs7 O3 2.892(9) 28_656 ?
Cs7 O3 2.892(9) . ?
Ga2 O2 1.849(4) . ?
Ga2 O3 1.806(2) . ?
Ga2 O3 1.806(2) 19_566 ?
Ga2 O4 1.8229(13) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
U1 U1 U1 161.013(13) 25 25_455 ?
U1 U1 Cs4 81.65(16) 25 19_576 ?
U1 U1 Cs4 88.56(17) 25_455 19_576 ?
Ga2 U1 U1 132.113(13) 25 25_455 ?
Ga2 U1 U1 132.113(13) 18_556 25 ?
Ga2 U1 U1 66.874(10) 25 25 ?
Ga2 U1 U1 66.874(10) 18_556 25_455 ?
Ga2 U1 Cs4 113.71(14) 25 19_576 ?
Ga2 U1 Cs4 117.88(12) 18_556 19_576 ?
Ga2 U1 Ga2 65.238(19) 18_556 25 ?
O1 U1 U1 90.10(2) . 25 ?
O1 U1 U1 90.10(2) 10_454 25 ?
O1 U1 U1 90.10(2) . 25_455 ?
O1 U1 U1 90.10(2) 10_454 25_455 ?
O1 U1 Cs4 149.25(17) 10_454 19_576 ?
O1 U1 Cs4 31.90(16) . 19_576 ?
O1 U1 Ga2 89.51(11) . 18_556 ?
O1 U1 Ga2 89.51(11) . 25 ?
O1 U1 Ga2 89.51(11) 10_454 18_556 ?
O1 U1 Ga2 89.51(11) 10_454 25 ?
O1 U1 O1 178.8(3) . 10_454 ?
O1 U1 O2 89.76(5) 10_454 18_556 ?
O1 U1 O2 90.42(9) 10_454 10_454 ?
O1 U1 O2 90.42(9) . . ?
O1 U1 O2 90.42(9) . 10_454 ?
O1 U1 O2 90.42(9) 10_454 . ?
O1 U1 O2 89.76(5) . 18_556 ?
O1 U1 O2 89.76(5) 10_454 25 ?
O1 U1 O2 89.76(5) . 25 ?
O1 U1 O4 89.42(13) 10_454 25 ?
O1 U1 O4 89.42(13) . 25 ?
O2 U1 U1 165.24(8) 25 25_455 ?
O2 U1 U1 33.74(8) 18_556 25_455 ?
O2 U1 U1 123.92(10) 10_454 25 ?
O2 U1 U1 37.09(10) . 25 ?
O2 U1 U1 123.92(10) . 25_455 ?
O2 U1 U1 37.10(10) 10_454 25_455 ?
O2 U1 U1 33.74(8) 25 25 ?
O2 U1 U1 165.24(8) 18_556 25 ?
O2 U1 Cs4 70.53(15) 10_454 19_576 ?
O2 U1 Cs4 99.01(17) 25 19_576 ?
O2 U1 Cs4 105.52(16) 18_556 19_576 ?
O2 U1 Cs4 65.36(14) . 19_576 ?
O2 U1 Ga2 103.97(10) 10_454 18_556 ?
O2 U1 Ga2 169.21(10) 10_454 25 ?
O2 U1 Ga2 33.13(8) 25 25 ?
O2 U1 Ga2 98.37(8) 25 18_556 ?
O2 U1 Ga2 33.13(8) 18_556 18_556 ?
O2 U1 Ga2 169.21(10) . 18_556 ?
O2 U1 Ga2 103.97(10) . 25 ?
O2 U1 Ga2 98.37(8) 18_556 25 ?
O2 U1 O2 157.66(11) . 18_556 ?
O2 U1 O2 70.84(14) 10_454 18_556 ?
O2 U1 O2 70.84(15) . 25 ?
O2 U1 O2 131.50(17) 18_556 25 ?
O2 U1 O2 86.8(2) . 10_454 ?
O2 U1 O2 157.66(11) 10_454 25 ?
O2 U1 O4 136.59(10) . 25 ?
O2 U1 O4 136.59(10) 10_454 25 ?
O2 U1 O4 65.75(8) 25 25 ?
O2 U1 O4 65.75(8) 18_556 25 ?
O4 U1 U1 99.493(7) 25 25 ?
O4 U1 U1 99.493(7) 25 25_455 ?
O4 U1 Cs4 121.09(11) 25 19_576 ?
O4 U1 Ga2 32.619(10) 25 18_556 ?
O4 U1 Ga2 32.619(9) 25 25 ?
Cs3 Cs1 Cs3 2.8(8) . 10_554 ?
Cs3 Cs1 Cs4 1.7(12) . . ?
Cs3 Cs1 Cs4 2.3(12) . 10_554 ?
Cs3 Cs1 Cs5 157.9(12) . . ?
Cs3 Cs1 Cs5 144.3(14) . 10_564 ?
Cs3 Cs1 Cs6 149.7(12) . . ?
Cs3 Cs1 O1 130.7(7) . 12_454 ?
Cs3 Cs1 O1 128.9(2) 10_554 12_454 ?
Cs3 Cs1 O1 128.9(2) 10_554 3_655 ?
Cs3 Cs1 O1 130.7(7) . 3_655 ?
Cs3 Cs1 O3 81.4(8) . . ?
Cs3 Cs1 O3 81.4(8) . 28_656 ?
Cs3 Cs1 O3 83.4(2) 10_554 28_656 ?
Cs3 Cs1 O3 83.4(2) 10_554 . ?
Cs4 Cs1 Cs3 1.2(5) . 10_554 ?
Cs4 Cs1 Cs3 0.5(4) 10_554 10_554 ?
Cs4 Cs1 Cs4 0.63(10) . 10_554 ?
Cs4 Cs1 Cs5 159.6(6) . . ?
Cs4 Cs1 Cs5 160.2(6) 10_554 . ?
Cs4 Cs1 Cs6 151.4(5) . . ?
Cs4 Cs1 Cs6 152.0(4) 10_554 . ?
Cs4 Cs1 O1 129.25(19) 10_554 3_655 ?
Cs4 Cs1 O1 129.25(19) 10_554 12_454 ?
Cs4 Cs1 O1 129.6(2) . 3_655 ?
Cs4 Cs1 O1 129.6(2) . 12_454 ?
Cs4 Cs1 O3 83.0(2) 10_554 28_656 ?
Cs4 Cs1 O3 82.6(3) . 28_656 ?
Cs4 Cs1 O3 83.0(2) 10_554 . ?
Cs4 Cs1 O3 82.6(3) . . ?
Cs5 Cs1 Cs3 147.2(9) 10_564 10_554 ?
Cs5 Cs1 Cs3 160.7(6) . 10_554 ?
Cs5 Cs1 Cs4 146.0(9) 10_564 . ?
Cs5 Cs1 Cs4 146.6(8) 10_564 10_554 ?
Cs5 Cs1 Cs5 13.6(6) 10_564 . ?
Cs5 Cs1 Cs6 5.4(10) 10_564 . ?
Cs5 Cs1 O1 74.7(6) 10_564 12_454 ?
Cs5 Cs1 O1 64.4(4) . 3_655 ?
Cs5 Cs1 O1 74.7(6) 10_564 3_655 ?
Cs5 Cs1 O1 64.4(4) . 12_454 ?
Cs5 Cs1 O3 83.1(3) . 28_656 ?
Cs5 Cs1 O3 73.8(5) 10_564 . ?
Cs5 Cs1 O3 83.1(3) . . ?
Cs5 Cs1 O3 73.8(5) 10_564 28_656 ?
Cs6 Cs1 Cs3 152.5(5) . 10_554 ?
Cs6 Cs1 Cs5 8.2(7) . . ?
Cs6 Cs1 O1 70.6(3) . 3_655 ?
Cs6 Cs1 O1 70.6(3) . 12_454 ?
Cs6 Cs1 O3 77.5(3) . 28_656 ?
Cs6 Cs1 O3 77.5(3) . . ?
Cs7 Cs1 Cs3 136.1(17) . . ?
Cs7 Cs1 Cs3 139.0(11) . 10_554 ?
Cs7 Cs1 Cs4 137.8(12) . . ?
Cs7 Cs1 Cs4 138.4(11) . 10_554 ?
Cs7 Cs1 Cs5 21.8(11) . . ?
Cs7 Cs1 Cs5 8.2(13) . 10_564 ?
Cs7 Cs1 Cs6 13.6(11) . . ?
Cs7 Cs1 O1 81.1(8) . 12_454 ?
Cs7 Cs1 O1 81.1(8) . 3_655 ?
Cs7 Cs1 O3 68.5(7) . . ?
Cs7 Cs1 O3 68.5(7) . 28_656 ?
O1 Cs1 O1 74.74(15) 3_655 12_454 ?
O1 Cs1 O3 147.30(13) 3_655 . ?
O1 Cs1 O3 147.30(13) 12_454 28_656 ?
O1 Cs1 O3 88.58(9) 3_655 28_656 ?
O1 Cs1 O3 88.58(9) 12_454 . ?
O3 Cs1 O3 91.07(11) 28_656 . ?
Cs2 Cs2 O1 131.9(2) 10_554 3_655 ?
Cs3 Cs2 Cs2 4.7(18) . 10_554 ?
Cs3 Cs2 Cs2 1.1(4) 10_554 10_554 ?
Cs3 Cs2 Cs3 3.6(14) . 10_554 ?
Cs3 Cs2 Cs4 3.0(18) . 10_554 ?
Cs3 Cs2 Cs4 2.3(18) . . ?
Cs3 Cs2 Cs5 149(2) . 10_564 ?
Cs3 Cs2 Cs5 159.3(19) . . ?
Cs3 Cs2 Cs5 162.9(6) 10_554 . ?
Cs3 Cs2 Cs6 152.5(18) . . ?
Cs3 Cs2 Cs7 147(2) . . ?
Cs3 Cs2 O1 134.7(11) . 3_655 ?
Cs3 Cs2 O1 132.6(4) 10_554 3_655 ?
Cs3 Cs2 O3 88.7(4) 10_554 . ?
Cs3 Cs2 O3 86.3(12) . . ?
Cs3 Cs2 O3 88.7(4) 10_554 28_656 ?
Cs3 Cs2 O3 86.3(12) . 28_656 ?
Cs4 Cs2 Cs2 1.7(4) 10_554 10_554 ?
Cs4 Cs2 Cs2 2.4(6) . 10_554 ?
Cs4 Cs2 Cs3 1.2(6) . 10_554 ?
Cs4 Cs2 Cs3 0.5(5) 10_554 10_554 ?
Cs4 Cs2 Cs4 0.69(17) . 10_554 ?
Cs4 Cs2 Cs5 161.7(8) . . ?
Cs4 Cs2 Cs5 151.2(10) . 10_564 ?
Cs4 Cs2 Cs5 162.4(6) 10_554 . ?
Cs4 Cs2 Cs6 155.5(6) 10_554 . ?
Cs4 Cs2 Cs6 154.8(7) . . ?
Cs4 Cs2 O1 132.9(4) 10_554 3_655 ?
Cs4 Cs2 O1 133.3(5) . 3_655 ?
Cs4 Cs2 O3 87.9(4) . 28_656 ?
Cs4 Cs2 O3 87.9(4) . . ?
Cs4 Cs2 O3 88.4(3) 10_554 28_656 ?
Cs4 Cs2 O3 88.4(3) 10_554 . ?
Cs5 Cs2 Cs2 164.0(5) . 10_554 ?
Cs5 Cs2 Cs2 153.6(7) 10_564 10_554 ?
Cs5 Cs2 Cs3 152.5(9) 10_564 10_554 ?
Cs5 Cs2 Cs4 151.9(9) 10_564 10_554 ?
Cs5 Cs2 Cs5 10.4(5) 10_564 . ?
Cs5 Cs2 Cs6 3.6(9) 10_564 . ?
Cs5 Cs2 O1 59.3(4) . 3_655 ?
Cs5 Cs2 O1 67.3(6) 10_564 3_655 ?
Cs5 Cs2 O3 72.5(5) 10_564 28_656 ?
Cs5 Cs2 O3 79.5(4) . 28_656 ?
Cs5 Cs2 O3 72.5(5) 10_564 . ?
Cs5 Cs2 O3 79.5(4) . . ?
Cs6 Cs2 Cs2 157.2(3) . 10_554 ?
Cs6 Cs2 Cs3 156.0(6) . 10_554 ?
Cs6 Cs2 Cs5 6.9(6) . . ?
Cs6 Cs2 O1 64.6(4) . 3_655 ?
Cs6 Cs2 O3 74.8(3) . . ?
Cs6 Cs2 O3 74.8(3) . 28_656 ?
Cs7 Cs2 Cs2 152.2(9) . 10_554 ?
Cs7 Cs2 Cs3 151.1(10) . 10_554 ?
Cs7 Cs2 Cs4 150.5(10) . 10_554 ?
Cs7 Cs2 Cs4 149.8(11) . . ?
Cs7 Cs2 Cs5 11.9(9) . . ?
Cs7 Cs2 Cs5 1.4(10) . 10_564 ?
Cs7 Cs2 Cs6 5.0(9) . . ?
Cs7 Cs2 O1 68.4(9) . 3_655 ?
Cs7 Cs2 O3 71.5(5) . . ?
Cs7 Cs2 O3 71.5(5) . 28_656 ?
O3 Cs2 Cs2 89.5(3) 28_656 10_554 ?
O3 Cs2 Cs2 89.5(3) . 10_554 ?
O3 Cs2 O1 138.4(5) . 3_655 ?
O3 Cs2 O1 85.69(19) 28_656 3_655 ?
O3 Cs2 O3 92.0(2) 28_656 . ?
Cs1 Cs3 Cs1 174.5(15) . 10_554 ?
Cs1 Cs3 Cs2 174.7(15) . 10_554 ?
Cs1 Cs3 Cs3 175.8(11) . 10_554 ?
Cs1 Cs3 Cs4 176(2) . 10_554 ?
Cs1 Cs3 Cs5 22.9(10) . 10_564 ?
Cs1 Cs3 Cs6 21.6(9) . . ?
Cs1 Cs3 Cs6 163.9(7) 10_554 . ?
Cs1 Cs3 Cs7 19.3(9) . . ?
Cs1 Cs3 O3 101.6(4) 10_554 28_656 ?
Cs1 Cs3 O3 82.2(10) . . ?
Cs1 Cs3 O3 101.6(4) 10_554 . ?
Cs1 Cs3 O3 82.2(10) . 28_656 ?
Cs2 Cs3 Cs1 174(2) . 10_554 ?
Cs2 Cs3 Cs1 0.2(2) 10_554 10_554 ?
Cs2 Cs3 Cs1 0.5(10) . . ?
Cs2 Cs3 Cs2 174(2) . 10_554 ?
Cs2 Cs3 Cs3 175.3(18) . 10_554 ?
Cs2 Cs3 Cs4 176(3) . . ?
Cs2 Cs3 Cs4 175(3) . 10_554 ?
Cs2 Cs3 Cs5 23.4(16) . 10_564 ?
Cs2 Cs3 Cs6 22.1(16) . . ?
Cs2 Cs3 Cs6 163.7(7) 10_554 . ?
Cs2 Cs3 Cs7 19.8(13) . . ?
Cs2 Cs3 O3 82.6(14) . . ?
Cs2 Cs3 O3 101.4(4) 10_554 28_656 ?
Cs2 Cs3 O3 101.4(4) 10_554 . ?
Cs2 Cs3 O3 82.6(14) . 28_656 ?
Cs3 Cs3 Cs1 1.3(3) 10_554 10_554 ?
Cs3 Cs3 Cs2 1.1(4) 10_554 10_554 ?
Cs3 Cs3 Cs5 161.3(6) 10_554 10_564 ?
Cs3 Cs3 Cs6 162.6(4) 10_554 . ?
Cs3 Cs3 O3 100.7(4) 10_554 28_656 ?
Cs3 Cs3 O3 100.7(4) 10_554 . ?
Cs4 Cs3 Cs1 176(3) . . ?
Cs4 Cs3 Cs1 1.6(14) . 10_554 ?
Cs4 Cs3 Cs1 1.5(7) 10_554 10_554 ?
Cs4 Cs3 Cs2 1.4(14) . 10_554 ?
Cs4 Cs3 Cs2 1.3(7) 10_554 10_554 ?
Cs4 Cs3 Cs3 0.3(17) . 10_554 ?
Cs4 Cs3 Cs3 0.2(9) 10_554 10_554 ?
Cs4 Cs3 Cs4 0.1(7) . 10_554 ?
Cs4 Cs3 Cs5 161(2) . 10_564 ?
Cs4 Cs3 Cs5 161.1(13) 10_554 10_564 ?
Cs4 Cs3 Cs6 162.4(12) 10_554 . ?
Cs4 Cs3 Cs6 162.3(19) . . ?
Cs4 Cs3 Cs7 165(2) . . ?
Cs4 Cs3 Cs7 164.7(16) 10_554 . ?
Cs4 Cs3 O3 100.5(7) 10_554 . ?
Cs4 Cs3 O3 100.4(11) . 28_656 ?
Cs4 Cs3 O3 100.4(11) . . ?
Cs4 Cs3 O3 100.5(7) 10_554 28_656 ?
Cs5 Cs3 Cs1 162.6(9) 10_564 10_554 ?
Cs5 Cs3 Cs2 162.4(9) 10_564 10_554 ?
Cs5 Cs3 Cs6 1.3(7) 10_564 . ?
Cs5 Cs3 O3 66.9(5) 10_564 28_656 ?
Cs5 Cs3 O3 66.9(5) 10_564 . ?
Cs6 Cs3 O3 67.8(5) . 28_656 ?
Cs6 Cs3 O3 67.8(5) . . ?
Cs7 Cs3 Cs1 166.2(11) . 10_554 ?
Cs7 Cs3 Cs2 166.0(11) . 10_554 ?
Cs7 Cs3 Cs3 164.9(8) . 10_554 ?
Cs7 Cs3 Cs5 3.6(8) . 10_564 ?
Cs7 Cs3 Cs6 2.3(7) . . ?
Cs7 Cs3 O3 69.2(6) . 28_656 ?
Cs7 Cs3 O3 69.2(6) . . ?
O3 Cs3 O3 91.3(5) 28_656 . ?
Cs1 Cs4 Cs1 175.7(6) . 10_554 ?
Cs1 Cs4 Cs2 175.9(7) . 10_554 ?
Cs1 Cs4 Cs5 167.4(6) 10_554 10_564 ?
Cs1 Cs4 Cs5 16.9(5) . 10_564 ?
Cs1 Cs4 Cs7 174.3(6) . 10_554 ?
Cs1 Cs4 Cs7 12.7(4) . . ?
Cs1 Cs4 Cs7 171.6(6) 10_554 . ?
Cs1 Cs4 Cs7 10.0(3) 10_554 10_554 ?
Cs1 Cs4 O1 83.4(3) 10_554 19_566 ?
Cs1 Cs4 O1 83.4(3) 10_554 28_656 ?
Cs1 Cs4 O1 93.2(4) . 28_656 ?
Cs1 Cs4 O1 93.2(4) . 19_566 ?
Cs2 Cs4 Cs1 175.8(8) . 10_554 ?
Cs2 Cs4 Cs1 0.1(4) . . ?
Cs2 Cs4 Cs1 0.2(3) 10_554 10_554 ?
Cs2 Cs4 Cs2 176.0(10) . 10_554 ?
Cs2 Cs4 Cs5 16.8(6) . 10_564 ?
Cs2 Cs4 Cs5 167.3(7) 10_554 10_564 ?
Cs2 Cs4 Cs7 12.6(5) . . ?
Cs2 Cs4 Cs7 174.2(9) . 10_554 ?
Cs2 Cs4 Cs7 171.5(8) 10_554 . ?
Cs2 Cs4 Cs7 9.8(3) 10_554 10_554 ?
Cs2 Cs4 O1 93.3(5) . 28_656 ?
Cs2 Cs4 O1 93.3(5) . 19_566 ?
Cs2 Cs4 O1 83.6(4) 10_554 28_656 ?
Cs2 Cs4 O1 83.6(4) 10_554 19_566 ?
Cs3 Cs4 Cs1 177.3(12) 10_554 . ?
Cs3 Cs4 Cs1 177.8(18) . 10_554 ?
Cs3 Cs4 Cs1 2.2(15) . . ?
Cs3 Cs4 Cs1 1.7(8) 10_554 10_554 ?
Cs3 Cs4 Cs2 1.5(8) 10_554 10_554 ?
Cs3 Cs4 Cs2 2.0(15) . . ?
Cs3 Cs4 Cs2 178.0(19) . 10_554 ?
Cs3 Cs4 Cs2 177.5(13) 10_554 . ?
Cs3 Cs4 Cs3 179(3) . 10_554 ?
Cs3 Cs4 Cs5 14.7(16) . 10_564 ?
Cs3 Cs4 Cs5 165.8(11) 10_554 10_564 ?
Cs3 Cs4 Cs7 10.5(16) . . ?
Cs3 Cs4 Cs7 170.0(12) 10_554 . ?
Cs3 Cs4 Cs7 172.1(18) . 10_554 ?
Cs3 Cs4 Cs7 8.4(9) 10_554 10_554 ?
Cs3 Cs4 O1 84.7(8) 10_554 28_656 ?
Cs3 Cs4 O1 94.9(13) . 28_656 ?
Cs3 Cs4 O1 94.9(13) . 19_566 ?
Cs3 Cs4 O1 84.7(8) 10_554 19_566 ?
Cs4 Cs4 Cs1 1.8(3) 10_554 10_554 ?
Cs4 Cs4 Cs1 177.5(4) 10_554 . ?
Cs4 Cs4 Cs2 1.7(4) 10_554 10_554 ?
Cs4 Cs4 Cs2 177.6(6) 10_554 . ?
Cs4 Cs4 Cs3 179.7(17) 10_554 . ?
Cs4 Cs4 Cs3 0.2(9) 10_554 10_554 ?
Cs4 Cs4 Cs5 165.6(5) 10_554 10_564 ?
Cs4 Cs4 Cs7 8.2(4) 10_554 10_554 ?
Cs4 Cs4 Cs7 169.8(5) 10_554 . ?
Cs4 Cs4 O1 84.8(2) 10_554 19_566 ?
Cs4 Cs4 O1 84.8(2) 10_554 28_656 ?
Cs7 Cs4 Cs5 157.4(7) 10_554 10_564 ?
Cs7 Cs4 Cs5 4.2(5) . 10_564 ?
Cs7 Cs4 Cs7 161.6(8) . 10_554 ?
Cs7 Cs4 O1 91.2(4) 10_554 19_566 ?
Cs7 Cs4 O1 91.2(4) 10_554 28_656 ?
Cs7 Cs4 O1 103.0(5) . 19_566 ?
Cs7 Cs4 O1 103.0(5) . 28_656 ?
O1 Cs4 Cs5 106.2(4) 28_656 10_564 ?
O1 Cs4 Cs5 106.2(4) 19_566 10_564 ?
O1 Cs4 O1 78.5(3) 28_656 19_566 ?
Cs1 Cs5 Cs1 130.5(11) 10_564 . ?
Cs1 Cs5 Cs2 5.1(3) 10_564 10_564 ?
Cs1 Cs5 Cs2 132.5(11) 10_564 . ?
Cs1 Cs5 Cs2 2.00(18) . . ?
Cs1 Cs5 Cs3 12.8(5) 10_564 10_564 ?
Cs1 Cs5 Cs5 95.5(7) . 19_576 ?
Cs1 Cs5 Cs5 132.7(11) 10_564 19_576 ?
Cs1 Cs5 Cs5 95.5(7) . 28_656 ?
Cs1 Cs5 Cs5 132.7(11) 10_564 28_656 ?
Cs1 Cs5 Cs6 134.5(11) 10_564 19_576 ?
Cs1 Cs5 Cs7 138.0(13) 10_564 . ?
Cs2 Cs5 Cs1 135.6(11) 10_564 . ?
Cs2 Cs5 Cs2 137.6(11) 10_564 . ?
Cs2 Cs5 Cs3 7.7(4) 10_564 10_564 ?
Cs2 Cs5 Cs5 127.8(10) 10_564 19_576 ?
Cs2 Cs5 Cs5 127.8(10) 10_564 28_656 ?
Cs2 Cs5 Cs6 129.4(10) 10_564 19_576 ?
Cs2 Cs5 Cs7 143.1(13) 10_564 . ?
Cs3 Cs5 Cs1 143.3(10) 10_564 . ?
Cs3 Cs5 Cs2 145.3(10) 10_564 . ?
Cs3 Cs5 Cs5 120.3(9) 10_564 19_576 ?
Cs3 Cs5 Cs5 120.3(9) 10_564 28_656 ?
Cs3 Cs5 Cs6 121.7(9) 10_564 19_576 ?
Cs5 Cs5 Cs1 148.5(8) 10_564 10_564 ?
Cs5 Cs5 Cs1 18.0(5) 10_564 . ?
Cs5 Cs5 Cs2 93.5(6) 28_656 . ?
Cs5 Cs5 Cs2 16.0(5) 10_564 . ?
Cs5 Cs5 Cs2 93.5(6) 19_576 . ?
Cs5 Cs5 Cs2 153.6(7) 10_564 10_564 ?
Cs5 Cs5 Cs3 161.3(6) 10_564 10_564 ?
Cs5 Cs5 Cs5 77.9(4) 10_564 28_656 ?
Cs5 Cs5 Cs5 77.9(4) 10_564 19_576 ?
Cs5 Cs5 Cs5 24.2(9) 28_656 19_576 ?
Cs5 Cs5 Cs6 77.0(5) 10_564 19_576 ?
Cs5 Cs5 Cs7 10.5(7) 10_564 . ?
Cs6 Cs5 Cs1 161(4) . 10_564 ?
Cs6 Cs5 Cs1 30(3) . . ?
Cs6 Cs5 Cs1 95.0(7) 19_576 . ?
Cs6 Cs5 Cs2 28(3) . . ?
Cs6 Cs5 Cs2 166(4) . 10_564 ?
Cs6 Cs5 Cs2 93.0(7) 19_576 . ?
Cs6 Cs5 Cs3 174(3) . 10_564 ?
Cs6 Cs5 Cs5 12(3) . 10_564 ?
Cs6 Cs5 Cs5 66(3) . 19_576 ?
Cs6 Cs5 Cs5 66(3) . 28_656 ?
Cs6 Cs5 Cs5 12.1(4) 19_576 28_656 ?
Cs6 Cs5 Cs5 12.1(4) 19_576 19_576 ?
Cs6 Cs5 Cs6 65(3) . 19_576 ?
Cs6 Cs5 Cs7 23(3) . . ?
Cs6 Cs5 Cs7 167(4) . 10_564 ?
Cs7 Cs5 Cs1 6.6(11) 10_564 10_564 ?
Cs7 Cs5 Cs1 7.5(4) . . ?
Cs7 Cs5 Cs1 137.1(19) 10_564 . ?
Cs7 Cs5 Cs2 1.5(11) 10_564 10_564 ?
Cs7 Cs5 Cs2 5.5(4) . . ?
Cs7 Cs5 Cs2 139.1(19) 10_564 . ?
Cs7 Cs5 Cs3 6.2(13) 10_564 10_564 ?
Cs7 Cs5 Cs3 150.8(12) . 10_564 ?
Cs7 Cs5 Cs5 155.1(16) 10_564 10_564 ?
Cs7 Cs5 Cs5 126.3(18) 10_564 28_656 ?
Cs7 Cs5 Cs5 126.3(18) 10_564 19_576 ?
Cs7 Cs5 Cs5 88.2(7) . 19_576 ?
Cs7 Cs5 Cs5 88.2(7) . 28_656 ?
Cs7 Cs5 Cs6 87.5(8) . 19_576 ?
Cs7 Cs5 Cs6 127.9(19) 10_564 19_576 ?
Cs7 Cs5 Cs7 145(2) 10_564 . ?
Cs1 Cs6 Cs1 127.7(7) . 10_564 ?
Cs1 Cs6 Cs2 3.3(2) 10_564 10_564 ?
Cs1 Cs6 Cs2 131.0(6) . 10_564 ?
Cs1 Cs6 Cs2 3.3(2) . . ?
Cs1 Cs6 Cs2 131.0(6) 10_564 . ?
Cs1 Cs6 Cs3 136.4(6) . 10_564 ?
Cs1 Cs6 Cs3 8.8(3) 10_564 10_564 ?
Cs1 Cs6 Cs5 115.4(3) . 28_656 ?
Cs1 Cs6 Cs5 115.4(3) 10_564 19_576 ?
Cs1 Cs6 Cs5 115.4(3) . 19_576 ?
Cs1 Cs6 Cs5 115.4(3) 10_564 28_656 ?
Cs1 Cs6 Cs6 116.2(3) 10_564 19_576 ?
Cs1 Cs6 Cs6 116.2(3) . 19_576 ?
Cs2 Cs6 Cs2 134.3(7) . 10_564 ?
Cs2 Cs6 Cs3 139.8(7) . 10_564 ?
Cs2 Cs6 Cs3 5.5(3) 10_564 10_564 ?
Cs2 Cs6 Cs5 112.2(4) . 28_656 ?
Cs2 Cs6 Cs5 112.2(4) 10_564 19_576 ?
Cs2 Cs6 Cs5 112.2(3) . 19_576 ?
Cs2 Cs6 Cs5 112.2(3) 10_564 28_656 ?
Cs2 Cs6 Cs6 112.9(3) 10_564 19_576 ?
Cs2 Cs6 Cs6 112.9(3) . 19_576 ?
Cs5 Cs6 Cs1 142(3) . . ?
Cs5 Cs6 Cs1 14(3) . 10_564 ?
Cs5 Cs6 Cs1 14(3) 10_564 . ?
Cs5 Cs6 Cs1 142(3) 10_564 10_564 ?
Cs5 Cs6 Cs2 145(3) 10_564 10_564 ?
Cs5 Cs6 Cs2 11(3) . 10_564 ?
Cs5 Cs6 Cs2 11(3) 10_564 . ?
Cs5 Cs6 Cs2 145(3) . . ?
Cs5 Cs6 Cs3 150(3) 10_564 10_564 ?
Cs5 Cs6 Cs3 5(3) . 10_564 ?
Cs5 Cs6 Cs3 106.9(4) 28_656 10_564 ?
Cs5 Cs6 Cs3 106.9(4) 19_576 10_564 ?
Cs5 Cs6 Cs5 102(3) . 28_656 ?
Cs5 Cs6 Cs5 102(3) 10_564 19_576 ?
Cs5 Cs6 Cs5 102(3) . 19_576 ?
Cs5 Cs6 Cs5 155(6) . 10_564 ?
Cs5 Cs6 Cs5 102(3) 10_564 28_656 ?
Cs5 Cs6 Cs5 25.9(9) 28_656 19_576 ?
Cs5 Cs6 Cs6 102(3) 10_564 19_576 ?
Cs5 Cs6 Cs6 102(3) . 19_576 ?
Cs5 Cs6 Cs7 148(3) . . ?
Cs5 Cs6 Cs7 7(3) . 10_564 ?
Cs5 Cs6 Cs7 148(3) 10_564 10_564 ?
Cs5 Cs6 Cs7 7(3) 10_564 . ?
Cs6 Cs6 Cs3 107.4(4) 19_576 10_564 ?
Cs6 Cs6 Cs5 13.0(5) 19_576 19_576 ?
Cs6 Cs6 Cs5 13.0(5) 19_576 28_656 ?
Cs7 Cs6 Cs1 134.1(10) 10_564 . ?
Cs7 Cs6 Cs1 134.1(10) . 10_564 ?
Cs7 Cs6 Cs1 6.5(6) 10_564 10_564 ?
Cs7 Cs6 Cs1 6.5(6) . . ?
Cs7 Cs6 Cs2 137.5(10) . 10_564 ?
Cs7 Cs6 Cs2 137.5(10) 10_564 . ?
Cs7 Cs6 Cs2 3.2(6) 10_564 10_564 ?
Cs7 Cs6 Cs2 3.2(6) . . ?
Cs7 Cs6 Cs3 142.9(10) . 10_564 ?
Cs7 Cs6 Cs3 2.3(7) 10_564 10_564 ?
Cs7 Cs6 Cs5 109.2(7) . 19_576 ?
Cs7 Cs6 Cs5 109.2(7) 10_564 28_656 ?
Cs7 Cs6 Cs5 109.2(7) 10_564 19_576 ?
Cs7 Cs6 Cs5 109.2(7) . 28_656 ?
Cs7 Cs6 Cs6 109.7(7) . 19_576 ?
Cs7 Cs6 Cs6 109.7(7) 10_564 19_576 ?
Cs7 Cs6 Cs7 140.6(15) . 10_564 ?
Cs1 Cs7 Cs2 11.9(7) . . ?
Cs1 Cs7 Cs3 24.6(9) . . ?
Cs1 Cs7 Cs4 31.5(9) . 10_554 ?
Cs1 Cs7 Cs4 29.5(8) . . ?
Cs1 Cs7 Cs5 150.8(15) . . ?
Cs1 Cs7 Cs5 165(2) . 10_564 ?
Cs1 Cs7 Cs6 160.0(16) . . ?
Cs1 Cs7 Cs7 140.3(10) . 10_564 ?
Cs1 Cs7 O1 85.8(9) . 3_655 ?
Cs1 Cs7 O3 98.7(8) . 28_656 ?
Cs1 Cs7 O3 98.7(8) . . ?
Cs2 Cs7 Cs3 12.7(8) . . ?
Cs2 Cs7 Cs4 17.6(7) . . ?
Cs2 Cs7 Cs4 19.6(8) . 10_554 ?
Cs2 Cs7 Cs5 162.7(14) . . ?
Cs2 Cs7 Cs6 171.9(15) . . ?
Cs2 Cs7 Cs7 152.2(9) . 10_564 ?
Cs2 Cs7 O1 95.2(9) . 3_655 ?
Cs2 Cs7 O3 91.0(7) . . ?
Cs2 Cs7 O3 91.0(7) . 28_656 ?
Cs3 Cs7 Cs4 7.0(7) . 10_554 ?
Cs3 Cs7 Cs4 4.9(7) . . ?
Cs3 Cs7 Cs5 175.4(12) . . ?
Cs3 Cs7 Cs7 164.9(8) . 10_564 ?
Cs3 Cs7 O1 105.2(8) . 3_655 ?
Cs3 Cs7 O3 82.7(5) . 28_656 ?
Cs3 Cs7 O3 82.7(5) . . ?
Cs4 Cs7 Cs4 2.03(13) . 10_554 ?
Cs4 Cs7 Cs7 171.8(4) 10_554 10_564 ?
Cs4 Cs7 Cs7 169.8(5) . 10_564 ?
Cs4 Cs7 O1 108.9(6) . 3_655 ?
Cs4 Cs7 O1 110.5(5) 10_554 3_655 ?
Cs4 Cs7 O3 78.3(3) 10_554 . ?
Cs4 Cs7 O3 79.6(4) . . ?
Cs4 Cs7 O3 78.3(3) 10_554 28_656 ?
Cs4 Cs7 O3 79.6(4) . 28_656 ?
Cs5 Cs7 Cs2 177(2) 10_564 . ?
Cs5 Cs7 Cs3 170(2) 10_564 . ?
Cs5 Cs7 Cs4 177.7(9) . 10_554 ?
Cs5 Cs7 Cs4 163.3(18) 10_564 10_554 ?
Cs5 Cs7 Cs4 179.7(10) . . ?
Cs5 Cs7 Cs4 165.3(18) 10_564 . ?
Cs5 Cs7 Cs5 14.4(11) 10_564 . ?
Cs5 Cs7 Cs6 5.2(18) 10_564 . ?
Cs5 Cs7 Cs7 10.5(7) . 10_564 ?
Cs5 Cs7 Cs7 24.9(16) 10_564 10_564 ?
Cs5 Cs7 O1 71.3(6) . 3_655 ?
Cs5 Cs7 O1 82.4(13) 10_564 3_655 ?
Cs5 Cs7 O3 91.0(11) 10_564 . ?
Cs5 Cs7 O3 100.3(6) . 28_656 ?
Cs5 Cs7 O3 91.0(11) 10_564 28_656 ?
Cs5 Cs7 O3 100.3(6) . . ?
Cs6 Cs7 Cs3 175.4(13) . . ?
Cs6 Cs7 Cs4 170.5(11) . . ?
Cs6 Cs7 Cs4 168.5(10) . 10_554 ?
Cs6 Cs7 Cs5 9.2(10) . . ?
Cs6 Cs7 Cs7 19.7(7) . 10_564 ?
Cs6 Cs7 O1 78.4(6) . 3_655 ?
Cs6 Cs7 O3 94.3(7) . 28_656 ?
Cs6 Cs7 O3 94.3(7) . . ?
Cs7 Cs7 O1 63.4(3) 10_564 3_655 ?
Cs7 Cs7 O3 106.8(3) 10_564 28_656 ?
Cs7 Cs7 O3 106.8(3) 10_564 . ?
O3 Cs7 O1 92.59(10) 28_656 3_655 ?
O3 Cs7 O1 167.1(4) . 3_655 ?
O3 Cs7 O3 98.7(4) 28_656 . ?
U1 Ga2 Cs2 114.31(8) 25 . ?
U1 Ga2 Cs3 115.31(16) 25 10_554 ?
U1 Ga2 Cs3 115.31(16) 25 . ?
U1 Ga2 Cs4 116.20(8) 25 10_554 ?
U1 Ga2 Cs4 116.20(8) 25 . ?
U1 Ga2 Cs7 76.37(18) 25 19_566 ?
U1 Ga2 Cs7 76.37(18) 25 19_576 ?
Cs3 Ga2 Cs2 39.0(5) 10_554 . ?
Cs3 Ga2 Cs2 8.4(3) . . ?
Cs3 Ga2 Cs3 30.6(7) 10_554 . ?
Cs3 Ga2 Cs7 111.9(4) . 19_566 ?
Cs3 Ga2 Cs7 81.9(5) 10_554 19_566 ?
Cs3 Ga2 Cs7 111.9(4) 10_554 19_576 ?
Cs3 Ga2 Cs7 81.9(5) . 19_576 ?
Cs4 Ga2 Cs2 28.1(3) 10_554 . ?
Cs4 Ga2 Cs2 19.4(3) . . ?
Cs4 Ga2 Cs3 19.7(4) 10_554 . ?
Cs4 Ga2 Cs3 10.9(4) . . ?
Cs4 Ga2 Cs3 19.7(4) . 10_554 ?
Cs4 Ga2 Cs3 10.9(4) 10_554 10_554 ?
Cs4 Ga2 Cs4 8.7(4) . 10_554 ?
Cs4 Ga2 Cs7 101.2(3) . 19_566 ?
Cs4 Ga2 Cs7 101.2(3) 10_554 19_576 ?
Cs4 Ga2 Cs7 92.6(3) 10_554 19_566 ?
Cs4 Ga2 Cs7 92.6(3) . 19_576 ?
Cs7 Ga2 Cs2 73.8(4) 19_576 . ?
Cs7 Ga2 Cs2 120.2(3) 19_566 . ?
Cs7 Ga2 Cs7 152.7(4) 19_566 19_576 ?
O2 Ga2 U1 45.21(12) . 25 ?
O2 Ga2 Cs2 150.5(2) . . ?
O2 Ga2 Cs3 156.2(3) . . ?
O2 Ga2 Cs3 156.2(3) . 10_554 ?
O2 Ga2 Cs4 161.00(15) . . ?
O2 Ga2 Cs4 161.00(15) . 10_554 ?
O2 Ga2 Cs7 79.7(2) . 19_576 ?
O2 Ga2 Cs7 79.7(2) . 19_566 ?
O3 Ga2 U1 122.65(13) . 25 ?
O3 Ga2 U1 122.65(12) 19_566 25 ?
O3 Ga2 Cs2 93.0(2) 19_566 . ?
O3 Ga2 Cs2 51.50(18) . . ?
O3 Ga2 Cs3 85.6(4) . 10_554 ?
O3 Ga2 Cs3 85.6(4) 19_566 . ?
O3 Ga2 Cs3 58.8(3) . . ?
O3 Ga2 Cs3 58.8(3) 19_566 10_554 ?
O3 Ga2 Cs4 75.93(19) . 10_554 ?
O3 Ga2 Cs4 68.23(19) 19_566 10_554 ?
O3 Ga2 Cs4 75.93(19) 19_566 . ?
O3 Ga2 Cs4 68.23(19) . . ?
O3 Ga2 Cs7 160.6(2) . 19_566 ?
O3 Ga2 Cs7 160.6(2) 19_566 19_576 ?
O3 Ga2 Cs7 46.7(2) . 19_576 ?
O3 Ga2 Cs7 46.7(2) 19_566 19_566 ?
O3 Ga2 O2 115.76(5) . . ?
O3 Ga2 O2 115.76(5) 19_566 . ?
O3 Ga2 O3 114.0(2) . 19_566 ?
O3 Ga2 O4 108.71(17) 19_566 . ?
O3 Ga2 O4 108.71(17) . . ?
O4 Ga2 U1 45.81(18) . 25 ?
O4 Ga2 Cs2 72.58(17) . . ?
O4 Ga2 Cs3 71.2(2) . 10_554 ?
O4 Ga2 Cs3 71.2(2) . . ?
O4 Ga2 Cs4 70.5(2) . . ?
O4 Ga2 Cs4 70.5(2) . 10_554 ?
O4 Ga2 Cs7 81.3(2) . 19_576 ?
O4 Ga2 Cs7 81.3(2) . 19_566 ?
O4 Ga2 O2 91.0(2) . . ?
U1 O1 Cs1 127.73(13) . 4_464 ?
U1 O1 Cs1 127.73(13) . 11_544 ?
U1 O1 Cs3 126.7(3) . 28_556 ?
U1 O1 Cs3 126.7(3) . 19_576 ?
U1 O1 Cs4 128.7(2) . 28_556 ?
U1 O1 Cs4 128.7(2) . 19_576 ?
U1 O1 Cs5 128.2(3) . 11_544 ?
U1 O1 Cs5 128.2(3) . 4_464 ?
U1 O1 Cs6 127.6(2) . 11_544 ?
U1 O1 Cs7 128.3(2) . 4_464 ?
U1 O1 Cs7 128.3(2) . 11_544 ?
Cs1 O1 Cs1 76.18(14) 11_544 4_464 ?
Cs1 O1 Cs3 101.0(3) 4_464 19_576 ?
Cs1 O1 Cs3 101.0(3) 11_544 28_556 ?
Cs1 O1 Cs3 79.1(3) 11_544 19_576 ?
Cs1 O1 Cs3 79.1(3) 4_464 28_556 ?
Cs1 O1 Cs6 40.04(9) 4_464 11_544 ?
Cs1 O1 Cs6 40.04(9) 11_544 11_544 ?
Cs3 O1 Cs3 35.9(7) 19_576 28_556 ?
Cs3 O1 Cs6 102.8(3) 28_556 11_544 ?
Cs3 O1 Cs6 102.8(3) 19_576 11_544 ?
Cs4 O1 Cs1 93.2(2) 28_556 11_544 ?
Cs4 O1 Cs1 86.9(2) 28_556 4_464 ?
Cs4 O1 Cs1 86.9(2) 19_576 11_544 ?
Cs4 O1 Cs1 93.2(2) 19_576 4_464 ?
Cs4 O1 Cs3 23.1(5) 28_556 19_576 ?
Cs4 O1 Cs3 12.8(4) 19_576 19_576 ?
Cs4 O1 Cs3 12.8(4) 28_556 28_556 ?
Cs4 O1 Cs3 23.1(5) 19_576 28_556 ?
Cs4 O1 Cs4 10.3(5) 19_576 28_556 ?
Cs4 O1 Cs5 100.8(3) 19_576 4_464 ?
Cs4 O1 Cs5 102.8(3) 19_576 11_544 ?
Cs4 O1 Cs5 100.8(3) 28_556 11_544 ?
Cs4 O1 Cs5 102.8(3) 28_556 4_464 ?
Cs4 O1 Cs6 103.4(2) 28_556 11_544 ?
Cs4 O1 Cs6 103.4(2) 19_576 11_544 ?
Cs4 O1 Cs7 98.8(3) 28_556 11_544 ?
Cs4 O1 Cs7 94.2(3) 28_556 4_464 ?
Cs4 O1 Cs7 98.8(3) 19_576 4_464 ?
Cs4 O1 Cs7 94.2(3) 19_576 11_544 ?
Cs5 O1 Cs1 29.1(4) 11_544 4_464 ?
Cs5 O1 Cs1 50.4(4) 4_464 4_464 ?
Cs5 O1 Cs1 50.4(4) 11_544 11_544 ?
Cs5 O1 Cs1 29.1(4) 4_464 11_544 ?
Cs5 O1 Cs3 97.8(4) 11_544 28_556 ?
Cs5 O1 Cs3 104.7(3) 11_544 19_576 ?
Cs5 O1 Cs3 97.8(4) 4_464 19_576 ?
Cs5 O1 Cs3 104.7(3) 4_464 28_556 ?
Cs5 O1 Cs5 22.1(8) 11_544 4_464 ?
Cs5 O1 Cs6 11.1(4) 4_464 11_544 ?
Cs5 O1 Cs6 11.1(4) 11_544 11_544 ?
Cs7 O1 Cs1 13.0(3) 4_464 4_464 ?
Cs7 O1 Cs1 13.0(3) 11_544 11_544 ?
Cs7 O1 Cs1 65.0(3) 4_464 11_544 ?
Cs7 O1 Cs1 65.0(3) 11_544 4_464 ?
Cs7 O1 Cs3 88.3(3) 4_464 28_556 ?
Cs7 O1 Cs3 104.2(3) 11_544 28_556 ?
Cs7 O1 Cs3 88.3(3) 11_544 19_576 ?
Cs7 O1 Cs3 104.2(3) 4_464 19_576 ?
Cs7 O1 Cs5 37.9(6) 4_464 4_464 ?
Cs7 O1 Cs5 16.1(4) 11_544 4_464 ?
Cs7 O1 Cs5 37.9(6) 11_544 11_544 ?
Cs7 O1 Cs5 16.1(4) 4_464 11_544 ?
Cs7 O1 Cs6 27.2(3) 4_464 11_544 ?
Cs7 O1 Cs6 27.2(3) 11_544 11_544 ?
Cs7 O1 Cs7 53.1(6) 4_464 11_544 ?
U1 O2 U1 109.16(15) . 25 ?
U1 O2 Cs1 89.41(7) 25 19_566 ?
U1 O2 Cs1 89.41(7) 25 19_576 ?
U1 O2 Cs1 99.45(7) . 19_576 ?
U1 O2 Cs1 99.45(7) . 19_566 ?
U1 O2 Cs2 96.7(2) . 19_576 ?
U1 O2 Cs2 93.4(2) 25 19_576 ?
U1 O2 Cs2 93.4(2) 25 19_566 ?
U1 O2 Cs2 96.7(2) . 19_566 ?
U1 O2 Cs3 101.9(3) 25 19_576 ?
U1 O2 Cs3 101.9(3) 25 19_566 ?
U1 O2 Cs3 91.0(3) . 19_566 ?
U1 O2 Cs3 91.0(3) . 19_576 ?
Cs1 O2 Cs1 160.36(14) 19_576 19_566 ?
Cs1 O2 Cs3 161.3(2) 19_576 19_566 ?
Cs1 O2 Cs3 161.3(2) 19_566 19_576 ?
Cs1 O2 Cs3 13.2(3) 19_576 19_576 ?
Cs1 O2 Cs3 13.2(3) 19_566 19_566 ?
Cs2 O2 Cs1 4.2(2) 19_576 19_576 ?
Cs2 O2 Cs1 4.2(2) 19_566 19_566 ?
Cs2 O2 Cs1 161.72(15) 19_566 19_576 ?
Cs2 O2 Cs1 161.72(15) 19_576 19_566 ?
Cs2 O2 Cs2 162.1(2) 19_576 19_566 ?
Cs2 O2 Cs3 159.7(3) 19_576 19_566 ?
Cs2 O2 Cs3 9.0(3) 19_566 19_566 ?
Cs2 O2 Cs3 159.7(3) 19_566 19_576 ?
Cs2 O2 Cs3 9.0(3) 19_576 19_576 ?
Cs3 O2 Cs3 154.1(5) 19_576 19_566 ?
Ga2 O2 U1 101.66(16) . 25 ?
Ga2 O2 U1 149.2(2) . . ?
Ga2 O2 Cs1 80.52(7) . 19_566 ?
Ga2 O2 Cs1 80.52(7) . 19_576 ?
Ga2 O2 Cs2 81.22(13) . 19_566 ?
Ga2 O2 Cs2 81.22(13) . 19_576 ?
Ga2 O2 Cs3 82.6(3) . 19_576 ?
Ga2 O2 Cs3 82.6(3) . 19_566 ?
Cs1 O3 Cs1 109.88(19) . 19_576 ?
Cs2 O3 Cs1 113.9(3) 19_576 . ?
Cs2 O3 Cs1 113.9(3) . 19_576 ?
Cs2 O3 Cs1 5.2(3) 19_576 19_576 ?
Cs2 O3 Cs1 5.2(3) . . ?
Cs2 O3 Cs2 118.1(5) . 19_576 ?
Cs2 O3 Cs3 126.5(5) . 19_576 ?
Cs2 O3 Cs3 11.2(3) 19_576 19_576 ?
Cs2 O3 Cs3 11.2(3) . . ?
Cs2 O3 Cs3 126.5(5) 19_576 . ?
Cs3 O3 Cs1 16.3(4) . . ?
Cs3 O3 Cs1 121.9(4) 19_576 . ?
Cs3 O3 Cs1 16.3(4) 19_576 19_576 ?
Cs3 O3 Cs1 121.9(4) . 19_576 ?
Cs3 O3 Cs3 136.0(8) 19_576 . ?
Cs5 O3 Cs1 29.1(4) 28_656 19_576 ?
Cs5 O3 Cs1 81.6(4) 10_564 19_576 ?
Cs5 O3 Cs1 29.1(4) 10_564 . ?
Cs5 O3 Cs1 81.6(4) 28_656 . ?
Cs5 O3 Cs2 85.2(5) 10_564 19_576 ?
Cs5 O3 Cs2 85.2(5) 28_656 . ?
Cs5 O3 Cs2 33.9(5) 10_564 . ?
Cs5 O3 Cs2 33.9(5) 28_656 19_576 ?
Cs5 O3 Cs3 92.9(6) 10_564 19_576 ?
Cs5 O3 Cs3 92.9(6) 28_656 . ?
Cs5 O3 Cs3 44.3(6) 28_656 19_576 ?
Cs5 O3 Cs3 44.3(6) 10_564 . ?
Cs5 O3 Cs5 54.7(8) 10_564 28_656 ?
Cs7 O3 Cs1 97.1(4) . 19_576 ?
Cs7 O3 Cs1 12.9(3) 19_576 19_576 ?
Cs7 O3 Cs1 97.1(4) 19_576 . ?
Cs7 O3 Cs1 12.9(3) . . ?
Cs7 O3 Cs2 17.5(4) . . ?
Cs7 O3 Cs2 101.0(5) . 19_576 ?
Cs7 O3 Cs2 101.0(5) 19_576 . ?
Cs7 O3 Cs2 17.5(4) 19_576 19_576 ?
Cs7 O3 Cs3 28.0(5) 19_576 19_576 ?
Cs7 O3 Cs3 28.0(5) . . ?
Cs7 O3 Cs3 109.1(6) 19_576 . ?
Cs7 O3 Cs3 109.1(6) . 19_576 ?
Cs7 O3 Cs5 69.1(6) . 28_656 ?
Cs7 O3 Cs5 16.4(4) 19_576 28_656 ?
Cs7 O3 Cs5 69.1(6) 19_576 10_564 ?
Cs7 O3 Cs5 16.4(4) . 10_564 ?
Cs7 O3 Cs7 84.4(7) . 19_576 ?
Ga2 O3 Cs1 105.39(7) 28_556 19_576 ?
Ga2 O3 Cs1 105.39(7) . . ?
Ga2 O3 Cs1 103.43(6) . 19_576 ?
Ga2 O3 Cs1 103.43(6) 28_556 . ?
Ga2 O3 Cs2 104.90(11) . 19_576 ?
Ga2 O3 Cs2 100.9(2) . . ?
Ga2 O3 Cs2 100.9(2) 28_556 19_576 ?
Ga2 O3 Cs2 104.90(11) 28_556 . ?
Ga2 O3 Cs3 107.9(2) . 19_576 ?
Ga2 O3 Cs3 91.0(3) . . ?
Ga2 O3 Cs3 107.9(2) 28_556 . ?
Ga2 O3 Cs3 91.0(3) 28_556 19_576 ?
Ga2 O3 Cs5 105.6(3) 28_556 10_564 ?
Ga2 O3 Cs5 120.0(3) . 10_564 ?
Ga2 O3 Cs5 105.6(3) . 28_656 ?
Ga2 O3 Cs5 120.0(3) 28_556 28_656 ?
Ga2 O3 Cs7 106.3(2) 28_556 . ?
Ga2 O3 Cs7 111.1(2) . . ?
Ga2 O3 Cs7 111.1(2) 28_556 19_576 ?
Ga2 O3 Cs7 106.3(2) . 19_576 ?
Ga2 O3 Ga2 128.7(3) . 28_556 ?
U1 O4 Cs2 155.5(2) 25 . ?
U1 O4 Cs2 155.5(2) 25 10_554 ?
U1 O4 Cs3 164.1(4) 25 10_554 ?
U1 O4 Cs3 164.1(4) 25 . ?
U1 O4 Cs4 175.5(2) 25 10_554 ?
U1 O4 Cs4 175.5(2) 25 . ?
U1 O4 Cs5 89.0(3) 25 28_646 ?
U1 O4 Cs6 90.9(2) 25 19_576 ?
U1 O4 Cs6 90.9(2) 25 19_566 ?
Cs2 O4 Cs2 49.0(4) . 10_554 ?
Cs2 O4 Cs5 66.9(4) 10_554 28_646 ?
Cs2 O4 Cs5 115.2(4) . 28_646 ?
Cs3 O4 Cs2 40.4(5) . 10_554 ?
Cs3 O4 Cs2 8.6(3) . . ?
Cs3 O4 Cs2 40.4(5) 10_554 . ?
Cs3 O4 Cs2 8.6(3) 10_554 10_554 ?
Cs3 O4 Cs3 31.8(8) 10_554 . ?
Cs3 O4 Cs5 106.7(5) . 28_646 ?
Cs3 O4 Cs5 75.4(5) 10_554 28_646 ?
Cs3 O4 Cs6 105.0(4) . 19_566 ?
Cs3 O4 Cs6 73.2(4) . 19_576 ?
Cs3 O4 Cs6 105.0(4) 10_554 19_576 ?
Cs3 O4 Cs6 73.2(4) 10_554 19_566 ?
Cs4 O4 Cs2 20.0(3) . . ?
Cs4 O4 Cs2 20.0(3) 10_554 10_554 ?
Cs4 O4 Cs2 29.0(3) 10_554 . ?
Cs4 O4 Cs2 29.0(3) . 10_554 ?
Cs4 O4 Cs3 20.4(5) 10_554 . ?
Cs4 O4 Cs3 11.3(4) . . ?
Cs4 O4 Cs3 20.4(5) . 10_554 ?
Cs4 O4 Cs3 11.3(4) 10_554 10_554 ?
Cs4 O4 Cs4 9.1(4) . 10_554 ?
Cs4 O4 Cs5 95.5(4) . 28_646 ?
Cs4 O4 Cs5 86.6(4) 10_554 28_646 ?
Cs4 O4 Cs6 84.6(3) 10_554 19_566 ?
Cs4 O4 Cs6 84.6(3) . 19_576 ?
Cs4 O4 Cs6 93.6(3) . 19_566 ?
Cs4 O4 Cs6 93.6(3) 10_554 19_576 ?
Cs6 O4 Cs2 113.6(3) 19_576 10_554 ?
Cs6 O4 Cs2 113.6(3) 19_566 . ?
Cs6 O4 Cs2 64.6(3) 19_576 . ?
Cs6 O4 Cs2 64.6(3) 19_566 10_554 ?
Cs6 O4 Cs5 171.1(3) 19_576 28_646 ?
Cs6 O4 Cs5 9.1(3) 19_566 28_646 ?
Cs6 O4 Cs6 178.2(5) 19_576 19_566 ?
Ga2 O4 U1 101.57(18) . 25 ?
Ga2 O4 U1 101.57(18) 10_554 25 ?
Ga2 O4 Cs2 79.48(17) 10_554 10_554 ?
Ga2 O4 Cs2 79.48(17) . 10_554 ?
Ga2 O4 Cs2 79.48(17) 10_554 . ?
Ga2 O4 Cs2 79.48(17) . . ?
Ga2 O4 Cs3 78.88(18) 10_554 10_554 ?
Ga2 O4 Cs3 78.87(18) . . ?
Ga2 O4 Cs3 78.88(18) 10_554 . ?
Ga2 O4 Cs3 78.87(18) . 10_554 ?
Ga2 O4 Cs4 78.46(18) . 10_554 ?
Ga2 O4 Cs4 78.47(18) 10_554 . ?
Ga2 O4 Cs4 78.47(18) 10_554 10_554 ?
Ga2 O4 Cs4 78.46(18) . . ?
Ga2 O4 Cs5 81.5(3) . 28_646 ?
Ga2 O4 Cs5 99.0(3) 10_554 28_646 ?
Ga2 O4 Cs6 89.82(5) 10_554 19_566 ?
Ga2 O4 Cs6 89.82(5) 10_554 19_576 ?
Ga2 O4 Cs6 89.82(5) . 19_576 ?
Ga2 O4 Cs6 89.82(5) . 19_566 ?
Ga2 O4 Ga2 156.9(4) . 10_554 ?


# start Validation Reply Form
_vrf_PLAT976_Cs2UO2Ga2O5         
;
PROBLEM: Check Calcd Resid. Dens.  0.93A   From O1             -1.54 eA-3  
RESPONSE: The residual electron density is relatively small 
and less than 10% of the heaviest atom in the structure, U.
;
_olex2_submission_original_sample_id CAJ1166D
_olex2_submission_special_instructions 'No special instructions were received'


_exptl_crystal_recrystallization_method 'From the Melt'
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_Rb6U5P4O28
_database_code_depnum_ccdc_archive 'CCDC 1984889'
loop_
_audit_author_name
_audit_author_address
'Christian Juillerat'
;University of South Carolina
United States of America
;
_audit_update_record             
;
2020-02-18 deposited with the CCDC.	2020-04-07 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2018/3
_shelx_SHELXL_version_number     2018/3
_chemical_name_systematic        Rb6(UO2)5O2(PO4)4
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         'O28 P4 Rb6 U5'
_chemical_formula_sum            'O28 P4 Rb6 U5'
_chemical_formula_weight         2274.85

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Rb Rb -0.9393 2.9676 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
U U -9.6767 9.6646 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'

_shelx_space_group_comment       
; 
The symmetry employed for this shelxl refinement is uniquely defined 
by the following loop, which should always be used as a source of 
symmetry information in preference to the above space-group names. 
They are only intended as comments. 
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   7.3052(8)
_cell_length_b                   9.0828(10)
_cell_length_c                   11.7254(13)
_cell_angle_alpha                75.857(4)
_cell_angle_beta                 72.834(4)
_cell_angle_gamma                86.974(4)
_cell_volume                     720.65(14)
_cell_formula_units_Z            1
_cell_measurement_temperature    301(2)
_cell_measurement_reflns_used    9416
_cell_measurement_theta_min      2.919
_cell_measurement_theta_max      37.883

_exptl_crystal_description       plate
_exptl_crystal_colour            yellow
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    5.242
_exptl_crystal_F_000             966
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          0.160
_exptl_crystal_size_mid          0.120
_exptl_crystal_size_min          0.040
_exptl_absorpt_coefficient_mu    38.389
_shelx_estimated_absorpt_T_min   0.064
_shelx_estimated_absorpt_T_max   0.309
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_correction_T_min  0.0087
_exptl_absorpt_correction_T_max  0.0625
_exptl_absorpt_process_details   'SADABS Version 2016/2 (Bruker, 2016)'
_diffrn_ambient_temperature      301(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_source                   'microfocus sealed X-ray tube'
_diffrn_measurement_device_type  'Bruker D8 QUEST'
_diffrn_measurement_method       'ω and φ scans'
_diffrn_detector_area_resol_mean 10.4
_diffrn_reflns_number            52660
_diffrn_reflns_av_unetI/netI     0.0284
_diffrn_reflns_av_R_equivalents  0.0499
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_k_min       -15
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_theta_min         2.313
_diffrn_reflns_theta_max         37.883
_diffrn_reflns_theta_full        25.242
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measured_fraction_theta_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 0.996
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 0.996
_diffrn_reflns_point_group_measured_fraction_full 1.000
_reflns_number_total             7778
_reflns_number_gt                7150
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
; 
 Reflections were merged by SHELXL according to the crystal 
 class for the calculation of statistics and refinement. 
  
 _reflns_Friedel_fraction is defined as the number of unique 
 Friedel pairs measured divided by the number that would be 
 possible theoretically, ignoring centric projections and 
 systematic absences. 
;

_computing_data_collection       'Bruker APEX3 v2016.5-0 (Bruker, 2016)'
_computing_cell_refinement       'SAINT Version 8.38a (Bruker, 2016)'
_computing_data_reduction        'SAINT Version 8.38a (Bruker, 2016)'
_computing_structure_solution    'SHELXT 2018/2 (Sheldrick, 2018)'
_computing_structure_refinement  'SHELXL-2018/3 (Sheldrick, 2018)'
_computing_molecular_graphics    various
_computing_publication_material  various
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0389P)²+2.8536P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   .
_refine_ls_hydrogen_treatment    undef
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_number_reflns         7778
_refine_ls_number_parameters     196
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0314
_refine_ls_R_factor_gt           0.0282
_refine_ls_wR_factor_ref         0.0746
_refine_ls_wR_factor_gt          0.0728
_refine_ls_goodness_of_fit_ref   1.056
_refine_ls_restrained_S_all      1.056
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
U1 U 0.51166(2) 0.61135(2) 0.22491(2) 0.01348(3) Uani 1 1 d . . . . .
U2 U 0.45152(2) -0.01756(2) 0.34399(2) 0.01460(3) Uani 1 1 d . . . . .
U3 U 0.500000 0.000000 0.000000 0.01707(4) Uani 1 2 d S . P . .
Rb1 Rb -0.12620(7) 0.31214(5) 0.02967(5) 0.02710(8) Uani 1 1 d . . . . .
Rb2 Rb -0.06513(7) 0.37821(6) 0.37724(5) 0.02811(8) Uani 1 1 d . . . . .
Rb3 Rb -0.00602(7) 0.13663(6) 0.73483(5) 0.03138(10) Uani 1 1 d . . . . .
P1 P 0.39247(15) 0.30537(11) 0.49561(9) 0.01519(15) Uani 1 1 d . . . . .
P2 P 0.35885(15) 0.31264(11) 0.11487(9) 0.01452(15) Uani 1 1 d . . . . .
O1 O 0.5302(5) 0.4090(4) 0.3842(3) 0.0210(5) Uani 1 1 d . . . . .
O2 O 0.4163(5) 0.1372(3) 0.4802(3) 0.0209(5) Uani 1 1 d . . . . .
O3 O 0.4673(6) 0.2834(3) 0.6106(3) 0.0223(6) Uani 1 1 d . . . . .
O4 O 0.1892(5) 0.3533(4) 0.5224(3) 0.0244(6) Uani 1 1 d . . . . .
O5 O 0.5010(5) 0.4110(4) 0.1401(3) 0.0196(5) Uani 1 1 d . . . . .
O6 O 0.3320(6) 0.1570(4) 0.2102(4) 0.0297(7) Uani 1 1 d . . . . .
O7 O 0.4647(5) 0.2682(4) -0.0097(3) 0.0213(5) Uani 1 1 d . . . . .
O8 O 0.1703(5) 0.3847(4) 0.1149(3) 0.0229(6) Uani 1 1 d . . . . .
O9 O 0.2111(5) -0.0879(4) 0.4274(3) 0.0240(6) Uani 1 1 d . . . . .
O10 O 0.6908(5) 0.0582(4) 0.2632(3) 0.0243(6) Uani 1 1 d . . . . .
O11 O 0.2476(5) -0.0284(4) 0.0197(3) 0.0249(6) Uani 1 1 d . . . . .
O12 O 0.4652(5) 0.8711(3) 0.1904(3) 0.0203(5) Uani 1 1 d . . . . .
O13 O 0.2545(5) 0.6023(4) 0.2730(3) 0.0233(6) Uani 1 1 d . . . . .
O14 O 0.7713(5) 0.6161(4) 0.1775(3) 0.0230(6) Uani 1 1 d . . . . .


_geom_special_details            
; 
 All esds (except the esd in the dihedral angle between two l.s. planes) 
 are estimated using the full covariance matrix.  The cell esds are taken 
 into account individually in the estimation of esds in distances, angles 
 and torsion angles; correlations between esds in cell parameters are only 
 used when they are defined by crystal symmetry.  An approximate (isotropic) 
 treatment of cell esds is used for estimating esds involving l.s. planes. 
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
U1 O13 1.795(3) . ?
U1 O14 1.812(3) . ?
U1 O5 2.292(3) . ?
U1 O1 2.308(3) . ?
U1 O12 2.318(3) . ?
U1 O3 2.398(3) 2_666 ?
U1 O7 2.451(3) 2_665 ?
U1 U3 3.8697(4) 1_565 ?
U1 U2 3.9095(4) 1_565 ?
U1 Rb3 4.2087(6) 2_566 ?
U1 Rb2 4.2371(6) 1_655 ?
U1 Rb1 4.2815(6) 1_655 ?
U2 O9 1.802(3) . ?
U2 O10 1.804(4) . ?
U2 O12 2.248(3) 1_545 ?
U2 O6 2.277(3) . ?
U2 O2 2.326(3) . ?
U2 O3 2.423(3) 2_656 ?
U2 O2 2.517(3) 2_656 ?
U2 P1 3.1965(10) 2_656 ?
U2 Rb3 3.9052(7) 2_556 ?
U2 U3 3.9074(5) . ?
U2 U2 4.0141(5) 2_656 ?
U3 O11 1.813(4) 2_655 ?
U3 O11 1.813(4) . ?
U3 O12 2.199(3) 2_665 ?
U3 O12 2.199(3) 1_545 ?
U3 O7 2.414(3) . ?
U3 O7 2.414(3) 2_655 ?
U3 Rb3 4.0242(6) 2_556 ?
U3 Rb3 4.0242(6) 1_654 ?
Rb1 O8 2.806(3) . ?
Rb1 O5 2.851(3) 1_455 ?
Rb1 O8 2.917(3) 2_565 ?
Rb1 O14 2.956(3) 2_665 ?
Rb1 O11 3.006(4) 2 ?
Rb1 O10 3.112(4) 1_455 ?
Rb1 O7 3.214(4) 1_455 ?
Rb1 O14 3.541(4) 1_455 ?
Rb1 P2 3.5961(12) 1_455 ?
Rb1 Rb1 3.7784(10) 2_565 ?
Rb1 P2 3.9550(11) 2_565 ?
Rb1 P2 3.9556(12) . ?
Rb2 O4 2.835(4) . ?
Rb2 O1 2.934(4) 1_455 ?
Rb2 O13 2.948(3) . ?
Rb2 O4 2.948(4) 2_566 ?
Rb2 O8 3.037(4) . ?
Rb2 O9 3.040(3) 2_556 ?
Rb2 O14 3.238(3) 1_455 ?
Rb2 P2 3.8063(12) . ?
Rb2 P1 3.8270(13) 1_455 ?
Rb2 P1 3.9325(12) 2_566 ?
Rb2 P1 3.9490(12) . ?
Rb3 O4 2.813(4) . ?
Rb3 O10 2.831(4) 2_656 ?
Rb3 O11 2.858(4) 2_556 ?
Rb3 O9 2.867(4) 2_556 ?
Rb3 O13 2.909(3) 2_566 ?
Rb3 O12 3.207(4) 2_566 ?
Rb3 O14 3.409(4) 2_666 ?
Rb3 O6 3.482(4) 2_556 ?
Rb3 P1 3.4987(12) . ?
Rb3 O3 3.524(4) . ?
Rb3 O2 3.604(4) . ?
P1 O4 1.488(4) . ?
P1 O1 1.526(3) . ?
P1 O3 1.565(3) . ?
P1 O2 1.576(3) . ?
P2 O8 1.493(3) . ?
P2 O5 1.540(3) . ?
P2 O6 1.554(3) . ?
P2 O7 1.576(3) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O13 U1 O14 178.76(15) . . ?
O13 U1 O5 86.87(14) . . ?
O14 U1 O5 92.24(14) . . ?
O13 U1 O1 92.39(14) . . ?
O14 U1 O1 86.58(14) . . ?
O5 U1 O1 79.06(12) . . ?
O13 U1 O12 83.31(14) . . ?
O14 U1 O12 97.92(15) . . ?
O5 U1 O12 140.92(11) . . ?
O1 U1 O12 138.91(11) . . ?
O13 U1 O3 94.36(15) . 2_666 ?
O14 U1 O3 86.02(15) . 2_666 ?
O5 U1 O3 152.38(11) . 2_666 ?
O1 U1 O3 73.32(11) . 2_666 ?
O12 U1 O3 66.36(10) . 2_666 ?
O13 U1 O7 94.11(14) . 2_665 ?
O14 U1 O7 86.52(13) . 2_665 ?
O5 U1 O7 76.11(11) . 2_665 ?
O1 U1 O7 153.91(11) . 2_665 ?
O12 U1 O7 67.05(10) . 2_665 ?
O3 U1 O7 131.14(11) 2_666 2_665 ?
O13 U1 U3 89.82(11) . 1_565 ?
O14 U1 U3 91.32(11) . 1_565 ?
O5 U1 U3 112.54(8) . 1_565 ?
O1 U1 U3 168.31(8) . 1_565 ?
O12 U1 U3 30.16(7) . 1_565 ?
O3 U1 U3 95.07(7) 2_666 1_565 ?
O7 U1 U3 36.99(7) 2_665 1_565 ?
O13 U1 U2 85.17(11) . 1_565 ?
O14 U1 U2 95.82(12) . 1_565 ?
O5 U1 U2 169.26(8) . 1_565 ?
O1 U1 U2 108.44(8) . 1_565 ?
O12 U1 U2 30.57(7) . 1_565 ?
O3 U1 U2 36.02(7) 2_666 1_565 ?
O7 U1 U2 97.27(7) 2_665 1_565 ?
U3 U1 U2 60.300(8) 1_565 1_565 ?
O13 U1 Rb3 34.37(11) . 2_566 ?
O14 U1 Rb3 146.87(12) . 2_566 ?
O5 U1 Rb3 112.52(8) . 2_566 ?
O1 U1 Rb3 118.49(9) . 2_566 ?
O12 U1 Rb3 48.99(9) . 2_566 ?
O3 U1 Rb3 81.61(9) 2_666 2_566 ?
O7 U1 Rb3 78.97(8) 2_665 2_566 ?
U3 U1 Rb3 59.578(9) 1_565 2_566 ?
U2 U1 Rb3 57.365(10) 1_565 2_566 ?
O13 U1 Rb2 133.49(11) . 1_655 ?
O14 U1 Rb2 45.56(11) . 1_655 ?
O5 U1 Rb2 88.12(8) . 1_655 ?
O1 U1 Rb2 41.39(9) . 1_655 ?
O12 U1 Rb2 125.16(8) . 1_655 ?
O3 U1 Rb2 71.08(8) 2_666 1_655 ?
O7 U1 Rb2 129.17(8) 2_665 1_655 ?
U3 U1 Rb2 134.095(9) 1_565 1_655 ?
U2 U1 Rb2 102.592(10) 1_565 1_655 ?
Rb3 U1 Rb2 149.716(11) 2_566 1_655 ?
O13 U1 Rb1 124.90(11) . 1_655 ?
O14 U1 Rb1 54.21(12) . 1_655 ?
O5 U1 Rb1 38.04(8) . 1_655 ?
O1 U1 Rb1 78.58(8) . 1_655 ?
O12 U1 Rb1 136.01(8) . 1_655 ?
O3 U1 Rb1 132.30(9) 2_666 1_655 ?
O7 U1 Rb1 76.98(8) 2_665 1_655 ?
U3 U1 Rb1 109.393(10) 1_565 1_655 ?
U2 U1 Rb1 149.418(8) 1_565 1_655 ?
Rb3 U1 Rb1 146.084(12) 2_566 1_655 ?
Rb2 U1 Rb1 62.382(12) 1_655 1_655 ?
O9 U2 O10 177.99(16) . . ?
O9 U2 O12 92.79(14) . 1_545 ?
O10 U2 O12 89.04(15) . 1_545 ?
O9 U2 O6 89.23(15) . . ?
O10 U2 O6 90.43(15) . . ?
O12 U2 O6 75.29(14) 1_545 . ?
O9 U2 O2 87.56(14) . . ?
O10 U2 O2 90.48(15) . . ?
O12 U2 O2 169.08(11) 1_545 . ?
O6 U2 O2 93.81(14) . . ?
O9 U2 O3 83.96(15) . 2_656 ?
O10 U2 O3 97.53(15) . 2_656 ?
O12 U2 O3 66.99(10) 1_545 2_656 ?
O6 U2 O3 141.20(13) . 2_656 ?
O2 U2 O3 123.86(10) . 2_656 ?
O9 U2 O2 93.67(14) . 2_656 ?
O10 U2 O2 86.02(14) . 2_656 ?
O12 U2 O2 122.75(10) 1_545 2_656 ?
O6 U2 O2 161.47(13) . 2_656 ?
O2 U2 O2 68.08(12) . 2_656 ?
O3 U2 O2 57.32(10) 2_656 2_656 ?
O9 U2 P1 88.55(12) . 2_656 ?
O10 U2 P1 92.13(12) . 2_656 ?
O12 U2 P1 94.55(8) 1_545 2_656 ?
O6 U2 P1 169.48(11) . 2_656 ?
O2 U2 P1 96.37(8) . 2_656 ?
O3 U2 P1 28.29(8) 2_656 2_656 ?
O2 U2 P1 29.04(7) 2_656 2_656 ?
O9 U2 Rb3 43.09(11) . 2_556 ?
O10 U2 Rb3 138.13(11) . 2_556 ?
O12 U2 Rb3 55.19(9) 1_545 2_556 ?
O6 U2 Rb3 62.13(9) . 2_556 ?
O2 U2 Rb3 120.34(9) . 2_556 ?
O3 U2 Rb3 88.18(9) 2_656 2_556 ?
O2 U2 Rb3 129.75(8) 2_656 2_556 ?
P1 U2 Rb3 109.95(2) 2_656 2_556 ?
O9 U2 U3 105.08(11) . . ?
O10 U2 U3 76.21(11) . . ?
O12 U2 U3 28.18(7) 1_545 . ?
O6 U2 U3 51.43(12) . . ?
O2 U2 U3 141.72(7) . . ?
O3 U2 U3 93.72(7) 2_656 . ?
O2 U2 U3 143.87(8) 2_656 . ?
P1 U2 U3 119.492(19) 2_656 . ?
Rb3 U2 U3 62.007(9) 2_556 . ?
O9 U2 U1 85.31(11) . 1_545 ?
O10 U2 U1 96.69(12) . 1_545 ?
O12 U2 U1 31.64(7) 1_545 1_545 ?
O6 U2 U1 105.88(11) . 1_545 ?
O2 U2 U1 158.93(7) . 1_545 ?
O3 U2 U1 35.60(7) 2_656 1_545 ?
O2 U2 U1 92.60(7) 2_656 1_545 ?
P1 U2 U1 63.688(19) 2_656 1_545 ?
Rb3 U2 U1 65.172(10) 2_556 1_545 ?
U3 U2 U1 59.345(5) . 1_545 ?
O9 U2 U2 90.89(11) . 2_656 ?
O10 U2 U2 87.79(11) . 2_656 ?
O12 U2 U2 155.23(8) 1_545 2_656 ?
O6 U2 U2 129.27(11) . 2_656 ?
O2 U2 U2 35.57(8) . 2_656 ?
O3 U2 U2 89.10(7) 2_656 2_656 ?
O2 U2 U2 32.51(7) 2_656 2_656 ?
P1 U2 U2 61.059(18) 2_656 2_656 ?
Rb3 U2 U2 133.915(10) 2_556 2_656 ?
U3 U2 U2 163.982(6) . 2_656 ?
U1 U2 U2 124.686(7) 1_545 2_656 ?
O11 U3 O11 180.0 2_655 . ?
O11 U3 O12 90.49(15) 2_655 2_665 ?
O11 U3 O12 89.51(15) . 2_665 ?
O11 U3 O12 89.51(15) 2_655 1_545 ?
O11 U3 O12 90.49(15) . 1_545 ?
O12 U3 O12 180.00(19) 2_665 1_545 ?
O11 U3 O7 87.06(15) 2_655 . ?
O11 U3 O7 92.94(15) . . ?
O12 U3 O7 69.52(11) 2_665 . ?
O12 U3 O7 110.48(11) 1_545 . ?
O11 U3 O7 92.95(15) 2_655 2_655 ?
O11 U3 O7 87.05(15) . 2_655 ?
O12 U3 O7 110.48(11) 2_665 2_655 ?
O12 U3 O7 69.52(11) 1_545 2_655 ?
O7 U3 O7 180.0 . 2_655 ?
O11 U3 U1 90.73(11) 2_655 2_665 ?
O11 U3 U1 89.27(11) . 2_665 ?
O12 U3 U1 31.98(8) 2_665 2_665 ?
O12 U3 U1 148.02(8) 1_545 2_665 ?
O7 U3 U1 37.65(7) . 2_665 ?
O7 U3 U1 142.35(7) 2_655 2_665 ?
O11 U3 U1 89.27(11) 2_655 1_545 ?
O11 U3 U1 90.73(11) . 1_545 ?
O12 U3 U1 148.02(8) 2_665 1_545 ?
O12 U3 U1 31.98(8) 1_545 1_545 ?
O7 U3 U1 142.35(7) . 1_545 ?
O7 U3 U1 37.65(7) 2_655 1_545 ?
U1 U3 U1 180.0 2_665 1_545 ?
O11 U3 U2 96.78(11) 2_655 2_655 ?
O11 U3 U2 83.22(11) . 2_655 ?
O12 U3 U2 28.86(8) 2_665 2_655 ?
O12 U3 U2 151.14(8) 1_545 2_655 ?
O7 U3 U2 97.99(7) . 2_655 ?
O7 U3 U2 82.00(7) 2_655 2_655 ?
U1 U3 U2 60.355(6) 2_665 2_655 ?
U1 U3 U2 119.645(7) 1_545 2_655 ?
O11 U3 U2 83.22(11) 2_655 . ?
O11 U3 U2 96.78(11) . . ?
O12 U3 U2 151.14(8) 2_665 . ?
O12 U3 U2 28.86(8) 1_545 . ?
O7 U3 U2 82.01(7) . . ?
O7 U3 U2 98.00(7) 2_655 . ?
U1 U3 U2 119.645(7) 2_665 . ?
U1 U3 U2 60.355(7) 1_545 . ?
U2 U3 U2 180.0 2_655 . ?
O11 U3 Rb3 140.82(11) 2_655 2_556 ?
O11 U3 Rb3 39.18(11) . 2_556 ?
O12 U3 Rb3 127.39(10) 2_665 2_556 ?
O12 U3 Rb3 52.61(10) 1_545 2_556 ?
O7 U3 Rb3 96.64(8) . 2_556 ?
O7 U3 Rb3 83.36(8) 2_655 2_556 ?
U1 U3 Rb3 115.596(10) 2_665 2_556 ?
U1 U3 Rb3 64.404(10) 1_545 2_556 ?
U2 U3 Rb3 121.030(10) 2_655 2_556 ?
U2 U3 Rb3 58.970(10) . 2_556 ?
O11 U3 Rb3 39.18(11) 2_655 1_654 ?
O11 U3 Rb3 140.82(11) . 1_654 ?
O12 U3 Rb3 52.61(10) 2_665 1_654 ?
O12 U3 Rb3 127.39(10) 1_545 1_654 ?
O7 U3 Rb3 83.36(8) . 1_654 ?
O7 U3 Rb3 96.64(8) 2_655 1_654 ?
U1 U3 Rb3 64.404(10) 2_665 1_654 ?
U1 U3 Rb3 115.596(10) 1_545 1_654 ?
U2 U3 Rb3 58.970(10) 2_655 1_654 ?
U2 U3 Rb3 121.030(10) . 1_654 ?
Rb3 U3 Rb3 180.0 2_556 1_654 ?
O8 Rb1 O5 116.37(9) . 1_455 ?
O8 Rb1 O8 97.40(9) . 2_565 ?
O5 Rb1 O8 72.63(9) 1_455 2_565 ?
O8 Rb1 O14 70.55(10) . 2_665 ?
O5 Rb1 O14 145.87(10) 1_455 2_665 ?
O8 Rb1 O14 73.32(10) 2_565 2_665 ?
O8 Rb1 O11 134.17(10) . 2 ?
O5 Rb1 O11 97.60(9) 1_455 2 ?
O8 Rb1 O11 122.70(10) 2_565 2 ?
O14 Rb1 O11 98.59(10) 2_665 2 ?
O8 Rb1 O10 94.95(10) . 1_455 ?
O5 Rb1 O10 73.35(9) 1_455 1_455 ?
O8 Rb1 O10 145.85(10) 2_565 1_455 ?
O14 Rb1 O10 140.78(10) 2_665 1_455 ?
O11 Rb1 O10 65.04(10) 2 1_455 ?
O8 Rb1 O7 164.56(9) . 1_455 ?
O5 Rb1 O7 48.26(8) 1_455 1_455 ?
O8 Rb1 O7 80.10(9) 2_565 1_455 ?
O14 Rb1 O7 122.41(9) 2_665 1_455 ?
O11 Rb1 O7 56.38(9) 2 1_455 ?
O10 Rb1 O7 79.61(9) 1_455 1_455 ?
O8 Rb1 O14 65.89(9) . 1_455 ?
O5 Rb1 O14 54.21(8) 1_455 1_455 ?
O8 Rb1 O14 61.17(9) 2_565 1_455 ?
O14 Rb1 O14 109.54(7) 2_665 1_455 ?
O11 Rb1 O14 150.75(9) 2 1_455 ?
O10 Rb1 O14 95.94(9) 1_455 1_455 ?
O7 Rb1 O14 100.07(8) 1_455 1_455 ?
O8 Rb1 P2 138.74(7) . 1_455 ?
O5 Rb1 P2 24.29(6) 1_455 1_455 ?
O8 Rb1 P2 82.10(7) 2_565 1_455 ?
O14 Rb1 P2 144.83(7) 2_665 1_455 ?
O11 Rb1 P2 73.83(7) 2 1_455 ?
O10 Rb1 P2 67.86(7) 1_455 1_455 ?
O7 Rb1 P2 25.98(6) 1_455 1_455 ?
O14 Rb1 P2 78.47(6) 1_455 1_455 ?
O8 Rb1 Rb1 49.96(7) . 2_565 ?
O5 Rb1 Rb1 95.71(6) 1_455 2_565 ?
O8 Rb1 Rb1 47.44(7) 2_565 2_565 ?
O14 Rb1 Rb1 62.04(7) 2_665 2_565 ?
O11 Rb1 Rb1 159.17(7) 2 2_565 ?
O10 Rb1 Rb1 134.67(7) 1_455 2_565 ?
O7 Rb1 Rb1 125.67(6) 1_455 2_565 ?
O14 Rb1 Rb1 47.50(5) 1_455 2_565 ?
P2 Rb1 Rb1 116.89(3) 1_455 2_565 ?
O8 Rb1 P2 110.16(7) . 2_565 ?
O5 Rb1 P2 55.77(7) 1_455 2_565 ?
O8 Rb1 P2 18.19(7) 2_565 2_565 ?
O14 Rb1 P2 90.15(7) 2_665 2_565 ?
O11 Rb1 P2 114.36(7) 2 2_565 ?
O10 Rb1 P2 128.92(7) 1_455 2_565 ?
O7 Rb1 P2 64.34(6) 1_455 2_565 ?
O14 Rb1 P2 59.23(6) 1_455 2_565 ?
P2 Rb1 P2 63.93(3) 1_455 2_565 ?
Rb1 Rb1 P2 61.48(2) 2_565 2_565 ?
O8 Rb1 P2 16.45(7) . . ?
O5 Rb1 P2 131.11(6) 1_455 . ?
O8 Rb1 P2 107.68(7) 2_565 . ?
O14 Rb1 P2 63.23(7) 2_665 . ?
O11 Rb1 P2 118.71(7) 2 . ?
O10 Rb1 P2 92.49(7) 1_455 . ?
O7 Rb1 P2 171.91(6) 1_455 . ?
O14 Rb1 P2 82.31(6) 1_455 . ?
P2 Rb1 P2 150.61(3) 1_455 . ?
Rb1 Rb1 P2 61.460(19) 2_565 . ?
P2 Rb1 P2 122.938(19) 2_565 . ?
O4 Rb2 O1 143.49(10) . 1_455 ?
O4 Rb2 O13 66.11(10) . . ?
O1 Rb2 O13 130.66(9) 1_455 . ?
O4 Rb2 O4 82.06(10) . 2_566 ?
O1 Rb2 O4 75.64(10) 1_455 2_566 ?
O13 Rb2 O4 72.55(10) . 2_566 ?
O4 Rb2 O8 108.25(10) . . ?
O1 Rb2 O8 108.22(9) 1_455 . ?
O13 Rb2 O8 64.88(10) . . ?
O4 Rb2 O8 125.60(10) 2_566 . ?
O4 Rb2 O9 78.16(10) . 2_556 ?
O1 Rb2 O9 83.08(9) 1_455 2_556 ?
O13 Rb2 O9 143.53(10) . 2_556 ?
O4 Rb2 O9 110.62(10) 2_566 2_556 ?
O8 Rb2 O9 123.77(9) . 2_556 ?
O4 Rb2 O14 142.95(10) . 1_455 ?
O1 Rb2 O14 54.69(8) 1_455 1_455 ?
O13 Rb2 O14 80.26(9) . 1_455 ?
O4 Rb2 O14 73.09(10) 2_566 1_455 ?
O8 Rb2 O14 67.87(9) . 1_455 ?
O9 Rb2 O14 136.12(9) 2_556 1_455 ?
O4 Rb2 P2 88.14(7) . . ?
O1 Rb2 P2 128.15(7) 1_455 . ?
O13 Rb2 P2 60.94(7) . . ?
O4 Rb2 P2 132.34(7) 2_566 . ?
O8 Rb2 P2 21.70(6) . . ?
O9 Rb2 P2 112.70(7) 2_556 . ?
O14 Rb2 P2 88.76(6) 1_455 . ?
O4 Rb2 P1 126.48(7) . 1_455 ?
O1 Rb2 P1 21.28(6) 1_455 1_455 ?
O13 Rb2 P1 147.63(7) . 1_455 ?
O4 Rb2 P1 79.67(7) 2_566 1_455 ?
O8 Rb2 P1 123.27(7) . 1_455 ?
O9 Rb2 P1 62.59(7) 2_556 1_455 ?
O14 Rb2 P1 75.96(6) 1_455 1_455 ?
P2 Rb2 P1 138.86(3) . 1_455 ?
O4 Rb2 P1 97.82(7) . 2_566 ?
O1 Rb2 P1 56.83(7) 1_455 2_566 ?
O13 Rb2 P1 88.45(7) . 2_566 ?
O4 Rb2 P1 18.87(7) 2_566 2_566 ?
O8 Rb2 P1 128.83(7) . 2_566 ?
O9 Rb2 P1 103.95(7) 2_556 2_566 ?
O14 Rb2 P1 64.95(7) 1_455 2_566 ?
P2 Rb2 P1 143.31(2) . 2_566 ?
P1 Rb2 P1 61.69(3) 1_455 2_566 ?
O4 Rb2 P1 16.96(7) . . ?
O1 Rb2 P1 159.50(7) 1_455 . ?
O13 Rb2 P1 60.81(7) . . ?
O4 Rb2 P1 95.54(7) 2_566 . ?
O8 Rb2 P1 92.01(7) . . ?
O9 Rb2 P1 82.86(7) 2_556 . ?
O14 Rb2 P1 141.02(6) 1_455 . ?
P2 Rb2 P1 71.40(2) . . ?
P1 Rb2 P1 139.91(3) 1_455 . ?
P1 Rb2 P1 112.77(2) 2_566 . ?
O4 Rb2 U1 151.68(7) . 1_455 ?
O1 Rb2 U1 31.35(6) 1_455 1_455 ?
O13 Rb2 U1 101.23(7) . 1_455 ?
O4 Rb2 U1 69.79(7) 2_566 1_455 ?
O8 Rb2 U1 86.58(6) . 1_455 ?
O9 Rb2 U1 114.11(7) 2_556 1_455 ?
O14 Rb2 U1 23.54(6) 1_455 1_455 ?
P2 Rb2 U1 108.27(2) . 1_455 ?
P1 Rb2 U1 52.531(17) 1_455 1_455 ?
P1 Rb2 U1 55.252(17) 2_566 1_455 ?
P1 Rb2 U1 160.32(2) . 1_455 ?
O4 Rb3 O10 95.35(10) . 2_656 ?
O4 Rb3 O11 156.74(11) . 2_556 ?
O10 Rb3 O11 100.83(10) 2_656 2_556 ?
O4 Rb3 O9 81.48(10) . 2_556 ?
O10 Rb3 O9 112.49(11) 2_656 2_556 ?
O11 Rb3 O9 107.12(10) 2_556 2_556 ?
O4 Rb3 O13 75.11(10) . 2_566 ?
O10 Rb3 O13 164.62(10) 2_656 2_566 ?
O11 Rb3 O13 85.32(10) 2_556 2_566 ?
O9 Rb3 O13 78.49(10) 2_556 2_566 ?
O4 Rb3 O12 117.47(9) . 2_566 ?
O10 Rb3 O12 141.27(9) 2_656 2_566 ?
O11 Rb3 O12 55.97(9) 2_556 2_566 ?
O9 Rb3 O12 57.77(9) 2_556 2_566 ?
O13 Rb3 O12 53.42(9) 2_566 2_566 ?
O4 Rb3 O14 72.06(10) . 2_666 ?
O10 Rb3 O14 87.69(10) 2_656 2_666 ?
O11 Rb3 O14 91.89(9) 2_556 2_666 ?
O9 Rb3 O14 148.23(9) 2_556 2_666 ?
O13 Rb3 O14 77.96(9) 2_566 2_666 ?
O12 Rb3 O14 120.34(8) 2_566 2_666 ?
O4 Rb3 O6 133.52(10) . 2_556 ?
O10 Rb3 O6 94.22(10) 2_656 2_556 ?
O11 Rb3 O6 62.05(10) 2_556 2_556 ?
O9 Rb3 O6 52.99(9) 2_556 2_556 ?
O13 Rb3 O6 101.10(10) 2_566 2_556 ?
O12 Rb3 O6 48.60(9) 2_566 2_556 ?
O14 Rb3 O6 153.78(9) 2_666 2_556 ?
O4 Rb3 P1 24.31(7) . . ?
O10 Rb3 P1 71.29(7) 2_656 . ?
O11 Rb3 P1 158.86(7) 2_556 . ?
O9 Rb3 P1 93.98(7) 2_556 . ?
O13 Rb3 P1 97.97(7) 2_566 . ?
O12 Rb3 P1 140.90(6) 2_566 . ?
O14 Rb3 P1 68.63(6) 2_666 . ?
O6 Rb3 P1 136.51(8) 2_556 . ?
O4 Rb3 O3 45.28(9) . . ?
O10 Rb3 O3 59.38(9) 2_656 . ?
O11 Rb3 O3 133.45(9) 2_556 . ?
O9 Rb3 O3 119.30(8) 2_556 . ?
O13 Rb3 O3 106.22(9) 2_566 . ?
O12 Rb3 O3 159.28(7) 2_566 . ?
O14 Rb3 O3 49.48(7) 2_666 . ?
O6 Rb3 O3 149.22(9) 2_556 . ?
P1 Rb3 O3 25.74(5) . . ?
O4 Rb3 O2 44.72(9) . . ?
O10 Rb3 O2 53.83(9) 2_656 . ?
O11 Rb3 O2 154.65(9) 2_556 . ?
O9 Rb3 O2 85.05(9) 2_556 . ?
O13 Rb3 O2 119.37(9) 2_566 . ?
O12 Rb3 O2 142.53(7) 2_566 . ?
O14 Rb3 O2 88.19(8) 2_666 . ?
O6 Rb3 O2 113.93(9) 2_556 . ?
P1 Rb3 O2 25.59(5) . . ?
O3 Rb3 O2 38.83(7) . . ?
O4 Rb3 U2 104.07(8) . 2_556 ?
O10 Rb3 U2 120.95(8) 2_656 2_556 ?
O11 Rb3 U2 81.78(7) 2_556 2_556 ?
O9 Rb3 U2 25.44(7) 2_556 2_556 ?
O13 Rb3 U2 73.67(7) 2_566 2_556 ?
O12 Rb3 U2 35.14(5) 2_566 2_556 ?
O14 Rb3 U2 151.32(6) 2_666 2_556 ?
O6 Rb3 U2 35.32(6) 2_556 2_556 ?
P1 Rb3 U2 119.24(2) . 2_556 ?
O3 Rb3 U2 144.72(5) . 2_556 ?
O2 Rb3 U2 109.29(5) . 2_556 ?
O4 P1 O1 114.61(19) . . ?
O4 P1 O3 111.6(2) . . ?
O1 P1 O3 110.1(2) . . ?
O4 P1 O2 112.5(2) . . ?
O1 P1 O2 108.76(19) . . ?
O3 P1 O2 98.01(17) . . ?
O4 P1 U2 124.96(14) . 2_656 ?
O1 P1 U2 120.40(13) . 2_656 ?
O3 P1 U2 47.21(11) . 2_656 ?
O2 P1 U2 50.81(11) . 2_656 ?
O4 P1 Rb3 51.08(14) . . ?
O1 P1 Rb3 165.65(13) . . ?
O3 P1 Rb3 78.03(15) . . ?
O2 P1 Rb3 80.94(14) . . ?
U2 P1 Rb3 73.88(2) 2_656 . ?
O4 P1 Rb2 153.84(15) . 1_655 ?
O1 P1 Rb2 44.24(13) . 1_655 ?
O3 P1 Rb2 72.72(15) . 1_655 ?
O2 P1 Rb2 91.69(14) . 1_655 ?
U2 P1 Rb2 77.77(2) 2_656 1_655 ?
Rb3 P1 Rb2 148.51(3) . 1_655 ?
O4 P1 Rb2 39.85(15) . 2_566 ?
O1 P1 Rb2 97.89(13) . 2_566 ?
O3 P1 Rb2 86.28(13) . 2_566 ?
O2 P1 Rb2 149.40(14) . 2_566 ?
U2 P1 Rb2 126.00(3) 2_656 2_566 ?
Rb3 P1 Rb2 70.29(2) . 2_566 ?
Rb2 P1 Rb2 118.30(3) 1_655 2_566 ?
O4 P1 Rb2 33.75(15) . . ?
O1 P1 Rb2 96.77(13) . . ?
O3 P1 Rb2 144.73(15) . . ?
O2 P1 Rb2 94.32(13) . . ?
U2 P1 Rb2 134.07(3) 2_656 . ?
Rb3 P1 Rb2 71.47(2) . . ?
Rb2 P1 Rb2 139.91(3) 1_655 . ?
Rb2 P1 Rb2 67.23(2) 2_566 . ?
O8 P2 O5 114.34(19) . . ?
O8 P2 O6 111.1(2) . . ?
O5 P2 O6 108.42(19) . . ?
O8 P2 O7 112.87(19) . . ?
O5 P2 O7 106.82(18) . . ?
O6 P2 O7 102.5(2) . . ?
O8 P2 Rb1 153.56(15) . 1_655 ?
O5 P2 Rb1 49.61(12) . 1_655 ?
O6 P2 Rb1 94.98(16) . 1_655 ?
O7 P2 Rb1 63.35(13) . 1_655 ?
O8 P2 Rb2 48.74(14) . . ?
O5 P2 Rb2 94.92(12) . . ?
O6 P2 Rb2 77.03(18) . . ?
O7 P2 Rb2 156.93(14) . . ?
Rb1 P2 Rb2 139.63(3) 1_655 . ?
O8 P2 Rb1 37.57(14) . 2_565 ?
O5 P2 Rb1 89.12(13) . 2_565 ?
O6 P2 Rb1 148.41(17) . 2_565 ?
O7 P2 Rb1 96.85(13) . 2_565 ?
Rb1 P2 Rb1 116.07(3) 1_655 2_565 ?
Rb2 P2 Rb1 75.42(2) . 2_565 ?
O8 P2 Rb1 32.15(14) . . ?
O5 P2 Rb1 144.83(13) . . ?
O6 P2 Rb1 98.59(15) . . ?
O7 P2 Rb1 88.21(13) . . ?
Rb1 P2 Rb1 150.61(3) 1_655 . ?
Rb2 P2 Rb1 69.25(2) . . ?
Rb1 P2 Rb1 57.062(19) 2_565 . ?
P1 O1 U1 137.7(2) . . ?
P1 O1 Rb2 114.48(16) . 1_655 ?
U1 O1 Rb2 107.26(12) . 1_655 ?
P1 O2 U2 145.19(18) . . ?
P1 O2 U2 100.16(14) . 2_656 ?
U2 O2 U2 111.92(12) . 2_656 ?
P1 O2 Rb3 73.47(13) . . ?
U2 O2 Rb3 123.85(13) . . ?
U2 O2 Rb3 80.24(8) 2_656 . ?
P1 O3 U1 146.04(18) . 2_666 ?
P1 O3 U2 104.51(15) . 2_656 ?
U1 O3 U2 108.38(11) 2_666 2_656 ?
P1 O3 Rb3 76.22(15) . . ?
U1 O3 Rb3 99.34(11) 2_666 . ?
U2 O3 Rb3 83.13(10) 2_656 . ?
P1 O4 Rb3 104.61(17) . . ?
P1 O4 Rb2 129.3(2) . . ?
Rb3 O4 Rb2 101.22(11) . . ?
P1 O4 Rb2 121.3(2) . 2_566 ?
Rb3 O4 Rb2 96.29(11) . 2_566 ?
Rb2 O4 Rb2 97.94(10) . 2_566 ?
P2 O5 U1 141.54(19) . . ?
P2 O5 Rb1 106.09(15) . 1_655 ?
U1 O5 Rb1 112.26(12) . 1_655 ?
P2 O6 U2 147.9(2) . . ?
P2 O6 Rb3 128.80(18) . 2_556 ?
U2 O6 Rb3 82.55(10) . 2_556 ?
P2 O7 U3 116.29(18) . . ?
P2 O7 U1 132.84(19) . 2_665 ?
U3 O7 U1 105.36(11) . 2_665 ?
P2 O7 Rb1 90.66(14) . 1_655 ?
U3 O7 Rb1 94.86(11) . 1_655 ?
U1 O7 Rb1 107.44(12) 2_665 1_655 ?
P2 O8 Rb1 131.40(19) . . ?
P2 O8 Rb1 124.24(19) . 2_565 ?
Rb1 O8 Rb1 82.60(9) . 2_565 ?
P2 O8 Rb2 109.56(17) . . ?
Rb1 O8 Rb2 97.99(10) . . ?
Rb1 O8 Rb2 105.78(10) 2_565 . ?
U2 O9 Rb3 111.47(14) . 2_556 ?
U2 O9 Rb2 130.98(17) . 2_556 ?
Rb3 O9 Rb2 95.24(10) 2_556 2_556 ?
U2 O10 Rb3 119.15(16) . 2_656 ?
U2 O10 Rb1 135.38(17) . 1_655 ?
Rb3 O10 Rb1 100.23(10) 2_656 1_655 ?
U3 O11 Rb3 117.19(15) . 2_556 ?
U3 O11 Rb1 118.19(17) . 2 ?
Rb3 O11 Rb1 86.04(10) 2_556 2 ?
U3 O12 U2 122.95(14) 1_565 1_565 ?
U3 O12 U1 117.86(13) 1_565 . ?
U2 O12 U1 117.79(12) 1_565 . ?
U3 O12 Rb3 94.37(11) 1_565 2_566 ?
U2 O12 Rb3 89.66(11) 1_565 2_566 ?
U1 O12 Rb3 97.96(11) . 2_566 ?
U1 O13 Rb3 125.24(16) . 2_566 ?
U1 O13 Rb2 140.51(16) . . ?
Rb3 O13 Rb2 94.25(10) 2_566 . ?
U1 O14 Rb1 146.53(17) . 2_665 ?
U1 O14 Rb2 110.90(14) . 1_655 ?
Rb1 O14 Rb2 100.00(9) 2_665 1_655 ?
U1 O14 Rb3 119.13(16) . 2_666 ?
Rb1 O14 Rb3 77.57(8) 2_665 2_666 ?
Rb2 O14 Rb3 80.40(8) 1_655 2_666 ?
U1 O14 Rb1 101.28(14) . 1_655 ?
Rb1 O14 Rb1 70.46(7) 2_665 1_655 ?
Rb2 O14 Rb1 81.07(8) 1_655 1_655 ?
Rb3 O14 Rb1 139.32(10) 2_666 1_655 ?

_refine_diff_density_max         2.800
_refine_diff_density_min         -2.897
_refine_diff_density_rms         0.386


# start Validation Reply Form
_vrf_PLAT971_Rb6U5P4O28          
;
PROBLEM: Check Calcd Resid. Dens.  0.71A   From U1              2.62 eA-3  
RESPONSE: The residual electron density is relatively small compared to the
heaviest atom, U, and is less than 10% of the electron density of U.
;
_vrf_PLAT972_Rb6U5P4O28          
;
PROBLEM: Check Calcd Resid. Dens.  0.55A   From U2             -2.97 eA-3  
RESPONSE: The residual electron density is relatively small compared to the
heaviest atom, U, and is less than 10% of the electron density of U.
;
# end Validation Reply Form
_exptl_crystal_recrystallization_method 'From the Melt'
_exptl_crystal_preparation       Luminescent
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_caj1183c2b
_database_code_depnum_ccdc_archive 'CCDC 1984890'
loop_
_audit_author_name
_audit_author_address
'Christian Juillerat'
;University of South Carolina
United States of America
;
_audit_update_record             
;
2020-02-18 deposited with the CCDC.	2020-04-07 downloaded from the CCDC.
;

# start Validation Reply Form
_vrf_PLAT241_caj1183c2b          
;
PROBLEM: High   'MainMol' Ueq as Compared to Neighbors of         O1 Check 
RESPONSE: O1 and O2 likely are affected by minor positional disorder,
which could not be reasonably modeled because of their small population.
O1 and O2 belong to a PO4 group bonded to a badly disordered uranium position;
this PO4 group (P1) is also likely to be disordered itself. O12 is mildly
prolate and reflects minor disorder of its PO4 group.
;
_vrf_PLAT971_caj1183c2b          
;
PROBLEM: Check Calcd Resid. Dens.  0.64A   From U4              3.11 eA-3  
RESPONSE: Normal non-chemically significant residual peak near a very heavy
atom. The peak near O4 represent a minor disorder contribution of PO4 group
P1, whcih could not be modeled.
;
_vrf_PLAT972_caj1183c2b          
;
PROBLEM: Check Calcd Resid. Dens.  0.51A   From U5B            -3.12 eA-3  
RESPONSE: Normal non-chemically significant residual hole near a very heavy
atom.
;
_vrf_PLAT976_caj1183c2b          
;
PROBLEM: Check Calcd Resid. Dens.  1.00A   From O28A           -1.59 eA-3  
RESPONSE: This density hole is closer to the U5 disorder site than to O5,
and may reflect a less-than-full occupancy of the site. Such partial site
occupancy and three-fold disorder could not be reliably modeled. The hole,
and other peaks, also reflect the low single crystallinity of the available
samples of this material.
;
# end Validation Reply Form

_audit_creation_method           SHELXL-2018/3
_shelx_SHELXL_version_number     2018/3
_chemical_name_systematic        Rb5.93Cl0.93[UO2)5(PO4)5]
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         'Cl0.95 O30 P5 Rb5.93 U5'
_chemical_formula_sum            'Cl0.95 O30 P5 Rb5.93 U5'
_chemical_formula_weight         2365.06

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Rb Rb -0.9393 2.9676 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
U U -9.6767 9.6646 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'

_shelx_space_group_comment       
; 
The symmetry employed for this shelxl refinement is uniquely defined 
by the following loop, which should always be used as a source of 
symmetry information in preference to the above space-group names. 
They are only intended as comments. 
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   9.548(4)
_cell_length_b                   13.488(5)
_cell_length_c                   14.898(6)
_cell_angle_alpha                64.755(16)
_cell_angle_beta                 72.369(16)
_cell_angle_gamma                89.511(16)
_cell_volume                     1637.7(11)
_cell_formula_units_Z            2
_cell_measurement_temperature    301(2)
_cell_measurement_reflns_used    8937
_cell_measurement_theta_min      2.260
_cell_measurement_theta_max      28.218

_exptl_crystal_description       plate
_exptl_crystal_colour            yellow
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    4.796
_exptl_crystal_F_000             2021
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          0.040
_exptl_crystal_size_mid          0.030
_exptl_crystal_size_min          0.020
_exptl_absorpt_coefficient_mu    33.813
_shelx_estimated_absorpt_T_min   0.345
_shelx_estimated_absorpt_T_max   0.551
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_correction_T_min  0.1786
_exptl_absorpt_correction_T_max  0.2627
_exptl_absorpt_process_details   'SADABS Version 2016/2 (Bruker, 2016)'
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      301(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_source                   'microfocus sealed X-ray tube'
_diffrn_measurement_device_type  'Bruker D8 QUEST'
_diffrn_measurement_method       'ω and φ scans'
_diffrn_detector_area_resol_mean 10.4
_diffrn_reflns_number            74700
_diffrn_reflns_av_unetI/netI     0.0432
_diffrn_reflns_av_R_equivalents  0.0882
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_l_min       -19
_diffrn_reflns_limit_l_max       19
_diffrn_reflns_theta_min         2.260
_diffrn_reflns_theta_max         28.437
_diffrn_reflns_theta_full        25.242
_diffrn_measured_fraction_theta_max 0.987
_diffrn_measured_fraction_theta_full 0.998
_diffrn_reflns_Laue_measured_fraction_max 0.987
_diffrn_reflns_Laue_measured_fraction_full 0.998
_diffrn_reflns_point_group_measured_fraction_max 0.987
_diffrn_reflns_point_group_measured_fraction_full 0.998
_reflns_number_total             8125
_reflns_number_gt                6452
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
; 
 Reflections were merged by SHELXL according to the crystal 
 class for the calculation of statistics and refinement. 
  
 _reflns_Friedel_fraction is defined as the number of unique 
 Friedel pairs measured divided by the number that would be 
 possible theoretically, ignoring centric projections and 
 systematic absences. 
;

_computing_data_collection       'Bruker APEX3 v2016.5-0 (Bruker, 2016)'
_computing_cell_refinement       'SAINT Version 8.38a (Bruker, 2016)'
_computing_data_reduction        'SAINT Version 8.38a (Bruker, 2016)'
_computing_structure_solution    'SHELXT (Sheldrick, 2015)'
_computing_structure_refinement  'SHELXL-2018/3 (Sheldrick, 2018)'
_computing_molecular_graphics    various
_computing_publication_material  various
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0162P)²+61.8101P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   .
_refine_ls_hydrogen_treatment    undef
_refine_ls_extinction_method     'SHELXL-2018/3 (Sheldrick 2018)'
_refine_ls_extinction_coef       0.00019(2)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_number_reflns         8125
_refine_ls_number_parameters     472
_refine_ls_number_restraints     8
_refine_ls_R_factor_all          0.0703
_refine_ls_R_factor_gt           0.0482
_refine_ls_wR_factor_ref         0.0960
_refine_ls_wR_factor_gt          0.0892
_refine_ls_goodness_of_fit_ref   1.098
_refine_ls_restrained_S_all      1.099
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
U1 U 0.68486(4) 0.48889(4) 0.54621(4) 0.01698(11) Uani 1 1 d . . . . .
U2 U 0.92318(5) 0.79011(4) 0.16061(4) 0.02543(12) Uani 1 1 d . . . . .
U3 U 0.41478(5) 0.07902(4) 0.15669(4) 0.02387(12) Uani 1 1 d . . . . .
U4 U 0.86921(5) 0.35047(4) 0.26189(4) 0.02531(12) Uani 1 1 d . . . . .
U5A U 0.22867(14) 0.03901(9) 0.48233(10) 0.0266(2) Uani 0.730(2) 1 d . . P . .
U5B U 0.2260(6) 0.0100(4) 0.5248(4) 0.0266(2) Uani 0.190(3) 1 d . . P . .
U5C U 0.2712(12) 0.0183(8) 0.5010(9) 0.0266(2) Uani 0.080(3) 1 d . . P . .
Rb1 Rb 0.46189(19) 0.18456(14) 0.58984(16) 0.0510(4) Uani 1 1 d . . . . .
Rb2 Rb 0.7856(2) 0.6224(2) 0.00237(16) 0.0705(6) Uani 1 1 d . . . . .
Rb3A Rb 0.355(2) 0.3704(9) 0.2573(7) 0.0474(19) Uani 0.69(8) 1 d . . P . .
Rb3B Rb 0.403(6) 0.3609(14) 0.252(2) 0.047(5) Uani 0.31(8) 1 d . . P . .
Rb4A Rb -0.0829(10) 0.2129(8) 0.5959(8) 0.0653(16) Uani 0.65(2) 1 d . . P . .
Rb4B Rb -0.0421(15) 0.2432(14) 0.5722(15) 0.0653(16) Uani 0.35(2) 1 d . . P . .
Rb5 Rb 0.8925(2) 0.07925(19) 0.15784(16) 0.0495(8) Uani 0.844(7) 1 d . . . . .
Rb6A Rb 0.3951(3) 0.7594(2) 0.15545(18) 0.0555(7) Uani 0.770(3) 1 d . . P . .
Rb6B Rb 0.3656(15) 0.7151(13) 0.1295(11) 0.031(3) Uiso 0.111(3) 1 d . . P . .
Rb6C Rb 0.3308(19) 0.6828(15) 0.1158(13) 0.055(4) Uiso 0.119(3) 1 d . . P . .
Cl1 Cl 0.5378(13) 0.4918(16) -0.0113(17) 0.071(5) Uani 0.5 1 d . . P . .
Cl2A Cl 0.2331(13) 0.6852(13) -0.0190(10) 0.060(4) Uiso 0.447(18) 1 d . . P . .
Rb7A Rb 0.229(3) 0.621(3) 0.007(2) 0.060(4) Uiso 0.082(6) 1 d . . P . .
P1 P 0.1082(5) 0.1353(3) 0.2933(4) 0.0406(10) Uani 1 1 d . . . . .
P2 P 0.6020(5) 0.1298(4) 0.3216(3) 0.0400(10) Uani 1 1 d . . . . .
P3 P 0.6278(3) 0.5561(3) 0.2885(2) 0.0177(6) Uani 1 1 d . . . . .
P4 P 0.0340(3) 0.5407(3) 0.3227(3) 0.0213(7) Uani 1 1 d . . . . .
P5 P 0.2566(3) 0.9937(3) 0.0000(3) 0.0204(6) Uani 1 1 d . . . . .
O1 O 0.1479(17) 0.0844(16) 0.2161(13) 0.095(6) Uani 1 1 d . . . . .
O2 O 0.0169(16) 0.0601(11) 0.3979(11) 0.084(5) Uani 1 1 d . . . . .
O3 O 0.0522(15) 0.2418(10) 0.2446(11) 0.070(4) Uani 1 1 d . . . . .
O4 O 0.2723(15) 0.1516(11) 0.2963(11) 0.062(4) Uani 1 1 d . . . . .
O5 O 0.5642(14) 0.0988(13) 0.2446(10) 0.065(4) Uani 1 1 d . . . . .
O6 O 0.4666(14) 0.1308(11) 0.4072(10) 0.060(4) Uani 1 1 d . . . . .
O7 O 0.6936(18) 0.2406(12) 0.2622(12) 0.081(5) Uani 1 1 d . . . . .
O8 O 0.6931(18) 0.0404(12) 0.3733(10) 0.072(4) Uani 1 1 d . . . . .
O9 O 0.4742(9) 0.5550(7) 0.2763(7) 0.0238(19) Uani 1 1 d . . . . .
O10 O 0.5894(10) 0.5147(12) 0.4085(8) 0.049(3) Uani 1 1 d . . . . .
O11 O 0.7162(13) 0.4805(11) 0.2505(10) 0.053(3) Uani 1 1 d . . . . .
O12 O 0.7136(15) 0.6718(10) 0.2287(13) 0.082(5) Uani 1 1 d . . . . .
O13 O 0.0302(12) 0.4754(10) 0.2619(10) 0.050(3) Uani 1 1 d . . . . .
O14 O -0.1036(10) 0.5087(11) 0.4176(9) 0.048(3) Uani 1 1 d . . . . .
O15 O 0.0485(15) 0.6620(10) 0.2477(12) 0.069(4) Uani 1 1 d . . . . .
O16 O 0.1694(12) 0.5221(11) 0.3576(9) 0.054(3) Uani 1 1 d . U . . .
O17 O 0.3623(12) 0.9319(11) -0.0502(10) 0.049(3) Uani 1 1 d . . . . .
O18 O 0.1340(12) 0.9101(10) 0.0928(10) 0.056(3) Uani 1 1 d . . . . .
O19 O 0.1865(15) 1.0716(11) -0.0779(13) 0.079(5) Uani 1 1 d . . . . .
O20 O 0.3419(11) 1.0599(10) 0.0326(9) 0.047(3) Uani 1 1 d . . . . .
O21 O 0.6970(13) 0.6326(8) 0.5112(9) 0.044(3) Uani 1 1 d . . . . .
O22 O 0.6670(12) 0.3427(9) 0.5889(9) 0.043(3) Uani 1 1 d . . . . .
O23 O 0.8657(13) 0.8248(11) 0.2694(9) 0.051(3) Uani 1 1 d . . . . .
O24 O 0.9817(16) 0.7564(12) 0.0530(11) 0.066(4) Uani 1 1 d . . . . .
O25 O 0.4464(15) 0.2236(9) 0.0715(10) 0.053(3) Uani 1 1 d . . . . .
O26 O 0.9351(12) 0.4147(10) 0.1197(9) 0.045(3) Uani 1 1 d . . . . .
O27 O 0.8082(14) 0.2884(10) 0.4009(9) 0.054(3) Uani 1 1 d . . . . .
O28A O 0.1842(19) 0.1568(12) 0.5077(11) 0.045(4) Uani 0.730(2) 1 d . . P . .
O28B O 0.193(5) 0.098(3) 0.585(3) 0.045(4) Uani 0.270(2) 1 d . . P . .
O29 O 0.2708(11) -0.0713(9) 0.4524(9) 0.039(2) Uani 1 1 d . . . . .
O30 O 0.3815(14) 0.9332(9) 0.2375(9) 0.050(3) Uani 1 1 d . . . . .


_geom_special_details            
; 
 All esds (except the esd in the dihedral angle between two l.s. planes) 
 are estimated using the full covariance matrix.  The cell esds are taken 
 into account individually in the estimation of esds in distances, angles 
 and torsion angles; correlations between esds in cell parameters are only 
 used when they are defined by crystal symmetry.  An approximate (isotropic) 
 treatment of cell esds is used for estimating esds involving l.s. planes. 
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
U1 O21 1.774(10) . ?
U1 O22 1.786(10) . ?
U1 O16 2.244(10) 2_666 ?
U1 O14 2.248(10) 1_655 ?
U1 O10 2.384(9) . ?
U1 O9 2.428(9) 2_666 ?
U1 O10 2.493(9) 2_666 ?
U1 P3 3.106(3) 2_666 ?
U1 Rb3A 4.045(7) 2_666 ?
U1 Rb6A 4.104(3) 2_666 ?
U1 Rb4B 4.159(16) 1_655 ?
U1 Rb3B 4.18(3) 2_666 ?
U2 O24 1.778(12) . ?
U2 O23 1.803(11) . ?
U2 O19 2.210(11) 2_675 ?
U2 O12 2.241(12) . ?
U2 O15 2.257(12) 1_655 ?
U2 O18 2.263(11) 1_655 ?
U2 Rb5 3.892(3) 1_565 ?
U2 Rb5 4.071(3) 2_765 ?
U2 Rb6C 4.104(16) 1_655 ?
U2 Rb6B 4.269(13) 1_655 ?
U2 Rb4B 4.306(17) 2_666 ?
U2 Rb4A 4.325(8) 2_666 ?
U3 O25 1.781(11) . ?
U3 O30 1.782(11) 1_545 ?
U3 O20 2.270(10) 1_545 ?
U3 O17 2.284(11) 2_665 ?
U3 O5 2.294(11) . ?
U3 O1 2.443(15) . ?
U3 O4 2.672(13) . ?
U3 P1 3.310(5) . ?
U3 Rb6B 3.857(14) 2_665 ?
U3 Rb6C 3.967(17) 2_665 ?
U3 Rb6A 3.997(3) 2_665 ?
U3 Rb6A 4.325(3) 1_545 ?
U4 O27 1.769(12) . ?
U4 O26 1.809(11) . ?
U4 O7 2.245(12) . ?
U4 O11 2.257(10) . ?
U4 O13 2.291(10) 1_655 ?
U4 O3 2.297(11) 1_655 ?
U4 Rb2 4.175(2) 2_765 ?
U4 Rb7A 4.25(3) 2_665 ?
U4 Rb2 4.331(3) . ?
U4 Rb7A 4.47(3) 1_655 ?
U4 Rb3B 4.49(5) . ?
U4 Rb5 4.522(2) . ?
U5A U5C 0.566(10) . ?
U5A U5B 0.578(4) . ?
U5A O29 1.738(10) . ?
U5A O28A 1.803(14) . ?
U5A O28B 1.95(4) . ?
U5A O6 2.296(12) . ?
U5A O8 2.308(13) 2_656 ?
U5A O4 2.425(14) . ?
U5A O2 2.440(14) 2_556 ?
U5A O2 2.641(18) . ?
U5A P1 3.123(4) . ?
U5A Rb1 4.037(2) . ?
U5B O28B 1.75(4) . ?
U5B O8 1.784(14) 2_656 ?
U5B O29 1.808(12) . ?
U5B O28A 1.940(15) . ?
U5B O2 2.255(16) 2_556 ?
U5B O6 2.489(13) . ?
U5B P2 3.167(7) 2_656 ?
U5B Rb1 3.862(5) . ?
U5B Rb5 4.124(5) 2_656 ?
U5B Rb4B 4.196(17) . ?
U5B Rb4A 4.214(9) . ?
U5C O29 1.654(14) . ?
U5C O8 1.835(17) 2_656 ?
U5C O28B 1.96(4) . ?
U5C O28A 2.066(17) . ?
U5C O6 2.096(17) . ?
U5C O2 2.671(18) 2_556 ?
U5C O4 2.800(19) . ?
U5C P2 3.135(12) 2_656 ?
U5C P2 3.304(12) . ?
U5C Rb1 3.762(10) . ?
U5C Rb1 4.095(10) 2_656 ?
Rb1 O28B 2.86(5) . ?
Rb1 O22 2.901(11) . ?
Rb1 O21 2.967(11) 2_666 ?
Rb1 O29 3.005(11) 2_656 ?
Rb1 O6 3.089(12) . ?
Rb1 O8 3.141(15) 2_656 ?
Rb1 O23 3.163(12) 2_666 ?
Rb1 O30 3.191(11) 2_666 ?
Rb1 O28A 3.322(17) . ?
Rb1 O27 3.449(13) . ?
Rb1 O5 3.516(16) 2_656 ?
Rb2 O26 2.913(11) 2_765 ?
Rb2 Cl1 3.068(19) . ?
Rb2 O24 3.069(14) . ?
Rb2 O25 3.144(13) 2_665 ?
Rb2 O3 3.185(14) 2_665 ?
Rb2 O26 3.194(12) . ?
Rb2 O11 3.205(13) . ?
Rb2 Rb7A 3.35(3) 2_665 ?
Rb2 Cl1 3.404(16) 2_665 ?
Rb2 O12 3.577(19) . ?
Rb2 P3 3.758(4) . ?
Rb2 P1 4.023(5) 2_665 ?
Rb3A O4 2.823(15) . ?
Rb3A O9 2.902(12) . ?
Rb3A Cl1 3.14(2) 2_665 ?
Rb3A O16 3.24(2) . ?
Rb3A O21 3.314(14) 2_666 ?
Rb3A O13 3.39(3) . ?
Rb3A O6 3.43(2) . ?
Rb3A Cl1 3.46(2) . ?
Rb3A O3 3.48(2) . ?
Rb3A O28A 3.479(17) . ?
Rb3A P1 3.716(11) . ?
Rb3A Rb6C 3.87(2) . ?
Rb3B O4 2.82(2) . ?
Rb3B O9 2.90(2) . ?
Rb3B Cl1 3.14(3) 2_665 ?
Rb3B O6 3.17(3) . ?
Rb3B O7 3.21(6) . ?
Rb3B Cl1 3.35(4) . ?
Rb3B O11 3.40(4) . ?
Rb3B O21 3.40(4) 2_666 ?
Rb3B P2 3.57(4) . ?
Rb3B O28A 3.58(4) . ?
Rb3B O16 3.59(5) . ?
Rb3B P3 3.720(19) . ?
Rb4A O28A 2.755(18) . ?
Rb4A O22 2.951(13) 1_455 ?
Rb4A O28B 3.04(4) . ?
Rb4A O29 3.066(13) 2_556 ?
Rb4A O30 3.132(16) 2_566 ?
Rb4A O27 3.138(14) 1_455 ?
Rb4A O23 3.196(14) 2_666 ?
Rb4A O15 3.494(18) 2_566 ?
Rb4A P4 4.067(9) 2_566 ?
Rb4A Rb6A 4.150(9) 2_566 ?
Rb4B O28A 2.57(2) . ?
Rb4B O28B 2.96(4) . ?
Rb4B O22 3.063(18) 1_455 ?
Rb4B O23 3.13(2) 2_666 ?
Rb4B O27 3.13(2) 1_455 ?
Rb4B O21 3.324(17) 2_666 ?
Rb4B O29 3.402(16) 2_556 ?
Rb4B O15 3.42(2) 2_566 ?
Rb4B O14 3.50(2) . ?
Rb4B O30 3.61(2) 2_566 ?
Rb4B P4 3.863(16) 2_566 ?
Rb4B P4 4.018(18) . ?
Rb5 O1 2.835(18) 1_655 ?
Rb5 O24 2.836(15) 2_765 ?
Rb5 O19 2.961(16) 2_665 ?
Rb5 O8 3.014(14) . ?
Rb5 O5 3.065(13) . ?
Rb5 O23 3.082(13) 1_545 ?
Rb5 O17 3.330(11) 2_665 ?
Rb5 O28B 3.38(4) 2_656 ?
Rb5 P2 3.377(5) . ?
Rb5 Cl2A 3.412(15) 2_665 ?
Rb5 O7 3.434(18) . ?
Rb5 O18 3.449(13) 1_645 ?
Rb6A Rb6B 0.922(17) . ?
Rb6A Rb6C 1.59(2) . ?
Rb6A O9 2.822(9) . ?
Rb6A O30 3.058(13) . ?
Rb6A O17 3.064(13) . ?
Rb6A O25 3.165(13) 2_665 ?
Rb6A O20 3.180(12) 2_675 ?
Rb6A O15 3.216(14) . ?
Rb6A O22 3.305(12) 2_666 ?
Rb6A O18 3.306(12) . ?
Rb6A O16 3.452(13) . ?
Rb6A P5 3.556(4) . ?
Rb6B Rb6C 0.680(18) . ?
Rb6B O25 2.745(19) 2_665 ?
Rb6B O9 2.798(16) . ?
Rb6B O15 2.917(19) . ?
Rb6B O17 3.016(19) . ?
Rb6B Cl2A 3.02(2) . ?
Rb6B Rb7A 3.17(3) . ?
Rb6B O16 3.242(18) . ?
Rb6B O18 3.394(18) . ?
Rb6B O20 3.556(19) 2_675 ?
Rb6B P4 3.560(14) . ?
Rb6C Cl2A 2.45(2) . ?
Rb6C Rb7A 2.52(3) . ?
Rb6C O25 2.71(2) 2_665 ?
Rb6C O15 2.75(2) . ?
Rb6C O9 2.999(19) . ?
Rb6C O17 3.16(2) . ?
Rb6C O16 3.18(2) . ?
Rb6C P4 3.312(17) . ?
Rb6C Cl1 3.38(3) 2_665 ?
Rb6C O13 3.46(2) . ?
Cl1 Cl1 0.77(3) 2_665 ?
Cl1 Rb7A 2.68(3) 2_665 ?
Cl1 Rb7A 3.41(3) . ?
Cl2A Rb7A 0.78(3) . ?
Rb7A O26 2.98(3) 2_665 ?
Rb7A O24 3.07(3) 1_455 ?
Rb7A O13 3.34(3) . ?
Rb7A O25 3.34(3) 2_665 ?
Rb7A O26 3.42(3) 1_455 ?
Rb7A O7 3.46(3) 2_665 ?
P1 O2 1.436(13) . ?
P1 O3 1.486(11) . ?
P1 O1 1.530(16) . ?
P1 O4 1.600(14) . ?
P2 O7 1.486(14) . ?
P2 O5 1.511(11) . ?
P2 O6 1.521(13) . ?
P2 O8 1.549(14) . ?
P3 O11 1.504(11) . ?
P3 O12 1.514(12) . ?
P3 O9 1.532(8) . ?
P3 O10 1.547(10) . ?
P4 O14 1.508(10) . ?
P4 O16 1.515(10) . ?
P4 O15 1.515(12) . ?
P4 O13 1.516(11) . ?
P5 O18 1.505(11) . ?
P5 O19 1.522(11) . ?
P5 O20 1.523(10) . ?
P5 O17 1.527(11) . ?
O28A O28B 1.11(4) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O21 U1 O22 176.8(5) . . ?
O21 U1 O16 87.2(5) . 2_666 ?
O22 U1 O16 91.5(5) . 2_666 ?
O21 U1 O14 93.5(5) . 1_655 ?
O22 U1 O14 89.3(5) . 1_655 ?
O16 U1 O14 85.7(4) 2_666 1_655 ?
O21 U1 O10 91.0(5) . . ?
O22 U1 O10 91.0(5) . . ?
O16 U1 O10 165.3(4) 2_666 . ?
O14 U1 O10 79.9(3) 1_655 . ?
O21 U1 O9 91.1(4) . 2_666 ?
O22 U1 O9 85.7(4) . 2_666 ?
O16 U1 O9 72.0(4) 2_666 2_666 ?
O14 U1 O9 157.0(3) 1_655 2_666 ?
O10 U1 O9 122.6(3) . 2_666 ?
O21 U1 O10 87.2(5) . 2_666 ?
O22 U1 O10 91.3(5) . 2_666 ?
O16 U1 O10 129.9(4) 2_666 2_666 ?
O14 U1 O10 144.3(3) 1_655 2_666 ?
O10 U1 O10 64.5(4) . 2_666 ?
O9 U1 O10 58.4(3) 2_666 2_666 ?
O21 U1 P3 91.3(4) . 2_666 ?
O22 U1 P3 86.0(4) . 2_666 ?
O16 U1 P3 100.9(3) 2_666 2_666 ?
O14 U1 P3 172.0(3) 1_655 2_666 ?
O10 U1 P3 93.7(2) . 2_666 ?
O9 U1 P3 28.98(19) 2_666 2_666 ?
O10 U1 P3 29.6(2) 2_666 2_666 ?
O21 U1 Rb3A 53.6(4) . 2_666 ?
O22 U1 Rb3A 123.4(4) . 2_666 ?
O16 U1 Rb3A 53.1(5) 2_666 2_666 ?
O14 U1 Rb3A 123.7(4) 1_655 2_666 ?
O10 U1 Rb3A 135.0(5) . 2_666 ?
O9 U1 Rb3A 45.2(3) 2_666 2_666 ?
O10 U1 Rb3A 84.7(4) 2_666 2_666 ?
P3 U1 Rb3A 64.3(3) 2_666 2_666 ?
O21 U1 Rb6A 125.4(4) . 2_666 ?
O22 U1 Rb6A 51.6(4) . 2_666 ?
O16 U1 Rb6A 57.3(3) 2_666 2_666 ?
O14 U1 Rb6A 120.0(3) 1_655 2_666 ?
O10 U1 Rb6A 133.5(3) . 2_666 ?
O9 U1 Rb6A 42.2(2) 2_666 2_666 ?
O10 U1 Rb6A 87.2(3) 2_666 2_666 ?
P3 U1 Rb6A 61.46(7) 2_666 2_666 ?
Rb3A U1 Rb6A 71.85(18) 2_666 2_666 ?
O21 U1 Rb4B 139.7(4) . 1_655 ?
O22 U1 Rb4B 41.6(4) . 1_655 ?
O16 U1 Rb4B 65.5(4) 2_666 1_655 ?
O14 U1 Rb4B 57.2(4) 1_655 1_655 ?
O10 U1 Rb4B 108.0(4) . 1_655 ?
O9 U1 Rb4B 106.5(3) 2_666 1_655 ?
O10 U1 Rb4B 133.0(4) 2_666 1_655 ?
P3 U1 Rb4B 121.4(2) 2_666 1_655 ?
Rb3A U1 Rb4B 117.1(4) 2_666 1_655 ?
Rb6A U1 Rb4B 64.5(3) 2_666 1_655 ?
O21 U1 Rb3B 52.4(4) . 2_666 ?
O22 U1 Rb3B 124.4(4) . 2_666 ?
O16 U1 Rb3B 59.2(7) 2_666 2_666 ?
O14 U1 Rb3B 128.7(7) 1_655 2_666 ?
O10 U1 Rb3B 129.6(6) . 2_666 ?
O9 U1 Rb3B 42.6(5) 2_666 2_666 ?
O10 U1 Rb3B 78.6(8) 2_666 2_666 ?
P3 U1 Rb3B 59.2(7) 2_666 2_666 ?
Rb3A U1 Rb3B 6.3(4) 2_666 2_666 ?
Rb6A U1 Rb3B 73.2(2) 2_666 2_666 ?
Rb4B U1 Rb3B 122.4(6) 1_655 2_666 ?
O24 U2 O23 179.4(6) . . ?
O24 U2 O19 92.6(7) . 2_675 ?
O23 U2 O19 87.6(6) . 2_675 ?
O24 U2 O12 89.7(7) . . ?
O23 U2 O12 90.8(6) . . ?
O19 U2 O12 90.9(5) 2_675 . ?
O24 U2 O15 91.0(6) . 1_655 ?
O23 U2 O15 88.8(6) . 1_655 ?
O19 U2 O15 173.9(5) 2_675 1_655 ?
O12 U2 O15 94.0(5) . 1_655 ?
O24 U2 O18 90.7(6) . 1_655 ?
O23 U2 O18 88.8(5) . 1_655 ?
O19 U2 O18 89.0(5) 2_675 1_655 ?
O12 U2 O18 179.5(6) . 1_655 ?
O15 U2 O18 86.0(5) 1_655 1_655 ?
O24 U2 Rb5 129.2(5) . 1_565 ?
O23 U2 Rb5 50.7(4) . 1_565 ?
O19 U2 Rb5 49.1(4) 2_675 1_565 ?
O12 U2 Rb5 118.0(4) . 1_565 ?
O15 U2 Rb5 125.0(4) 1_655 1_565 ?
O18 U2 Rb5 61.6(3) 1_655 1_565 ?
O24 U2 Rb5 36.1(5) . 2_765 ?
O23 U2 Rb5 143.6(4) . 2_765 ?
O19 U2 Rb5 67.4(5) 2_675 2_765 ?
O12 U2 Rb5 114.6(5) . 2_765 ?
O15 U2 Rb5 113.5(4) 1_655 2_765 ?
O18 U2 Rb5 65.8(3) 1_655 2_765 ?
Rb5 U2 Rb5 93.32(4) 1_565 2_765 ?
O24 U2 Rb6C 65.7(6) . 1_655 ?
O23 U2 Rb6C 113.8(5) . 1_655 ?
O19 U2 Rb6C 139.4(5) 2_675 1_655 ?
O12 U2 Rb6C 121.1(5) . 1_655 ?
O15 U2 Rb6C 39.0(4) 1_655 1_655 ?
O18 U2 Rb6C 59.2(4) 1_655 1_655 ?
Rb5 U2 Rb6C 118.8(3) 1_565 1_655 ?
Rb5 U2 Rb6C 76.2(2) 2_765 1_655 ?
O24 U2 Rb6B 73.2(5) . 1_655 ?
O23 U2 Rb6B 106.3(5) . 1_655 ?
O19 U2 Rb6B 137.3(4) 2_675 1_655 ?
O12 U2 Rb6B 128.0(4) . 1_655 ?
O15 U2 Rb6B 39.8(4) 1_655 1_655 ?
O18 U2 Rb6B 52.3(4) 1_655 1_655 ?
Rb5 U2 Rb6B 110.4(2) 1_565 1_655 ?
Rb5 U2 Rb6B 79.1(2) 2_765 1_655 ?
Rb6C U2 Rb6B 9.0(3) 1_655 1_655 ?
O24 U2 Rb4B 140.3(5) . 2_666 ?
O23 U2 Rb4B 39.3(4) . 2_666 ?
O19 U2 Rb4B 123.1(5) 2_675 2_666 ?
O12 U2 Rb4B 105.0(5) . 2_666 ?
O15 U2 Rb4B 52.0(5) 1_655 2_666 ?
O18 U2 Rb4B 74.7(4) 1_655 2_666 ?
Rb5 U2 Rb4B 76.0(2) 1_565 2_666 ?
Rb5 U2 Rb4B 139.2(2) 2_765 2_666 ?
Rb6C U2 Rb4B 75.2(3) 1_655 2_666 ?
Rb6B U2 Rb4B 68.7(3) 1_655 2_666 ?
O24 U2 Rb4A 138.4(5) . 2_666 ?
O23 U2 Rb4A 41.2(4) . 2_666 ?
O19 U2 Rb4A 121.1(4) 2_675 2_666 ?
O12 U2 Rb4A 111.4(5) . 2_666 ?
O15 U2 Rb4A 53.6(4) 1_655 2_666 ?
O18 U2 Rb4A 68.3(4) 1_655 2_666 ?
Rb5 U2 Rb4A 72.76(12) 1_565 2_666 ?
Rb5 U2 Rb4A 133.07(15) 2_765 2_666 ?
Rb6C U2 Rb4A 72.7(3) 1_655 2_666 ?
Rb6B U2 Rb4A 65.5(3) 1_655 2_666 ?
Rb4B U2 Rb4A 6.49(18) 2_666 2_666 ?
O25 U3 O30 177.4(6) . 1_545 ?
O25 U3 O20 85.4(5) . 1_545 ?
O30 U3 O20 92.0(5) 1_545 1_545 ?
O25 U3 O17 87.2(5) . 2_665 ?
O30 U3 O17 92.1(5) 1_545 2_665 ?
O20 U3 O17 79.8(4) 1_545 2_665 ?
O25 U3 O5 92.4(6) . . ?
O30 U3 O5 89.9(5) 1_545 . ?
O20 U3 O5 160.8(4) 1_545 . ?
O17 U3 O5 81.0(4) 2_665 . ?
O25 U3 O1 90.5(6) . . ?
O30 U3 O1 89.3(6) 1_545 . ?
O20 U3 O1 77.4(5) 1_545 . ?
O17 U3 O1 157.2(5) 2_665 . ?
O5 U3 O1 121.8(5) . . ?
O25 U3 O4 80.9(5) . . ?
O30 U3 O4 101.0(5) 1_545 . ?
O20 U3 O4 129.2(4) 1_545 . ?
O17 U3 O4 147.0(4) 2_665 . ?
O5 U3 O4 69.0(4) . . ?
O1 U3 O4 54.2(5) . . ?
O25 U3 P1 84.6(4) . . ?
O30 U3 P1 96.3(4) 1_545 . ?
O20 U3 P1 101.8(3) 1_545 . ?
O17 U3 P1 171.4(3) 2_665 . ?
O5 U3 P1 97.0(3) . . ?
O1 U3 P1 25.6(4) . . ?
O4 U3 P1 28.6(3) . . ?
O25 U3 Rb6B 40.1(5) . 2_665 ?
O30 U3 Rb6B 138.2(5) 1_545 2_665 ?
O20 U3 Rb6B 65.1(4) 1_545 2_665 ?
O17 U3 Rb6B 51.4(4) 2_665 2_665 ?
O5 U3 Rb6B 101.5(4) . 2_665 ?
O1 U3 Rb6B 116.5(5) . 2_665 ?
O4 U3 Rb6B 120.7(4) . 2_665 ?
P1 U3 Rb6B 121.5(2) . 2_665 ?
O25 U3 Rb6C 35.1(5) . 2_665 ?
O30 U3 Rb6C 143.6(5) 1_545 2_665 ?
O20 U3 Rb6C 74.7(4) 1_545 2_665 ?
O17 U3 Rb6C 52.7(4) 2_665 2_665 ?
O5 U3 Rb6C 92.6(5) . 2_665 ?
O1 U3 Rb6C 119.3(5) . 2_665 ?
O4 U3 Rb6C 113.7(4) . 2_665 ?
P1 U3 Rb6C 119.3(2) . 2_665 ?
Rb6B U3 Rb6C 9.8(3) 2_665 2_665 ?
O25 U3 Rb6A 50.1(4) . 2_665 ?
O30 U3 Rb6A 127.8(4) 1_545 2_665 ?
O20 U3 Rb6A 52.6(3) 1_545 2_665 ?
O17 U3 Rb6A 49.7(3) 2_665 2_665 ?
O5 U3 Rb6A 112.4(4) . 2_665 ?
O1 U3 Rb6A 113.4(4) . 2_665 ?
O4 U3 Rb6A 130.7(3) . 2_665 ?
P1 U3 Rb6A 124.73(8) . 2_665 ?
Rb6B U3 Rb6A 13.3(3) 2_665 2_665 ?
Rb6C U3 Rb6A 23.1(3) 2_665 2_665 ?
O25 U3 Rb6A 142.0(4) . 1_545 ?
O30 U3 Rb6A 35.6(4) 1_545 1_545 ?
O20 U3 Rb6A 60.7(3) 1_545 1_545 ?
O17 U3 Rb6A 71.2(3) 2_665 1_545 ?
O5 U3 Rb6A 113.7(4) . 1_545 ?
O1 U3 Rb6A 97.7(4) . 1_545 ?
O4 U3 Rb6A 133.1(3) . 1_545 ?
P1 U3 Rb6A 117.00(8) . 1_545 ?
Rb6B U3 Rb6A 105.0(3) 2_665 1_545 ?
Rb6C U3 Rb6A 112.9(3) 2_665 1_545 ?
Rb6A U3 Rb6A 93.10(5) 2_665 1_545 ?
O27 U4 O26 178.9(5) . . ?
O27 U4 O7 91.7(6) . . ?
O26 U4 O7 89.3(5) . . ?
O27 U4 O11 93.5(5) . . ?
O26 U4 O11 87.0(5) . . ?
O7 U4 O11 89.6(6) . . ?
O27 U4 O13 88.2(5) . 1_655 ?
O26 U4 O13 90.9(5) . 1_655 ?
O7 U4 O13 173.9(6) . 1_655 ?
O11 U4 O13 84.3(4) . 1_655 ?
O27 U4 O3 95.5(6) . 1_655 ?
O26 U4 O3 83.9(5) . 1_655 ?
O7 U4 O3 95.2(6) . 1_655 ?
O11 U4 O3 169.7(5) . 1_655 ?
O13 U4 O3 90.9(5) 1_655 1_655 ?
O27 U4 Rb2 143.2(4) . 2_765 ?
O26 U4 Rb2 36.0(3) . 2_765 ?
O7 U4 Rb2 100.1(5) . 2_765 ?
O11 U4 Rb2 121.1(3) . 2_765 ?
O13 U4 Rb2 83.6(3) 1_655 2_765 ?
O3 U4 Rb2 49.1(3) 1_655 2_765 ?
O27 U4 Rb7A 145.4(5) . 2_665 ?
O26 U4 Rb7A 35.7(5) . 2_665 ?
O7 U4 Rb7A 54.4(5) . 2_665 ?
O11 U4 Rb7A 80.9(5) . 2_665 ?
O13 U4 Rb7A 124.7(5) 1_655 2_665 ?
O3 U4 Rb7A 94.4(6) 1_655 2_665 ?
Rb2 U4 Rb7A 60.7(3) 2_765 2_665 ?
O27 U4 Rb2 139.5(4) . . ?
O26 U4 Rb2 41.0(4) . . ?
O7 U4 Rb2 88.5(4) . . ?
O11 U4 Rb2 46.0(3) . . ?
O13 U4 Rb2 87.6(3) 1_655 . ?
O3 U4 Rb2 124.8(3) 1_655 . ?
Rb2 U4 Rb2 76.03(6) 2_765 . ?
Rb7A U4 Rb2 45.9(4) 2_665 . ?
O27 U4 Rb7A 134.6(5) . 1_655 ?
O26 U4 Rb7A 44.5(5) . 1_655 ?
O7 U4 Rb7A 133.7(5) . 1_655 ?
O11 U4 Rb7A 87.6(5) . 1_655 ?
O13 U4 Rb7A 46.6(4) 1_655 1_655 ?
O3 U4 Rb7A 82.5(5) 1_655 1_655 ?
Rb2 U4 Rb7A 45.4(4) 2_765 1_655 ?
Rb7A U4 Rb7A 79.7(5) 2_665 1_655 ?
Rb2 U4 Rb7A 57.8(3) . 1_655 ?
O27 U4 Rb3B 92.8(6) . . ?
O26 U4 Rb3B 88.3(5) . . ?
O7 U4 Rb3B 42.3(6) . . ?
O11 U4 Rb3B 47.3(4) . . ?
O13 U4 Rb3B 131.6(4) 1_655 . ?
O3 U4 Rb3B 136.9(6) 1_655 . ?
Rb2 U4 Rb3B 119.2(5) 2_765 . ?
Rb7A U4 Rb3B 58.5(6) 2_665 . ?
Rb2 U4 Rb3B 61.5(2) . . ?
Rb7A U4 Rb3B 119.4(4) 1_655 . ?
O27 U4 Rb5 108.4(4) . . ?
O26 U4 Rb5 72.0(4) . . ?
O7 U4 Rb5 47.6(5) . . ?
O11 U4 Rb5 130.7(3) . . ?
O13 U4 Rb5 138.0(3) 1_655 . ?
O3 U4 Rb5 50.4(4) 1_655 . ?
Rb2 U4 Rb5 59.84(5) 2_765 . ?
Rb7A U4 Rb5 55.9(4) 2_665 . ?
Rb2 U4 Rb5 101.33(5) . . ?
Rb7A U4 Rb5 104.8(4) 1_655 . ?
Rb3B U4 Rb5 87.0(4) . . ?
U5C U5A U5B 45.9(10) . . ?
U5C U5A O29 72.1(10) . . ?
U5B U5A O29 87.6(6) . . ?
U5C U5A O28A 110.0(11) . . ?
U5B U5A O28A 94.9(7) . . ?
O29 U5A O28A 177.5(6) . . ?
U5C U5A O28B 82.7(17) . . ?
U5B U5A O28B 61.0(12) . . ?
O29 U5A O28B 148.4(12) . . ?
O28A U5A O28B 34.1(12) . . ?
U5C U5A O6 62.6(12) . . ?
U5B U5A O6 102.8(6) . . ?
O29 U5A O6 96.1(5) . . ?
O28A U5A O6 83.7(6) . . ?
O28B U5A O6 88.5(14) . . ?
U5C U5A O8 29.3(13) . 2_656 ?
U5B U5A O8 21.8(7) . 2_656 ?
O29 U5A O8 91.1(5) . 2_656 ?
O28A U5A O8 91.3(6) . 2_656 ?
O28B U5A O8 58.6(12) . 2_656 ?
O6 U5A O8 81.1(5) . 2_656 ?
U5C U5A O4 126.5(13) . . ?
U5B U5A O4 172.0(7) . . ?
O29 U5A O4 87.0(5) . . ?
O28A U5A O4 90.5(6) . . ?
O28B U5A O4 123.9(12) . . ?
O6 U5A O4 71.9(4) . . ?
O8 U5A O4 152.6(5) 2_656 . ?
U5C U5A O2 108.2(13) . 2_556 ?
U5B U5A O2 64.8(7) . 2_556 ?
O29 U5A O2 90.9(5) . 2_556 ?
O28A U5A O2 89.8(6) . 2_556 ?
O28B U5A O2 79.1(14) . 2_556 ?
O6 U5A O2 165.6(5) . 2_556 ?
O8 U5A O2 86.3(6) 2_656 2_556 ?
O4 U5A O2 121.1(5) . 2_556 ?
U5C U5A O2 158.0(10) . . ?
U5B U5A O2 128.0(6) . . ?
O29 U5A O2 87.3(5) . . ?
O28A U5A O2 90.8(6) . . ?
O28B U5A O2 113.7(14) . . ?
O6 U5A O2 129.2(4) . . ?
O8 U5A O2 149.7(5) 2_656 . ?
O4 U5A O2 57.6(4) . . ?
O2 U5A O2 63.6(5) 2_556 . ?
U5C U5A P1 151.9(12) . . ?
U5B U5A P1 155.0(6) . . ?
O29 U5A P1 87.5(4) . . ?
O28A U5A P1 90.0(5) . . ?
O28B U5A P1 122.1(12) . . ?
O6 U5A P1 102.0(3) . . ?
O8 U5A P1 176.7(4) 2_656 . ?
O4 U5A P1 30.3(3) . . ?
O2 U5A P1 90.8(4) 2_556 . ?
O2 U5A P1 27.2(3) . . ?
U5C U5A Rb1 57.4(10) . . ?
U5B U5A Rb1 68.5(5) . . ?
O29 U5A Rb1 127.4(3) . . ?
O28A U5A Rb1 54.2(5) . . ?
O28B U5A Rb1 40.8(14) . . ?
O6 U5A Rb1 49.6(3) . . ?
O8 U5A Rb1 50.9(4) 2_656 . ?
O4 U5A Rb1 110.6(3) . . ?
O2 U5A Rb1 116.6(4) 2_556 . ?
O2 U5A Rb1 144.4(3) . . ?
P1 U5A Rb1 132.05(9) . . ?
U5A U5B O28B 102.2(14) . . ?
U5A U5B O8 151.3(9) . 2_656 ?
O28B U5B O8 73.3(15) . 2_656 ?
U5A U5B O29 73.8(6) . . ?
O28B U5B O29 174.9(15) . . ?
O8 U5B O29 108.6(6) 2_656 . ?
U5A U5B O28A 67.8(6) . . ?
O28B U5B O28A 34.6(13) . . ?
O8 U5B O28A 105.3(7) 2_656 . ?
O29 U5B O28A 141.6(6) . . ?
U5A U5B O2 101.8(7) . 2_556 ?
O28B U5B O2 88.7(16) . 2_556 ?
O8 U5B O2 106.4(7) 2_656 2_556 ?
O29 U5B O2 95.3(6) . 2_556 ?
O28A U5B O2 92.1(7) . 2_556 ?
U5A U5B O6 64.1(6) . . ?
O28B U5B O6 87.4(15) . . ?
O8 U5B O6 87.2(6) 2_656 . ?
O29 U5B O6 87.9(5) . . ?
O28A U5B O6 76.0(6) . . ?
O2 U5B O6 164.0(5) 2_556 . ?
U5A U5B P2 147.6(7) . 2_656 ?
O28B U5B P2 90.2(14) . 2_656 ?
O8 U5B P2 16.9(5) 2_656 2_656 ?
O29 U5B P2 91.7(4) . 2_656 ?
O28A U5B P2 121.4(5) . 2_656 ?
O2 U5B P2 108.4(4) 2_556 2_656 ?
O6 U5B P2 87.1(4) . 2_656 ?
U5A U5B Rb1 103.5(5) . . ?
O28B U5B Rb1 43.4(16) . . ?
O8 U5B Rb1 53.3(5) 2_656 . ?
O29 U5B Rb1 133.7(4) . . ?
O28A U5B Rb1 59.3(5) . . ?
O2 U5B Rb1 129.4(5) 2_556 . ?
O6 U5B Rb1 53.0(3) . . ?
P2 U5B Rb1 65.69(12) 2_656 . ?
U5A U5B Rb5 153.3(6) . 2_656 ?
O28B U5B Rb5 53.1(13) . 2_656 ?
O8 U5B Rb5 41.0(5) 2_656 2_656 ?
O29 U5B Rb5 131.5(4) . 2_656 ?
O28A U5B Rb5 86.5(4) . 2_656 ?
O2 U5B Rb5 71.0(5) 2_556 2_656 ?
O6 U5B Rb5 117.9(3) . 2_656 ?
P2 U5B Rb5 53.24(11) 2_656 2_656 ?
Rb1 U5B Rb5 66.72(9) . 2_656 ?
U5A U5B Rb4B 78.7(6) . . ?
O28B U5B Rb4B 35.8(15) . . ?
O8 U5B Rb4B 107.0(5) 2_656 . ?
O29 U5B Rb4B 143.7(4) . . ?
O28A U5B Rb4B 24.9(5) . . ?
O2 U5B Rb4B 67.6(4) 2_556 . ?
O6 U5B Rb4B 100.9(4) . . ?
P2 U5B Rb4B 123.6(3) 2_656 . ?
Rb1 U5B Rb4B 75.44(19) . . ?
Rb5 U5B Rb4B 74.9(3) 2_656 . ?
U5A U5B Rb4A 82.3(5) . . ?
O28B U5B Rb4A 38.3(15) . . ?
O8 U5B Rb4A 106.5(5) 2_656 . ?
O29 U5B Rb4A 142.2(4) . . ?
O28A U5B Rb4A 31.6(5) . . ?
O2 U5B Rb4A 61.2(4) 2_556 . ?
O6 U5B Rb4A 107.6(4) . . ?
P2 U5B Rb4A 122.62(19) 2_656 . ?
Rb1 U5B Rb4A 79.82(15) . . ?
Rb5 U5B Rb4A 71.74(15) 2_656 . ?
Rb4B U5B Rb4A 6.66(18) . . ?
U5A U5C O29 88.9(11) . . ?
U5A U5C O8 142.0(16) . 2_656 ?
O29 U5C O8 113.3(8) . 2_656 ?
U5A U5C O28B 80.7(17) . . ?
O29 U5C O28B 158.3(16) . . ?
O8 U5C O28B 67.3(13) 2_656 . ?
U5A U5C O28A 55.1(10) . . ?
O29 U5C O28A 144.0(9) . . ?
O8 U5C O28A 98.6(8) 2_656 . ?
O28B U5C O28A 31.9(12) . . ?
U5A U5C O6 103.6(14) . . ?
O29 U5C O6 106.8(8) . . ?
O8 U5C O6 98.9(8) 2_656 . ?
O28B U5C O6 94.2(14) . . ?
O28A U5C O6 83.1(7) . . ?
U5A U5C O2 60.2(11) . 2_556 ?
O29 U5C O2 85.0(7) . 2_556 ?
O8 U5C O2 90.2(8) 2_656 2_556 ?
O28B U5C O2 73.2(15) . 2_556 ?
O28A U5C O2 78.3(7) . 2_556 ?
O6 U5C O2 160.3(7) . 2_556 ?
U5A U5C O4 44.1(11) . . ?
O29 U5C O4 76.8(6) . . ?
O8 U5C O4 165.3(8) 2_656 . ?
O28B U5C O4 107.4(13) . . ?
O28A U5C O4 75.5(6) . . ?
O6 U5C O4 67.3(5) . . ?
O2 U5C O4 101.5(6) 2_556 . ?
U5A U5C P2 158.3(15) . 2_656 ?
O29 U5C P2 95.9(6) . 2_656 ?
O8 U5C P2 20.2(5) 2_656 2_656 ?
O28B U5C P2 87.4(13) . 2_656 ?
O28A U5C P2 118.1(6) . 2_656 ?
O6 U5C P2 95.3(5) . 2_656 ?
O2 U5C P2 99.1(5) 2_556 2_656 ?
O4 U5C P2 157.4(5) . 2_656 ?
U5A U5C P2 107.2(13) . . ?
O29 U5C P2 86.9(6) . . ?
O8 U5C P2 104.5(7) 2_656 . ?
O28B U5C P2 114.4(14) . . ?
O28A U5C P2 101.3(6) . . ?
O6 U5C P2 20.2(4) . . ?
O2 U5C P2 165.1(6) 2_556 . ?
O4 U5C P2 64.4(4) . . ?
P2 U5C P2 94.2(3) 2_656 . ?
U5A U5C Rb1 115.3(10) . . ?
O29 U5C Rb1 151.6(6) . . ?
O8 U5C Rb1 56.3(5) 2_656 . ?
O28B U5C Rb1 48.2(14) . . ?
O28A U5C Rb1 61.6(5) . . ?
O6 U5C Rb1 55.2(4) . . ?
O2 U5C Rb1 119.1(5) 2_556 . ?
O4 U5C Rb1 109.6(4) . . ?
P2 U5C Rb1 67.3(2) 2_656 . ?
P2 U5C Rb1 72.4(2) . . ?
U5A U5C Rb1 123.8(12) . 2_656 ?
O29 U5C Rb1 39.3(4) . 2_656 ?
O8 U5C Rb1 89.6(6) 2_656 2_656 ?
O28B U5C Rb1 155.5(14) . 2_656 ?
O28A U5C Rb1 162.7(7) . 2_656 ?
O6 U5C Rb1 80.6(5) . 2_656 ?
O2 U5C Rb1 117.0(4) 2_556 2_656 ?
O4 U5C Rb1 92.8(4) . 2_656 ?
P2 U5C Rb1 69.4(2) 2_656 2_656 ?
P2 U5C Rb1 61.8(2) . 2_656 ?
Rb1 U5C Rb1 112.3(3) . 2_656 ?
O28B Rb1 O22 157.5(8) . . ?
O28B Rb1 O21 69.5(8) . 2_666 ?
O22 Rb1 O21 89.6(3) . 2_666 ?
O28B Rb1 O29 117.2(8) . 2_656 ?
O22 Rb1 O29 84.6(3) . 2_656 ?
O21 Rb1 O29 143.6(3) 2_666 2_656 ?
O28B Rb1 O6 59.9(8) . . ?
O22 Rb1 O6 128.0(3) . . ?
O21 Rb1 O6 83.2(4) 2_666 . ?
O29 Rb1 O6 72.6(3) 2_656 . ?
O28B Rb1 O8 40.8(8) . 2_656 ?
O22 Rb1 O8 160.9(3) . 2_656 ?
O21 Rb1 O8 109.5(3) 2_666 2_656 ?
O29 Rb1 O8 80.1(3) 2_656 2_656 ?
O6 Rb1 O8 57.4(3) . 2_656 ?
O28B Rb1 O23 52.9(8) . 2_666 ?
O22 Rb1 O23 111.2(3) . 2_666 ?
O21 Rb1 O23 65.0(3) 2_666 2_666 ?
O29 Rb1 O23 149.5(3) 2_656 2_666 ?
O6 Rb1 O23 111.8(3) . 2_666 ?
O8 Rb1 O23 78.1(4) 2_656 2_666 ?
O28B Rb1 O30 126.4(8) . 2_666 ?
O22 Rb1 O30 68.6(3) . 2_666 ?
O21 Rb1 O30 149.3(3) 2_666 2_666 ?
O29 Rb1 O30 58.4(3) 2_656 2_666 ?
O6 Rb1 O30 127.1(4) . 2_666 ?
O8 Rb1 O30 93.5(3) 2_656 2_666 ?
O23 Rb1 O30 101.9(3) 2_666 2_666 ?
O28B Rb1 O28A 18.9(8) . . ?
O22 Rb1 O28A 144.6(3) . . ?
O21 Rb1 O28A 55.3(3) 2_666 . ?
O29 Rb1 O28A 119.7(3) 2_656 . ?
O6 Rb1 O28A 50.8(4) . . ?
O8 Rb1 O28A 54.5(4) 2_656 . ?
O23 Rb1 O28A 61.6(3) 2_666 . ?
O30 Rb1 O28A 145.0(3) 2_666 . ?
O28B Rb1 O27 131.3(8) . . ?
O22 Rb1 O27 57.8(3) . . ?
O21 Rb1 O27 97.6(3) 2_666 . ?
O29 Rb1 O27 49.6(3) 2_656 . ?
O6 Rb1 O27 72.2(3) . . ?
O8 Rb1 O27 117.6(4) 2_656 . ?
O23 Rb1 O27 160.6(3) 2_666 . ?
O30 Rb1 O27 89.0(3) 2_666 . ?
O28A Rb1 O27 116.6(3) . . ?
O28B Rb1 O5 78.7(8) . 2_656 ?
O22 Rb1 O5 119.5(3) . 2_656 ?
O21 Rb1 O5 146.4(3) 2_666 2_656 ?
O29 Rb1 O5 62.1(3) 2_656 2_656 ?
O6 Rb1 O5 90.2(3) . 2_656 ?
O8 Rb1 O5 42.5(3) 2_656 2_656 ?
O23 Rb1 O5 87.5(3) 2_666 2_656 ?
O30 Rb1 O5 51.0(3) 2_666 2_656 ?
O28A Rb1 O5 95.5(3) . 2_656 ?
O27 Rb1 O5 111.7(3) . 2_656 ?
O28B Rb1 U5C 30.8(8) . . ?
O22 Rb1 U5C 161.8(3) . . ?
O21 Rb1 U5C 86.4(3) 2_666 . ?
O29 Rb1 U5C 88.1(3) 2_656 . ?
O6 Rb1 U5C 33.9(3) . . ?
O8 Rb1 U5C 29.1(3) 2_656 . ?
O23 Rb1 U5C 83.1(3) 2_666 . ?
O30 Rb1 U5C 120.8(3) 2_666 . ?
O28A Rb1 U5C 33.2(3) . . ?
O27 Rb1 U5C 105.2(3) . . ?
O5 Rb1 U5C 70.7(2) 2_656 . ?
O26 Rb2 Cl1 106.5(4) 2_765 . ?
O26 Rb2 O24 85.1(3) 2_765 . ?
Cl1 Rb2 O24 168.1(5) . . ?
O26 Rb2 O25 130.4(3) 2_765 2_665 ?
Cl1 Rb2 O25 69.5(4) . 2_665 ?
O24 Rb2 O25 105.2(4) . 2_665 ?
O26 Rb2 O3 53.8(3) 2_765 2_665 ?
Cl1 Rb2 O3 96.2(5) . 2_665 ?
O24 Rb2 O3 92.9(4) . 2_665 ?
O25 Rb2 O3 77.0(3) 2_665 2_665 ?
O26 Rb2 O26 61.9(4) 2_765 . ?
Cl1 Rb2 O26 96.9(4) . . ?
O24 Rb2 O26 86.1(3) . . ?
O25 Rb2 O26 163.1(3) 2_665 . ?
O3 Rb2 O26 115.5(3) 2_665 . ?
O26 Rb2 O11 112.2(3) 2_765 . ?
Cl1 Rb2 O11 95.7(5) . . ?
O24 Rb2 O11 76.9(4) . . ?
O25 Rb2 O11 117.4(3) 2_665 . ?
O3 Rb2 O11 163.9(3) 2_665 . ?
O26 Rb2 O11 52.2(3) . . ?
O26 Rb2 Rb7A 65.9(5) 2_765 2_665 ?
Cl1 Rb2 Rb7A 49.2(5) . 2_665 ?
O24 Rb2 Rb7A 138.0(5) . 2_665 ?
O25 Rb2 Rb7A 116.6(5) 2_665 2_665 ?
O3 Rb2 Rb7A 93.3(5) 2_665 2_665 ?
O26 Rb2 Rb7A 54.0(5) . 2_665 ?
O11 Rb2 Rb7A 86.4(5) . 2_665 ?
O26 Rb2 Cl1 118.7(4) 2_765 2_665 ?
Cl1 Rb2 Cl1 12.4(7) . 2_665 ?
O24 Rb2 Cl1 156.2(4) . 2_665 ?
O25 Rb2 Cl1 60.6(4) 2_665 2_665 ?
O3 Rb2 Cl1 101.4(5) 2_665 2_665 ?
O26 Rb2 Cl1 104.3(4) . 2_665 ?
O11 Rb2 Cl1 92.5(4) . 2_665 ?
Rb7A Rb2 Cl1 60.6(5) 2_665 2_665 ?
O26 Rb2 O12 128.0(3) 2_765 . ?
Cl1 Rb2 O12 118.3(4) . . ?
O24 Rb2 O12 50.2(3) . . ?
O25 Rb2 O12 91.0(3) 2_665 . ?
O3 Rb2 O12 136.9(3) 2_665 . ?
O26 Rb2 O12 86.8(3) . . ?
O11 Rb2 O12 42.1(3) . . ?
Rb7A Rb2 O12 128.3(5) 2_665 . ?
Cl1 Rb2 O12 108.3(4) 2_665 . ?
O26 Rb2 P3 131.7(2) 2_765 . ?
Cl1 Rb2 P3 98.9(4) . . ?
O24 Rb2 P3 70.7(3) . . ?
O25 Rb2 P3 96.7(2) 2_665 . ?
O3 Rb2 P3 160.5(3) 2_665 . ?
O26 Rb2 P3 75.0(2) . . ?
O11 Rb2 P3 23.24(19) . . ?
Rb7A Rb2 P3 105.9(5) 2_665 . ?
Cl1 Rb2 P3 91.2(4) 2_665 . ?
O12 Rb2 P3 23.65(19) . . ?
O26 Rb2 P1 73.0(2) 2_765 2_665 ?
Cl1 Rb2 P1 95.7(4) . 2_665 ?
O24 Rb2 P1 90.3(3) . 2_665 ?
O25 Rb2 P1 58.9(2) 2_665 2_665 ?
O3 Rb2 P1 19.7(2) 2_665 2_665 ?
O26 Rb2 P1 134.8(2) . 2_665 ?
O11 Rb2 P1 165.4(2) . 2_665 ?
Rb7A Rb2 P1 107.9(5) 2_665 2_665 ?
Cl1 Rb2 P1 96.7(4) 2_665 2_665 ?
O12 Rb2 P1 123.7(2) . 2_665 ?
P3 Rb2 P1 144.67(11) . 2_665 ?
O4 Rb3A O9 160.8(8) . . ?
O4 Rb3A Cl1 105.2(5) . 2_665 ?
O9 Rb3A Cl1 90.3(5) . 2_665 ?
O4 Rb3A O16 129.2(6) . . ?
O9 Rb3A O16 52.8(3) . . ?
Cl1 Rb3A O16 107.6(6) 2_665 . ?
O4 Rb3A O21 107.0(4) . 2_666 ?
O9 Rb3A O21 58.0(3) . 2_666 ?
Cl1 Rb3A O21 147.8(5) 2_665 2_666 ?
O16 Rb3A O21 50.4(3) . 2_666 ?
O4 Rb3A O13 101.5(7) . . ?
O9 Rb3A O13 90.2(5) . . ?
Cl1 Rb3A O13 87.4(6) 2_665 . ?
O16 Rb3A O13 43.7(4) . . ?
O21 Rb3A O13 87.2(5) 2_666 . ?
O4 Rb3A O6 51.5(4) . . ?
O9 Rb3A O6 109.8(7) . . ?
Cl1 Rb3A O6 128.9(7) 2_665 . ?
O16 Rb3A O6 122.2(4) . . ?
O21 Rb3A O6 73.2(4) 2_666 . ?
O13 Rb3A O6 136.5(4) . . ?
O4 Rb3A Cl1 101.1(5) . . ?
O9 Rb3A Cl1 91.7(5) . . ?
Cl1 Rb3A Cl1 12.3(4) 2_665 . ?
O16 Rb3A Cl1 117.8(6) . . ?
O21 Rb3A Cl1 149.1(5) 2_666 . ?
O13 Rb3A Cl1 99.6(6) . . ?
O6 Rb3A Cl1 117.2(6) . . ?
O4 Rb3A O3 46.8(4) . . ?
O9 Rb3A O3 147.0(8) . . ?
Cl1 Rb3A O3 89.1(6) 2_665 . ?
O16 Rb3A O3 96.2(7) . . ?
O21 Rb3A O3 113.9(5) 2_666 . ?
O13 Rb3A O3 56.8(5) . . ?
O6 Rb3A O3 96.0(3) . . ?
Cl1 Rb3A O3 94.6(5) . . ?
O4 Rb3A O28A 56.4(4) . . ?
O9 Rb3A O28A 109.0(4) . . ?
Cl1 Rb3A O28A 160.7(6) 2_665 . ?
O16 Rb3A O28A 83.6(4) . . ?
O21 Rb3A O28A 51.1(3) 2_666 . ?
O13 Rb3A O28A 90.4(5) . . ?
O6 Rb3A O28A 47.1(4) . . ?
Cl1 Rb3A O28A 157.1(5) . . ?
O3 Rb3A O28A 73.7(4) . . ?
O4 Rb3A P1 23.7(3) . . ?
O9 Rb3A P1 163.5(6) . . ?
Cl1 Rb3A P1 100.7(5) 2_665 . ?
O16 Rb3A P1 111.5(6) . . ?
O21 Rb3A P1 109.2(3) 2_666 . ?
O13 Rb3A P1 78.2(5) . . ?
O6 Rb3A P1 72.7(3) . . ?
Cl1 Rb3A P1 101.7(4) . . ?
O3 Rb3A P1 23.5(2) . . ?
O28A Rb3A P1 60.1(3) . . ?
O4 Rb3A Rb6C 148.8(8) . . ?
O9 Rb3A Rb6C 50.1(4) . . ?
Cl1 Rb3A Rb6C 56.5(5) 2_665 . ?
O16 Rb3A Rb6C 52.2(4) . . ?
O21 Rb3A Rb6C 94.6(4) 2_666 . ?
O13 Rb3A Rb6C 56.4(5) . . ?
O6 Rb3A Rb6C 159.6(6) . . ?
Cl1 Rb3A Rb6C 65.8(5) . . ?
O3 Rb3A Rb6C 104.0(7) . . ?
O28A Rb3A Rb6C 135.6(6) . . ?
P1 Rb3A Rb6C 127.5(7) . . ?
O4 Rb3B O9 161.2(18) . . ?
O4 Rb3B Cl1 105.5(7) . 2_665 ?
O9 Rb3B Cl1 90.4(6) . 2_665 ?
O4 Rb3B O6 54.9(5) . . ?
O9 Rb3B O6 117.5(7) . . ?
Cl1 Rb3B O6 140.5(17) 2_665 . ?
O4 Rb3B O7 83.5(10) . . ?
O9 Rb3B O7 102.5(12) . . ?
Cl1 Rb3B O7 104.6(16) 2_665 . ?
O6 Rb3B O7 45.4(7) . . ?
O4 Rb3B Cl1 103.8(9) . . ?
O9 Rb3B Cl1 93.9(7) . . ?
Cl1 Rb3B Cl1 13.2(5) 2_665 . ?
O6 Rb3B Cl1 129.0(18) . . ?
O7 Rb3B Cl1 91.5(15) . . ?
O4 Rb3B O11 139.8(16) . . ?
O9 Rb3B O11 45.9(5) . . ?
Cl1 Rb3B O11 93.8(10) 2_665 . ?
O6 Rb3B O11 88.0(10) . . ?
O7 Rb3B O11 57.3(9) . . ?
Cl1 Rb3B O11 87.2(11) . . ?
O4 Rb3B O21 104.8(10) . 2_666 ?
O9 Rb3B O21 56.9(6) . 2_666 ?
Cl1 Rb3B O21 143.1(11) 2_665 2_666 ?
O6 Rb3B O21 75.4(5) . 2_666 ?
O7 Rb3B O21 99.3(7) . 2_666 ?
Cl1 Rb3B O21 150.3(7) . 2_666 ?
O11 Rb3B O21 75.9(4) . 2_666 ?
O4 Rb3B P2 60.4(7) . . ?
O9 Rb3B P2 121.3(11) . . ?
Cl1 Rb3B P2 116.9(16) 2_665 . ?
O6 Rb3B P2 25.2(4) . . ?
O7 Rb3B P2 24.6(4) . . ?
Cl1 Rb3B P2 104.5(15) . . ?
O11 Rb3B P2 79.4(11) . . ?
O21 Rb3B P2 96.3(5) 2_666 . ?
O4 Rb3B O28A 55.2(6) . . ?
O9 Rb3B O28A 106.4(11) . . ?
Cl1 Rb3B O28A 152.9(13) 2_665 . ?
O6 Rb3B O28A 47.9(4) . . ?
O7 Rb3B O28A 92.5(6) . . ?
Cl1 Rb3B O28A 157.9(7) . . ?
O11 Rb3B O28A 113.1(6) . . ?
O21 Rb3B O28A 49.7(6) 2_666 . ?
P2 Rb3B O28A 72.6(4) . . ?
O4 Rb3B O16 117.0(18) . . ?
O9 Rb3B O16 48.7(7) . . ?
Cl1 Rb3B O16 99.7(10) 2_665 . ?
O6 Rb3B O16 119.6(11) . . ?
O7 Rb3B O16 142.4(6) . . ?
Cl1 Rb3B O16 111.4(8) . . ?
O11 Rb3B O16 93.2(5) . . ?
O21 Rb3B O16 46.9(7) 2_666 . ?
P2 Rb3B O16 142.9(7) . . ?
O28A Rb3B O16 77.4(11) . . ?
O4 Rb3B P3 155.3(9) . . ?
O9 Rb3B P3 22.7(3) . . ?
Cl1 Rb3B P3 96.2(7) 2_665 . ?
O6 Rb3B P3 100.7(8) . . ?
O7 Rb3B P3 79.7(9) . . ?
Cl1 Rb3B P3 94.6(8) . . ?
O11 Rb3B P3 23.8(2) . . ?
O21 Rb3B P3 60.8(4) 2_666 . ?
P2 Rb3B P3 99.4(10) . . ?
O28A Rb3B P3 107.5(6) . . ?
O16 Rb3B P3 69.4(5) . . ?
O28A Rb4A O22 154.0(6) . 1_455 ?
O28A Rb4A O28B 21.4(8) . . ?
O22 Rb4A O28B 174.5(9) 1_455 . ?
O28A Rb4A O29 95.1(4) . 2_556 ?
O22 Rb4A O29 82.7(3) 1_455 2_556 ?
O28B Rb4A O29 99.6(9) . 2_556 ?
O28A Rb4A O30 131.4(5) . 2_566 ?
O22 Rb4A O30 68.9(4) 1_455 2_566 ?
O28B Rb4A O30 116.6(9) . 2_566 ?
O29 Rb4A O30 58.4(4) 2_556 2_566 ?
O28A Rb4A O27 96.9(5) . 1_455 ?
O22 Rb4A O27 61.3(4) 1_455 1_455 ?
O28B Rb4A O27 116.3(8) . 1_455 ?
O29 Rb4A O27 52.4(3) 2_556 1_455 ?
O30 Rb4A O27 95.9(4) 2_566 1_455 ?
O28A Rb4A O23 67.5(4) . 2_666 ?
O22 Rb4A O23 129.6(4) 1_455 2_666 ?
O28B Rb4A O23 51.1(8) . 2_666 ?
O29 Rb4A O23 137.6(4) 2_556 2_666 ?
O30 Rb4A O23 103.6(4) 2_566 2_666 ?
O27 Rb4A O23 160.2(5) 1_455 2_666 ?
O28A Rb4A O15 111.3(5) . 2_566 ?
O22 Rb4A O15 79.6(3) 1_455 2_566 ?
O28B Rb4A O15 100.3(8) . 2_566 ?
O29 Rb4A O15 150.0(5) 2_556 2_566 ?
O30 Rb4A O15 92.4(4) 2_566 2_566 ?
O27 Rb4A O15 133.2(4) 1_455 2_566 ?
O23 Rb4A O15 50.4(3) 2_666 2_566 ?
O28A Rb4A P4 112.9(4) . 2_566 ?
O22 Rb4A P4 68.6(3) 1_455 2_566 ?
O28B Rb4A P4 109.4(8) . 2_566 ?
O29 Rb4A P4 150.8(3) 2_556 2_566 ?
O30 Rb4A P4 104.4(3) 2_566 2_566 ?
O27 Rb4A P4 113.2(3) 1_455 2_566 ?
O23 Rb4A P4 65.5(3) 2_666 2_566 ?
O15 Rb4A P4 21.4(2) 2_566 2_566 ?
O28A Rb4A Rb6A 151.9(4) . 2_566 ?
O22 Rb4A Rb6A 52.2(3) 1_455 2_566 ?
O28B Rb4A Rb6A 131.5(8) . 2_566 ?
O29 Rb4A Rb6A 101.3(3) 2_556 2_566 ?
O30 Rb4A Rb6A 47.1(3) 2_566 2_566 ?
O27 Rb4A Rb6A 111.2(3) 1_455 2_566 ?
O23 Rb4A Rb6A 85.2(3) 2_666 2_566 ?
O15 Rb4A Rb6A 48.8(3) 2_566 2_566 ?
P4 Rb4A Rb6A 57.24(12) 2_566 2_566 ?
O28A Rb4A U5A 18.9(3) . . ?
O22 Rb4A U5A 153.0(3) 1_455 . ?
O28B Rb4A U5A 25.8(8) . . ?
O29 Rb4A U5A 77.7(3) 2_556 . ?
O30 Rb4A U5A 114.5(3) 2_566 . ?
O27 Rb4A U5A 91.9(3) 1_455 . ?
O23 Rb4A U5A 76.9(3) 2_666 . ?
O15 Rb4A U5A 125.7(3) 2_566 . ?
P4 Rb4A U5A 131.0(2) 2_566 . ?
Rb6A Rb4A U5A 150.3(3) 2_566 . ?
O28A Rb4A U5B 21.6(3) . . ?
O22 Rb4A U5B 159.2(3) 1_455 . ?
O28B Rb4A U5B 20.9(8) . . ?
O29 Rb4A U5B 79.6(3) 2_556 . ?
O30 Rb4A U5B 109.9(3) 2_566 . ?
O27 Rb4A U5B 98.9(3) 1_455 . ?
O23 Rb4A U5B 71.2(3) 2_666 . ?
O15 Rb4A U5B 121.0(3) 2_566 . ?
P4 Rb4A U5B 129.6(2) 2_566 . ?
Rb6A Rb4A U5B 142.6(3) 2_566 . ?
U5A Rb4A U5B 7.88(6) . . ?
O28A Rb4B O28B 21.8(8) . . ?
O28A Rb4B O22 161.3(8) . 1_455 ?
O28B Rb4B O22 166.9(11) . 1_455 ?
O28A Rb4B O23 70.6(5) . 2_666 ?
O28B Rb4B O23 52.5(8) . 2_666 ?
O22 Rb4B O23 127.9(7) 1_455 2_666 ?
O28A Rb4B O27 101.2(7) . 1_455 ?
O28B Rb4B O27 119.0(10) . 1_455 ?
O22 Rb4B O27 60.2(4) 1_455 1_455 ?
O23 Rb4B O27 171.5(7) 2_666 1_455 ?
O28A Rb4B O21 58.1(5) . 2_666 ?
O28B Rb4B O21 63.5(9) . 2_666 ?
O22 Rb4B O21 129.3(6) 1_455 2_666 ?
O23 Rb4B O21 61.4(4) 2_666 2_666 ?
O27 Rb4B O21 116.7(6) 1_455 2_666 ?
O28A Rb4B O29 91.0(6) . 2_556 ?
O28B Rb4B O29 94.1(10) . 2_556 ?
O22 Rb4B O29 75.7(4) 1_455 2_556 ?
O23 Rb4B O29 126.8(6) 2_666 2_556 ?
O27 Rb4B O29 49.4(3) 1_455 2_556 ?
O21 Rb4B O29 145.3(6) 2_666 2_556 ?
O28A Rb4B O15 119.0(6) . 2_566 ?
O28B Rb4B O15 103.8(9) . 2_566 ?
O22 Rb4B O15 79.3(5) 1_455 2_566 ?
O23 Rb4B O15 51.6(4) 2_666 2_566 ?
O27 Rb4B O15 136.9(6) 1_455 2_566 ?
O21 Rb4B O15 76.8(4) 2_666 2_566 ?
O29 Rb4B O15 136.7(6) 2_556 2_566 ?
O28A Rb4B O14 122.4(7) . . ?
O28B Rb4B O14 141.1(10) . . ?
O22 Rb4B O14 51.1(4) 1_455 . ?
O23 Rb4B O14 128.1(5) 2_666 . ?
O27 Rb4B O14 57.9(4) 1_455 . ?
O21 Rb4B O14 83.1(4) 2_666 . ?
O29 Rb4B O14 104.2(5) 2_556 . ?
O15 Rb4B O14 86.0(4) 2_566 . ?
O28A Rb4B O30 119.8(7) . 2_566 ?
O28B Rb4B O30 105.8(10) . 2_566 ?
O22 Rb4B O30 61.5(4) 1_455 2_566 ?
O23 Rb4B O30 94.9(6) 2_666 2_566 ?
O27 Rb4B O30 87.2(4) 1_455 2_566 ?
O21 Rb4B O30 156.1(6) 2_666 2_566 ?
O29 Rb4B O30 51.1(3) 2_556 2_566 ?
O15 Rb4B O30 86.0(5) 2_566 2_566 ?
O14 Rb4B O30 112.4(4) . 2_566 ?
O28A Rb4B P4 124.7(5) . 2_566 ?
O28B Rb4B P4 116.8(9) . 2_566 ?
O22 Rb4B P4 70.7(4) 1_455 2_566 ?
O23 Rb4B P4 68.8(4) 2_666 2_566 ?
O27 Rb4B P4 119.0(5) 1_455 2_566 ?
O21 Rb4B P4 70.0(3) 2_666 2_566 ?
O29 Rb4B P4 143.8(5) 2_556 2_566 ?
O15 Rb4B P4 23.0(2) 2_566 2_566 ?
O14 Rb4B P4 63.8(3) . 2_566 ?
O30 Rb4B P4 99.8(5) 2_566 2_566 ?
O28A Rb4B P4 100.6(6) . . ?
O28B Rb4B P4 119.8(10) . . ?
O22 Rb4B P4 71.8(4) 1_455 . ?
O23 Rb4B P4 124.2(4) 2_666 . ?
O27 Rb4B P4 58.5(4) 1_455 . ?
O21 Rb4B P4 67.6(4) 2_666 . ?
O29 Rb4B P4 107.9(5) 2_556 . ?
O15 Rb4B P4 96.9(4) 2_566 . ?
O14 Rb4B P4 21.8(2) . . ?
O30 Rb4B P4 131.9(4) 2_566 . ?
P4 Rb4B P4 74.0(3) 2_566 . ?
O1 Rb5 O24 96.3(5) 1_655 2_765 ?
O1 Rb5 O19 125.9(4) 1_655 2_665 ?
O24 Rb5 O19 88.8(4) 2_765 2_665 ?
O1 Rb5 O8 90.9(4) 1_655 . ?
O24 Rb5 O8 143.3(4) 2_765 . ?
O19 Rb5 O8 115.6(4) 2_665 . ?
O1 Rb5 O5 135.8(4) 1_655 . ?
O24 Rb5 O5 110.0(4) 2_765 . ?
O19 Rb5 O5 90.5(4) 2_665 . ?
O8 Rb5 O5 47.2(4) . . ?
O1 Rb5 O23 87.1(5) 1_655 1_545 ?
O24 Rb5 O23 134.8(3) 2_765 1_545 ?
O19 Rb5 O23 55.0(3) 2_665 1_545 ?
O8 Rb5 O23 81.3(3) . 1_545 ?
O5 Rb5 O23 97.6(4) . 1_545 ?
O1 Rb5 O17 168.9(3) 1_655 2_665 ?
O24 Rb5 O17 76.8(4) 2_765 2_665 ?
O19 Rb5 O17 46.3(3) 2_665 2_665 ?
O8 Rb5 O17 99.8(4) . 2_665 ?
O5 Rb5 O17 55.2(3) . 2_665 ?
O23 Rb5 O17 91.7(3) 1_545 2_665 ?
O1 Rb5 O28B 72.0(9) 1_655 2_656 ?
O24 Rb5 O28B 168.1(8) 2_765 2_656 ?
O19 Rb5 O28B 100.0(7) 2_665 2_656 ?
O8 Rb5 O28B 38.0(7) . 2_656 ?
O5 Rb5 O28B 78.3(8) . 2_656 ?
O23 Rb5 O28B 49.1(7) 1_545 2_656 ?
O17 Rb5 O28B 115.1(8) 2_665 2_656 ?
O1 Rb5 P2 109.4(3) 1_655 . ?
O24 Rb5 P2 118.8(3) 2_765 . ?
O19 Rb5 P2 114.7(3) 2_665 . ?
O8 Rb5 P2 27.3(3) . . ?
O5 Rb5 P2 26.6(2) . . ?
O23 Rb5 P2 102.0(2) 1_545 . ?
O17 Rb5 P2 81.6(2) 2_665 . ?
O28B Rb5 P2 64.9(7) 2_656 . ?
O1 Rb5 Cl2A 122.2(4) 1_655 2_665 ?
O24 Rb5 Cl2A 49.5(4) 2_765 2_665 ?
O19 Rb5 Cl2A 101.5(3) 2_665 2_665 ?
O8 Rb5 Cl2A 96.9(3) . 2_665 ?
O5 Rb5 Cl2A 62.4(4) . 2_665 ?
O23 Rb5 Cl2A 150.7(3) 1_545 2_665 ?
O17 Rb5 Cl2A 59.5(3) 2_665 2_665 ?
O28B Rb5 Cl2A 134.9(7) 2_656 2_665 ?
P2 Rb5 Cl2A 70.1(2) . 2_665 ?
O1 Rb5 O7 99.4(4) 1_655 . ?
O24 Rb5 O7 98.4(4) 2_765 . ?
O19 Rb5 O7 133.1(4) 2_665 . ?
O8 Rb5 O7 44.9(4) . . ?
O5 Rb5 O7 43.5(3) . . ?
O23 Rb5 O7 125.6(3) 1_545 . ?
O17 Rb5 O7 90.3(3) 2_665 . ?
O28B Rb5 O7 81.6(7) 2_656 . ?
P2 Rb5 O7 25.2(2) . . ?
Cl2A Rb5 O7 55.0(3) 2_665 . ?
O1 Rb5 O18 68.5(4) 1_655 1_645 ?
O24 Rb5 O18 87.8(3) 2_765 1_645 ?
O19 Rb5 O18 58.0(3) 2_665 1_645 ?
O8 Rb5 O18 127.9(3) . 1_645 ?
O5 Rb5 O18 144.1(3) . 1_645 ?
O23 Rb5 O18 51.6(3) 1_545 1_645 ?
O17 Rb5 O18 102.3(3) 2_665 1_645 ?
O28B Rb5 O18 89.9(7) 2_656 1_645 ?
P2 Rb5 O18 153.1(2) . 1_645 ?
Cl2A Rb5 O18 134.9(3) 2_665 1_645 ?
O7 Rb5 O18 167.0(3) . 1_645 ?
Rb6B Rb6A Rb6C 4.6(11) . . ?
Rb6B Rb6A O9 79.1(9) . . ?
Rb6C Rb6A O9 80.3(6) . . ?
Rb6B Rb6A O30 158.7(9) . . ?
Rb6C Rb6A O30 154.7(6) . . ?
O9 Rb6A O30 115.9(3) . . ?
Rb6B Rb6A O17 78.3(9) . . ?
Rb6C Rb6A O17 78.4(6) . . ?
O9 Rb6A O17 151.9(3) . . ?
O30 Rb6A O17 90.6(3) . . ?
Rb6B Rb6A O25 55.1(9) . 2_665 ?
Rb6C Rb6A O25 58.9(6) . 2_665 ?
O9 Rb6A O25 99.1(3) . 2_665 ?
O30 Rb6A O25 130.8(3) . 2_665 ?
O17 Rb6A O25 53.9(3) . 2_665 ?
Rb6B Rb6A O20 106.7(9) . 2_675 ?
Rb6C Rb6A O20 110.1(6) . 2_675 ?
O9 Rb6A O20 116.6(3) . 2_675 ?
O30 Rb6A O20 81.0(3) . 2_675 ?
O17 Rb6A O20 55.8(3) . 2_675 ?
O25 Rb6A O20 51.8(3) 2_665 2_675 ?
Rb6B Rb6A O15 63.1(9) . . ?
Rb6C Rb6A O15 58.6(7) . . ?
O9 Rb6A O15 92.8(3) . . ?
O30 Rb6A O15 99.5(4) . . ?
O17 Rb6A O15 91.6(3) . . ?
O25 Rb6A O15 112.7(4) 2_665 . ?
O20 Rb6A O15 147.3(3) 2_675 . ?
Rb6B Rb6A O22 118.9(9) . 2_666 ?
Rb6C Rb6A O22 116.9(6) . 2_666 ?
O9 Rb6A O22 55.9(3) . 2_666 ?
O30 Rb6A O22 65.4(3) . 2_666 ?
O17 Rb6A O22 151.8(3) . 2_666 ?
O25 Rb6A O22 153.9(3) 2_665 2_666 ?
O20 Rb6A O22 128.6(3) 2_675 2_666 ?
O15 Rb6A O22 78.9(3) . 2_666 ?
Rb6B Rb6A O18 87.6(9) . . ?
Rb6C Rb6A O18 84.4(6) . . ?
O9 Rb6A O18 149.2(3) . . ?
O30 Rb6A O18 71.9(3) . . ?
O17 Rb6A O18 45.2(3) . . ?
O25 Rb6A O18 95.6(3) 2_665 . ?
O20 Rb6A O18 93.8(3) 2_675 . ?
O15 Rb6A O18 56.4(3) . . ?
O22 Rb6A O18 109.9(3) 2_666 . ?
Rb6B Rb6A O16 69.2(9) . . ?
Rb6C Rb6A O16 66.6(6) . . ?
O9 Rb6A O16 50.8(3) . . ?
O30 Rb6A O16 107.4(3) . . ?
O17 Rb6A O16 132.5(3) . . ?
O25 Rb6A O16 121.6(3) 2_665 . ?
O20 Rb6A O16 166.8(3) 2_675 . ?
O15 Rb6A O16 43.1(3) . . ?
O22 Rb6A O16 50.9(3) 2_666 . ?
O18 Rb6A O16 98.5(3) . . ?
Rb6B Rb6A P5 93.5(9) . . ?
Rb6C Rb6A P5 92.0(6) . . ?
O9 Rb6A P5 171.8(2) . . ?
O30 Rb6A P5 70.3(2) . . ?
O17 Rb6A P5 25.3(2) . . ?
O25 Rb6A P5 79.2(2) 2_665 . ?
O20 Rb6A P5 68.8(2) 2_675 . ?
O15 Rb6A P5 80.5(2) . . ?
O22 Rb6A P5 126.6(2) 2_666 . ?
O18 Rb6A P5 25.0(2) . . ?
O16 Rb6A P5 123.29(19) . . ?
Rb6C Rb6B Rb6A 169(3) . . ?
Rb6C Rb6B O25 80(2) . 2_665 ?
Rb6A Rb6B O25 108.9(11) . 2_665 ?
Rb6C Rb6B O9 101(2) . . ?
Rb6A Rb6B O9 82.1(9) . . ?
O25 Rb6B O9 110.8(6) 2_665 . ?
Rb6C Rb6B O15 68.8(19) . . ?
Rb6A Rb6B O15 100.5(10) . . ?
O25 Rb6B O15 139.5(7) 2_665 . ?
O9 Rb6B O15 100.1(5) . . ?
Rb6C Rb6B O17 96(2) . . ?
Rb6A Rb6B O17 84.3(9) . . ?
O25 Rb6B O17 58.5(4) 2_665 . ?
O9 Rb6B O17 158.4(7) . . ?
O15 Rb6B O17 98.7(5) . . ?
Rb6C Rb6B Cl2A 28.5(19) . . ?
Rb6A Rb6B Cl2A 150.5(11) . . ?
O25 Rb6B Cl2A 63.6(5) 2_665 . ?
O9 Rb6B Cl2A 127.4(7) . . ?
O15 Rb6B Cl2A 77.1(5) . . ?
O17 Rb6B Cl2A 67.4(5) . . ?
Rb6C Rb6B Rb7A 15.1(19) . . ?
Rb6A Rb6B Rb7A 164.5(12) . . ?
O25 Rb6B Rb7A 68.4(7) 2_665 . ?
O9 Rb6B Rb7A 113.3(8) . . ?
O15 Rb6B Rb7A 75.8(7) . . ?
O17 Rb6B Rb7A 81.5(7) . . ?
Cl2A Rb6B Rb7A 14.3(5) . . ?
Rb6C Rb6B O16 78(2) . . ?
Rb6A Rb6B O16 95.3(10) . . ?
O25 Rb6B O16 149.6(7) 2_665 . ?
O9 Rb6B O16 53.6(3) . . ?
O15 Rb6B O16 46.7(4) . . ?
O17 Rb6B O16 144.9(5) . . ?
Cl2A Rb6B O16 103.2(6) . . ?
Rb7A Rb6B O16 92.8(7) . . ?
Rb6C Rb6B O18 96(2) . . ?
Rb6A Rb6B O18 76.7(9) . . ?
O25 Rb6B O18 102.2(5) 2_665 . ?
O9 Rb6B O18 145.1(6) . . ?
O15 Rb6B O18 57.9(4) . . ?
O17 Rb6B O18 44.6(3) . . ?
Cl2A Rb6B O18 77.4(5) . . ?
Rb7A Rb6B O18 88.9(7) . . ?
O16 Rb6B O18 101.0(5) . . ?
Rb6C Rb6B O20 129(2) . 2_675 ?
Rb6A Rb6B O20 58.9(8) . 2_675 ?
O25 Rb6B O20 50.2(4) 2_665 2_675 ?
O9 Rb6B O20 106.5(5) . 2_675 ?
O15 Rb6B O20 142.7(6) . 2_675 ?
O17 Rb6B O20 52.0(4) . 2_675 ?
Cl2A Rb6B O20 105.4(5) . 2_675 ?
Rb7A Rb6B O20 115.2(7) . 2_675 ?
O16 Rb6B O20 151.4(6) . 2_675 ?
O18 Rb6B O20 85.9(4) . 2_675 ?
Rb6C Rb6B P4 63.4(19) . . ?
Rb6A Rb6B P4 107.5(10) . . ?
O25 Rb6B P4 143.5(7) 2_665 . ?
O9 Rb6B P4 77.9(4) . . ?
O15 Rb6B P4 24.6(3) . . ?
O17 Rb6B P4 122.4(5) . . ?
Cl2A Rb6B P4 82.7(5) . . ?
Rb7A Rb6B P4 75.6(6) . . ?
O16 Rb6B P4 25.2(2) . . ?
O18 Rb6B P4 82.5(3) . . ?
O20 Rb6B P4 164.0(6) 2_675 . ?
Rb6B Rb6C Rb6A 6.2(16) . . ?
Rb6B Rb6C Cl2A 144(2) . . ?
Rb6A Rb6C Cl2A 143.9(10) . . ?
Rb6B Rb6C Rb7A 161(2) . . ?
Rb6A Rb6C Rb7A 161.9(12) . . ?
Cl2A Rb6C Rb7A 18.1(6) . . ?
Rb6B Rb6C O25 86(2) . 2_665 ?
Rb6A Rb6C O25 90.8(8) . 2_665 ?
Cl2A Rb6C O25 72.2(6) . 2_665 ?
Rb7A Rb6C O25 79.3(8) . 2_665 ?
Rb6B Rb6C O15 98(2) . . ?
Rb6A Rb6C O15 91.7(8) . . ?
Cl2A Rb6C O15 90.8(7) . . ?
Rb7A Rb6C O15 90.6(9) . . ?
O25 Rb6C O15 153.7(8) 2_665 . ?
Rb6B Rb6C O9 66.4(19) . . ?
Rb6A Rb6C O9 68.1(6) . . ?
Cl2A Rb6C O9 146.6(8) . . ?
Rb7A Rb6C O9 129.2(10) . . ?
O25 Rb6C O9 105.9(6) 2_665 . ?
O15 Rb6C O9 99.4(6) . . ?
Rb6B Rb6C O17 72(2) . . ?
Rb6A Rb6C O17 71.9(6) . . ?
Cl2A Rb6C O17 72.1(6) . . ?
Rb7A Rb6C O17 90.0(9) . . ?
O25 Rb6C O17 57.0(4) 2_665 . ?
O15 Rb6C O17 99.2(6) . . ?
O9 Rb6C O17 136.1(7) . . ?
Rb6B Rb6C O16 90(2) . . ?
Rb6A Rb6C O16 86.0(7) . . ?
Cl2A Rb6C O16 121.2(8) . . ?
Rb7A Rb6C O16 108.7(9) . . ?
O25 Rb6C O16 157.9(7) 2_665 . ?
O15 Rb6C O16 48.4(4) . . ?
O9 Rb6C O16 52.8(4) . . ?
O17 Rb6C O16 140.8(7) . . ?
Rb6B Rb6C P4 106(2) . . ?
Rb6A Rb6C P4 100.8(7) . . ?
Cl2A Rb6C P4 97.5(7) . . ?
Rb7A Rb6C P4 89.2(8) . . ?
O25 Rb6C P4 168.3(8) 2_665 . ?
O15 Rb6C P4 26.9(3) . . ?
O9 Rb6C P4 79.4(4) . . ?
O17 Rb6C P4 126.1(5) . . ?
O16 Rb6C P4 26.9(2) . . ?
Rb6B Rb6C Cl1 131(2) . 2_665 ?
Rb6A Rb6C Cl1 136.7(9) . 2_665 ?
Cl2A Rb6C Cl1 64.4(6) . 2_665 ?
Rb7A Rb6C Cl1 51.6(8) . 2_665 ?
O25 Rb6C Cl1 64.7(5) 2_665 2_665 ?
O15 Rb6C Cl1 126.3(8) . 2_665 ?
O9 Rb6C Cl1 84.3(5) . 2_665 ?
O17 Rb6C Cl1 114.8(6) . 2_665 ?
O16 Rb6C Cl1 103.5(6) . 2_665 ?
P4 Rb6C Cl1 106.2(6) . 2_665 ?
Rb6B Rb6C O13 131(2) . . ?
Rb6A Rb6C O13 126.2(8) . . ?
Cl2A Rb6C O13 77.8(6) . . ?
Rb7A Rb6C O13 65.8(8) . . ?
O25 Rb6C O13 142.7(8) 2_665 . ?
O15 Rb6C O13 44.4(4) . . ?
O9 Rb6C O13 87.4(5) . . ?
O17 Rb6C O13 132.1(6) . . ?
O16 Rb6C O13 43.6(4) . . ?
P4 Rb6C O13 25.8(2) . . ?
Cl1 Rb6C O13 82.7(5) 2_665 . ?
Cl1 Cl1 Rb7A 157(4) 2_665 2_665 ?
Cl1 Cl1 Rb2 109(4) 2_665 . ?
Rb7A Cl1 Rb2 70.9(7) 2_665 . ?
Cl1 Cl1 Rb3B 99(3) 2_665 2_665 ?
Rb7A Cl1 Rb3B 103.6(14) 2_665 2_665 ?
Rb2 Cl1 Rb3B 95.4(7) . 2_665 ?
Cl1 Cl1 Rb3A 108(3) 2_665 2_665 ?
Rb7A Cl1 Rb3A 95.2(9) 2_665 2_665 ?
Rb2 Cl1 Rb3A 90.9(5) . 2_665 ?
Rb3B Cl1 Rb3A 8.6(6) 2_665 2_665 ?
Cl1 Cl1 Rb3B 67(3) 2_665 . ?
Rb7A Cl1 Rb3B 89.6(12) 2_665 . ?
Rb2 Cl1 Rb3B 89.3(8) . . ?
Rb3B Cl1 Rb3B 166.8(5) 2_665 . ?
Rb3A Cl1 Rb3B 175.0(8) 2_665 . ?
Cl1 Cl1 Rb6C 138(3) 2_665 2_665 ?
Rb7A Cl1 Rb6C 47.5(7) 2_665 2_665 ?
Rb2 Cl1 Rb6C 112.3(5) . 2_665 ?
Rb3B Cl1 Rb6C 77.6(9) 2_665 2_665 ?
Rb3A Cl1 Rb6C 72.6(6) 2_665 2_665 ?
Rb3B Cl1 Rb6C 111.9(9) . 2_665 ?
Cl1 Cl1 Rb2 58(3) 2_665 2_665 ?
Rb7A Cl1 Rb2 120.3(10) 2_665 2_665 ?
Rb2 Cl1 Rb2 167.6(7) . 2_665 ?
Rb3B Cl1 Rb2 87.2(9) 2_665 2_665 ?
Rb3A Cl1 Rb2 93.2(6) 2_665 2_665 ?
Rb3B Cl1 Rb2 85.6(7) . 2_665 ?
Rb6C Cl1 Rb2 80.1(6) 2_665 2_665 ?
Cl1 Cl1 Rb7A 18(3) 2_665 . ?
Rb7A Cl1 Rb7A 174.9(8) 2_665 . ?
Rb2 Cl1 Rb7A 109.5(8) . . ?
Rb3B Cl1 Rb7A 81.5(12) 2_665 . ?
Rb3A Cl1 Rb7A 89.9(8) 2_665 . ?
Rb3B Cl1 Rb7A 85.3(11) . . ?
Rb6C Cl1 Rb7A 134.6(8) 2_665 . ?
Rb2 Cl1 Rb7A 58.9(5) 2_665 . ?
Cl1 Cl1 Rb3A 60(3) 2_665 . ?
Rb7A Cl1 Rb3A 97.1(9) 2_665 . ?
Rb2 Cl1 Rb3A 93.4(7) . . ?
Rb3B Cl1 Rb3A 159.2(8) 2_665 . ?
Rb3A Cl1 Rb3A 167.7(4) 2_665 . ?
Rb3B Cl1 Rb3A 7.7(5) . . ?
Rb6C Cl1 Rb3A 116.0(7) 2_665 . ?
Rb2 Cl1 Rb3A 80.3(5) 2_665 . ?
Rb7A Cl1 Rb3A 77.8(7) . . ?
Cl1 Cl1 Rb6B 131(3) 2_665 2_665 ?
Rb7A Cl1 Rb6B 54.5(7) 2_665 2_665 ?
Rb2 Cl1 Rb6B 119.9(4) . 2_665 ?
Rb3B Cl1 Rb6B 76.8(8) 2_665 2_665 ?
Rb3A Cl1 Rb6B 72.8(5) 2_665 2_665 ?
Rb3B Cl1 Rb6B 111.4(8) . 2_665 ?
Rb6C Cl1 Rb6B 7.7(3) 2_665 2_665 ?
Rb2 Cl1 Rb6B 72.5(5) 2_665 2_665 ?
Rb7A Cl1 Rb6B 127.3(7) . 2_665 ?
Rb3A Cl1 Rb6B 114.5(6) . 2_665 ?
Rb7A Cl2A Rb6C 87(2) . . ?
Rb7A Cl2A Rb6B 94(2) . . ?
Rb6C Cl2A Rb6B 7.6(5) . . ?
Rb7A Cl2A Rb5 151(2) . 2_665 ?
Rb6C Cl2A Rb5 118.0(6) . 2_665 ?
Rb6B Cl2A Rb5 111.3(5) . 2_665 ?
Rb7A Cl2A Rb6A 101(2) . . ?
Rb6C Cl2A Rb6A 14.1(4) . . ?
Rb6B Cl2A Rb6A 6.8(3) . . ?
Rb5 Cl2A Rb6A 104.5(4) 2_665 . ?
Cl2A Rb7A Rb6C 75(2) . . ?
Cl2A Rb7A Cl1 126(3) . 2_665 ?
Rb6C Rb7A Cl1 81.0(10) . 2_665 ?
Cl2A Rb7A O26 95(2) . 2_665 ?
Rb6C Rb7A O26 167.1(13) . 2_665 ?
Cl1 Rb7A O26 111.7(11) 2_665 2_665 ?
Cl2A Rb7A O24 53(2) . 1_455 ?
Rb6C Rb7A O24 83.4(9) . 1_455 ?
Cl1 Rb7A O24 163.9(12) 2_665 1_455 ?
O26 Rb7A O24 84.0(7) 2_665 1_455 ?
Cl2A Rb7A Rb6B 72(2) . . ?
Rb6C Rb7A Rb6B 4.0(5) . . ?
Cl1 Rb7A Rb6B 82.0(9) 2_665 . ?
O26 Rb7A Rb6B 165.1(12) 2_665 . ?
O24 Rb7A Rb6B 82.7(8) 1_455 . ?
Cl2A Rb7A O13 119(3) . . ?
Rb6C Rb7A O13 70.7(8) . . ?
Cl1 Rb7A O13 96.6(10) 2_665 . ?
O26 Rb7A O13 108.3(8) 2_665 . ?
O24 Rb7A O13 74.3(7) 1_455 . ?
Rb6B Rb7A O13 74.3(6) . . ?
Cl2A Rb7A O25 61(2) . 2_665 ?
Rb6C Rb7A O25 52.8(7) . 2_665 ?
Cl1 Rb7A O25 65.6(7) 2_665 2_665 ?
O26 Rb7A O25 129.6(10) 2_665 2_665 ?
O24 Rb7A O25 107.6(10) 1_455 2_665 ?
Rb6B Rb7A O25 49.7(5) . 2_665 ?
O13 Rb7A O25 122.0(8) . 2_665 ?
Cl2A Rb7A Rb2 151(3) . 2_665 ?
Rb6C Rb7A Rb2 131.3(12) . 2_665 ?
Cl1 Rb7A Rb2 60.0(8) 2_665 2_665 ?
O26 Rb7A Rb2 60.3(6) 2_665 2_665 ?
O24 Rb7A Rb2 130.6(9) 1_455 2_665 ?
Rb6B Rb7A Rb2 134.3(10) . 2_665 ?
O13 Rb7A Rb2 85.2(8) . 2_665 ?
O25 Rb7A Rb2 121.3(8) 2_665 2_665 ?
Cl2A Rb7A Cl1 123(2) . . ?
Rb6C Rb7A Cl1 83.2(9) . . ?
Cl1 Rb7A Cl1 5.1(8) 2_665 . ?
O26 Rb7A Cl1 109.3(9) 2_665 . ?
O24 Rb7A Cl1 166.6(10) 1_455 . ?
Rb6B Rb7A Cl1 84.0(7) . . ?
O13 Rb7A Cl1 101.7(9) . . ?
O25 Rb7A Cl1 63.3(6) 2_665 . ?
Rb2 Rb7A Cl1 60.5(6) 2_665 . ?
Cl2A Rb7A O26 131(2) . 1_455 ?
Rb6C Rb7A O26 122.1(11) . 1_455 ?
Cl1 Rb7A O26 102.8(11) 2_665 1_455 ?
O26 Rb7A O26 58.4(6) 2_665 1_455 ?
O24 Rb7A O26 82.2(7) 1_455 1_455 ?
Rb6B Rb7A O26 125.8(9) . 1_455 ?
O13 Rb7A O26 51.5(5) . 1_455 ?
O25 Rb7A O26 167.1(11) 2_665 1_455 ?
Rb2 Rb7A O26 50.9(5) 2_665 1_455 ?
Cl1 Rb7A O26 105.5(10) . 1_455 ?
Cl2A Rb7A O7 61(2) . 2_665 ?
Rb6C Rb7A O7 126.1(12) . 2_665 ?
Cl1 Rb7A O7 99.0(9) 2_665 2_665 ?
O26 Rb7A O7 52.2(5) 2_665 2_665 ?
O24 Rb7A O7 93.4(9) 1_455 2_665 ?
Rb6B Rb7A O7 122.1(10) . 2_665 ?
O13 Rb7A O7 158.7(9) . 2_665 ?
O25 Rb7A O7 77.9(7) 2_665 2_665 ?
Rb2 Rb7A O7 90.2(7) 2_665 2_665 ?
Cl1 Rb7A O7 94.0(8) . 2_665 ?
O26 Rb7A O7 110.5(7) 1_455 2_665 ?
O2 P1 O3 115.5(8) . . ?
O2 P1 O1 114.2(10) . . ?
O3 P1 O1 108.9(10) . . ?
O2 P1 O4 107.2(9) . . ?
O3 P1 O4 112.9(8) . . ?
O1 P1 O4 96.6(8) . . ?
O2 P1 U5A 57.3(7) . . ?
O3 P1 U5A 131.6(7) . . ?
O1 P1 U5A 117.3(7) . . ?
O4 P1 U5A 49.9(5) . . ?
O2 P1 U3 124.3(6) . . ?
O3 P1 U3 120.1(6) . . ?
O1 P1 U3 43.7(6) . . ?
O4 P1 U3 53.0(5) . . ?
U5A P1 U3 86.77(10) . . ?
O2 P1 Rb5 97.0(8) . 1_455 ?
O3 P1 Rb5 76.5(7) . 1_455 ?
O1 P1 Rb5 49.9(7) . 1_455 ?
O4 P1 Rb5 145.2(5) . 1_455 ?
U5A P1 Rb5 146.61(14) . 1_455 ?
U3 P1 Rb5 92.73(13) . 1_455 ?
O2 P1 Rb3A 118.6(8) . . ?
O3 P1 Rb3A 69.2(7) . . ?
O1 P1 Rb3A 121.3(7) . . ?
O4 P1 Rb3A 45.0(6) . . ?
U5A P1 Rb3A 74.9(3) . . ?
U3 P1 Rb3A 84.7(3) . . ?
Rb5 P1 Rb3A 138.3(3) 1_455 . ?
O2 P1 Rb3B 119.7(9) . . ?
O3 P1 Rb3B 75.0(9) . . ?
O1 P1 Rb3B 116.9(10) . . ?
O4 P1 Rb3B 38.7(9) . . ?
U5A P1 Rb3B 72.0(3) . . ?
U3 P1 Rb3B 78.7(8) . . ?
Rb5 P1 Rb3B 140.5(3) 1_455 . ?
Rb3A P1 Rb3B 6.6(5) . . ?
O2 P1 Rb2 158.6(6) . 2_665 ?
O3 P1 Rb2 46.4(6) . 2_665 ?
O1 P1 Rb2 70.6(7) . 2_665 ?
O4 P1 Rb2 92.4(5) . 2_665 ?
U5A P1 Rb2 141.01(13) . 2_665 ?
U3 P1 Rb2 74.38(10) . 2_665 ?
Rb5 P1 Rb2 69.59(9) 1_455 2_665 ?
Rb3A P1 Rb2 69.7(2) . 2_665 ?
Rb3B P1 Rb2 71.0(3) . 2_665 ?
O7 P2 O5 108.5(9) . . ?
O7 P2 O6 109.8(9) . . ?
O5 P2 O6 113.6(7) . . ?
O7 P2 O8 110.5(9) . . ?
O5 P2 O8 105.5(8) . . ?
O6 P2 O8 108.9(8) . . ?
O7 P2 U5C 108.2(6) . 2_656 ?
O5 P2 U5C 126.8(6) . 2_656 ?
O6 P2 U5C 88.1(6) . 2_656 ?
O8 P2 U5C 24.1(5) . 2_656 ?
O7 P2 U5B 103.1(6) . 2_656 ?
O5 P2 U5B 124.9(6) . 2_656 ?
O6 P2 U5B 95.8(6) . 2_656 ?
O8 P2 U5B 19.6(5) . 2_656 ?
U5C P2 U5B 8.11(19) 2_656 2_656 ?
O7 P2 U5C 137.2(8) . . ?
O5 P2 U5C 92.5(6) . . ?
O6 P2 U5C 28.5(5) . . ?
O8 P2 U5C 98.5(6) . . ?
U5C P2 U5C 85.8(3) 2_656 . ?
U5B P2 U5C 93.8(2) 2_656 . ?
O7 P2 Rb5 79.5(8) . . ?
O5 P2 Rb5 65.1(5) . . ?
O6 P2 Rb5 170.0(6) . . ?
O8 P2 Rb5 63.2(5) . . ?
U5C P2 Rb5 85.4(2) 2_656 . ?
U5B P2 Rb5 78.07(14) 2_656 . ?
U5C P2 Rb5 143.0(2) . . ?
O7 P2 Rb3B 64.1(10) . . ?
O5 P2 Rb3B 90.0(6) . . ?
O6 P2 Rb3B 62.5(9) . . ?
O8 P2 Rb3B 164.4(6) . . ?
U5C P2 Rb3B 141.1(5) 2_656 . ?
U5B P2 Rb3B 144.9(3) 2_656 . ?
U5C P2 Rb3B 79.5(8) . . ?
Rb5 P2 Rb3B 126.6(7) . . ?
O7 P2 Rb1 153.4(8) . 2_656 ?
O5 P2 Rb1 65.7(6) . 2_656 ?
O6 P2 Rb1 95.8(5) . 2_656 ?
O8 P2 Rb1 51.7(6) . 2_656 ?
U5C P2 Rb1 64.13(19) 2_656 2_656 ?
U5B P2 Rb1 65.87(12) 2_656 2_656 ?
U5C P2 Rb1 69.26(19) . 2_656 ?
Rb5 P2 Rb1 74.54(10) . 2_656 ?
Rb3B P2 Rb1 138.6(5) . 2_656 ?
O7 P2 Rb3A 68.2(7) . . ?
O5 P2 Rb3A 89.0(6) . . ?
O6 P2 Rb3A 59.4(6) . . ?
O8 P2 Rb3A 164.6(6) . . ?
U5C P2 Rb3A 140.5(3) 2_656 . ?
U5B P2 Rb3A 145.2(2) 2_656 . ?
U5C P2 Rb3A 75.5(3) . . ?
Rb5 P2 Rb3A 129.53(18) . . ?
Rb3B P2 Rb3A 4.2(6) . . ?
Rb1 P2 Rb3A 134.7(2) 2_656 . ?
O11 P3 O12 109.2(9) . . ?
O11 P3 O9 110.8(6) . . ?
O12 P3 O9 111.4(6) . . ?
O11 P3 O10 112.1(7) . . ?
O12 P3 O10 110.7(9) . . ?
O9 P3 O10 102.5(5) . . ?
O11 P3 U1 130.8(6) . 2_666 ?
O12 P3 U1 119.9(7) . 2_666 ?
O9 P3 U1 50.2(3) . 2_666 ?
O10 P3 U1 52.7(3) . 2_666 ?
O11 P3 Rb3B 65.9(10) . . ?
O12 P3 Rb3B 140.5(7) . . ?
O9 P3 Rb3B 47.1(9) . . ?
O10 P3 Rb3B 106.8(7) . . ?
U1 P3 Rb3B 74.9(9) 2_666 . ?
O11 P3 Rb2 57.3(5) . . ?
O12 P3 Rb2 71.4(7) . . ?
O9 P3 Rb2 86.9(4) . . ?
O10 P3 Rb2 168.2(4) . . ?
U1 P3 Rb2 137.07(9) 2_666 . ?
Rb3B P3 Rb2 74.3(6) . . ?
O11 P3 Rb6A 127.1(5) . . ?
O12 P3 Rb6A 70.0(5) . . ?
O9 P3 Rb6A 41.4(4) . . ?
O10 P3 Rb6A 117.2(4) . . ?
U1 P3 Rb6A 72.38(7) 2_666 . ?
Rb3B P3 Rb6A 82.4(6) . . ?
Rb2 P3 Rb6A 74.51(8) . . ?
O11 P3 Rb3A 72.5(6) . . ?
O12 P3 Rb3A 139.1(6) . . ?
O9 P3 Rb3A 40.6(5) . . ?
O10 P3 Rb3A 105.5(5) . . ?
U1 P3 Rb3A 69.6(2) 2_666 . ?
Rb3B P3 Rb3A 6.6(6) . . ?
Rb2 P3 Rb3A 76.97(14) . . ?
Rb6A P3 Rb3A 77.1(3) . . ?
O11 P3 Rb6B 115.8(5) . . ?
O12 P3 Rb6B 79.6(5) . . ?
O9 P3 Rb6B 33.0(4) . . ?
O10 P3 Rb6B 123.7(4) . . ?
U1 P3 Rb6B 73.7(2) 2_666 . ?
Rb3B P3 Rb6B 69.6(6) . . ?
Rb2 P3 Rb6B 67.9(2) . . ?
Rb6A P3 Rb6B 13.4(2) . . ?
Rb3A P3 Rb6B 64.7(4) . . ?
O14 P4 O16 109.4(6) . . ?
O14 P4 O15 110.2(8) . . ?
O16 P4 O15 108.5(7) . . ?
O14 P4 O13 112.1(6) . . ?
O16 P4 O13 109.5(7) . . ?
O15 P4 O13 107.0(8) . . ?
O14 P4 Rb6C 163.0(6) . . ?
O16 P4 Rb6C 71.5(6) . . ?
O15 P4 Rb6C 55.2(6) . . ?
O13 P4 Rb6C 82.5(6) . . ?
O14 P4 Rb6B 154.2(6) . . ?
O16 P4 Rb6B 65.6(5) . . ?
O15 P4 Rb6B 53.2(6) . . ?
O13 P4 Rb6B 92.9(5) . . ?
Rb6C P4 Rb6B 10.6(3) . . ?
O14 P4 Rb4B 73.1(5) . 2_566 ?
O16 P4 Rb4B 77.0(6) . 2_566 ?
O15 P4 Rb4B 61.7(7) . 2_566 ?
O13 P4 Rb4B 168.6(6) . 2_566 ?
Rb6C P4 Rb4B 91.0(4) . 2_566 ?
Rb6B P4 Rb4B 81.2(4) . 2_566 ?
O14 P4 Rb6A 141.8(5) . . ?
O16 P4 Rb6A 60.5(5) . . ?
O15 P4 Rb6A 51.4(5) . . ?
O13 P4 Rb6A 105.7(5) . . ?
Rb6C P4 Rb6A 23.5(3) . . ?
Rb6B P4 Rb6A 12.9(3) . . ?
Rb4B P4 Rb6A 68.8(2) 2_566 . ?
O14 P4 Rb3A 130.9(5) . . ?
O16 P4 Rb3A 51.8(6) . . ?
O15 P4 Rb3A 118.6(6) . . ?
O13 P4 Rb3A 57.8(5) . . ?
Rb6C P4 Rb3A 63.7(3) . . ?
Rb6B P4 Rb3A 67.7(3) . . ?
Rb4B P4 Rb3A 127.2(3) 2_566 . ?
Rb6A P4 Rb3A 74.66(15) . . ?
O14 P4 Rb4B 59.3(6) . . ?
O16 P4 Rb4B 70.7(5) . . ?
O15 P4 Rb4B 166.8(7) . . ?
O13 P4 Rb4B 85.2(6) . . ?
Rb6C P4 Rb4B 133.4(4) . . ?
Rb6B P4 Rb4B 132.8(3) . . ?
Rb4B P4 Rb4B 106.0(3) 2_566 . ?
Rb6A P4 Rb4B 130.99(19) . . ?
Rb3A P4 Rb4B 71.8(3) . . ?
O14 P4 Rb4A 79.4(5) . 2_566 ?
O16 P4 Rb4A 75.0(6) . 2_566 ?
O15 P4 Rb4A 57.5(6) . 2_566 ?
O13 P4 Rb4A 164.0(5) . 2_566 ?
Rb6C P4 Rb4A 84.6(4) . 2_566 ?
Rb6B P4 Rb4A 74.8(3) . 2_566 ?
Rb4B P4 Rb4A 6.4(3) 2_566 2_566 ?
Rb6A P4 Rb4A 62.44(17) . 2_566 ?
Rb3A P4 Rb4A 123.6(2) . 2_566 ?
Rb4B P4 Rb4A 110.6(3) . 2_566 ?
O18 P5 O19 107.8(8) . . ?
O18 P5 O20 111.6(7) . . ?
O19 P5 O20 109.6(8) . . ?
O18 P5 O17 108.3(7) . . ?
O19 P5 O17 110.0(9) . . ?
O20 P5 O17 109.6(6) . . ?
O18 P5 Rb5 86.4(5) . 2_665 ?
O19 P5 Rb5 55.5(6) . 2_665 ?
O20 P5 Rb5 160.6(5) . 2_665 ?
O17 P5 Rb5 69.4(4) . 2_665 ?
O18 P5 Rb6A 68.2(5) . . ?
O19 P5 Rb6A 163.7(6) . . ?
O20 P5 Rb6A 86.2(5) . . ?
O17 P5 Rb6A 59.0(5) . . ?
Rb5 P5 Rb6A 108.19(11) 2_665 . ?
O18 P5 Rb6B 65.6(5) . . ?
O19 P5 Rb6B 149.4(7) . . ?
O20 P5 Rb6B 100.2(6) . . ?
O17 P5 Rb6B 51.2(5) . . ?
Rb5 P5 Rb6B 93.9(3) 2_665 . ?
Rb6A P5 Rb6B 14.3(3) . . ?
O18 P5 Rb6C 63.0(5) . . ?
O19 P5 Rb6C 140.0(7) . . ?
O20 P5 Rb6C 109.8(6) . . ?
O17 P5 Rb6C 48.8(6) . . ?
Rb5 P5 Rb6C 84.5(3) 2_665 . ?
Rb6A P5 Rb6C 23.8(3) . . ?
Rb6B P5 Rb6C 9.6(3) . . ?
O18 P5 Rb5 57.0(5) . 1_465 ?
O19 P5 Rb5 71.0(7) . 1_465 ?
O20 P5 Rb5 85.1(4) . 1_465 ?
O17 P5 Rb5 163.2(5) . 1_465 ?
Rb5 P5 Rb5 99.60(8) 2_665 1_465 ?
Rb6A P5 Rb5 115.72(10) . 1_465 ?
Rb6B P5 Rb5 119.5(2) . 1_465 ?
Rb6C P5 Rb5 119.3(3) . 1_465 ?
O18 P5 Rb6A 157.1(5) . 2_675 ?
O19 P5 Rb6A 84.6(5) . 2_675 ?
O20 P5 Rb6A 45.5(5) . 2_675 ?
O17 P5 Rb6A 84.3(5) . 2_675 ?
Rb5 P5 Rb6A 116.32(10) 2_665 2_675 ?
Rb6A P5 Rb6A 104.99(9) . 2_675 ?
Rb6B P5 Rb6A 113.1(2) . 2_675 ?
Rb6C P5 Rb6A 119.5(3) . 2_675 ?
Rb5 P5 Rb6A 112.38(9) 1_465 2_675 ?
P1 O1 U3 110.7(10) . . ?
P1 O1 Rb5 105.7(7) . 1_455 ?
U3 O1 Rb5 141.3(7) . 1_455 ?
P1 O2 U5B 134.7(11) . 2_556 ?
P1 O2 U5A 148.1(11) . 2_556 ?
U5B O2 U5A 13.41(14) 2_556 2_556 ?
P1 O2 U5A 95.4(8) . . ?
U5B O2 U5A 129.7(6) 2_556 . ?
U5A O2 U5A 116.4(5) 2_556 . ?
P1 O2 U5C 136.9(10) . 2_556 ?
U5B O2 U5C 3.8(3) 2_556 2_556 ?
U5A O2 U5C 11.6(2) 2_556 2_556 ?
U5A O2 U5C 127.1(6) . 2_556 ?
P1 O3 U4 147.3(8) . 1_455 ?
P1 O3 Rb2 113.9(7) . 2_665 ?
U4 O3 Rb2 97.9(4) 1_455 2_665 ?
P1 O3 Rb3A 87.2(7) . . ?
U4 O3 Rb3A 104.6(6) 1_455 . ?
Rb2 O3 Rb3A 83.2(4) 2_665 . ?
P1 O3 Rb5 79.3(7) . 1_455 ?
U4 O3 Rb5 99.6(5) 1_455 1_455 ?
Rb2 O3 Rb5 80.5(4) 2_665 1_455 ?
Rb3A O3 Rb5 152.4(5) . 1_455 ?
P1 O4 U5A 99.7(6) . . ?
P1 O4 U3 98.5(6) . . ?
U5A O4 U3 120.2(6) . . ?
P1 O4 U5C 108.2(7) . . ?
U5A O4 U5C 9.4(2) . . ?
U3 O4 U5C 113.9(5) . . ?
P1 O4 Rb3B 120.5(13) . . ?
U5A O4 Rb3B 105.0(6) . . ?
U3 O4 Rb3B 113.1(12) . . ?
U5C O4 Rb3B 103.0(6) . . ?
P1 O4 Rb3A 111.3(9) . . ?
U5A O4 Rb3A 105.6(5) . . ?
U3 O4 Rb3A 119.3(5) . . ?
U5C O4 Rb3A 105.3(5) . . ?
Rb3B O4 Rb3A 9.6(7) . . ?
P2 O5 U3 154.9(8) . . ?
P2 O5 Rb5 88.3(5) . . ?
U3 O5 Rb5 116.2(5) . . ?
P2 O5 Rb1 91.3(6) . 2_656 ?
U3 O5 Rb1 96.5(5) . 2_656 ?
Rb5 O5 Rb1 83.6(3) . 2_656 ?
P2 O6 U5C 131.3(8) . . ?
P2 O6 U5A 132.9(7) . . ?
U5C O6 U5A 13.9(3) . . ?
P2 O6 U5B 136.6(7) . . ?
U5C O6 U5B 5.3(3) . . ?
U5A O6 U5B 13.08(12) . . ?
P2 O6 Rb1 127.4(6) . . ?
U5C O6 Rb1 91.0(5) . . ?
U5A O6 Rb1 96.0(4) . . ?
U5B O6 Rb1 86.9(4) . . ?
P2 O6 Rb3B 92.3(12) . . ?
U5C O6 Rb3B 111.7(11) . . ?
U5A O6 Rb3B 98.1(10) . . ?
U5B O6 Rb3B 109.0(11) . . ?
Rb1 O6 Rb3B 99.4(6) . . ?
P2 O6 Rb3A 98.2(7) . . ?
U5C O6 Rb3A 105.2(7) . . ?
U5A O6 Rb3A 91.7(5) . . ?
U5B O6 Rb3A 102.3(5) . . ?
Rb1 O6 Rb3A 98.0(4) . . ?
Rb3B O6 Rb3A 6.7(8) . . ?
P2 O7 U4 144.1(9) . . ?
P2 O7 Rb3B 91.3(8) . . ?
U4 O7 Rb3B 109.7(7) . . ?
P2 O7 Rb5 75.3(7) . . ?
U4 O7 Rb5 103.6(6) . . ?
Rb3B O7 Rb5 138.1(6) . . ?
P2 O7 Rb7A 119.0(8) . 2_665 ?
U4 O7 Rb7A 93.9(6) . 2_665 ?
Rb3B O7 Rb7A 79.6(8) . 2_665 ?
Rb5 O7 Rb7A 73.3(6) . 2_665 ?
P2 O8 U5B 143.5(9) . 2_656 ?
P2 O8 U5C 135.7(10) . 2_656 ?
U5B O8 U5C 14.1(3) 2_656 2_656 ?
P2 O8 U5A 143.2(8) . 2_656 ?
U5B O8 U5A 6.9(2) 2_656 2_656 ?
U5C O8 U5A 8.7(4) 2_656 2_656 ?
P2 O8 Rb5 89.5(6) . . ?
U5B O8 Rb5 116.2(7) 2_656 . ?
U5C O8 Rb5 129.8(8) 2_656 . ?
U5A O8 Rb5 121.1(6) 2_656 . ?
P2 O8 Rb1 105.6(7) . 2_656 ?
U5B O8 Rb1 99.6(6) 2_656 2_656 ?
U5C O8 Rb1 94.6(6) 2_656 2_656 ?
U5A O8 Rb1 94.4(4) 2_656 2_656 ?
Rb5 O8 Rb1 91.2(4) . 2_656 ?
P3 O9 U1 100.9(4) . 2_666 ?
P3 O9 Rb6B 129.6(6) . . ?
U1 O9 Rb6B 110.2(4) 2_666 . ?
P3 O9 Rb6A 117.5(5) . . ?
U1 O9 Rb6A 102.6(3) 2_666 . ?
Rb6B O9 Rb6A 18.9(4) . . ?
P3 O9 Rb3A 119.2(7) . . ?
U1 O9 Rb3A 98.3(4) 2_666 . ?
Rb6B O9 Rb3A 94.8(6) . . ?
Rb6A O9 Rb3A 113.3(5) . . ?
P3 O9 Rb3B 110.2(11) . . ?
U1 O9 Rb3B 102.9(9) 2_666 . ?
Rb6B O9 Rb3B 100.5(7) . . ?
Rb6A O9 Rb3B 119.4(6) . . ?
Rb3A O9 Rb3B 9.3(7) . . ?
P3 O9 Rb6C 138.0(6) . . ?
U1 O9 Rb6C 112.0(4) 2_666 . ?
Rb6B O9 Rb6C 12.9(4) . . ?
Rb6A O9 Rb6C 31.6(4) . . ?
Rb3A O9 Rb6C 81.9(6) . . ?
Rb3B O9 Rb6C 87.8(7) . . ?
P3 O10 U1 145.3(6) . . ?
P3 O10 U1 97.7(4) . 2_666 ?
U1 O10 U1 115.5(4) . 2_666 ?
P3 O11 U4 153.7(7) . . ?
P3 O11 Rb2 99.5(6) . . ?
U4 O11 Rb2 103.6(4) . . ?
P3 O11 Rb3B 90.3(10) . . ?
U4 O11 Rb3B 103.5(8) . . ?
Rb2 O11 Rb3B 86.3(5) . . ?
P3 O12 U2 152.0(8) . . ?
P3 O12 Rb6A 86.4(5) . . ?
U2 O12 Rb6A 120.9(4) . . ?
P3 O12 Rb2 84.9(7) . . ?
U2 O12 Rb2 93.8(6) . . ?
Rb6A O12 Rb2 79.5(3) . . ?
P4 O13 U4 139.1(7) . 1_455 ?
P4 O13 Rb7A 110.9(8) . . ?
U4 O13 Rb7A 103.5(6) 1_455 . ?
P4 O13 Rb3A 100.0(5) . . ?
U4 O13 Rb3A 107.4(4) 1_455 . ?
Rb7A O13 Rb3A 79.6(5) . . ?
P4 O13 Rb6C 71.7(5) . . ?
U4 O13 Rb6C 146.8(6) 1_455 . ?
Rb7A O13 Rb6C 43.5(6) . . ?
Rb3A O13 Rb6C 68.7(4) . . ?
P4 O14 U1 170.9(9) . 1_455 ?
P4 O14 Rb4B 99.0(6) . . ?
U1 O14 Rb4B 90.1(5) 1_455 . ?
P4 O15 U2 142.7(8) . 1_455 ?
P4 O15 Rb6C 97.8(7) . . ?
U2 O15 Rb6C 109.8(6) 1_455 . ?
P4 O15 Rb6B 102.2(7) . . ?
U2 O15 Rb6B 110.5(6) 1_455 . ?
Rb6C O15 Rb6B 13.3(4) . . ?
P4 O15 Rb6A 107.0(6) . . ?
U2 O15 Rb6A 109.4(4) 1_455 . ?
Rb6C O15 Rb6A 29.7(4) . . ?
Rb6B O15 Rb6A 16.4(4) . . ?
P4 O15 Rb4B 95.4(8) . 2_566 ?
U2 O15 Rb4B 96.6(5) 1_455 2_566 ?
Rb6C O15 Rb4B 112.4(6) . 2_566 ?
Rb6B O15 Rb4B 99.3(6) . 2_566 ?
Rb6A O15 Rb4B 83.2(4) . 2_566 ?
P4 O15 Rb4A 101.1(7) . 2_566 ?
U2 O15 Rb4A 95.1(5) 1_455 2_566 ?
Rb6C O15 Rb4A 105.8(6) . 2_566 ?
Rb6B O15 Rb4A 92.5(5) . 2_566 ?
Rb6A O15 Rb4A 76.3(3) . 2_566 ?
Rb4B O15 Rb4A 8.0(2) 2_566 2_566 ?
P4 O16 U1 158.9(8) . 2_666 ?
P4 O16 Rb6C 81.6(6) . . ?
U1 O16 Rb6C 111.5(5) 2_666 . ?
P4 O16 Rb3A 106.6(7) . . ?
U1 O16 Rb3A 93.3(5) 2_666 . ?
Rb6C O16 Rb3A 74.1(4) . . ?
P4 O16 Rb6B 89.2(6) . . ?
U1 O16 Rb6B 101.4(5) 2_666 . ?
Rb6C O16 Rb6B 12.1(3) . . ?
Rb3A O16 Rb6B 80.6(4) . . ?
P4 O16 Rb6A 97.0(6) . . ?
U1 O16 Rb6A 89.6(4) 2_666 . ?
Rb6C O16 Rb6A 27.4(4) . . ?
Rb3A O16 Rb6A 91.1(3) . . ?
Rb6B O16 Rb6A 15.4(3) . . ?
P4 O16 Rb3B 111.7(8) . . ?
U1 O16 Rb3B 88.4(5) 2_666 . ?
Rb6C O16 Rb3B 74.1(5) . . ?
Rb3A O16 Rb3B 5.3(3) . . ?
Rb6B O16 Rb3B 79.6(5) . . ?
Rb6A O16 Rb3B 89.1(5) . . ?
P5 O17 U3 152.1(8) . 2_665 ?
P5 O17 Rb6B 105.5(6) . . ?
U3 O17 Rb6B 92.3(5) 2_665 . ?
P5 O17 Rb6A 95.6(5) . . ?
U3 O17 Rb6A 95.6(4) 2_665 . ?
Rb6B O17 Rb6A 17.4(3) . . ?
P5 O17 Rb6C 109.8(7) . . ?
U3 O17 Rb6C 92.2(5) 2_665 . ?
Rb6B O17 Rb6C 12.4(3) . . ?
Rb6A O17 Rb6C 29.7(4) . . ?
P5 O17 Rb5 85.1(4) . 2_665 ?
U3 O17 Rb5 107.4(4) 2_665 2_665 ?
Rb6B O17 Rb5 113.7(5) . 2_665 ?
Rb6A O17 Rb5 128.1(4) . 2_665 ?
Rb6C O17 Rb5 102.0(5) . 2_665 ?
P5 O18 U2 150.8(8) . 1_455 ?
P5 O18 Rb6A 86.8(5) . . ?
U2 O18 Rb6A 106.4(4) 1_455 . ?
P5 O18 Rb6B 90.6(6) . . ?
U2 O18 Rb6B 95.9(5) 1_455 . ?
Rb6A O18 Rb6B 15.7(3) . . ?
P5 O18 Rb5 101.5(6) . 1_465 ?
U2 O18 Rb5 83.1(3) 1_455 1_465 ?
Rb6A O18 Rb5 144.2(4) . 1_465 ?
Rb6B O18 Rb5 156.8(5) . 1_465 ?
P5 O18 Rb6C 94.7(6) . . ?
U2 O18 Rb6C 87.4(5) 1_455 . ?
Rb6A O18 Rb6C 26.7(3) . . ?
Rb6B O18 Rb6C 11.1(3) . . ?
Rb5 O18 Rb6C 161.2(5) 1_465 . ?
P5 O19 U2 162.8(11) . 2_675 ?
P5 O19 Rb5 99.4(7) . 2_665 ?
U2 O19 Rb5 96.6(4) 2_675 2_665 ?
P5 O20 U3 150.8(8) . 1_565 ?
P5 O20 Rb6A 114.5(6) . 2_675 ?
U3 O20 Rb6A 92.8(3) 1_565 2_675 ?
P5 O20 Rb6B 128.6(7) . 2_675 ?
U3 O20 Rb6B 79.6(4) 1_565 2_675 ?
Rb6A O20 Rb6B 14.4(3) 2_675 2_675 ?
U1 O21 Rb1 135.6(6) . 2_666 ?
U1 O21 Rb3A 100.9(5) . 2_666 ?
Rb1 O21 Rb3A 103.2(5) 2_666 2_666 ?
U1 O21 Rb4B 113.7(5) . 2_666 ?
Rb1 O21 Rb4B 103.3(4) 2_666 2_666 ?
Rb3A O21 Rb4B 89.4(5) 2_666 2_666 ?
U1 O21 Rb3B 103.2(5) . 2_666 ?
Rb1 O21 Rb3B 96.8(8) 2_666 2_666 ?
Rb3A O21 Rb3B 7.9(5) 2_666 2_666 ?
Rb4B O21 Rb3B 95.3(9) 2_666 2_666 ?
U1 O22 Rb1 134.3(6) . . ?
U1 O22 Rb4A 124.2(5) . 1_655 ?
Rb1 O22 Rb4A 97.5(4) . 1_655 ?
U1 O22 Rb4B 115.6(5) . 1_655 ?
Rb1 O22 Rb4B 104.5(4) . 1_655 ?
Rb4A O22 Rb4B 9.1(3) 1_655 1_655 ?
U1 O22 Rb6A 103.4(4) . 2_666 ?
Rb1 O22 Rb6A 99.3(3) . 2_666 ?
Rb4A O22 Rb6A 82.9(3) 1_655 2_666 ?
Rb4B O22 Rb6A 87.5(5) 1_655 2_666 ?
U2 O23 Rb5 102.4(5) . 1_565 ?
U2 O23 Rb4B 119.2(6) . 2_666 ?
Rb5 O23 Rb4B 109.1(5) 1_565 2_666 ?
U2 O23 Rb1 127.8(6) . 2_666 ?
Rb5 O23 Rb1 89.5(3) 1_565 2_666 ?
Rb4B O23 Rb1 103.4(4) 2_666 2_666 ?
U2 O23 Rb4A 117.0(5) . 2_666 ?
Rb5 O23 Rb4A 102.2(4) 1_565 2_666 ?
Rb4B O23 Rb4A 8.8(3) 2_666 2_666 ?
Rb1 O23 Rb4A 109.4(4) 2_666 2_666 ?
U2 O24 Rb5 122.2(7) . 2_765 ?
U2 O24 Rb7A 127.8(8) . 1_655 ?
Rb5 O24 Rb7A 88.3(7) 2_765 1_655 ?
U2 O24 Rb2 125.2(7) . . ?
Rb5 O24 Rb2 94.8(4) 2_765 . ?
Rb7A O24 Rb2 87.9(6) 1_655 . ?
U3 O25 Rb6C 122.7(7) . 2_665 ?
U3 O25 Rb6B 115.2(7) . 2_665 ?
Rb6C O25 Rb6B 14.3(4) 2_665 2_665 ?
U3 O25 Rb2 128.1(6) . 2_665 ?
Rb6C O25 Rb2 96.1(5) 2_665 2_665 ?
Rb6B O25 Rb2 93.8(4) 2_665 2_665 ?
U3 O25 Rb6A 104.3(5) . 2_665 ?
Rb6C O25 Rb6A 30.3(4) 2_665 2_665 ?
Rb6B O25 Rb6A 16.0(4) 2_665 2_665 ?
Rb2 O25 Rb6A 92.7(3) 2_665 2_665 ?
U3 O25 Rb7A 122.1(8) . 2_665 ?
Rb6C O25 Rb7A 47.8(6) 2_665 2_665 ?
Rb6B O25 Rb7A 61.9(6) 2_665 2_665 ?
Rb2 O25 Rb7A 109.2(6) 2_665 2_665 ?
Rb6A O25 Rb7A 77.3(5) 2_665 2_665 ?
U4 O26 Rb2 122.6(5) . 2_765 ?
U4 O26 Rb7A 123.6(7) . 2_665 ?
Rb2 O26 Rb7A 92.6(6) 2_765 2_665 ?
U4 O26 Rb2 117.2(5) . . ?
Rb2 O26 Rb2 118.1(4) 2_765 . ?
Rb7A O26 Rb2 65.6(7) 2_665 . ?
U4 O26 Rb7A 113.8(6) . 1_655 ?
Rb2 O26 Rb7A 63.2(5) 2_765 1_655 ?
Rb7A O26 Rb7A 121.6(6) 2_665 1_655 ?
Rb2 O26 Rb7A 80.0(6) . 1_655 ?
U4 O27 Rb4B 135.6(7) . 1_655 ?
U4 O27 Rb4A 143.6(6) . 1_655 ?
Rb4B O27 Rb4A 8.9(2) 1_655 1_655 ?
U4 O27 Rb1 132.8(6) . . ?
Rb4B O27 Rb1 91.5(4) 1_655 . ?
Rb4A O27 Rb1 83.6(3) 1_655 . ?
O28B O28A U5A 80(2) . . ?
O28B O28A U5B 63(2) . . ?
U5A O28A U5B 17.26(18) . . ?
O28B O28A U5C 69(2) . . ?
U5A O28A U5C 14.9(3) . . ?
U5B O28A U5C 12.3(3) . . ?
O28B O28A Rb4B 99(2) . . ?
U5A O28A Rb4B 140.3(9) . . ?
U5B O28A Rb4B 136.5(9) . . ?
U5C O28A Rb4B 148.6(9) . . ?
O28B O28A Rb4A 94(2) . . ?
U5A O28A Rb4A 131.6(9) . . ?
U5B O28A Rb4A 126.8(8) . . ?
U5C O28A Rb4A 138.9(8) . . ?
Rb4B O28A Rb4A 9.8(3) . . ?
O28B O28A Rb1 56(3) . . ?
U5A O28A Rb1 99.6(6) . . ?
U5B O28A Rb1 90.5(6) . . ?
U5C O28A Rb1 85.2(6) . . ?
Rb4B O28A Rb1 113.2(6) . . ?
Rb4A O28A Rb1 116.9(5) . . ?
O28B O28A Rb3A 148(3) . . ?
U5A O28A Rb3A 100.0(6) . . ?
U5B O28A Rb3A 115.3(6) . . ?
U5C O28A Rb3A 104.5(7) . . ?
Rb4B O28A Rb3A 100.0(7) . . ?
Rb4A O28A Rb3A 108.2(6) . . ?
Rb1 O28A Rb3A 92.9(5) . . ?
O28B O28A Rb3B 142(3) . . ?
U5A O28A Rb3B 95.9(8) . . ?
U5B O28A Rb3B 110.2(9) . . ?
U5C O28A Rb3B 98.9(10) . . ?
Rb4B O28A Rb3B 106.9(10) . . ?
Rb4A O28A Rb3B 115.3(10) . . ?
Rb1 O28A Rb3B 87.4(7) . . ?
Rb3A O28A Rb3B 7.5(5) . . ?
O28A O28B U5B 82(2) . . ?
O28A O28B U5A 65(2) . . ?
U5B O28B U5A 16.8(4) . . ?
O28A O28B U5C 79(2) . . ?
U5B O28B U5C 12.1(4) . . ?
U5A O28B U5C 16.6(4) . . ?
O28A O28B Rb1 105(3) . . ?
U5B O28B Rb1 112(2) . . ?
U5A O28B Rb1 112.7(18) . . ?
U5C O28B Rb1 100.9(18) . . ?
O28A O28B Rb4B 59(2) . . ?
U5B O28B Rb4B 124(2) . . ?
U5A O28B Rb4B 112.3(18) . . ?
U5C O28B Rb4B 128.9(19) . . ?
Rb1 O28B Rb4B 116.1(13) . . ?
O28A O28B Rb4A 65(2) . . ?
U5B O28B Rb4A 121(2) . . ?
U5A O28B Rb4A 111.5(18) . . ?
U5C O28B Rb4A 127.8(19) . . ?
Rb1 O28B Rb4A 123.1(13) . . ?
Rb4B O28B Rb4A 9.2(3) . . ?
O28A O28B Rb5 162(3) . 2_656 ?
U5B O28B Rb5 102.5(16) . 2_656 ?
U5A O28B Rb5 118.9(16) . 2_656 ?
U5C O28B Rb5 108.8(15) . 2_656 ?
Rb1 O28B Rb5 89.3(11) . 2_656 ?
Rb4B O28B Rb5 105.7(12) . 2_656 ?
Rb4A O28B Rb5 99.0(12) . 2_656 ?
U5C O29 U5A 19.0(4) . . ?
U5C O29 U5B 13.9(4) . . ?
U5A O29 U5B 18.62(17) . . ?
U5C O29 Rb1 120.2(6) . 2_656 ?
U5A O29 Rb1 136.9(5) . 2_656 ?
U5B O29 Rb1 130.1(5) . 2_656 ?
U5C O29 Rb4A 146.2(7) . 2_556 ?
U5A O29 Rb4A 130.1(5) . 2_556 ?
U5B O29 Rb4A 133.6(5) . 2_556 ?
Rb1 O29 Rb4A 92.9(3) 2_656 2_556 ?
U5C O29 Rb4B 142.9(7) . 2_556 ?
U5A O29 Rb4B 128.5(5) . 2_556 ?
U5B O29 Rb4B 129.6(6) . 2_556 ?
Rb1 O29 Rb4B 94.6(4) 2_656 2_556 ?
Rb4A O29 Rb4B 6.3(4) 2_556 2_556 ?
U3 O30 Rb6A 124.5(6) 1_565 . ?
U3 O30 Rb4A 128.2(6) 1_565 2_566 ?
Rb6A O30 Rb4A 84.2(3) . 2_566 ?
U3 O30 Rb1 122.4(5) 1_565 2_666 ?
Rb6A O30 Rb1 98.6(3) . 2_666 ?
Rb4A O30 Rb1 88.1(3) 2_566 2_666 ?
U3 O30 Rb4B 129.9(6) 1_565 2_566 ?
Rb6A O30 Rb4B 82.3(4) . 2_566 ?
Rb4A O30 Rb4B 2.0(4) 2_566 2_566 ?
Rb1 O30 Rb4B 87.7(4) 2_666 2_566 ?

_refine_diff_density_max         2.772
_refine_diff_density_min         -3.161
_refine_diff_density_rms         0.340


_exptl_crystal_recrystallization_method 'From the Melt'
_exptl_crystal_preparation       Luminescent
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_Rb76U8P2O326F04
_database_code_depnum_ccdc_archive 'CCDC 1984891'
loop_
_audit_author_name
_audit_author_address
'Christian Juillerat'
;University of South Carolina
United States of America
;
_audit_update_record             
;
2020-02-18 deposited with the CCDC.	2020-04-07 downloaded from the CCDC.
;
_audit_creation_date             2020-02-04
_audit_creation_method           
;
Olex2 1.2
(compiled May 18 2018 14:05:52 for OlexSys, GUI svn.r5506)
;
_shelx_SHELXL_version_number     2016/6
_chemical_name_common            ?
_chemical_name_systematic        Rb7.5[(UO2)8O8.6F0.4(PO4)2]
_chemical_formula_moiety         '0.5(F0.8 O65.2 P4 Rb15.2 U16)'
_chemical_formula_sum            'F0.40 O32.60 P2 Rb7.60 U8'
_chemical_formula_weight         3144.95
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Rb Rb -0.9393 2.9676 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
U U -9.6767 9.6646 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_H-M_alt        'P 1 21/n 1'
_space_group_name_Hall           '-P 2yn'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'

_cell_length_a                   9.5935(5)
_cell_length_b                   13.7652(8)
_cell_length_c                   13.2983(8)
_cell_angle_alpha                90
_cell_angle_beta                 101.343(2)
_cell_angle_gamma                90
_cell_volume                     1721.82(17)
_cell_formula_units_Z            2
_cell_measurement_reflns_used    9562
_cell_measurement_temperature    303(2)
_cell_measurement_theta_max      35.67
_cell_measurement_theta_min      2.83
_shelx_estimated_absorpt_T_max   0.643
_shelx_estimated_absorpt_T_min   0.325
_exptl_absorpt_coefficient_mu    48.351
_exptl_absorpt_correction_T_max  0.1661
_exptl_absorpt_correction_T_min  0.0738
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
SADABS-2016/2 (Bruker,2016) was used for absorption correction.
wR2(int) was 0.1673 before and 0.0776 after correction.
The Ratio of minimum to maximum transmission is 0.4443.
The λ/2 correction factor is Not present.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            orange
_exptl_crystal_colour_primary    orange
_exptl_crystal_density_diffrn    6.066
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       shard
_exptl_crystal_F_000             2623
_exptl_crystal_size_max          0.03
_exptl_crystal_size_mid          0.02
_exptl_crystal_size_min          0.01
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0674
_diffrn_reflns_av_unetI/netI     0.0177
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 1.000
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_l_max       17
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_number            109936
_diffrn_reflns_point_group_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 1.000
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         27.492
_diffrn_reflns_theta_min         2.151
_diffrn_ambient_temperature      302.88
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_diffrn_standards_number         0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                3757
_reflns_number_total             3952
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       ?
_computing_data_collection       ?
_computing_data_reduction        ?
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    'ShelXT (Sheldrick, 2015)'
_refine_diff_density_max         2.573
_refine_diff_density_min         -2.114
_refine_diff_density_rms         0.382
_refine_ls_extinction_coef       0.000081(9)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     'SHELXL-2016/6 (Sheldrick 2016)'
_refine_ls_goodness_of_fit_ref   1.362
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     271
_refine_ls_number_reflns         3952
_refine_ls_number_restraints     18
_refine_ls_R_factor_all          0.0428
_refine_ls_R_factor_gt           0.0405
_refine_ls_restrained_S_all      1.362
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0056P)²+99.4920P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0865
_refine_ls_wR_factor_ref         0.0874
_refine_special_details          ?
_olex2_refinement_description    
;
1. Shared sites
{F4, O4}
2. Uiso/Uaniso restraints and constraints
Uanis(O13) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.01
Uanis(F4) \\sim Ueq, Uanis(O4) \\sim Ueq: with sigma of 0.01 and sigma for
terminal atoms of 0.01
Uanis(F4) = Uanis(O4)
3. Others
 Sof(Rb3A)=1-FVAR(1)
 Sof(Rb3B)=FVAR(1)
 Sof(Rb4B)=1-FVAR(2)
 Sof(Rb4A)=FVAR(2)
 Fixed Sof: U4A(0.5) U4B(0.5) Rb5(0.3) F4(0.2) O4(0.8) O11(0.5)
;
_atom_sites_solution_hydrogens   .
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
U1 U 0.51046(6) 0.13148(3) 0.51401(4) 0.01359(12) Uani 1 1 d . . . . .
U2 U 0.10209(6) 0.11260(4) 0.92938(4) 0.01353(12) Uani 1 1 d . . . . .
U3 U 0.31119(6) 0.04304(4) 0.70874(4) 0.01519(13) Uani 1 1 d . . . . .
U4A U 0.3593(4) 0.3335(2) 0.6456(3) 0.0145(5) Uani 0.5 1 d . . . . .
U4B U 0.3686(4) 0.3546(2) 0.6263(3) 0.0129(5) Uani 0.5 1 d . . . . .
Rb1 Rb 0.000000 0.500000 0.500000 0.0262(4) Uani 1 2 d S T P . .
Rb2A Rb 0.1706(2) 0.30497(18) 0.33269(14) 0.0460(5) Uani 1 1 d . . . . .
Rb3A Rb 0.6265(7) 0.4777(5) 0.8996(14) 0.039(3) Uani 0.79(5) 1 d . . . . .
Rb3B Rb 0.604(3) 0.459(2) 0.9323(18) 0.028(4) Uani 0.21(5) 1 d . . . . .
Rb4A Rb 0.4590(15) 0.2532(11) 1.1405(10) 0.036(2) Uani 0.66(12) 1 d . . . . .
Rb4B Rb 0.451(4) 0.234(6) 1.155(5) 0.060(8) Uani 0.34(12) 1 d . . . . .
Rb5 Rb 0.7532(5) 0.4724(4) 0.7196(4) 0.0255(10) Uani 0.3 1 d . . . . .
P1 P 0.2838(4) 0.2876(3) 0.8664(3) 0.0200(8) Uani 1 1 d . . . . .
F4 F 0.3888(11) 0.1768(7) 0.6441(8) 0.021(2) Uani 0.2 1 d . U . . .
O1 O 0.6669(12) 0.1258(8) 0.6154(8) 0.023(2) Uani 1 1 d . . . . .
O2 O 0.3595(12) 0.1399(8) 0.4077(8) 0.023(2) Uani 1 1 d . . . . .
O3 O 0.4055(11) -0.0023(7) 0.5701(8) 0.019(2) Uani 1 1 d . . . . .
O4 O 0.3888(11) 0.1768(7) 0.6441(8) 0.021(2) Uani 0.8 1 d . U . . .
O5 O 0.4816(12) 0.0213(9) 0.7902(8) 0.026(2) Uani 1 1 d . . . . .
O6 O 0.1392(11) 0.0631(8) 0.6290(9) 0.024(2) Uani 1 1 d . . . . .
O7 O 0.2748(16) 0.1829(9) 0.8184(11) 0.044(4) Uani 1 1 d . . . . .
O8 O 0.1992(16) -0.0018(9) 0.8466(9) 0.037(3) Uani 1 1 d . . . . .
O9 O -0.0438(12) 0.1244(9) 0.8192(9) 0.026(2) Uani 1 1 d . . . . .
O10 O 0.2577(12) 0.1069(9) 1.0342(8) 0.026(2) Uani 1 1 d . . . . .
O11 O 0.041(2) -0.0237(15) 0.9830(15) 0.020(4) Uani 0.5 1 d . . . . .
O12 O 0.1568(13) 0.2848(7) 0.9217(9) 0.027(3) Uani 1 1 d . . . . .
O13 O 0.4207(18) 0.3139(12) 0.9365(14) 0.063(5) Uani 1 1 d . U . . .
O14 O 0.2415(12) 0.3628(8) 0.7771(8) 0.024(2) Uani 1 1 d . . . . .
O15 O 0.5290(13) 0.3593(10) 0.7255(10) 0.036(3) Uani 1 1 d . . . . .
O16 O 0.1933(13) 0.3310(9) 0.5493(10) 0.035(3) Uani 1 1 d . . . . .
O17 O 0.4799(13) 0.3000(8) 0.5211(9) 0.029(3) Uani 1 1 d . . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
U1 U1 3.6402(10) 3_656 ?
U1 U3 3.7135(7) . ?
U1 U4A 3.728(4) . ?
U1 U4B 3.784(4) . ?
U1 F4 2.354(10) . ?
U1 O1 1.811(11) . ?
U1 O2 1.817(11) . ?
U1 O3 2.328(10) 3_656 ?
U1 O3 2.293(10) . ?
U1 O12 2.342(10) 4_665 ?
U1 O17 2.343(12) . ?
U2 U4B 3.792(3) 4_566 ?
U2 U4B 3.649(3) 2_546 ?
U2 P1 3.181(4) . ?
U2 O7 2.612(14) . ?
U2 O8 2.228(11) . ?
U2 O9 1.824(12) . ?
U2 O10 1.833(11) . ?
U2 O11 2.31(2) 3_557 ?
U2 O11 2.13(2) . ?
U2 O12 2.435(11) . ?
U2 O17 2.207(11) 4_566 ?
U3 Rb1 3.9842(6) 2_546 ?
U3 Rb3B 3.821(16) 4_565 ?
U3 F4 2.221(9) . ?
U3 O3 2.294(10) . ?
U3 O5 1.800(11) . ?
U3 O6 1.799(11) . ?
U3 O7 2.481(13) . ?
U3 O8 2.381(13) . ?
U3 O14 2.547(11) 2_546 ?
U4A Rb2A 3.977(4) 4_666 ?
U4A P1 3.222(5) . ?
U4A F4 2.177(10) . ?
U4A O8 2.343(13) 2_556 ?
U4A O11 2.890(19) 2_556 ?
U4A O14 2.297(11) . ?
U4A O15 1.796(13) . ?
U4A O16 1.837(13) . ?
U4A O17 2.246(12) . ?
U4B Rb5 3.997(6) . ?
U4B F4 2.464(10) . ?
U4B O8 2.133(14) 2_556 ?
U4B O11 2.484(19) 2_556 ?
U4B O14 2.547(11) . ?
U4B O15 1.820(13) . ?
U4B O16 1.818(13) . ?
U4B O17 2.061(12) . ?
Rb1 Rb4B 3.90(4) 4_565 ?
Rb1 Rb4B 3.90(4) 2_556 ?
Rb1 O5 2.776(11) 2_556 ?
Rb1 O5 2.776(11) 4_565 ?
Rb1 O8 3.189(14) 2_556 ?
Rb1 O8 3.189(14) 4_565 ?
Rb1 O10 2.861(11) 2_556 ?
Rb1 O10 2.861(11) 4_565 ?
Rb1 O16 2.967(12) . ?
Rb1 O16 2.967(12) 3_566 ?
Rb2A Rb3B 3.96(2) 4_565 ?
Rb2A Rb5 3.257(6) 3_666 ?
Rb2A F4 3.316(11) 4_565 ?
Rb2A O1 3.036(10) 4_565 ?
Rb2A O2 2.955(11) . ?
Rb2A O5 2.987(12) 4_565 ?
Rb2A O9 2.946(11) 4_665 ?
Rb2A O13 3.41(2) 4_565 ?
Rb2A O15 2.868(15) 4_565 ?
Rb2A O16 2.869(13) . ?
Rb2A O17 3.487(13) . ?
Rb3A Rb3B 3.55(4) 3_667 ?
Rb3A Rb3B 0.59(2) . ?
Rb3A Rb4A 3.808(17) 3_667 ?
Rb3A Rb5 2.89(2) . ?
Rb3A O1 2.878(17) 2_656 ?
Rb3A O2 2.745(12) 4_666 ?
Rb3A O3 3.168(12) 4_666 ?
Rb3A O6 3.08(2) 4_666 ?
Rb3A O6 2.764(12) 2_556 ?
Rb3A O9 3.50(2) 2_556 ?
Rb3A O13 3.10(2) . ?
Rb3A O15 2.836(15) . ?
Rb3B Rb3B 3.14(5) 3_667 ?
Rb3B Rb5 3.42(4) . ?
Rb3B O1 3.33(5) 2_656 ?
Rb3B O2 2.882(19) 4_666 ?
Rb3B O3 3.17(2) 4_666 ?
Rb3B O6 2.59(3) 4_666 ?
Rb3B O6 2.719(17) 2_556 ?
Rb3B O13 3.61(3) 3_667 ?
Rb3B O13 2.67(4) . ?
Rb3B O15 3.030(18) . ?
Rb4A Rb5 3.934(14) 4_566 ?
Rb4A P1 3.731(15) . ?
Rb4A P1 3.921(16) 4_666 ?
Rb4A O1 3.220(18) 4_566 ?
Rb4A O6 3.084(17) 4_666 ?
Rb4A O7 3.57(2) 4_666 ?
Rb4A O9 2.917(17) 4_666 ?
Rb4A O10 2.952(19) . ?
Rb4A O13 2.79(2) . ?
Rb4A O14 3.36(2) 4_666 ?
Rb4A O16 2.990(19) 4_666 ?
Rb4B Rb5 3.62(11) 4_566 ?
Rb4B P1 3.83(4) 4_666 ?
Rb4B O1 3.30(4) 4_566 ?
Rb4B O5 3.62(9) 3_657 ?
Rb4B O6 3.38(10) 4_666 ?
Rb4B O7 3.61(4) 4_666 ?
Rb4B O9 2.93(3) 4_666 ?
Rb4B O10 2.81(5) . ?
Rb4B O13 3.06(10) . ?
Rb4B O14 3.22(5) 4_666 ?
Rb4B O16 3.07(5) 4_666 ?
Rb5 O1 3.033(12) 2_656 ?
Rb5 O2 2.947(12) 4_666 ?
Rb5 O5 2.660(12) 2_656 ?
Rb5 O9 2.875(13) 2_556 ?
Rb5 O10 2.705(12) 4_665 ?
Rb5 O11 3.47(2) 4_665 ?
Rb5 O11 3.50(2) 2_556 ?
Rb5 O15 2.669(14) . ?
P1 O7 1.572(14) . ?
P1 O12 1.543(11) . ?
P1 O13 1.497(17) . ?
P1 O14 1.567(10) . ?
O11 O11 1.17(4) 3_557 ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
U1 U1 U3 73.730(17) 3_656 . ?
U1 U1 U4A 140.46(4) 3_656 . ?
U1 U1 U4B 146.19(4) 3_656 . ?
U3 U1 U4A 67.43(4) . . ?
U3 U1 U4B 73.54(4) . . ?
U4A U1 U4B 6.19(5) . . ?
F4 U1 U1 108.3(2) . 3_656 ?
F4 U1 U3 34.6(2) . . ?
F4 U1 U4A 33.1(2) . . ?
F4 U1 U4B 39.3(2) . . ?
O1 U1 U1 93.1(3) . 3_656 ?
O1 U1 U3 86.1(3) . . ?
O1 U1 U4A 91.4(3) . . ?
O1 U1 U4B 92.9(3) . . ?
O1 U1 F4 85.5(4) . . ?
O1 U1 O2 176.9(5) . . ?
O1 U1 O3 94.3(4) . . ?
O1 U1 O3 90.6(4) . 3_656 ?
O1 U1 O12 85.3(5) . 4_665 ?
O1 U1 O17 96.0(5) . . ?
O2 U1 U1 88.0(3) . 3_656 ?
O2 U1 U3 97.0(3) . . ?
O2 U1 U4A 89.6(4) . . ?
O2 U1 U4B 87.8(4) . . ?
O2 U1 F4 96.9(4) . . ?
O2 U1 O3 88.5(4) . 3_656 ?
O2 U1 O3 88.3(4) . . ?
O2 U1 O12 91.7(5) . 4_665 ?
O2 U1 O17 83.2(5) . . ?
O3 U1 U1 38.4(2) . 3_656 ?
O3 U1 U1 37.7(2) 3_656 3_656 ?
O3 U1 U3 111.1(2) 3_656 . ?
O3 U1 U3 35.9(2) . . ?
O3 U1 U4A 177.4(3) 3_656 . ?
O3 U1 U4A 102.1(2) . . ?
O3 U1 U4B 108.0(2) . . ?
O3 U1 U4B 174.4(3) 3_656 . ?
O3 U1 F4 70.1(3) . . ?
O3 U1 F4 145.5(3) 3_656 . ?
O3 U1 O3 76.0(4) . 3_656 ?
O3 U1 O12 155.9(3) . 4_665 ?
O3 U1 O12 79.8(3) 3_656 4_665 ?
O3 U1 O17 146.5(4) 3_656 . ?
O3 U1 O17 135.7(4) . . ?
O12 U1 U1 117.5(2) 4_665 3_656 ?
O12 U1 U3 166.1(3) 4_665 . ?
O12 U1 U4A 102.0(3) 4_665 . ?
O12 U1 U4B 96.1(3) 4_665 . ?
O12 U1 F4 133.7(3) 4_665 . ?
O12 U1 O17 68.1(4) 4_665 . ?
O17 U1 U1 169.7(3) . 3_656 ?
O17 U1 U3 102.2(3) . . ?
O17 U1 U4A 34.8(3) . . ?
O17 U1 U4B 28.7(3) . . ?
O17 U1 F4 67.9(4) . . ?
U4B U2 U1 168.58(6) 2_546 4_566 ?
U4B U2 U1 59.33(5) 4_566 4_566 ?
U4B U2 U4B 109.58(4) 2_546 4_566 ?
P1 U2 U1 63.43(7) . 4_566 ?
P1 U2 U4B 121.36(9) . 4_566 ?
P1 U2 U4B 127.99(9) . 2_546 ?
O7 U2 U1 91.9(3) . 4_566 ?
O7 U2 U4B 99.4(3) . 2_546 ?
O7 U2 U4B 150.8(3) . 4_566 ?
O7 U2 P1 29.5(3) . . ?
O8 U2 U1 158.8(4) . 4_566 ?
O8 U2 U4B 141.8(4) . 4_566 ?
O8 U2 U4B 32.4(4) . 2_546 ?
O8 U2 P1 95.8(4) . . ?
O8 U2 O7 67.0(5) . . ?
O8 U2 O11 102.8(6) . 3_557 ?
O8 U2 O12 123.6(4) . . ?
O9 U2 U1 88.3(4) . 4_566 ?
O9 U2 U4B 90.1(4) . 2_546 ?
O9 U2 U4B 94.6(3) . 4_566 ?
O9 U2 P1 95.5(4) . . ?
O9 U2 O7 89.1(5) . . ?
O9 U2 O8 89.7(5) . . ?
O9 U2 O10 175.2(5) . . ?
O9 U2 O11 90.8(6) . 3_557 ?
O9 U2 O11 97.4(7) . . ?
O9 U2 O12 91.0(5) . . ?
O9 U2 O17 89.3(5) . 4_566 ?
O10 U2 U1 90.9(4) . 4_566 ?
O10 U2 U4B 91.6(4) . 2_546 ?
O10 U2 U4B 89.1(4) . 4_566 ?
O10 U2 P1 80.0(4) . . ?
O10 U2 O7 86.2(5) . . ?
O10 U2 O8 89.3(5) . . ?
O10 U2 O11 93.9(6) . 3_557 ?
O10 U2 O11 86.8(7) . . ?
O10 U2 O12 85.6(5) . . ?
O10 U2 O17 92.6(5) . 4_566 ?
O11 U2 U1 98.3(5) 3_557 4_566 ?
O11 U2 U1 127.8(5) . 4_566 ?
O11 U2 U4B 70.4(5) 3_557 2_546 ?
O11 U2 U4B 68.5(5) . 4_566 ?
O11 U2 U4B 39.4(5) 3_557 4_566 ?
O11 U2 U4B 41.3(5) . 2_546 ?
O11 U2 P1 163.1(6) . . ?
O11 U2 P1 160.4(5) 3_557 . ?
O11 U2 O7 169.8(5) 3_557 . ?
O11 U2 O7 139.7(6) . . ?
O11 U2 O8 73.3(6) . . ?
O11 U2 O11 30.2(10) . 3_557 ?
O11 U2 O12 133.6(5) 3_557 . ?
O11 U2 O12 161.3(6) . . ?
O11 U2 O17 94.8(6) . 4_566 ?
O12 U2 U1 35.4(2) . 4_566 ?
O12 U2 U4B 155.9(2) . 2_546 ?
O12 U2 U4B 94.3(2) . 4_566 ?
O12 U2 P1 28.1(2) . . ?
O12 U2 O7 56.6(4) . . ?
O17 U2 U1 33.2(3) 4_566 4_566 ?
O17 U2 U4B 135.5(3) 4_566 2_546 ?
O17 U2 U4B 26.3(3) 4_566 4_566 ?
O17 U2 P1 96.4(3) 4_566 . ?
O17 U2 O7 125.1(4) 4_566 . ?
O17 U2 O8 167.8(5) 4_566 . ?
O17 U2 O11 65.1(6) 4_566 3_557 ?
O17 U2 O12 68.6(4) 4_566 . ?
U1 U3 U2 146.910(18) . . ?
U1 U3 Rb1 121.918(16) . 2_546 ?
U1 U3 Rb3B 64.8(3) . 4_565 ?
U2 U3 Rb1 61.195(11) . 2_546 ?
Rb3B U3 U2 117.9(6) 4_565 . ?
Rb3B U3 Rb1 170.2(3) 4_565 2_546 ?
F4 U3 U1 36.9(3) . . ?
F4 U3 U2 110.0(3) . . ?
F4 U3 Rb1 112.1(3) . 2_546 ?
F4 U3 Rb3B 77.6(4) . 4_565 ?
F4 U3 O3 72.5(4) . . ?
F4 U3 O7 71.4(4) . . ?
F4 U3 O8 138.5(4) . . ?
F4 U3 O14 157.3(3) . 2_546 ?
O3 U3 U1 35.9(2) . . ?
O3 U3 U2 173.1(3) . . ?
O3 U3 Rb1 124.4(3) . 2_546 ?
O3 U3 Rb3B 55.8(7) . 4_565 ?
O3 U3 O7 143.8(4) . . ?
O3 U3 O8 149.0(4) . . ?
O3 U3 O14 84.8(3) . 2_546 ?
O5 U3 U1 86.7(4) . . ?
O5 U3 U2 97.2(4) . . ?
O5 U3 Rb1 37.3(4) . 2_546 ?
O5 U3 Rb3B 144.9(7) . 4_565 ?
O5 U3 F4 92.1(5) . . ?
O5 U3 O3 89.0(5) . . ?
O5 U3 O7 89.5(5) . . ?
O5 U3 O8 89.3(5) . . ?
O5 U3 O14 87.9(5) . 2_546 ?
O6 U3 U1 94.4(4) . . ?
O6 U3 U2 82.0(4) . . ?
O6 U3 Rb1 141.7(4) . 2_546 ?
O6 U3 Rb3B 35.9(7) . 4_565 ?
O6 U3 F4 89.0(5) . . ?
O6 U3 O3 91.7(4) . . ?
O6 U3 O5 178.8(5) . . ?
O6 U3 O7 90.5(5) . . ?
O6 U3 O8 89.6(5) . . ?
O6 U3 O14 91.2(5) . 2_546 ?
O7 U3 U1 107.9(3) . . ?
O7 U3 U2 39.7(3) . . ?
O7 U3 Rb1 68.5(3) . 2_546 ?
O7 U3 Rb3B 117.6(7) . 4_565 ?
O7 U3 O14 131.3(4) . 2_546 ?
O8 U3 U1 173.7(3) . . ?
O8 U3 U2 29.1(3) . . ?
O8 U3 Rb1 53.2(3) . 2_546 ?
O8 U3 Rb3B 120.7(5) . 4_565 ?
O8 U3 O7 67.1(4) . . ?
O8 U3 O14 64.2(4) . 2_546 ?
O14 U3 U1 120.5(2) 2_546 . ?
O14 U3 U2 92.5(2) 2_546 . ?
O14 U3 Rb1 80.9(3) 2_546 2_546 ?
O14 U3 Rb3B 89.5(5) 2_546 4_565 ?
U1 U4A U3 177.88(7) . 2_556 ?
U1 U4A Rb2A 67.82(7) . 4_666 ?
Rb2A U4A U3 111.78(10) 4_666 2_556 ?
P1 U4A U1 117.35(11) . . ?
P1 U4A U3 60.88(9) . 2_556 ?
P1 U4A Rb2A 67.14(10) . 4_666 ?
F4 U4A U1 36.2(3) . . ?
F4 U4A U3 141.8(3) . 2_556 ?
F4 U4A Rb2A 56.5(3) . 4_666 ?
F4 U4A P1 82.3(3) . . ?
F4 U4A O8 172.9(5) . 2_556 ?
F4 U4A O11 127.6(5) . 2_556 ?
F4 U4A O14 105.4(4) . . ?
F4 U4A O17 72.7(4) . . ?
O8 U4A U1 149.5(3) 2_556 . ?
O8 U4A U3 32.5(3) 2_556 2_556 ?
O8 U4A Rb2A 126.4(4) 2_556 4_666 ?
O8 U4A P1 92.9(3) 2_556 . ?
O8 U4A O11 58.6(5) 2_556 2_556 ?
O11 U4A U1 91.4(5) 2_556 . ?
O11 U4A U3 90.6(5) 2_556 2_556 ?
O11 U4A Rb2A 113.6(5) 2_556 4_666 ?
O11 U4A P1 146.4(4) 2_556 . ?
O14 U4A U1 141.6(3) . . ?
O14 U4A U3 36.4(3) . 2_556 ?
O14 U4A Rb2A 91.7(3) . 4_666 ?
O14 U4A P1 26.9(3) . . ?
O14 U4A O8 68.8(4) . 2_556 ?
O14 U4A O11 127.0(5) . 2_556 ?
O15 U4A U1 91.9(4) . . ?
O15 U4A U3 88.9(4) . 2_556 ?
O15 U4A Rb2A 40.8(5) . 4_666 ?
O15 U4A P1 80.8(4) . . ?
O15 U4A F4 95.6(6) . . ?
O15 U4A O8 88.9(6) . 2_556 ?
O15 U4A O11 81.3(6) . 2_556 ?
O15 U4A O14 92.3(5) . . ?
O15 U4A O16 167.7(7) . . ?
O15 U4A O17 86.5(5) . . ?
O16 U4A U1 91.3(4) . . ?
O16 U4A U3 88.3(4) . 2_556 ?
O16 U4A Rb2A 150.2(4) . 4_666 ?
O16 U4A P1 108.2(5) . . ?
O16 U4A F4 94.1(5) . . ?
O16 U4A O8 82.3(5) . 2_556 ?
O16 U4A O11 86.8(6) . 2_556 ?
O16 U4A O14 92.6(5) . . ?
O16 U4A O17 89.1(5) . . ?
O17 U4A U1 36.5(3) . . ?
O17 U4A U3 145.5(3) . 2_556 ?
O17 U4A Rb2A 86.0(4) . 4_666 ?
O17 U4A P1 150.7(4) . . ?
O17 U4A O8 113.2(4) . 2_556 ?
O17 U4A O11 54.9(5) . 2_556 ?
O17 U4A O14 177.6(5) . . ?
U1 U4B U2 61.12(6) . 4_665 ?
U1 U4B Rb5 94.03(11) . . ?
U2 U4B U1 131.45(8) 2_556 . ?
U2 U4B U2 70.42(4) 2_556 4_665 ?
U2 U4B Rb5 62.09(9) 4_665 . ?
U2 U4B Rb5 64.23(9) 2_556 . ?
F4 U4B U1 37.2(2) . . ?
F4 U4B U2 98.0(3) . 4_665 ?
F4 U4B U2 168.2(3) . 2_556 ?
F4 U4B Rb5 108.9(3) . . ?
F4 U4B O11 134.1(6) . 2_556 ?
F4 U4B O14 90.5(3) . . ?
O8 U4B U1 164.6(3) 2_556 . ?
O8 U4B U2 34.0(3) 2_556 2_556 ?
O8 U4B U2 104.3(3) 2_556 4_665 ?
O8 U4B Rb5 82.3(4) 2_556 . ?
O8 U4B F4 157.7(4) 2_556 . ?
O8 U4B O11 68.2(6) 2_556 2_556 ?
O8 U4B O14 67.5(4) 2_556 . ?
O11 U4B U1 97.0(5) 2_556 . ?
O11 U4B U2 34.5(5) 2_556 2_556 ?
O11 U4B U2 36.3(5) 2_556 4_665 ?
O11 U4B Rb5 60.0(5) 2_556 . ?
O11 U4B O14 135.1(6) 2_556 . ?
O14 U4B U1 127.7(2) . . ?
O14 U4B U2 167.9(3) . 4_665 ?
O14 U4B U2 100.7(3) . 2_556 ?
O14 U4B Rb5 107.1(3) . . ?
O15 U4B U1 89.8(4) . . ?
O15 U4B U2 91.4(5) . 2_556 ?
O15 U4B U2 88.1(4) . 4_665 ?
O15 U4B Rb5 33.3(5) . . ?
O15 U4B F4 85.8(5) . . ?
O15 U4B O8 95.0(6) . 2_556 ?
O15 U4B O11 93.3(7) . 2_556 ?
O15 U4B O14 84.0(5) . . ?
O15 U4B O17 91.6(5) . . ?
O16 U4B U1 89.8(4) . . ?
O16 U4B U2 99.2(4) . 2_556 ?
O16 U4B U2 103.9(5) . 4_665 ?
O16 U4B Rb5 160.5(5) . . ?
O16 U4B F4 85.6(5) . . ?
O16 U4B O8 88.9(6) . 2_556 ?
O16 U4B O11 100.6(7) . 2_556 ?
O16 U4B O14 85.3(5) . . ?
O16 U4B O15 166.1(7) . . ?
O16 U4B O17 95.6(6) . . ?
O17 U4B U1 33.0(3) . . ?
O17 U4B U2 98.4(3) . 2_556 ?
O17 U4B U2 28.3(3) . 4_665 ?
O17 U4B Rb5 77.8(3) . . ?
O17 U4B F4 70.2(4) . . ?
O17 U4B O8 132.0(5) . 2_556 ?
O17 U4B O11 64.0(6) . 2_556 ?
O17 U4B O14 160.5(4) . . ?
U3 Rb1 U3 180.0 2_556 4_565 ?
Rb4B Rb1 U3 108.2(11) 2_556 2_556 ?
Rb4B Rb1 U3 108.2(12) 4_565 4_565 ?
Rb4B Rb1 U3 71.8(11) 2_556 4_565 ?
Rb4B Rb1 U3 71.8(12) 4_565 2_556 ?
Rb4B Rb1 Rb4B 180.0 4_565 2_556 ?
O5 Rb1 U3 23.1(2) 4_565 4_565 ?
O5 Rb1 U3 156.9(2) 2_556 4_565 ?
O5 Rb1 U3 23.1(2) 2_556 2_556 ?
O5 Rb1 U3 156.9(2) 4_565 2_556 ?
O5 Rb1 Rb4B 63.1(15) 2_556 4_565 ?
O5 Rb1 Rb4B 116.9(15) 2_556 2_556 ?
O5 Rb1 Rb4B 63.1(15) 4_565 2_556 ?
O5 Rb1 Rb4B 116.9(15) 4_565 4_565 ?
O5 Rb1 O5 180.0 4_565 2_556 ?
O5 Rb1 O8 120.8(3) 4_565 2_556 ?
O5 Rb1 O8 59.2(3) 4_565 4_565 ?
O5 Rb1 O8 59.2(3) 2_556 2_556 ?
O5 Rb1 O8 120.8(3) 2_556 4_565 ?
O5 Rb1 O10 77.8(3) 2_556 4_565 ?
O5 Rb1 O10 102.2(3) 2_556 2_556 ?
O5 Rb1 O10 77.8(3) 4_565 2_556 ?
O5 Rb1 O10 102.2(3) 4_565 4_565 ?
O5 Rb1 O16 93.0(3) 2_556 3_566 ?
O5 Rb1 O16 87.0(3) 4_565 3_566 ?
O5 Rb1 O16 87.0(3) 2_556 . ?
O5 Rb1 O16 93.0(3) 4_565 . ?
O8 Rb1 U3 36.7(2) 2_556 2_556 ?
O8 Rb1 U3 143.3(2) 4_565 2_556 ?
O8 Rb1 U3 36.7(2) 4_565 4_565 ?
O8 Rb1 U3 143.3(2) 2_556 4_565 ?
O8 Rb1 Rb4B 99.0(5) 4_565 4_565 ?
O8 Rb1 Rb4B 81.0(5) 4_565 2_556 ?
O8 Rb1 Rb4B 81.0(5) 2_556 4_565 ?
O8 Rb1 Rb4B 99.0(5) 2_556 2_556 ?
O8 Rb1 O8 180.0 4_565 2_556 ?
O10 Rb1 U3 81.4(2) 4_565 4_565 ?
O10 Rb1 U3 98.6(2) 2_556 4_565 ?
O10 Rb1 U3 98.6(2) 4_565 2_556 ?
O10 Rb1 U3 81.4(2) 2_556 2_556 ?
O10 Rb1 Rb4B 46.1(6) 2_556 2_556 ?
O10 Rb1 Rb4B 133.9(6) 4_565 2_556 ?
O10 Rb1 Rb4B 133.9(6) 2_556 4_565 ?
O10 Rb1 Rb4B 46.1(6) 4_565 4_565 ?
O10 Rb1 O8 56.3(3) 2_556 2_556 ?
O10 Rb1 O8 56.3(3) 4_565 4_565 ?
O10 Rb1 O8 123.7(3) 4_565 2_556 ?
O10 Rb1 O8 123.7(3) 2_556 4_565 ?
O10 Rb1 O10 180.0(4) 4_565 2_556 ?
O10 Rb1 O16 86.9(4) 2_556 . ?
O10 Rb1 O16 86.9(4) 4_565 3_566 ?
O10 Rb1 O16 93.1(4) 4_565 . ?
O10 Rb1 O16 93.1(4) 2_556 3_566 ?
O16 Rb1 U3 104.1(2) 3_566 2_556 ?
O16 Rb1 U3 75.9(2) . 2_556 ?
O16 Rb1 U3 75.9(2) 3_566 4_565 ?
O16 Rb1 U3 104.1(2) . 4_565 ?
O16 Rb1 Rb4B 50.9(12) . 4_565 ?
O16 Rb1 Rb4B 129.1(12) 3_566 4_565 ?
O16 Rb1 Rb4B 129.1(12) . 2_556 ?
O16 Rb1 Rb4B 50.9(12) 3_566 2_556 ?
O16 Rb1 O8 126.5(3) . 4_565 ?
O16 Rb1 O8 53.5(3) 3_566 4_565 ?
O16 Rb1 O8 126.5(3) 3_566 2_556 ?
O16 Rb1 O8 53.5(3) . 2_556 ?
O16 Rb1 O16 180.0 3_566 . ?
Rb3B Rb2A U4A 67.6(2) 4_565 4_565 ?
Rb5 Rb2A U4A 119.33(12) 3_666 4_565 ?
Rb5 Rb2A Rb3B 172.7(3) 3_666 4_565 ?
Rb5 Rb2A F4 87.2(2) 3_666 4_565 ?
Rb5 Rb2A O13 138.0(3) 3_666 4_565 ?
Rb5 Rb2A O17 88.7(2) 3_666 . ?
F4 Rb2A U4A 33.18(18) 4_565 4_565 ?
F4 Rb2A Rb3B 99.2(2) 4_565 4_565 ?
F4 Rb2A O13 79.0(3) 4_565 4_565 ?
F4 Rb2A O17 175.4(3) 4_565 . ?
O1 Rb2A U4A 71.8(2) 4_565 4_565 ?
O1 Rb2A Rb3B 129.3(5) 4_565 4_565 ?
O1 Rb2A Rb5 57.5(2) 4_565 3_666 ?
O1 Rb2A F4 53.2(3) 4_565 4_565 ?
O1 Rb2A O13 131.2(4) 4_565 4_565 ?
O1 Rb2A O17 122.6(3) 4_565 . ?
O2 Rb2A U4A 100.2(2) . 4_565 ?
O2 Rb2A Rb3B 46.5(5) . 4_565 ?
O2 Rb2A Rb5 130.3(2) . 3_666 ?
O2 Rb2A F4 131.9(3) . 4_565 ?
O2 Rb2A O1 117.0(3) . 4_565 ?
O2 Rb2A O5 171.4(3) . 4_565 ?
O2 Rb2A O13 85.8(3) . 4_565 ?
O2 Rb2A O17 50.5(3) . . ?
O5 Rb2A U4A 85.0(2) 4_565 4_565 ?
O5 Rb2A Rb3B 131.7(6) 4_565 4_565 ?
O5 Rb2A Rb5 50.2(2) 4_565 3_666 ?
O5 Rb2A F4 54.7(3) 4_565 4_565 ?
O5 Rb2A O1 71.1(3) 4_565 4_565 ?
O5 Rb2A O13 90.7(4) 4_565 4_565 ?
O5 Rb2A O17 123.4(3) 4_565 . ?
O9 Rb2A U4A 135.5(2) 4_665 4_565 ?
O9 Rb2A Rb3B 122.5(5) 4_665 4_565 ?
O9 Rb2A Rb5 54.9(2) 4_665 3_666 ?
O9 Rb2A F4 124.0(3) 4_665 4_565 ?
O9 Rb2A O1 71.1(3) 4_665 4_565 ?
O9 Rb2A O2 76.0(3) 4_665 . ?
O9 Rb2A O5 105.1(3) 4_665 4_565 ?
O9 Rb2A O13 156.8(4) 4_665 4_565 ?
O9 Rb2A O17 51.7(3) 4_665 . ?
O13 Rb2A U4A 61.5(3) 4_565 4_565 ?
O13 Rb2A Rb3B 41.5(6) 4_565 4_565 ?
O13 Rb2A O17 105.4(3) 4_565 . ?
O15 Rb2A U4A 24.1(3) 4_565 4_565 ?
O15 Rb2A Rb3B 49.6(4) 4_565 4_565 ?
O15 Rb2A Rb5 137.7(3) 4_565 3_666 ?
O15 Rb2A F4 56.5(3) 4_565 4_565 ?
O15 Rb2A O1 81.9(3) 4_565 4_565 ?
O15 Rb2A O2 76.2(3) 4_565 . ?
O15 Rb2A O5 109.1(3) 4_565 4_565 ?
O15 Rb2A O9 125.8(3) 4_565 4_665 ?
O15 Rb2A O13 61.4(4) 4_565 4_565 ?
O15 Rb2A O16 122.2(4) 4_565 . ?
O15 Rb2A O17 126.5(3) 4_565 . ?
O16 Rb2A U4A 126.0(3) . 4_565 ?
O16 Rb2A Rb3B 76.4(5) . 4_565 ?
O16 Rb2A Rb5 97.0(3) . 3_666 ?
O16 Rb2A F4 129.8(3) . 4_565 ?
O16 Rb2A O1 154.3(3) . 4_565 ?
O16 Rb2A O2 80.6(3) . . ?
O16 Rb2A O5 90.8(3) . 4_565 ?
O16 Rb2A O9 97.6(3) . 4_665 ?
O16 Rb2A O13 64.8(4) . 4_565 ?
O16 Rb2A O17 52.8(3) . . ?
O17 Rb2A U4A 150.2(2) . 4_565 ?
O17 Rb2A Rb3B 85.0(3) . 4_565 ?
Rb3B Rb3A Rb3B 43(2) . 3_667 ?
Rb3B Rb3A Rb4A 72.9(5) 3_667 3_667 ?
Rb3B Rb3A Rb4A 116(2) . 3_667 ?
Rb3B Rb3A Rb5 152(2) . . ?
Rb3B Rb3A O1 137(3) . 2_656 ?
Rb3B Rb3A O2 97.7(15) . 4_666 ?
Rb3B Rb3A O3 84(2) . 4_666 ?
Rb3B Rb3A O6 30(2) . 4_666 ?
Rb3B Rb3A O6 79.5(15) . 2_556 ?
Rb3B Rb3A O9 144.6(15) . 2_556 ?
Rb3B Rb3A O13 38(2) . . ?
Rb3B Rb3A O15 104(2) . . ?
Rb5 Rb3A Rb3B 160.7(7) . 3_667 ?
Rb5 Rb3A Rb4A 91.3(5) . 3_667 ?
Rb5 Rb3A O3 99.3(4) . 4_666 ?
Rb5 Rb3A O6 151.0(3) . 4_666 ?
Rb5 Rb3A O9 52.4(4) . 2_556 ?
Rb5 Rb3A O13 119.9(4) . . ?
O1 Rb3A Rb3B 113.1(5) 2_656 3_667 ?
O1 Rb3A Rb4A 55.5(3) 2_656 3_667 ?
O1 Rb3A Rb5 63.4(5) 2_656 . ?
O1 Rb3A O3 58.5(3) 2_656 4_666 ?
O1 Rb3A O6 107.7(4) 2_656 4_666 ?
O1 Rb3A O9 65.2(5) 2_656 2_556 ?
O1 Rb3A O13 174.5(7) 2_656 . ?
O2 Rb3A Rb3B 136.3(10) 4_666 3_667 ?
O2 Rb3A Rb4A 136.9(6) 4_666 3_667 ?
O2 Rb3A Rb5 63.0(4) 4_666 . ?
O2 Rb3A O1 81.6(4) 4_666 2_656 ?
O2 Rb3A O3 57.9(3) 4_666 4_666 ?
O2 Rb3A O6 88.9(5) 4_666 4_666 ?
O2 Rb3A O6 167.9(4) 4_666 2_556 ?
O2 Rb3A O9 115.0(7) 4_666 2_556 ?
O2 Rb3A O13 96.0(5) 4_666 . ?
O2 Rb3A O15 80.1(4) 4_666 . ?
O3 Rb3A Rb3B 93.7(4) 4_666 3_667 ?
O3 Rb3A Rb4A 97.2(3) 4_666 3_667 ?
O3 Rb3A O9 123.7(5) 4_666 2_556 ?
O6 Rb3A Rb3B 47.8(6) 4_666 3_667 ?
O6 Rb3A Rb3B 46.4(3) 2_556 3_667 ?
O6 Rb3A Rb4A 53.1(3) 2_556 3_667 ?
O6 Rb3A Rb4A 106.3(4) 4_666 3_667 ?
O6 Rb3A Rb5 115.0(6) 2_556 . ?
O6 Rb3A O1 108.6(4) 2_556 2_656 ?
O6 Rb3A O3 56.4(4) 4_666 4_666 ?
O6 Rb3A O3 132.8(5) 2_556 4_666 ?
O6 Rb3A O6 94.0(6) 2_556 4_666 ?
O6 Rb3A O9 65.7(4) 2_556 2_556 ?
O6 Rb3A O9 152.4(3) 4_666 2_556 ?
O6 Rb3A O13 74.4(5) 2_556 . ?
O6 Rb3A O13 67.2(6) 4_666 . ?
O6 Rb3A O15 89.1(4) 2_556 . ?
O9 Rb3A Rb3B 108.3(5) 2_556 3_667 ?
O9 Rb3A Rb4A 46.8(3) 2_556 3_667 ?
O13 Rb3A Rb3B 65.4(10) . 3_667 ?
O13 Rb3A Rb4A 127.1(5) . 3_667 ?
O13 Rb3A O3 116.1(7) . 4_666 ?
O13 Rb3A O9 120.3(4) . 2_556 ?
O15 Rb3A Rb3B 120.7(7) . 3_667 ?
O15 Rb3A Rb4A 114.7(6) . 3_667 ?
O15 Rb3A Rb5 55.6(4) . . ?
O15 Rb3A O1 118.1(8) . 2_656 ?
O15 Rb3A O3 138.0(4) . 4_666 ?
O15 Rb3A O6 130.3(6) . 4_666 ?
O15 Rb3A O9 70.6(5) . 2_556 ?
O15 Rb3A O13 66.0(5) . . ?
Rb3A Rb3B Rb3A 137(2) . 3_667 ?
Rb3A Rb3B Rb3B 130(3) . 3_667 ?
Rb3A Rb3B Rb5 23.1(17) . . ?
Rb3A Rb3B O1 36(2) . 2_656 ?
Rb3A Rb3B O2 70.7(14) . 4_666 ?
Rb3A Rb3B O3 85(3) . 4_666 ?
Rb3A Rb3B O6 144(3) . 4_666 ?
Rb3A Rb3B O6 88.3(17) . 2_556 ?
Rb3A Rb3B O13 51.3(3) 3_667 3_667 ?
Rb3A Rb3B O13 134(2) . . ?
Rb3A Rb3B O13 93(3) . 3_667 ?
Rb3A Rb3B O15 65.2(18) . . ?
Rb3B Rb3B Rb3A 7.3(7) 3_667 3_667 ?
Rb3B Rb3B Rb5 150.5(16) 3_667 . ?
Rb3B Rb3B O1 112.2(15) 3_667 2_656 ?
Rb3B Rb3B O3 102.1(6) 3_667 4_666 ?
Rb3B Rb3B O13 45.9(8) 3_667 3_667 ?
Rb5 Rb3B Rb3A 157.4(10) . 3_667 ?
Rb5 Rb3B O13 115.5(12) . 3_667 ?
O1 Rb3B Rb3A 117.9(7) 2_656 3_667 ?
O1 Rb3B Rb5 53.4(7) 2_656 . ?
O1 Rb3B O13 66.6(7) 2_656 3_667 ?
O2 Rb3B Rb3A 146.9(11) 4_666 3_667 ?
O2 Rb3B Rb3B 152.1(12) 4_666 3_667 ?
O2 Rb3B Rb5 55.0(6) 4_666 . ?
O2 Rb3B O1 72.2(9) 4_666 2_656 ?
O2 Rb3B O3 56.7(4) 4_666 4_666 ?
O2 Rb3B O13 126.9(10) 4_666 3_667 ?
O2 Rb3B O15 74.8(5) 4_666 . ?
O3 Rb3B Rb3A 101.6(5) 4_666 3_667 ?
O3 Rb3B Rb5 89.0(9) 4_666 . ?
O3 Rb3B O1 54.3(6) 4_666 2_656 ?
O3 Rb3B O13 72.3(5) 4_666 3_667 ?
O6 Rb3B Rb3A 50.7(7) 4_666 3_667 ?
O6 Rb3B Rb3A 57.1(3) 2_556 3_667 ?
O6 Rb3B Rb3B 55.6(9) 4_666 3_667 ?
O6 Rb3B Rb3B 51.8(4) 2_556 3_667 ?
O6 Rb3B Rb5 101.4(9) 2_556 . ?
O6 Rb3B Rb5 148.1(8) 4_666 . ?
O6 Rb3B O1 98.0(11) 2_556 2_656 ?
O6 Rb3B O1 108.2(8) 4_666 2_656 ?
O6 Rb3B O2 156.0(13) 2_556 4_666 ?
O6 Rb3B O2 96.5(6) 4_666 4_666 ?
O6 Rb3B O3 135.0(10) 2_556 4_666 ?
O6 Rb3B O3 60.8(4) 4_666 4_666 ?
O6 Rb3B O6 107.5(9) 4_666 2_556 ?
O6 Rb3B O13 81.2(13) 4_666 . ?
O6 Rb3B O13 63.6(5) 2_556 3_667 ?
O6 Rb3B O13 67.7(5) 4_666 3_667 ?
O6 Rb3B O15 145.6(16) 4_666 . ?
O6 Rb3B O15 86.1(5) 2_556 . ?
O13 Rb3B Rb3A 71.2(10) . 3_667 ?
O13 Rb3B Rb3B 76.4(17) . 3_667 ?
O13 Rb3B Rb5 116.3(6) . . ?
O13 Rb3B O1 169.7(9) . 2_656 ?
O13 Rb3B O2 103.2(10) . 4_666 ?
O13 Rb3B O3 131.3(12) . 4_666 ?
O13 Rb3B O6 82.7(9) . 2_556 ?
O13 Rb3B O13 122.2(10) . 3_667 ?
O13 Rb3B O15 69.0(7) . . ?
O15 Rb3B Rb3A 128.2(8) . 3_667 ?
O15 Rb3B Rb3B 128.3(11) . 3_667 ?
O15 Rb3B Rb5 48.4(5) . . ?
O15 Rb3B O1 100.7(11) . 2_656 ?
O15 Rb3B O3 129.5(8) . 4_666 ?
O15 Rb3B O13 143.6(10) . 3_667 ?
Rb3A Rb4A Rb5 134.4(4) 3_667 4_566 ?
Rb3A Rb4A P1 111.3(4) 3_667 4_666 ?
P1 Rb4A Rb3A 72.3(3) . 3_667 ?
P1 Rb4A Rb5 102.0(3) . 4_566 ?
P1 Rb4A Rb5 92.7(3) 4_666 4_566 ?
P1 Rb4A P1 154.7(3) . 4_666 ?
O1 Rb4A Rb3A 47.4(3) 4_566 3_667 ?
O1 Rb4A Rb5 87.9(3) 4_566 4_566 ?
O1 Rb4A P1 134.3(4) 4_566 4_666 ?
O1 Rb4A P1 67.5(3) 4_566 . ?
O1 Rb4A O7 123.3(5) 4_566 4_666 ?
O1 Rb4A O14 153.6(5) 4_566 4_666 ?
O6 Rb4A Rb3A 45.8(3) 4_666 3_667 ?
O6 Rb4A Rb5 167.6(5) 4_666 4_566 ?
O6 Rb4A P1 89.8(4) 4_666 . ?
O6 Rb4A P1 77.7(4) 4_666 4_666 ?
O6 Rb4A O1 93.2(5) 4_666 4_566 ?
O6 Rb4A O7 54.5(4) 4_666 4_666 ?
O6 Rb4A O14 90.9(5) 4_666 4_666 ?
O7 Rb4A Rb3A 89.1(4) 4_666 3_667 ?
O7 Rb4A Rb5 115.0(4) 4_666 4_566 ?
O7 Rb4A P1 23.6(2) 4_666 4_666 ?
O7 Rb4A P1 141.0(4) 4_666 . ?
O9 Rb4A Rb3A 61.1(4) 4_666 3_667 ?
O9 Rb4A Rb5 98.8(4) 4_666 4_566 ?
O9 Rb4A P1 130.4(6) 4_666 . ?
O9 Rb4A P1 65.9(4) 4_666 4_666 ?
O9 Rb4A O1 68.8(4) 4_666 4_566 ?
O9 Rb4A O6 70.2(4) 4_666 4_666 ?
O9 Rb4A O7 57.3(4) 4_666 4_666 ?
O9 Rb4A O10 132.4(5) 4_666 . ?
O9 Rb4A O14 88.3(5) 4_666 4_666 ?
O9 Rb4A O16 133.0(6) 4_666 4_666 ?
O10 Rb4A Rb3A 119.6(5) . 3_667 ?
O10 Rb4A Rb5 43.4(3) . 4_566 ?
O10 Rb4A P1 128.0(5) . 4_666 ?
O10 Rb4A P1 59.5(3) . . ?
O10 Rb4A O1 80.2(4) . 4_566 ?
O10 Rb4A O6 148.9(6) . 4_666 ?
O10 Rb4A O7 151.2(6) . 4_666 ?
O10 Rb4A O14 108.5(5) . 4_666 ?
O10 Rb4A O16 90.8(5) . 4_666 ?
O13 Rb4A Rb3A 65.8(6) . 3_667 ?
O13 Rb4A Rb5 121.3(6) . 4_566 ?
O13 Rb4A P1 136.1(5) . 4_666 ?
O13 Rb4A P1 20.8(4) . . ?
O13 Rb4A O1 78.4(6) . 4_566 ?
O13 Rb4A O6 71.0(5) . 4_666 ?
O13 Rb4A O7 120.2(5) . 4_666 ?
O13 Rb4A O9 126.7(7) . 4_666 ?
O13 Rb4A O10 77.9(5) . . ?
O13 Rb4A O14 127.3(6) . 4_666 ?
O13 Rb4A O16 71.8(5) . 4_666 ?
O14 Rb4A Rb3A 131.9(5) 4_666 3_667 ?
O14 Rb4A Rb5 82.7(4) 4_666 4_566 ?
O14 Rb4A P1 138.6(4) 4_666 . ?
O14 Rb4A P1 23.2(2) 4_666 4_666 ?
O14 Rb4A O7 43.0(3) 4_666 4_666 ?
O16 Rb4A Rb3A 118.6(5) 4_666 3_667 ?
O16 Rb4A Rb5 105.0(5) 4_666 4_566 ?
O16 Rb4A P1 73.0(4) 4_666 4_666 ?
O16 Rb4A P1 83.3(4) 4_666 . ?
O16 Rb4A O1 150.1(6) 4_666 4_566 ?
O16 Rb4A O6 79.9(4) 4_666 4_666 ?
O16 Rb4A O7 75.9(5) 4_666 4_666 ?
O16 Rb4A O14 56.2(4) 4_666 4_666 ?
Rb5 Rb4B Rb1 66.4(13) 4_566 2_546 ?
Rb5 Rb4B P1 99(2) 4_566 4_666 ?
Rb5 Rb4B O5 43.1(12) 4_566 3_657 ?
P1 Rb4B Rb1 99.0(11) 4_666 2_546 ?
O1 Rb4B Rb1 125.5(8) 4_566 2_546 ?
O1 Rb4B Rb5 92.3(16) 4_566 4_566 ?
O1 Rb4B P1 134.8(9) 4_566 4_666 ?
O1 Rb4B O5 135(3) 4_566 3_657 ?
O1 Rb4B O6 87(2) 4_566 4_666 ?
O1 Rb4B O7 119.7(15) 4_566 4_666 ?
O5 Rb4B Rb1 43.2(7) 3_657 2_546 ?
O5 Rb4B P1 71.8(13) 3_657 4_666 ?
O6 Rb4B Rb1 121(2) 4_666 2_546 ?
O6 Rb4B Rb5 171.8(17) 4_666 4_566 ?
O6 Rb4B P1 75.8(9) 4_666 4_666 ?
O6 Rb4B O5 138.3(10) 4_666 3_657 ?
O6 Rb4B O7 52.1(10) 4_666 4_666 ?
O7 Rb4B Rb1 113.8(8) 4_666 2_546 ?
O7 Rb4B Rb5 122(3) 4_666 4_566 ?
O7 Rb4B P1 24.2(3) 4_666 4_666 ?
O7 Rb4B O5 95.1(14) 4_666 3_657 ?
O9 Rb4B Rb1 164(3) 4_666 2_546 ?
O9 Rb4B Rb5 106(3) 4_666 4_566 ?
O9 Rb4B P1 67.3(7) 4_666 4_666 ?
O9 Rb4B O1 67.6(8) 4_666 4_566 ?
O9 Rb4B O5 121(3) 4_666 3_657 ?
O9 Rb4B O6 66.0(15) 4_666 4_666 ?
O9 Rb4B O7 56.8(6) 4_666 4_666 ?
O9 Rb4B O13 117(3) 4_666 . ?
O9 Rb4B O14 90.7(10) 4_666 4_666 ?
O9 Rb4B O16 129(2) 4_666 4_666 ?
O10 Rb4B Rb1 47.1(6) . 2_546 ?
O10 Rb4B Rb5 47.8(15) . 4_566 ?
O10 Rb4B P1 137(3) . 4_666 ?
O10 Rb4B O1 80.8(8) . 4_566 ?
O10 Rb4B O5 65.4(17) . 3_657 ?
O10 Rb4B O6 140(3) . 4_666 ?
O10 Rb4B O7 159(2) . 4_666 ?
O10 Rb4B O9 139(2) . 4_666 ?
O10 Rb4B O13 75.8(12) . . ?
O10 Rb4B O14 116(2) . 4_666 ?
O10 Rb4B O16 91.9(9) . 4_666 ?
O13 Rb4B Rb1 78.3(9) . 2_546 ?
O13 Rb4B Rb5 123.5(10) . 4_566 ?
O13 Rb4B P1 129(2) . 4_666 ?
O13 Rb4B O1 73.6(17) . 4_566 ?
O13 Rb4B O5 121.4(9) . 3_657 ?
O13 Rb4B O6 64(2) . 4_666 ?
O13 Rb4B O7 112(3) . 4_666 ?
O13 Rb4B O14 123(2) . 4_666 ?
O13 Rb4B O16 67.2(18) . 4_666 ?
O14 Rb4B Rb1 75.2(9) 4_666 2_546 ?
O14 Rb4B Rb5 90(2) 4_666 4_566 ?
O14 Rb4B P1 23.7(3) 4_666 4_666 ?
O14 Rb4B O1 157.9(13) 4_666 4_566 ?
O14 Rb4B O5 52.8(12) 4_666 3_657 ?
O14 Rb4B O6 88.2(13) 4_666 4_666 ?
O14 Rb4B O7 43.3(5) 4_666 4_666 ?
O16 Rb4B Rb1 48.6(5) 4_666 2_546 ?
O16 Rb4B Rb5 111.2(19) 4_666 4_566 ?
O16 Rb4B P1 73.6(6) 4_666 4_666 ?
O16 Rb4B O1 141(3) 4_666 4_566 ?
O16 Rb4B O5 72.0(11) 4_666 3_657 ?
O16 Rb4B O6 74(2) 4_666 4_666 ?
O16 Rb4B O7 74.4(10) 4_666 4_666 ?
O16 Rb4B O14 57.0(6) 4_666 4_666 ?
Rb2A Rb5 Rb3B 112.1(6) 3_666 . ?
Rb2A Rb5 Rb4B 122.5(5) 3_666 4_665 ?
Rb2A Rb5 O11 90.1(3) 3_666 2_556 ?
Rb2A Rb5 O11 74.4(3) 3_666 4_665 ?
Rb3A Rb5 Rb2A 107.6(2) . 3_666 ?
Rb3A Rb5 Rb3B 4.5(4) . . ?
Rb3A Rb5 Rb4B 123.0(7) . 4_665 ?
Rb3A Rb5 O1 58.1(2) . 2_656 ?
Rb3A Rb5 O2 56.1(3) . 4_666 ?
Rb3A Rb5 O11 103.4(4) . 2_556 ?
Rb3A Rb5 O11 118.6(4) . 4_665 ?
Rb3B Rb5 Rb4B 118.8(8) . 4_665 ?
Rb3B Rb5 O11 103.4(4) . 2_556 ?
Rb3B Rb5 O11 119.6(4) . 4_665 ?
O1 Rb5 Rb2A 57.6(2) 2_656 3_666 ?
O1 Rb5 Rb3B 61.8(6) 2_656 . ?
O1 Rb5 Rb4B 130.5(8) 2_656 4_665 ?
O1 Rb5 O11 126.7(5) 2_656 2_556 ?
O1 Rb5 O11 122.3(4) 2_656 4_665 ?
O2 Rb5 Rb2A 128.3(3) 4_666 3_666 ?
O2 Rb5 Rb3B 53.2(4) 4_666 . ?
O2 Rb5 Rb4B 71.3(8) 4_666 4_665 ?
O2 Rb5 O1 75.8(3) 4_666 2_656 ?
O2 Rb5 O11 139.0(4) 4_666 2_556 ?
O2 Rb5 O11 157.0(4) 4_666 4_665 ?
O5 Rb5 Rb2A 59.6(3) 2_656 3_666 ?
O5 Rb5 Rb3A 126.6(3) 2_656 . ?
O5 Rb5 Rb3B 128.0(5) 2_656 . ?
O5 Rb5 Rb4B 68.5(6) 2_656 4_665 ?
O5 Rb5 O1 75.6(3) 2_656 2_656 ?
O5 Rb5 O2 90.0(4) 2_656 4_666 ?
O5 Rb5 O9 116.6(4) 2_656 2_556 ?
O5 Rb5 O10 82.5(4) 2_656 4_665 ?
O5 Rb5 O11 126.3(4) 2_656 2_556 ?
O5 Rb5 O11 107.5(4) 2_656 4_665 ?
O5 Rb5 O15 158.9(4) 2_656 . ?
O9 Rb5 Rb2A 57.0(3) 2_556 3_666 ?
O9 Rb5 Rb3A 74.8(3) 2_556 . ?
O9 Rb5 Rb3B 78.2(4) 2_556 . ?
O9 Rb5 Rb4B 155.5(9) 2_556 4_665 ?
O9 Rb5 O1 72.0(3) 2_556 2_656 ?
O9 Rb5 O2 130.3(3) 2_556 4_666 ?
O9 Rb5 O11 54.8(4) 2_556 4_665 ?
O9 Rb5 O11 54.7(4) 2_556 2_556 ?
O10 Rb5 Rb2A 98.1(3) 4_665 3_666 ?
O10 Rb5 Rb3A 148.2(3) 4_665 . ?
O10 Rb5 Rb3B 144.8(6) 4_665 . ?
O10 Rb5 Rb4B 50.3(8) 4_665 4_665 ?
O10 Rb5 O1 153.3(4) 4_665 2_656 ?
O10 Rb5 O2 119.8(4) 4_665 4_666 ?
O10 Rb5 O9 105.4(4) 4_665 2_556 ?
O10 Rb5 O11 57.2(5) 4_665 2_556 ?
O10 Rb5 O11 50.7(5) 4_665 4_665 ?
O11 Rb5 Rb4B 102.1(9) 2_556 4_665 ?
O11 Rb5 Rb4B 100.7(9) 4_665 4_665 ?
O11 Rb5 O11 19.4(6) 4_665 2_556 ?
O15 Rb5 Rb2A 140.5(4) . 3_666 ?
O15 Rb5 Rb3A 61.2(3) . . ?
O15 Rb5 Rb3B 58.1(5) . . ?
O15 Rb5 Rb4B 90.8(6) . 4_665 ?
O15 Rb5 O1 118.4(4) . 2_656 ?
O15 Rb5 O2 79.3(4) . 4_666 ?
O15 Rb5 O9 83.8(4) . 2_556 ?
O15 Rb5 O10 87.1(4) . 4_665 ?
O15 Rb5 O11 79.2(5) . 4_665 ?
O15 Rb5 O11 60.0(4) . 2_556 ?
U2 P1 U4A 128.41(15) . . ?
U2 P1 Rb2A 110.72(11) . 4_666 ?
U2 P1 Rb3B 149.5(5) . . ?
U2 P1 Rb4A 72.5(2) . 4_565 ?
U2 P1 Rb4A 79.1(2) . . ?
U2 P1 Rb4B 75.0(13) . . ?
U2 P1 Rb4B 73.4(5) . 4_565 ?
U4A P1 Rb2A 65.41(10) . 4_666 ?
U4A P1 Rb3B 77.0(5) . . ?
U4A P1 Rb4A 140.9(2) . . ?
U4A P1 Rb4A 67.5(2) . 4_565 ?
U4A P1 Rb4B 69.4(9) . 4_565 ?
U4A P1 Rb4B 143.6(10) . . ?
Rb3B P1 Rb2A 60.5(2) . 4_666 ?
Rb3B P1 Rb4A 138.0(5) . 4_565 ?
Rb3B P1 Rb4B 74.7(14) . . ?
Rb4A P1 Rb2A 79.7(2) . 4_666 ?
Rb4A P1 Rb2A 118.66(19) 4_565 4_666 ?
Rb4A P1 Rb3B 70.6(5) . . ?
Rb4A P1 Rb4A 150.2(3) . 4_565 ?
Rb4A P1 Rb4B 4.2(13) . . ?
Rb4A P1 Rb4B 146.4(13) 4_565 . ?
Rb4A P1 Rb4B 149.2(8) . 4_565 ?
Rb4B P1 Rb2A 123.1(16) 4_565 4_666 ?
Rb4B P1 Rb2A 80.8(6) . 4_666 ?
Rb4B P1 Rb3B 136.8(7) 4_565 . ?
Rb4B P1 Rb4A 4.9(16) 4_565 4_565 ?
Rb4B P1 Rb4B 145.7(18) 4_565 . ?
O7 P1 U2 54.8(5) . . ?
O7 P1 U4A 79.3(5) . . ?
O7 P1 Rb2A 69.1(6) . 4_666 ?
O7 P1 Rb3B 129.4(6) . . ?
O7 P1 Rb4A 105.0(6) . . ?
O7 P1 Rb4A 65.5(6) . 4_565 ?
O7 P1 Rb4B 70.0(17) . 4_565 ?
O7 P1 Rb4B 101.7(11) . . ?
O12 P1 U2 48.0(4) . . ?
O12 P1 U4A 141.2(5) . . ?
O12 P1 Rb2A 151.2(5) . 4_666 ?
O12 P1 Rb3B 125.3(6) . . ?
O12 P1 Rb4A 77.2(5) . . ?
O12 P1 Rb4A 77.2(5) . 4_565 ?
O12 P1 Rb4B 74.1(13) . 4_565 ?
O12 P1 Rb4B 75.0(10) . . ?
O12 P1 O7 100.7(7) . . ?
O12 P1 O14 105.4(6) . . ?
O13 P1 U2 118.5(6) . . ?
O13 P1 U4A 101.2(7) . . ?
O13 P1 Rb2A 55.4(8) . 4_666 ?
O13 P1 Rb3B 31.2(8) . . ?
O13 P1 Rb4A 168.3(7) . 4_565 ?
O13 P1 Rb4A 41.5(7) . . ?
O13 P1 Rb4B 45.3(14) . . ?
O13 P1 Rb4B 168.0(8) . 4_565 ?
O13 P1 O7 116.5(10) . . ?
O13 P1 O12 112.8(9) . . ?
O13 P1 O14 112.2(8) . . ?
O14 P1 U2 128.7(5) . . ?
O14 P1 U4A 41.5(4) . . ?
O14 P1 Rb2A 103.4(4) . 4_666 ?
O14 P1 Rb3B 81.0(6) . . ?
O14 P1 Rb4A 145.5(5) . . ?
O14 P1 Rb4A 57.7(5) . 4_565 ?
O14 P1 Rb4B 149.3(13) . . ?
O14 P1 Rb4B 55.9(8) . 4_565 ?
O14 P1 O7 108.2(7) . . ?
U1 F4 U4B 103.5(4) . . ?
U1 F4 Rb2A 97.3(3) . 4_666 ?
U3 F4 U1 108.5(4) . . ?
U3 F4 U4B 146.6(5) . . ?
U3 F4 Rb2A 93.2(3) . 4_666 ?
U4A F4 U1 110.7(4) . . ?
U4A F4 U3 139.8(5) . . ?
U4A F4 U4B 7.23(15) . . ?
U4A F4 Rb2A 90.3(3) . 4_666 ?
U4B F4 Rb2A 92.0(3) . 4_666 ?
U1 O1 Rb2A 123.2(5) . 4_666 ?
U1 O1 Rb3A 117.4(5) . 2_646 ?
U1 O1 Rb3B 111.7(5) . 2_646 ?
U1 O1 Rb4A 129.2(5) . 4_665 ?
U1 O1 Rb4B 129.1(7) . 4_665 ?
U1 O1 Rb5 128.5(5) . 2_646 ?
Rb2A O1 Rb3B 120.9(5) 4_666 2_646 ?
Rb2A O1 Rb4A 83.8(3) 4_666 4_665 ?
Rb2A O1 Rb4B 79.1(16) 4_666 4_665 ?
Rb3A O1 Rb2A 114.1(5) 2_646 4_666 ?
Rb3A O1 Rb3B 6.9(2) 2_646 2_646 ?
Rb3A O1 Rb4A 77.1(4) 2_646 4_665 ?
Rb3A O1 Rb4B 82.3(17) 2_646 4_665 ?
Rb3A O1 Rb5 58.5(4) 2_646 2_646 ?
Rb4A O1 Rb3B 77.4(4) 4_665 2_646 ?
Rb4A O1 Rb4B 5.9(18) 4_665 4_665 ?
Rb4B O1 Rb3B 82.9(18) 4_665 2_646 ?
Rb5 O1 Rb2A 64.9(2) 2_646 4_666 ?
Rb5 O1 Rb3B 64.8(4) 2_646 2_646 ?
Rb5 O1 Rb4A 101.2(4) 2_646 4_665 ?
Rb5 O1 Rb4B 102.1(6) 2_646 4_665 ?
U1 O2 Rb2A 130.8(5) . . ?
U1 O2 Rb3A 120.7(5) . 4_565 ?
U1 O2 Rb3B 116.6(5) . 4_565 ?
U1 O2 Rb5 135.7(5) . 4_565 ?
Rb3A O2 Rb2A 90.0(3) 4_565 . ?
Rb3A O2 Rb3B 11.6(4) 4_565 4_565 ?
Rb3A O2 Rb5 60.9(5) 4_565 4_565 ?
Rb3B O2 Rb2A 85.5(7) 4_565 . ?
Rb3B O2 Rb5 71.8(7) 4_565 4_565 ?
Rb5 O2 Rb2A 91.7(3) 4_565 . ?
U1 O3 U1 104.0(4) . 3_656 ?
U1 O3 U3 108.1(4) . . ?
U1 O3 Rb3A 93.5(5) 3_656 4_565 ?
U1 O3 Rb3A 92.5(4) . 4_565 ?
U1 O3 Rb3B 94.0(4) . 4_565 ?
U1 O3 Rb3B 103.3(9) 3_656 4_565 ?
U3 O3 U1 145.4(5) . 3_656 ?
U3 O3 Rb3A 97.8(5) . 4_565 ?
U3 O3 Rb3B 87.3(8) . 4_565 ?
Rb3B O3 Rb3A 10.6(4) 4_565 4_565 ?
U3 O5 Rb1 119.5(5) . 2_546 ?
U3 O5 Rb2A 115.3(5) . 4_666 ?
U3 O5 Rb4B 112.8(7) . 3_657 ?
U3 O5 Rb5 141.0(6) . 2_646 ?
Rb1 O5 Rb2A 88.8(3) 2_546 4_666 ?
Rb1 O5 Rb4B 73.8(10) 2_546 3_657 ?
Rb2A O5 Rb4B 131.4(7) 4_666 3_657 ?
Rb5 O5 Rb1 98.6(4) 2_646 2_546 ?
Rb5 O5 Rb2A 70.2(3) 2_646 4_666 ?
Rb5 O5 Rb4B 68.3(11) 2_646 3_657 ?
U3 O6 Rb3A 136.9(6) . 2_546 ?
U3 O6 Rb3A 114.1(5) . 4_565 ?
U3 O6 Rb3B 136.7(8) . 2_546 ?
U3 O6 Rb3B 120.1(9) . 4_565 ?
U3 O6 Rb4A 123.7(6) . 4_565 ?
U3 O6 Rb4B 120.8(11) . 4_565 ?
Rb3A O6 Rb3A 86.0(6) 2_546 4_565 ?
Rb3A O6 Rb4A 81.1(5) 2_546 4_565 ?
Rb3A O6 Rb4A 106.6(4) 4_565 4_565 ?
Rb3A O6 Rb4B 109.4(11) 4_565 4_565 ?
Rb3A O6 Rb4B 82.5(7) 2_546 4_565 ?
Rb3B O6 Rb3A 75.1(8) 2_546 4_565 ?
Rb3B O6 Rb3A 82.9(8) 4_565 2_546 ?
Rb3B O6 Rb3A 6.4(7) 4_565 4_565 ?
Rb3B O6 Rb3A 12.2(5) 2_546 2_546 ?
Rb3B O6 Rb3B 72.5(9) 4_565 2_546 ?
Rb3B O6 Rb4A 100.5(9) 4_565 4_565 ?
Rb3B O6 Rb4A 89.5(10) 2_546 4_565 ?
Rb3B O6 Rb4B 91.4(12) 2_546 4_565 ?
Rb3B O6 Rb4B 103.4(14) 4_565 4_565 ?
Rb4A O6 Rb4B 3.1(11) 4_565 4_565 ?
U2 O7 Rb4A 85.2(5) . 4_565 ?
U2 O7 Rb4B 83.9(8) . 4_565 ?
U3 O7 U2 102.9(5) . . ?
U3 O7 Rb4A 90.1(5) . 4_565 ?
U3 O7 Rb4B 95.5(19) . 4_565 ?
Rb4A O7 Rb4B 5.4(17) 4_565 4_565 ?
P1 O7 U2 95.8(6) . . ?
P1 O7 U3 161.3(8) . . ?
P1 O7 Rb4A 90.9(6) . 4_565 ?
P1 O7 Rb4B 85.8(17) . 4_565 ?
U2 O8 U3 119.5(5) . . ?
U2 O8 U4A 122.3(6) . 2_546 ?
U2 O8 Rb1 95.3(4) . 2_546 ?
U3 O8 Rb1 90.1(5) . 2_546 ?
U4A O8 U3 115.7(5) 2_546 . ?
U4A O8 Rb1 100.0(4) 2_546 2_546 ?
U4B O8 U2 113.6(6) 2_546 . ?
U4B O8 U3 124.7(5) 2_546 . ?
U4B O8 U4A 9.03(13) 2_546 2_546 ?
U4B O8 Rb1 99.6(4) 2_546 2_546 ?
U2 O9 Rb2A 123.8(5) . 4_566 ?
U2 O9 Rb3A 129.0(5) . 2_546 ?
U2 O9 Rb4A 125.2(6) . 4_565 ?
U2 O9 Rb4B 123.8(9) . 4_565 ?
U2 O9 Rb5 118.6(5) . 2_546 ?
Rb2A O9 Rb3A 100.3(4) 4_566 2_546 ?
Rb4A O9 Rb2A 91.0(4) 4_565 4_566 ?
Rb4A O9 Rb3A 72.1(4) 4_565 2_546 ?
Rb4A O9 Rb4B 7(2) 4_565 4_565 ?
Rb4B O9 Rb2A 87.0(15) 4_565 4_566 ?
Rb4B O9 Rb3A 78(2) 4_565 2_546 ?
Rb5 O9 Rb2A 68.0(3) 2_546 4_566 ?
Rb5 O9 Rb3A 52.8(3) 2_546 2_546 ?
Rb5 O9 Rb4A 113.1(5) 2_546 4_565 ?
Rb5 O9 Rb4B 116.3(12) 2_546 4_565 ?
U2 O10 Rb1 117.9(5) . 2_546 ?
U2 O10 Rb4A 133.9(6) . . ?
U2 O10 Rb4B 139.0(18) . . ?
U2 O10 Rb5 123.6(6) . 4_566 ?
Rb1 O10 Rb4A 87.2(4) 2_546 . ?
Rb4B O10 Rb1 86.8(7) . 2_546 ?
Rb4B O10 Rb4A 6(2) . . ?
Rb5 O10 Rb1 95.5(4) 4_566 2_546 ?
Rb5 O10 Rb4A 88.0(4) 4_566 . ?
Rb5 O10 Rb4B 82(2) 4_566 . ?
U2 O11 U2 149.7(9) . 3_557 ?
U2 O11 U4A 103.7(7) 3_557 2_546 ?
U2 O11 U4A 104.8(8) . 2_546 ?
U2 O11 U4B 104.4(8) 3_557 2_546 ?
U2 O11 U4B 104.2(8) . 2_546 ?
U2 O11 Rb5 88.4(7) . 4_566 ?
U2 O11 Rb5 85.0(6) 3_557 2_546 ?
U2 O11 Rb5 89.4(6) . 2_546 ?
U2 O11 Rb5 87.2(6) 3_557 4_566 ?
U4A O11 Rb5 81.1(5) 2_546 2_546 ?
U4A O11 Rb5 118.1(6) 2_546 4_566 ?
U4B O11 U4A 1.09(19) 2_546 2_546 ?
U4B O11 Rb5 82.0(5) 2_546 2_546 ?
U4B O11 Rb5 117.2(7) 2_546 4_566 ?
Rb5 O11 Rb5 160.6(6) 4_566 2_546 ?
O11 O11 U2 66(2) 3_557 3_557 ?
O11 O11 U2 84(2) 3_557 . ?
O11 O11 U4A 158(3) 3_557 2_546 ?
O11 O11 U4B 159(3) 3_557 2_546 ?
O11 O11 Rb5 79(2) 3_557 2_546 ?
O11 O11 Rb5 82(2) 3_557 4_566 ?
U1 O12 U2 107.5(4) 4_566 . ?
P1 O12 U1 148.1(7) . 4_566 ?
P1 O12 U2 104.0(5) . . ?
Rb2A O13 Rb3B 136.7(8) 4_666 3_667 ?
Rb3A O13 Rb2A 76.4(4) . 4_666 ?
Rb3A O13 Rb3B 63.3(9) . 3_667 ?
Rb3B O13 Rb2A 80.4(6) . 4_666 ?
Rb3B O13 Rb3A 7.8(3) . . ?
Rb3B O13 Rb3B 57.8(10) . 3_667 ?
Rb3B O13 Rb4A 106.4(8) . . ?
Rb3B O13 Rb4B 110.4(15) . . ?
Rb4A O13 Rb2A 106.3(6) . 4_666 ?
Rb4A O13 Rb3A 113.9(7) . . ?
Rb4A O13 Rb3B 78.4(8) . 3_667 ?
Rb4A O13 Rb4B 4.1(13) . . ?
Rb4B O13 Rb2A 105.4(7) . 4_666 ?
Rb4B O13 Rb3A 117.8(14) . . ?
Rb4B O13 Rb3B 81.8(13) . 3_667 ?
P1 O13 Rb2A 103.4(9) . 4_666 ?
P1 O13 Rb3A 125.8(9) . . ?
P1 O13 Rb3B 131.9(10) . . ?
P1 O13 Rb3B 112.2(9) . 3_667 ?
P1 O13 Rb4A 117.7(9) . . ?
P1 O13 Rb4B 114.4(14) . . ?
U3 O14 U4B 103.5(4) 2_556 . ?
U3 O14 Rb4A 110.7(4) 2_556 4_565 ?
U3 O14 Rb4B 106.0(17) 2_556 4_565 ?
U4A O14 U3 111.2(4) . 2_556 ?
U4A O14 U4B 7.69(13) . . ?
U4A O14 Rb4A 88.3(4) . 4_565 ?
U4A O14 Rb4B 92.8(17) . 4_565 ?
U4B O14 Rb4A 90.8(4) . 4_565 ?
U4B O14 Rb4B 94.8(16) . 4_565 ?
Rb4B O14 Rb4A 5.5(18) 4_565 4_565 ?
P1 O14 U3 127.8(6) . 2_556 ?
P1 O14 U4A 111.6(6) . . ?
P1 O14 U4B 118.4(6) . . ?
P1 O14 Rb4A 99.1(6) . 4_565 ?
P1 O14 Rb4B 100.4(8) . 4_565 ?
U4A O15 U4B 12.98(14) . . ?
U4A O15 Rb2A 115.1(6) . 4_666 ?
U4A O15 Rb3A 135.4(6) . . ?
U4A O15 Rb3B 130.6(7) . . ?
U4A O15 Rb5 137.7(7) . . ?
U4B O15 Rb2A 125.6(7) . 4_666 ?
U4B O15 Rb3A 135.1(6) . . ?
U4B O15 Rb3B 133.5(6) . . ?
U4B O15 Rb5 124.8(7) . . ?
Rb2A O15 Rb3B 84.4(6) 4_666 . ?
Rb3A O15 Rb2A 90.0(4) . 4_666 ?
Rb3A O15 Rb3B 10.8(5) . . ?
Rb5 O15 Rb2A 99.7(4) . 4_666 ?
Rb5 O15 Rb3A 63.3(5) . . ?
Rb5 O15 Rb3B 73.4(9) . . ?
U4A O16 Rb1 123.9(5) . . ?
U4A O16 Rb2A 125.9(6) . . ?
U4A O16 Rb4A 110.0(7) . 4_565 ?
U4A O16 Rb4B 108.5(10) . 4_565 ?
U4B O16 U4A 12.85(13) . . ?
U4B O16 Rb1 116.9(5) . . ?
U4B O16 Rb2A 117.8(6) . . ?
U4B O16 Rb4A 121.8(7) . 4_565 ?
U4B O16 Rb4B 119.6(11) . 4_565 ?
Rb1 O16 Rb4A 84.7(4) . 4_565 ?
Rb1 O16 Rb4B 80.4(14) . 4_565 ?
Rb2A O16 Rb1 87.4(4) . . ?
Rb2A O16 Rb4A 116.4(5) . 4_565 ?
Rb2A O16 Rb4B 120.5(14) . 4_565 ?
Rb4A O16 Rb4B 6.3(19) 4_565 4_565 ?
U1 O17 Rb2A 94.9(4) . . ?
U2 O17 U1 115.7(5) 4_665 . ?
U2 O17 U4A 134.6(6) 4_665 . ?
U2 O17 Rb2A 93.5(4) 4_665 . ?
U4A O17 U1 108.6(4) . . ?
U4A O17 Rb2A 92.1(4) . . ?
U4B O17 U1 118.3(5) . . ?
U4B O17 U2 125.3(6) . 4_665 ?
U4B O17 U4A 9.73(13) . . ?
U4B O17 Rb2A 90.0(4) . . ?

_olex2_submission_special_instructions 'No special instructions were received'

# start Validation Reply Form
_vrf_PLAT976_Rb7.6U8P2O32.6F0.4  
;
PROBLEM: Check Calcd Resid. Dens.  0.85A   From O11            -2.32 eA-3  
RESPONSE: All residual electron density peaks are of acceptable magnitude 
and are less than 10% of the heaviest atom, U.
;
_vrf_PLAT971_Rb7.6U8P2O32.6F0.4  
;
PROBLEM: Check Calcd Resid. Dens.  0.89A   From U2              2.89 eA-3  
RESPONSE: Normal non-chemically significant residual peak near a very heavy 
atom, U. All residual electron density peaks are of acceptable magnitude 
and are less than 10% of the heaviest atom, U.
;
_vrf_PLAT975_Rb7.6U8P2O32.6F0.4  
;
PROBLEM: Check Calcd Resid. Dens.  0.90A   From O8              1.63 eA-3  
RESPONSE: All residual electron density peaks are of acceptable magnitude 
and are less than 10% of the heaviest atom, U.
;
# end Validation Reply Form

_exptl_crystal_recrystallization_method 'From the Melt'
_exptl_crystal_preparation       Luminescent
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_Rb11U8P9O52
_database_code_depnum_ccdc_archive 'CCDC 1984892'
loop_
_audit_author_name
_audit_author_address
'Christian Juillerat'
;University of South Carolina
United States of America
;
_audit_update_record             
;
2020-02-18 deposited with the CCDC.	2020-04-07 downloaded from the CCDC.
;
_audit_creation_date             2020-01-31
_audit_creation_method           
;
Olex2 1.2
(compiled May 18 2018 14:05:52 for OlexSys, GUI svn.r5506)
;
_shelx_SHELXL_version_number     2016/6
_chemical_name_common            ?
_chemical_name_systematic        Rb11[(UO2)8(PO4)9]
_chemical_formula_moiety         '0.25(O208 P36 Rb44 U32)'
_chemical_formula_sum            'O52 P9 Rb11.02 U8'
_chemical_formula_weight         3957.28
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Rb Rb -0.9393 2.9676 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
U U -9.6767 9.6646 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      tetragonal
_space_group_IT_number           135
_space_group_name_H-M_alt        'P 42/m b c'
_space_group_name_Hall           '-P 4c 2ab'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, z'
'-y, x, z+1/2'
'y, -x, z+1/2'
'-x+1/2, y+1/2, -z'
'x+1/2, -y+1/2, -z'
'y+1/2, x+1/2, -z+1/2'
'-y+1/2, -x+1/2, -z+1/2'
'-x, -y, -z'
'x, y, -z'
'y, -x, -z-1/2'
'-y, x, -z-1/2'
'x-1/2, -y-1/2, z'
'-x-1/2, y-1/2, z'
'-y-1/2, -x-1/2, z-1/2'
'y-1/2, x-1/2, z-1/2'

_cell_length_a                   25.7697(6)
_cell_length_b                   25.7697(6)
_cell_length_c                   9.3962(2)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_volume                     6239.8(3)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    9908
_cell_measurement_temperature    301(2)
_cell_measurement_theta_max      33.09
_cell_measurement_theta_min      2.50
_shelx_estimated_absorpt_T_max   0.589
_shelx_estimated_absorpt_T_min   0.156
_exptl_absorpt_coefficient_mu    29.564
_exptl_absorpt_correction_T_max  0.1605
_exptl_absorpt_correction_T_min  0.0668
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
SADABS-2016/2 (Bruker,2016) was used for absorption correction.
wR2(int) was 0.1592 before and 0.0684 after correction.
The Ratio of minimum to maximum transmission is 0.4162.
The λ/2 correction factor is Not present.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            yellow
_exptl_crystal_colour_primary    yellow
_exptl_crystal_density_diffrn    4.212
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       needle
_exptl_crystal_F_000             6780
_exptl_crystal_size_max          0.1
_exptl_crystal_size_mid          0.02
_exptl_crystal_size_min          0.02
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0452
_diffrn_reflns_av_unetI/netI     0.0144
_diffrn_reflns_Laue_measured_fraction_full 0.997
_diffrn_reflns_Laue_measured_fraction_max 0.998
_diffrn_reflns_limit_h_max       33
_diffrn_reflns_limit_h_min       -33
_diffrn_reflns_limit_k_max       32
_diffrn_reflns_limit_k_min       -33
_diffrn_reflns_limit_l_max       12
_diffrn_reflns_limit_l_min       -12
_diffrn_reflns_number            100392
_diffrn_reflns_point_group_measured_fraction_full 0.997
_diffrn_reflns_point_group_measured_fraction_max 0.998
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         27.500
_diffrn_reflns_theta_min         2.499
_diffrn_ambient_temperature      301.14
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_diffrn_standards_number         0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                3640
_reflns_number_total             3807
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       ?
_computing_data_collection       ?
_computing_data_reduction        ?
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    'ShelXT (Sheldrick, 2015)'
_refine_diff_density_max         2.126
_refine_diff_density_min         -1.686
_refine_diff_density_rms         0.266
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.326
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     341
_refine_ls_number_reflns         3807
_refine_ls_number_restraints     32
_refine_ls_R_factor_all          0.0366
_refine_ls_R_factor_gt           0.0350
_refine_ls_restrained_S_all      1.328
_refine_ls_shift/su_max          0.009
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0239P)²+153.3181P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0903
_refine_ls_wR_factor_ref         0.0910
_refine_special_details          ?
_olex2_refinement_description    
;
1. Uiso/Uaniso restraints and constraints
Uanis(Rb4A) \\sim Ueq, Uanis(Rb4B) \\sim Ueq: with sigma of 0.01 and sigma for
terminal atoms of 0.01
Uanis(O12A) \\sim Ueq, Uanis(O9A) \\sim Ueq, Uanis(O11A) \\sim Ueq: with sigma
of 0.01 and sigma for terminal atoms of 0.01
2. Others
 1*[Sof(Rb5A)]+2*[Sof(Rb5B)]+1*[Sof(Rb5C)]=1 with esd of 0.0001
 2*[Sof(Rb4A)]+1*[Sof(Rb4B)]=0.5 with esd of 0.0001
 Sof(P2B)=Sof(O9B)=Sof(O10B)=Sof(O11B)=Sof(O12B)=1-FVAR(1)
 Sof(P2A)=Sof(O9A)=Sof(O10A)=Sof(O11A)=Sof(O12A)=FVAR(1)
 Sof(P3B)=Sof(O4B)=Sof(O5B)=Sof(O6B)=1-FVAR(2)
 Sof(P3A)=Sof(O4A)=Sof(O5A)=Sof(O6A)=FVAR(2)
 Fixed Sof: U4(0.5) O8(0.5) O15A(0.5) O15B(0.5) O16(0.5) O17(0.5)
;
_atom_sites_solution_hydrogens   .
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
U1 U 0.43306(2) 0.74606(2) 0.500000 0.01371(11) Uani 1 2 d S T P . .
U2 U 0.26957(2) 0.58312(2) 0.500000 0.01998(12) Uani 1 2 d S T P . .
U3 U 0.11404(2) 0.50708(2) 0.500000 0.01539(11) Uani 1 2 d S T P . .
U4 U 0.23298(3) 0.77002(3) 0.54454(7) 0.01552(14) Uani 0.5 1 d . . . . .
Rb1 Rb 0.10402(5) 0.49348(5) 0.000000 0.0269(3) Uani 1 2 d S T P . .
Rb2 Rb 0.14831(6) 0.64831(6) 0.250000 0.0474(4) Uani 1 2 d S T P . .
Rb3 Rb 0.28578(9) 0.42430(7) 0.500000 0.0570(5) Uani 1 2 d S T P . .
Rb4A Rb 0.4213(2) 0.5896(2) 0.4107(10) 0.0515(17) Uani 0.2159(14) 1 d . U . . .
Rb4B Rb 0.4225(10) 0.5866(10) 0.500000 0.032(5) Uani 0.068(3) 2 d S TU P . .
Rb5A Rb 0.36269(17) 0.86269(17) 0.750000 0.0484(13) Uani 0.471(3) 2 d S T P . .
Rb5B Rb 0.3351(9) 0.8515(7) 0.722(4) 0.049(5) Uani 0.1688(16) 1 d . . . . .
Rb5C Rb 0.3342(10) 0.8342(10) 0.750000 0.054(12) Uani 0.191(3) 2 d S T P . .
Rb6 Rb 0.29981(7) 0.58402(6) 0.000000 0.0494(5) Uani 1 2 d S T P . .
P1 P 0.000000 0.500000 0.250000 0.0138(8) Uani 1 4 d S T P . .
P2A P 0.2145(3) 0.5082(2) 0.2266(10) 0.0145(15) Uani 0.492(15) 1 d . . . . .
P2B P 0.2039(3) 0.5150(2) 0.2850(10) 0.0157(14) Uani 0.508(15) 1 d . . . . .
P3A P 0.3298(5) 0.6804(5) 0.2909(14) 0.0127(19) Uani 0.48(3) 1 d . . . . .
P3B P 0.3197(5) 0.6940(5) 0.3039(13) 0.015(2) Uani 0.52(3) 1 d . . . . .
O1 O 0.4010(4) 0.8086(4) 0.500000 0.026(2) Uani 1 2 d S T P . .
O2 O 0.4686(4) 0.6865(4) 0.500000 0.030(2) Uani 1 2 d S T P . .
O3 O 0.3745(3) 0.7104(4) 0.3483(10) 0.048(2) Uani 1 1 d . . . . .
O4A O 0.2789(6) 0.7131(6) 0.304(2) 0.024(4) Uani 0.48(3) 1 d . . . . .
O4B O 0.2795(7) 0.7246(8) 0.385(2) 0.044(5) Uani 0.52(3) 1 d . . . . .
O5A O 0.3351(5) 0.6748(6) 0.1288(13) 0.016(4) Uani 0.48(3) 1 d . . . . .
O5B O 0.3136(6) 0.7038(7) 0.1462(15) 0.037(5) Uani 0.52(3) 1 d . . . . .
O6A O 0.3239(13) 0.6311(15) 0.370(3) 0.027(6) Uani 0.48(3) 1 d . . . . .
O6B O 0.3135(13) 0.6348(13) 0.326(3) 0.031(6) Uani 0.52(3) 1 d . . . . .
O7 O 0.2175(4) 0.6277(4) 0.500000 0.025(2) Uani 1 2 d S T P . .
O8 O 0.3206(5) 0.5359(5) 0.4643(18) 0.033(6) Uani 0.5 1 d . . . . .
O9A O 0.2486(9) 0.5482(9) 0.292(2) 0.041(5) Uani 0.492(15) 1 d . U . . .
O9B O 0.2329(6) 0.5649(6) 0.2550(19) 0.024(3) Uani 0.508(15) 1 d . . . . .
O10A O 0.2131(5) 0.5142(5) 0.0618(13) 0.017(3) Uani 0.492(15) 1 d . . . . .
O10B O 0.2087(5) 0.5101(4) 0.4519(11) 0.012(3) Uani 0.508(15) 1 d . . . . .
O11A O 0.2376(9) 0.4557(9) 0.247(2) 0.029(5) Uani 0.492(15) 1 d . U . . .
O11B O 0.2278(9) 0.4699(8) 0.214(2) 0.033(5) Uani 0.508(15) 1 d . . . . .
O12A O 0.1577(13) 0.5098(12) 0.282(4) 0.040(8) Uani 0.492(15) 1 d . U . . .
O12B O 0.1465(11) 0.5219(10) 0.263(3) 0.033(6) Uani 0.508(15) 1 d . . . . .
O13 O 0.1078(4) 0.5758(4) 0.500000 0.037(3) Uani 1 2 d S T P . .
O14 O 0.1205(4) 0.4383(4) 0.500000 0.033(3) Uani 1 2 d S T P . .
O15A O 0.0423(9) 0.5053(10) 0.362(3) 0.027(4) Uani 0.5 1 d . . . . .
O15B O 0.0532(10) 0.4943(15) 0.328(3) 0.055(9) Uani 0.5 1 d . . . . .
O16 O 0.1781(5) 0.7269(5) 0.5311(15) 0.025(5) Uani 0.5 1 d . . . . .
O17 O 0.2843(6) 0.8174(6) 0.5615(18) 0.035(3) Uani 0.5 1 d . . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
U1 P2A 3.052(10) 4_565 ?
U1 P2A 3.052(10) 11_566 ?
U1 O1 1.810(10) . ?
U1 O2 1.787(10) . ?
U1 O3 2.270(8) . ?
U1 O3 2.270(8) 10_556 ?
U1 O10A 2.413(13) 11_566 ?
U1 O10A 2.413(13) 4_565 ?
U1 O11A 2.43(2) 4_565 ?
U1 O11A 2.43(2) 11_566 ?
U1 O11B 2.323(19) 11_566 ?
U1 O11B 2.323(19) 4_565 ?
U2 O6A 2.23(3) . ?
U2 O6A 2.23(3) 10_556 ?
U2 O6B 2.39(3) 10_556 ?
U2 O6B 2.39(3) . ?
U2 O7 1.766(10) . ?
U2 O8 1.822(14) 10_556 ?
U2 O8 1.822(14) . ?
U2 O9A 2.22(2) . ?
U2 O9A 2.22(2) 10_556 ?
U2 O9B 2.532(18) . ?
U2 O10B 2.490(11) . ?
U2 O10B 2.490(11) 10_556 ?
U3 O10B 2.483(12) 10_556 ?
U3 O10B 2.483(12) . ?
U3 O12A 2.34(3) 10_556 ?
U3 O12A 2.34(3) . ?
U3 O12B 2.41(3) 10_556 ?
U3 O12B 2.41(3) . ?
U3 O13 1.778(10) . ?
U3 O14 1.780(10) . ?
U3 O15A 2.26(3) 10_556 ?
U3 O15A 2.26(3) . ?
U3 O15B 2.28(3) 10_556 ?
U3 O15B 2.28(3) . ?
U4 U4 0.8370(12) 10_556 ?
U4 O4A 2.506(19) 16_566 ?
U4 O4A 2.359(17) 10_556 ?
U4 O4B 2.25(2) . ?
U4 O4B 1.803(19) 10_556 ?
U4 O5A 2.385(14) 16_566 ?
U4 O5B 1.656(15) 16_566 ?
U4 O5B 2.246(14) 7_455 ?
U4 O16 1.804(12) . ?
U4 O16 1.935(13) 10_556 ?
U4 O17 1.807(15) . ?
U4 O17 2.057(16) 10_556 ?
Rb1 O10A 2.919(12) . ?
Rb1 O10A 2.919(12) 10 ?
Rb1 O12A 3.02(3) . ?
Rb1 O12A 3.02(3) 10 ?
Rb1 O12B 2.80(3) . ?
Rb1 O12B 2.80(3) 10 ?
Rb1 O13 3.034(11) 7_455 ?
Rb1 O14 3.133(11) 15_665 ?
Rb1 O15A 3.12(2) 7_455 ?
Rb1 O15A 3.24(3) 8 ?
Rb1 O15A 3.12(2) 16_565 ?
Rb1 O15A 3.24(3) 15_665 ?
Rb2 O7 2.997(6) . ?
Rb2 O7 2.997(6) 7_455 ?
Rb2 O9B 3.062(17) . ?
Rb2 O9B 3.062(17) 7_455 ?
Rb2 O12B 3.26(3) . ?
Rb2 O12B 3.26(3) 7_455 ?
Rb2 O13 3.178(7) . ?
Rb2 O13 3.178(7) 7_455 ?
Rb2 O16 2.987(13) 16_565 ?
Rb2 O16 2.987(13) 10_556 ?
Rb2 O16 3.415(14) 7_455 ?
Rb2 O16 3.415(14) . ?
Rb3 O5A 2.790(13) 12_656 ?
Rb3 O5A 2.790(13) 3_655 ?
Rb3 O5B 3.177(17) 12_656 ?
Rb3 O5B 3.177(17) 3_655 ?
Rb3 O8 3.032(13) 10_556 ?
Rb3 O8 3.032(13) . ?
Rb3 O10B 3.006(11) 10_556 ?
Rb3 O10B 3.006(11) . ?
Rb3 O11A 2.80(2) . ?
Rb3 O11A 2.80(2) 10_556 ?
Rb3 O11B 3.29(2) 10_556 ?
Rb3 O11B 3.29(2) . ?
Rb4A Rb4A 1.678(18) 10_556 ?
Rb4A Rb4B 0.843(10) . ?
Rb4A P3A 3.507(16) . ?
Rb4A P3B 3.887(15) . ?
Rb4A O2 2.902(11) . ?
Rb4A O3 3.389(12) . ?
Rb4A O6A 2.75(3) . ?
Rb4A O6A 3.42(2) 10_556 ?
Rb4A O6B 3.11(3) . ?
Rb4A O8 3.166(14) 10_556 ?
Rb4A O8 2.983(14) . ?
Rb4B P3A 3.92(3) . ?
Rb4B P3A 3.92(3) 10_556 ?
Rb4B O2 2.83(2) . ?
Rb4B O6A 3.04(4) 10_556 ?
Rb4B O6A 3.04(4) . ?
Rb4B O6B 3.48(4) . ?
Rb4B O6B 3.48(4) 10_556 ?
Rb4B O8 2.95(3) . ?
Rb4B O8 2.95(3) 10_556 ?
Rb5A Rb5B 0.81(3) . ?
Rb5A Rb5B 0.81(3) 7_456 ?
Rb5A Rb5C 1.04(4) . ?
Rb5A O1 2.905(6) . ?
Rb5A O1 2.905(6) 7_456 ?
Rb5A O11A 3.52(2) 4_565 ?
Rb5A O11A 3.52(2) 5_556 ?
Rb5A O11B 3.63(2) 5_556 ?
Rb5A O14 3.083(7) 5_556 ?
Rb5A O14 3.083(7) 11_567 ?
Rb5A O17 2.929(16) 7_456 ?
Rb5A O17 2.929(16) . ?
Rb5B Rb5B 0.79(6) 7_456 ?
Rb5B Rb5C 0.51(2) . ?
Rb5B O1 2.98(3) 7_456 ?
Rb5B O1 2.91(2) . ?
Rb5B O3 3.475(19) 16_566 ?
Rb5B O11A 3.29(3) 5_556 ?
Rb5B O11B 3.51(3) 5_556 ?
Rb5B O14 3.269(19) 5_556 ?
Rb5B O17 3.10(4) 10_556 ?
Rb5B O17 2.18(4) . ?
Rb5B O17 2.71(3) 7_456 ?
Rb5C O1 2.986(11) 7_456 ?
Rb5C O1 2.986(11) . ?
Rb5C O4A 3.47(4) 10_556 ?
Rb5C O4B 3.40(4) 16_566 ?
Rb5C O4B 3.40(4) 10_556 ?
Rb5C O17 3.23(2) 10_556 ?
Rb5C O17 2.23(3) . ?
Rb5C O17 2.23(3) 7_456 ?
Rb5C O17 3.23(2) 16_566 ?
Rb6 O2 2.996(11) 3_654 ?
Rb6 O5A 2.786(13) . ?
Rb6 O5A 2.786(13) 10 ?
Rb6 O6B 3.35(3) 10 ?
Rb6 O9A 3.18(2) 10 ?
Rb6 O9A 3.18(2) . ?
Rb6 O9B 2.992(16) 10 ?
Rb6 O9B 2.992(16) . ?
Rb6 O10A 2.927(13) 10 ?
Rb6 O10A 2.927(13) . ?
Rb6 O16 3.080(13) 16_565 ?
Rb6 O16 3.080(13) 7_455 ?
P1 O15A 1.52(3) . ?
P1 O15A 1.52(3) 2_565 ?
P1 O15A 1.52(3) 7_455 ?
P1 O15A 1.52(3) 8 ?
P1 O15B 1.56(3) . ?
P1 O15B 1.56(3) 2_565 ?
P1 O15B 1.56(3) 8 ?
P1 O15B 1.56(3) 7_455 ?
P2A P2B 0.637(5) . ?
P2A O9A 1.49(2) . ?
P2A O9B 1.561(16) . ?
P2A O10A 1.556(15) . ?
P2A O10B 2.123(14) . ?
P2A O11A 1.49(2) . ?
P2A O11B 1.05(2) . ?
P2A O12A 1.55(3) . ?
P2A O12B 1.82(3) . ?
P2B O9A 1.44(2) . ?
P2B O9B 1.515(17) . ?
P2B O10A 2.110(15) . ?
P2B O10B 1.579(13) . ?
P2B O11A 1.80(2) . ?
P2B O11B 1.47(2) . ?
P2B O12A 1.20(3) . ?
P2B O12B 1.50(3) . ?
P3A O3 1.487(16) . ?
P3A O4A 1.565(18) . ?
P3A O4B 1.94(2) . ?
P3A O5A 1.536(18) . ?
P3A O5B 1.54(2) . ?
P3A O6A 1.48(3) . ?
P3A O6B 1.29(3) . ?
P3B O3 1.533(16) . ?
P3B O4A 1.16(2) . ?
P3B O4B 1.505(19) . ?
P3B O5A 1.763(17) . ?
P3B O5B 1.511(19) . ?
P3B O6A 1.74(4) . ?
P3B O6B 1.55(3) . ?
O4A O4B 0.81(2) . ?
O4A O5B 1.75(2) . ?
O5A O5B 0.944(18) . ?
O8 O8 0.67(3) 10_556 ?
O9A O9B 0.68(2) . ?
O10A O10A 1.16(2) 10 ?
O10B O10B 0.90(2) 10_556 ?
O11A O11B 0.541(19) . ?
O15A O15B 0.51(3) . ?
O16 O16 0.58(3) 10_556 ?
O17 O17 1.16(3) 10_556 ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
P2A U1 P2A 88.5(2) 4_565 11_566 ?
O1 U1 P2A 89.6(3) . 4_565 ?
O1 U1 P2A 89.6(3) . 11_566 ?
O1 U1 O3 93.3(4) . . ?
O1 U1 O3 93.3(4) . 10_556 ?
O1 U1 O10A 90.4(4) . 11_566 ?
O1 U1 O10A 90.4(4) . 4_565 ?
O1 U1 O11A 87.4(6) . 11_566 ?
O1 U1 O11A 87.4(6) . 4_565 ?
O1 U1 O11B 85.9(6) . 4_565 ?
O1 U1 O11B 85.9(6) . 11_566 ?
O2 U1 P2A 87.8(3) . 11_566 ?
O2 U1 P2A 87.8(3) . 4_565 ?
O2 U1 O1 176.3(5) . . ?
O2 U1 O3 89.6(4) . . ?
O2 U1 O3 89.6(4) . 10_556 ?
O2 U1 O10A 86.0(4) . 4_565 ?
O2 U1 O10A 86.0(4) . 11_566 ?
O2 U1 O11A 91.5(6) . 4_565 ?
O2 U1 O11A 91.5(6) . 11_566 ?
O2 U1 O11B 92.3(6) . 4_565 ?
O2 U1 O11B 92.3(6) . 11_566 ?
O3 U1 P2A 96.8(3) 10_556 4_565 ?
O3 U1 P2A 96.8(3) . 11_566 ?
O3 U1 P2A 174.0(3) . 4_565 ?
O3 U1 P2A 174.0(3) 10_556 11_566 ?
O3 U1 O3 77.8(5) . 10_556 ?
O3 U1 O10A 127.0(4) 10_556 4_565 ?
O3 U1 O10A 154.7(4) 10_556 11_566 ?
O3 U1 O10A 154.7(4) . 4_565 ?
O3 U1 O10A 127.0(4) . 11_566 ?
O3 U1 O11A 146.0(5) . 4_565 ?
O3 U1 O11A 146.0(5) 10_556 11_566 ?
O3 U1 O11A 68.3(5) . 11_566 ?
O3 U1 O11A 68.3(5) 10_556 4_565 ?
O3 U1 O11B 158.8(6) 10_556 11_566 ?
O3 U1 O11B 81.1(6) 10_556 4_565 ?
O3 U1 O11B 158.8(6) . 4_565 ?
O3 U1 O11B 81.1(6) . 11_566 ?
O10A U1 P2A 58.2(3) 11_566 4_565 ?
O10A U1 P2A 30.3(3) 4_565 4_565 ?
O10A U1 P2A 30.3(3) 11_566 11_566 ?
O10A U1 P2A 58.2(3) 4_565 11_566 ?
O10A U1 O10A 27.9(6) 4_565 11_566 ?
O10A U1 O11A 86.9(6) 11_566 4_565 ?
O10A U1 O11A 59.1(6) 11_566 11_566 ?
O10A U1 O11A 59.1(6) 4_565 4_565 ?
O10A U1 O11A 86.9(6) 4_565 11_566 ?
O11A U1 P2A 28.8(5) 11_566 11_566 ?
O11A U1 P2A 117.1(5) 4_565 11_566 ?
O11A U1 P2A 28.8(5) 4_565 4_565 ?
O11A U1 P2A 117.1(5) 11_566 4_565 ?
O11A U1 O11A 145.6(10) 4_565 11_566 ?
O11B U1 P2A 16.4(5) 11_566 11_566 ?
O11B U1 P2A 16.4(5) 4_565 4_565 ?
O11B U1 P2A 104.4(5) 11_566 4_565 ?
O11B U1 P2A 104.4(5) 4_565 11_566 ?
O11B U1 O10A 74.2(6) 4_565 11_566 ?
O11B U1 O10A 74.2(6) 11_566 4_565 ?
O11B U1 O10A 46.5(6) 11_566 11_566 ?
O11B U1 O10A 46.5(6) 4_565 4_565 ?
O11B U1 O11A 132.7(9) 4_565 11_566 ?
O11B U1 O11A 12.8(5) 11_566 11_566 ?
O11B U1 O11A 12.8(5) 4_565 4_565 ?
O11B U1 O11A 132.7(9) 11_566 4_565 ?
O11B U1 O11B 119.9(10) 4_565 11_566 ?
O6A U2 O6A 66.4(15) . 10_556 ?
O6A U2 O6B 76.6(9) 10_556 . ?
O6A U2 O6B 11.7(9) 10_556 10_556 ?
O6A U2 O6B 11.7(9) . . ?
O6A U2 O6B 76.6(9) . 10_556 ?
O6A U2 O9B 146.6(9) 10_556 . ?
O6A U2 O9B 80.7(8) . . ?
O6A U2 O10B 135.5(9) 10_556 10_556 ?
O6A U2 O10B 135.5(9) . . ?
O6A U2 O10B 155.9(9) . 10_556 ?
O6A U2 O10B 155.9(9) 10_556 . ?
O6B U2 O6B 86.0(14) . 10_556 ?
O6B U2 O9B 154.2(8) 10_556 . ?
O6B U2 O9B 70.1(8) . . ?
O6B U2 O10B 147.4(7) . 10_556 ?
O6B U2 O10B 147.4(7) 10_556 . ?
O6B U2 O10B 126.5(7) 10_556 10_556 ?
O6B U2 O10B 126.5(7) . . ?
O7 U2 O6A 96.7(9) . 10_556 ?
O7 U2 O6A 96.7(9) . . ?
O7 U2 O6B 89.8(8) . . ?
O7 U2 O6B 89.8(8) . 10_556 ?
O7 U2 O8 169.2(5) . 10_556 ?
O7 U2 O8 169.2(5) . . ?
O7 U2 O9A 94.5(7) . 10_556 ?
O7 U2 O9A 94.5(7) . . ?
O7 U2 O9B 80.6(4) . . ?
O7 U2 O10B 90.8(4) . 10_556 ?
O7 U2 O10B 90.8(4) . . ?
O8 U2 O6A 79.4(10) 10_556 10_556 ?
O8 U2 O6A 91.0(9) 10_556 . ?
O8 U2 O6A 79.4(10) . . ?
O8 U2 O6A 91.0(9) . 10_556 ?
O8 U2 O6B 98.9(9) . 10_556 ?
O8 U2 O6B 84.5(9) 10_556 10_556 ?
O8 U2 O6B 84.5(9) . . ?
O8 U2 O6B 98.9(9) 10_556 . ?
O8 U2 O8 21.2(10) 10_556 . ?
O8 U2 O9A 93.9(8) . 10_556 ?
O8 U2 O9A 93.9(8) 10_556 . ?
O8 U2 O9A 75.1(8) . . ?
O8 U2 O9A 75.1(8) 10_556 10_556 ?
O8 U2 O9B 88.8(6) . . ?
O8 U2 O9B 108.2(6) 10_556 . ?
O8 U2 O10B 89.1(5) 10_556 . ?
O8 U2 O10B 85.2(5) . . ?
O8 U2 O10B 85.2(5) 10_556 10_556 ?
O8 U2 O10B 89.1(5) . 10_556 ?
O9A U2 O6A 83.9(10) 10_556 10_556 ?
O9A U2 O6A 149.3(9) 10_556 . ?
O9A U2 O6A 83.9(10) . . ?
O9A U2 O6A 149.3(9) . 10_556 ?
O9A U2 O6B 160.4(9) 10_556 . ?
O9A U2 O6B 160.4(9) . 10_556 ?
O9A U2 O6B 74.9(9) . . ?
O9A U2 O6B 74.9(9) 10_556 10_556 ?
O9A U2 O9A 123.6(11) . 10_556 ?
O9A U2 O9B 14.8(6) . . ?
O9A U2 O9B 129.5(5) 10_556 . ?
O9A U2 O10B 72.6(6) 10_556 . ?
O9A U2 O10B 51.8(6) 10_556 10_556 ?
O9A U2 O10B 51.8(6) . . ?
O9A U2 O10B 72.6(6) . 10_556 ?
O10B U2 O9B 77.9(4) 10_556 . ?
O10B U2 O9B 57.3(4) . . ?
O10B U2 O10B 20.9(5) . 10_556 ?
O10B U3 O10B 21.0(5) 10_556 . ?
O12A U3 O10B 50.7(8) . . ?
O12A U3 O10B 71.7(8) 10_556 . ?
O12A U3 O10B 71.7(8) . 10_556 ?
O12A U3 O10B 50.7(8) 10_556 10_556 ?
O12A U3 O12A 122.4(16) 10_556 . ?
O12A U3 O12B 129.6(7) . 10_556 ?
O12A U3 O12B 129.6(7) 10_556 . ?
O12A U3 O12B 10.9(9) 10_556 10_556 ?
O12A U3 O12B 10.9(9) . . ?
O12B U3 O10B 59.0(7) 10_556 10_556 ?
O12B U3 O10B 79.7(7) 10_556 . ?
O12B U3 O10B 59.0(7) . . ?
O12B U3 O10B 79.7(7) . 10_556 ?
O12B U3 O12B 135.1(15) 10_556 . ?
O13 U3 O10B 93.3(4) . 10_556 ?
O13 U3 O10B 93.3(4) . . ?
O13 U3 O12A 90.8(8) . . ?
O13 U3 O12A 90.8(8) . 10_556 ?
O13 U3 O12B 82.8(6) . . ?
O13 U3 O12B 82.8(6) . 10_556 ?
O13 U3 O14 179.8(5) . . ?
O13 U3 O15A 86.9(7) . . ?
O13 U3 O15A 86.9(7) . 10_556 ?
O13 U3 O15B 94.7(10) . . ?
O13 U3 O15B 94.7(10) . 10_556 ?
O14 U3 O10B 86.5(4) . 10_556 ?
O14 U3 O10B 86.5(4) . . ?
O14 U3 O12A 89.2(8) . . ?
O14 U3 O12A 89.2(8) . 10_556 ?
O14 U3 O12B 97.2(6) . . ?
O14 U3 O12B 97.2(6) . 10_556 ?
O14 U3 O15A 93.2(7) . 10_556 ?
O14 U3 O15A 93.2(7) . . ?
O14 U3 O15B 85.4(10) . . ?
O14 U3 O15B 85.4(10) . 10_556 ?
O15A U3 O10B 134.5(6) 10_556 10_556 ?
O15A U3 O10B 155.5(6) 10_556 . ?
O15A U3 O10B 134.5(6) . . ?
O15A U3 O10B 155.5(6) . 10_556 ?
O15A U3 O12A 83.8(10) 10_556 10_556 ?
O15A U3 O12A 153.8(9) . 10_556 ?
O15A U3 O12A 153.8(9) 10_556 . ?
O15A U3 O12A 83.8(10) . . ?
O15A U3 O12B 76.0(9) . . ?
O15A U3 O12B 144.9(8) 10_556 . ?
O15A U3 O12B 144.9(8) . 10_556 ?
O15A U3 O12B 76.0(9) 10_556 10_556 ?
O15A U3 O15A 70.0(11) . 10_556 ?
O15A U3 O15B 80.9(7) 10_556 . ?
O15A U3 O15B 13.0(6) 10_556 10_556 ?
O15A U3 O15B 13.0(6) . . ?
O15A U3 O15B 80.9(7) . 10_556 ?
O15B U3 O10B 144.1(6) . 10_556 ?
O15B U3 O10B 123.5(6) 10_556 10_556 ?
O15B U3 O10B 144.1(6) 10_556 . ?
O15B U3 O10B 123.5(6) . . ?
O15B U3 O12A 73.3(10) 10_556 10_556 ?
O15B U3 O12A 163.4(12) 10_556 . ?
O15B U3 O12A 163.4(12) . 10_556 ?
O15B U3 O12A 73.3(10) . . ?
O15B U3 O12B 66.7(10) 10_556 10_556 ?
O15B U3 O12B 156.8(9) 10_556 . ?
O15B U3 O12B 66.7(10) . . ?
O15B U3 O12B 156.8(9) . 10_556 ?
O15B U3 O15B 90.6(14) 10_556 . ?
U4 U4 O4A 127.0(4) 10_556 10_556 ?
U4 U4 O4A 167.1(4) 10_556 16_566 ?
U4 U4 O4B 48.1(4) 10_556 . ?
U4 U4 O4B 111.7(6) 10_556 10_556 ?
U4 U4 O5A 109.4(3) 10_556 16_566 ?
U4 U4 O5B 125.2(6) 10_556 16_566 ?
U4 U4 O5B 37.0(4) 10_556 7_455 ?
U4 U4 O16 68.4(4) 10_556 10_556 ?
U4 U4 O16 86.0(5) 10_556 . ?
U4 U4 O17 95.1(5) 10_556 . ?
U4 U4 O17 61.0(5) 10_556 10_556 ?
O4A U4 O4A 64.7(6) 10_556 16_566 ?
O4A U4 O5A 123.6(5) 10_556 16_566 ?
O4B U4 O4A 143.8(6) . 16_566 ?
O4B U4 O4A 80.5(6) 10_556 16_566 ?
O4B U4 O4A 79.1(6) . 10_556 ?
O4B U4 O4A 16.4(7) 10_556 10_556 ?
O4B U4 O4B 63.6(10) 10_556 . ?
O4B U4 O5A 138.7(6) 10_556 16_566 ?
O4B U4 O5A 157.3(5) . 16_566 ?
O4B U4 O5B 147.4(8) 10_556 7_455 ?
O4B U4 O16 98.5(8) 10_556 . ?
O4B U4 O16 104.5(7) 10_556 10_556 ?
O4B U4 O17 85.3(8) 10_556 . ?
O4B U4 O17 97.8(9) 10_556 10_556 ?
O5A U4 O4A 58.9(4) 16_566 16_566 ?
O5B U4 O4A 44.2(6) 16_566 16_566 ?
O5B U4 O4A 107.6(7) 16_566 10_556 ?
O5B U4 O4A 131.6(6) 7_455 16_566 ?
O5B U4 O4A 163.6(7) 7_455 10_556 ?
O5B U4 O4B 168.5(8) 16_566 . ?
O5B U4 O4B 122.0(7) 16_566 10_556 ?
O5B U4 O4B 84.6(6) 7_455 . ?
O5B U4 O5A 17.3(6) 16_566 16_566 ?
O5B U4 O5A 72.7(6) 7_455 16_566 ?
O5B U4 O5B 88.2(10) 16_566 7_455 ?
O5B U4 O16 95.9(8) 16_566 . ?
O5B U4 O16 105.6(8) 16_566 10_556 ?
O5B U4 O17 99.7(8) 16_566 10_556 ?
O5B U4 O17 79.8(8) 16_566 . ?
O16 U4 O4A 88.0(6) . 16_566 ?
O16 U4 O4A 103.4(5) 10_556 10_556 ?
O16 U4 O4A 105.1(6) 10_556 16_566 ?
O16 U4 O4A 93.0(6) . 10_556 ?
O16 U4 O4B 92.9(7) . . ?
O16 U4 O4B 81.2(7) 10_556 . ?
O16 U4 O5A 87.9(5) . 16_566 ?
O16 U4 O5A 93.8(5) 10_556 16_566 ?
O16 U4 O5B 75.5(6) 10_556 7_455 ?
O16 U4 O5B 89.4(6) . 7_455 ?
O16 U4 O16 17.5(9) . 10_556 ?
O16 U4 O17 146.7(6) . 10_556 ?
O16 U4 O17 175.3(6) . . ?
O16 U4 O17 129.3(6) 10_556 10_556 ?
O17 U4 O4A 90.1(6) . 16_566 ?
O17 U4 O4A 90.0(6) . 10_556 ?
O17 U4 O4A 109.7(6) 10_556 10_556 ?
O17 U4 O4A 123.3(6) 10_556 16_566 ?
O17 U4 O4B 69.0(7) 10_556 . ?
O17 U4 O4B 91.1(8) . . ?
O17 U4 O5A 98.5(5) 10_556 16_566 ?
O17 U4 O5A 87.5(6) . 16_566 ?
O17 U4 O5B 88.7(7) . 7_455 ?
O17 U4 O5B 62.1(7) 10_556 7_455 ?
O17 U4 O16 162.9(7) . 10_556 ?
O17 U4 O17 34.0(10) . 10_556 ?
O10A Rb1 O10A 23.0(5) 10 . ?
O10A Rb1 O12A 73.0(7) . 10 ?
O10A Rb1 O12A 50.1(7) 10 10 ?
O10A Rb1 O12A 50.1(7) . . ?
O10A Rb1 O12A 73.0(7) 10 . ?
O10A Rb1 O13 93.0(3) 10 7_455 ?
O10A Rb1 O13 93.0(3) . 7_455 ?
O10A Rb1 O14 120.5(3) . 15_665 ?
O10A Rb1 O14 120.5(3) 10 15_665 ?
O10A Rb1 O15A 144.2(5) 10 15_665 ?
O10A Rb1 O15A 166.0(4) 10 8 ?
O10A Rb1 O15A 128.9(5) 10 16_565 ?
O10A Rb1 O15A 142.5(5) . 16_565 ?
O10A Rb1 O15A 166.0(4) . 15_665 ?
O10A Rb1 O15A 142.5(5) 10 7_455 ?
O10A Rb1 O15A 144.2(5) . 8 ?
O10A Rb1 O15A 128.9(5) . 7_455 ?
O12A Rb1 O12A 122.7(13) 10 . ?
O12A Rb1 O13 88.5(6) 10 7_455 ?
O12A Rb1 O13 88.5(6) . 7_455 ?
O12A Rb1 O14 106.9(6) . 15_665 ?
O12A Rb1 O14 106.9(6) 10 15_665 ?
O12A Rb1 O15A 95.0(8) . 8 ?
O12A Rb1 O15A 142.2(8) . 15_665 ?
O12A Rb1 O15A 87.3(7) 10 16_565 ?
O12A Rb1 O15A 133.0(7) . 16_565 ?
O12A Rb1 O15A 95.0(8) 10 15_665 ?
O12A Rb1 O15A 133.0(7) 10 7_455 ?
O12A Rb1 O15A 142.2(8) 10 8 ?
O12A Rb1 O15A 87.3(7) . 7_455 ?
O12B Rb1 O10A 75.6(6) . 10 ?
O12B Rb1 O10A 75.6(6) 10 . ?
O12B Rb1 O10A 53.2(6) 10 10 ?
O12B Rb1 O10A 53.2(6) . . ?
O12B Rb1 O12A 124.0(4) 10 . ?
O12B Rb1 O12A 8.0(8) . . ?
O12B Rb1 O12A 8.0(8) 10 10 ?
O12B Rb1 O12A 124.0(4) . 10 ?
O12B Rb1 O12B 124.0(11) . 10 ?
O12B Rb1 O13 80.8(5) 10 7_455 ?
O12B Rb1 O13 80.8(5) . 7_455 ?
O12B Rb1 O14 112.4(5) 10 15_665 ?
O12B Rb1 O14 112.4(5) . 15_665 ?
O12B Rb1 O15A 140.2(7) . 15_665 ?
O12B Rb1 O15A 125.4(7) . 16_565 ?
O12B Rb1 O15A 81.2(7) . 7_455 ?
O12B Rb1 O15A 93.5(7) 10 15_665 ?
O12B Rb1 O15A 81.2(7) 10 16_565 ?
O12B Rb1 O15A 125.4(7) 10 7_455 ?
O12B Rb1 O15A 140.2(7) 10 8 ?
O12B Rb1 O15A 93.5(7) . 8 ?
O13 Rb1 O14 145.8(3) 7_455 15_665 ?
O13 Rb1 O15A 93.9(4) 7_455 15_665 ?
O13 Rb1 O15A 93.9(4) 7_455 8 ?
O13 Rb1 O15A 54.0(5) 7_455 7_455 ?
O13 Rb1 O15A 54.0(5) 7_455 16_565 ?
O14 Rb1 O15A 55.2(5) 15_665 15_665 ?
O14 Rb1 O15A 55.2(5) 15_665 8 ?
O15A Rb1 O14 95.4(5) 16_565 15_665 ?
O15A Rb1 O14 95.4(5) 7_455 15_665 ?
O15A Rb1 O15A 49.1(9) 16_565 7_455 ?
O15A Rb1 O15A 40.4(9) 16_565 15_665 ?
O15A Rb1 O15A 47.2(8) 15_665 8 ?
O15A Rb1 O15A 64.6(6) 7_455 15_665 ?
O15A Rb1 O15A 64.6(6) 16_565 8 ?
O15A Rb1 O15A 40.4(9) 7_455 8 ?
O7 Rb2 O7 145.6(4) 7_455 . ?
O7 Rb2 O9B 55.9(4) . . ?
O7 Rb2 O9B 123.8(4) . 7_455 ?
O7 Rb2 O9B 55.9(4) 7_455 7_455 ?
O7 Rb2 O9B 123.8(4) 7_455 . ?
O7 Rb2 O12B 128.5(5) 7_455 . ?
O7 Rb2 O12B 128.5(5) . 7_455 ?
O7 Rb2 O12B 78.5(6) 7_455 7_455 ?
O7 Rb2 O12B 78.5(6) . . ?
O7 Rb2 O13 60.8(2) 7_455 7_455 ?
O7 Rb2 O13 150.6(3) 7_455 . ?
O7 Rb2 O13 150.6(3) . 7_455 ?
O7 Rb2 O13 60.8(2) . . ?
O7 Rb2 O16 50.6(3) 7_455 7_455 ?
O7 Rb2 O16 107.0(3) 7_455 . ?
O7 Rb2 O16 50.6(3) . . ?
O7 Rb2 O16 107.0(3) . 7_455 ?
O9B Rb2 O9B 179.1(6) . 7_455 ?
O9B Rb2 O12B 134.6(6) . 7_455 ?
O9B Rb2 O12B 46.2(6) . . ?
O9B Rb2 O12B 46.2(6) 7_455 7_455 ?
O9B Rb2 O12B 134.6(6) 7_455 . ?
O9B Rb2 O13 101.5(4) . 7_455 ?
O9B Rb2 O13 79.1(4) . . ?
O9B Rb2 O13 79.1(4) 7_455 7_455 ?
O9B Rb2 O13 101.5(4) 7_455 . ?
O9B Rb2 O16 75.3(4) 7_455 . ?
O9B Rb2 O16 104.1(4) 7_455 7_455 ?
O9B Rb2 O16 104.1(4) . . ?
O9B Rb2 O16 75.3(4) . 7_455 ?
O12B Rb2 O12B 88.5(10) 7_455 . ?
O12B Rb2 O16 105.2(5) . 7_455 ?
O12B Rb2 O16 124.5(6) 7_455 7_455 ?
O12B Rb2 O16 105.2(5) 7_455 . ?
O12B Rb2 O16 124.5(6) . . ?
O13 Rb2 O12B 51.6(5) 7_455 7_455 ?
O13 Rb2 O12B 72.1(6) 7_455 . ?
O13 Rb2 O12B 72.1(6) . 7_455 ?
O13 Rb2 O12B 51.6(5) . . ?
O13 Rb2 O13 99.2(3) 7_455 . ?
O13 Rb2 O16 81.4(3) 7_455 7_455 ?
O13 Rb2 O16 153.9(3) . 7_455 ?
O13 Rb2 O16 154.0(3) 7_455 . ?
O13 Rb2 O16 81.4(3) . . ?
O16 Rb2 O7 55.1(3) 10_556 . ?
O16 Rb2 O7 100.5(3) 10_556 7_455 ?
O16 Rb2 O7 100.5(3) 16_565 . ?
O16 Rb2 O7 55.1(3) 16_565 7_455 ?
O16 Rb2 O9B 73.0(4) 16_565 . ?
O16 Rb2 O9B 106.4(4) 16_565 7_455 ?
O16 Rb2 O9B 106.4(4) 10_556 . ?
O16 Rb2 O9B 73.0(4) 10_556 7_455 ?
O16 Rb2 O12B 130.9(6) 16_565 7_455 ?
O16 Rb2 O12B 130.9(6) 10_556 . ?
O16 Rb2 O12B 107.0(5) 16_565 . ?
O16 Rb2 O12B 107.0(5) 10_556 7_455 ?
O16 Rb2 O13 152.0(3) 10_556 7_455 ?
O16 Rb2 O13 152.0(3) 16_565 . ?
O16 Rb2 O13 88.5(3) 16_565 7_455 ?
O16 Rb2 O13 88.5(3) 10_556 . ?
O16 Rb2 O16 109.4(4) 7_455 . ?
O16 Rb2 O16 97.3(5) 10_556 16_565 ?
O16 Rb2 O16 103.2(4) 10_556 7_455 ?
O16 Rb2 O16 103.2(4) 16_565 . ?
O16 Rb2 O16 7.1(4) 16_565 7_455 ?
O16 Rb2 O16 7.1(4) 10_556 . ?
O5A Rb3 O5A 51.4(5) 12_656 3_655 ?
O5A Rb3 O5B 16.6(4) 12_656 12_656 ?
O5A Rb3 O5B 16.6(4) 3_655 3_655 ?
O5A Rb3 O5B 54.4(4) 12_656 3_655 ?
O5A Rb3 O5B 54.4(4) 3_655 12_656 ?
O5A Rb3 O8 136.2(4) 3_655 . ?
O5A Rb3 O8 128.7(4) 12_656 . ?
O5A Rb3 O8 128.7(4) 3_655 10_556 ?
O5A Rb3 O8 136.2(4) 12_656 10_556 ?
O5A Rb3 O10B 155.8(4) 12_656 10_556 ?
O5A Rb3 O10B 155.8(4) 3_655 . ?
O5A Rb3 O10B 141.4(3) 12_656 . ?
O5A Rb3 O10B 141.4(3) 3_655 10_556 ?
O5A Rb3 O11A 140.1(5) 3_655 . ?
O5A Rb3 O11A 91.7(5) 3_655 10_556 ?
O5A Rb3 O11A 91.7(5) 12_656 . ?
O5A Rb3 O11A 140.1(5) 12_656 10_556 ?
O5A Rb3 O11B 144.5(4) 12_656 10_556 ?
O5A Rb3 O11B 96.0(4) 12_656 . ?
O5A Rb3 O11B 144.5(4) 3_655 . ?
O5A Rb3 O11B 96.0(4) 3_655 10_556 ?
O5B Rb3 O5B 51.3(5) 12_656 3_655 ?
O5B Rb3 O11B 90.3(5) 3_655 10_556 ?
O5B Rb3 O11B 135.4(5) 12_656 10_556 ?
O5B Rb3 O11B 90.3(5) 12_656 . ?
O5B Rb3 O11B 135.4(5) 3_655 . ?
O8 Rb3 O5B 141.1(4) 10_556 3_655 ?
O8 Rb3 O5B 141.1(4) . 12_656 ?
O8 Rb3 O5B 151.0(4) . 3_655 ?
O8 Rb3 O5B 151.0(4) 10_556 12_656 ?
O8 Rb3 O8 12.7(6) 10_556 . ?
O8 Rb3 O11B 72.9(5) . . ?
O8 Rb3 O11B 83.5(5) 10_556 . ?
O8 Rb3 O11B 83.5(5) . 10_556 ?
O8 Rb3 O11B 72.9(5) 10_556 10_556 ?
O10B Rb3 O5B 141.4(4) . 3_655 ?
O10B Rb3 O5B 130.6(4) 10_556 3_655 ?
O10B Rb3 O5B 130.6(4) . 12_656 ?
O10B Rb3 O5B 141.4(4) 10_556 12_656 ?
O10B Rb3 O8 58.7(3) . . ?
O10B Rb3 O8 60.9(3) 10_556 . ?
O10B Rb3 O8 60.9(3) . 10_556 ?
O10B Rb3 O8 58.7(3) 10_556 10_556 ?
O10B Rb3 O10B 17.3(4) . 10_556 ?
O10B Rb3 O11B 63.9(4) 10_556 . ?
O10B Rb3 O11B 63.9(4) . 10_556 ?
O10B Rb3 O11B 46.8(4) 10_556 10_556 ?
O10B Rb3 O11B 46.8(4) . . ?
O11A Rb3 O5B 85.9(5) . 12_656 ?
O11A Rb3 O5B 131.6(5) 10_556 12_656 ?
O11A Rb3 O5B 131.6(5) . 3_655 ?
O11A Rb3 O5B 85.9(5) 10_556 3_655 ?
O11A Rb3 O8 76.3(6) . . ?
O11A Rb3 O8 76.3(6) 10_556 10_556 ?
O11A Rb3 O8 87.2(6) . 10_556 ?
O11A Rb3 O8 87.2(6) 10_556 . ?
O11A Rb3 O10B 50.8(5) 10_556 10_556 ?
O11A Rb3 O10B 50.8(5) . . ?
O11A Rb3 O10B 67.9(5) . 10_556 ?
O11A Rb3 O10B 67.9(5) 10_556 . ?
O11A Rb3 O11A 116.2(9) . 10_556 ?
O11A Rb3 O11B 4.4(7) 10_556 10_556 ?
O11A Rb3 O11B 4.4(7) . . ?
O11A Rb3 O11B 112.9(4) . 10_556 ?
O11A Rb3 O11B 112.9(4) 10_556 . ?
O11B Rb3 O11B 109.5(7) 10_556 . ?
Rb4A Rb4A U2 77.90(12) 10_556 . ?
Rb4A Rb4A P3A 108.7(3) 10_556 . ?
Rb4A Rb4A P3B 105.0(2) 10_556 . ?
Rb4A Rb4A O2 73.20(19) 10_556 . ?
Rb4A Rb4A O3 100.0(2) 10_556 . ?
Rb4A Rb4A O6A 52.9(6) 10_556 10_556 ?
Rb4A Rb4A O6A 98.0(6) 10_556 . ?
Rb4A Rb4A O6B 104.7(5) 10_556 . ?
Rb4A Rb4A O8 68.2(3) 10_556 10_556 ?
Rb4A Rb4A O8 80.3(4) 10_556 . ?
Rb4B Rb4A U2 79.8(19) . . ?
Rb4B Rb4A Rb4A 6(2) . 10_556 ?
Rb4B Rb4A P3A 114(2) . . ?
Rb4B Rb4A P3B 110(2) . . ?
Rb4B Rb4A O2 77.0(17) . . ?
Rb4B Rb4A O3 106(2) . . ?
Rb4B Rb4A O6A 57(2) . 10_556 ?
Rb4B Rb4A O6A 102(2) . . ?
Rb4B Rb4A O6B 109(2) . . ?
Rb4B Rb4A O8 79.7(17) . . ?
Rb4B Rb4A O8 67.7(17) . 10_556 ?
P3A Rb4A U2 55.8(2) . . ?
P3A Rb4A P3B 3.9(3) . . ?
P3B Rb4A U2 54.9(2) . . ?
O2 Rb4A U2 112.7(3) . . ?
O2 Rb4A P3A 78.5(3) . . ?
O2 Rb4A P3B 76.2(3) . . ?
O2 Rb4A O3 53.8(3) . . ?
O2 Rb4A O6A 82.2(7) . 10_556 ?
O2 Rb4A O6B 97.2(7) . . ?
O2 Rb4A O8 135.6(4) . . ?
O2 Rb4A O8 127.8(4) . 10_556 ?
O3 Rb4A U2 74.16(19) . . ?
O3 Rb4A P3A 24.8(3) . . ?
O3 Rb4A P3B 23.0(2) . . ?
O3 Rb4A O6A 63.6(7) . 10_556 ?
O6A Rb4A U2 33.9(6) 10_556 . ?
O6A Rb4A U2 32.4(7) . . ?
O6A Rb4A P3A 59.5(7) 10_556 . ?
O6A Rb4A P3A 23.6(7) . . ?
O6A Rb4A P3B 56.3(7) 10_556 . ?
O6A Rb4A P3B 23.3(8) . . ?
O6A Rb4A O2 95.1(9) . . ?
O6A Rb4A O3 45.2(8) . . ?
O6A Rb4A O6A 45.1(12) . 10_556 ?
O6A Rb4A O6B 6.7(10) . . ?
O6A Rb4A O8 53.9(8) . . ?
O6A Rb4A O8 58.3(8) . 10_556 ?
O6B Rb4A U2 36.7(6) . . ?
O6B Rb4A P3A 21.5(6) . . ?
O6B Rb4A P3B 22.2(6) . . ?
O6B Rb4A O3 45.2(6) . . ?
O6B Rb4A O6A 51.8(5) . 10_556 ?
O6B Rb4A O8 61.8(6) . 10_556 ?
O8 Rb4A U2 26.3(3) 10_556 . ?
O8 Rb4A U2 25.2(3) . . ?
O8 Rb4A P3A 81.9(4) 10_556 . ?
O8 Rb4A P3A 77.2(4) . . ?
O8 Rb4A P3B 81.1(3) 10_556 . ?
O8 Rb4A P3B 77.2(4) . . ?
O8 Rb4A O3 98.4(3) . . ?
O8 Rb4A O3 100.0(3) 10_556 . ?
O8 Rb4A O6A 53.5(7) . 10_556 ?
O8 Rb4A O6A 46.5(7) 10_556 10_556 ?
O8 Rb4A O6B 56.0(6) . . ?
O8 Rb4A O8 12.1(6) . 10_556 ?
Rb4A Rb4B U2 88.1(19) . . ?
Rb4A Rb4B U2 88.1(19) 10_556 . ?
Rb4A Rb4B Rb4A 169(4) . 10_556 ?
Rb4A Rb4B P3A 54.8(19) . . ?
Rb4A Rb4B P3A 115(2) 10_556 . ?
Rb4A Rb4B P3A 54.8(19) 10_556 10_556 ?
Rb4A Rb4B P3A 115(2) . 10_556 ?
Rb4A Rb4B O2 86.1(17) 10_556 . ?
Rb4A Rb4B O2 86.1(17) . . ?
Rb4A Rb4B O6A 110(2) 10_556 . ?
Rb4A Rb4B O6A 110(2) . 10_556 ?
Rb4A Rb4B O6A 62(2) . . ?
Rb4A Rb4B O6A 62(2) 10_556 10_556 ?
Rb4A Rb4B O6B 58.1(19) . . ?
Rb4A Rb4B O6B 114(2) . 10_556 ?
Rb4A Rb4B O6B 114(2) 10_556 . ?
Rb4A Rb4B O6B 58.1(19) 10_556 10_556 ?
Rb4A Rb4B O8 97.0(18) 10_556 . ?
Rb4A Rb4B O8 97.0(18) . 10_556 ?
Rb4A Rb4B O8 84.0(17) . . ?
Rb4A Rb4B O8 84.0(17) 10_556 10_556 ?
P3A Rb4B U2 53.6(4) 10_556 . ?
P3A Rb4B U2 53.6(4) . . ?
P3A Rb4B P3A 60.1(6) 10_556 . ?
O2 Rb4B U2 116.1(9) . . ?
O2 Rb4B P3A 72.3(6) . 10_556 ?
O2 Rb4B P3A 72.3(6) . . ?
O2 Rb4B O6A 90.4(10) . 10_556 ?
O2 Rb4B O6A 90.4(10) . . ?
O2 Rb4B O6B 90.8(9) . . ?
O2 Rb4B O6B 90.8(9) . 10_556 ?
O2 Rb4B O8 140.8(11) . . ?
O2 Rb4B O8 140.8(11) . 10_556 ?
O6A Rb4B U2 34.3(7) . . ?
O6A Rb4B U2 34.3(7) 10_556 . ?
O6A Rb4B P3A 19.8(7) 10_556 10_556 ?
O6A Rb4B P3A 57.4(8) 10_556 . ?
O6A Rb4B P3A 19.8(7) . . ?
O6A Rb4B P3A 57.4(8) . 10_556 ?
O6A Rb4B O6A 47.4(13) . 10_556 ?
O6A Rb4B O6B 51.7(6) . 10_556 ?
O6A Rb4B O6B 4.3(10) 10_556 10_556 ?
O6A Rb4B O6B 4.3(10) . . ?
O6A Rb4B O6B 51.7(6) 10_556 . ?
O6B Rb4B U2 36.9(6) . . ?
O6B Rb4B U2 37.0(6) 10_556 . ?
O6B Rb4B P3A 18.9(6) . . ?
O6B Rb4B P3A 61.6(7) 10_556 . ?
O6B Rb4B P3A 18.9(6) 10_556 10_556 ?
O6B Rb4B P3A 61.6(7) . 10_556 ?
O6B Rb4B O6B 56.0(11) . 10_556 ?
O8 Rb4B U2 25.9(4) . . ?
O8 Rb4B U2 25.9(4) 10_556 . ?
O8 Rb4B P3A 71.0(6) 10_556 10_556 ?
O8 Rb4B P3A 71.0(6) . . ?
O8 Rb4B P3A 77.8(6) 10_556 . ?
O8 Rb4B P3A 77.8(6) . 10_556 ?
O8 Rb4B O6A 51.6(8) 10_556 10_556 ?
O8 Rb4B O6A 51.6(8) . . ?
O8 Rb4B O6A 58.0(9) 10_556 . ?
O8 Rb4B O6A 58.0(9) . 10_556 ?
O8 Rb4B O6B 52.1(7) 10_556 10_556 ?
O8 Rb4B O6B 59.5(7) . 10_556 ?
O8 Rb4B O6B 52.1(7) . . ?
O8 Rb4B O6B 59.5(7) 10_556 . ?
O8 Rb4B O8 13.0(6) . 10_556 ?
Rb5B Rb5A Rb5B 58(3) 7_456 . ?
Rb5B Rb5A Rb5C 29.2(15) 7_456 . ?
Rb5B Rb5A Rb5C 29.2(15) . . ?
Rb5B Rb5A O1 87.6(18) . 7_456 ?
Rb5B Rb5A O1 82.4(17) . . ?
Rb5B Rb5A O1 87.6(18) 7_456 . ?
Rb5B Rb5A O1 82.4(17) 7_456 7_456 ?
Rb5B Rb5A O11A 109.4(12) 7_456 5_556 ?
Rb5B Rb5A O11A 66.5(12) . 5_556 ?
Rb5B Rb5A O11A 109.4(12) . 4_565 ?
Rb5B Rb5A O11A 66.5(13) 7_456 4_565 ?
Rb5B Rb5A O11B 114.1(13) 7_456 5_556 ?
Rb5B Rb5A O11B 74.8(13) . 5_556 ?
Rb5B Rb5A O14 96.0(17) 7_456 11_567 ?
Rb5B Rb5A O14 96.0(17) . 5_556 ?
Rb5B Rb5A O14 148.1(19) 7_456 5_556 ?
Rb5B Rb5A O14 148.1(19) . 11_567 ?
Rb5B Rb5A O17 19.8(18) 7_456 7_456 ?
Rb5B Rb5A O17 19.8(18) . . ?
Rb5B Rb5A O17 66.3(18) . 7_456 ?
Rb5B Rb5A O17 66.3(18) 7_456 . ?
Rb5C Rb5A O1 84.3(2) . . ?
Rb5C Rb5A O1 84.3(2) . 7_456 ?
Rb5C Rb5A O11A 87.8(4) . 5_556 ?
Rb5C Rb5A O11A 87.8(4) . 4_565 ?
Rb5C Rb5A O11B 94.8(4) . 5_556 ?
Rb5C Rb5A O14 123.12(19) . 11_567 ?
Rb5C Rb5A O14 123.12(19) . 5_556 ?
Rb5C Rb5A O17 39.7(3) . . ?
Rb5C Rb5A O17 39.7(3) . 7_456 ?
O1 Rb5A O1 168.6(5) 7_456 . ?
O1 Rb5A O11A 53.8(4) . 4_565 ?
O1 Rb5A O11A 53.8(4) 7_456 5_556 ?
O1 Rb5A O11A 125.6(4) . 5_556 ?
O1 Rb5A O11A 125.6(4) 7_456 4_565 ?
O1 Rb5A O11B 131.2(3) . 5_556 ?
O1 Rb5A O11B 50.0(3) 7_456 5_556 ?
O1 Rb5A O14 68.9(2) . 5_556 ?
O1 Rb5A O14 118.0(3) . 11_567 ?
O1 Rb5A O14 68.9(2) 7_456 11_567 ?
O1 Rb5A O14 118.0(3) 7_456 5_556 ?
O1 Rb5A O17 107.1(4) 7_456 . ?
O1 Rb5A O17 63.5(4) . . ?
O1 Rb5A O17 107.1(4) . 7_456 ?
O1 Rb5A O17 63.5(4) 7_456 7_456 ?
O11A Rb5A O11A 175.6(7) 5_556 4_565 ?
O11A Rb5A O11B 8.5(3) 5_556 5_556 ?
O11A Rb5A O11B 174.5(5) 4_565 5_556 ?
O14 Rb5A O11A 71.3(4) 5_556 5_556 ?
O14 Rb5A O11A 111.2(4) 11_567 5_556 ?
O14 Rb5A O11A 111.2(4) 5_556 4_565 ?
O14 Rb5A O11A 71.3(4) 11_567 4_565 ?
O14 Rb5A O11B 71.4(4) 5_556 5_556 ?
O14 Rb5A O11B 103.2(4) 11_567 5_556 ?
O14 Rb5A O14 113.8(4) 11_567 5_556 ?
O17 Rb5A O11A 76.7(5) . 5_556 ?
O17 Rb5A O11A 99.8(5) . 4_565 ?
O17 Rb5A O11A 76.7(4) 7_456 4_565 ?
O17 Rb5A O11A 99.8(5) 7_456 5_556 ?
O17 Rb5A O11B 102.3(5) 7_456 5_556 ?
O17 Rb5A O11B 85.2(4) . 5_556 ?
O17 Rb5A O14 83.6(4) . 5_556 ?
O17 Rb5A O14 162.3(4) . 11_567 ?
O17 Rb5A O14 83.6(4) 7_456 11_567 ?
O17 Rb5A O14 162.3(4) 7_456 5_556 ?
O17 Rb5A O17 79.4(6) 7_456 . ?
Rb5A Rb5B O1 77(2) . 7_456 ?
Rb5A Rb5B O1 81.6(13) . . ?
Rb5A Rb5B O3 130(2) . 16_566 ?
Rb5A Rb5B O11A 100.4(15) . 5_556 ?
Rb5A Rb5B O11B 92.3(14) . 5_556 ?
Rb5A Rb5B O14 69.7(13) . 5_556 ?
Rb5A Rb5B O17 138(2) . 10_556 ?
Rb5A Rb5B O17 153(2) . . ?
Rb5A Rb5B O17 98(2) . 7_456 ?
Rb5B Rb5B Rb5A 60.8(15) 7_456 . ?
Rb5B Rb5B O1 77(4) 7_456 7_456 ?
Rb5B Rb5B O1 88(3) 7_456 . ?
Rb5B Rb5B O3 111(3) 7_456 16_566 ?
Rb5B Rb5B O11A 133(4) 7_456 5_556 ?
Rb5B Rb5B O11B 127(4) 7_456 5_556 ?
Rb5B Rb5B O14 126.7(12) 7_456 5_556 ?
Rb5B Rb5B O17 130(3) 7_456 10_556 ?
Rb5B Rb5B O17 124.0(18) 7_456 . ?
Rb5B Rb5B O17 42(2) 7_456 7_456 ?
Rb5C Rb5B Rb5A 100(8) . . ?
Rb5C Rb5B Rb5B 40(7) . 7_456 ?
Rb5C Rb5B O1 85(4) . 7_456 ?
Rb5C Rb5B O1 93(2) . . ?
Rb5C Rb5B O3 86(3) . 16_566 ?
Rb5C Rb5B O11A 130(2) . 5_556 ?
Rb5C Rb5B O11B 130(2) . 5_556 ?
Rb5C Rb5B O14 158(3) . 5_556 ?
Rb5C Rb5B O17 20(3) . 7_456 ?
Rb5C Rb5B O17 100(7) . 10_556 ?
Rb5C Rb5B O17 89(7) . . ?
O1 Rb5B O1 157.5(13) . 7_456 ?
O1 Rb5B O3 54.4(4) 7_456 16_566 ?
O1 Rb5B O3 148.1(13) . 16_566 ?
O1 Rb5B O11A 56.1(5) 7_456 5_556 ?
O1 Rb5B O11A 135.0(10) . 5_556 ?
O1 Rb5B O11B 51.2(5) 7_456 5_556 ?
O1 Rb5B O11B 136.3(8) . 5_556 ?
O1 Rb5B O14 66.2(5) . 5_556 ?
O1 Rb5B O14 110.3(7) 7_456 5_556 ?
O1 Rb5B O17 141.0(9) 7_456 10_556 ?
O1 Rb5B O17 61.4(7) . 10_556 ?
O3 Rb5B O11B 50.6(4) 16_566 5_556 ?
O11A Rb5B O3 45.8(5) 5_556 16_566 ?
O11A Rb5B O11B 8.3(4) 5_556 5_556 ?
O14 Rb5B O3 115.1(6) 5_556 16_566 ?
O14 Rb5B O11A 72.4(6) 5_556 5_556 ?
O14 Rb5B O11B 71.0(5) 5_556 5_556 ?
O17 Rb5B O1 72.5(9) . . ?
O17 Rb5B O1 113.2(7) 7_456 . ?
O17 Rb5B O1 65.1(7) 7_456 7_456 ?
O17 Rb5B O1 129.8(9) . 7_456 ?
O17 Rb5B O3 72.4(5) 7_456 16_566 ?
O17 Rb5B O3 87.2(8) 10_556 16_566 ?
O17 Rb5B O3 75.6(8) . 16_566 ?
O17 Rb5B O11A 93.9(9) 10_556 5_556 ?
O17 Rb5B O11A 111.1(8) 7_456 5_556 ?
O17 Rb5B O11A 92.8(10) . 5_556 ?
O17 Rb5B O11B 110.5(8) 7_456 5_556 ?
O17 Rb5B O11B 101.0(10) . 5_556 ?
O17 Rb5B O11B 101.4(9) 10_556 5_556 ?
O17 Rb5B O14 92.5(11) . 5_556 ?
O17 Rb5B O14 78.0(8) 10_556 5_556 ?
O17 Rb5B O14 167.5(14) 7_456 5_556 ?
O17 Rb5B O17 15.6(5) . 10_556 ?
O17 Rb5B O17 99.3(10) . 7_456 ?
O17 Rb5B O17 113.2(10) 7_456 10_556 ?
Rb5A Rb5C O1 75.5(7) . . ?
Rb5A Rb5C O1 75.5(7) . 7_456 ?
Rb5A Rb5C O4A 157.9(4) . 10_556 ?
Rb5A Rb5C O4B 151.7(5) . 10_556 ?
Rb5A Rb5C O4B 151.7(5) . 16_566 ?
Rb5A Rb5C O17 123.0(9) . . ?
Rb5A Rb5C O17 123.0(9) . 7_456 ?
Rb5A Rb5C O17 112.2(7) . 10_556 ?
Rb5A Rb5C O17 112.2(7) . 16_566 ?
Rb5B Rb5C Rb5A 50(7) 7_456 . ?
Rb5B Rb5C Rb5A 50(7) . . ?
Rb5B Rb5C Rb5B 101(10) 7_456 . ?
Rb5B Rb5C O1 85(4) . 7_456 ?
Rb5B Rb5C O1 85(4) 7_456 . ?
Rb5B Rb5C O1 77(2) 7_456 7_456 ?
Rb5B Rb5C O1 77(2) . . ?
Rb5B Rb5C O4A 136(7) . 10_556 ?
Rb5B Rb5C O4A 118(5) 7_456 10_556 ?
Rb5B Rb5C O4B 123(7) . 10_556 ?
Rb5B Rb5C O4B 123(7) 7_456 16_566 ?
Rb5B Rb5C O4B 125(5) . 16_566 ?
Rb5B Rb5C O4B 125(5) 7_456 10_556 ?
Rb5B Rb5C O17 144(4) . 16_566 ?
Rb5B Rb5C O17 71(6) 7_456 16_566 ?
Rb5B Rb5C O17 71(6) . 10_556 ?
Rb5B Rb5C O17 78(6) . . ?
Rb5B Rb5C O17 144(4) 7_456 10_556 ?
Rb5B Rb5C O17 78(6) 7_456 7_456 ?
Rb5B Rb5C O17 155(3) . 7_456 ?
Rb5B Rb5C O17 155(3) 7_456 . ?
O1 Rb5C O1 151.0(14) 7_456 . ?
O1 Rb5C O4A 122.9(9) 7_456 10_556 ?
O1 Rb5C O4A 85.5(6) . 10_556 ?
O1 Rb5C O4B 132.8(11) 7_456 10_556 ?
O1 Rb5C O4B 76.2(6) 7_456 16_566 ?
O1 Rb5C O4B 76.2(6) . 10_556 ?
O1 Rb5C O4B 132.8(11) . 16_566 ?
O1 Rb5C O17 134.7(4) 7_456 10_556 ?
O1 Rb5C O17 134.6(4) . 16_566 ?
O1 Rb5C O17 59.1(3) . 10_556 ?
O1 Rb5C O17 59.1(3) 7_456 16_566 ?
O4B Rb5C O4A 13.5(4) 10_556 10_556 ?
O4B Rb5C O4A 48.7(7) 16_566 10_556 ?
O4B Rb5C O4B 56.6(9) 10_556 16_566 ?
O17 Rb5C O1 127.5(6) . 7_456 ?
O17 Rb5C O1 70.4(4) 7_456 7_456 ?
O17 Rb5C O1 70.4(4) . . ?
O17 Rb5C O1 127.5(6) 7_456 . ?
O17 Rb5C O4A 73.7(8) 16_566 10_556 ?
O17 Rb5C O4A 65.2(7) 10_556 10_556 ?
O17 Rb5C O4A 61.2(9) 7_456 10_556 ?
O17 Rb5C O4A 58.1(9) . 10_556 ?
O17 Rb5C O4B 87.1(9) 10_556 16_566 ?
O17 Rb5C O4B 45.9(8) 7_456 16_566 ?
O17 Rb5C O4B 45.9(8) . 10_556 ?
O17 Rb5C O4B 52.1(6) 16_566 16_566 ?
O17 Rb5C O4B 74.7(11) . 16_566 ?
O17 Rb5C O4B 52.1(6) 10_556 10_556 ?
O17 Rb5C O4B 87.1(9) 16_566 10_556 ?
O17 Rb5C O4B 74.7(11) 7_456 10_556 ?
O17 Rb5C O17 12.6(4) 7_456 16_566 ?
O17 Rb5C O17 12.6(4) . 10_556 ?
O17 Rb5C O17 124.4(15) 7_456 10_556 ?
O17 Rb5C O17 135.7(14) 10_556 16_566 ?
O17 Rb5C O17 113.9(18) 7_456 . ?
O17 Rb5C O17 124.4(15) . 16_566 ?
O2 Rb6 O6B 112.0(5) 3_654 10 ?
O2 Rb6 O9A 76.2(4) 3_654 . ?
O2 Rb6 O9A 76.2(4) 3_654 10 ?
O2 Rb6 O16 148.5(3) 3_654 7_455 ?
O2 Rb6 O16 148.5(3) 3_654 16_565 ?
O5A Rb6 O2 142.7(3) 10 3_654 ?
O5A Rb6 O2 142.7(3) . 3_654 ?
O5A Rb6 O5A 51.5(5) . 10 ?
O5A Rb6 O6B 92.0(6) . 10 ?
O5A Rb6 O6B 40.6(6) 10 10 ?
O5A Rb6 O9A 90.2(4) . . ?
O5A Rb6 O9A 138.9(5) 10 . ?
O5A Rb6 O9A 90.2(4) 10 10 ?
O5A Rb6 O9A 138.9(5) . 10 ?
O5A Rb6 O9B 132.4(4) . 10 ?
O5A Rb6 O9B 88.7(4) . . ?
O5A Rb6 O9B 88.7(4) 10 10 ?
O5A Rb6 O9B 132.4(4) 10 . ?
O5A Rb6 O10A 132.8(4) 10 10 ?
O5A Rb6 O10A 132.7(4) . . ?
O5A Rb6 O10A 148.3(4) 10 . ?
O5A Rb6 O10A 148.3(4) . 10 ?
O5A Rb6 O16 59.8(4) . 16_565 ?
O5A Rb6 O16 65.2(4) . 7_455 ?
O5A Rb6 O16 65.2(4) 10 16_565 ?
O5A Rb6 O16 59.8(4) 10 7_455 ?
O9A Rb6 O6B 50.8(6) 10 10 ?
O9A Rb6 O6B 161.0(7) . 10 ?
O9A Rb6 O9A 119.2(8) . 10 ?
O9B Rb6 O2 84.5(3) . 3_654 ?
O9B Rb6 O2 84.5(3) 10 3_654 ?
O9B Rb6 O6B 149.0(7) . 10 ?
O9B Rb6 O6B 52.6(6) 10 10 ?
O9B Rb6 O9A 113.8(5) 10 . ?
O9B Rb6 O9A 12.3(4) . . ?
O9B Rb6 O9A 12.3(4) 10 10 ?
O9B Rb6 O9A 113.8(5) . 10 ?
O9B Rb6 O9B 106.4(7) 10 . ?
O9B Rb6 O16 72.7(4) . 16_565 ?
O9B Rb6 O16 81.6(4) 10 16_565 ?
O9B Rb6 O16 72.7(4) 10 7_455 ?
O9B Rb6 O16 81.6(4) . 7_455 ?
O10A Rb6 O2 58.7(3) 10 3_654 ?
O10A Rb6 O2 58.7(3) . 3_654 ?
O10A Rb6 O6B 98.0(6) 10 10 ?
O10A Rb6 O6B 120.1(6) . 10 ?
O10A Rb6 O9A 48.2(4) 10 10 ?
O10A Rb6 O9A 71.1(4) . 10 ?
O10A Rb6 O9A 48.2(4) . . ?
O10A Rb6 O9A 71.1(4) 10 . ?
O10A Rb6 O9B 67.5(4) . 10 ?
O10A Rb6 O9B 45.6(4) . . ?
O10A Rb6 O9B 67.5(4) 10 . ?
O10A Rb6 O9B 45.6(4) 10 10 ?
O10A Rb6 O10A 22.9(5) . 10 ?
O10A Rb6 O16 92.1(3) . 7_455 ?
O10A Rb6 O16 89.9(3) . 16_565 ?
O10A Rb6 O16 89.9(3) 10 7_455 ?
O10A Rb6 O16 92.1(3) 10 16_565 ?
O16 Rb6 O6B 81.0(6) 16_565 10 ?
O16 Rb6 O6B 70.8(6) 7_455 10 ?
O16 Rb6 O9A 83.9(5) 7_455 10 ?
O16 Rb6 O9A 93.3(5) 7_455 . ?
O16 Rb6 O9A 83.9(5) 16_565 . ?
O16 Rb6 O9A 93.3(5) 16_565 10 ?
O16 Rb6 O16 10.9(5) 16_565 7_455 ?
Rb1 P1 Rb1 97.65(3) 7_455 15_666 ?
Rb1 P1 Rb1 111.26(4) 7_455 9_565 ?
Rb1 P1 Rb1 97.66(3) 9_565 . ?
Rb1 P1 Rb1 120.27(4) 9_565 15_666 ?
Rb1 P1 Rb1 111.26(4) 15_666 . ?
Rb1 P1 Rb1 120.27(4) 7_455 . ?
O15A P1 Rb1 85.5(8) . . ?
O15A P1 Rb1 85.5(8) 8 15_666 ?
O15A P1 Rb1 65.1(10) 8 . ?
O15A P1 Rb1 171.6(9) 8 7_455 ?
O15A P1 Rb1 60.7(8) 2_565 15_666 ?
O15A P1 Rb1 65.1(10) 2_565 7_455 ?
O15A P1 Rb1 171.6(9) 2_565 . ?
O15A P1 Rb1 60.7(8) . 7_455 ?
O15A P1 Rb1 171.6(9) 7_455 15_666 ?
O15A P1 Rb1 60.7(8) 8 9_565 ?
O15A P1 Rb1 65.1(10) . 15_666 ?
O15A P1 Rb1 65.1(10) 7_455 9_565 ?
O15A P1 Rb1 60.7(8) 7_455 . ?
O15A P1 Rb1 85.5(8) 2_565 9_565 ?
O15A P1 Rb1 171.6(9) . 9_565 ?
O15A P1 Rb1 85.5(8) 7_455 7_455 ?
O15A P1 O15A 92.4(16) 8 7_455 ?
O15A P1 O15A 127.5(16) 7_455 2_565 ?
O15A P1 O15A 110(2) 8 2_565 ?
O15A P1 O15A 110(2) 7_455 . ?
O15A P1 O15A 92.4(16) 2_565 . ?
O15A P1 O15A 127.5(16) 8 . ?
O15A P1 O15B 19.2(10) 8 8 ?
O15A P1 O15B 107.3(12) . 2_565 ?
O15A P1 O15B 19.2(10) 2_565 2_565 ?
O15A P1 O15B 19.2(10) . . ?
O15A P1 O15B 109.6(12) . 8 ?
O15A P1 O15B 19.2(10) 7_455 7_455 ?
O15A P1 O15B 107.3(12) 7_455 8 ?
O15A P1 O15B 108.1(10) 8 2_565 ?
O15A P1 O15B 108.1(10) 7_455 . ?
O15A P1 O15B 108.1(10) 2_565 8 ?
O15A P1 O15B 107.3(12) 2_565 . ?
O15A P1 O15B 109.6(12) 7_455 2_565 ?
O15A P1 O15B 109.6(12) 2_565 7_455 ?
O15A P1 O15B 108.1(10) . 7_455 ?
O15A P1 O15B 109.6(12) 8 . ?
O15A P1 O15B 107.3(12) 8 7_455 ?
O15B P1 Rb1 78.7(10) 2_565 15_666 ?
O15B P1 Rb1 69.1(9) . . ?
O15B P1 Rb1 166.5(8) . 9_565 ?
O15B P1 Rb1 166.5(8) 7_455 15_666 ?
O15B P1 Rb1 78.7(10) 7_455 . ?
O15B P1 Rb1 78.7(10) 8 9_565 ?
O15B P1 Rb1 69.1(9) 8 15_666 ?
O15B P1 Rb1 69.1(9) 2_565 9_565 ?
O15B P1 Rb1 65.2(14) 8 . ?
O15B P1 Rb1 65.2(14) 7_455 9_565 ?
O15B P1 Rb1 69.1(9) 7_455 7_455 ?
O15B P1 Rb1 78.7(10) . 7_455 ?
O15B P1 Rb1 65.2(14) . 15_666 ?
O15B P1 Rb1 166.5(8) 8 7_455 ?
O15B P1 Rb1 65.2(14) 2_565 7_455 ?
O15B P1 Rb1 166.5(8) 2_565 . ?
O15B P1 O15B 113(3) . 7_455 ?
O15B P1 O15B 113(3) 8 2_565 ?
O15B P1 O15B 124.3(18) . 2_565 ?
O15B P1 O15B 124.3(18) 8 7_455 ?
O15B P1 O15B 93(2) . 8 ?
O15B P1 O15B 93(2) 2_565 7_455 ?
U1 P2A Rb1 77.45(18) 3_654 . ?
U1 P2A Rb6 74.4(2) 3_654 . ?
Rb1 P2A Rb6 101.0(2) . . ?
P2B P2A U1 156.7(9) . 3_654 ?
P2B P2A Rb1 101.7(8) . . ?
P2B P2A Rb6 127.9(9) . . ?
P2B P2A O9A 72.9(12) . . ?
P2B P2A O9B 74.0(10) . . ?
P2B P2A O10A 145.0(11) . . ?
P2B P2A O10B 26.5(8) . . ?
P2B P2A O11A 108.2(13) . . ?
P2B P2A O11B 119.7(16) . . ?
P2B P2A O12A 45.8(15) . . ?
P2B P2A O12B 51.1(12) . . ?
O9A P2A U1 122.0(9) . 3_654 ?
O9A P2A Rb1 142.1(10) . . ?
O9A P2A Rb6 60.7(9) . . ?
O9A P2A O9B 25.8(8) . . ?
O9A P2A O10A 110.7(11) . . ?
O9A P2A O10B 67.3(10) . . ?
O9A P2A O11A 109.9(14) . . ?
O9A P2A O12A 113.6(16) . . ?
O9A P2A O12B 110.9(13) . . ?
O9B P2A U1 127.7(7) . 3_654 ?
O9B P2A Rb1 116.4(7) . . ?
O9B P2A Rb6 53.9(7) . . ?
O9B P2A O10B 80.1(9) . . ?
O9B P2A O12B 94.6(11) . . ?
O10A P2A U1 51.5(6) . 3_654 ?
O10A P2A Rb1 53.1(5) . . ?
O10A P2A Rb6 51.5(5) . . ?
O10A P2A O9B 94.8(9) . . ?
O10A P2A O10B 171.1(7) . . ?
O10A P2A O12B 98.5(11) . . ?
O10B P2A U1 137.2(4) . 3_654 ?
O10B P2A Rb1 122.8(4) . . ?
O10B P2A Rb6 127.9(4) . . ?
O11A P2A U1 51.6(9) . 3_654 ?
O11A P2A Rb1 107.3(10) . . ?
O11A P2A Rb6 108.7(10) . . ?
O11A P2A O9B 135.0(12) . . ?
O11A P2A O10A 103.1(12) . . ?
O11A P2A O10B 85.6(10) . . ?
O11A P2A O12A 111.1(15) . . ?
O11A P2A O12B 122.5(13) . . ?
O11B P2A U1 38.5(12) . 3_654 ?
O11B P2A Rb1 95.4(13) . . ?
O11B P2A Rb6 104.0(14) . . ?
O11B P2A O9A 120.2(17) . . ?
O11B P2A O9B 143.0(15) . . ?
O11B P2A O10A 89.4(15) . . ?
O11B P2A O10B 99.0(12) . . ?
O11B P2A O11A 14.5(15) . . ?
O11B P2A O12A 111.8(18) . . ?
O11B P2A O12B 121.2(17) . . ?
O12A P2A U1 124.4(13) . 3_654 ?
O12A P2A Rb1 56.8(13) . . ?
O12A P2A Rb6 138.7(11) . . ?
O12A P2A O9B 101.8(14) . . ?
O12A P2A O10A 107.9(14) . . ?
O12A P2A O10B 66.5(14) . . ?
O12A P2A O12B 12.7(16) . . ?
O12B P2A U1 125.2(10) . 3_654 ?
O12B P2A Rb1 50.8(10) . . ?
O12B P2A Rb6 126.2(9) . . ?
O12B P2A O10B 74.9(11) . . ?
U2 P2B Rb2 75.60(15) . . ?
U3 P2B U2 91.1(3) . . ?
U3 P2B Rb2 80.2(2) . . ?
P2A P2B U2 118.4(9) . . ?
P2A P2B U3 150.1(9) . . ?
P2A P2B Rb2 110.0(8) . . ?
P2A P2B O9A 82.0(12) . . ?
P2A P2B O9B 82.2(11) . . ?
P2A P2B O10A 25.0(8) . . ?
P2A P2B O10B 143.2(11) . . ?
P2A P2B O11A 52.1(11) . . ?
P2A P2B O11B 38.3(11) . . ?
P2A P2B O12A 111.8(19) . . ?
P2A P2B O12B 109.6(14) . . ?
O9A P2B U2 38.1(9) . . ?
O9A P2B U3 127.8(10) . . ?
O9A P2B Rb2 76.3(10) . . ?
O9A P2B O9B 26.6(9) . . ?
O9A P2B O10A 87.8(11) . . ?
O9A P2B O10B 86.5(11) . . ?
O9A P2B O11A 97.4(13) . . ?
O9A P2B O11B 99.0(14) . . ?
O9A P2B O12B 136.5(15) . . ?
O9B P2B U2 52.0(8) . . ?
O9B P2B U3 123.3(7) . . ?
O9B P2B Rb2 52.6(6) . . ?
O9B P2B O10A 76.6(9) . . ?
O9B P2B O10B 102.3(9) . . ?
O9B P2B O11A 116.6(11) . . ?
O10A P2B U2 125.4(4) . . ?
O10A P2B U3 137.3(4) . . ?
O10A P2B Rb2 87.9(4) . . ?
O10B P2B U2 50.8(4) . . ?
O10B P2B U3 53.3(5) . . ?
O10B P2B Rb2 101.0(6) . . ?
O10B P2B O10A 167.9(7) . . ?
O10B P2B O11A 95.3(9) . . ?
O11A P2B U2 110.0(8) . . ?
O11A P2B U3 116.0(8) . . ?
O11A P2B Rb2 162.0(9) . . ?
O11A P2B O10A 74.9(9) . . ?
O11B P2B U2 120.2(9) . . ?
O11B P2B U3 123.9(10) . . ?
O11B P2B Rb2 147.7(10) . . ?
O11B P2B O9B 112.3(12) . . ?
O11B P2B O10A 59.8(10) . . ?
O11B P2B O10B 110.7(9) . . ?
O11B P2B O11A 15.4(10) . . ?
O11B P2B O12B 116.3(15) . . ?
O12A P2B U2 127.4(17) . . ?
O12A P2B U3 42.4(17) . . ?
O12A P2B Rb2 73.7(14) . . ?
O12A P2B O9A 149.7(18) . . ?
O12A P2B O9B 125.5(16) . . ?
O12A P2B O10A 94.9(18) . . ?
O12A P2B O10B 95.4(18) . . ?
O12A P2B O11A 112.4(17) . . ?
O12A P2B O11B 108.4(19) . . ?
O12A P2B O12B 15(2) . . ?
O12B P2B U2 123.1(12) . . ?
O12B P2B U3 49.9(11) . . ?
O12B P2B Rb2 60.2(10) . . ?
O12B P2B O9B 111.2(13) . . ?
O12B P2B O10A 88.7(12) . . ?
O12B P2B O10B 102.8(13) . . ?
O12B P2B O11A 123.3(13) . . ?
U4 P3A Rb3 71.2(3) 16_565 11_566 ?
U4 P3A Rb4A 150.1(5) 16_565 . ?
U4 P3A Rb4B 161.3(5) 16_565 . ?
U4 P3A Rb6 69.1(3) 16_565 . ?
Rb3 P3A Rb4B 96.5(4) 11_566 . ?
Rb3 P3A Rb6 76.0(3) 11_566 . ?
Rb4A P3A Rb3 87.3(3) . 11_566 ?
Rb4A P3A Rb4B 11.3(3) . . ?
Rb4A P3A Rb6 86.0(3) . . ?
Rb6 P3A Rb4B 94.7(4) . . ?
O3 P3A U4 115.5(8) . 16_565 ?
O3 P3A Rb3 69.1(6) . 11_566 ?
O3 P3A Rb4A 73.1(7) . . ?
O3 P3A Rb4B 70.6(7) . . ?
O3 P3A Rb6 139.7(8) . . ?
O3 P3A O4A 109.9(10) . . ?
O3 P3A O4B 92.8(9) . . ?
O3 P3A O5A 109.9(10) . . ?
O3 P3A O5B 109.0(11) . . ?
O4A P3A U4 53.6(9) . 16_565 ?
O4A P3A Rb3 118.5(9) . 11_566 ?
O4A P3A Rb4A 153.8(9) . . ?
O4A P3A Rb4B 143.2(9) . . ?
O4A P3A Rb6 104.0(9) . . ?
O4A P3A O4B 23.8(7) . . ?
O4B P3A U4 75.5(8) . 16_565 ?
O4B P3A Rb3 128.8(7) . 11_566 ?
O4B P3A Rb4A 134.1(8) . . ?
O4B P3A Rb4B 122.8(8) . . ?
O4B P3A Rb6 125.4(9) . . ?
O5A P3A U4 49.0(6) . 16_565 ?
O5A P3A Rb3 40.9(6) . 11_566 ?
O5A P3A Rb4A 101.3(7) . . ?
O5A P3A Rb4B 112.6(7) . . ?
O5A P3A Rb6 40.3(6) . . ?
O5A P3A O4A 101.9(12) . . ?
O5A P3A O4B 124.4(11) . . ?
O5A P3A O5B 35.7(8) . . ?
O5B P3A U4 15.4(6) . 16_565 ?
O5B P3A Rb3 56.3(7) . 11_566 ?
O5B P3A Rb4A 136.4(8) . . ?
O5B P3A Rb4B 147.7(8) . . ?
O5B P3A Rb6 64.1(8) . . ?
O5B P3A O4A 68.6(11) . . ?
O5B P3A O4B 89.4(10) . . ?
O6A P3A U4 134.4(13) . 16_565 ?
O6A P3A Rb3 129.0(16) . 11_566 ?
O6A P3A Rb4A 48.3(13) . . ?
O6A P3A Rb4B 44.2(12) . . ?
O6A P3A Rb6 77.0(15) . . ?
O6A P3A O3 110.1(14) . . ?
O6A P3A O4A 109.6(17) . . ?
O6A P3A O4B 102.1(17) . . ?
O6A P3A O5A 115.1(18) . . ?
O6A P3A O5B 138.4(17) . . ?
O6B P3A U4 115.4(14) . 16_565 ?
O6B P3A Rb3 127.5(16) . 11_566 ?
O6B P3A Rb4A 61.9(14) . . ?
O6B P3A Rb4B 60.6(14) . . ?
O6B P3A Rb6 61.4(14) . . ?
O6B P3A O3 129.1(15) . . ?
O6B P3A O4A 101.3(18) . . ?
O6B P3A O4B 101.6(18) . . ?
O6B P3A O5A 101.4(17) . . ?
O6B P3A O5B 119.6(17) . . ?
O6B P3A O6A 19.2(16) . . ?
U4 P3B U4 81.9(3) 16_565 10_556 ?
U4 P3B Rb4A 138.3(5) 16_565 . ?
U4 P3B Rb4A 139.2(4) 10_556 . ?
U4 P3B Rb5B 70.4(4) 10_556 16_565 ?
U4 P3B Rb5B 66.4(6) 16_565 16_565 ?
U4 P3B Rb5C 62.8(4) 10_556 10_556 ?
U4 P3B Rb5C 65.9(3) 16_565 10_556 ?
Rb5B P3B Rb4A 124.6(5) 16_565 . ?
Rb5C P3B Rb4A 130.4(5) 10_556 . ?
Rb5C P3B Rb5B 7.6(3) 10_556 16_565 ?
O3 P3B U4 110.1(7) . 10_556 ?
O3 P3B U4 122.3(7) . 16_565 ?
O3 P3B Rb4A 59.9(6) . . ?
O3 P3B Rb5B 66.0(7) . 16_565 ?
O3 P3B Rb5C 70.9(7) . 10_556 ?
O3 P3B O5A 97.1(9) . . ?
O3 P3B O6A 95.8(12) . . ?
O3 P3B O6B 109.2(13) . . ?
O4A P3B U4 57.5(11) . 16_565 ?
O4A P3B U4 29.7(9) . 10_556 ?
O4A P3B Rb4A 154.5(11) . . ?
O4A P3B Rb5B 77.9(10) . 16_565 ?
O4A P3B Rb5C 71.0(10) . 10_556 ?
O4A P3B O3 135.8(13) . . ?
O4A P3B O4B 32.1(10) . . ?
O4A P3B O5A 109.1(13) . . ?
O4A P3B O5B 80.8(13) . . ?
O4A P3B O6A 116.8(16) . . ?
O4A P3B O6B 109.0(17) . . ?
O4B P3B U4 5.7(7) . 10_556 ?
O4B P3B U4 86.5(10) . 16_565 ?
O4B P3B Rb4A 134.1(9) . . ?
O4B P3B Rb5B 75.4(9) . 16_565 ?
O4B P3B Rb5C 67.9(8) . 10_556 ?
O4B P3B O3 110.6(11) . . ?
O4B P3B O5A 140.5(12) . . ?
O4B P3B O5B 109.6(12) . . ?
O4B P3B O6A 110.7(15) . . ?
O4B P3B O6B 112.2(16) . . ?
O5A P3B U4 136.3(7) . 10_556 ?
O5A P3B U4 54.5(5) . 16_565 ?
O5A P3B Rb4A 83.9(6) . . ?
O5A P3B Rb5B 91.8(8) . 16_565 ?
O5A P3B Rb5C 97.2(6) . 10_556 ?
O5B P3B U4 23.4(6) . 16_565 ?
O5B P3B U4 104.8(8) . 10_556 ?
O5B P3B Rb4A 116.0(8) . . ?
O5B P3B Rb5B 70.5(10) . 16_565 ?
O5B P3B Rb5C 73.2(8) . 10_556 ?
O5B P3B O3 108.4(11) . . ?
O5B P3B O5A 32.4(7) . . ?
O5B P3B O6A 120.7(15) . . ?
O5B P3B O6B 106.7(15) . . ?
O6A P3B U4 116.3(13) . 10_556 ?
O6A P3B U4 130.0(12) . 16_565 ?
O6A P3B Rb4A 38.8(11) . . ?
O6A P3B Rb5B 161.6(12) . 16_565 ?
O6A P3B Rb5C 164.0(12) . 10_556 ?
O6A P3B O5A 93.2(14) . . ?
O6B P3B U4 114.0(12) . 16_565 ?
O6B P3B U4 117.2(14) . 10_556 ?
O6B P3B Rb4A 49.6(11) . . ?
O6B P3B Rb5B 172.3(14) . 16_565 ?
O6B P3B Rb5C 179.9(14) . 10_556 ?
O6B P3B O5A 82.7(13) . . ?
O6B P3B O6A 16.1(13) . . ?
U1 O1 Rb1 106.2(4) . 11_566 ?
U1 O1 Rb5A 125.62(17) . . ?
U1 O1 Rb5A 125.62(17) . 10_556 ?
U1 O1 Rb5B 113.5(6) . 7_456 ?
U1 O1 Rb5B 127.2(5) . . ?
U1 O1 Rb5B 127.2(5) . 10_556 ?
U1 O1 Rb5B 113.5(6) . 16_565 ?
U1 O1 Rb5C 117.4(4) . 10_556 ?
U1 O1 Rb5C 117.4(4) . . ?
Rb5A O1 Rb1 85.2(3) . 11_566 ?
Rb5A O1 Rb1 85.2(3) 10_556 11_566 ?
Rb5A O1 Rb5A 107.9(3) 10_556 . ?
Rb5A O1 Rb5B 116.9(6) . 16_565 ?
Rb5A O1 Rb5B 16.0(6) . . ?
Rb5A O1 Rb5B 15.8(5) . 7_456 ?
Rb5A O1 Rb5B 16.0(6) 10_556 10_556 ?
Rb5A O1 Rb5B 15.8(5) 10_556 16_565 ?
Rb5A O1 Rb5B 101.5(7) 10_556 . ?
Rb5A O1 Rb5B 116.9(6) 10_556 7_456 ?
Rb5A O1 Rb5B 101.5(7) . 10_556 ?
Rb5A O1 Rb5C 20.2(8) 10_556 10_556 ?
Rb5A O1 Rb5C 20.2(8) . . ?
Rb5A O1 Rb5C 109.5(3) . 10_556 ?
Rb5A O1 Rb5C 109.5(3) 10_556 . ?
Rb5B O1 Rb1 99.4(6) 10_556 11_566 ?
Rb5B O1 Rb1 99.4(6) . 11_566 ?
Rb5B O1 Rb1 98.8(5) 16_565 11_566 ?
Rb5B O1 Rb1 98.8(5) 7_456 11_566 ?
Rb5B O1 Rb5B 15.4(11) . 7_456 ?
Rb5B O1 Rb5B 91.7(13) 10_556 . ?
Rb5B O1 Rb5B 106.9(4) 10_556 7_456 ?
Rb5B O1 Rb5B 15.4(11) 10_556 16_565 ?
Rb5B O1 Rb5B 122.0(10) 16_565 7_456 ?
Rb5B O1 Rb5B 106.9(4) . 16_565 ?
Rb5B O1 Rb5C 113.0(6) 7_456 10_556 ?
Rb5B O1 Rb5C 9.9(4) . . ?
Rb5B O1 Rb5C 9.9(5) 7_456 . ?
Rb5B O1 Rb5C 9.9(4) 10_556 10_556 ?
Rb5B O1 Rb5C 113.0(6) 16_565 . ?
Rb5B O1 Rb5C 98.3(6) . 10_556 ?
Rb5B O1 Rb5C 9.9(5) 16_565 10_556 ?
Rb5B O1 Rb5C 98.3(6) 10_556 . ?
Rb5C O1 Rb1 105.5(7) . 11_566 ?
Rb5C O1 Rb1 105.4(7) 10_556 11_566 ?
Rb5C O1 Rb5C 103.8(5) 10_556 . ?
U1 O2 Rb4A 121.6(5) . . ?
U1 O2 Rb4A 121.6(5) . 10_556 ?
U1 O2 Rb4B 124.4(8) . . ?
U1 O2 Rb6 114.0(5) . 11_566 ?
Rb4A O2 Rb4A 33.6(4) . 10_556 ?
Rb4A O2 Rb6 121.2(4) . 11_566 ?
Rb4A O2 Rb6 121.2(4) 10_556 11_566 ?
Rb4B O2 Rb4A 16.85(19) . 10_556 ?
Rb4B O2 Rb4A 16.85(19) . . ?
Rb4B O2 Rb6 121.5(7) . 11_566 ?
U1 O3 Rb3 109.3(3) . 11_566 ?
U1 O3 Rb4A 91.6(3) . . ?
U1 O3 Rb5B 87.3(6) . 16_565 ?
U1 O3 Rb5C 89.6(5) . 10_556 ?
Rb4A O3 Rb3 93.3(3) . 11_566 ?
Rb4A O3 Rb5B 165.7(5) . 16_565 ?
Rb4A O3 Rb5C 173.8(4) . 10_556 ?
Rb5B O3 Rb3 73.7(5) 16_565 11_566 ?
Rb5B O3 Rb5C 8.5(4) 16_565 10_556 ?
Rb5C O3 Rb3 80.6(3) 10_556 11_566 ?
P3A O3 U1 162.2(8) . . ?
P3A O3 Rb3 87.7(6) . 11_566 ?
P3A O3 Rb4A 82.0(7) . . ?
P3A O3 Rb5B 102.9(9) . 16_565 ?
P3A O3 Rb5C 98.6(9) . 10_556 ?
P3A O3 P3B 17.2(4) . . ?
P3B O3 U1 153.5(8) . . ?
P3B O3 Rb3 95.2(6) . 11_566 ?
P3B O3 Rb4A 97.0(6) . . ?
P3B O3 Rb5B 90.2(8) . 16_565 ?
P3B O3 Rb5C 84.6(8) . 10_556 ?
U4 O4A U4 127.6(5) 16_565 . ?
U4 O4A U4 13.15(14) 10_556 . ?
U4 O4A U4 114.4(6) 10_556 16_565 ?
U4 O4A Rb5C 74.7(4) 10_556 10_556 ?
U4 O4A Rb5C 80.2(4) . 10_556 ?
U4 O4A Rb5C 73.2(4) 16_565 10_556 ?
P3A O4A U4 143.6(12) . 10_556 ?
P3A O4A U4 132.0(11) . . ?
P3A O4A U4 96.2(10) . 16_565 ?
P3A O4A Rb5C 97.3(8) . 10_556 ?
P3A O4A O5B 55.1(9) . . ?
P3B O4A U4 99.5(12) . 16_565 ?
P3B O4A U4 136.1(14) . 10_556 ?
P3B O4A U4 125.4(13) . . ?
P3B O4A Rb5C 90.5(11) . 10_556 ?
P3B O4A P3A 8.8(10) . . ?
P3B O4A O5B 58.3(10) . . ?
O4B O4A U4 27.3(16) . . ?
O4B O4A U4 39.0(15) . 10_556 ?
O4B O4A U4 146.5(19) . 16_565 ?
O4B O4A Rb5C 78.4(18) . 10_556 ?
O4B O4A P3A 105(2) . . ?
O4B O4A P3B 98(2) . . ?
O4B O4A O5B 146(2) . . ?
O5B O4A U4 157.8(10) . . ?
O5B O4A U4 148.5(10) . 10_556 ?
O5B O4A U4 41.2(7) . 16_565 ?
O5B O4A Rb5C 77.8(8) . 10_556 ?
U4 O4B U4 20.2(3) 10_556 . ?
U4 O4B Rb5C 82.8(6) 10_556 10_556 ?
U4 O4B Rb5C 92.2(6) . 10_556 ?
U4 O4B P3A 174.0(11) 10_556 . ?
P3A O4B U4 164.9(11) . . ?
P3A O4B Rb5C 92.4(8) . 10_556 ?
P3B O4B U4 167.1(14) . . ?
P3B O4B U4 169.5(12) . 10_556 ?
P3B O4B Rb5C 87.9(9) . 10_556 ?
P3B O4B P3A 4.7(8) . . ?
O4A O4B U4 125(2) . 10_556 ?
O4A O4B U4 143(2) . . ?
O4A O4B Rb5C 88.1(17) . 10_556 ?
O4A O4B P3A 51.4(17) . . ?
O4A O4B P3B 49.7(17) . . ?
U4 O5A U4 16.51(10) 16_565 7_455 ?
U4 O5A Rb3 101.9(5) 16_565 11_566 ?
U4 O5A Rb3 92.7(4) 7_455 11_566 ?
U4 O5A Rb6 90.1(4) 7_455 . ?
U4 O5A Rb6 98.9(4) 16_565 . ?
Rb6 O5A Rb3 112.7(5) . 11_566 ?
P3A O5A U4 102.0(7) . 16_565 ?
P3A O5A U4 118.5(8) . 7_455 ?
P3A O5A Rb3 117.9(8) . 11_566 ?
P3A O5A Rb6 118.8(9) . . ?
P3A O5A P3B 13.7(5) . . ?
P3B O5A U4 88.5(6) . 16_565 ?
P3B O5A U4 105.0(7) . 7_455 ?
P3B O5A Rb3 119.2(7) . 11_566 ?
P3B O5A Rb6 124.6(8) . . ?
O5B O5A U4 47.2(11) . 7_455 ?
O5B O5A U4 31.5(10) . 16_565 ?
O5B O5A Rb3 105.6(15) . 11_566 ?
O5B O5A Rb6 123.3(14) . . ?
O5B O5A P3A 72.6(12) . . ?
O5B O5A P3B 58.9(11) . . ?
U4 O5B U4 17.72(19) 16_565 7_455 ?
U4 O5B Rb3 94.3(5) 7_455 11_566 ?
U4 O5B Rb3 108.7(7) 16_565 11_566 ?
U4 O5B Rb5B 88.8(7) 7_455 16_565 ?
U4 O5B Rb5B 82.6(8) 16_565 16_565 ?
U4 O5B Rb5C 88.7(6) 7_455 10_556 ?
U4 O5B Rb5C 80.2(7) 16_565 10_556 ?
U4 O5B Rb6 96.2(7) 16_565 . ?
U4 O5B Rb6 85.9(5) 7_455 . ?
U4 O5B O4A 94.6(10) 16_565 . ?
Rb3 O5B Rb5B 76.3(5) 11_566 16_565 ?
Rb3 O5B Rb5C 84.5(6) 11_566 10_556 ?
Rb3 O5B Rb6 89.8(4) 11_566 . ?
Rb5C O5B Rb5B 8.2(3) 10_556 16_565 ?
Rb6 O5B Rb5B 164.7(7) . 16_565 ?
Rb6 O5B Rb5C 171.8(6) . 10_556 ?
P3A O5B U4 165.6(12) . 7_455 ?
P3A O5B U4 150.3(12) . 16_565 ?
P3A O5B Rb3 99.9(8) . 11_566 ?
P3A O5B Rb5B 96.8(10) . 16_565 ?
P3A O5B Rb5C 95.0(8) . 10_556 ?
P3A O5B Rb6 91.7(9) . . ?
P3A O5B O4A 56.3(9) . . ?
P3B O5B U4 152.9(10) . 7_455 ?
P3B O5B U4 135.3(11) . 16_565 ?
P3B O5B Rb3 110.2(9) . 11_566 ?
P3B O5B Rb5B 86.2(10) . 16_565 ?
P3B O5B Rb5C 82.7(8) . 10_556 ?
P3B O5B Rb6 104.8(9) . . ?
P3B O5B P3A 17.0(4) . . ?
P3B O5B O4A 40.8(9) . . ?
O4A O5B U4 112.1(10) . 7_455 ?
O4A O5B Rb3 144.5(10) . 11_566 ?
O4A O5B Rb5B 80.8(9) . 16_565 ?
O4A O5B Rb5C 73.3(8) . 10_556 ?
O4A O5B Rb6 114.5(10) . . ?
O5A O5B U4 114.9(13) . 7_455 ?
O5A O5B U4 131.1(15) . 16_565 ?
O5A O5B Rb3 57.7(13) . 11_566 ?
O5A O5B Rb5B 128.4(15) . 16_565 ?
O5A O5B Rb5C 135.4(16) . 10_556 ?
O5A O5B Rb6 43.3(12) . . ?
O5A O5B P3A 71.7(12) . . ?
O5A O5B P3B 88.7(13) . . ?
O5A O5B O4A 123.7(16) . . ?
U2 O6A Rb4A 106.3(10) . . ?
U2 O6A Rb4A 87.5(7) . 10_556 ?
U2 O6A Rb4B 95.4(9) . . ?
Rb4A O6A Rb4A 29.1(4) . 10_556 ?
Rb4A O6A Rb4B 15.7(3) . . ?
Rb4B O6A Rb4A 13.4(3) . 10_556 ?
P3A O6A U2 145(2) . . ?
P3A O6A Rb4A 108.0(18) . . ?
P3A O6A Rb4A 119.7(17) . 10_556 ?
P3A O6A Rb4B 116.0(18) . . ?
P3A O6A P3B 13.3(7) . . ?
P3B O6A U2 132.2(19) . . ?
P3B O6A Rb4A 123.5(16) . 10_556 ?
P3B O6A Rb4A 118.0(17) . . ?
P3B O6A Rb4B 123.1(17) . . ?
U2 O6B Rb4A 92.3(9) . . ?
U2 O6B Rb4B 82.1(8) . . ?
U2 O6B Rb6 110.9(11) . . ?
Rb4A O6B Rb4B 13.3(3) . . ?
Rb4A O6B Rb6 100.4(9) . . ?
Rb6 O6B Rb4B 112.0(10) . . ?
P3A O6B U2 147(2) . . ?
P3A O6B Rb4A 96.6(16) . . ?
P3A O6B Rb4B 100.5(16) . . ?
P3A O6B Rb6 98.9(15) . . ?
P3A O6B P3B 15.2(8) . . ?
P3B O6B U2 133.6(19) . . ?
P3B O6B Rb4A 108.2(15) . . ?
P3B O6B Rb4B 109.5(15) . . ?
P3B O6B Rb6 105.7(13) . . ?
U2 O7 Rb2 124.6(2) . 10_556 ?
U2 O7 Rb2 124.6(2) . . ?
Rb2 O7 Rb2 103.2(3) . 10_556 ?
U2 O8 Rb3 113.5(6) . . ?
U2 O8 Rb4A 110.5(5) . . ?
U2 O8 Rb4A 103.4(5) . 10_556 ?
U2 O8 Rb4B 109.0(7) . . ?
Rb3 O8 Rb4A 128.0(5) . 10_556 ?
Rb4A O8 Rb3 135.7(5) . . ?
Rb4A O8 Rb4A 31.5(3) . 10_556 ?
Rb4B O8 Rb3 132.1(7) . . ?
Rb4B O8 Rb4A 16.3(2) . . ?
Rb4B O8 Rb4A 15.33(19) . 10_556 ?
O8 O8 U2 79.4(5) 10_556 . ?
O8 O8 Rb3 83.7(3) 10_556 . ?
O8 O8 Rb4A 99.7(4) 10_556 . ?
O8 O8 Rb4A 68.2(3) 10_556 10_556 ?
O8 O8 Rb4B 83.5(3) 10_556 . ?
U2 O9A Rb6 122.8(8) . . ?
P2A O9A U2 142.0(14) . . ?
P2A O9A Rb6 95.2(10) . . ?
P2B O9A U2 118.4(13) . . ?
P2B O9A Rb6 117.8(12) . . ?
P2B O9A P2A 25.1(4) . . ?
O9B O9A U2 110(3) . . ?
O9B O9A Rb6 68(2) . . ?
O9B O9A P2A 83(3) . . ?
O9B O9A P2B 83(3) . . ?
U2 O9B Rb2 98.6(5) . . ?
U2 O9B Rb6 118.9(6) . . ?
Rb6 O9B Rb2 106.4(6) . . ?
P2A O9B U2 116.3(10) . . ?
P2A O9B Rb2 115.9(8) . . ?
P2A O9B Rb6 101.1(8) . . ?
P2B O9B U2 99.9(10) . . ?
P2B O9B Rb2 104.3(8) . . ?
P2B O9B Rb6 124.9(9) . . ?
P2B O9B P2A 23.8(3) . . ?
O9A O9B U2 56(2) . . ?
O9A O9B Rb2 150(3) . . ?
O9A O9B Rb6 100(3) . . ?
O9A O9B P2A 71(2) . . ?
O9A O9B P2B 70(2) . . ?
U1 O10A Rb1 102.3(4) 3_654 . ?
U1 O10A Rb6 98.7(4) 3_654 . ?
Rb1 O10A Rb6 143.9(5) . . ?
P2A O10A U1 98.2(7) . 3_654 ?
P2A O10A Rb1 101.6(6) . . ?
P2A O10A Rb6 104.0(6) . . ?
P2A O10A P2B 10.0(3) . . ?
P2B O10A U1 107.2(6) . 3_654 ?
P2B O10A Rb1 95.3(5) . . ?
P2B O10A Rb6 106.1(5) . . ?
O10A O10A U1 76.1(3) 10 3_654 ?
O10A O10A Rb1 78.5(2) 10 . ?
O10A O10A Rb6 78.6(2) 10 . ?
O10A O10A P2A 174.1(6) 10 . ?
O10A O10A P2B 173.6(4) 10 . ?
U2 O10B Rb3 96.5(4) . . ?
U3 O10B U2 127.6(5) . . ?
U3 O10B Rb3 126.8(4) . . ?
P2A O10B U2 98.9(5) . . ?
P2A O10B U3 104.4(5) . . ?
P2A O10B Rb3 95.0(4) . . ?
P2B O10B U2 99.8(6) . . ?
P2B O10B U3 96.1(6) . . ?
P2B O10B Rb3 105.1(6) . . ?
P2B O10B P2A 10.4(3) . . ?
O10B O10B U2 79.5(3) 10_556 . ?
O10B O10B U3 79.5(2) 10_556 . ?
O10B O10B Rb3 81.4(2) 10_556 . ?
O10B O10B P2A 175.8(4) 10_556 . ?
O10B O10B P2B 173.6(5) 10_556 . ?
U1 O11A Rb3 131.7(8) 3_654 . ?
U1 O11A Rb5A 88.4(7) 3_654 3_654 ?
U1 O11A Rb5B 89.3(8) 3_654 5_546 ?
U1 O11A Rb5C 83.7(6) 3_654 3_654 ?
Rb3 O11A Rb5A 97.0(6) . 3_654 ?
Rb3 O11A Rb5B 86.7(9) . 5_546 ?
Rb3 O11A Rb5C 88.3(6) . 3_654 ?
Rb5A O11A Rb5C 16.5(6) 3_654 3_654 ?
Rb5B O11A Rb5A 13.1(5) 5_546 3_654 ?
Rb5B O11A Rb5C 6.3(4) 5_546 3_654 ?
P2A O11A U1 99.6(12) . 3_654 ?
P2A O11A Rb3 123.1(12) . . ?
P2A O11A Rb5A 108.9(11) . 3_654 ?
P2A O11A Rb5B 121.6(13) . 5_546 ?
P2A O11A Rb5C 125.3(13) . 3_654 ?
P2A O11A P2B 19.7(4) . . ?
P2B O11A U1 118.7(11) . 3_654 ?
P2B O11A Rb3 106.8(10) . . ?
P2B O11A Rb5A 102.9(9) . 3_654 ?
P2B O11A Rb5B 113.7(11) . 5_546 ?
P2B O11A Rb5C 119.0(11) . 3_654 ?
O11B O11A U1 73(4) . 3_654 ?
O11B O11A Rb3 152(4) . . ?
O11B O11A Rb5A 97(5) . 3_654 ?
O11B O11A Rb5B 110(5) . 5_546 ?
O11B O11A Rb5C 110(5) . 3_654 ?
O11B O11A P2A 29(3) . . ?
O11B O11A P2B 46(4) . . ?
U1 O11B Rb3 115.4(8) 3_654 . ?
U1 O11B Rb5A 87.5(6) 3_654 3_654 ?
U1 O11B Rb5B 85.8(7) 3_654 5_546 ?
Rb3 O11B Rb5A 86.8(5) . 3_654 ?
Rb3 O11B Rb5B 76.1(8) . 5_546 ?
Rb5B O11B Rb5A 12.9(5) 5_546 3_654 ?
P2A O11B U1 125.1(16) . 3_654 ?
P2A O11B Rb3 113.1(14) . . ?
P2A O11B Rb5A 119.6(16) . 3_654 ?
P2A O11B Rb5B 130.3(16) . 5_546 ?
P2A O11B P2B 22.0(6) . . ?
P2B O11B U1 146.5(13) . 3_654 ?
P2B O11B Rb3 95.9(9) . . ?
P2B O11B Rb5A 106.8(11) . 3_654 ?
P2B O11B Rb5B 114.6(12) . 5_546 ?
O11A O11B U1 95(4) . 3_654 ?
O11A O11B Rb3 23(4) . . ?
O11A O11B Rb5A 74(4) . 3_654 ?
O11A O11B Rb5B 62(4) . 5_546 ?
O11A O11B P2A 136(5) . . ?
O11A O11B P2B 118(4) . . ?
U3 O12A Rb1 123.0(13) . . ?
U3 O12A Rb2 94.1(9) . . ?
Rb1 O12A Rb2 92.0(7) . . ?
P2A O12A U3 138.2(19) . . ?
P2A O12A Rb1 97.7(16) . . ?
P2A O12A Rb2 93.6(14) . . ?
P2B O12A U3 117(2) . . ?
P2B O12A Rb1 119(2) . . ?
P2B O12A Rb2 87.6(17) . . ?
P2B O12A P2A 22.4(7) . . ?
U3 O12B Rb1 129.7(12) . . ?
U3 O12B Rb2 101.5(9) . . ?
Rb1 O12B Rb2 103.4(8) . . ?
P2A O12B U3 118.7(14) . . ?
P2A O12B Rb1 99.1(11) . . ?
P2A O12B Rb2 99.9(11) . . ?
P2B O12B U3 101.5(15) . . ?
P2B O12B Rb1 118.2(14) . . ?
P2B O12B Rb2 96.2(13) . . ?
P2B O12B P2A 19.3(4) . . ?
U3 O13 Rb1 109.1(5) . 7_455 ?
U3 O13 Rb2 123.8(3) . . ?
U3 O13 Rb2 123.8(3) . 10_556 ?
Rb1 O13 Rb2 100.3(2) 7_455 . ?
Rb1 O13 Rb2 100.3(2) 7_455 10_556 ?
Rb2 O13 Rb2 95.3(3) 10_556 . ?
U3 O14 Rb1 105.0(4) . 15_666 ?
U3 O14 Rb5A 129.98(16) . 12_657 ?
U3 O14 Rb5A 129.98(16) . 3_654 ?
U3 O14 Rb5B 135.6(5) . 5_546 ?
U3 O14 Rb5B 135.6(5) . 14_655 ?
Rb1 O14 Rb5B 95.2(5) 15_666 5_546 ?
Rb1 O14 Rb5B 95.2(5) 15_666 14_655 ?
Rb5A O14 Rb1 84.9(2) 12_657 15_666 ?
Rb5A O14 Rb1 84.9(2) 3_654 15_666 ?
Rb5A O14 Rb5A 99.3(3) 3_654 12_657 ?
Rb5A O14 Rb5B 14.3(6) 3_654 5_546 ?
Rb5A O14 Rb5B 90.3(7) 12_657 5_546 ?
Rb5A O14 Rb5B 90.3(7) 3_654 14_655 ?
Rb5A O14 Rb5B 14.3(6) 12_657 14_655 ?
Rb5B O14 Rb5B 79.5(13) 5_546 14_655 ?
U3 O15A Rb1 91.2(8) . 15_666 ?
U3 O15A Rb1 94.3(8) . 7_455 ?
Rb1 O15A Rb1 115.4(6) 7_455 15_666 ?
P1 O15A U3 170.2(12) . . ?
P1 O15A Rb1 89.7(11) . 15_666 ?
P1 O15A Rb1 94.1(9) . 7_455 ?
O15B O15A U3 86(6) . . ?
O15B O15A Rb1 86(7) . 15_666 ?
O15B O15A Rb1 159(7) . 7_455 ?
O15B O15A P1 84(6) . . ?
U3 O15B Rb1 82.0(8) . 7_455 ?
U3 O15B Rb1 90.7(11) . 15_666 ?
U3 O15B Rb1 112.7(9) . . ?
Rb1 O15B Rb1 126.9(10) 15_666 . ?
Rb1 O15B Rb1 103.3(6) 15_666 7_455 ?
Rb1 O15B Rb1 125.9(12) . 7_455 ?
P1 O15B U3 157.5(14) . . ?
P1 O15B Rb1 76.2(10) . 7_455 ?
P1 O15B Rb1 88.9(15) . 15_666 ?
P1 O15B Rb1 85.1(11) . . ?
O15A O15B U3 81(6) . . ?
O15A O15B Rb1 18(6) . 7_455 ?
O15A O15B Rb1 143(7) . . ?
O15A O15B Rb1 85(7) . 15_666 ?
O15A O15B P1 76(6) . . ?
U4 O16 U4 25.57(18) . 10_556 ?
U4 O16 Rb2 146.1(6) 10_556 10_556 ?
U4 O16 Rb2 102.8(5) 10_556 . ?
U4 O16 Rb2 126.6(6) . . ?
U4 O16 Rb2 124.8(6) . 10_556 ?
U4 O16 Rb6 104.4(5) . 7_455 ?
U4 O16 Rb6 101.0(5) 10_556 7_455 ?
Rb2 O16 Rb2 94.2(3) 10_556 . ?
Rb2 O16 Rb6 106.1(4) 10_556 7_455 ?
Rb6 O16 Rb2 96.4(4) 7_455 . ?
O16 O16 U4 94.0(4) 10_556 . ?
O16 O16 U4 68.5(4) 10_556 10_556 ?
O16 O16 Rb2 39.3(2) 10_556 . ?
O16 O16 Rb2 133.5(3) 10_556 10_556 ?
O16 O16 Rb6 84.6(3) 10_556 7_455 ?
U4 O17 U4 23.9(2) . 10_556 ?
U4 O17 Rb3 98.4(6) . 5_556 ?
U4 O17 Rb3 93.3(5) 10_556 5_556 ?
U4 O17 Rb5A 145.8(8) . . ?
U4 O17 Rb5A 166.6(7) 10_556 . ?
U4 O17 Rb5B 163.6(10) 10_556 . ?
U4 O17 Rb5B 91.3(6) 10_556 10_556 ?
U4 O17 Rb5B 140.5(10) . . ?
U4 O17 Rb5B 130.4(11) . 7_456 ?
U4 O17 Rb5B 151.0(10) 10_556 7_456 ?
U4 O17 Rb5B 115.1(8) . 10_556 ?
U4 O17 Rb5C 128.6(11) . . ?
U4 O17 Rb5C 107.6(9) . 10_556 ?
U4 O17 Rb5C 150.5(11) 10_556 . ?
U4 O17 Rb5C 84.1(8) 10_556 10_556 ?
Rb5A O17 Rb3 98.5(4) . 5_556 ?
Rb5A O17 Rb5B 96.7(5) . 10_556 ?
Rb5A O17 Rb5C 102.7(7) . 10_556 ?
Rb5B O17 Rb3 81.1(5) 10_556 5_556 ?
Rb5B O17 Rb3 109.6(6) 7_456 5_556 ?
Rb5B O17 Rb3 96.4(7) . 5_556 ?
Rb5B O17 Rb5A 7.2(4) . . ?
Rb5B O17 Rb5A 15.9(7) 7_456 . ?
Rb5B O17 Rb5B 14.0(9) . 7_456 ?
Rb5B O17 Rb5B 109.2(10) 7_456 10_556 ?
Rb5B O17 Rb5B 103.2(9) . 10_556 ?
Rb5B O17 Rb5C 109.6(10) . 10_556 ?
Rb5B O17 Rb5C 13.3(7) . . ?
Rb5B O17 Rb5C 113.8(6) 7_456 10_556 ?
Rb5B O17 Rb5C 9.0(6) 10_556 10_556 ?
Rb5C O17 Rb3 106.7(7) . 5_556 ?
Rb5C O17 Rb3 87.0(4) 10_556 5_556 ?
Rb5C O17 Rb5A 17.3(8) . . ?
Rb5C O17 Rb5B 4.6(7) . 7_456 ?
Rb5C O17 Rb5B 112.6(9) . 10_556 ?
Rb5C O17 Rb5C 117.6(13) . 10_556 ?
O17 O17 U4 85.0(5) 10_556 . ?
O17 O17 U4 61.0(5) 10_556 10_556 ?
O17 O17 Rb3 80.1(3) 10_556 5_556 ?
O17 O17 Rb5A 127.2(3) 10_556 . ?
O17 O17 Rb5B 30.6(4) 10_556 10_556 ?
O17 O17 Rb5B 138.6(8) 10_556 7_456 ?
O17 O17 Rb5B 133.8(6) 10_556 . ?
O17 O17 Rb5C 24.9(6) 10_556 10_556 ?
O17 O17 Rb5C 142.5(8) 10_556 . ?

_olex2_submission_special_instructions 'No special instructions were received'

# start Validation Reply Form
_vrf_PLAT971_Rb11U8P9O52         
;
PROBLEM: Check Calcd Resid. Dens.  0.84A   From Rb2             3.83 eA-3  
RESPONSE: The SHELXS 2016 refinement program calculates the residual 
electron density and hole to be 2.1 and -1.7. The electron density 
map produced by PLATON checked is different and inferior because if 
does not consider the complete data set as in SHELXS 2016.The largest 
residual electron density peak, 2.1, is near the disordered Rb4A site 
and is too small to be worth modeling, considering the extreme disorder. 
Regardless, the magnitude of the residual electron densities and holes are 
acceptable by the most stringent measures considering the presence of the 
heavy scatterer U. 
;
_vrf_PLAT975_Rb11U8P9O52         
;
PROBLEM: Check Calcd Resid. Dens.  0.97A   From O1              1.52 eA-3  
RESPONSE: The residual electron density is smaller than 10% of nearby U, 
and is in a location that does not make chemical sense to model as any 
atom as it would not produce reasonable bond distances. 
;
# end Validation Reply Form
_exptl_crystal_recrystallization_method 'From the Melt'
_exptl_crystal_preparation       Luminescent
