# Electronic Supplementary Material (ESI) for CrystEngComm.
# This journal is © The Royal Society of Chemistry 2020

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_yb2_0m_a_sq_sq
_database_code_depnum_ccdc_archive 'CCDC 1917559'
loop_
_audit_author_name
_audit_author_address
'Yue ZHAO'
;Nanjing University
China
;
_audit_update_record             
;
2020-09-23 deposited with the CCDC.	2020-12-10 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2018/3
_shelx_SHELXL_version_number     2018/3
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C44 H48 B12 Cl12 Cu N4 O4'
_chemical_formula_weight         1315.52

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      monoclinic
_space_group_IT_number           15
_space_group_name_H-M_alt        'C 2/c'
_space_group_name_Hall           '-C 2yc'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'

_cell_length_a                   43.481(7)
_cell_length_b                   21.109(3)
_cell_length_c                   22.589(4)
_cell_angle_alpha                90
_cell_angle_beta                 109.211(3)
_cell_angle_gamma                90
_cell_volume                     19578(5)
_cell_formula_units_Z            8
_cell_measurement_temperature    296(2)
_cell_measurement_reflns_used    9925
_cell_measurement_theta_min      2.23
_cell_measurement_theta_max      26.25

_exptl_crystal_description       block
_exptl_crystal_colour            ?
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    0.893
_exptl_crystal_F_000             5320
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          0.200
_exptl_crystal_size_mid          0.200
_exptl_crystal_size_min          0.200
_exptl_absorpt_coefficient_mu    0.578
_shelx_estimated_absorpt_T_min   0.893
_shelx_estimated_absorpt_T_max   0.893
_exptl_absorpt_correction_type   ?
_exptl_absorpt_correction_T_min  ?
_exptl_absorpt_correction_T_max  ?
_exptl_absorpt_process_details   ?
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      296(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_source                   ?
_diffrn_measurement_device_type  'BRUKER D8 VENTURE PHOTON 100'
_diffrn_measurement_method       ?
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            70145
_diffrn_reflns_av_unetI/netI     0.0753
_diffrn_reflns_av_R_equivalents  0.0735
_diffrn_reflns_limit_h_min       -54
_diffrn_reflns_limit_h_max       52
_diffrn_reflns_limit_k_min       -26
_diffrn_reflns_limit_k_max       26
_diffrn_reflns_limit_l_min       -23
_diffrn_reflns_limit_l_max       28
_diffrn_reflns_theta_min         0.992
_diffrn_reflns_theta_max         26.574
_diffrn_reflns_theta_full        25.242
_diffrn_measured_fraction_theta_max 0.985
_diffrn_measured_fraction_theta_full 0.998
_diffrn_reflns_Laue_measured_fraction_max 0.985
_diffrn_reflns_Laue_measured_fraction_full 0.998
_diffrn_reflns_point_group_measured_fraction_max 0.985
_diffrn_reflns_point_group_measured_fraction_full 0.998
_reflns_number_total             20151
_reflns_number_gt                11887
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       ?
_computing_cell_refinement       ?
_computing_data_reduction        ?
_computing_structure_solution    'SHELXT 2014/5 (Sheldrick, 2014)'
_computing_structure_refinement  'SHELXL-2018/3 (Sheldrick, 2018)'
_computing_molecular_graphics    ?
_computing_publication_material  ?
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0600P)²+175.0000P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_number_reflns         20151
_refine_ls_number_parameters     702
_refine_ls_number_restraints     24
_refine_ls_R_factor_all          0.1325
_refine_ls_R_factor_gt           0.0983
_refine_ls_wR_factor_ref         0.2738
_refine_ls_wR_factor_gt          0.2539
_refine_ls_goodness_of_fit_ref   1.110
_refine_ls_restrained_S_all      1.111
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C 0.35440(15) 0.1316(3) -0.0690(3) 0.0487(15) Uani 1 1 d . . . . .
H1 H 0.339846 0.128243 -0.109634 0.058 Uiso 1 1 calc R U . . .
C2 C 0.35396(16) 0.0847(3) -0.0269(3) 0.0520(16) Uani 1 1 d . . . . .
H2 H 0.339288 0.051222 -0.038827 0.062 Uiso 1 1 calc R U . . .
C1S C 0.26237(19) 0.2979(4) -0.2069(4) 0.073(2) Uani 1 1 d . . . . .
H1SA H 0.255757 0.306938 -0.250975 0.110 Uiso 1 1 calc R U . . .
H1SB H 0.273458 0.333938 -0.183687 0.110 Uiso 1 1 calc R U . . .
H1SC H 0.243513 0.288548 -0.195282 0.110 Uiso 1 1 calc R U . . .
C3 C 0.37608(15) 0.0883(3) 0.0347(2) 0.0458(14) Uani 1 1 d . . . . .
C2S C 0.28440(16) 0.2429(3) -0.1928(3) 0.0498(15) Uani 1 1 d . . . . .
C4 C 0.39700(16) 0.1394(3) 0.0484(3) 0.0484(15) Uani 1 1 d . . . . .
H4 H 0.411766 0.143477 0.088727 0.058 Uiso 1 1 calc R U . . .
C3S C 0.26965(19) 0.1821(4) -0.2230(3) 0.069(2) Uani 1 1 d . . . . .
H3SA H 0.267305 0.183100 -0.266711 0.104 Uiso 1 1 calc R U . . .
H3SB H 0.248651 0.176637 -0.218275 0.104 Uiso 1 1 calc R U . . .
H3SC H 0.283533 0.147392 -0.203208 0.104 Uiso 1 1 calc R U . . .
C5 C 0.39665(15) 0.1846(3) 0.0040(2) 0.0458(14) Uani 1 1 d . . . . .
H5 H 0.411692 0.217472 0.014527 0.055 Uiso 1 1 calc R U . . .
C4S C 0.1945(4) 0.4998(6) 0.2655(5) 0.141(5) Uani 1 1 d . . . . .
H4SA H 0.172139 0.505370 0.262533 0.211 Uiso 1 1 calc R U . . .
H4SB H 0.207833 0.529381 0.295305 0.211 Uiso 1 1 calc R U . . .
H4SC H 0.201255 0.457372 0.279091 0.211 Uiso 1 1 calc R U . . .
C6 C 0.37657(15) 0.0386(3) 0.0819(2) 0.0473(15) Uani 1 1 d . . . . .
C5S C 0.3301(4) 0.4861(7) 0.4018(6) 0.172(6) Uani 1 1 d . U . . .
H5SA H 0.345770 0.460520 0.391262 0.258 Uiso 1 1 calc R U . . .
H5SB H 0.323164 0.464687 0.432737 0.258 Uiso 1 1 calc R U . . .
H5SC H 0.339709 0.526031 0.418200 0.258 Uiso 1 1 calc R U . . .
C7 C 0.34934(16) 0.0046(3) 0.0788(3) 0.0551(17) Uani 1 1 d . . . . .
H7 H 0.330380 0.011511 0.045188 0.066 Uiso 1 1 calc R U . . .
C6S C 0.2142(3) 0.5730(6) 0.1953(5) 0.151(6) Uani 1 1 d . . . . .
H6SA H 0.221514 0.571566 0.159642 0.226 Uiso 1 1 calc R U . . .
H6SB H 0.232443 0.580122 0.232578 0.226 Uiso 1 1 calc R U . . .
H6SC H 0.198772 0.606886 0.190161 0.226 Uiso 1 1 calc R U . . .
C8 C 0.34884(16) -0.0408(3) 0.1246(3) 0.0563(17) Uani 1 1 d . . . . .
H8 H 0.329998 -0.063384 0.121371 0.068 Uiso 1 1 calc R U . . .
C7S C 0.3017(2) 0.4970(5) 0.3452(4) 0.082(2) Uani 1 1 d . U . . .
C9 C 0.37794(16) -0.0508(3) 0.1757(3) 0.0500(15) Uani 1 1 d . . . . .
C8S C 0.2877(4) 0.4374(7) 0.3092(8) 0.190(7) Uani 1 1 d . U . . .
H8SA H 0.277418 0.447537 0.265675 0.285 Uiso 1 1 calc R U . . .
H8SB H 0.271869 0.419442 0.325606 0.285 Uiso 1 1 calc R U . . .
H8SC H 0.304837 0.407317 0.313370 0.285 Uiso 1 1 calc R U . . .
C10 C 0.40558(17) -0.0166(3) 0.1779(3) 0.0601(18) Uani 1 1 d . . . . .
H10 H 0.424843 -0.023302 0.210871 0.072 Uiso 1 1 calc R U . . .
C9S C 0.4868(3) 0.3032(6) -0.0416(7) 0.152(6) Uani 1 1 d . . . . .
H9SA H 0.509097 0.290226 -0.032072 0.228 Uiso 1 1 calc R U . . .
H9SB H 0.484176 0.323738 -0.005621 0.228 Uiso 1 1 calc R U . . .
H9SC H 0.481165 0.332172 -0.076263 0.228 Uiso 1 1 calc R U . . .
C11 C 0.40497(16) 0.0270(3) 0.1323(3) 0.0568(17) Uani 1 1 d . . . . .
H11 H 0.423855 0.049242 0.134969 0.068 Uiso 1 1 calc R U . . .
C10S C 0.4654(2) 0.2470(4) -0.0581(3) 0.069(2) Uani 1 1 d . . . . .
C12 C 0.37732(15) -0.0967(3) 0.2248(2) 0.0457(14) Uani 1 1 d . . . . .
C11S C 0.4835(3) 0.1832(6) -0.0525(6) 0.136(5) Uani 1 1 d . . . . .
H11A H 0.469457 0.149454 -0.048491 0.205 Uiso 1 1 calc R U . . .
H11B H 0.502716 0.183891 -0.016204 0.205 Uiso 1 1 calc R U . . .
H11C H 0.489434 0.176486 -0.089313 0.205 Uiso 1 1 calc R U . . .
C13 C 0.39920(17) -0.0942(3) 0.2866(3) 0.0556(17) Uani 1 1 d . . . . .
H13 H 0.414944 -0.062568 0.297984 0.067 Uiso 1 1 calc R U . . .
C14 C 0.39748(16) -0.1377(3) 0.3299(3) 0.0505(16) Uani 1 1 d . . . . .
H14 H 0.412239 -0.134012 0.370325 0.061 Uiso 1 1 calc R U . . .
C15 C 0.35549(16) -0.1474(3) 0.2127(3) 0.0515(16) Uani 1 1 d . . . . .
H15 H 0.340907 -0.152883 0.172416 0.062 Uiso 1 1 calc R U . . .
C16 C 0.35496(15) -0.1895(3) 0.2589(2) 0.0482(15) Uani 1 1 d . . . . .
H16 H 0.339637 -0.221961 0.248989 0.058 Uiso 1 1 calc R U . . .
C17 C 0.34803(16) 0.3155(3) -0.0283(3) 0.0482(14) Uani 1 1 d . . . . .
H17 H 0.331988 0.284540 -0.040922 0.058 Uiso 1 1 calc R U . . .
C18 C 0.34647(16) 0.3592(3) 0.0166(3) 0.0519(16) Uani 1 1 d . . . . .
H18 H 0.329567 0.357557 0.033214 0.062 Uiso 1 1 calc R U . . .
C19 C 0.37045(15) 0.4053(3) 0.0363(2) 0.0459(14) Uani 1 1 d . . . . .
C20 C 0.39492(16) 0.4050(3) 0.0106(3) 0.0498(15) Uani 1 1 d . . . . .
H20 H 0.411547 0.434817 0.023380 0.060 Uiso 1 1 calc R U . . .
C21 C 0.39501(16) 0.3602(3) -0.0346(3) 0.0486(15) Uani 1 1 d . . . . .
H21 H 0.411723 0.360792 -0.051831 0.058 Uiso 1 1 calc R U . . .
C22 C 0.36945(16) 0.4535(3) 0.0853(3) 0.0505(16) Uani 1 1 d . . . . .
C23 C 0.34087(17) 0.4765(3) 0.0900(3) 0.0537(16) Uani 1 1 d . . . . .
H23 H 0.321150 0.462006 0.062514 0.064 Uiso 1 1 calc R U . . .
C24 C 0.34081(16) 0.5215(3) 0.1355(3) 0.0546(16) Uani 1 1 d . . . . .
H24 H 0.321207 0.536614 0.138125 0.066 Uiso 1 1 calc R U . . .
C25 C 0.37063(16) 0.5439(3) 0.1774(3) 0.0495(15) Uani 1 1 d . . . . .
C26 C 0.39914(17) 0.5192(3) 0.1729(3) 0.0560(17) Uani 1 1 d . . . . .
H26 H 0.419015 0.532131 0.201141 0.067 Uiso 1 1 calc R U . . .
C27 C 0.39851(16) 0.4748(3) 0.1263(3) 0.0584(18) Uani 1 1 d . . . . .
H27 H 0.417988 0.459628 0.123038 0.070 Uiso 1 1 calc R U . . .
C28 C 0.37129(15) 0.5909(3) 0.2273(3) 0.0463(14) Uani 1 1 d . . . . .
C29 C 0.34771(16) 0.5923(3) 0.2564(3) 0.0497(15) Uani 1 1 d . . . . .
H29 H 0.330581 0.563480 0.244578 0.060 Uiso 1 1 calc R U . . .
C30 C 0.34959(16) 0.6365(3) 0.3030(3) 0.0464(14) Uani 1 1 d . . . . .
H30 H 0.333918 0.636215 0.322757 0.056 Uiso 1 1 calc R U . . .
C31 C 0.39667(16) 0.6784(3) 0.2924(3) 0.0497(15) Uani 1 1 d . . . . .
H31 H 0.413547 0.707760 0.304824 0.060 Uiso 1 1 calc R U . . .
C32 C 0.39658(17) 0.6358(3) 0.2466(3) 0.0527(16) Uani 1 1 d . . . . .
H32 H 0.412964 0.636523 0.228546 0.063 Uiso 1 1 calc R U . . .
C39 C 0.1982(2) 0.5113(4) 0.2009(4) 0.074(2) Uani 1 1 d . . . . .
B1 B 0.4799(2) 0.3455(4) 0.2493(4) 0.066(2) Uani 1 1 d . . . . .
B2 B 0.4895(2) 0.3173(5) 0.1818(4) 0.066(2) Uani 1 1 d . . . . .
B3 B 0.4601(2) 0.2754(4) 0.2058(4) 0.065(2) Uani 1 1 d . . . . .
B4 B 0.4897(2) 0.2334(4) 0.1825(4) 0.062(2) Uani 1 1 d . . . . .
B5 B 0.47901(19) 0.2078(4) 0.2483(4) 0.060(2) Uani 1 1 d . . . . .
B6 B 0.47184(19) 0.2757(4) 0.2900(4) 0.060(2) Uani 1 1 d . . . . .
B7 B 0.2608(2) 0.1776(4) 0.4783(3) 0.058(2) Uani 1 1 d . . . . .
B8 B 0.2292(2) 0.2248(4) 0.4266(3) 0.0565(19) Uani 1 1 d . . . . .
B9 B 0.20961(19) 0.2689(4) 0.4717(3) 0.0550(19) Uani 1 1 d . . . . .
B10 B 0.2381(2) 0.3057(4) 0.4427(3) 0.057(2) Uani 1 1 d . . . . .
B11 B 0.26962(18) 0.2500(4) 0.4463(3) 0.0509(17) Uani 1 1 d . . . . .
B12 B 0.2768(2) 0.3114(4) 0.5058(3) 0.057(2) Uani 1 1 d . . . . .
Cl1 Cl 0.45805(6) 0.41699(11) 0.24995(11) 0.0895(7) Uani 1 1 d . . . . .
Cl2 Cl 0.47779(5) 0.36381(13) 0.11099(9) 0.0915(7) Uani 1 1 d . . . . .
Cl3 Cl 0.41782(4) 0.27696(11) 0.15740(9) 0.0739(5) Uani 1 1 d . . . . .
Cl4 Cl 0.47933(5) 0.18944(12) 0.11065(10) 0.0862(7) Uani 1 1 d . . . . .
Cl04 Cl 0.29090(5) 0.25097(10) 0.39015(8) 0.0705(5) Uani 1 1 d . . . . .
Cl5 Cl 0.45678(5) 0.13522(10) 0.24583(12) 0.0820(6) Uani 1 1 d . . . . .
Cl6 Cl 0.27228(6) 0.10161(10) 0.45813(9) 0.0854(7) Uani 1 1 d . . . . .
Cl7 Cl 0.20636(5) 0.19696(11) 0.34871(7) 0.0756(6) Uani 1 1 d . . . . .
Cl07 Cl 0.44402(5) 0.27668(12) 0.33102(9) 0.0815(6) Uani 1 1 d . . . . .
Cl8 Cl 0.16719(5) 0.28789(12) 0.44404(9) 0.0807(6) Uani 1 1 d . . . . .
Cl9 Cl 0.22771(5) 0.36670(9) 0.38383(7) 0.0658(5) Uani 1 1 d . . . . .
Cl10 Cl 0.30430(6) 0.37458(12) 0.51138(9) 0.0871(7) Uani 1 1 d . . . . .
Cu1 Cu 0.37390(2) 0.25028(3) -0.11757(3) 0.04109(19) Uani 1 1 d . . . . .
N1 N 0.37448(12) 0.1817(2) -0.05522(19) 0.0417(11) Uani 1 1 d . . . . .
N2 N 0.37605(12) -0.1853(2) 0.31839(19) 0.0415(11) Uani 1 1 d . . . . .
N3 N 0.37164(12) 0.3162(2) -0.05395(19) 0.0398(11) Uani 1 1 d . . . . .
N4 N 0.37401(12) 0.6803(2) 0.32029(19) 0.0403(11) Uani 1 1 d . . . . .
O1S O 0.31272(10) 0.2462(2) -0.15930(18) 0.0513(10) Uani 1 1 d . . . . .
O2S O 0.19172(17) 0.4729(3) 0.1595(3) 0.101(2) Uani 1 1 d . . . . .
O3S O 0.43604(12) 0.2506(2) -0.07784(19) 0.0572(11) Uani 1 1 d . . . . .
O4S O 0.2918(2) 0.5490(4) 0.3287(5) 0.146(3) Uani 1 1 d . U . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C1 N1 1.342(7) . ?
C1 C2 1.378(8) . ?
C1 H1 0.9300 . ?
C2 C3 1.408(7) . ?
C2 H2 0.9300 . ?
C1S C2S 1.471(10) . ?
C1S H1SA 0.9600 . ?
C1S H1SB 0.9600 . ?
C1S H1SC 0.9600 . ?
C3 C4 1.379(8) . ?
C3 C6 1.490(8) . ?
C2S O1S 1.217(7) . ?
C2S C3S 1.495(9) . ?
C4 C5 1.380(8) . ?
C4 H4 0.9300 . ?
C3S H3SA 0.9600 . ?
C3S H3SB 0.9600 . ?
C3S H3SC 0.9600 . ?
C5 N1 1.369(7) . ?
C5 H5 0.9300 . ?
C4S C39 1.540(12) . ?
C4S H4SA 0.9600 . ?
C4S H4SB 0.9600 . ?
C4S H4SC 0.9600 . ?
C6 C7 1.367(9) . ?
C6 C11 1.398(8) . ?
C5S C7S 1.473(15) . ?
C5S H5SA 0.9600 . ?
C5S H5SB 0.9600 . ?
C5S H5SC 0.9600 . ?
C7 C8 1.416(8) . ?
C7 H7 0.9300 . ?
C6S C39 1.500(13) . ?
C6S H6SA 0.9600 . ?
C6S H6SB 0.9600 . ?
C6S H6SC 0.9600 . ?
C8 C9 1.420(8) . ?
C8 H8 0.9300 . ?
C7S O4S 1.193(11) . ?
C7S C8S 1.513(15) . ?
C9 C10 1.388(9) . ?
C9 C12 1.480(8) . ?
C8S H8SA 0.9600 . ?
C8S H8SB 0.9600 . ?
C8S H8SC 0.9600 . ?
C10 C11 1.377(8) . ?
C10 H10 0.9300 . ?
C9S C10S 1.479(13) . ?
C9S H9SA 0.9600 . ?
C9S H9SB 0.9600 . ?
C9S H9SC 0.9600 . ?
C11 H11 0.9300 . ?
C10S O3S 1.207(9) . ?
C10S C11S 1.545(13) . ?
C12 C15 1.397(8) . ?
C12 C13 1.409(8) . ?
C11S H11A 0.9600 . ?
C11S H11B 0.9600 . ?
C11S H11C 0.9600 . ?
C13 C14 1.361(8) . ?
C13 H13 0.9300 . ?
C14 N2 1.336(7) . ?
C14 H14 0.9300 . ?
C15 C16 1.375(8) . ?
C15 H15 0.9300 . ?
C16 N2 1.358(7) . ?
C16 H16 0.9300 . ?
C17 N3 1.335(8) . ?
C17 C18 1.387(8) . ?
C17 H17 0.9300 . ?
C18 C19 1.389(9) . ?
C18 H18 0.9300 . ?
C19 C20 1.370(9) . ?
C19 C22 1.515(8) . ?
C20 C21 1.394(8) . ?
C20 H20 0.9300 . ?
C21 N3 1.338(8) . ?
C21 H21 0.9300 . ?
C22 C23 1.371(9) . ?
C22 C27 1.373(9) . ?
C23 C24 1.399(8) . ?
C23 H23 0.9300 . ?
C24 C25 1.411(9) . ?
C24 H24 0.9300 . ?
C25 C26 1.378(9) . ?
C25 C28 1.495(8) . ?
C26 C27 1.405(8) . ?
C26 H26 0.9300 . ?
C27 H27 0.9300 . ?
C28 C29 1.388(9) . ?
C28 C32 1.408(9) . ?
C29 C30 1.389(8) . ?
C29 H29 0.9300 . ?
C30 N4 1.365(8) . ?
C30 H30 0.9300 . ?
C31 N4 1.333(8) . ?
C31 C32 1.371(8) . ?
C31 H31 0.9300 . ?
C32 H32 0.9300 . ?
C39 O2S 1.199(9) . ?
B1 B1 1.739(18) 2_655 ?
B1 B2 1.784(11) 2_655 ?
B1 Cl1 1.786(9) . ?
B1 B2 1.808(13) . ?
B1 B3 1.827(12) . ?
B1 B6 1.830(13) . ?
B2 B4 1.770(13) . ?
B2 B3 1.778(14) . ?
B2 Cl2 1.802(8) . ?
B2 B6 1.817(12) 2_655 ?
B3 B5 1.767(12) . ?
B3 B4 1.780(13) . ?
B3 B6 1.800(11) . ?
B3 Cl3 1.802(8) . ?
B4 B5 1.782(12) . ?
B4 B5 1.786(11) 2_655 ?
B4 Cl4 1.793(8) . ?
B4 B6 1.815(11) 2_655 ?
B5 B6 1.797(12) . ?
B5 Cl5 1.802(8) . ?
B5 B5 1.802(17) 2_655 ?
B6 Cl07 1.750(9) . ?
B7 Cl6 1.782(8) . ?
B7 B11 1.785(12) . ?
B7 B8 1.786(11) . ?
B7 B12 1.801(12) 7_556 ?
B7 B9 1.803(11) 7_556 ?
B7 B10 1.804(10) 7_556 ?
B8 B11 1.747(11) . ?
B8 B10 1.762(12) . ?
B8 B9 1.790(11) . ?
B8 B12 1.802(11) 7_556 ?
B8 Cl7 1.811(7) . ?
B9 B10 1.762(12) . ?
B9 Cl8 1.787(8) . ?
B9 B12 1.813(12) 7_556 ?
B9 B11 1.817(9) 7_556 ?
B10 B11 1.787(11) . ?
B10 Cl9 1.799(8) . ?
B10 B12 1.815(11) . ?
B11 Cl04 1.799(7) . ?
B11 B12 1.820(11) . ?
B12 Cl10 1.767(9) . ?
Cu1 N1 2.015(4) . ?
Cu1 N2 2.018(4) 6 ?
Cu1 N3 2.027(4) . ?
Cu1 N4 2.030(4) 6_565 ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N1 C1 C2 124.2(5) . . ?
N1 C1 H1 117.9 . . ?
C2 C1 H1 117.9 . . ?
C1 C2 C3 118.9(6) . . ?
C1 C2 H2 120.6 . . ?
C3 C2 H2 120.6 . . ?
C2S C1S H1SA 109.5 . . ?
C2S C1S H1SB 109.5 . . ?
H1SA C1S H1SB 109.5 . . ?
C2S C1S H1SC 109.5 . . ?
H1SA C1S H1SC 109.5 . . ?
H1SB C1S H1SC 109.5 . . ?
C4 C3 C2 116.8(5) . . ?
C4 C3 C6 122.4(5) . . ?
C2 C3 C6 120.9(5) . . ?
O1S C2S C1S 122.9(6) . . ?
O1S C2S C3S 121.8(6) . . ?
C1S C2S C3S 115.3(6) . . ?
C3 C4 C5 121.9(5) . . ?
C3 C4 H4 119.1 . . ?
C5 C4 H4 119.1 . . ?
C2S C3S H3SA 109.5 . . ?
C2S C3S H3SB 109.5 . . ?
H3SA C3S H3SB 109.5 . . ?
C2S C3S H3SC 109.5 . . ?
H3SA C3S H3SC 109.5 . . ?
H3SB C3S H3SC 109.5 . . ?
N1 C5 C4 121.0(5) . . ?
N1 C5 H5 119.5 . . ?
C4 C5 H5 119.5 . . ?
C39 C4S H4SA 109.5 . . ?
C39 C4S H4SB 109.5 . . ?
H4SA C4S H4SB 109.5 . . ?
C39 C4S H4SC 109.5 . . ?
H4SA C4S H4SC 109.5 . . ?
H4SB C4S H4SC 109.5 . . ?
C7 C6 C11 117.9(5) . . ?
C7 C6 C3 121.6(5) . . ?
C11 C6 C3 120.4(6) . . ?
C7S C5S H5SA 109.5 . . ?
C7S C5S H5SB 109.5 . . ?
H5SA C5S H5SB 109.5 . . ?
C7S C5S H5SC 109.5 . . ?
H5SA C5S H5SC 109.5 . . ?
H5SB C5S H5SC 109.5 . . ?
C6 C7 C8 122.6(6) . . ?
C6 C7 H7 118.7 . . ?
C8 C7 H7 118.7 . . ?
C39 C6S H6SA 109.5 . . ?
C39 C6S H6SB 109.5 . . ?
H6SA C6S H6SB 109.5 . . ?
C39 C6S H6SC 109.5 . . ?
H6SA C6S H6SC 109.5 . . ?
H6SB C6S H6SC 109.5 . . ?
C7 C8 C9 118.1(6) . . ?
C7 C8 H8 121.0 . . ?
C9 C8 H8 121.0 . . ?
O4S C7S C5S 121.9(11) . . ?
O4S C7S C8S 123.8(12) . . ?
C5S C7S C8S 114.3(11) . . ?
C10 C9 C8 118.8(5) . . ?
C10 C9 C12 122.8(5) . . ?
C8 C9 C12 118.4(6) . . ?
C7S C8S H8SA 109.5 . . ?
C7S C8S H8SB 109.5 . . ?
H8SA C8S H8SB 109.5 . . ?
C7S C8S H8SC 109.5 . . ?
H8SA C8S H8SC 109.5 . . ?
H8SB C8S H8SC 109.5 . . ?
C11 C10 C9 121.2(6) . . ?
C11 C10 H10 119.4 . . ?
C9 C10 H10 119.4 . . ?
C10S C9S H9SA 109.5 . . ?
C10S C9S H9SB 109.5 . . ?
H9SA C9S H9SB 109.5 . . ?
C10S C9S H9SC 109.5 . . ?
H9SA C9S H9SC 109.5 . . ?
H9SB C9S H9SC 109.5 . . ?
C10 C11 C6 121.4(6) . . ?
C10 C11 H11 119.3 . . ?
C6 C11 H11 119.3 . . ?
O3S C10S C9S 123.1(9) . . ?
O3S C10S C11S 122.1(8) . . ?
C9S C10S C11S 114.7(9) . . ?
C15 C12 C13 114.6(5) . . ?
C15 C12 C9 122.4(5) . . ?
C13 C12 C9 123.1(6) . . ?
C10S C11S H11A 109.5 . . ?
C10S C11S H11B 109.5 . . ?
H11A C11S H11B 109.5 . . ?
C10S C11S H11C 109.5 . . ?
H11A C11S H11C 109.5 . . ?
H11B C11S H11C 109.5 . . ?
C14 C13 C12 120.6(6) . . ?
C14 C13 H13 119.7 . . ?
C12 C13 H13 119.7 . . ?
N2 C14 C13 124.5(5) . . ?
N2 C14 H14 117.8 . . ?
C13 C14 H14 117.8 . . ?
C16 C15 C12 121.8(5) . . ?
C16 C15 H15 119.1 . . ?
C12 C15 H15 119.1 . . ?
N2 C16 C15 122.2(6) . . ?
N2 C16 H16 118.9 . . ?
C15 C16 H16 118.9 . . ?
N3 C17 C18 122.6(6) . . ?
N3 C17 H17 118.7 . . ?
C18 C17 H17 118.7 . . ?
C17 C18 C19 119.2(6) . . ?
C17 C18 H18 120.4 . . ?
C19 C18 H18 120.4 . . ?
C20 C19 C18 117.8(6) . . ?
C20 C19 C22 121.8(6) . . ?
C18 C19 C22 120.4(6) . . ?
C19 C20 C21 120.3(6) . . ?
C19 C20 H20 119.9 . . ?
C21 C20 H20 119.9 . . ?
N3 C21 C20 121.6(6) . . ?
N3 C21 H21 119.2 . . ?
C20 C21 H21 119.2 . . ?
C23 C22 C27 119.3(6) . . ?
C23 C22 C19 122.7(6) . . ?
C27 C22 C19 118.1(6) . . ?
C22 C23 C24 121.2(6) . . ?
C22 C23 H23 119.4 . . ?
C24 C23 H23 119.4 . . ?
C23 C24 C25 119.7(6) . . ?
C23 C24 H24 120.1 . . ?
C25 C24 H24 120.1 . . ?
C26 C25 C24 118.3(6) . . ?
C26 C25 C28 120.8(6) . . ?
C24 C25 C28 120.8(6) . . ?
C25 C26 C27 120.8(6) . . ?
C25 C26 H26 119.6 . . ?
C27 C26 H26 119.6 . . ?
C22 C27 C26 120.7(6) . . ?
C22 C27 H27 119.7 . . ?
C26 C27 H27 119.7 . . ?
C29 C28 C32 117.6(5) . . ?
C29 C28 C25 122.4(6) . . ?
C32 C28 C25 120.0(6) . . ?
C28 C29 C30 120.3(6) . . ?
C28 C29 H29 119.9 . . ?
C30 C29 H29 119.9 . . ?
N4 C30 C29 121.3(6) . . ?
N4 C30 H30 119.4 . . ?
C29 C30 H30 119.4 . . ?
N4 C31 C32 123.9(6) . . ?
N4 C31 H31 118.1 . . ?
C32 C31 H31 118.1 . . ?
C31 C32 C28 118.9(6) . . ?
C31 C32 H32 120.5 . . ?
C28 C32 H32 120.5 . . ?
O2S C39 C6S 121.3(8) . . ?
O2S C39 C4S 124.1(9) . . ?
C6S C39 C4S 114.4(8) . . ?
B1 B1 B2 61.7(5) 2_655 2_655 ?
B1 B1 Cl1 122.3(3) 2_655 . ?
B2 B1 Cl1 121.4(6) 2_655 . ?
B1 B1 B2 60.4(6) 2_655 . ?
B2 B1 B2 108.2(6) 2_655 . ?
Cl1 B1 B2 123.8(6) . . ?
B1 B1 B3 107.6(6) 2_655 . ?
B2 B1 B3 106.5(6) 2_655 . ?
Cl1 B1 B3 122.0(5) . . ?
B2 B1 B3 58.6(5) . . ?
B1 B1 B6 110.4(5) 2_655 . ?
B2 B1 B6 60.4(5) 2_655 . ?
Cl1 B1 B6 119.1(6) . . ?
B2 B1 B6 107.1(6) . . ?
B3 B1 B6 59.0(5) . . ?
B4 B2 B3 60.2(5) . . ?
B4 B2 B1 109.0(6) . 2_655 ?
B3 B2 B1 107.8(6) . 2_655 ?
B4 B2 Cl2 123.4(6) . . ?
B3 B2 Cl2 121.3(5) . . ?
B1 B2 Cl2 120.3(6) 2_655 . ?
B4 B2 B1 108.9(6) . . ?
B3 B2 B1 61.2(5) . . ?
B1 B2 B1 57.9(6) 2_655 . ?
Cl2 B2 B1 119.6(6) . . ?
B4 B2 B6 60.8(5) . 2_655 ?
B3 B2 B6 109.2(6) . 2_655 ?
B1 B2 B6 61.1(5) 2_655 2_655 ?
Cl2 B2 B6 122.2(6) . 2_655 ?
B1 B2 B6 107.9(5) . 2_655 ?
B5 B3 B2 108.3(6) . . ?
B5 B3 B4 60.3(5) . . ?
B2 B3 B4 59.7(5) . . ?
B5 B3 B6 60.5(5) . . ?
B2 B3 B6 109.7(6) . . ?
B4 B3 B6 109.4(5) . . ?
B5 B3 Cl3 122.9(6) . . ?
B2 B3 Cl3 119.9(5) . . ?
B4 B3 Cl3 121.5(5) . . ?
B6 B3 Cl3 121.3(6) . . ?
B5 B3 B1 108.0(5) . . ?
B2 B3 B1 60.2(5) . . ?
B4 B3 B1 107.7(6) . . ?
B6 B3 B1 60.6(5) . . ?
Cl3 B3 B1 121.2(6) . . ?
B2 B4 B3 60.1(5) . . ?
B2 B4 B5 108.0(6) . . ?
B3 B4 B5 59.5(5) . . ?
B2 B4 B5 108.1(5) . 2_655 ?
B3 B4 B5 108.0(6) . 2_655 ?
B5 B4 B5 60.7(6) . 2_655 ?
B2 B4 Cl4 120.8(6) . . ?
B3 B4 Cl4 122.3(5) . . ?
B5 B4 Cl4 122.7(6) . . ?
B5 B4 Cl4 121.8(6) 2_655 . ?
B2 B4 B6 60.9(5) . 2_655 ?
B3 B4 B6 109.2(6) . 2_655 ?
B5 B4 B6 109.1(5) . 2_655 ?
B5 B4 B6 59.9(4) 2_655 2_655 ?
Cl4 B4 B6 119.6(6) . 2_655 ?
B3 B5 B4 60.2(5) . . ?
B3 B5 B4 108.4(6) . 2_655 ?
B4 B5 B4 107.8(6) . 2_655 ?
B3 B5 B6 60.6(5) . . ?
B4 B5 B6 109.4(6) . . ?
B4 B5 B6 60.9(5) 2_655 . ?
B3 B5 Cl5 121.4(5) . . ?
B4 B5 Cl5 121.1(6) . . ?
B4 B5 Cl5 122.1(6) 2_655 . ?
B6 B5 Cl5 120.7(6) . . ?
B3 B5 B5 107.9(6) . 2_655 ?
B4 B5 B5 59.8(5) . 2_655 ?
B4 B5 B5 59.6(5) 2_655 2_655 ?
B6 B5 B5 109.0(5) . 2_655 ?
Cl5 B5 B5 121.8(3) . 2_655 ?
Cl07 B6 B5 123.8(6) . . ?
Cl07 B6 B3 123.7(5) . . ?
B5 B6 B3 58.8(5) . . ?
Cl07 B6 B4 122.9(5) . 2_655 ?
B5 B6 B4 59.3(5) . 2_655 ?
B3 B6 B4 105.7(6) . 2_655 ?
Cl07 B6 B2 122.0(5) . 2_655 ?
B5 B6 B2 105.6(6) . 2_655 ?
B3 B6 B2 106.3(6) . 2_655 ?
B4 B6 B2 58.3(5) 2_655 2_655 ?
Cl07 B6 B1 122.4(6) . . ?
B5 B6 B1 106.5(6) . . ?
B3 B6 B1 60.4(5) . . ?
B4 B6 B1 105.1(6) 2_655 . ?
B2 B6 B1 58.6(5) 2_655 . ?
Cl6 B7 B11 123.5(5) . . ?
Cl6 B7 B8 123.7(5) . . ?
B11 B7 B8 58.6(4) . . ?
Cl6 B7 B12 121.0(6) . 7_556 ?
B11 B7 B12 107.5(6) . 7_556 ?
B8 B7 B12 60.3(4) . 7_556 ?
Cl6 B7 B9 121.5(5) . 7_556 ?
B11 B7 B9 60.9(4) . 7_556 ?
B8 B7 B9 107.2(6) . 7_556 ?
B12 B7 B9 107.6(5) 7_556 7_556 ?
Cl6 B7 B10 120.7(5) . 7_556 ?
B11 B7 B10 107.1(6) . 7_556 ?
B8 B7 B10 107.5(6) . 7_556 ?
B12 B7 B10 60.5(4) 7_556 7_556 ?
B9 B7 B10 58.5(4) 7_556 7_556 ?
B11 B8 B10 61.2(5) . . ?
B11 B8 B7 60.7(5) . . ?
B10 B8 B7 109.6(5) . . ?
B11 B8 B9 108.9(5) . . ?
B10 B8 B9 59.5(5) . . ?
B7 B8 B9 109.0(5) . . ?
B11 B8 B12 109.1(5) . 7_556 ?
B10 B8 B12 108.6(5) . 7_556 ?
B7 B8 B12 60.3(5) . 7_556 ?
B9 B8 B12 60.6(5) . 7_556 ?
B11 B8 Cl7 122.0(5) . . ?
B10 B8 Cl7 121.9(5) . . ?
B7 B8 Cl7 120.8(5) . . ?
B9 B8 Cl7 120.7(5) . . ?
B12 B8 Cl7 120.0(6) 7_556 . ?
B10 B9 Cl8 122.9(5) . . ?
B10 B9 B8 59.5(5) . . ?
Cl8 B9 B8 123.2(5) . . ?
B10 B9 B7 60.8(4) . 7_556 ?
Cl8 B9 B7 121.3(5) . 7_556 ?
B8 B9 B7 107.9(6) . 7_556 ?
B10 B9 B12 108.2(6) . 7_556 ?
Cl8 B9 B12 120.8(6) . 7_556 ?
B8 B9 B12 60.0(4) . 7_556 ?
B7 B9 B12 108.2(5) 7_556 7_556 ?
B10 B9 B11 107.5(5) . 7_556 ?
Cl8 B9 B11 121.0(5) . 7_556 ?
B8 B9 B11 107.2(5) . 7_556 ?
B7 B9 B11 59.1(4) 7_556 7_556 ?
B12 B9 B11 60.2(4) 7_556 7_556 ?
B9 B10 B8 61.0(5) . . ?
B9 B10 B11 108.4(6) . . ?
B8 B10 B11 59.0(5) . . ?
B9 B10 Cl9 123.6(5) . . ?
B8 B10 Cl9 123.8(5) . . ?
B11 B10 Cl9 120.5(5) . . ?
B9 B10 B7 60.7(4) . 7_556 ?
B8 B10 B7 109.1(5) . 7_556 ?
B11 B10 B7 108.3(5) . 7_556 ?
Cl9 B10 B7 120.6(5) . 7_556 ?
B9 B10 B12 108.7(5) . . ?
B8 B10 B12 108.1(5) . . ?
B11 B10 B12 60.7(4) . . ?
Cl9 B10 B12 118.4(6) . . ?
B7 B10 B12 59.7(4) 7_556 . ?
B8 B11 B7 60.7(5) . . ?
B8 B11 B10 59.8(5) . . ?
B7 B11 B10 108.6(5) . . ?
B8 B11 Cl04 122.1(5) . . ?
B7 B11 Cl04 121.6(5) . . ?
B10 B11 Cl04 121.6(5) . . ?
B8 B11 B9 108.3(5) . 7_556 ?
B7 B11 B9 60.0(4) . 7_556 ?
B10 B11 B9 107.9(5) . 7_556 ?
Cl04 B11 B9 121.5(5) . 7_556 ?
B8 B11 B12 108.6(5) . . ?
B7 B11 B12 108.6(5) . . ?
B10 B11 B12 60.4(4) . . ?
Cl04 B11 B12 120.6(5) . . ?
B9 B11 B12 59.8(4) 7_556 . ?
Cl10 B12 B7 121.7(6) . 7_556 ?
Cl10 B12 B8 122.9(5) . 7_556 ?
B7 B12 B8 59.5(4) 7_556 7_556 ?
Cl10 B12 B9 122.3(5) . 7_556 ?
B7 B12 B9 107.4(6) 7_556 7_556 ?
B8 B12 B9 59.4(4) 7_556 7_556 ?
Cl10 B12 B10 122.5(5) . . ?
B7 B12 B10 59.9(4) 7_556 . ?
B8 B12 B10 106.4(6) 7_556 . ?
B9 B12 B10 106.8(6) 7_556 . ?
Cl10 B12 B11 122.5(5) . . ?
B7 B12 B11 107.0(5) 7_556 . ?
B8 B12 B11 106.6(6) 7_556 . ?
B9 B12 B11 60.0(4) 7_556 . ?
B10 B12 B11 58.9(4) . . ?
N1 Cu1 N2 91.11(18) . 6 ?
N1 Cu1 N3 89.45(17) . . ?
N2 Cu1 N3 179.43(18) 6 . ?
N1 Cu1 N4 179.2(2) . 6_565 ?
N2 Cu1 N4 89.07(18) 6 6_565 ?
N3 Cu1 N4 90.37(18) . 6_565 ?
C1 N1 C5 117.2(5) . . ?
C1 N1 Cu1 123.2(4) . . ?
C5 N1 Cu1 119.6(4) . . ?
C14 N2 C16 116.3(5) . . ?
C14 N2 Cu1 124.4(4) . 6_556 ?
C16 N2 Cu1 119.3(4) . 6_556 ?
C17 N3 C21 118.4(5) . . ?
C17 N3 Cu1 121.6(4) . . ?
C21 N3 Cu1 119.9(4) . . ?
C31 N4 C30 118.1(5) . . ?
C31 N4 Cu1 121.2(4) . 6_566 ?
C30 N4 Cu1 120.6(4) . 6_566 ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
N1 C1 C2 C3 -0.9(10) . . . . ?
C1 C2 C3 C4 -0.1(10) . . . . ?
C1 C2 C3 C6 -179.9(6) . . . . ?
C2 C3 C4 C5 -0.7(10) . . . . ?
C6 C3 C4 C5 179.0(6) . . . . ?
C3 C4 C5 N1 2.5(10) . . . . ?
C4 C3 C6 C7 152.5(7) . . . . ?
C2 C3 C6 C7 -27.7(10) . . . . ?
C4 C3 C6 C11 -25.4(10) . . . . ?
C2 C3 C6 C11 154.4(7) . . . . ?
C11 C6 C7 C8 0.8(11) . . . . ?
C3 C6 C7 C8 -177.1(6) . . . . ?
C6 C7 C8 C9 0.1(11) . . . . ?
C7 C8 C9 C10 -1.1(10) . . . . ?
C7 C8 C9 C12 178.2(6) . . . . ?
C8 C9 C10 C11 1.0(11) . . . . ?
C12 C9 C10 C11 -178.2(7) . . . . ?
C9 C10 C11 C6 0.0(12) . . . . ?
C7 C6 C11 C10 -0.9(11) . . . . ?
C3 C6 C11 C10 177.1(7) . . . . ?
C10 C9 C12 C15 -154.3(7) . . . . ?
C8 C9 C12 C15 26.4(10) . . . . ?
C10 C9 C12 C13 23.7(11) . . . . ?
C8 C9 C12 C13 -155.6(7) . . . . ?
C15 C12 C13 C14 -2.0(10) . . . . ?
C9 C12 C13 C14 179.9(7) . . . . ?
C12 C13 C14 N2 0.7(11) . . . . ?
C13 C12 C15 C16 2.4(10) . . . . ?
C9 C12 C15 C16 -179.4(6) . . . . ?
C12 C15 C16 N2 -1.6(10) . . . . ?
N3 C17 C18 C19 -0.6(9) . . . . ?
C17 C18 C19 C20 -0.6(9) . . . . ?
C17 C18 C19 C22 -179.8(5) . . . . ?
C18 C19 C20 C21 1.1(9) . . . . ?
C22 C19 C20 C21 -179.7(5) . . . . ?
C19 C20 C21 N3 -0.4(9) . . . . ?
C20 C19 C22 C23 147.1(6) . . . . ?
C18 C19 C22 C23 -33.7(9) . . . . ?
C20 C19 C22 C27 -32.6(9) . . . . ?
C18 C19 C22 C27 146.6(7) . . . . ?
C27 C22 C23 C24 0.3(10) . . . . ?
C19 C22 C23 C24 -179.4(6) . . . . ?
C22 C23 C24 C25 0.1(10) . . . . ?
C23 C24 C25 C26 -1.5(10) . . . . ?
C23 C24 C25 C28 -178.8(6) . . . . ?
C24 C25 C26 C27 2.5(10) . . . . ?
C28 C25 C26 C27 179.7(6) . . . . ?
C23 C22 C27 C26 0.6(11) . . . . ?
C19 C22 C27 C26 -179.7(6) . . . . ?
C25 C26 C27 C22 -2.1(11) . . . . ?
C26 C25 C28 C29 -144.5(7) . . . . ?
C24 C25 C28 C29 32.7(9) . . . . ?
C26 C25 C28 C32 35.1(9) . . . . ?
C24 C25 C28 C32 -147.7(6) . . . . ?
C32 C28 C29 C30 -0.4(9) . . . . ?
C25 C28 C29 C30 179.2(5) . . . . ?
C28 C29 C30 N4 1.5(9) . . . . ?
N4 C31 C32 C28 -0.1(10) . . . . ?
C29 C28 C32 C31 -0.3(9) . . . . ?
C25 C28 C32 C31 -179.9(6) . . . . ?
B1 B1 B2 B4 101.0(5) 2_655 . . . ?
B2 B1 B2 B4 60.5(7) 2_655 . . . ?
Cl1 B1 B2 B4 -147.9(6) . . . . ?
B3 B1 B2 B4 -38.1(5) . . . . ?
B6 B1 B2 B4 -3.1(7) . . . . ?
B1 B1 B2 B3 139.1(5) 2_655 . . . ?
B2 B1 B2 B3 98.6(6) 2_655 . . . ?
Cl1 B1 B2 B3 -109.8(7) . . . . ?
B6 B1 B2 B3 35.0(5) . . . . ?
B2 B1 B2 B1 -40.5(8) 2_655 . . 2_655 ?
Cl1 B1 B2 B1 111.0(5) . . . 2_655 ?
B3 B1 B2 B1 -139.1(5) . . . 2_655 ?
B6 B1 B2 B1 -104.2(5) . . . 2_655 ?
B1 B1 B2 Cl2 -109.2(7) 2_655 . . . ?
B2 B1 B2 Cl2 -149.7(6) 2_655 . . . ?
Cl1 B1 B2 Cl2 1.9(10) . . . . ?
B3 B1 B2 Cl2 111.7(7) . . . . ?
B6 B1 B2 Cl2 146.7(6) . . . . ?
B1 B1 B2 B6 36.6(5) 2_655 . . 2_655 ?
B2 B1 B2 B6 -3.9(10) 2_655 . . 2_655 ?
Cl1 B1 B2 B6 147.6(6) . . . 2_655 ?
B3 B1 B2 B6 -102.5(7) . . . 2_655 ?
B6 B1 B2 B6 -67.5(8) . . . 2_655 ?
B4 B2 B3 B5 37.1(5) . . . . ?
B1 B2 B3 B5 -65.1(8) 2_655 . . . ?
Cl2 B2 B3 B5 150.4(6) . . . . ?
B1 B2 B3 B5 -100.7(6) . . . . ?
B6 B2 B3 B5 -0.3(8) 2_655 . . . ?
B1 B2 B3 B4 -102.2(6) 2_655 . . . ?
Cl2 B2 B3 B4 113.3(7) . . . . ?
B1 B2 B3 B4 -137.8(6) . . . . ?
B6 B2 B3 B4 -37.4(5) 2_655 . . . ?
B4 B2 B3 B6 101.5(6) . . . . ?
B1 B2 B3 B6 -0.7(8) 2_655 . . . ?
Cl2 B2 B3 B6 -145.2(6) . . . . ?
B1 B2 B3 B6 -36.3(6) . . . . ?
B6 B2 B3 B6 64.1(7) 2_655 . . . ?
B4 B2 B3 Cl3 -111.2(6) . . . . ?
B1 B2 B3 Cl3 146.7(6) 2_655 . . . ?
Cl2 B2 B3 Cl3 2.1(10) . . . . ?
B1 B2 B3 Cl3 111.0(7) . . . . ?
B6 B2 B3 Cl3 -148.6(6) 2_655 . . . ?
B4 B2 B3 B1 137.8(6) . . . . ?
B1 B2 B3 B1 35.6(5) 2_655 . . . ?
Cl2 B2 B3 B1 -109.0(7) . . . . ?
B6 B2 B3 B1 100.4(6) 2_655 . . . ?
B1 B1 B3 B5 64.6(9) 2_655 . . . ?
B2 B1 B3 B5 -0.3(9) 2_655 . . . ?
Cl1 B1 B3 B5 -146.1(6) . . . . ?
B2 B1 B3 B5 101.2(7) . . . . ?
B6 B1 B3 B5 -39.0(6) . . . . ?
B1 B1 B3 B2 -36.7(6) 2_655 . . . ?
B2 B1 B3 B2 -101.5(6) 2_655 . . . ?
Cl1 B1 B3 B2 112.7(7) . . . . ?
B6 B1 B3 B2 -140.3(6) . . . . ?
B1 B1 B3 B4 0.9(9) 2_655 . . . ?
B2 B1 B3 B4 -64.0(8) 2_655 . . . ?
Cl1 B1 B3 B4 150.2(6) . . . . ?
B2 B1 B3 B4 37.5(6) . . . . ?
B6 B1 B3 B4 -102.7(6) . . . . ?
B1 B1 B3 B6 103.6(7) 2_655 . . . ?
B2 B1 B3 B6 38.7(6) 2_655 . . . ?
Cl1 B1 B3 B6 -107.0(7) . . . . ?
B2 B1 B3 B6 140.3(6) . . . . ?
B1 B1 B3 Cl3 -145.6(6) 2_655 . . . ?
B2 B1 B3 Cl3 149.5(6) 2_655 . . . ?
Cl1 B1 B3 Cl3 3.7(10) . . . . ?
B2 B1 B3 Cl3 -109.0(7) . . . . ?
B6 B1 B3 Cl3 110.8(7) . . . . ?
B1 B2 B4 B3 100.1(7) 2_655 . . . ?
Cl2 B2 B4 B3 -109.8(7) . . . . ?
B1 B2 B4 B3 38.5(5) . . . . ?
B6 B2 B4 B3 138.9(5) 2_655 . . . ?
B3 B2 B4 B5 -36.6(5) . . . . ?
B1 B2 B4 B5 63.5(8) 2_655 . . . ?
Cl2 B2 B4 B5 -146.5(6) . . . . ?
B1 B2 B4 B5 1.9(7) . . . . ?
B6 B2 B4 B5 102.3(6) 2_655 . . . ?
B3 B2 B4 B5 -100.8(6) . . . 2_655 ?
B1 B2 B4 B5 -0.7(9) 2_655 . . 2_655 ?
Cl2 B2 B4 B5 149.4(6) . . . 2_655 ?
B1 B2 B4 B5 -62.3(8) . . . 2_655 ?
B6 B2 B4 B5 38.1(6) 2_655 . . 2_655 ?
B3 B2 B4 Cl4 112.0(6) . . . . ?
B1 B2 B4 Cl4 -147.9(6) 2_655 . . . ?
Cl2 B2 B4 Cl4 2.2(10) . . . . ?
B1 B2 B4 Cl4 150.5(5) . . . . ?
B6 B2 B4 Cl4 -109.1(7) 2_655 . . . ?
B3 B2 B4 B6 -138.9(5) . . . 2_655 ?
B1 B2 B4 B6 -38.8(6) 2_655 . . 2_655 ?
Cl2 B2 B4 B6 111.2(7) . . . 2_655 ?
B1 B2 B4 B6 -100.4(6) . . . 2_655 ?
B5 B3 B4 B2 -138.8(6) . . . . ?
B6 B3 B4 B2 -102.0(6) . . . . ?
Cl3 B3 B4 B2 108.6(7) . . . . ?
B1 B3 B4 B2 -37.7(5) . . . . ?
B2 B3 B4 B5 138.8(6) . . . . ?
B6 B3 B4 B5 36.8(6) . . . . ?
Cl3 B3 B4 B5 -112.6(7) . . . . ?
B1 B3 B4 B5 101.0(6) . . . . ?
B5 B3 B4 B5 -37.8(5) . . . 2_655 ?
B2 B3 B4 B5 100.9(6) . . . 2_655 ?
B6 B3 B4 B5 -1.0(9) . . . 2_655 ?
Cl3 B3 B4 B5 -150.4(6) . . . 2_655 ?
B1 B3 B4 B5 63.2(8) . . . 2_655 ?
B5 B3 B4 Cl4 111.7(7) . . . . ?
B2 B3 B4 Cl4 -109.6(7) . . . . ?
B6 B3 B4 Cl4 148.4(6) . . . . ?
Cl3 B3 B4 Cl4 -0.9(11) . . . . ?
B1 B3 B4 Cl4 -147.3(6) . . . . ?
B5 B3 B4 B6 -101.3(6) . . . 2_655 ?
B2 B3 B4 B6 37.4(5) . . . 2_655 ?
B6 B3 B4 B6 -64.6(7) . . . 2_655 ?
Cl3 B3 B4 B6 146.0(6) . . . 2_655 ?
B1 B3 B4 B6 -0.3(8) . . . 2_655 ?
B2 B3 B5 B4 -36.8(5) . . . . ?
B6 B3 B5 B4 -139.6(6) . . . . ?
Cl3 B3 B5 B4 110.3(7) . . . . ?
B1 B3 B5 B4 -100.5(7) . . . . ?
B2 B3 B5 B4 63.6(8) . . . 2_655 ?
B4 B3 B5 B4 100.4(6) . . . 2_655 ?
B6 B3 B5 B4 -39.1(6) . . . 2_655 ?
Cl3 B3 B5 B4 -149.3(6) . . . 2_655 ?
B1 B3 B5 B4 -0.1(9) . . . 2_655 ?
B2 B3 B5 B6 102.8(6) . . . . ?
B4 B3 B5 B6 139.6(6) . . . . ?
Cl3 B3 B5 B6 -110.1(7) . . . . ?
B1 B3 B5 B6 39.1(6) . . . . ?
B2 B3 B5 Cl5 -147.2(6) . . . . ?
B4 B3 B5 Cl5 -110.4(7) . . . . ?
B6 B3 B5 Cl5 110.0(7) . . . . ?
Cl3 B3 B5 Cl5 -0.1(10) . . . . ?
B1 B3 B5 Cl5 149.1(6) . . . . ?
B2 B3 B5 B5 0.6(9) . . . 2_655 ?
B4 B3 B5 B5 37.4(6) . . . 2_655 ?
B6 B3 B5 B5 -102.2(7) . . . 2_655 ?
Cl3 B3 B5 B5 147.7(6) . . . 2_655 ?
B1 B3 B5 B5 -63.1(9) . . . 2_655 ?
B2 B4 B5 B3 36.9(5) . . . . ?
B5 B4 B5 B3 138.0(5) 2_655 . . . ?
Cl4 B4 B5 B3 -111.0(7) . . . . ?
B6 B4 B5 B3 101.5(7) 2_655 . . . ?
B2 B4 B5 B4 -64.5(7) . . . 2_655 ?
B3 B4 B5 B4 -101.4(6) . . . 2_655 ?
B5 B4 B5 B4 36.6(7) 2_655 . . 2_655 ?
Cl4 B4 B5 B4 147.6(6) . . . 2_655 ?
B6 B4 B5 B4 0.1(9) 2_655 . . 2_655 ?
B2 B4 B5 B6 0.1(7) . . . . ?
B3 B4 B5 B6 -36.8(5) . . . . ?
B5 B4 B5 B6 101.2(6) 2_655 . . . ?
Cl4 B4 B5 B6 -147.8(6) . . . . ?
B6 B4 B5 B6 64.7(8) 2_655 . . . ?
B2 B4 B5 Cl5 147.8(5) . . . . ?
B3 B4 B5 Cl5 110.8(6) . . . . ?
B5 B4 B5 Cl5 -111.1(4) 2_655 . . . ?
Cl4 B4 B5 Cl5 -0.1(9) . . . . ?
B6 B4 B5 Cl5 -147.7(6) 2_655 . . . ?
B2 B4 B5 B5 -101.1(5) . . . 2_655 ?
B3 B4 B5 B5 -138.0(5) . . . 2_655 ?
Cl4 B4 B5 B5 111.0(7) . . . 2_655 ?
B6 B4 B5 B5 -36.5(5) 2_655 . . 2_655 ?
B3 B5 B6 Cl07 112.0(6) . . . . ?
B4 B5 B6 Cl07 148.7(5) . . . . ?
B4 B5 B6 Cl07 -111.3(7) 2_655 . . . ?
Cl5 B5 B6 Cl07 0.8(8) . . . . ?
B5 B5 B6 Cl07 -147.6(6) 2_655 . . . ?
B4 B5 B6 B3 36.6(6) . . . . ?
B4 B5 B6 B3 136.7(6) 2_655 . . . ?
Cl5 B5 B6 B3 -111.2(7) . . . . ?
B5 B5 B6 B3 100.3(7) 2_655 . . . ?
B3 B5 B6 B4 -136.7(6) . . . 2_655 ?
B4 B5 B6 B4 -100.1(6) . . . 2_655 ?
Cl5 B5 B6 B4 112.1(7) . . . 2_655 ?
B5 B5 B6 B4 -36.4(6) 2_655 . . 2_655 ?
B3 B5 B6 B2 -99.8(6) . . . 2_655 ?
B4 B5 B6 B2 -63.2(7) . . . 2_655 ?
B4 B5 B6 B2 36.9(5) 2_655 . . 2_655 ?
Cl5 B5 B6 B2 149.0(5) . . . 2_655 ?
B5 B5 B6 B2 0.5(8) 2_655 . . 2_655 ?
B3 B5 B6 B1 -38.6(5) . . . . ?
B4 B5 B6 B1 -2.0(7) . . . . ?
B4 B5 B6 B1 98.1(6) 2_655 . . . ?
Cl5 B5 B6 B1 -149.8(5) . . . . ?
B5 B5 B6 B1 61.7(7) 2_655 . . . ?
B5 B3 B6 Cl07 -112.2(7) . . . . ?
B2 B3 B6 Cl07 147.4(6) . . . . ?
B4 B3 B6 Cl07 -148.9(6) . . . . ?
Cl3 B3 B6 Cl07 0.6(10) . . . . ?
B1 B3 B6 Cl07 111.3(7) . . . . ?
B2 B3 B6 B5 -100.4(7) . . . . ?
B4 B3 B6 B5 -36.7(6) . . . . ?
Cl3 B3 B6 B5 112.8(7) . . . . ?
B1 B3 B6 B5 -136.5(6) . . . . ?
B5 B3 B6 B4 37.8(6) . . . 2_655 ?
B2 B3 B6 B4 -62.7(8) . . . 2_655 ?
B4 B3 B6 B4 1.1(8) . . . 2_655 ?
Cl3 B3 B6 B4 150.5(6) . . . 2_655 ?
B1 B3 B6 B4 -98.8(7) . . . 2_655 ?
B5 B3 B6 B2 98.7(6) . . . 2_655 ?
B2 B3 B6 B2 -1.7(7) . . . 2_655 ?
B4 B3 B6 B2 62.0(8) . . . 2_655 ?
Cl3 B3 B6 B2 -148.5(6) . . . 2_655 ?
B1 B3 B6 B2 -37.8(6) . . . 2_655 ?
B5 B3 B6 B1 136.5(6) . . . . ?
B2 B3 B6 B1 36.1(6) . . . . ?
B4 B3 B6 B1 99.8(7) . . . . ?
Cl3 B3 B6 B1 -110.7(7) . . . . ?
B1 B1 B6 Cl07 147.9(6) 2_655 . . . ?
B2 B1 B6 Cl07 110.3(6) 2_655 . . . ?
Cl1 B1 B6 Cl07 -1.3(8) . . . . ?
B2 B1 B6 Cl07 -148.1(5) . . . . ?
B3 B1 B6 Cl07 -113.3(6) . . . . ?
B1 B1 B6 B5 -61.0(8) 2_655 . . . ?
B2 B1 B6 B5 -98.5(6) 2_655 . . . ?
Cl1 B1 B6 B5 149.9(5) . . . . ?
B2 B1 B6 B5 3.1(7) . . . . ?
B3 B1 B6 B5 37.9(5) . . . . ?
B1 B1 B6 B3 -98.9(7) 2_655 . . . ?
B2 B1 B6 B3 -136.4(7) 2_655 . . . ?
Cl1 B1 B6 B3 112.0(6) . . . . ?
B2 B1 B6 B3 -34.8(5) . . . . ?
B1 B1 B6 B4 0.9(8) 2_655 . . 2_655 ?
B2 B1 B6 B4 -36.7(6) 2_655 . . 2_655 ?
Cl1 B1 B6 B4 -148.3(5) . . . 2_655 ?
B2 B1 B6 B4 64.9(6) . . . 2_655 ?
B3 B1 B6 B4 99.7(6) . . . 2_655 ?
B1 B1 B6 B2 37.5(6) 2_655 . . 2_655 ?
Cl1 B1 B6 B2 -111.7(6) . . . 2_655 ?
B2 B1 B6 B2 101.6(6) . . . 2_655 ?
B3 B1 B6 B2 136.4(7) . . . 2_655 ?
Cl6 B7 B8 B11 -111.7(7) . . . . ?
B12 B7 B8 B11 138.9(6) 7_556 . . . ?
B9 B7 B8 B11 38.1(5) 7_556 . . . ?
B10 B7 B8 B11 99.7(6) 7_556 . . . ?
Cl6 B7 B8 B10 -149.8(6) . . . . ?
B11 B7 B8 B10 -38.1(5) . . . . ?
B12 B7 B8 B10 100.8(6) 7_556 . . . ?
B9 B7 B8 B10 0.0(7) 7_556 . . . ?
B10 B7 B8 B10 61.6(8) 7_556 . . . ?
Cl6 B7 B8 B9 146.8(6) . . . . ?
B11 B7 B8 B9 -101.5(6) . . . . ?
B12 B7 B8 B9 37.4(6) 7_556 . . . ?
B9 B7 B8 B9 -63.4(8) 7_556 . . . ?
B10 B7 B8 B9 -1.8(8) 7_556 . . . ?
Cl6 B7 B8 B12 109.5(7) . . . 7_556 ?
B11 B7 B8 B12 -138.9(6) . . . 7_556 ?
B9 B7 B8 B12 -100.8(6) 7_556 . . 7_556 ?
B10 B7 B8 B12 -39.2(6) 7_556 . . 7_556 ?
Cl6 B7 B8 Cl7 0.2(10) . . . . ?
B11 B7 B8 Cl7 111.9(6) . . . . ?
B12 B7 B8 Cl7 -109.2(7) 7_556 . . . ?
B9 B7 B8 Cl7 150.0(5) 7_556 . . . ?
B10 B7 B8 Cl7 -148.4(6) 7_556 . . . ?
B11 B8 B9 B10 37.5(5) . . . . ?
B7 B8 B9 B10 102.1(6) . . . . ?
B12 B8 B9 B10 139.3(5) 7_556 . . . ?
Cl7 B8 B9 B10 -111.3(6) . . . . ?
B11 B8 B9 Cl8 149.1(6) . . . . ?
B10 B8 B9 Cl8 111.5(7) . . . . ?
B7 B8 B9 Cl8 -146.4(6) . . . . ?
B12 B8 B9 Cl8 -109.2(7) 7_556 . . . ?
Cl7 B8 B9 Cl8 0.2(10) . . . . ?
B11 B8 B9 B7 -0.7(7) . . . 7_556 ?
B10 B8 B9 B7 -38.2(5) . . . 7_556 ?
B7 B8 B9 B7 63.9(8) . . . 7_556 ?
B12 B8 B9 B7 101.1(6) 7_556 . . 7_556 ?
Cl7 B8 B9 B7 -149.5(5) . . . 7_556 ?
B11 B8 B9 B12 -101.8(6) . . . 7_556 ?
B10 B8 B9 B12 -139.3(5) . . . 7_556 ?
B7 B8 B9 B12 -37.2(6) . . . 7_556 ?
Cl7 B8 B9 B12 109.4(7) . . . 7_556 ?
B11 B8 B9 B11 -63.0(8) . . . 7_556 ?
B10 B8 B9 B11 -100.5(6) . . . 7_556 ?
B7 B8 B9 B11 1.6(8) . . . 7_556 ?
B12 B8 B9 B11 38.7(5) 7_556 . . 7_556 ?
Cl7 B8 B9 B11 148.2(5) . . . 7_556 ?
Cl8 B9 B10 B8 -112.1(6) . . . . ?
B7 B9 B10 B8 137.6(5) 7_556 . . . ?
B12 B9 B10 B8 36.5(5) 7_556 . . . ?
B11 B9 B10 B8 100.1(6) 7_556 . . . ?
Cl8 B9 B10 B11 -148.5(5) . . . . ?
B8 B9 B10 B11 -36.4(5) . . . . ?
B7 B9 B10 B11 101.2(5) 7_556 . . . ?
B12 B9 B10 B11 0.1(7) 7_556 . . . ?
B11 B9 B10 B11 63.6(7) 7_556 . . . ?
Cl8 B9 B10 Cl9 1.2(9) . . . . ?
B8 B9 B10 Cl9 113.3(6) . . . . ?
B7 B9 B10 Cl9 -109.1(7) 7_556 . . . ?
B12 B9 B10 Cl9 149.8(5) 7_556 . . . ?
B11 B9 B10 Cl9 -146.7(5) 7_556 . . . ?
Cl8 B9 B10 B7 110.4(7) . . . 7_556 ?
B8 B9 B10 B7 -137.6(5) . . . 7_556 ?
B12 B9 B10 B7 -101.1(5) 7_556 . . 7_556 ?
B11 B9 B10 B7 -37.5(5) 7_556 . . 7_556 ?
Cl8 B9 B10 B12 147.1(5) . . . . ?
B8 B9 B10 B12 -100.8(6) . . . . ?
B7 B9 B10 B12 36.7(5) 7_556 . . . ?
B12 B9 B10 B12 -64.3(7) 7_556 . . . ?
B11 B9 B10 B12 -0.8(8) 7_556 . . . ?
B11 B8 B10 B9 -138.9(5) . . . . ?
B7 B8 B10 B9 -101.1(6) . . . . ?
B12 B8 B10 B9 -36.9(5) 7_556 . . . ?
Cl7 B8 B10 B9 109.3(6) . . . . ?
B7 B8 B10 B11 37.9(5) . . . . ?
B9 B8 B10 B11 138.9(5) . . . . ?
B12 B8 B10 B11 102.0(6) 7_556 . . . ?
Cl7 B8 B10 B11 -111.8(6) . . . . ?
B11 B8 B10 Cl9 108.1(6) . . . . ?
B7 B8 B10 Cl9 145.9(6) . . . . ?
B9 B8 B10 Cl9 -113.0(7) . . . . ?
B12 B8 B10 Cl9 -149.9(6) 7_556 . . . ?
Cl7 B8 B10 Cl9 -3.7(10) . . . . ?
B11 B8 B10 B7 -100.4(6) . . . 7_556 ?
B7 B8 B10 B7 -62.6(8) . . . 7_556 ?
B9 B8 B10 B7 38.5(5) . . . 7_556 ?
B12 B8 B10 B7 1.6(8) 7_556 . . 7_556 ?
Cl7 B8 B10 B7 147.8(6) . . . 7_556 ?
B11 B8 B10 B12 -37.1(5) . . . . ?
B7 B8 B10 B12 0.8(7) . . . . ?
B9 B8 B10 B12 101.8(6) . . . . ?
B12 B8 B10 B12 65.0(8) 7_556 . . . ?
Cl7 B8 B10 B12 -148.9(5) . . . . ?
B10 B8 B11 B7 138.5(5) . . . . ?
B9 B8 B11 B7 101.7(6) . . . . ?
B12 B8 B11 B7 37.2(5) 7_556 . . . ?
Cl7 B8 B11 B7 -110.0(7) . . . . ?
B7 B8 B11 B10 -138.5(5) . . . . ?
B9 B8 B11 B10 -36.8(5) . . . . ?
B12 B8 B11 B10 -101.3(6) 7_556 . . . ?
Cl7 B8 B11 B10 111.6(6) . . . . ?
B10 B8 B11 Cl04 -110.6(6) . . . . ?
B7 B8 B11 Cl04 111.0(7) . . . . ?
B9 B8 B11 Cl04 -147.3(5) . . . . ?
B12 B8 B11 Cl04 148.1(6) 7_556 . . . ?
Cl7 B8 B11 Cl04 1.0(9) . . . . ?
B10 B8 B11 B9 100.5(6) . . . 7_556 ?
B7 B8 B11 B9 -38.0(5) . . . 7_556 ?
B9 B8 B11 B9 63.7(8) . . . 7_556 ?
B12 B8 B11 B9 -0.8(8) 7_556 . . 7_556 ?
Cl7 B8 B11 B9 -148.0(6) . . . 7_556 ?
B10 B8 B11 B12 37.1(5) . . . . ?
B7 B8 B11 B12 -101.4(5) . . . . ?
B9 B8 B11 B12 0.3(7) . . . . ?
B12 B8 B11 B12 -64.2(8) 7_556 . . . ?
Cl7 B8 B11 B12 148.6(5) . . . . ?
Cl6 B7 B11 B8 112.1(6) . . . . ?
B12 B7 B11 B8 -36.8(5) 7_556 . . . ?
B9 B7 B11 B8 -137.6(6) 7_556 . . . ?
B10 B7 B11 B8 -100.4(6) 7_556 . . . ?
Cl6 B7 B11 B10 149.3(5) . . . . ?
B8 B7 B11 B10 37.2(5) . . . . ?
B12 B7 B11 B10 0.4(7) 7_556 . . . ?
B9 B7 B11 B10 -100.4(5) 7_556 . . . ?
B10 B7 B11 B10 -63.2(7) 7_556 . . . ?
Cl6 B7 B11 Cl04 0.3(9) . . . . ?
B8 B7 B11 Cl04 -111.7(6) . . . . ?
B12 B7 B11 Cl04 -148.5(5) 7_556 . . . ?
B9 B7 B11 Cl04 110.7(6) 7_556 . . . ?
B10 B7 B11 Cl04 147.8(5) 7_556 . . . ?
Cl6 B7 B11 B9 -110.4(7) . . . 7_556 ?
B8 B7 B11 B9 137.6(5) . . . 7_556 ?
B12 B7 B11 B9 100.8(6) 7_556 . . 7_556 ?
B10 B7 B11 B9 37.1(5) 7_556 . . 7_556 ?
Cl6 B7 B11 B12 -146.6(5) . . . . ?
B8 B7 B11 B12 101.3(6) . . . . ?
B12 B7 B11 B12 64.5(7) 7_556 . . . ?
B9 B7 B11 B12 -36.2(5) 7_556 . . . ?
B10 B7 B11 B12 0.9(7) 7_556 . . . ?
B9 B10 B11 B8 37.3(5) . . . . ?
Cl9 B10 B11 B8 -113.5(6) . . . . ?
B7 B10 B11 B8 101.7(6) 7_556 . . . ?
B12 B10 B11 B8 138.9(5) . . . . ?
B9 B10 B11 B7 -0.3(7) . . . . ?
B8 B10 B11 B7 -37.6(5) . . . . ?
Cl9 B10 B11 B7 -151.1(5) . . . . ?
B7 B10 B11 B7 64.1(7) 7_556 . . . ?
B12 B10 B11 B7 101.3(5) . . . . ?
B9 B10 B11 Cl04 148.6(5) . . . . ?
B8 B10 B11 Cl04 111.3(6) . . . . ?
Cl9 B10 B11 Cl04 -2.2(9) . . . . ?
B7 B10 B11 Cl04 -147.0(5) 7_556 . . . ?
B12 B10 B11 Cl04 -109.8(6) . . . . ?
B9 B10 B11 B9 -63.9(7) . . . 7_556 ?
B8 B10 B11 B9 -101.2(6) . . . 7_556 ?
Cl9 B10 B11 B9 145.3(5) . . . 7_556 ?
B7 B10 B11 B9 0.5(8) 7_556 . . 7_556 ?
B12 B10 B11 B9 37.7(5) . . . 7_556 ?
B9 B10 B11 B12 -101.6(5) . . . . ?
B8 B10 B11 B12 -138.9(5) . . . . ?
Cl9 B10 B11 B12 107.6(6) . . . . ?
B7 B10 B11 B12 -37.3(5) 7_556 . . . ?
B9 B10 B12 Cl10 -147.8(6) . . . . ?
B8 B10 B12 Cl10 147.5(6) . . . . ?
B11 B10 B12 Cl10 111.1(7) . . . . ?
Cl9 B10 B12 Cl10 0.1(9) . . . . ?
B7 B10 B12 Cl10 -110.6(7) 7_556 . . . ?
B9 B10 B12 B7 -37.2(6) . . . 7_556 ?
B8 B10 B12 B7 -101.9(6) . . . 7_556 ?
B11 B10 B12 B7 -138.3(6) . . . 7_556 ?
Cl9 B10 B12 B7 110.7(6) . . . 7_556 ?
B9 B10 B12 B8 1.3(8) . . . 7_556 ?
B8 B10 B12 B8 -63.5(7) . . . 7_556 ?
B11 B10 B12 B8 -99.8(6) . . . 7_556 ?
Cl9 B10 B12 B8 149.2(5) . . . 7_556 ?
B7 B10 B12 B8 38.5(5) 7_556 . . 7_556 ?
B9 B10 B12 B9 63.5(7) . . . 7_556 ?
B8 B10 B12 B9 -1.2(7) . . . 7_556 ?
B11 B10 B12 B9 -37.6(5) . . . 7_556 ?
Cl9 B10 B12 B9 -148.6(5) . . . 7_556 ?
B7 B10 B12 B9 100.7(6) 7_556 . . 7_556 ?
B9 B10 B12 B11 101.1(6) . . . . ?
B8 B10 B12 B11 36.3(5) . . . . ?
Cl9 B10 B12 B11 -111.0(6) . . . . ?
B7 B10 B12 B11 138.3(6) 7_556 . . . ?
B8 B11 B12 Cl10 -147.8(5) . . . . ?
B7 B11 B12 Cl10 147.7(5) . . . . ?
B10 B11 B12 Cl10 -111.0(6) . . . . ?
Cl04 B11 B12 Cl10 0.4(8) . . . . ?
B9 B11 B12 Cl10 111.4(7) 7_556 . . . ?
B8 B11 B12 B7 0.2(7) . . . 7_556 ?
B7 B11 B12 B7 -64.3(7) . . . 7_556 ?
B10 B11 B12 B7 37.0(5) . . . 7_556 ?
Cl04 B11 B12 B7 148.4(5) . . . 7_556 ?
B9 B11 B12 B7 -100.6(6) 7_556 . . 7_556 ?
B8 B11 B12 B8 62.6(7) . . . 7_556 ?
B7 B11 B12 B8 -1.9(7) . . . 7_556 ?
B10 B11 B12 B8 99.4(6) . . . 7_556 ?
Cl04 B11 B12 B8 -149.2(5) . . . 7_556 ?
B9 B11 B12 B8 -38.2(5) 7_556 . . 7_556 ?
B8 B11 B12 B9 100.8(6) . . . 7_556 ?
B7 B11 B12 B9 36.3(5) . . . 7_556 ?
B10 B11 B12 B9 137.6(6) . . . 7_556 ?
Cl04 B11 B12 B9 -111.0(6) . . . 7_556 ?
B8 B11 B12 B10 -36.8(5) . . . . ?
B7 B11 B12 B10 -101.3(6) . . . . ?
Cl04 B11 B12 B10 111.4(6) . . . . ?
B9 B11 B12 B10 -137.6(6) 7_556 . . . ?
C2 C1 N1 C5 2.6(9) . . . . ?
C2 C1 N1 Cu1 -178.8(5) . . . . ?
C4 C5 N1 C1 -3.3(9) . . . . ?
C4 C5 N1 Cu1 178.0(5) . . . . ?
C13 C14 N2 C16 0.3(10) . . . . ?
C13 C14 N2 Cu1 179.2(5) . . . 6_556 ?
C15 C16 N2 C14 0.1(9) . . . . ?
C15 C16 N2 Cu1 -178.9(5) . . . 6_556 ?
C18 C17 N3 C21 1.3(8) . . . . ?
C18 C17 N3 Cu1 178.3(4) . . . . ?
C20 C21 N3 C17 -0.8(8) . . . . ?
C20 C21 N3 Cu1 -177.8(4) . . . . ?
C32 C31 N4 C30 1.3(9) . . . . ?
C32 C31 N4 Cu1 -174.7(5) . . . 6_566 ?
C29 C30 N4 C31 -1.9(8) . . . . ?
C29 C30 N4 Cu1 174.1(4) . . . 6_566 ?

_refine_diff_density_max         1.047
_refine_diff_density_min         -1.235
_refine_diff_density_rms         0.126



####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_p-1_a_sq
_database_code_depnum_ccdc_archive 'CCDC 2033519'
loop_
_audit_author_name
_audit_author_address
'Yue ZHAO'
;Nanjing University
China
;
_audit_update_record             
;
2020-09-23 deposited with the CCDC.	2020-12-10 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2018/3
_shelx_SHELXL_version_number     2018/3
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C48 H42 B12 Cl12 Cu2 N6 O4'
_chemical_formula_weight         1449.07

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   13.943(3)
_cell_length_b                   14.893(3)
_cell_length_c                   15.010(3)
_cell_angle_alpha                94.689(4)
_cell_angle_beta                 104.281(4)
_cell_angle_gamma                115.487(4)
_cell_volume                     2663.0(8)
_cell_formula_units_Z            1
_cell_measurement_reflns_used    3506
_cell_measurement_theta_min      2.3273
_cell_measurement_theta_max      24.7720
_cell_measurement_temperature    296.(2)

_exptl_crystal_description       block
_exptl_crystal_colour            ?
_exptl_crystal_size_max          0.250
_exptl_crystal_size_mid          0.200
_exptl_crystal_size_min          0.150
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    0.904
_exptl_crystal_F_000             726
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_absorpt_coefficient_mu    0.729
_shelx_estimated_absorpt_T_min   ?
_shelx_estimated_absorpt_T_max   ?
_exptl_absorpt_correction_type   ?
_exptl_absorpt_correction_T_min  ?
_exptl_absorpt_correction_T_max  ?
_exptl_absorpt_process_details   ?
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      296(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_source                   ?
_diffrn_measurement_device_type  'BRUKER D8 VENTURE PHOTON 100'
_diffrn_measurement_method       ?
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            14419
_diffrn_reflns_av_unetI/netI     0.1298
_diffrn_reflns_av_R_equivalents  0.0460
_diffrn_reflns_limit_h_min       -16
_diffrn_reflns_limit_h_max       16
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_l_min       -10
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_theta_min         2.079
_diffrn_reflns_theta_max         25.463
_diffrn_reflns_theta_full        25.242
_diffrn_measured_fraction_theta_max 0.987
_diffrn_measured_fraction_theta_full 0.990
_diffrn_reflns_Laue_measured_fraction_max 0.987
_diffrn_reflns_Laue_measured_fraction_full 0.990
_diffrn_reflns_point_group_measured_fraction_max 0.987
_diffrn_reflns_point_group_measured_fraction_full 0.990
_reflns_number_total             9750
_reflns_number_gt                4264
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       ?
_computing_cell_refinement       ?
_computing_data_reduction        ?
_computing_structure_solution    'SHELXT 2014/5 (Sheldrick, 2014)'
_computing_structure_refinement  'SHELXL-2018/3 (Sheldrick, 2018)'
_computing_molecular_graphics    ?
_computing_publication_material  ?
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0700P)²+7.0000P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_number_reflns         9750
_refine_ls_number_parameters     374
_refine_ls_number_restraints     389
_refine_ls_R_factor_all          0.1434
_refine_ls_R_factor_gt           0.0697
_refine_ls_wR_factor_ref         0.2251
_refine_ls_wR_factor_gt          0.1963
_refine_ls_goodness_of_fit_ref   0.988
_refine_ls_restrained_S_all      0.973
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Cu1 Cu 0.59268(8) 0.95931(6) 0.52913(6) 0.0565(3) Uani 1 1 d . U . . .
Cl1 Cl -0.19718(19) 0.24899(14) -0.02134(14) 0.0759(7) Uani 1 1 d . U . . .
B1 B -0.0965(8) 0.3787(6) -0.0101(6) 0.059(2) Uani 1 1 d . U . . .
C1 C 0.4297(6) 0.8117(5) 0.6030(5) 0.0566(19) Uani 1 1 d . U . . .
H1 H 0.459592 0.866954 0.653030 0.068 Uiso 1 1 calc R U . . .
N1 N 0.4734(5) 0.8235(4) 0.5318(4) 0.0508(14) Uani 1 1 d . U . . .
Cl2 Cl 0.0980(2) 0.34794(16) 0.11639(14) 0.0865(8) Uani 1 1 d . U . . .
B2 B 0.0057(8) 0.4083(6) -0.0702(5) 0.056(2) Uani 1 1 d . U . . .
C2 C 0.3419(6) 0.7208(5) 0.6054(5) 0.0562(19) Uani 1 1 d . U . . .
H2 H 0.314139 0.716347 0.656061 0.067 Uiso 1 1 calc R U . . .
N2 N -0.2793(5) 0.0905(4) 0.5227(4) 0.0505(15) Uani 1 1 d . U . . .
Cl3 Cl 0.01318(19) 0.31164(14) -0.14381(13) 0.0723(6) Uani 1 1 d . U . . .
O3 O 0.4966(4) 0.9576(3) 0.4104(3) 0.0565(3) Uani 1 1 d . U . . .
H3A H 0.425668 0.902550 0.383112 0.068 Uiso 1 1 calc R U . . .
H3B H 0.521383 1.011788 0.380661 0.068 Uiso 1 1 calc R U . . .
B3 B 0.0469(8) 0.4271(6) 0.0572(6) 0.059(2) Uani 1 1 d . U . . .
N3 N 0.6877(5) 0.9624(4) 0.6554(4) 0.0589(16) Uani 1 1 d . U . . .
C3 C 0.2947(6) 0.6346(5) 0.5302(4) 0.0484(17) Uani 1 1 d . U . . .
Cl4 Cl 0.21025(18) 0.61857(15) 0.21618(12) 0.0726(6) Uani 1 1 d . U . . .
O4 O 0.6735(5) 0.8647(5) 0.4388(4) 0.0902(17) Uani 1 1 d . U . . .
H4A H 0.630250 0.836560 0.385345 0.108 Uiso 1 1 calc R U . . .
B4 B 0.1012(7) 0.5573(6) 0.1065(5) 0.053(2) Uani 1 1 d . U . . .
C4 C 0.3413(6) 0.6481(5) 0.4578(5) 0.0576(19) Uani 1 1 d . U . . .
H4 H 0.314069 0.593672 0.407474 0.069 Uiso 1 1 calc R U . . .
B5 B 0.1287(8) 0.5195(6) 0.0009(6) 0.057(2) Uani 1 1 d . U . . .
C5 C 0.4279(6) 0.7412(5) 0.4588(5) 0.0560(18) Uani 1 1 d . U . . .
H5 H 0.455874 0.747879 0.408181 0.067 Uiso 1 1 calc R U . . .
Cl5 Cl 0.26651(19) 0.54109(18) 0.00431(16) 0.0870(7) Uani 1 1 d . U . . .
B6 B 0.0356(7) 0.5291(6) -0.0987(5) 0.052(2) Uani 1 1 d . U . . .
C6 C 0.1992(6) 0.5394(5) 0.5290(5) 0.0528(18) Uani 1 1 d . U . . .
Cl6 Cl 0.0751(2) 0.56180(15) -0.20002(13) 0.0788(7) Uani 1 1 d . U . . .
C7 C 0.1850(6) 0.5078(5) 0.6113(5) 0.0552(18) Uani 1 1 d . U . . .
H7 H 0.238797 0.547511 0.668403 0.066 Uiso 1 1 calc R U . . .
C8 C 0.0936(6) 0.4192(5) 0.6115(5) 0.0568(19) Uani 1 1 d . U . . .
H8 H 0.087323 0.398781 0.667618 0.068 Uiso 1 1 calc R U . . .
C9 C 0.0108(6) 0.3607(5) 0.5256(5) 0.0525(17) Uani 1 1 d . U . . .
C10 C 0.0236(6) 0.3912(6) 0.4428(5) 0.060(2) Uani 1 1 d . U . . .
H10 H -0.029819 0.352074 0.385391 0.072 Uiso 1 1 calc R U . . .
C11 C 0.1177(7) 0.4815(6) 0.4461(5) 0.062(2) Uani 1 1 d . U . . .
H11 H 0.124708 0.502432 0.390272 0.075 Uiso 1 1 calc R U . . .
C12 C -0.0890(6) 0.2680(5) 0.5240(5) 0.0507(17) Uani 1 1 d . U . . .
C13 C -0.1395(6) 0.2633(5) 0.5960(4) 0.0538(18) Uani 1 1 d . U . . .
H13 H -0.110267 0.319239 0.645164 0.065 Uiso 1 1 calc R U . . .
C14 C -0.2320(6) 0.1749(5) 0.5922(5) 0.0548(18) Uani 1 1 d . U . . .
H14 H -0.263941 0.172956 0.640002 0.066 Uiso 1 1 calc R U . . .
C15 C -0.2336(6) 0.0955(5) 0.4534(5) 0.0546(19) Uani 1 1 d . U . . .
H15 H -0.266991 0.039070 0.403981 0.066 Uiso 1 1 calc R U . . .
C16 C -0.1410(6) 0.1784(5) 0.4514(5) 0.060(2) Uani 1 1 d . U . . .
H16 H -0.111387 0.176762 0.402540 0.071 Uiso 1 1 calc R U . . .
C17 C 0.6970(7) 1.0154(6) 0.7368(5) 0.071(2) Uani 1 1 d . U . . .
H17 H 0.651298 1.046308 0.735294 0.085 Uiso 1 1 calc R U . . .
C18 C 0.7710(7) 1.0265(6) 0.8225(5) 0.075(2) Uani 1 1 d . U . . .
H18 H 0.774333 1.063779 0.877052 0.090 Uiso 1 1 calc R U . . .
C19 C 0.8410(7) 0.9806(5) 0.8262(5) 0.072(2) Uani 1 1 d . U . . .
C20 C 0.8285(9) 0.9263(8) 0.7425(6) 0.118(4) Uani 1 1 d . U . . .
H20 H 0.871390 0.892918 0.741747 0.141 Uiso 1 1 calc R U . . .
C21 C 0.7550(9) 0.9197(8) 0.6604(6) 0.112(4) Uani 1 1 d . U . . .
H21 H 0.751586 0.883662 0.605060 0.134 Uiso 1 1 calc R U . . .
C22 C 0.9218(8) 0.9912(6) 0.9169(5) 0.084(3) Uani 1 1 d . U . . .
C23 C 0.9447(10) 0.9132(7) 0.9357(6) 0.130(5) Uani 1 1 d . U . . .
H23 H 0.906278 0.851727 0.891727 0.156 Uiso 1 1 calc R U . . .
C24 C 0.9772(9) 1.0780(6) 0.9825(6) 0.108(4) Uani 1 1 d . U . . .
H24 H 0.962950 1.132525 0.972785 0.130 Uiso 1 1 calc R U . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Cu1 O3 1.939(4) . ?
Cu1 N1 2.003(6) . ?
Cu1 N3 2.011(5) . ?
Cu1 N2 2.032(6) 1_665 ?
Cu1 O3 2.367(5) 2_676 ?
Cu1 O4 2.627(6) . ?
Cl1 B1 1.796(8) . ?
B1 B5 1.763(12) 2_565 ?
B1 B3 1.783(13) . ?
B1 B2 1.787(13) . ?
B1 B6 1.794(11) 2_565 ?
B1 B4 1.800(11) 2_565 ?
C1 N1 1.341(8) . ?
C1 C2 1.392(9) . ?
C1 H1 0.9300 . ?
N1 C5 1.369(8) . ?
Cl2 B3 1.808(8) . ?
B2 B4 1.757(12) 2_565 ?
B2 B6 1.779(11) . ?
B2 B5 1.785(11) . ?
B2 Cl3 1.797(8) . ?
B2 B3 1.815(11) . ?
C2 C3 1.423(9) . ?
C2 H2 0.9300 . ?
N2 C15 1.339(8) . ?
N2 C14 1.354(8) . ?
O3 H3A 0.9300 . ?
O3 H3B 0.9300 . ?
B3 B6 1.752(13) 2_565 ?
B3 B4 1.762(11) . ?
B3 B5 1.795(12) . ?
N3 C21 1.335(10) . ?
N3 C17 1.344(9) . ?
C3 C4 1.383(9) . ?
C3 C6 1.463(9) . ?
Cl4 B4 1.783(8) . ?
O4 H4A 0.8200 . ?
B4 B6 1.750(12) 2_565 ?
B4 B5 1.820(12) . ?
C4 C5 1.388(9) . ?
C4 H4 0.9300 . ?
B5 B6 1.783(11) . ?
B5 Cl5 1.793(10) . ?
C5 H5 0.9300 . ?
B6 Cl6 1.777(8) . ?
C6 C11 1.367(9) . ?
C6 C7 1.387(9) . ?
C7 C8 1.386(9) . ?
C7 H7 0.9300 . ?
C8 C9 1.404(9) . ?
C8 H8 0.9300 . ?
C9 C10 1.383(9) . ?
C9 C12 1.473(9) . ?
C10 C11 1.405(10) . ?
C10 H10 0.9300 . ?
C11 H11 0.9300 . ?
C12 C13 1.418(9) . ?
C12 C16 1.426(9) . ?
C13 C14 1.375(9) . ?
C13 H13 0.9300 . ?
C14 H14 0.9300 . ?
C15 C16 1.359(9) . ?
C15 H15 0.9300 . ?
C16 H16 0.9300 . ?
C17 C18 1.382(9) . ?
C17 H17 0.9300 . ?
C18 C19 1.406(11) . ?
C18 H18 0.9300 . ?
C19 C20 1.366(10) . ?
C19 C22 1.485(10) . ?
C20 C21 1.359(10) . ?
C20 H20 0.9300 . ?
C21 H21 0.9300 . ?
C22 C24 1.339(10) . ?
C22 C23 1.365(10) . ?
C23 C24 1.378(10) 2_777 ?
C23 H23 0.9300 . ?
C24 H24 0.9300 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O3 Cu1 N1 89.8(2) . . ?
O3 Cu1 N3 177.2(2) . . ?
N1 Cu1 N3 89.4(2) . . ?
O3 Cu1 N2 91.2(2) . 1_665 ?
N1 Cu1 N2 174.9(2) . 1_665 ?
N3 Cu1 N2 89.8(2) . 1_665 ?
O3 Cu1 O3 81.83(17) . 2_676 ?
N1 Cu1 O3 90.8(2) . 2_676 ?
N3 Cu1 O3 95.5(2) . 2_676 ?
N2 Cu1 O3 94.3(2) 1_665 2_676 ?
O3 Cu1 O4 90.21(18) . . ?
N1 Cu1 O4 88.8(2) . . ?
N3 Cu1 O4 92.4(2) . . ?
N2 Cu1 O4 86.2(2) 1_665 . ?
O3 Cu1 O4 172.03(16) 2_676 . ?
B5 B1 B3 107.0(6) 2_565 . ?
B5 B1 B2 108.2(6) 2_565 . ?
B3 B1 B2 61.1(5) . . ?
B5 B1 B6 60.2(4) 2_565 2_565 ?
B3 B1 B6 58.6(5) . 2_565 ?
B2 B1 B6 108.2(6) . 2_565 ?
B5 B1 Cl1 122.6(6) 2_565 . ?
B3 B1 Cl1 121.4(5) . . ?
B2 B1 Cl1 120.7(5) . . ?
B6 B1 Cl1 122.0(5) 2_565 . ?
B5 B1 B4 61.4(5) 2_565 2_565 ?
B3 B1 B4 107.6(6) . 2_565 ?
B2 B1 B4 58.7(5) . 2_565 ?
B6 B1 B4 109.0(5) 2_565 2_565 ?
Cl1 B1 B4 121.8(5) . 2_565 ?
N1 C1 C2 123.1(6) . . ?
N1 C1 H1 118.4 . . ?
C2 C1 H1 118.4 . . ?
C1 N1 C5 117.4(6) . . ?
C1 N1 Cu1 120.8(5) . . ?
C5 N1 Cu1 121.7(5) . . ?
B4 B2 B6 59.3(5) 2_565 . ?
B4 B2 B5 107.7(6) 2_565 . ?
B6 B2 B5 60.0(4) . . ?
B4 B2 B1 61.0(5) 2_565 . ?
B6 B2 B1 108.0(6) . . ?
B5 B2 B1 107.5(6) . . ?
B4 B2 Cl3 121.5(5) 2_565 . ?
B6 B2 Cl3 121.3(5) . . ?
B5 B2 Cl3 121.6(6) . . ?
B1 B2 Cl3 122.3(5) . . ?
B4 B2 B3 108.0(6) 2_565 . ?
B6 B2 B3 107.6(5) . . ?
B5 B2 B3 59.8(5) . . ?
B1 B2 B3 59.3(5) . . ?
Cl3 B2 B3 122.6(5) . . ?
C1 C2 C3 119.9(7) . . ?
C1 C2 H2 120.0 . . ?
C3 C2 H2 120.0 . . ?
C15 N2 C14 117.3(6) . . ?
C15 N2 Cu1 121.7(5) . 1_445 ?
C14 N2 Cu1 120.9(5) . 1_445 ?
Cu1 O3 Cu1 98.17(17) . 2_676 ?
Cu1 O3 H3A 120.0 . . ?
Cu1 O3 H3A 86.6 2_676 . ?
Cu1 O3 H3B 120.0 . . ?
Cu1 O3 H3B 85.2 2_676 . ?
H3A O3 H3B 120.0 . . ?
B6 B3 B4 59.7(5) 2_565 . ?
B6 B3 B1 61.0(5) 2_565 . ?
B4 B3 B1 108.6(6) . . ?
B6 B3 B5 108.9(6) 2_565 . ?
B4 B3 B5 61.5(5) . . ?
B1 B3 B5 107.3(6) . . ?
B6 B3 Cl2 121.7(6) 2_565 . ?
B4 B3 Cl2 121.5(5) . . ?
B1 B3 Cl2 121.7(5) . . ?
B5 B3 Cl2 121.3(6) . . ?
B6 B3 B2 108.9(6) 2_565 . ?
B4 B3 B2 109.0(5) . . ?
B1 B3 B2 59.6(5) . . ?
B5 B3 B2 59.3(4) . . ?
Cl2 B3 B2 120.9(5) . . ?
C21 N3 C17 116.5(6) . . ?
C21 N3 Cu1 119.8(5) . . ?
C17 N3 Cu1 123.3(5) . . ?
C4 C3 C2 116.1(7) . . ?
C4 C3 C6 122.9(6) . . ?
C2 C3 C6 121.0(6) . . ?
Cu1 O4 H4A 109.5 . . ?
B6 B4 B2 61.0(5) 2_565 2_565 ?
B6 B4 B3 59.8(5) 2_565 . ?
B2 B4 B3 108.2(6) 2_565 . ?
B6 B4 Cl4 122.5(5) 2_565 . ?
B2 B4 Cl4 122.1(5) 2_565 . ?
B3 B4 Cl4 122.2(5) . . ?
B6 B4 B1 108.7(6) 2_565 2_565 ?
B2 B4 B1 60.3(5) 2_565 2_565 ?
B3 B4 B1 107.0(5) . 2_565 ?
Cl4 B4 B1 121.2(5) . 2_565 ?
B6 B4 B5 107.9(5) 2_565 . ?
B2 B4 B5 107.0(5) 2_565 . ?
B3 B4 B5 60.1(5) . . ?
Cl4 B4 B5 121.4(6) . . ?
B1 B4 B5 58.3(5) 2_565 . ?
C3 C4 C5 121.3(7) . . ?
C3 C4 H4 119.3 . . ?
C5 C4 H4 119.3 . . ?
B1 B5 B6 60.8(5) 2_565 . ?
B1 B5 B2 108.5(6) 2_565 . ?
B6 B5 B2 59.8(4) . . ?
B1 B5 Cl5 121.1(6) 2_565 . ?
B6 B5 Cl5 122.1(6) . . ?
B2 B5 Cl5 122.4(6) . . ?
B1 B5 B3 107.2(6) 2_565 . ?
B6 B5 B3 108.3(6) . . ?
B2 B5 B3 60.9(5) . . ?
Cl5 B5 B3 121.9(6) . . ?
B1 B5 B4 60.3(5) 2_565 . ?
B6 B5 B4 108.6(6) . . ?
B2 B5 B4 107.7(6) . . ?
Cl5 B5 B4 120.9(5) . . ?
B3 B5 B4 58.3(5) . . ?
N1 C5 C4 122.2(7) . . ?
N1 C5 H5 118.9 . . ?
C4 C5 H5 118.9 . . ?
B4 B6 B3 60.4(5) 2_565 2_565 ?
B4 B6 Cl6 122.1(5) 2_565 . ?
B3 B6 Cl6 121.7(5) 2_565 . ?
B4 B6 B2 59.7(5) 2_565 . ?
B3 B6 B2 107.7(6) 2_565 . ?
Cl6 B6 B2 122.5(5) . . ?
B4 B6 B5 108.1(6) 2_565 . ?
B3 B6 B5 107.5(5) 2_565 . ?
Cl6 B6 B5 121.6(6) . . ?
B2 B6 B5 60.1(5) . . ?
B4 B6 B1 108.6(6) 2_565 2_565 ?
B3 B6 B1 60.4(5) 2_565 2_565 ?
Cl6 B6 B1 121.1(5) . 2_565 ?
B2 B6 B1 107.3(5) . 2_565 ?
B5 B6 B1 59.0(4) . 2_565 ?
C11 C6 C7 117.8(7) . . ?
C11 C6 C3 120.4(6) . . ?
C7 C6 C3 121.7(6) . . ?
C8 C7 C6 122.4(6) . . ?
C8 C7 H7 118.8 . . ?
C6 C7 H7 118.8 . . ?
C7 C8 C9 118.9(7) . . ?
C7 C8 H8 120.6 . . ?
C9 C8 H8 120.6 . . ?
C10 C9 C8 119.5(7) . . ?
C10 C9 C12 120.5(6) . . ?
C8 C9 C12 120.1(6) . . ?
C9 C10 C11 119.6(7) . . ?
C9 C10 H10 120.2 . . ?
C11 C10 H10 120.2 . . ?
C6 C11 C10 121.8(7) . . ?
C6 C11 H11 119.1 . . ?
C10 C11 H11 119.1 . . ?
C13 C12 C16 115.9(7) . . ?
C13 C12 C9 121.1(6) . . ?
C16 C12 C9 123.0(7) . . ?
C14 C13 C12 119.2(6) . . ?
C14 C13 H13 120.4 . . ?
C12 C13 H13 120.4 . . ?
N2 C14 C13 123.7(7) . . ?
N2 C14 H14 118.1 . . ?
C13 C14 H14 118.1 . . ?
N2 C15 C16 123.6(7) . . ?
N2 C15 H15 118.2 . . ?
C16 C15 H15 118.2 . . ?
C15 C16 C12 120.3(7) . . ?
C15 C16 H16 119.9 . . ?
C12 C16 H16 119.9 . . ?
N3 C17 C18 123.5(7) . . ?
N3 C17 H17 118.3 . . ?
C18 C17 H17 118.3 . . ?
C17 C18 C19 119.1(7) . . ?
C17 C18 H18 120.4 . . ?
C19 C18 H18 120.4 . . ?
C20 C19 C18 115.9(7) . . ?
C20 C19 C22 123.4(8) . . ?
C18 C19 C22 120.6(7) . . ?
C21 C20 C19 121.9(8) . . ?
C21 C20 H20 119.0 . . ?
C19 C20 H20 119.0 . . ?
N3 C21 C20 123.1(8) . . ?
N3 C21 H21 118.5 . . ?
C20 C21 H21 118.5 . . ?
C24 C22 C23 117.2(7) . . ?
C24 C22 C19 121.8(7) . . ?
C23 C22 C19 121.0(7) . . ?
C22 C23 C24 122.4(8) . 2_777 ?
C22 C23 H23 118.8 . . ?
C24 C23 H23 118.8 2_777 . ?
C22 C24 C23 120.4(7) . 2_777 ?
C22 C24 H24 119.8 . . ?
C23 C24 H24 119.8 2_777 . ?

_refine_diff_density_max         1.252
_refine_diff_density_min         -0.511
_refine_diff_density_rms         0.074



####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_ZH_ZJU4
_database_code_depnum_ccdc_archive 'CCDC 2042563'
loop_
_audit_author_name
_audit_author_address
'Yue Zhao'
;Nanjing University
China
;
_audit_update_record             
;
2020-11-05 deposited with the CCDC.	2020-12-10 downloaded from the CCDC.
;
_chemical_name_systematic        BSF-72
_chemical_name_common            ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C48 H36 B12 Cl12 Cu2 N6 O4'
_chemical_formula_iupac          ?
_chemical_formula_weight         1443.03

_chemical_melting_point          ?

_space_group_crystal_system      triclinic
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   13.943(3)
_cell_length_b                   14.893(3)
_cell_length_c                   15.010(3)
_cell_angle_alpha                94.689(4)
_cell_angle_beta                 104.281(4)
_cell_angle_gamma                115.487(4)
_cell_volume                     2663.0(8)
_cell_formula_units_Z            1
_cell_measurement_reflns_used    3506
_cell_measurement_theta_min      2.3273
_cell_measurement_theta_max      24.7720
_cell_measurement_temperature    296.(2)

_exptl_crystal_description       block
_exptl_crystal_colour            ?
_exptl_crystal_size_max          0.250
_exptl_crystal_size_mid          0.200
_exptl_crystal_size_min          0.150
_exptl_crystal_density_diffrn    0.900
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             720

_exptl_absorpt_coefficient_mu    0.728
_exptl_absorpt_correction_type   Multi-Scan
_exptl_absorpt_process_details   
;
SADABS-2016/2 - Bruker AXS area detector scaling and absorption correction
;
_exptl_absorpt_correction_T_min  0.6165
_exptl_absorpt_correction_T_max  0.7452

_exptl_special_details           
;
;

_diffrn_ambient_temperature      296.(2)

_diffrn_source                   TXS
_diffrn_source_type              'Rotaing Anode'

_diffrn_radiation_type           ' Mo K\a'
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_monochromator  'Helios Multi-layer Optic'

_diffrn_measurement_device_type  'Bruker D8 VENTURE PHOTON 100'
_diffrn_measurement_method       ?

_diffrn_detector_area_resol_mean 10.4167

_diffrn_reflns_number            14419
_diffrn_reflns_av_R_equivalents  0.0460
_diffrn_reflns_av_unetI/netI     0.1298
_diffrn_reflns_theta_min         2.08
_diffrn_reflns_theta_max         25.46
_diffrn_reflns_theta_full        25.46
_diffrn_measured_fraction_theta_max 0.987
_diffrn_measured_fraction_theta_full 0.987
_diffrn_reflns_limit_h_min       -16
_diffrn_reflns_limit_h_max       16
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_l_min       -10
_diffrn_reflns_limit_l_max       18

_refine_special_details          
;
;

_reflns_number_total             9750
_reflns_number_gt                4264
_reflns_threshold_expression     'I > 2σ(I)'

_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_R_factor_all          0.1483
_refine_ls_R_factor_gt           0.0754
_refine_ls_wR_factor_gt          0.2213
_refine_ls_wR_factor_ref         0.2465
_refine_ls_goodness_of_fit_ref   1.085
_refine_ls_restrained_S_all      1.068
_refine_ls_number_reflns         9750
_refine_ls_number_parameters     373
_refine_ls_number_restraints     389
_refine_ls_number_constraints    ?
_refine_ls_hydrogen_treatment    constr
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0700P)²+7.0000P] where P=(Fo²+2Fc²)/3'

_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?

_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_diff_density_max         1.489
_refine_diff_density_min         -0.401
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       ?

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_computing_data_collection       ?
_computing_cell_refinement       'SAINT V8.38A (Bruker AXS Inc., 2017)'
_computing_data_reduction        'SAINT V8.38A (Bruker AXS Inc., 2017)'
_computing_structure_solution    'SHELXT 2014/5 (Sheldrick, 2014)'
_computing_structure_refinement  'SHELXL-2018/3 (Sheldrick, 2018)'
_computing_molecular_graphics    'shelXle (C.B. Huebschle, rev 924)'
_computing_publication_material  ?

loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_refinement_flags_posn
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Cu Cu1 0.59281(9) 0.95941(7) 0.52920(6) 0.0568(3) Uani d U . . 1 . .
Cl Cl1 -0.1973(2) 0.24889(15) -0.02137(15) 0.0768(7) Uani d U . . 1 . .
B B1 -0.0939(9) 0.3797(7) -0.0106(6) 0.059(2) Uani d U . . 1 . .
C C1 0.4291(7) 0.8111(6) 0.6034(5) 0.058(2) Uani d U . . 1 . .
H H1 0.458384 0.866108 0.653517 0.069 Uiso calc U . R 1 . .
N N1 0.4732(5) 0.8233(4) 0.5321(4) 0.0525(16) Uani d U . . 1 . .
Cl Cl2 0.0977(2) 0.34785(17) 0.11613(16) 0.0871(8) Uani d U . . 1 . .
B B2 0.0058(8) 0.4082(6) -0.0690(6) 0.056(2) Uani d U . . 1 . .
C C2 0.3429(7) 0.7208(6) 0.6051(5) 0.056(2) Uani d U . . 1 . .
H H2 0.315259 0.715775 0.655893 0.067 Uiso calc U . R 1 . .
N N2 -0.2800(5) 0.0898(4) 0.5236(4) 0.0514(16) Uani d U . . 1 . .
Cl Cl3 0.0126(2) 0.31128(16) -0.14369(14) 0.0725(7) Uani d U . . 1 . .
O O3 0.4953(4) 0.9570(3) 0.4093(3) 0.0568(3) Uani d U . . 1 . .
B B3 0.0480(8) 0.4270(7) 0.0565(6) 0.057(2) Uani d U . . 1 . .
N N3 0.6875(6) 0.9628(5) 0.6551(4) 0.0606(18) Uani d U . . 1 . .
C C3 0.2958(7) 0.6355(5) 0.5301(5) 0.0482(18) Uani d U . . 1 . .
Cl Cl4 0.2106(2) 0.61865(17) 0.21619(13) 0.0731(7) Uani d U . . 1 . .
O O4 0.6711(6) 0.8635(5) 0.4375(4) 0.0882(19) Uani d U . . 1 . .
B B4 0.1010(8) 0.5560(6) 0.1052(6) 0.053(2) Uani d U . . 1 . .
C C4 0.3408(7) 0.6477(6) 0.4585(5) 0.055(2) Uani d U . . 1 . .
H H4 0.313487 0.592754 0.408638 0.066 Uiso calc U . R 1 . .
B B5 0.1272(8) 0.5179(7) 0.0019(6) 0.058(2) Uani d U . . 1 . .
C C5 0.4269(7) 0.7406(6) 0.4584(5) 0.056(2) Uani d U . . 1 . .
H H5 0.453964 0.747143 0.407315 0.067 Uiso calc U . R 1 . .
Cl Cl5 0.2665(2) 0.54092(19) 0.00442(18) 0.0874(8) Uani d U . . 1 . .
B B6 0.0352(8) 0.5292(7) -0.0978(6) 0.054(2) Uani d U . . 1 . .
C C6 0.2006(7) 0.5401(6) 0.5277(5) 0.055(2) Uani d U . . 1 . .
Cl Cl6 0.0753(2) 0.56199(17) -0.20013(14) 0.0783(7) Uani d U . . 1 . .
C C7 0.1845(7) 0.5065(6) 0.6117(5) 0.058(2) Uani d U . . 1 . .
H H7 0.238361 0.545129 0.669086 0.069 Uiso calc U . R 1 . .
C C8 0.0920(7) 0.4185(6) 0.6112(5) 0.056(2) Uani d U . . 1 . .
H H8 0.084879 0.398331 0.667261 0.068 Uiso calc U . R 1 . .
C C9 0.0098(7) 0.3607(6) 0.5260(5) 0.0537(19) Uani d U . . 1 . .
C C10 0.0229(7) 0.3910(6) 0.4421(5) 0.060(2) Uani d U . . 1 . .
H H10 -0.03053 0.351966 0.384698 0.072 Uiso calc U . R 1 . .
C C11 0.1184(7) 0.4817(6) 0.4456(5) 0.061(2) Uani d U . . 1 . .
H H11 0.125276 0.502201 0.389614 0.074 Uiso calc U . R 1 . .
C C12 -0.0889(7) 0.2682(6) 0.5243(5) 0.0515(18) Uani d U . . 1 . .
C C13 -0.1382(7) 0.2636(6) 0.5953(5) 0.054(2) Uani d U . . 1 . .
H H13 -0.108249 0.31978 0.644465 0.065 Uiso calc U . R 1 . .
C C14 -0.2324(7) 0.1747(6) 0.5925(5) 0.054(2) Uani d U . . 1 . .
H H14 -0.264146 0.173699 0.640362 0.065 Uiso calc U . R 1 . .
C C15 -0.2339(7) 0.0955(6) 0.4537(5) 0.056(2) Uani d U . . 1 . .
H H15 -0.267299 0.03919 0.404125 0.067 Uiso calc U . R 1 . .
C C16 -0.1401(7) 0.1801(6) 0.4513(5) 0.062(2) Uani d U . . 1 . .
H H16 -0.110805 0.179127 0.402074 0.075 Uiso calc U . R 1 . .
C C17 0.6973(8) 1.0155(7) 0.7366(5) 0.069(2) Uani d U . . 1 . .
H H17 0.651883 1.046713 0.734834 0.083 Uiso calc U . R 1 . .
C C18 0.7705(8) 1.0266(7) 0.8234(6) 0.077(3) Uani d U . . 1 . .
H H18 0.773673 1.064221 0.87759 0.093 Uiso calc U . R 1 . .
C C19 0.8388(8) 0.9803(6) 0.8276(5) 0.076(3) Uani d U . . 1 . .
C C20 0.8282(11) 0.9269(9) 0.7419(6) 0.129(5) Uani d U . . 1 . .
H H20 0.872489 0.894925 0.740906 0.155 Uiso calc U . R 1 . .
C C21 0.7548(10) 0.9206(9) 0.6598(6) 0.114(4) Uani d U . . 1 . .
H H21 0.751541 0.885005 0.604325 0.137 Uiso calc U . R 1 . .
C C22 0.9215(9) 0.9917(6) 0.9175(6) 0.083(3) Uani d U . . 1 . .
C C23 0.9475(11) 0.9142(8) 0.9351(7) 0.130(5) Uani d U . . 1 . .
H H23 0.910887 0.853804 0.889852 0.155 Uiso calc U . R 1 . .
C C24 0.9743(10) 1.0778(7) 0.9828(6) 0.107(4) Uani d U . . 1 . .
H H24 0.958899 1.131848 0.97359 0.128 Uiso calc U . R 1 . .


_geom_special_details            
;

All esds (except the esd in the dihedral angle between two l.s. planes)
are estimated using the full covariance matrix.  The cell esds are taken
into account individually in the estimation of esds in distances, angles
and torsion angles; correlations between esds in cell parameters are only
used when they are defined by crystal symmetry.  An approximate (isotropic)
treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Cu1 O3 . 1.957(5) ?
Cu1 N3 . 2.003(6) ?
Cu1 N1 . 2.008(6) ?
Cu1 N2 1_665 2.015(6) ?
Cu1 O3 2_676 2.366(5) ?
Cu1 O4 . 2.626(6) ?
Cl1 B1 . 1.821(9) ?
B1 B2 . 1.741(14) ?
B1 B3 . 1.767(14) ?
B1 B5 2_565 1.780(13) ?
B1 B4 2_565 1.782(12) ?
B1 B6 2_565 1.784(12) ?
C1 N1 . 1.348(9) ?
C1 C2 . 1.373(10) ?
C1 H1 . 0.93 ?
N1 C5 . 1.377(9) ?
Cl2 B3 . 1.801(9) ?
B2 B5 . 1.764(12) ?
B2 B4 2_565 1.768(14) ?
B2 B6 . 1.784(12) ?
B2 B3 . 1.787(12) ?
B2 Cl3 . 1.804(9) ?
C2 C3 . 1.413(9) ?
C2 H2 . 0.93 ?
N2 C15 . 1.350(9) ?
N2 C14 . 1.354(9) ?
B3 B4 . 1.748(12) ?
B3 B5 . 1.749(14) ?
B3 B6 2_565 1.758(14) ?
N3 C21 . 1.327(11) ?
N3 C17 . 1.341(9) ?
C3 C4 . 1.360(10) ?
C3 C6 . 1.458(10) ?
Cl4 B4 . 1.802(8) ?
B4 B6 2_565 1.739(13) ?
B4 B5 . 1.781(13) ?
C4 C5 . 1.388(10) ?
C4 H4 . 0.93 ?
B5 B6 . 1.787(13) ?
B5 Cl5 . 1.811(11) ?
C5 H5 . 0.93 ?
B6 Cl6 . 1.796(9) ?
C6 C11 . 1.363(10) ?
C6 C7 . 1.428(10) ?
C7 C8 . 1.385(10) ?
C7 H7 . 0.93 ?
C8 C9 . 1.392(10) ?
C8 H8 . 0.93 ?
C9 C10 . 1.399(10) ?
C9 C12 . 1.462(10) ?
C10 C11 . 1.417(11) ?
C10 H10 . 0.93 ?
C11 H11 . 0.93 ?
C12 C13 . 1.395(10) ?
C12 C16 . 1.416(10) ?
C13 C14 . 1.396(10) ?
C13 H13 . 0.93 ?
C14 H14 . 0.93 ?
C15 C16 . 1.383(11) ?
C15 H15 . 0.93 ?
C16 H16 . 0.93 ?
C17 C18 . 1.390(10) ?
C17 H17 . 0.93 ?
C18 C19 . 1.389(12) ?
C18 H18 . 0.93 ?
C19 C20 . 1.395(12) ?
C19 C22 . 1.484(10) ?
C20 C21 . 1.361(11) ?
C20 H20 . 0.93 ?
C21 H21 . 0.93 ?
C22 C24 . 1.332(11) ?
C22 C23 . 1.377(11) ?
C23 C24 2_777 1.387(11) ?
C23 H23 . 0.93 ?
C24 H24 . 0.93 ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
O3 Cu1 N3 . . 177.2(3) ?
O3 Cu1 N1 . . 89.6(2) ?
N3 Cu1 N1 . . 89.4(2) ?
O3 Cu1 N2 . 1_665 91.8(2) ?
N3 Cu1 N2 . 1_665 89.4(2) ?
N1 Cu1 N2 . 1_665 175.1(3) ?
O3 Cu1 O3 . 2_676 82.27(19) ?
N3 Cu1 O3 . 2_676 95.1(2) ?
N1 Cu1 O3 . 2_676 90.9(2) ?
N2 Cu1 O3 1_665 2_676 93.9(2) ?
O3 Cu1 O4 . . 89.6(2) ?
N3 Cu1 O4 . . 93.0(2) ?
N1 Cu1 O4 . . 88.4(2) ?
N2 Cu1 O4 1_665 . 86.9(2) ?
O3 Cu1 O4 2_676 . 171.86(18) ?
B2 B1 B3 . . 61.2(5) ?
B2 B1 B5 . 2_565 108.4(6) ?
B3 B1 B5 . 2_565 107.6(6) ?
B2 B1 B4 . 2_565 60.2(5) ?
B3 B1 B4 . 2_565 108.8(7) ?
B5 B1 B4 2_565 2_565 60.0(5) ?
B2 B1 B6 . 2_565 109.0(7) ?
B3 B1 B6 . 2_565 59.3(5) ?
B5 B1 B6 2_565 2_565 60.2(5) ?
B4 B1 B6 2_565 2_565 108.6(6) ?
B2 B1 Cl1 . . 121.4(6) ?
B3 B1 Cl1 . . 121.6(6) ?
B5 B1 Cl1 2_565 . 121.6(7) ?
B4 B1 Cl1 2_565 . 121.7(6) ?
B6 B1 Cl1 2_565 . 120.9(6) ?
N1 C1 C2 . . 122.8(7) ?
N1 C1 H1 . . 118.6 ?
C2 C1 H1 . . 118.6 ?
C1 N1 C5 . . 117.0(7) ?
C1 N1 Cu1 . . 121.1(5) ?
C5 N1 Cu1 . . 121.7(5) ?
B1 B2 B5 . . 107.2(6) ?
B1 B2 B4 . 2_565 61.0(5) ?
B5 B2 B4 . 2_565 107.2(6) ?
B1 B2 B6 . . 107.6(7) ?
B5 B2 B6 . . 60.5(5) ?
B4 B2 B6 2_565 . 58.6(5) ?
B1 B2 B3 . . 60.1(5) ?
B5 B2 B3 . . 59.0(5) ?
B4 B2 B3 2_565 . 108.5(7) ?
B6 B2 B3 . . 107.7(6) ?
B1 B2 Cl3 . . 122.5(6) ?
B5 B2 Cl3 . . 122.0(7) ?
B4 B2 Cl3 2_565 . 121.4(5) ?
B6 B2 Cl3 . . 121.0(6) ?
B3 B2 Cl3 . . 122.7(6) ?
C1 C2 C3 . . 120.4(7) ?
C1 C2 H2 . . 119.8 ?
C3 C2 H2 . . 119.8 ?
C15 N2 C14 . . 116.5(7) ?
C15 N2 Cu1 . 1_445 121.7(5) ?
C14 N2 Cu1 . 1_445 121.7(5) ?
Cu1 O3 Cu1 . 2_676 97.73(19) ?
B4 B3 B5 . . 61.2(5) ?
B4 B3 B6 . 2_565 59.5(5) ?
B5 B3 B6 . 2_565 108.3(6) ?
B4 B3 B1 . . 108.0(7) ?
B5 B3 B1 . . 106.7(6) ?
B6 B3 B1 2_565 . 60.8(5) ?
B4 B3 B2 . . 108.9(6) ?
B5 B3 B2 . . 59.8(5) ?
B6 B3 B2 2_565 . 108.1(7) ?
B1 B3 B2 . . 58.7(5) ?
B4 B3 Cl2 . . 121.7(6) ?
B5 B3 Cl2 . . 122.4(7) ?
B6 B3 Cl2 2_565 . 121.2(6) ?
B1 B3 Cl2 . . 121.7(6) ?
B2 B3 Cl2 . . 121.6(6) ?
C21 N3 C17 . . 116.2(7) ?
C21 N3 Cu1 . . 119.6(6) ?
C17 N3 Cu1 . . 123.8(6) ?
C4 C3 C2 . . 116.8(7) ?
C4 C3 C6 . . 121.5(7) ?
C2 C3 C6 . . 121.7(7) ?
B6 B4 B3 2_565 . 60.6(5) ?
B6 B4 B2 2_565 2_565 61.1(5) ?
B3 B4 B2 . 2_565 109.1(6) ?
B6 B4 B5 2_565 . 107.8(6) ?
B3 B4 B5 . . 59.4(5) ?
B2 B4 B5 2_565 . 107.2(6) ?
B6 B4 B1 2_565 2_565 107.8(6) ?
B3 B4 B1 . 2_565 107.7(6) ?
B2 B4 B1 2_565 2_565 58.7(5) ?
B5 B4 B1 . 2_565 59.9(5) ?
B6 B4 Cl4 2_565 . 122.2(6) ?
B3 B4 Cl4 . . 122.3(6) ?
B2 B4 Cl4 2_565 . 121.2(6) ?
B5 B4 Cl4 . . 121.9(7) ?
B1 B4 Cl4 2_565 . 121.1(6) ?
C3 C4 C5 . . 121.2(7) ?
C3 C4 H4 . . 119.4 ?
C5 C4 H4 . . 119.4 ?
B3 B5 B2 . . 61.1(5) ?
B3 B5 B1 . 2_565 107.7(7) ?
B2 B5 B1 . 2_565 108.1(7) ?
B3 B5 B4 . . 59.3(5) ?
B2 B5 B4 . . 108.5(7) ?
B1 B5 B4 2_565 . 60.1(5) ?
B3 B5 B6 . . 109.2(7) ?
B2 B5 B6 . . 60.3(5) ?
B1 B5 B6 2_565 . 60.0(5) ?
B4 B5 B6 . . 108.5(7) ?
B3 B5 Cl5 . . 122.1(6) ?
B2 B5 Cl5 . . 122.4(6) ?
B1 B5 Cl5 2_565 . 120.7(6) ?
B4 B5 Cl5 . . 121.0(6) ?
B6 B5 Cl5 . . 121.1(6) ?
N1 C5 C4 . . 121.8(7) ?
N1 C5 H5 . . 119.1 ?
C4 C5 H5 . . 119.1 ?
B4 B6 B3 2_565 2_565 59.9(5) ?
B4 B6 B2 2_565 . 60.2(5) ?
B3 B6 B2 2_565 . 107.9(7) ?
B4 B6 B1 2_565 2_565 107.6(6) ?
B3 B6 B1 2_565 2_565 59.9(5) ?
B2 B6 B1 . 2_565 107.1(6) ?
B4 B6 B5 2_565 . 107.5(6) ?
B3 B6 B5 2_565 . 107.7(6) ?
B2 B6 B5 . . 59.2(5) ?
B1 B6 B5 2_565 . 59.8(5) ?
B4 B6 Cl6 2_565 . 122.2(6) ?
B3 B6 Cl6 2_565 . 121.8(6) ?
B2 B6 Cl6 . . 122.3(6) ?
B1 B6 Cl6 2_565 . 121.7(6) ?
B5 B6 Cl6 . . 121.8(7) ?
C11 C6 C7 . . 116.4(8) ?
C11 C6 C3 . . 121.7(7) ?
C7 C6 C3 . . 121.8(7) ?
C8 C7 C6 . . 122.7(7) ?
C8 C7 H7 . . 118.7 ?
C6 C7 H7 . . 118.7 ?
C7 C8 C9 . . 119.3(7) ?
C7 C8 H8 . . 120.3 ?
C9 C8 H8 . . 120.3 ?
C8 C9 C10 . . 119.6(8) ?
C8 C9 C12 . . 120.0(7) ?
C10 C9 C12 . . 120.3(7) ?
C9 C10 C11 . . 119.3(7) ?
C9 C10 H10 . . 120.3 ?
C11 C10 H10 . . 120.3 ?
C6 C11 C10 . . 122.6(7) ?
C6 C11 H11 . . 118.7 ?
C10 C11 H11 . . 118.7 ?
C13 C12 C16 . . 116.7(7) ?
C13 C12 C9 . . 120.7(7) ?
C16 C12 C9 . . 122.6(7) ?
C12 C13 C14 . . 119.9(7) ?
C12 C13 H13 . . 120.0 ?
C14 C13 H13 . . 120.0 ?
N2 C14 C13 . . 123.3(7) ?
N2 C14 H14 . . 118.3 ?
C13 C14 H14 . . 118.3 ?
N2 C15 C16 . . 123.9(7) ?
N2 C15 H15 . . 118.0 ?
C16 C15 H15 . . 118.0 ?
C15 C16 C12 . . 119.6(8) ?
C15 C16 H16 . . 120.2 ?
C12 C16 H16 . . 120.2 ?
N3 C17 C18 . . 124.5(8) ?
N3 C17 H17 . . 117.7 ?
C18 C17 H17 . . 117.7 ?
C19 C18 C17 . . 118.7(8) ?
C19 C18 H18 . . 120.7 ?
C17 C18 H18 . . 120.7 ?
C18 C19 C20 . . 115.8(8) ?
C18 C19 C22 . . 121.5(8) ?
C20 C19 C22 . . 122.6(9) ?
C21 C20 C19 . . 121.6(9) ?
C21 C20 H20 . . 119.2 ?
C19 C20 H20 . . 119.2 ?
N3 C21 C20 . . 123.1(9) ?
N3 C21 H21 . . 118.4 ?
C20 C21 H21 . . 118.4 ?
C24 C22 C23 . . 117.9(8) ?
C24 C22 C19 . . 121.1(7) ?
C23 C22 C19 . . 121.0(8) ?
C22 C23 C24 . 2_777 123.0(9) ?
C22 C23 H23 . . 118.5 ?
C24 C23 H23 2_777 . 118.5 ?
C22 C24 C23 . 2_777 119.1(8) ?
C22 C24 H24 . . 120.5 ?
C23 C24 H24 2_777 . 120.5 ?



####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_ZH_ZJU3
_database_code_depnum_ccdc_archive 'CCDC 2033521'
loop_
_audit_author_name
_audit_author_address
'Yue ZHAO'
;Nanjing University
China
;
_audit_update_record             
;
2020-09-23 deposited with the CCDC.	2020-12-10 downloaded from the CCDC.
;
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C34 H30 Cu N4 O2'
_chemical_formula_iupac          ?
_chemical_formula_weight         590.16
_chemical_absolute_configuration ?

_chemical_melting_point          ?

_space_group_crystal_system      tetragonal
_space_group_name_H-M_alt        'I -4'
_space_group_name_Hall           'I -4'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, z'
'y, -x, -z'
'-y, x, -z'
'x+1/2, y+1/2, z+1/2'
'-x+1/2, -y+1/2, z+1/2'
'y+1/2, -x+1/2, -z+1/2'
'-y+1/2, x+1/2, -z+1/2'

_cell_length_a                   16.7900(6)
_cell_length_b                   16.7900(6)
_cell_length_c                   19.5452(7)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_volume                     5509.9(4)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    9069
_cell_measurement_theta_min      2.4261
_cell_measurement_theta_max      25.2579
_cell_measurement_temperature    296.(2)

_exptl_crystal_description       block
_exptl_crystal_colour            ?
_exptl_crystal_size_max          0.200
_exptl_crystal_size_mid          0.200
_exptl_crystal_size_min          0.200
_exptl_crystal_density_diffrn    0.711
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             1228

_exptl_absorpt_coefficient_mu    0.416
_exptl_absorpt_correction_type   Multi-Scan
_exptl_absorpt_process_details   
;
SADABS-2016/2 - Bruker AXS area detector scaling and absorption correction
;
_exptl_absorpt_correction_T_min  0.78
_exptl_absorpt_correction_T_max  0.92

_exptl_special_details           
;
;

_diffrn_ambient_temperature      296.(2)

_diffrn_source                   TXS
_diffrn_source_type              'Rotaing Anode'

_diffrn_radiation_type           ' Mo K\a'
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_monochromator  'Helios Multi-layer Optic'

_diffrn_measurement_device_type  'Bruker D8 VENTURE PHOTON 100'
_diffrn_measurement_method       ?

_diffrn_detector_area_resol_mean 10.4167

_diffrn_reflns_number            20978
_diffrn_reflns_av_R_equivalents  0.0473
_diffrn_reflns_av_unetI/netI     0.0426
_diffrn_reflns_theta_min         2.43
_diffrn_reflns_theta_max         25.41
_diffrn_reflns_theta_full        25.41
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measured_fraction_theta_full 0.998
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_h_max       20
_diffrn_reflns_limit_k_min       -20
_diffrn_reflns_limit_k_max       20
_diffrn_reflns_limit_l_min       -22
_diffrn_reflns_limit_l_max       23

_refine_special_details          
;

Refined as a 4-component inversion twin.
;

_reflns_number_total             5074
_reflns_number_gt                4631
_reflns_threshold_expression     'I > 2σ(I)'

_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_R_factor_all          0.0670
_refine_ls_R_factor_gt           0.0606
_refine_ls_wR_factor_gt          0.1818
_refine_ls_wR_factor_ref         0.1881
_refine_ls_goodness_of_fit_ref   1.067
_refine_ls_restrained_S_all      1.068
_refine_ls_number_reflns         5074
_refine_ls_number_parameters     154
_refine_ls_number_restraints     455
_refine_ls_number_constraints    ?
_refine_ls_hydrogen_treatment    constr
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.1271P)²+7.7864P] where P=(Fo²+2Fc²)/3'

_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?

_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_diff_density_max         0.496
_refine_diff_density_min         -0.584
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       ?
_refine_ls_abs_structure_details 
;

Twinning involves inversion, so Flack parameter cannot be determined
;
_refine_ls_abs_structure_Flack   .

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_computing_data_collection       ?
_computing_cell_refinement       'SAINT V8.38A (Bruker AXS Inc., 2017)'
_computing_data_reduction        'SAINT V8.38A (Bruker AXS Inc., 2017)'
_computing_structure_solution    'SHELXT 2014/5 (Sheldrick, 2014)'
_computing_structure_refinement  'SHELXL-2018/3 (Sheldrick, 2018)'
_computing_molecular_graphics    'shelXle (C.B. Huebschle, rev 924)'
_computing_publication_material  ?

loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_refinement_flags_posn
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Cu Cu1 0.5 0.5 0.78545(5) 0.0286(3) Uani d TU P S 1 . .
C C1 0.6611(7) 0.6349(6) 0.8284(6) 0.058(3) Uani d U . . 1 . .
H H1A 0.706116 0.648621 0.800529 0.087 Uiso calc U . R 1 . .
H H1B 0.676815 0.595939 0.86178 0.087 Uiso calc U . R 1 . .
H H1C 0.641868 0.681664 0.851337 0.087 Uiso calc U . R 1 . .
O O1 0.6028(5) 0.6046(5) 0.7886(3) 0.0445(12) Uani d U . . 1 . .
N N1_1 0.4380(3) 0.5589(3) 0.7129(2) 0.0272(10) Uani d U . G 1 . .
C C1_1 0.4338(3) 0.6412(3) 0.7193(3) 0.0399(17) Uani d U . G 1 . .
H H1_1 0.46318 0.667035 0.752932 0.048 Uiso calc U . R 1 . .
C C2_1 0.3856(4) 0.6850(3) 0.6753(3) 0.0423(19) Uani d U . G 1 . .
H H2_1 0.38273 0.740074 0.679606 0.051 Uiso calc U . R 1 . .
C C3_1 0.3416(4) 0.6464(4) 0.6250(3) 0.0373(16) Uani d U . G 1 . .
C C4_1 0.3458(4) 0.5640(4) 0.6186(3) 0.0443(19) Uani d U . G 1 . .
H H4_1 0.316352 0.538233 0.584984 0.053 Uiso calc U . R 1 . .
C C5_1 0.3940(4) 0.5203(3) 0.6626(3) 0.051(2) Uani d U . G 1 . .
H H5_1 0.396801 0.465193 0.658309 0.061 Uiso calc U . R 1 . .
C C6_1 0.3007(4) 0.7026(4) 0.5736(3) 0.0435(16) Uani d U . G 1 . .
C C7_1 0.3244(4) 0.7800(5) 0.5585(4) 0.045(2) Uani d U . G 1 . .
H H7_1 0.371627 0.799927 0.576505 0.054 Uiso calc U . R 1 . .
C C8_1 0.2775(5) 0.8276(4) 0.5165(4) 0.0420(19) Uani d U . G 1 . .
H H8_1 0.293284 0.879321 0.506444 0.05 Uiso calc U . R 1 . .
C C9_1 0.2069(4) 0.7977(4) 0.4896(3) 0.0405(15) Uani d U . G 1 . .
C C10_1 0.1832(3) 0.7204(5) 0.5047(4) 0.0448(19) Uani d U . G 1 . .
H H10_1 0.135979 0.700428 0.486646 0.054 Uiso calc U . R 1 . .
C C11_1 0.2301(4) 0.6728(4) 0.5466(4) 0.0411(19) Uani d U . G 1 . .
H H11_1 0.214321 0.621032 0.556708 0.049 Uiso calc U . R 1 . .
N N2_1 0.0651(3) 0.9443(4) 0.3588(2) 0.0405(15) Uani d U . G 1 . .
C C12_1 0.0294(2) 0.9009(5) 0.4110(3) 0.048(2) Uani d U . G 1 . .
H H12_1 -0.025649 0.902345 0.416528 0.057 Uiso calc U . R 1 . .
C C13_1 0.0758(3) 0.8554(4) 0.4550(3) 0.050(2) Uani d U . G 1 . .
H H13_1 0.051908 0.826417 0.489987 0.06 Uiso calc U . R 1 . .
C C14_1 0.1580(3) 0.8533(4) 0.4468(3) 0.0408(17) Uani d U . G 1 . .
C C15_1 0.1938(2) 0.8966(5) 0.3946(3) 0.050(2) Uani d U . G 1 . .
H H15_1 0.24876 0.8952 0.389084 0.06 Uiso calc U . R 1 . .
C C16_1 0.1473(3) 0.9421(4) 0.3506(3) 0.053(2) Uani d U . G 1 . .
H H16_1 0.171203 0.971128 0.315624 0.063 Uiso calc U . R 1 . .


_geom_special_details            
;

All esds (except the esd in the dihedral angle between two l.s. planes)
are estimated using the full covariance matrix.  The cell esds are taken
into account individually in the estimation of esds in distances, angles
and torsion angles; correlations between esds in cell parameters are only
used when they are defined by crystal symmetry.  An approximate (isotropic)
treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Cu1 N1_1 . 2.018(3) ?
Cu1 N1_1 2_665 2.018(3) ?
Cu1 N2_1 5_545 2.031(4) ?
Cu1 N2_1 6_565 2.031(4) ?
Cu1 O1 . 2.463(6) ?
C1 O1 . 1.350(13) ?
C1 H1A . 0.96 ?
C1 H1B . 0.96 ?
C1 H1C . 0.96 ?
N1_1 C1_1 . 1.39 ?
N1_1 C5_1 . 1.39 ?
C1_1 C2_1 . 1.39 ?
C1_1 H1_1 . 0.93 ?
C2_1 C3_1 . 1.39 ?
C2_1 H2_1 . 0.93 ?
C3_1 C4_1 . 1.39 ?
C3_1 C6_1 . 1.540(5) ?
C4_1 C5_1 . 1.39 ?
C4_1 H4_1 . 0.93 ?
C5_1 H5_1 . 0.93 ?
C6_1 C7_1 . 1.39 ?
C6_1 C11_1 . 1.39 ?
C7_1 C8_1 . 1.39 ?
C7_1 H7_1 . 0.93 ?
C8_1 C9_1 . 1.39 ?
C8_1 H8_1 . 0.93 ?
C9_1 C10_1 . 1.39 ?
C9_1 C14_1 . 1.497(6) ?
C10_1 C11_1 . 1.39 ?
C10_1 H10_1 . 0.93 ?
C11_1 H11_1 . 0.93 ?
N2_1 C12_1 . 1.39 ?
N2_1 C16_1 . 1.39 ?
C12_1 C13_1 . 1.39 ?
C12_1 H12_1 . 0.93 ?
C13_1 C14_1 . 1.39 ?
C13_1 H13_1 . 0.93 ?
C14_1 C15_1 . 1.39 ?
C15_1 C16_1 . 1.39 ?
C15_1 H15_1 . 0.93 ?
C16_1 H16_1 . 0.93 ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
N1_1 Cu1 N1_1 . 2_665 90.7(3) ?
N1_1 Cu1 N2_1 . 5_545 177.9(3) ?
N1_1 Cu1 N2_1 2_665 5_545 89.58(18) ?
N1_1 Cu1 N2_1 . 6_565 89.58(18) ?
N1_1 Cu1 N2_1 2_665 6_565 177.9(3) ?
N2_1 Cu1 N2_1 5_545 6_565 90.2(3) ?
N1_1 Cu1 O1 . . 91.7(3) ?
N1_1 Cu1 O1 2_665 . 90.3(3) ?
N2_1 Cu1 O1 5_545 . 86.2(3) ?
N2_1 Cu1 O1 6_565 . 91.8(3) ?
O1 C1 H1A . . 109.5 ?
O1 C1 H1B . . 109.5 ?
H1A C1 H1B . . 109.5 ?
O1 C1 H1C . . 109.5 ?
H1A C1 H1C . . 109.5 ?
H1B C1 H1C . . 109.5 ?
C1 O1 Cu1 . . 142.3(6) ?
C1_1 N1_1 C5_1 . . 120.0 ?
C1_1 N1_1 Cu1 . . 116.8(3) ?
C5_1 N1_1 Cu1 . . 122.9(3) ?
C2_1 C1_1 N1_1 . . 120.0 ?
C2_1 C1_1 H1_1 . . 120.0 ?
N1_1 C1_1 H1_1 . . 120.0 ?
C1_1 C2_1 C3_1 . . 120.0 ?
C1_1 C2_1 H2_1 . . 120.0 ?
C3_1 C2_1 H2_1 . . 120.0 ?
C4_1 C3_1 C2_1 . . 120.0 ?
C4_1 C3_1 C6_1 . . 125.0(5) ?
C2_1 C3_1 C6_1 . . 114.4(5) ?
C5_1 C4_1 C3_1 . . 120.0 ?
C5_1 C4_1 H4_1 . . 120.0 ?
C3_1 C4_1 H4_1 . . 120.0 ?
C4_1 C5_1 N1_1 . . 120.0 ?
C4_1 C5_1 H5_1 . . 120.0 ?
N1_1 C5_1 H5_1 . . 120.0 ?
C7_1 C6_1 C11_1 . . 120.0 ?
C7_1 C6_1 C3_1 . . 125.7(6) ?
C11_1 C6_1 C3_1 . . 114.0(6) ?
C6_1 C7_1 C8_1 . . 120.0 ?
C6_1 C7_1 H7_1 . . 120.0 ?
C8_1 C7_1 H7_1 . . 120.0 ?
C9_1 C8_1 C7_1 . . 120.0 ?
C9_1 C8_1 H8_1 . . 120.0 ?
C7_1 C8_1 H8_1 . . 120.0 ?
C8_1 C9_1 C10_1 . . 120.0 ?
C8_1 C9_1 C14_1 . . 117.0(6) ?
C10_1 C9_1 C14_1 . . 122.9(6) ?
C11_1 C10_1 C9_1 . . 120.0 ?
C11_1 C10_1 H10_1 . . 120.0 ?
C9_1 C10_1 H10_1 . . 120.0 ?
C10_1 C11_1 C6_1 . . 120.0 ?
C10_1 C11_1 H11_1 . . 120.0 ?
C6_1 C11_1 H11_1 . . 120.0 ?
C12_1 N2_1 C16_1 . . 120.0 ?
C12_1 N2_1 Cu1 . 5_454 121.8(3) ?
C16_1 N2_1 Cu1 . 5_454 117.7(3) ?
C13_1 C12_1 N2_1 . . 120.0 ?
C13_1 C12_1 H12_1 . . 120.0 ?
N2_1 C12_1 H12_1 . . 120.0 ?
C12_1 C13_1 C14_1 . . 120.0 ?
C12_1 C13_1 H13_1 . . 120.0 ?
C14_1 C13_1 H13_1 . . 120.0 ?
C15_1 C14_1 C13_1 . . 120.0 ?
C15_1 C14_1 C9_1 . . 120.0(5) ?
C13_1 C14_1 C9_1 . . 119.7(5) ?
C14_1 C15_1 C16_1 . . 120.0 ?
C14_1 C15_1 H15_1 . . 120.0 ?
C16_1 C15_1 H15_1 . . 120.0 ?
C15_1 C16_1 N2_1 . . 120.0 ?
C15_1 C16_1 H16_1 . . 120.0 ?
N2_1 C16_1 H16_1 . . 120.0 ?



####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_1121ZH_ZJU2
_database_code_depnum_ccdc_archive 'CCDC 2033517'
loop_
_audit_author_name
_audit_author_address
'Yue ZHAO'
;Nanjing University
China
;
_audit_update_record             
;
2020-09-23 deposited with the CCDC.	2020-12-10 downloaded from the CCDC.
;
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C32 H30 B12 Cl12 Cu N4 O3'
_chemical_formula_iupac          ?
_chemical_formula_weight         1137.26
_chemical_absolute_configuration ?

_chemical_melting_point          ?

_space_group_crystal_system      orthorhombic
_space_group_name_H-M_alt        'A m a 2'
_space_group_name_Hall           'A 2 -2a'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, z'
'x+1/2, -y, z'
'-x+1/2, y, z'
'x, y+1/2, z+1/2'
'-x, -y+1/2, z+1/2'
'x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, z+1/2'

_cell_length_a                   17.1465(8)
_cell_length_b                   20.3849(8)
_cell_length_c                   23.1008(8)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_volume                     8074.4(6)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    9311
_cell_measurement_theta_min      2.3246
_cell_measurement_theta_max      27.0930
_cell_measurement_temperature    296.(2)

_exptl_crystal_description       block
_exptl_crystal_colour            ?
_exptl_crystal_size_max          0.2
_exptl_crystal_size_mid          0.2
_exptl_crystal_size_min          0.2
_exptl_crystal_density_diffrn    0.936
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             2268

_exptl_absorpt_coefficient_mu    0.691
_exptl_absorpt_correction_type   Multi-Scan
_exptl_absorpt_process_details   
;
SADABS-2016/2 - Bruker AXS area detector scaling and absorption correction
;
_exptl_absorpt_correction_T_min  0.6201
_exptl_absorpt_correction_T_max  0.7455

_exptl_special_details           
;
;

_diffrn_ambient_temperature      296.(2)

_diffrn_source                   TXS
_diffrn_source_type              'Rotaing Anode'

_diffrn_radiation_type           ' Mo K\a'
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_monochromator  'Helios Multi-layer Optic'

_diffrn_measurement_device_type  'Bruker D8 VENTURE PHOTON 100'
_diffrn_measurement_method       ?

_diffrn_detector_area_resol_mean 10.4167

_diffrn_reflns_number            22928
_diffrn_reflns_av_R_equivalents  0.0400
_diffrn_reflns_av_unetI/netI     0.0524
_diffrn_reflns_theta_min         2.33
_diffrn_reflns_theta_max         27.17
_diffrn_reflns_theta_full        27.17
_diffrn_measured_fraction_theta_max 0.990
_diffrn_measured_fraction_theta_full 0.990
_diffrn_reflns_limit_h_min       -22
_diffrn_reflns_limit_h_max       20
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_k_max       26
_diffrn_reflns_limit_l_min       -27
_diffrn_reflns_limit_l_max       29

_refine_special_details          
;

Refined as a 2-component inversion twin.
;

_reflns_number_total             8985
_reflns_number_gt                7353
_reflns_threshold_expression     'I > 2σ(I)'

_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_R_factor_all          0.0501
_refine_ls_R_factor_gt           0.0367
_refine_ls_wR_factor_gt          0.0904
_refine_ls_wR_factor_ref         0.0959
_refine_ls_goodness_of_fit_ref   1.019
_refine_ls_restrained_S_all      1.012
_refine_ls_number_reflns         8985
_refine_ls_number_parameters     329
_refine_ls_number_restraints     221
_refine_ls_number_constraints    ?
_refine_ls_hydrogen_treatment    constr
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0502P)²] where P=(Fo²+2Fc²)/3'

_atom_sites_solution_hydrogens   mixed
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?

_refine_ls_shift/su_max          0.050
_refine_ls_shift/su_mean         0.002
_refine_diff_density_max         0.269
_refine_diff_density_min         -0.312
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       ?
_refine_ls_abs_structure_details 
;

Refined as an inversion twin.
;
_refine_ls_abs_structure_Flack   0.471(16)

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_computing_data_collection       ?
_computing_cell_refinement       'SAINT V8.38A (Bruker AXS Inc., 2017)'
_computing_data_reduction        'SAINT V8.38A (Bruker AXS Inc., 2017)'
_computing_structure_solution    'SHELXT 2018/2 (Sheldrick, 2018)'
_computing_structure_refinement  'SHELXL-2018/3 (Sheldrick, 2018)'
_computing_molecular_graphics    'shelXle (C.B. Huebschle, rev 924)'
_computing_publication_material  ?

loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_refinement_flags_posn
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Cu Cu1 0.5 0.5 0.62406(3) 0.01828(13) Uani d T P S 1.0 . .
O O1 0.25 0.42723(18) 0.55952(17) 0.0351(10) Uani d T P DS 1.0 . .
H H1 0.25 0.427605 0.522304 0.053 Uiso d U P DR 1.0 . .
H H1A 0.25 0.387865 0.573405 0.053 Uiso d U P DR 1.0 . .
Cl Cl1 0.25 -0.01224(7) 0.54389(7) 0.0437(4) Uani d T P S 1.0 . .
B B1 0.25 0.0673(3) 0.5752(3) 0.0292(14) Uani d T P S 1.0 . .
Cl Cl2 0.42290(7) 0.05468(6) 0.61561(6) 0.0509(3) Uani d . . . 1.0 . .
O O2 0.35811(15) 0.49806(12) 0.62698(13) 0.0291(5) Uani d . . . 1.0 . .
H H2A 0.323735 0.528221 0.632709 0.044 Uiso d U . R 1.0 . .
H H2B 0.320635 0.470523 0.615911 0.044 Uiso d U . DR 1.0 . .
B B2 0.3347(3) 0.1003(2) 0.60965(18) 0.0297(10) Uani d . . . 1.0 . .
Cl Cl3 0.35587(7) 0.12522(5) 0.47746(5) 0.0443(3) Uani d . . . 1.0 . .
B B3 0.3020(3) 0.1348(2) 0.5448(2) 0.0286(10) Uani d . . . 1.0 . .
Cl Cl4 0.42261(6) 0.23449(6) 0.59374(5) 0.0440(3) Uani d . . . 1.0 . .
B B4 0.3336(3) 0.1874(2) 0.5993(2) 0.0323(11) Uani d . . . 1.0 . .
B B5 0.25 0.2079(3) 0.5588(3) 0.0257(13) Uani d T P S 1.0 . .
Cl Cl5 0.25 0.27613(7) 0.50851(6) 0.0391(4) Uani d T P S 1.0 . .
Cl Cl6 0.25 0.30149(7) 0.66587(7) 0.0391(4) Uani d T P S 1.0 . .
B B6 0.25 0.2190(3) 0.6349(3) 0.0304(15) Uani d T P S 1.0 . .
Cl Cl7 0.14317(8) 0.16376(6) 0.73200(5) 0.0472(3) Uani d . . . 1.0 . .
B B7 0.1966(3) 0.1542(2) 0.6669(2) 0.0302(10) Uani d . . . 1.0 . .
B B8 0.25 0.0795(3) 0.6517(3) 0.0304(15) Uani d T P S 1.0 . .
Cl Cl8 0.25 0.01239(8) 0.70110(7) 0.0484(5) Uani d T P S 1.0 . .
N N1_1 0.49597(18) 0.07006(16) 0.18642(12) 0.0206(7) Uani d U . . 1.0 . .
N N2_1 0.49687(18) 0.43054(16) 0.56111(12) 0.0203(7) Uani d U . . 1.0 . .
C C1_1 0.4469(2) 0.06511(18) 0.23062(16) 0.0258(8) Uani d U . . 1.0 . .
H H1_1 0.410908 0.031 0.230125 0.031 Uiso calc U . R 1.0 . .
C C2_1 0.4459(3) 0.10702(18) 0.27691(16) 0.0291(9) Uani d U . . 1.0 . .
H H2_1 0.410911 0.100467 0.307111 0.035 Uiso calc U . R 1.0 . .
C C3_1 0.4971(2) 0.15883(18) 0.27834(16) 0.0220(9) Uani d U . . 1.0 . .
C C4_1 0.5482(3) 0.1649(2) 0.23148(18) 0.0331(10) Uani d U . . 1.0 . .
H H4_1 0.583488 0.199534 0.230289 0.04 Uiso calc U . R 1.0 . .
C C5_1 0.5467(3) 0.11998(18) 0.18726(15) 0.0274(9) Uani d U . . 1.0 . .
H H5_1 0.581991 0.124341 0.156936 0.033 Uiso calc U . R 1.0 . .
C C6_1 0.4989(2) 0.20732(16) 0.32765(13) 0.0241(9) Uani d U . DG 1.0 . .
C C7_1 0.5010(3) 0.18367(15) 0.38406(14) 0.0294(19) Uani d U P DG 0.463(4) A 1
H H7_1 0.502441 0.138708 0.390821 0.035 Uiso calc U P R 0.463(4) A 1
C C8_1 0.5009(3) 0.22720(17) 0.43037(12) 0.0266(19) Uani d U P DG 0.463(4) A 1
H H8_1 0.502291 0.211376 0.468112 0.032 Uiso calc U P R 0.463(4) A 1
C C9_1 0.4987(2) 0.29440(16) 0.42026(14) 0.0256(9) Uani d U . DG 1.0 A .
C C10_1 0.4966(3) 0.31805(15) 0.36385(15) 0.031(2) Uani d U P DG 0.463(4) A 1
H H10_1 0.495164 0.363012 0.357093 0.037 Uiso calc U P R 0.463(4) A 1
C C11_1 0.4967(3) 0.27452(17) 0.31754(13) 0.0296(19) Uani d U P DG 0.463(4) A 1
H H11_1 0.495314 0.290345 0.2798 0.036 Uiso calc U P R 0.463(4) A 1
C C7A_1 0.4271(5) 0.2271(4) 0.3522(3) 0.0317(17) Uani d U P D 0.537(4) A 2
H H7A_1 0.380266 0.212332 0.336592 0.038 Uiso calc U P R 0.537(4) A 2
C C8A_1 0.4268(4) 0.2684(4) 0.3996(3) 0.0288(17) Uani d U P D 0.537(4) A 2
H H8A_1 0.380134 0.279081 0.417779 0.035 Uiso calc U P R 0.537(4) A 2
C C10A_1 0.5650(4) 0.2772(4) 0.3938(3) 0.0288(17) Uani d U P D 0.537(4) A 2
H H10A_1 0.611743 0.295578 0.406182 0.035 Uiso calc U P R 0.537(4) A 2
C C11A_1 0.5658(5) 0.2329(4) 0.3487(3) 0.0290(17) Uani d U P D 0.537(4) A 2
H H11A_1 0.613235 0.22042 0.332466 0.035 Uiso calc U P R 0.537(4) A 2
C C12_1 0.4968(2) 0.3404(2) 0.46959(18) 0.0268(10) Uani d U . . 1.0 . .
C C13_1 0.5495(3) 0.33486(18) 0.51585(16) 0.0269(9) Uani d U . . 1.0 . .
H H13_1 0.585457 0.300744 0.516863 0.032 Uiso calc U . R 1.0 . .
C C14_1 0.5472(3) 0.38030(18) 0.55951(15) 0.0253(9) Uani d U . . 1.0 . .
H H14_1 0.582657 0.376031 0.58976 0.03 Uiso calc U . R 1.0 . .
C C15_1 0.4453(2) 0.43519(18) 0.51746(16) 0.0265(9) Uani d U . . 1.0 . .
H H15_1 0.409666 0.469551 0.517564 0.032 Uiso calc U . R 1.0 . .
C C16_1 0.4437(2) 0.3908(2) 0.47268(17) 0.0312(9) Uani d U . . 1.0 . .
H H16_1 0.405953 0.394969 0.443975 0.037 Uiso calc U . R 1.0 . .


_geom_special_details            
;

All esds (except the esd in the dihedral angle between two l.s. planes)
are estimated using the full covariance matrix.  The cell esds are taken
into account individually in the estimation of esds in distances, angles
and torsion angles; correlations between esds in cell parameters are only
used when they are defined by crystal symmetry.  An approximate (isotropic)
treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Cu1 N1_1 5 2.030(3) ?
Cu1 N1_1 6_655 2.030(3) ?
Cu1 N2_1 2_665 2.030(3) ?
Cu1 N2_1 . 2.030(3) ?
Cu1 O2 . 2.434(3) ?
Cu1 O2 2_665 2.434(3) ?
Cl1 B1 . 1.776(7) ?
B1 B3 4 1.784(7) ?
B1 B3 . 1.784(7) ?
B1 B8 . 1.784(9) ?
B1 B2 . 1.786(6) ?
B1 B2 4 1.787(6) ?
Cl2 B2 . 1.781(5) ?
B2 B3 . 1.746(6) ?
B2 B4 . 1.793(6) ?
B2 B8 . 1.798(6) ?
B2 B7 4 1.800(6) ?
Cl3 B3 . 1.820(5) ?
B3 B4 . 1.741(6) ?
B3 B5 . 1.768(7) ?
B3 B3 4 1.784(9) ?
Cl4 B4 . 1.807(5) ?
B4 B5 . 1.762(6) ?
B4 B6 . 1.774(6) ?
B4 B7 4 1.779(7) ?
B5 B6 . 1.773(9) ?
B5 Cl5 . 1.812(6) ?
Cl6 B6 . 1.827(6) ?
B6 B7 4 1.769(7) ?
B6 B7 . 1.769(7) ?
Cl7 B7 . 1.773(5) ?
B7 B8 . 1.810(7) ?
B7 B7 4 1.830(10) ?
B8 Cl8 . 1.781(7) ?
N1_1 C1_1 . 1.327(5) ?
N1_1 C5_1 . 1.339(5) ?
N2_1 C14_1 . 1.340(5) ?
N2_1 C15_1 . 1.344(5) ?
C1_1 C2_1 . 1.369(5) ?
C2_1 C3_1 . 1.374(5) ?
C3_1 C4_1 . 1.399(5) ?
C3_1 C6_1 . 1.508(4) ?
C4_1 C5_1 . 1.372(5) ?
C6_1 C11A_1 . 1.351(8) ?
C6_1 C7_1 . 1.39 ?
C6_1 C11_1 . 1.39 ?
C6_1 C7A_1 . 1.415(8) ?
C7_1 C8_1 . 1.39 ?
C8_1 C9_1 . 1.39 ?
C9_1 C10A_1 . 1.337(8) ?
C9_1 C10_1 . 1.39 ?
C9_1 C8A_1 . 1.425(8) ?
C9_1 C12_1 . 1.476(5) ?
C10_1 C11_1 . 1.39 ?
C7A_1 C8A_1 . 1.379(8) ?
C10A_1 C11A_1 . 1.380(8) ?
C12_1 C16_1 . 1.376(6) ?
C12_1 C13_1 . 1.403(6) ?
C13_1 C14_1 . 1.370(5) ?
C15_1 C16_1 . 1.374(5) ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
N1_1 Cu1 N1_1 5 6_655 89.56(17) ?
N1_1 Cu1 N2_1 5 2_665 91.07(9) ?
N1_1 Cu1 N2_1 6_655 2_665 176.50(12) ?
N1_1 Cu1 N2_1 5 . 176.50(12) ?
N1_1 Cu1 N2_1 6_655 . 91.07(9) ?
N2_1 Cu1 N2_1 2_665 . 88.51(18) ?
N1_1 Cu1 O2 5 . 87.58(11) ?
N1_1 Cu1 O2 6_655 . 90.17(11) ?
N2_1 Cu1 O2 2_665 . 93.30(11) ?
N2_1 Cu1 O2 . . 88.98(11) ?
N1_1 Cu1 O2 5 2_665 90.17(11) ?
N1_1 Cu1 O2 6_655 2_665 87.58(11) ?
N2_1 Cu1 O2 2_665 2_665 88.97(11) ?
N2_1 Cu1 O2 . 2_665 93.30(11) ?
O2 Cu1 O2 . 2_665 176.82(14) ?
Cl1 B1 B3 . 4 122.9(3) ?
Cl1 B1 B3 . . 122.9(3) ?
B3 B1 B3 4 . 60.0(4) ?
Cl1 B1 B8 . . 122.1(4) ?
B3 B1 B8 4 . 106.4(4) ?
B3 B1 B8 . . 106.4(4) ?
Cl1 B1 B2 . . 121.7(2) ?
B3 B1 B2 4 . 106.9(4) ?
B3 B1 B2 . . 58.6(2) ?
B8 B1 B2 . . 60.5(2) ?
Cl1 B1 B2 . 4 121.7(2) ?
B3 B1 B2 4 4 58.6(2) ?
B3 B1 B2 . 4 106.9(4) ?
B8 B1 B2 . 4 60.5(2) ?
B2 B1 B2 . 4 108.7(4) ?
B3 B2 Cl2 . . 123.3(3) ?
B3 B2 B1 . . 60.6(3) ?
Cl2 B2 B1 . . 121.9(3) ?
B3 B2 B4 . . 58.9(3) ?
Cl2 B2 B4 . . 122.4(3) ?
B1 B2 B4 . . 107.8(4) ?
B3 B2 B8 . . 107.4(3) ?
Cl2 B2 B8 . . 121.4(3) ?
B1 B2 B8 . . 59.7(3) ?
B4 B2 B8 . . 107.3(4) ?
B3 B2 B7 . 4 106.8(3) ?
Cl2 B2 B7 . 4 121.0(3) ?
B1 B2 B7 . 4 108.3(3) ?
B4 B2 B7 . 4 59.4(2) ?
B8 B2 B7 . 4 60.4(3) ?
B4 B3 B2 . . 61.9(3) ?
B4 B3 B5 . . 60.3(3) ?
B2 B3 B5 . . 110.2(3) ?
B4 B3 B1 . . 110.3(4) ?
B2 B3 B1 . . 60.8(3) ?
B5 B3 B1 . . 109.0(3) ?
B4 B3 B3 . 4 108.1(2) ?
B2 B3 B3 . 4 108.7(2) ?
B5 B3 B3 . 4 59.69(18) ?
B1 B3 B3 . 4 59.99(18) ?
B4 B3 Cl3 . . 121.7(3) ?
B2 B3 Cl3 . . 121.9(3) ?
B5 B3 Cl3 . . 120.2(3) ?
B1 B3 Cl3 . . 120.6(3) ?
B3 B3 Cl3 4 . 120.49(15) ?
B3 B4 B5 . . 60.6(3) ?
B3 B4 B6 . . 107.9(3) ?
B5 B4 B6 . . 60.2(3) ?
B3 B4 B7 . 4 108.0(3) ?
B5 B4 B7 . 4 108.6(3) ?
B6 B4 B7 . 4 59.7(3) ?
B3 B4 B2 . . 59.2(2) ?
B5 B4 B2 . . 108.3(4) ?
B6 B4 B2 . . 107.8(4) ?
B7 B4 B2 4 . 60.5(3) ?
B3 B4 Cl4 . . 122.6(3) ?
B5 B4 Cl4 . . 121.6(3) ?
B6 B4 Cl4 . . 121.5(3) ?
B7 B4 Cl4 4 . 120.7(3) ?
B2 B4 Cl4 . . 121.8(3) ?
B4 B5 B4 . 4 108.9(4) ?
B4 B5 B3 . . 59.1(2) ?
B4 B5 B3 4 . 107.9(4) ?
B4 B5 B3 . 4 107.9(4) ?
B4 B5 B3 4 4 59.1(2) ?
B3 B5 B3 . 4 60.6(4) ?
B4 B5 B6 . . 60.3(2) ?
B4 B5 B6 4 . 60.3(2) ?
B3 B5 B6 . . 106.8(4) ?
B3 B5 B6 4 . 106.8(4) ?
B4 B5 Cl5 . . 121.5(2) ?
B4 B5 Cl5 4 . 121.5(2) ?
B3 B5 Cl5 . . 122.0(3) ?
B3 B5 Cl5 4 . 122.0(3) ?
B6 B5 Cl5 . . 122.5(4) ?
B7 B6 B7 4 . 62.3(4) ?
B7 B6 B5 4 . 108.6(4) ?
B7 B6 B5 . . 108.5(4) ?
B7 B6 B4 4 4 109.9(4) ?
B7 B6 B4 . 4 60.3(3) ?
B5 B6 B4 . 4 59.6(2) ?
B7 B6 B4 4 . 60.3(3) ?
B7 B6 B4 . . 109.9(4) ?
B5 B6 B4 . . 59.6(2) ?
B4 B6 B4 4 . 107.8(4) ?
B7 B6 Cl6 4 . 121.6(3) ?
B7 B6 Cl6 . . 121.6(3) ?
B5 B6 Cl6 . . 120.4(4) ?
B4 B6 Cl6 4 . 121.0(3) ?
B4 B6 Cl6 . . 121.0(3) ?
B6 B7 Cl7 . . 122.6(3) ?
B6 B7 B4 . 4 60.0(3) ?
Cl7 B7 B4 . 4 123.5(3) ?
B6 B7 B2 . 4 107.7(3) ?
Cl7 B7 B2 . 4 122.4(3) ?
B4 B7 B2 4 4 60.1(2) ?
B6 B7 B8 . . 106.6(3) ?
Cl7 B7 B8 . . 121.2(3) ?
B4 B7 B8 4 . 107.4(3) ?
B2 B7 B8 4 . 59.7(3) ?
B6 B7 B7 . 4 58.85(19) ?
Cl7 B7 B7 . 4 121.12(16) ?
B4 B7 B7 4 4 106.9(2) ?
B2 B7 B7 4 4 107.3(2) ?
B8 B7 B7 . 4 59.63(18) ?
Cl8 B8 B1 . . 121.8(4) ?
Cl8 B8 B2 . . 121.8(2) ?
B1 B8 B2 . . 59.8(2) ?
Cl8 B8 B2 . 4 121.8(2) ?
B1 B8 B2 . 4 59.8(2) ?
B2 B8 B2 . 4 107.7(4) ?
Cl8 B8 B7 . . 121.5(3) ?
B1 B8 B7 . . 108.0(4) ?
B2 B8 B7 . . 108.3(4) ?
B2 B8 B7 4 . 59.9(2) ?
Cl8 B8 B7 . 4 121.5(3) ?
B1 B8 B7 . 4 108.0(4) ?
B2 B8 B7 . 4 59.9(2) ?
B2 B8 B7 4 4 108.3(4) ?
B7 B8 B7 . 4 60.7(4) ?
C1_1 N1_1 C5_1 . . 117.3(3) ?
C1_1 N1_1 Cu1 . 5_544 121.0(3) ?
C5_1 N1_1 Cu1 . 5_544 121.5(2) ?
C14_1 N2_1 C15_1 . . 117.2(3) ?
C14_1 N2_1 Cu1 . . 122.4(2) ?
C15_1 N2_1 Cu1 . . 120.4(3) ?
N1_1 C1_1 C2_1 . . 124.2(4) ?
C1_1 C2_1 C3_1 . . 119.4(4) ?
C2_1 C3_1 C4_1 . . 116.7(3) ?
C2_1 C3_1 C6_1 . . 122.4(3) ?
C4_1 C3_1 C6_1 . . 120.9(3) ?
C5_1 C4_1 C3_1 . . 120.4(4) ?
N1_1 C5_1 C4_1 . . 122.0(4) ?
C7_1 C6_1 C11_1 . . 120.0 ?
C11A_1 C6_1 C7A_1 . . 119.0(5) ?
C11A_1 C6_1 C3_1 . . 122.8(4) ?
C7_1 C6_1 C3_1 . . 118.8(2) ?
C11_1 C6_1 C3_1 . . 121.2(2) ?
C7A_1 C6_1 C3_1 . . 118.2(4) ?
C6_1 C7_1 C8_1 . . 120.0 ?
C9_1 C8_1 C7_1 . . 120.0 ?
C8_1 C9_1 C10_1 . . 120.0 ?
C10A_1 C9_1 C8A_1 . . 119.0(5) ?
C10A_1 C9_1 C12_1 . . 122.5(4) ?
C8_1 C9_1 C12_1 . . 119.8(3) ?
C10_1 C9_1 C12_1 . . 120.2(3) ?
C8A_1 C9_1 C12_1 . . 118.5(4) ?
C11_1 C10_1 C9_1 . . 120.0 ?
C10_1 C11_1 C6_1 . . 120.0 ?
C8A_1 C7A_1 C6_1 . . 119.7(7) ?
C7A_1 C8A_1 C9_1 . . 119.4(7) ?
C9_1 C10A_1 C11A_1 . . 121.8(7) ?
C6_1 C11A_1 C10A_1 . . 121.0(7) ?
C16_1 C12_1 C13_1 . . 116.5(4) ?
C16_1 C12_1 C9_1 . . 121.9(4) ?
C13_1 C12_1 C9_1 . . 121.5(4) ?
C14_1 C13_1 C12_1 . . 119.2(4) ?
N2_1 C14_1 C13_1 . . 123.7(4) ?
N2_1 C15_1 C16_1 . . 122.1(4) ?
C15_1 C16_1 C12_1 . . 121.1(4) ?



####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_zju_b2_2_0m_b_sq
_database_code_depnum_ccdc_archive 'CCDC 2033516'
loop_
_audit_author_name
_audit_author_address
'Yue ZHAO'
;Nanjing University
China
;
_audit_update_record             
;
2020-09-23 deposited with the CCDC.	2020-12-10 downloaded from the CCDC.
;
_audit_creation_date             2020-03-26
_audit_creation_method           'Materials Studio'
_symmetry_space_group_name_H-M   P1
_symmetry_Int_Tables_number      1
_symmetry_cell_setting           triclinic
loop_
_symmetry_equiv_pos_as_xyz
x,y,z
_cell_length_a                   13.5920
_cell_length_b                   13.5920
_cell_length_c                   10.2670
_cell_angle_alpha                90.0000
_cell_angle_beta                 90.0000
_cell_angle_gamma                90.0000
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
C1 C 0.49483 0.04236 0.77494 0.08200 Uani 1.00
N2 N 0.50001 0.34944 0.78310 0.05783 Uani 1.00
C3 C 0.54780 0.29706 0.87415 0.06867 Uani 1.00
H4 H 0.58713 0.33763 0.94967 0.08200 Uiso 1.00
C5 C 0.54781 0.19540 0.87445 0.07267 Uani 1.00
H6 H 0.58584 0.15548 0.95147 0.08700 Uiso 1.00
C7 C 0.49803 0.14568 0.77459 0.07567 Uani 1.00
C8 C 0.45108 0.20081 0.67690 0.07267 Uani 1.00
H9 H 0.41392 0.16468 0.59575 0.08700 Uiso 1.00
C10 C 0.45276 0.30227 0.68600 0.06900 Uani 1.00
H11 H 0.41622 0.34812 0.61330 0.08300 Uiso 1.00
H12 H 0.51694 0.49829 0.00271 0.08900 Uiso 1.00
B13 B 0.43720 0.56682 0.21317 0.07367 Uani 1.00
H14 H 0.38597 0.62893 0.16443 0.08800 Uiso 1.00
B15 B 0.39898 0.44769 0.19622 0.07400 Uani 1.00
H16 H 0.31775 0.42907 0.15707 0.08800 Uiso 1.00
B17 B 0.49387 0.36918 0.19311 0.07400 Uani 1.00
H18 H 0.49574 0.28764 0.14885 0.08800 Uiso 1.00
B19 B 0.48174 0.61408 0.36208 0.07300 Uani 1.00
H20 H 0.44298 0.68961 0.39571 0.08800 Uiso 1.00
C21 C 0.49223 0.95318 0.78163 0.08200 Uani 1.00
N22 N 0.49966 0.64682 0.79834 0.05783 Uani 1.00
C23 C 0.45185 0.69734 0.89142 0.06867 Uani 1.00
H24 H 0.41750 0.65461 0.96930 0.08200 Uiso 1.00
C25 C 0.44795 0.79902 0.89050 0.07267 Uani 1.00
H26 H 0.41095 0.83865 0.96858 0.08700 Uiso 1.00
C27 C 0.49318 0.84996 0.78752 0.07567 Uani 1.00
C28 C 0.54153 0.79626 0.68996 0.07267 Uani 1.00
H29 H 0.57673 0.83287 0.60778 0.08700 Uiso 1.00
C30 C 0.54429 0.69513 0.70051 0.06900 Uani 1.00
H31 H 0.58253 0.65098 0.62758 0.08300 Uiso 1.00
B32 B 0.41488 0.49901 0.36022 0.07300 Uani 1.00
H33 H 0.33945 0.48708 0.41916 0.08800 Uiso 1.00
B34 B 0.63264 0.48552 0.36208 0.07400 Uani 1.00
H35 H 0.71322 0.46167 0.39737 0.08900 Uiso 1.00
B36 B 0.52134 0.50833 0.45611 0.07133 Uani 1.00
I37 I 0.73670 0.35622 0.13691 0.08700 Uiso 1.00
C38 C 0.95760 0.50019 0.76975 0.08200 Uani 1.00
N39 N 0.65080 0.49978 0.77750 0.05783 Uani 1.00
C40 C 0.70188 0.54820 0.86958 0.06867 Uani 1.00
H41 H 0.65918 0.58517 0.94515 0.08200 Uiso 1.00
C42 C 0.80349 0.54987 0.87096 0.07267 Uani 1.00
H43 H 0.84315 0.58733 0.94866 0.08700 Uiso 1.00
C44 C 0.85430 0.50039 0.77176 0.07567 Uani 1.00
C45 C 0.80063 0.44977 0.67619 0.07267 Uani 1.00
H46 H 0.83754 0.41109 0.59707 0.08700 Uiso 1.00
C47 C 0.69917 0.45037 0.68386 0.06900 Uani 1.00
H48 H 0.65456 0.41206 0.61173 0.08300 Uiso 1.00
B49 B 0.50907 0.48614 0.11937 0.07400 Uani 1.00
B50 B 0.60030 0.60037 0.39789 0.07333 Uani 1.00
H51 H 0.65488 0.65740 0.44923 0.08800 Uiso 1.00
C52 C 0.04692 0.49941 0.76950 0.08200 Uani 1.00
N53 N 0.35337 0.49971 0.77911 0.05783 Uani 1.00
C54 C 0.30227 0.45184 0.87161 0.06867 Uani 1.00
H55 H 0.34469 0.41487 0.94755 0.08200 Uiso 1.00
C56 C 0.20067 0.45065 0.87262 0.07267 Uani 1.00
H57 H 0.16078 0.41308 0.95008 0.08700 Uiso 1.00
C58 C 0.15019 0.49882 0.77171 0.07567 Uani 1.00
C59 C 0.20432 0.54686 0.67404 0.07267 Uani 1.00
H60 H 0.16739 0.58365 0.59321 0.08700 Uiso 1.00
C61 C 0.30581 0.54685 0.68272 0.06900 Uani 1.00
H62 H 0.35118 0.58409 0.61010 0.08300 Uiso 1.00
B63 B 0.60023 0.42989 0.21505 0.07300 Uani 1.00
B64 B 0.52634 0.40068 0.35974 0.07300 Uani 1.00
H65 H 0.52752 0.32552 0.42114 0.08800 Uiso 1.00
B66 B 0.57711 0.57158 0.22919 0.07367 Uani 1.00
H67 H 0.62566 0.62622 0.16309 0.08800 Uiso 1.00
H68 H 0.51102 0.49731 0.57275 0.08600 Uiso 1.00
Cu69 Cu 0.50167 0.49841 0.78713 0.06013 Uani 1.00
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_ccdc_geom_bond_type
C1 C7 1.405 . S
C1 C21 1.215 1_545 T
N2 Cu69 2.025 . S
N2 C3 1.343 . D
N2 C10 1.348 . S
C3 C5 1.382 . S
C3 H4 1.091 . S
C5 C7 1.402 . D
C5 H6 1.089 . S
C7 C8 1.405 . S
C8 C10 1.382 . D
C8 H9 1.091 . S
C10 H11 1.092 . S
H12 B49 1.214 . S
B13 H14 1.203 . S
B15 H16 1.202 . S
B17 H18 1.198 . S
B19 H20 1.205 . S
C21 C27 1.404 . S
C21 C1 1.215 1_565 T
N22 Cu69 2.021 . S
N22 C23 1.344 . S
N22 C30 1.345 . D
C23 C25 1.383 . D
C23 H24 1.093 . S
C25 C27 1.405 . S
C25 H26 1.089 . S
C27 C28 1.403 . D
C28 C30 1.379 . S
C28 H29 1.090 . S
C30 H31 1.091 . S
B32 H33 1.201 . S
B34 H35 1.198 . S
B36 H68 1.215 . S
I37 B63 2.255 . S
C38 C44 1.404 . S
C38 C52 1.214 1_655 T
N39 Cu69 2.029 . S
N39 C40 1.345 . D
N39 C47 1.345 . S
C40 C42 1.381 . S
C40 H41 1.092 . S
C42 C44 1.402 . D
C42 H43 1.089 . S
C44 C45 1.403 . S
C45 C47 1.381 . D
C45 H46 1.090 . S
C47 H48 1.090 . S
B50 H51 1.195 . S
C52 C58 1.404 . S
C52 C38 1.214 1_455 T
N53 Cu69 2.017 . S
N53 C54 1.345 . S
N53 C61 1.345 . D
C54 C56 1.381 . D
C54 H55 1.092 . S
C56 C58 1.405 . S
C56 H57 1.090 . S
C58 C59 1.405 . D
C59 C61 1.382 . S
C59 H60 1.091 . S
C61 H62 1.092 . S
B64 H65 1.201 . S
B66 H67 1.203 . S
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_1121ZJU1
_database_code_depnum_ccdc_archive 'CCDC 2033518'
loop_
_audit_author_name
_audit_author_address
'Yue ZHAO'
;Nanjing University
China
;
_audit_update_record             
;
2020-09-23 deposited with the CCDC.	2020-12-10 downloaded from the CCDC.
;
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C48 H40 B12 Cl12 Cu N6 Na0 O2'
_chemical_formula_iupac          ?
_chemical_formula_weight         1351.52
_chemical_absolute_configuration ?

_chemical_melting_point          ?

_space_group_crystal_system      monoclinic
_space_group_name_H-M_alt        'C 1 c 1'
_space_group_name_Hall           'C -2yc'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'x, -y, z+1/2'
'x+1/2, y+1/2, z'
'x+1/2, -y+1/2, z+1/2'

_cell_length_a                   18.7071(12)
_cell_length_b                   24.2785(14)
_cell_length_c                   15.2180(9)
_cell_angle_alpha                90
_cell_angle_beta                 96.297(2)
_cell_angle_gamma                90
_cell_volume                     6870.0(7)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    7225
_cell_measurement_theta_min      2.6931
_cell_measurement_theta_max      23.3072
_cell_measurement_temperature    296.(2)

_exptl_crystal_description       block
_exptl_crystal_colour            ?
_exptl_crystal_size_max          0.200
_exptl_crystal_size_mid          0.200
_exptl_crystal_size_min          0.100
_exptl_crystal_density_diffrn    1.307
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             2716

_exptl_absorpt_coefficient_mu    0.824
_exptl_absorpt_correction_type   Multi-Scan
_exptl_absorpt_process_details   
'TWINABS - Bruker AXS scaling for twinned crystals - Version 2012/1'
_exptl_absorpt_correction_T_min  0.72
_exptl_absorpt_correction_T_max  0.92

_exptl_special_details           
;
;

_diffrn_ambient_temperature      296.(2)

_diffrn_source                   TXS
_diffrn_source_type              'Rotaing Anode'

_diffrn_radiation_type           ' Mo K\a'
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_monochromator  'Helios Multi-layer Optic'

_diffrn_measurement_device_type  'Bruker D8 VENTURE PHOTON 100'
_diffrn_measurement_method       ?

_diffrn_detector_area_resol_mean 10.4167

_diffrn_reflns_number            6331
_diffrn_reflns_av_R_equivalents  ?
_diffrn_reflns_av_unetI/netI     0.0958
_diffrn_reflns_theta_min         2.01
_diffrn_reflns_theta_max         25.41
_diffrn_reflns_theta_full        25.41
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measured_fraction_theta_full 0.999
_diffrn_reflns_limit_h_min       -22
_diffrn_reflns_limit_h_max       22
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_k_max       29
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_limit_l_max       18

_refine_special_details          
;

Refined as a 2-component twin.
;

_reflns_number_total             6331
_reflns_number_gt                4366
_reflns_threshold_expression     'I > 2σ(I)'

_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_R_factor_all          0.1103
_refine_ls_R_factor_gt           0.0671
_refine_ls_wR_factor_gt          0.1496
_refine_ls_wR_factor_ref         0.1713
_refine_ls_goodness_of_fit_ref   1.060
_refine_ls_restrained_S_all      1.036
_refine_ls_number_reflns         6331
_refine_ls_number_parameters     731
_refine_ls_number_restraints     383
_refine_ls_number_constraints    ?
_refine_ls_hydrogen_treatment    constr
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.1000P)²] where P=(Fo²+2Fc²)/3'

_atom_sites_solution_hydrogens   mixed
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?

_refine_ls_shift/su_max          0.039
_refine_ls_shift/su_mean         0.002
_refine_diff_density_max         0.561
_refine_diff_density_min         -0.516
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       ?
_refine_ls_abs_structure_details 
;

No quotients, so Flack parameter determined by classical intensity fit
;
_refine_ls_abs_structure_Flack   0.05(2)

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_computing_data_collection       ?
_computing_cell_refinement       'SAINT V8.38A (Bruker AXS Inc., 2017)'
_computing_data_reduction        'SAINT V8.38A (Bruker AXS Inc., 2017)'
_computing_structure_solution    'SHELXT 2014/5 (Sheldrick, 2014)'
_computing_structure_refinement  'SHELXL-2018/3 (Sheldrick, 2018)'
_computing_molecular_graphics    'shelXle (C.B. Huebschle, rev 924)'
_computing_publication_material  ?

loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_refinement_flags_posn
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
O O1_4 0.2383(9) 0.4778(5) 0.1576(14) 0.096(5) Uani d . . D 1 . .
H H1_4 0.276708 0.469542 0.202722 0.145 Uiso d U . DR 1 . .
H H2_4 0.252712 0.460943 0.105331 0.145 Uiso d U . DR 1 . .
C C1_1 0.4875(12) 0.4922(9) 0.8801(16) 0.090(5) Uani d U . D 1 . .
H H1_1 0.462782 0.458928 0.875249 0.108 Uiso calc U . R 1 . .
C C2_1 0.5621(11) 0.4909(8) 0.8803(15) 0.080(5) Uani d U . D 1 . .
H H2_1 0.585212 0.458124 0.868855 0.096 Uiso calc U . R 1 . .
C C3_1 0.6011(11) 0.5383(7) 0.8976(14) 0.075(4) Uani d U . D 1 . .
C C4_1 0.5639(13) 0.5868(8) 0.9114(18) 0.090(5) Uani d U . D 1 . .
H H4_1 0.58731 0.619751 0.926584 0.108 Uiso calc U . R 1 . .
C C5_1 0.4892(13) 0.5823(9) 0.9010(17) 0.093(5) Uani d U . D 1 . .
H H5_1 0.463799 0.614985 0.904774 0.112 Uiso calc U . R 1 . .
C C6_1 0.6813(11) 0.5362(7) 0.9052(13) 0.070(4) Uani d U . D 1 . .
C C7_1 0.7179(11) 0.4935(7) 0.8675(13) 0.065(4) Uani d U . D 1 . .
H H7_1 0.691765 0.465125 0.838141 0.078 Uiso calc U . R 1 . .
C C8_1 0.7912(11) 0.4927(8) 0.8731(12) 0.067(4) Uani d U . D 1 . .
H H8_1 0.814276 0.464539 0.8458 0.08 Uiso calc U . R 1 . .
C C9_1 0.8320(11) 0.5337(8) 0.9193(12) 0.067(4) Uani d U . D 1 . .
C C10_1 0.7968(12) 0.5764(8) 0.9553(13) 0.075(4) Uani d U . D 1 . .
H H10_1 0.82317 0.604763 0.98435 0.09 Uiso calc U . R 1 . .
C C11_1 0.7234(12) 0.5775(8) 0.9488(14) 0.074(4) Uani d U . D 1 . .
H H11_1 0.70079 0.606583 0.974263 0.088 Uiso calc U . R 1 . .
C C12_1 0.9136(11) 0.5302(8) 0.9233(14) 0.072(4) Uani d U . D 1 . .
C C13_1 0.9510(12) 0.4816(9) 0.9332(14) 0.083(5) Uani d U . D 1 . .
H H13_1 0.926808 0.448293 0.93589 0.1 Uiso calc U . R 1 . .
C C14_1 1.0257(13) 0.4828(10) 0.9390(16) 0.092(5) Uani d U . D 1 . .
H H14_1 1.050186 0.449544 0.947214 0.111 Uiso calc U . R 1 . .
C C15_1 1.0272(13) 0.5753(9) 0.9240(16) 0.090(5) Uani d U . D 1 . .
H H15_1 1.052646 0.607876 0.919725 0.108 Uiso calc U . R 1 . .
C C16_1 0.9534(13) 0.5784(9) 0.9199(14) 0.084(5) Uani d U . D 1 . .
H H16_1 0.930397 0.612364 0.914934 0.101 Uiso calc U . R 1 . .
N N1_1 0.4499(11) 0.5373(8) 0.8863(14) 0.092(5) Uani d U . D 1 . .
N N2_1 1.0645(12) 0.5282(9) 0.9337(14) 0.095(5) Uani d U . D 1 . .
C C1_2 0.1824(8) 0.3620(6) 0.7200(11) 0.036(4) Uani d . . . 1 . .
H H1_2 0.227115 0.362183 0.753414 0.043 Uiso calc U . R 1 . .
C C2_2 0.1390(9) 0.4062(7) 0.7232(14) 0.049(5) Uani d . . . 1 . .
H H2_2 0.154726 0.436245 0.758121 0.059 Uiso calc U . R 1 . .
C C3_2 0.0703(9) 0.4077(7) 0.6747(12) 0.043(5) Uani d . . . 1 . .
C C4_2 0.0507(9) 0.3599(6) 0.6267(11) 0.037(4) Uani d . . . 1 . .
H H4_2 0.004906 0.356769 0.596561 0.044 Uiso calc U . R 1 . .
C C5_2 0.0985(9) 0.3183(7) 0.6240(11) 0.038(4) Uani d . . . 1 . .
H H5_2 0.085351 0.288269 0.587869 0.046 Uiso calc U . R 1 . .
C C6_2 0.0242(9) 0.4565(7) 0.6748(13) 0.045(5) Uani d . . . 1 . .
C C7_2 0.0568(9) 0.5077(7) 0.6766(13) 0.045(5) Uani d . . . 1 . .
H H7_2 0.106711 0.510571 0.681885 0.054 Uiso calc U . R 1 . .
C C8_2 0.0136(10) 0.5556(7) 0.6704(12) 0.048(5) Uani d . . . 1 . .
H H8_2 0.035089 0.590067 0.668147 0.058 Uiso calc U . R 1 . .
C C9_2 -0.0591(10) 0.5518(6) 0.6677(10) 0.037(4) Uani d . . . 1 . .
C C10_2 -0.0913(9) 0.4994(6) 0.6665(12) 0.042(4) Uani d . . . 1 . .
H H10_2 -0.141024 0.496073 0.663104 0.051 Uiso calc U . R 1 . .
C C11_2 -0.0486(9) 0.4533(7) 0.6703(10) 0.039(4) Uani d . . . 1 . .
H H11_2 -0.070168 0.418826 0.66977 0.047 Uiso calc U . R 1 . .
C C12_2 -0.1039(9) 0.6026(6) 0.6683(11) 0.034(4) Uani d . . . 1 . .
C C13_2 -0.0941(9) 0.6470(6) 0.6093(12) 0.039(4) Uani d . . . 1 . .
H H13_2 -0.059522 0.645452 0.569896 0.047 Uiso calc U . R 1 . .
C C14_2 -0.1383(7) 0.6923(7) 0.6130(10) 0.030(4) Uani d . . . 1 . .
H H14_2 -0.131913 0.721557 0.57516 0.036 Uiso calc U . R 1 . .
C C15_2 -0.1570(8) 0.6076(6) 0.7225(11) 0.036(4) Uani d . . . 1 . .
H H15_2 -0.167077 0.578203 0.758484 0.043 Uiso calc U . R 1 . .
C C16_2 -0.1956(9) 0.6553(6) 0.7245(12) 0.040(4) Uani d . . . 1 . .
H H16_2 -0.227518 0.659382 0.766704 0.048 Uiso calc U . R 1 . .
N N1_2 0.1632(6) 0.3177(5) 0.6702(9) 0.033(3) Uani d . . . 1 . .
N N2_2 -0.1884(7) 0.6970(5) 0.6661(8) 0.028(3) Uani d . . . 1 . .
C C1_3 0.1121(8) 0.1888(6) 0.6949(11) 0.040(3) Uani d U . D 1 . .
H H1_3 0.104509 0.216028 0.735884 0.048 Uiso calc U . R 1 . .
C C2_3 0.0684(9) 0.1422(6) 0.6928(12) 0.042(3) Uani d U . D 1 . .
H H2_3 0.03174 0.139369 0.729202 0.05 Uiso calc U . R 1 . .
C C3_3 0.0811(9) 0.1003(6) 0.6351(12) 0.041(3) Uani d U . D 1 . .
C C4_3 0.1326(8) 0.1074(6) 0.5775(11) 0.036(3) Uani d U . D 1 . .
H H4_3 0.140721 0.081017 0.535412 0.044 Uiso calc U . R 1 . .
C C5_3 0.1714(8) 0.1561(6) 0.5861(11) 0.038(3) Uani d U . D 1 . .
H H5_3 0.206796 0.160721 0.548346 0.046 Uiso calc U . R 1 . .
C C6_3 0.0378(8) 0.0486(6) 0.6371(14) 0.048(3) Uani d U . D 1 . .
C C7_3 -0.0368(9) 0.0529(7) 0.6366(16) 0.058(4) Uani d U . D 1 . .
H H7_3 -0.057843 0.087503 0.638526 0.069 Uiso calc U . R 1 . .
C C8_3 -0.0793(9) 0.0071(7) 0.6332(15) 0.055(4) Uani d U . D 1 . .
H H8_3 -0.128939 0.010399 0.631285 0.066 Uiso calc U . R 1 . .
C C9_3 -0.0471(8) -0.0450(6) 0.6328(14) 0.049(3) Uani d U . D 1 . .
C C10_3 0.0259(8) -0.0496(6) 0.6347(14) 0.046(4) Uani d U . D 1 . .
H H10_3 0.047228 -0.084282 0.636309 0.055 Uiso calc U . R 1 . .
C C11_3 0.0677(8) -0.0035(6) 0.6341(12) 0.044(4) Uani d U . D 1 . .
H H11_3 0.116932 -0.007116 0.631551 0.053 Uiso calc U . R 1 . .
C C12_3 -0.0956(8) -0.0950(6) 0.6318(13) 0.042(3) Uani d U . D 1 . .
C C13_3 -0.0761(9) -0.1390(6) 0.6873(12) 0.043(4) Uani d U . D 1 . .
H H13_3 -0.032284 -0.139207 0.722673 0.052 Uiso calc U . R 1 . .
C C14_3 -0.1240(9) -0.1830(6) 0.6888(13) 0.043(4) Uani d U . D 1 . .
H H14_3 -0.109829 -0.213236 0.724068 0.051 Uiso calc U . R 1 . .
C C15_3 -0.2035(9) -0.1424(6) 0.5842(12) 0.041(4) Uani d U . D 1 . .
H H15_3 -0.245813 -0.144167 0.545957 0.049 Uiso calc U . R 1 . .
C C16_3 -0.1592(8) -0.0977(6) 0.5790(13) 0.046(4) Uani d U . D 1 . .
H H16_3 -0.172597 -0.069322 0.539571 0.055 Uiso calc U . R 1 . .
N N1_3 0.1634(7) 0.1976(5) 0.6433(9) 0.035(3) Uani d U . D 1 . .
N N2_3 -0.1882(7) -0.1844(5) 0.6432(9) 0.042(3) Uani d U . D 1 . .
O O1 0.2457(6) 0.2545(4) 0.8089(7) 0.032(2) Uani d . . . 1 . .
H H2 0.201363 0.243529 0.834139 0.048 Uiso d U . R 1 . .
H H1 0.294062 0.265829 0.846139 0.048 Uiso d U . R 1 . .
Cu Cu1 0.23798(12) 0.25774(6) 0.66182(14) 0.0330(4) Uani d . . . 1 . .
B B1 0.2576(10) 0.2013(8) 0.3183(13) 0.036(5) Uani d . . . 1 . .
B B2 0.2244(12) 0.1815(8) 0.2071(13) 0.040(5) Uani d . . . 1 . .
B B3 0.3024(11) 0.2249(8) 0.2285(15) 0.043(5) Uani d . . . 1 . .
B B4 0.2348(13) 0.2375(8) 0.1376(13) 0.045(5) Uani d . . . 1 . .
B B5 0.1478(11) 0.2232(7) 0.1700(14) 0.037(5) Uani d . . . 1 . .
B B6 0.1810(13) 0.2917(7) 0.1687(15) 0.046(6) Uani d . . . 1 . .
B B7 0.1338(12) 0.2699(7) 0.2557(15) 0.042(5) Uani d . . . 1 . .
B B8 0.2098(13) 0.3137(8) 0.2736(16) 0.050(6) Uani d . . . 1 . .
B B9 0.1979(13) 0.2573(7) 0.3454(14) 0.041(5) Uani d . . . 1 . .
B B10 0.2855(11) 0.2711(9) 0.3140(14) 0.043(5) Uani d . . . 1 . .
B B11 0.1600(11) 0.2008(8) 0.2809(13) 0.034(5) Uani d . . . 1 . .
B B12 0.2745(14) 0.2934(9) 0.2029(19) 0.059(7) Uani d . . . 1 . .
Cl Cl1 0.2942(2) 0.15457(18) 0.3991(3) 0.0472(11) Uani d . . . 1 . .
Cl Cl2 0.3901(3) 0.2008(2) 0.2115(3) 0.0570(14) Uani d . . . 1 . .
Cl Cl3 0.1032(3) 0.15195(19) 0.3248(3) 0.0504(12) Uani d . . . 1 . .
Cl Cl4 0.2330(3) 0.11069(15) 0.1735(3) 0.0522(11) Uani d . . . 1 . .
Cl Cl5 0.2556(3) 0.2264(2) 0.0251(3) 0.0555(14) Uani d . . . 1 . .
Cl Cl6 0.0790(3) 0.1978(2) 0.0896(3) 0.0528(13) Uani d . . . 1 . .
Cl Cl7 0.1422(3) 0.34102(19) 0.0849(4) 0.0598(14) Uani d . . . 1 . .
Cl Cl8 0.0449(3) 0.2929(2) 0.2672(4) 0.0587(13) Uani d . . . 1 . .
Cl Cl9 0.2011(3) 0.38269(18) 0.3112(4) 0.0685(16) Uani d . . . 1 . .
Cl Cl10 0.1773(2) 0.26767(19) 0.4563(3) 0.0475(12) Uani d . . . 1 . .
Cl Cl11 0.3560(3) 0.2963(2) 0.3929(4) 0.0650(15) Uani d . . . 1 . .
Cl Cl12 0.3315(3) 0.3431(2) 0.1604(4) 0.0659(15) Uani d . . . 1 . .


_geom_special_details            
;

All esds (except the esd in the dihedral angle between two l.s. planes)
are estimated using the full covariance matrix.  The cell esds are taken
into account individually in the estimation of esds in distances, angles
and torsion angles; correlations between esds in cell parameters are only
used when they are defined by crystal symmetry.  An approximate (isotropic)
treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
O1_4 H1_4 . 0.9585 ?
O1_4 H2_4 . 0.9586 ?
C1_1 N1_1 . 1.31(2) ?
C1_1 C2_1 . 1.40(2) ?
C1_1 H1_1 . 0.93 ?
C2_1 C3_1 . 1.37(2) ?
C2_1 H2_1 . 0.93 ?
C3_1 C4_1 . 1.40(2) ?
C3_1 C6_1 . 1.49(2) ?
C4_1 C5_1 . 1.39(3) ?
C4_1 H4_1 . 0.93 ?
C5_1 N1_1 . 1.32(2) ?
C5_1 H5_1 . 0.93 ?
C6_1 C11_1 . 1.40(2) ?
C6_1 C7_1 . 1.40(2) ?
C7_1 C8_1 . 1.37(2) ?
C7_1 H7_1 . 0.93 ?
C8_1 C9_1 . 1.40(2) ?
C8_1 H8_1 . 0.93 ?
C9_1 C10_1 . 1.37(2) ?
C9_1 C12_1 . 1.52(2) ?
C10_1 C11_1 . 1.37(2) ?
C10_1 H10_1 . 0.93 ?
C11_1 H11_1 . 0.93 ?
C12_1 C13_1 . 1.37(2) ?
C12_1 C16_1 . 1.39(2) ?
C13_1 C14_1 . 1.39(2) ?
C13_1 H13_1 . 0.93 ?
C14_1 N2_1 . 1.33(2) ?
C14_1 H14_1 . 0.93 ?
C15_1 N2_1 . 1.34(2) ?
C15_1 C16_1 . 1.38(2) ?
C15_1 H15_1 . 0.93 ?
C16_1 H16_1 . 0.93 ?
C1_2 N1_2 . 1.340(19) ?
C1_2 C2_2 . 1.35(2) ?
C1_2 H1_2 . 0.93 ?
C2_2 C3_2 . 1.41(2) ?
C2_2 H2_2 . 0.93 ?
C3_2 C4_2 . 1.40(2) ?
C3_2 C6_2 . 1.47(2) ?
C4_2 C5_2 . 1.35(2) ?
C4_2 H4_2 . 0.93 ?
C5_2 N1_2 . 1.332(19) ?
C5_2 H5_2 . 0.93 ?
C6_2 C11_2 . 1.36(2) ?
C6_2 C7_2 . 1.38(2) ?
C7_2 C8_2 . 1.41(2) ?
C7_2 H7_2 . 0.93 ?
C8_2 C9_2 . 1.36(2) ?
C8_2 H8_2 . 0.93 ?
C9_2 C10_2 . 1.41(2) ?
C9_2 C12_2 . 1.49(2) ?
C10_2 C11_2 . 1.37(2) ?
C10_2 H10_2 . 0.93 ?
C11_2 H11_2 . 0.93 ?
C12_2 C15_2 . 1.36(2) ?
C12_2 C13_2 . 1.43(2) ?
C13_2 C14_2 . 1.38(2) ?
C13_2 H13_2 . 0.93 ?
C14_2 N2_2 . 1.308(18) ?
C14_2 H14_2 . 0.93 ?
C15_2 C16_2 . 1.37(2) ?
C15_2 H15_2 . 0.93 ?
C16_2 N2_2 . 1.36(2) ?
C16_2 H16_2 . 0.93 ?
N1_2 Cu1 . 2.032(12) ?
N2_2 Cu1 3_455 2.014(12) ?
C1_3 N1_3 . 1.322(18) ?
C1_3 C2_3 . 1.40(2) ?
C1_3 H1_3 . 0.93 ?
C2_3 C3_3 . 1.38(2) ?
C2_3 H2_3 . 0.93 ?
C3_3 C4_3 . 1.38(2) ?
C3_3 C6_3 . 1.50(2) ?
C4_3 C5_3 . 1.387(19) ?
C4_3 H4_3 . 0.93 ?
C5_3 N1_3 . 1.349(18) ?
C5_3 H5_3 . 0.93 ?
C6_3 C11_3 . 1.39(2) ?
C6_3 C7_3 . 1.40(2) ?
C7_3 C8_3 . 1.36(2) ?
C7_3 H7_3 . 0.93 ?
C8_3 C9_3 . 1.40(2) ?
C8_3 H8_3 . 0.93 ?
C9_3 C10_3 . 1.37(2) ?
C9_3 C12_3 . 1.52(2) ?
C10_3 C11_3 . 1.366(19) ?
C10_3 H10_3 . 0.93 ?
C11_3 H11_3 . 0.93 ?
C12_3 C16_3 . 1.36(2) ?
C12_3 C13_3 . 1.39(2) ?
C13_3 C14_3 . 1.40(2) ?
C13_3 H13_3 . 0.93 ?
C14_3 N2_3 . 1.319(19) ?
C14_3 H14_3 . 0.93 ?
C15_3 N2_3 . 1.369(19) ?
C15_3 C16_3 . 1.37(2) ?
C15_3 H15_3 . 0.93 ?
C16_3 H16_3 . 0.93 ?
N1_3 Cu1 . 2.018(12) ?
N2_3 Cu1 3_445 2.011(14) ?
O1 Cu1 . 2.229(10) ?
O1 H2 . 0.9876 ?
O1 H1 . 1.0502 ?
B1 Cl1 . 1.76(2) ?
B1 B3 . 1.78(3) ?
B1 B10 . 1.78(3) ?
B1 B2 . 1.80(3) ?
B1 B9 . 1.83(3) ?
B1 B11 . 1.85(3) ?
B2 B4 . 1.75(3) ?
B2 B5 . 1.80(3) ?
B2 B11 . 1.80(3) ?
B2 B3 . 1.80(3) ?
B2 Cl4 . 1.805(19) ?
B3 B10 . 1.77(3) ?
B3 B12 . 1.77(3) ?
B3 Cl2 . 1.79(2) ?
B3 B4 . 1.80(3) ?
B4 B6 . 1.75(3) ?
B4 B5 . 1.79(3) ?
B4 B12 . 1.79(3) ?
B4 Cl5 . 1.82(2) ?
B5 B11 . 1.76(3) ?
B5 B7 . 1.77(3) ?
B5 B6 . 1.78(3) ?
B5 Cl6 . 1.79(2) ?
B6 B8 . 1.71(3) ?
B6 B7 . 1.75(3) ?
B6 B12 . 1.77(3) ?
B6 Cl7 . 1.84(2) ?
B7 B9 . 1.74(3) ?
B7 B8 . 1.77(3) ?
B7 B11 . 1.78(3) ?
B7 Cl8 . 1.78(2) ?
B8 B12 . 1.77(3) ?
B8 B9 . 1.78(3) ?
B8 Cl9 . 1.78(2) ?
B8 B10 . 1.81(3) ?
B9 B11 . 1.79(2) ?
B9 B10 . 1.79(3) ?
B9 Cl10 . 1.789(19) ?
B10 B12 . 1.77(3) ?
B10 Cl11 . 1.79(2) ?
B11 Cl3 . 1.770(19) ?
B12 Cl12 . 1.78(2) ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
H1_4 O1_4 H2_4 . . 104.4 ?
N1_1 C1_1 C2_1 . . 124.(2) ?
N1_1 C1_1 H1_1 . . 117.8 ?
C2_1 C1_1 H1_1 . . 117.8 ?
C3_1 C2_1 C1_1 . . 119.4(19) ?
C3_1 C2_1 H2_1 . . 120.3 ?
C1_1 C2_1 H2_1 . . 120.3 ?
C2_1 C3_1 C4_1 . . 118.2(19) ?
C2_1 C3_1 C6_1 . . 119.7(16) ?
C4_1 C3_1 C6_1 . . 122.0(18) ?
C5_1 C4_1 C3_1 . . 115.(2) ?
C5_1 C4_1 H4_1 . . 122.3 ?
C3_1 C4_1 H4_1 . . 122.3 ?
N1_1 C5_1 C4_1 . . 128.(2) ?
N1_1 C5_1 H5_1 . . 116.0 ?
C4_1 C5_1 H5_1 . . 116.0 ?
C11_1 C6_1 C7_1 . . 116.8(18) ?
C11_1 C6_1 C3_1 . . 121.5(16) ?
C7_1 C6_1 C3_1 . . 121.7(17) ?
C8_1 C7_1 C6_1 . . 121.2(18) ?
C8_1 C7_1 H7_1 . . 119.4 ?
C6_1 C7_1 H7_1 . . 119.4 ?
C7_1 C8_1 C9_1 . . 120.7(18) ?
C7_1 C8_1 H8_1 . . 119.6 ?
C9_1 C8_1 H8_1 . . 119.6 ?
C10_1 C9_1 C8_1 . . 118.6(19) ?
C10_1 C9_1 C12_1 . . 123.2(18) ?
C8_1 C9_1 C12_1 . . 118.1(17) ?
C11_1 C10_1 C9_1 . . 120.(2) ?
C11_1 C10_1 H10_1 . . 119.8 ?
C9_1 C10_1 H10_1 . . 119.8 ?
C10_1 C11_1 C6_1 . . 122.1(19) ?
C10_1 C11_1 H11_1 . . 119.0 ?
C6_1 C11_1 H11_1 . . 119.0 ?
C13_1 C12_1 C16_1 . . 117.(2) ?
C13_1 C12_1 C9_1 . . 123.3(18) ?
C16_1 C12_1 C9_1 . . 119.3(18) ?
C12_1 C13_1 C14_1 . . 119.(2) ?
C12_1 C13_1 H13_1 . . 120.5 ?
C14_1 C13_1 H13_1 . . 120.5 ?
N2_1 C14_1 C13_1 . . 124.(2) ?
N2_1 C14_1 H14_1 . . 117.8 ?
C13_1 C14_1 H14_1 . . 117.8 ?
N2_1 C15_1 C16_1 . . 124.(2) ?
N2_1 C15_1 H15_1 . . 118.0 ?
C16_1 C15_1 H15_1 . . 118.0 ?
C15_1 C16_1 C12_1 . . 119.(2) ?
C15_1 C16_1 H16_1 . . 120.3 ?
C12_1 C16_1 H16_1 . . 120.3 ?
C1_1 N1_1 C5_1 . . 114.(2) ?
C14_1 N2_1 C15_1 . . 116.(2) ?
N1_2 C1_2 C2_2 . . 122.3(15) ?
N1_2 C1_2 H1_2 . . 118.9 ?
C2_2 C1_2 H1_2 . . 118.9 ?
C1_2 C2_2 C3_2 . . 121.2(17) ?
C1_2 C2_2 H2_2 . . 119.4 ?
C3_2 C2_2 H2_2 . . 119.4 ?
C4_2 C3_2 C2_2 . . 115.0(15) ?
C4_2 C3_2 C6_2 . . 123.4(16) ?
C2_2 C3_2 C6_2 . . 121.5(16) ?
C5_2 C4_2 C3_2 . . 120.0(15) ?
C5_2 C4_2 H4_2 . . 120.0 ?
C3_2 C4_2 H4_2 . . 120.0 ?
N1_2 C5_2 C4_2 . . 123.9(16) ?
N1_2 C5_2 H5_2 . . 118.1 ?
C4_2 C5_2 H5_2 . . 118.1 ?
C11_2 C6_2 C7_2 . . 119.4(16) ?
C11_2 C6_2 C3_2 . . 122.8(16) ?
C7_2 C6_2 C3_2 . . 117.8(16) ?
C6_2 C7_2 C8_2 . . 119.3(16) ?
C6_2 C7_2 H7_2 . . 120.4 ?
C8_2 C7_2 H7_2 . . 120.4 ?
C9_2 C8_2 C7_2 . . 120.6(17) ?
C9_2 C8_2 H8_2 . . 119.7 ?
C7_2 C8_2 H8_2 . . 119.7 ?
C8_2 C9_2 C10_2 . . 119.3(15) ?
C8_2 C9_2 C12_2 . . 120.2(15) ?
C10_2 C9_2 C12_2 . . 120.5(15) ?
C11_2 C10_2 C9_2 . . 119.3(16) ?
C11_2 C10_2 H10_2 . . 120.3 ?
C9_2 C10_2 H10_2 . . 120.3 ?
C6_2 C11_2 C10_2 . . 122.1(16) ?
C6_2 C11_2 H11_2 . . 118.9 ?
C10_2 C11_2 H11_2 . . 118.9 ?
C15_2 C12_2 C13_2 . . 117.8(14) ?
C15_2 C12_2 C9_2 . . 121.6(14) ?
C13_2 C12_2 C9_2 . . 120.6(14) ?
C14_2 C13_2 C12_2 . . 117.2(16) ?
C14_2 C13_2 H13_2 . . 121.4 ?
C12_2 C13_2 H13_2 . . 121.4 ?
N2_2 C14_2 C13_2 . . 124.5(15) ?
N2_2 C14_2 H14_2 . . 117.7 ?
C13_2 C14_2 H14_2 . . 117.7 ?
C12_2 C15_2 C16_2 . . 120.6(15) ?
C12_2 C15_2 H15_2 . . 119.7 ?
C16_2 C15_2 H15_2 . . 119.7 ?
N2_2 C16_2 C15_2 . . 121.7(16) ?
N2_2 C16_2 H16_2 . . 119.1 ?
C15_2 C16_2 H16_2 . . 119.1 ?
C5_2 N1_2 C1_2 . . 117.5(13) ?
C5_2 N1_2 Cu1 . . 124.5(11) ?
C1_2 N1_2 Cu1 . . 117.8(10) ?
C14_2 N2_2 C16_2 . . 117.8(13) ?
C14_2 N2_2 Cu1 . 3_455 125.3(11) ?
C16_2 N2_2 Cu1 . 3_455 116.7(10) ?
N1_3 C1_3 C2_3 . . 125.4(15) ?
N1_3 C1_3 H1_3 . . 117.3 ?
C2_3 C1_3 H1_3 . . 117.3 ?
C3_3 C2_3 C1_3 . . 118.1(15) ?
C3_3 C2_3 H2_3 . . 121.0 ?
C1_3 C2_3 H2_3 . . 121.0 ?
C2_3 C3_3 C4_3 . . 119.4(14) ?
C2_3 C3_3 C6_3 . . 118.3(15) ?
C4_3 C3_3 C6_3 . . 122.3(14) ?
C3_3 C4_3 C5_3 . . 116.2(14) ?
C3_3 C4_3 H4_3 . . 121.9 ?
C5_3 C4_3 H4_3 . . 121.9 ?
N1_3 C5_3 C4_3 . . 127.1(15) ?
N1_3 C5_3 H5_3 . . 116.4 ?
C4_3 C5_3 H5_3 . . 116.4 ?
C11_3 C6_3 C7_3 . . 118.3(14) ?
C11_3 C6_3 C3_3 . . 123.0(14) ?
C7_3 C6_3 C3_3 . . 118.7(14) ?
C8_3 C7_3 C6_3 . . 121.1(16) ?
C8_3 C7_3 H7_3 . . 119.5 ?
C6_3 C7_3 H7_3 . . 119.5 ?
C7_3 C8_3 C9_3 . . 119.2(15) ?
C7_3 C8_3 H8_3 . . 120.4 ?
C9_3 C8_3 H8_3 . . 120.4 ?
C10_3 C9_3 C8_3 . . 120.2(14) ?
C10_3 C9_3 C12_3 . . 122.0(14) ?
C8_3 C9_3 C12_3 . . 117.8(13) ?
C11_3 C10_3 C9_3 . . 120.2(15) ?
C11_3 C10_3 H10_3 . . 119.9 ?
C9_3 C10_3 H10_3 . . 119.9 ?
C10_3 C11_3 C6_3 . . 121.0(15) ?
C10_3 C11_3 H11_3 . . 119.5 ?
C6_3 C11_3 H11_3 . . 119.5 ?
C16_3 C12_3 C13_3 . . 118.5(14) ?
C16_3 C12_3 C9_3 . . 121.8(15) ?
C13_3 C12_3 C9_3 . . 119.6(15) ?
C12_3 C13_3 C14_3 . . 118.2(15) ?
C12_3 C13_3 H13_3 . . 120.9 ?
C14_3 C13_3 H13_3 . . 120.9 ?
N2_3 C14_3 C13_3 . . 124.0(16) ?
N2_3 C14_3 H14_3 . . 118.0 ?
C13_3 C14_3 H14_3 . . 118.0 ?
N2_3 C15_3 C16_3 . . 122.9(16) ?
N2_3 C15_3 H15_3 . . 118.6 ?
C16_3 C15_3 H15_3 . . 118.6 ?
C12_3 C16_3 C15_3 . . 119.8(16) ?
C12_3 C16_3 H16_3 . . 120.1 ?
C15_3 C16_3 H16_3 . . 120.1 ?
C1_3 N1_3 C5_3 . . 113.7(13) ?
C1_3 N1_3 Cu1 . . 124.7(11) ?
C5_3 N1_3 Cu1 . . 120.4(10) ?
C14_3 N2_3 C15_3 . . 116.0(14) ?
C14_3 N2_3 Cu1 . 3_445 122.9(11) ?
C15_3 N2_3 Cu1 . 3_445 121.0(10) ?
Cu1 O1 H2 . . 115.8 ?
Cu1 O1 H1 . . 119.3 ?
H2 O1 H1 . . 124.9 ?
N2_3 Cu1 N2_2 3 3_545 92.2(5) ?
N2_3 Cu1 N1_3 3 . 163.8(6) ?
N2_2 Cu1 N1_3 3_545 . 86.2(4) ?
N2_3 Cu1 N1_2 3 . 89.8(4) ?
N2_2 Cu1 N1_2 3_545 . 174.5(6) ?
N1_3 Cu1 N1_2 . . 93.3(5) ?
N2_3 Cu1 O1 3 . 101.3(5) ?
N2_2 Cu1 O1 3_545 . 88.5(4) ?
N1_3 Cu1 O1 . . 94.7(5) ?
N1_2 Cu1 O1 . . 86.1(5) ?
Cl1 B1 B3 . . 124.5(13) ?
Cl1 B1 B10 . . 123.3(13) ?
B3 B1 B10 . . 59.9(11) ?
Cl1 B1 B2 . . 123.5(13) ?
B3 B1 B2 . . 60.4(11) ?
B10 B1 B2 . . 107.0(14) ?
Cl1 B1 B9 . . 121.5(13) ?
B3 B1 B9 . . 106.5(14) ?
B10 B1 B9 . . 59.3(11) ?
B2 B1 B9 . . 104.7(13) ?
Cl1 B1 B11 . . 120.4(13) ?
B3 B1 B11 . . 107.4(13) ?
B10 B1 B11 . . 106.2(13) ?
B2 B1 B11 . . 58.9(10) ?
B9 B1 B11 . . 58.0(10) ?
B4 B2 B5 . . 60.5(13) ?
B4 B2 B11 . . 107.6(14) ?
B5 B2 B11 . . 58.8(11) ?
B4 B2 B3 . . 60.8(12) ?
B5 B2 B3 . . 109.2(13) ?
B11 B2 B3 . . 108.7(13) ?
B4 B2 B1 . . 108.1(14) ?
B5 B2 B1 . . 109.0(13) ?
B11 B2 B1 . . 61.9(11) ?
B3 B2 B1 . . 59.0(11) ?
B4 B2 Cl4 . . 123.4(12) ?
B5 B2 Cl4 . . 122.8(14) ?
B11 B2 Cl4 . . 120.8(12) ?
B3 B2 Cl4 . . 120.9(13) ?
B1 B2 Cl4 . . 119.2(13) ?
B10 B3 B12 . . 59.7(13) ?
B10 B3 B1 . . 60.1(12) ?
B12 B3 B1 . . 108.6(15) ?
B10 B3 Cl2 . . 123.6(14) ?
B12 B3 Cl2 . . 121.9(14) ?
B1 B3 Cl2 . . 121.6(14) ?
B10 B3 B4 . . 106.9(15) ?
B12 B3 B4 . . 60.4(13) ?
B1 B3 B4 . . 107.2(14) ?
Cl2 B3 B4 . . 121.6(15) ?
B10 B3 B2 . . 107.3(14) ?
B12 B3 B2 . . 107.2(15) ?
B1 B3 B2 . . 60.5(11) ?
Cl2 B3 B2 . . 121.4(13) ?
B4 B3 B2 . . 58.1(11) ?
B2 B4 B6 . . 108.4(16) ?
B2 B4 B5 . . 61.1(12) ?
B6 B4 B5 . . 60.3(12) ?
B2 B4 B12 . . 108.6(15) ?
B6 B4 B12 . . 59.8(12) ?
B5 B4 B12 . . 109.1(16) ?
B2 B4 B3 . . 61.1(12) ?
B6 B4 B3 . . 107.2(14) ?
B5 B4 B3 . . 109.9(15) ?
B12 B4 B3 . . 59.2(12) ?
B2 B4 Cl5 . . 120.3(13) ?
B6 B4 Cl5 . . 123.7(14) ?
B5 B4 Cl5 . . 121.9(13) ?
B12 B4 Cl5 . . 121.1(15) ?
B3 B4 Cl5 . . 119.6(16) ?
B11 B5 B7 . . 60.5(12) ?
B11 B5 B6 . . 107.0(14) ?
B7 B5 B6 . . 59.2(12) ?
B11 B5 B4 . . 107.4(13) ?
B7 B5 B4 . . 107.0(14) ?
B6 B5 B4 . . 59.0(12) ?
B11 B5 Cl6 . . 123.8(13) ?
B7 B5 Cl6 . . 124.9(14) ?
B6 B5 Cl6 . . 122.8(13) ?
B4 B5 Cl6 . . 119.1(14) ?
B11 B5 B2 . . 60.7(11) ?
B7 B5 B2 . . 107.9(14) ?
B6 B5 B2 . . 105.3(14) ?
B4 B5 B2 . . 58.4(11) ?
Cl6 B5 B2 . . 120.7(12) ?
B8 B6 B7 . . 61.5(13) ?
B8 B6 B4 . . 110.7(15) ?
B7 B6 B4 . . 109.2(14) ?
B8 B6 B12 . . 61.2(13) ?
B7 B6 B12 . . 110.4(16) ?
B4 B6 B12 . . 61.3(14) ?
B8 B6 B5 . . 110.8(15) ?
B7 B6 B5 . . 60.1(11) ?
B4 B6 B5 . . 60.8(12) ?
B12 B6 B5 . . 110.7(15) ?
B8 B6 Cl7 . . 120.3(13) ?
B7 B6 Cl7 . . 121.8(16) ?
B4 B6 Cl7 . . 119.7(15) ?
B12 B6 Cl7 . . 119.4(16) ?
B5 B6 Cl7 . . 120.3(13) ?
B9 B7 B6 . . 106.5(15) ?
B9 B7 B5 . . 108.7(14) ?
B6 B7 B5 . . 60.6(12) ?
B9 B7 B8 . . 60.9(12) ?
B6 B7 B8 . . 58.1(12) ?
B5 B7 B8 . . 108.4(16) ?
B9 B7 B11 . . 61.0(11) ?
B6 B7 B11 . . 107.4(14) ?
B5 B7 B11 . . 59.7(10) ?
B8 B7 B11 . . 109.6(15) ?
B9 B7 Cl8 . . 123.2(14) ?
B6 B7 Cl8 . . 122.2(15) ?
B5 B7 Cl8 . . 119.3(14) ?
B8 B7 Cl8 . . 122.6(13) ?
B11 B7 Cl8 . . 120.8(13) ?
B6 B8 B7 . . 60.3(12) ?
B6 B8 B12 . . 61.0(14) ?
B7 B8 B12 . . 109.2(15) ?
B6 B8 B9 . . 106.6(14) ?
B7 B8 B9 . . 58.7(12) ?
B12 B8 B9 . . 107.4(15) ?
B6 B8 Cl9 . . 124.1(15) ?
B7 B8 Cl9 . . 120.8(15) ?
B12 B8 Cl9 . . 123.2(15) ?
B9 B8 Cl9 . . 120.2(15) ?
B6 B8 B10 . . 107.1(15) ?
B7 B8 B10 . . 107.2(14) ?
B12 B8 B10 . . 59.1(13) ?
B9 B8 B10 . . 59.8(12) ?
Cl9 B8 B10 . . 121.6(14) ?
B7 B9 B8 . . 60.4(12) ?
B7 B9 B11 . . 60.5(11) ?
B8 B9 B11 . . 108.8(14) ?
B7 B9 B10 . . 109.3(14) ?
B8 B9 B10 . . 60.8(12) ?
B11 B9 B10 . . 108.5(13) ?
B7 B9 Cl10 . . 120.9(15) ?
B8 B9 Cl10 . . 121.7(12) ?
B11 B9 Cl10 . . 120.8(12) ?
B10 B9 Cl10 . . 121.6(14) ?
B7 B9 B1 . . 109.7(13) ?
B8 B9 B1 . . 108.1(14) ?
B11 B9 B1 . . 61.5(10) ?
B10 B9 B1 . . 58.7(11) ?
Cl10 B9 B1 . . 121.0(14) ?
B12 B10 B3 . . 60.2(13) ?
B12 B10 B1 . . 108.9(15) ?
B3 B10 B1 . . 60.0(11) ?
B12 B10 B9 . . 107.4(15) ?
B3 B10 B9 . . 108.6(14) ?
B1 B10 B9 . . 61.9(10) ?
B12 B10 Cl11 . . 122.5(14) ?
B3 B10 Cl11 . . 122.1(13) ?
B1 B10 Cl11 . . 119.9(14) ?
B9 B10 Cl11 . . 120.9(13) ?
B12 B10 B8 . . 59.5(13) ?
B3 B10 B8 . . 107.9(15) ?
B1 B10 B8 . . 109.6(14) ?
B9 B10 B8 . . 59.4(12) ?
Cl11 B10 B8 . . 121.7(14) ?
B5 B11 Cl3 . . 123.2(13) ?
B5 B11 B7 . . 59.9(11) ?
Cl3 B11 B7 . . 123.4(14) ?
B5 B11 B9 . . 106.8(13) ?
Cl3 B11 B9 . . 121.7(13) ?
B7 B11 B9 . . 58.5(12) ?
B5 B11 B2 . . 60.5(12) ?
Cl3 B11 B2 . . 122.2(13) ?
B7 B11 B2 . . 107.4(13) ?
B9 B11 B2 . . 106.8(13) ?
B5 B11 B1 . . 108.1(14) ?
Cl3 B11 B1 . . 120.0(12) ?
B7 B11 B1 . . 107.4(13) ?
B9 B11 B1 . . 60.5(11) ?
B2 B11 B1 . . 59.2(11) ?
B10 B12 B6 . . 106.4(16) ?
B10 B12 B8 . . 61.3(14) ?
B6 B12 B8 . . 57.8(13) ?
B10 B12 B3 . . 60.1(13) ?
B6 B12 B3 . . 107.5(15) ?
B8 B12 B3 . . 109.3(17) ?
B10 B12 Cl12 . . 123.0(17) ?
B6 B12 Cl12 . . 121.4(17) ?
B8 B12 Cl12 . . 120.5(15) ?
B3 B12 Cl12 . . 122.8(16) ?
B10 B12 B4 . . 107.3(15) ?
B6 B12 B4 . . 58.9(14) ?
B8 B12 B4 . . 106.1(16) ?
B3 B12 B4 . . 60.4(12) ?
Cl12 B12 B4 . . 122.7(17) ?



####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_ZJU_Yb1_0m_sq
_database_code_depnum_ccdc_archive 'CCDC 2033520'
loop_
_audit_author_name
_audit_author_address
'Yue ZHAO'
;Nanjing University
China
;
_audit_update_record             
;
2020-09-23 deposited with the CCDC.	2020-12-10 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2018/3
_shelx_SHELXL_version_number     2018/3
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C68 H64 B24 Cl24 Cu2 N8 O4'
_chemical_formula_weight         2294.59

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      tetragonal
_space_group_IT_number           114
_space_group_name_H-M_alt        'P -4 21 c'
_space_group_name_Hall           'P -4 2n'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, z'
'y, -x, -z'
'-y, x, -z'
'-x+1/2, y+1/2, -z+1/2'
'x+1/2, -y+1/2, -z+1/2'
'-y+1/2, -x+1/2, z+1/2'
'y+1/2, x+1/2, z+1/2'

_cell_length_a                   33.475(3)
_cell_length_b                   33.475(3)
_cell_length_c                   39.463(5)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_volume                     44221(10)
_cell_formula_units_Z            16
_cell_measurement_temperature    296(2)
_cell_measurement_reflns_used    9754
_cell_measurement_theta_min      2.19
_cell_measurement_theta_max      28.23

_exptl_crystal_description       block
_exptl_crystal_colour            ?
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    1.379
_exptl_crystal_F_000             18336
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          0.200
_exptl_crystal_size_mid          0.200
_exptl_crystal_size_min          0.200
_exptl_absorpt_coefficient_mu    1.009
_shelx_estimated_absorpt_T_min   0.824
_shelx_estimated_absorpt_T_max   0.824
_exptl_absorpt_correction_type   ?
_exptl_absorpt_correction_T_min  ?
_exptl_absorpt_correction_T_max  ?
_exptl_absorpt_process_details   ?
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      296(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_source                   ?
_diffrn_measurement_device_type  'bruker d8 venture PHOTON100'
_diffrn_measurement_method       ?
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            238555
_diffrn_reflns_av_unetI/netI     0.0871
_diffrn_reflns_av_R_equivalents  0.0975
_diffrn_reflns_limit_h_min       -39
_diffrn_reflns_limit_h_max       44
_diffrn_reflns_limit_k_min       -44
_diffrn_reflns_limit_k_max       40
_diffrn_reflns_limit_l_min       -52
_diffrn_reflns_limit_l_max       41
_diffrn_reflns_theta_min         0.860
_diffrn_reflns_theta_max         28.294
_diffrn_reflns_theta_full        25.242
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measured_fraction_theta_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.997
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.996
_diffrn_reflns_point_group_measured_fraction_full 0.998
_reflns_number_total             54700
_reflns_number_gt                39976
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.907
_reflns_Friedel_fraction_max     0.994
_reflns_Friedel_fraction_full    0.998

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences. Completness statistics refer to single and
 composite reflections containing twin component 1 only.
;

_computing_data_collection       ?
_computing_cell_refinement       ?
_computing_data_reduction        ?
_computing_structure_solution    'SHELXT 2014/5 (Sheldrick, 2014)'
_computing_structure_refinement  'SHELXL-2018/3 (Sheldrick, 2018)'
_computing_molecular_graphics    ?
_computing_publication_material  ?
_refine_special_details          
;
 Refined as a 2-component twin.
;
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0832P)²+97.8601P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_abs_structure_details 
;
 Flack x determined using 15355 quotients [(I+)-(I-)]/[(I+)+(I-)]
 (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259).
;
_refine_ls_abs_structure_Flack   0.002(7)
_chemical_absolute_configuration ?
_refine_ls_number_reflns         54700
_refine_ls_number_parameters     2360
_refine_ls_number_restraints     2514
_refine_ls_R_factor_all          0.0921
_refine_ls_R_factor_gt           0.0626
_refine_ls_wR_factor_ref         0.1892
_refine_ls_wR_factor_gt          0.1689
_refine_ls_goodness_of_fit_ref   1.021
_refine_ls_restrained_S_all      0.998
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C 0.4292(3) -0.0802(2) 0.6643(2) 0.0343(19) Uani 1 1 d . . . . .
H1A H 0.402400 -0.073199 0.670508 0.052 Uiso 1 1 calc R U . . .
H1B H 0.445306 -0.082323 0.684420 0.052 Uiso 1 1 calc R U . . .
H1C H 0.429176 -0.105332 0.652640 0.052 Uiso 1 1 calc R U . . .
C6 C 0.4236(3) 0.5751(3) 0.3346(2) 0.0342(19) Uani 1 1 d . . . . .
H6A H 0.435832 0.573930 0.312635 0.051 Uiso 1 1 calc R U . . .
H6B H 0.424127 0.602105 0.342773 0.051 Uiso 1 1 calc R U . . .
H6C H 0.396463 0.566083 0.333093 0.051 Uiso 1 1 calc R U . . .
C9 C -0.0774(3) 0.4255(3) 0.6637(2) 0.0348(19) Uani 1 1 d . . . . .
H9A H -0.101415 0.418598 0.651822 0.052 Uiso 1 1 calc R U . . .
H9B H -0.083753 0.442630 0.682450 0.052 Uiso 1 1 calc R U . . .
H9C H -0.064873 0.401569 0.672036 0.052 Uiso 1 1 calc R U . . .
C12 C 0.1871(3) 0.1653(3) 0.4092(3) 0.042(2) Uani 1 1 d . . . . .
H12A H 0.158949 0.164378 0.413849 0.063 Uiso 1 1 calc R U . . .
H12B H 0.201681 0.164795 0.430099 0.063 Uiso 1 1 calc R U . . .
H12C H 0.194415 0.142525 0.395700 0.063 Uiso 1 1 calc R U . . .
C13 C 0.1789(3) 0.3170(3) 0.0759(2) 0.038(2) Uani 1 1 d . . . . .
H13A H 0.197682 0.330031 0.061130 0.057 Uiso 1 1 calc R U . . .
H13B H 0.160643 0.336432 0.084826 0.057 Uiso 1 1 calc R U . . .
H13C H 0.164381 0.297209 0.063354 0.057 Uiso 1 1 calc R U . . .
C14 C 0.3176(3) 0.1603(3) 0.0915(3) 0.043(2) Uani 1 1 d . . . . .
H14A H 0.301872 0.159272 0.071200 0.064 Uiso 1 1 calc R U . . .
H14B H 0.311325 0.137736 0.105553 0.064 Uiso 1 1 calc R U . . .
H14C H 0.345446 0.159736 0.085752 0.064 Uiso 1 1 calc R U . . .
C16 C 0.3304(4) 0.3192(4) 0.4153(3) 0.071(4) Uani 1 1 d . . . . .
H16A H 0.352753 0.331758 0.404388 0.085 Uiso 1 1 calc R U . . .
H16B H 0.339859 0.299786 0.431275 0.085 Uiso 1 1 calc R U . . .
H16C H 0.314884 0.339068 0.426921 0.085 Uiso 1 1 calc R U . . .
C17 C 0.0795(3) -0.0711(3) 0.3342(2) 0.039(2) Uani 1 1 d . . . . .
H17A H 0.077927 -0.059459 0.312039 0.059 Uiso 1 1 calc R U . . .
H17B H 0.076126 -0.099463 0.332636 0.059 Uiso 1 1 calc R U . . .
H17C H 0.105146 -0.065232 0.343992 0.059 Uiso 1 1 calc R U . . .
Cu1 Cu 0.500000 0.000000 0.64095(3) 0.0128(2) Uani 1 2 d S T P . .
Cu2 Cu 0.000000 0.500000 0.64053(3) 0.0148(2) Uani 1 2 d S T P . .
Cu3 Cu 0.500000 0.500000 0.35915(3) 0.0139(2) Uani 1 2 d S T P . .
Cu4 Cu 0.000000 0.000000 0.35637(2) 0.0129(2) Uani 1 2 d S T P . .
Cu5 Cu 0.24982(2) 0.24966(2) 0.39099(2) 0.01588(16) Uani 1 1 d . . . . .
Cu6 Cu 0.25643(2) 0.24538(2) 0.10757(2) 0.01674(16) Uani 1 1 d . . . . .
O1 O 0.44520(15) -0.05041(15) 0.64300(12) 0.0208(10) Uani 1 1 d . . . . .
H1 H 0.434850 -0.052021 0.624219 0.031 Uiso 1 1 calc R U . . .
O2 O -0.05073(16) 0.44561(15) 0.64130(14) 0.0240(11) Uani 1 1 d . . . . .
H2 H -0.052279 0.435635 0.622368 0.036 Uiso 1 1 calc R U . . .
O3 O 0.19627(16) 0.20103(15) 0.39110(13) 0.0238(11) Uani 1 1 d . . . . .
H3 H 0.185986 0.200186 0.372257 0.036 Uiso 1 1 calc R U . . .
O4 O 0.20019(16) 0.29807(15) 0.10346(14) 0.0253(11) Uani 1 1 d . . . . .
H4 H 0.194567 0.309258 0.121317 0.038 Uiso 1 1 calc R U . . .
O5 O 0.30890(15) 0.19620(15) 0.10944(14) 0.0228(10) Uani 1 1 d . . . . .
H5 H 0.319261 0.195338 0.128251 0.034 Uiso 1 1 calc R U . . .
O6 O 0.44559(15) 0.54950(16) 0.35798(13) 0.0230(11) Uani 1 1 d . . . . .
H6 H 0.434399 0.549442 0.376459 0.035 Uiso 1 1 calc R U . . .
O7 O 0.04849(15) -0.05450(16) 0.35542(13) 0.0231(11) Uani 1 1 d . . . . .
H7 H 0.043080 -0.070342 0.370594 0.035 Uiso 1 1 calc R U . . .
O8 O 0.30712(18) 0.30075(16) 0.39145(14) 0.0301(12) Uani 1 1 d . . . . .
H8 H 0.306622 0.314315 0.374157 0.045 Uiso 1 1 calc R U . . .
C1_1 C 0.4700(2) 0.0726(2) 0.67458(17) 0.0180(13) Uani 1 1 d . . . . .
H1_1 H 0.484258 0.084990 0.657297 0.022 Uiso 1 1 calc R U . . .
C2_1 C 0.4480(2) 0.0956(2) 0.69653(17) 0.0186(13) Uani 1 1 d . . . . .
H2_1 H 0.447651 0.123241 0.693866 0.022 Uiso 1 1 calc R U . . .
C3_1 C 0.4262(2) 0.0781(2) 0.72275(17) 0.0174(13) Uani 1 1 d . . . . .
C4_1 C 0.4291(2) 0.0369(2) 0.72581(17) 0.0221(14) Uani 1 1 d . . . . .
H4_1 H 0.415925 0.023850 0.743403 0.027 Uiso 1 1 calc R U . . .
C5_1 C 0.4515(2) 0.0149(2) 0.70269(17) 0.0196(14) Uani 1 1 d . . . . .
H5_1 H 0.452591 -0.012744 0.704871 0.023 Uiso 1 1 calc R U . . .
C6_1 C 0.4017(2) 0.1029(2) 0.74636(16) 0.0171(13) Uani 1 1 d . . . . .
C7_1 C 0.4130(2) 0.1420(2) 0.75318(17) 0.0210(14) Uani 1 1 d . . . . .
H7_1 H 0.435911 0.152508 0.743295 0.025 Uiso 1 1 calc R U . . .
C8_1 C 0.3898(2) 0.1658(2) 0.77501(17) 0.0205(14) Uani 1 1 d . . . . .
H8_1 H 0.397664 0.191715 0.780076 0.025 Uiso 1 1 calc R U . . .
C9_1 C 0.3549(2) 0.1501(2) 0.78902(17) 0.0197(14) Uani 1 1 d . . . . .
C10_1 C 0.3438(2) 0.1106(2) 0.78211(18) 0.0203(14) Uani 1 1 d . . . . .
H10_1 H 0.320884 0.100029 0.791879 0.024 Uiso 1 1 calc R U . . .
C11_1 C 0.3674(2) 0.0868(2) 0.76039(18) 0.0223(14) Uani 1 1 d . . . . .
H11_1 H 0.359983 0.060598 0.755573 0.027 Uiso 1 1 calc R U . . .
C12_1 C 0.3296(2) 0.1747(2) 0.81224(16) 0.0172(13) Uani 1 1 d . . . . .
C13_1 C 0.3264(2) 0.2159(2) 0.80873(18) 0.0226(14) Uani 1 1 d . . . . .
H13_1 H 0.340518 0.229105 0.791811 0.027 Uiso 1 1 calc R U . . .
C14_1 C 0.3022(2) 0.2369(2) 0.83053(16) 0.0208(14) Uani 1 1 d . . . . .
H14_1 H 0.300598 0.264461 0.828080 0.025 Uiso 1 1 calc R U . . .
C15_1 C 0.2839(2) 0.1791(2) 0.85838(16) 0.0179(13) Uani 1 1 d . . . . .
H15_1 H 0.268913 0.166299 0.874971 0.022 Uiso 1 1 calc R U . . .
C16_1 C 0.3082(2) 0.1567(2) 0.83820(17) 0.0199(14) Uani 1 1 d . . . . .
H16_1 H 0.310539 0.129389 0.841852 0.024 Uiso 1 1 calc R U . . .
N1_1 N 0.47166(17) 0.03244(17) 0.67738(13) 0.0155(11) Uani 1 1 d . . . . .
N2_1 N 0.28085(16) 0.21946(17) 0.85514(13) 0.0150(11) Uani 1 1 d . . . . .
C1_2 C 0.2004(2) 0.2643(2) 0.82896(16) 0.0202(14) Uani 1 1 d . . . . .
H1_2 H 0.202928 0.236805 0.826056 0.024 Uiso 1 1 calc R U . . .
C2_2 C 0.1768(2) 0.2847(2) 0.80628(18) 0.0213(14) Uani 1 1 d . . . . .
H2_2 H 0.163942 0.271377 0.788693 0.026 Uiso 1 1 calc R U . . .
C3_2 C 0.17280(19) 0.3260(2) 0.81040(16) 0.0147(12) Uani 1 1 d . . . . .
C4_2 C 0.1924(2) 0.3435(2) 0.83694(17) 0.0225(14) Uani 1 1 d . . . . .
H4_2 H 0.190446 0.370902 0.840172 0.027 Uiso 1 1 calc R U . . .
C5_2 C 0.2151(2) 0.3209(2) 0.85903(17) 0.0221(14) Uani 1 1 d . . . . .
H5_2 H 0.227439 0.333443 0.877244 0.027 Uiso 1 1 calc R U . . .
C6_2 C 0.1482(2) 0.3505(2) 0.78666(17) 0.0174(13) Uani 1 1 d . . . . .
C7_2 C 0.1604(2) 0.3898(2) 0.77915(18) 0.0223(15) Uani 1 1 d . . . . .
H7_2 H 0.183639 0.399990 0.788719 0.027 Uiso 1 1 calc R U . . .
C8_2 C 0.1377(2) 0.4135(2) 0.75747(18) 0.0223(15) Uani 1 1 d . . . . .
H8_2 H 0.146114 0.439205 0.752034 0.027 Uiso 1 1 calc R U . . .
C9_2 C 0.10241(19) 0.3987(2) 0.74403(16) 0.0149(12) Uani 1 1 d . . . . .
C10_2 C 0.0899(2) 0.3598(2) 0.75088(18) 0.0211(14) Uani 1 1 d . . . . .
H10_2 H 0.066486 0.350060 0.741309 0.025 Uiso 1 1 calc R U . . .
C11_2 C 0.1129(2) 0.3355(2) 0.77232(17) 0.0185(13) Uani 1 1 d . . . . .
H11_2 H 0.104774 0.309476 0.776989 0.022 Uiso 1 1 calc R U . . .
C12_2 C 0.0780(2) 0.4244(2) 0.72076(16) 0.0169(13) Uani 1 1 d . . . . .
C13_2 C 0.0366(2) 0.4256(2) 0.72268(17) 0.0209(14) Uani 1 1 d . . . . .
H13_2 H 0.023380 0.410356 0.738856 0.025 Uiso 1 1 calc R U . . .
C14_2 C 0.0150(2) 0.4494(2) 0.70065(16) 0.0193(13) Uani 1 1 d . . . . .
H14_2 H -0.012740 0.449760 0.702351 0.023 Uiso 1 1 calc R U . . .
C15_2 C 0.0729(2) 0.4714(2) 0.67480(17) 0.0201(14) Uani 1 1 d . . . . .
H15_2 H 0.085338 0.486952 0.658340 0.024 Uiso 1 1 calc R U . . .
C16_2 C 0.0961(2) 0.4488(2) 0.69597(17) 0.0213(14) Uani 1 1 d . . . . .
H16_2 H 0.123796 0.449590 0.694047 0.026 Uiso 1 1 calc R U . . .
N1_2 N 0.21992(17) 0.28110(17) 0.85503(13) 0.0156(11) Uani 1 1 d . . . . .
N2_2 N 0.03266(17) 0.47200(17) 0.67694(13) 0.0164(11) Uani 1 1 d . . . . .
C1_3 C 0.4896(2) 0.0506(2) 0.57898(17) 0.0203(14) Uani 1 1 d . . . . .
H1_3 H 0.517055 0.047155 0.576571 0.024 Uiso 1 1 calc R U . . .
C2_3 C 0.4702(2) 0.0745(2) 0.55658(17) 0.0213(14) Uani 1 1 d . . . . .
H2_3 H 0.484258 0.086951 0.539207 0.026 Uiso 1 1 calc R U . . .
C3_3 C 0.4285(2) 0.0804(2) 0.55979(16) 0.0180(13) Uani 1 1 d . . . . .
C4_3 C 0.4098(2) 0.0603(2) 0.58578(17) 0.0214(14) Uani 1 1 d . . . . .
H4_3 H 0.382330 0.062808 0.588629 0.026 Uiso 1 1 calc R U . . .
C5_3 C 0.4315(2) 0.0365(2) 0.60769(18) 0.0225(14) Uani 1 1 d . . . . .
H5_3 H 0.418232 0.023410 0.625170 0.027 Uiso 1 1 calc R U . . .
C6_3 C 0.4055(2) 0.1055(2) 0.53605(17) 0.0198(13) Uani 1 1 d . . . . .
C7_3 C 0.4193(2) 0.1421(2) 0.52332(19) 0.0238(15) Uani 1 1 d . . . . .
H7_3 H 0.444822 0.150907 0.528877 0.029 Uiso 1 1 calc R U . . .
C8_3 C 0.3950(2) 0.1655(2) 0.50228(19) 0.0237(15) Uani 1 1 d . . . . .
H8_3 H 0.404425 0.189751 0.493972 0.028 Uiso 1 1 calc R U . . .
C9_3 C 0.3566(2) 0.1525(2) 0.49377(18) 0.0227(15) Uani 1 1 d . . . . .
C10_3 C 0.3431(2) 0.1157(2) 0.50538(19) 0.0277(17) Uani 1 1 d . . . . .
H10_3 H 0.318087 0.106259 0.499047 0.033 Uiso 1 1 calc R U . . .
C11_3 C 0.3676(2) 0.0929(2) 0.52665(19) 0.0290(17) Uani 1 1 d . . . . .
H11_3 H 0.358143 0.068508 0.534719 0.035 Uiso 1 1 calc R U . . .
C12_3 C 0.3301(2) 0.1757(2) 0.47077(18) 0.0208(14) Uani 1 1 d . . . . .
C13_3 C 0.3256(2) 0.2166(2) 0.47365(19) 0.0283(17) Uani 1 1 d . . . . .
H13_3 H 0.340047 0.230635 0.489886 0.034 Uiso 1 1 calc R U . . .
C14_3 C 0.2995(2) 0.2368(2) 0.45233(17) 0.0266(16) Uani 1 1 d . . . . .
H14_3 H 0.295792 0.264108 0.455498 0.032 Uiso 1 1 calc R U . . .
C15_3 C 0.2840(2) 0.1784(2) 0.42413(18) 0.0220(14) Uani 1 1 d . . . . .
H15_3 H 0.270549 0.165372 0.406746 0.026 Uiso 1 1 calc R U . . .
C16_3 C 0.3079(2) 0.1561(2) 0.44538(18) 0.0224(14) Uani 1 1 d . . . . .
H16_3 H 0.309239 0.128540 0.443001 0.027 Uiso 1 1 calc R U . . .
N1_3 N 0.47089(16) 0.03169(16) 0.60450(13) 0.0150(11) Uani 1 1 d . . . . .
N2_3 N 0.27925(18) 0.21851(18) 0.42730(14) 0.0192(12) Uani 1 1 d . . . . .
C1_4 C 0.4501(2) 0.4845(2) 0.29844(17) 0.0210(14) Uani 1 1 d . . . . .
H1_4 H 0.449813 0.512186 0.296953 0.025 Uiso 1 1 calc R U . . .
C2_4 C 0.4274(2) 0.4635(2) 0.27611(18) 0.0240(15) Uani 1 1 d . . . . .
H2_4 H 0.412593 0.477003 0.259798 0.029 Uiso 1 1 calc R U . . .
C3_4 C 0.4261(2) 0.4217(2) 0.27744(17) 0.0179(13) Uani 1 1 d . . . . .
C4_4 C 0.4508(2) 0.4032(2) 0.30241(17) 0.0201(14) Uani 1 1 d . . . . .
H4_4 H 0.451988 0.375520 0.303849 0.024 Uiso 1 1 calc R U . . .
C5_4 C 0.4728(2) 0.4266(2) 0.32451(17) 0.0192(13) Uani 1 1 d . . . . .
H5_4 H 0.487965 0.414018 0.341156 0.023 Uiso 1 1 calc R U . . .
C6_4 C 0.4015(2) 0.3976(2) 0.25467(16) 0.0180(13) Uani 1 1 d . . . . .
C7_4 C 0.4165(2) 0.3615(2) 0.24077(17) 0.0199(14) Uani 1 1 d . . . . .
H7_4 H 0.442102 0.352971 0.246283 0.024 Uiso 1 1 calc R U . . .
C8_4 C 0.3936(2) 0.3394(2) 0.21946(18) 0.0220(14) Uani 1 1 d . . . . .
H8_4 H 0.404096 0.316028 0.210381 0.026 Uiso 1 1 calc R U . . .
C9_4 C 0.3544(2) 0.3508(2) 0.21066(17) 0.0184(13) Uani 1 1 d . . . . .
C10_4 C 0.3394(2) 0.3865(2) 0.22486(17) 0.0185(13) Uani 1 1 d . . . . .
H10_4 H 0.313515 0.394607 0.219842 0.022 Uiso 1 1 calc R U . . .
C11_4 C 0.3628(2) 0.4094(2) 0.24614(17) 0.0190(13) Uani 1 1 d . . . . .
H11_4 H 0.352613 0.433117 0.254918 0.023 Uiso 1 1 calc R U . . .
C12_4 C 0.3305(2) 0.3257(2) 0.18752(16) 0.0178(13) Uani 1 1 d . . . . .
C13_4 C 0.3490(2) 0.3049(2) 0.16168(17) 0.0203(14) Uani 1 1 d . . . . .
H13_4 H 0.376474 0.306812 0.158831 0.024 Uiso 1 1 calc R U . . .
C14_4 C 0.3265(2) 0.2810(2) 0.13981(16) 0.0193(13) Uani 1 1 d . . . . .
H14_4 H 0.339427 0.267213 0.122527 0.023 Uiso 1 1 calc R U . . .
C15_4 C 0.2686(2) 0.2974(2) 0.16826(16) 0.0186(13) Uani 1 1 d . . . . .
H15_4 H 0.241168 0.294475 0.170933 0.022 Uiso 1 1 calc R U . . .
C16_4 C 0.2891(2) 0.3224(2) 0.19061(17) 0.0209(14) Uani 1 1 d . . . . .
H16_4 H 0.275408 0.336511 0.207245 0.025 Uiso 1 1 calc R U . . .
N1_4 N 0.47327(17) 0.46746(17) 0.32282(14) 0.0173(11) Uani 1 1 d . . . . .
N2_4 N 0.28663(16) 0.27736(17) 0.14311(14) 0.0168(11) Uani 1 1 d . . . . .
C1_5 C 0.0155(2) 0.0494(2) 0.29435(17) 0.0211(14) Uani 1 1 d . . . . .
H1_5 H -0.012039 0.048313 0.291518 0.025 Uiso 1 1 calc R U . . .
C2_5 C 0.0371(2) 0.0722(2) 0.27243(17) 0.0204(14) Uani 1 1 d . . . . .
H2_5 H 0.024110 0.086018 0.255202 0.024 Uiso 1 1 calc R U . . .
C3_5 C 0.0789(2) 0.07528(19) 0.27551(16) 0.0155(12) Uani 1 1 d . . . . .
C4_5 C 0.0963(2) 0.0526(2) 0.30174(17) 0.0185(13) Uani 1 1 d . . . . .
H4_5 H 0.123851 0.052984 0.304766 0.022 Uiso 1 1 calc R U . . .
C5_5 C 0.0727(2) 0.0297(2) 0.32303(17) 0.0194(13) Uani 1 1 d . . . . .
H5_5 H 0.084963 0.014869 0.339985 0.023 Uiso 1 1 calc R U . . .
C6_5 C 0.1036(2) 0.0995(2) 0.25314(17) 0.0171(13) Uani 1 1 d . . . . .
C7_5 C 0.1428(2) 0.0885(2) 0.24558(18) 0.0199(14) Uani 1 1 d . . . . .
H7_5 H 0.153232 0.065095 0.254674 0.024 Uiso 1 1 calc R U . . .
C8_5 C 0.1662(2) 0.1118(2) 0.22484(17) 0.0195(13) Uani 1 1 d . . . . .
H8_5 H 0.192368 0.103980 0.220570 0.023 Uiso 1 1 calc R U . . .
C9_5 C 0.1518(2) 0.1469(2) 0.20996(19) 0.0195(14) Uani 1 1 d . . . . .
C10_5 C 0.1123(2) 0.1579(2) 0.21756(18) 0.0204(14) Uani 1 1 d . . . . .
H10_5 H 0.101886 0.181304 0.208395 0.025 Uiso 1 1 calc R U . . .
C11_5 C 0.0886(2) 0.1346(2) 0.23845(17) 0.0185(13) Uani 1 1 d . . . . .
H11_5 H 0.062353 0.142333 0.242790 0.022 Uiso 1 1 calc R U . . .
C12_5 C 0.1767(2) 0.1712(2) 0.18730(16) 0.0165(13) Uani 1 1 d . . . . .
C13_5 C 0.2186(2) 0.1731(2) 0.19106(17) 0.0196(13) Uani 1 1 d . . . . .
H13_5 H 0.231448 0.158751 0.208041 0.023 Uiso 1 1 calc R U . . .
C14_5 C 0.2402(2) 0.1968(2) 0.16895(16) 0.0188(13) Uani 1 1 d . . . . .
H14_5 H 0.267715 0.198296 0.171705 0.023 Uiso 1 1 calc R U . . .
C15_5 C 0.1835(2) 0.2161(2) 0.14011(17) 0.0186(13) Uani 1 1 d . . . . .
H15_5 H 0.171609 0.231159 0.123032 0.022 Uiso 1 1 calc R U . . .
C16_5 C 0.1594(2) 0.1931(2) 0.16071(17) 0.0185(13) Uani 1 1 d . . . . .
H16_5 H 0.131954 0.192068 0.157012 0.022 Uiso 1 1 calc R U . . .
N1_5 N 0.03200(16) 0.02815(17) 0.32012(13) 0.0142(11) Uani 1 1 d . . . . .
N2_5 N 0.22334(16) 0.21779(17) 0.14371(14) 0.0161(11) Uani 1 1 d . . . . .
C1_6 C 0.4877(2) 0.4511(2) 0.42191(17) 0.0201(14) Uani 1 1 d . . . . .
H1_6 H 0.515108 0.454225 0.424876 0.024 Uiso 1 1 calc R U . . .
C2_6 C 0.4674(2) 0.4280(2) 0.44508(18) 0.0228(14) Uani 1 1 d . . . . .
H2_6 H 0.480882 0.415645 0.462798 0.027 Uiso 1 1 calc R U . . .
C3_6 C 0.4257(2) 0.4235(2) 0.44146(17) 0.0179(13) Uani 1 1 d . . . . .
C4_6 C 0.4075(2) 0.4429(2) 0.41436(17) 0.0203(14) Uani 1 1 d . . . . .
H4_6 H 0.380024 0.441182 0.411284 0.024 Uiso 1 1 calc R U . . .
C5_6 C 0.4307(2) 0.4649(2) 0.39196(17) 0.0208(14) Uani 1 1 d . . . . .
H5_6 H 0.418081 0.477189 0.373737 0.025 Uiso 1 1 calc R U . . .
C6_6 C 0.4019(2) 0.3985(2) 0.46479(19) 0.0206(14) Uani 1 1 d . . . . .
C7_6 C 0.4176(2) 0.3627(2) 0.4771(2) 0.0281(17) Uani 1 1 d . . . . .
H7_6 H 0.443583 0.355432 0.471435 0.034 Uiso 1 1 calc R U . . .
C8_6 C 0.3952(2) 0.3379(2) 0.4976(2) 0.0280(17) Uani 1 1 d . . . . .
H8_6 H 0.405844 0.313874 0.505276 0.034 Uiso 1 1 calc R U . . .
C9_6 C 0.3565(2) 0.3490(2) 0.50689(17) 0.0211(14) Uani 1 1 d . . . . .
C10_6 C 0.3406(2) 0.3845(2) 0.49473(19) 0.0245(15) Uani 1 1 d . . . . .
H10_6 H 0.314695 0.391706 0.500676 0.029 Uiso 1 1 calc R U . . .
C11_6 C 0.3626(2) 0.4090(2) 0.47398(18) 0.0219(14) Uani 1 1 d . . . . .
H11_6 H 0.351537 0.432701 0.465979 0.026 Uiso 1 1 calc R U . . .
C12_6 C 0.3325(2) 0.3222(2) 0.52889(17) 0.0189(13) Uani 1 1 d . . . . .
C13_6 C 0.3503(2) 0.3020(2) 0.55635(17) 0.0205(14) Uani 1 1 d . . . . .
H13_6 H 0.377614 0.304522 0.560315 0.025 Uiso 1 1 calc R U . . .
C14_6 C 0.3273(2) 0.2786(2) 0.57721(17) 0.0206(14) Uani 1 1 d . . . . .
H14_6 H 0.339374 0.266500 0.595797 0.025 Uiso 1 1 calc R U . . .
C15_6 C 0.2714(2) 0.2895(2) 0.54504(17) 0.0228(15) Uani 1 1 d . . . . .
H15_6 H 0.244711 0.283958 0.540407 0.027 Uiso 1 1 calc R U . . .
C16_6 C 0.2920(2) 0.3151(2) 0.52357(17) 0.0208(14) Uani 1 1 d . . . . .
H16_6 H 0.278823 0.327524 0.505700 0.025 Uiso 1 1 calc R U . . .
N1_6 N 0.47058(15) 0.46923(16) 0.39529(13) 0.0124(10) Uani 1 1 d . . . . .
N2_6 N 0.28829(17) 0.27242(17) 0.57199(13) 0.0166(11) Uani 1 1 d . . . . .
C1_8 C 0.2407(2) 0.1902(2) 0.54926(16) 0.0238(15) Uani 1 1 d . . . . .
H1_8 H 0.268481 0.189628 0.548578 0.029 Uiso 1 1 calc R U . . .
C2_8 C 0.2196(2) 0.1653(2) 0.52716(17) 0.0234(15) Uani 1 1 d . . . . .
H2_8 H 0.233143 0.148224 0.512535 0.028 Uiso 1 1 calc R U . . .
C3_8 C 0.1777(2) 0.1664(2) 0.52737(18) 0.0202(14) Uani 1 1 d . . . . .
C4_8 C 0.1595(2) 0.1928(2) 0.55092(17) 0.0204(14) Uani 1 1 d . . . . .
H4_8 H 0.131803 0.194316 0.552172 0.024 Uiso 1 1 calc R U . . .
C5_8 C 0.1828(2) 0.2163(2) 0.57203(17) 0.0203(14) Uani 1 1 d . . . . .
H5_8 H 0.170339 0.233550 0.587179 0.024 Uiso 1 1 calc R U . . .
C6_8 C 0.1531(2) 0.1410(2) 0.50490(17) 0.0202(14) Uani 1 1 d . . . . .
C7_8 C 0.1650(2) 0.1023(2) 0.49601(19) 0.0244(15) Uani 1 1 d . . . . .
H7_8 H 0.189017 0.092286 0.504141 0.029 Uiso 1 1 calc R U . . .
C8_8 C 0.1413(2) 0.0788(2) 0.47523(19) 0.0225(14) Uani 1 1 d . . . . .
H8_8 H 0.149072 0.052776 0.470346 0.027 Uiso 1 1 calc R U . . .
C9_8 C 0.1058(2) 0.0939(2) 0.46153(18) 0.0230(15) Uani 1 1 d . . . . .
C10_8 C 0.0938(2) 0.1330(2) 0.47157(18) 0.0242(15) Uani 1 1 d . . . . .
H10_8 H 0.069643 0.143330 0.463838 0.029 Uiso 1 1 calc R U . . .
C11_8 C 0.1174(2) 0.1554(2) 0.49249(18) 0.0235(15) Uani 1 1 d . . . . .
H11_8 H 0.109212 0.181026 0.498475 0.028 Uiso 1 1 calc R U . . .
C12_8 C 0.0800(2) 0.0709(2) 0.43854(16) 0.0178(13) Uani 1 1 d . . . . .
C13_8 C 0.0738(2) 0.0297(2) 0.44209(17) 0.0210(14) Uani 1 1 d . . . . .
H13_8 H 0.085833 0.015485 0.459566 0.025 Uiso 1 1 calc R U . . .
C14_8 C 0.0488(2) 0.0105(2) 0.41844(17) 0.0208(14) Uani 1 1 d . . . . .
H14_8 H 0.044523 -0.016819 0.420905 0.025 Uiso 1 1 calc R U . . .
C15_8 C 0.0367(2) 0.0688(2) 0.38973(16) 0.0182(13) Uani 1 1 d . . . . .
H15_8 H 0.024258 0.082324 0.372019 0.022 Uiso 1 1 calc R U . . .
C16_8 C 0.0604(2) 0.0904(2) 0.41229(17) 0.0206(14) Uani 1 1 d . . . . .
H16_8 H 0.063200 0.117880 0.409715 0.025 Uiso 1 1 calc R U . . .
N1_8 N 0.22316(17) 0.21471(18) 0.57116(14) 0.0194(12) Uani 1 1 d . . . . .
N2_8 N 0.03110(15) 0.02915(16) 0.39276(13) 0.0129(10) Uani 1 1 d . . . . .
C1_9 C 0.0345(2) 0.4309(2) 0.60737(17) 0.0204(14) Uani 1 1 d . . . . .
H1_9 H 0.020813 0.418322 0.624919 0.025 Uiso 1 1 calc R U . . .
C2_9 C 0.0574(2) 0.4078(2) 0.58563(17) 0.0185(13) Uani 1 1 d . . . . .
H2_9 H 0.058831 0.380250 0.588654 0.022 Uiso 1 1 calc R U . . .
C3_9 C 0.0781(2) 0.4257(2) 0.55952(16) 0.0153(12) Uani 1 1 d . . . . .
C4_9 C 0.0749(2) 0.4673(2) 0.55683(17) 0.0208(14) Uani 1 1 d . . . . .
H4_9 H 0.088658 0.480710 0.539834 0.025 Uiso 1 1 calc R U . . .
C5_9 C 0.0515(2) 0.4883(2) 0.57916(16) 0.0199(13) Uani 1 1 d . . . . .
H5_9 H 0.049623 0.515883 0.576966 0.024 Uiso 1 1 calc R U . . .
C6_9 C 0.1030(2) 0.4018(2) 0.53591(16) 0.0162(13) Uani 1 1 d . . . . .
C7_9 C 0.1406(2) 0.4163(2) 0.52557(17) 0.0216(14) Uani 1 1 d . . . . .
H7_9 H 0.149264 0.441345 0.532585 0.026 Uiso 1 1 calc R U . . .
C8_9 C 0.1647(2) 0.3927(2) 0.50461(17) 0.0192(14) Uani 1 1 d . . . . .
H8_9 H 0.189297 0.402315 0.497362 0.023 Uiso 1 1 calc R U . . .
C9_9 C 0.1521(2) 0.3547(2) 0.49453(17) 0.0190(13) Uani 1 1 d . . . . .
C10_9 C 0.1144(2) 0.3410(2) 0.50445(18) 0.0234(15) Uani 1 1 d . . . . .
H10_9 H 0.105518 0.316202 0.496888 0.028 Uiso 1 1 calc R U . . .
C11_9 C 0.0900(2) 0.3638(2) 0.52547(18) 0.0216(14) Uani 1 1 d . . . . .
H11_9 H 0.065386 0.353951 0.532534 0.026 Uiso 1 1 calc R U . . .
C12_9 C 0.1778(2) 0.3298(2) 0.47176(16) 0.0161(13) Uani 1 1 d . . . . .
C13_9 C 0.2030(2) 0.3476(2) 0.44807(17) 0.0209(14) Uani 1 1 d . . . . .
H13_9 H 0.205150 0.375228 0.446822 0.025 Uiso 1 1 calc R U . . .
C14_9 C 0.2249(2) 0.3232(2) 0.42627(17) 0.0217(14) Uani 1 1 d . . . . .
H14_9 H 0.241645 0.335174 0.410407 0.026 Uiso 1 1 calc R U . . .
C15_9 C 0.1989(2) 0.2658(2) 0.45076(17) 0.0243(15) Uani 1 1 d . . . . .
H15_9 H 0.197400 0.238067 0.451954 0.029 Uiso 1 1 calc R U . . .
C16_9 C 0.1765(2) 0.2883(2) 0.47301(18) 0.0252(16) Uani 1 1 d . . . . .
H16_9 H 0.160366 0.275625 0.488947 0.030 Uiso 1 1 calc R U . . .
N1_9 N 0.03128(17) 0.46994(16) 0.60412(13) 0.0146(11) Uani 1 1 d . . . . .
N2_9 N 0.22287(17) 0.28269(17) 0.42729(14) 0.0170(11) Uani 1 1 d . . . . .
B1_10 B 0.5007(3) 0.2912(2) 0.1181(2) 0.0232(15) Uani 1 1 d . . . . .
B2_10 B 0.5013(3) 0.2908(2) 0.07258(19) 0.0217(15) Uani 1 1 d . . . . .
B3_10 B 0.5444(2) 0.2761(2) 0.0963(2) 0.0221(15) Uani 1 1 d . . . . .
B4_10 B 0.5274(3) 0.2496(2) 0.1326(2) 0.0228(15) Uani 1 1 d . . . . .
B5_10 B 0.4577(3) 0.2741(2) 0.0949(2) 0.0228(15) Uani 1 1 d . . . . .
B6_10 B 0.4744(3) 0.2480(3) 0.1319(2) 0.0251(16) Uani 1 1 d . . . . .
B7_10 B 0.4586(2) 0.2209(2) 0.0952(2) 0.0210(15) Uani 1 1 d . . . . .
B8_10 B 0.5027(3) 0.2055(2) 0.11871(19) 0.0217(15) Uani 1 1 d . . . . .
B9_10 B 0.5458(2) 0.2227(2) 0.09622(19) 0.0192(14) Uani 1 1 d . . . . .
B10_10 B 0.5295(2) 0.2486(3) 0.0589(2) 0.0225(15) Uani 1 1 d . . . . .
B11_10 B 0.4756(2) 0.2467(3) 0.0584(2) 0.0227(15) Uani 1 1 d . . . . .
B12_10 B 0.5036(2) 0.2048(2) 0.0735(2) 0.0219(15) Uani 1 1 d . . . . .
Cl1_10 Cl 0.49827(6) 0.33720(5) 0.14221(4) 0.0265(4) Uani 1 1 d . . . . .
Cl2_10 Cl 0.41258(5) 0.30168(5) 0.09245(4) 0.0253(4) Uani 1 1 d . . . . .
Cl3_10 Cl 0.49696(5) 0.33594(5) 0.04775(4) 0.0247(3) Uani 1 1 d . . . . .
Cl4_10 Cl 0.59020(5) 0.30331(6) 0.09753(5) 0.0281(4) Uani 1 1 d . . . . .
Cl5_10 Cl 0.44538(5) 0.24786(6) 0.17004(4) 0.0255(4) Uani 1 1 d . . . . .
Cl6_10 Cl 0.55560(6) 0.25000(6) 0.17146(4) 0.0268(4) Uani 1 1 d . . . . .
Cl7_10 Cl 0.59112(5) 0.19453(6) 0.09563(5) 0.0266(4) Uani 1 1 d . . . . .
Cl8_10 Cl 0.55878(6) 0.24901(6) 0.02125(4) 0.0279(4) Uani 1 1 d . . . . .
Cl9_10 Cl 0.50737(6) 0.15970(5) 0.04879(5) 0.0259(4) Uani 1 1 d . . . . .
Cl10_10 Cl 0.45016(6) 0.24435(6) 0.01844(4) 0.0267(4) Uani 1 1 d . . . . .
Cl11_10 Cl 0.41298(5) 0.19432(5) 0.09574(5) 0.0275(4) Uani 1 1 d . . . . .
Cl12_10 Cl 0.50321(6) 0.16038(5) 0.14362(4) 0.0266(4) Uani 1 1 d . . . . .
B1_11 B 0.2599(3) 0.5335(3) 0.1055(2) 0.0259(16) Uani 1 1 d . . . . .
B2_11 B 0.2179(3) 0.5014(3) 0.1012(2) 0.0227(15) Uani 1 1 d . . . . .
B3_11 B 0.2193(3) 0.5361(3) 0.1356(2) 0.0239(16) Uani 1 1 d . . . . .
B4_11 B 0.2702(3) 0.5396(2) 0.1499(2) 0.0234(16) Uani 1 1 d . . . . .
B5_11 B 0.2996(2) 0.5069(3) 0.1245(2) 0.0231(15) Uani 1 1 d . . . . .
B6_11 B 0.2679(3) 0.4829(3) 0.0945(2) 0.0253(16) Uani 1 1 d . . . . .
B7_11 B 0.2317(3) 0.4530(3) 0.1174(2) 0.0246(16) Uani 1 1 d . . . . .
B8_11 B 0.2827(3) 0.4568(2) 0.1320(2) 0.0211(15) Uani 1 1 d . . . . .
B9_11 B 0.2845(2) 0.4921(2) 0.1662(2) 0.0225(15) Uani 1 1 d . . . . .
B10_11 B 0.2350(2) 0.5101(3) 0.1729(2) 0.0223(15) Uani 1 1 d . . . . .
B11_11 B 0.2029(2) 0.4864(3) 0.1429(2) 0.0243(16) Uani 1 1 d . . . . .
B12_11 B 0.2427(2) 0.4586(2) 0.1615(2) 0.0207(15) Uani 1 1 d . . . . .
Cl1_11 Cl 0.26752(6) 0.57294(6) 0.07526(5) 0.0323(4) Uani 1 1 d . . . . .
Cl2_11 Cl 0.18627(6) 0.57825(6) 0.13660(5) 0.0322(4) Uani 1 1 d . . . . .
Cl3_11 Cl 0.28982(7) 0.58478(6) 0.16746(5) 0.0363(5) Uani 1 1 d . . . . .
Cl4_11 Cl 0.35059(6) 0.51722(7) 0.11421(5) 0.0366(5) Uani 1 1 d . . . . .
Cl5_11 Cl 0.28588(7) 0.46829(7) 0.05343(5) 0.0364(5) Uani 1 1 d . . . . .
Cl6_11 Cl 0.18307(5) 0.50625(6) 0.06654(4) 0.0273(4) Uani 1 1 d . . . . .
Cl7_11 Cl 0.21198(6) 0.40810(6) 0.10005(5) 0.0330(4) Uani 1 1 d . . . . .
Cl8_11 Cl 0.31476(6) 0.41378(6) 0.13005(5) 0.0302(4) Uani 1 1 d . . . . .
Cl9_11 Cl 0.31931(5) 0.48674(6) 0.20061(5) 0.0261(4) Uani 1 1 d . . . . .
Cl10_11 Cl 0.21767(6) 0.52185(6) 0.21480(5) 0.0323(4) Uani 1 1 d . . . . .
Cl11_11 Cl 0.15222(5) 0.47532(7) 0.15450(5) 0.0333(4) Uani 1 1 d . . . . .
Cl12_11 Cl 0.23335(5) 0.41937(5) 0.19169(5) 0.0258(4) Uani 1 1 d . . . . .
B1_12 B 0.5024(3) 0.2776(2) 0.3510(2) 0.0269(17) Uani 1 1 d . . . . .
B2_12 B 0.4575(3) 0.2581(3) 0.3658(2) 0.0274(17) Uani 1 1 d . . . . .
B3_12 B 0.4803(3) 0.2984(3) 0.3877(2) 0.0269(17) Uani 1 1 d . . . . .
B4_12 B 0.4955(3) 0.2248(3) 0.3517(2) 0.0259(16) Uani 1 1 d . . . . .
B5_12 B 0.5327(3) 0.2908(3) 0.3868(2) 0.0289(17) Uani 1 1 d . . . . .
B6_12 B 0.5425(3) 0.2447(3) 0.3646(2) 0.0293(17) Uani 1 1 d . . . . .
B7_12 B 0.5439(3) 0.2455(3) 0.4097(2) 0.0311(18) Uani 1 1 d . . . . .
B8_12 B 0.5208(3) 0.2051(2) 0.3877(2) 0.0262(16) Uani 1 1 d . . . . .
B9_12 B 0.5055(3) 0.2792(3) 0.4246(2) 0.0292(18) Uani 1 1 d . . . . .
B10_12 B 0.4680(3) 0.2127(3) 0.3897(2) 0.0277(17) Uani 1 1 d . . . . .
B11_12 B 0.4587(3) 0.2585(3) 0.4112(2) 0.0301(18) Uani 1 1 d . . . . .
B12_12 B 0.4978(3) 0.2261(3) 0.4256(2) 0.0291(17) Uani 1 1 d . . . . .
Cl1_12 Cl 0.50591(7) 0.30461(6) 0.31153(5) 0.0358(5) Uani 1 1 d . . . . .
Cl2_12 Cl 0.41214(7) 0.26496(7) 0.34175(6) 0.0385(5) Uani 1 1 d . . . . .
Cl3_12 Cl 0.45883(6) 0.34748(6) 0.38708(5) 0.0335(4) Uani 1 1 d . . . . .
Cl4_12 Cl 0.49014(7) 0.19586(6) 0.31324(5) 0.0367(5) Uani 1 1 d . . . . .
Cl5_12 Cl 0.56753(7) 0.33111(6) 0.38509(7) 0.0438(5) Uani 1 1 d . . . . .
Cl6_12 Cl 0.58521(6) 0.23713(6) 0.33800(6) 0.0370(5) Uani 1 1 d . . . . .
Cl7_12 Cl 0.58994(7) 0.24047(7) 0.43213(6) 0.0424(5) Uani 1 1 d . . . . .
Cl8_12 Cl 0.54181(7) 0.15594(6) 0.38725(5) 0.0338(4) Uani 1 1 d . . . . .
Cl9_12 Cl 0.43291(7) 0.17245(7) 0.39074(6) 0.0442(5) Uani 1 1 d . . . . .
Cl10_12 Cl 0.41410(7) 0.26432(8) 0.43634(6) 0.0458(6) Uani 1 1 d . . . . .
Cl11_12 Cl 0.51217(7) 0.30705(7) 0.46248(6) 0.0429(5) Uani 1 1 d . . . . .
Cl12_12 Cl 0.49359(7) 0.19942(7) 0.46445(5) 0.0426(5) Uani 1 1 d . . . . .
B1_13 B 0.2642(2) 0.5123(3) 0.3284(2) 0.0220(15) Uani 1 1 d . . . . .
B2_13 B 0.2589(3) 0.4608(2) 0.3385(2) 0.0229(15) Uani 1 1 d . . . . .
B3_13 B 0.2981(2) 0.4886(2) 0.3562(2) 0.0202(15) Uani 1 1 d . . . . .
B4_13 B 0.2795(2) 0.5378(2) 0.36583(19) 0.0183(14) Uani 1 1 d . . . . .
B5_13 B 0.2283(2) 0.5395(2) 0.3529(2) 0.0214(15) Uani 1 1 d . . . . .
B6_13 B 0.2155(2) 0.4906(2) 0.3362(2) 0.0208(15) Uani 1 1 d . . . . .
B7_13 B 0.2014(2) 0.5037(3) 0.3789(2) 0.0244(16) Uani 1 1 d . . . . .
B8_13 B 0.2413(2) 0.5328(2) 0.3971(2) 0.0207(15) Uani 1 1 d . . . . .
B9_13 B 0.2361(2) 0.4808(2) 0.4073(2) 0.0220(15) Uani 1 1 d . . . . .
B10_13 B 0.2845(2) 0.5018(2) 0.39897(19) 0.0208(14) Uani 1 1 d . . . . .
B11_13 B 0.2721(2) 0.4536(2) 0.3824(2) 0.0200(15) Uani 1 1 d . . . . .
B12_13 B 0.2202(2) 0.4547(3) 0.3692(2) 0.0206(15) Uani 1 1 d . . . . .
Cl1_13 Cl 0.27791(6) 0.52634(6) 0.28619(4) 0.0284(4) Uani 1 1 d . . . . .
Cl2_13 Cl 0.17912(5) 0.48550(5) 0.30317(4) 0.0245(4) Uani 1 1 d . . . . .
Cl3_13 Cl 0.20558(6) 0.58380(6) 0.33725(5) 0.0308(4) Uani 1 1 d . . . . .
Cl4_13 Cl 0.31092(6) 0.58127(5) 0.36443(4) 0.0261(4) Uani 1 1 d . . . . .
Cl5_13 Cl 0.34883(5) 0.48078(6) 0.34302(5) 0.0268(4) Uani 1 1 d . . . . .
Cl6_13 Cl 0.26855(5) 0.42213(5) 0.30711(4) 0.0239(3) Uani 1 1 d . . . . .
Cl7_13 Cl 0.29459(5) 0.40888(5) 0.39776(4) 0.0259(4) Uani 1 1 d . . . . .
Cl8_13 Cl 0.19010(5) 0.41105(5) 0.37124(4) 0.0237(3) Uani 1 1 d . . . . .
Cl9_13 Cl 0.32035(5) 0.50770(5) 0.43289(4) 0.0241(4) Uani 1 1 d . . . . .
Cl10_13 Cl 0.22185(6) 0.46462(6) 0.44891(4) 0.0291(4) Uani 1 1 d . . . . .
Cl11_13 Cl 0.23228(6) 0.57010(5) 0.42845(5) 0.0269(4) Uani 1 1 d . . . . .
Cl12_13 Cl 0.15064(5) 0.51213(6) 0.39063(5) 0.0282(4) Uani 1 1 d . . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C1 O1 1.410(9) . ?
C1 H1A 0.9600 . ?
C1 H1B 0.9600 . ?
C1 H1C 0.9600 . ?
C6 O6 1.457(9) . ?
C6 H6A 0.9600 . ?
C6 H6B 0.9600 . ?
C6 H6C 0.9600 . ?
C9 O2 1.426(9) . ?
C9 H9A 0.9600 . ?
C9 H9B 0.9600 . ?
C9 H9C 0.9600 . ?
C12 O3 1.427(9) . ?
C12 H12A 0.9600 . ?
C12 H12B 0.9600 . ?
C12 H12C 0.9600 . ?
C13 O4 1.447(10) . ?
C13 H13A 0.9600 . ?
C13 H13B 0.9600 . ?
C13 H13C 0.9600 . ?
C14 O5 1.424(10) . ?
C14 H14A 0.9600 . ?
C14 H14B 0.9600 . ?
C14 H14C 0.9600 . ?
C16 O8 1.369(13) . ?
C16 H16A 0.9600 . ?
C16 H16B 0.9600 . ?
C16 H16C 0.9600 . ?
C17 O7 1.444(9) . ?
C17 H17A 0.9600 . ?
C17 H17B 0.9600 . ?
C17 H17C 0.9600 . ?
Cu1 N1_3 2.036(5) . ?
Cu1 N1_3 2.036(5) 2_655 ?
Cu1 N1_1 2.036(5) 2_655 ?
Cu1 N1_1 2.036(5) . ?
Cu2 N2_2 2.034(5) . ?
Cu2 N2_2 2.034(5) 2_565 ?
Cu2 N1_9 2.043(5) 2_565 ?
Cu2 N1_9 2.043(5) . ?
Cu3 N1_4 2.011(5) . ?
Cu3 N1_4 2.011(5) 2_665 ?
Cu3 N1_6 2.016(5) . ?
Cu3 N1_6 2.016(5) 2_665 ?
Cu4 N1_5 2.020(5) . ?
Cu4 N1_5 2.020(5) 2 ?
Cu4 N2_8 2.025(5) 2 ?
Cu4 N2_8 2.025(5) . ?
Cu5 N2_9 2.022(5) . ?
Cu5 N2_1 2.026(5) 7_554 ?
Cu5 N2_3 2.027(6) . ?
Cu5 N1_2 2.030(5) 7_554 ?
Cu6 N1_8 2.027(6) 7_554 ?
Cu6 N2_5 2.028(5) . ?
Cu6 N2_4 2.033(5) . ?
Cu6 N2_6 2.043(5) 7_554 ?
O1 H1 0.8200 . ?
O2 H2 0.8200 . ?
O3 H3 0.8200 . ?
O4 H4 0.8200 . ?
O5 H5 0.8200 . ?
O6 H6 0.8200 . ?
O7 H7 0.8200 . ?
O8 H8 0.8200 . ?
C1_1 N1_1 1.349(9) . ?
C1_1 C2_1 1.375(9) . ?
C1_1 H1_1 0.9300 . ?
C2_1 C3_1 1.396(9) . ?
C2_1 H2_1 0.9300 . ?
C3_1 C4_1 1.390(10) . ?
C3_1 C6_1 1.492(9) . ?
C4_1 C5_1 1.392(9) . ?
C4_1 H4_1 0.9300 . ?
C5_1 N1_1 1.341(8) . ?
C5_1 H5_1 0.9300 . ?
C6_1 C11_1 1.385(10) . ?
C6_1 C7_1 1.388(10) . ?
C7_1 C8_1 1.406(9) . ?
C7_1 H7_1 0.9300 . ?
C8_1 C9_1 1.394(10) . ?
C8_1 H8_1 0.9300 . ?
C9_1 C10_1 1.400(10) . ?
C9_1 C12_1 1.496(9) . ?
C10_1 C11_1 1.412(9) . ?
C10_1 H10_1 0.9300 . ?
C11_1 H11_1 0.9300 . ?
C12_1 C16_1 1.386(9) . ?
C12_1 C13_1 1.389(10) . ?
C13_1 C14_1 1.375(9) . ?
C13_1 H13_1 0.9300 . ?
C14_1 N2_1 1.339(9) . ?
C14_1 H14_1 0.9300 . ?
C15_1 N2_1 1.361(8) . ?
C15_1 C16_1 1.362(9) . ?
C15_1 H15_1 0.9300 . ?
C16_1 H16_1 0.9300 . ?
C1_2 N1_2 1.344(9) . ?
C1_2 C2_2 1.374(9) . ?
C1_2 H1_2 0.9300 . ?
C2_2 C3_2 1.401(10) . ?
C2_2 H2_2 0.9300 . ?
C3_2 C4_2 1.367(10) . ?
C3_2 C6_2 1.492(9) . ?
C4_2 C5_2 1.382(9) . ?
C4_2 H4_2 0.9300 . ?
C5_2 N1_2 1.350(9) . ?
C5_2 H5_2 0.9300 . ?
C6_2 C11_2 1.402(10) . ?
C6_2 C7_2 1.411(10) . ?
C7_2 C8_2 1.392(9) . ?
C7_2 H7_2 0.9300 . ?
C8_2 C9_2 1.386(9) . ?
C8_2 H8_2 0.9300 . ?
C9_2 C10_2 1.393(10) . ?
C9_2 C12_2 1.501(9) . ?
C10_2 C11_2 1.405(9) . ?
C10_2 H10_2 0.9300 . ?
C11_2 H11_2 0.9300 . ?
C12_2 C13_2 1.386(10) . ?
C12_2 C16_2 1.413(9) . ?
C13_2 C14_2 1.385(9) . ?
C13_2 H13_2 0.9300 . ?
C14_2 N2_2 1.341(9) . ?
C14_2 H14_2 0.9300 . ?
C15_2 N2_2 1.350(9) . ?
C15_2 C16_2 1.368(9) . ?
C15_2 H15_2 0.9300 . ?
C16_2 H16_2 0.9300 . ?
C1_3 N1_3 1.345(9) . ?
C1_3 C2_3 1.358(10) . ?
C1_3 H1_3 0.9300 . ?
C2_3 C3_3 1.416(10) . ?
C2_3 H2_3 0.9300 . ?
C3_3 C4_3 1.377(10) . ?
C3_3 C6_3 1.476(9) . ?
C4_3 C5_3 1.382(9) . ?
C4_3 H4_3 0.9300 . ?
C5_3 N1_3 1.334(9) . ?
C5_3 H5_3 0.9300 . ?
C6_3 C11_3 1.389(11) . ?
C6_3 C7_3 1.401(10) . ?
C7_3 C8_3 1.402(9) . ?
C7_3 H7_3 0.9300 . ?
C8_3 C9_3 1.398(10) . ?
C8_3 H8_3 0.9300 . ?
C9_3 C10_3 1.391(10) . ?
C9_3 C12_3 1.486(9) . ?
C10_3 C11_3 1.398(10) . ?
C10_3 H10_3 0.9300 . ?
C11_3 H11_3 0.9300 . ?
C12_3 C13_3 1.384(10) . ?
C12_3 C16_3 1.409(10) . ?
C13_3 C14_3 1.389(10) . ?
C13_3 H13_3 0.9300 . ?
C14_3 N2_3 1.345(9) . ?
C14_3 H14_3 0.9300 . ?
C15_3 N2_3 1.357(9) . ?
C15_3 C16_3 1.377(9) . ?
C15_3 H15_3 0.9300 . ?
C16_3 H16_3 0.9300 . ?
C1_4 C2_4 1.359(10) . ?
C1_4 N1_4 1.360(9) . ?
C1_4 H1_4 0.9300 . ?
C2_4 C3_4 1.400(10) . ?
C2_4 H2_4 0.9300 . ?
C3_4 C4_4 1.426(9) . ?
C3_4 C6_4 1.462(9) . ?
C4_4 C5_4 1.385(9) . ?
C4_4 H4_4 0.9300 . ?
C5_4 N1_4 1.370(9) . ?
C5_4 H5_4 0.9300 . ?
C6_4 C11_4 1.397(10) . ?
C6_4 C7_4 1.417(9) . ?
C7_4 C8_4 1.357(9) . ?
C7_4 H7_4 0.9300 . ?
C8_4 C9_4 1.410(10) . ?
C8_4 H8_4 0.9300 . ?
C9_4 C10_4 1.410(10) . ?
C9_4 C12_4 1.477(9) . ?
C10_4 C11_4 1.382(9) . ?
C10_4 H10_4 0.9300 . ?
C11_4 H11_4 0.9300 . ?
C12_4 C13_4 1.381(10) . ?
C12_4 C16_4 1.395(10) . ?
C13_4 C14_4 1.396(9) . ?
C13_4 H13_4 0.9300 . ?
C14_4 N2_4 1.347(9) . ?
C14_4 H14_4 0.9300 . ?
C15_4 N2_4 1.341(9) . ?
C15_4 C16_4 1.395(9) . ?
C15_4 H15_4 0.9300 . ?
C16_4 H16_4 0.9300 . ?
C1_5 N1_5 1.358(9) . ?
C1_5 C2_5 1.363(9) . ?
C1_5 H1_5 0.9300 . ?
C2_5 C3_5 1.407(9) . ?
C2_5 H2_5 0.9300 . ?
C3_5 C4_5 1.410(9) . ?
C3_5 C6_5 1.457(9) . ?
C4_5 C5_5 1.384(9) . ?
C4_5 H4_5 0.9300 . ?
C5_5 N1_5 1.368(8) . ?
C5_5 H5_5 0.9300 . ?
C6_5 C7_5 1.395(10) . ?
C6_5 C11_5 1.404(9) . ?
C7_5 C8_5 1.375(9) . ?
C7_5 H7_5 0.9300 . ?
C8_5 C9_5 1.400(10) . ?
C8_5 H8_5 0.9300 . ?
C9_5 C10_5 1.405(9) . ?
C9_5 C12_5 1.467(9) . ?
C10_5 C11_5 1.385(9) . ?
C10_5 H10_5 0.9300 . ?
C11_5 H11_5 0.9300 . ?
C12_5 C16_5 1.405(9) . ?
C12_5 C13_5 1.413(10) . ?
C13_5 C14_5 1.382(9) . ?
C13_5 H13_5 0.9300 . ?
C14_5 N2_5 1.343(9) . ?
C14_5 H14_5 0.9300 . ?
C15_5 N2_5 1.343(9) . ?
C15_5 C16_5 1.381(9) . ?
C15_5 H15_5 0.9300 . ?
C16_5 H16_5 0.9300 . ?
C1_6 N1_6 1.343(8) . ?
C1_6 C2_6 1.376(9) . ?
C1_6 H1_6 0.9300 . ?
C2_6 C3_6 1.412(10) . ?
C2_6 H2_6 0.9300 . ?
C3_6 C4_6 1.391(9) . ?
C3_6 C6_6 1.477(9) . ?
C4_6 C5_6 1.386(9) . ?
C4_6 H4_6 0.9300 . ?
C5_6 N1_6 1.351(8) . ?
C5_6 H5_6 0.9300 . ?
C6_6 C7_6 1.397(10) . ?
C6_6 C11_6 1.408(9) . ?
C7_6 C8_6 1.381(10) . ?
C7_6 H7_6 0.9300 . ?
C8_6 C9_6 1.398(10) . ?
C8_6 H8_6 0.9300 . ?
C9_6 C10_6 1.385(10) . ?
C9_6 C12_6 1.485(9) . ?
C10_6 C11_6 1.375(9) . ?
C10_6 H10_6 0.9300 . ?
C11_6 H11_6 0.9300 . ?
C12_6 C16_6 1.390(10) . ?
C12_6 C13_6 1.411(9) . ?
C13_6 C14_6 1.373(9) . ?
C13_6 H13_6 0.9300 . ?
C14_6 N2_6 1.339(9) . ?
C14_6 H14_6 0.9300 . ?
C15_6 N2_6 1.333(9) . ?
C15_6 C16_6 1.391(9) . ?
C15_6 H15_6 0.9300 . ?
C16_6 H16_6 0.9300 . ?
C1_8 N1_8 1.328(9) . ?
C1_8 C2_8 1.399(9) . ?
C1_8 H1_8 0.9300 . ?
C2_8 C3_8 1.403(10) . ?
C2_8 H2_8 0.9300 . ?
C3_8 C4_8 1.420(10) . ?
C3_8 C6_8 1.480(9) . ?
C4_8 C5_8 1.385(9) . ?
C4_8 H4_8 0.9300 . ?
C5_8 N1_8 1.353(9) . ?
C5_8 H5_8 0.9300 . ?
C6_8 C11_8 1.379(10) . ?
C6_8 C7_8 1.398(10) . ?
C7_8 C8_8 1.385(10) . ?
C7_8 H7_8 0.9300 . ?
C8_8 C9_8 1.400(10) . ?
C8_8 H8_8 0.9300 . ?
C9_8 C10_8 1.425(10) . ?
C9_8 C12_8 1.471(9) . ?
C10_8 C11_8 1.368(10) . ?
C10_8 H10_8 0.9300 . ?
C11_8 H11_8 0.9300 . ?
C12_8 C16_8 1.387(10) . ?
C12_8 C13_8 1.403(10) . ?
C13_8 C14_8 1.408(9) . ?
C13_8 H13_8 0.9300 . ?
C14_8 N2_8 1.331(8) . ?
C14_8 H14_8 0.9300 . ?
C15_8 N2_8 1.347(8) . ?
C15_8 C16_8 1.395(9) . ?
C15_8 H15_8 0.9300 . ?
C16_8 H16_8 0.9300 . ?
C1_9 N1_9 1.318(8) . ?
C1_9 C2_9 1.388(9) . ?
C1_9 H1_9 0.9300 . ?
C2_9 C3_9 1.379(9) . ?
C2_9 H2_9 0.9300 . ?
C3_9 C4_9 1.401(9) . ?
C3_9 C6_9 1.484(9) . ?
C4_9 C5_9 1.373(9) . ?
C4_9 H4_9 0.9300 . ?
C5_9 N1_9 1.344(8) . ?
C5_9 H5_9 0.9300 . ?
C6_9 C11_9 1.407(9) . ?
C6_9 C7_9 1.408(9) . ?
C7_9 C8_9 1.401(9) . ?
C7_9 H7_9 0.9300 . ?
C8_9 C9_9 1.397(10) . ?
C8_9 H8_9 0.9300 . ?
C9_9 C10_9 1.398(10) . ?
C9_9 C12_9 1.497(9) . ?
C10_9 C11_9 1.392(9) . ?
C10_9 H10_9 0.9300 . ?
C11_9 H11_9 0.9300 . ?
C12_9 C16_9 1.391(10) . ?
C12_9 C13_9 1.394(9) . ?
C13_9 C14_9 1.395(9) . ?
C13_9 H13_9 0.9300 . ?
C14_9 N2_9 1.359(9) . ?
C14_9 H14_9 0.9300 . ?
C15_9 N2_9 1.351(9) . ?
C15_9 C16_9 1.379(9) . ?
C15_9 H15_9 0.9300 . ?
C16_9 H16_9 0.9300 . ?
B1_10 B4_10 1.750(12) . ?
B1_10 B3_10 1.770(12) . ?
B1_10 B6_10 1.779(12) . ?
B1_10 B2_10 1.797(11) . ?
B1_10 B5_10 1.802(12) . ?
B1_10 Cl1_10 1.811(8) . ?
B2_10 B10_10 1.784(12) . ?
B2_10 B3_10 1.790(12) . ?
B2_10 B5_10 1.794(12) . ?
B2_10 B11_10 1.796(12) . ?
B2_10 Cl3_10 1.806(8) . ?
B3_10 B4_10 1.778(11) . ?
B3_10 Cl4_10 1.785(8) . ?
B3_10 B9_10 1.788(11) . ?
B3_10 B10_10 1.809(12) . ?
B4_10 B6_10 1.776(13) . ?
B4_10 B8_10 1.779(12) . ?
B4_10 Cl6_10 1.800(8) . ?
B4_10 B9_10 1.805(11) . ?
B5_10 Cl2_10 1.773(9) . ?
B5_10 B7_10 1.779(11) . ?
B5_10 B6_10 1.789(12) . ?
B5_10 B11_10 1.807(12) . ?
B6_10 B7_10 1.786(12) . ?
B6_10 B8_10 1.788(12) . ?
B6_10 Cl5_10 1.792(8) . ?
B7_10 Cl11_10 1.768(8) . ?
B7_10 B11_10 1.783(12) . ?
B7_10 B12_10 1.815(12) . ?
B7_10 B8_10 1.818(12) . ?
B8_10 B12_10 1.783(11) . ?
B8_10 B9_10 1.788(12) . ?
B8_10 Cl12_10 1.803(8) . ?
B9_10 B12_10 1.777(11) . ?
B9_10 Cl7_10 1.786(8) . ?
B9_10 B10_10 1.792(11) . ?
B10_10 Cl8_10 1.781(8) . ?
B10_10 B12_10 1.797(12) . ?
B10_10 B11_10 1.804(12) . ?
B11_10 B12_10 1.788(12) . ?
B11_10 Cl10_10 1.796(8) . ?
B12_10 Cl9_10 1.803(8) . ?
B1_11 B5_11 1.768(12) . ?
B1_11 B6_11 1.769(13) . ?
B1_11 B2_11 1.775(12) . ?
B1_11 B4_11 1.797(12) . ?
B1_11 Cl1_11 1.799(9) . ?
B1_11 B3_11 1.807(13) . ?
B2_11 B3_11 1.788(11) . ?
B2_11 B11_11 1.793(12) . ?
B2_11 B6_11 1.803(12) . ?
B2_11 B7_11 1.804(12) . ?
B2_11 Cl6_11 1.804(8) . ?
B3_11 B11_11 1.775(12) . ?
B3_11 B10_11 1.789(11) . ?
B3_11 Cl2_11 1.793(9) . ?
B3_11 B4_11 1.800(12) . ?
B4_11 B5_11 1.780(12) . ?
B4_11 B9_11 1.781(12) . ?
B4_11 B10_11 1.785(12) . ?
B4_11 Cl3_11 1.788(8) . ?
B5_11 B6_11 1.785(12) . ?
B5_11 Cl4_11 1.787(8) . ?
B5_11 B9_11 1.791(12) . ?
B5_11 B8_11 1.795(12) . ?
B6_11 B8_11 1.788(12) . ?
B6_11 Cl5_11 1.797(8) . ?
B6_11 B7_11 1.812(12) . ?
B7_11 Cl7_11 1.778(8) . ?
B7_11 B11_11 1.787(12) . ?
B7_11 B12_11 1.790(11) . ?
B7_11 B8_11 1.806(12) . ?
B8_11 B12_11 1.776(12) . ?
B8_11 B9_11 1.792(11) . ?
B8_11 Cl8_11 1.799(9) . ?
B9_11 B10_11 1.781(12) . ?
B9_11 Cl9_11 1.800(8) . ?
B9_11 B12_11 1.800(11) . ?
B10_11 B11_11 1.786(11) . ?
B10_11 Cl10_11 1.795(8) . ?
B10_11 B12_11 1.801(12) . ?
B11_11 B12_11 1.782(12) . ?
B11_11 Cl11_11 1.797(8) . ?
B12_11 Cl12_11 1.800(8) . ?
B1_12 B2_12 1.741(13) . ?
B1_12 B3_12 1.770(12) . ?
B1_12 B4_12 1.782(12) . ?
B1_12 B5_12 1.794(13) . ?
B1_12 Cl1_12 1.804(8) . ?
B1_12 B6_12 1.817(13) . ?
B2_12 B3_12 1.778(13) . ?
B2_12 B4_12 1.781(13) . ?
B2_12 B11_12 1.793(13) . ?
B2_12 Cl2_12 1.804(9) . ?
B2_12 B10_12 1.821(12) . ?
B3_12 B5_12 1.774(13) . ?
B3_12 B11_12 1.779(13) . ?
B3_12 Cl3_12 1.792(9) . ?
B3_12 B9_12 1.803(13) . ?
B4_12 B6_12 1.780(13) . ?
B4_12 B8_12 1.781(12) . ?
B4_12 B10_12 1.807(12) . ?
B4_12 Cl4_12 1.809(8) . ?
B5_12 Cl5_12 1.784(9) . ?
B5_12 B9_12 1.792(13) . ?
B5_12 B6_12 1.804(12) . ?
B5_12 B7_12 1.805(14) . ?
B6_12 B8_12 1.764(13) . ?
B6_12 B7_12 1.783(13) . ?
B6_12 Cl6_12 1.792(10) . ?
B7_12 B8_12 1.783(13) . ?
B7_12 B12_12 1.785(14) . ?
B7_12 Cl7_12 1.785(9) . ?
B7_12 B9_12 1.808(13) . ?
B8_12 Cl8_12 1.790(9) . ?
B8_12 B10_12 1.790(13) . ?
B8_12 B12_12 1.823(13) . ?
B9_12 Cl11_12 1.775(9) . ?
B9_12 B11_12 1.792(13) . ?
B9_12 B12_12 1.794(14) . ?
B10_12 B11_12 1.780(13) . ?
B10_12 Cl9_12 1.788(9) . ?
B10_12 B12_12 1.792(13) . ?
B11_12 B12_12 1.792(13) . ?
B11_12 Cl10_12 1.804(9) . ?
B12_12 Cl12_12 1.782(8) . ?
B1_13 B3_13 1.767(11) . ?
B1_13 B2_13 1.778(12) . ?
B1_13 B4_13 1.782(11) . ?
B1_13 B5_13 1.790(12) . ?
B1_13 Cl1_13 1.791(8) . ?
B1_13 B6_13 1.809(11) . ?
B2_13 B3_13 1.755(12) . ?
B2_13 B6_13 1.762(12) . ?
B2_13 B12_13 1.784(12) . ?
B2_13 B11_13 1.803(11) . ?
B2_13 Cl6_13 1.821(8) . ?
B3_13 B11_13 1.788(11) . ?
B3_13 Cl5_13 1.794(8) . ?
B3_13 B4_13 1.803(11) . ?
B3_13 B10_13 1.805(11) . ?
B4_13 B8_13 1.783(11) . ?
B4_13 B10_13 1.785(11) . ?
B4_13 B5_13 1.788(11) . ?
B4_13 Cl4_13 1.797(8) . ?
B5_13 Cl3_13 1.777(8) . ?
B5_13 B8_13 1.811(11) . ?
B5_13 B6_13 1.817(11) . ?
B5_13 B7_13 1.820(12) . ?
B6_13 B12_13 1.779(12) . ?
B6_13 Cl2_13 1.792(8) . ?
B6_13 B7_13 1.807(12) . ?
B7_13 Cl12_13 1.783(8) . ?
B7_13 B9_13 1.788(12) . ?
B7_13 B12_13 1.797(12) . ?
B7_13 B8_13 1.803(12) . ?
B8_13 B10_13 1.780(11) . ?
B8_13 Cl11_13 1.784(8) . ?
B8_13 B9_13 1.795(11) . ?
B9_13 Cl10_13 1.793(8) . ?
B9_13 B10_13 1.794(11) . ?
B9_13 B11_13 1.804(12) . ?
B9_13 B12_13 1.820(11) . ?
B10_13 B11_13 1.791(11) . ?
B10_13 Cl9_13 1.810(8) . ?
B11_13 Cl7_13 1.782(8) . ?
B11_13 B12_13 1.814(11) . ?
B12_13 Cl8_13 1.778(8) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O1 C1 H1A 109.5 . . ?
O1 C1 H1B 109.5 . . ?
H1A C1 H1B 109.5 . . ?
O1 C1 H1C 109.5 . . ?
H1A C1 H1C 109.5 . . ?
H1B C1 H1C 109.5 . . ?
O6 C6 H6A 109.5 . . ?
O6 C6 H6B 109.5 . . ?
H6A C6 H6B 109.5 . . ?
O6 C6 H6C 109.5 . . ?
H6A C6 H6C 109.5 . . ?
H6B C6 H6C 109.5 . . ?
O2 C9 H9A 109.5 . . ?
O2 C9 H9B 109.5 . . ?
H9A C9 H9B 109.5 . . ?
O2 C9 H9C 109.5 . . ?
H9A C9 H9C 109.5 . . ?
H9B C9 H9C 109.5 . . ?
O3 C12 H12A 109.5 . . ?
O3 C12 H12B 109.5 . . ?
H12A C12 H12B 109.5 . . ?
O3 C12 H12C 109.5 . . ?
H12A C12 H12C 109.5 . . ?
H12B C12 H12C 109.5 . . ?
O4 C13 H13A 109.5 . . ?
O4 C13 H13B 109.5 . . ?
H13A C13 H13B 109.5 . . ?
O4 C13 H13C 109.5 . . ?
H13A C13 H13C 109.5 . . ?
H13B C13 H13C 109.5 . . ?
O5 C14 H14A 109.5 . . ?
O5 C14 H14B 109.5 . . ?
H14A C14 H14B 109.5 . . ?
O5 C14 H14C 109.5 . . ?
H14A C14 H14C 109.5 . . ?
H14B C14 H14C 109.5 . . ?
O8 C16 H16A 109.5 . . ?
O8 C16 H16B 109.5 . . ?
H16A C16 H16B 109.5 . . ?
O8 C16 H16C 109.5 . . ?
H16A C16 H16C 109.5 . . ?
H16B C16 H16C 109.5 . . ?
O7 C17 H17A 109.5 . . ?
O7 C17 H17B 109.5 . . ?
H17A C17 H17B 109.5 . . ?
O7 C17 H17C 109.5 . . ?
H17A C17 H17C 109.5 . . ?
H17B C17 H17C 109.5 . . ?
N1_3 Cu1 N1_3 90.1(3) . 2_655 ?
N1_3 Cu1 N1_1 179.0(2) . 2_655 ?
N1_3 Cu1 N1_1 89.9(2) 2_655 2_655 ?
N1_3 Cu1 N1_1 89.9(2) . . ?
N1_3 Cu1 N1_1 179.0(2) 2_655 . ?
N1_1 Cu1 N1_1 90.2(3) 2_655 . ?
N2_2 Cu2 N2_2 90.1(3) . 2_565 ?
N2_2 Cu2 N1_9 177.7(2) . 2_565 ?
N2_2 Cu2 N1_9 89.7(2) 2_565 2_565 ?
N2_2 Cu2 N1_9 89.7(2) . . ?
N2_2 Cu2 N1_9 177.7(2) 2_565 . ?
N1_9 Cu2 N1_9 90.6(3) 2_565 . ?
N1_4 Cu3 N1_4 89.0(3) . 2_665 ?
N1_4 Cu3 N1_6 90.6(2) . . ?
N1_4 Cu3 N1_6 176.9(2) 2_665 . ?
N1_4 Cu3 N1_6 176.9(2) . 2_665 ?
N1_4 Cu3 N1_6 90.6(2) 2_665 2_665 ?
N1_6 Cu3 N1_6 90.0(3) . 2_665 ?
N1_5 Cu4 N1_5 89.8(3) . 2 ?
N1_5 Cu4 N2_8 178.7(2) . 2 ?
N1_5 Cu4 N2_8 90.3(2) 2 2 ?
N1_5 Cu4 N2_8 90.3(2) . . ?
N1_5 Cu4 N2_8 178.7(2) 2 . ?
N2_8 Cu4 N2_8 89.6(3) 2 . ?
N2_9 Cu5 N2_1 175.7(2) . 7_554 ?
N2_9 Cu5 N2_3 89.8(2) . . ?
N2_1 Cu5 N2_3 89.3(2) 7_554 . ?
N2_9 Cu5 N1_2 89.6(2) . 7_554 ?
N2_1 Cu5 N1_2 91.3(2) 7_554 7_554 ?
N2_3 Cu5 N1_2 178.4(2) . 7_554 ?
N1_8 Cu6 N2_5 174.6(2) 7_554 . ?
N1_8 Cu6 N2_4 88.8(2) 7_554 . ?
N2_5 Cu6 N2_4 91.5(2) . . ?
N1_8 Cu6 N2_6 91.4(2) 7_554 7_554 ?
N2_5 Cu6 N2_6 88.5(2) . 7_554 ?
N2_4 Cu6 N2_6 178.0(2) . 7_554 ?
C1 O1 H1 109.5 . . ?
C9 O2 H2 109.5 . . ?
C12 O3 H3 109.5 . . ?
C13 O4 H4 109.5 . . ?
C14 O5 H5 109.5 . . ?
C6 O6 H6 109.5 . . ?
C17 O7 H7 109.5 . . ?
C16 O8 H8 109.5 . . ?
N1_1 C1_1 C2_1 122.0(6) . . ?
N1_1 C1_1 H1_1 119.0 . . ?
C2_1 C1_1 H1_1 119.0 . . ?
C1_1 C2_1 C3_1 120.8(6) . . ?
C1_1 C2_1 H2_1 119.6 . . ?
C3_1 C2_1 H2_1 119.6 . . ?
C4_1 C3_1 C2_1 116.4(6) . . ?
C4_1 C3_1 C6_1 122.5(6) . . ?
C2_1 C3_1 C6_1 121.1(6) . . ?
C3_1 C4_1 C5_1 120.4(6) . . ?
C3_1 C4_1 H4_1 119.8 . . ?
C5_1 C4_1 H4_1 119.8 . . ?
N1_1 C5_1 C4_1 121.9(6) . . ?
N1_1 C5_1 H5_1 119.0 . . ?
C4_1 C5_1 H5_1 119.0 . . ?
C11_1 C6_1 C7_1 121.1(6) . . ?
C11_1 C6_1 C3_1 119.1(6) . . ?
C7_1 C6_1 C3_1 119.8(6) . . ?
C6_1 C7_1 C8_1 120.1(7) . . ?
C6_1 C7_1 H7_1 120.0 . . ?
C8_1 C7_1 H7_1 120.0 . . ?
C9_1 C8_1 C7_1 119.6(7) . . ?
C9_1 C8_1 H8_1 120.2 . . ?
C7_1 C8_1 H8_1 120.2 . . ?
C8_1 C9_1 C10_1 119.9(6) . . ?
C8_1 C9_1 C12_1 120.8(6) . . ?
C10_1 C9_1 C12_1 119.3(6) . . ?
C9_1 C10_1 C11_1 120.3(7) . . ?
C9_1 C10_1 H10_1 119.9 . . ?
C11_1 C10_1 H10_1 119.9 . . ?
C6_1 C11_1 C10_1 119.0(7) . . ?
C6_1 C11_1 H11_1 120.5 . . ?
C10_1 C11_1 H11_1 120.5 . . ?
C16_1 C12_1 C13_1 117.7(6) . . ?
C16_1 C12_1 C9_1 120.4(6) . . ?
C13_1 C12_1 C9_1 121.9(6) . . ?
C14_1 C13_1 C12_1 119.3(7) . . ?
C14_1 C13_1 H13_1 120.3 . . ?
C12_1 C13_1 H13_1 120.3 . . ?
N2_1 C14_1 C13_1 123.1(7) . . ?
N2_1 C14_1 H14_1 118.5 . . ?
C13_1 C14_1 H14_1 118.5 . . ?
N2_1 C15_1 C16_1 122.4(6) . . ?
N2_1 C15_1 H15_1 118.8 . . ?
C16_1 C15_1 H15_1 118.8 . . ?
C15_1 C16_1 C12_1 120.1(6) . . ?
C15_1 C16_1 H16_1 120.0 . . ?
C12_1 C16_1 H16_1 120.0 . . ?
C5_1 N1_1 C1_1 118.5(6) . . ?
C5_1 N1_1 Cu1 121.8(5) . . ?
C1_1 N1_1 Cu1 119.5(4) . . ?
C14_1 N2_1 C15_1 117.4(6) . . ?
C14_1 N2_1 Cu5 123.7(5) . 7 ?
C15_1 N2_1 Cu5 118.5(4) . 7 ?
N1_2 C1_2 C2_2 124.7(7) . . ?
N1_2 C1_2 H1_2 117.6 . . ?
C2_2 C1_2 H1_2 117.6 . . ?
C1_2 C2_2 C3_2 118.1(7) . . ?
C1_2 C2_2 H2_2 121.0 . . ?
C3_2 C2_2 H2_2 121.0 . . ?
C4_2 C3_2 C2_2 117.7(6) . . ?
C4_2 C3_2 C6_2 120.8(6) . . ?
C2_2 C3_2 C6_2 121.5(6) . . ?
C3_2 C4_2 C5_2 120.9(7) . . ?
C3_2 C4_2 H4_2 119.5 . . ?
C5_2 C4_2 H4_2 119.5 . . ?
N1_2 C5_2 C4_2 122.1(7) . . ?
N1_2 C5_2 H5_2 118.9 . . ?
C4_2 C5_2 H5_2 118.9 . . ?
C11_2 C6_2 C7_2 119.6(6) . . ?
C11_2 C6_2 C3_2 121.4(6) . . ?
C7_2 C6_2 C3_2 119.0(6) . . ?
C8_2 C7_2 C6_2 120.2(7) . . ?
C8_2 C7_2 H7_2 119.9 . . ?
C6_2 C7_2 H7_2 119.9 . . ?
C9_2 C8_2 C7_2 119.7(7) . . ?
C9_2 C8_2 H8_2 120.1 . . ?
C7_2 C8_2 H8_2 120.1 . . ?
C8_2 C9_2 C10_2 121.1(6) . . ?
C8_2 C9_2 C12_2 119.5(6) . . ?
C10_2 C9_2 C12_2 119.4(6) . . ?
C9_2 C10_2 C11_2 119.6(6) . . ?
C9_2 C10_2 H10_2 120.2 . . ?
C11_2 C10_2 H10_2 120.2 . . ?
C6_2 C11_2 C10_2 119.8(6) . . ?
C6_2 C11_2 H11_2 120.1 . . ?
C10_2 C11_2 H11_2 120.1 . . ?
C13_2 C12_2 C16_2 116.7(6) . . ?
C13_2 C12_2 C9_2 121.8(6) . . ?
C16_2 C12_2 C9_2 121.4(6) . . ?
C14_2 C13_2 C12_2 120.4(6) . . ?
C14_2 C13_2 H13_2 119.8 . . ?
C12_2 C13_2 H13_2 119.8 . . ?
N2_2 C14_2 C13_2 122.1(6) . . ?
N2_2 C14_2 H14_2 119.0 . . ?
C13_2 C14_2 H14_2 119.0 . . ?
N2_2 C15_2 C16_2 122.4(7) . . ?
N2_2 C15_2 H15_2 118.8 . . ?
C16_2 C15_2 H15_2 118.8 . . ?
C15_2 C16_2 C12_2 119.9(7) . . ?
C15_2 C16_2 H16_2 120.0 . . ?
C12_2 C16_2 H16_2 120.0 . . ?
C1_2 N1_2 C5_2 116.4(6) . . ?
C1_2 N1_2 Cu5 124.4(5) . 7 ?
C5_2 N1_2 Cu5 118.8(4) . 7 ?
C14_2 N2_2 C15_2 118.5(6) . . ?
C14_2 N2_2 Cu2 121.0(5) . . ?
C15_2 N2_2 Cu2 119.9(5) . . ?
N1_3 C1_3 C2_3 122.8(7) . . ?
N1_3 C1_3 H1_3 118.6 . . ?
C2_3 C1_3 H1_3 118.6 . . ?
C1_3 C2_3 C3_3 119.8(7) . . ?
C1_3 C2_3 H2_3 120.1 . . ?
C3_3 C2_3 H2_3 120.1 . . ?
C4_3 C3_3 C2_3 116.5(6) . . ?
C4_3 C3_3 C6_3 121.0(6) . . ?
C2_3 C3_3 C6_3 122.5(6) . . ?
C3_3 C4_3 C5_3 120.6(7) . . ?
C3_3 C4_3 H4_3 119.7 . . ?
C5_3 C4_3 H4_3 119.7 . . ?
N1_3 C5_3 C4_3 122.0(7) . . ?
N1_3 C5_3 H5_3 119.0 . . ?
C4_3 C5_3 H5_3 119.0 . . ?
C11_3 C6_3 C7_3 118.2(6) . . ?
C11_3 C6_3 C3_3 118.2(6) . . ?
C7_3 C6_3 C3_3 123.6(7) . . ?
C6_3 C7_3 C8_3 120.6(7) . . ?
C6_3 C7_3 H7_3 119.7 . . ?
C8_3 C7_3 H7_3 119.7 . . ?
C9_3 C8_3 C7_3 120.1(7) . . ?
C9_3 C8_3 H8_3 119.9 . . ?
C7_3 C8_3 H8_3 119.9 . . ?
C10_3 C9_3 C8_3 119.6(6) . . ?
C10_3 C9_3 C12_3 118.1(7) . . ?
C8_3 C9_3 C12_3 122.2(7) . . ?
C9_3 C10_3 C11_3 119.5(7) . . ?
C9_3 C10_3 H10_3 120.2 . . ?
C11_3 C10_3 H10_3 120.2 . . ?
C6_3 C11_3 C10_3 121.8(7) . . ?
C6_3 C11_3 H11_3 119.1 . . ?
C10_3 C11_3 H11_3 119.1 . . ?
C13_3 C12_3 C16_3 117.4(7) . . ?
C13_3 C12_3 C9_3 122.1(7) . . ?
C16_3 C12_3 C9_3 120.5(6) . . ?
C12_3 C13_3 C14_3 120.1(7) . . ?
C12_3 C13_3 H13_3 120.0 . . ?
C14_3 C13_3 H13_3 120.0 . . ?
N2_3 C14_3 C13_3 122.7(7) . . ?
N2_3 C14_3 H14_3 118.7 . . ?
C13_3 C14_3 H14_3 118.7 . . ?
N2_3 C15_3 C16_3 123.2(7) . . ?
N2_3 C15_3 H15_3 118.4 . . ?
C16_3 C15_3 H15_3 118.4 . . ?
C15_3 C16_3 C12_3 119.2(7) . . ?
C15_3 C16_3 H16_3 120.4 . . ?
C12_3 C16_3 H16_3 120.4 . . ?
C5_3 N1_3 C1_3 118.4(6) . . ?
C5_3 N1_3 Cu1 118.0(5) . . ?
C1_3 N1_3 Cu1 123.4(5) . . ?
C14_3 N2_3 C15_3 117.3(6) . . ?
C14_3 N2_3 Cu5 121.9(5) . . ?
C15_3 N2_3 Cu5 120.0(5) . . ?
C2_4 C1_4 N1_4 124.1(7) . . ?
C2_4 C1_4 H1_4 117.9 . . ?
N1_4 C1_4 H1_4 117.9 . . ?
C1_4 C2_4 C3_4 120.6(7) . . ?
C1_4 C2_4 H2_4 119.7 . . ?
C3_4 C2_4 H2_4 119.7 . . ?
C2_4 C3_4 C4_4 116.2(6) . . ?
C2_4 C3_4 C6_4 123.1(6) . . ?
C4_4 C3_4 C6_4 120.7(6) . . ?
C5_4 C4_4 C3_4 119.9(6) . . ?
C5_4 C4_4 H4_4 120.0 . . ?
C3_4 C4_4 H4_4 120.0 . . ?
N1_4 C5_4 C4_4 122.6(6) . . ?
N1_4 C5_4 H5_4 118.7 . . ?
C4_4 C5_4 H5_4 118.7 . . ?
C11_4 C6_4 C7_4 118.4(6) . . ?
C11_4 C6_4 C3_4 120.9(6) . . ?
C7_4 C6_4 C3_4 120.6(6) . . ?
C8_4 C7_4 C6_4 120.3(7) . . ?
C8_4 C7_4 H7_4 119.8 . . ?
C6_4 C7_4 H7_4 119.8 . . ?
C7_4 C8_4 C9_4 122.0(7) . . ?
C7_4 C8_4 H8_4 119.0 . . ?
C9_4 C8_4 H8_4 119.0 . . ?
C8_4 C9_4 C10_4 117.5(6) . . ?
C8_4 C9_4 C12_4 120.2(6) . . ?
C10_4 C9_4 C12_4 122.3(6) . . ?
C11_4 C10_4 C9_4 120.7(6) . . ?
C11_4 C10_4 H10_4 119.7 . . ?
C9_4 C10_4 H10_4 119.7 . . ?
C10_4 C11_4 C6_4 121.0(7) . . ?
C10_4 C11_4 H11_4 119.5 . . ?
C6_4 C11_4 H11_4 119.5 . . ?
C13_4 C12_4 C16_4 118.0(6) . . ?
C13_4 C12_4 C9_4 120.0(6) . . ?
C16_4 C12_4 C9_4 122.0(6) . . ?
C12_4 C13_4 C14_4 120.3(7) . . ?
C12_4 C13_4 H13_4 119.9 . . ?
C14_4 C13_4 H13_4 119.9 . . ?
N2_4 C14_4 C13_4 121.7(6) . . ?
N2_4 C14_4 H14_4 119.1 . . ?
C13_4 C14_4 H14_4 119.1 . . ?
N2_4 C15_4 C16_4 123.1(6) . . ?
N2_4 C15_4 H15_4 118.4 . . ?
C16_4 C15_4 H15_4 118.4 . . ?
C15_4 C16_4 C12_4 118.7(7) . . ?
C15_4 C16_4 H16_4 120.6 . . ?
C12_4 C16_4 H16_4 120.6 . . ?
C1_4 N1_4 C5_4 116.5(6) . . ?
C1_4 N1_4 Cu3 122.1(5) . . ?
C5_4 N1_4 Cu3 120.7(4) . . ?
C15_4 N2_4 C14_4 118.2(6) . . ?
C15_4 N2_4 Cu6 123.4(4) . . ?
C14_4 N2_4 Cu6 118.3(5) . . ?
N1_5 C1_5 C2_5 123.6(7) . . ?
N1_5 C1_5 H1_5 118.2 . . ?
C2_5 C1_5 H1_5 118.2 . . ?
C1_5 C2_5 C3_5 120.9(7) . . ?
C1_5 C2_5 H2_5 119.6 . . ?
C3_5 C2_5 H2_5 119.6 . . ?
C2_5 C3_5 C4_5 115.8(6) . . ?
C2_5 C3_5 C6_5 123.5(6) . . ?
C4_5 C3_5 C6_5 120.7(6) . . ?
C5_5 C4_5 C3_5 120.5(6) . . ?
C5_5 C4_5 H4_5 119.8 . . ?
C3_5 C4_5 H4_5 119.8 . . ?
N1_5 C5_5 C4_5 122.6(6) . . ?
N1_5 C5_5 H5_5 118.7 . . ?
C4_5 C5_5 H5_5 118.7 . . ?
C7_5 C6_5 C11_5 118.1(6) . . ?
C7_5 C6_5 C3_5 121.1(6) . . ?
C11_5 C6_5 C3_5 120.8(6) . . ?
C8_5 C7_5 C6_5 120.9(7) . . ?
C8_5 C7_5 H7_5 119.6 . . ?
C6_5 C7_5 H7_5 119.6 . . ?
C7_5 C8_5 C9_5 122.0(7) . . ?
C7_5 C8_5 H8_5 119.0 . . ?
C9_5 C8_5 H8_5 119.0 . . ?
C8_5 C9_5 C10_5 117.0(6) . . ?
C8_5 C9_5 C12_5 121.7(6) . . ?
C10_5 C9_5 C12_5 121.3(6) . . ?
C11_5 C10_5 C9_5 121.3(7) . . ?
C11_5 C10_5 H10_5 119.3 . . ?
C9_5 C10_5 H10_5 119.3 . . ?
C10_5 C11_5 C6_5 120.7(7) . . ?
C10_5 C11_5 H11_5 119.6 . . ?
C6_5 C11_5 H11_5 119.6 . . ?
C16_5 C12_5 C13_5 117.7(6) . . ?
C16_5 C12_5 C9_5 120.7(6) . . ?
C13_5 C12_5 C9_5 121.7(6) . . ?
C14_5 C13_5 C12_5 118.6(6) . . ?
C14_5 C13_5 H13_5 120.7 . . ?
C12_5 C13_5 H13_5 120.7 . . ?
N2_5 C14_5 C13_5 123.3(6) . . ?
N2_5 C14_5 H14_5 118.3 . . ?
C13_5 C14_5 H14_5 118.3 . . ?
N2_5 C15_5 C16_5 122.8(6) . . ?
N2_5 C15_5 H15_5 118.6 . . ?
C16_5 C15_5 H15_5 118.6 . . ?
C15_5 C16_5 C12_5 119.4(6) . . ?
C15_5 C16_5 H16_5 120.3 . . ?
C12_5 C16_5 H16_5 120.3 . . ?
C1_5 N1_5 C5_5 116.5(6) . . ?
C1_5 N1_5 Cu4 124.0(5) . . ?
C5_5 N1_5 Cu4 119.1(4) . . ?
C14_5 N2_5 C15_5 118.3(6) . . ?
C14_5 N2_5 Cu6 122.1(4) . . ?
C15_5 N2_5 Cu6 119.2(5) . . ?
N1_6 C1_6 C2_6 124.2(6) . . ?
N1_6 C1_6 H1_6 117.9 . . ?
C2_6 C1_6 H1_6 117.9 . . ?
C1_6 C2_6 C3_6 118.8(6) . . ?
C1_6 C2_6 H2_6 120.6 . . ?
C3_6 C2_6 H2_6 120.6 . . ?
C4_6 C3_6 C2_6 117.4(6) . . ?
C4_6 C3_6 C6_6 120.5(6) . . ?
C2_6 C3_6 C6_6 122.1(6) . . ?
C5_6 C4_6 C3_6 119.6(6) . . ?
C5_6 C4_6 H4_6 120.2 . . ?
C3_6 C4_6 H4_6 120.2 . . ?
N1_6 C5_6 C4_6 123.3(6) . . ?
N1_6 C5_6 H5_6 118.4 . . ?
C4_6 C5_6 H5_6 118.4 . . ?
C7_6 C6_6 C11_6 118.5(6) . . ?
C7_6 C6_6 C3_6 120.0(6) . . ?
C11_6 C6_6 C3_6 121.4(6) . . ?
C8_6 C7_6 C6_6 121.0(7) . . ?
C8_6 C7_6 H7_6 119.5 . . ?
C6_6 C7_6 H7_6 119.5 . . ?
C7_6 C8_6 C9_6 119.8(7) . . ?
C7_6 C8_6 H8_6 120.1 . . ?
C9_6 C8_6 H8_6 120.1 . . ?
C10_6 C9_6 C8_6 119.6(6) . . ?
C10_6 C9_6 C12_6 120.9(6) . . ?
C8_6 C9_6 C12_6 119.5(7) . . ?
C11_6 C10_6 C9_6 120.8(7) . . ?
C11_6 C10_6 H10_6 119.6 . . ?
C9_6 C10_6 H10_6 119.6 . . ?
C10_6 C11_6 C6_6 120.3(7) . . ?
C10_6 C11_6 H11_6 119.9 . . ?
C6_6 C11_6 H11_6 119.9 . . ?
C16_6 C12_6 C13_6 116.6(6) . . ?
C16_6 C12_6 C9_6 122.8(6) . . ?
C13_6 C12_6 C9_6 120.6(6) . . ?
C14_6 C13_6 C12_6 119.7(7) . . ?
C14_6 C13_6 H13_6 120.1 . . ?
C12_6 C13_6 H13_6 120.1 . . ?
N2_6 C14_6 C13_6 122.9(7) . . ?
N2_6 C14_6 H14_6 118.5 . . ?
C13_6 C14_6 H14_6 118.5 . . ?
N2_6 C15_6 C16_6 122.7(6) . . ?
N2_6 C15_6 H15_6 118.7 . . ?
C16_6 C15_6 H15_6 118.7 . . ?
C12_6 C16_6 C15_6 119.8(6) . . ?
C12_6 C16_6 H16_6 120.1 . . ?
C15_6 C16_6 H16_6 120.1 . . ?
C1_6 N1_6 C5_6 116.7(6) . . ?
C1_6 N1_6 Cu3 125.2(4) . . ?
C5_6 N1_6 Cu3 118.0(4) . . ?
C15_6 N2_6 C14_6 118.1(6) . . ?
C15_6 N2_6 Cu6 121.1(5) . 7 ?
C14_6 N2_6 Cu6 120.4(4) . 7 ?
N1_8 C1_8 C2_8 123.4(7) . . ?
N1_8 C1_8 H1_8 118.3 . . ?
C2_8 C1_8 H1_8 118.3 . . ?
C1_8 C2_8 C3_8 119.0(7) . . ?
C1_8 C2_8 H2_8 120.5 . . ?
C3_8 C2_8 H2_8 120.5 . . ?
C2_8 C3_8 C4_8 116.7(6) . . ?
C2_8 C3_8 C6_8 122.5(7) . . ?
C4_8 C3_8 C6_8 120.7(6) . . ?
C5_8 C4_8 C3_8 120.3(7) . . ?
C5_8 C4_8 H4_8 119.8 . . ?
C3_8 C4_8 H4_8 119.8 . . ?
N1_8 C5_8 C4_8 121.6(7) . . ?
N1_8 C5_8 H5_8 119.2 . . ?
C4_8 C5_8 H5_8 119.2 . . ?
C11_8 C6_8 C7_8 118.8(7) . . ?
C11_8 C6_8 C3_8 119.6(7) . . ?
C7_8 C6_8 C3_8 121.6(7) . . ?
C8_8 C7_8 C6_8 120.8(7) . . ?
C8_8 C7_8 H7_8 119.6 . . ?
C6_8 C7_8 H7_8 119.6 . . ?
C7_8 C8_8 C9_8 120.6(7) . . ?
C7_8 C8_8 H8_8 119.7 . . ?
C9_8 C8_8 H8_8 119.7 . . ?
C8_8 C9_8 C10_8 117.6(6) . . ?
C8_8 C9_8 C12_8 123.3(7) . . ?
C10_8 C9_8 C12_8 119.0(6) . . ?
C11_8 C10_8 C9_8 120.6(7) . . ?
C11_8 C10_8 H10_8 119.7 . . ?
C9_8 C10_8 H10_8 119.7 . . ?
C10_8 C11_8 C6_8 121.5(7) . . ?
C10_8 C11_8 H11_8 119.2 . . ?
C6_8 C11_8 H11_8 119.2 . . ?
C16_8 C12_8 C13_8 117.9(6) . . ?
C16_8 C12_8 C9_8 119.5(6) . . ?
C13_8 C12_8 C9_8 122.7(6) . . ?
C12_8 C13_8 C14_8 118.1(6) . . ?
C12_8 C13_8 H13_8 120.9 . . ?
C14_8 C13_8 H13_8 120.9 . . ?
N2_8 C14_8 C13_8 123.7(7) . . ?
N2_8 C14_8 H14_8 118.2 . . ?
C13_8 C14_8 H14_8 118.2 . . ?
N2_8 C15_8 C16_8 122.2(6) . . ?
N2_8 C15_8 H15_8 118.9 . . ?
C16_8 C15_8 H15_8 118.9 . . ?
C12_8 C16_8 C15_8 120.2(6) . . ?
C12_8 C16_8 H16_8 119.9 . . ?
C15_8 C16_8 H16_8 119.9 . . ?
C1_8 N1_8 C5_8 118.9(6) . . ?
C1_8 N1_8 Cu6 121.7(5) . 7 ?
C5_8 N1_8 Cu6 118.8(5) . 7 ?
C14_8 N2_8 C15_8 118.0(6) . . ?
C14_8 N2_8 Cu4 122.9(5) . . ?
C15_8 N2_8 Cu4 118.9(4) . . ?
N1_9 C1_9 C2_9 122.5(6) . . ?
N1_9 C1_9 H1_9 118.7 . . ?
C2_9 C1_9 H1_9 118.7 . . ?
C3_9 C2_9 C1_9 119.9(6) . . ?
C3_9 C2_9 H2_9 120.0 . . ?
C1_9 C2_9 H2_9 120.0 . . ?
C2_9 C3_9 C4_9 116.7(6) . . ?
C2_9 C3_9 C6_9 121.2(6) . . ?
C4_9 C3_9 C6_9 122.1(6) . . ?
C5_9 C4_9 C3_9 120.3(7) . . ?
C5_9 C4_9 H4_9 119.8 . . ?
C3_9 C4_9 H4_9 119.8 . . ?
N1_9 C5_9 C4_9 121.6(7) . . ?
N1_9 C5_9 H5_9 119.2 . . ?
C4_9 C5_9 H5_9 119.2 . . ?
C11_9 C6_9 C7_9 120.2(6) . . ?
C11_9 C6_9 C3_9 119.9(6) . . ?
C7_9 C6_9 C3_9 119.8(6) . . ?
C8_9 C7_9 C6_9 119.4(6) . . ?
C8_9 C7_9 H7_9 120.3 . . ?
C6_9 C7_9 H7_9 120.3 . . ?
C9_9 C8_9 C7_9 120.5(6) . . ?
C9_9 C8_9 H8_9 119.7 . . ?
C7_9 C8_9 H8_9 119.7 . . ?
C8_9 C9_9 C10_9 119.4(6) . . ?
C8_9 C9_9 C12_9 120.3(6) . . ?
C10_9 C9_9 C12_9 120.2(6) . . ?
C11_9 C10_9 C9_9 121.1(7) . . ?
C11_9 C10_9 H10_9 119.5 . . ?
C9_9 C10_9 H10_9 119.5 . . ?
C10_9 C11_9 C6_9 119.3(7) . . ?
C10_9 C11_9 H11_9 120.4 . . ?
C6_9 C11_9 H11_9 120.4 . . ?
C16_9 C12_9 C13_9 118.0(6) . . ?
C16_9 C12_9 C9_9 121.2(6) . . ?
C13_9 C12_9 C9_9 120.8(6) . . ?
C12_9 C13_9 C14_9 118.9(7) . . ?
C12_9 C13_9 H13_9 120.5 . . ?
C14_9 C13_9 H13_9 120.5 . . ?
N2_9 C14_9 C13_9 122.6(7) . . ?
N2_9 C14_9 H14_9 118.7 . . ?
C13_9 C14_9 H14_9 118.7 . . ?
N2_9 C15_9 C16_9 122.1(7) . . ?
N2_9 C15_9 H15_9 119.0 . . ?
C16_9 C15_9 H15_9 119.0 . . ?
C15_9 C16_9 C12_9 120.4(7) . . ?
C15_9 C16_9 H16_9 119.8 . . ?
C12_9 C16_9 H16_9 119.8 . . ?
C1_9 N1_9 C5_9 119.0(6) . . ?
C1_9 N1_9 Cu2 117.5(4) . . ?
C5_9 N1_9 Cu2 123.3(5) . . ?
C15_9 N2_9 C14_9 118.0(6) . . ?
C15_9 N2_9 Cu5 121.5(5) . . ?
C14_9 N2_9 Cu5 120.2(5) . . ?
B4_10 B1_10 B3_10 60.7(5) . . ?
B4_10 B1_10 B6_10 60.4(5) . . ?
B3_10 B1_10 B6_10 109.0(6) . . ?
B4_10 B1_10 B2_10 108.4(6) . . ?
B3_10 B1_10 B2_10 60.2(5) . . ?
B6_10 B1_10 B2_10 107.7(6) . . ?
B4_10 B1_10 B5_10 108.7(6) . . ?
B3_10 B1_10 B5_10 108.8(6) . . ?
B6_10 B1_10 B5_10 60.0(5) . . ?
B2_10 B1_10 B5_10 59.8(5) . . ?
B4_10 B1_10 Cl1_10 121.8(5) . . ?
B3_10 B1_10 Cl1_10 122.4(6) . . ?
B6_10 B1_10 Cl1_10 120.5(5) . . ?
B2_10 B1_10 Cl1_10 122.2(5) . . ?
B5_10 B1_10 Cl1_10 120.2(5) . . ?
B10_10 B2_10 B3_10 60.8(5) . . ?
B10_10 B2_10 B5_10 109.4(6) . . ?
B3_10 B2_10 B5_10 108.2(5) . . ?
B10_10 B2_10 B11_10 60.5(5) . . ?
B3_10 B2_10 B11_10 108.8(6) . . ?
B5_10 B2_10 B11_10 60.5(5) . . ?
B10_10 B2_10 B1_10 108.3(6) . . ?
B3_10 B2_10 B1_10 59.1(5) . . ?
B5_10 B2_10 B1_10 60.2(5) . . ?
B11_10 B2_10 B1_10 108.2(6) . . ?
B10_10 B2_10 Cl3_10 122.8(5) . . ?
B3_10 B2_10 Cl3_10 125.4(6) . . ?
B5_10 B2_10 Cl3_10 117.5(5) . . ?
B11_10 B2_10 Cl3_10 118.7(5) . . ?
B1_10 B2_10 Cl3_10 122.3(5) . . ?
B1_10 B3_10 B4_10 59.1(5) . . ?
B1_10 B3_10 Cl4_10 123.4(5) . . ?
B4_10 B3_10 Cl4_10 120.5(5) . . ?
B1_10 B3_10 B9_10 108.0(6) . . ?
B4_10 B3_10 B9_10 60.8(5) . . ?
Cl4_10 B3_10 B9_10 119.2(5) . . ?
B1_10 B3_10 B2_10 60.6(5) . . ?
B4_10 B3_10 B2_10 107.5(6) . . ?
Cl4_10 B3_10 B2_10 124.5(5) . . ?
B9_10 B3_10 B2_10 107.2(6) . . ?
B1_10 B3_10 B10_10 108.4(6) . . ?
B4_10 B3_10 B10_10 108.4(6) . . ?
Cl4_10 B3_10 B10_10 121.2(5) . . ?
B9_10 B3_10 B10_10 59.8(4) . . ?
B2_10 B3_10 B10_10 59.4(5) . . ?
B1_10 B4_10 B6_10 60.6(5) . . ?
B1_10 B4_10 B3_10 60.2(5) . . ?
B6_10 B4_10 B3_10 108.7(6) . . ?
B1_10 B4_10 B8_10 108.8(6) . . ?
B6_10 B4_10 B8_10 60.4(5) . . ?
B3_10 B4_10 B8_10 108.3(6) . . ?
B1_10 B4_10 Cl6_10 122.7(5) . . ?
B6_10 B4_10 Cl6_10 122.6(5) . . ?
B3_10 B4_10 Cl6_10 121.0(6) . . ?
B8_10 B4_10 Cl6_10 120.8(5) . . ?
B1_10 B4_10 B9_10 108.1(6) . . ?
B6_10 B4_10 B9_10 108.2(6) . . ?
B3_10 B4_10 B9_10 59.9(4) . . ?
B8_10 B4_10 B9_10 59.9(4) . . ?
Cl6_10 B4_10 B9_10 120.1(5) . . ?
Cl2_10 B5_10 B7_10 122.4(6) . . ?
Cl2_10 B5_10 B6_10 124.3(6) . . ?
B7_10 B5_10 B6_10 60.1(5) . . ?
Cl2_10 B5_10 B2_10 120.2(5) . . ?
B7_10 B5_10 B2_10 107.6(6) . . ?
B6_10 B5_10 B2_10 107.4(6) . . ?
Cl2_10 B5_10 B1_10 122.8(5) . . ?
B7_10 B5_10 B1_10 107.5(6) . . ?
B6_10 B5_10 B1_10 59.4(5) . . ?
B2_10 B5_10 B1_10 60.0(5) . . ?
Cl2_10 B5_10 B11_10 120.3(5) . . ?
B7_10 B5_10 B11_10 59.6(5) . . ?
B6_10 B5_10 B11_10 107.4(6) . . ?
B2_10 B5_10 B11_10 59.8(5) . . ?
B1_10 B5_10 B11_10 107.5(6) . . ?
B4_10 B6_10 B1_10 59.0(5) . . ?
B4_10 B6_10 B7_10 108.9(6) . . ?
B1_10 B6_10 B7_10 108.2(6) . . ?
B4_10 B6_10 B8_10 59.9(5) . . ?
B1_10 B6_10 B8_10 107.2(6) . . ?
B7_10 B6_10 B8_10 61.2(5) . . ?
B4_10 B6_10 B5_10 108.1(6) . . ?
B1_10 B6_10 B5_10 60.7(5) . . ?
B7_10 B6_10 B5_10 59.7(5) . . ?
B8_10 B6_10 B5_10 108.4(6) . . ?
B4_10 B6_10 Cl5_10 121.8(5) . . ?
B1_10 B6_10 Cl5_10 121.9(6) . . ?
B7_10 B6_10 Cl5_10 121.2(6) . . ?
B8_10 B6_10 Cl5_10 121.9(5) . . ?
B5_10 B6_10 Cl5_10 121.3(6) . . ?
Cl11_10 B7_10 B5_10 119.3(5) . . ?
Cl11_10 B7_10 B11_10 122.0(5) . . ?
B5_10 B7_10 B11_10 61.0(5) . . ?
Cl11_10 B7_10 B6_10 120.1(5) . . ?
B5_10 B7_10 B6_10 60.2(5) . . ?
B11_10 B7_10 B6_10 108.6(6) . . ?
Cl11_10 B7_10 B12_10 124.9(5) . . ?
B5_10 B7_10 B12_10 107.9(6) . . ?
B11_10 B7_10 B12_10 59.6(5) . . ?
B6_10 B7_10 B12_10 106.7(6) . . ?
Cl11_10 B7_10 B8_10 123.6(5) . . ?
B5_10 B7_10 B8_10 107.6(6) . . ?
B11_10 B7_10 B8_10 107.0(6) . . ?
B6_10 B7_10 B8_10 59.5(5) . . ?
B12_10 B7_10 B8_10 58.8(4) . . ?
B4_10 B8_10 B12_10 108.2(6) . . ?
B4_10 B8_10 B6_10 59.7(5) . . ?
B12_10 B8_10 B6_10 108.0(6) . . ?
B4_10 B8_10 B9_10 60.8(5) . . ?
B12_10 B8_10 B9_10 59.7(4) . . ?
B6_10 B8_10 B9_10 108.5(6) . . ?
B4_10 B8_10 Cl12_10 121.5(5) . . ?
B12_10 B8_10 Cl12_10 122.3(5) . . ?
B6_10 B8_10 Cl12_10 120.9(5) . . ?
B9_10 B8_10 Cl12_10 122.2(5) . . ?
B4_10 B8_10 B7_10 107.4(6) . . ?
B12_10 B8_10 B7_10 60.5(5) . . ?
B6_10 B8_10 B7_10 59.4(5) . . ?
B9_10 B8_10 B7_10 108.1(5) . . ?
Cl12_10 B8_10 B7_10 121.5(5) . . ?
B12_10 B9_10 Cl7_10 119.4(5) . . ?
B12_10 B9_10 B8_10 60.0(4) . . ?
Cl7_10 B9_10 B8_10 121.5(5) . . ?
B12_10 B9_10 B3_10 108.5(6) . . ?
Cl7_10 B9_10 B3_10 123.4(5) . . ?
B8_10 B9_10 B3_10 107.4(6) . . ?
B12_10 B9_10 B10_10 60.5(5) . . ?
Cl7_10 B9_10 B10_10 120.2(5) . . ?
B8_10 B9_10 B10_10 108.5(5) . . ?
B3_10 B9_10 B10_10 60.7(5) . . ?
B12_10 B9_10 B4_10 107.3(6) . . ?
Cl7_10 B9_10 B4_10 124.4(5) . . ?
B8_10 B9_10 B4_10 59.3(5) . . ?
B3_10 B9_10 B4_10 59.3(5) . . ?
B10_10 B9_10 B4_10 107.9(6) . . ?
Cl8_10 B10_10 B2_10 122.5(5) . . ?
Cl8_10 B10_10 B9_10 121.5(5) . . ?
B2_10 B10_10 B9_10 107.3(5) . . ?
Cl8_10 B10_10 B12_10 122.7(6) . . ?
B2_10 B10_10 B12_10 107.0(6) . . ?
B9_10 B10_10 B12_10 59.3(4) . . ?
Cl8_10 B10_10 B11_10 122.7(5) . . ?
B2_10 B10_10 B11_10 60.0(5) . . ?
B9_10 B10_10 B11_10 107.2(6) . . ?
B12_10 B10_10 B11_10 59.5(5) . . ?
Cl8_10 B10_10 B3_10 121.7(5) . . ?
B2_10 B10_10 B3_10 59.7(5) . . ?
B9_10 B10_10 B3_10 59.5(4) . . ?
B12_10 B10_10 B3_10 106.6(5) . . ?
B11_10 B10_10 B3_10 107.5(6) . . ?
B7_10 B11_10 B12_10 61.1(5) . . ?
B7_10 B11_10 B2_10 107.3(5) . . ?
B12_10 B11_10 B2_10 106.9(6) . . ?
B7_10 B11_10 Cl10_10 122.8(5) . . ?
B12_10 B11_10 Cl10_10 120.4(5) . . ?
B2_10 B11_10 Cl10_10 122.4(5) . . ?
B7_10 B11_10 B10_10 109.1(6) . . ?
B12_10 B11_10 B10_10 60.0(5) . . ?
B2_10 B11_10 B10_10 59.4(5) . . ?
Cl10_10 B11_10 B10_10 119.1(5) . . ?
B7_10 B11_10 B5_10 59.4(4) . . ?
B12_10 B11_10 B5_10 107.8(6) . . ?
B2_10 B11_10 B5_10 59.7(5) . . ?
Cl10_10 B11_10 B5_10 124.3(5) . . ?
B10_10 B11_10 B5_10 107.9(6) . . ?
B9_10 B12_10 B8_10 60.3(5) . . ?
B9_10 B12_10 B11_10 108.6(6) . . ?
B8_10 B12_10 B11_10 108.3(6) . . ?
B9_10 B12_10 B10_10 60.2(4) . . ?
B8_10 B12_10 B10_10 108.5(6) . . ?
B11_10 B12_10 B10_10 60.4(5) . . ?
B9_10 B12_10 Cl9_10 119.9(5) . . ?
B8_10 B12_10 Cl9_10 123.6(5) . . ?
B11_10 B12_10 Cl9_10 120.9(5) . . ?
B10_10 B12_10 Cl9_10 118.4(5) . . ?
B9_10 B12_10 B7_10 108.8(5) . . ?
B8_10 B12_10 B7_10 60.7(5) . . ?
B11_10 B12_10 B7_10 59.3(5) . . ?
B10_10 B12_10 B7_10 108.1(6) . . ?
Cl9_10 B12_10 B7_10 124.3(5) . . ?
B5_11 B1_11 B6_11 60.6(5) . . ?
B5_11 B1_11 B2_11 109.5(6) . . ?
B6_11 B1_11 B2_11 61.2(5) . . ?
B5_11 B1_11 B4_11 59.9(5) . . ?
B6_11 B1_11 B4_11 108.6(6) . . ?
B2_11 B1_11 B4_11 108.4(6) . . ?
B5_11 B1_11 Cl1_11 122.9(6) . . ?
B6_11 B1_11 Cl1_11 121.2(6) . . ?
B2_11 B1_11 Cl1_11 119.5(5) . . ?
B4_11 B1_11 Cl1_11 122.3(6) . . ?
B5_11 B1_11 B3_11 108.2(6) . . ?
B6_11 B1_11 B3_11 108.8(6) . . ?
B2_11 B1_11 B3_11 59.9(5) . . ?
B4_11 B1_11 B3_11 59.9(5) . . ?
Cl1_11 B1_11 B3_11 120.5(6) . . ?
B1_11 B2_11 B3_11 61.0(5) . . ?
B1_11 B2_11 B11_11 107.6(6) . . ?
B3_11 B2_11 B11_11 59.4(5) . . ?
B1_11 B2_11 B6_11 59.2(5) . . ?
B3_11 B2_11 B6_11 108.1(6) . . ?
B11_11 B2_11 B6_11 107.3(6) . . ?
B1_11 B2_11 B7_11 107.9(6) . . ?
B3_11 B2_11 B7_11 107.9(6) . . ?
B11_11 B2_11 B7_11 59.6(5) . . ?
B6_11 B2_11 B7_11 60.3(5) . . ?
B1_11 B2_11 Cl6_11 122.0(5) . . ?
B3_11 B2_11 Cl6_11 122.3(5) . . ?
B11_11 B2_11 Cl6_11 122.7(5) . . ?
B6_11 B2_11 Cl6_11 121.3(5) . . ?
B7_11 B2_11 Cl6_11 121.0(5) . . ?
B11_11 B3_11 B2_11 60.5(5) . . ?
B11_11 B3_11 B10_11 60.2(5) . . ?
B2_11 B3_11 B10_11 108.5(6) . . ?
B11_11 B3_11 Cl2_11 123.0(6) . . ?
B2_11 B3_11 Cl2_11 120.8(5) . . ?
B10_11 B3_11 Cl2_11 123.1(5) . . ?
B11_11 B3_11 B4_11 107.6(6) . . ?
B2_11 B3_11 B4_11 107.7(6) . . ?
B10_11 B3_11 B4_11 59.6(5) . . ?
Cl2_11 B3_11 B4_11 121.7(6) . . ?
B11_11 B3_11 B1_11 107.0(6) . . ?
B2_11 B3_11 B1_11 59.2(5) . . ?
B10_11 B3_11 B1_11 107.2(6) . . ?
Cl2_11 B3_11 B1_11 121.0(6) . . ?
B4_11 B3_11 B1_11 59.8(5) . . ?
B5_11 B4_11 B9_11 60.4(5) . . ?
B5_11 B4_11 B10_11 108.2(6) . . ?
B9_11 B4_11 B10_11 59.9(5) . . ?
B5_11 B4_11 Cl3_11 122.3(6) . . ?
B9_11 B4_11 Cl3_11 121.2(5) . . ?
B10_11 B4_11 Cl3_11 120.8(5) . . ?
B5_11 B4_11 B1_11 59.2(5) . . ?
B9_11 B4_11 B1_11 107.5(6) . . ?
B10_11 B4_11 B1_11 107.8(6) . . ?
Cl3_11 B4_11 B1_11 123.1(6) . . ?
B5_11 B4_11 B3_11 108.0(6) . . ?
B9_11 B4_11 B3_11 107.9(6) . . ?
B10_11 B4_11 B3_11 59.9(5) . . ?
Cl3_11 B4_11 B3_11 121.6(6) . . ?
B1_11 B4_11 B3_11 60.3(5) . . ?
B1_11 B5_11 B4_11 60.9(5) . . ?
B1_11 B5_11 B6_11 59.7(5) . . ?
B4_11 B5_11 B6_11 108.7(6) . . ?
B1_11 B5_11 Cl4_11 121.7(6) . . ?
B4_11 B5_11 Cl4_11 122.6(5) . . ?
B6_11 B5_11 Cl4_11 120.3(5) . . ?
B1_11 B5_11 B9_11 108.4(6) . . ?
B4_11 B5_11 B9_11 59.8(5) . . ?
B6_11 B5_11 B9_11 108.3(6) . . ?
Cl4_11 B5_11 B9_11 122.2(5) . . ?
B1_11 B5_11 B8_11 107.5(6) . . ?
B4_11 B5_11 B8_11 107.8(6) . . ?
B6_11 B5_11 B8_11 59.9(5) . . ?
Cl4_11 B5_11 B8_11 121.3(6) . . ?
B9_11 B5_11 B8_11 59.9(4) . . ?
B1_11 B6_11 B5_11 59.7(5) . . ?
B1_11 B6_11 B8_11 107.8(6) . . ?
B5_11 B6_11 B8_11 60.3(5) . . ?
B1_11 B6_11 Cl5_11 122.2(6) . . ?
B5_11 B6_11 Cl5_11 121.4(5) . . ?
B8_11 B6_11 Cl5_11 121.4(6) . . ?
B1_11 B6_11 B2_11 59.6(5) . . ?
B5_11 B6_11 B2_11 107.5(6) . . ?
B8_11 B6_11 B2_11 107.7(6) . . ?
Cl5_11 B6_11 B2_11 122.5(5) . . ?
B1_11 B6_11 B7_11 107.8(6) . . ?
B5_11 B6_11 B7_11 108.5(6) . . ?
B8_11 B6_11 B7_11 60.2(5) . . ?
Cl5_11 B6_11 B7_11 121.6(6) . . ?
B2_11 B6_11 B7_11 59.9(5) . . ?
Cl7_11 B7_11 B11_11 123.1(6) . . ?
Cl7_11 B7_11 B12_11 122.7(6) . . ?
B11_11 B7_11 B12_11 59.8(5) . . ?
Cl7_11 B7_11 B2_11 121.9(5) . . ?
B11_11 B7_11 B2_11 59.9(5) . . ?
B12_11 B7_11 B2_11 107.6(5) . . ?
Cl7_11 B7_11 B8_11 122.3(6) . . ?
B11_11 B7_11 B8_11 106.5(5) . . ?
B12_11 B7_11 B8_11 59.2(4) . . ?
B2_11 B7_11 B8_11 106.9(6) . . ?
Cl7_11 B7_11 B6_11 121.5(5) . . ?
B11_11 B7_11 B6_11 107.2(6) . . ?
B12_11 B7_11 B6_11 106.8(6) . . ?
B2_11 B7_11 B6_11 59.8(5) . . ?
B8_11 B7_11 B6_11 59.2(5) . . ?
B12_11 B8_11 B6_11 108.5(6) . . ?
B12_11 B8_11 B9_11 60.6(5) . . ?
B6_11 B8_11 B9_11 108.1(6) . . ?
B12_11 B8_11 B5_11 108.4(6) . . ?
B6_11 B8_11 B5_11 59.7(5) . . ?
B9_11 B8_11 B5_11 59.9(5) . . ?
B12_11 B8_11 Cl8_11 120.3(5) . . ?
B6_11 B8_11 Cl8_11 121.4(5) . . ?
B9_11 B8_11 Cl8_11 122.7(5) . . ?
B5_11 B8_11 Cl8_11 123.6(5) . . ?
B12_11 B8_11 B7_11 59.9(5) . . ?
B6_11 B8_11 B7_11 60.6(5) . . ?
B9_11 B8_11 B7_11 108.6(6) . . ?
B5_11 B8_11 B7_11 108.3(6) . . ?
Cl8_11 B8_11 B7_11 119.5(5) . . ?
B10_11 B9_11 B4_11 60.1(5) . . ?
B10_11 B9_11 B5_11 107.8(6) . . ?
B4_11 B9_11 B5_11 59.8(5) . . ?
B10_11 B9_11 B8_11 107.8(6) . . ?
B4_11 B9_11 B8_11 107.9(6) . . ?
B5_11 B9_11 B8_11 60.1(5) . . ?
B10_11 B9_11 Cl9_11 121.5(5) . . ?
B4_11 B9_11 Cl9_11 122.3(5) . . ?
B5_11 B9_11 Cl9_11 122.4(5) . . ?
B8_11 B9_11 Cl9_11 121.6(5) . . ?
B10_11 B9_11 B12_11 60.4(5) . . ?
B4_11 B9_11 B12_11 108.1(6) . . ?
B5_11 B9_11 B12_11 107.5(5) . . ?
B8_11 B9_11 B12_11 59.2(5) . . ?
Cl9_11 B9_11 B12_11 121.3(5) . . ?
B9_11 B10_11 B4_11 59.9(5) . . ?
B9_11 B10_11 B11_11 108.0(6) . . ?
B4_11 B10_11 B11_11 107.8(6) . . ?
B9_11 B10_11 B3_11 108.4(6) . . ?
B4_11 B10_11 B3_11 60.5(5) . . ?
B11_11 B10_11 B3_11 59.5(5) . . ?
B9_11 B10_11 Cl10_11 120.8(5) . . ?
B4_11 B10_11 Cl10_11 124.2(5) . . ?
B11_11 B10_11 Cl10_11 120.8(6) . . ?
B3_11 B10_11 Cl10_11 123.8(5) . . ?
B9_11 B10_11 B12_11 60.3(5) . . ?
B4_11 B10_11 B12_11 108.0(6) . . ?
B11_11 B10_11 B12_11 59.6(5) . . ?
B3_11 B10_11 B12_11 107.5(5) . . ?
Cl10_11 B10_11 B12_11 119.0(5) . . ?
B3_11 B11_11 B12_11 109.0(6) . . ?
B3_11 B11_11 B10_11 60.3(5) . . ?
B12_11 B11_11 B10_11 60.6(5) . . ?
B3_11 B11_11 B7_11 109.2(6) . . ?
B12_11 B11_11 B7_11 60.2(5) . . ?
B10_11 B11_11 B7_11 109.1(6) . . ?
B3_11 B11_11 B2_11 60.1(5) . . ?
B12_11 B11_11 B2_11 108.4(6) . . ?
B10_11 B11_11 B2_11 108.4(6) . . ?
B7_11 B11_11 B2_11 60.5(5) . . ?
B3_11 B11_11 Cl11_11 121.7(6) . . ?
B12_11 B11_11 Cl11_11 119.6(6) . . ?
B10_11 B11_11 Cl11_11 119.5(6) . . ?
B7_11 B11_11 Cl11_11 121.6(6) . . ?
B2_11 B11_11 Cl11_11 123.8(5) . . ?
B8_11 B12_11 B11_11 108.1(6) . . ?
B8_11 B12_11 B7_11 60.9(5) . . ?
B11_11 B12_11 B7_11 60.1(5) . . ?
B8_11 B12_11 Cl12_11 122.7(5) . . ?
B11_11 B12_11 Cl12_11 121.6(5) . . ?
B7_11 B12_11 Cl12_11 122.0(5) . . ?
B8_11 B12_11 B9_11 60.1(5) . . ?
B11_11 B12_11 B9_11 107.3(6) . . ?
B7_11 B12_11 B9_11 108.9(6) . . ?
Cl12_11 B12_11 B9_11 121.4(5) . . ?
B8_11 B12_11 B10_11 107.6(6) . . ?
B11_11 B12_11 B10_11 59.8(5) . . ?
B7_11 B12_11 B10_11 108.4(6) . . ?
Cl12_11 B12_11 B10_11 120.6(5) . . ?
B9_11 B12_11 B10_11 59.3(4) . . ?
B2_12 B1_12 B3_12 60.8(5) . . ?
B2_12 B1_12 B4_12 60.7(5) . . ?
B3_12 B1_12 B4_12 108.9(6) . . ?
B2_12 B1_12 B5_12 108.5(6) . . ?
B3_12 B1_12 B5_12 59.7(5) . . ?
B4_12 B1_12 B5_12 107.7(6) . . ?
B2_12 B1_12 Cl1_12 122.2(6) . . ?
B3_12 B1_12 Cl1_12 122.5(6) . . ?
B4_12 B1_12 Cl1_12 121.2(6) . . ?
B5_12 B1_12 Cl1_12 121.3(6) . . ?
B2_12 B1_12 B6_12 108.1(6) . . ?
B3_12 B1_12 B6_12 107.8(6) . . ?
B4_12 B1_12 B6_12 59.3(5) . . ?
B5_12 B1_12 B6_12 60.0(5) . . ?
Cl1_12 B1_12 B6_12 120.7(6) . . ?
B1_12 B2_12 B3_12 60.4(5) . . ?
B1_12 B2_12 B4_12 60.8(5) . . ?
B3_12 B2_12 B4_12 108.6(6) . . ?
B1_12 B2_12 B11_12 108.1(6) . . ?
B3_12 B2_12 B11_12 59.8(5) . . ?
B4_12 B2_12 B11_12 107.5(6) . . ?
B1_12 B2_12 Cl2_12 120.2(6) . . ?
B3_12 B2_12 Cl2_12 121.4(6) . . ?
B4_12 B2_12 Cl2_12 121.2(6) . . ?
B11_12 B2_12 Cl2_12 123.0(6) . . ?
B1_12 B2_12 B10_12 108.7(6) . . ?
B3_12 B2_12 B10_12 107.4(6) . . ?
B4_12 B2_12 B10_12 60.2(5) . . ?
B11_12 B2_12 B10_12 59.0(5) . . ?
Cl2_12 B2_12 B10_12 122.7(6) . . ?
B1_12 B3_12 B5_12 60.8(5) . . ?
B1_12 B3_12 B2_12 58.8(5) . . ?
B5_12 B3_12 B2_12 107.8(6) . . ?
B1_12 B3_12 B11_12 107.5(6) . . ?
B5_12 B3_12 B11_12 107.7(6) . . ?
B2_12 B3_12 B11_12 60.5(5) . . ?
B1_12 B3_12 Cl3_12 121.1(6) . . ?
B5_12 B3_12 Cl3_12 121.9(6) . . ?
B2_12 B3_12 Cl3_12 121.1(6) . . ?
B11_12 B3_12 Cl3_12 122.2(6) . . ?
B1_12 B3_12 B9_12 109.0(6) . . ?
B5_12 B3_12 B9_12 60.1(5) . . ?
B2_12 B3_12 B9_12 108.8(6) . . ?
B11_12 B3_12 B9_12 60.0(5) . . ?
Cl3_12 B3_12 B9_12 121.8(6) . . ?
B6_12 B4_12 B2_12 108.0(6) . . ?
B6_12 B4_12 B8_12 59.4(5) . . ?
B2_12 B4_12 B8_12 108.8(6) . . ?
B6_12 B4_12 B1_12 61.3(5) . . ?
B2_12 B4_12 B1_12 58.5(5) . . ?
B8_12 B4_12 B1_12 108.6(6) . . ?
B6_12 B4_12 B10_12 107.3(6) . . ?
B2_12 B4_12 B10_12 61.0(5) . . ?
B8_12 B4_12 B10_12 59.9(5) . . ?
B1_12 B4_12 B10_12 107.5(6) . . ?
B6_12 B4_12 Cl4_12 121.9(6) . . ?
B2_12 B4_12 Cl4_12 121.7(6) . . ?
B8_12 B4_12 Cl4_12 121.2(6) . . ?
B1_12 B4_12 Cl4_12 122.1(5) . . ?
B10_12 B4_12 Cl4_12 121.6(6) . . ?
B3_12 B5_12 Cl5_12 122.5(6) . . ?
B3_12 B5_12 B9_12 60.8(5) . . ?
Cl5_12 B5_12 B9_12 121.8(6) . . ?
B3_12 B5_12 B1_12 59.5(5) . . ?
Cl5_12 B5_12 B1_12 121.7(6) . . ?
B9_12 B5_12 B1_12 108.4(6) . . ?
B3_12 B5_12 B6_12 108.2(6) . . ?
Cl5_12 B5_12 B6_12 120.7(6) . . ?
B9_12 B5_12 B6_12 108.1(6) . . ?
B1_12 B5_12 B6_12 60.6(5) . . ?
B3_12 B5_12 B7_12 108.4(6) . . ?
Cl5_12 B5_12 B7_12 121.3(6) . . ?
B9_12 B5_12 B7_12 60.3(5) . . ?
B1_12 B5_12 B7_12 107.8(6) . . ?
B6_12 B5_12 B7_12 59.2(5) . . ?
B8_12 B6_12 B4_12 60.3(5) . . ?
B8_12 B6_12 B7_12 60.3(5) . . ?
B4_12 B6_12 B7_12 108.3(6) . . ?
B8_12 B6_12 Cl6_12 121.6(6) . . ?
B4_12 B6_12 Cl6_12 119.0(6) . . ?
B7_12 B6_12 Cl6_12 124.5(7) . . ?
B8_12 B6_12 B5_12 108.5(6) . . ?
B4_12 B6_12 B5_12 107.4(6) . . ?
B7_12 B6_12 B5_12 60.4(5) . . ?
Cl6_12 B6_12 B5_12 123.3(6) . . ?
B8_12 B6_12 B1_12 107.8(7) . . ?
B4_12 B6_12 B1_12 59.4(5) . . ?
B7_12 B6_12 B1_12 107.8(6) . . ?
Cl6_12 B6_12 B1_12 120.2(6) . . ?
B5_12 B6_12 B1_12 59.4(5) . . ?
B8_12 B7_12 B6_12 59.3(5) . . ?
B8_12 B7_12 B12_12 61.5(5) . . ?
B6_12 B7_12 B12_12 108.8(6) . . ?
B8_12 B7_12 Cl7_12 123.0(6) . . ?
B6_12 B7_12 Cl7_12 121.1(6) . . ?
B12_12 B7_12 Cl7_12 122.5(6) . . ?
B8_12 B7_12 B5_12 107.6(6) . . ?
B6_12 B7_12 B5_12 60.4(5) . . ?
B12_12 B7_12 B5_12 107.6(6) . . ?
Cl7_12 B7_12 B5_12 120.4(6) . . ?
B8_12 B7_12 B9_12 108.9(6) . . ?
B6_12 B7_12 B9_12 108.4(6) . . ?
B12_12 B7_12 B9_12 59.9(5) . . ?
Cl7_12 B7_12 B9_12 120.7(6) . . ?
B5_12 B7_12 B9_12 59.5(5) . . ?
B6_12 B8_12 B4_12 60.3(5) . . ?
B6_12 B8_12 B7_12 60.3(5) . . ?
B4_12 B8_12 B7_12 108.3(6) . . ?
B6_12 B8_12 Cl8_12 121.7(6) . . ?
B4_12 B8_12 Cl8_12 121.3(6) . . ?
B7_12 B8_12 Cl8_12 122.1(6) . . ?
B6_12 B8_12 B10_12 108.8(6) . . ?
B4_12 B8_12 B10_12 60.8(5) . . ?
B7_12 B8_12 B10_12 107.4(6) . . ?
Cl8_12 B8_12 B10_12 121.3(6) . . ?
B6_12 B8_12 B12_12 107.9(6) . . ?
B4_12 B8_12 B12_12 108.1(6) . . ?
B7_12 B8_12 B12_12 59.3(5) . . ?
Cl8_12 B8_12 B12_12 121.9(6) . . ?
B10_12 B8_12 B12_12 59.5(5) . . ?
Cl11_12 B9_12 B5_12 121.6(6) . . ?
Cl11_12 B9_12 B11_12 124.1(6) . . ?
B5_12 B9_12 B11_12 106.3(6) . . ?
Cl11_12 B9_12 B12_12 121.4(6) . . ?
B5_12 B9_12 B12_12 107.8(6) . . ?
B11_12 B9_12 B12_12 60.0(5) . . ?
Cl11_12 B9_12 B3_12 123.4(6) . . ?
B5_12 B9_12 B3_12 59.1(5) . . ?
B11_12 B9_12 B3_12 59.3(5) . . ?
B12_12 B9_12 B3_12 107.7(6) . . ?
Cl11_12 B9_12 B7_12 120.9(6) . . ?
B5_12 B9_12 B7_12 60.2(5) . . ?
B11_12 B9_12 B7_12 106.5(6) . . ?
B12_12 B9_12 B7_12 59.4(5) . . ?
B3_12 B9_12 B7_12 107.0(6) . . ?
B11_12 B10_12 Cl9_12 121.6(6) . . ?
B11_12 B10_12 B8_12 108.4(6) . . ?
Cl9_12 B10_12 B8_12 122.9(6) . . ?
B11_12 B10_12 B12_12 60.2(5) . . ?
Cl9_12 B10_12 B12_12 122.4(6) . . ?
B8_12 B10_12 B12_12 61.2(5) . . ?
B11_12 B10_12 B4_12 106.9(6) . . ?
Cl9_12 B10_12 B4_12 121.6(6) . . ?
B8_12 B10_12 B4_12 59.4(5) . . ?
B12_12 B10_12 B4_12 108.3(6) . . ?
B11_12 B10_12 B2_12 59.7(5) . . ?
Cl9_12 B10_12 B2_12 121.0(6) . . ?
B8_12 B10_12 B2_12 106.7(6) . . ?
B12_12 B10_12 B2_12 108.0(6) . . ?
B4_12 B10_12 B2_12 58.8(5) . . ?
B3_12 B11_12 B10_12 109.2(6) . . ?
B3_12 B11_12 B12_12 108.8(6) . . ?
B10_12 B11_12 B12_12 60.2(5) . . ?
B3_12 B11_12 B9_12 60.7(5) . . ?
B10_12 B11_12 B9_12 108.8(6) . . ?
B12_12 B11_12 B9_12 60.1(5) . . ?
B3_12 B11_12 B2_12 59.7(5) . . ?
B10_12 B11_12 B2_12 61.3(5) . . ?
B12_12 B11_12 B2_12 109.2(6) . . ?
B9_12 B11_12 B2_12 108.7(6) . . ?
B3_12 B11_12 Cl10_12 122.8(6) . . ?
B10_12 B11_12 Cl10_12 119.9(6) . . ?
B12_12 B11_12 Cl10_12 119.7(6) . . ?
B9_12 B11_12 Cl10_12 121.3(6) . . ?
B2_12 B11_12 Cl10_12 122.1(6) . . ?
Cl12_12 B12_12 B7_12 123.6(6) . . ?
Cl12_12 B12_12 B11_12 121.2(6) . . ?
B7_12 B12_12 B11_12 107.5(6) . . ?
Cl12_12 B12_12 B10_12 120.7(6) . . ?
B7_12 B12_12 B10_12 107.2(6) . . ?
B11_12 B12_12 B10_12 59.5(5) . . ?
Cl12_12 B12_12 B9_12 121.7(6) . . ?
B7_12 B12_12 B9_12 60.7(5) . . ?
B11_12 B12_12 B9_12 60.0(5) . . ?
B10_12 B12_12 B9_12 108.1(6) . . ?
Cl12_12 B12_12 B8_12 123.1(6) . . ?
B7_12 B12_12 B8_12 59.2(5) . . ?
B11_12 B12_12 B8_12 106.4(6) . . ?
B10_12 B12_12 B8_12 59.4(5) . . ?
B9_12 B12_12 B8_12 107.7(6) . . ?
B3_13 B1_13 B2_13 59.3(5) . . ?
B3_13 B1_13 B4_13 61.0(5) . . ?
B2_13 B1_13 B4_13 107.9(5) . . ?
B3_13 B1_13 B5_13 109.0(6) . . ?
B2_13 B1_13 B5_13 107.8(6) . . ?
B4_13 B1_13 B5_13 60.1(5) . . ?
B3_13 B1_13 Cl1_13 122.0(5) . . ?
B2_13 B1_13 Cl1_13 119.3(6) . . ?
B4_13 B1_13 Cl1_13 124.8(5) . . ?
B5_13 B1_13 Cl1_13 122.7(5) . . ?
B3_13 B1_13 B6_13 107.1(5) . . ?
B2_13 B1_13 B6_13 58.8(5) . . ?
B4_13 B1_13 B6_13 108.1(5) . . ?
B5_13 B1_13 B6_13 60.7(4) . . ?
Cl1_13 B1_13 B6_13 119.6(5) . . ?
B3_13 B2_13 B6_13 109.7(6) . . ?
B3_13 B2_13 B1_13 60.0(5) . . ?
B6_13 B2_13 B1_13 61.5(5) . . ?
B3_13 B2_13 B12_13 109.5(6) . . ?
B6_13 B2_13 B12_13 60.2(5) . . ?
B1_13 B2_13 B12_13 109.6(6) . . ?
B3_13 B2_13 B11_13 60.3(4) . . ?
B6_13 B2_13 B11_13 109.2(6) . . ?
B1_13 B2_13 B11_13 108.7(6) . . ?
B12_13 B2_13 B11_13 60.8(5) . . ?
B3_13 B2_13 Cl6_13 120.9(5) . . ?
B6_13 B2_13 Cl6_13 120.9(5) . . ?
B1_13 B2_13 Cl6_13 121.2(5) . . ?
B12_13 B2_13 Cl6_13 120.7(5) . . ?
B11_13 B2_13 Cl6_13 121.0(5) . . ?
B2_13 B3_13 B1_13 60.6(5) . . ?
B2_13 B3_13 B11_13 61.2(5) . . ?
B1_13 B3_13 B11_13 109.8(5) . . ?
B2_13 B3_13 Cl5_13 121.1(5) . . ?
B1_13 B3_13 Cl5_13 119.6(5) . . ?
B11_13 B3_13 Cl5_13 122.2(5) . . ?
B2_13 B3_13 B4_13 108.0(5) . . ?
B1_13 B3_13 B4_13 59.9(5) . . ?
B11_13 B3_13 B4_13 107.9(5) . . ?
Cl5_13 B3_13 B4_13 121.5(5) . . ?
B2_13 B3_13 B10_13 108.2(6) . . ?
B1_13 B3_13 B10_13 107.9(6) . . ?
B11_13 B3_13 B10_13 59.8(4) . . ?
Cl5_13 B3_13 B10_13 123.1(5) . . ?
B4_13 B3_13 B10_13 59.3(4) . . ?
B1_13 B4_13 B8_13 108.8(5) . . ?
B1_13 B4_13 B10_13 108.1(5) . . ?
B8_13 B4_13 B10_13 59.9(4) . . ?
B1_13 B4_13 B5_13 60.2(5) . . ?
B8_13 B4_13 B5_13 61.0(5) . . ?
B10_13 B4_13 B5_13 108.7(5) . . ?
B1_13 B4_13 Cl4_13 122.1(5) . . ?
B8_13 B4_13 Cl4_13 121.1(5) . . ?
B10_13 B4_13 Cl4_13 120.9(5) . . ?
B5_13 B4_13 Cl4_13 121.8(5) . . ?
B1_13 B4_13 B3_13 59.1(4) . . ?
B8_13 B4_13 B3_13 108.0(5) . . ?
B10_13 B4_13 B3_13 60.4(4) . . ?
B5_13 B4_13 B3_13 107.5(5) . . ?
Cl4_13 B4_13 B3_13 122.0(5) . . ?
Cl3_13 B5_13 B4_13 122.4(5) . . ?
Cl3_13 B5_13 B1_13 121.7(5) . . ?
B4_13 B5_13 B1_13 59.7(4) . . ?
Cl3_13 B5_13 B8_13 122.7(5) . . ?
B4_13 B5_13 B8_13 59.4(4) . . ?
B1_13 B5_13 B8_13 107.2(5) . . ?
Cl3_13 B5_13 B6_13 121.7(5) . . ?
B4_13 B5_13 B6_13 107.5(5) . . ?
B1_13 B5_13 B6_13 60.2(5) . . ?
B8_13 B5_13 B6_13 107.1(5) . . ?
Cl3_13 B5_13 B7_13 122.2(5) . . ?
B4_13 B5_13 B7_13 107.0(5) . . ?
B1_13 B5_13 B7_13 107.5(6) . . ?
B8_13 B5_13 B7_13 59.5(5) . . ?
B6_13 B5_13 B7_13 59.6(4) . . ?
B2_13 B6_13 B12_13 60.5(5) . . ?
B2_13 B6_13 Cl2_13 123.0(5) . . ?
B12_13 B6_13 Cl2_13 121.9(5) . . ?
B2_13 B6_13 B7_13 107.7(6) . . ?
B12_13 B6_13 B7_13 60.2(5) . . ?
Cl2_13 B6_13 B7_13 121.5(5) . . ?
B2_13 B6_13 B1_13 59.7(5) . . ?
B12_13 B6_13 B1_13 108.4(5) . . ?
Cl2_13 B6_13 B1_13 121.8(5) . . ?
B7_13 B6_13 B1_13 107.3(5) . . ?
B2_13 B6_13 B5_13 107.3(6) . . ?
B12_13 B6_13 B5_13 108.8(5) . . ?
Cl2_13 B6_13 B5_13 120.6(5) . . ?
B7_13 B6_13 B5_13 60.3(5) . . ?
B1_13 B6_13 B5_13 59.2(5) . . ?
Cl12_13 B7_13 B9_13 121.7(5) . . ?
Cl12_13 B7_13 B12_13 122.3(6) . . ?
B9_13 B7_13 B12_13 61.0(5) . . ?
Cl12_13 B7_13 B8_13 121.1(5) . . ?
B9_13 B7_13 B8_13 60.0(4) . . ?
B12_13 B7_13 B8_13 108.6(6) . . ?
Cl12_13 B7_13 B6_13 122.1(5) . . ?
B9_13 B7_13 B6_13 108.1(6) . . ?
B12_13 B7_13 B6_13 59.2(5) . . ?
B8_13 B7_13 B6_13 107.9(6) . . ?
Cl12_13 B7_13 B5_13 120.9(6) . . ?
B9_13 B7_13 B5_13 108.3(6) . . ?
B12_13 B7_13 B5_13 107.9(6) . . ?
B8_13 B7_13 B5_13 60.0(4) . . ?
B6_13 B7_13 B5_13 60.1(5) . . ?
B10_13 B8_13 B4_13 60.1(4) . . ?
B10_13 B8_13 Cl11_13 121.0(5) . . ?
B4_13 B8_13 Cl11_13 122.4(5) . . ?
B10_13 B8_13 B9_13 60.2(4) . . ?
B4_13 B8_13 B9_13 108.4(5) . . ?
Cl11_13 B8_13 B9_13 120.3(5) . . ?
B10_13 B8_13 B7_13 107.6(6) . . ?
B4_13 B8_13 B7_13 107.9(5) . . ?
Cl11_13 B8_13 B7_13 122.0(5) . . ?
B9_13 B8_13 B7_13 59.6(5) . . ?
B10_13 B8_13 B5_13 107.9(5) . . ?
B4_13 B8_13 B5_13 59.6(4) . . ?
Cl11_13 B8_13 B5_13 122.8(5) . . ?
B9_13 B8_13 B5_13 108.3(5) . . ?
B7_13 B8_13 B5_13 60.5(5) . . ?
B7_13 B9_13 Cl10_13 122.0(5) . . ?
B7_13 B9_13 B10_13 107.7(6) . . ?
Cl10_13 B9_13 B10_13 121.8(5) . . ?
B7_13 B9_13 B8_13 60.4(5) . . ?
Cl10_13 B9_13 B8_13 121.7(5) . . ?
B10_13 B9_13 B8_13 59.5(4) . . ?
B7_13 B9_13 B11_13 107.9(6) . . ?
Cl10_13 B9_13 B11_13 121.7(5) . . ?
B10_13 B9_13 B11_13 59.7(4) . . ?
B8_13 B9_13 B11_13 107.6(5) . . ?
B7_13 B9_13 B12_13 59.7(5) . . ?
Cl10_13 B9_13 B12_13 122.2(5) . . ?
B10_13 B9_13 B12_13 107.5(5) . . ?
B8_13 B9_13 B12_13 107.9(6) . . ?
B11_13 B9_13 B12_13 60.1(4) . . ?
B8_13 B10_13 B4_13 60.0(4) . . ?
B8_13 B10_13 B11_13 108.8(6) . . ?
B4_13 B10_13 B11_13 108.6(5) . . ?
B8_13 B10_13 B9_13 60.3(5) . . ?
B4_13 B10_13 B9_13 108.3(5) . . ?
B11_13 B10_13 B9_13 60.4(4) . . ?
B8_13 B10_13 B3_13 108.0(5) . . ?
B4_13 B10_13 B3_13 60.3(4) . . ?
B11_13 B10_13 B3_13 59.6(4) . . ?
B9_13 B10_13 B3_13 107.7(5) . . ?
B8_13 B10_13 Cl9_13 120.5(5) . . ?
B4_13 B10_13 Cl9_13 122.1(5) . . ?
B11_13 B10_13 Cl9_13 121.4(5) . . ?
B9_13 B10_13 Cl9_13 120.3(5) . . ?
B3_13 B10_13 Cl9_13 123.4(5) . . ?
Cl7_13 B11_13 B3_13 122.8(5) . . ?
Cl7_13 B11_13 B10_13 122.4(5) . . ?
B3_13 B11_13 B10_13 60.6(4) . . ?
Cl7_13 B11_13 B2_13 122.9(5) . . ?
B3_13 B11_13 B2_13 58.5(4) . . ?
B10_13 B11_13 B2_13 106.7(5) . . ?
Cl7_13 B11_13 B9_13 121.3(5) . . ?
B3_13 B11_13 B9_13 108.0(6) . . ?
B10_13 B11_13 B9_13 59.9(4) . . ?
B2_13 B11_13 B9_13 107.0(5) . . ?
Cl7_13 B11_13 B12_13 121.3(5) . . ?
B3_13 B11_13 B12_13 106.7(5) . . ?
B10_13 B11_13 B12_13 107.9(6) . . ?
B2_13 B11_13 B12_13 59.1(4) . . ?
B9_13 B11_13 B12_13 60.4(4) . . ?
Cl8_13 B12_13 B6_13 122.6(5) . . ?
Cl8_13 B12_13 B2_13 122.4(5) . . ?
B6_13 B12_13 B2_13 59.3(5) . . ?
Cl8_13 B12_13 B7_13 122.8(5) . . ?
B6_13 B12_13 B7_13 60.7(5) . . ?
B2_13 B12_13 B7_13 107.2(6) . . ?
Cl8_13 B12_13 B11_13 120.9(5) . . ?
B6_13 B12_13 B11_13 107.9(6) . . ?
B2_13 B12_13 B11_13 60.1(4) . . ?
B7_13 B12_13 B11_13 107.1(6) . . ?
Cl8_13 B12_13 B9_13 121.6(5) . . ?
B6_13 B12_13 B9_13 107.9(6) . . ?
B2_13 B12_13 B9_13 107.1(6) . . ?
B7_13 B12_13 B9_13 59.2(5) . . ?
B11_13 B12_13 B9_13 59.5(4) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
N1_1 C1_1 C2_1 C3_1 -0.2(11) . . . . ?
C1_1 C2_1 C3_1 C4_1 1.9(10) . . . . ?
C1_1 C2_1 C3_1 C6_1 -179.1(6) . . . . ?
C2_1 C3_1 C4_1 C5_1 -2.5(11) . . . . ?
C6_1 C3_1 C4_1 C5_1 178.5(7) . . . . ?
C3_1 C4_1 C5_1 N1_1 1.5(11) . . . . ?
C4_1 C3_1 C6_1 C11_1 -31.8(10) . . . . ?
C2_1 C3_1 C6_1 C11_1 149.3(7) . . . . ?
C4_1 C3_1 C6_1 C7_1 150.0(7) . . . . ?
C2_1 C3_1 C6_1 C7_1 -28.9(10) . . . . ?
C11_1 C6_1 C7_1 C8_1 0.9(11) . . . . ?
C3_1 C6_1 C7_1 C8_1 179.1(7) . . . . ?
C6_1 C7_1 C8_1 C9_1 -1.7(11) . . . . ?
C7_1 C8_1 C9_1 C10_1 1.9(11) . . . . ?
C7_1 C8_1 C9_1 C12_1 -179.8(7) . . . . ?
C8_1 C9_1 C10_1 C11_1 -1.4(11) . . . . ?
C12_1 C9_1 C10_1 C11_1 -179.7(7) . . . . ?
C7_1 C6_1 C11_1 C10_1 -0.4(11) . . . . ?
C3_1 C6_1 C11_1 C10_1 -178.6(7) . . . . ?
C9_1 C10_1 C11_1 C6_1 0.7(11) . . . . ?
C8_1 C9_1 C12_1 C16_1 -148.0(7) . . . . ?
C10_1 C9_1 C12_1 C16_1 30.3(10) . . . . ?
C8_1 C9_1 C12_1 C13_1 32.0(11) . . . . ?
C10_1 C9_1 C12_1 C13_1 -149.7(7) . . . . ?
C16_1 C12_1 C13_1 C14_1 -0.8(11) . . . . ?
C9_1 C12_1 C13_1 C14_1 179.1(7) . . . . ?
C12_1 C13_1 C14_1 N2_1 -0.7(11) . . . . ?
N2_1 C15_1 C16_1 C12_1 -3.0(11) . . . . ?
C13_1 C12_1 C16_1 C15_1 2.6(11) . . . . ?
C9_1 C12_1 C16_1 C15_1 -177.3(7) . . . . ?
C4_1 C5_1 N1_1 C1_1 0.3(10) . . . . ?
C4_1 C5_1 N1_1 Cu1 -173.9(5) . . . . ?
C2_1 C1_1 N1_1 C5_1 -1.0(10) . . . . ?
C2_1 C1_1 N1_1 Cu1 173.4(5) . . . . ?
C13_1 C14_1 N2_1 C15_1 0.5(10) . . . . ?
C13_1 C14_1 N2_1 Cu5 172.3(6) . . . 7 ?
C16_1 C15_1 N2_1 C14_1 1.4(10) . . . . ?
C16_1 C15_1 N2_1 Cu5 -170.9(5) . . . 7 ?
N1_2 C1_2 C2_2 C3_2 0.1(11) . . . . ?
C1_2 C2_2 C3_2 C4_2 -0.4(10) . . . . ?
C1_2 C2_2 C3_2 C6_2 179.3(6) . . . . ?
C2_2 C3_2 C4_2 C5_2 -0.5(10) . . . . ?
C6_2 C3_2 C4_2 C5_2 179.8(6) . . . . ?
C3_2 C4_2 C5_2 N1_2 1.9(11) . . . . ?
C4_2 C3_2 C6_2 C11_2 -144.9(7) . . . . ?
C2_2 C3_2 C6_2 C11_2 35.4(10) . . . . ?
C4_2 C3_2 C6_2 C7_2 33.8(10) . . . . ?
C2_2 C3_2 C6_2 C7_2 -145.9(7) . . . . ?
C11_2 C6_2 C7_2 C8_2 -0.4(11) . . . . ?
C3_2 C6_2 C7_2 C8_2 -179.1(7) . . . . ?
C6_2 C7_2 C8_2 C9_2 1.8(12) . . . . ?
C7_2 C8_2 C9_2 C10_2 -2.3(11) . . . . ?
C7_2 C8_2 C9_2 C12_2 179.8(7) . . . . ?
C8_2 C9_2 C10_2 C11_2 1.4(11) . . . . ?
C12_2 C9_2 C10_2 C11_2 179.3(6) . . . . ?
C7_2 C6_2 C11_2 C10_2 -0.5(10) . . . . ?
C3_2 C6_2 C11_2 C10_2 178.1(6) . . . . ?
C9_2 C10_2 C11_2 C6_2 0.1(11) . . . . ?
C8_2 C9_2 C12_2 C13_2 -139.0(7) . . . . ?
C10_2 C9_2 C12_2 C13_2 43.0(10) . . . . ?
C8_2 C9_2 C12_2 C16_2 40.4(10) . . . . ?
C10_2 C9_2 C12_2 C16_2 -137.6(7) . . . . ?
C16_2 C12_2 C13_2 C14_2 1.1(11) . . . . ?
C9_2 C12_2 C13_2 C14_2 -179.5(7) . . . . ?
C12_2 C13_2 C14_2 N2_2 -0.1(11) . . . . ?
N2_2 C15_2 C16_2 C12_2 1.3(11) . . . . ?
C13_2 C12_2 C16_2 C15_2 -1.6(11) . . . . ?
C9_2 C12_2 C16_2 C15_2 179.0(6) . . . . ?
C2_2 C1_2 N1_2 C5_2 1.2(10) . . . . ?
C2_2 C1_2 N1_2 Cu5 173.9(5) . . . 7 ?
C4_2 C5_2 N1_2 C1_2 -2.1(10) . . . . ?
C4_2 C5_2 N1_2 Cu5 -175.3(5) . . . 7 ?
C13_2 C14_2 N2_2 C15_2 -0.3(10) . . . . ?
C13_2 C14_2 N2_2 Cu2 170.7(5) . . . . ?
C16_2 C15_2 N2_2 C14_2 -0.3(10) . . . . ?
C16_2 C15_2 N2_2 Cu2 -171.4(5) . . . . ?
N1_3 C1_3 C2_3 C3_3 0.3(11) . . . . ?
C1_3 C2_3 C3_3 C4_3 -1.2(10) . . . . ?
C1_3 C2_3 C3_3 C6_3 -179.1(7) . . . . ?
C2_3 C3_3 C4_3 C5_3 1.3(10) . . . . ?
C6_3 C3_3 C4_3 C5_3 179.3(7) . . . . ?
C3_3 C4_3 C5_3 N1_3 -0.6(11) . . . . ?
C4_3 C3_3 C6_3 C11_3 -36.4(10) . . . . ?
C2_3 C3_3 C6_3 C11_3 141.4(7) . . . . ?
C4_3 C3_3 C6_3 C7_3 141.5(8) . . . . ?
C2_3 C3_3 C6_3 C7_3 -40.7(11) . . . . ?
C11_3 C6_3 C7_3 C8_3 1.4(11) . . . . ?
C3_3 C6_3 C7_3 C8_3 -176.5(7) . . . . ?
C6_3 C7_3 C8_3 C9_3 0.0(12) . . . . ?
C7_3 C8_3 C9_3 C10_3 -2.1(12) . . . . ?
C7_3 C8_3 C9_3 C12_3 -178.2(7) . . . . ?
C8_3 C9_3 C10_3 C11_3 2.8(12) . . . . ?
C12_3 C9_3 C10_3 C11_3 179.0(7) . . . . ?
C7_3 C6_3 C11_3 C10_3 -0.7(12) . . . . ?
C3_3 C6_3 C11_3 C10_3 177.3(7) . . . . ?
C9_3 C10_3 C11_3 C6_3 -1.4(13) . . . . ?
C10_3 C9_3 C12_3 C13_3 139.2(8) . . . . ?
C8_3 C9_3 C12_3 C13_3 -44.6(11) . . . . ?
C10_3 C9_3 C12_3 C16_3 -39.4(11) . . . . ?
C8_3 C9_3 C12_3 C16_3 136.7(8) . . . . ?
C16_3 C12_3 C13_3 C14_3 0.9(12) . . . . ?
C9_3 C12_3 C13_3 C14_3 -177.8(7) . . . . ?
C12_3 C13_3 C14_3 N2_3 -3.4(13) . . . . ?
N2_3 C15_3 C16_3 C12_3 -3.2(11) . . . . ?
C13_3 C12_3 C16_3 C15_3 2.2(11) . . . . ?
C9_3 C12_3 C16_3 C15_3 -179.1(7) . . . . ?
C4_3 C5_3 N1_3 C1_3 -0.4(10) . . . . ?
C4_3 C5_3 N1_3 Cu1 174.4(5) . . . . ?
C2_3 C1_3 N1_3 C5_3 0.5(10) . . . . ?
C2_3 C1_3 N1_3 Cu1 -174.0(5) . . . . ?
C13_3 C14_3 N2_3 C15_3 2.5(11) . . . . ?
C13_3 C14_3 N2_3 Cu5 -167.9(6) . . . . ?
C16_3 C15_3 N2_3 C14_3 0.9(11) . . . . ?
C16_3 C15_3 N2_3 Cu5 171.5(6) . . . . ?
N1_4 C1_4 C2_4 C3_4 1.1(12) . . . . ?
C1_4 C2_4 C3_4 C4_4 -2.1(11) . . . . ?
C1_4 C2_4 C3_4 C6_4 178.5(7) . . . . ?
C2_4 C3_4 C4_4 C5_4 2.7(10) . . . . ?
C6_4 C3_4 C4_4 C5_4 -177.9(7) . . . . ?
C3_4 C4_4 C5_4 N1_4 -2.3(11) . . . . ?
C2_4 C3_4 C6_4 C11_4 -40.8(11) . . . . ?
C4_4 C3_4 C6_4 C11_4 139.9(7) . . . . ?
C2_4 C3_4 C6_4 C7_4 139.4(8) . . . . ?
C4_4 C3_4 C6_4 C7_4 -40.0(10) . . . . ?
C11_4 C6_4 C7_4 C8_4 0.6(11) . . . . ?
C3_4 C6_4 C7_4 C8_4 -179.5(7) . . . . ?
C6_4 C7_4 C8_4 C9_4 -0.8(12) . . . . ?
C7_4 C8_4 C9_4 C10_4 0.0(11) . . . . ?
C7_4 C8_4 C9_4 C12_4 -179.6(7) . . . . ?
C8_4 C9_4 C10_4 C11_4 1.0(10) . . . . ?
C12_4 C9_4 C10_4 C11_4 -179.4(7) . . . . ?
C9_4 C10_4 C11_4 C6_4 -1.3(11) . . . . ?
C7_4 C6_4 C11_4 C10_4 0.5(10) . . . . ?
C3_4 C6_4 C11_4 C10_4 -179.4(7) . . . . ?
C8_4 C9_4 C12_4 C13_4 -33.7(10) . . . . ?
C10_4 C9_4 C12_4 C13_4 146.7(7) . . . . ?
C8_4 C9_4 C12_4 C16_4 146.9(7) . . . . ?
C10_4 C9_4 C12_4 C16_4 -32.7(10) . . . . ?
C16_4 C12_4 C13_4 C14_4 -0.8(10) . . . . ?
C9_4 C12_4 C13_4 C14_4 179.8(6) . . . . ?
C12_4 C13_4 C14_4 N2_4 -0.1(11) . . . . ?
N2_4 C15_4 C16_4 C12_4 -2.3(11) . . . . ?
C13_4 C12_4 C16_4 C15_4 1.9(10) . . . . ?
C9_4 C12_4 C16_4 C15_4 -178.7(6) . . . . ?
C2_4 C1_4 N1_4 C5_4 -0.5(11) . . . . ?
C2_4 C1_4 N1_4 Cu3 -171.2(6) . . . . ?
C4_4 C5_4 N1_4 C1_4 1.1(10) . . . . ?
C4_4 C5_4 N1_4 Cu3 172.0(5) . . . . ?
C16_4 C15_4 N2_4 C14_4 1.4(10) . . . . ?
C16_4 C15_4 N2_4 Cu6 -173.6(5) . . . . ?
C13_4 C14_4 N2_4 C15_4 -0.2(10) . . . . ?
C13_4 C14_4 N2_4 Cu6 175.1(5) . . . . ?
N1_5 C1_5 C2_5 C3_5 -0.3(11) . . . . ?
C1_5 C2_5 C3_5 C4_5 1.7(10) . . . . ?
C1_5 C2_5 C3_5 C6_5 -179.3(7) . . . . ?
C2_5 C3_5 C4_5 C5_5 -1.2(10) . . . . ?
C6_5 C3_5 C4_5 C5_5 179.7(6) . . . . ?
C3_5 C4_5 C5_5 N1_5 -0.6(11) . . . . ?
C2_5 C3_5 C6_5 C7_5 -148.9(7) . . . . ?
C4_5 C3_5 C6_5 C7_5 30.0(10) . . . . ?
C2_5 C3_5 C6_5 C11_5 30.8(10) . . . . ?
C4_5 C3_5 C6_5 C11_5 -150.2(7) . . . . ?
C11_5 C6_5 C7_5 C8_5 1.2(11) . . . . ?
C3_5 C6_5 C7_5 C8_5 -179.0(7) . . . . ?
C6_5 C7_5 C8_5 C9_5 -1.2(11) . . . . ?
C7_5 C8_5 C9_5 C10_5 1.0(11) . . . . ?
C7_5 C8_5 C9_5 C12_5 -178.7(7) . . . . ?
C8_5 C9_5 C10_5 C11_5 -1.0(11) . . . . ?
C12_5 C9_5 C10_5 C11_5 178.8(7) . . . . ?
C9_5 C10_5 C11_5 C6_5 1.1(11) . . . . ?
C7_5 C6_5 C11_5 C10_5 -1.2(10) . . . . ?
C3_5 C6_5 C11_5 C10_5 179.1(7) . . . . ?
C8_5 C9_5 C12_5 C16_5 148.7(7) . . . . ?
C10_5 C9_5 C12_5 C16_5 -31.0(10) . . . . ?
C8_5 C9_5 C12_5 C13_5 -30.6(10) . . . . ?
C10_5 C9_5 C12_5 C13_5 149.7(7) . . . . ?
C16_5 C12_5 C13_5 C14_5 1.1(10) . . . . ?
C9_5 C12_5 C13_5 C14_5 -179.5(6) . . . . ?
C12_5 C13_5 C14_5 N2_5 -0.9(11) . . . . ?
N2_5 C15_5 C16_5 C12_5 2.0(11) . . . . ?
C13_5 C12_5 C16_5 C15_5 -1.7(10) . . . . ?
C9_5 C12_5 C16_5 C15_5 179.0(6) . . . . ?
C2_5 C1_5 N1_5 C5_5 -1.5(10) . . . . ?
C2_5 C1_5 N1_5 Cu4 171.8(6) . . . . ?
C4_5 C5_5 N1_5 C1_5 1.9(10) . . . . ?
C4_5 C5_5 N1_5 Cu4 -171.6(5) . . . . ?
C13_5 C14_5 N2_5 C15_5 1.1(10) . . . . ?
C13_5 C14_5 N2_5 Cu6 -170.5(5) . . . . ?
C16_5 C15_5 N2_5 C14_5 -1.6(10) . . . . ?
C16_5 C15_5 N2_5 Cu6 170.2(5) . . . . ?
N1_6 C1_6 C2_6 C3_6 -1.4(11) . . . . ?
C1_6 C2_6 C3_6 C4_6 0.0(11) . . . . ?
C1_6 C2_6 C3_6 C6_6 178.5(7) . . . . ?
C2_6 C3_6 C4_6 C5_6 1.2(11) . . . . ?
C6_6 C3_6 C4_6 C5_6 -177.3(7) . . . . ?
C3_6 C4_6 C5_6 N1_6 -1.3(11) . . . . ?
C4_6 C3_6 C6_6 C7_6 140.9(8) . . . . ?
C2_6 C3_6 C6_6 C7_6 -37.5(11) . . . . ?
C4_6 C3_6 C6_6 C11_6 -36.4(11) . . . . ?
C2_6 C3_6 C6_6 C11_6 145.2(8) . . . . ?
C11_6 C6_6 C7_6 C8_6 0.5(13) . . . . ?
C3_6 C6_6 C7_6 C8_6 -176.9(8) . . . . ?
C6_6 C7_6 C8_6 C9_6 -1.4(13) . . . . ?
C7_6 C8_6 C9_6 C10_6 1.5(13) . . . . ?
C7_6 C8_6 C9_6 C12_6 179.8(8) . . . . ?
C8_6 C9_6 C10_6 C11_6 -0.7(12) . . . . ?
C12_6 C9_6 C10_6 C11_6 -179.1(7) . . . . ?
C9_6 C10_6 C11_6 C6_6 -0.1(12) . . . . ?
C7_6 C6_6 C11_6 C10_6 0.2(12) . . . . ?
C3_6 C6_6 C11_6 C10_6 177.6(7) . . . . ?
C10_6 C9_6 C12_6 C16_6 39.4(11) . . . . ?
C8_6 C9_6 C12_6 C16_6 -138.9(8) . . . . ?
C10_6 C9_6 C12_6 C13_6 -141.5(8) . . . . ?
C8_6 C9_6 C12_6 C13_6 40.2(11) . . . . ?
C16_6 C12_6 C13_6 C14_6 -3.5(11) . . . . ?
C9_6 C12_6 C13_6 C14_6 177.3(7) . . . . ?
C12_6 C13_6 C14_6 N2_6 2.9(11) . . . . ?
C13_6 C12_6 C16_6 C15_6 0.5(11) . . . . ?
C9_6 C12_6 C16_6 C15_6 179.7(7) . . . . ?
N2_6 C15_6 C16_6 C12_6 3.4(12) . . . . ?
C2_6 C1_6 N1_6 C5_6 1.4(10) . . . . ?
C2_6 C1_6 N1_6 Cu3 -175.6(6) . . . . ?
C4_6 C5_6 N1_6 C1_6 -0.1(10) . . . . ?
C4_6 C5_6 N1_6 Cu3 177.1(6) . . . . ?
C16_6 C15_6 N2_6 C14_6 -4.1(11) . . . . ?
C16_6 C15_6 N2_6 Cu6 168.4(6) . . . 7 ?
C13_6 C14_6 N2_6 C15_6 0.9(11) . . . . ?
C13_6 C14_6 N2_6 Cu6 -171.6(6) . . . 7 ?
N1_8 C1_8 C2_8 C3_8 1.3(12) . . . . ?
C1_8 C2_8 C3_8 C4_8 -1.1(11) . . . . ?
C1_8 C2_8 C3_8 C6_8 -179.9(7) . . . . ?
C2_8 C3_8 C4_8 C5_8 0.8(11) . . . . ?
C6_8 C3_8 C4_8 C5_8 179.5(7) . . . . ?
C3_8 C4_8 C5_8 N1_8 -0.5(11) . . . . ?
C2_8 C3_8 C6_8 C11_8 -146.0(8) . . . . ?
C4_8 C3_8 C6_8 C11_8 35.3(10) . . . . ?
C2_8 C3_8 C6_8 C7_8 34.4(11) . . . . ?
C4_8 C3_8 C6_8 C7_8 -144.3(7) . . . . ?
C11_8 C6_8 C7_8 C8_8 -0.3(11) . . . . ?
C3_8 C6_8 C7_8 C8_8 179.3(7) . . . . ?
C6_8 C7_8 C8_8 C9_8 2.7(12) . . . . ?
C7_8 C8_8 C9_8 C10_8 -4.2(11) . . . . ?
C7_8 C8_8 C9_8 C12_8 178.2(7) . . . . ?
C8_8 C9_8 C10_8 C11_8 3.3(11) . . . . ?
C12_8 C9_8 C10_8 C11_8 -178.9(7) . . . . ?
C9_8 C10_8 C11_8 C6_8 -1.0(12) . . . . ?
C7_8 C6_8 C11_8 C10_8 -0.6(11) . . . . ?
C3_8 C6_8 C11_8 C10_8 179.8(7) . . . . ?
C8_8 C9_8 C12_8 C16_8 -143.9(8) . . . . ?
C10_8 C9_8 C12_8 C16_8 38.5(10) . . . . ?
C8_8 C9_8 C12_8 C13_8 36.6(11) . . . . ?
C10_8 C9_8 C12_8 C13_8 -141.0(8) . . . . ?
C16_8 C12_8 C13_8 C14_8 1.2(10) . . . . ?
C9_8 C12_8 C13_8 C14_8 -179.2(7) . . . . ?
C12_8 C13_8 C14_8 N2_8 0.6(11) . . . . ?
C13_8 C12_8 C16_8 C15_8 -2.1(10) . . . . ?
C9_8 C12_8 C16_8 C15_8 178.3(7) . . . . ?
N2_8 C15_8 C16_8 C12_8 1.3(11) . . . . ?
C2_8 C1_8 N1_8 C5_8 -1.0(11) . . . . ?
C2_8 C1_8 N1_8 Cu6 170.1(6) . . . 7 ?
C4_8 C5_8 N1_8 C1_8 0.6(10) . . . . ?
C4_8 C5_8 N1_8 Cu6 -170.8(5) . . . 7 ?
C13_8 C14_8 N2_8 C15_8 -1.5(10) . . . . ?
C13_8 C14_8 N2_8 Cu4 173.6(5) . . . . ?
C16_8 C15_8 N2_8 C14_8 0.5(10) . . . . ?
C16_8 C15_8 N2_8 Cu4 -174.7(5) . . . . ?
N1_9 C1_9 C2_9 C3_9 0.3(11) . . . . ?
C1_9 C2_9 C3_9 C4_9 0.7(10) . . . . ?
C1_9 C2_9 C3_9 C6_9 179.8(6) . . . . ?
C2_9 C3_9 C4_9 C5_9 -1.0(10) . . . . ?
C6_9 C3_9 C4_9 C5_9 179.9(6) . . . . ?
C3_9 C4_9 C5_9 N1_9 0.2(11) . . . . ?
C2_9 C3_9 C6_9 C11_9 37.6(10) . . . . ?
C4_9 C3_9 C6_9 C11_9 -143.3(7) . . . . ?
C2_9 C3_9 C6_9 C7_9 -138.8(7) . . . . ?
C4_9 C3_9 C6_9 C7_9 40.3(10) . . . . ?
C11_9 C6_9 C7_9 C8_9 0.5(11) . . . . ?
C3_9 C6_9 C7_9 C8_9 176.8(6) . . . . ?
C6_9 C7_9 C8_9 C9_9 -1.2(11) . . . . ?
C7_9 C8_9 C9_9 C10_9 2.4(11) . . . . ?
C7_9 C8_9 C9_9 C12_9 179.2(6) . . . . ?
C8_9 C9_9 C10_9 C11_9 -2.9(11) . . . . ?
C12_9 C9_9 C10_9 C11_9 -179.7(7) . . . . ?
C9_9 C10_9 C11_9 C6_9 2.2(11) . . . . ?
C7_9 C6_9 C11_9 C10_9 -0.9(11) . . . . ?
C3_9 C6_9 C11_9 C10_9 -177.3(7) . . . . ?
C8_9 C9_9 C12_9 C16_9 151.1(7) . . . . ?
C10_9 C9_9 C12_9 C16_9 -32.1(10) . . . . ?
C8_9 C9_9 C12_9 C13_9 -30.4(10) . . . . ?
C10_9 C9_9 C12_9 C13_9 146.3(7) . . . . ?
C16_9 C12_9 C13_9 C14_9 1.5(10) . . . . ?
C9_9 C12_9 C13_9 C14_9 -177.0(6) . . . . ?
C12_9 C13_9 C14_9 N2_9 -0.3(11) . . . . ?
N2_9 C15_9 C16_9 C12_9 0.4(12) . . . . ?
C13_9 C12_9 C16_9 C15_9 -1.6(11) . . . . ?
C9_9 C12_9 C16_9 C15_9 176.9(7) . . . . ?
C2_9 C1_9 N1_9 C5_9 -1.1(10) . . . . ?
C2_9 C1_9 N1_9 Cu2 -175.1(6) . . . . ?
C4_9 C5_9 N1_9 C1_9 0.9(10) . . . . ?
C4_9 C5_9 N1_9 Cu2 174.5(5) . . . . ?
C16_9 C15_9 N2_9 C14_9 0.8(11) . . . . ?
C16_9 C15_9 N2_9 Cu5 -171.8(6) . . . . ?
C13_9 C14_9 N2_9 C15_9 -0.8(11) . . . . ?
C13_9 C14_9 N2_9 Cu5 171.9(5) . . . . ?
B4_10 B1_10 B2_10 B10_10 -0.9(8) . . . . ?
B3_10 B1_10 B2_10 B10_10 37.3(6) . . . . ?
B6_10 B1_10 B2_10 B10_10 -64.9(8) . . . . ?
B5_10 B1_10 B2_10 B10_10 -102.3(6) . . . . ?
Cl1_10 B1_10 B2_10 B10_10 149.0(6) . . . . ?
B4_10 B1_10 B2_10 B3_10 -38.3(6) . . . . ?
B6_10 B1_10 B2_10 B3_10 -102.2(6) . . . . ?
B5_10 B1_10 B2_10 B3_10 -139.6(6) . . . . ?
Cl1_10 B1_10 B2_10 B3_10 111.7(7) . . . . ?
B4_10 B1_10 B2_10 B5_10 101.4(6) . . . . ?
B3_10 B1_10 B2_10 B5_10 139.6(6) . . . . ?
B6_10 B1_10 B2_10 B5_10 37.5(6) . . . . ?
Cl1_10 B1_10 B2_10 B5_10 -108.7(7) . . . . ?
B4_10 B1_10 B2_10 B11_10 63.2(8) . . . . ?
B3_10 B1_10 B2_10 B11_10 101.4(6) . . . . ?
B6_10 B1_10 B2_10 B11_10 -0.8(8) . . . . ?
B5_10 B1_10 B2_10 B11_10 -38.2(6) . . . . ?
Cl1_10 B1_10 B2_10 B11_10 -146.9(6) . . . . ?
B4_10 B1_10 B2_10 Cl3_10 -153.1(6) . . . . ?
B3_10 B1_10 B2_10 Cl3_10 -114.8(7) . . . . ?
B6_10 B1_10 B2_10 Cl3_10 143.0(6) . . . . ?
B5_10 B1_10 B2_10 Cl3_10 105.6(7) . . . . ?
Cl1_10 B1_10 B2_10 Cl3_10 -3.1(10) . . . . ?
B6_10 B1_10 B3_10 B4_10 -37.6(6) . . . . ?
B2_10 B1_10 B3_10 B4_10 -137.6(6) . . . . ?
B5_10 B1_10 B3_10 B4_10 -101.4(6) . . . . ?
Cl1_10 B1_10 B3_10 B4_10 111.1(7) . . . . ?
B4_10 B1_10 B3_10 Cl4_10 -108.3(7) . . . . ?
B6_10 B1_10 B3_10 Cl4_10 -146.0(6) . . . . ?
B2_10 B1_10 B3_10 Cl4_10 114.0(7) . . . . ?
B5_10 B1_10 B3_10 Cl4_10 150.3(6) . . . . ?
Cl1_10 B1_10 B3_10 Cl4_10 2.7(9) . . . . ?
B4_10 B1_10 B3_10 B9_10 37.6(5) . . . . ?
B6_10 B1_10 B3_10 B9_10 0.0(8) . . . . ?
B2_10 B1_10 B3_10 B9_10 -100.0(6) . . . . ?
B5_10 B1_10 B3_10 B9_10 -63.7(7) . . . . ?
Cl1_10 B1_10 B3_10 B9_10 148.7(5) . . . . ?
B4_10 B1_10 B3_10 B2_10 137.6(6) . . . . ?
B6_10 B1_10 B3_10 B2_10 100.0(6) . . . . ?
B5_10 B1_10 B3_10 B2_10 36.2(5) . . . . ?
Cl1_10 B1_10 B3_10 B2_10 -111.3(7) . . . . ?
B4_10 B1_10 B3_10 B10_10 100.9(6) . . . . ?
B6_10 B1_10 B3_10 B10_10 63.3(7) . . . . ?
B2_10 B1_10 B3_10 B10_10 -36.7(5) . . . . ?
B5_10 B1_10 B3_10 B10_10 -0.5(7) . . . . ?
Cl1_10 B1_10 B3_10 B10_10 -148.0(5) . . . . ?
B10_10 B2_10 B3_10 B1_10 -138.8(6) . . . . ?
B5_10 B2_10 B3_10 B1_10 -36.3(5) . . . . ?
B11_10 B2_10 B3_10 B1_10 -100.4(6) . . . . ?
Cl3_10 B2_10 B3_10 B1_10 109.9(7) . . . . ?
B10_10 B2_10 B3_10 B4_10 -101.4(6) . . . . ?
B5_10 B2_10 B3_10 B4_10 1.0(7) . . . . ?
B11_10 B2_10 B3_10 B4_10 -63.1(7) . . . . ?
B1_10 B2_10 B3_10 B4_10 37.3(5) . . . . ?
Cl3_10 B2_10 B3_10 B4_10 147.2(6) . . . . ?
B10_10 B2_10 B3_10 Cl4_10 108.9(7) . . . . ?
B5_10 B2_10 B3_10 Cl4_10 -148.6(6) . . . . ?
B11_10 B2_10 B3_10 Cl4_10 147.2(6) . . . . ?
B1_10 B2_10 B3_10 Cl4_10 -112.3(7) . . . . ?
Cl3_10 B2_10 B3_10 Cl4_10 -2.4(10) . . . . ?
B10_10 B2_10 B3_10 B9_10 -37.3(5) . . . . ?
B5_10 B2_10 B3_10 B9_10 65.1(7) . . . . ?
B11_10 B2_10 B3_10 B9_10 1.0(7) . . . . ?
B1_10 B2_10 B3_10 B9_10 101.4(6) . . . . ?
Cl3_10 B2_10 B3_10 B9_10 -148.7(6) . . . . ?
B5_10 B2_10 B3_10 B10_10 102.5(6) . . . . ?
B11_10 B2_10 B3_10 B10_10 38.3(5) . . . . ?
B1_10 B2_10 B3_10 B10_10 138.8(6) . . . . ?
Cl3_10 B2_10 B3_10 B10_10 -111.4(7) . . . . ?
B3_10 B1_10 B4_10 B6_10 -138.4(6) . . . . ?
B2_10 B1_10 B4_10 B6_10 -100.3(6) . . . . ?
B5_10 B1_10 B4_10 B6_10 -36.9(5) . . . . ?
Cl1_10 B1_10 B4_10 B6_10 109.6(7) . . . . ?
B6_10 B1_10 B4_10 B3_10 138.4(6) . . . . ?
B2_10 B1_10 B4_10 B3_10 38.1(6) . . . . ?
B5_10 B1_10 B4_10 B3_10 101.5(6) . . . . ?
Cl1_10 B1_10 B4_10 B3_10 -112.0(7) . . . . ?
B3_10 B1_10 B4_10 B8_10 -100.7(6) . . . . ?
B6_10 B1_10 B4_10 B8_10 37.7(5) . . . . ?
B2_10 B1_10 B4_10 B8_10 -62.7(7) . . . . ?
B5_10 B1_10 B4_10 B8_10 0.8(8) . . . . ?
Cl1_10 B1_10 B4_10 B8_10 147.3(6) . . . . ?
B3_10 B1_10 B4_10 Cl6_10 109.7(7) . . . . ?
B6_10 B1_10 B4_10 Cl6_10 -111.9(7) . . . . ?
B2_10 B1_10 B4_10 Cl6_10 147.8(6) . . . . ?
B5_10 B1_10 B4_10 Cl6_10 -148.8(6) . . . . ?
Cl1_10 B1_10 B4_10 Cl6_10 -2.3(10) . . . . ?
B3_10 B1_10 B4_10 B9_10 -37.3(5) . . . . ?
B6_10 B1_10 B4_10 B9_10 101.1(6) . . . . ?
B2_10 B1_10 B4_10 B9_10 0.8(8) . . . . ?
B5_10 B1_10 B4_10 B9_10 64.2(7) . . . . ?
Cl1_10 B1_10 B4_10 B9_10 -149.2(6) . . . . ?
Cl4_10 B3_10 B4_10 B1_10 113.1(7) . . . . ?
B9_10 B3_10 B4_10 B1_10 -138.3(6) . . . . ?
B2_10 B3_10 B4_10 B1_10 -38.0(6) . . . . ?
B10_10 B3_10 B4_10 B1_10 -100.8(6) . . . . ?
B1_10 B3_10 B4_10 B6_10 37.6(6) . . . . ?
Cl4_10 B3_10 B4_10 B6_10 150.7(6) . . . . ?
B9_10 B3_10 B4_10 B6_10 -100.7(6) . . . . ?
B2_10 B3_10 B4_10 B6_10 -0.4(8) . . . . ?
B10_10 B3_10 B4_10 B6_10 -63.2(7) . . . . ?
B1_10 B3_10 B4_10 B8_10 101.7(6) . . . . ?
Cl4_10 B3_10 B4_10 B8_10 -145.2(6) . . . . ?
B9_10 B3_10 B4_10 B8_10 -36.6(5) . . . . ?
B2_10 B3_10 B4_10 B8_10 63.7(7) . . . . ?
B10_10 B3_10 B4_10 B8_10 0.9(8) . . . . ?
B1_10 B3_10 B4_10 Cl6_10 -112.5(7) . . . . ?
Cl4_10 B3_10 B4_10 Cl6_10 0.6(9) . . . . ?
B9_10 B3_10 B4_10 Cl6_10 109.2(7) . . . . ?
B2_10 B3_10 B4_10 Cl6_10 -150.6(5) . . . . ?
B10_10 B3_10 B4_10 Cl6_10 146.6(6) . . . . ?
B1_10 B3_10 B4_10 B9_10 138.3(6) . . . . ?
Cl4_10 B3_10 B4_10 B9_10 -108.6(6) . . . . ?
B2_10 B3_10 B4_10 B9_10 100.3(6) . . . . ?
B10_10 B3_10 B4_10 B9_10 37.5(5) . . . . ?
B10_10 B2_10 B5_10 Cl2_10 -146.7(6) . . . . ?
B3_10 B2_10 B5_10 Cl2_10 148.7(6) . . . . ?
B11_10 B2_10 B5_10 Cl2_10 -109.7(7) . . . . ?
B1_10 B2_10 B5_10 Cl2_10 112.8(7) . . . . ?
Cl3_10 B2_10 B5_10 Cl2_10 -0.5(9) . . . . ?
B10_10 B2_10 B5_10 B7_10 0.0(8) . . . . ?
B3_10 B2_10 B5_10 B7_10 -64.6(7) . . . . ?
B11_10 B2_10 B5_10 B7_10 37.1(5) . . . . ?
B1_10 B2_10 B5_10 B7_10 -100.5(6) . . . . ?
Cl3_10 B2_10 B5_10 B7_10 146.2(5) . . . . ?
B10_10 B2_10 B5_10 B6_10 63.3(7) . . . . ?
B3_10 B2_10 B5_10 B6_10 -1.3(7) . . . . ?
B11_10 B2_10 B5_10 B6_10 100.4(6) . . . . ?
B1_10 B2_10 B5_10 B6_10 -37.1(5) . . . . ?
Cl3_10 B2_10 B5_10 B6_10 -150.5(5) . . . . ?
B10_10 B2_10 B5_10 B1_10 100.5(6) . . . . ?
B3_10 B2_10 B5_10 B1_10 35.8(5) . . . . ?
B11_10 B2_10 B5_10 B1_10 137.5(6) . . . . ?
Cl3_10 B2_10 B5_10 B1_10 -113.4(6) . . . . ?
B10_10 B2_10 B5_10 B11_10 -37.0(5) . . . . ?
B3_10 B2_10 B5_10 B11_10 -101.7(6) . . . . ?
B1_10 B2_10 B5_10 B11_10 -137.5(6) . . . . ?
Cl3_10 B2_10 B5_10 B11_10 109.1(6) . . . . ?
B4_10 B1_10 B5_10 Cl2_10 150.5(6) . . . . ?
B3_10 B1_10 B5_10 Cl2_10 -145.0(6) . . . . ?
B6_10 B1_10 B5_10 Cl2_10 113.4(7) . . . . ?
B2_10 B1_10 B5_10 Cl2_10 -108.6(7) . . . . ?
Cl1_10 B1_10 B5_10 Cl2_10 3.4(9) . . . . ?
B4_10 B1_10 B5_10 B7_10 -0.3(8) . . . . ?
B3_10 B1_10 B5_10 B7_10 64.2(7) . . . . ?
B6_10 B1_10 B5_10 B7_10 -37.4(6) . . . . ?
B2_10 B1_10 B5_10 B7_10 100.6(6) . . . . ?
Cl1_10 B1_10 B5_10 B7_10 -147.4(6) . . . . ?
B4_10 B1_10 B5_10 B6_10 37.1(6) . . . . ?
B3_10 B1_10 B5_10 B6_10 101.5(6) . . . . ?
B2_10 B1_10 B5_10 B6_10 138.0(6) . . . . ?
Cl1_10 B1_10 B5_10 B6_10 -110.1(7) . . . . ?
B4_10 B1_10 B5_10 B2_10 -100.9(6) . . . . ?
B3_10 B1_10 B5_10 B2_10 -36.4(5) . . . . ?
B6_10 B1_10 B5_10 B2_10 -138.0(6) . . . . ?
Cl1_10 B1_10 B5_10 B2_10 112.0(6) . . . . ?
B4_10 B1_10 B5_10 B11_10 -63.1(7) . . . . ?
B3_10 B1_10 B5_10 B11_10 1.3(7) . . . . ?
B6_10 B1_10 B5_10 B11_10 -100.2(6) . . . . ?
B2_10 B1_10 B5_10 B11_10 37.8(5) . . . . ?
Cl1_10 B1_10 B5_10 B11_10 149.7(5) . . . . ?
B3_10 B4_10 B6_10 B1_10 -37.5(6) . . . . ?
B8_10 B4_10 B6_10 B1_10 -138.3(6) . . . . ?
Cl6_10 B4_10 B6_10 B1_10 112.1(7) . . . . ?
B9_10 B4_10 B6_10 B1_10 -101.0(6) . . . . ?
B1_10 B4_10 B6_10 B7_10 100.4(6) . . . . ?
B3_10 B4_10 B6_10 B7_10 62.9(8) . . . . ?
B8_10 B4_10 B6_10 B7_10 -37.9(5) . . . . ?
Cl6_10 B4_10 B6_10 B7_10 -147.5(5) . . . . ?
B9_10 B4_10 B6_10 B7_10 -0.6(8) . . . . ?
B1_10 B4_10 B6_10 B8_10 138.3(6) . . . . ?
B3_10 B4_10 B6_10 B8_10 100.8(6) . . . . ?
Cl6_10 B4_10 B6_10 B8_10 -109.6(7) . . . . ?
B9_10 B4_10 B6_10 B8_10 37.3(5) . . . . ?
B1_10 B4_10 B6_10 B5_10 37.1(6) . . . . ?
B3_10 B4_10 B6_10 B5_10 -0.4(8) . . . . ?
B8_10 B4_10 B6_10 B5_10 -101.2(6) . . . . ?
Cl6_10 B4_10 B6_10 B5_10 149.2(5) . . . . ?
B9_10 B4_10 B6_10 B5_10 -63.9(7) . . . . ?
B1_10 B4_10 B6_10 Cl5_10 -110.6(7) . . . . ?
B3_10 B4_10 B6_10 Cl5_10 -148.1(6) . . . . ?
B8_10 B4_10 B6_10 Cl5_10 111.1(7) . . . . ?
Cl6_10 B4_10 B6_10 Cl5_10 1.5(10) . . . . ?
B9_10 B4_10 B6_10 Cl5_10 148.4(5) . . . . ?
B3_10 B1_10 B6_10 B4_10 37.7(5) . . . . ?
B2_10 B1_10 B6_10 B4_10 101.5(6) . . . . ?
B5_10 B1_10 B6_10 B4_10 138.9(6) . . . . ?
Cl1_10 B1_10 B6_10 B4_10 -111.7(7) . . . . ?
B4_10 B1_10 B6_10 B7_10 -101.6(6) . . . . ?
B3_10 B1_10 B6_10 B7_10 -63.8(7) . . . . ?
B2_10 B1_10 B6_10 B7_10 0.0(8) . . . . ?
B5_10 B1_10 B6_10 B7_10 37.4(6) . . . . ?
Cl1_10 B1_10 B6_10 B7_10 146.8(6) . . . . ?
B4_10 B1_10 B6_10 B8_10 -37.0(5) . . . . ?
B3_10 B1_10 B6_10 B8_10 0.7(8) . . . . ?
B2_10 B1_10 B6_10 B8_10 64.5(7) . . . . ?
B5_10 B1_10 B6_10 B8_10 101.9(6) . . . . ?
Cl1_10 B1_10 B6_10 B8_10 -148.7(6) . . . . ?
B4_10 B1_10 B6_10 B5_10 -138.9(6) . . . . ?
B3_10 B1_10 B6_10 B5_10 -101.2(6) . . . . ?
B2_10 B1_10 B6_10 B5_10 -37.4(6) . . . . ?
Cl1_10 B1_10 B6_10 B5_10 109.4(7) . . . . ?
B4_10 B1_10 B6_10 Cl5_10 110.5(7) . . . . ?
B3_10 B1_10 B6_10 Cl5_10 148.2(6) . . . . ?
B2_10 B1_10 B6_10 Cl5_10 -148.0(6) . . . . ?
B5_10 B1_10 B6_10 Cl5_10 -110.6(7) . . . . ?
Cl1_10 B1_10 B6_10 Cl5_10 -1.2(9) . . . . ?
Cl2_10 B5_10 B6_10 B4_10 -147.4(6) . . . . ?
B7_10 B5_10 B6_10 B4_10 101.8(6) . . . . ?
B2_10 B5_10 B6_10 B4_10 1.1(8) . . . . ?
B1_10 B5_10 B6_10 B4_10 -36.3(6) . . . . ?
B11_10 B5_10 B6_10 B4_10 64.1(7) . . . . ?
Cl2_10 B5_10 B6_10 B1_10 -111.0(7) . . . . ?
B7_10 B5_10 B6_10 B1_10 138.1(6) . . . . ?
B2_10 B5_10 B6_10 B1_10 37.4(5) . . . . ?
B11_10 B5_10 B6_10 B1_10 100.4(6) . . . . ?
Cl2_10 B5_10 B6_10 B7_10 110.9(7) . . . . ?
B2_10 B5_10 B6_10 B7_10 -100.7(6) . . . . ?
B1_10 B5_10 B6_10 B7_10 -138.1(6) . . . . ?
B11_10 B5_10 B6_10 B7_10 -37.7(5) . . . . ?
Cl2_10 B5_10 B6_10 B8_10 149.2(6) . . . . ?
B7_10 B5_10 B6_10 B8_10 38.4(6) . . . . ?
B2_10 B5_10 B6_10 B8_10 -62.3(7) . . . . ?
B1_10 B5_10 B6_10 B8_10 -99.7(6) . . . . ?
B11_10 B5_10 B6_10 B8_10 0.7(8) . . . . ?
Cl2_10 B5_10 B6_10 Cl5_10 0.5(10) . . . . ?
B7_10 B5_10 B6_10 Cl5_10 -110.4(7) . . . . ?
B2_10 B5_10 B6_10 Cl5_10 148.9(6) . . . . ?
B1_10 B5_10 B6_10 Cl5_10 111.5(7) . . . . ?
B11_10 B5_10 B6_10 Cl5_10 -148.1(6) . . . . ?
Cl2_10 B5_10 B7_10 Cl11_10 -3.8(9) . . . . ?
B6_10 B5_10 B7_10 Cl11_10 110.0(7) . . . . ?
B2_10 B5_10 B7_10 Cl11_10 -149.7(5) . . . . ?
B1_10 B5_10 B7_10 Cl11_10 147.1(5) . . . . ?
B11_10 B5_10 B7_10 Cl11_10 -112.5(6) . . . . ?
Cl2_10 B5_10 B7_10 B11_10 108.7(7) . . . . ?
B6_10 B5_10 B7_10 B11_10 -137.4(6) . . . . ?
B2_10 B5_10 B7_10 B11_10 -37.1(5) . . . . ?
B1_10 B5_10 B7_10 B11_10 -100.4(6) . . . . ?
Cl2_10 B5_10 B7_10 B6_10 -113.9(7) . . . . ?
B2_10 B5_10 B7_10 B6_10 100.3(6) . . . . ?
B1_10 B5_10 B7_10 B6_10 37.1(6) . . . . ?
B11_10 B5_10 B7_10 B6_10 137.4(6) . . . . ?
Cl2_10 B5_10 B7_10 B12_10 146.7(6) . . . . ?
B6_10 B5_10 B7_10 B12_10 -99.4(6) . . . . ?
B2_10 B5_10 B7_10 B12_10 0.9(8) . . . . ?
B1_10 B5_10 B7_10 B12_10 -62.4(7) . . . . ?
B11_10 B5_10 B7_10 B12_10 38.0(5) . . . . ?
Cl2_10 B5_10 B7_10 B8_10 -151.3(5) . . . . ?
B6_10 B5_10 B7_10 B8_10 -37.4(5) . . . . ?
B2_10 B5_10 B7_10 B8_10 62.9(7) . . . . ?
B1_10 B5_10 B7_10 B8_10 -0.3(8) . . . . ?
B11_10 B5_10 B7_10 B8_10 100.1(6) . . . . ?
B4_10 B6_10 B7_10 Cl11_10 151.0(5) . . . . ?
B1_10 B6_10 B7_10 Cl11_10 -146.4(6) . . . . ?
B8_10 B6_10 B7_10 Cl11_10 113.6(6) . . . . ?
B5_10 B6_10 B7_10 Cl11_10 -108.6(6) . . . . ?
Cl5_10 B6_10 B7_10 Cl11_10 1.7(9) . . . . ?
B4_10 B6_10 B7_10 B5_10 -100.4(6) . . . . ?
B1_10 B6_10 B7_10 B5_10 -37.8(6) . . . . ?
B8_10 B6_10 B7_10 B5_10 -137.8(6) . . . . ?
Cl5_10 B6_10 B7_10 B5_10 110.4(7) . . . . ?
B4_10 B6_10 B7_10 B11_10 -61.8(7) . . . . ?
B1_10 B6_10 B7_10 B11_10 0.8(8) . . . . ?
B8_10 B6_10 B7_10 B11_10 -99.2(6) . . . . ?
B5_10 B6_10 B7_10 B11_10 38.6(5) . . . . ?
Cl5_10 B6_10 B7_10 B11_10 149.0(6) . . . . ?
B4_10 B6_10 B7_10 B12_10 1.0(8) . . . . ?
B1_10 B6_10 B7_10 B12_10 63.6(7) . . . . ?
B8_10 B6_10 B7_10 B12_10 -36.4(5) . . . . ?
B5_10 B6_10 B7_10 B12_10 101.4(6) . . . . ?
Cl5_10 B6_10 B7_10 B12_10 -148.2(6) . . . . ?
B4_10 B6_10 B7_10 B8_10 37.4(5) . . . . ?
B1_10 B6_10 B7_10 B8_10 100.0(6) . . . . ?
B5_10 B6_10 B7_10 B8_10 137.8(6) . . . . ?
Cl5_10 B6_10 B7_10 B8_10 -111.8(7) . . . . ?
B1_10 B4_10 B8_10 B12_10 62.9(7) . . . . ?
B6_10 B4_10 B8_10 B12_10 100.7(6) . . . . ?
B3_10 B4_10 B8_10 B12_10 -1.0(8) . . . . ?
Cl6_10 B4_10 B8_10 B12_10 -146.8(6) . . . . ?
B9_10 B4_10 B8_10 B12_10 -37.6(5) . . . . ?
B1_10 B4_10 B8_10 B6_10 -37.7(5) . . . . ?
B3_10 B4_10 B8_10 B6_10 -101.6(6) . . . . ?
Cl6_10 B4_10 B8_10 B6_10 112.5(7) . . . . ?
B9_10 B4_10 B8_10 B6_10 -138.2(6) . . . . ?
B1_10 B4_10 B8_10 B9_10 100.5(6) . . . . ?
B6_10 B4_10 B8_10 B9_10 138.2(6) . . . . ?
B3_10 B4_10 B8_10 B9_10 36.6(5) . . . . ?
Cl6_10 B4_10 B8_10 B9_10 -109.2(7) . . . . ?
B1_10 B4_10 B8_10 Cl12_10 -147.6(6) . . . . ?
B6_10 B4_10 B8_10 Cl12_10 -109.9(7) . . . . ?
B3_10 B4_10 B8_10 Cl12_10 148.5(6) . . . . ?
Cl6_10 B4_10 B8_10 Cl12_10 2.7(9) . . . . ?
B9_10 B4_10 B8_10 Cl12_10 111.9(7) . . . . ?
B1_10 B4_10 B8_10 B7_10 -1.0(7) . . . . ?
B6_10 B4_10 B8_10 B7_10 36.8(5) . . . . ?
B3_10 B4_10 B8_10 B7_10 -64.8(7) . . . . ?
Cl6_10 B4_10 B8_10 B7_10 149.3(5) . . . . ?
B9_10 B4_10 B8_10 B7_10 -101.5(6) . . . . ?
B1_10 B6_10 B8_10 B4_10 36.6(5) . . . . ?
B7_10 B6_10 B8_10 B4_10 138.4(6) . . . . ?
B5_10 B6_10 B8_10 B4_10 100.7(6) . . . . ?
Cl5_10 B6_10 B8_10 B4_10 -110.8(7) . . . . ?
B4_10 B6_10 B8_10 B12_10 -101.0(6) . . . . ?
B1_10 B6_10 B8_10 B12_10 -64.3(7) . . . . ?
B7_10 B6_10 B8_10 B12_10 37.4(6) . . . . ?
B5_10 B6_10 B8_10 B12_10 -0.3(8) . . . . ?
Cl5_10 B6_10 B8_10 B12_10 148.2(6) . . . . ?
B4_10 B6_10 B8_10 B9_10 -37.8(5) . . . . ?
B1_10 B6_10 B8_10 B9_10 -1.2(7) . . . . ?
B7_10 B6_10 B8_10 B9_10 100.6(6) . . . . ?
B5_10 B6_10 B8_10 B9_10 62.9(7) . . . . ?
Cl5_10 B6_10 B8_10 B9_10 -148.6(6) . . . . ?
B4_10 B6_10 B8_10 Cl12_10 110.9(7) . . . . ?
B1_10 B6_10 B8_10 Cl12_10 147.5(6) . . . . ?
B7_10 B6_10 B8_10 Cl12_10 -110.7(7) . . . . ?
B5_10 B6_10 B8_10 Cl12_10 -148.4(6) . . . . ?
Cl5_10 B6_10 B8_10 Cl12_10 0.1(10) . . . . ?
B4_10 B6_10 B8_10 B7_10 -138.4(6) . . . . ?
B1_10 B6_10 B8_10 B7_10 -101.7(6) . . . . ?
B5_10 B6_10 B8_10 B7_10 -37.7(6) . . . . ?
Cl5_10 B6_10 B8_10 B7_10 110.8(7) . . . . ?
Cl11_10 B7_10 B8_10 B4_10 -144.9(6) . . . . ?
B5_10 B7_10 B8_10 B4_10 0.8(7) . . . . ?
B11_10 B7_10 B8_10 B4_10 65.0(7) . . . . ?
B6_10 B7_10 B8_10 B4_10 -36.9(5) . . . . ?
B12_10 B7_10 B8_10 B4_10 101.5(6) . . . . ?
Cl11_10 B7_10 B8_10 B12_10 113.6(7) . . . . ?
B5_10 B7_10 B8_10 B12_10 -100.7(6) . . . . ?
B11_10 B7_10 B8_10 B12_10 -36.5(5) . . . . ?
B6_10 B7_10 B8_10 B12_10 -138.4(6) . . . . ?
Cl11_10 B7_10 B8_10 B6_10 -108.0(7) . . . . ?
B5_10 B7_10 B8_10 B6_10 37.7(5) . . . . ?
B11_10 B7_10 B8_10 B6_10 101.9(6) . . . . ?
B12_10 B7_10 B8_10 B6_10 138.4(6) . . . . ?
Cl11_10 B7_10 B8_10 B9_10 150.9(6) . . . . ?
B5_10 B7_10 B8_10 B9_10 -63.4(7) . . . . ?
B11_10 B7_10 B8_10 B9_10 0.8(7) . . . . ?
B6_10 B7_10 B8_10 B9_10 -101.1(6) . . . . ?
B12_10 B7_10 B8_10 B9_10 37.3(5) . . . . ?
Cl11_10 B7_10 B8_10 Cl12_10 1.7(9) . . . . ?
B5_10 B7_10 B8_10 Cl12_10 147.4(5) . . . . ?
B11_10 B7_10 B8_10 Cl12_10 -148.4(5) . . . . ?
B6_10 B7_10 B8_10 Cl12_10 109.7(6) . . . . ?
B12_10 B7_10 B8_10 Cl12_10 -111.9(6) . . . . ?
B4_10 B8_10 B9_10 B12_10 -137.8(6) . . . . ?
B6_10 B8_10 B9_10 B12_10 -100.5(6) . . . . ?
Cl12_10 B8_10 B9_10 B12_10 111.3(6) . . . . ?
B7_10 B8_10 B9_10 B12_10 -37.6(5) . . . . ?
B4_10 B8_10 B9_10 Cl7_10 114.0(6) . . . . ?
B12_10 B8_10 B9_10 Cl7_10 -108.2(6) . . . . ?
B6_10 B8_10 B9_10 Cl7_10 151.3(5) . . . . ?
Cl12_10 B8_10 B9_10 Cl7_10 3.1(9) . . . . ?
B7_10 B8_10 B9_10 Cl7_10 -145.8(5) . . . . ?
B4_10 B8_10 B9_10 B3_10 -36.2(5) . . . . ?
B12_10 B8_10 B9_10 B3_10 101.7(6) . . . . ?
B6_10 B8_10 B9_10 B3_10 1.2(7) . . . . ?
Cl12_10 B8_10 B9_10 B3_10 -147.0(5) . . . . ?
B7_10 B8_10 B9_10 B3_10 64.0(7) . . . . ?
B4_10 B8_10 B9_10 B10_10 -100.3(6) . . . . ?
B12_10 B8_10 B9_10 B10_10 37.5(5) . . . . ?
B6_10 B8_10 B9_10 B10_10 -63.0(7) . . . . ?
Cl12_10 B8_10 B9_10 B10_10 148.8(5) . . . . ?
B7_10 B8_10 B9_10 B10_10 -0.1(7) . . . . ?
B12_10 B8_10 B9_10 B4_10 137.8(6) . . . . ?
B6_10 B8_10 B9_10 B4_10 37.3(5) . . . . ?
Cl12_10 B8_10 B9_10 B4_10 -110.9(6) . . . . ?
B7_10 B8_10 B9_10 B4_10 100.2(6) . . . . ?
B1_10 B3_10 B9_10 B12_10 62.7(7) . . . . ?
B4_10 B3_10 B9_10 B12_10 99.6(6) . . . . ?
Cl4_10 B3_10 B9_10 B12_10 -149.6(5) . . . . ?
B2_10 B3_10 B9_10 B12_10 -1.3(7) . . . . ?
B10_10 B3_10 B9_10 B12_10 -38.5(5) . . . . ?
B1_10 B3_10 B9_10 Cl7_10 -150.1(5) . . . . ?
B4_10 B3_10 B9_10 Cl7_10 -113.2(6) . . . . ?
Cl4_10 B3_10 B9_10 Cl7_10 -2.5(9) . . . . ?
B2_10 B3_10 B9_10 Cl7_10 145.9(5) . . . . ?
B10_10 B3_10 B9_10 Cl7_10 108.7(6) . . . . ?
B1_10 B3_10 B9_10 B8_10 -0.7(7) . . . . ?
B4_10 B3_10 B9_10 B8_10 36.2(5) . . . . ?
Cl4_10 B3_10 B9_10 B8_10 146.9(5) . . . . ?
B2_10 B3_10 B9_10 B8_10 -64.7(7) . . . . ?
B10_10 B3_10 B9_10 B8_10 -101.9(6) . . . . ?
B1_10 B3_10 B9_10 B10_10 101.2(6) . . . . ?
B4_10 B3_10 B9_10 B10_10 138.1(6) . . . . ?
Cl4_10 B3_10 B9_10 B10_10 -111.2(6) . . . . ?
B2_10 B3_10 B9_10 B10_10 37.2(5) . . . . ?
B1_10 B3_10 B9_10 B4_10 -36.9(5) . . . . ?
Cl4_10 B3_10 B9_10 B4_10 110.8(6) . . . . ?
B2_10 B3_10 B9_10 B4_10 -100.8(6) . . . . ?
B10_10 B3_10 B9_10 B4_10 -138.1(6) . . . . ?
B1_10 B4_10 B9_10 B12_10 -64.2(7) . . . . ?
B6_10 B4_10 B9_10 B12_10 0.0(7) . . . . ?
B3_10 B4_10 B9_10 B12_10 -101.6(6) . . . . ?
B8_10 B4_10 B9_10 B12_10 37.5(5) . . . . ?
Cl6_10 B4_10 B9_10 B12_10 147.9(5) . . . . ?
B1_10 B4_10 B9_10 Cl7_10 149.1(6) . . . . ?
B6_10 B4_10 B9_10 Cl7_10 -146.8(6) . . . . ?
B3_10 B4_10 B9_10 Cl7_10 111.7(7) . . . . ?
B8_10 B4_10 B9_10 Cl7_10 -109.2(7) . . . . ?
Cl6_10 B4_10 B9_10 Cl7_10 1.1(9) . . . . ?
B1_10 B4_10 B9_10 B8_10 -101.7(6) . . . . ?
B6_10 B4_10 B9_10 B8_10 -37.6(5) . . . . ?
B3_10 B4_10 B9_10 B8_10 -139.1(6) . . . . ?
Cl6_10 B4_10 B9_10 B8_10 110.3(6) . . . . ?
B1_10 B4_10 B9_10 B3_10 37.4(6) . . . . ?
B6_10 B4_10 B9_10 B3_10 101.5(6) . . . . ?
B8_10 B4_10 B9_10 B3_10 139.1(6) . . . . ?
Cl6_10 B4_10 B9_10 B3_10 -110.6(7) . . . . ?
B1_10 B4_10 B9_10 B10_10 -0.4(8) . . . . ?
B6_10 B4_10 B9_10 B10_10 63.7(7) . . . . ?
B3_10 B4_10 B9_10 B10_10 -37.8(5) . . . . ?
B8_10 B4_10 B9_10 B10_10 101.3(6) . . . . ?
Cl6_10 B4_10 B9_10 B10_10 -148.4(6) . . . . ?
B3_10 B2_10 B10_10 Cl8_10 -110.5(7) . . . . ?
B5_10 B2_10 B10_10 Cl8_10 148.9(6) . . . . ?
B11_10 B2_10 B10_10 Cl8_10 111.9(7) . . . . ?
B1_10 B2_10 B10_10 Cl8_10 -147.1(6) . . . . ?
Cl3_10 B2_10 B10_10 Cl8_10 4.9(9) . . . . ?
B3_10 B2_10 B10_10 B9_10 37.3(5) . . . . ?
B5_10 B2_10 B10_10 B9_10 -63.3(7) . . . . ?
B11_10 B2_10 B10_10 B9_10 -100.3(6) . . . . ?
B1_10 B2_10 B10_10 B9_10 0.7(8) . . . . ?
Cl3_10 B2_10 B10_10 B9_10 152.7(5) . . . . ?
B3_10 B2_10 B10_10 B12_10 99.7(6) . . . . ?
B5_10 B2_10 B10_10 B12_10 -0.9(7) . . . . ?
B11_10 B2_10 B10_10 B12_10 -37.9(5) . . . . ?
B1_10 B2_10 B10_10 B12_10 63.1(7) . . . . ?
Cl3_10 B2_10 B10_10 B12_10 -144.9(6) . . . . ?
B3_10 B2_10 B10_10 B11_10 137.6(6) . . . . ?
B5_10 B2_10 B10_10 B11_10 37.0(5) . . . . ?
B1_10 B2_10 B10_10 B11_10 101.0(6) . . . . ?
Cl3_10 B2_10 B10_10 B11_10 -107.0(7) . . . . ?
B5_10 B2_10 B10_10 B3_10 -100.6(6) . . . . ?
B11_10 B2_10 B10_10 B3_10 -137.6(6) . . . . ?
B1_10 B2_10 B10_10 B3_10 -36.6(6) . . . . ?
Cl3_10 B2_10 B10_10 B3_10 115.4(7) . . . . ?
B12_10 B9_10 B10_10 Cl8_10 -111.9(7) . . . . ?
Cl7_10 B9_10 B10_10 Cl8_10 -3.0(9) . . . . ?
B8_10 B9_10 B10_10 Cl8_10 -149.2(6) . . . . ?
B3_10 B9_10 B10_10 Cl8_10 110.8(7) . . . . ?
B4_10 B9_10 B10_10 Cl8_10 147.9(6) . . . . ?
B12_10 B9_10 B10_10 B2_10 99.9(6) . . . . ?
Cl7_10 B9_10 B10_10 B2_10 -151.2(5) . . . . ?
B8_10 B9_10 B10_10 B2_10 62.6(7) . . . . ?
B3_10 B9_10 B10_10 B2_10 -37.4(5) . . . . ?
B4_10 B9_10 B10_10 B2_10 -0.2(7) . . . . ?
Cl7_10 B9_10 B10_10 B12_10 108.9(6) . . . . ?
B8_10 B9_10 B10_10 B12_10 -37.3(5) . . . . ?
B3_10 B9_10 B10_10 B12_10 -137.3(6) . . . . ?
B4_10 B9_10 B10_10 B12_10 -100.1(6) . . . . ?
B12_10 B9_10 B10_10 B11_10 36.8(5) . . . . ?
Cl7_10 B9_10 B10_10 B11_10 145.6(6) . . . . ?
B8_10 B9_10 B10_10 B11_10 -0.6(8) . . . . ?
B3_10 B9_10 B10_10 B11_10 -100.6(6) . . . . ?
B4_10 B9_10 B10_10 B11_10 -63.4(7) . . . . ?
B12_10 B9_10 B10_10 B3_10 137.3(6) . . . . ?
Cl7_10 B9_10 B10_10 B3_10 -113.8(6) . . . . ?
B8_10 B9_10 B10_10 B3_10 100.0(6) . . . . ?
B4_10 B9_10 B10_10 B3_10 37.2(5) . . . . ?
B1_10 B3_10 B10_10 Cl8_10 149.0(6) . . . . ?
B4_10 B3_10 B10_10 Cl8_10 -148.4(6) . . . . ?
Cl4_10 B3_10 B10_10 Cl8_10 -2.6(9) . . . . ?
B9_10 B3_10 B10_10 Cl8_10 -110.4(7) . . . . ?
B2_10 B3_10 B10_10 Cl8_10 111.7(7) . . . . ?
B1_10 B3_10 B10_10 B2_10 37.3(5) . . . . ?
B4_10 B3_10 B10_10 B2_10 99.9(6) . . . . ?
Cl4_10 B3_10 B10_10 B2_10 -114.3(7) . . . . ?
B9_10 B3_10 B10_10 B2_10 137.9(6) . . . . ?
B1_10 B3_10 B10_10 B9_10 -100.6(6) . . . . ?
B4_10 B3_10 B10_10 B9_10 -38.0(5) . . . . ?
Cl4_10 B3_10 B10_10 B9_10 107.9(6) . . . . ?
B2_10 B3_10 B10_10 B9_10 -137.9(6) . . . . ?
B1_10 B3_10 B10_10 B12_10 -63.1(7) . . . . ?
B4_10 B3_10 B10_10 B12_10 -0.5(7) . . . . ?
Cl4_10 B3_10 B10_10 B12_10 145.4(5) . . . . ?
B9_10 B3_10 B10_10 B12_10 37.5(5) . . . . ?
B2_10 B3_10 B10_10 B12_10 -100.4(6) . . . . ?
B1_10 B3_10 B10_10 B11_10 -0.5(8) . . . . ?
B4_10 B3_10 B10_10 B11_10 62.1(7) . . . . ?
Cl4_10 B3_10 B10_10 B11_10 -152.1(6) . . . . ?
B9_10 B3_10 B10_10 B11_10 100.1(6) . . . . ?
B2_10 B3_10 B10_10 B11_10 -37.8(5) . . . . ?
Cl11_10 B7_10 B11_10 B12_10 -114.6(6) . . . . ?
B5_10 B7_10 B11_10 B12_10 137.2(6) . . . . ?
B6_10 B7_10 B11_10 B12_10 98.9(6) . . . . ?
B8_10 B7_10 B11_10 B12_10 36.1(5) . . . . ?
Cl11_10 B7_10 B11_10 B2_10 145.3(5) . . . . ?
B5_10 B7_10 B11_10 B2_10 37.0(6) . . . . ?
B6_10 B7_10 B11_10 B2_10 -1.3(8) . . . . ?
B12_10 B7_10 B11_10 B2_10 -100.2(6) . . . . ?
B8_10 B7_10 B11_10 B2_10 -64.0(7) . . . . ?
Cl11_10 B7_10 B11_10 Cl10_10 -5.2(9) . . . . ?
B5_10 B7_10 B11_10 Cl10_10 -113.4(7) . . . . ?
B6_10 B7_10 B11_10 Cl10_10 -151.7(6) . . . . ?
B12_10 B7_10 B11_10 Cl10_10 109.4(7) . . . . ?
B8_10 B7_10 B11_10 Cl10_10 145.5(6) . . . . ?
Cl11_10 B7_10 B11_10 B10_10 -151.9(6) . . . . ?
B5_10 B7_10 B11_10 B10_10 99.9(6) . . . . ?
B6_10 B7_10 B11_10 B10_10 61.6(7) . . . . ?
B12_10 B7_10 B11_10 B10_10 -37.3(6) . . . . ?
B8_10 B7_10 B11_10 B10_10 -1.1(8) . . . . ?
Cl11_10 B7_10 B11_10 B5_10 108.2(7) . . . . ?
B6_10 B7_10 B11_10 B5_10 -38.3(6) . . . . ?
B12_10 B7_10 B11_10 B5_10 -137.2(6) . . . . ?
B8_10 B7_10 B11_10 B5_10 -101.0(6) . . . . ?
B10_10 B2_10 B11_10 B7_10 102.4(6) . . . . ?
B3_10 B2_10 B11_10 B7_10 63.9(7) . . . . ?
B5_10 B2_10 B11_10 B7_10 -36.9(5) . . . . ?
B1_10 B2_10 B11_10 B7_10 1.2(8) . . . . ?
Cl3_10 B2_10 B11_10 B7_10 -144.1(5) . . . . ?
B10_10 B2_10 B11_10 B12_10 38.1(5) . . . . ?
B3_10 B2_10 B11_10 B12_10 -0.3(7) . . . . ?
B5_10 B2_10 B11_10 B12_10 -101.1(6) . . . . ?
B1_10 B2_10 B11_10 B12_10 -63.0(7) . . . . ?
Cl3_10 B2_10 B11_10 B12_10 151.7(6) . . . . ?
B10_10 B2_10 B11_10 Cl10_10 -107.0(7) . . . . ?
B3_10 B2_10 B11_10 Cl10_10 -145.5(6) . . . . ?
B5_10 B2_10 B11_10 Cl10_10 113.7(7) . . . . ?
B1_10 B2_10 B11_10 Cl10_10 151.8(6) . . . . ?
Cl3_10 B2_10 B11_10 Cl10_10 6.5(9) . . . . ?
B3_10 B2_10 B11_10 B10_10 -38.4(5) . . . . ?
B5_10 B2_10 B11_10 B10_10 -139.2(6) . . . . ?
B1_10 B2_10 B11_10 B10_10 -101.1(6) . . . . ?
Cl3_10 B2_10 B11_10 B10_10 113.6(6) . . . . ?
B10_10 B2_10 B11_10 B5_10 139.2(6) . . . . ?
B3_10 B2_10 B11_10 B5_10 100.8(6) . . . . ?
B1_10 B2_10 B11_10 B5_10 38.1(6) . . . . ?
Cl3_10 B2_10 B11_10 B5_10 -107.2(6) . . . . ?
Cl8_10 B10_10 B11_10 B7_10 149.3(5) . . . . ?
B2_10 B10_10 B11_10 B7_10 -99.3(6) . . . . ?
B9_10 B10_10 B11_10 B7_10 1.1(8) . . . . ?
B12_10 B10_10 B11_10 B7_10 37.7(6) . . . . ?
B3_10 B10_10 B11_10 B7_10 -61.6(7) . . . . ?
Cl8_10 B10_10 B11_10 B12_10 111.5(7) . . . . ?
B2_10 B10_10 B11_10 B12_10 -137.0(6) . . . . ?
B9_10 B10_10 B11_10 B12_10 -36.7(5) . . . . ?
B3_10 B10_10 B11_10 B12_10 -99.4(6) . . . . ?
Cl8_10 B10_10 B11_10 B2_10 -111.5(7) . . . . ?
B9_10 B10_10 B11_10 B2_10 100.3(6) . . . . ?
B12_10 B10_10 B11_10 B2_10 137.0(6) . . . . ?
B3_10 B10_10 B11_10 B2_10 37.6(5) . . . . ?
Cl8_10 B10_10 B11_10 Cl10_10 1.1(10) . . . . ?
B2_10 B10_10 B11_10 Cl10_10 112.6(6) . . . . ?
B9_10 B10_10 B11_10 Cl10_10 -147.1(5) . . . . ?
B12_10 B10_10 B11_10 Cl10_10 -110.4(7) . . . . ?
B3_10 B10_10 B11_10 Cl10_10 150.2(5) . . . . ?
Cl8_10 B10_10 B11_10 B5_10 -147.8(6) . . . . ?
B2_10 B10_10 B11_10 B5_10 -36.3(5) . . . . ?
B9_10 B10_10 B11_10 B5_10 64.0(7) . . . . ?
B12_10 B10_10 B11_10 B5_10 100.7(6) . . . . ?
B3_10 B10_10 B11_10 B5_10 1.3(8) . . . . ?
Cl2_10 B5_10 B11_10 B7_10 -112.2(6) . . . . ?
B6_10 B5_10 B11_10 B7_10 37.9(5) . . . . ?
B2_10 B5_10 B11_10 B7_10 138.3(6) . . . . ?
B1_10 B5_10 B11_10 B7_10 100.5(6) . . . . ?
Cl2_10 B5_10 B11_10 B12_10 -150.9(5) . . . . ?
B7_10 B5_10 B11_10 B12_10 -38.7(6) . . . . ?
B6_10 B5_10 B11_10 B12_10 -0.8(8) . . . . ?
B2_10 B5_10 B11_10 B12_10 99.6(6) . . . . ?
B1_10 B5_10 B11_10 B12_10 61.8(7) . . . . ?
Cl2_10 B5_10 B11_10 B2_10 109.5(6) . . . . ?
B7_10 B5_10 B11_10 B2_10 -138.3(6) . . . . ?
B6_10 B5_10 B11_10 B2_10 -100.4(6) . . . . ?
B1_10 B5_10 B11_10 B2_10 -37.8(5) . . . . ?
Cl2_10 B5_10 B11_10 Cl10_10 -1.1(9) . . . . ?
B7_10 B5_10 B11_10 Cl10_10 111.0(7) . . . . ?
B6_10 B5_10 B11_10 Cl10_10 148.9(6) . . . . ?
B2_10 B5_10 B11_10 Cl10_10 -110.7(7) . . . . ?
B1_10 B5_10 B11_10 Cl10_10 -148.5(6) . . . . ?
Cl2_10 B5_10 B11_10 B10_10 145.7(6) . . . . ?
B7_10 B5_10 B11_10 B10_10 -102.1(6) . . . . ?
B6_10 B5_10 B11_10 B10_10 -64.2(7) . . . . ?
B2_10 B5_10 B11_10 B10_10 36.2(5) . . . . ?
B1_10 B5_10 B11_10 B10_10 -1.6(7) . . . . ?
Cl7_10 B9_10 B12_10 B8_10 111.5(6) . . . . ?
B3_10 B9_10 B12_10 B8_10 -99.8(6) . . . . ?
B10_10 B9_10 B12_10 B8_10 -138.4(6) . . . . ?
B4_10 B9_10 B12_10 B8_10 -37.2(5) . . . . ?
Cl7_10 B9_10 B12_10 B11_10 -147.6(5) . . . . ?
B8_10 B9_10 B12_10 B11_10 100.9(6) . . . . ?
B3_10 B9_10 B12_10 B11_10 1.1(8) . . . . ?
B10_10 B9_10 B12_10 B11_10 -37.5(5) . . . . ?
B4_10 B9_10 B12_10 B11_10 63.7(7) . . . . ?
Cl7_10 B9_10 B12_10 B10_10 -110.1(6) . . . . ?
B8_10 B9_10 B12_10 B10_10 138.4(6) . . . . ?
B3_10 B9_10 B12_10 B10_10 38.6(5) . . . . ?
B4_10 B9_10 B12_10 B10_10 101.2(6) . . . . ?
Cl7_10 B9_10 B12_10 Cl9_10 -2.5(8) . . . . ?
B8_10 B9_10 B12_10 Cl9_10 -114.0(6) . . . . ?
B3_10 B9_10 B12_10 Cl9_10 146.1(5) . . . . ?
B10_10 B9_10 B12_10 Cl9_10 107.6(6) . . . . ?
B4_10 B9_10 B12_10 Cl9_10 -151.2(5) . . . . ?
Cl7_10 B9_10 B12_10 B7_10 149.4(5) . . . . ?
B8_10 B9_10 B12_10 B7_10 37.9(5) . . . . ?
B3_10 B9_10 B12_10 B7_10 -61.9(7) . . . . ?
B10_10 B9_10 B12_10 B7_10 -100.5(6) . . . . ?
B4_10 B9_10 B12_10 B7_10 0.7(7) . . . . ?
B4_10 B8_10 B12_10 B9_10 38.1(6) . . . . ?
B6_10 B8_10 B12_10 B9_10 101.3(6) . . . . ?
Cl12_10 B8_10 B12_10 B9_10 -111.1(7) . . . . ?
B7_10 B8_10 B12_10 B9_10 138.2(6) . . . . ?
B4_10 B8_10 B12_10 B11_10 -63.4(7) . . . . ?
B6_10 B8_10 B12_10 B11_10 -0.2(8) . . . . ?
B9_10 B8_10 B12_10 B11_10 -101.5(6) . . . . ?
Cl12_10 B8_10 B12_10 B11_10 147.4(6) . . . . ?
B7_10 B8_10 B12_10 B11_10 36.7(5) . . . . ?
B4_10 B8_10 B12_10 B10_10 0.7(8) . . . . ?
B6_10 B8_10 B12_10 B10_10 63.9(7) . . . . ?
B9_10 B8_10 B12_10 B10_10 -37.4(5) . . . . ?
Cl12_10 B8_10 B12_10 B10_10 -148.5(6) . . . . ?
B7_10 B8_10 B12_10 B10_10 100.8(6) . . . . ?
B4_10 B8_10 B12_10 Cl9_10 146.2(6) . . . . ?
B6_10 B8_10 B12_10 Cl9_10 -150.6(6) . . . . ?
B9_10 B8_10 B12_10 Cl9_10 108.1(7) . . . . ?
Cl12_10 B8_10 B12_10 Cl9_10 -3.0(10) . . . . ?
B7_10 B8_10 B12_10 Cl9_10 -113.7(7) . . . . ?
B4_10 B8_10 B12_10 B7_10 -100.1(6) . . . . ?
B6_10 B8_10 B12_10 B7_10 -36.9(6) . . . . ?
B9_10 B8_10 B12_10 B7_10 -138.2(6) . . . . ?
Cl12_10 B8_10 B12_10 B7_10 110.7(7) . . . . ?
B7_10 B11_10 B12_10 B9_10 -101.3(6) . . . . ?
B2_10 B11_10 B12_10 B9_10 -0.5(7) . . . . ?
Cl10_10 B11_10 B12_10 B9_10 145.5(6) . . . . ?
B10_10 B11_10 B12_10 B9_10 37.4(5) . . . . ?
B5_10 B11_10 B12_10 B9_10 -63.3(7) . . . . ?
B7_10 B11_10 B12_10 B8_10 -37.3(6) . . . . ?
B2_10 B11_10 B12_10 B8_10 63.5(7) . . . . ?
Cl10_10 B11_10 B12_10 B8_10 -150.5(6) . . . . ?
B10_10 B11_10 B12_10 B8_10 101.3(6) . . . . ?
B5_10 B11_10 B12_10 B8_10 0.6(8) . . . . ?
B7_10 B11_10 B12_10 B10_10 -138.6(6) . . . . ?
B2_10 B11_10 B12_10 B10_10 -37.9(5) . . . . ?
Cl10_10 B11_10 B12_10 B10_10 108.2(6) . . . . ?
B5_10 B11_10 B12_10 B10_10 -100.7(6) . . . . ?
B7_10 B11_10 B12_10 Cl9_10 114.1(7) . . . . ?
B2_10 B11_10 B12_10 Cl9_10 -145.1(6) . . . . ?
Cl10_10 B11_10 B12_10 Cl9_10 0.9(9) . . . . ?
B10_10 B11_10 B12_10 Cl9_10 -107.3(7) . . . . ?
B5_10 B11_10 B12_10 Cl9_10 152.0(5) . . . . ?
B2_10 B11_10 B12_10 B7_10 100.8(6) . . . . ?
Cl10_10 B11_10 B12_10 B7_10 -113.2(7) . . . . ?
B10_10 B11_10 B12_10 B7_10 138.6(6) . . . . ?
B5_10 B11_10 B12_10 B7_10 37.9(5) . . . . ?
Cl8_10 B10_10 B12_10 B9_10 109.9(7) . . . . ?
B2_10 B10_10 B12_10 B9_10 -100.3(6) . . . . ?
B11_10 B10_10 B12_10 B9_10 -138.5(6) . . . . ?
B3_10 B10_10 B12_10 B9_10 -37.6(5) . . . . ?
Cl8_10 B10_10 B12_10 B8_10 147.4(6) . . . . ?
B2_10 B10_10 B12_10 B8_10 -62.8(7) . . . . ?
B9_10 B10_10 B12_10 B8_10 37.5(6) . . . . ?
B11_10 B10_10 B12_10 B8_10 -101.0(6) . . . . ?
B3_10 B10_10 B12_10 B8_10 -0.1(8) . . . . ?
Cl8_10 B10_10 B12_10 B11_10 -111.6(6) . . . . ?
B2_10 B10_10 B12_10 B11_10 38.2(5) . . . . ?
B9_10 B10_10 B12_10 B11_10 138.5(6) . . . . ?
B3_10 B10_10 B12_10 B11_10 100.9(6) . . . . ?
Cl8_10 B10_10 B12_10 Cl9_10 -0.2(9) . . . . ?
B2_10 B10_10 B12_10 Cl9_10 149.6(5) . . . . ?
B9_10 B10_10 B12_10 Cl9_10 -110.1(6) . . . . ?
B11_10 B10_10 B12_10 Cl9_10 111.4(6) . . . . ?
B3_10 B10_10 B12_10 Cl9_10 -147.7(5) . . . . ?
Cl8_10 B10_10 B12_10 B7_10 -148.3(5) . . . . ?
B2_10 B10_10 B12_10 B7_10 1.4(7) . . . . ?
B9_10 B10_10 B12_10 B7_10 101.8(6) . . . . ?
B11_10 B10_10 B12_10 B7_10 -36.7(5) . . . . ?
B3_10 B10_10 B12_10 B7_10 64.2(7) . . . . ?
Cl11_10 B7_10 B12_10 B9_10 -149.2(6) . . . . ?
B5_10 B7_10 B12_10 B9_10 62.4(7) . . . . ?
B11_10 B7_10 B12_10 B9_10 101.0(6) . . . . ?
B6_10 B7_10 B12_10 B9_10 -1.1(7) . . . . ?
B8_10 B7_10 B12_10 B9_10 -37.7(5) . . . . ?
Cl11_10 B7_10 B12_10 B8_10 -111.5(7) . . . . ?
B5_10 B7_10 B12_10 B8_10 100.1(6) . . . . ?
B11_10 B7_10 B12_10 B8_10 138.7(6) . . . . ?
B6_10 B7_10 B12_10 B8_10 36.7(5) . . . . ?
Cl11_10 B7_10 B12_10 B11_10 109.8(7) . . . . ?
B5_10 B7_10 B12_10 B11_10 -38.7(6) . . . . ?
B6_10 B7_10 B12_10 B11_10 -102.1(6) . . . . ?
B8_10 B7_10 B12_10 B11_10 -138.7(6) . . . . ?
Cl11_10 B7_10 B12_10 B10_10 147.0(6) . . . . ?
B5_10 B7_10 B12_10 B10_10 -1.5(7) . . . . ?
B11_10 B7_10 B12_10 B10_10 37.2(5) . . . . ?
B6_10 B7_10 B12_10 B10_10 -64.9(7) . . . . ?
B8_10 B7_10 B12_10 B10_10 -101.5(6) . . . . ?
Cl11_10 B7_10 B12_10 Cl9_10 1.2(10) . . . . ?
B5_10 B7_10 B12_10 Cl9_10 -147.2(6) . . . . ?
B11_10 B7_10 B12_10 Cl9_10 -108.6(7) . . . . ?
B6_10 B7_10 B12_10 Cl9_10 149.4(6) . . . . ?
B8_10 B7_10 B12_10 Cl9_10 112.7(7) . . . . ?
B5_11 B1_11 B2_11 B3_11 100.2(7) . . . . ?
B6_11 B1_11 B2_11 B3_11 138.1(6) . . . . ?
B4_11 B1_11 B2_11 B3_11 36.5(6) . . . . ?
Cl1_11 B1_11 B2_11 B3_11 -110.2(7) . . . . ?
B5_11 B1_11 B2_11 B11_11 62.1(8) . . . . ?
B6_11 B1_11 B2_11 B11_11 100.0(6) . . . . ?
B4_11 B1_11 B2_11 B11_11 -1.6(8) . . . . ?
Cl1_11 B1_11 B2_11 B11_11 -148.3(6) . . . . ?
B3_11 B1_11 B2_11 B11_11 -38.1(6) . . . . ?
B5_11 B1_11 B2_11 B6_11 -37.9(6) . . . . ?
B4_11 B1_11 B2_11 B6_11 -101.6(6) . . . . ?
Cl1_11 B1_11 B2_11 B6_11 111.6(7) . . . . ?
B3_11 B1_11 B2_11 B6_11 -138.1(6) . . . . ?
B5_11 B1_11 B2_11 B7_11 -0.8(8) . . . . ?
B6_11 B1_11 B2_11 B7_11 37.1(5) . . . . ?
B4_11 B1_11 B2_11 B7_11 -64.5(7) . . . . ?
Cl1_11 B1_11 B2_11 B7_11 148.8(6) . . . . ?
B3_11 B1_11 B2_11 B7_11 -101.0(6) . . . . ?
B5_11 B1_11 B2_11 Cl6_11 -147.9(6) . . . . ?
B6_11 B1_11 B2_11 Cl6_11 -109.9(6) . . . . ?
B4_11 B1_11 B2_11 Cl6_11 148.4(6) . . . . ?
Cl1_11 B1_11 B2_11 Cl6_11 1.7(9) . . . . ?
B3_11 B1_11 B2_11 Cl6_11 111.9(7) . . . . ?
B1_11 B2_11 B3_11 B11_11 -136.9(6) . . . . ?
B6_11 B2_11 B3_11 B11_11 -99.8(6) . . . . ?
B7_11 B2_11 B3_11 B11_11 -36.0(6) . . . . ?
Cl6_11 B2_11 B3_11 B11_11 111.6(7) . . . . ?
B1_11 B2_11 B3_11 B10_11 -99.4(6) . . . . ?
B11_11 B2_11 B3_11 B10_11 37.5(6) . . . . ?
B6_11 B2_11 B3_11 B10_11 -62.2(7) . . . . ?
B7_11 B2_11 B3_11 B10_11 1.5(8) . . . . ?
Cl6_11 B2_11 B3_11 B10_11 149.1(6) . . . . ?
B1_11 B2_11 B3_11 Cl2_11 110.1(7) . . . . ?
B11_11 B2_11 B3_11 Cl2_11 -113.0(7) . . . . ?
B6_11 B2_11 B3_11 Cl2_11 147.2(6) . . . . ?
B7_11 B2_11 B3_11 Cl2_11 -149.0(6) . . . . ?
Cl6_11 B2_11 B3_11 Cl2_11 -1.4(10) . . . . ?
B1_11 B2_11 B3_11 B4_11 -36.3(5) . . . . ?
B11_11 B2_11 B3_11 B4_11 100.6(6) . . . . ?
B6_11 B2_11 B3_11 B4_11 0.9(8) . . . . ?
B7_11 B2_11 B3_11 B4_11 64.6(7) . . . . ?
Cl6_11 B2_11 B3_11 B4_11 -147.8(6) . . . . ?
B11_11 B2_11 B3_11 B1_11 136.9(6) . . . . ?
B6_11 B2_11 B3_11 B1_11 37.1(5) . . . . ?
B7_11 B2_11 B3_11 B1_11 100.9(6) . . . . ?
Cl6_11 B2_11 B3_11 B1_11 -111.5(7) . . . . ?
B5_11 B1_11 B3_11 B11_11 -64.0(7) . . . . ?
B6_11 B1_11 B3_11 B11_11 0.3(7) . . . . ?
B2_11 B1_11 B3_11 B11_11 38.4(5) . . . . ?
B4_11 B1_11 B3_11 B11_11 -100.8(6) . . . . ?
Cl1_11 B1_11 B3_11 B11_11 147.1(6) . . . . ?
B5_11 B1_11 B3_11 B2_11 -102.4(6) . . . . ?
B6_11 B1_11 B3_11 B2_11 -38.2(6) . . . . ?
B4_11 B1_11 B3_11 B2_11 -139.3(6) . . . . ?
Cl1_11 B1_11 B3_11 B2_11 108.6(7) . . . . ?
B5_11 B1_11 B3_11 B10_11 -0.7(8) . . . . ?
B6_11 B1_11 B3_11 B10_11 63.6(7) . . . . ?
B2_11 B1_11 B3_11 B10_11 101.7(6) . . . . ?
B4_11 B1_11 B3_11 B10_11 -37.6(5) . . . . ?
Cl1_11 B1_11 B3_11 B10_11 -149.7(6) . . . . ?
B5_11 B1_11 B3_11 Cl2_11 147.9(5) . . . . ?
B6_11 B1_11 B3_11 Cl2_11 -147.8(6) . . . . ?
B2_11 B1_11 B3_11 Cl2_11 -109.7(6) . . . . ?
B4_11 B1_11 B3_11 Cl2_11 111.1(6) . . . . ?
Cl1_11 B1_11 B3_11 Cl2_11 -1.0(9) . . . . ?
B5_11 B1_11 B3_11 B4_11 36.8(6) . . . . ?
B6_11 B1_11 B3_11 B4_11 101.1(6) . . . . ?
B2_11 B1_11 B3_11 B4_11 139.3(6) . . . . ?
Cl1_11 B1_11 B3_11 B4_11 -112.1(7) . . . . ?
B6_11 B1_11 B4_11 B5_11 37.4(6) . . . . ?
B2_11 B1_11 B4_11 B5_11 102.3(6) . . . . ?
Cl1_11 B1_11 B4_11 B5_11 -112.1(7) . . . . ?
B3_11 B1_11 B4_11 B5_11 138.8(6) . . . . ?
B5_11 B1_11 B4_11 B9_11 -37.8(6) . . . . ?
B6_11 B1_11 B4_11 B9_11 -0.3(8) . . . . ?
B2_11 B1_11 B4_11 B9_11 64.6(7) . . . . ?
Cl1_11 B1_11 B4_11 B9_11 -149.8(6) . . . . ?
B3_11 B1_11 B4_11 B9_11 101.1(6) . . . . ?
B5_11 B1_11 B4_11 B10_11 -101.0(6) . . . . ?
B6_11 B1_11 B4_11 B10_11 -63.6(7) . . . . ?
B2_11 B1_11 B4_11 B10_11 1.3(8) . . . . ?
Cl1_11 B1_11 B4_11 B10_11 147.0(6) . . . . ?
B3_11 B1_11 B4_11 B10_11 37.8(6) . . . . ?
B5_11 B1_11 B4_11 Cl3_11 110.8(7) . . . . ?
B6_11 B1_11 B4_11 Cl3_11 148.2(6) . . . . ?
B2_11 B1_11 B4_11 Cl3_11 -146.9(6) . . . . ?
Cl1_11 B1_11 B4_11 Cl3_11 -1.3(10) . . . . ?
B3_11 B1_11 B4_11 Cl3_11 -110.4(7) . . . . ?
B5_11 B1_11 B4_11 B3_11 -138.8(6) . . . . ?
B6_11 B1_11 B4_11 B3_11 -101.4(7) . . . . ?
B2_11 B1_11 B4_11 B3_11 -36.5(6) . . . . ?
Cl1_11 B1_11 B4_11 B3_11 109.1(7) . . . . ?
B11_11 B3_11 B4_11 B5_11 63.3(7) . . . . ?
B2_11 B3_11 B4_11 B5_11 -0.5(8) . . . . ?
B10_11 B3_11 B4_11 B5_11 101.0(6) . . . . ?
Cl2_11 B3_11 B4_11 B5_11 -146.5(6) . . . . ?
B1_11 B3_11 B4_11 B5_11 -36.5(6) . . . . ?
B11_11 B3_11 B4_11 B9_11 -0.5(8) . . . . ?
B2_11 B3_11 B4_11 B9_11 -64.3(7) . . . . ?
B10_11 B3_11 B4_11 B9_11 37.2(5) . . . . ?
Cl2_11 B3_11 B4_11 B9_11 149.7(6) . . . . ?
B1_11 B3_11 B4_11 B9_11 -100.4(6) . . . . ?
B11_11 B3_11 B4_11 B10_11 -37.7(5) . . . . ?
B2_11 B3_11 B4_11 B10_11 -101.5(6) . . . . ?
Cl2_11 B3_11 B4_11 B10_11 112.5(7) . . . . ?
B1_11 B3_11 B4_11 B10_11 -137.5(6) . . . . ?
B11_11 B3_11 B4_11 Cl3_11 -147.5(6) . . . . ?
B2_11 B3_11 B4_11 Cl3_11 148.7(6) . . . . ?
B10_11 B3_11 B4_11 Cl3_11 -109.7(7) . . . . ?
Cl2_11 B3_11 B4_11 Cl3_11 2.8(9) . . . . ?
B1_11 B3_11 B4_11 Cl3_11 112.7(7) . . . . ?
B11_11 B3_11 B4_11 B1_11 99.8(6) . . . . ?
B2_11 B3_11 B4_11 B1_11 36.0(5) . . . . ?
B10_11 B3_11 B4_11 B1_11 137.5(6) . . . . ?
Cl2_11 B3_11 B4_11 B1_11 -110.0(7) . . . . ?
B6_11 B1_11 B5_11 B4_11 -138.6(6) . . . . ?
B2_11 B1_11 B5_11 B4_11 -100.5(7) . . . . ?
Cl1_11 B1_11 B5_11 B4_11 111.2(7) . . . . ?
B3_11 B1_11 B5_11 B4_11 -36.9(6) . . . . ?
B2_11 B1_11 B5_11 B6_11 38.2(6) . . . . ?
B4_11 B1_11 B5_11 B6_11 138.6(6) . . . . ?
Cl1_11 B1_11 B5_11 B6_11 -110.2(7) . . . . ?
B3_11 B1_11 B5_11 B6_11 101.8(6) . . . . ?
B6_11 B1_11 B5_11 Cl4_11 109.0(7) . . . . ?
B2_11 B1_11 B5_11 Cl4_11 147.2(6) . . . . ?
B4_11 B1_11 B5_11 Cl4_11 -112.3(7) . . . . ?
Cl1_11 B1_11 B5_11 Cl4_11 -1.1(10) . . . . ?
B3_11 B1_11 B5_11 Cl4_11 -149.2(6) . . . . ?
B6_11 B1_11 B5_11 B9_11 -100.9(6) . . . . ?
B2_11 B1_11 B5_11 B9_11 -62.8(7) . . . . ?
B4_11 B1_11 B5_11 B9_11 37.7(6) . . . . ?
Cl1_11 B1_11 B5_11 B9_11 148.9(6) . . . . ?
B3_11 B1_11 B5_11 B9_11 0.9(8) . . . . ?
B6_11 B1_11 B5_11 B8_11 -37.6(5) . . . . ?
B2_11 B1_11 B5_11 B8_11 0.6(8) . . . . ?
B4_11 B1_11 B5_11 B8_11 101.1(6) . . . . ?
Cl1_11 B1_11 B5_11 B8_11 -147.8(6) . . . . ?
B3_11 B1_11 B5_11 B8_11 64.2(7) . . . . ?
B9_11 B4_11 B5_11 B1_11 137.8(6) . . . . ?
B10_11 B4_11 B5_11 B1_11 100.3(6) . . . . ?
Cl3_11 B4_11 B5_11 B1_11 -112.0(7) . . . . ?
B3_11 B4_11 B5_11 B1_11 37.0(6) . . . . ?
B9_11 B4_11 B5_11 B6_11 100.8(6) . . . . ?
B10_11 B4_11 B5_11 B6_11 63.2(7) . . . . ?
Cl3_11 B4_11 B5_11 B6_11 -149.1(6) . . . . ?
B1_11 B4_11 B5_11 B6_11 -37.1(6) . . . . ?
B3_11 B4_11 B5_11 B6_11 -0.1(8) . . . . ?
B9_11 B4_11 B5_11 Cl4_11 -111.2(7) . . . . ?
B10_11 B4_11 B5_11 Cl4_11 -148.7(6) . . . . ?
Cl3_11 B4_11 B5_11 Cl4_11 -1.0(10) . . . . ?
B1_11 B4_11 B5_11 Cl4_11 111.0(7) . . . . ?
B3_11 B4_11 B5_11 Cl4_11 148.0(6) . . . . ?
B10_11 B4_11 B5_11 B9_11 -37.5(5) . . . . ?
Cl3_11 B4_11 B5_11 B9_11 110.2(7) . . . . ?
B1_11 B4_11 B5_11 B9_11 -137.8(6) . . . . ?
B3_11 B4_11 B5_11 B9_11 -100.8(6) . . . . ?
B9_11 B4_11 B5_11 B8_11 37.3(5) . . . . ?
B10_11 B4_11 B5_11 B8_11 -0.2(8) . . . . ?
Cl3_11 B4_11 B5_11 B8_11 147.5(6) . . . . ?
B1_11 B4_11 B5_11 B8_11 -100.5(6) . . . . ?
B3_11 B4_11 B5_11 B8_11 -63.5(7) . . . . ?
B2_11 B1_11 B6_11 B5_11 -138.3(6) . . . . ?
B4_11 B1_11 B6_11 B5_11 -37.1(6) . . . . ?
Cl1_11 B1_11 B6_11 B5_11 112.8(7) . . . . ?
B3_11 B1_11 B6_11 B5_11 -100.7(6) . . . . ?
B5_11 B1_11 B6_11 B8_11 37.8(6) . . . . ?
B2_11 B1_11 B6_11 B8_11 -100.5(6) . . . . ?
B4_11 B1_11 B6_11 B8_11 0.7(8) . . . . ?
Cl1_11 B1_11 B6_11 B8_11 150.6(6) . . . . ?
B3_11 B1_11 B6_11 B8_11 -62.9(7) . . . . ?
B5_11 B1_11 B6_11 Cl5_11 -110.2(7) . . . . ?
B2_11 B1_11 B6_11 Cl5_11 111.5(7) . . . . ?
B4_11 B1_11 B6_11 Cl5_11 -147.3(6) . . . . ?
Cl1_11 B1_11 B6_11 Cl5_11 2.5(9) . . . . ?
B3_11 B1_11 B6_11 Cl5_11 149.0(6) . . . . ?
B5_11 B1_11 B6_11 B2_11 138.3(6) . . . . ?
B4_11 B1_11 B6_11 B2_11 101.2(7) . . . . ?
Cl1_11 B1_11 B6_11 B2_11 -108.9(7) . . . . ?
B3_11 B1_11 B6_11 B2_11 37.6(5) . . . . ?
B5_11 B1_11 B6_11 B7_11 101.4(6) . . . . ?
B2_11 B1_11 B6_11 B7_11 -36.9(5) . . . . ?
B4_11 B1_11 B6_11 B7_11 64.3(7) . . . . ?
Cl1_11 B1_11 B6_11 B7_11 -145.8(6) . . . . ?
B3_11 B1_11 B6_11 B7_11 0.7(8) . . . . ?
B4_11 B5_11 B6_11 B1_11 37.6(6) . . . . ?
Cl4_11 B5_11 B6_11 B1_11 -111.4(7) . . . . ?
B9_11 B5_11 B6_11 B1_11 101.0(6) . . . . ?
B8_11 B5_11 B6_11 B1_11 137.8(6) . . . . ?
B1_11 B5_11 B6_11 B8_11 -137.8(6) . . . . ?
B4_11 B5_11 B6_11 B8_11 -100.2(6) . . . . ?
Cl4_11 B5_11 B6_11 B8_11 110.9(7) . . . . ?
B9_11 B5_11 B6_11 B8_11 -36.7(6) . . . . ?
B1_11 B5_11 B6_11 Cl5_11 111.4(7) . . . . ?
B4_11 B5_11 B6_11 Cl5_11 149.0(6) . . . . ?
Cl4_11 B5_11 B6_11 Cl5_11 0.0(10) . . . . ?
B9_11 B5_11 B6_11 Cl5_11 -147.6(6) . . . . ?
B8_11 B5_11 B6_11 Cl5_11 -110.8(7) . . . . ?
B1_11 B5_11 B6_11 B2_11 -36.9(6) . . . . ?
B4_11 B5_11 B6_11 B2_11 0.6(8) . . . . ?
Cl4_11 B5_11 B6_11 B2_11 -148.3(6) . . . . ?
B9_11 B5_11 B6_11 B2_11 64.1(7) . . . . ?
B8_11 B5_11 B6_11 B2_11 100.8(6) . . . . ?
B1_11 B5_11 B6_11 B7_11 -100.2(6) . . . . ?
B4_11 B5_11 B6_11 B7_11 -62.7(7) . . . . ?
Cl4_11 B5_11 B6_11 B7_11 148.4(6) . . . . ?
B9_11 B5_11 B6_11 B7_11 0.8(8) . . . . ?
B8_11 B5_11 B6_11 B7_11 37.6(6) . . . . ?
B3_11 B2_11 B6_11 B1_11 -37.9(6) . . . . ?
B11_11 B2_11 B6_11 B1_11 -100.6(6) . . . . ?
B7_11 B2_11 B6_11 B1_11 -138.6(6) . . . . ?
Cl6_11 B2_11 B6_11 B1_11 111.1(7) . . . . ?
B1_11 B2_11 B6_11 B5_11 37.0(6) . . . . ?
B3_11 B2_11 B6_11 B5_11 -0.9(8) . . . . ?
B11_11 B2_11 B6_11 B5_11 -63.6(7) . . . . ?
B7_11 B2_11 B6_11 B5_11 -101.6(6) . . . . ?
Cl6_11 B2_11 B6_11 B5_11 148.1(6) . . . . ?
B1_11 B2_11 B6_11 B8_11 100.6(6) . . . . ?
B3_11 B2_11 B6_11 B8_11 62.7(7) . . . . ?
B11_11 B2_11 B6_11 B8_11 0.0(8) . . . . ?
B7_11 B2_11 B6_11 B8_11 -38.0(5) . . . . ?
Cl6_11 B2_11 B6_11 B8_11 -148.3(6) . . . . ?
B1_11 B2_11 B6_11 Cl5_11 -111.0(7) . . . . ?
B3_11 B2_11 B6_11 Cl5_11 -148.9(6) . . . . ?
B11_11 B2_11 B6_11 Cl5_11 148.4(6) . . . . ?
B7_11 B2_11 B6_11 Cl5_11 110.4(7) . . . . ?
Cl6_11 B2_11 B6_11 Cl5_11 0.1(10) . . . . ?
B1_11 B2_11 B6_11 B7_11 138.6(6) . . . . ?
B3_11 B2_11 B6_11 B7_11 100.7(6) . . . . ?
B11_11 B2_11 B6_11 B7_11 38.0(5) . . . . ?
Cl6_11 B2_11 B6_11 B7_11 -110.3(7) . . . . ?
B1_11 B2_11 B7_11 Cl7_11 -147.2(6) . . . . ?
B3_11 B2_11 B7_11 Cl7_11 148.4(6) . . . . ?
B11_11 B2_11 B7_11 Cl7_11 112.5(7) . . . . ?
B6_11 B2_11 B7_11 Cl7_11 -110.5(7) . . . . ?
Cl6_11 B2_11 B7_11 Cl7_11 0.3(9) . . . . ?
B1_11 B2_11 B7_11 B11_11 100.3(6) . . . . ?
B3_11 B2_11 B7_11 B11_11 35.9(6) . . . . ?
B6_11 B2_11 B7_11 B11_11 137.0(6) . . . . ?
Cl6_11 B2_11 B7_11 B11_11 -112.2(7) . . . . ?
B1_11 B2_11 B7_11 B12_11 62.9(7) . . . . ?
B3_11 B2_11 B7_11 B12_11 -1.5(8) . . . . ?
B11_11 B2_11 B7_11 B12_11 -37.4(5) . . . . ?
B6_11 B2_11 B7_11 B12_11 99.6(6) . . . . ?
Cl6_11 B2_11 B7_11 B12_11 -149.6(5) . . . . ?
B1_11 B2_11 B7_11 B8_11 0.7(7) . . . . ?
B3_11 B2_11 B7_11 B8_11 -63.7(7) . . . . ?
B11_11 B2_11 B7_11 B8_11 -99.7(6) . . . . ?
B6_11 B2_11 B7_11 B8_11 37.3(5) . . . . ?
Cl6_11 B2_11 B7_11 B8_11 148.1(5) . . . . ?
B1_11 B2_11 B7_11 B6_11 -36.7(5) . . . . ?
B3_11 B2_11 B7_11 B6_11 -101.1(6) . . . . ?
B11_11 B2_11 B7_11 B6_11 -137.0(6) . . . . ?
Cl6_11 B2_11 B7_11 B6_11 110.8(6) . . . . ?
B1_11 B6_11 B7_11 Cl7_11 147.9(6) . . . . ?
B5_11 B6_11 B7_11 Cl7_11 -149.0(6) . . . . ?
B8_11 B6_11 B7_11 Cl7_11 -111.4(7) . . . . ?
Cl5_11 B6_11 B7_11 Cl7_11 -0.7(10) . . . . ?
B2_11 B6_11 B7_11 Cl7_11 111.1(7) . . . . ?
B1_11 B6_11 B7_11 B11_11 -1.4(7) . . . . ?
B5_11 B6_11 B7_11 B11_11 61.7(7) . . . . ?
B8_11 B6_11 B7_11 B11_11 99.4(6) . . . . ?
Cl5_11 B6_11 B7_11 B11_11 -149.9(6) . . . . ?
B2_11 B6_11 B7_11 B11_11 -38.1(5) . . . . ?
B1_11 B6_11 B7_11 B12_11 -64.1(7) . . . . ?
B5_11 B6_11 B7_11 B12_11 -1.0(8) . . . . ?
B8_11 B6_11 B7_11 B12_11 36.6(5) . . . . ?
Cl5_11 B6_11 B7_11 B12_11 147.3(6) . . . . ?
B2_11 B6_11 B7_11 B12_11 -100.9(6) . . . . ?
B1_11 B6_11 B7_11 B2_11 36.8(5) . . . . ?
B5_11 B6_11 B7_11 B2_11 99.9(6) . . . . ?
B8_11 B6_11 B7_11 B2_11 137.5(6) . . . . ?
Cl5_11 B6_11 B7_11 B2_11 -111.8(7) . . . . ?
B1_11 B6_11 B7_11 B8_11 -100.7(6) . . . . ?
B5_11 B6_11 B7_11 B8_11 -37.6(6) . . . . ?
Cl5_11 B6_11 B7_11 B8_11 110.7(7) . . . . ?
B2_11 B6_11 B7_11 B8_11 -137.5(6) . . . . ?
B1_11 B6_11 B8_11 B12_11 63.4(7) . . . . ?
B5_11 B6_11 B8_11 B12_11 100.9(6) . . . . ?
Cl5_11 B6_11 B8_11 B12_11 -148.3(6) . . . . ?
B2_11 B6_11 B8_11 B12_11 0.5(8) . . . . ?
B7_11 B6_11 B8_11 B12_11 -37.3(5) . . . . ?
B1_11 B6_11 B8_11 B9_11 -0.8(8) . . . . ?
B5_11 B6_11 B8_11 B9_11 36.7(6) . . . . ?
Cl5_11 B6_11 B8_11 B9_11 147.5(6) . . . . ?
B2_11 B6_11 B8_11 B9_11 -63.7(7) . . . . ?
B7_11 B6_11 B8_11 B9_11 -101.5(6) . . . . ?
B1_11 B6_11 B8_11 B5_11 -37.5(6) . . . . ?
Cl5_11 B6_11 B8_11 B5_11 110.8(7) . . . . ?
B2_11 B6_11 B8_11 B5_11 -100.4(6) . . . . ?
B7_11 B6_11 B8_11 B5_11 -138.2(6) . . . . ?
B1_11 B6_11 B8_11 Cl8_11 -150.7(6) . . . . ?
B5_11 B6_11 B8_11 Cl8_11 -113.2(7) . . . . ?
Cl5_11 B6_11 B8_11 Cl8_11 -2.4(9) . . . . ?
B2_11 B6_11 B8_11 Cl8_11 146.4(6) . . . . ?
B7_11 B6_11 B8_11 Cl8_11 108.6(6) . . . . ?
B1_11 B6_11 B8_11 B7_11 100.7(6) . . . . ?
B5_11 B6_11 B8_11 B7_11 138.2(6) . . . . ?
Cl5_11 B6_11 B8_11 B7_11 -111.0(7) . . . . ?
B2_11 B6_11 B8_11 B7_11 37.8(5) . . . . ?
B1_11 B5_11 B8_11 B12_11 -63.7(7) . . . . ?
B4_11 B5_11 B8_11 B12_11 0.6(7) . . . . ?
B6_11 B5_11 B8_11 B12_11 -101.1(6) . . . . ?
Cl4_11 B5_11 B8_11 B12_11 149.5(6) . . . . ?
B9_11 B5_11 B8_11 B12_11 37.8(5) . . . . ?
B1_11 B5_11 B8_11 B6_11 37.5(6) . . . . ?
B4_11 B5_11 B8_11 B6_11 101.7(6) . . . . ?
Cl4_11 B5_11 B8_11 B6_11 -109.3(7) . . . . ?
B9_11 B5_11 B8_11 B6_11 139.0(6) . . . . ?
B1_11 B5_11 B8_11 B9_11 -101.5(6) . . . . ?
B4_11 B5_11 B8_11 B9_11 -37.2(5) . . . . ?
B6_11 B5_11 B8_11 B9_11 -139.0(6) . . . . ?
Cl4_11 B5_11 B8_11 B9_11 111.7(7) . . . . ?
B1_11 B5_11 B8_11 Cl8_11 147.1(6) . . . . ?
B4_11 B5_11 B8_11 Cl8_11 -148.6(5) . . . . ?
B6_11 B5_11 B8_11 Cl8_11 109.6(6) . . . . ?
Cl4_11 B5_11 B8_11 Cl8_11 0.3(9) . . . . ?
B9_11 B5_11 B8_11 Cl8_11 -111.4(6) . . . . ?
B1_11 B5_11 B8_11 B7_11 -0.2(8) . . . . ?
B4_11 B5_11 B8_11 B7_11 64.1(7) . . . . ?
B6_11 B5_11 B8_11 B7_11 -37.7(5) . . . . ?
Cl4_11 B5_11 B8_11 B7_11 -147.0(6) . . . . ?
B9_11 B5_11 B8_11 B7_11 101.3(6) . . . . ?
Cl7_11 B7_11 B8_11 B12_11 -111.6(7) . . . . ?
B11_11 B7_11 B8_11 B12_11 37.9(5) . . . . ?
B2_11 B7_11 B8_11 B12_11 100.8(6) . . . . ?
B6_11 B7_11 B8_11 B12_11 138.4(6) . . . . ?
Cl7_11 B7_11 B8_11 B6_11 110.1(7) . . . . ?
B11_11 B7_11 B8_11 B6_11 -100.5(6) . . . . ?
B12_11 B7_11 B8_11 B6_11 -138.4(6) . . . . ?
B2_11 B7_11 B8_11 B6_11 -37.6(5) . . . . ?
Cl7_11 B7_11 B8_11 B9_11 -149.1(6) . . . . ?
B11_11 B7_11 B8_11 B9_11 0.3(8) . . . . ?
B12_11 B7_11 B8_11 B9_11 -37.6(5) . . . . ?
B2_11 B7_11 B8_11 B9_11 63.2(7) . . . . ?
B6_11 B7_11 B8_11 B9_11 100.8(6) . . . . ?
Cl7_11 B7_11 B8_11 B5_11 147.4(6) . . . . ?
B11_11 B7_11 B8_11 B5_11 -63.2(7) . . . . ?
B12_11 B7_11 B8_11 B5_11 -101.1(6) . . . . ?
B2_11 B7_11 B8_11 B5_11 -0.3(7) . . . . ?
B6_11 B7_11 B8_11 B5_11 37.3(5) . . . . ?
Cl7_11 B7_11 B8_11 Cl8_11 -1.5(9) . . . . ?
B11_11 B7_11 B8_11 Cl8_11 148.0(5) . . . . ?
B12_11 B7_11 B8_11 Cl8_11 110.1(6) . . . . ?
B2_11 B7_11 B8_11 Cl8_11 -149.2(5) . . . . ?
B6_11 B7_11 B8_11 Cl8_11 -111.5(6) . . . . ?
B5_11 B4_11 B9_11 B10_11 -138.1(6) . . . . ?
Cl3_11 B4_11 B9_11 B10_11 109.9(7) . . . . ?
B1_11 B4_11 B9_11 B10_11 -100.8(6) . . . . ?
B3_11 B4_11 B9_11 B10_11 -37.2(5) . . . . ?
B10_11 B4_11 B9_11 B5_11 138.1(6) . . . . ?
Cl3_11 B4_11 B9_11 B5_11 -112.0(7) . . . . ?
B1_11 B4_11 B9_11 B5_11 37.2(6) . . . . ?
B3_11 B4_11 B9_11 B5_11 100.9(6) . . . . ?
B5_11 B4_11 B9_11 B8_11 -37.4(6) . . . . ?
B10_11 B4_11 B9_11 B8_11 100.7(6) . . . . ?
Cl3_11 B4_11 B9_11 B8_11 -149.4(6) . . . . ?
B1_11 B4_11 B9_11 B8_11 -0.2(8) . . . . ?
B3_11 B4_11 B9_11 B8_11 63.5(7) . . . . ?
B5_11 B4_11 B9_11 Cl9_11 111.5(7) . . . . ?
B10_11 B4_11 B9_11 Cl9_11 -110.5(7) . . . . ?
Cl3_11 B4_11 B9_11 Cl9_11 -0.6(10) . . . . ?
B1_11 B4_11 B9_11 Cl9_11 148.7(6) . . . . ?
B3_11 B4_11 B9_11 Cl9_11 -147.7(6) . . . . ?
B5_11 B4_11 B9_11 B12_11 -100.0(6) . . . . ?
B10_11 B4_11 B9_11 B12_11 38.0(5) . . . . ?
Cl3_11 B4_11 B9_11 B12_11 148.0(6) . . . . ?
B1_11 B4_11 B9_11 B12_11 -62.8(7) . . . . ?
B3_11 B4_11 B9_11 B12_11 0.9(8) . . . . ?
B1_11 B5_11 B9_11 B10_11 -0.7(8) . . . . ?
B4_11 B5_11 B9_11 B10_11 37.5(5) . . . . ?
B6_11 B5_11 B9_11 B10_11 -64.0(7) . . . . ?
Cl4_11 B5_11 B9_11 B10_11 149.2(6) . . . . ?
B8_11 B5_11 B9_11 B10_11 -100.7(6) . . . . ?
B1_11 B5_11 B9_11 B4_11 -38.2(6) . . . . ?
B6_11 B5_11 B9_11 B4_11 -101.5(6) . . . . ?
Cl4_11 B5_11 B9_11 B4_11 111.7(7) . . . . ?
B8_11 B5_11 B9_11 B4_11 -138.2(6) . . . . ?
B1_11 B5_11 B9_11 B8_11 100.0(6) . . . . ?
B4_11 B5_11 B9_11 B8_11 138.2(6) . . . . ?
B6_11 B5_11 B9_11 B8_11 36.7(6) . . . . ?
Cl4_11 B5_11 B9_11 B8_11 -110.1(7) . . . . ?
B1_11 B5_11 B9_11 Cl9_11 -149.4(6) . . . . ?
B4_11 B5_11 B9_11 Cl9_11 -111.2(7) . . . . ?
B6_11 B5_11 B9_11 Cl9_11 147.3(6) . . . . ?
Cl4_11 B5_11 B9_11 Cl9_11 0.4(9) . . . . ?
B8_11 B5_11 B9_11 Cl9_11 110.6(7) . . . . ?
B1_11 B5_11 B9_11 B12_11 63.0(7) . . . . ?
B4_11 B5_11 B9_11 B12_11 101.2(6) . . . . ?
B6_11 B5_11 B9_11 B12_11 -0.3(8) . . . . ?
Cl4_11 B5_11 B9_11 B12_11 -147.1(6) . . . . ?
B8_11 B5_11 B9_11 B12_11 -37.0(5) . . . . ?
B12_11 B8_11 B9_11 B10_11 -37.3(5) . . . . ?
B6_11 B8_11 B9_11 B10_11 64.1(7) . . . . ?
B5_11 B8_11 B9_11 B10_11 100.8(6) . . . . ?
Cl8_11 B8_11 B9_11 B10_11 -146.4(6) . . . . ?
B7_11 B8_11 B9_11 B10_11 0.0(8) . . . . ?
B12_11 B8_11 B9_11 B4_11 -100.8(6) . . . . ?
B6_11 B8_11 B9_11 B4_11 0.6(8) . . . . ?
B5_11 B8_11 B9_11 B4_11 37.2(6) . . . . ?
Cl8_11 B8_11 B9_11 B4_11 150.0(6) . . . . ?
B7_11 B8_11 B9_11 B4_11 -63.6(7) . . . . ?
B12_11 B8_11 B9_11 B5_11 -138.1(6) . . . . ?
B6_11 B8_11 B9_11 B5_11 -36.6(5) . . . . ?
Cl8_11 B8_11 B9_11 B5_11 112.8(7) . . . . ?
B7_11 B8_11 B9_11 B5_11 -100.8(6) . . . . ?
B12_11 B8_11 B9_11 Cl9_11 110.0(7) . . . . ?
B6_11 B8_11 B9_11 Cl9_11 -148.5(6) . . . . ?
B5_11 B8_11 B9_11 Cl9_11 -111.9(7) . . . . ?
Cl8_11 B8_11 B9_11 Cl9_11 0.9(9) . . . . ?
B7_11 B8_11 B9_11 Cl9_11 147.3(6) . . . . ?
B6_11 B8_11 B9_11 B12_11 101.5(6) . . . . ?
B5_11 B8_11 B9_11 B12_11 138.1(6) . . . . ?
Cl8_11 B8_11 B9_11 B12_11 -109.1(7) . . . . ?
B7_11 B8_11 B9_11 B12_11 37.3(5) . . . . ?
B5_11 B9_11 B10_11 B4_11 -37.3(5) . . . . ?
B8_11 B9_11 B10_11 B4_11 -100.9(6) . . . . ?
Cl9_11 B9_11 B10_11 B4_11 111.7(7) . . . . ?
B12_11 B9_11 B10_11 B4_11 -137.7(6) . . . . ?
B4_11 B9_11 B10_11 B11_11 100.6(6) . . . . ?
B5_11 B9_11 B10_11 B11_11 63.2(7) . . . . ?
B8_11 B9_11 B10_11 B11_11 -0.3(8) . . . . ?
Cl9_11 B9_11 B10_11 B11_11 -147.7(6) . . . . ?
B12_11 B9_11 B10_11 B11_11 -37.1(5) . . . . ?
B4_11 B9_11 B10_11 B3_11 37.6(5) . . . . ?
B5_11 B9_11 B10_11 B3_11 0.2(8) . . . . ?
B8_11 B9_11 B10_11 B3_11 -63.3(7) . . . . ?
Cl9_11 B9_11 B10_11 B3_11 149.3(6) . . . . ?
B12_11 B9_11 B10_11 B3_11 -100.1(6) . . . . ?
B4_11 B9_11 B10_11 Cl10_11 -114.3(7) . . . . ?
B5_11 B9_11 B10_11 Cl10_11 -151.6(5) . . . . ?
B8_11 B9_11 B10_11 Cl10_11 144.9(6) . . . . ?
Cl9_11 B9_11 B10_11 Cl10_11 -2.5(9) . . . . ?
B12_11 B9_11 B10_11 Cl10_11 108.1(6) . . . . ?
B4_11 B9_11 B10_11 B12_11 137.7(6) . . . . ?
B5_11 B9_11 B10_11 B12_11 100.3(6) . . . . ?
B8_11 B9_11 B10_11 B12_11 36.8(5) . . . . ?
Cl9_11 B9_11 B10_11 B12_11 -110.6(7) . . . . ?
B5_11 B4_11 B10_11 B9_11 37.7(5) . . . . ?
Cl3_11 B4_11 B10_11 B9_11 -110.6(7) . . . . ?
B1_11 B4_11 B10_11 B9_11 100.3(6) . . . . ?
B3_11 B4_11 B10_11 B9_11 138.4(6) . . . . ?
B5_11 B4_11 B10_11 B11_11 -63.1(7) . . . . ?
B9_11 B4_11 B10_11 B11_11 -100.9(6) . . . . ?
Cl3_11 B4_11 B10_11 B11_11 148.6(6) . . . . ?
B1_11 B4_11 B10_11 B11_11 -0.5(8) . . . . ?
B3_11 B4_11 B10_11 B11_11 37.5(6) . . . . ?
B5_11 B4_11 B10_11 B3_11 -100.6(6) . . . . ?
B9_11 B4_11 B10_11 B3_11 -138.4(6) . . . . ?
Cl3_11 B4_11 B10_11 B3_11 111.1(7) . . . . ?
B1_11 B4_11 B10_11 B3_11 -38.0(6) . . . . ?
B5_11 B4_11 B10_11 Cl10_11 146.6(6) . . . . ?
B9_11 B4_11 B10_11 Cl10_11 108.8(7) . . . . ?
Cl3_11 B4_11 B10_11 Cl10_11 -1.7(9) . . . . ?
B1_11 B4_11 B10_11 Cl10_11 -150.8(6) . . . . ?
B3_11 B4_11 B10_11 Cl10_11 -112.8(7) . . . . ?
B5_11 B4_11 B10_11 B12_11 -0.2(7) . . . . ?
B9_11 B4_11 B10_11 B12_11 -38.0(5) . . . . ?
Cl3_11 B4_11 B10_11 B12_11 -148.5(5) . . . . ?
B1_11 B4_11 B10_11 B12_11 62.4(7) . . . . ?
B3_11 B4_11 B10_11 B12_11 100.4(6) . . . . ?
B11_11 B3_11 B10_11 B9_11 100.4(6) . . . . ?
B2_11 B3_11 B10_11 B9_11 62.8(7) . . . . ?
Cl2_11 B3_11 B10_11 B9_11 -147.5(6) . . . . ?
B4_11 B3_11 B10_11 B9_11 -37.3(5) . . . . ?
B1_11 B3_11 B10_11 B9_11 0.3(8) . . . . ?
B11_11 B3_11 B10_11 B4_11 137.8(6) . . . . ?
B2_11 B3_11 B10_11 B4_11 100.1(6) . . . . ?
Cl2_11 B3_11 B10_11 B4_11 -110.2(7) . . . . ?
B1_11 B3_11 B10_11 B4_11 37.6(5) . . . . ?
B2_11 B3_11 B10_11 B11_11 -37.6(6) . . . . ?
Cl2_11 B3_11 B10_11 B11_11 112.1(7) . . . . ?
B4_11 B3_11 B10_11 B11_11 -137.8(6) . . . . ?
B1_11 B3_11 B10_11 B11_11 -100.1(6) . . . . ?
B11_11 B3_11 B10_11 Cl10_11 -108.8(7) . . . . ?
B2_11 B3_11 B10_11 Cl10_11 -146.4(6) . . . . ?
Cl2_11 B3_11 B10_11 Cl10_11 3.3(10) . . . . ?
B4_11 B3_11 B10_11 Cl10_11 113.5(7) . . . . ?
B1_11 B3_11 B10_11 Cl10_11 151.1(6) . . . . ?
B11_11 B3_11 B10_11 B12_11 36.6(5) . . . . ?
B2_11 B3_11 B10_11 B12_11 -1.0(8) . . . . ?
Cl2_11 B3_11 B10_11 B12_11 148.7(6) . . . . ?
B4_11 B3_11 B10_11 B12_11 -101.1(6) . . . . ?
B1_11 B3_11 B10_11 B12_11 -63.5(7) . . . . ?
B2_11 B3_11 B11_11 B12_11 100.8(6) . . . . ?
B10_11 B3_11 B11_11 B12_11 -37.5(6) . . . . ?
Cl2_11 B3_11 B11_11 B12_11 -149.7(5) . . . . ?
B4_11 B3_11 B11_11 B12_11 0.0(8) . . . . ?
B1_11 B3_11 B11_11 B12_11 62.9(7) . . . . ?
B2_11 B3_11 B11_11 B10_11 138.3(6) . . . . ?
Cl2_11 B3_11 B11_11 B10_11 -112.3(7) . . . . ?
B4_11 B3_11 B11_11 B10_11 37.5(5) . . . . ?
B1_11 B3_11 B11_11 B10_11 100.4(6) . . . . ?
B2_11 B3_11 B11_11 B7_11 36.7(6) . . . . ?
B10_11 B3_11 B11_11 B7_11 -101.6(6) . . . . ?
Cl2_11 B3_11 B11_11 B7_11 146.2(6) . . . . ?
B4_11 B3_11 B11_11 B7_11 -64.1(7) . . . . ?
B1_11 B3_11 B11_11 B7_11 -1.2(7) . . . . ?
B10_11 B3_11 B11_11 B2_11 -138.3(6) . . . . ?
Cl2_11 B3_11 B11_11 B2_11 109.5(6) . . . . ?
B4_11 B3_11 B11_11 B2_11 -100.8(6) . . . . ?
B1_11 B3_11 B11_11 B2_11 -37.9(5) . . . . ?
B2_11 B3_11 B11_11 Cl11_11 -113.5(7) . . . . ?
B10_11 B3_11 B11_11 Cl11_11 108.2(7) . . . . ?
Cl2_11 B3_11 B11_11 Cl11_11 -4.0(9) . . . . ?
B4_11 B3_11 B11_11 Cl11_11 145.7(6) . . . . ?
B1_11 B3_11 B11_11 Cl11_11 -151.3(6) . . . . ?
B9_11 B10_11 B11_11 B3_11 -101.2(6) . . . . ?
B4_11 B10_11 B11_11 B3_11 -37.9(6) . . . . ?
Cl10_11 B10_11 B11_11 B3_11 113.6(7) . . . . ?
B12_11 B10_11 B11_11 B3_11 -138.7(6) . . . . ?
B9_11 B10_11 B11_11 B12_11 37.5(6) . . . . ?
B4_11 B10_11 B11_11 B12_11 100.8(6) . . . . ?
B3_11 B10_11 B11_11 B12_11 138.7(6) . . . . ?
Cl10_11 B10_11 B11_11 B12_11 -107.7(6) . . . . ?
B9_11 B10_11 B11_11 B7_11 0.5(8) . . . . ?
B4_11 B10_11 B11_11 B7_11 63.8(7) . . . . ?
B3_11 B10_11 B11_11 B7_11 101.7(7) . . . . ?
Cl10_11 B10_11 B11_11 B7_11 -144.7(6) . . . . ?
B12_11 B10_11 B11_11 B7_11 -36.9(6) . . . . ?
B9_11 B10_11 B11_11 B2_11 -63.8(7) . . . . ?
B4_11 B10_11 B11_11 B2_11 -0.4(8) . . . . ?
B3_11 B10_11 B11_11 B2_11 37.5(6) . . . . ?
Cl10_11 B10_11 B11_11 B2_11 151.0(6) . . . . ?
B12_11 B10_11 B11_11 B2_11 -101.2(6) . . . . ?
B9_11 B10_11 B11_11 Cl11_11 146.9(6) . . . . ?
B4_11 B10_11 B11_11 Cl11_11 -149.8(6) . . . . ?
B3_11 B10_11 B11_11 Cl11_11 -111.9(7) . . . . ?
Cl10_11 B10_11 B11_11 Cl11_11 1.7(9) . . . . ?
B12_11 B10_11 B11_11 Cl11_11 109.4(7) . . . . ?
Cl7_11 B7_11 B11_11 B3_11 -147.1(6) . . . . ?
B12_11 B7_11 B11_11 B3_11 101.4(6) . . . . ?
B2_11 B7_11 B11_11 B3_11 -36.5(6) . . . . ?
B8_11 B7_11 B11_11 B3_11 63.7(7) . . . . ?
B6_11 B7_11 B11_11 B3_11 1.6(8) . . . . ?
Cl7_11 B7_11 B11_11 B12_11 111.5(7) . . . . ?
B2_11 B7_11 B11_11 B12_11 -137.9(6) . . . . ?
B8_11 B7_11 B11_11 B12_11 -37.7(5) . . . . ?
B6_11 B7_11 B11_11 B12_11 -99.8(6) . . . . ?
Cl7_11 B7_11 B11_11 B10_11 148.7(6) . . . . ?
B12_11 B7_11 B11_11 B10_11 37.1(6) . . . . ?
B2_11 B7_11 B11_11 B10_11 -100.8(6) . . . . ?
B8_11 B7_11 B11_11 B10_11 -0.5(8) . . . . ?
B6_11 B7_11 B11_11 B10_11 -62.7(7) . . . . ?
Cl7_11 B7_11 B11_11 B2_11 -110.5(7) . . . . ?
B12_11 B7_11 B11_11 B2_11 137.9(6) . . . . ?
B8_11 B7_11 B11_11 B2_11 100.3(6) . . . . ?
B6_11 B7_11 B11_11 B2_11 38.1(5) . . . . ?
Cl7_11 B7_11 B11_11 Cl11_11 3.2(10) . . . . ?
B12_11 B7_11 B11_11 Cl11_11 -108.4(7) . . . . ?
B2_11 B7_11 B11_11 Cl11_11 113.7(7) . . . . ?
B8_11 B7_11 B11_11 Cl11_11 -146.0(6) . . . . ?
B6_11 B7_11 B11_11 Cl11_11 151.8(6) . . . . ?
B1_11 B2_11 B11_11 B3_11 38.8(6) . . . . ?
B6_11 B2_11 B11_11 B3_11 101.2(6) . . . . ?
B7_11 B2_11 B11_11 B3_11 139.6(6) . . . . ?
Cl6_11 B2_11 B11_11 B3_11 -111.0(7) . . . . ?
B1_11 B2_11 B11_11 B12_11 -63.0(7) . . . . ?
B3_11 B2_11 B11_11 B12_11 -101.8(6) . . . . ?
B6_11 B2_11 B11_11 B12_11 -0.6(8) . . . . ?
B7_11 B2_11 B11_11 B12_11 37.8(5) . . . . ?
Cl6_11 B2_11 B11_11 B12_11 147.2(6) . . . . ?
B1_11 B2_11 B11_11 B10_11 1.3(8) . . . . ?
B3_11 B2_11 B11_11 B10_11 -37.5(6) . . . . ?
B6_11 B2_11 B11_11 B10_11 63.7(7) . . . . ?
B7_11 B2_11 B11_11 B10_11 102.0(6) . . . . ?
Cl6_11 B2_11 B11_11 B10_11 -148.5(6) . . . . ?
B1_11 B2_11 B11_11 B7_11 -100.8(6) . . . . ?
B3_11 B2_11 B11_11 B7_11 -139.6(6) . . . . ?
B6_11 B2_11 B11_11 B7_11 -38.4(5) . . . . ?
Cl6_11 B2_11 B11_11 B7_11 109.4(7) . . . . ?
B1_11 B2_11 B11_11 Cl11_11 149.0(6) . . . . ?
B3_11 B2_11 B11_11 Cl11_11 110.2(7) . . . . ?
B6_11 B2_11 B11_11 Cl11_11 -148.6(6) . . . . ?
B7_11 B2_11 B11_11 Cl11_11 -110.2(7) . . . . ?
Cl6_11 B2_11 B11_11 Cl11_11 -0.8(10) . . . . ?
B6_11 B8_11 B12_11 B11_11 -0.9(8) . . . . ?
B9_11 B8_11 B12_11 B11_11 100.0(6) . . . . ?
B5_11 B8_11 B12_11 B11_11 62.5(7) . . . . ?
Cl8_11 B8_11 B12_11 B11_11 -147.1(5) . . . . ?
B7_11 B8_11 B12_11 B11_11 -38.5(5) . . . . ?
B6_11 B8_11 B12_11 B7_11 37.6(6) . . . . ?
B9_11 B8_11 B12_11 B7_11 138.4(6) . . . . ?
B5_11 B8_11 B12_11 B7_11 100.9(6) . . . . ?
Cl8_11 B8_11 B12_11 B7_11 -108.7(6) . . . . ?
B6_11 B8_11 B12_11 Cl12_11 148.9(6) . . . . ?
B9_11 B8_11 B12_11 Cl12_11 -110.2(6) . . . . ?
B5_11 B8_11 B12_11 Cl12_11 -147.8(5) . . . . ?
Cl8_11 B8_11 B12_11 Cl12_11 2.7(9) . . . . ?
B7_11 B8_11 B12_11 Cl12_11 111.3(6) . . . . ?
B6_11 B8_11 B12_11 B9_11 -100.9(6) . . . . ?
B5_11 B8_11 B12_11 B9_11 -37.5(5) . . . . ?
Cl8_11 B8_11 B12_11 B9_11 112.9(6) . . . . ?
B7_11 B8_11 B12_11 B9_11 -138.4(6) . . . . ?
B6_11 B8_11 B12_11 B10_11 -64.1(7) . . . . ?
B9_11 B8_11 B12_11 B10_11 36.8(5) . . . . ?
B5_11 B8_11 B12_11 B10_11 -0.7(7) . . . . ?
Cl8_11 B8_11 B12_11 B10_11 149.7(5) . . . . ?
B7_11 B8_11 B12_11 B10_11 -101.6(6) . . . . ?
B3_11 B11_11 B12_11 B8_11 -63.0(7) . . . . ?
B10_11 B11_11 B12_11 B8_11 -100.3(6) . . . . ?
B7_11 B11_11 B12_11 B8_11 38.8(6) . . . . ?
B2_11 B11_11 B12_11 B8_11 0.9(7) . . . . ?
Cl11_11 B11_11 B12_11 B8_11 150.5(6) . . . . ?
B3_11 B11_11 B12_11 B7_11 -101.8(6) . . . . ?
B10_11 B11_11 B12_11 B7_11 -139.1(6) . . . . ?
B2_11 B11_11 B12_11 B7_11 -37.9(6) . . . . ?
Cl11_11 B11_11 B12_11 B7_11 111.6(7) . . . . ?
B3_11 B11_11 B12_11 Cl12_11 146.8(5) . . . . ?
B10_11 B11_11 B12_11 Cl12_11 109.5(6) . . . . ?
B7_11 B11_11 B12_11 Cl12_11 -111.4(6) . . . . ?
B2_11 B11_11 B12_11 Cl12_11 -149.3(5) . . . . ?
Cl11_11 B11_11 B12_11 Cl12_11 0.3(9) . . . . ?
B3_11 B11_11 B12_11 B9_11 0.5(8) . . . . ?
B10_11 B11_11 B12_11 B9_11 -36.8(5) . . . . ?
B7_11 B11_11 B12_11 B9_11 102.3(6) . . . . ?
B2_11 B11_11 B12_11 B9_11 64.4(7) . . . . ?
Cl11_11 B11_11 B12_11 B9_11 -146.1(6) . . . . ?
B3_11 B11_11 B12_11 B10_11 37.3(5) . . . . ?
B7_11 B11_11 B12_11 B10_11 139.1(6) . . . . ?
B2_11 B11_11 B12_11 B10_11 101.2(6) . . . . ?
Cl11_11 B11_11 B12_11 B10_11 -109.2(7) . . . . ?
Cl7_11 B7_11 B12_11 B8_11 110.9(7) . . . . ?
B11_11 B7_11 B12_11 B8_11 -137.0(6) . . . . ?
B2_11 B7_11 B12_11 B8_11 -99.5(6) . . . . ?
B6_11 B7_11 B12_11 B8_11 -36.6(6) . . . . ?
Cl7_11 B7_11 B12_11 B11_11 -112.1(7) . . . . ?
B2_11 B7_11 B12_11 B11_11 37.5(5) . . . . ?
B8_11 B7_11 B12_11 B11_11 137.0(6) . . . . ?
B6_11 B7_11 B12_11 B11_11 100.4(6) . . . . ?
Cl7_11 B7_11 B12_11 Cl12_11 -1.4(10) . . . . ?
B11_11 B7_11 B12_11 Cl12_11 110.6(7) . . . . ?
B2_11 B7_11 B12_11 Cl12_11 148.1(6) . . . . ?
B8_11 B7_11 B12_11 Cl12_11 -112.4(7) . . . . ?
B6_11 B7_11 B12_11 Cl12_11 -149.0(6) . . . . ?
Cl7_11 B7_11 B12_11 B9_11 148.4(6) . . . . ?
B11_11 B7_11 B12_11 B9_11 -99.5(6) . . . . ?
B2_11 B7_11 B12_11 B9_11 -62.1(7) . . . . ?
B8_11 B7_11 B12_11 B9_11 37.5(5) . . . . ?
B6_11 B7_11 B12_11 B9_11 0.9(8) . . . . ?
Cl7_11 B7_11 B12_11 B10_11 -148.7(6) . . . . ?
B11_11 B7_11 B12_11 B10_11 -36.6(6) . . . . ?
B2_11 B7_11 B12_11 B10_11 0.9(8) . . . . ?
B8_11 B7_11 B12_11 B10_11 100.4(6) . . . . ?
B6_11 B7_11 B12_11 B10_11 63.8(7) . . . . ?
B10_11 B9_11 B12_11 B8_11 138.4(6) . . . . ?
B4_11 B9_11 B12_11 B8_11 100.5(6) . . . . ?
B5_11 B9_11 B12_11 B8_11 37.4(5) . . . . ?
Cl9_11 B9_11 B12_11 B8_11 -110.6(7) . . . . ?
B10_11 B9_11 B12_11 B11_11 37.1(5) . . . . ?
B4_11 B9_11 B12_11 B11_11 -0.8(7) . . . . ?
B5_11 B9_11 B12_11 B11_11 -63.9(7) . . . . ?
B8_11 B9_11 B12_11 B11_11 -101.3(6) . . . . ?
Cl9_11 B9_11 B12_11 B11_11 148.1(6) . . . . ?
B10_11 B9_11 B12_11 B7_11 100.6(6) . . . . ?
B4_11 B9_11 B12_11 B7_11 62.7(7) . . . . ?
B5_11 B9_11 B12_11 B7_11 -0.4(8) . . . . ?
B8_11 B9_11 B12_11 B7_11 -37.8(6) . . . . ?
Cl9_11 B9_11 B12_11 B7_11 -148.4(6) . . . . ?
B10_11 B9_11 B12_11 Cl12_11 -109.3(6) . . . . ?
B4_11 B9_11 B12_11 Cl12_11 -147.2(6) . . . . ?
B5_11 B9_11 B12_11 Cl12_11 149.7(6) . . . . ?
B8_11 B9_11 B12_11 Cl12_11 112.3(7) . . . . ?
Cl9_11 B9_11 B12_11 Cl12_11 1.6(9) . . . . ?
B4_11 B9_11 B12_11 B10_11 -37.9(5) . . . . ?
B5_11 B9_11 B12_11 B10_11 -101.0(6) . . . . ?
B8_11 B9_11 B12_11 B10_11 -138.4(6) . . . . ?
Cl9_11 B9_11 B12_11 B10_11 111.0(6) . . . . ?
B9_11 B10_11 B12_11 B8_11 -37.2(5) . . . . ?
B4_11 B10_11 B12_11 B8_11 0.6(7) . . . . ?
B11_11 B10_11 B12_11 B8_11 101.1(6) . . . . ?
B3_11 B10_11 B12_11 B8_11 64.5(7) . . . . ?
Cl10_11 B10_11 B12_11 B8_11 -148.2(5) . . . . ?
B9_11 B10_11 B12_11 B11_11 -138.3(6) . . . . ?
B4_11 B10_11 B12_11 B11_11 -100.5(6) . . . . ?
B3_11 B10_11 B12_11 B11_11 -36.6(5) . . . . ?
Cl10_11 B10_11 B12_11 B11_11 110.7(6) . . . . ?
B9_11 B10_11 B12_11 B7_11 -101.6(6) . . . . ?
B4_11 B10_11 B12_11 B7_11 -63.8(7) . . . . ?
B11_11 B10_11 B12_11 B7_11 36.7(6) . . . . ?
B3_11 B10_11 B12_11 B7_11 0.1(8) . . . . ?
Cl10_11 B10_11 B12_11 B7_11 147.4(5) . . . . ?
B9_11 B10_11 B12_11 Cl12_11 110.7(6) . . . . ?
B4_11 B10_11 B12_11 Cl12_11 148.4(5) . . . . ?
B11_11 B10_11 B12_11 Cl12_11 -111.1(6) . . . . ?
B3_11 B10_11 B12_11 Cl12_11 -147.7(5) . . . . ?
Cl10_11 B10_11 B12_11 Cl12_11 -0.4(8) . . . . ?
B4_11 B10_11 B12_11 B9_11 37.8(5) . . . . ?
B11_11 B10_11 B12_11 B9_11 138.3(6) . . . . ?
B3_11 B10_11 B12_11 B9_11 101.6(6) . . . . ?
Cl10_11 B10_11 B12_11 B9_11 -111.0(6) . . . . ?
B4_12 B1_12 B2_12 B3_12 137.6(6) . . . . ?
B5_12 B1_12 B2_12 B3_12 37.2(6) . . . . ?
Cl1_12 B1_12 B2_12 B3_12 -112.0(7) . . . . ?
B6_12 B1_12 B2_12 B3_12 100.7(7) . . . . ?
B3_12 B1_12 B2_12 B4_12 -137.6(6) . . . . ?
B5_12 B1_12 B2_12 B4_12 -100.4(6) . . . . ?
Cl1_12 B1_12 B2_12 B4_12 110.4(7) . . . . ?
B6_12 B1_12 B2_12 B4_12 -36.9(6) . . . . ?
B3_12 B1_12 B2_12 B11_12 -37.3(6) . . . . ?
B4_12 B1_12 B2_12 B11_12 100.3(7) . . . . ?
B5_12 B1_12 B2_12 B11_12 -0.1(8) . . . . ?
Cl1_12 B1_12 B2_12 B11_12 -149.3(6) . . . . ?
B6_12 B1_12 B2_12 B11_12 63.4(8) . . . . ?
B3_12 B1_12 B2_12 Cl2_12 111.2(7) . . . . ?
B4_12 B1_12 B2_12 Cl2_12 -111.2(7) . . . . ?
B5_12 B1_12 B2_12 Cl2_12 148.4(6) . . . . ?
Cl1_12 B1_12 B2_12 Cl2_12 -0.8(10) . . . . ?
B6_12 B1_12 B2_12 Cl2_12 -148.1(6) . . . . ?
B3_12 B1_12 B2_12 B10_12 -99.8(7) . . . . ?
B4_12 B1_12 B2_12 B10_12 37.8(6) . . . . ?
B5_12 B1_12 B2_12 B10_12 -62.6(8) . . . . ?
Cl1_12 B1_12 B2_12 B10_12 148.2(6) . . . . ?
B6_12 B1_12 B2_12 B10_12 0.9(8) . . . . ?
B2_12 B1_12 B3_12 B5_12 138.4(6) . . . . ?
B4_12 B1_12 B3_12 B5_12 99.9(7) . . . . ?
Cl1_12 B1_12 B3_12 B5_12 -110.0(8) . . . . ?
B6_12 B1_12 B3_12 B5_12 37.1(6) . . . . ?
B4_12 B1_12 B3_12 B2_12 -38.4(6) . . . . ?
B5_12 B1_12 B3_12 B2_12 -138.4(6) . . . . ?
Cl1_12 B1_12 B3_12 B2_12 111.6(8) . . . . ?
B6_12 B1_12 B3_12 B2_12 -101.2(6) . . . . ?
B2_12 B1_12 B3_12 B11_12 37.5(6) . . . . ?
B4_12 B1_12 B3_12 B11_12 -0.9(9) . . . . ?
B5_12 B1_12 B3_12 B11_12 -100.9(7) . . . . ?
Cl1_12 B1_12 B3_12 B11_12 149.1(6) . . . . ?
B6_12 B1_12 B3_12 B11_12 -63.7(8) . . . . ?
B2_12 B1_12 B3_12 Cl3_12 -109.9(7) . . . . ?
B4_12 B1_12 B3_12 Cl3_12 -148.3(6) . . . . ?
B5_12 B1_12 B3_12 Cl3_12 111.8(7) . . . . ?
Cl1_12 B1_12 B3_12 Cl3_12 1.7(10) . . . . ?
B6_12 B1_12 B3_12 Cl3_12 148.9(6) . . . . ?
B2_12 B1_12 B3_12 B9_12 101.0(7) . . . . ?
B4_12 B1_12 B3_12 B9_12 62.6(8) . . . . ?
B5_12 B1_12 B3_12 B9_12 -37.3(6) . . . . ?
Cl1_12 B1_12 B3_12 B9_12 -147.3(7) . . . . ?
B6_12 B1_12 B3_12 B9_12 -0.2(8) . . . . ?
B4_12 B2_12 B3_12 B1_12 38.4(6) . . . . ?
B11_12 B2_12 B3_12 B1_12 138.2(7) . . . . ?
Cl2_12 B2_12 B3_12 B1_12 -109.3(7) . . . . ?
B10_12 B2_12 B3_12 B1_12 102.0(7) . . . . ?
B1_12 B2_12 B3_12 B5_12 -37.6(6) . . . . ?
B4_12 B2_12 B3_12 B5_12 0.8(8) . . . . ?
B11_12 B2_12 B3_12 B5_12 100.6(7) . . . . ?
Cl2_12 B2_12 B3_12 B5_12 -146.9(6) . . . . ?
B10_12 B2_12 B3_12 B5_12 64.5(8) . . . . ?
B1_12 B2_12 B3_12 B11_12 -138.2(7) . . . . ?
B4_12 B2_12 B3_12 B11_12 -99.8(6) . . . . ?
Cl2_12 B2_12 B3_12 B11_12 112.5(7) . . . . ?
B10_12 B2_12 B3_12 B11_12 -36.2(6) . . . . ?
B1_12 B2_12 B3_12 Cl3_12 109.9(7) . . . . ?
B4_12 B2_12 B3_12 Cl3_12 148.3(6) . . . . ?
B11_12 B2_12 B3_12 Cl3_12 -111.9(7) . . . . ?
Cl2_12 B2_12 B3_12 Cl3_12 0.5(10) . . . . ?
B10_12 B2_12 B3_12 Cl3_12 -148.1(6) . . . . ?
B1_12 B2_12 B3_12 B9_12 -101.2(6) . . . . ?
B4_12 B2_12 B3_12 B9_12 -62.8(7) . . . . ?
B11_12 B2_12 B3_12 B9_12 37.0(6) . . . . ?
Cl2_12 B2_12 B3_12 B9_12 149.4(6) . . . . ?
B10_12 B2_12 B3_12 B9_12 0.8(8) . . . . ?
B1_12 B2_12 B4_12 B6_12 37.7(6) . . . . ?
B3_12 B2_12 B4_12 B6_12 -0.5(8) . . . . ?
B11_12 B2_12 B4_12 B6_12 -63.6(8) . . . . ?
Cl2_12 B2_12 B4_12 B6_12 147.3(6) . . . . ?
B10_12 B2_12 B4_12 B6_12 -100.2(6) . . . . ?
B1_12 B2_12 B4_12 B8_12 100.7(7) . . . . ?
B3_12 B2_12 B4_12 B8_12 62.5(8) . . . . ?
B11_12 B2_12 B4_12 B8_12 -0.7(8) . . . . ?
Cl2_12 B2_12 B4_12 B8_12 -149.7(6) . . . . ?
B10_12 B2_12 B4_12 B8_12 -37.3(6) . . . . ?
B3_12 B2_12 B4_12 B1_12 -38.2(6) . . . . ?
B11_12 B2_12 B4_12 B1_12 -101.4(7) . . . . ?
Cl2_12 B2_12 B4_12 B1_12 109.6(7) . . . . ?
B10_12 B2_12 B4_12 B1_12 -138.0(6) . . . . ?
B1_12 B2_12 B4_12 B10_12 138.0(6) . . . . ?
B3_12 B2_12 B4_12 B10_12 99.8(7) . . . . ?
B11_12 B2_12 B4_12 B10_12 36.6(6) . . . . ?
Cl2_12 B2_12 B4_12 B10_12 -112.4(7) . . . . ?
B1_12 B2_12 B4_12 Cl4_12 -110.8(7) . . . . ?
B3_12 B2_12 B4_12 Cl4_12 -149.0(6) . . . . ?
B11_12 B2_12 B4_12 Cl4_12 147.8(6) . . . . ?
Cl2_12 B2_12 B4_12 Cl4_12 -1.2(9) . . . . ?
B10_12 B2_12 B4_12 Cl4_12 111.2(7) . . . . ?
B2_12 B1_12 B4_12 B6_12 -138.4(6) . . . . ?
B3_12 B1_12 B4_12 B6_12 -100.0(7) . . . . ?
B5_12 B1_12 B4_12 B6_12 -36.7(6) . . . . ?
Cl1_12 B1_12 B4_12 B6_12 109.5(8) . . . . ?
B3_12 B1_12 B4_12 B2_12 38.5(6) . . . . ?
B5_12 B1_12 B4_12 B2_12 101.7(7) . . . . ?
Cl1_12 B1_12 B4_12 B2_12 -112.0(8) . . . . ?
B6_12 B1_12 B4_12 B2_12 138.4(6) . . . . ?
B2_12 B1_12 B4_12 B8_12 -101.2(7) . . . . ?
B3_12 B1_12 B4_12 B8_12 -62.7(9) . . . . ?
B5_12 B1_12 B4_12 B8_12 0.5(9) . . . . ?
Cl1_12 B1_12 B4_12 B8_12 146.8(6) . . . . ?
B6_12 B1_12 B4_12 B8_12 37.3(6) . . . . ?
B2_12 B1_12 B4_12 B10_12 -37.9(6) . . . . ?
B3_12 B1_12 B4_12 B10_12 0.6(9) . . . . ?
B5_12 B1_12 B4_12 B10_12 63.8(8) . . . . ?
Cl1_12 B1_12 B4_12 B10_12 -149.9(6) . . . . ?
B6_12 B1_12 B4_12 B10_12 100.6(7) . . . . ?
B2_12 B1_12 B4_12 Cl4_12 110.0(8) . . . . ?
B3_12 B1_12 B4_12 Cl4_12 148.5(6) . . . . ?
B5_12 B1_12 B4_12 Cl4_12 -148.3(6) . . . . ?
Cl1_12 B1_12 B4_12 Cl4_12 -2.0(11) . . . . ?
B6_12 B1_12 B4_12 Cl4_12 -111.6(8) . . . . ?
B1_12 B3_12 B5_12 Cl5_12 110.3(8) . . . . ?
B2_12 B3_12 B5_12 Cl5_12 147.0(6) . . . . ?
B11_12 B3_12 B5_12 Cl5_12 -149.1(7) . . . . ?
Cl3_12 B3_12 B5_12 Cl5_12 -0.2(11) . . . . ?
B9_12 B3_12 B5_12 Cl5_12 -111.1(8) . . . . ?
B1_12 B3_12 B5_12 B9_12 -138.6(6) . . . . ?
B2_12 B3_12 B5_12 B9_12 -101.9(7) . . . . ?
B11_12 B3_12 B5_12 B9_12 -38.0(6) . . . . ?
Cl3_12 B3_12 B5_12 B9_12 111.0(8) . . . . ?
B2_12 B3_12 B5_12 B1_12 36.6(6) . . . . ?
B11_12 B3_12 B5_12 B1_12 100.6(7) . . . . ?
Cl3_12 B3_12 B5_12 B1_12 -110.5(7) . . . . ?
B9_12 B3_12 B5_12 B1_12 138.6(6) . . . . ?
B1_12 B3_12 B5_12 B6_12 -37.5(6) . . . . ?
B2_12 B3_12 B5_12 B6_12 -0.9(9) . . . . ?
B11_12 B3_12 B5_12 B6_12 63.0(8) . . . . ?
Cl3_12 B3_12 B5_12 B6_12 -148.0(6) . . . . ?
B9_12 B3_12 B5_12 B6_12 101.1(7) . . . . ?
B1_12 B3_12 B5_12 B7_12 -100.2(6) . . . . ?
B2_12 B3_12 B5_12 B7_12 -63.6(8) . . . . ?
B11_12 B3_12 B5_12 B7_12 0.3(9) . . . . ?
Cl3_12 B3_12 B5_12 B7_12 149.3(6) . . . . ?
B9_12 B3_12 B5_12 B7_12 38.4(6) . . . . ?
B2_12 B1_12 B5_12 B3_12 -37.7(6) . . . . ?
B4_12 B1_12 B5_12 B3_12 -102.0(7) . . . . ?
Cl1_12 B1_12 B5_12 B3_12 111.8(7) . . . . ?
B6_12 B1_12 B5_12 B3_12 -138.4(6) . . . . ?
B2_12 B1_12 B5_12 Cl5_12 -149.4(6) . . . . ?
B3_12 B1_12 B5_12 Cl5_12 -111.7(7) . . . . ?
B4_12 B1_12 B5_12 Cl5_12 146.4(6) . . . . ?
Cl1_12 B1_12 B5_12 Cl5_12 0.2(10) . . . . ?
B6_12 B1_12 B5_12 Cl5_12 109.9(7) . . . . ?
B2_12 B1_12 B5_12 B9_12 -0.3(8) . . . . ?
B3_12 B1_12 B5_12 B9_12 37.5(6) . . . . ?
B4_12 B1_12 B5_12 B9_12 -64.5(8) . . . . ?
Cl1_12 B1_12 B5_12 B9_12 149.3(6) . . . . ?
B6_12 B1_12 B5_12 B9_12 -100.9(7) . . . . ?
B2_12 B1_12 B5_12 B6_12 100.7(6) . . . . ?
B3_12 B1_12 B5_12 B6_12 138.4(6) . . . . ?
B4_12 B1_12 B5_12 B6_12 36.4(6) . . . . ?
Cl1_12 B1_12 B5_12 B6_12 -109.8(7) . . . . ?
B2_12 B1_12 B5_12 B7_12 63.6(8) . . . . ?
B3_12 B1_12 B5_12 B7_12 101.3(7) . . . . ?
B4_12 B1_12 B5_12 B7_12 -0.7(8) . . . . ?
Cl1_12 B1_12 B5_12 B7_12 -146.9(6) . . . . ?
B6_12 B1_12 B5_12 B7_12 -37.1(6) . . . . ?
B2_12 B4_12 B6_12 B8_12 101.7(6) . . . . ?
B1_12 B4_12 B6_12 B8_12 138.2(6) . . . . ?
B10_12 B4_12 B6_12 B8_12 37.3(6) . . . . ?
Cl4_12 B4_12 B6_12 B8_12 -109.9(7) . . . . ?
B2_12 B4_12 B6_12 B7_12 63.7(8) . . . . ?
B8_12 B4_12 B6_12 B7_12 -37.9(6) . . . . ?
B1_12 B4_12 B6_12 B7_12 100.2(7) . . . . ?
B10_12 B4_12 B6_12 B7_12 -0.6(8) . . . . ?
Cl4_12 B4_12 B6_12 B7_12 -147.8(6) . . . . ?
B2_12 B4_12 B6_12 Cl6_12 -146.4(6) . . . . ?
B8_12 B4_12 B6_12 Cl6_12 112.0(7) . . . . ?
B1_12 B4_12 B6_12 Cl6_12 -109.9(7) . . . . ?
B10_12 B4_12 B6_12 Cl6_12 149.2(6) . . . . ?
Cl4_12 B4_12 B6_12 Cl6_12 2.1(9) . . . . ?
B2_12 B4_12 B6_12 B5_12 -0.1(8) . . . . ?
B8_12 B4_12 B6_12 B5_12 -101.7(7) . . . . ?
B1_12 B4_12 B6_12 B5_12 36.4(6) . . . . ?
B10_12 B4_12 B6_12 B5_12 -64.5(8) . . . . ?
Cl4_12 B4_12 B6_12 B5_12 148.4(6) . . . . ?
B2_12 B4_12 B6_12 B1_12 -36.5(6) . . . . ?
B8_12 B4_12 B6_12 B1_12 -138.2(6) . . . . ?
B10_12 B4_12 B6_12 B1_12 -100.9(7) . . . . ?
Cl4_12 B4_12 B6_12 B1_12 112.0(7) . . . . ?
B3_12 B5_12 B6_12 B8_12 -63.2(8) . . . . ?
Cl5_12 B5_12 B6_12 B8_12 148.3(7) . . . . ?
B9_12 B5_12 B6_12 B8_12 1.2(9) . . . . ?
B1_12 B5_12 B6_12 B8_12 -100.2(7) . . . . ?
B7_12 B5_12 B6_12 B8_12 37.9(6) . . . . ?
B3_12 B5_12 B6_12 B4_12 0.6(9) . . . . ?
Cl5_12 B5_12 B6_12 B4_12 -147.9(6) . . . . ?
B9_12 B5_12 B6_12 B4_12 64.9(8) . . . . ?
B1_12 B5_12 B6_12 B4_12 -36.4(6) . . . . ?
B7_12 B5_12 B6_12 B4_12 101.6(7) . . . . ?
B3_12 B5_12 B6_12 B7_12 -101.0(7) . . . . ?
Cl5_12 B5_12 B6_12 B7_12 110.5(8) . . . . ?
B9_12 B5_12 B6_12 B7_12 -36.7(6) . . . . ?
B1_12 B5_12 B6_12 B7_12 -138.0(7) . . . . ?
B3_12 B5_12 B6_12 Cl6_12 145.1(7) . . . . ?
Cl5_12 B5_12 B6_12 Cl6_12 -3.5(11) . . . . ?
B9_12 B5_12 B6_12 Cl6_12 -150.6(6) . . . . ?
B1_12 B5_12 B6_12 Cl6_12 108.1(7) . . . . ?
B7_12 B5_12 B6_12 Cl6_12 -113.9(8) . . . . ?
B3_12 B5_12 B6_12 B1_12 37.0(6) . . . . ?
Cl5_12 B5_12 B6_12 B1_12 -111.5(8) . . . . ?
B9_12 B5_12 B6_12 B1_12 101.3(7) . . . . ?
B7_12 B5_12 B6_12 B1_12 138.0(7) . . . . ?
B2_12 B1_12 B6_12 B8_12 0.0(8) . . . . ?
B3_12 B1_12 B6_12 B8_12 64.3(8) . . . . ?
B4_12 B1_12 B6_12 B8_12 -37.5(6) . . . . ?
B5_12 B1_12 B6_12 B8_12 101.3(7) . . . . ?
Cl1_12 B1_12 B6_12 B8_12 -147.8(6) . . . . ?
B2_12 B1_12 B6_12 B4_12 37.5(6) . . . . ?
B3_12 B1_12 B6_12 B4_12 101.8(7) . . . . ?
B5_12 B1_12 B6_12 B4_12 138.8(6) . . . . ?
Cl1_12 B1_12 B6_12 B4_12 -110.3(7) . . . . ?
B2_12 B1_12 B6_12 B7_12 -63.7(8) . . . . ?
B3_12 B1_12 B6_12 B7_12 0.6(8) . . . . ?
B4_12 B1_12 B6_12 B7_12 -101.2(7) . . . . ?
B5_12 B1_12 B6_12 B7_12 37.6(6) . . . . ?
Cl1_12 B1_12 B6_12 B7_12 148.5(6) . . . . ?
B2_12 B1_12 B6_12 Cl6_12 145.4(6) . . . . ?
B3_12 B1_12 B6_12 Cl6_12 -150.3(6) . . . . ?
B4_12 B1_12 B6_12 Cl6_12 107.9(7) . . . . ?
B5_12 B1_12 B6_12 Cl6_12 -113.3(7) . . . . ?
Cl1_12 B1_12 B6_12 Cl6_12 -2.4(10) . . . . ?
B2_12 B1_12 B6_12 B5_12 -101.3(7) . . . . ?
B3_12 B1_12 B6_12 B5_12 -37.0(6) . . . . ?
B4_12 B1_12 B6_12 B5_12 -138.8(6) . . . . ?
Cl1_12 B1_12 B6_12 B5_12 110.8(7) . . . . ?
B4_12 B6_12 B7_12 B8_12 37.9(6) . . . . ?
Cl6_12 B6_12 B7_12 B8_12 -109.9(8) . . . . ?
B5_12 B6_12 B7_12 B8_12 137.9(7) . . . . ?
B1_12 B6_12 B7_12 B8_12 100.7(7) . . . . ?
B8_12 B6_12 B7_12 B12_12 -38.0(6) . . . . ?
B4_12 B6_12 B7_12 B12_12 0.0(9) . . . . ?
Cl6_12 B6_12 B7_12 B12_12 -147.9(6) . . . . ?
B5_12 B6_12 B7_12 B12_12 100.0(7) . . . . ?
B1_12 B6_12 B7_12 B12_12 62.8(8) . . . . ?
B8_12 B6_12 B7_12 Cl7_12 112.4(8) . . . . ?
B4_12 B6_12 B7_12 Cl7_12 150.3(6) . . . . ?
Cl6_12 B6_12 B7_12 Cl7_12 2.5(11) . . . . ?
B5_12 B6_12 B7_12 Cl7_12 -109.7(8) . . . . ?
B1_12 B6_12 B7_12 Cl7_12 -146.9(6) . . . . ?
B8_12 B6_12 B7_12 B5_12 -137.9(7) . . . . ?
B4_12 B6_12 B7_12 B5_12 -100.0(7) . . . . ?
Cl6_12 B6_12 B7_12 B5_12 112.2(8) . . . . ?
B1_12 B6_12 B7_12 B5_12 -37.2(6) . . . . ?
B8_12 B6_12 B7_12 B9_12 -101.5(7) . . . . ?
B4_12 B6_12 B7_12 B9_12 -63.6(8) . . . . ?
Cl6_12 B6_12 B7_12 B9_12 148.5(6) . . . . ?
B5_12 B6_12 B7_12 B9_12 36.4(6) . . . . ?
B1_12 B6_12 B7_12 B9_12 -0.8(9) . . . . ?
B3_12 B5_12 B7_12 B8_12 63.4(8) . . . . ?
Cl5_12 B5_12 B7_12 B8_12 -146.7(6) . . . . ?
B9_12 B5_12 B7_12 B8_12 102.0(7) . . . . ?
B1_12 B5_12 B7_12 B8_12 0.5(8) . . . . ?
B6_12 B5_12 B7_12 B8_12 -37.2(6) . . . . ?
B3_12 B5_12 B7_12 B6_12 100.6(7) . . . . ?
Cl5_12 B5_12 B7_12 B6_12 -109.4(7) . . . . ?
B9_12 B5_12 B7_12 B6_12 139.2(7) . . . . ?
B1_12 B5_12 B7_12 B6_12 37.7(6) . . . . ?
B3_12 B5_12 B7_12 B12_12 -1.4(9) . . . . ?
Cl5_12 B5_12 B7_12 B12_12 148.5(6) . . . . ?
B9_12 B5_12 B7_12 B12_12 37.1(6) . . . . ?
B1_12 B5_12 B7_12 B12_12 -64.3(8) . . . . ?
B6_12 B5_12 B7_12 B12_12 -102.1(7) . . . . ?
B3_12 B5_12 B7_12 Cl7_12 -148.5(6) . . . . ?
Cl5_12 B5_12 B7_12 Cl7_12 1.4(10) . . . . ?
B9_12 B5_12 B7_12 Cl7_12 -110.0(7) . . . . ?
B1_12 B5_12 B7_12 Cl7_12 148.6(6) . . . . ?
B6_12 B5_12 B7_12 Cl7_12 110.8(8) . . . . ?
B3_12 B5_12 B7_12 B9_12 -38.6(6) . . . . ?
Cl5_12 B5_12 B7_12 B9_12 111.4(7) . . . . ?
B1_12 B5_12 B7_12 B9_12 -101.5(7) . . . . ?
B6_12 B5_12 B7_12 B9_12 -139.2(7) . . . . ?
B7_12 B6_12 B8_12 B4_12 137.8(7) . . . . ?
Cl6_12 B6_12 B8_12 B4_12 -107.7(7) . . . . ?
B5_12 B6_12 B8_12 B4_12 99.9(7) . . . . ?
B1_12 B6_12 B8_12 B4_12 37.1(6) . . . . ?
B4_12 B6_12 B8_12 B7_12 -137.8(7) . . . . ?
Cl6_12 B6_12 B8_12 B7_12 114.5(8) . . . . ?
B5_12 B6_12 B8_12 B7_12 -37.9(6) . . . . ?
B1_12 B6_12 B8_12 B7_12 -100.7(7) . . . . ?
B4_12 B6_12 B8_12 Cl8_12 110.6(7) . . . . ?
B7_12 B6_12 B8_12 Cl8_12 -111.6(7) . . . . ?
Cl6_12 B6_12 B8_12 Cl8_12 2.9(10) . . . . ?
B5_12 B6_12 B8_12 Cl8_12 -149.5(6) . . . . ?
B1_12 B6_12 B8_12 Cl8_12 147.6(6) . . . . ?
B4_12 B6_12 B8_12 B10_12 -38.0(6) . . . . ?
B7_12 B6_12 B8_12 B10_12 99.8(7) . . . . ?
Cl6_12 B6_12 B8_12 B10_12 -145.8(6) . . . . ?
B5_12 B6_12 B8_12 B10_12 61.9(8) . . . . ?
B1_12 B6_12 B8_12 B10_12 -1.0(8) . . . . ?
B4_12 B6_12 B8_12 B12_12 -101.0(7) . . . . ?
B7_12 B6_12 B8_12 B12_12 36.8(6) . . . . ?
Cl6_12 B6_12 B8_12 B12_12 151.2(6) . . . . ?
B5_12 B6_12 B8_12 B12_12 -1.1(9) . . . . ?
B1_12 B6_12 B8_12 B12_12 -64.0(8) . . . . ?
B2_12 B4_12 B8_12 B6_12 -100.3(7) . . . . ?
B1_12 B4_12 B8_12 B6_12 -38.1(6) . . . . ?
B10_12 B4_12 B8_12 B6_12 -138.0(6) . . . . ?
Cl4_12 B4_12 B8_12 B6_12 111.1(7) . . . . ?
B6_12 B4_12 B8_12 B7_12 37.9(6) . . . . ?
B2_12 B4_12 B8_12 B7_12 -62.3(8) . . . . ?
B1_12 B4_12 B8_12 B7_12 -0.2(9) . . . . ?
B10_12 B4_12 B8_12 B7_12 -100.1(7) . . . . ?
Cl4_12 B4_12 B8_12 B7_12 149.0(6) . . . . ?
B6_12 B4_12 B8_12 Cl8_12 -111.1(7) . . . . ?
B2_12 B4_12 B8_12 Cl8_12 148.7(6) . . . . ?
B1_12 B4_12 B8_12 Cl8_12 -149.2(6) . . . . ?
B10_12 B4_12 B8_12 Cl8_12 110.9(7) . . . . ?
Cl4_12 B4_12 B8_12 Cl8_12 0.0(10) . . . . ?
B6_12 B4_12 B8_12 B10_12 138.0(6) . . . . ?
B2_12 B4_12 B8_12 B10_12 37.8(6) . . . . ?
B1_12 B4_12 B8_12 B10_12 99.9(7) . . . . ?
Cl4_12 B4_12 B8_12 B10_12 -110.9(7) . . . . ?
B6_12 B4_12 B8_12 B12_12 100.7(7) . . . . ?
B2_12 B4_12 B8_12 B12_12 0.4(8) . . . . ?
B1_12 B4_12 B8_12 B12_12 62.6(8) . . . . ?
B10_12 B4_12 B8_12 B12_12 -37.3(6) . . . . ?
Cl4_12 B4_12 B8_12 B12_12 -148.2(6) . . . . ?
B12_12 B7_12 B8_12 B6_12 138.5(7) . . . . ?
Cl7_12 B7_12 B8_12 B6_12 -109.3(8) . . . . ?
B5_12 B7_12 B8_12 B6_12 37.7(6) . . . . ?
B9_12 B7_12 B8_12 B6_12 100.6(7) . . . . ?
B6_12 B7_12 B8_12 B4_12 -37.9(6) . . . . ?
B12_12 B7_12 B8_12 B4_12 100.6(7) . . . . ?
Cl7_12 B7_12 B8_12 B4_12 -147.2(7) . . . . ?
B5_12 B7_12 B8_12 B4_12 -0.2(8) . . . . ?
B9_12 B7_12 B8_12 B4_12 62.8(8) . . . . ?
B6_12 B7_12 B8_12 Cl8_12 110.8(8) . . . . ?
B12_12 B7_12 B8_12 Cl8_12 -110.7(7) . . . . ?
Cl7_12 B7_12 B8_12 Cl8_12 1.5(11) . . . . ?
B5_12 B7_12 B8_12 Cl8_12 148.5(6) . . . . ?
B9_12 B7_12 B8_12 Cl8_12 -148.5(6) . . . . ?
B6_12 B7_12 B8_12 B10_12 -102.1(7) . . . . ?
B12_12 B7_12 B8_12 B10_12 36.4(6) . . . . ?
Cl7_12 B7_12 B8_12 B10_12 148.6(6) . . . . ?
B5_12 B7_12 B8_12 B10_12 -64.4(8) . . . . ?
B9_12 B7_12 B8_12 B10_12 -1.4(8) . . . . ?
B6_12 B7_12 B8_12 B12_12 -138.5(7) . . . . ?
Cl7_12 B7_12 B8_12 B12_12 112.2(8) . . . . ?
B5_12 B7_12 B8_12 B12_12 -100.8(7) . . . . ?
B9_12 B7_12 B8_12 B12_12 -37.9(6) . . . . ?
B3_12 B5_12 B9_12 Cl11_12 -112.7(7) . . . . ?
Cl5_12 B5_12 B9_12 Cl11_12 -0.5(10) . . . . ?
B1_12 B5_12 B9_12 Cl11_12 -149.6(6) . . . . ?
B6_12 B5_12 B9_12 Cl11_12 146.2(6) . . . . ?
B7_12 B5_12 B9_12 Cl11_12 110.0(7) . . . . ?
B3_12 B5_12 B9_12 B11_12 37.4(6) . . . . ?
Cl5_12 B5_12 B9_12 B11_12 149.5(6) . . . . ?
B1_12 B5_12 B9_12 B11_12 0.5(8) . . . . ?
B6_12 B5_12 B9_12 B11_12 -63.8(8) . . . . ?
B7_12 B5_12 B9_12 B11_12 -100.0(7) . . . . ?
B3_12 B5_12 B9_12 B12_12 100.4(7) . . . . ?
Cl5_12 B5_12 B9_12 B12_12 -147.5(6) . . . . ?
B1_12 B5_12 B9_12 B12_12 63.5(8) . . . . ?
B6_12 B5_12 B9_12 B12_12 -0.8(9) . . . . ?
B7_12 B5_12 B9_12 B12_12 -37.0(6) . . . . ?
Cl5_12 B5_12 B9_12 B3_12 112.2(7) . . . . ?
B1_12 B5_12 B9_12 B3_12 -36.9(6) . . . . ?
B6_12 B5_12 B9_12 B3_12 -101.1(7) . . . . ?
B7_12 B5_12 B9_12 B3_12 -137.3(7) . . . . ?
B3_12 B5_12 B9_12 B7_12 137.3(7) . . . . ?
Cl5_12 B5_12 B9_12 B7_12 -110.5(7) . . . . ?
B1_12 B5_12 B9_12 B7_12 100.4(7) . . . . ?
B6_12 B5_12 B9_12 B7_12 36.2(6) . . . . ?
B1_12 B3_12 B9_12 Cl11_12 147.3(6) . . . . ?
B5_12 B3_12 B9_12 Cl11_12 109.7(8) . . . . ?
B2_12 B3_12 B9_12 Cl11_12 -150.2(6) . . . . ?
B11_12 B3_12 B9_12 Cl11_12 -113.0(8) . . . . ?
Cl3_12 B3_12 B9_12 Cl11_12 -1.5(10) . . . . ?
B1_12 B3_12 B9_12 B5_12 37.6(6) . . . . ?
B2_12 B3_12 B9_12 B5_12 100.1(7) . . . . ?
B11_12 B3_12 B9_12 B5_12 137.3(6) . . . . ?
Cl3_12 B3_12 B9_12 B5_12 -111.2(7) . . . . ?
B1_12 B3_12 B9_12 B11_12 -99.7(7) . . . . ?
B5_12 B3_12 B9_12 B11_12 -137.3(6) . . . . ?
B2_12 B3_12 B9_12 B11_12 -37.2(6) . . . . ?
Cl3_12 B3_12 B9_12 B11_12 111.5(7) . . . . ?
B1_12 B3_12 B9_12 B12_12 -62.8(8) . . . . ?
B5_12 B3_12 B9_12 B12_12 -100.5(7) . . . . ?
B2_12 B3_12 B9_12 B12_12 -0.4(8) . . . . ?
B11_12 B3_12 B9_12 B12_12 36.8(6) . . . . ?
Cl3_12 B3_12 B9_12 B12_12 148.3(6) . . . . ?
B1_12 B3_12 B9_12 B7_12 -0.3(9) . . . . ?
B5_12 B3_12 B9_12 B7_12 -37.9(6) . . . . ?
B2_12 B3_12 B9_12 B7_12 62.2(8) . . . . ?
B11_12 B3_12 B9_12 B7_12 99.4(7) . . . . ?
Cl3_12 B3_12 B9_12 B7_12 -149.1(6) . . . . ?
B8_12 B7_12 B9_12 Cl11_12 149.1(6) . . . . ?
B6_12 B7_12 B9_12 Cl11_12 -147.9(6) . . . . ?
B12_12 B7_12 B9_12 Cl11_12 110.6(7) . . . . ?
Cl7_12 B7_12 B9_12 Cl11_12 -1.7(11) . . . . ?
B5_12 B7_12 B9_12 Cl11_12 -111.1(8) . . . . ?
B8_12 B7_12 B9_12 B5_12 -99.8(7) . . . . ?
B6_12 B7_12 B9_12 B5_12 -36.8(6) . . . . ?
B12_12 B7_12 B9_12 B5_12 -138.3(6) . . . . ?
Cl7_12 B7_12 B9_12 B5_12 109.4(8) . . . . ?
B8_12 B7_12 B9_12 B11_12 -0.1(8) . . . . ?
B6_12 B7_12 B9_12 B11_12 62.9(8) . . . . ?
B12_12 B7_12 B9_12 B11_12 -38.6(6) . . . . ?
Cl7_12 B7_12 B9_12 B11_12 -150.9(6) . . . . ?
B5_12 B7_12 B9_12 B11_12 99.7(7) . . . . ?
B8_12 B7_12 B9_12 B12_12 38.5(6) . . . . ?
B6_12 B7_12 B9_12 B12_12 101.5(7) . . . . ?
Cl7_12 B7_12 B9_12 B12_12 -112.3(8) . . . . ?
B5_12 B7_12 B9_12 B12_12 138.3(6) . . . . ?
B8_12 B7_12 B9_12 B3_12 -62.3(8) . . . . ?
B6_12 B7_12 B9_12 B3_12 0.7(9) . . . . ?
B12_12 B7_12 B9_12 B3_12 -100.8(7) . . . . ?
Cl7_12 B7_12 B9_12 B3_12 146.9(6) . . . . ?
B5_12 B7_12 B9_12 B3_12 37.5(6) . . . . ?
B6_12 B8_12 B10_12 B11_12 -61.4(8) . . . . ?
B4_12 B8_12 B10_12 B11_12 -99.2(7) . . . . ?
B7_12 B8_12 B10_12 B11_12 2.4(8) . . . . ?
Cl8_12 B8_12 B10_12 B11_12 149.8(6) . . . . ?
B12_12 B8_12 B10_12 B11_12 38.8(6) . . . . ?
B6_12 B8_12 B10_12 Cl9_12 147.9(6) . . . . ?
B4_12 B8_12 B10_12 Cl9_12 110.1(7) . . . . ?
B7_12 B8_12 B10_12 Cl9_12 -148.3(6) . . . . ?
Cl8_12 B8_12 B10_12 Cl9_12 -0.9(10) . . . . ?
B12_12 B8_12 B10_12 Cl9_12 -111.9(7) . . . . ?
B6_12 B8_12 B10_12 B12_12 -100.2(7) . . . . ?
B4_12 B8_12 B10_12 B12_12 -138.0(6) . . . . ?
B7_12 B8_12 B10_12 B12_12 -36.4(6) . . . . ?
Cl8_12 B8_12 B10_12 B12_12 111.1(7) . . . . ?
B6_12 B8_12 B10_12 B4_12 37.8(6) . . . . ?
B7_12 B8_12 B10_12 B4_12 101.6(7) . . . . ?
Cl8_12 B8_12 B10_12 B4_12 -110.9(7) . . . . ?
B12_12 B8_12 B10_12 B4_12 138.0(6) . . . . ?
B6_12 B8_12 B10_12 B2_12 1.5(8) . . . . ?
B4_12 B8_12 B10_12 B2_12 -36.3(6) . . . . ?
B7_12 B8_12 B10_12 B2_12 65.3(8) . . . . ?
Cl8_12 B8_12 B10_12 B2_12 -147.2(6) . . . . ?
B12_12 B8_12 B10_12 B2_12 101.7(7) . . . . ?
B6_12 B4_12 B10_12 B11_12 64.6(8) . . . . ?
B2_12 B4_12 B10_12 B11_12 -36.8(6) . . . . ?
B8_12 B4_12 B10_12 B11_12 101.7(7) . . . . ?
B1_12 B4_12 B10_12 B11_12 0.0(8) . . . . ?
Cl4_12 B4_12 B10_12 B11_12 -148.1(6) . . . . ?
B6_12 B4_12 B10_12 Cl9_12 -149.1(6) . . . . ?
B2_12 B4_12 B10_12 Cl9_12 109.5(7) . . . . ?
B8_12 B4_12 B10_12 Cl9_12 -112.1(7) . . . . ?
B1_12 B4_12 B10_12 Cl9_12 146.2(6) . . . . ?
Cl4_12 B4_12 B10_12 Cl9_12 -1.9(10) . . . . ?
B6_12 B4_12 B10_12 B8_12 -37.1(6) . . . . ?
B2_12 B4_12 B10_12 B8_12 -138.5(6) . . . . ?
B1_12 B4_12 B10_12 B8_12 -101.7(7) . . . . ?
Cl4_12 B4_12 B10_12 B8_12 110.2(7) . . . . ?
B6_12 B4_12 B10_12 B12_12 1.1(8) . . . . ?
B2_12 B4_12 B10_12 B12_12 -100.3(7) . . . . ?
B8_12 B4_12 B10_12 B12_12 38.2(6) . . . . ?
B1_12 B4_12 B10_12 B12_12 -63.6(8) . . . . ?
Cl4_12 B4_12 B10_12 B12_12 148.3(6) . . . . ?
B6_12 B4_12 B10_12 B2_12 101.4(7) . . . . ?
B8_12 B4_12 B10_12 B2_12 138.5(6) . . . . ?
B1_12 B4_12 B10_12 B2_12 36.8(6) . . . . ?
Cl4_12 B4_12 B10_12 B2_12 -111.3(7) . . . . ?
B1_12 B2_12 B10_12 B11_12 100.3(7) . . . . ?
B3_12 B2_12 B10_12 B11_12 36.5(6) . . . . ?
B4_12 B2_12 B10_12 B11_12 138.4(7) . . . . ?
Cl2_12 B2_12 B10_12 B11_12 -111.6(8) . . . . ?
B1_12 B2_12 B10_12 Cl9_12 -148.7(6) . . . . ?
B3_12 B2_12 B10_12 Cl9_12 147.5(6) . . . . ?
B4_12 B2_12 B10_12 Cl9_12 -110.6(7) . . . . ?
B11_12 B2_12 B10_12 Cl9_12 111.0(7) . . . . ?
Cl2_12 B2_12 B10_12 Cl9_12 -0.6(10) . . . . ?
B1_12 B2_12 B10_12 B8_12 -1.5(8) . . . . ?
B3_12 B2_12 B10_12 B8_12 -65.4(8) . . . . ?
B4_12 B2_12 B10_12 B8_12 36.5(6) . . . . ?
B11_12 B2_12 B10_12 B8_12 -101.9(7) . . . . ?
Cl2_12 B2_12 B10_12 B8_12 146.5(6) . . . . ?
B1_12 B2_12 B10_12 B12_12 62.9(8) . . . . ?
B3_12 B2_12 B10_12 B12_12 -0.9(8) . . . . ?
B4_12 B2_12 B10_12 B12_12 101.0(7) . . . . ?
B11_12 B2_12 B10_12 B12_12 -37.5(6) . . . . ?
Cl2_12 B2_12 B10_12 B12_12 -149.1(6) . . . . ?
B1_12 B2_12 B10_12 B4_12 -38.1(6) . . . . ?
B3_12 B2_12 B10_12 B4_12 -101.9(7) . . . . ?
B11_12 B2_12 B10_12 B4_12 -138.4(7) . . . . ?
Cl2_12 B2_12 B10_12 B4_12 110.0(7) . . . . ?
B1_12 B3_12 B11_12 B10_12 0.9(9) . . . . ?
B5_12 B3_12 B11_12 B10_12 -63.2(8) . . . . ?
B2_12 B3_12 B11_12 B10_12 37.6(6) . . . . ?
Cl3_12 B3_12 B11_12 B10_12 147.9(6) . . . . ?
B9_12 B3_12 B11_12 B10_12 -101.3(7) . . . . ?
B1_12 B3_12 B11_12 B12_12 65.0(8) . . . . ?
B5_12 B3_12 B11_12 B12_12 0.9(9) . . . . ?
B2_12 B3_12 B11_12 B12_12 101.7(7) . . . . ?
Cl3_12 B3_12 B11_12 B12_12 -148.0(6) . . . . ?
B9_12 B3_12 B11_12 B12_12 -37.2(6) . . . . ?
B1_12 B3_12 B11_12 B9_12 102.2(7) . . . . ?
B5_12 B3_12 B11_12 B9_12 38.1(6) . . . . ?
B2_12 B3_12 B11_12 B9_12 138.9(6) . . . . ?
Cl3_12 B3_12 B11_12 B9_12 -110.8(7) . . . . ?
B1_12 B3_12 B11_12 B2_12 -36.7(6) . . . . ?
B5_12 B3_12 B11_12 B2_12 -100.9(7) . . . . ?
Cl3_12 B3_12 B11_12 B2_12 110.3(7) . . . . ?
B9_12 B3_12 B11_12 B2_12 -138.9(6) . . . . ?
B1_12 B3_12 B11_12 Cl10_12 -147.5(6) . . . . ?
B5_12 B3_12 B11_12 Cl10_12 148.3(6) . . . . ?
B2_12 B3_12 B11_12 Cl10_12 -110.8(8) . . . . ?
Cl3_12 B3_12 B11_12 Cl10_12 -0.5(11) . . . . ?
B9_12 B3_12 B11_12 Cl10_12 110.3(7) . . . . ?
Cl9_12 B10_12 B11_12 B3_12 -146.8(6) . . . . ?
B8_12 B10_12 B11_12 B3_12 62.1(8) . . . . ?
B12_12 B10_12 B11_12 B3_12 101.3(7) . . . . ?
B4_12 B10_12 B11_12 B3_12 -0.5(8) . . . . ?
B2_12 B10_12 B11_12 B3_12 -36.9(6) . . . . ?
Cl9_12 B10_12 B11_12 B12_12 111.9(7) . . . . ?
B8_12 B10_12 B11_12 B12_12 -39.2(6) . . . . ?
B4_12 B10_12 B11_12 B12_12 -101.8(7) . . . . ?
B2_12 B10_12 B11_12 B12_12 -138.2(7) . . . . ?
Cl9_12 B10_12 B11_12 B9_12 148.6(6) . . . . ?
B8_12 B10_12 B11_12 B9_12 -2.5(8) . . . . ?
B12_12 B10_12 B11_12 B9_12 36.7(6) . . . . ?
B4_12 B10_12 B11_12 B9_12 -65.1(8) . . . . ?
B2_12 B10_12 B11_12 B9_12 -101.5(7) . . . . ?
Cl9_12 B10_12 B11_12 B2_12 -109.9(7) . . . . ?
B8_12 B10_12 B11_12 B2_12 99.0(7) . . . . ?
B12_12 B10_12 B11_12 B2_12 138.2(7) . . . . ?
B4_12 B10_12 B11_12 B2_12 36.4(6) . . . . ?
Cl9_12 B10_12 B11_12 Cl10_12 2.7(10) . . . . ?
B8_12 B10_12 B11_12 Cl10_12 -148.5(6) . . . . ?
B12_12 B10_12 B11_12 Cl10_12 -109.3(7) . . . . ?
B4_12 B10_12 B11_12 Cl10_12 148.9(6) . . . . ?
B2_12 B10_12 B11_12 Cl10_12 112.5(7) . . . . ?
Cl11_12 B9_12 B11_12 B3_12 111.8(8) . . . . ?
B5_12 B9_12 B11_12 B3_12 -37.3(6) . . . . ?
B12_12 B9_12 B11_12 B3_12 -138.7(6) . . . . ?
B7_12 B9_12 B11_12 B3_12 -100.3(7) . . . . ?
Cl11_12 B9_12 B11_12 B10_12 -146.3(7) . . . . ?
B5_12 B9_12 B11_12 B10_12 64.6(8) . . . . ?
B12_12 B9_12 B11_12 B10_12 -36.8(6) . . . . ?
B3_12 B9_12 B11_12 B10_12 101.9(7) . . . . ?
B7_12 B9_12 B11_12 B10_12 1.6(8) . . . . ?
Cl11_12 B9_12 B11_12 B12_12 -109.5(8) . . . . ?
B5_12 B9_12 B11_12 B12_12 101.4(6) . . . . ?
B3_12 B9_12 B11_12 B12_12 138.7(6) . . . . ?
B7_12 B9_12 B11_12 B12_12 38.4(6) . . . . ?
Cl11_12 B9_12 B11_12 B2_12 148.5(7) . . . . ?
B5_12 B9_12 B11_12 B2_12 -0.5(8) . . . . ?
B12_12 B9_12 B11_12 B2_12 -101.9(7) . . . . ?
B3_12 B9_12 B11_12 B2_12 36.8(6) . . . . ?
B7_12 B9_12 B11_12 B2_12 -63.6(8) . . . . ?
Cl11_12 B9_12 B11_12 Cl10_12 -0.9(11) . . . . ?
B5_12 B9_12 B11_12 Cl10_12 -150.0(6) . . . . ?
B12_12 B9_12 B11_12 Cl10_12 108.6(7) . . . . ?
B3_12 B9_12 B11_12 Cl10_12 -112.7(8) . . . . ?
B7_12 B9_12 B11_12 Cl10_12 147.0(6) . . . . ?
B1_12 B2_12 B11_12 B3_12 37.6(6) . . . . ?
B4_12 B2_12 B11_12 B3_12 101.7(7) . . . . ?
Cl2_12 B2_12 B11_12 B3_12 -109.9(7) . . . . ?
B10_12 B2_12 B11_12 B3_12 138.9(6) . . . . ?
B1_12 B2_12 B11_12 B10_12 -101.3(7) . . . . ?
B3_12 B2_12 B11_12 B10_12 -138.9(6) . . . . ?
B4_12 B2_12 B11_12 B10_12 -37.1(6) . . . . ?
Cl2_12 B2_12 B11_12 B10_12 111.2(7) . . . . ?
B1_12 B2_12 B11_12 B12_12 -63.5(8) . . . . ?
B3_12 B2_12 B11_12 B12_12 -101.1(7) . . . . ?
B4_12 B2_12 B11_12 B12_12 0.6(9) . . . . ?
Cl2_12 B2_12 B11_12 B12_12 149.0(6) . . . . ?
B10_12 B2_12 B11_12 B12_12 37.8(6) . . . . ?
B1_12 B2_12 B11_12 B9_12 0.4(9) . . . . ?
B3_12 B2_12 B11_12 B9_12 -37.2(6) . . . . ?
B4_12 B2_12 B11_12 B9_12 64.5(8) . . . . ?
Cl2_12 B2_12 B11_12 B9_12 -147.1(6) . . . . ?
B10_12 B2_12 B11_12 B9_12 101.7(7) . . . . ?
B1_12 B2_12 B11_12 Cl10_12 149.5(6) . . . . ?
B3_12 B2_12 B11_12 Cl10_12 112.0(8) . . . . ?
B4_12 B2_12 B11_12 Cl10_12 -146.3(6) . . . . ?
Cl2_12 B2_12 B11_12 Cl10_12 2.1(11) . . . . ?
B10_12 B2_12 B11_12 Cl10_12 -109.1(8) . . . . ?
B8_12 B7_12 B12_12 Cl12_12 111.6(8) . . . . ?
B6_12 B7_12 B12_12 Cl12_12 148.6(7) . . . . ?
Cl7_12 B7_12 B12_12 Cl12_12 -1.3(11) . . . . ?
B5_12 B7_12 B12_12 Cl12_12 -147.5(7) . . . . ?
B9_12 B7_12 B12_12 Cl12_12 -110.6(8) . . . . ?
B8_12 B7_12 B12_12 B11_12 -99.0(6) . . . . ?
B6_12 B7_12 B12_12 B11_12 -62.0(8) . . . . ?
Cl7_12 B7_12 B12_12 B11_12 148.2(7) . . . . ?
B5_12 B7_12 B12_12 B11_12 1.9(8) . . . . ?
B9_12 B7_12 B12_12 B11_12 38.9(6) . . . . ?
B8_12 B7_12 B12_12 B10_12 -36.3(6) . . . . ?
B6_12 B7_12 B12_12 B10_12 0.7(9) . . . . ?
Cl7_12 B7_12 B12_12 B10_12 -149.2(6) . . . . ?
B5_12 B7_12 B12_12 B10_12 64.6(8) . . . . ?
B9_12 B7_12 B12_12 B10_12 101.5(7) . . . . ?
B8_12 B7_12 B12_12 B9_12 -137.9(6) . . . . ?
B6_12 B7_12 B12_12 B9_12 -100.8(7) . . . . ?
Cl7_12 B7_12 B12_12 B9_12 109.3(8) . . . . ?
B5_12 B7_12 B12_12 B9_12 -36.9(6) . . . . ?
B6_12 B7_12 B12_12 B8_12 37.0(6) . . . . ?
Cl7_12 B7_12 B12_12 B8_12 -112.8(8) . . . . ?
B5_12 B7_12 B12_12 B8_12 100.9(7) . . . . ?
B9_12 B7_12 B12_12 B8_12 137.9(6) . . . . ?
B3_12 B11_12 B12_12 Cl12_12 148.6(6) . . . . ?
B10_12 B11_12 B12_12 Cl12_12 -109.7(8) . . . . ?
B9_12 B11_12 B12_12 Cl12_12 111.1(7) . . . . ?
B2_12 B11_12 B12_12 Cl12_12 -147.9(6) . . . . ?
Cl10_12 B11_12 B12_12 Cl12_12 -0.1(11) . . . . ?
B3_12 B11_12 B12_12 B7_12 -1.7(8) . . . . ?
B10_12 B11_12 B12_12 B7_12 100.0(7) . . . . ?
B9_12 B11_12 B12_12 B7_12 -39.2(6) . . . . ?
B2_12 B11_12 B12_12 B7_12 61.8(8) . . . . ?
Cl10_12 B11_12 B12_12 B7_12 -150.4(6) . . . . ?
B3_12 B11_12 B12_12 B10_12 -101.8(7) . . . . ?
B9_12 B11_12 B12_12 B10_12 -139.2(6) . . . . ?
B2_12 B11_12 B12_12 B10_12 -38.3(6) . . . . ?
Cl10_12 B11_12 B12_12 B10_12 109.6(7) . . . . ?
B3_12 B11_12 B12_12 B9_12 37.4(6) . . . . ?
B10_12 B11_12 B12_12 B9_12 139.2(6) . . . . ?
B2_12 B11_12 B12_12 B9_12 101.0(7) . . . . ?
Cl10_12 B11_12 B12_12 B9_12 -111.2(7) . . . . ?
B3_12 B11_12 B12_12 B8_12 -63.9(8) . . . . ?
B10_12 B11_12 B12_12 B8_12 37.9(6) . . . . ?
B9_12 B11_12 B12_12 B8_12 -101.3(7) . . . . ?
B2_12 B11_12 B12_12 B8_12 -0.4(9) . . . . ?
Cl10_12 B11_12 B12_12 B8_12 147.5(6) . . . . ?
B11_12 B10_12 B12_12 Cl12_12 110.5(7) . . . . ?
Cl9_12 B10_12 B12_12 Cl12_12 -0.2(10) . . . . ?
B8_12 B10_12 B12_12 Cl12_12 -112.7(7) . . . . ?
B4_12 B10_12 B12_12 Cl12_12 -150.1(6) . . . . ?
B2_12 B10_12 B12_12 Cl12_12 147.7(6) . . . . ?
B11_12 B10_12 B12_12 B7_12 -100.5(7) . . . . ?
Cl9_12 B10_12 B12_12 B7_12 148.8(6) . . . . ?
B8_12 B10_12 B12_12 B7_12 36.3(6) . . . . ?
B4_12 B10_12 B12_12 B7_12 -1.1(8) . . . . ?
B2_12 B10_12 B12_12 B7_12 -63.3(8) . . . . ?
Cl9_12 B10_12 B12_12 B11_12 -110.6(8) . . . . ?
B8_12 B10_12 B12_12 B11_12 136.8(6) . . . . ?
B4_12 B10_12 B12_12 B11_12 99.4(7) . . . . ?
B2_12 B10_12 B12_12 B11_12 37.2(6) . . . . ?
B11_12 B10_12 B12_12 B9_12 -36.5(6) . . . . ?
Cl9_12 B10_12 B12_12 B9_12 -147.1(6) . . . . ?
B8_12 B10_12 B12_12 B9_12 100.3(7) . . . . ?
B4_12 B10_12 B12_12 B9_12 62.9(8) . . . . ?
B2_12 B10_12 B12_12 B9_12 0.7(8) . . . . ?
B11_12 B10_12 B12_12 B8_12 -136.8(6) . . . . ?
Cl9_12 B10_12 B12_12 B8_12 112.6(7) . . . . ?
B4_12 B10_12 B12_12 B8_12 -37.3(6) . . . . ?
B2_12 B10_12 B12_12 B8_12 -99.5(7) . . . . ?
Cl11_12 B9_12 B12_12 Cl12_12 3.8(11) . . . . ?
B5_12 B9_12 B12_12 Cl12_12 150.8(6) . . . . ?
B11_12 B9_12 B12_12 Cl12_12 -110.3(8) . . . . ?
B3_12 B9_12 B12_12 Cl12_12 -146.8(6) . . . . ?
B7_12 B9_12 B12_12 Cl12_12 113.5(8) . . . . ?
Cl11_12 B9_12 B12_12 B7_12 -109.7(7) . . . . ?
B5_12 B9_12 B12_12 B7_12 37.3(6) . . . . ?
B11_12 B9_12 B12_12 B7_12 136.3(6) . . . . ?
B3_12 B9_12 B12_12 B7_12 99.7(7) . . . . ?
Cl11_12 B9_12 B12_12 B11_12 114.0(7) . . . . ?
B5_12 B9_12 B12_12 B11_12 -99.0(7) . . . . ?
B3_12 B9_12 B12_12 B11_12 -36.6(6) . . . . ?
B7_12 B9_12 B12_12 B11_12 -136.3(6) . . . . ?
Cl11_12 B9_12 B12_12 B10_12 150.3(6) . . . . ?
B5_12 B9_12 B12_12 B10_12 -62.6(8) . . . . ?
B11_12 B9_12 B12_12 B10_12 36.3(6) . . . . ?
B3_12 B9_12 B12_12 B10_12 -0.2(8) . . . . ?
B7_12 B9_12 B12_12 B10_12 -99.9(7) . . . . ?
Cl11_12 B9_12 B12_12 B8_12 -147.0(6) . . . . ?
B5_12 B9_12 B12_12 B8_12 0.1(8) . . . . ?
B11_12 B9_12 B12_12 B8_12 99.0(6) . . . . ?
B3_12 B9_12 B12_12 B8_12 62.5(8) . . . . ?
B7_12 B9_12 B12_12 B8_12 -37.2(6) . . . . ?
B6_12 B8_12 B12_12 Cl12_12 -149.6(7) . . . . ?
B4_12 B8_12 B12_12 Cl12_12 146.7(6) . . . . ?
B7_12 B8_12 B12_12 Cl12_12 -112.3(8) . . . . ?
Cl8_12 B8_12 B12_12 Cl12_12 -1.3(11) . . . . ?
B10_12 B8_12 B12_12 Cl12_12 108.8(8) . . . . ?
B6_12 B8_12 B12_12 B7_12 -37.2(6) . . . . ?
B4_12 B8_12 B12_12 B7_12 -101.0(7) . . . . ?
Cl8_12 B8_12 B12_12 B7_12 111.1(7) . . . . ?
B10_12 B8_12 B12_12 B7_12 -138.9(6) . . . . ?
B6_12 B8_12 B12_12 B11_12 63.7(8) . . . . ?
B4_12 B8_12 B12_12 B11_12 0.0(8) . . . . ?
B7_12 B8_12 B12_12 B11_12 100.9(7) . . . . ?
Cl8_12 B8_12 B12_12 B11_12 -148.0(6) . . . . ?
B10_12 B8_12 B12_12 B11_12 -38.0(6) . . . . ?
B6_12 B8_12 B12_12 B10_12 101.6(7) . . . . ?
B4_12 B8_12 B12_12 B10_12 37.9(6) . . . . ?
B7_12 B8_12 B12_12 B10_12 138.9(6) . . . . ?
Cl8_12 B8_12 B12_12 B10_12 -110.1(7) . . . . ?
B6_12 B8_12 B12_12 B9_12 0.6(9) . . . . ?
B4_12 B8_12 B12_12 B9_12 -63.1(8) . . . . ?
B7_12 B8_12 B12_12 B9_12 37.9(6) . . . . ?
Cl8_12 B8_12 B12_12 B9_12 148.9(6) . . . . ?
B10_12 B8_12 B12_12 B9_12 -101.0(7) . . . . ?
B4_13 B1_13 B2_13 B3_13 -38.5(5) . . . . ?
B5_13 B1_13 B2_13 B3_13 -101.9(6) . . . . ?
Cl1_13 B1_13 B2_13 B3_13 112.0(6) . . . . ?
B6_13 B1_13 B2_13 B3_13 -139.2(6) . . . . ?
B3_13 B1_13 B2_13 B6_13 139.2(6) . . . . ?
B4_13 B1_13 B2_13 B6_13 100.7(6) . . . . ?
B5_13 B1_13 B2_13 B6_13 37.3(5) . . . . ?
Cl1_13 B1_13 B2_13 B6_13 -108.8(6) . . . . ?
B3_13 B1_13 B2_13 B12_13 101.7(6) . . . . ?
B4_13 B1_13 B2_13 B12_13 63.3(7) . . . . ?
B5_13 B1_13 B2_13 B12_13 -0.2(8) . . . . ?
Cl1_13 B1_13 B2_13 B12_13 -146.3(5) . . . . ?
B6_13 B1_13 B2_13 B12_13 -37.5(5) . . . . ?
B3_13 B1_13 B2_13 B11_13 37.0(5) . . . . ?
B4_13 B1_13 B2_13 B11_13 -1.5(7) . . . . ?
B5_13 B1_13 B2_13 B11_13 -64.9(7) . . . . ?
Cl1_13 B1_13 B2_13 B11_13 149.0(5) . . . . ?
B6_13 B1_13 B2_13 B11_13 -102.2(6) . . . . ?
B3_13 B1_13 B2_13 Cl6_13 -110.1(7) . . . . ?
B4_13 B1_13 B2_13 Cl6_13 -148.6(5) . . . . ?
B5_13 B1_13 B2_13 Cl6_13 148.0(6) . . . . ?
Cl1_13 B1_13 B2_13 Cl6_13 1.8(9) . . . . ?
B6_13 B1_13 B2_13 Cl6_13 110.7(7) . . . . ?
B6_13 B2_13 B3_13 B1_13 -37.6(5) . . . . ?
B12_13 B2_13 B3_13 B1_13 -101.9(6) . . . . ?
B11_13 B2_13 B3_13 B1_13 -139.0(6) . . . . ?
Cl6_13 B2_13 B3_13 B1_13 110.6(6) . . . . ?
B6_13 B2_13 B3_13 B11_13 101.4(6) . . . . ?
B1_13 B2_13 B3_13 B11_13 139.0(6) . . . . ?
B12_13 B2_13 B3_13 B11_13 37.0(5) . . . . ?
Cl6_13 B2_13 B3_13 B11_13 -110.4(6) . . . . ?
B6_13 B2_13 B3_13 Cl5_13 -146.4(5) . . . . ?
B1_13 B2_13 B3_13 Cl5_13 -108.8(6) . . . . ?
B12_13 B2_13 B3_13 Cl5_13 149.2(5) . . . . ?
B11_13 B2_13 B3_13 Cl5_13 112.2(6) . . . . ?
Cl6_13 B2_13 B3_13 Cl5_13 1.8(9) . . . . ?
B6_13 B2_13 B3_13 B4_13 0.4(7) . . . . ?
B1_13 B2_13 B3_13 B4_13 38.0(5) . . . . ?
B12_13 B2_13 B3_13 B4_13 -64.0(7) . . . . ?
B11_13 B2_13 B3_13 B4_13 -101.0(6) . . . . ?
Cl6_13 B2_13 B3_13 B4_13 148.6(5) . . . . ?
B6_13 B2_13 B3_13 B10_13 63.1(7) . . . . ?
B1_13 B2_13 B3_13 B10_13 100.7(6) . . . . ?
B12_13 B2_13 B3_13 B10_13 -1.2(7) . . . . ?
B11_13 B2_13 B3_13 B10_13 -38.2(5) . . . . ?
Cl6_13 B2_13 B3_13 B10_13 -148.7(5) . . . . ?
B4_13 B1_13 B3_13 B2_13 137.4(6) . . . . ?
B5_13 B1_13 B3_13 B2_13 99.9(6) . . . . ?
Cl1_13 B1_13 B3_13 B2_13 -107.5(7) . . . . ?
B6_13 B1_13 B3_13 B2_13 35.8(5) . . . . ?
B2_13 B1_13 B3_13 B11_13 -37.7(6) . . . . ?
B4_13 B1_13 B3_13 B11_13 99.7(6) . . . . ?
B5_13 B1_13 B3_13 B11_13 62.2(7) . . . . ?
Cl1_13 B1_13 B3_13 B11_13 -145.2(6) . . . . ?
B6_13 B1_13 B3_13 B11_13 -1.9(8) . . . . ?
B2_13 B1_13 B3_13 Cl5_13 111.2(7) . . . . ?
B4_13 B1_13 B3_13 Cl5_13 -111.4(6) . . . . ?
B5_13 B1_13 B3_13 Cl5_13 -148.9(5) . . . . ?
Cl1_13 B1_13 B3_13 Cl5_13 3.7(9) . . . . ?
B6_13 B1_13 B3_13 Cl5_13 147.0(5) . . . . ?
B2_13 B1_13 B3_13 B4_13 -137.4(6) . . . . ?
B5_13 B1_13 B3_13 B4_13 -37.5(5) . . . . ?
Cl1_13 B1_13 B3_13 B4_13 115.1(7) . . . . ?
B6_13 B1_13 B3_13 B4_13 -101.6(6) . . . . ?
B2_13 B1_13 B3_13 B10_13 -101.2(6) . . . . ?
B4_13 B1_13 B3_13 B10_13 36.2(5) . . . . ?
B5_13 B1_13 B3_13 B10_13 -1.3(7) . . . . ?
Cl1_13 B1_13 B3_13 B10_13 151.3(5) . . . . ?
B6_13 B1_13 B3_13 B10_13 -65.4(7) . . . . ?
B3_13 B1_13 B4_13 B8_13 -100.2(6) . . . . ?
B2_13 B1_13 B4_13 B8_13 -62.5(7) . . . . ?
B5_13 B1_13 B4_13 B8_13 38.2(5) . . . . ?
Cl1_13 B1_13 B4_13 B8_13 149.2(6) . . . . ?
B6_13 B1_13 B4_13 B8_13 -0.3(7) . . . . ?
B3_13 B1_13 B4_13 B10_13 -36.7(5) . . . . ?
B2_13 B1_13 B4_13 B10_13 1.0(7) . . . . ?
B5_13 B1_13 B4_13 B10_13 101.6(6) . . . . ?
Cl1_13 B1_13 B4_13 B10_13 -147.4(6) . . . . ?
B6_13 B1_13 B4_13 B10_13 63.2(7) . . . . ?
B3_13 B1_13 B4_13 B5_13 -138.3(6) . . . . ?
B2_13 B1_13 B4_13 B5_13 -100.6(6) . . . . ?
Cl1_13 B1_13 B4_13 B5_13 111.0(7) . . . . ?
B6_13 B1_13 B4_13 B5_13 -38.4(5) . . . . ?
B3_13 B1_13 B4_13 Cl4_13 110.8(6) . . . . ?
B2_13 B1_13 B4_13 Cl4_13 148.5(6) . . . . ?
B5_13 B1_13 B4_13 Cl4_13 -110.9(6) . . . . ?
Cl1_13 B1_13 B4_13 Cl4_13 0.1(10) . . . . ?
B6_13 B1_13 B4_13 Cl4_13 -149.3(5) . . . . ?
B2_13 B1_13 B4_13 B3_13 37.7(5) . . . . ?
B5_13 B1_13 B4_13 B3_13 138.3(6) . . . . ?
Cl1_13 B1_13 B4_13 B3_13 -110.7(7) . . . . ?
B6_13 B1_13 B4_13 B3_13 99.9(6) . . . . ?
B2_13 B3_13 B4_13 B1_13 -38.3(5) . . . . ?
B11_13 B3_13 B4_13 B1_13 -103.0(6) . . . . ?
Cl5_13 B3_13 B4_13 B1_13 108.3(6) . . . . ?
B10_13 B3_13 B4_13 B1_13 -139.2(6) . . . . ?
B2_13 B3_13 B4_13 B8_13 63.3(7) . . . . ?
B1_13 B3_13 B4_13 B8_13 101.6(6) . . . . ?
B11_13 B3_13 B4_13 B8_13 -1.4(7) . . . . ?
Cl5_13 B3_13 B4_13 B8_13 -150.1(5) . . . . ?
B10_13 B3_13 B4_13 B8_13 -37.6(5) . . . . ?
B2_13 B3_13 B4_13 B10_13 100.9(6) . . . . ?
B1_13 B3_13 B4_13 B10_13 139.2(6) . . . . ?
B11_13 B3_13 B4_13 B10_13 36.2(5) . . . . ?
Cl5_13 B3_13 B4_13 B10_13 -112.5(6) . . . . ?
B2_13 B3_13 B4_13 B5_13 -1.1(7) . . . . ?
B1_13 B3_13 B4_13 B5_13 37.2(5) . . . . ?
B11_13 B3_13 B4_13 B5_13 -65.8(7) . . . . ?
Cl5_13 B3_13 B4_13 B5_13 145.5(5) . . . . ?
B10_13 B3_13 B4_13 B5_13 -102.0(6) . . . . ?
B2_13 B3_13 B4_13 Cl4_13 -149.1(5) . . . . ?
B1_13 B3_13 B4_13 Cl4_13 -110.8(6) . . . . ?
B11_13 B3_13 B4_13 Cl4_13 146.2(5) . . . . ?
Cl5_13 B3_13 B4_13 Cl4_13 -2.5(8) . . . . ?
B10_13 B3_13 B4_13 Cl4_13 110.0(6) . . . . ?
B1_13 B4_13 B5_13 Cl3_13 -110.5(7) . . . . ?
B8_13 B4_13 B5_13 Cl3_13 111.5(7) . . . . ?
B10_13 B4_13 B5_13 Cl3_13 148.9(6) . . . . ?
Cl4_13 B4_13 B5_13 Cl3_13 0.9(9) . . . . ?
B3_13 B4_13 B5_13 Cl3_13 -147.2(6) . . . . ?
B8_13 B4_13 B5_13 B1_13 -138.0(6) . . . . ?
B10_13 B4_13 B5_13 B1_13 -100.6(6) . . . . ?
Cl4_13 B4_13 B5_13 B1_13 111.4(6) . . . . ?
B3_13 B4_13 B5_13 B1_13 -36.7(5) . . . . ?
B1_13 B4_13 B5_13 B8_13 138.0(6) . . . . ?
B10_13 B4_13 B5_13 B8_13 37.4(5) . . . . ?
Cl4_13 B4_13 B5_13 B8_13 -110.6(6) . . . . ?
B3_13 B4_13 B5_13 B8_13 101.3(6) . . . . ?
B1_13 B4_13 B5_13 B6_13 38.1(5) . . . . ?
B8_13 B4_13 B5_13 B6_13 -99.9(6) . . . . ?
B10_13 B4_13 B5_13 B6_13 -62.5(7) . . . . ?
Cl4_13 B4_13 B5_13 B6_13 149.5(5) . . . . ?
B3_13 B4_13 B5_13 B6_13 1.4(7) . . . . ?
B1_13 B4_13 B5_13 B7_13 100.8(6) . . . . ?
B8_13 B4_13 B5_13 B7_13 -37.2(5) . . . . ?
B10_13 B4_13 B5_13 B7_13 0.2(7) . . . . ?
Cl4_13 B4_13 B5_13 B7_13 -147.8(5) . . . . ?
B3_13 B4_13 B5_13 B7_13 64.1(7) . . . . ?
B3_13 B1_13 B5_13 Cl3_13 149.6(5) . . . . ?
B2_13 B1_13 B5_13 Cl3_13 -147.5(5) . . . . ?
B4_13 B1_13 B5_13 Cl3_13 111.7(6) . . . . ?
Cl1_13 B1_13 B5_13 Cl3_13 -2.8(9) . . . . ?
B6_13 B1_13 B5_13 Cl3_13 -111.0(6) . . . . ?
B3_13 B1_13 B5_13 B4_13 38.0(5) . . . . ?
B2_13 B1_13 B5_13 B4_13 100.8(6) . . . . ?
Cl1_13 B1_13 B5_13 B4_13 -114.5(7) . . . . ?
B6_13 B1_13 B5_13 B4_13 137.3(6) . . . . ?
B3_13 B1_13 B5_13 B8_13 0.9(7) . . . . ?
B2_13 B1_13 B5_13 B8_13 63.7(7) . . . . ?
B4_13 B1_13 B5_13 B8_13 -37.1(5) . . . . ?
Cl1_13 B1_13 B5_13 B8_13 -151.5(5) . . . . ?
B6_13 B1_13 B5_13 B8_13 100.2(6) . . . . ?
B3_13 B1_13 B5_13 B6_13 -99.4(6) . . . . ?
B2_13 B1_13 B5_13 B6_13 -36.5(5) . . . . ?
B4_13 B1_13 B5_13 B6_13 -137.3(6) . . . . ?
Cl1_13 B1_13 B5_13 B6_13 108.2(6) . . . . ?
B3_13 B1_13 B5_13 B7_13 -61.8(7) . . . . ?
B2_13 B1_13 B5_13 B7_13 1.0(7) . . . . ?
B4_13 B1_13 B5_13 B7_13 -99.8(6) . . . . ?
Cl1_13 B1_13 B5_13 B7_13 145.8(6) . . . . ?
B6_13 B1_13 B5_13 B7_13 37.5(5) . . . . ?
B3_13 B2_13 B6_13 B12_13 -101.7(6) . . . . ?
B1_13 B2_13 B6_13 B12_13 -138.7(6) . . . . ?
B11_13 B2_13 B6_13 B12_13 -37.4(5) . . . . ?
Cl6_13 B2_13 B6_13 B12_13 110.1(6) . . . . ?
B3_13 B2_13 B6_13 Cl2_13 147.4(6) . . . . ?
B1_13 B2_13 B6_13 Cl2_13 110.4(7) . . . . ?
B12_13 B2_13 B6_13 Cl2_13 -110.9(7) . . . . ?
B11_13 B2_13 B6_13 Cl2_13 -148.3(5) . . . . ?
Cl6_13 B2_13 B6_13 Cl2_13 -0.8(9) . . . . ?
B3_13 B2_13 B6_13 B7_13 -63.1(7) . . . . ?
B1_13 B2_13 B6_13 B7_13 -100.0(6) . . . . ?
B12_13 B2_13 B6_13 B7_13 38.6(5) . . . . ?
B11_13 B2_13 B6_13 B7_13 1.3(8) . . . . ?
Cl6_13 B2_13 B6_13 B7_13 148.7(5) . . . . ?
B3_13 B2_13 B6_13 B1_13 37.0(5) . . . . ?
B12_13 B2_13 B6_13 B1_13 138.7(6) . . . . ?
B11_13 B2_13 B6_13 B1_13 101.3(6) . . . . ?
Cl6_13 B2_13 B6_13 B1_13 -111.3(6) . . . . ?
B3_13 B2_13 B6_13 B5_13 0.5(8) . . . . ?
B1_13 B2_13 B6_13 B5_13 -36.5(5) . . . . ?
B12_13 B2_13 B6_13 B5_13 102.2(6) . . . . ?
B11_13 B2_13 B6_13 B5_13 64.8(7) . . . . ?
Cl6_13 B2_13 B6_13 B5_13 -147.8(5) . . . . ?
B3_13 B1_13 B6_13 B2_13 -36.0(5) . . . . ?
B4_13 B1_13 B6_13 B2_13 -100.4(6) . . . . ?
B5_13 B1_13 B6_13 B2_13 -138.6(6) . . . . ?
Cl1_13 B1_13 B6_13 B2_13 108.3(7) . . . . ?
B3_13 B1_13 B6_13 B12_13 1.3(8) . . . . ?
B2_13 B1_13 B6_13 B12_13 37.3(5) . . . . ?
B4_13 B1_13 B6_13 B12_13 -63.1(7) . . . . ?
B5_13 B1_13 B6_13 B12_13 -101.3(6) . . . . ?
Cl1_13 B1_13 B6_13 B12_13 145.6(6) . . . . ?
B3_13 B1_13 B6_13 Cl2_13 -148.3(6) . . . . ?
B2_13 B1_13 B6_13 Cl2_13 -112.3(7) . . . . ?
B4_13 B1_13 B6_13 Cl2_13 147.3(5) . . . . ?
B5_13 B1_13 B6_13 Cl2_13 109.1(6) . . . . ?
Cl1_13 B1_13 B6_13 Cl2_13 -4.0(9) . . . . ?
B3_13 B1_13 B6_13 B7_13 64.8(7) . . . . ?
B2_13 B1_13 B6_13 B7_13 100.8(6) . . . . ?
B4_13 B1_13 B6_13 B7_13 0.4(7) . . . . ?
B5_13 B1_13 B6_13 B7_13 -37.8(5) . . . . ?
Cl1_13 B1_13 B6_13 B7_13 -150.9(6) . . . . ?
B3_13 B1_13 B6_13 B5_13 102.6(6) . . . . ?
B2_13 B1_13 B6_13 B5_13 138.6(6) . . . . ?
B4_13 B1_13 B6_13 B5_13 38.2(5) . . . . ?
Cl1_13 B1_13 B6_13 B5_13 -113.1(7) . . . . ?
Cl3_13 B5_13 B6_13 B2_13 147.7(6) . . . . ?
B4_13 B5_13 B6_13 B2_13 -1.1(7) . . . . ?
B1_13 B5_13 B6_13 B2_13 36.8(5) . . . . ?
B8_13 B5_13 B6_13 B2_13 -63.7(7) . . . . ?
B7_13 B5_13 B6_13 B2_13 -100.9(6) . . . . ?
Cl3_13 B5_13 B6_13 B12_13 -148.3(6) . . . . ?
B4_13 B5_13 B6_13 B12_13 62.8(7) . . . . ?
B1_13 B5_13 B6_13 B12_13 100.7(6) . . . . ?
B8_13 B5_13 B6_13 B12_13 0.3(7) . . . . ?
B7_13 B5_13 B6_13 B12_13 -36.9(5) . . . . ?
Cl3_13 B5_13 B6_13 Cl2_13 -0.2(9) . . . . ?
B4_13 B5_13 B6_13 Cl2_13 -149.0(5) . . . . ?
B1_13 B5_13 B6_13 Cl2_13 -111.1(6) . . . . ?
B8_13 B5_13 B6_13 Cl2_13 148.5(5) . . . . ?
B7_13 B5_13 B6_13 Cl2_13 111.2(6) . . . . ?
Cl3_13 B5_13 B6_13 B7_13 -111.4(7) . . . . ?
B4_13 B5_13 B6_13 B7_13 99.8(6) . . . . ?
B1_13 B5_13 B6_13 B7_13 137.7(6) . . . . ?
B8_13 B5_13 B6_13 B7_13 37.3(5) . . . . ?
Cl3_13 B5_13 B6_13 B1_13 111.0(7) . . . . ?
B4_13 B5_13 B6_13 B1_13 -37.9(5) . . . . ?
B8_13 B5_13 B6_13 B1_13 -100.4(6) . . . . ?
B7_13 B5_13 B6_13 B1_13 -137.7(6) . . . . ?
B2_13 B6_13 B7_13 Cl12_13 -149.9(6) . . . . ?
B12_13 B6_13 B7_13 Cl12_13 -111.1(7) . . . . ?
Cl2_13 B6_13 B7_13 Cl12_13 0.1(9) . . . . ?
B1_13 B6_13 B7_13 Cl12_13 147.1(6) . . . . ?
B5_13 B6_13 B7_13 Cl12_13 109.9(7) . . . . ?
B2_13 B6_13 B7_13 B9_13 -0.9(8) . . . . ?
B12_13 B6_13 B7_13 B9_13 37.9(5) . . . . ?
Cl2_13 B6_13 B7_13 B9_13 149.2(5) . . . . ?
B1_13 B6_13 B7_13 B9_13 -63.8(7) . . . . ?
B5_13 B6_13 B7_13 B9_13 -101.1(6) . . . . ?
B2_13 B6_13 B7_13 B12_13 -38.8(5) . . . . ?
Cl2_13 B6_13 B7_13 B12_13 111.3(6) . . . . ?
B1_13 B6_13 B7_13 B12_13 -101.7(6) . . . . ?
B5_13 B6_13 B7_13 B12_13 -139.0(6) . . . . ?
B2_13 B6_13 B7_13 B8_13 62.5(7) . . . . ?
B12_13 B6_13 B7_13 B8_13 101.3(6) . . . . ?
Cl2_13 B6_13 B7_13 B8_13 -147.4(5) . . . . ?
B1_13 B6_13 B7_13 B8_13 -0.4(7) . . . . ?
B5_13 B6_13 B7_13 B8_13 -37.7(5) . . . . ?
B2_13 B6_13 B7_13 B5_13 100.2(6) . . . . ?
B12_13 B6_13 B7_13 B5_13 139.0(6) . . . . ?
Cl2_13 B6_13 B7_13 B5_13 -109.7(6) . . . . ?
B1_13 B6_13 B7_13 B5_13 37.3(5) . . . . ?
Cl3_13 B5_13 B7_13 Cl12_13 -1.2(9) . . . . ?
B4_13 B5_13 B7_13 Cl12_13 147.7(5) . . . . ?
B1_13 B5_13 B7_13 Cl12_13 -149.5(5) . . . . ?
B8_13 B5_13 B7_13 Cl12_13 110.5(7) . . . . ?
B6_13 B5_13 B7_13 Cl12_13 -111.7(6) . . . . ?
Cl3_13 B5_13 B7_13 B9_13 -148.6(6) . . . . ?
B4_13 B5_13 B7_13 B9_13 0.2(7) . . . . ?
B1_13 B5_13 B7_13 B9_13 63.1(7) . . . . ?
B8_13 B5_13 B7_13 B9_13 -37.0(5) . . . . ?
B6_13 B5_13 B7_13 B9_13 100.8(6) . . . . ?
Cl3_13 B5_13 B7_13 B12_13 146.8(5) . . . . ?
B4_13 B5_13 B7_13 B12_13 -64.4(7) . . . . ?
B1_13 B5_13 B7_13 B12_13 -1.5(7) . . . . ?
B8_13 B5_13 B7_13 B12_13 -101.5(6) . . . . ?
B6_13 B5_13 B7_13 B12_13 36.3(5) . . . . ?
Cl3_13 B5_13 B7_13 B8_13 -111.7(7) . . . . ?
B4_13 B5_13 B7_13 B8_13 37.2(5) . . . . ?
B1_13 B5_13 B7_13 B8_13 100.0(6) . . . . ?
B6_13 B5_13 B7_13 B8_13 137.8(6) . . . . ?
Cl3_13 B5_13 B7_13 B6_13 110.5(6) . . . . ?
B4_13 B5_13 B7_13 B6_13 -100.7(6) . . . . ?
B1_13 B5_13 B7_13 B6_13 -37.8(5) . . . . ?
B8_13 B5_13 B7_13 B6_13 -137.8(6) . . . . ?
B1_13 B4_13 B8_13 B10_13 100.5(6) . . . . ?
B5_13 B4_13 B8_13 B10_13 138.3(6) . . . . ?
Cl4_13 B4_13 B8_13 B10_13 -110.1(6) . . . . ?
B3_13 B4_13 B8_13 B10_13 37.9(5) . . . . ?
B1_13 B4_13 B8_13 Cl11_13 -149.7(6) . . . . ?
B10_13 B4_13 B8_13 Cl11_13 109.8(7) . . . . ?
B5_13 B4_13 B8_13 Cl11_13 -111.8(6) . . . . ?
Cl4_13 B4_13 B8_13 Cl11_13 -0.3(9) . . . . ?
B3_13 B4_13 B8_13 Cl11_13 147.7(5) . . . . ?
B1_13 B4_13 B8_13 B9_13 63.1(7) . . . . ?
B10_13 B4_13 B8_13 B9_13 -37.4(5) . . . . ?
B5_13 B4_13 B8_13 B9_13 100.9(6) . . . . ?
Cl4_13 B4_13 B8_13 B9_13 -147.5(5) . . . . ?
B3_13 B4_13 B8_13 B9_13 0.5(7) . . . . ?
B1_13 B4_13 B8_13 B7_13 0.0(7) . . . . ?
B10_13 B4_13 B8_13 B7_13 -100.5(6) . . . . ?
B5_13 B4_13 B8_13 B7_13 37.9(5) . . . . ?
Cl4_13 B4_13 B8_13 B7_13 149.4(5) . . . . ?
B3_13 B4_13 B8_13 B7_13 -62.6(7) . . . . ?
B1_13 B4_13 B8_13 B5_13 -37.8(5) . . . . ?
B10_13 B4_13 B8_13 B5_13 -138.3(6) . . . . ?
Cl4_13 B4_13 B8_13 B5_13 111.6(6) . . . . ?
B3_13 B4_13 B8_13 B5_13 -100.4(6) . . . . ?
Cl12_13 B7_13 B8_13 B10_13 148.9(6) . . . . ?
B9_13 B7_13 B8_13 B10_13 37.8(5) . . . . ?
B12_13 B7_13 B8_13 B10_13 -0.6(7) . . . . ?
B6_13 B7_13 B8_13 B10_13 -63.2(7) . . . . ?
B5_13 B7_13 B8_13 B10_13 -101.0(6) . . . . ?
Cl12_13 B7_13 B8_13 B4_13 -147.7(6) . . . . ?
B9_13 B7_13 B8_13 B4_13 101.2(6) . . . . ?
B12_13 B7_13 B8_13 B4_13 62.9(7) . . . . ?
B6_13 B7_13 B8_13 B4_13 0.2(7) . . . . ?
B5_13 B7_13 B8_13 B4_13 -37.5(5) . . . . ?
Cl12_13 B7_13 B8_13 Cl11_13 2.2(9) . . . . ?
B9_13 B7_13 B8_13 Cl11_13 -108.9(6) . . . . ?
B12_13 B7_13 B8_13 Cl11_13 -147.3(5) . . . . ?
B6_13 B7_13 B8_13 Cl11_13 150.1(5) . . . . ?
B5_13 B7_13 B8_13 Cl11_13 112.4(6) . . . . ?
Cl12_13 B7_13 B8_13 B9_13 111.1(7) . . . . ?
B12_13 B7_13 B8_13 B9_13 -38.4(5) . . . . ?
B6_13 B7_13 B8_13 B9_13 -101.0(6) . . . . ?
B5_13 B7_13 B8_13 B9_13 -138.7(6) . . . . ?
Cl12_13 B7_13 B8_13 B5_13 -110.2(7) . . . . ?
B9_13 B7_13 B8_13 B5_13 138.7(6) . . . . ?
B12_13 B7_13 B8_13 B5_13 100.3(6) . . . . ?
B6_13 B7_13 B8_13 B5_13 37.7(5) . . . . ?
Cl3_13 B5_13 B8_13 B10_13 -148.5(5) . . . . ?
B4_13 B5_13 B8_13 B10_13 -37.3(5) . . . . ?
B1_13 B5_13 B8_13 B10_13 0.0(7) . . . . ?
B6_13 B5_13 B8_13 B10_13 63.3(7) . . . . ?
B7_13 B5_13 B8_13 B10_13 100.5(6) . . . . ?
Cl3_13 B5_13 B8_13 B4_13 -111.2(7) . . . . ?
B1_13 B5_13 B8_13 B4_13 37.2(5) . . . . ?
B6_13 B5_13 B8_13 B4_13 100.6(6) . . . . ?
B7_13 B5_13 B8_13 B4_13 137.8(6) . . . . ?
Cl3_13 B5_13 B8_13 Cl11_13 0.0(9) . . . . ?
B4_13 B5_13 B8_13 Cl11_13 111.2(6) . . . . ?
B1_13 B5_13 B8_13 Cl11_13 148.4(5) . . . . ?
B6_13 B5_13 B8_13 Cl11_13 -148.3(5) . . . . ?
B7_13 B5_13 B8_13 Cl11_13 -111.0(7) . . . . ?
Cl3_13 B5_13 B8_13 B9_13 147.8(5) . . . . ?
B4_13 B5_13 B8_13 B9_13 -101.0(6) . . . . ?
B1_13 B5_13 B8_13 B9_13 -63.8(7) . . . . ?
B6_13 B5_13 B8_13 B9_13 -0.5(7) . . . . ?
B7_13 B5_13 B8_13 B9_13 36.8(5) . . . . ?
Cl3_13 B5_13 B8_13 B7_13 111.0(7) . . . . ?
B4_13 B5_13 B8_13 B7_13 -137.8(6) . . . . ?
B1_13 B5_13 B8_13 B7_13 -100.6(6) . . . . ?
B6_13 B5_13 B8_13 B7_13 -37.3(5) . . . . ?
Cl12_13 B7_13 B9_13 Cl10_13 0.8(9) . . . . ?
B12_13 B7_13 B9_13 Cl10_13 -111.3(6) . . . . ?
B8_13 B7_13 B9_13 Cl10_13 111.0(6) . . . . ?
B6_13 B7_13 B9_13 Cl10_13 -148.3(5) . . . . ?
B5_13 B7_13 B9_13 Cl10_13 148.0(5) . . . . ?
Cl12_13 B7_13 B9_13 B10_13 -147.6(6) . . . . ?
B12_13 B7_13 B9_13 B10_13 100.3(6) . . . . ?
B8_13 B7_13 B9_13 B10_13 -37.4(5) . . . . ?
B6_13 B7_13 B9_13 B10_13 63.2(7) . . . . ?
B5_13 B7_13 B9_13 B10_13 -0.4(7) . . . . ?
Cl12_13 B7_13 B9_13 B8_13 -110.2(7) . . . . ?
B12_13 B7_13 B9_13 B8_13 137.7(6) . . . . ?
B6_13 B7_13 B9_13 B8_13 100.7(6) . . . . ?
B5_13 B7_13 B9_13 B8_13 37.0(5) . . . . ?
Cl12_13 B7_13 B9_13 B11_13 149.3(6) . . . . ?
B12_13 B7_13 B9_13 B11_13 37.3(5) . . . . ?
B8_13 B7_13 B9_13 B11_13 -100.5(6) . . . . ?
B6_13 B7_13 B9_13 B11_13 0.2(7) . . . . ?
B5_13 B7_13 B9_13 B11_13 -63.5(7) . . . . ?
Cl12_13 B7_13 B9_13 B12_13 112.1(7) . . . . ?
B8_13 B7_13 B9_13 B12_13 -137.7(6) . . . . ?
B6_13 B7_13 B9_13 B12_13 -37.1(5) . . . . ?
B5_13 B7_13 B9_13 B12_13 -100.7(6) . . . . ?
B10_13 B8_13 B9_13 B7_13 -137.8(6) . . . . ?
B4_13 B8_13 B9_13 B7_13 -100.4(6) . . . . ?
Cl11_13 B8_13 B9_13 B7_13 111.6(6) . . . . ?
B5_13 B8_13 B9_13 B7_13 -37.2(5) . . . . ?
B10_13 B8_13 B9_13 Cl10_13 110.8(6) . . . . ?
B4_13 B8_13 B9_13 Cl10_13 148.2(5) . . . . ?
Cl11_13 B8_13 B9_13 Cl10_13 0.2(9) . . . . ?
B7_13 B8_13 B9_13 Cl10_13 -111.4(7) . . . . ?
B5_13 B8_13 B9_13 Cl10_13 -148.6(5) . . . . ?
B4_13 B8_13 B9_13 B10_13 37.4(5) . . . . ?
Cl11_13 B8_13 B9_13 B10_13 -110.7(6) . . . . ?
B7_13 B8_13 B9_13 B10_13 137.8(6) . . . . ?
B5_13 B8_13 B9_13 B10_13 100.6(6) . . . . ?
B10_13 B8_13 B9_13 B11_13 -36.7(5) . . . . ?
B4_13 B8_13 B9_13 B11_13 0.6(7) . . . . ?
Cl11_13 B8_13 B9_13 B11_13 -147.4(5) . . . . ?
B7_13 B8_13 B9_13 B11_13 101.0(6) . . . . ?
B5_13 B8_13 B9_13 B11_13 63.8(7) . . . . ?
B10_13 B8_13 B9_13 B12_13 -100.1(6) . . . . ?
B4_13 B8_13 B9_13 B12_13 -62.8(7) . . . . ?
Cl11_13 B8_13 B9_13 B12_13 149.2(5) . . . . ?
B7_13 B8_13 B9_13 B12_13 37.6(5) . . . . ?
B5_13 B8_13 B9_13 B12_13 0.4(7) . . . . ?
Cl11_13 B8_13 B10_13 B4_13 -112.0(6) . . . . ?
B9_13 B8_13 B10_13 B4_13 138.4(6) . . . . ?
B7_13 B8_13 B10_13 B4_13 100.9(6) . . . . ?
B5_13 B8_13 B10_13 B4_13 37.1(5) . . . . ?
B4_13 B8_13 B10_13 B11_13 -101.0(6) . . . . ?
Cl11_13 B8_13 B10_13 B11_13 146.9(5) . . . . ?
B9_13 B8_13 B10_13 B11_13 37.3(5) . . . . ?
B7_13 B8_13 B10_13 B11_13 -0.1(7) . . . . ?
B5_13 B8_13 B10_13 B11_13 -64.0(7) . . . . ?
B4_13 B8_13 B10_13 B9_13 -138.4(6) . . . . ?
Cl11_13 B8_13 B10_13 B9_13 109.6(6) . . . . ?
B7_13 B8_13 B10_13 B9_13 -37.5(5) . . . . ?
B5_13 B8_13 B10_13 B9_13 -101.3(6) . . . . ?
B4_13 B8_13 B10_13 B3_13 -37.8(5) . . . . ?
Cl11_13 B8_13 B10_13 B3_13 -149.9(5) . . . . ?
B9_13 B8_13 B10_13 B3_13 100.5(6) . . . . ?
B7_13 B8_13 B10_13 B3_13 63.1(7) . . . . ?
B5_13 B8_13 B10_13 B3_13 -0.8(7) . . . . ?
B4_13 B8_13 B10_13 Cl9_13 111.8(6) . . . . ?
Cl11_13 B8_13 B10_13 Cl9_13 -0.2(9) . . . . ?
B9_13 B8_13 B10_13 Cl9_13 -109.8(6) . . . . ?
B7_13 B8_13 B10_13 Cl9_13 -147.3(5) . . . . ?
B5_13 B8_13 B10_13 Cl9_13 148.9(5) . . . . ?
B1_13 B4_13 B10_13 B8_13 -101.7(6) . . . . ?
B5_13 B4_13 B10_13 B8_13 -37.9(5) . . . . ?
Cl4_13 B4_13 B10_13 B8_13 110.4(6) . . . . ?
B3_13 B4_13 B10_13 B8_13 -137.8(6) . . . . ?
B1_13 B4_13 B10_13 B11_13 -0.2(7) . . . . ?
B8_13 B4_13 B10_13 B11_13 101.5(6) . . . . ?
B5_13 B4_13 B10_13 B11_13 63.6(7) . . . . ?
Cl4_13 B4_13 B10_13 B11_13 -148.1(5) . . . . ?
B3_13 B4_13 B10_13 B11_13 -36.3(5) . . . . ?
B1_13 B4_13 B10_13 B9_13 -64.2(7) . . . . ?
B8_13 B4_13 B10_13 B9_13 37.4(5) . . . . ?
B5_13 B4_13 B10_13 B9_13 -0.4(7) . . . . ?
Cl4_13 B4_13 B10_13 B9_13 147.8(5) . . . . ?
B3_13 B4_13 B10_13 B9_13 -100.4(6) . . . . ?
B1_13 B4_13 B10_13 B3_13 36.1(5) . . . . ?
B8_13 B4_13 B10_13 B3_13 137.8(6) . . . . ?
B5_13 B4_13 B10_13 B3_13 99.9(6) . . . . ?
Cl4_13 B4_13 B10_13 B3_13 -111.8(6) . . . . ?
B1_13 B4_13 B10_13 Cl9_13 149.1(5) . . . . ?
B8_13 B4_13 B10_13 Cl9_13 -109.2(6) . . . . ?
B5_13 B4_13 B10_13 Cl9_13 -147.1(6) . . . . ?
Cl4_13 B4_13 B10_13 Cl9_13 1.2(9) . . . . ?
B3_13 B4_13 B10_13 Cl9_13 113.0(6) . . . . ?
B7_13 B9_13 B10_13 B8_13 37.9(5) . . . . ?
Cl10_13 B9_13 B10_13 B8_13 -110.6(6) . . . . ?
B11_13 B9_13 B10_13 B8_13 138.7(6) . . . . ?
B12_13 B9_13 B10_13 B8_13 100.8(6) . . . . ?
B7_13 B9_13 B10_13 B4_13 0.5(7) . . . . ?
Cl10_13 B9_13 B10_13 B4_13 -147.9(6) . . . . ?
B8_13 B9_13 B10_13 B4_13 -37.3(5) . . . . ?
B11_13 B9_13 B10_13 B4_13 101.4(6) . . . . ?
B12_13 B9_13 B10_13 B4_13 63.5(7) . . . . ?
B7_13 B9_13 B10_13 B11_13 -100.8(6) . . . . ?
Cl10_13 B9_13 B10_13 B11_13 110.7(6) . . . . ?
B8_13 B9_13 B10_13 B11_13 -138.7(6) . . . . ?
B12_13 B9_13 B10_13 B11_13 -37.9(5) . . . . ?
B7_13 B9_13 B10_13 B3_13 -63.2(7) . . . . ?
Cl10_13 B9_13 B10_13 B3_13 148.3(5) . . . . ?
B8_13 B9_13 B10_13 B3_13 -101.0(6) . . . . ?
B11_13 B9_13 B10_13 B3_13 37.6(5) . . . . ?
B12_13 B9_13 B10_13 B3_13 -0.2(7) . . . . ?
B7_13 B9_13 B10_13 Cl9_13 147.9(6) . . . . ?
Cl10_13 B9_13 B10_13 Cl9_13 -0.6(9) . . . . ?
B8_13 B9_13 B10_13 Cl9_13 110.0(6) . . . . ?
B11_13 B9_13 B10_13 Cl9_13 -111.3(6) . . . . ?
B12_13 B9_13 B10_13 Cl9_13 -149.1(5) . . . . ?
B2_13 B3_13 B10_13 B8_13 -62.8(7) . . . . ?
B1_13 B3_13 B10_13 B8_13 1.3(7) . . . . ?
B11_13 B3_13 B10_13 B8_13 -101.7(6) . . . . ?
Cl5_13 B3_13 B10_13 B8_13 147.5(5) . . . . ?
B4_13 B3_13 B10_13 B8_13 37.7(5) . . . . ?
B2_13 B3_13 B10_13 B4_13 -100.6(6) . . . . ?
B1_13 B3_13 B10_13 B4_13 -36.4(5) . . . . ?
B11_13 B3_13 B10_13 B4_13 -139.4(6) . . . . ?
Cl5_13 B3_13 B10_13 B4_13 109.7(7) . . . . ?
B2_13 B3_13 B10_13 B11_13 38.9(5) . . . . ?
B1_13 B3_13 B10_13 B11_13 103.0(6) . . . . ?
Cl5_13 B3_13 B10_13 B11_13 -110.8(6) . . . . ?
B4_13 B3_13 B10_13 B11_13 139.4(6) . . . . ?
B2_13 B3_13 B10_13 B9_13 0.9(7) . . . . ?
B1_13 B3_13 B10_13 B9_13 65.0(7) . . . . ?
B11_13 B3_13 B10_13 B9_13 -38.0(5) . . . . ?
Cl5_13 B3_13 B10_13 B9_13 -148.8(6) . . . . ?
B4_13 B3_13 B10_13 B9_13 101.4(6) . . . . ?
B2_13 B3_13 B10_13 Cl9_13 148.6(6) . . . . ?
B1_13 B3_13 B10_13 Cl9_13 -147.3(5) . . . . ?
B11_13 B3_13 B10_13 Cl9_13 109.7(6) . . . . ?
Cl5_13 B3_13 B10_13 Cl9_13 -1.1(9) . . . . ?
B4_13 B3_13 B10_13 Cl9_13 -110.8(6) . . . . ?
B2_13 B3_13 B11_13 Cl7_13 111.3(7) . . . . ?
B1_13 B3_13 B11_13 Cl7_13 148.8(6) . . . . ?
Cl5_13 B3_13 B11_13 Cl7_13 0.8(9) . . . . ?
B4_13 B3_13 B11_13 Cl7_13 -147.6(5) . . . . ?
B10_13 B3_13 B11_13 Cl7_13 -111.6(6) . . . . ?
B2_13 B3_13 B11_13 B10_13 -137.1(6) . . . . ?
B1_13 B3_13 B11_13 B10_13 -99.7(6) . . . . ?
Cl5_13 B3_13 B11_13 B10_13 112.4(6) . . . . ?
B4_13 B3_13 B11_13 B10_13 -36.0(5) . . . . ?
B1_13 B3_13 B11_13 B2_13 37.5(6) . . . . ?
Cl5_13 B3_13 B11_13 B2_13 -110.5(7) . . . . ?
B4_13 B3_13 B11_13 B2_13 101.1(6) . . . . ?
B10_13 B3_13 B11_13 B2_13 137.1(6) . . . . ?
B2_13 B3_13 B11_13 B9_13 -99.3(6) . . . . ?
B1_13 B3_13 B11_13 B9_13 -61.8(7) . . . . ?
Cl5_13 B3_13 B11_13 B9_13 150.2(5) . . . . ?
B4_13 B3_13 B11_13 B9_13 1.8(7) . . . . ?
B10_13 B3_13 B11_13 B9_13 37.8(5) . . . . ?
B2_13 B3_13 B11_13 B12_13 -35.7(5) . . . . ?
B1_13 B3_13 B11_13 B12_13 1.8(8) . . . . ?
Cl5_13 B3_13 B11_13 B12_13 -146.2(5) . . . . ?
B4_13 B3_13 B11_13 B12_13 65.4(7) . . . . ?
B10_13 B3_13 B11_13 B12_13 101.5(6) . . . . ?
B8_13 B10_13 B11_13 Cl7_13 -147.4(5) . . . . ?
B4_13 B10_13 B11_13 Cl7_13 148.9(5) . . . . ?
B9_13 B10_13 B11_13 Cl7_13 -110.1(6) . . . . ?
B3_13 B10_13 B11_13 Cl7_13 112.3(6) . . . . ?
Cl9_13 B10_13 B11_13 Cl7_13 -0.6(9) . . . . ?
B8_13 B10_13 B11_13 B3_13 100.3(6) . . . . ?
B4_13 B10_13 B11_13 B3_13 36.6(5) . . . . ?
B9_13 B10_13 B11_13 B3_13 137.6(6) . . . . ?
Cl9_13 B10_13 B11_13 B3_13 -112.9(6) . . . . ?
B8_13 B10_13 B11_13 B2_13 63.0(7) . . . . ?
B4_13 B10_13 B11_13 B2_13 -0.7(7) . . . . ?
B9_13 B10_13 B11_13 B2_13 100.3(6) . . . . ?
B3_13 B10_13 B11_13 B2_13 -37.3(5) . . . . ?
Cl9_13 B10_13 B11_13 B2_13 -150.2(5) . . . . ?
B8_13 B10_13 B11_13 B9_13 -37.3(5) . . . . ?
B4_13 B10_13 B11_13 B9_13 -101.0(6) . . . . ?
B3_13 B10_13 B11_13 B9_13 -137.6(6) . . . . ?
Cl9_13 B10_13 B11_13 B9_13 109.5(6) . . . . ?
B8_13 B10_13 B11_13 B12_13 0.8(7) . . . . ?
B4_13 B10_13 B11_13 B12_13 -62.9(7) . . . . ?
B9_13 B10_13 B11_13 B12_13 38.1(5) . . . . ?
B3_13 B10_13 B11_13 B12_13 -99.5(6) . . . . ?
Cl9_13 B10_13 B11_13 B12_13 147.6(5) . . . . ?
B3_13 B2_13 B11_13 Cl7_13 -111.1(6) . . . . ?
B6_13 B2_13 B11_13 Cl7_13 146.6(5) . . . . ?
B1_13 B2_13 B11_13 Cl7_13 -148.0(5) . . . . ?
B12_13 B2_13 B11_13 Cl7_13 109.5(6) . . . . ?
Cl6_13 B2_13 B11_13 Cl7_13 -0.8(9) . . . . ?
B6_13 B2_13 B11_13 B3_13 -102.3(6) . . . . ?
B1_13 B2_13 B11_13 B3_13 -36.9(5) . . . . ?
B12_13 B2_13 B11_13 B3_13 -139.4(6) . . . . ?
Cl6_13 B2_13 B11_13 B3_13 110.4(7) . . . . ?
B3_13 B2_13 B11_13 B10_13 38.2(5) . . . . ?
B6_13 B2_13 B11_13 B10_13 -64.0(7) . . . . ?
B1_13 B2_13 B11_13 B10_13 1.4(7) . . . . ?
B12_13 B2_13 B11_13 B10_13 -101.2(6) . . . . ?
Cl6_13 B2_13 B11_13 B10_13 148.6(6) . . . . ?
B3_13 B2_13 B11_13 B9_13 101.1(6) . . . . ?
B6_13 B2_13 B11_13 B9_13 -1.2(7) . . . . ?
B1_13 B2_13 B11_13 B9_13 64.2(7) . . . . ?
B12_13 B2_13 B11_13 B9_13 -38.3(5) . . . . ?
Cl6_13 B2_13 B11_13 B9_13 -148.5(5) . . . . ?
B3_13 B2_13 B11_13 B12_13 139.4(6) . . . . ?
B6_13 B2_13 B11_13 B12_13 37.1(5) . . . . ?
B1_13 B2_13 B11_13 B12_13 102.5(6) . . . . ?
Cl6_13 B2_13 B11_13 B12_13 -110.3(7) . . . . ?
B7_13 B9_13 B11_13 Cl7_13 -147.8(5) . . . . ?
Cl10_13 B9_13 B11_13 Cl7_13 0.9(9) . . . . ?
B10_13 B9_13 B11_13 Cl7_13 111.8(6) . . . . ?
B8_13 B9_13 B11_13 Cl7_13 148.4(5) . . . . ?
B12_13 B9_13 B11_13 Cl7_13 -110.7(6) . . . . ?
B7_13 B9_13 B11_13 B3_13 62.3(7) . . . . ?
Cl10_13 B9_13 B11_13 B3_13 -149.1(5) . . . . ?
B10_13 B9_13 B11_13 B3_13 -38.2(5) . . . . ?
B8_13 B9_13 B11_13 B3_13 -1.5(7) . . . . ?
B12_13 B9_13 B11_13 B3_13 99.4(6) . . . . ?
B7_13 B9_13 B11_13 B10_13 100.4(6) . . . . ?
Cl10_13 B9_13 B11_13 B10_13 -110.9(6) . . . . ?
B8_13 B9_13 B11_13 B10_13 36.6(5) . . . . ?
B12_13 B9_13 B11_13 B10_13 137.5(6) . . . . ?
B7_13 B9_13 B11_13 B2_13 0.6(7) . . . . ?
Cl10_13 B9_13 B11_13 B2_13 149.2(5) . . . . ?
B10_13 B9_13 B11_13 B2_13 -99.8(6) . . . . ?
B8_13 B9_13 B11_13 B2_13 -63.2(7) . . . . ?
B12_13 B9_13 B11_13 B2_13 37.7(5) . . . . ?
B7_13 B9_13 B11_13 B12_13 -37.1(5) . . . . ?
Cl10_13 B9_13 B11_13 B12_13 111.5(6) . . . . ?
B10_13 B9_13 B11_13 B12_13 -137.5(6) . . . . ?
B8_13 B9_13 B11_13 B12_13 -100.9(6) . . . . ?
B2_13 B6_13 B12_13 Cl8_13 -111.1(7) . . . . ?
Cl2_13 B6_13 B12_13 Cl8_13 1.5(9) . . . . ?
B7_13 B6_13 B12_13 Cl8_13 112.2(6) . . . . ?
B1_13 B6_13 B12_13 Cl8_13 -148.0(6) . . . . ?
B5_13 B6_13 B12_13 Cl8_13 149.2(5) . . . . ?
Cl2_13 B6_13 B12_13 B2_13 112.6(7) . . . . ?
B7_13 B6_13 B12_13 B2_13 -136.7(6) . . . . ?
B1_13 B6_13 B12_13 B2_13 -36.9(5) . . . . ?
B5_13 B6_13 B12_13 B2_13 -99.7(6) . . . . ?
B2_13 B6_13 B12_13 B7_13 136.7(6) . . . . ?
Cl2_13 B6_13 B12_13 B7_13 -110.7(7) . . . . ?
B1_13 B6_13 B12_13 B7_13 99.8(6) . . . . ?
B5_13 B6_13 B12_13 B7_13 37.0(5) . . . . ?
B2_13 B6_13 B12_13 B11_13 36.8(5) . . . . ?
Cl2_13 B6_13 B12_13 B11_13 149.4(5) . . . . ?
B7_13 B6_13 B12_13 B11_13 -99.9(6) . . . . ?
B1_13 B6_13 B12_13 B11_13 -0.2(7) . . . . ?
B5_13 B6_13 B12_13 B11_13 -62.9(7) . . . . ?
B2_13 B6_13 B12_13 B9_13 99.6(6) . . . . ?
Cl2_13 B6_13 B12_13 B9_13 -147.7(5) . . . . ?
B7_13 B6_13 B12_13 B9_13 -37.1(5) . . . . ?
B1_13 B6_13 B12_13 B9_13 62.7(7) . . . . ?
B5_13 B6_13 B12_13 B9_13 -0.1(7) . . . . ?
B3_13 B2_13 B12_13 Cl8_13 -146.5(6) . . . . ?
B6_13 B2_13 B12_13 Cl8_13 111.4(6) . . . . ?
B1_13 B2_13 B12_13 Cl8_13 149.4(5) . . . . ?
B11_13 B2_13 B12_13 Cl8_13 -109.7(7) . . . . ?
Cl6_13 B2_13 B12_13 Cl8_13 1.0(9) . . . . ?
B3_13 B2_13 B12_13 B6_13 102.1(6) . . . . ?
B1_13 B2_13 B12_13 B6_13 38.0(5) . . . . ?
B11_13 B2_13 B12_13 B6_13 138.9(6) . . . . ?
Cl6_13 B2_13 B12_13 B6_13 -110.4(7) . . . . ?
B3_13 B2_13 B12_13 B7_13 63.3(7) . . . . ?
B6_13 B2_13 B12_13 B7_13 -38.8(5) . . . . ?
B1_13 B2_13 B12_13 B7_13 -0.8(8) . . . . ?
B11_13 B2_13 B12_13 B7_13 100.2(6) . . . . ?
Cl6_13 B2_13 B12_13 B7_13 -149.1(5) . . . . ?
B3_13 B2_13 B12_13 B11_13 -36.8(5) . . . . ?
B6_13 B2_13 B12_13 B11_13 -138.9(6) . . . . ?
B1_13 B2_13 B12_13 B11_13 -101.0(6) . . . . ?
Cl6_13 B2_13 B12_13 B11_13 110.7(6) . . . . ?
B3_13 B2_13 B12_13 B9_13 1.1(8) . . . . ?
B6_13 B2_13 B12_13 B9_13 -101.0(6) . . . . ?
B1_13 B2_13 B12_13 B9_13 -63.0(7) . . . . ?
B11_13 B2_13 B12_13 B9_13 37.9(5) . . . . ?
Cl6_13 B2_13 B12_13 B9_13 148.6(5) . . . . ?
Cl12_13 B7_13 B12_13 Cl8_13 -1.2(9) . . . . ?
B9_13 B7_13 B12_13 Cl8_13 110.0(7) . . . . ?
B8_13 B7_13 B12_13 Cl8_13 147.9(5) . . . . ?
B6_13 B7_13 B12_13 Cl8_13 -111.9(7) . . . . ?
B5_13 B7_13 B12_13 Cl8_13 -148.6(5) . . . . ?
Cl12_13 B7_13 B12_13 B6_13 110.7(7) . . . . ?
B9_13 B7_13 B12_13 B6_13 -138.1(6) . . . . ?
B8_13 B7_13 B12_13 B6_13 -100.2(6) . . . . ?
B5_13 B7_13 B12_13 B6_13 -36.7(5) . . . . ?
Cl12_13 B7_13 B12_13 B2_13 148.8(6) . . . . ?
B9_13 B7_13 B12_13 B2_13 -100.0(6) . . . . ?
B8_13 B7_13 B12_13 B2_13 -62.1(7) . . . . ?
B6_13 B7_13 B12_13 B2_13 38.1(5) . . . . ?
B5_13 B7_13 B12_13 B2_13 1.4(7) . . . . ?
Cl12_13 B7_13 B12_13 B11_13 -147.9(5) . . . . ?
B9_13 B7_13 B12_13 B11_13 -36.8(5) . . . . ?
B8_13 B7_13 B12_13 B11_13 1.1(7) . . . . ?
B6_13 B7_13 B12_13 B11_13 101.3(6) . . . . ?
B5_13 B7_13 B12_13 B11_13 64.6(7) . . . . ?
Cl12_13 B7_13 B12_13 B9_13 -111.1(7) . . . . ?
B8_13 B7_13 B12_13 B9_13 37.9(5) . . . . ?
B6_13 B7_13 B12_13 B9_13 138.1(6) . . . . ?
B5_13 B7_13 B12_13 B9_13 101.4(6) . . . . ?
Cl7_13 B11_13 B12_13 Cl8_13 -0.1(9) . . . . ?
B3_13 B11_13 B12_13 Cl8_13 147.5(5) . . . . ?
B10_13 B11_13 B12_13 Cl8_13 -148.7(5) . . . . ?
B2_13 B11_13 B12_13 Cl8_13 112.1(6) . . . . ?
B9_13 B11_13 B12_13 Cl8_13 -110.9(6) . . . . ?
Cl7_13 B11_13 B12_13 B6_13 -148.6(5) . . . . ?
B3_13 B11_13 B12_13 B6_13 -1.0(7) . . . . ?
B10_13 B11_13 B12_13 B6_13 62.8(7) . . . . ?
B2_13 B11_13 B12_13 B6_13 -36.4(5) . . . . ?
B9_13 B11_13 B12_13 B6_13 100.7(6) . . . . ?
Cl7_13 B11_13 B12_13 B2_13 -112.2(6) . . . . ?
B3_13 B11_13 B12_13 B2_13 35.4(5) . . . . ?
B10_13 B11_13 B12_13 B2_13 99.2(6) . . . . ?
B9_13 B11_13 B12_13 B2_13 137.0(6) . . . . ?
Cl7_13 B11_13 B12_13 B7_13 147.5(6) . . . . ?
B3_13 B11_13 B12_13 B7_13 -65.0(7) . . . . ?
B10_13 B11_13 B12_13 B7_13 -1.2(7) . . . . ?
B2_13 B11_13 B12_13 B7_13 -100.4(6) . . . . ?
B9_13 B11_13 B12_13 B7_13 36.7(5) . . . . ?
Cl7_13 B11_13 B12_13 B9_13 110.8(6) . . . . ?
B3_13 B11_13 B12_13 B9_13 -101.6(6) . . . . ?
B10_13 B11_13 B12_13 B9_13 -37.9(5) . . . . ?
B2_13 B11_13 B12_13 B9_13 -137.0(6) . . . . ?
B7_13 B9_13 B12_13 Cl8_13 -111.9(6) . . . . ?
Cl10_13 B9_13 B12_13 Cl8_13 -1.0(9) . . . . ?
B10_13 B9_13 B12_13 Cl8_13 147.4(5) . . . . ?
B8_13 B9_13 B12_13 Cl8_13 -149.9(5) . . . . ?
B11_13 B9_13 B12_13 Cl8_13 109.7(6) . . . . ?
B7_13 B9_13 B12_13 B6_13 37.7(5) . . . . ?
Cl10_13 B9_13 B12_13 B6_13 148.6(6) . . . . ?
B10_13 B9_13 B12_13 B6_13 -63.0(7) . . . . ?
B8_13 B9_13 B12_13 B6_13 -0.2(7) . . . . ?
B11_13 B9_13 B12_13 B6_13 -100.7(6) . . . . ?
B7_13 B9_13 B12_13 B2_13 100.2(6) . . . . ?
Cl10_13 B9_13 B12_13 B2_13 -148.9(6) . . . . ?
B10_13 B9_13 B12_13 B2_13 -0.5(7) . . . . ?
B8_13 B9_13 B12_13 B2_13 62.2(7) . . . . ?
B11_13 B9_13 B12_13 B2_13 -38.2(5) . . . . ?
Cl10_13 B9_13 B12_13 B7_13 110.9(7) . . . . ?
B10_13 B9_13 B12_13 B7_13 -100.7(6) . . . . ?
B8_13 B9_13 B12_13 B7_13 -37.9(5) . . . . ?
B11_13 B9_13 B12_13 B7_13 -138.4(6) . . . . ?
B7_13 B9_13 B12_13 B11_13 138.4(6) . . . . ?
Cl10_13 B9_13 B12_13 B11_13 -110.7(7) . . . . ?
B10_13 B9_13 B12_13 B11_13 37.7(5) . . . . ?
B8_13 B9_13 B12_13 B11_13 100.4(6) . . . . ?

_refine_diff_density_max         2.534
_refine_diff_density_min         -0.882
_refine_diff_density_rms         0.124



####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_zju_yb1_0m_a_sq_sq
_database_code_depnum_ccdc_archive 'CCDC 2042564'
loop_
_audit_author_name
_audit_author_address
'Yue Zhao'
;Nanjing University
China
;
_audit_update_record             
;
2020-11-05 deposited with the CCDC.	2020-12-10 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2018/3
_shelx_SHELXL_version_number     2018/3
_chemical_name_systematic        BSF-74
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C68 H60 B24 Cl24 Cu2 N8 O4'
_chemical_formula_weight         2290.56

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      tetragonal
_space_group_IT_number           114
_space_group_name_H-M_alt        'P -4 21 c'
_space_group_name_Hall           'P -4 2n'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, z'
'y, -x, -z'
'-y, x, -z'
'-x+1/2, y+1/2, -z+1/2'
'x+1/2, -y+1/2, -z+1/2'
'-y+1/2, -x+1/2, z+1/2'
'y+1/2, x+1/2, z+1/2'

_cell_length_a                   33.475(3)
_cell_length_b                   33.475(3)
_cell_length_c                   39.463(5)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_volume                     44221(10)
_cell_formula_units_Z            16
_cell_measurement_temperature    296(2)
_cell_measurement_reflns_used    9754
_cell_measurement_theta_min      2.19
_cell_measurement_theta_max      28.23

_exptl_crystal_description       block
_exptl_crystal_colour            ?
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    1.376
_exptl_crystal_F_000             18272
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          0.200
_exptl_crystal_size_mid          0.200
_exptl_crystal_size_min          0.200
_exptl_absorpt_coefficient_mu    1.009
_shelx_estimated_absorpt_T_min   0.824
_shelx_estimated_absorpt_T_max   0.824
_exptl_absorpt_correction_type   ?
_exptl_absorpt_correction_T_min  ?
_exptl_absorpt_correction_T_max  ?
_exptl_absorpt_process_details   ?
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      296(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_source                   ?
_diffrn_measurement_device_type  'Bruker D8 VENTURE PHOTON 100'
_diffrn_measurement_method       ?
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            238555
_diffrn_reflns_av_unetI/netI     0.0871
_diffrn_reflns_av_R_equivalents  0.0975
_diffrn_reflns_limit_h_min       -39
_diffrn_reflns_limit_h_max       44
_diffrn_reflns_limit_k_min       -44
_diffrn_reflns_limit_k_max       40
_diffrn_reflns_limit_l_min       -52
_diffrn_reflns_limit_l_max       41
_diffrn_reflns_theta_min         0.860
_diffrn_reflns_theta_max         28.294
_diffrn_reflns_theta_full        25.242
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measured_fraction_theta_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.997
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.996
_diffrn_reflns_point_group_measured_fraction_full 0.998
_reflns_number_total             54700
_reflns_number_gt                39976
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.907
_reflns_Friedel_fraction_max     0.994
_reflns_Friedel_fraction_full    0.998

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences. Completness statistics refer to single and
 composite reflections containing twin component 1 only.
;

_computing_data_collection       ?
_computing_cell_refinement       ?
_computing_data_reduction        ?
_computing_structure_solution    'SHELXT 2014/5 (Sheldrick, 2014)'
_computing_structure_refinement  'SHELXL-2018/3 (Sheldrick, 2018)'
_computing_molecular_graphics    ?
_computing_publication_material  ?
_refine_special_details          
;
 Refined as a 2-component twin.
;
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0832P)²+97.8601P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_abs_structure_details 
;
 Flack x determined using 15351 quotients [(I+)-(I-)]/[(I+)+(I-)]
 (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259).
;
_refine_ls_abs_structure_Flack   0.002(7)
_chemical_absolute_configuration ?
_refine_ls_number_reflns         54700
_refine_ls_number_parameters     2352
_refine_ls_number_restraints     2534
_refine_ls_R_factor_all          0.0922
_refine_ls_R_factor_gt           0.0627
_refine_ls_wR_factor_ref         0.1896
_refine_ls_wR_factor_gt          0.1693
_refine_ls_goodness_of_fit_ref   1.023
_refine_ls_restrained_S_all      1.000
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C 0.4292(3) -0.0802(2) 0.6643(2) 0.0343(19) Uani 1 1 d . . . . .
H1A H 0.402290 -0.073342 0.670296 0.051 Uiso 1 1 calc R U . . .
H1B H 0.445146 -0.081993 0.684533 0.051 Uiso 1 1 calc R U . . .
H1C H 0.429490 -0.105396 0.652790 0.051 Uiso 1 1 calc R U . . .
C6 C 0.4236(3) 0.5751(3) 0.3347(2) 0.0340(19) Uani 1 1 d . . . . .
H6A H 0.435592 0.573587 0.312591 0.051 Uiso 1 1 calc R U . . .
H6B H 0.424498 0.602178 0.342614 0.051 Uiso 1 1 calc R U . . .
H6C H 0.396336 0.566382 0.333373 0.051 Uiso 1 1 calc R U . . .
C9 C -0.0773(3) 0.4255(3) 0.6637(2) 0.0347(19) Uani 1 1 d . . . . .
H9A H -0.101470 0.418739 0.651884 0.052 Uiso 1 1 calc R U . . .
H9B H -0.083545 0.442633 0.682480 0.052 Uiso 1 1 calc R U . . .
H9C H -0.064908 0.401503 0.671946 0.052 Uiso 1 1 calc R U . . .
C12 C 0.1871(3) 0.1653(3) 0.4092(3) 0.042(2) Uani 1 1 d . . . . .
H12A H 0.158945 0.164398 0.413923 0.063 Uiso 1 1 calc R U . . .
H12B H 0.201729 0.164879 0.430073 0.063 Uiso 1 1 calc R U . . .
H12C H 0.194366 0.142524 0.395729 0.063 Uiso 1 1 calc R U . . .
C13 C 0.1790(3) 0.3170(3) 0.0759(2) 0.038(2) Uani 1 1 d . . . . .
H13A H 0.197831 0.329669 0.061006 0.057 Uiso 1 1 calc R U . . .
H13B H 0.160943 0.336677 0.084747 0.057 Uiso 1 1 calc R U . . .
H13C H 0.164226 0.297192 0.063568 0.057 Uiso 1 1 calc R U . . .
C14 C 0.3176(3) 0.1603(3) 0.0915(3) 0.043(2) Uani 1 1 d . . . . .
H14A H 0.301472 0.159039 0.071473 0.065 Uiso 1 1 calc R U . . .
H14B H 0.311893 0.137741 0.105730 0.065 Uiso 1 1 calc R U . . .
H14C H 0.345358 0.159970 0.085316 0.065 Uiso 1 1 calc R U . . .
C16 C 0.3304(4) 0.3193(4) 0.4153(3) 0.071(4) Uani 1 1 d . . . . .
H16A H 0.352241 0.332625 0.404354 0.085 Uiso 1 1 calc R U . . .
H16B H 0.340590 0.299641 0.430766 0.085 Uiso 1 1 calc R U . . .
H16C H 0.314622 0.338422 0.427497 0.085 Uiso 1 1 calc R U . . .
C17 C 0.0795(3) -0.0711(3) 0.3343(2) 0.039(2) Uani 1 1 d . . . . .
H17A H 0.077652 -0.059674 0.312003 0.059 Uiso 1 1 calc R U . . .
H17B H 0.076361 -0.099528 0.332836 0.059 Uiso 1 1 calc R U . . .
H17C H 0.105099 -0.064920 0.343882 0.059 Uiso 1 1 calc R U . . .
Cu1 Cu 0.500000 0.000000 0.64095(3) 0.0128(2) Uani 1 2 d S T P . .
Cu2 Cu 0.000000 0.500000 0.64053(3) 0.0148(2) Uani 1 2 d S T P . .
Cu3 Cu 0.500000 0.500000 0.35915(3) 0.0139(2) Uani 1 2 d S T P . .
Cu4 Cu 0.000000 0.000000 0.35636(2) 0.0129(2) Uani 1 2 d S T P . .
Cu5 Cu 0.24982(2) 0.24966(2) 0.39099(2) 0.01588(16) Uani 1 1 d . . . . .
Cu6 Cu 0.25643(2) 0.24538(2) 0.10757(2) 0.01674(16) Uani 1 1 d . . . . .
O1 O 0.44516(15) -0.05039(15) 0.64291(12) 0.0209(10) Uani 1 1 d . . . . .
O2 O -0.05068(16) 0.44556(15) 0.64119(14) 0.0241(11) Uani 1 1 d . . . . .
O3 O 0.19619(16) 0.20109(15) 0.39099(13) 0.0240(11) Uani 1 1 d . . . . .
O4 O 0.20018(15) 0.29814(15) 0.10357(14) 0.0256(11) Uani 1 1 d . . . . .
O5 O 0.30900(15) 0.19623(15) 0.10949(13) 0.0228(10) Uani 1 1 d . . . . .
O6 O 0.44553(15) 0.54946(16) 0.35805(13) 0.0232(11) Uani 1 1 d . . . . .
O7 O 0.04839(14) -0.05466(16) 0.35548(13) 0.0233(11) Uani 1 1 d . . . . .
O8 O 0.30710(18) 0.30088(16) 0.39138(14) 0.0302(12) Uani 1 1 d . . . . .
C1_1 C 0.4701(2) 0.0726(2) 0.67460(17) 0.0181(13) Uani 1 1 d . . . . .
H1_1 H 0.484321 0.085004 0.657327 0.022 Uiso 1 1 calc R U . . .
C2_1 C 0.4480(2) 0.0957(2) 0.69653(17) 0.0186(13) Uani 1 1 d . . . . .
H2_1 H 0.447658 0.123260 0.693883 0.022 Uiso 1 1 calc R U . . .
C3_1 C 0.4262(2) 0.0781(2) 0.72275(17) 0.0174(13) Uani 1 1 d . . . . .
C4_1 C 0.4291(2) 0.0369(2) 0.72581(17) 0.0221(14) Uani 1 1 d . . . . .
H4_1 H 0.415942 0.023865 0.743401 0.027 Uiso 1 1 calc R U . . .
C5_1 C 0.4515(2) 0.0149(2) 0.70269(17) 0.0195(14) Uani 1 1 d . . . . .
H5_1 H 0.452572 -0.012736 0.704865 0.023 Uiso 1 1 calc R U . . .
C6_1 C 0.4017(2) 0.1030(2) 0.74636(16) 0.0172(13) Uani 1 1 d . . . . .
C7_1 C 0.4130(2) 0.1420(2) 0.75318(17) 0.0209(14) Uani 1 1 d . . . . .
H7_1 H 0.435903 0.152486 0.743302 0.025 Uiso 1 1 calc R U . . .
C8_1 C 0.3898(2) 0.1657(2) 0.77499(17) 0.0205(14) Uani 1 1 d . . . . .
H8_1 H 0.397691 0.191705 0.780040 0.025 Uiso 1 1 calc R U . . .
C9_1 C 0.3549(2) 0.1502(2) 0.78903(17) 0.0197(14) Uani 1 1 d . . . . .
C10_1 C 0.3438(2) 0.1106(2) 0.78210(18) 0.0205(14) Uani 1 1 d . . . . .
H10_1 H 0.320850 0.099984 0.791846 0.025 Uiso 1 1 calc R U . . .
C11_1 C 0.3674(2) 0.0868(2) 0.76039(18) 0.0222(14) Uani 1 1 d . . . . .
H11_1 H 0.360023 0.060588 0.755575 0.027 Uiso 1 1 calc R U . . .
C12_1 C 0.3296(2) 0.1747(2) 0.81222(16) 0.0172(13) Uani 1 1 d . . . . .
C13_1 C 0.3264(2) 0.2159(2) 0.80874(18) 0.0227(14) Uani 1 1 d . . . . .
H13_1 H 0.340572 0.229137 0.791849 0.027 Uiso 1 1 calc R U . . .
C14_1 C 0.3022(2) 0.2369(2) 0.83054(17) 0.0208(14) Uani 1 1 d . . . . .
H14_1 H 0.300533 0.264478 0.828077 0.025 Uiso 1 1 calc R U . . .
C15_1 C 0.2839(2) 0.1791(2) 0.85837(16) 0.0180(13) Uani 1 1 d . . . . .
H15_1 H 0.268884 0.166318 0.874961 0.022 Uiso 1 1 calc R U . . .
C16_1 C 0.3082(2) 0.1567(2) 0.83820(17) 0.0200(14) Uani 1 1 d . . . . .
H16_1 H 0.310488 0.129360 0.841846 0.024 Uiso 1 1 calc R U . . .
N1_1 N 0.47166(17) 0.03241(17) 0.67740(13) 0.0156(11) Uani 1 1 d . . . . .
N2_1 N 0.28085(16) 0.21946(17) 0.85515(13) 0.0151(11) Uani 1 1 d . . . . .
C1_2 C 0.2004(2) 0.2643(2) 0.82894(16) 0.0202(14) Uani 1 1 d . . . . .
H1_2 H 0.202986 0.236830 0.826026 0.024 Uiso 1 1 calc R U . . .
C2_2 C 0.1768(2) 0.2846(2) 0.80626(18) 0.0213(14) Uani 1 1 d . . . . .
H2_2 H 0.163961 0.271325 0.788684 0.026 Uiso 1 1 calc R U . . .
C3_2 C 0.17279(19) 0.3260(2) 0.81038(16) 0.0149(12) Uani 1 1 d . . . . .
C4_2 C 0.1924(2) 0.3435(2) 0.83695(17) 0.0225(14) Uani 1 1 d . . . . .
H4_2 H 0.190444 0.370925 0.840185 0.027 Uiso 1 1 calc R U . . .
C5_2 C 0.2151(2) 0.3209(2) 0.85905(17) 0.0220(14) Uani 1 1 d . . . . .
H5_2 H 0.227492 0.333447 0.877261 0.026 Uiso 1 1 calc R U . . .
C6_2 C 0.1482(2) 0.3505(2) 0.78666(17) 0.0174(13) Uani 1 1 d . . . . .
C7_2 C 0.1604(2) 0.3898(2) 0.77914(18) 0.0223(15) Uani 1 1 d . . . . .
H7_2 H 0.183643 0.399965 0.788683 0.027 Uiso 1 1 calc R U . . .
C8_2 C 0.1377(2) 0.4135(2) 0.75748(18) 0.0224(15) Uani 1 1 d . . . . .
H8_2 H 0.146085 0.439244 0.752075 0.027 Uiso 1 1 calc R U . . .
C9_2 C 0.10244(19) 0.3987(2) 0.74404(16) 0.0150(12) Uani 1 1 d . . . . .
C10_2 C 0.0899(2) 0.3598(2) 0.75089(18) 0.0211(14) Uani 1 1 d . . . . .
H10_2 H 0.066453 0.350070 0.741341 0.025 Uiso 1 1 calc R U . . .
C11_2 C 0.1129(2) 0.3354(2) 0.77230(17) 0.0185(13) Uani 1 1 d . . . . .
H11_2 H 0.104817 0.309442 0.776944 0.022 Uiso 1 1 calc R U . . .
C12_2 C 0.0779(2) 0.4244(2) 0.72076(16) 0.0169(13) Uani 1 1 d . . . . .
C13_2 C 0.0366(2) 0.4256(2) 0.72268(17) 0.0209(14) Uani 1 1 d . . . . .
H13_2 H 0.023387 0.410318 0.738845 0.025 Uiso 1 1 calc R U . . .
C14_2 C 0.0150(2) 0.4494(2) 0.70066(16) 0.0193(13) Uani 1 1 d . . . . .
H14_2 H -0.012735 0.449773 0.702367 0.023 Uiso 1 1 calc R U . . .
C15_2 C 0.0729(2) 0.4714(2) 0.67483(17) 0.0202(14) Uani 1 1 d . . . . .
H15_2 H 0.085375 0.486969 0.658375 0.024 Uiso 1 1 calc R U . . .
C16_2 C 0.0961(2) 0.4489(2) 0.69597(17) 0.0214(14) Uani 1 1 d . . . . .
H16_2 H 0.123795 0.449605 0.694056 0.026 Uiso 1 1 calc R U . . .
N1_2 N 0.21995(17) 0.28108(17) 0.85503(13) 0.0155(11) Uani 1 1 d . . . . .
N2_2 N 0.03264(17) 0.47202(17) 0.67695(13) 0.0165(11) Uani 1 1 d . . . . .
C1_3 C 0.4897(2) 0.0506(2) 0.57897(17) 0.0202(14) Uani 1 1 d . . . . .
H1_3 H 0.517070 0.047132 0.576539 0.024 Uiso 1 1 calc R U . . .
C2_3 C 0.4702(2) 0.0745(2) 0.55658(17) 0.0212(14) Uani 1 1 d . . . . .
H2_3 H 0.484261 0.086914 0.539190 0.025 Uiso 1 1 calc R U . . .
C3_3 C 0.4285(2) 0.0804(2) 0.55977(17) 0.0181(13) Uani 1 1 d . . . . .
C4_3 C 0.4098(2) 0.0603(2) 0.58577(17) 0.0214(14) Uani 1 1 d . . . . .
H4_3 H 0.382318 0.062835 0.588606 0.026 Uiso 1 1 calc R U . . .
C5_3 C 0.4315(2) 0.0365(2) 0.60772(18) 0.0224(14) Uani 1 1 d . . . . .
H5_3 H 0.418227 0.023358 0.625200 0.027 Uiso 1 1 calc R U . . .
C6_3 C 0.4055(2) 0.1055(2) 0.53608(17) 0.0197(13) Uani 1 1 d . . . . .
C7_3 C 0.4193(2) 0.1421(2) 0.52332(19) 0.0238(15) Uani 1 1 d . . . . .
H7_3 H 0.444832 0.150913 0.528869 0.029 Uiso 1 1 calc R U . . .
C8_3 C 0.3950(2) 0.1655(2) 0.50230(19) 0.0237(15) Uani 1 1 d . . . . .
H8_3 H 0.404430 0.189780 0.494009 0.028 Uiso 1 1 calc R U . . .
C9_3 C 0.3566(2) 0.1525(2) 0.49376(18) 0.0227(15) Uani 1 1 d . . . . .
C10_3 C 0.3432(2) 0.1156(2) 0.50537(19) 0.0278(17) Uani 1 1 d . . . . .
H10_3 H 0.318103 0.106241 0.499025 0.033 Uiso 1 1 calc R U . . .
C11_3 C 0.3675(2) 0.0928(2) 0.52663(19) 0.0291(17) Uani 1 1 d . . . . .
H11_3 H 0.358139 0.068462 0.534679 0.035 Uiso 1 1 calc R U . . .
C12_3 C 0.3301(2) 0.1757(2) 0.47077(18) 0.0209(14) Uani 1 1 d . . . . .
C13_3 C 0.3256(2) 0.2166(2) 0.47367(19) 0.0284(17) Uani 1 1 d . . . . .
H13_3 H 0.340102 0.230654 0.489882 0.034 Uiso 1 1 calc R U . . .
C14_3 C 0.2995(2) 0.2368(2) 0.45234(17) 0.0266(16) Uani 1 1 d . . . . .
H14_3 H 0.295798 0.264091 0.455504 0.032 Uiso 1 1 calc R U . . .
C15_3 C 0.2840(2) 0.1784(2) 0.42412(18) 0.0220(14) Uani 1 1 d . . . . .
H15_3 H 0.270530 0.165339 0.406747 0.026 Uiso 1 1 calc R U . . .
C16_3 C 0.3079(2) 0.1561(2) 0.44537(18) 0.0223(14) Uani 1 1 d . . . . .
H16_3 H 0.309287 0.128541 0.442993 0.027 Uiso 1 1 calc R U . . .
N1_3 N 0.47091(16) 0.03167(16) 0.60453(13) 0.0149(11) Uani 1 1 d . . . . .
N2_3 N 0.27922(18) 0.21854(18) 0.42732(14) 0.0193(12) Uani 1 1 d . . . . .
C1_4 C 0.4501(2) 0.4845(2) 0.29845(17) 0.0210(14) Uani 1 1 d . . . . .
H1_4 H 0.449787 0.512195 0.296981 0.025 Uiso 1 1 calc R U . . .
C2_4 C 0.4274(2) 0.4635(2) 0.27610(18) 0.0240(15) Uani 1 1 d . . . . .
H2_4 H 0.412535 0.476996 0.259793 0.029 Uiso 1 1 calc R U . . .
C3_4 C 0.4261(2) 0.4217(2) 0.27746(17) 0.0179(13) Uani 1 1 d . . . . .
C4_4 C 0.4508(2) 0.4032(2) 0.30242(17) 0.0201(14) Uani 1 1 d . . . . .
H4_4 H 0.452039 0.375505 0.303843 0.024 Uiso 1 1 calc R U . . .
C5_4 C 0.4728(2) 0.4266(2) 0.32450(17) 0.0193(13) Uani 1 1 d . . . . .
H5_4 H 0.487932 0.414013 0.341165 0.023 Uiso 1 1 calc R U . . .
C6_4 C 0.4015(2) 0.3976(2) 0.25465(16) 0.0180(13) Uani 1 1 d . . . . .
C7_4 C 0.4165(2) 0.3615(2) 0.24076(17) 0.0200(14) Uani 1 1 d . . . . .
H7_4 H 0.442141 0.353005 0.246249 0.024 Uiso 1 1 calc R U . . .
C8_4 C 0.3936(2) 0.3394(2) 0.21949(18) 0.0220(14) Uani 1 1 d . . . . .
H8_4 H 0.404106 0.315979 0.210446 0.026 Uiso 1 1 calc R U . . .
C9_4 C 0.3544(2) 0.3508(2) 0.21067(17) 0.0183(13) Uani 1 1 d . . . . .
C10_4 C 0.3394(2) 0.3865(2) 0.22486(17) 0.0186(13) Uani 1 1 d . . . . .
H10_4 H 0.313503 0.394647 0.219827 0.022 Uiso 1 1 calc R U . . .
C11_4 C 0.3628(2) 0.4094(2) 0.24614(17) 0.0191(13) Uani 1 1 d . . . . .
H11_4 H 0.352600 0.433127 0.254925 0.023 Uiso 1 1 calc R U . . .
C12_4 C 0.3305(2) 0.3257(2) 0.18754(16) 0.0178(13) Uani 1 1 d . . . . .
C13_4 C 0.3490(2) 0.3049(2) 0.16168(17) 0.0202(14) Uani 1 1 d . . . . .
H13_4 H 0.376508 0.306763 0.158829 0.024 Uiso 1 1 calc R U . . .
C14_4 C 0.3265(2) 0.2810(2) 0.13980(16) 0.0192(13) Uani 1 1 d . . . . .
H14_4 H 0.339394 0.267205 0.122505 0.023 Uiso 1 1 calc R U . . .
C15_4 C 0.2686(2) 0.2974(2) 0.16828(16) 0.0186(13) Uani 1 1 d . . . . .
H15_4 H 0.241151 0.294451 0.170963 0.022 Uiso 1 1 calc R U . . .
C16_4 C 0.2891(2) 0.3224(2) 0.19062(17) 0.0209(14) Uani 1 1 d . . . . .
H16_4 H 0.275402 0.336502 0.207249 0.025 Uiso 1 1 calc R U . . .
N1_4 N 0.47328(17) 0.46748(17) 0.32282(14) 0.0173(11) Uani 1 1 d . . . . .
N2_4 N 0.28662(16) 0.27732(17) 0.14309(14) 0.0168(11) Uani 1 1 d . . . . .
C1_5 C 0.0155(2) 0.0494(2) 0.29436(17) 0.0211(14) Uani 1 1 d . . . . .
H1_5 H -0.012057 0.048376 0.291532 0.025 Uiso 1 1 calc R U . . .
C2_5 C 0.0371(2) 0.0723(2) 0.27243(17) 0.0204(14) Uani 1 1 d . . . . .
H2_5 H 0.024102 0.086057 0.255202 0.024 Uiso 1 1 calc R U . . .
C3_5 C 0.0789(2) 0.07529(19) 0.27552(17) 0.0155(12) Uani 1 1 d . . . . .
C4_5 C 0.0963(2) 0.0526(2) 0.30176(17) 0.0186(13) Uani 1 1 d . . . . .
H4_5 H 0.123826 0.052984 0.304775 0.022 Uiso 1 1 calc R U . . .
C5_5 C 0.0727(2) 0.0297(2) 0.32303(17) 0.0193(13) Uani 1 1 d . . . . .
H5_5 H 0.085008 0.014886 0.339987 0.023 Uiso 1 1 calc R U . . .
C6_5 C 0.1036(2) 0.0995(2) 0.25313(17) 0.0172(13) Uani 1 1 d . . . . .
C7_5 C 0.1428(2) 0.0885(2) 0.24558(18) 0.0199(14) Uani 1 1 d . . . . .
H7_5 H 0.153228 0.065114 0.254681 0.024 Uiso 1 1 calc R U . . .
C8_5 C 0.1662(2) 0.1118(2) 0.22485(17) 0.0194(13) Uani 1 1 d . . . . .
H8_5 H 0.192372 0.103942 0.220596 0.023 Uiso 1 1 calc R U . . .
C9_5 C 0.1518(2) 0.1469(2) 0.20994(19) 0.0196(14) Uani 1 1 d . . . . .
C10_5 C 0.1123(2) 0.1579(2) 0.21757(18) 0.0204(14) Uani 1 1 d . . . . .
H10_5 H 0.101860 0.181319 0.208404 0.024 Uiso 1 1 calc R U . . .
C11_5 C 0.0886(2) 0.1346(2) 0.23846(17) 0.0186(13) Uani 1 1 d . . . . .
H11_5 H 0.062368 0.142330 0.242812 0.022 Uiso 1 1 calc R U . . .
C12_5 C 0.1766(2) 0.1712(2) 0.18731(16) 0.0166(13) Uani 1 1 d . . . . .
C13_5 C 0.2186(2) 0.1731(2) 0.19106(17) 0.0195(13) Uani 1 1 d . . . . .
H13_5 H 0.231474 0.158738 0.208034 0.023 Uiso 1 1 calc R U . . .
C14_5 C 0.2402(2) 0.1968(2) 0.16894(16) 0.0188(13) Uani 1 1 d . . . . .
H14_5 H 0.267707 0.198326 0.171688 0.023 Uiso 1 1 calc R U . . .
C15_5 C 0.1835(2) 0.2162(2) 0.14011(17) 0.0186(13) Uani 1 1 d . . . . .
H15_5 H 0.171618 0.231227 0.123048 0.022 Uiso 1 1 calc R U . . .
C16_5 C 0.1594(2) 0.1931(2) 0.16071(17) 0.0185(13) Uani 1 1 d . . . . .
H16_5 H 0.131937 0.192035 0.156994 0.022 Uiso 1 1 calc R U . . .
N1_5 N 0.03197(16) 0.02814(17) 0.32011(14) 0.0142(11) Uani 1 1 d . . . . .
N2_5 N 0.22334(16) 0.21779(17) 0.14370(14) 0.0162(11) Uani 1 1 d . . . . .
C1_6 C 0.4877(2) 0.4511(2) 0.42191(17) 0.0201(14) Uani 1 1 d . . . . .
H1_6 H 0.515090 0.454269 0.424884 0.024 Uiso 1 1 calc R U . . .
C2_6 C 0.4674(2) 0.4280(2) 0.44508(18) 0.0229(15) Uani 1 1 d . . . . .
H2_6 H 0.480897 0.415703 0.462810 0.027 Uiso 1 1 calc R U . . .
C3_6 C 0.4257(2) 0.4235(2) 0.44147(17) 0.0180(13) Uani 1 1 d . . . . .
C4_6 C 0.4075(2) 0.4429(2) 0.41435(17) 0.0203(14) Uani 1 1 d . . . . .
H4_6 H 0.380006 0.441197 0.411288 0.024 Uiso 1 1 calc R U . . .
C5_6 C 0.4307(2) 0.4649(2) 0.39193(17) 0.0208(14) Uani 1 1 d . . . . .
H5_6 H 0.418110 0.477273 0.373707 0.025 Uiso 1 1 calc R U . . .
C6_6 C 0.4019(2) 0.3985(2) 0.46478(19) 0.0205(14) Uani 1 1 d . . . . .
C7_6 C 0.4176(2) 0.3627(2) 0.4771(2) 0.0280(17) Uani 1 1 d . . . . .
H7_6 H 0.443626 0.355442 0.471491 0.034 Uiso 1 1 calc R U . . .
C8_6 C 0.3952(2) 0.3379(2) 0.4976(2) 0.0280(17) Uani 1 1 d . . . . .
H8_6 H 0.405768 0.313831 0.505248 0.034 Uiso 1 1 calc R U . . .
C9_6 C 0.3565(2) 0.3491(2) 0.50688(17) 0.0211(14) Uani 1 1 d . . . . .
C10_6 C 0.3406(2) 0.3844(2) 0.49473(19) 0.0244(15) Uani 1 1 d . . . . .
H10_6 H 0.314681 0.391654 0.500649 0.029 Uiso 1 1 calc R U . . .
C11_6 C 0.3626(2) 0.4091(2) 0.47402(18) 0.0219(14) Uani 1 1 d . . . . .
H11_6 H 0.351550 0.432768 0.466078 0.026 Uiso 1 1 calc R U . . .
C12_6 C 0.3324(2) 0.3222(2) 0.52891(17) 0.0189(13) Uani 1 1 d . . . . .
C13_6 C 0.3504(2) 0.3020(2) 0.55636(17) 0.0205(14) Uani 1 1 d . . . . .
H13_6 H 0.377631 0.304530 0.560310 0.025 Uiso 1 1 calc R U . . .
C14_6 C 0.3274(2) 0.2786(2) 0.57721(17) 0.0207(14) Uani 1 1 d . . . . .
H14_6 H 0.339404 0.266471 0.595790 0.025 Uiso 1 1 calc R U . . .
C15_6 C 0.2714(2) 0.2894(2) 0.54504(17) 0.0227(15) Uani 1 1 d . . . . .
H15_6 H 0.244720 0.283938 0.540397 0.027 Uiso 1 1 calc R U . . .
C16_6 C 0.2921(2) 0.3151(2) 0.52356(17) 0.0208(14) Uani 1 1 d . . . . .
H16_6 H 0.278866 0.327549 0.505692 0.025 Uiso 1 1 calc R U . . .
N1_6 N 0.47060(15) 0.46924(16) 0.39529(13) 0.0124(10) Uani 1 1 d . . . . .
N2_6 N 0.28827(17) 0.27243(17) 0.57197(13) 0.0167(11) Uani 1 1 d . . . . .
C1_8 C 0.2407(2) 0.1902(2) 0.54924(16) 0.0237(15) Uani 1 1 d . . . . .
H1_8 H 0.268466 0.189604 0.548571 0.028 Uiso 1 1 calc R U . . .
C2_8 C 0.2196(2) 0.1653(2) 0.52716(17) 0.0234(15) Uani 1 1 d . . . . .
H2_8 H 0.233170 0.148198 0.512545 0.028 Uiso 1 1 calc R U . . .
C3_8 C 0.1777(2) 0.1664(2) 0.52738(18) 0.0202(14) Uani 1 1 d . . . . .
C4_8 C 0.1595(2) 0.1928(2) 0.55092(17) 0.0204(14) Uani 1 1 d . . . . .
H4_8 H 0.131805 0.194274 0.552189 0.024 Uiso 1 1 calc R U . . .
C5_8 C 0.1828(2) 0.2163(2) 0.57202(17) 0.0203(14) Uani 1 1 d . . . . .
H5_8 H 0.170314 0.233575 0.587161 0.024 Uiso 1 1 calc R U . . .
C6_8 C 0.1531(2) 0.1410(2) 0.50488(17) 0.0201(14) Uani 1 1 d . . . . .
C7_8 C 0.1650(2) 0.1023(2) 0.49601(19) 0.0243(15) Uani 1 1 d . . . . .
H7_8 H 0.189029 0.092291 0.504156 0.029 Uiso 1 1 calc R U . . .
C8_8 C 0.1413(2) 0.0788(2) 0.47523(19) 0.0224(14) Uani 1 1 d . . . . .
H8_8 H 0.149084 0.052779 0.470333 0.027 Uiso 1 1 calc R U . . .
C9_8 C 0.1058(2) 0.0939(2) 0.46153(18) 0.0230(15) Uani 1 1 d . . . . .
C10_8 C 0.0938(2) 0.1330(2) 0.47160(18) 0.0242(15) Uani 1 1 d . . . . .
H10_8 H 0.069625 0.143333 0.463879 0.029 Uiso 1 1 calc R U . . .
C11_8 C 0.1174(2) 0.1554(2) 0.49250(18) 0.0235(15) Uani 1 1 d . . . . .
H11_8 H 0.109185 0.181013 0.498500 0.028 Uiso 1 1 calc R U . . .
C12_8 C 0.0800(2) 0.0709(2) 0.43857(16) 0.0179(13) Uani 1 1 d . . . . .
C13_8 C 0.0738(2) 0.0297(2) 0.44210(17) 0.0209(14) Uani 1 1 d . . . . .
H13_8 H 0.085784 0.015496 0.459586 0.025 Uiso 1 1 calc R U . . .
C14_8 C 0.0488(2) 0.0105(2) 0.41844(17) 0.0207(14) Uani 1 1 d . . . . .
H14_8 H 0.044500 -0.016801 0.420922 0.025 Uiso 1 1 calc R U . . .
C15_8 C 0.0366(2) 0.0689(2) 0.38972(16) 0.0181(13) Uani 1 1 d . . . . .
H15_8 H 0.024204 0.082332 0.372014 0.022 Uiso 1 1 calc R U . . .
C16_8 C 0.0604(2) 0.0904(2) 0.41226(17) 0.0206(14) Uani 1 1 d . . . . .
H16_8 H 0.063177 0.117915 0.409692 0.025 Uiso 1 1 calc R U . . .
N1_8 N 0.22316(17) 0.21474(18) 0.57114(14) 0.0194(12) Uani 1 1 d . . . . .
N2_8 N 0.03109(15) 0.02913(16) 0.39273(13) 0.0129(10) Uani 1 1 d . . . . .
C1_9 C 0.0344(2) 0.4309(2) 0.60740(17) 0.0203(14) Uani 1 1 d . . . . .
H1_9 H 0.020746 0.418352 0.624943 0.024 Uiso 1 1 calc R U . . .
C2_9 C 0.0574(2) 0.4078(2) 0.58563(17) 0.0185(13) Uani 1 1 d . . . . .
H2_9 H 0.058831 0.380241 0.588656 0.022 Uiso 1 1 calc R U . . .
C3_9 C 0.0782(2) 0.4256(2) 0.55951(16) 0.0153(12) Uani 1 1 d . . . . .
C4_9 C 0.0749(2) 0.4673(2) 0.55684(17) 0.0208(14) Uani 1 1 d . . . . .
H4_9 H 0.088632 0.480726 0.539832 0.025 Uiso 1 1 calc R U . . .
C5_9 C 0.0515(2) 0.4883(2) 0.57916(16) 0.0198(13) Uani 1 1 d . . . . .
H5_9 H 0.049633 0.515882 0.576962 0.024 Uiso 1 1 calc R U . . .
C6_9 C 0.1030(2) 0.4018(2) 0.53590(17) 0.0163(13) Uani 1 1 d . . . . .
C7_9 C 0.1406(2) 0.4163(2) 0.52556(17) 0.0216(14) Uani 1 1 d . . . . .
H7_9 H 0.149299 0.441324 0.532574 0.026 Uiso 1 1 calc R U . . .
C8_9 C 0.1647(2) 0.3927(2) 0.50464(17) 0.0191(14) Uani 1 1 d . . . . .
H8_9 H 0.189320 0.402303 0.497416 0.023 Uiso 1 1 calc R U . . .
C9_9 C 0.1521(2) 0.3547(2) 0.49453(17) 0.0190(13) Uani 1 1 d . . . . .
C10_9 C 0.1144(2) 0.3410(2) 0.50446(18) 0.0235(15) Uani 1 1 d . . . . .
H10_9 H 0.105555 0.316220 0.496894 0.028 Uiso 1 1 calc R U . . .
C11_9 C 0.0900(2) 0.3637(2) 0.52545(18) 0.0217(14) Uani 1 1 d . . . . .
H11_9 H 0.065402 0.353889 0.532511 0.026 Uiso 1 1 calc R U . . .
C12_9 C 0.1778(2) 0.3298(2) 0.47173(16) 0.0160(13) Uani 1 1 d . . . . .
C13_9 C 0.2030(2) 0.3476(2) 0.44807(17) 0.0208(14) Uani 1 1 d . . . . .
H13_9 H 0.205146 0.375224 0.446827 0.025 Uiso 1 1 calc R U . . .
C14_9 C 0.2249(2) 0.3232(2) 0.42627(17) 0.0217(14) Uani 1 1 d . . . . .
H14_9 H 0.241653 0.335191 0.410418 0.026 Uiso 1 1 calc R U . . .
C15_9 C 0.1988(2) 0.2658(2) 0.45075(18) 0.0243(15) Uani 1 1 d . . . . .
H15_9 H 0.197335 0.238054 0.451915 0.029 Uiso 1 1 calc R U . . .
C16_9 C 0.1764(2) 0.2883(2) 0.47301(18) 0.0252(16) Uani 1 1 d . . . . .
H16_9 H 0.160377 0.275631 0.488972 0.030 Uiso 1 1 calc R U . . .
N1_9 N 0.03126(17) 0.46995(16) 0.60411(13) 0.0146(11) Uani 1 1 d . . . . .
N2_9 N 0.22289(17) 0.28268(17) 0.42728(14) 0.0170(11) Uani 1 1 d . . . . .
B1_10 B 0.5007(3) 0.2912(2) 0.1181(2) 0.0232(15) Uani 1 1 d . . . . .
B2_10 B 0.5013(3) 0.2908(2) 0.07259(19) 0.0217(15) Uani 1 1 d . . . . .
B3_10 B 0.5444(2) 0.2761(2) 0.0963(2) 0.0221(15) Uani 1 1 d . . . . .
B4_10 B 0.5274(3) 0.2496(2) 0.1326(2) 0.0227(15) Uani 1 1 d . . . . .
B5_10 B 0.4577(3) 0.2741(2) 0.0949(2) 0.0227(15) Uani 1 1 d . . . . .
B6_10 B 0.4743(3) 0.2481(3) 0.1319(2) 0.0250(16) Uani 1 1 d . . . . .
B7_10 B 0.4586(2) 0.2209(2) 0.0953(2) 0.0210(15) Uani 1 1 d . . . . .
B8_10 B 0.5027(3) 0.2055(2) 0.11872(19) 0.0218(15) Uani 1 1 d . . . . .
B9_10 B 0.5458(2) 0.2227(2) 0.09623(19) 0.0192(14) Uani 1 1 d . . . . .
B10_10 B 0.5295(2) 0.2486(3) 0.0590(2) 0.0225(15) Uani 1 1 d . . . . .
B11_10 B 0.4756(2) 0.2467(3) 0.0585(2) 0.0227(15) Uani 1 1 d . . . . .
B12_10 B 0.5036(2) 0.2048(2) 0.0735(2) 0.0218(15) Uani 1 1 d . . . . .
Cl1_10 Cl 0.49827(6) 0.33721(5) 0.14222(4) 0.0265(4) Uani 1 1 d . . . . .
Cl2_10 Cl 0.41258(5) 0.30168(5) 0.09245(4) 0.0253(4) Uani 1 1 d . . . . .
Cl3_10 Cl 0.49696(6) 0.33594(5) 0.04776(4) 0.0248(3) Uani 1 1 d . . . . .
Cl4_10 Cl 0.59020(5) 0.30331(6) 0.09753(5) 0.0281(4) Uani 1 1 d . . . . .
Cl5_10 Cl 0.44539(5) 0.24787(6) 0.17005(4) 0.0256(4) Uani 1 1 d . . . . .
Cl6_10 Cl 0.55559(6) 0.24999(6) 0.17146(4) 0.0268(4) Uani 1 1 d . . . . .
Cl7_10 Cl 0.59112(5) 0.19453(6) 0.09563(5) 0.0267(4) Uani 1 1 d . . . . .
Cl8_10 Cl 0.55878(6) 0.24902(6) 0.02125(5) 0.0279(4) Uani 1 1 d . . . . .
Cl9_10 Cl 0.50738(6) 0.15970(5) 0.04879(5) 0.0259(4) Uani 1 1 d . . . . .
Cl10_10 Cl 0.45015(6) 0.24436(6) 0.01844(4) 0.0267(4) Uani 1 1 d . . . . .
Cl11_10 Cl 0.41297(5) 0.19433(5) 0.09574(5) 0.0275(4) Uani 1 1 d . . . . .
Cl12_10 Cl 0.50321(6) 0.16038(5) 0.14363(4) 0.0266(4) Uani 1 1 d . . . . .
B1_11 B 0.2598(3) 0.5335(3) 0.1055(2) 0.0259(16) Uani 1 1 d . . . . .
B2_11 B 0.2179(3) 0.5014(3) 0.1012(2) 0.0228(15) Uani 1 1 d . . . . .
B3_11 B 0.2193(3) 0.5361(3) 0.1356(2) 0.0240(16) Uani 1 1 d . . . . .
B4_11 B 0.2702(3) 0.5396(2) 0.1499(2) 0.0235(16) Uani 1 1 d . . . . .
B5_11 B 0.2997(2) 0.5070(3) 0.1245(2) 0.0230(15) Uani 1 1 d . . . . .
B6_11 B 0.2679(3) 0.4829(3) 0.0945(2) 0.0253(16) Uani 1 1 d . . . . .
B7_11 B 0.2317(3) 0.4529(3) 0.1174(2) 0.0246(16) Uani 1 1 d . . . . .
B8_11 B 0.2827(3) 0.4568(2) 0.1320(2) 0.0210(15) Uani 1 1 d . . . . .
B9_11 B 0.2844(3) 0.4921(3) 0.1662(2) 0.0226(15) Uani 1 1 d . . . . .
B10_11 B 0.2351(2) 0.5102(3) 0.1729(2) 0.0223(15) Uani 1 1 d . . . . .
B11_11 B 0.2029(2) 0.4864(3) 0.1429(2) 0.0243(16) Uani 1 1 d . . . . .
B12_11 B 0.2427(2) 0.4586(2) 0.1615(2) 0.0207(15) Uani 1 1 d . . . . .
Cl1_11 Cl 0.26752(6) 0.57295(6) 0.07526(5) 0.0323(4) Uani 1 1 d . . . . .
Cl2_11 Cl 0.18628(6) 0.57825(6) 0.13659(5) 0.0322(4) Uani 1 1 d . . . . .
Cl3_11 Cl 0.28982(7) 0.58478(6) 0.16746(5) 0.0363(5) Uani 1 1 d . . . . .
Cl4_11 Cl 0.35058(6) 0.51722(7) 0.11420(5) 0.0365(5) Uani 1 1 d . . . . .
Cl5_11 Cl 0.28588(7) 0.46829(7) 0.05343(5) 0.0365(5) Uani 1 1 d . . . . .
Cl6_11 Cl 0.18307(5) 0.50624(6) 0.06654(4) 0.0273(4) Uani 1 1 d . . . . .
Cl7_11 Cl 0.21198(6) 0.40810(6) 0.10005(5) 0.0330(4) Uani 1 1 d . . . . .
Cl8_11 Cl 0.31477(6) 0.41378(6) 0.13005(5) 0.0302(4) Uani 1 1 d . . . . .
Cl9_11 Cl 0.31931(5) 0.48675(6) 0.20061(5) 0.0261(4) Uani 1 1 d . . . . .
Cl10_11 Cl 0.21767(6) 0.52186(6) 0.21480(5) 0.0323(4) Uani 1 1 d . . . . .
Cl11_11 Cl 0.15221(6) 0.47532(7) 0.15450(5) 0.0334(4) Uani 1 1 d . . . . .
Cl12_11 Cl 0.23335(5) 0.41937(5) 0.19168(5) 0.0258(4) Uani 1 1 d . . . . .
B1_12 B 0.5024(3) 0.2776(2) 0.3510(2) 0.0269(17) Uani 1 1 d . . . . .
B2_12 B 0.4574(3) 0.2580(3) 0.3658(2) 0.0275(17) Uani 1 1 d . . . . .
B3_12 B 0.4803(3) 0.2985(3) 0.3877(2) 0.0269(17) Uani 1 1 d . . . . .
B4_12 B 0.4956(3) 0.2249(3) 0.3517(2) 0.0260(16) Uani 1 1 d . . . . .
B5_12 B 0.5327(3) 0.2908(3) 0.3868(2) 0.0288(17) Uani 1 1 d . . . . .
B6_12 B 0.5425(3) 0.2447(3) 0.3646(2) 0.0294(18) Uani 1 1 d . . . . .
B7_12 B 0.5439(3) 0.2455(3) 0.4097(2) 0.0312(18) Uani 1 1 d . . . . .
B8_12 B 0.5208(3) 0.2051(2) 0.3877(2) 0.0261(16) Uani 1 1 d . . . . .
B9_12 B 0.5055(3) 0.2792(3) 0.4246(2) 0.0291(18) Uani 1 1 d . . . . .
B10_12 B 0.4679(3) 0.2127(3) 0.3897(2) 0.0277(17) Uani 1 1 d . . . . .
B11_12 B 0.4588(3) 0.2585(3) 0.4112(2) 0.0302(18) Uani 1 1 d . . . . .
B12_12 B 0.4979(3) 0.2261(3) 0.4256(2) 0.0290(17) Uani 1 1 d . . . . .
Cl1_12 Cl 0.50592(7) 0.30461(6) 0.31153(5) 0.0358(5) Uani 1 1 d . . . . .
Cl2_12 Cl 0.41213(7) 0.26495(7) 0.34176(6) 0.0385(5) Uani 1 1 d . . . . .
Cl3_12 Cl 0.45883(6) 0.34749(6) 0.38708(5) 0.0335(4) Uani 1 1 d . . . . .
Cl4_12 Cl 0.49016(7) 0.19586(6) 0.31324(5) 0.0367(5) Uani 1 1 d . . . . .
Cl5_12 Cl 0.56754(7) 0.33111(6) 0.38509(7) 0.0438(5) Uani 1 1 d . . . . .
Cl6_12 Cl 0.58522(6) 0.23713(6) 0.33800(6) 0.0369(5) Uani 1 1 d . . . . .
Cl7_12 Cl 0.58994(7) 0.24047(7) 0.43213(6) 0.0425(5) Uani 1 1 d . . . . .
Cl8_12 Cl 0.54181(7) 0.15594(6) 0.38725(5) 0.0338(4) Uani 1 1 d . . . . .
Cl9_12 Cl 0.43292(7) 0.17245(7) 0.39074(6) 0.0442(5) Uani 1 1 d . . . . .
Cl10_12 Cl 0.41409(7) 0.26431(8) 0.43634(6) 0.0459(6) Uani 1 1 d . . . . .
Cl11_12 Cl 0.51217(7) 0.30706(7) 0.46247(6) 0.0429(5) Uani 1 1 d . . . . .
Cl12_12 Cl 0.49360(7) 0.19942(7) 0.46445(5) 0.0426(5) Uani 1 1 d . . . . .
B1_13 B 0.2642(2) 0.5123(3) 0.3284(2) 0.0219(15) Uani 1 1 d . . . . .
B2_13 B 0.2589(3) 0.4608(2) 0.3385(2) 0.0229(15) Uani 1 1 d . . . . .
B3_13 B 0.2981(2) 0.4886(2) 0.3562(2) 0.0202(15) Uani 1 1 d . . . . .
B4_13 B 0.2795(2) 0.5378(2) 0.36585(19) 0.0183(14) Uani 1 1 d . . . . .
B5_13 B 0.2283(2) 0.5395(2) 0.3529(2) 0.0214(15) Uani 1 1 d . . . . .
B6_13 B 0.2155(2) 0.4906(2) 0.3362(2) 0.0209(15) Uani 1 1 d . . . . .
B7_13 B 0.2013(2) 0.5037(3) 0.3789(2) 0.0243(16) Uani 1 1 d . . . . .
B8_13 B 0.2413(2) 0.5328(2) 0.3970(2) 0.0209(15) Uani 1 1 d . . . . .
B9_13 B 0.2361(2) 0.4808(2) 0.4073(2) 0.0219(15) Uani 1 1 d . . . . .
B10_13 B 0.2845(2) 0.5018(2) 0.39896(19) 0.0208(14) Uani 1 1 d . . . . .
B11_13 B 0.2721(2) 0.4536(2) 0.3823(2) 0.0200(15) Uani 1 1 d . . . . .
B12_13 B 0.2202(2) 0.4547(3) 0.3692(2) 0.0205(15) Uani 1 1 d . . . . .
Cl1_13 Cl 0.27790(6) 0.52635(6) 0.28619(4) 0.0284(4) Uani 1 1 d . . . . .
Cl2_13 Cl 0.17912(5) 0.48550(5) 0.30317(4) 0.0245(4) Uani 1 1 d . . . . .
Cl3_13 Cl 0.20558(6) 0.58381(6) 0.33725(5) 0.0308(4) Uani 1 1 d . . . . .
Cl4_13 Cl 0.31091(6) 0.58126(5) 0.36443(5) 0.0262(4) Uani 1 1 d . . . . .
Cl5_13 Cl 0.34883(5) 0.48079(6) 0.34302(5) 0.0269(4) Uani 1 1 d . . . . .
Cl6_13 Cl 0.26854(5) 0.42213(5) 0.30711(4) 0.0239(3) Uani 1 1 d . . . . .
Cl7_13 Cl 0.29459(5) 0.40888(5) 0.39776(4) 0.0259(4) Uani 1 1 d . . . . .
Cl8_13 Cl 0.19009(5) 0.41105(5) 0.37124(4) 0.0237(3) Uani 1 1 d . . . . .
Cl9_13 Cl 0.32035(5) 0.50770(5) 0.43289(4) 0.0241(4) Uani 1 1 d . . . . .
Cl10_13 Cl 0.22184(6) 0.46461(6) 0.44891(5) 0.0291(4) Uani 1 1 d . . . . .
Cl11_13 Cl 0.23228(6) 0.57011(5) 0.42846(5) 0.0269(4) Uani 1 1 d . . . . .
Cl12_13 Cl 0.15064(5) 0.51213(6) 0.39063(5) 0.0282(4) Uani 1 1 d . . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C1 O1 1.412(9) . ?
C1 H1A 0.9600 . ?
C1 H1B 0.9600 . ?
C1 H1C 0.9600 . ?
C6 O6 1.458(9) . ?
C6 H6A 0.9600 . ?
C6 H6B 0.9600 . ?
C6 H6C 0.9600 . ?
C9 O2 1.428(9) . ?
C9 H9A 0.9600 . ?
C9 H9B 0.9600 . ?
C9 H9C 0.9600 . ?
C12 O3 1.430(9) . ?
C12 H12A 0.9600 . ?
C12 H12B 0.9600 . ?
C12 H12C 0.9600 . ?
C13 O4 1.447(10) . ?
C13 H13A 0.9600 . ?
C13 H13B 0.9600 . ?
C13 H13C 0.9600 . ?
C14 O5 1.425(10) . ?
C14 H14A 0.9600 . ?
C14 H14B 0.9600 . ?
C14 H14C 0.9600 . ?
C16 O8 1.370(13) . ?
C16 H16A 0.9600 . ?
C16 H16B 0.9600 . ?
C16 H16C 0.9600 . ?
C17 O7 1.444(9) . ?
C17 H17A 0.9600 . ?
C17 H17B 0.9600 . ?
C17 H17C 0.9600 . ?
Cu1 N1_3 2.034(5) . ?
Cu1 N1_3 2.034(5) 2_655 ?
Cu1 N1_1 2.036(5) . ?
Cu1 N1_1 2.036(5) 2_655 ?
Cu2 N2_2 2.034(5) 2_565 ?
Cu2 N2_2 2.034(5) . ?
Cu2 N1_9 2.043(5) 2_565 ?
Cu2 N1_9 2.043(5) . ?
Cu3 N1_4 2.010(6) 2_665 ?
Cu3 N1_4 2.010(5) . ?
Cu3 N1_6 2.016(5) 2_665 ?
Cu3 N1_6 2.016(5) . ?
Cu4 N1_5 2.020(5) 2 ?
Cu4 N1_5 2.020(5) . ?
Cu4 N2_8 2.023(5) . ?
Cu4 N2_8 2.023(5) 2 ?
Cu5 N2_9 2.021(6) . ?
Cu5 N2_1 2.025(5) 7_554 ?
Cu5 N2_3 2.027(6) . ?
Cu5 N1_2 2.029(5) 7_554 ?
Cu5 O3 2.422(5) . ?
Cu6 N1_8 2.027(6) 7_554 ?
Cu6 N2_5 2.028(5) . ?
Cu6 N2_4 2.032(5) . ?
Cu6 N2_6 2.044(5) 7_554 ?
Cu6 O5 2.411(5) . ?
C1_1 N1_1 1.350(9) . ?
C1_1 C2_1 1.375(9) . ?
C1_1 H1_1 0.9300 . ?
C2_1 C3_1 1.397(9) . ?
C2_1 H2_1 0.9300 . ?
C3_1 C4_1 1.388(10) . ?
C3_1 C6_1 1.495(9) . ?
C4_1 C5_1 1.392(9) . ?
C4_1 H4_1 0.9300 . ?
C5_1 N1_1 1.339(8) . ?
C5_1 H5_1 0.9300 . ?
C6_1 C11_1 1.385(10) . ?
C6_1 C7_1 1.386(10) . ?
C7_1 C8_1 1.405(9) . ?
C7_1 H7_1 0.9300 . ?
C8_1 C9_1 1.394(10) . ?
C8_1 H8_1 0.9300 . ?
C9_1 C10_1 1.403(10) . ?
C9_1 C12_1 1.492(9) . ?
C10_1 C11_1 1.412(9) . ?
C10_1 H10_1 0.9300 . ?
C11_1 H11_1 0.9300 . ?
C12_1 C16_1 1.387(9) . ?
C12_1 C13_1 1.391(10) . ?
C13_1 C14_1 1.376(9) . ?
C13_1 H13_1 0.9300 . ?
C14_1 N2_1 1.339(9) . ?
C14_1 H14_1 0.9300 . ?
C15_1 N2_1 1.361(8) . ?
C15_1 C16_1 1.363(9) . ?
C15_1 H15_1 0.9300 . ?
C16_1 H16_1 0.9300 . ?
C1_2 N1_2 1.344(9) . ?
C1_2 C2_2 1.374(9) . ?
C1_2 H1_2 0.9300 . ?
C2_2 C3_2 1.402(10) . ?
C2_2 H2_2 0.9300 . ?
C3_2 C4_2 1.368(10) . ?
C3_2 C6_2 1.491(9) . ?
C4_2 C5_2 1.383(9) . ?
C4_2 H4_2 0.9300 . ?
C5_2 N1_2 1.351(9) . ?
C5_2 H5_2 0.9300 . ?
C6_2 C11_2 1.402(10) . ?
C6_2 C7_2 1.411(10) . ?
C7_2 C8_2 1.392(9) . ?
C7_2 H7_2 0.9300 . ?
C8_2 C9_2 1.386(9) . ?
C8_2 H8_2 0.9300 . ?
C9_2 C10_2 1.393(10) . ?
C9_2 C12_2 1.503(9) . ?
C10_2 C11_2 1.405(9) . ?
C10_2 H10_2 0.9300 . ?
C11_2 H11_2 0.9300 . ?
C12_2 C13_2 1.386(10) . ?
C12_2 C16_2 1.413(9) . ?
C13_2 C14_2 1.385(9) . ?
C13_2 H13_2 0.9300 . ?
C14_2 N2_2 1.341(9) . ?
C14_2 H14_2 0.9300 . ?
C15_2 N2_2 1.352(9) . ?
C15_2 C16_2 1.367(9) . ?
C15_2 H15_2 0.9300 . ?
C16_2 H16_2 0.9300 . ?
C1_3 N1_3 1.346(9) . ?
C1_3 C2_3 1.358(10) . ?
C1_3 H1_3 0.9300 . ?
C2_3 C3_3 1.417(10) . ?
C2_3 H2_3 0.9300 . ?
C3_3 C4_3 1.377(10) . ?
C3_3 C6_3 1.473(9) . ?
C4_3 C5_3 1.385(9) . ?
C4_3 H4_3 0.9300 . ?
C5_3 N1_3 1.335(9) . ?
C5_3 H5_3 0.9300 . ?
C6_3 C11_3 1.391(11) . ?
C6_3 C7_3 1.402(10) . ?
C7_3 C8_3 1.402(9) . ?
C7_3 H7_3 0.9300 . ?
C8_3 C9_3 1.399(10) . ?
C8_3 H8_3 0.9300 . ?
C9_3 C10_3 1.391(11) . ?
C9_3 C12_3 1.488(9) . ?
C10_3 C11_3 1.398(10) . ?
C10_3 H10_3 0.9300 . ?
C11_3 H11_3 0.9300 . ?
C12_3 C13_3 1.384(10) . ?
C12_3 C16_3 1.409(10) . ?
C13_3 C14_3 1.390(10) . ?
C13_3 H13_3 0.9300 . ?
C14_3 N2_3 1.345(9) . ?
C14_3 H14_3 0.9300 . ?
C15_3 N2_3 1.359(9) . ?
C15_3 C16_3 1.377(9) . ?
C15_3 H15_3 0.9300 . ?
C16_3 H16_3 0.9300 . ?
C1_4 C2_4 1.361(10) . ?
C1_4 N1_4 1.360(9) . ?
C1_4 H1_4 0.9300 . ?
C2_4 C3_4 1.400(10) . ?
C2_4 H2_4 0.9300 . ?
C3_4 C4_4 1.427(9) . ?
C3_4 C6_4 1.464(9) . ?
C4_4 C5_4 1.384(9) . ?
C4_4 H4_4 0.9300 . ?
C5_4 N1_4 1.371(9) . ?
C5_4 H5_4 0.9300 . ?
C6_4 C11_4 1.397(10) . ?
C6_4 C7_4 1.417(10) . ?
C7_4 C8_4 1.356(9) . ?
C7_4 H7_4 0.9300 . ?
C8_4 C9_4 1.412(10) . ?
C8_4 H8_4 0.9300 . ?
C9_4 C10_4 1.411(10) . ?
C9_4 C12_4 1.475(9) . ?
C10_4 C11_4 1.382(9) . ?
C10_4 H10_4 0.9300 . ?
C11_4 H11_4 0.9300 . ?
C12_4 C13_4 1.383(10) . ?
C12_4 C16_4 1.396(10) . ?
C13_4 C14_4 1.398(9) . ?
C13_4 H13_4 0.9300 . ?
C14_4 N2_4 1.346(9) . ?
C14_4 H14_4 0.9300 . ?
C15_4 N2_4 1.342(9) . ?
C15_4 C16_4 1.395(9) . ?
C15_4 H15_4 0.9300 . ?
C16_4 H16_4 0.9300 . ?
C1_5 N1_5 1.358(9) . ?
C1_5 C2_5 1.363(9) . ?
C1_5 H1_5 0.9300 . ?
C2_5 C3_5 1.407(9) . ?
C2_5 H2_5 0.9300 . ?
C3_5 C4_5 1.410(9) . ?
C3_5 C6_5 1.458(9) . ?
C4_5 C5_5 1.383(9) . ?
C4_5 H4_5 0.9300 . ?
C5_5 N1_5 1.370(8) . ?
C5_5 H5_5 0.9300 . ?
C6_5 C7_5 1.394(10) . ?
C6_5 C11_5 1.404(9) . ?
C7_5 C8_5 1.374(9) . ?
C7_5 H7_5 0.9300 . ?
C8_5 C9_5 1.401(10) . ?
C8_5 H8_5 0.9300 . ?
C9_5 C10_5 1.406(9) . ?
C9_5 C12_5 1.465(9) . ?
C10_5 C11_5 1.385(9) . ?
C10_5 H10_5 0.9300 . ?
C11_5 H11_5 0.9300 . ?
C12_5 C16_5 1.405(9) . ?
C12_5 C13_5 1.415(10) . ?
C13_5 C14_5 1.383(9) . ?
C13_5 H13_5 0.9300 . ?
C14_5 N2_5 1.342(9) . ?
C14_5 H14_5 0.9300 . ?
C15_5 N2_5 1.343(9) . ?
C15_5 C16_5 1.383(9) . ?
C15_5 H15_5 0.9300 . ?
C16_5 H16_5 0.9300 . ?
C1_6 N1_6 1.342(8) . ?
C1_6 C2_6 1.376(9) . ?
C1_6 H1_6 0.9300 . ?
C2_6 C3_6 1.412(10) . ?
C2_6 H2_6 0.9300 . ?
C3_6 C4_6 1.393(9) . ?
C3_6 C6_6 1.476(9) . ?
C4_6 C5_6 1.388(9) . ?
C4_6 H4_6 0.9300 . ?
C5_6 N1_6 1.351(8) . ?
C5_6 H5_6 0.9300 . ?
C6_6 C7_6 1.397(10) . ?
C6_6 C11_6 1.410(9) . ?
C7_6 C8_6 1.382(10) . ?
C7_6 H7_6 0.9300 . ?
C8_6 C9_6 1.396(10) . ?
C8_6 H8_6 0.9300 . ?
C9_6 C10_6 1.384(10) . ?
C9_6 C12_6 1.488(9) . ?
C10_6 C11_6 1.375(9) . ?
C10_6 H10_6 0.9300 . ?
C11_6 H11_6 0.9300 . ?
C12_6 C16_6 1.388(10) . ?
C12_6 C13_6 1.411(9) . ?
C13_6 C14_6 1.373(9) . ?
C13_6 H13_6 0.9300 . ?
C14_6 N2_6 1.340(9) . ?
C14_6 H14_6 0.9300 . ?
C15_6 N2_6 1.331(9) . ?
C15_6 C16_6 1.392(9) . ?
C15_6 H15_6 0.9300 . ?
C16_6 H16_6 0.9300 . ?
C1_8 N1_8 1.329(9) . ?
C1_8 C2_8 1.398(9) . ?
C1_8 H1_8 0.9300 . ?
C2_8 C3_8 1.403(10) . ?
C2_8 H2_8 0.9300 . ?
C3_8 C4_8 1.419(10) . ?
C3_8 C6_8 1.482(9) . ?
C4_8 C5_8 1.385(9) . ?
C4_8 H4_8 0.9300 . ?
C5_8 N1_8 1.354(9) . ?
C5_8 H5_8 0.9300 . ?
C6_8 C11_8 1.379(10) . ?
C6_8 C7_8 1.397(10) . ?
C7_8 C8_8 1.385(10) . ?
C7_8 H7_8 0.9300 . ?
C8_8 C9_8 1.400(10) . ?
C8_8 H8_8 0.9300 . ?
C9_8 C10_8 1.426(10) . ?
C9_8 C12_8 1.469(9) . ?
C10_8 C11_8 1.367(10) . ?
C10_8 H10_8 0.9300 . ?
C11_8 H11_8 0.9300 . ?
C12_8 C16_8 1.390(10) . ?
C12_8 C13_8 1.402(10) . ?
C13_8 C14_8 1.409(9) . ?
C13_8 H13_8 0.9300 . ?
C14_8 N2_8 1.331(8) . ?
C14_8 H14_8 0.9300 . ?
C15_8 N2_8 1.348(8) . ?
C15_8 C16_8 1.395(9) . ?
C15_8 H15_8 0.9300 . ?
C16_8 H16_8 0.9300 . ?
C1_9 N1_9 1.318(8) . ?
C1_9 C2_9 1.390(9) . ?
C1_9 H1_9 0.9300 . ?
C2_9 C3_9 1.380(9) . ?
C2_9 H2_9 0.9300 . ?
C3_9 C4_9 1.402(9) . ?
C3_9 C6_9 1.481(9) . ?
C4_9 C5_9 1.372(9) . ?
C4_9 H4_9 0.9300 . ?
C5_9 N1_9 1.344(8) . ?
C5_9 H5_9 0.9300 . ?
C6_9 C7_9 1.409(10) . ?
C6_9 C11_9 1.409(9) . ?
C7_9 C8_9 1.399(9) . ?
C7_9 H7_9 0.9300 . ?
C8_9 C9_9 1.397(10) . ?
C8_9 H8_9 0.9300 . ?
C9_9 C10_9 1.397(10) . ?
C9_9 C12_9 1.499(9) . ?
C10_9 C11_9 1.390(9) . ?
C10_9 H10_9 0.9300 . ?
C11_9 H11_9 0.9300 . ?
C12_9 C16_9 1.391(10) . ?
C12_9 C13_9 1.393(9) . ?
C13_9 C14_9 1.394(9) . ?
C13_9 H13_9 0.9300 . ?
C14_9 N2_9 1.359(9) . ?
C14_9 H14_9 0.9300 . ?
C15_9 N2_9 1.352(9) . ?
C15_9 C16_9 1.379(9) . ?
C15_9 H15_9 0.9300 . ?
C16_9 H16_9 0.9300 . ?
B1_10 B4_10 1.751(12) . ?
B1_10 B3_10 1.769(12) . ?
B1_10 B6_10 1.779(12) . ?
B1_10 B2_10 1.797(11) . ?
B1_10 B5_10 1.802(12) . ?
B1_10 Cl1_10 1.811(8) . ?
B2_10 B10_10 1.784(12) . ?
B2_10 B3_10 1.789(12) . ?
B2_10 B11_10 1.796(12) . ?
B2_10 B5_10 1.795(12) . ?
B2_10 Cl3_10 1.807(8) . ?
B3_10 B4_10 1.777(11) . ?
B3_10 Cl4_10 1.785(8) . ?
B3_10 B9_10 1.789(11) . ?
B3_10 B10_10 1.809(12) . ?
B4_10 B6_10 1.778(13) . ?
B4_10 B8_10 1.779(12) . ?
B4_10 Cl6_10 1.800(8) . ?
B4_10 B9_10 1.805(11) . ?
B5_10 Cl2_10 1.772(9) . ?
B5_10 B7_10 1.779(11) . ?
B5_10 B6_10 1.788(12) . ?
B5_10 B11_10 1.808(12) . ?
B6_10 B7_10 1.785(12) . ?
B6_10 B8_10 1.789(12) . ?
B6_10 Cl5_10 1.792(8) . ?
B7_10 Cl11_10 1.769(8) . ?
B7_10 B11_10 1.783(12) . ?
B7_10 B12_10 1.814(12) . ?
B7_10 B8_10 1.817(12) . ?
B8_10 B12_10 1.784(11) . ?
B8_10 B9_10 1.789(12) . ?
B8_10 Cl12_10 1.802(8) . ?
B9_10 B12_10 1.778(11) . ?
B9_10 Cl7_10 1.785(8) . ?
B9_10 B10_10 1.792(11) . ?
B10_10 Cl8_10 1.781(8) . ?
B10_10 B12_10 1.798(12) . ?
B10_10 B11_10 1.806(12) . ?
B11_10 B12_10 1.787(12) . ?
B11_10 Cl10_10 1.797(8) . ?
B12_10 Cl9_10 1.803(8) . ?
B1_11 B5_11 1.768(12) . ?
B1_11 B6_11 1.770(13) . ?
B1_11 B2_11 1.776(12) . ?
B1_11 B4_11 1.797(12) . ?
B1_11 Cl1_11 1.800(9) . ?
B1_11 B3_11 1.806(13) . ?
B2_11 B3_11 1.788(11) . ?
B2_11 B11_11 1.793(12) . ?
B2_11 Cl6_11 1.804(8) . ?
B2_11 B6_11 1.804(12) . ?
B2_11 B7_11 1.804(12) . ?
B3_11 B11_11 1.776(12) . ?
B3_11 B10_11 1.788(12) . ?
B3_11 Cl2_11 1.793(9) . ?
B3_11 B4_11 1.799(12) . ?
B4_11 B5_11 1.779(12) . ?
B4_11 B9_11 1.782(12) . ?
B4_11 B10_11 1.784(12) . ?
B4_11 Cl3_11 1.788(8) . ?
B5_11 Cl4_11 1.786(8) . ?
B5_11 B6_11 1.786(12) . ?
B5_11 B9_11 1.792(12) . ?
B5_11 B8_11 1.798(12) . ?
B6_11 B8_11 1.790(12) . ?
B6_11 Cl5_11 1.796(8) . ?
B6_11 B7_11 1.813(12) . ?
B7_11 Cl7_11 1.778(8) . ?
B7_11 B11_11 1.788(12) . ?
B7_11 B12_11 1.789(11) . ?
B7_11 B8_11 1.806(12) . ?
B8_11 B12_11 1.775(12) . ?
B8_11 B9_11 1.793(11) . ?
B8_11 Cl8_11 1.797(9) . ?
B9_11 B10_11 1.781(12) . ?
B9_11 Cl9_11 1.800(8) . ?
B9_11 B12_11 1.800(11) . ?
B10_11 B11_11 1.788(12) . ?
B10_11 Cl10_11 1.796(8) . ?
B10_11 B12_11 1.802(12) . ?
B11_11 B12_11 1.782(12) . ?
B11_11 Cl11_11 1.796(8) . ?
B12_11 Cl12_11 1.800(8) . ?
B1_12 B2_12 1.742(13) . ?
B1_12 B3_12 1.770(13) . ?
B1_12 B4_12 1.781(12) . ?
B1_12 B5_12 1.795(13) . ?
B1_12 Cl1_12 1.804(8) . ?
B1_12 B6_12 1.818(13) . ?
B2_12 B3_12 1.780(13) . ?
B2_12 B4_12 1.781(13) . ?
B2_12 B11_12 1.794(13) . ?
B2_12 Cl2_12 1.803(9) . ?
B2_12 B10_12 1.821(12) . ?
B3_12 B5_12 1.775(13) . ?
B3_12 B11_12 1.780(13) . ?
B3_12 Cl3_12 1.791(9) . ?
B3_12 B9_12 1.803(13) . ?
B4_12 B6_12 1.781(13) . ?
B4_12 B8_12 1.782(12) . ?
B4_12 B10_12 1.808(12) . ?
B4_12 Cl4_12 1.810(8) . ?
B5_12 Cl5_12 1.784(9) . ?
B5_12 B9_12 1.793(13) . ?
B5_12 B6_12 1.804(12) . ?
B5_12 B7_12 1.805(14) . ?
B6_12 B8_12 1.766(13) . ?
B6_12 B7_12 1.783(13) . ?
B6_12 Cl6_12 1.790(10) . ?
B7_12 B8_12 1.783(13) . ?
B7_12 B12_12 1.785(14) . ?
B7_12 Cl7_12 1.785(9) . ?
B7_12 B9_12 1.809(13) . ?
B8_12 Cl8_12 1.789(9) . ?
B8_12 B10_12 1.791(13) . ?
B8_12 B12_12 1.823(13) . ?
B9_12 Cl11_12 1.775(9) . ?
B9_12 B11_12 1.791(13) . ?
B9_12 B12_12 1.795(14) . ?
B10_12 B11_12 1.781(13) . ?
B10_12 Cl9_12 1.787(9) . ?
B10_12 B12_12 1.793(13) . ?
B11_12 B12_12 1.793(13) . ?
B11_12 Cl10_12 1.804(9) . ?
B12_12 Cl12_12 1.782(8) . ?
B1_13 B3_13 1.767(11) . ?
B1_13 B2_13 1.777(12) . ?
B1_13 B4_13 1.783(11) . ?
B1_13 B5_13 1.791(12) . ?
B1_13 Cl1_13 1.791(8) . ?
B1_13 B6_13 1.809(11) . ?
B2_13 B3_13 1.755(12) . ?
B2_13 B6_13 1.762(12) . ?
B2_13 B12_13 1.784(12) . ?
B2_13 B11_13 1.802(11) . ?
B2_13 Cl6_13 1.821(9) . ?
B3_13 B11_13 1.788(11) . ?
B3_13 Cl5_13 1.793(8) . ?
B3_13 B4_13 1.803(11) . ?
B3_13 B10_13 1.805(11) . ?
B4_13 B8_13 1.782(11) . ?
B4_13 B10_13 1.785(11) . ?
B4_13 B5_13 1.789(11) . ?
B4_13 Cl4_13 1.796(8) . ?
B5_13 Cl3_13 1.776(8) . ?
B5_13 B8_13 1.810(11) . ?
B5_13 B7_13 1.819(12) . ?
B5_13 B6_13 1.818(11) . ?
B6_13 B12_13 1.779(12) . ?
B6_13 Cl2_13 1.791(8) . ?
B6_13 B7_13 1.807(12) . ?
B7_13 Cl12_13 1.782(8) . ?
B7_13 B9_13 1.789(12) . ?
B7_13 B12_13 1.798(12) . ?
B7_13 B8_13 1.803(12) . ?
B8_13 B10_13 1.782(12) . ?
B8_13 Cl11_13 1.784(8) . ?
B8_13 B9_13 1.796(11) . ?
B9_13 Cl10_13 1.793(8) . ?
B9_13 B10_13 1.795(11) . ?
B9_13 B11_13 1.804(12) . ?
B9_13 B12_13 1.820(11) . ?
B10_13 B11_13 1.790(11) . ?
B10_13 Cl9_13 1.809(8) . ?
B11_13 Cl7_13 1.783(8) . ?
B11_13 B12_13 1.814(11) . ?
B12_13 Cl8_13 1.777(8) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O1 C1 H1A 109.5 . . ?
O1 C1 H1B 109.5 . . ?
H1A C1 H1B 109.5 . . ?
O1 C1 H1C 109.5 . . ?
H1A C1 H1C 109.5 . . ?
H1B C1 H1C 109.5 . . ?
O6 C6 H6A 109.5 . . ?
O6 C6 H6B 109.5 . . ?
H6A C6 H6B 109.5 . . ?
O6 C6 H6C 109.5 . . ?
H6A C6 H6C 109.5 . . ?
H6B C6 H6C 109.5 . . ?
O2 C9 H9A 109.5 . . ?
O2 C9 H9B 109.5 . . ?
H9A C9 H9B 109.5 . . ?
O2 C9 H9C 109.5 . . ?
H9A C9 H9C 109.5 . . ?
H9B C9 H9C 109.5 . . ?
O3 C12 H12A 109.5 . . ?
O3 C12 H12B 109.5 . . ?
H12A C12 H12B 109.5 . . ?
O3 C12 H12C 109.5 . . ?
H12A C12 H12C 109.5 . . ?
H12B C12 H12C 109.5 . . ?
O4 C13 H13A 109.5 . . ?
O4 C13 H13B 109.5 . . ?
H13A C13 H13B 109.5 . . ?
O4 C13 H13C 109.5 . . ?
H13A C13 H13C 109.5 . . ?
H13B C13 H13C 109.5 . . ?
O5 C14 H14A 109.5 . . ?
O5 C14 H14B 109.5 . . ?
H14A C14 H14B 109.5 . . ?
O5 C14 H14C 109.5 . . ?
H14A C14 H14C 109.5 . . ?
H14B C14 H14C 109.5 . . ?
O8 C16 H16A 109.5 . . ?
O8 C16 H16B 109.5 . . ?
H16A C16 H16B 109.5 . . ?
O8 C16 H16C 109.5 . . ?
H16A C16 H16C 109.5 . . ?
H16B C16 H16C 109.5 . . ?
O7 C17 H17A 109.5 . . ?
O7 C17 H17B 109.5 . . ?
H17A C17 H17B 109.5 . . ?
O7 C17 H17C 109.5 . . ?
H17A C17 H17C 109.5 . . ?
H17B C17 H17C 109.5 . . ?
N1_3 Cu1 N1_3 90.1(3) . 2_655 ?
N1_3 Cu1 N1_1 89.9(2) . . ?
N1_3 Cu1 N1_1 179.0(2) 2_655 . ?
N1_3 Cu1 N1_1 179.0(2) . 2_655 ?
N1_3 Cu1 N1_1 89.9(2) 2_655 2_655 ?
N1_1 Cu1 N1_1 90.1(3) . 2_655 ?
N2_2 Cu2 N2_2 90.1(3) 2_565 . ?
N2_2 Cu2 N1_9 89.7(2) 2_565 2_565 ?
N2_2 Cu2 N1_9 177.7(2) . 2_565 ?
N2_2 Cu2 N1_9 177.7(2) 2_565 . ?
N2_2 Cu2 N1_9 89.7(2) . . ?
N1_9 Cu2 N1_9 90.6(3) 2_565 . ?
N1_4 Cu3 N1_4 89.0(3) 2_665 . ?
N1_4 Cu3 N1_6 90.6(2) 2_665 2_665 ?
N1_4 Cu3 N1_6 176.9(2) . 2_665 ?
N1_4 Cu3 N1_6 176.9(2) 2_665 . ?
N1_4 Cu3 N1_6 90.6(2) . . ?
N1_6 Cu3 N1_6 89.9(3) 2_665 . ?
N1_5 Cu4 N1_5 89.8(3) 2 . ?
N1_5 Cu4 N2_8 178.7(2) 2 . ?
N1_5 Cu4 N2_8 90.3(2) . . ?
N1_5 Cu4 N2_8 90.3(2) 2 2 ?
N1_5 Cu4 N2_8 178.7(2) . 2 ?
N2_8 Cu4 N2_8 89.6(3) . 2 ?
N2_9 Cu5 N2_1 175.7(2) . 7_554 ?
N2_9 Cu5 N2_3 89.8(2) . . ?
N2_1 Cu5 N2_3 89.3(2) 7_554 . ?
N2_9 Cu5 N1_2 89.7(2) . 7_554 ?
N2_1 Cu5 N1_2 91.3(2) 7_554 7_554 ?
N2_3 Cu5 N1_2 178.4(2) . 7_554 ?
N2_9 Cu5 O3 92.1(2) . . ?
N2_1 Cu5 O3 92.2(2) 7_554 . ?
N2_3 Cu5 O3 90.8(2) . . ?
N1_2 Cu5 O3 87.6(2) 7_554 . ?
N1_8 Cu6 N2_5 174.5(2) 7_554 . ?
N1_8 Cu6 N2_4 88.8(2) 7_554 . ?
N2_5 Cu6 N2_4 91.5(2) . . ?
N1_8 Cu6 N2_6 91.4(2) 7_554 7_554 ?
N2_5 Cu6 N2_6 88.5(2) . 7_554 ?
N2_4 Cu6 N2_6 178.0(2) . 7_554 ?
N1_8 Cu6 O5 91.7(2) 7_554 . ?
N2_5 Cu6 O5 93.8(2) . . ?
N2_4 Cu6 O5 88.5(2) . . ?
N2_6 Cu6 O5 89.5(2) 7_554 . ?
C12 O3 Cu5 136.2(5) . . ?
C14 O5 Cu6 135.1(5) . . ?
N1_1 C1_1 C2_1 121.9(6) . . ?
N1_1 C1_1 H1_1 119.0 . . ?
C2_1 C1_1 H1_1 119.0 . . ?
C1_1 C2_1 C3_1 120.7(6) . . ?
C1_1 C2_1 H2_1 119.6 . . ?
C3_1 C2_1 H2_1 119.6 . . ?
C4_1 C3_1 C2_1 116.5(6) . . ?
C4_1 C3_1 C6_1 122.5(6) . . ?
C2_1 C3_1 C6_1 121.0(6) . . ?
C3_1 C4_1 C5_1 120.4(6) . . ?
C3_1 C4_1 H4_1 119.8 . . ?
C5_1 C4_1 H4_1 119.8 . . ?
N1_1 C5_1 C4_1 121.9(6) . . ?
N1_1 C5_1 H5_1 119.0 . . ?
C4_1 C5_1 H5_1 119.0 . . ?
C11_1 C6_1 C7_1 121.2(6) . . ?
C11_1 C6_1 C3_1 119.0(6) . . ?
C7_1 C6_1 C3_1 119.8(6) . . ?
C6_1 C7_1 C8_1 120.1(7) . . ?
C6_1 C7_1 H7_1 119.9 . . ?
C8_1 C7_1 H7_1 119.9 . . ?
C9_1 C8_1 C7_1 119.6(7) . . ?
C9_1 C8_1 H8_1 120.2 . . ?
C7_1 C8_1 H8_1 120.2 . . ?
C8_1 C9_1 C10_1 119.8(6) . . ?
C8_1 C9_1 C12_1 120.9(6) . . ?
C10_1 C9_1 C12_1 119.3(6) . . ?
C9_1 C10_1 C11_1 120.3(7) . . ?
C9_1 C10_1 H10_1 119.9 . . ?
C11_1 C10_1 H10_1 119.9 . . ?
C6_1 C11_1 C10_1 119.0(7) . . ?
C6_1 C11_1 H11_1 120.5 . . ?
C10_1 C11_1 H11_1 120.5 . . ?
C16_1 C12_1 C13_1 117.6(6) . . ?
C16_1 C12_1 C9_1 120.5(6) . . ?
C13_1 C12_1 C9_1 121.9(6) . . ?
C14_1 C13_1 C12_1 119.3(7) . . ?
C14_1 C13_1 H13_1 120.3 . . ?
C12_1 C13_1 H13_1 120.3 . . ?
N2_1 C14_1 C13_1 123.0(7) . . ?
N2_1 C14_1 H14_1 118.5 . . ?
C13_1 C14_1 H14_1 118.5 . . ?
N2_1 C15_1 C16_1 122.4(6) . . ?
N2_1 C15_1 H15_1 118.8 . . ?
C16_1 C15_1 H15_1 118.8 . . ?
C15_1 C16_1 C12_1 120.1(6) . . ?
C15_1 C16_1 H16_1 120.0 . . ?
C12_1 C16_1 H16_1 120.0 . . ?
C5_1 N1_1 C1_1 118.5(6) . . ?
C5_1 N1_1 Cu1 121.9(5) . . ?
C1_1 N1_1 Cu1 119.4(4) . . ?
C14_1 N2_1 C15_1 117.4(6) . . ?
C14_1 N2_1 Cu5 123.6(5) . 7 ?
C15_1 N2_1 Cu5 118.5(4) . 7 ?
N1_2 C1_2 C2_2 124.9(7) . . ?
N1_2 C1_2 H1_2 117.6 . . ?
C2_2 C1_2 H1_2 117.6 . . ?
C1_2 C2_2 C3_2 118.0(7) . . ?
C1_2 C2_2 H2_2 121.0 . . ?
C3_2 C2_2 H2_2 121.0 . . ?
C4_2 C3_2 C2_2 117.7(6) . . ?
C4_2 C3_2 C6_2 120.8(6) . . ?
C2_2 C3_2 C6_2 121.5(6) . . ?
C3_2 C4_2 C5_2 120.9(7) . . ?
C3_2 C4_2 H4_2 119.5 . . ?
C5_2 C4_2 H4_2 119.5 . . ?
N1_2 C5_2 C4_2 122.1(7) . . ?
N1_2 C5_2 H5_2 119.0 . . ?
C4_2 C5_2 H5_2 119.0 . . ?
C11_2 C6_2 C7_2 119.5(6) . . ?
C11_2 C6_2 C3_2 121.4(6) . . ?
C7_2 C6_2 C3_2 119.0(6) . . ?
C8_2 C7_2 C6_2 120.3(7) . . ?
C8_2 C7_2 H7_2 119.9 . . ?
C6_2 C7_2 H7_2 119.9 . . ?
C9_2 C8_2 C7_2 119.6(7) . . ?
C9_2 C8_2 H8_2 120.2 . . ?
C7_2 C8_2 H8_2 120.2 . . ?
C8_2 C9_2 C10_2 121.2(6) . . ?
C8_2 C9_2 C12_2 119.5(6) . . ?
C10_2 C9_2 C12_2 119.3(6) . . ?
C9_2 C10_2 C11_2 119.6(6) . . ?
C9_2 C10_2 H10_2 120.2 . . ?
C11_2 C10_2 H10_2 120.2 . . ?
C6_2 C11_2 C10_2 119.8(6) . . ?
C6_2 C11_2 H11_2 120.1 . . ?
C10_2 C11_2 H11_2 120.1 . . ?
C13_2 C12_2 C16_2 116.8(6) . . ?
C13_2 C12_2 C9_2 121.9(6) . . ?
C16_2 C12_2 C9_2 121.4(6) . . ?
C14_2 C13_2 C12_2 120.3(6) . . ?
C14_2 C13_2 H13_2 119.8 . . ?
C12_2 C13_2 H13_2 119.8 . . ?
N2_2 C14_2 C13_2 122.1(6) . . ?
N2_2 C14_2 H14_2 118.9 . . ?
C13_2 C14_2 H14_2 118.9 . . ?
N2_2 C15_2 C16_2 122.4(7) . . ?
N2_2 C15_2 H15_2 118.8 . . ?
C16_2 C15_2 H15_2 118.8 . . ?
C15_2 C16_2 C12_2 119.9(7) . . ?
C15_2 C16_2 H16_2 120.0 . . ?
C12_2 C16_2 H16_2 120.0 . . ?
C1_2 N1_2 C5_2 116.4(6) . . ?
C1_2 N1_2 Cu5 124.5(5) . 7 ?
C5_2 N1_2 Cu5 118.7(4) . 7 ?
C14_2 N2_2 C15_2 118.4(6) . . ?
C14_2 N2_2 Cu2 121.1(5) . . ?
C15_2 N2_2 Cu2 119.9(5) . . ?
N1_3 C1_3 C2_3 122.8(7) . . ?
N1_3 C1_3 H1_3 118.6 . . ?
C2_3 C1_3 H1_3 118.6 . . ?
C1_3 C2_3 C3_3 119.8(7) . . ?
C1_3 C2_3 H2_3 120.1 . . ?
C3_3 C2_3 H2_3 120.1 . . ?
C4_3 C3_3 C2_3 116.5(6) . . ?
C4_3 C3_3 C6_3 121.0(6) . . ?
C2_3 C3_3 C6_3 122.6(6) . . ?
C3_3 C4_3 C5_3 120.6(7) . . ?
C3_3 C4_3 H4_3 119.7 . . ?
C5_3 C4_3 H4_3 119.7 . . ?
N1_3 C5_3 C4_3 121.9(7) . . ?
N1_3 C5_3 H5_3 119.0 . . ?
C4_3 C5_3 H5_3 119.0 . . ?
C11_3 C6_3 C7_3 118.2(6) . . ?
C11_3 C6_3 C3_3 118.2(6) . . ?
C7_3 C6_3 C3_3 123.6(7) . . ?
C6_3 C7_3 C8_3 120.7(7) . . ?
C6_3 C7_3 H7_3 119.7 . . ?
C8_3 C7_3 H7_3 119.7 . . ?
C9_3 C8_3 C7_3 120.1(7) . . ?
C9_3 C8_3 H8_3 120.0 . . ?
C7_3 C8_3 H8_3 120.0 . . ?
C10_3 C9_3 C8_3 119.7(6) . . ?
C10_3 C9_3 C12_3 118.1(7) . . ?
C8_3 C9_3 C12_3 122.2(7) . . ?
C9_3 C10_3 C11_3 119.6(7) . . ?
C9_3 C10_3 H10_3 120.2 . . ?
C11_3 C10_3 H10_3 120.2 . . ?
C6_3 C11_3 C10_3 121.8(7) . . ?
C6_3 C11_3 H11_3 119.1 . . ?
C10_3 C11_3 H11_3 119.1 . . ?
C13_3 C12_3 C16_3 117.5(7) . . ?
C13_3 C12_3 C9_3 122.1(7) . . ?
C16_3 C12_3 C9_3 120.4(6) . . ?
C12_3 C13_3 C14_3 120.0(7) . . ?
C12_3 C13_3 H13_3 120.0 . . ?
C14_3 C13_3 H13_3 120.0 . . ?
N2_3 C14_3 C13_3 122.8(7) . . ?
N2_3 C14_3 H14_3 118.6 . . ?
C13_3 C14_3 H14_3 118.6 . . ?
N2_3 C15_3 C16_3 123.1(7) . . ?
N2_3 C15_3 H15_3 118.4 . . ?
C16_3 C15_3 H15_3 118.4 . . ?
C15_3 C16_3 C12_3 119.2(7) . . ?
C15_3 C16_3 H16_3 120.4 . . ?
C12_3 C16_3 H16_3 120.4 . . ?
C5_3 N1_3 C1_3 118.4(6) . . ?
C5_3 N1_3 Cu1 118.0(5) . . ?
C1_3 N1_3 Cu1 123.5(5) . . ?
C14_3 N2_3 C15_3 117.3(6) . . ?
C14_3 N2_3 Cu5 122.0(5) . . ?
C15_3 N2_3 Cu5 120.0(5) . . ?
C2_4 C1_4 N1_4 124.2(7) . . ?
C2_4 C1_4 H1_4 117.9 . . ?
N1_4 C1_4 H1_4 117.9 . . ?
C1_4 C2_4 C3_4 120.5(7) . . ?
C1_4 C2_4 H2_4 119.8 . . ?
C3_4 C2_4 H2_4 119.8 . . ?
C2_4 C3_4 C4_4 116.3(6) . . ?
C2_4 C3_4 C6_4 123.0(6) . . ?
C4_4 C3_4 C6_4 120.7(6) . . ?
C5_4 C4_4 C3_4 119.8(6) . . ?
C5_4 C4_4 H4_4 120.1 . . ?
C3_4 C4_4 H4_4 120.1 . . ?
N1_4 C5_4 C4_4 122.7(6) . . ?
N1_4 C5_4 H5_4 118.7 . . ?
C4_4 C5_4 H5_4 118.7 . . ?
C11_4 C6_4 C7_4 118.5(6) . . ?
C11_4 C6_4 C3_4 120.9(6) . . ?
C7_4 C6_4 C3_4 120.6(6) . . ?
C8_4 C7_4 C6_4 120.3(7) . . ?
C8_4 C7_4 H7_4 119.9 . . ?
C6_4 C7_4 H7_4 119.9 . . ?
C7_4 C8_4 C9_4 122.0(7) . . ?
C7_4 C8_4 H8_4 119.0 . . ?
C9_4 C8_4 H8_4 119.0 . . ?
C10_4 C9_4 C8_4 117.5(6) . . ?
C10_4 C9_4 C12_4 122.4(6) . . ?
C8_4 C9_4 C12_4 120.2(6) . . ?
C11_4 C10_4 C9_4 120.7(6) . . ?
C11_4 C10_4 H10_4 119.6 . . ?
C9_4 C10_4 H10_4 119.6 . . ?
C10_4 C11_4 C6_4 120.9(7) . . ?
C10_4 C11_4 H11_4 119.5 . . ?
C6_4 C11_4 H11_4 119.5 . . ?
C13_4 C12_4 C16_4 117.9(6) . . ?
C13_4 C12_4 C9_4 120.1(6) . . ?
C16_4 C12_4 C9_4 122.0(6) . . ?
C12_4 C13_4 C14_4 120.2(7) . . ?
C12_4 C13_4 H13_4 119.9 . . ?
C14_4 C13_4 H13_4 119.9 . . ?
N2_4 C14_4 C13_4 121.8(6) . . ?
N2_4 C14_4 H14_4 119.1 . . ?
C13_4 C14_4 H14_4 119.1 . . ?
N2_4 C15_4 C16_4 123.1(6) . . ?
N2_4 C15_4 H15_4 118.4 . . ?
C16_4 C15_4 H15_4 118.4 . . ?
C15_4 C16_4 C12_4 118.8(7) . . ?
C15_4 C16_4 H16_4 120.6 . . ?
C12_4 C16_4 H16_4 120.6 . . ?
C1_4 N1_4 C5_4 116.5(6) . . ?
C1_4 N1_4 Cu3 122.1(5) . . ?
C5_4 N1_4 Cu3 120.7(4) . . ?
C15_4 N2_4 C14_4 118.1(6) . . ?
C15_4 N2_4 Cu6 123.4(5) . . ?
C14_4 N2_4 Cu6 118.3(5) . . ?
N1_5 C1_5 C2_5 123.7(7) . . ?
N1_5 C1_5 H1_5 118.2 . . ?
C2_5 C1_5 H1_5 118.2 . . ?
C1_5 C2_5 C3_5 120.8(7) . . ?
C1_5 C2_5 H2_5 119.6 . . ?
C3_5 C2_5 H2_5 119.6 . . ?
C2_5 C3_5 C4_5 115.8(6) . . ?
C2_5 C3_5 C6_5 123.5(6) . . ?
C4_5 C3_5 C6_5 120.7(6) . . ?
C5_5 C4_5 C3_5 120.5(6) . . ?
C5_5 C4_5 H4_5 119.7 . . ?
C3_5 C4_5 H4_5 119.7 . . ?
N1_5 C5_5 C4_5 122.6(6) . . ?
N1_5 C5_5 H5_5 118.7 . . ?
C4_5 C5_5 H5_5 118.7 . . ?
C7_5 C6_5 C11_5 118.1(6) . . ?
C7_5 C6_5 C3_5 121.1(6) . . ?
C11_5 C6_5 C3_5 120.8(6) . . ?
C8_5 C7_5 C6_5 120.9(7) . . ?
C8_5 C7_5 H7_5 119.6 . . ?
C6_5 C7_5 H7_5 119.6 . . ?
C7_5 C8_5 C9_5 122.0(7) . . ?
C7_5 C8_5 H8_5 119.0 . . ?
C9_5 C8_5 H8_5 119.0 . . ?
C8_5 C9_5 C10_5 117.0(6) . . ?
C8_5 C9_5 C12_5 121.7(6) . . ?
C10_5 C9_5 C12_5 121.3(6) . . ?
C11_5 C10_5 C9_5 121.3(7) . . ?
C11_5 C10_5 H10_5 119.4 . . ?
C9_5 C10_5 H10_5 119.4 . . ?
C10_5 C11_5 C6_5 120.7(7) . . ?
C10_5 C11_5 H11_5 119.6 . . ?
C6_5 C11_5 H11_5 119.6 . . ?
C16_5 C12_5 C13_5 117.6(6) . . ?
C16_5 C12_5 C9_5 120.7(6) . . ?
C13_5 C12_5 C9_5 121.7(6) . . ?
C14_5 C13_5 C12_5 118.6(6) . . ?
C14_5 C13_5 H13_5 120.7 . . ?
C12_5 C13_5 H13_5 120.7 . . ?
N2_5 C14_5 C13_5 123.4(6) . . ?
N2_5 C14_5 H14_5 118.3 . . ?
C13_5 C14_5 H14_5 118.3 . . ?
N2_5 C15_5 C16_5 122.7(6) . . ?
N2_5 C15_5 H15_5 118.6 . . ?
C16_5 C15_5 H15_5 118.6 . . ?
C15_5 C16_5 C12_5 119.4(6) . . ?
C15_5 C16_5 H16_5 120.3 . . ?
C12_5 C16_5 H16_5 120.3 . . ?
C1_5 N1_5 C5_5 116.5(6) . . ?
C1_5 N1_5 Cu4 124.0(5) . . ?
C5_5 N1_5 Cu4 119.1(4) . . ?
C14_5 N2_5 C15_5 118.3(6) . . ?
C14_5 N2_5 Cu6 122.1(5) . . ?
C15_5 N2_5 Cu6 119.1(5) . . ?
N1_6 C1_6 C2_6 124.2(6) . . ?
N1_6 C1_6 H1_6 117.9 . . ?
C2_6 C1_6 H1_6 117.9 . . ?
C1_6 C2_6 C3_6 118.9(6) . . ?
C1_6 C2_6 H2_6 120.6 . . ?
C3_6 C2_6 H2_6 120.6 . . ?
C4_6 C3_6 C2_6 117.3(6) . . ?
C4_6 C3_6 C6_6 120.5(6) . . ?
C2_6 C3_6 C6_6 122.1(6) . . ?
C5_6 C4_6 C3_6 119.6(6) . . ?
C5_6 C4_6 H4_6 120.2 . . ?
C3_6 C4_6 H4_6 120.2 . . ?
N1_6 C5_6 C4_6 123.2(6) . . ?
N1_6 C5_6 H5_6 118.4 . . ?
C4_6 C5_6 H5_6 118.4 . . ?
C7_6 C6_6 C11_6 118.5(6) . . ?
C7_6 C6_6 C3_6 120.0(6) . . ?
C11_6 C6_6 C3_6 121.5(6) . . ?
C8_6 C7_6 C6_6 121.0(7) . . ?
C8_6 C7_6 H7_6 119.5 . . ?
C6_6 C7_6 H7_6 119.5 . . ?
C7_6 C8_6 C9_6 119.8(7) . . ?
C7_6 C8_6 H8_6 120.1 . . ?
C9_6 C8_6 H8_6 120.1 . . ?
C10_6 C9_6 C8_6 119.7(6) . . ?
C10_6 C9_6 C12_6 120.8(6) . . ?
C8_6 C9_6 C12_6 119.5(7) . . ?
C11_6 C10_6 C9_6 120.8(7) . . ?
C11_6 C10_6 H10_6 119.6 . . ?
C9_6 C10_6 H10_6 119.6 . . ?
C10_6 C11_6 C6_6 120.2(7) . . ?
C10_6 C11_6 H11_6 119.9 . . ?
C6_6 C11_6 H11_6 119.9 . . ?
C16_6 C12_6 C13_6 116.7(6) . . ?
C16_6 C12_6 C9_6 122.8(6) . . ?
C13_6 C12_6 C9_6 120.5(6) . . ?
C14_6 C13_6 C12_6 119.7(7) . . ?
C14_6 C13_6 H13_6 120.2 . . ?
C12_6 C13_6 H13_6 120.2 . . ?
N2_6 C14_6 C13_6 122.9(7) . . ?
N2_6 C14_6 H14_6 118.6 . . ?
C13_6 C14_6 H14_6 118.6 . . ?
N2_6 C15_6 C16_6 122.7(6) . . ?
N2_6 C15_6 H15_6 118.7 . . ?
C16_6 C15_6 H15_6 118.7 . . ?
C12_6 C16_6 C15_6 119.8(6) . . ?
C12_6 C16_6 H16_6 120.1 . . ?
C15_6 C16_6 H16_6 120.1 . . ?
C1_6 N1_6 C5_6 116.8(6) . . ?
C1_6 N1_6 Cu3 125.2(4) . . ?
C5_6 N1_6 Cu3 117.9(4) . . ?
C15_6 N2_6 C14_6 118.1(6) . . ?
C15_6 N2_6 Cu6 121.1(5) . 7 ?
C14_6 N2_6 Cu6 120.3(4) . 7 ?
N1_8 C1_8 C2_8 123.5(7) . . ?
N1_8 C1_8 H1_8 118.3 . . ?
C2_8 C1_8 H1_8 118.3 . . ?
C1_8 C2_8 C3_8 119.0(7) . . ?
C1_8 C2_8 H2_8 120.5 . . ?
C3_8 C2_8 H2_8 120.5 . . ?
C2_8 C3_8 C4_8 116.8(6) . . ?
C2_8 C3_8 C6_8 122.5(7) . . ?
C4_8 C3_8 C6_8 120.7(6) . . ?
C5_8 C4_8 C3_8 120.3(7) . . ?
C5_8 C4_8 H4_8 119.8 . . ?
C3_8 C4_8 H4_8 119.8 . . ?
N1_8 C5_8 C4_8 121.6(7) . . ?
N1_8 C5_8 H5_8 119.2 . . ?
C4_8 C5_8 H5_8 119.2 . . ?
C11_8 C6_8 C7_8 118.9(7) . . ?
C11_8 C6_8 C3_8 119.5(7) . . ?
C7_8 C6_8 C3_8 121.6(7) . . ?
C8_8 C7_8 C6_8 120.7(7) . . ?
C8_8 C7_8 H7_8 119.6 . . ?
C6_8 C7_8 H7_8 119.6 . . ?
C7_8 C8_8 C9_8 120.6(7) . . ?
C7_8 C8_8 H8_8 119.7 . . ?
C9_8 C8_8 H8_8 119.7 . . ?
C8_8 C9_8 C10_8 117.6(6) . . ?
C8_8 C9_8 C12_8 123.3(7) . . ?
C10_8 C9_8 C12_8 119.1(7) . . ?
C11_8 C10_8 C9_8 120.6(7) . . ?
C11_8 C10_8 H10_8 119.7 . . ?
C9_8 C10_8 H10_8 119.7 . . ?
C10_8 C11_8 C6_8 121.5(7) . . ?
C10_8 C11_8 H11_8 119.3 . . ?
C6_8 C11_8 H11_8 119.3 . . ?
C16_8 C12_8 C13_8 117.8(6) . . ?
C16_8 C12_8 C9_8 119.5(6) . . ?
C13_8 C12_8 C9_8 122.7(6) . . ?
C12_8 C13_8 C14_8 118.2(6) . . ?
C12_8 C13_8 H13_8 120.9 . . ?
C14_8 C13_8 H13_8 120.9 . . ?
N2_8 C14_8 C13_8 123.7(7) . . ?
N2_8 C14_8 H14_8 118.1 . . ?
C13_8 C14_8 H14_8 118.1 . . ?
N2_8 C15_8 C16_8 122.2(6) . . ?
N2_8 C15_8 H15_8 118.9 . . ?
C16_8 C15_8 H15_8 118.9 . . ?
C12_8 C16_8 C15_8 120.1(6) . . ?
C12_8 C16_8 H16_8 119.9 . . ?
C15_8 C16_8 H16_8 119.9 . . ?
C1_8 N1_8 C5_8 118.8(6) . . ?
C1_8 N1_8 Cu6 121.7(5) . 7 ?
C5_8 N1_8 Cu6 118.9(5) . 7 ?
C14_8 N2_8 C15_8 117.9(6) . . ?
C14_8 N2_8 Cu4 123.0(5) . . ?
C15_8 N2_8 Cu4 118.9(4) . . ?
N1_9 C1_9 C2_9 122.4(6) . . ?
N1_9 C1_9 H1_9 118.8 . . ?
C2_9 C1_9 H1_9 118.8 . . ?
C3_9 C2_9 C1_9 119.9(6) . . ?
C3_9 C2_9 H2_9 120.0 . . ?
C1_9 C2_9 H2_9 120.0 . . ?
C2_9 C3_9 C4_9 116.6(6) . . ?
C2_9 C3_9 C6_9 121.2(6) . . ?
C4_9 C3_9 C6_9 122.1(6) . . ?
C5_9 C4_9 C3_9 120.4(7) . . ?
C5_9 C4_9 H4_9 119.8 . . ?
C3_9 C4_9 H4_9 119.8 . . ?
N1_9 C5_9 C4_9 121.6(7) . . ?
N1_9 C5_9 H5_9 119.2 . . ?
C4_9 C5_9 H5_9 119.2 . . ?
C7_9 C6_9 C11_9 120.1(6) . . ?
C7_9 C6_9 C3_9 119.9(6) . . ?
C11_9 C6_9 C3_9 119.9(6) . . ?
C8_9 C7_9 C6_9 119.5(6) . . ?
C8_9 C7_9 H7_9 120.3 . . ?
C6_9 C7_9 H7_9 120.3 . . ?
C9_9 C8_9 C7_9 120.5(6) . . ?
C9_9 C8_9 H8_9 119.7 . . ?
C7_9 C8_9 H8_9 119.7 . . ?
C8_9 C9_9 C10_9 119.5(6) . . ?
C8_9 C9_9 C12_9 120.3(6) . . ?
C10_9 C9_9 C12_9 120.2(6) . . ?
C11_9 C10_9 C9_9 121.1(7) . . ?
C11_9 C10_9 H10_9 119.4 . . ?
C9_9 C10_9 H10_9 119.4 . . ?
C10_9 C11_9 C6_9 119.2(7) . . ?
C10_9 C11_9 H11_9 120.4 . . ?
C6_9 C11_9 H11_9 120.4 . . ?
C16_9 C12_9 C13_9 118.1(6) . . ?
C16_9 C12_9 C9_9 121.1(6) . . ?
C13_9 C12_9 C9_9 120.8(6) . . ?
C12_9 C13_9 C14_9 118.9(7) . . ?
C12_9 C13_9 H13_9 120.6 . . ?
C14_9 C13_9 H13_9 120.6 . . ?
N2_9 C14_9 C13_9 122.6(7) . . ?
N2_9 C14_9 H14_9 118.7 . . ?
C13_9 C14_9 H14_9 118.7 . . ?
N2_9 C15_9 C16_9 122.1(7) . . ?
N2_9 C15_9 H15_9 118.9 . . ?
C16_9 C15_9 H15_9 118.9 . . ?
C15_9 C16_9 C12_9 120.4(7) . . ?
C15_9 C16_9 H16_9 119.8 . . ?
C12_9 C16_9 H16_9 119.8 . . ?
C1_9 N1_9 C5_9 119.0(6) . . ?
C1_9 N1_9 Cu2 117.4(4) . . ?
C5_9 N1_9 Cu2 123.3(5) . . ?
C15_9 N2_9 C14_9 117.9(6) . . ?
C15_9 N2_9 Cu5 121.5(5) . . ?
C14_9 N2_9 Cu5 120.2(5) . . ?
B4_10 B1_10 B3_10 60.6(5) . . ?
B4_10 B1_10 B6_10 60.5(5) . . ?
B3_10 B1_10 B6_10 109.0(6) . . ?
B4_10 B1_10 B2_10 108.4(6) . . ?
B3_10 B1_10 B2_10 60.2(5) . . ?
B6_10 B1_10 B2_10 107.7(6) . . ?
B4_10 B1_10 B5_10 108.7(6) . . ?
B3_10 B1_10 B5_10 108.8(6) . . ?
B6_10 B1_10 B5_10 59.9(5) . . ?
B2_10 B1_10 B5_10 59.8(5) . . ?
B4_10 B1_10 Cl1_10 121.8(5) . . ?
B3_10 B1_10 Cl1_10 122.4(6) . . ?
B6_10 B1_10 Cl1_10 120.5(5) . . ?
B2_10 B1_10 Cl1_10 122.2(5) . . ?
B5_10 B1_10 Cl1_10 120.1(5) . . ?
B10_10 B2_10 B3_10 60.8(5) . . ?
B10_10 B2_10 B11_10 60.6(5) . . ?
B3_10 B2_10 B11_10 108.8(6) . . ?
B10_10 B2_10 B5_10 109.4(6) . . ?
B3_10 B2_10 B5_10 108.3(5) . . ?
B11_10 B2_10 B5_10 60.5(5) . . ?
B10_10 B2_10 B1_10 108.3(6) . . ?
B3_10 B2_10 B1_10 59.1(5) . . ?
B11_10 B2_10 B1_10 108.2(6) . . ?
B5_10 B2_10 B1_10 60.2(5) . . ?
B10_10 B2_10 Cl3_10 122.8(5) . . ?
B3_10 B2_10 Cl3_10 125.4(6) . . ?
B11_10 B2_10 Cl3_10 118.7(5) . . ?
B5_10 B2_10 Cl3_10 117.5(5) . . ?
B1_10 B2_10 Cl3_10 122.3(5) . . ?
B1_10 B3_10 B4_10 59.2(5) . . ?
B1_10 B3_10 Cl4_10 123.4(5) . . ?
B4_10 B3_10 Cl4_10 120.5(5) . . ?
B1_10 B3_10 B9_10 108.1(6) . . ?
B4_10 B3_10 B9_10 60.8(5) . . ?
Cl4_10 B3_10 B9_10 119.1(5) . . ?
B1_10 B3_10 B2_10 60.6(5) . . ?
B4_10 B3_10 B2_10 107.6(6) . . ?
Cl4_10 B3_10 B2_10 124.5(5) . . ?
B9_10 B3_10 B2_10 107.2(6) . . ?
B1_10 B3_10 B10_10 108.4(6) . . ?
B4_10 B3_10 B10_10 108.4(6) . . ?
Cl4_10 B3_10 B10_10 121.1(5) . . ?
B9_10 B3_10 B10_10 59.8(5) . . ?
B2_10 B3_10 B10_10 59.4(5) . . ?
B1_10 B4_10 B3_10 60.2(5) . . ?
B1_10 B4_10 B6_10 60.5(5) . . ?
B3_10 B4_10 B6_10 108.7(6) . . ?
B1_10 B4_10 B8_10 108.8(6) . . ?
B3_10 B4_10 B8_10 108.3(6) . . ?
B6_10 B4_10 B8_10 60.4(5) . . ?
B1_10 B4_10 Cl6_10 122.7(5) . . ?
B3_10 B4_10 Cl6_10 121.0(6) . . ?
B6_10 B4_10 Cl6_10 122.6(5) . . ?
B8_10 B4_10 Cl6_10 120.8(5) . . ?
B1_10 B4_10 B9_10 108.2(6) . . ?
B3_10 B4_10 B9_10 59.9(4) . . ?
B6_10 B4_10 B9_10 108.3(6) . . ?
B8_10 B4_10 B9_10 59.9(4) . . ?
Cl6_10 B4_10 B9_10 120.1(5) . . ?
Cl2_10 B5_10 B7_10 122.5(6) . . ?
Cl2_10 B5_10 B6_10 124.3(6) . . ?
B7_10 B5_10 B6_10 60.0(5) . . ?
Cl2_10 B5_10 B2_10 120.2(5) . . ?
B7_10 B5_10 B2_10 107.5(6) . . ?
B6_10 B5_10 B2_10 107.3(6) . . ?
Cl2_10 B5_10 B1_10 122.8(5) . . ?
B7_10 B5_10 B1_10 107.5(6) . . ?
B6_10 B5_10 B1_10 59.4(5) . . ?
B2_10 B5_10 B1_10 59.9(5) . . ?
Cl2_10 B5_10 B11_10 120.3(6) . . ?
B7_10 B5_10 B11_10 59.6(5) . . ?
B6_10 B5_10 B11_10 107.3(6) . . ?
B2_10 B5_10 B11_10 59.8(5) . . ?
B1_10 B5_10 B11_10 107.4(6) . . ?
B4_10 B6_10 B1_10 59.0(5) . . ?
B4_10 B6_10 B7_10 108.9(6) . . ?
B1_10 B6_10 B7_10 108.2(6) . . ?
B4_10 B6_10 B8_10 59.9(5) . . ?
B1_10 B6_10 B8_10 107.2(6) . . ?
B7_10 B6_10 B8_10 61.1(5) . . ?
B4_10 B6_10 B5_10 108.1(6) . . ?
B1_10 B6_10 B5_10 60.7(5) . . ?
B7_10 B6_10 B5_10 59.7(5) . . ?
B8_10 B6_10 B5_10 108.5(6) . . ?
B4_10 B6_10 Cl5_10 121.8(5) . . ?
B1_10 B6_10 Cl5_10 121.9(6) . . ?
B7_10 B6_10 Cl5_10 121.3(6) . . ?
B8_10 B6_10 Cl5_10 121.9(5) . . ?
B5_10 B6_10 Cl5_10 121.3(6) . . ?
Cl11_10 B7_10 B5_10 119.2(5) . . ?
Cl11_10 B7_10 B11_10 121.9(5) . . ?
B5_10 B7_10 B11_10 61.0(5) . . ?
Cl11_10 B7_10 B6_10 120.1(5) . . ?
B5_10 B7_10 B6_10 60.2(5) . . ?
B11_10 B7_10 B6_10 108.6(6) . . ?
Cl11_10 B7_10 B12_10 124.9(5) . . ?
B5_10 B7_10 B12_10 107.9(6) . . ?
B11_10 B7_10 B12_10 59.6(5) . . ?
B6_10 B7_10 B12_10 106.8(6) . . ?
Cl11_10 B7_10 B8_10 123.6(5) . . ?
B5_10 B7_10 B8_10 107.6(6) . . ?
B11_10 B7_10 B8_10 107.0(6) . . ?
B6_10 B7_10 B8_10 59.5(5) . . ?
B12_10 B7_10 B8_10 58.8(4) . . ?
B4_10 B8_10 B12_10 108.1(6) . . ?
B4_10 B8_10 B9_10 60.7(5) . . ?
B12_10 B8_10 B9_10 59.7(4) . . ?
B4_10 B8_10 B6_10 59.8(5) . . ?
B12_10 B8_10 B6_10 108.0(6) . . ?
B9_10 B8_10 B6_10 108.4(6) . . ?
B4_10 B8_10 Cl12_10 121.6(5) . . ?
B12_10 B8_10 Cl12_10 122.3(5) . . ?
B9_10 B8_10 Cl12_10 122.2(5) . . ?
B6_10 B8_10 Cl12_10 120.9(5) . . ?
B4_10 B8_10 B7_10 107.4(6) . . ?
B12_10 B8_10 B7_10 60.5(5) . . ?
B9_10 B8_10 B7_10 108.1(5) . . ?
B6_10 B8_10 B7_10 59.3(5) . . ?
Cl12_10 B8_10 B7_10 121.6(5) . . ?
B12_10 B9_10 Cl7_10 119.4(5) . . ?
B12_10 B9_10 B8_10 60.0(4) . . ?
Cl7_10 B9_10 B8_10 121.5(5) . . ?
B12_10 B9_10 B3_10 108.4(6) . . ?
Cl7_10 B9_10 B3_10 123.4(5) . . ?
B8_10 B9_10 B3_10 107.3(6) . . ?
B12_10 B9_10 B10_10 60.5(5) . . ?
Cl7_10 B9_10 B10_10 120.2(5) . . ?
B8_10 B9_10 B10_10 108.5(6) . . ?
B3_10 B9_10 B10_10 60.7(5) . . ?
B12_10 B9_10 B4_10 107.3(6) . . ?
Cl7_10 B9_10 B4_10 124.4(5) . . ?
B8_10 B9_10 B4_10 59.4(5) . . ?
B3_10 B9_10 B4_10 59.3(5) . . ?
B10_10 B9_10 B4_10 107.9(6) . . ?
Cl8_10 B10_10 B2_10 122.5(5) . . ?
Cl8_10 B10_10 B9_10 121.5(5) . . ?
B2_10 B10_10 B9_10 107.3(5) . . ?
Cl8_10 B10_10 B12_10 122.7(6) . . ?
B2_10 B10_10 B12_10 107.0(6) . . ?
B9_10 B10_10 B12_10 59.4(4) . . ?
Cl8_10 B10_10 B11_10 122.7(5) . . ?
B2_10 B10_10 B11_10 60.1(5) . . ?
B9_10 B10_10 B11_10 107.2(6) . . ?
B12_10 B10_10 B11_10 59.4(5) . . ?
Cl8_10 B10_10 B3_10 121.8(5) . . ?
B2_10 B10_10 B3_10 59.7(5) . . ?
B9_10 B10_10 B3_10 59.6(4) . . ?
B12_10 B10_10 B3_10 106.7(5) . . ?
B11_10 B10_10 B3_10 107.5(6) . . ?
B7_10 B11_10 B12_10 61.1(5) . . ?
B7_10 B11_10 B2_10 107.3(5) . . ?
B12_10 B11_10 B2_10 106.9(6) . . ?
B7_10 B11_10 Cl10_10 122.9(5) . . ?
B12_10 B11_10 Cl10_10 120.4(5) . . ?
B2_10 B11_10 Cl10_10 122.4(5) . . ?
B7_10 B11_10 B5_10 59.4(4) . . ?
B12_10 B11_10 B5_10 107.9(6) . . ?
B2_10 B11_10 B5_10 59.7(5) . . ?
Cl10_10 B11_10 B5_10 124.3(5) . . ?
B7_10 B11_10 B10_10 109.1(6) . . ?
B12_10 B11_10 B10_10 60.1(5) . . ?
B2_10 B11_10 B10_10 59.4(5) . . ?
Cl10_10 B11_10 B10_10 119.0(5) . . ?
B5_10 B11_10 B10_10 107.9(6) . . ?
B9_10 B12_10 B8_10 60.3(5) . . ?
B9_10 B12_10 B11_10 108.7(6) . . ?
B8_10 B12_10 B11_10 108.3(6) . . ?
B9_10 B12_10 B10_10 60.2(4) . . ?
B8_10 B12_10 B10_10 108.5(6) . . ?
B11_10 B12_10 B10_10 60.5(5) . . ?
B9_10 B12_10 Cl9_10 119.9(5) . . ?
B8_10 B12_10 Cl9_10 123.6(5) . . ?
B11_10 B12_10 Cl9_10 121.0(5) . . ?
B10_10 B12_10 Cl9_10 118.4(5) . . ?
B9_10 B12_10 B7_10 108.8(5) . . ?
B8_10 B12_10 B7_10 60.7(5) . . ?
B11_10 B12_10 B7_10 59.3(5) . . ?
B10_10 B12_10 B7_10 108.1(6) . . ?
Cl9_10 B12_10 B7_10 124.3(5) . . ?
B5_11 B1_11 B6_11 60.6(5) . . ?
B5_11 B1_11 B2_11 109.5(6) . . ?
B6_11 B1_11 B2_11 61.2(5) . . ?
B5_11 B1_11 B4_11 59.9(5) . . ?
B6_11 B1_11 B4_11 108.7(6) . . ?
B2_11 B1_11 B4_11 108.4(6) . . ?
B5_11 B1_11 Cl1_11 122.8(6) . . ?
B6_11 B1_11 Cl1_11 121.2(6) . . ?
B2_11 B1_11 Cl1_11 119.5(5) . . ?
B4_11 B1_11 Cl1_11 122.3(6) . . ?
B5_11 B1_11 B3_11 108.2(6) . . ?
B6_11 B1_11 B3_11 108.8(6) . . ?
B2_11 B1_11 B3_11 59.9(5) . . ?
B4_11 B1_11 B3_11 59.9(5) . . ?
Cl1_11 B1_11 B3_11 120.5(6) . . ?
B1_11 B2_11 B3_11 60.9(5) . . ?
B1_11 B2_11 B11_11 107.6(6) . . ?
B3_11 B2_11 B11_11 59.4(5) . . ?
B1_11 B2_11 Cl6_11 122.0(6) . . ?
B3_11 B2_11 Cl6_11 122.3(5) . . ?
B11_11 B2_11 Cl6_11 122.7(5) . . ?
B1_11 B2_11 B6_11 59.2(5) . . ?
B3_11 B2_11 B6_11 108.1(6) . . ?
B11_11 B2_11 B6_11 107.3(6) . . ?
Cl6_11 B2_11 B6_11 121.3(5) . . ?
B1_11 B2_11 B7_11 107.8(6) . . ?
B3_11 B2_11 B7_11 107.9(6) . . ?
B11_11 B2_11 B7_11 59.6(5) . . ?
Cl6_11 B2_11 B7_11 121.0(5) . . ?
B6_11 B2_11 B7_11 60.3(5) . . ?
B11_11 B3_11 B2_11 60.4(5) . . ?
B11_11 B3_11 B10_11 60.2(5) . . ?
B2_11 B3_11 B10_11 108.5(6) . . ?
B11_11 B3_11 Cl2_11 123.0(6) . . ?
B2_11 B3_11 Cl2_11 120.7(5) . . ?
B10_11 B3_11 Cl2_11 123.1(5) . . ?
B11_11 B3_11 B4_11 107.7(6) . . ?
B2_11 B3_11 B4_11 107.8(6) . . ?
B10_11 B3_11 B4_11 59.7(5) . . ?
Cl2_11 B3_11 B4_11 121.7(6) . . ?
B11_11 B3_11 B1_11 107.0(6) . . ?
B2_11 B3_11 B1_11 59.2(5) . . ?
B10_11 B3_11 B1_11 107.2(6) . . ?
Cl2_11 B3_11 B1_11 121.0(6) . . ?
B4_11 B3_11 B1_11 59.8(5) . . ?
B5_11 B4_11 B9_11 60.4(5) . . ?
B5_11 B4_11 B10_11 108.2(6) . . ?
B9_11 B4_11 B10_11 59.9(5) . . ?
B5_11 B4_11 Cl3_11 122.3(6) . . ?
B9_11 B4_11 Cl3_11 121.2(5) . . ?
B10_11 B4_11 Cl3_11 120.8(5) . . ?
B5_11 B4_11 B1_11 59.3(5) . . ?
B9_11 B4_11 B1_11 107.5(6) . . ?
B10_11 B4_11 B1_11 107.8(6) . . ?
Cl3_11 B4_11 B1_11 123.1(6) . . ?
B5_11 B4_11 B3_11 108.0(6) . . ?
B9_11 B4_11 B3_11 107.9(6) . . ?
B10_11 B4_11 B3_11 59.9(5) . . ?
Cl3_11 B4_11 B3_11 121.6(6) . . ?
B1_11 B4_11 B3_11 60.3(5) . . ?
B1_11 B5_11 B4_11 60.9(5) . . ?
B1_11 B5_11 Cl4_11 121.8(6) . . ?
B4_11 B5_11 Cl4_11 122.6(6) . . ?
B1_11 B5_11 B6_11 59.7(5) . . ?
B4_11 B5_11 B6_11 108.7(6) . . ?
Cl4_11 B5_11 B6_11 120.2(5) . . ?
B1_11 B5_11 B9_11 108.4(6) . . ?
B4_11 B5_11 B9_11 59.9(5) . . ?
Cl4_11 B5_11 B9_11 122.3(5) . . ?
B6_11 B5_11 B9_11 108.3(6) . . ?
B1_11 B5_11 B8_11 107.5(6) . . ?
B4_11 B5_11 B8_11 107.9(6) . . ?
Cl4_11 B5_11 B8_11 121.2(6) . . ?
B6_11 B5_11 B8_11 59.9(5) . . ?
B9_11 B5_11 B8_11 59.9(4) . . ?
B1_11 B6_11 B5_11 59.6(5) . . ?
B1_11 B6_11 B8_11 107.8(6) . . ?
B5_11 B6_11 B8_11 60.4(5) . . ?
B1_11 B6_11 Cl5_11 122.2(6) . . ?
B5_11 B6_11 Cl5_11 121.5(5) . . ?
B8_11 B6_11 Cl5_11 121.4(6) . . ?
B1_11 B6_11 B2_11 59.6(5) . . ?
B5_11 B6_11 B2_11 107.4(6) . . ?
B8_11 B6_11 B2_11 107.6(6) . . ?
Cl5_11 B6_11 B2_11 122.5(5) . . ?
B1_11 B6_11 B7_11 107.7(6) . . ?
B5_11 B6_11 B7_11 108.4(6) . . ?
B8_11 B6_11 B7_11 60.2(5) . . ?
Cl5_11 B6_11 B7_11 121.6(6) . . ?
B2_11 B6_11 B7_11 59.8(5) . . ?
Cl7_11 B7_11 B11_11 123.0(6) . . ?
Cl7_11 B7_11 B12_11 122.7(6) . . ?
B11_11 B7_11 B12_11 59.8(5) . . ?
Cl7_11 B7_11 B2_11 121.8(5) . . ?
B11_11 B7_11 B2_11 59.9(5) . . ?
B12_11 B7_11 B2_11 107.6(6) . . ?
Cl7_11 B7_11 B8_11 122.3(6) . . ?
B11_11 B7_11 B8_11 106.6(5) . . ?
B12_11 B7_11 B8_11 59.2(4) . . ?
B2_11 B7_11 B8_11 107.0(6) . . ?
Cl7_11 B7_11 B6_11 121.5(5) . . ?
B11_11 B7_11 B6_11 107.2(6) . . ?
B12_11 B7_11 B6_11 106.9(6) . . ?
B2_11 B7_11 B6_11 59.9(5) . . ?
B8_11 B7_11 B6_11 59.3(5) . . ?
B12_11 B8_11 B6_11 108.5(6) . . ?
B12_11 B8_11 B9_11 60.6(5) . . ?
B6_11 B8_11 B9_11 108.1(6) . . ?
B12_11 B8_11 Cl8_11 120.4(5) . . ?
B6_11 B8_11 Cl8_11 121.3(5) . . ?
B9_11 B8_11 Cl8_11 122.7(5) . . ?
B12_11 B8_11 B5_11 108.3(6) . . ?
B6_11 B8_11 B5_11 59.7(5) . . ?
B9_11 B8_11 B5_11 59.9(5) . . ?
Cl8_11 B8_11 B5_11 123.5(5) . . ?
B12_11 B8_11 B7_11 60.0(5) . . ?
B6_11 B8_11 B7_11 60.6(5) . . ?
B9_11 B8_11 B7_11 108.5(6) . . ?
Cl8_11 B8_11 B7_11 119.6(5) . . ?
B5_11 B8_11 B7_11 108.2(6) . . ?
B10_11 B9_11 B4_11 60.1(5) . . ?
B10_11 B9_11 B5_11 107.8(6) . . ?
B4_11 B9_11 B5_11 59.7(5) . . ?
B10_11 B9_11 B8_11 107.8(6) . . ?
B4_11 B9_11 B8_11 107.9(6) . . ?
B5_11 B9_11 B8_11 60.2(5) . . ?
B10_11 B9_11 Cl9_11 121.5(5) . . ?
B4_11 B9_11 Cl9_11 122.3(5) . . ?
B5_11 B9_11 Cl9_11 122.4(5) . . ?
B8_11 B9_11 Cl9_11 121.6(5) . . ?
B10_11 B9_11 B12_11 60.4(5) . . ?
B4_11 B9_11 B12_11 108.1(6) . . ?
B5_11 B9_11 B12_11 107.5(5) . . ?
B8_11 B9_11 B12_11 59.2(5) . . ?
Cl9_11 B9_11 B12_11 121.3(5) . . ?
B9_11 B10_11 B4_11 60.0(5) . . ?
B9_11 B10_11 B11_11 108.0(6) . . ?
B4_11 B10_11 B11_11 107.8(6) . . ?
B9_11 B10_11 B3_11 108.5(6) . . ?
B4_11 B10_11 B3_11 60.5(5) . . ?
B11_11 B10_11 B3_11 59.6(5) . . ?
B9_11 B10_11 Cl10_11 120.8(5) . . ?
B4_11 B10_11 Cl10_11 124.2(5) . . ?
B11_11 B10_11 Cl10_11 120.8(6) . . ?
B3_11 B10_11 Cl10_11 123.8(5) . . ?
B9_11 B10_11 B12_11 60.3(5) . . ?
B4_11 B10_11 B12_11 108.0(6) . . ?
B11_11 B10_11 B12_11 59.5(5) . . ?
B3_11 B10_11 B12_11 107.5(5) . . ?
Cl10_11 B10_11 B12_11 119.0(5) . . ?
B3_11 B11_11 B12_11 108.9(6) . . ?
B3_11 B11_11 B10_11 60.2(5) . . ?
B12_11 B11_11 B10_11 60.6(5) . . ?
B3_11 B11_11 B7_11 109.2(6) . . ?
B12_11 B11_11 B7_11 60.2(5) . . ?
B10_11 B11_11 B7_11 109.1(6) . . ?
B3_11 B11_11 B2_11 60.1(5) . . ?
B12_11 B11_11 B2_11 108.4(6) . . ?
B10_11 B11_11 B2_11 108.3(6) . . ?
B7_11 B11_11 B2_11 60.5(5) . . ?
B3_11 B11_11 Cl11_11 121.7(6) . . ?
B12_11 B11_11 Cl11_11 119.6(6) . . ?
B10_11 B11_11 Cl11_11 119.5(6) . . ?
B7_11 B11_11 Cl11_11 121.6(6) . . ?
B2_11 B11_11 Cl11_11 123.8(5) . . ?
B8_11 B12_11 B11_11 108.2(6) . . ?
B8_11 B12_11 B7_11 60.9(5) . . ?
B11_11 B12_11 B7_11 60.1(5) . . ?
B8_11 B12_11 B9_11 60.2(5) . . ?
B11_11 B12_11 B9_11 107.3(6) . . ?
B7_11 B12_11 B9_11 108.9(6) . . ?
B8_11 B12_11 Cl12_11 122.6(5) . . ?
B11_11 B12_11 Cl12_11 121.6(5) . . ?
B7_11 B12_11 Cl12_11 122.0(5) . . ?
B9_11 B12_11 Cl12_11 121.4(5) . . ?
B8_11 B12_11 B10_11 107.7(6) . . ?
B11_11 B12_11 B10_11 59.8(5) . . ?
B7_11 B12_11 B10_11 108.4(6) . . ?
B9_11 B12_11 B10_11 59.3(4) . . ?
Cl12_11 B12_11 B10_11 120.6(5) . . ?
B2_12 B1_12 B3_12 60.9(5) . . ?
B2_12 B1_12 B4_12 60.7(5) . . ?
B3_12 B1_12 B4_12 109.0(6) . . ?
B2_12 B1_12 B5_12 108.6(6) . . ?
B3_12 B1_12 B5_12 59.7(5) . . ?
B4_12 B1_12 B5_12 107.7(6) . . ?
B2_12 B1_12 Cl1_12 122.3(6) . . ?
B3_12 B1_12 Cl1_12 122.5(6) . . ?
B4_12 B1_12 Cl1_12 121.2(6) . . ?
B5_12 B1_12 Cl1_12 121.3(6) . . ?
B2_12 B1_12 B6_12 108.1(6) . . ?
B3_12 B1_12 B6_12 107.8(6) . . ?
B4_12 B1_12 B6_12 59.3(5) . . ?
B5_12 B1_12 B6_12 59.9(5) . . ?
Cl1_12 B1_12 B6_12 120.6(6) . . ?
B1_12 B2_12 B3_12 60.3(5) . . ?
B1_12 B2_12 B4_12 60.7(5) . . ?
B3_12 B2_12 B4_12 108.5(6) . . ?
B1_12 B2_12 B11_12 108.0(6) . . ?
B3_12 B2_12 B11_12 59.7(5) . . ?
B4_12 B2_12 B11_12 107.5(6) . . ?
B1_12 B2_12 Cl2_12 120.2(6) . . ?
B3_12 B2_12 Cl2_12 121.3(6) . . ?
B4_12 B2_12 Cl2_12 121.3(6) . . ?
B11_12 B2_12 Cl2_12 123.0(6) . . ?
B1_12 B2_12 B10_12 108.7(6) . . ?
B3_12 B2_12 B10_12 107.4(6) . . ?
B4_12 B2_12 B10_12 60.2(5) . . ?
B11_12 B2_12 B10_12 59.0(5) . . ?
Cl2_12 B2_12 B10_12 122.8(6) . . ?
B1_12 B3_12 B5_12 60.9(5) . . ?
B1_12 B3_12 B11_12 107.5(6) . . ?
B5_12 B3_12 B11_12 107.6(6) . . ?
B1_12 B3_12 B2_12 58.8(5) . . ?
B5_12 B3_12 B2_12 107.8(6) . . ?
B11_12 B3_12 B2_12 60.5(5) . . ?
B1_12 B3_12 Cl3_12 121.1(6) . . ?
B5_12 B3_12 Cl3_12 122.0(6) . . ?
B11_12 B3_12 Cl3_12 122.2(6) . . ?
B2_12 B3_12 Cl3_12 121.1(6) . . ?
B1_12 B3_12 B9_12 109.0(6) . . ?
B5_12 B3_12 B9_12 60.1(5) . . ?
B11_12 B3_12 B9_12 60.0(5) . . ?
B2_12 B3_12 B9_12 108.8(6) . . ?
Cl3_12 B3_12 B9_12 121.8(6) . . ?
B6_12 B4_12 B8_12 59.4(5) . . ?
B6_12 B4_12 B2_12 108.1(6) . . ?
B8_12 B4_12 B2_12 108.8(6) . . ?
B6_12 B4_12 B1_12 61.4(5) . . ?
B8_12 B4_12 B1_12 108.6(6) . . ?
B2_12 B4_12 B1_12 58.6(5) . . ?
B6_12 B4_12 B10_12 107.4(6) . . ?
B8_12 B4_12 B10_12 59.8(5) . . ?
B2_12 B4_12 B10_12 61.0(5) . . ?
B1_12 B4_12 B10_12 107.5(6) . . ?
B6_12 B4_12 Cl4_12 121.9(6) . . ?
B8_12 B4_12 Cl4_12 121.1(6) . . ?
B2_12 B4_12 Cl4_12 121.6(6) . . ?
B1_12 B4_12 Cl4_12 122.2(5) . . ?
B10_12 B4_12 Cl4_12 121.5(6) . . ?
B3_12 B5_12 Cl5_12 122.5(6) . . ?
B3_12 B5_12 B9_12 60.7(5) . . ?
Cl5_12 B5_12 B9_12 121.8(6) . . ?
B3_12 B5_12 B1_12 59.4(5) . . ?
Cl5_12 B5_12 B1_12 121.7(6) . . ?
B9_12 B5_12 B1_12 108.3(6) . . ?
B3_12 B5_12 B6_12 108.2(6) . . ?
Cl5_12 B5_12 B6_12 120.7(6) . . ?
B9_12 B5_12 B6_12 108.2(6) . . ?
B1_12 B5_12 B6_12 60.7(5) . . ?
B3_12 B5_12 B7_12 108.4(6) . . ?
Cl5_12 B5_12 B7_12 121.3(6) . . ?
B9_12 B5_12 B7_12 60.4(5) . . ?
B1_12 B5_12 B7_12 107.8(6) . . ?
B6_12 B5_12 B7_12 59.2(5) . . ?
B8_12 B6_12 B4_12 60.3(5) . . ?
B8_12 B6_12 B7_12 60.3(5) . . ?
B4_12 B6_12 B7_12 108.3(6) . . ?
B8_12 B6_12 Cl6_12 121.6(6) . . ?
B4_12 B6_12 Cl6_12 119.0(6) . . ?
B7_12 B6_12 Cl6_12 124.5(7) . . ?
B8_12 B6_12 B5_12 108.4(6) . . ?
B4_12 B6_12 B5_12 107.3(6) . . ?
B7_12 B6_12 B5_12 60.4(5) . . ?
Cl6_12 B6_12 B5_12 123.4(6) . . ?
B8_12 B6_12 B1_12 107.7(7) . . ?
B4_12 B6_12 B1_12 59.3(5) . . ?
B7_12 B6_12 B1_12 107.7(6) . . ?
Cl6_12 B6_12 B1_12 120.2(6) . . ?
B5_12 B6_12 B1_12 59.4(5) . . ?
B8_12 B7_12 B6_12 59.4(5) . . ?
B8_12 B7_12 B12_12 61.4(5) . . ?
B6_12 B7_12 B12_12 108.8(6) . . ?
B8_12 B7_12 Cl7_12 123.0(6) . . ?
B6_12 B7_12 Cl7_12 121.1(6) . . ?
B12_12 B7_12 Cl7_12 122.5(6) . . ?
B8_12 B7_12 B5_12 107.6(6) . . ?
B6_12 B7_12 B5_12 60.4(5) . . ?
B12_12 B7_12 B5_12 107.6(6) . . ?
Cl7_12 B7_12 B5_12 120.4(6) . . ?
B8_12 B7_12 B9_12 108.9(6) . . ?
B6_12 B7_12 B9_12 108.4(6) . . ?
B12_12 B7_12 B9_12 59.9(5) . . ?
Cl7_12 B7_12 B9_12 120.7(6) . . ?
B5_12 B7_12 B9_12 59.5(5) . . ?
B6_12 B8_12 B4_12 60.2(5) . . ?
B6_12 B8_12 B7_12 60.3(5) . . ?
B4_12 B8_12 B7_12 108.2(6) . . ?
B6_12 B8_12 Cl8_12 121.6(6) . . ?
B4_12 B8_12 Cl8_12 121.3(6) . . ?
B7_12 B8_12 Cl8_12 122.2(6) . . ?
B6_12 B8_12 B10_12 108.8(6) . . ?
B4_12 B8_12 B10_12 60.8(5) . . ?
B7_12 B8_12 B10_12 107.4(6) . . ?
Cl8_12 B8_12 B10_12 121.3(6) . . ?
B6_12 B8_12 B12_12 107.9(6) . . ?
B4_12 B8_12 B12_12 108.1(6) . . ?
B7_12 B8_12 B12_12 59.3(5) . . ?
Cl8_12 B8_12 B12_12 121.9(6) . . ?
B10_12 B8_12 B12_12 59.5(5) . . ?
Cl11_12 B9_12 B11_12 124.2(6) . . ?
Cl11_12 B9_12 B5_12 121.5(6) . . ?
B11_12 B9_12 B5_12 106.4(6) . . ?
Cl11_12 B9_12 B12_12 121.4(6) . . ?
B11_12 B9_12 B12_12 60.0(5) . . ?
B5_12 B9_12 B12_12 107.7(6) . . ?
Cl11_12 B9_12 B3_12 123.4(6) . . ?
B11_12 B9_12 B3_12 59.4(5) . . ?
B5_12 B9_12 B3_12 59.1(5) . . ?
B12_12 B9_12 B3_12 107.7(6) . . ?
Cl11_12 B9_12 B7_12 120.8(6) . . ?
B11_12 B9_12 B7_12 106.5(6) . . ?
B5_12 B9_12 B7_12 60.2(5) . . ?
B12_12 B9_12 B7_12 59.4(5) . . ?
B3_12 B9_12 B7_12 107.0(6) . . ?
B11_12 B10_12 Cl9_12 121.7(6) . . ?
B11_12 B10_12 B8_12 108.3(6) . . ?
Cl9_12 B10_12 B8_12 122.8(6) . . ?
B11_12 B10_12 B12_12 60.2(5) . . ?
Cl9_12 B10_12 B12_12 122.5(6) . . ?
B8_12 B10_12 B12_12 61.1(5) . . ?
B11_12 B10_12 B4_12 106.9(6) . . ?
Cl9_12 B10_12 B4_12 121.7(6) . . ?
B8_12 B10_12 B4_12 59.4(5) . . ?
B12_12 B10_12 B4_12 108.3(6) . . ?
B11_12 B10_12 B2_12 59.7(5) . . ?
Cl9_12 B10_12 B2_12 120.9(6) . . ?
B8_12 B10_12 B2_12 106.7(6) . . ?
B12_12 B10_12 B2_12 108.0(6) . . ?
B4_12 B10_12 B2_12 58.8(5) . . ?
B3_12 B11_12 B10_12 109.2(6) . . ?
B3_12 B11_12 B9_12 60.7(5) . . ?
B10_12 B11_12 B9_12 108.8(6) . . ?
B3_12 B11_12 B2_12 59.7(5) . . ?
B10_12 B11_12 B2_12 61.2(5) . . ?
B9_12 B11_12 B2_12 108.7(6) . . ?
B3_12 B11_12 B12_12 108.9(6) . . ?
B10_12 B11_12 B12_12 60.2(5) . . ?
B9_12 B11_12 B12_12 60.1(5) . . ?
B2_12 B11_12 B12_12 109.2(6) . . ?
B3_12 B11_12 Cl10_12 122.8(6) . . ?
B10_12 B11_12 Cl10_12 119.8(6) . . ?
B9_12 B11_12 Cl10_12 121.3(6) . . ?
B2_12 B11_12 Cl10_12 122.0(6) . . ?
B12_12 B11_12 Cl10_12 119.7(6) . . ?
Cl12_12 B12_12 B7_12 123.6(6) . . ?
Cl12_12 B12_12 B10_12 120.7(6) . . ?
B7_12 B12_12 B10_12 107.2(6) . . ?
Cl12_12 B12_12 B11_12 121.2(6) . . ?
B7_12 B12_12 B11_12 107.5(6) . . ?
B10_12 B12_12 B11_12 59.6(5) . . ?
Cl12_12 B12_12 B9_12 121.7(6) . . ?
B7_12 B12_12 B9_12 60.7(5) . . ?
B10_12 B12_12 B9_12 108.1(6) . . ?
B11_12 B12_12 B9_12 59.9(5) . . ?
Cl12_12 B12_12 B8_12 123.1(6) . . ?
B7_12 B12_12 B8_12 59.2(5) . . ?
B10_12 B12_12 B8_12 59.4(5) . . ?
B11_12 B12_12 B8_12 106.4(6) . . ?
B9_12 B12_12 B8_12 107.8(6) . . ?
B3_13 B1_13 B2_13 59.3(5) . . ?
B3_13 B1_13 B4_13 61.1(5) . . ?
B2_13 B1_13 B4_13 107.9(5) . . ?
B3_13 B1_13 B5_13 109.0(6) . . ?
B2_13 B1_13 B5_13 107.8(6) . . ?
B4_13 B1_13 B5_13 60.1(5) . . ?
B3_13 B1_13 Cl1_13 122.0(5) . . ?
B2_13 B1_13 Cl1_13 119.3(6) . . ?
B4_13 B1_13 Cl1_13 124.8(5) . . ?
B5_13 B1_13 Cl1_13 122.7(5) . . ?
B3_13 B1_13 B6_13 107.1(5) . . ?
B2_13 B1_13 B6_13 58.8(5) . . ?
B4_13 B1_13 B6_13 108.1(5) . . ?
B5_13 B1_13 B6_13 60.7(4) . . ?
Cl1_13 B1_13 B6_13 119.6(5) . . ?
B3_13 B2_13 B6_13 109.8(6) . . ?
B3_13 B2_13 B1_13 60.0(5) . . ?
B6_13 B2_13 B1_13 61.5(5) . . ?
B3_13 B2_13 B12_13 109.5(6) . . ?
B6_13 B2_13 B12_13 60.2(5) . . ?
B1_13 B2_13 B12_13 109.6(6) . . ?
B3_13 B2_13 B11_13 60.3(4) . . ?
B6_13 B2_13 B11_13 109.2(6) . . ?
B1_13 B2_13 B11_13 108.7(6) . . ?
B12_13 B2_13 B11_13 60.8(5) . . ?
B3_13 B2_13 Cl6_13 120.9(6) . . ?
B6_13 B2_13 Cl6_13 120.8(5) . . ?
B1_13 B2_13 Cl6_13 121.2(5) . . ?
B12_13 B2_13 Cl6_13 120.6(5) . . ?
B11_13 B2_13 Cl6_13 121.0(5) . . ?
B2_13 B3_13 B1_13 60.6(5) . . ?
B2_13 B3_13 B11_13 61.1(5) . . ?
B1_13 B3_13 B11_13 109.8(5) . . ?
B2_13 B3_13 Cl5_13 121.1(5) . . ?
B1_13 B3_13 Cl5_13 119.6(5) . . ?
B11_13 B3_13 Cl5_13 122.2(5) . . ?
B2_13 B3_13 B4_13 108.0(5) . . ?
B1_13 B3_13 B4_13 59.9(5) . . ?
B11_13 B3_13 B4_13 107.9(5) . . ?
Cl5_13 B3_13 B4_13 121.5(5) . . ?
B2_13 B3_13 B10_13 108.2(6) . . ?
B1_13 B3_13 B10_13 107.9(6) . . ?
B11_13 B3_13 B10_13 59.8(4) . . ?
Cl5_13 B3_13 B10_13 123.1(5) . . ?
B4_13 B3_13 B10_13 59.3(4) . . ?
B8_13 B4_13 B1_13 108.8(5) . . ?
B8_13 B4_13 B10_13 59.9(4) . . ?
B1_13 B4_13 B10_13 108.1(5) . . ?
B8_13 B4_13 B5_13 60.9(5) . . ?
B1_13 B4_13 B5_13 60.2(5) . . ?
B10_13 B4_13 B5_13 108.7(5) . . ?
B8_13 B4_13 Cl4_13 121.2(5) . . ?
B1_13 B4_13 Cl4_13 122.1(5) . . ?
B10_13 B4_13 Cl4_13 121.0(5) . . ?
B5_13 B4_13 Cl4_13 121.7(5) . . ?
B8_13 B4_13 B3_13 108.0(5) . . ?
B1_13 B4_13 B3_13 59.0(4) . . ?
B10_13 B4_13 B3_13 60.4(4) . . ?
B5_13 B4_13 B3_13 107.5(5) . . ?
Cl4_13 B4_13 B3_13 122.0(5) . . ?
Cl3_13 B5_13 B4_13 122.4(5) . . ?
Cl3_13 B5_13 B1_13 121.6(5) . . ?
B4_13 B5_13 B1_13 59.7(4) . . ?
Cl3_13 B5_13 B8_13 122.7(5) . . ?
B4_13 B5_13 B8_13 59.4(4) . . ?
B1_13 B5_13 B8_13 107.2(5) . . ?
Cl3_13 B5_13 B7_13 122.3(5) . . ?
B4_13 B5_13 B7_13 107.0(5) . . ?
B1_13 B5_13 B7_13 107.5(6) . . ?
B8_13 B5_13 B7_13 59.6(5) . . ?
Cl3_13 B5_13 B6_13 121.7(5) . . ?
B4_13 B5_13 B6_13 107.5(5) . . ?
B1_13 B5_13 B6_13 60.2(5) . . ?
B8_13 B5_13 B6_13 107.1(5) . . ?
B7_13 B5_13 B6_13 59.6(4) . . ?
B2_13 B6_13 B12_13 60.5(5) . . ?
B2_13 B6_13 Cl2_13 123.0(5) . . ?
B12_13 B6_13 Cl2_13 121.9(5) . . ?
B2_13 B6_13 B7_13 107.7(6) . . ?
B12_13 B6_13 B7_13 60.2(5) . . ?
Cl2_13 B6_13 B7_13 121.5(5) . . ?
B2_13 B6_13 B1_13 59.7(5) . . ?
B12_13 B6_13 B1_13 108.4(5) . . ?
Cl2_13 B6_13 B1_13 121.8(5) . . ?
B7_13 B6_13 B1_13 107.3(5) . . ?
B2_13 B6_13 B5_13 107.3(6) . . ?
B12_13 B6_13 B5_13 108.7(5) . . ?
Cl2_13 B6_13 B5_13 120.6(5) . . ?
B7_13 B6_13 B5_13 60.2(5) . . ?
B1_13 B6_13 B5_13 59.2(5) . . ?
Cl12_13 B7_13 B9_13 121.7(5) . . ?
Cl12_13 B7_13 B12_13 122.3(6) . . ?
B9_13 B7_13 B12_13 61.0(5) . . ?
Cl12_13 B7_13 B8_13 121.2(5) . . ?
B9_13 B7_13 B8_13 60.0(4) . . ?
B12_13 B7_13 B8_13 108.5(6) . . ?
Cl12_13 B7_13 B6_13 122.1(5) . . ?
B9_13 B7_13 B6_13 108.1(6) . . ?
B12_13 B7_13 B6_13 59.1(5) . . ?
B8_13 B7_13 B6_13 107.9(6) . . ?
Cl12_13 B7_13 B5_13 121.0(6) . . ?
B9_13 B7_13 B5_13 108.3(6) . . ?
B12_13 B7_13 B5_13 107.9(6) . . ?
B8_13 B7_13 B5_13 60.0(4) . . ?
B6_13 B7_13 B5_13 60.2(5) . . ?
B4_13 B8_13 B10_13 60.1(4) . . ?
B4_13 B8_13 Cl11_13 122.4(5) . . ?
B10_13 B8_13 Cl11_13 121.0(5) . . ?
B4_13 B8_13 B9_13 108.4(5) . . ?
B10_13 B8_13 B9_13 60.2(4) . . ?
Cl11_13 B8_13 B9_13 120.3(5) . . ?
B4_13 B8_13 B7_13 108.0(5) . . ?
B10_13 B8_13 B7_13 107.6(6) . . ?
Cl11_13 B8_13 B7_13 121.9(5) . . ?
B9_13 B8_13 B7_13 59.6(5) . . ?
B4_13 B8_13 B5_13 59.7(4) . . ?
B10_13 B8_13 B5_13 107.9(5) . . ?
Cl11_13 B8_13 B5_13 122.8(5) . . ?
B9_13 B8_13 B5_13 108.4(5) . . ?
B7_13 B8_13 B5_13 60.5(5) . . ?
B7_13 B9_13 Cl10_13 122.0(5) . . ?
B7_13 B9_13 B8_13 60.4(5) . . ?
Cl10_13 B9_13 B8_13 121.8(5) . . ?
B7_13 B9_13 B10_13 107.7(6) . . ?
Cl10_13 B9_13 B10_13 121.8(5) . . ?
B8_13 B9_13 B10_13 59.5(4) . . ?
B7_13 B9_13 B11_13 107.9(6) . . ?
Cl10_13 B9_13 B11_13 121.7(5) . . ?
B8_13 B9_13 B11_13 107.6(5) . . ?
B10_13 B9_13 B11_13 59.6(4) . . ?
B7_13 B9_13 B12_13 59.8(5) . . ?
Cl10_13 B9_13 B12_13 122.2(5) . . ?
B8_13 B9_13 B12_13 107.9(6) . . ?
B10_13 B9_13 B12_13 107.4(5) . . ?
B11_13 B9_13 B12_13 60.1(4) . . ?
B8_13 B10_13 B4_13 60.0(4) . . ?
B8_13 B10_13 B11_13 108.8(6) . . ?
B4_13 B10_13 B11_13 108.6(5) . . ?
B8_13 B10_13 B9_13 60.3(5) . . ?
B4_13 B10_13 B9_13 108.3(5) . . ?
B11_13 B10_13 B9_13 60.4(4) . . ?
B8_13 B10_13 B3_13 108.0(5) . . ?
B4_13 B10_13 B3_13 60.3(4) . . ?
B11_13 B10_13 B3_13 59.6(4) . . ?
B9_13 B10_13 B3_13 107.8(5) . . ?
B8_13 B10_13 Cl9_13 120.4(5) . . ?
B4_13 B10_13 Cl9_13 122.0(5) . . ?
B11_13 B10_13 Cl9_13 121.5(5) . . ?
B9_13 B10_13 Cl9_13 120.3(5) . . ?
B3_13 B10_13 Cl9_13 123.4(5) . . ?
Cl7_13 B11_13 B3_13 122.8(5) . . ?
Cl7_13 B11_13 B10_13 122.3(5) . . ?
B3_13 B11_13 B10_13 60.6(4) . . ?
Cl7_13 B11_13 B2_13 122.9(5) . . ?
B3_13 B11_13 B2_13 58.5(4) . . ?
B10_13 B11_13 B2_13 106.8(5) . . ?
Cl7_13 B11_13 B9_13 121.3(5) . . ?
B3_13 B11_13 B9_13 108.1(6) . . ?
B10_13 B11_13 B9_13 59.9(4) . . ?
B2_13 B11_13 B9_13 107.0(5) . . ?
Cl7_13 B11_13 B12_13 121.2(5) . . ?
B3_13 B11_13 B12_13 106.8(5) . . ?
B10_13 B11_13 B12_13 107.9(6) . . ?
B2_13 B11_13 B12_13 59.1(4) . . ?
B9_13 B11_13 B12_13 60.4(4) . . ?
Cl8_13 B12_13 B6_13 122.5(5) . . ?
Cl8_13 B12_13 B2_13 122.4(5) . . ?
B6_13 B12_13 B2_13 59.3(5) . . ?
Cl8_13 B12_13 B7_13 122.8(5) . . ?
B6_13 B12_13 B7_13 60.7(5) . . ?
B2_13 B12_13 B7_13 107.2(6) . . ?
Cl8_13 B12_13 B11_13 120.9(5) . . ?
B6_13 B12_13 B11_13 107.9(6) . . ?
B2_13 B12_13 B11_13 60.1(4) . . ?
B7_13 B12_13 B11_13 107.1(6) . . ?
Cl8_13 B12_13 B9_13 121.6(5) . . ?
B6_13 B12_13 B9_13 107.9(6) . . ?
B2_13 B12_13 B9_13 107.1(6) . . ?
B7_13 B12_13 B9_13 59.2(5) . . ?
B11_13 B12_13 B9_13 59.5(4) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
N1_1 C1_1 C2_1 C3_1 -0.1(11) . . . . ?
C1_1 C2_1 C3_1 C4_1 1.9(10) . . . . ?
C1_1 C2_1 C3_1 C6_1 -179.1(6) . . . . ?
C2_1 C3_1 C4_1 C5_1 -2.5(11) . . . . ?
C6_1 C3_1 C4_1 C5_1 178.5(7) . . . . ?
C3_1 C4_1 C5_1 N1_1 1.5(11) . . . . ?
C4_1 C3_1 C6_1 C11_1 -31.7(10) . . . . ?
C2_1 C3_1 C6_1 C11_1 149.4(7) . . . . ?
C4_1 C3_1 C6_1 C7_1 150.0(7) . . . . ?
C2_1 C3_1 C6_1 C7_1 -29.0(10) . . . . ?
C11_1 C6_1 C7_1 C8_1 0.8(11) . . . . ?
C3_1 C6_1 C7_1 C8_1 179.1(7) . . . . ?
C6_1 C7_1 C8_1 C9_1 -1.6(11) . . . . ?
C7_1 C8_1 C9_1 C10_1 1.9(11) . . . . ?
C7_1 C8_1 C9_1 C12_1 -179.9(7) . . . . ?
C8_1 C9_1 C10_1 C11_1 -1.4(11) . . . . ?
C12_1 C9_1 C10_1 C11_1 -179.7(7) . . . . ?
C7_1 C6_1 C11_1 C10_1 -0.3(11) . . . . ?
C3_1 C6_1 C11_1 C10_1 -178.6(7) . . . . ?
C9_1 C10_1 C11_1 C6_1 0.6(11) . . . . ?
C8_1 C9_1 C12_1 C16_1 -148.1(7) . . . . ?
C10_1 C9_1 C12_1 C16_1 30.2(10) . . . . ?
C8_1 C9_1 C12_1 C13_1 32.1(11) . . . . ?
C10_1 C9_1 C12_1 C13_1 -149.7(7) . . . . ?
C16_1 C12_1 C13_1 C14_1 -0.9(11) . . . . ?
C9_1 C12_1 C13_1 C14_1 179.0(7) . . . . ?
C12_1 C13_1 C14_1 N2_1 -0.6(11) . . . . ?
N2_1 C15_1 C16_1 C12_1 -3.0(11) . . . . ?
C13_1 C12_1 C16_1 C15_1 2.6(11) . . . . ?
C9_1 C12_1 C16_1 C15_1 -177.3(7) . . . . ?
C4_1 C5_1 N1_1 C1_1 0.3(10) . . . . ?
C4_1 C5_1 N1_1 Cu1 -173.9(5) . . . . ?
C2_1 C1_1 N1_1 C5_1 -1.0(10) . . . . ?
C2_1 C1_1 N1_1 Cu1 173.4(5) . . . . ?
C13_1 C14_1 N2_1 C15_1 0.3(10) . . . . ?
C13_1 C14_1 N2_1 Cu5 172.3(6) . . . 7 ?
C16_1 C15_1 N2_1 C14_1 1.5(10) . . . . ?
C16_1 C15_1 N2_1 Cu5 -170.9(5) . . . 7 ?
N1_2 C1_2 C2_2 C3_2 0.1(11) . . . . ?
C1_2 C2_2 C3_2 C4_2 -0.4(10) . . . . ?
C1_2 C2_2 C3_2 C6_2 179.3(6) . . . . ?
C2_2 C3_2 C4_2 C5_2 -0.5(10) . . . . ?
C6_2 C3_2 C4_2 C5_2 179.8(6) . . . . ?
C3_2 C4_2 C5_2 N1_2 1.9(11) . . . . ?
C4_2 C3_2 C6_2 C11_2 -144.9(7) . . . . ?
C2_2 C3_2 C6_2 C11_2 35.4(10) . . . . ?
C4_2 C3_2 C6_2 C7_2 33.8(10) . . . . ?
C2_2 C3_2 C6_2 C7_2 -145.9(7) . . . . ?
C11_2 C6_2 C7_2 C8_2 -0.3(11) . . . . ?
C3_2 C6_2 C7_2 C8_2 -179.0(7) . . . . ?
C6_2 C7_2 C8_2 C9_2 1.7(12) . . . . ?
C7_2 C8_2 C9_2 C10_2 -2.1(11) . . . . ?
C7_2 C8_2 C9_2 C12_2 179.8(7) . . . . ?
C8_2 C9_2 C10_2 C11_2 1.2(11) . . . . ?
C12_2 C9_2 C10_2 C11_2 179.2(6) . . . . ?
C7_2 C6_2 C11_2 C10_2 -0.6(11) . . . . ?
C3_2 C6_2 C11_2 C10_2 178.0(6) . . . . ?
C9_2 C10_2 C11_2 C6_2 0.2(11) . . . . ?
C8_2 C9_2 C12_2 C13_2 -139.0(7) . . . . ?
C10_2 C9_2 C12_2 C13_2 42.9(10) . . . . ?
C8_2 C9_2 C12_2 C16_2 40.4(10) . . . . ?
C10_2 C9_2 C12_2 C16_2 -137.7(7) . . . . ?
C16_2 C12_2 C13_2 C14_2 1.0(11) . . . . ?
C9_2 C12_2 C13_2 C14_2 -179.5(7) . . . . ?
C12_2 C13_2 C14_2 N2_2 -0.1(11) . . . . ?
N2_2 C15_2 C16_2 C12_2 1.2(11) . . . . ?
C13_2 C12_2 C16_2 C15_2 -1.6(11) . . . . ?
C9_2 C12_2 C16_2 C15_2 179.0(7) . . . . ?
C2_2 C1_2 N1_2 C5_2 1.1(10) . . . . ?
C2_2 C1_2 N1_2 Cu5 173.9(5) . . . 7 ?
C4_2 C5_2 N1_2 C1_2 -2.1(10) . . . . ?
C4_2 C5_2 N1_2 Cu5 -175.3(5) . . . 7 ?
C13_2 C14_2 N2_2 C15_2 -0.4(10) . . . . ?
C13_2 C14_2 N2_2 Cu2 170.6(5) . . . . ?
C16_2 C15_2 N2_2 C14_2 -0.2(10) . . . . ?
C16_2 C15_2 N2_2 Cu2 -171.3(5) . . . . ?
N1_3 C1_3 C2_3 C3_3 0.3(11) . . . . ?
C1_3 C2_3 C3_3 C4_3 -1.3(10) . . . . ?
C1_3 C2_3 C3_3 C6_3 -179.1(7) . . . . ?
C2_3 C3_3 C4_3 C5_3 1.4(10) . . . . ?
C6_3 C3_3 C4_3 C5_3 179.3(7) . . . . ?
C3_3 C4_3 C5_3 N1_3 -0.5(11) . . . . ?
C4_3 C3_3 C6_3 C11_3 -36.5(10) . . . . ?
C2_3 C3_3 C6_3 C11_3 141.3(7) . . . . ?
C4_3 C3_3 C6_3 C7_3 141.5(8) . . . . ?
C2_3 C3_3 C6_3 C7_3 -40.7(11) . . . . ?
C11_3 C6_3 C7_3 C8_3 1.5(11) . . . . ?
C3_3 C6_3 C7_3 C8_3 -176.5(7) . . . . ?
C6_3 C7_3 C8_3 C9_3 -0.1(12) . . . . ?
C7_3 C8_3 C9_3 C10_3 -2.0(12) . . . . ?
C7_3 C8_3 C9_3 C12_3 -178.2(7) . . . . ?
C8_3 C9_3 C10_3 C11_3 2.7(12) . . . . ?
C12_3 C9_3 C10_3 C11_3 179.1(7) . . . . ?
C7_3 C6_3 C11_3 C10_3 -0.8(12) . . . . ?
C3_3 C6_3 C11_3 C10_3 177.3(7) . . . . ?
C9_3 C10_3 C11_3 C6_3 -1.4(13) . . . . ?
C10_3 C9_3 C12_3 C13_3 139.3(8) . . . . ?
C8_3 C9_3 C12_3 C13_3 -44.5(11) . . . . ?
C10_3 C9_3 C12_3 C16_3 -39.5(11) . . . . ?
C8_3 C9_3 C12_3 C16_3 136.8(8) . . . . ?
C16_3 C12_3 C13_3 C14_3 1.0(12) . . . . ?
C9_3 C12_3 C13_3 C14_3 -177.8(7) . . . . ?
C12_3 C13_3 C14_3 N2_3 -3.4(13) . . . . ?
N2_3 C15_3 C16_3 C12_3 -3.2(11) . . . . ?
C13_3 C12_3 C16_3 C15_3 2.1(11) . . . . ?
C9_3 C12_3 C16_3 C15_3 -179.1(7) . . . . ?
C4_3 C5_3 N1_3 C1_3 -0.5(10) . . . . ?
C4_3 C5_3 N1_3 Cu1 174.4(5) . . . . ?
C2_3 C1_3 N1_3 C5_3 0.6(10) . . . . ?
C2_3 C1_3 N1_3 Cu1 -174.0(5) . . . . ?
C13_3 C14_3 N2_3 C15_3 2.4(11) . . . . ?
C13_3 C14_3 N2_3 Cu5 -167.9(6) . . . . ?
C16_3 C15_3 N2_3 C14_3 0.9(11) . . . . ?
C16_3 C15_3 N2_3 Cu5 171.4(6) . . . . ?
N1_4 C1_4 C2_4 C3_4 1.1(12) . . . . ?
C1_4 C2_4 C3_4 C4_4 -2.1(11) . . . . ?
C1_4 C2_4 C3_4 C6_4 178.5(7) . . . . ?
C2_4 C3_4 C4_4 C5_4 2.8(11) . . . . ?
C6_4 C3_4 C4_4 C5_4 -177.8(7) . . . . ?
C3_4 C4_4 C5_4 N1_4 -2.4(11) . . . . ?
C2_4 C3_4 C6_4 C11_4 -40.7(11) . . . . ?
C4_4 C3_4 C6_4 C11_4 139.9(7) . . . . ?
C2_4 C3_4 C6_4 C7_4 139.4(8) . . . . ?
C4_4 C3_4 C6_4 C7_4 -40.0(10) . . . . ?
C11_4 C6_4 C7_4 C8_4 0.5(11) . . . . ?
C3_4 C6_4 C7_4 C8_4 -179.6(7) . . . . ?
C6_4 C7_4 C8_4 C9_4 -0.7(12) . . . . ?
C7_4 C8_4 C9_4 C10_4 0.0(11) . . . . ?
C7_4 C8_4 C9_4 C12_4 -179.8(7) . . . . ?
C8_4 C9_4 C10_4 C11_4 1.0(10) . . . . ?
C12_4 C9_4 C10_4 C11_4 -179.3(7) . . . . ?
C9_4 C10_4 C11_4 C6_4 -1.2(11) . . . . ?
C7_4 C6_4 C11_4 C10_4 0.5(10) . . . . ?
C3_4 C6_4 C11_4 C10_4 -179.4(7) . . . . ?
C10_4 C9_4 C12_4 C13_4 146.7(7) . . . . ?
C8_4 C9_4 C12_4 C13_4 -33.6(10) . . . . ?
C10_4 C9_4 C12_4 C16_4 -32.8(10) . . . . ?
C8_4 C9_4 C12_4 C16_4 146.9(7) . . . . ?
C16_4 C12_4 C13_4 C14_4 -0.7(10) . . . . ?
C9_4 C12_4 C13_4 C14_4 179.8(6) . . . . ?
C12_4 C13_4 C14_4 N2_4 -0.2(11) . . . . ?
N2_4 C15_4 C16_4 C12_4 -2.3(11) . . . . ?
C13_4 C12_4 C16_4 C15_4 1.9(10) . . . . ?
C9_4 C12_4 C16_4 C15_4 -178.6(6) . . . . ?
C2_4 C1_4 N1_4 C5_4 -0.5(11) . . . . ?
C2_4 C1_4 N1_4 Cu3 -171.2(6) . . . . ?
C4_4 C5_4 N1_4 C1_4 1.2(10) . . . . ?
C4_4 C5_4 N1_4 Cu3 172.0(5) . . . . ?
C16_4 C15_4 N2_4 C14_4 1.4(10) . . . . ?
C16_4 C15_4 N2_4 Cu6 -173.6(5) . . . . ?
C13_4 C14_4 N2_4 C15_4 -0.2(10) . . . . ?
C13_4 C14_4 N2_4 Cu6 175.1(5) . . . . ?
N1_5 C1_5 C2_5 C3_5 -0.4(11) . . . . ?
C1_5 C2_5 C3_5 C4_5 1.6(10) . . . . ?
C1_5 C2_5 C3_5 C6_5 -179.3(7) . . . . ?
C2_5 C3_5 C4_5 C5_5 -1.2(10) . . . . ?
C6_5 C3_5 C4_5 C5_5 179.7(6) . . . . ?
C3_5 C4_5 C5_5 N1_5 -0.6(11) . . . . ?
C2_5 C3_5 C6_5 C7_5 -149.0(7) . . . . ?
C4_5 C3_5 C6_5 C7_5 30.0(10) . . . . ?
C2_5 C3_5 C6_5 C11_5 30.8(10) . . . . ?
C4_5 C3_5 C6_5 C11_5 -150.2(7) . . . . ?
C11_5 C6_5 C7_5 C8_5 1.2(11) . . . . ?
C3_5 C6_5 C7_5 C8_5 -179.0(7) . . . . ?
C6_5 C7_5 C8_5 C9_5 -1.2(11) . . . . ?
C7_5 C8_5 C9_5 C10_5 1.1(11) . . . . ?
C7_5 C8_5 C9_5 C12_5 -178.7(7) . . . . ?
C8_5 C9_5 C10_5 C11_5 -1.0(11) . . . . ?
C12_5 C9_5 C10_5 C11_5 178.8(7) . . . . ?
C9_5 C10_5 C11_5 C6_5 1.1(11) . . . . ?
C7_5 C6_5 C11_5 C10_5 -1.1(10) . . . . ?
C3_5 C6_5 C11_5 C10_5 179.1(7) . . . . ?
C8_5 C9_5 C12_5 C16_5 148.7(7) . . . . ?
C10_5 C9_5 C12_5 C16_5 -31.0(10) . . . . ?
C8_5 C9_5 C12_5 C13_5 -30.6(10) . . . . ?
C10_5 C9_5 C12_5 C13_5 149.7(7) . . . . ?
C16_5 C12_5 C13_5 C14_5 1.2(10) . . . . ?
C9_5 C12_5 C13_5 C14_5 -179.5(6) . . . . ?
C12_5 C13_5 C14_5 N2_5 -0.9(11) . . . . ?
N2_5 C15_5 C16_5 C12_5 2.1(11) . . . . ?
C13_5 C12_5 C16_5 C15_5 -1.7(10) . . . . ?
C9_5 C12_5 C16_5 C15_5 179.0(6) . . . . ?
C2_5 C1_5 N1_5 C5_5 -1.4(10) . . . . ?
C2_5 C1_5 N1_5 Cu4 171.7(6) . . . . ?
C4_5 C5_5 N1_5 C1_5 1.8(10) . . . . ?
C4_5 C5_5 N1_5 Cu4 -171.6(5) . . . . ?
C13_5 C14_5 N2_5 C15_5 1.2(10) . . . . ?
C13_5 C14_5 N2_5 Cu6 -170.5(5) . . . . ?
C16_5 C15_5 N2_5 C14_5 -1.7(10) . . . . ?
C16_5 C15_5 N2_5 Cu6 170.2(5) . . . . ?
N1_6 C1_6 C2_6 C3_6 -1.3(11) . . . . ?
C1_6 C2_6 C3_6 C4_6 -0.2(11) . . . . ?
C1_6 C2_6 C3_6 C6_6 178.5(7) . . . . ?
C2_6 C3_6 C4_6 C5_6 1.4(11) . . . . ?
C6_6 C3_6 C4_6 C5_6 -177.3(7) . . . . ?
C3_6 C4_6 C5_6 N1_6 -1.3(11) . . . . ?
C4_6 C3_6 C6_6 C7_6 141.0(8) . . . . ?
C2_6 C3_6 C6_6 C7_6 -37.6(11) . . . . ?
C4_6 C3_6 C6_6 C11_6 -36.4(11) . . . . ?
C2_6 C3_6 C6_6 C11_6 145.0(8) . . . . ?
C11_6 C6_6 C7_6 C8_6 0.7(13) . . . . ?
C3_6 C6_6 C7_6 C8_6 -176.8(8) . . . . ?
C6_6 C7_6 C8_6 C9_6 -1.6(13) . . . . ?
C7_6 C8_6 C9_6 C10_6 1.6(13) . . . . ?
C7_6 C8_6 C9_6 C12_6 179.9(8) . . . . ?
C8_6 C9_6 C10_6 C11_6 -0.9(12) . . . . ?
C12_6 C9_6 C10_6 C11_6 -179.2(7) . . . . ?
C9_6 C10_6 C11_6 C6_6 0.1(12) . . . . ?
C7_6 C6_6 C11_6 C10_6 0.0(12) . . . . ?
C3_6 C6_6 C11_6 C10_6 177.5(7) . . . . ?
C10_6 C9_6 C12_6 C16_6 39.4(11) . . . . ?
C8_6 C9_6 C12_6 C16_6 -138.9(8) . . . . ?
C10_6 C9_6 C12_6 C13_6 -141.5(8) . . . . ?
C8_6 C9_6 C12_6 C13_6 40.2(11) . . . . ?
C16_6 C12_6 C13_6 C14_6 -3.5(11) . . . . ?
C9_6 C12_6 C13_6 C14_6 177.4(7) . . . . ?
C12_6 C13_6 C14_6 N2_6 2.9(11) . . . . ?
C13_6 C12_6 C16_6 C15_6 0.5(11) . . . . ?
C9_6 C12_6 C16_6 C15_6 179.6(7) . . . . ?
N2_6 C15_6 C16_6 C12_6 3.4(12) . . . . ?
C2_6 C1_6 N1_6 C5_6 1.5(10) . . . . ?
C2_6 C1_6 N1_6 Cu3 -175.6(6) . . . . ?
C4_6 C5_6 N1_6 C1_6 -0.1(10) . . . . ?
C4_6 C5_6 N1_6 Cu3 177.1(6) . . . . ?
C16_6 C15_6 N2_6 C14_6 -4.1(11) . . . . ?
C16_6 C15_6 N2_6 Cu6 168.4(6) . . . 7 ?
C13_6 C14_6 N2_6 C15_6 0.9(11) . . . . ?
C13_6 C14_6 N2_6 Cu6 -171.6(6) . . . 7 ?
N1_8 C1_8 C2_8 C3_8 1.3(12) . . . . ?
C1_8 C2_8 C3_8 C4_8 -1.2(11) . . . . ?
C1_8 C2_8 C3_8 C6_8 -179.9(7) . . . . ?
C2_8 C3_8 C4_8 C5_8 0.9(11) . . . . ?
C6_8 C3_8 C4_8 C5_8 179.6(7) . . . . ?
C3_8 C4_8 C5_8 N1_8 -0.6(11) . . . . ?
C2_8 C3_8 C6_8 C11_8 -146.1(8) . . . . ?
C4_8 C3_8 C6_8 C11_8 35.3(10) . . . . ?
C2_8 C3_8 C6_8 C7_8 34.4(11) . . . . ?
C4_8 C3_8 C6_8 C7_8 -144.2(7) . . . . ?
C11_8 C6_8 C7_8 C8_8 -0.2(11) . . . . ?
C3_8 C6_8 C7_8 C8_8 179.3(7) . . . . ?
C6_8 C7_8 C8_8 C9_8 2.7(12) . . . . ?
C7_8 C8_8 C9_8 C10_8 -4.2(11) . . . . ?
C7_8 C8_8 C9_8 C12_8 178.2(7) . . . . ?
C8_8 C9_8 C10_8 C11_8 3.3(12) . . . . ?
C12_8 C9_8 C10_8 C11_8 -178.9(7) . . . . ?
C9_8 C10_8 C11_8 C6_8 -1.0(12) . . . . ?
C7_8 C6_8 C11_8 C10_8 -0.6(11) . . . . ?
C3_8 C6_8 C11_8 C10_8 179.8(7) . . . . ?
C8_8 C9_8 C12_8 C16_8 -143.9(8) . . . . ?
C10_8 C9_8 C12_8 C16_8 38.5(10) . . . . ?
C8_8 C9_8 C12_8 C13_8 36.7(11) . . . . ?
C10_8 C9_8 C12_8 C13_8 -140.9(8) . . . . ?
C16_8 C12_8 C13_8 C14_8 1.3(10) . . . . ?
C9_8 C12_8 C13_8 C14_8 -179.2(7) . . . . ?
C12_8 C13_8 C14_8 N2_8 0.6(11) . . . . ?
C13_8 C12_8 C16_8 C15_8 -2.2(10) . . . . ?
C9_8 C12_8 C16_8 C15_8 178.3(7) . . . . ?
N2_8 C15_8 C16_8 C12_8 1.3(11) . . . . ?
C2_8 C1_8 N1_8 C5_8 -0.9(11) . . . . ?
C2_8 C1_8 N1_8 Cu6 170.1(6) . . . 7 ?
C4_8 C5_8 N1_8 C1_8 0.5(10) . . . . ?
C4_8 C5_8 N1_8 Cu6 -170.7(5) . . . 7 ?
C13_8 C14_8 N2_8 C15_8 -1.6(10) . . . . ?
C13_8 C14_8 N2_8 Cu4 173.6(5) . . . . ?
C16_8 C15_8 N2_8 C14_8 0.7(10) . . . . ?
C16_8 C15_8 N2_8 Cu4 -174.7(5) . . . . ?
N1_9 C1_9 C2_9 C3_9 0.3(11) . . . . ?
C1_9 C2_9 C3_9 C4_9 0.7(10) . . . . ?
C1_9 C2_9 C3_9 C6_9 179.9(6) . . . . ?
C2_9 C3_9 C4_9 C5_9 -0.9(10) . . . . ?
C6_9 C3_9 C4_9 C5_9 179.8(6) . . . . ?
C3_9 C4_9 C5_9 N1_9 0.2(11) . . . . ?
C2_9 C3_9 C6_9 C7_9 -138.7(7) . . . . ?
C4_9 C3_9 C6_9 C7_9 40.5(10) . . . . ?
C2_9 C3_9 C6_9 C11_9 37.5(10) . . . . ?
C4_9 C3_9 C6_9 C11_9 -143.3(7) . . . . ?
C11_9 C6_9 C7_9 C8_9 0.5(11) . . . . ?
C3_9 C6_9 C7_9 C8_9 176.7(6) . . . . ?
C6_9 C7_9 C8_9 C9_9 -1.2(11) . . . . ?
C7_9 C8_9 C9_9 C10_9 2.3(11) . . . . ?
C7_9 C8_9 C9_9 C12_9 179.2(7) . . . . ?
C8_9 C9_9 C10_9 C11_9 -2.8(11) . . . . ?
C12_9 C9_9 C10_9 C11_9 -179.7(7) . . . . ?
C9_9 C10_9 C11_9 C6_9 2.2(11) . . . . ?
C7_9 C6_9 C11_9 C10_9 -1.0(11) . . . . ?
C3_9 C6_9 C11_9 C10_9 -177.2(7) . . . . ?
C8_9 C9_9 C12_9 C16_9 151.0(7) . . . . ?
C10_9 C9_9 C12_9 C16_9 -32.1(10) . . . . ?
C8_9 C9_9 C12_9 C13_9 -30.5(10) . . . . ?
C10_9 C9_9 C12_9 C13_9 146.4(7) . . . . ?
C16_9 C12_9 C13_9 C14_9 1.6(10) . . . . ?
C9_9 C12_9 C13_9 C14_9 -177.0(6) . . . . ?
C12_9 C13_9 C14_9 N2_9 -0.3(11) . . . . ?
N2_9 C15_9 C16_9 C12_9 0.6(12) . . . . ?
C13_9 C12_9 C16_9 C15_9 -1.7(11) . . . . ?
C9_9 C12_9 C16_9 C15_9 176.9(7) . . . . ?
C2_9 C1_9 N1_9 C5_9 -1.1(10) . . . . ?
C2_9 C1_9 N1_9 Cu2 -175.1(6) . . . . ?
C4_9 C5_9 N1_9 C1_9 0.9(10) . . . . ?
C4_9 C5_9 N1_9 Cu2 174.4(5) . . . . ?
C16_9 C15_9 N2_9 C14_9 0.7(11) . . . . ?
C16_9 C15_9 N2_9 Cu5 -171.9(6) . . . . ?
C13_9 C14_9 N2_9 C15_9 -0.8(11) . . . . ?
C13_9 C14_9 N2_9 Cu5 171.9(5) . . . . ?
B4_10 B1_10 B2_10 B10_10 -0.9(8) . . . . ?
B3_10 B1_10 B2_10 B10_10 37.3(6) . . . . ?
B6_10 B1_10 B2_10 B10_10 -64.9(8) . . . . ?
B5_10 B1_10 B2_10 B10_10 -102.4(6) . . . . ?
Cl1_10 B1_10 B2_10 B10_10 149.0(6) . . . . ?
B4_10 B1_10 B2_10 B3_10 -38.2(6) . . . . ?
B6_10 B1_10 B2_10 B3_10 -102.2(6) . . . . ?
B5_10 B1_10 B2_10 B3_10 -139.7(6) . . . . ?
Cl1_10 B1_10 B2_10 B3_10 111.7(7) . . . . ?
B4_10 B1_10 B2_10 B11_10 63.2(8) . . . . ?
B3_10 B1_10 B2_10 B11_10 101.4(6) . . . . ?
B6_10 B1_10 B2_10 B11_10 -0.7(8) . . . . ?
B5_10 B1_10 B2_10 B11_10 -38.2(6) . . . . ?
Cl1_10 B1_10 B2_10 B11_10 -146.9(6) . . . . ?
B4_10 B1_10 B2_10 B5_10 101.4(6) . . . . ?
B3_10 B1_10 B2_10 B5_10 139.7(6) . . . . ?
B6_10 B1_10 B2_10 B5_10 37.5(6) . . . . ?
Cl1_10 B1_10 B2_10 B5_10 -108.7(7) . . . . ?
B4_10 B1_10 B2_10 Cl3_10 -153.1(6) . . . . ?
B3_10 B1_10 B2_10 Cl3_10 -114.8(7) . . . . ?
B6_10 B1_10 B2_10 Cl3_10 143.0(6) . . . . ?
B5_10 B1_10 B2_10 Cl3_10 105.5(7) . . . . ?
Cl1_10 B1_10 B2_10 Cl3_10 -3.2(10) . . . . ?
B6_10 B1_10 B3_10 B4_10 -37.6(6) . . . . ?
B2_10 B1_10 B3_10 B4_10 -137.6(6) . . . . ?
B5_10 B1_10 B3_10 B4_10 -101.4(6) . . . . ?
Cl1_10 B1_10 B3_10 B4_10 111.1(7) . . . . ?
B4_10 B1_10 B3_10 Cl4_10 -108.3(7) . . . . ?
B6_10 B1_10 B3_10 Cl4_10 -146.0(6) . . . . ?
B2_10 B1_10 B3_10 Cl4_10 114.0(7) . . . . ?
B5_10 B1_10 B3_10 Cl4_10 150.3(6) . . . . ?
Cl1_10 B1_10 B3_10 Cl4_10 2.7(9) . . . . ?
B4_10 B1_10 B3_10 B9_10 37.6(5) . . . . ?
B6_10 B1_10 B3_10 B9_10 0.0(8) . . . . ?
B2_10 B1_10 B3_10 B9_10 -100.0(6) . . . . ?
B5_10 B1_10 B3_10 B9_10 -63.7(7) . . . . ?
Cl1_10 B1_10 B3_10 B9_10 148.7(5) . . . . ?
B4_10 B1_10 B3_10 B2_10 137.6(6) . . . . ?
B6_10 B1_10 B3_10 B2_10 100.0(6) . . . . ?
B5_10 B1_10 B3_10 B2_10 36.2(5) . . . . ?
Cl1_10 B1_10 B3_10 B2_10 -111.3(7) . . . . ?
B4_10 B1_10 B3_10 B10_10 100.9(6) . . . . ?
B6_10 B1_10 B3_10 B10_10 63.2(7) . . . . ?
B2_10 B1_10 B3_10 B10_10 -36.7(5) . . . . ?
B5_10 B1_10 B3_10 B10_10 -0.5(7) . . . . ?
Cl1_10 B1_10 B3_10 B10_10 -148.1(5) . . . . ?
B10_10 B2_10 B3_10 B1_10 -138.8(6) . . . . ?
B11_10 B2_10 B3_10 B1_10 -100.4(6) . . . . ?
B5_10 B2_10 B3_10 B1_10 -36.3(5) . . . . ?
Cl3_10 B2_10 B3_10 B1_10 109.9(7) . . . . ?
B10_10 B2_10 B3_10 B4_10 -101.4(6) . . . . ?
B11_10 B2_10 B3_10 B4_10 -63.0(7) . . . . ?
B5_10 B2_10 B3_10 B4_10 1.1(7) . . . . ?
B1_10 B2_10 B3_10 B4_10 37.4(5) . . . . ?
Cl3_10 B2_10 B3_10 B4_10 147.2(6) . . . . ?
B10_10 B2_10 B3_10 Cl4_10 108.8(7) . . . . ?
B11_10 B2_10 B3_10 Cl4_10 147.2(6) . . . . ?
B5_10 B2_10 B3_10 Cl4_10 -148.6(6) . . . . ?
B1_10 B2_10 B3_10 Cl4_10 -112.4(7) . . . . ?
Cl3_10 B2_10 B3_10 Cl4_10 -2.5(10) . . . . ?
B10_10 B2_10 B3_10 B9_10 -37.3(5) . . . . ?
B11_10 B2_10 B3_10 B9_10 1.0(7) . . . . ?
B5_10 B2_10 B3_10 B9_10 65.2(7) . . . . ?
B1_10 B2_10 B3_10 B9_10 101.4(6) . . . . ?
Cl3_10 B2_10 B3_10 B9_10 -148.7(6) . . . . ?
B11_10 B2_10 B3_10 B10_10 38.4(5) . . . . ?
B5_10 B2_10 B3_10 B10_10 102.5(6) . . . . ?
B1_10 B2_10 B3_10 B10_10 138.8(6) . . . . ?
Cl3_10 B2_10 B3_10 B10_10 -111.4(7) . . . . ?
B6_10 B1_10 B4_10 B3_10 138.4(6) . . . . ?
B2_10 B1_10 B4_10 B3_10 38.1(6) . . . . ?
B5_10 B1_10 B4_10 B3_10 101.5(6) . . . . ?
Cl1_10 B1_10 B4_10 B3_10 -112.0(7) . . . . ?
B3_10 B1_10 B4_10 B6_10 -138.4(6) . . . . ?
B2_10 B1_10 B4_10 B6_10 -100.3(6) . . . . ?
B5_10 B1_10 B4_10 B6_10 -36.9(5) . . . . ?
Cl1_10 B1_10 B4_10 B6_10 109.6(7) . . . . ?
B3_10 B1_10 B4_10 B8_10 -100.8(6) . . . . ?
B6_10 B1_10 B4_10 B8_10 37.6(5) . . . . ?
B2_10 B1_10 B4_10 B8_10 -62.7(7) . . . . ?
B5_10 B1_10 B4_10 B8_10 0.7(8) . . . . ?
Cl1_10 B1_10 B4_10 B8_10 147.2(6) . . . . ?
B3_10 B1_10 B4_10 Cl6_10 109.7(7) . . . . ?
B6_10 B1_10 B4_10 Cl6_10 -111.8(7) . . . . ?
B2_10 B1_10 B4_10 Cl6_10 147.8(6) . . . . ?
B5_10 B1_10 B4_10 Cl6_10 -148.7(6) . . . . ?
Cl1_10 B1_10 B4_10 Cl6_10 -2.2(10) . . . . ?
B3_10 B1_10 B4_10 B9_10 -37.3(5) . . . . ?
B6_10 B1_10 B4_10 B9_10 101.1(6) . . . . ?
B2_10 B1_10 B4_10 B9_10 0.8(8) . . . . ?
B5_10 B1_10 B4_10 B9_10 64.3(7) . . . . ?
Cl1_10 B1_10 B4_10 B9_10 -149.2(6) . . . . ?
Cl4_10 B3_10 B4_10 B1_10 113.1(7) . . . . ?
B9_10 B3_10 B4_10 B1_10 -138.3(6) . . . . ?
B2_10 B3_10 B4_10 B1_10 -38.1(6) . . . . ?
B10_10 B3_10 B4_10 B1_10 -100.9(6) . . . . ?
B1_10 B3_10 B4_10 B6_10 37.6(6) . . . . ?
Cl4_10 B3_10 B4_10 B6_10 150.8(6) . . . . ?
B9_10 B3_10 B4_10 B6_10 -100.7(6) . . . . ?
B2_10 B3_10 B4_10 B6_10 -0.4(8) . . . . ?
B10_10 B3_10 B4_10 B6_10 -63.3(7) . . . . ?
B1_10 B3_10 B4_10 B8_10 101.7(6) . . . . ?
Cl4_10 B3_10 B4_10 B8_10 -145.2(6) . . . . ?
B9_10 B3_10 B4_10 B8_10 -36.7(5) . . . . ?
B2_10 B3_10 B4_10 B8_10 63.6(7) . . . . ?
B10_10 B3_10 B4_10 B8_10 0.8(8) . . . . ?
B1_10 B3_10 B4_10 Cl6_10 -112.5(7) . . . . ?
Cl4_10 B3_10 B4_10 Cl6_10 0.6(9) . . . . ?
B9_10 B3_10 B4_10 Cl6_10 109.2(7) . . . . ?
B2_10 B3_10 B4_10 Cl6_10 -150.6(5) . . . . ?
B10_10 B3_10 B4_10 Cl6_10 146.6(6) . . . . ?
B1_10 B3_10 B4_10 B9_10 138.3(6) . . . . ?
Cl4_10 B3_10 B4_10 B9_10 -108.5(6) . . . . ?
B2_10 B3_10 B4_10 B9_10 100.3(6) . . . . ?
B10_10 B3_10 B4_10 B9_10 37.5(5) . . . . ?
B10_10 B2_10 B5_10 Cl2_10 -146.7(6) . . . . ?
B3_10 B2_10 B5_10 Cl2_10 148.6(6) . . . . ?
B11_10 B2_10 B5_10 Cl2_10 -109.7(7) . . . . ?
B1_10 B2_10 B5_10 Cl2_10 112.8(7) . . . . ?
Cl3_10 B2_10 B5_10 Cl2_10 -0.5(9) . . . . ?
B10_10 B2_10 B5_10 B7_10 0.0(8) . . . . ?
B3_10 B2_10 B5_10 B7_10 -64.6(7) . . . . ?
B11_10 B2_10 B5_10 B7_10 37.1(5) . . . . ?
B1_10 B2_10 B5_10 B7_10 -100.4(6) . . . . ?
Cl3_10 B2_10 B5_10 B7_10 146.2(5) . . . . ?
B10_10 B2_10 B5_10 B6_10 63.3(7) . . . . ?
B3_10 B2_10 B5_10 B6_10 -1.4(7) . . . . ?
B11_10 B2_10 B5_10 B6_10 100.3(6) . . . . ?
B1_10 B2_10 B5_10 B6_10 -37.2(6) . . . . ?
Cl3_10 B2_10 B5_10 B6_10 -150.5(5) . . . . ?
B10_10 B2_10 B5_10 B1_10 100.5(6) . . . . ?
B3_10 B2_10 B5_10 B1_10 35.8(5) . . . . ?
B11_10 B2_10 B5_10 B1_10 137.5(6) . . . . ?
Cl3_10 B2_10 B5_10 B1_10 -113.4(6) . . . . ?
B10_10 B2_10 B5_10 B11_10 -37.0(5) . . . . ?
B3_10 B2_10 B5_10 B11_10 -101.7(6) . . . . ?
B1_10 B2_10 B5_10 B11_10 -137.5(6) . . . . ?
Cl3_10 B2_10 B5_10 B11_10 109.1(6) . . . . ?
B4_10 B1_10 B5_10 Cl2_10 150.6(6) . . . . ?
B3_10 B1_10 B5_10 Cl2_10 -145.0(6) . . . . ?
B6_10 B1_10 B5_10 Cl2_10 113.5(7) . . . . ?
B2_10 B1_10 B5_10 Cl2_10 -108.6(7) . . . . ?
Cl1_10 B1_10 B5_10 Cl2_10 3.4(9) . . . . ?
B4_10 B1_10 B5_10 B7_10 -0.3(8) . . . . ?
B3_10 B1_10 B5_10 B7_10 64.1(7) . . . . ?
B6_10 B1_10 B5_10 B7_10 -37.4(6) . . . . ?
B2_10 B1_10 B5_10 B7_10 100.5(6) . . . . ?
Cl1_10 B1_10 B5_10 B7_10 -147.4(6) . . . . ?
B4_10 B1_10 B5_10 B6_10 37.1(6) . . . . ?
B3_10 B1_10 B5_10 B6_10 101.5(6) . . . . ?
B2_10 B1_10 B5_10 B6_10 137.9(6) . . . . ?
Cl1_10 B1_10 B5_10 B6_10 -110.0(7) . . . . ?
B4_10 B1_10 B5_10 B2_10 -100.8(6) . . . . ?
B3_10 B1_10 B5_10 B2_10 -36.4(5) . . . . ?
B6_10 B1_10 B5_10 B2_10 -137.9(6) . . . . ?
Cl1_10 B1_10 B5_10 B2_10 112.0(6) . . . . ?
B4_10 B1_10 B5_10 B11_10 -63.1(7) . . . . ?
B3_10 B1_10 B5_10 B11_10 1.3(7) . . . . ?
B6_10 B1_10 B5_10 B11_10 -100.2(6) . . . . ?
B2_10 B1_10 B5_10 B11_10 37.7(5) . . . . ?
Cl1_10 B1_10 B5_10 B11_10 149.8(5) . . . . ?
B3_10 B4_10 B6_10 B1_10 -37.5(6) . . . . ?
B8_10 B4_10 B6_10 B1_10 -138.3(6) . . . . ?
Cl6_10 B4_10 B6_10 B1_10 112.1(7) . . . . ?
B9_10 B4_10 B6_10 B1_10 -101.0(6) . . . . ?
B1_10 B4_10 B6_10 B7_10 100.4(6) . . . . ?
B3_10 B4_10 B6_10 B7_10 62.9(8) . . . . ?
B8_10 B4_10 B6_10 B7_10 -38.0(5) . . . . ?
Cl6_10 B4_10 B6_10 B7_10 -147.5(5) . . . . ?
B9_10 B4_10 B6_10 B7_10 -0.6(8) . . . . ?
B1_10 B4_10 B6_10 B8_10 138.3(6) . . . . ?
B3_10 B4_10 B6_10 B8_10 100.9(6) . . . . ?
Cl6_10 B4_10 B6_10 B8_10 -109.6(7) . . . . ?
B9_10 B4_10 B6_10 B8_10 37.3(5) . . . . ?
B1_10 B4_10 B6_10 B5_10 37.1(6) . . . . ?
B3_10 B4_10 B6_10 B5_10 -0.4(8) . . . . ?
B8_10 B4_10 B6_10 B5_10 -101.3(6) . . . . ?
Cl6_10 B4_10 B6_10 B5_10 149.2(5) . . . . ?
B9_10 B4_10 B6_10 B5_10 -63.9(7) . . . . ?
B1_10 B4_10 B6_10 Cl5_10 -110.6(7) . . . . ?
B3_10 B4_10 B6_10 Cl5_10 -148.1(6) . . . . ?
B8_10 B4_10 B6_10 Cl5_10 111.0(7) . . . . ?
Cl6_10 B4_10 B6_10 Cl5_10 1.5(10) . . . . ?
B9_10 B4_10 B6_10 Cl5_10 148.4(5) . . . . ?
B3_10 B1_10 B6_10 B4_10 37.7(5) . . . . ?
B2_10 B1_10 B6_10 B4_10 101.5(6) . . . . ?
B5_10 B1_10 B6_10 B4_10 138.9(6) . . . . ?
Cl1_10 B1_10 B6_10 B4_10 -111.7(7) . . . . ?
B4_10 B1_10 B6_10 B7_10 -101.5(6) . . . . ?
B3_10 B1_10 B6_10 B7_10 -63.8(7) . . . . ?
B2_10 B1_10 B6_10 B7_10 0.0(8) . . . . ?
B5_10 B1_10 B6_10 B7_10 37.4(6) . . . . ?
Cl1_10 B1_10 B6_10 B7_10 146.8(6) . . . . ?
B4_10 B1_10 B6_10 B8_10 -37.0(5) . . . . ?
B3_10 B1_10 B6_10 B8_10 0.7(8) . . . . ?
B2_10 B1_10 B6_10 B8_10 64.5(7) . . . . ?
B5_10 B1_10 B6_10 B8_10 102.0(6) . . . . ?
Cl1_10 B1_10 B6_10 B8_10 -148.6(6) . . . . ?
B4_10 B1_10 B6_10 B5_10 -138.9(6) . . . . ?
B3_10 B1_10 B6_10 B5_10 -101.2(6) . . . . ?
B2_10 B1_10 B6_10 B5_10 -37.4(6) . . . . ?
Cl1_10 B1_10 B6_10 B5_10 109.4(7) . . . . ?
B4_10 B1_10 B6_10 Cl5_10 110.5(7) . . . . ?
B3_10 B1_10 B6_10 Cl5_10 148.2(6) . . . . ?
B2_10 B1_10 B6_10 Cl5_10 -148.0(6) . . . . ?
B5_10 B1_10 B6_10 Cl5_10 -110.6(7) . . . . ?
Cl1_10 B1_10 B6_10 Cl5_10 -1.2(9) . . . . ?
Cl2_10 B5_10 B6_10 B4_10 -147.4(6) . . . . ?
B7_10 B5_10 B6_10 B4_10 101.7(6) . . . . ?
B2_10 B5_10 B6_10 B4_10 1.1(8) . . . . ?
B1_10 B5_10 B6_10 B4_10 -36.3(6) . . . . ?
B11_10 B5_10 B6_10 B4_10 64.0(7) . . . . ?
Cl2_10 B5_10 B6_10 B1_10 -111.0(7) . . . . ?
B7_10 B5_10 B6_10 B1_10 138.0(6) . . . . ?
B2_10 B5_10 B6_10 B1_10 37.4(5) . . . . ?
B11_10 B5_10 B6_10 B1_10 100.4(6) . . . . ?
Cl2_10 B5_10 B6_10 B7_10 110.9(7) . . . . ?
B2_10 B5_10 B6_10 B7_10 -100.6(6) . . . . ?
B1_10 B5_10 B6_10 B7_10 -138.0(6) . . . . ?
B11_10 B5_10 B6_10 B7_10 -37.7(5) . . . . ?
Cl2_10 B5_10 B6_10 B8_10 149.2(6) . . . . ?
B7_10 B5_10 B6_10 B8_10 38.3(6) . . . . ?
B2_10 B5_10 B6_10 B8_10 -62.3(7) . . . . ?
B1_10 B5_10 B6_10 B8_10 -99.7(6) . . . . ?
B11_10 B5_10 B6_10 B8_10 0.6(8) . . . . ?
Cl2_10 B5_10 B6_10 Cl5_10 0.5(10) . . . . ?
B7_10 B5_10 B6_10 Cl5_10 -110.4(7) . . . . ?
B2_10 B5_10 B6_10 Cl5_10 148.9(6) . . . . ?
B1_10 B5_10 B6_10 Cl5_10 111.5(7) . . . . ?
B11_10 B5_10 B6_10 Cl5_10 -148.1(6) . . . . ?
Cl2_10 B5_10 B7_10 Cl11_10 -3.8(9) . . . . ?
B6_10 B5_10 B7_10 Cl11_10 110.1(7) . . . . ?
B2_10 B5_10 B7_10 Cl11_10 -149.7(5) . . . . ?
B1_10 B5_10 B7_10 Cl11_10 147.2(5) . . . . ?
B11_10 B5_10 B7_10 Cl11_10 -112.5(6) . . . . ?
Cl2_10 B5_10 B7_10 B11_10 108.7(7) . . . . ?
B6_10 B5_10 B7_10 B11_10 -137.5(6) . . . . ?
B2_10 B5_10 B7_10 B11_10 -37.2(5) . . . . ?
B1_10 B5_10 B7_10 B11_10 -100.3(6) . . . . ?
Cl2_10 B5_10 B7_10 B6_10 -113.9(7) . . . . ?
B2_10 B5_10 B7_10 B6_10 100.3(6) . . . . ?
B1_10 B5_10 B7_10 B6_10 37.1(6) . . . . ?
B11_10 B5_10 B7_10 B6_10 137.5(6) . . . . ?
Cl2_10 B5_10 B7_10 B12_10 146.6(6) . . . . ?
B6_10 B5_10 B7_10 B12_10 -99.5(6) . . . . ?
B2_10 B5_10 B7_10 B12_10 0.8(8) . . . . ?
B1_10 B5_10 B7_10 B12_10 -62.4(7) . . . . ?
B11_10 B5_10 B7_10 B12_10 38.0(5) . . . . ?
Cl2_10 B5_10 B7_10 B8_10 -151.3(5) . . . . ?
B6_10 B5_10 B7_10 B8_10 -37.4(5) . . . . ?
B2_10 B5_10 B7_10 B8_10 62.9(7) . . . . ?
B1_10 B5_10 B7_10 B8_10 -0.3(8) . . . . ?
B11_10 B5_10 B7_10 B8_10 100.1(6) . . . . ?
B4_10 B6_10 B7_10 Cl11_10 151.0(5) . . . . ?
B1_10 B6_10 B7_10 Cl11_10 -146.4(6) . . . . ?
B8_10 B6_10 B7_10 Cl11_10 113.6(6) . . . . ?
B5_10 B6_10 B7_10 Cl11_10 -108.6(6) . . . . ?
Cl5_10 B6_10 B7_10 Cl11_10 1.8(9) . . . . ?
B4_10 B6_10 B7_10 B5_10 -100.4(6) . . . . ?
B1_10 B6_10 B7_10 B5_10 -37.9(6) . . . . ?
B8_10 B6_10 B7_10 B5_10 -137.8(6) . . . . ?
Cl5_10 B6_10 B7_10 B5_10 110.4(7) . . . . ?
B4_10 B6_10 B7_10 B11_10 -61.8(7) . . . . ?
B1_10 B6_10 B7_10 B11_10 0.7(8) . . . . ?
B8_10 B6_10 B7_10 B11_10 -99.2(6) . . . . ?
B5_10 B6_10 B7_10 B11_10 38.6(5) . . . . ?
Cl5_10 B6_10 B7_10 B11_10 149.0(6) . . . . ?
B4_10 B6_10 B7_10 B12_10 1.0(8) . . . . ?
B1_10 B6_10 B7_10 B12_10 63.5(7) . . . . ?
B8_10 B6_10 B7_10 B12_10 -36.4(5) . . . . ?
B5_10 B6_10 B7_10 B12_10 101.4(6) . . . . ?
Cl5_10 B6_10 B7_10 B12_10 -148.2(6) . . . . ?
B4_10 B6_10 B7_10 B8_10 37.4(6) . . . . ?
B1_10 B6_10 B7_10 B8_10 100.0(6) . . . . ?
B5_10 B6_10 B7_10 B8_10 137.8(6) . . . . ?
Cl5_10 B6_10 B7_10 B8_10 -111.8(7) . . . . ?
B1_10 B4_10 B8_10 B12_10 62.9(7) . . . . ?
B3_10 B4_10 B8_10 B12_10 -0.9(8) . . . . ?
B6_10 B4_10 B8_10 B12_10 100.6(6) . . . . ?
Cl6_10 B4_10 B8_10 B12_10 -146.9(6) . . . . ?
B9_10 B4_10 B8_10 B12_10 -37.6(5) . . . . ?
B1_10 B4_10 B8_10 B9_10 100.6(6) . . . . ?
B3_10 B4_10 B8_10 B9_10 36.7(5) . . . . ?
B6_10 B4_10 B8_10 B9_10 138.2(6) . . . . ?
Cl6_10 B4_10 B8_10 B9_10 -109.3(7) . . . . ?
B1_10 B4_10 B8_10 B6_10 -37.7(5) . . . . ?
B3_10 B4_10 B8_10 B6_10 -101.6(6) . . . . ?
Cl6_10 B4_10 B8_10 B6_10 112.5(7) . . . . ?
B9_10 B4_10 B8_10 B6_10 -138.2(6) . . . . ?
B1_10 B4_10 B8_10 Cl12_10 -147.6(6) . . . . ?
B3_10 B4_10 B8_10 Cl12_10 148.5(6) . . . . ?
B6_10 B4_10 B8_10 Cl12_10 -109.9(7) . . . . ?
Cl6_10 B4_10 B8_10 Cl12_10 2.6(9) . . . . ?
B9_10 B4_10 B8_10 Cl12_10 111.9(7) . . . . ?
B1_10 B4_10 B8_10 B7_10 -0.9(7) . . . . ?
B3_10 B4_10 B8_10 B7_10 -64.8(7) . . . . ?
B6_10 B4_10 B8_10 B7_10 36.8(5) . . . . ?
Cl6_10 B4_10 B8_10 B7_10 149.3(5) . . . . ?
B9_10 B4_10 B8_10 B7_10 -101.5(6) . . . . ?
B1_10 B6_10 B8_10 B4_10 36.6(5) . . . . ?
B7_10 B6_10 B8_10 B4_10 138.3(6) . . . . ?
B5_10 B6_10 B8_10 B4_10 100.7(6) . . . . ?
Cl5_10 B6_10 B8_10 B4_10 -110.8(7) . . . . ?
B4_10 B6_10 B8_10 B12_10 -100.9(6) . . . . ?
B1_10 B6_10 B8_10 B12_10 -64.3(7) . . . . ?
B7_10 B6_10 B8_10 B12_10 37.4(6) . . . . ?
B5_10 B6_10 B8_10 B12_10 -0.3(8) . . . . ?
Cl5_10 B6_10 B8_10 B12_10 148.2(6) . . . . ?
B4_10 B6_10 B8_10 B9_10 -37.8(5) . . . . ?
B1_10 B6_10 B8_10 B9_10 -1.2(7) . . . . ?
B7_10 B6_10 B8_10 B9_10 100.6(6) . . . . ?
B5_10 B6_10 B8_10 B9_10 62.9(7) . . . . ?
Cl5_10 B6_10 B8_10 B9_10 -148.6(6) . . . . ?
B4_10 B6_10 B8_10 Cl12_10 110.9(7) . . . . ?
B1_10 B6_10 B8_10 Cl12_10 147.5(6) . . . . ?
B7_10 B6_10 B8_10 Cl12_10 -110.7(7) . . . . ?
B5_10 B6_10 B8_10 Cl12_10 -148.4(6) . . . . ?
Cl5_10 B6_10 B8_10 Cl12_10 0.1(10) . . . . ?
B4_10 B6_10 B8_10 B7_10 -138.3(6) . . . . ?
B1_10 B6_10 B8_10 B7_10 -101.8(6) . . . . ?
B5_10 B6_10 B8_10 B7_10 -37.7(6) . . . . ?
Cl5_10 B6_10 B8_10 B7_10 110.8(7) . . . . ?
Cl11_10 B7_10 B8_10 B4_10 -145.0(6) . . . . ?
B5_10 B7_10 B8_10 B4_10 0.7(7) . . . . ?
B11_10 B7_10 B8_10 B4_10 64.9(7) . . . . ?
B6_10 B7_10 B8_10 B4_10 -37.0(5) . . . . ?
B12_10 B7_10 B8_10 B4_10 101.4(6) . . . . ?
Cl11_10 B7_10 B8_10 B12_10 113.6(7) . . . . ?
B5_10 B7_10 B8_10 B12_10 -100.7(6) . . . . ?
B11_10 B7_10 B8_10 B12_10 -36.5(5) . . . . ?
B6_10 B7_10 B8_10 B12_10 -138.4(6) . . . . ?
Cl11_10 B7_10 B8_10 B9_10 150.9(6) . . . . ?
B5_10 B7_10 B8_10 B9_10 -63.4(7) . . . . ?
B11_10 B7_10 B8_10 B9_10 0.8(7) . . . . ?
B6_10 B7_10 B8_10 B9_10 -101.1(6) . . . . ?
B12_10 B7_10 B8_10 B9_10 37.3(5) . . . . ?
Cl11_10 B7_10 B8_10 B6_10 -108.0(7) . . . . ?
B5_10 B7_10 B8_10 B6_10 37.7(5) . . . . ?
B11_10 B7_10 B8_10 B6_10 101.9(6) . . . . ?
B12_10 B7_10 B8_10 B6_10 138.4(6) . . . . ?
Cl11_10 B7_10 B8_10 Cl12_10 1.7(9) . . . . ?
B5_10 B7_10 B8_10 Cl12_10 147.4(5) . . . . ?
B11_10 B7_10 B8_10 Cl12_10 -148.4(5) . . . . ?
B6_10 B7_10 B8_10 Cl12_10 109.7(6) . . . . ?
B12_10 B7_10 B8_10 Cl12_10 -111.9(6) . . . . ?
B4_10 B8_10 B9_10 B12_10 -137.8(6) . . . . ?
B6_10 B8_10 B9_10 B12_10 -100.5(6) . . . . ?
Cl12_10 B8_10 B9_10 B12_10 111.3(6) . . . . ?
B7_10 B8_10 B9_10 B12_10 -37.6(5) . . . . ?
B4_10 B8_10 B9_10 Cl7_10 114.0(6) . . . . ?
B12_10 B8_10 B9_10 Cl7_10 -108.2(6) . . . . ?
B6_10 B8_10 B9_10 Cl7_10 151.3(5) . . . . ?
Cl12_10 B8_10 B9_10 Cl7_10 3.1(9) . . . . ?
B7_10 B8_10 B9_10 Cl7_10 -145.8(5) . . . . ?
B4_10 B8_10 B9_10 B3_10 -36.2(5) . . . . ?
B12_10 B8_10 B9_10 B3_10 101.6(6) . . . . ?
B6_10 B8_10 B9_10 B3_10 1.2(7) . . . . ?
Cl12_10 B8_10 B9_10 B3_10 -147.1(5) . . . . ?
B7_10 B8_10 B9_10 B3_10 64.0(7) . . . . ?
B4_10 B8_10 B9_10 B10_10 -100.3(6) . . . . ?
B12_10 B8_10 B9_10 B10_10 37.5(5) . . . . ?
B6_10 B8_10 B9_10 B10_10 -63.0(7) . . . . ?
Cl12_10 B8_10 B9_10 B10_10 148.8(5) . . . . ?
B7_10 B8_10 B9_10 B10_10 -0.1(7) . . . . ?
B12_10 B8_10 B9_10 B4_10 137.8(6) . . . . ?
B6_10 B8_10 B9_10 B4_10 37.3(5) . . . . ?
Cl12_10 B8_10 B9_10 B4_10 -110.9(6) . . . . ?
B7_10 B8_10 B9_10 B4_10 100.2(6) . . . . ?
B1_10 B3_10 B9_10 B12_10 62.7(7) . . . . ?
B4_10 B3_10 B9_10 B12_10 99.6(6) . . . . ?
Cl4_10 B3_10 B9_10 B12_10 -149.6(5) . . . . ?
B2_10 B3_10 B9_10 B12_10 -1.3(7) . . . . ?
B10_10 B3_10 B9_10 B12_10 -38.5(5) . . . . ?
B1_10 B3_10 B9_10 Cl7_10 -150.2(5) . . . . ?
B4_10 B3_10 B9_10 Cl7_10 -113.2(6) . . . . ?
Cl4_10 B3_10 B9_10 Cl7_10 -2.5(9) . . . . ?
B2_10 B3_10 B9_10 Cl7_10 145.9(5) . . . . ?
B10_10 B3_10 B9_10 Cl7_10 108.7(6) . . . . ?
B1_10 B3_10 B9_10 B8_10 -0.7(7) . . . . ?
B4_10 B3_10 B9_10 B8_10 36.2(5) . . . . ?
Cl4_10 B3_10 B9_10 B8_10 147.0(5) . . . . ?
B2_10 B3_10 B9_10 B8_10 -64.7(7) . . . . ?
B10_10 B3_10 B9_10 B8_10 -101.9(6) . . . . ?
B1_10 B3_10 B9_10 B10_10 101.2(6) . . . . ?
B4_10 B3_10 B9_10 B10_10 138.1(6) . . . . ?
Cl4_10 B3_10 B9_10 B10_10 -111.1(6) . . . . ?
B2_10 B3_10 B9_10 B10_10 37.2(5) . . . . ?
B1_10 B3_10 B9_10 B4_10 -36.9(5) . . . . ?
Cl4_10 B3_10 B9_10 B4_10 110.8(6) . . . . ?
B2_10 B3_10 B9_10 B4_10 -100.9(6) . . . . ?
B10_10 B3_10 B9_10 B4_10 -138.1(6) . . . . ?
B1_10 B4_10 B9_10 B12_10 -64.1(7) . . . . ?
B3_10 B4_10 B9_10 B12_10 -101.5(6) . . . . ?
B6_10 B4_10 B9_10 B12_10 0.0(7) . . . . ?
B8_10 B4_10 B9_10 B12_10 37.6(5) . . . . ?
Cl6_10 B4_10 B9_10 B12_10 147.9(5) . . . . ?
B1_10 B4_10 B9_10 Cl7_10 149.1(6) . . . . ?
B3_10 B4_10 B9_10 Cl7_10 111.7(7) . . . . ?
B6_10 B4_10 B9_10 Cl7_10 -146.8(6) . . . . ?
B8_10 B4_10 B9_10 Cl7_10 -109.2(7) . . . . ?
Cl6_10 B4_10 B9_10 Cl7_10 1.1(9) . . . . ?
B1_10 B4_10 B9_10 B8_10 -101.7(6) . . . . ?
B3_10 B4_10 B9_10 B8_10 -139.0(6) . . . . ?
B6_10 B4_10 B9_10 B8_10 -37.6(5) . . . . ?
Cl6_10 B4_10 B9_10 B8_10 110.3(6) . . . . ?
B1_10 B4_10 B9_10 B3_10 37.4(6) . . . . ?
B6_10 B4_10 B9_10 B3_10 101.5(6) . . . . ?
B8_10 B4_10 B9_10 B3_10 139.0(6) . . . . ?
Cl6_10 B4_10 B9_10 B3_10 -110.6(7) . . . . ?
B1_10 B4_10 B9_10 B10_10 -0.3(8) . . . . ?
B3_10 B4_10 B9_10 B10_10 -37.7(5) . . . . ?
B6_10 B4_10 B9_10 B10_10 63.8(7) . . . . ?
B8_10 B4_10 B9_10 B10_10 101.3(6) . . . . ?
Cl6_10 B4_10 B9_10 B10_10 -148.4(6) . . . . ?
B3_10 B2_10 B10_10 Cl8_10 -110.6(7) . . . . ?
B11_10 B2_10 B10_10 Cl8_10 111.9(7) . . . . ?
B5_10 B2_10 B10_10 Cl8_10 148.9(6) . . . . ?
B1_10 B2_10 B10_10 Cl8_10 -147.1(6) . . . . ?
Cl3_10 B2_10 B10_10 Cl8_10 4.8(9) . . . . ?
B3_10 B2_10 B10_10 B9_10 37.3(5) . . . . ?
B11_10 B2_10 B10_10 B9_10 -100.3(6) . . . . ?
B5_10 B2_10 B10_10 B9_10 -63.3(7) . . . . ?
B1_10 B2_10 B10_10 B9_10 0.7(8) . . . . ?
Cl3_10 B2_10 B10_10 B9_10 152.7(6) . . . . ?
B3_10 B2_10 B10_10 B12_10 99.7(6) . . . . ?
B11_10 B2_10 B10_10 B12_10 -37.8(5) . . . . ?
B5_10 B2_10 B10_10 B12_10 -0.9(7) . . . . ?
B1_10 B2_10 B10_10 B12_10 63.2(7) . . . . ?
Cl3_10 B2_10 B10_10 B12_10 -144.9(6) . . . . ?
B3_10 B2_10 B10_10 B11_10 137.6(6) . . . . ?
B5_10 B2_10 B10_10 B11_10 37.0(5) . . . . ?
B1_10 B2_10 B10_10 B11_10 101.0(6) . . . . ?
Cl3_10 B2_10 B10_10 B11_10 -107.0(7) . . . . ?
B11_10 B2_10 B10_10 B3_10 -137.6(6) . . . . ?
B5_10 B2_10 B10_10 B3_10 -100.6(6) . . . . ?
B1_10 B2_10 B10_10 B3_10 -36.6(6) . . . . ?
Cl3_10 B2_10 B10_10 B3_10 115.4(7) . . . . ?
B12_10 B9_10 B10_10 Cl8_10 -111.9(7) . . . . ?
Cl7_10 B9_10 B10_10 Cl8_10 -3.0(9) . . . . ?
B8_10 B9_10 B10_10 Cl8_10 -149.2(6) . . . . ?
B3_10 B9_10 B10_10 Cl8_10 110.9(7) . . . . ?
B4_10 B9_10 B10_10 Cl8_10 148.0(6) . . . . ?
B12_10 B9_10 B10_10 B2_10 99.9(6) . . . . ?
Cl7_10 B9_10 B10_10 B2_10 -151.2(5) . . . . ?
B8_10 B9_10 B10_10 B2_10 62.6(7) . . . . ?
B3_10 B9_10 B10_10 B2_10 -37.4(5) . . . . ?
B4_10 B9_10 B10_10 B2_10 -0.2(7) . . . . ?
Cl7_10 B9_10 B10_10 B12_10 108.9(6) . . . . ?
B8_10 B9_10 B10_10 B12_10 -37.3(5) . . . . ?
B3_10 B9_10 B10_10 B12_10 -137.2(6) . . . . ?
B4_10 B9_10 B10_10 B12_10 -100.1(6) . . . . ?
B12_10 B9_10 B10_10 B11_10 36.7(5) . . . . ?
Cl7_10 B9_10 B10_10 B11_10 145.6(6) . . . . ?
B8_10 B9_10 B10_10 B11_10 -0.6(8) . . . . ?
B3_10 B9_10 B10_10 B11_10 -100.5(6) . . . . ?
B4_10 B9_10 B10_10 B11_10 -63.4(7) . . . . ?
B12_10 B9_10 B10_10 B3_10 137.2(6) . . . . ?
Cl7_10 B9_10 B10_10 B3_10 -113.8(6) . . . . ?
B8_10 B9_10 B10_10 B3_10 99.9(6) . . . . ?
B4_10 B9_10 B10_10 B3_10 37.1(5) . . . . ?
B1_10 B3_10 B10_10 Cl8_10 149.0(6) . . . . ?
B4_10 B3_10 B10_10 Cl8_10 -148.3(6) . . . . ?
Cl4_10 B3_10 B10_10 Cl8_10 -2.6(9) . . . . ?
B9_10 B3_10 B10_10 Cl8_10 -110.4(7) . . . . ?
B2_10 B3_10 B10_10 Cl8_10 111.7(7) . . . . ?
B1_10 B3_10 B10_10 B2_10 37.2(5) . . . . ?
B4_10 B3_10 B10_10 B2_10 99.9(6) . . . . ?
Cl4_10 B3_10 B10_10 B2_10 -114.3(7) . . . . ?
B9_10 B3_10 B10_10 B2_10 137.9(6) . . . . ?
B1_10 B3_10 B10_10 B9_10 -100.6(6) . . . . ?
B4_10 B3_10 B10_10 B9_10 -37.9(5) . . . . ?
Cl4_10 B3_10 B10_10 B9_10 107.8(6) . . . . ?
B2_10 B3_10 B10_10 B9_10 -137.9(6) . . . . ?
B1_10 B3_10 B10_10 B12_10 -63.1(7) . . . . ?
B4_10 B3_10 B10_10 B12_10 -0.3(7) . . . . ?
Cl4_10 B3_10 B10_10 B12_10 145.4(5) . . . . ?
B9_10 B3_10 B10_10 B12_10 37.6(5) . . . . ?
B2_10 B3_10 B10_10 B12_10 -100.3(6) . . . . ?
B1_10 B3_10 B10_10 B11_10 -0.6(8) . . . . ?
B4_10 B3_10 B10_10 B11_10 62.1(7) . . . . ?
Cl4_10 B3_10 B10_10 B11_10 -152.1(6) . . . . ?
B9_10 B3_10 B10_10 B11_10 100.1(6) . . . . ?
B2_10 B3_10 B10_10 B11_10 -37.8(5) . . . . ?
Cl11_10 B7_10 B11_10 B12_10 -114.5(6) . . . . ?
B5_10 B7_10 B11_10 B12_10 137.3(6) . . . . ?
B6_10 B7_10 B11_10 B12_10 99.0(6) . . . . ?
B8_10 B7_10 B11_10 B12_10 36.1(5) . . . . ?
Cl11_10 B7_10 B11_10 B2_10 145.3(6) . . . . ?
B5_10 B7_10 B11_10 B2_10 37.1(6) . . . . ?
B6_10 B7_10 B11_10 B2_10 -1.2(8) . . . . ?
B12_10 B7_10 B11_10 B2_10 -100.2(6) . . . . ?
B8_10 B7_10 B11_10 B2_10 -64.0(7) . . . . ?
Cl11_10 B7_10 B11_10 Cl10_10 -5.2(9) . . . . ?
B5_10 B7_10 B11_10 Cl10_10 -113.4(7) . . . . ?
B6_10 B7_10 B11_10 Cl10_10 -151.6(6) . . . . ?
B12_10 B7_10 B11_10 Cl10_10 109.4(7) . . . . ?
B8_10 B7_10 B11_10 Cl10_10 145.5(6) . . . . ?
Cl11_10 B7_10 B11_10 B5_10 108.2(7) . . . . ?
B6_10 B7_10 B11_10 B5_10 -38.3(6) . . . . ?
B12_10 B7_10 B11_10 B5_10 -137.3(6) . . . . ?
B8_10 B7_10 B11_10 B5_10 -101.1(6) . . . . ?
Cl11_10 B7_10 B11_10 B10_10 -151.9(6) . . . . ?
B5_10 B7_10 B11_10 B10_10 99.9(6) . . . . ?
B6_10 B7_10 B11_10 B10_10 61.6(7) . . . . ?
B12_10 B7_10 B11_10 B10_10 -37.3(6) . . . . ?
B8_10 B7_10 B11_10 B10_10 -1.2(8) . . . . ?
B10_10 B2_10 B11_10 B7_10 102.4(6) . . . . ?
B3_10 B2_10 B11_10 B7_10 63.9(7) . . . . ?
B5_10 B2_10 B11_10 B7_10 -36.9(5) . . . . ?
B1_10 B2_10 B11_10 B7_10 1.2(8) . . . . ?
Cl3_10 B2_10 B11_10 B7_10 -144.1(5) . . . . ?
B10_10 B2_10 B11_10 B12_10 38.1(5) . . . . ?
B3_10 B2_10 B11_10 B12_10 -0.4(7) . . . . ?
B5_10 B2_10 B11_10 B12_10 -101.2(6) . . . . ?
B1_10 B2_10 B11_10 B12_10 -63.1(7) . . . . ?
Cl3_10 B2_10 B11_10 B12_10 151.7(6) . . . . ?
B10_10 B2_10 B11_10 Cl10_10 -107.0(7) . . . . ?
B3_10 B2_10 B11_10 Cl10_10 -145.5(6) . . . . ?
B5_10 B2_10 B11_10 Cl10_10 113.7(7) . . . . ?
B1_10 B2_10 B11_10 Cl10_10 151.8(6) . . . . ?
Cl3_10 B2_10 B11_10 Cl10_10 6.6(9) . . . . ?
B10_10 B2_10 B11_10 B5_10 139.3(6) . . . . ?
B3_10 B2_10 B11_10 B5_10 100.8(6) . . . . ?
B1_10 B2_10 B11_10 B5_10 38.1(6) . . . . ?
Cl3_10 B2_10 B11_10 B5_10 -107.1(6) . . . . ?
B3_10 B2_10 B11_10 B10_10 -38.5(5) . . . . ?
B5_10 B2_10 B11_10 B10_10 -139.3(6) . . . . ?
B1_10 B2_10 B11_10 B10_10 -101.2(6) . . . . ?
Cl3_10 B2_10 B11_10 B10_10 113.6(6) . . . . ?
Cl2_10 B5_10 B11_10 B7_10 -112.2(6) . . . . ?
B6_10 B5_10 B11_10 B7_10 37.9(5) . . . . ?
B2_10 B5_10 B11_10 B7_10 138.2(6) . . . . ?
B1_10 B5_10 B11_10 B7_10 100.4(6) . . . . ?
Cl2_10 B5_10 B11_10 B12_10 -150.9(5) . . . . ?
B7_10 B5_10 B11_10 B12_10 -38.6(6) . . . . ?
B6_10 B5_10 B11_10 B12_10 -0.8(8) . . . . ?
B2_10 B5_10 B11_10 B12_10 99.6(6) . . . . ?
B1_10 B5_10 B11_10 B12_10 61.8(7) . . . . ?
Cl2_10 B5_10 B11_10 B2_10 109.6(6) . . . . ?
B7_10 B5_10 B11_10 B2_10 -138.2(6) . . . . ?
B6_10 B5_10 B11_10 B2_10 -100.3(6) . . . . ?
B1_10 B5_10 B11_10 B2_10 -37.8(5) . . . . ?
Cl2_10 B5_10 B11_10 Cl10_10 -1.1(9) . . . . ?
B7_10 B5_10 B11_10 Cl10_10 111.1(7) . . . . ?
B6_10 B5_10 B11_10 Cl10_10 149.0(6) . . . . ?
B2_10 B5_10 B11_10 Cl10_10 -110.7(7) . . . . ?
B1_10 B5_10 B11_10 Cl10_10 -148.5(6) . . . . ?
Cl2_10 B5_10 B11_10 B10_10 145.7(6) . . . . ?
B7_10 B5_10 B11_10 B10_10 -102.1(6) . . . . ?
B6_10 B5_10 B11_10 B10_10 -64.2(7) . . . . ?
B2_10 B5_10 B11_10 B10_10 36.1(5) . . . . ?
B1_10 B5_10 B11_10 B10_10 -1.7(7) . . . . ?
Cl8_10 B10_10 B11_10 B7_10 149.2(6) . . . . ?
B2_10 B10_10 B11_10 B7_10 -99.3(6) . . . . ?
B9_10 B10_10 B11_10 B7_10 1.1(8) . . . . ?
B12_10 B10_10 B11_10 B7_10 37.8(6) . . . . ?
B3_10 B10_10 B11_10 B7_10 -61.6(7) . . . . ?
Cl8_10 B10_10 B11_10 B12_10 111.4(7) . . . . ?
B2_10 B10_10 B11_10 B12_10 -137.1(6) . . . . ?
B9_10 B10_10 B11_10 B12_10 -36.7(5) . . . . ?
B3_10 B10_10 B11_10 B12_10 -99.4(6) . . . . ?
Cl8_10 B10_10 B11_10 B2_10 -111.5(7) . . . . ?
B9_10 B10_10 B11_10 B2_10 100.4(6) . . . . ?
B12_10 B10_10 B11_10 B2_10 137.1(6) . . . . ?
B3_10 B10_10 B11_10 B2_10 37.7(5) . . . . ?
Cl8_10 B10_10 B11_10 Cl10_10 1.0(10) . . . . ?
B2_10 B10_10 B11_10 Cl10_10 112.5(6) . . . . ?
B9_10 B10_10 B11_10 Cl10_10 -147.1(5) . . . . ?
B12_10 B10_10 B11_10 Cl10_10 -110.4(7) . . . . ?
B3_10 B10_10 B11_10 Cl10_10 150.2(5) . . . . ?
Cl8_10 B10_10 B11_10 B5_10 -147.8(6) . . . . ?
B2_10 B10_10 B11_10 B5_10 -36.3(5) . . . . ?
B9_10 B10_10 B11_10 B5_10 64.1(7) . . . . ?
B12_10 B10_10 B11_10 B5_10 100.8(6) . . . . ?
B3_10 B10_10 B11_10 B5_10 1.4(8) . . . . ?
Cl7_10 B9_10 B12_10 B8_10 111.5(6) . . . . ?
B3_10 B9_10 B12_10 B8_10 -99.8(6) . . . . ?
B10_10 B9_10 B12_10 B8_10 -138.4(6) . . . . ?
B4_10 B9_10 B12_10 B8_10 -37.3(5) . . . . ?
Cl7_10 B9_10 B12_10 B11_10 -147.6(5) . . . . ?
B8_10 B9_10 B12_10 B11_10 100.9(6) . . . . ?
B3_10 B9_10 B12_10 B11_10 1.1(8) . . . . ?
B10_10 B9_10 B12_10 B11_10 -37.5(6) . . . . ?
B4_10 B9_10 B12_10 B11_10 63.6(7) . . . . ?
Cl7_10 B9_10 B12_10 B10_10 -110.1(6) . . . . ?
B8_10 B9_10 B12_10 B10_10 138.4(6) . . . . ?
B3_10 B9_10 B12_10 B10_10 38.6(5) . . . . ?
B4_10 B9_10 B12_10 B10_10 101.2(6) . . . . ?
Cl7_10 B9_10 B12_10 Cl9_10 -2.5(8) . . . . ?
B8_10 B9_10 B12_10 Cl9_10 -114.0(6) . . . . ?
B3_10 B9_10 B12_10 Cl9_10 146.2(5) . . . . ?
B10_10 B9_10 B12_10 Cl9_10 107.6(6) . . . . ?
B4_10 B9_10 B12_10 Cl9_10 -151.2(5) . . . . ?
Cl7_10 B9_10 B12_10 B7_10 149.4(5) . . . . ?
B8_10 B9_10 B12_10 B7_10 37.9(5) . . . . ?
B3_10 B9_10 B12_10 B7_10 -62.0(7) . . . . ?
B10_10 B9_10 B12_10 B7_10 -100.5(6) . . . . ?
B4_10 B9_10 B12_10 B7_10 0.6(7) . . . . ?
B4_10 B8_10 B12_10 B9_10 38.1(6) . . . . ?
B6_10 B8_10 B12_10 B9_10 101.3(6) . . . . ?
Cl12_10 B8_10 B12_10 B9_10 -111.1(7) . . . . ?
B7_10 B8_10 B12_10 B9_10 138.2(6) . . . . ?
B4_10 B8_10 B12_10 B11_10 -63.4(7) . . . . ?
B9_10 B8_10 B12_10 B11_10 -101.5(6) . . . . ?
B6_10 B8_10 B12_10 B11_10 -0.2(8) . . . . ?
Cl12_10 B8_10 B12_10 B11_10 147.4(6) . . . . ?
B7_10 B8_10 B12_10 B11_10 36.7(5) . . . . ?
B4_10 B8_10 B12_10 B10_10 0.7(8) . . . . ?
B9_10 B8_10 B12_10 B10_10 -37.4(5) . . . . ?
B6_10 B8_10 B12_10 B10_10 63.9(7) . . . . ?
Cl12_10 B8_10 B12_10 B10_10 -148.5(6) . . . . ?
B7_10 B8_10 B12_10 B10_10 100.8(6) . . . . ?
B4_10 B8_10 B12_10 Cl9_10 146.1(6) . . . . ?
B9_10 B8_10 B12_10 Cl9_10 108.0(7) . . . . ?
B6_10 B8_10 B12_10 Cl9_10 -150.7(6) . . . . ?
Cl12_10 B8_10 B12_10 Cl9_10 -3.1(10) . . . . ?
B7_10 B8_10 B12_10 Cl9_10 -113.8(7) . . . . ?
B4_10 B8_10 B12_10 B7_10 -100.1(6) . . . . ?
B9_10 B8_10 B12_10 B7_10 -138.2(6) . . . . ?
B6_10 B8_10 B12_10 B7_10 -36.9(6) . . . . ?
Cl12_10 B8_10 B12_10 B7_10 110.7(7) . . . . ?
B7_10 B11_10 B12_10 B9_10 -101.2(6) . . . . ?
B2_10 B11_10 B12_10 B9_10 -0.4(7) . . . . ?
Cl10_10 B11_10 B12_10 B9_10 145.5(6) . . . . ?
B5_10 B11_10 B12_10 B9_10 -63.3(7) . . . . ?
B10_10 B11_10 B12_10 B9_10 37.4(5) . . . . ?
B7_10 B11_10 B12_10 B8_10 -37.2(6) . . . . ?
B2_10 B11_10 B12_10 B8_10 63.5(7) . . . . ?
Cl10_10 B11_10 B12_10 B8_10 -150.5(6) . . . . ?
B5_10 B11_10 B12_10 B8_10 0.6(8) . . . . ?
B10_10 B11_10 B12_10 B8_10 101.3(6) . . . . ?
B7_10 B11_10 B12_10 B10_10 -138.6(6) . . . . ?
B2_10 B11_10 B12_10 B10_10 -37.8(5) . . . . ?
Cl10_10 B11_10 B12_10 B10_10 108.1(6) . . . . ?
B5_10 B11_10 B12_10 B10_10 -100.7(6) . . . . ?
B7_10 B11_10 B12_10 Cl9_10 114.1(7) . . . . ?
B2_10 B11_10 B12_10 Cl9_10 -145.1(6) . . . . ?
Cl10_10 B11_10 B12_10 Cl9_10 0.8(9) . . . . ?
B5_10 B11_10 B12_10 Cl9_10 152.0(5) . . . . ?
B10_10 B11_10 B12_10 Cl9_10 -107.3(7) . . . . ?
B2_10 B11_10 B12_10 B7_10 100.8(6) . . . . ?
Cl10_10 B11_10 B12_10 B7_10 -113.3(7) . . . . ?
B5_10 B11_10 B12_10 B7_10 37.9(5) . . . . ?
B10_10 B11_10 B12_10 B7_10 138.6(6) . . . . ?
Cl8_10 B10_10 B12_10 B9_10 110.0(7) . . . . ?
B2_10 B10_10 B12_10 B9_10 -100.4(6) . . . . ?
B11_10 B10_10 B12_10 B9_10 -138.5(6) . . . . ?
B3_10 B10_10 B12_10 B9_10 -37.7(5) . . . . ?
Cl8_10 B10_10 B12_10 B8_10 147.4(6) . . . . ?
B2_10 B10_10 B12_10 B8_10 -62.9(7) . . . . ?
B9_10 B10_10 B12_10 B8_10 37.4(6) . . . . ?
B11_10 B10_10 B12_10 B8_10 -101.0(6) . . . . ?
B3_10 B10_10 B12_10 B8_10 -0.2(8) . . . . ?
Cl8_10 B10_10 B12_10 B11_10 -111.5(6) . . . . ?
B2_10 B10_10 B12_10 B11_10 38.1(5) . . . . ?
B9_10 B10_10 B12_10 B11_10 138.5(6) . . . . ?
B3_10 B10_10 B12_10 B11_10 100.8(6) . . . . ?
Cl8_10 B10_10 B12_10 Cl9_10 -0.1(9) . . . . ?
B2_10 B10_10 B12_10 Cl9_10 149.6(5) . . . . ?
B9_10 B10_10 B12_10 Cl9_10 -110.0(6) . . . . ?
B11_10 B10_10 B12_10 Cl9_10 111.5(6) . . . . ?
B3_10 B10_10 B12_10 Cl9_10 -147.7(5) . . . . ?
Cl8_10 B10_10 B12_10 B7_10 -148.3(5) . . . . ?
B2_10 B10_10 B12_10 B7_10 1.3(7) . . . . ?
B9_10 B10_10 B12_10 B7_10 101.7(6) . . . . ?
B11_10 B10_10 B12_10 B7_10 -36.8(5) . . . . ?
B3_10 B10_10 B12_10 B7_10 64.0(7) . . . . ?
Cl11_10 B7_10 B12_10 B9_10 -149.2(6) . . . . ?
B5_10 B7_10 B12_10 B9_10 62.4(7) . . . . ?
B11_10 B7_10 B12_10 B9_10 101.1(6) . . . . ?
B6_10 B7_10 B12_10 B9_10 -1.0(7) . . . . ?
B8_10 B7_10 B12_10 B9_10 -37.7(5) . . . . ?
Cl11_10 B7_10 B12_10 B8_10 -111.5(7) . . . . ?
B5_10 B7_10 B12_10 B8_10 100.2(6) . . . . ?
B11_10 B7_10 B12_10 B8_10 138.8(6) . . . . ?
B6_10 B7_10 B12_10 B8_10 36.7(5) . . . . ?
Cl11_10 B7_10 B12_10 B11_10 109.7(7) . . . . ?
B5_10 B7_10 B12_10 B11_10 -38.6(6) . . . . ?
B6_10 B7_10 B12_10 B11_10 -102.0(6) . . . . ?
B8_10 B7_10 B12_10 B11_10 -138.8(6) . . . . ?
Cl11_10 B7_10 B12_10 B10_10 147.0(6) . . . . ?
B5_10 B7_10 B12_10 B10_10 -1.3(7) . . . . ?
B11_10 B7_10 B12_10 B10_10 37.3(5) . . . . ?
B6_10 B7_10 B12_10 B10_10 -64.8(7) . . . . ?
B8_10 B7_10 B12_10 B10_10 -101.5(6) . . . . ?
Cl11_10 B7_10 B12_10 Cl9_10 1.1(10) . . . . ?
B5_10 B7_10 B12_10 Cl9_10 -147.2(6) . . . . ?
B11_10 B7_10 B12_10 Cl9_10 -108.6(7) . . . . ?
B6_10 B7_10 B12_10 Cl9_10 149.3(6) . . . . ?
B8_10 B7_10 B12_10 Cl9_10 112.6(7) . . . . ?
B5_11 B1_11 B2_11 B3_11 100.2(7) . . . . ?
B6_11 B1_11 B2_11 B3_11 138.2(6) . . . . ?
B4_11 B1_11 B2_11 B3_11 36.5(6) . . . . ?
Cl1_11 B1_11 B2_11 B3_11 -110.3(7) . . . . ?
B5_11 B1_11 B2_11 B11_11 62.1(8) . . . . ?
B6_11 B1_11 B2_11 B11_11 100.1(6) . . . . ?
B4_11 B1_11 B2_11 B11_11 -1.6(8) . . . . ?
Cl1_11 B1_11 B2_11 B11_11 -148.4(6) . . . . ?
B3_11 B1_11 B2_11 B11_11 -38.1(6) . . . . ?
B5_11 B1_11 B2_11 Cl6_11 -147.9(6) . . . . ?
B6_11 B1_11 B2_11 Cl6_11 -109.9(6) . . . . ?
B4_11 B1_11 B2_11 Cl6_11 148.4(6) . . . . ?
Cl1_11 B1_11 B2_11 Cl6_11 1.7(9) . . . . ?
B3_11 B1_11 B2_11 Cl6_11 111.9(7) . . . . ?
B5_11 B1_11 B2_11 B6_11 -38.0(6) . . . . ?
B4_11 B1_11 B2_11 B6_11 -101.7(6) . . . . ?
Cl1_11 B1_11 B2_11 B6_11 111.6(7) . . . . ?
B3_11 B1_11 B2_11 B6_11 -138.2(6) . . . . ?
B5_11 B1_11 B2_11 B7_11 -0.8(8) . . . . ?
B6_11 B1_11 B2_11 B7_11 37.2(5) . . . . ?
B4_11 B1_11 B2_11 B7_11 -64.5(7) . . . . ?
Cl1_11 B1_11 B2_11 B7_11 148.7(6) . . . . ?
B3_11 B1_11 B2_11 B7_11 -101.0(6) . . . . ?
B1_11 B2_11 B3_11 B11_11 -136.9(6) . . . . ?
Cl6_11 B2_11 B3_11 B11_11 111.7(7) . . . . ?
B6_11 B2_11 B3_11 B11_11 -99.8(6) . . . . ?
B7_11 B2_11 B3_11 B11_11 -36.1(6) . . . . ?
B1_11 B2_11 B3_11 B10_11 -99.4(6) . . . . ?
B11_11 B2_11 B3_11 B10_11 37.5(6) . . . . ?
Cl6_11 B2_11 B3_11 B10_11 149.2(6) . . . . ?
B6_11 B2_11 B3_11 B10_11 -62.3(7) . . . . ?
B7_11 B2_11 B3_11 B10_11 1.5(8) . . . . ?
B1_11 B2_11 B3_11 Cl2_11 110.1(7) . . . . ?
B11_11 B2_11 B3_11 Cl2_11 -113.0(7) . . . . ?
Cl6_11 B2_11 B3_11 Cl2_11 -1.3(10) . . . . ?
B6_11 B2_11 B3_11 Cl2_11 147.2(6) . . . . ?
B7_11 B2_11 B3_11 Cl2_11 -149.0(6) . . . . ?
B1_11 B2_11 B3_11 B4_11 -36.3(6) . . . . ?
B11_11 B2_11 B3_11 B4_11 100.7(6) . . . . ?
Cl6_11 B2_11 B3_11 B4_11 -147.7(6) . . . . ?
B6_11 B2_11 B3_11 B4_11 0.8(8) . . . . ?
B7_11 B2_11 B3_11 B4_11 64.6(7) . . . . ?
B11_11 B2_11 B3_11 B1_11 136.9(6) . . . . ?
Cl6_11 B2_11 B3_11 B1_11 -111.4(7) . . . . ?
B6_11 B2_11 B3_11 B1_11 37.1(6) . . . . ?
B7_11 B2_11 B3_11 B1_11 100.9(6) . . . . ?
B5_11 B1_11 B3_11 B11_11 -64.1(7) . . . . ?
B6_11 B1_11 B3_11 B11_11 0.2(7) . . . . ?
B2_11 B1_11 B3_11 B11_11 38.4(5) . . . . ?
B4_11 B1_11 B3_11 B11_11 -100.9(6) . . . . ?
Cl1_11 B1_11 B3_11 B11_11 147.0(6) . . . . ?
B5_11 B1_11 B3_11 B2_11 -102.5(6) . . . . ?
B6_11 B1_11 B3_11 B2_11 -38.1(6) . . . . ?
B4_11 B1_11 B3_11 B2_11 -139.3(6) . . . . ?
Cl1_11 B1_11 B3_11 B2_11 108.6(7) . . . . ?
B5_11 B1_11 B3_11 B10_11 -0.7(8) . . . . ?
B6_11 B1_11 B3_11 B10_11 63.6(7) . . . . ?
B2_11 B1_11 B3_11 B10_11 101.7(6) . . . . ?
B4_11 B1_11 B3_11 B10_11 -37.6(5) . . . . ?
Cl1_11 B1_11 B3_11 B10_11 -149.6(6) . . . . ?
B5_11 B1_11 B3_11 Cl2_11 147.9(5) . . . . ?
B6_11 B1_11 B3_11 Cl2_11 -147.8(6) . . . . ?
B2_11 B1_11 B3_11 Cl2_11 -109.6(6) . . . . ?
B4_11 B1_11 B3_11 Cl2_11 111.1(7) . . . . ?
Cl1_11 B1_11 B3_11 Cl2_11 -1.0(9) . . . . ?
B5_11 B1_11 B3_11 B4_11 36.8(6) . . . . ?
B6_11 B1_11 B3_11 B4_11 101.2(6) . . . . ?
B2_11 B1_11 B3_11 B4_11 139.3(6) . . . . ?
Cl1_11 B1_11 B3_11 B4_11 -112.1(7) . . . . ?
B6_11 B1_11 B4_11 B5_11 37.4(6) . . . . ?
B2_11 B1_11 B4_11 B5_11 102.3(6) . . . . ?
Cl1_11 B1_11 B4_11 B5_11 -112.0(7) . . . . ?
B3_11 B1_11 B4_11 B5_11 138.8(6) . . . . ?
B5_11 B1_11 B4_11 B9_11 -37.8(6) . . . . ?
B6_11 B1_11 B4_11 B9_11 -0.4(8) . . . . ?
B2_11 B1_11 B4_11 B9_11 64.5(7) . . . . ?
Cl1_11 B1_11 B4_11 B9_11 -149.8(6) . . . . ?
B3_11 B1_11 B4_11 B9_11 101.0(6) . . . . ?
B5_11 B1_11 B4_11 B10_11 -101.0(6) . . . . ?
B6_11 B1_11 B4_11 B10_11 -63.6(8) . . . . ?
B2_11 B1_11 B4_11 B10_11 1.3(8) . . . . ?
Cl1_11 B1_11 B4_11 B10_11 147.0(6) . . . . ?
B3_11 B1_11 B4_11 B10_11 37.8(6) . . . . ?
B5_11 B1_11 B4_11 Cl3_11 110.8(7) . . . . ?
B6_11 B1_11 B4_11 Cl3_11 148.1(6) . . . . ?
B2_11 B1_11 B4_11 Cl3_11 -146.9(6) . . . . ?
Cl1_11 B1_11 B4_11 Cl3_11 -1.3(10) . . . . ?
B3_11 B1_11 B4_11 Cl3_11 -110.4(7) . . . . ?
B5_11 B1_11 B4_11 B3_11 -138.8(6) . . . . ?
B6_11 B1_11 B4_11 B3_11 -101.4(7) . . . . ?
B2_11 B1_11 B4_11 B3_11 -36.5(6) . . . . ?
Cl1_11 B1_11 B4_11 B3_11 109.2(7) . . . . ?
B11_11 B3_11 B4_11 B5_11 63.3(7) . . . . ?
B2_11 B3_11 B4_11 B5_11 -0.5(8) . . . . ?
B10_11 B3_11 B4_11 B5_11 101.0(6) . . . . ?
Cl2_11 B3_11 B4_11 B5_11 -146.5(6) . . . . ?
B1_11 B3_11 B4_11 B5_11 -36.5(6) . . . . ?
B11_11 B3_11 B4_11 B9_11 -0.6(8) . . . . ?
B2_11 B3_11 B4_11 B9_11 -64.3(7) . . . . ?
B10_11 B3_11 B4_11 B9_11 37.2(5) . . . . ?
Cl2_11 B3_11 B4_11 B9_11 149.7(6) . . . . ?
B1_11 B3_11 B4_11 B9_11 -100.4(6) . . . . ?
B11_11 B3_11 B4_11 B10_11 -37.7(5) . . . . ?
B2_11 B3_11 B4_11 B10_11 -101.5(6) . . . . ?
Cl2_11 B3_11 B4_11 B10_11 112.5(7) . . . . ?
B1_11 B3_11 B4_11 B10_11 -137.5(6) . . . . ?
B11_11 B3_11 B4_11 Cl3_11 -147.4(6) . . . . ?
B2_11 B3_11 B4_11 Cl3_11 148.8(6) . . . . ?
B10_11 B3_11 B4_11 Cl3_11 -109.7(7) . . . . ?
Cl2_11 B3_11 B4_11 Cl3_11 2.8(9) . . . . ?
B1_11 B3_11 B4_11 Cl3_11 112.8(7) . . . . ?
B11_11 B3_11 B4_11 B1_11 99.8(6) . . . . ?
B2_11 B3_11 B4_11 B1_11 36.0(6) . . . . ?
B10_11 B3_11 B4_11 B1_11 137.5(6) . . . . ?
Cl2_11 B3_11 B4_11 B1_11 -109.9(7) . . . . ?
B6_11 B1_11 B5_11 B4_11 -138.7(6) . . . . ?
B2_11 B1_11 B5_11 B4_11 -100.5(7) . . . . ?
Cl1_11 B1_11 B5_11 B4_11 111.2(7) . . . . ?
B3_11 B1_11 B5_11 B4_11 -36.9(6) . . . . ?
B6_11 B1_11 B5_11 Cl4_11 108.9(7) . . . . ?
B2_11 B1_11 B5_11 Cl4_11 147.1(6) . . . . ?
B4_11 B1_11 B5_11 Cl4_11 -112.4(7) . . . . ?
Cl1_11 B1_11 B5_11 Cl4_11 -1.2(10) . . . . ?
B3_11 B1_11 B5_11 Cl4_11 -149.2(6) . . . . ?
B2_11 B1_11 B5_11 B6_11 38.2(6) . . . . ?
B4_11 B1_11 B5_11 B6_11 138.7(6) . . . . ?
Cl1_11 B1_11 B5_11 B6_11 -110.1(7) . . . . ?
B3_11 B1_11 B5_11 B6_11 101.9(6) . . . . ?
B6_11 B1_11 B5_11 B9_11 -100.9(6) . . . . ?
B2_11 B1_11 B5_11 B9_11 -62.7(7) . . . . ?
B4_11 B1_11 B5_11 B9_11 37.8(6) . . . . ?
Cl1_11 B1_11 B5_11 B9_11 149.0(6) . . . . ?
B3_11 B1_11 B5_11 B9_11 0.9(8) . . . . ?
B6_11 B1_11 B5_11 B8_11 -37.6(5) . . . . ?
B2_11 B1_11 B5_11 B8_11 0.6(8) . . . . ?
B4_11 B1_11 B5_11 B8_11 101.1(6) . . . . ?
Cl1_11 B1_11 B5_11 B8_11 -147.7(6) . . . . ?
B3_11 B1_11 B5_11 B8_11 64.2(7) . . . . ?
B9_11 B4_11 B5_11 B1_11 137.8(6) . . . . ?
B10_11 B4_11 B5_11 B1_11 100.3(6) . . . . ?
Cl3_11 B4_11 B5_11 B1_11 -112.1(7) . . . . ?
B3_11 B4_11 B5_11 B1_11 37.0(6) . . . . ?
B9_11 B4_11 B5_11 Cl4_11 -111.2(7) . . . . ?
B10_11 B4_11 B5_11 Cl4_11 -148.7(6) . . . . ?
Cl3_11 B4_11 B5_11 Cl4_11 -1.1(10) . . . . ?
B1_11 B4_11 B5_11 Cl4_11 111.0(7) . . . . ?
B3_11 B4_11 B5_11 Cl4_11 148.0(6) . . . . ?
B9_11 B4_11 B5_11 B6_11 100.8(6) . . . . ?
B10_11 B4_11 B5_11 B6_11 63.3(7) . . . . ?
Cl3_11 B4_11 B5_11 B6_11 -149.1(6) . . . . ?
B1_11 B4_11 B5_11 B6_11 -37.0(6) . . . . ?
B3_11 B4_11 B5_11 B6_11 0.0(8) . . . . ?
B10_11 B4_11 B5_11 B9_11 -37.5(5) . . . . ?
Cl3_11 B4_11 B5_11 B9_11 110.2(7) . . . . ?
B1_11 B4_11 B5_11 B9_11 -137.8(6) . . . . ?
B3_11 B4_11 B5_11 B9_11 -100.8(6) . . . . ?
B9_11 B4_11 B5_11 B8_11 37.3(5) . . . . ?
B10_11 B4_11 B5_11 B8_11 -0.2(8) . . . . ?
Cl3_11 B4_11 B5_11 B8_11 147.5(6) . . . . ?
B1_11 B4_11 B5_11 B8_11 -100.5(6) . . . . ?
B3_11 B4_11 B5_11 B8_11 -63.5(7) . . . . ?
B2_11 B1_11 B6_11 B5_11 -138.3(6) . . . . ?
B4_11 B1_11 B6_11 B5_11 -37.0(6) . . . . ?
Cl1_11 B1_11 B6_11 B5_11 112.8(7) . . . . ?
B3_11 B1_11 B6_11 B5_11 -100.7(6) . . . . ?
B5_11 B1_11 B6_11 B8_11 37.9(6) . . . . ?
B2_11 B1_11 B6_11 B8_11 -100.4(6) . . . . ?
B4_11 B1_11 B6_11 B8_11 0.8(8) . . . . ?
Cl1_11 B1_11 B6_11 B8_11 150.6(6) . . . . ?
B3_11 B1_11 B6_11 B8_11 -62.8(7) . . . . ?
B5_11 B1_11 B6_11 Cl5_11 -110.3(7) . . . . ?
B2_11 B1_11 B6_11 Cl5_11 111.4(7) . . . . ?
B4_11 B1_11 B6_11 Cl5_11 -147.3(6) . . . . ?
Cl1_11 B1_11 B6_11 Cl5_11 2.5(9) . . . . ?
B3_11 B1_11 B6_11 Cl5_11 149.0(6) . . . . ?
B5_11 B1_11 B6_11 B2_11 138.3(6) . . . . ?
B4_11 B1_11 B6_11 B2_11 101.2(7) . . . . ?
Cl1_11 B1_11 B6_11 B2_11 -109.0(7) . . . . ?
B3_11 B1_11 B6_11 B2_11 37.6(5) . . . . ?
B5_11 B1_11 B6_11 B7_11 101.4(6) . . . . ?
B2_11 B1_11 B6_11 B7_11 -36.9(5) . . . . ?
B4_11 B1_11 B6_11 B7_11 64.3(7) . . . . ?
Cl1_11 B1_11 B6_11 B7_11 -145.9(6) . . . . ?
B3_11 B1_11 B6_11 B7_11 0.7(8) . . . . ?
B4_11 B5_11 B6_11 B1_11 37.5(6) . . . . ?
Cl4_11 B5_11 B6_11 B1_11 -111.4(7) . . . . ?
B9_11 B5_11 B6_11 B1_11 101.0(6) . . . . ?
B8_11 B5_11 B6_11 B1_11 137.7(6) . . . . ?
B1_11 B5_11 B6_11 B8_11 -137.7(6) . . . . ?
B4_11 B5_11 B6_11 B8_11 -100.2(6) . . . . ?
Cl4_11 B5_11 B6_11 B8_11 110.9(7) . . . . ?
B9_11 B5_11 B6_11 B8_11 -36.7(6) . . . . ?
B1_11 B5_11 B6_11 Cl5_11 111.5(7) . . . . ?
B4_11 B5_11 B6_11 Cl5_11 148.9(6) . . . . ?
Cl4_11 B5_11 B6_11 Cl5_11 0.1(10) . . . . ?
B9_11 B5_11 B6_11 Cl5_11 -147.5(6) . . . . ?
B8_11 B5_11 B6_11 Cl5_11 -110.8(7) . . . . ?
B1_11 B5_11 B6_11 B2_11 -37.0(6) . . . . ?
B4_11 B5_11 B6_11 B2_11 0.5(8) . . . . ?
Cl4_11 B5_11 B6_11 B2_11 -148.4(6) . . . . ?
B9_11 B5_11 B6_11 B2_11 64.0(7) . . . . ?
B8_11 B5_11 B6_11 B2_11 100.8(6) . . . . ?
B1_11 B5_11 B6_11 B7_11 -100.2(6) . . . . ?
B4_11 B5_11 B6_11 B7_11 -62.7(7) . . . . ?
Cl4_11 B5_11 B6_11 B7_11 148.4(6) . . . . ?
B9_11 B5_11 B6_11 B7_11 0.8(8) . . . . ?
B8_11 B5_11 B6_11 B7_11 37.6(6) . . . . ?
B3_11 B2_11 B6_11 B1_11 -37.8(6) . . . . ?
B11_11 B2_11 B6_11 B1_11 -100.5(6) . . . . ?
Cl6_11 B2_11 B6_11 B1_11 111.1(7) . . . . ?
B7_11 B2_11 B6_11 B1_11 -138.6(6) . . . . ?
B1_11 B2_11 B6_11 B5_11 37.0(6) . . . . ?
B3_11 B2_11 B6_11 B5_11 -0.8(8) . . . . ?
B11_11 B2_11 B6_11 B5_11 -63.5(7) . . . . ?
Cl6_11 B2_11 B6_11 B5_11 148.1(6) . . . . ?
B7_11 B2_11 B6_11 B5_11 -101.6(6) . . . . ?
B1_11 B2_11 B6_11 B8_11 100.7(6) . . . . ?
B3_11 B2_11 B6_11 B8_11 62.8(7) . . . . ?
B11_11 B2_11 B6_11 B8_11 0.1(8) . . . . ?
Cl6_11 B2_11 B6_11 B8_11 -148.3(6) . . . . ?
B7_11 B2_11 B6_11 B8_11 -37.9(5) . . . . ?
B1_11 B2_11 B6_11 Cl5_11 -111.1(7) . . . . ?
B3_11 B2_11 B6_11 Cl5_11 -148.9(6) . . . . ?
B11_11 B2_11 B6_11 Cl5_11 148.4(6) . . . . ?
Cl6_11 B2_11 B6_11 Cl5_11 0.0(10) . . . . ?
B7_11 B2_11 B6_11 Cl5_11 110.4(7) . . . . ?
B1_11 B2_11 B6_11 B7_11 138.6(6) . . . . ?
B3_11 B2_11 B6_11 B7_11 100.7(6) . . . . ?
B11_11 B2_11 B6_11 B7_11 38.0(5) . . . . ?
Cl6_11 B2_11 B6_11 B7_11 -110.4(7) . . . . ?
B1_11 B2_11 B7_11 Cl7_11 -147.2(6) . . . . ?
B3_11 B2_11 B7_11 Cl7_11 148.4(6) . . . . ?
B11_11 B2_11 B7_11 Cl7_11 112.4(7) . . . . ?
Cl6_11 B2_11 B7_11 Cl7_11 0.2(9) . . . . ?
B6_11 B2_11 B7_11 Cl7_11 -110.5(7) . . . . ?
B1_11 B2_11 B7_11 B11_11 100.3(6) . . . . ?
B3_11 B2_11 B7_11 B11_11 36.0(6) . . . . ?
Cl6_11 B2_11 B7_11 B11_11 -112.2(7) . . . . ?
B6_11 B2_11 B7_11 B11_11 137.0(6) . . . . ?
B1_11 B2_11 B7_11 B12_11 63.0(7) . . . . ?
B3_11 B2_11 B7_11 B12_11 -1.4(8) . . . . ?
B11_11 B2_11 B7_11 B12_11 -37.4(5) . . . . ?
Cl6_11 B2_11 B7_11 B12_11 -149.6(5) . . . . ?
B6_11 B2_11 B7_11 B12_11 99.6(6) . . . . ?
B1_11 B2_11 B7_11 B8_11 0.7(7) . . . . ?
B3_11 B2_11 B7_11 B8_11 -63.7(7) . . . . ?
B11_11 B2_11 B7_11 B8_11 -99.7(6) . . . . ?
Cl6_11 B2_11 B7_11 B8_11 148.1(5) . . . . ?
B6_11 B2_11 B7_11 B8_11 37.4(5) . . . . ?
B1_11 B2_11 B7_11 B6_11 -36.7(6) . . . . ?
B3_11 B2_11 B7_11 B6_11 -101.0(6) . . . . ?
B11_11 B2_11 B7_11 B6_11 -137.0(6) . . . . ?
Cl6_11 B2_11 B7_11 B6_11 110.8(6) . . . . ?
B1_11 B6_11 B7_11 Cl7_11 147.9(6) . . . . ?
B5_11 B6_11 B7_11 Cl7_11 -149.1(6) . . . . ?
B8_11 B6_11 B7_11 Cl7_11 -111.4(7) . . . . ?
Cl5_11 B6_11 B7_11 Cl7_11 -0.7(10) . . . . ?
B2_11 B6_11 B7_11 Cl7_11 111.1(7) . . . . ?
B1_11 B6_11 B7_11 B11_11 -1.3(7) . . . . ?
B5_11 B6_11 B7_11 B11_11 61.8(7) . . . . ?
B8_11 B6_11 B7_11 B11_11 99.4(6) . . . . ?
Cl5_11 B6_11 B7_11 B11_11 -149.9(6) . . . . ?
B2_11 B6_11 B7_11 B11_11 -38.1(5) . . . . ?
B1_11 B6_11 B7_11 B12_11 -64.1(7) . . . . ?
B5_11 B6_11 B7_11 B12_11 -1.0(8) . . . . ?
B8_11 B6_11 B7_11 B12_11 36.6(5) . . . . ?
Cl5_11 B6_11 B7_11 B12_11 147.3(6) . . . . ?
B2_11 B6_11 B7_11 B12_11 -100.9(6) . . . . ?
B1_11 B6_11 B7_11 B2_11 36.8(5) . . . . ?
B5_11 B6_11 B7_11 B2_11 99.9(6) . . . . ?
B8_11 B6_11 B7_11 B2_11 137.5(6) . . . . ?
Cl5_11 B6_11 B7_11 B2_11 -111.8(7) . . . . ?
B1_11 B6_11 B7_11 B8_11 -100.7(6) . . . . ?
B5_11 B6_11 B7_11 B8_11 -37.7(6) . . . . ?
Cl5_11 B6_11 B7_11 B8_11 110.7(7) . . . . ?
B2_11 B6_11 B7_11 B8_11 -137.5(6) . . . . ?
B1_11 B6_11 B8_11 B12_11 63.3(7) . . . . ?
B5_11 B6_11 B8_11 B12_11 100.8(6) . . . . ?
Cl5_11 B6_11 B8_11 B12_11 -148.3(6) . . . . ?
B2_11 B6_11 B8_11 B12_11 0.4(8) . . . . ?
B7_11 B6_11 B8_11 B12_11 -37.4(5) . . . . ?
B1_11 B6_11 B8_11 B9_11 -0.9(8) . . . . ?
B5_11 B6_11 B8_11 B9_11 36.6(6) . . . . ?
Cl5_11 B6_11 B8_11 B9_11 147.5(6) . . . . ?
B2_11 B6_11 B8_11 B9_11 -63.8(7) . . . . ?
B7_11 B6_11 B8_11 B9_11 -101.5(6) . . . . ?
B1_11 B6_11 B8_11 Cl8_11 -150.7(6) . . . . ?
B5_11 B6_11 B8_11 Cl8_11 -113.2(7) . . . . ?
Cl5_11 B6_11 B8_11 Cl8_11 -2.3(9) . . . . ?
B2_11 B6_11 B8_11 Cl8_11 146.4(6) . . . . ?
B7_11 B6_11 B8_11 Cl8_11 108.7(6) . . . . ?
B1_11 B6_11 B8_11 B5_11 -37.6(6) . . . . ?
Cl5_11 B6_11 B8_11 B5_11 110.9(7) . . . . ?
B2_11 B6_11 B8_11 B5_11 -100.4(6) . . . . ?
B7_11 B6_11 B8_11 B5_11 -138.2(6) . . . . ?
B1_11 B6_11 B8_11 B7_11 100.6(6) . . . . ?
B5_11 B6_11 B8_11 B7_11 138.2(6) . . . . ?
Cl5_11 B6_11 B8_11 B7_11 -110.9(7) . . . . ?
B2_11 B6_11 B8_11 B7_11 37.8(5) . . . . ?
B1_11 B5_11 B8_11 B12_11 -63.6(7) . . . . ?
B4_11 B5_11 B8_11 B12_11 0.6(7) . . . . ?
Cl4_11 B5_11 B8_11 B12_11 149.6(6) . . . . ?
B6_11 B5_11 B8_11 B12_11 -101.2(6) . . . . ?
B9_11 B5_11 B8_11 B12_11 37.8(5) . . . . ?
B1_11 B5_11 B8_11 B6_11 37.5(6) . . . . ?
B4_11 B5_11 B8_11 B6_11 101.7(6) . . . . ?
Cl4_11 B5_11 B8_11 B6_11 -109.2(7) . . . . ?
B9_11 B5_11 B8_11 B6_11 139.0(6) . . . . ?
B1_11 B5_11 B8_11 B9_11 -101.5(6) . . . . ?
B4_11 B5_11 B8_11 B9_11 -37.3(5) . . . . ?
Cl4_11 B5_11 B8_11 B9_11 111.8(7) . . . . ?
B6_11 B5_11 B8_11 B9_11 -139.0(6) . . . . ?
B1_11 B5_11 B8_11 Cl8_11 147.1(6) . . . . ?
B4_11 B5_11 B8_11 Cl8_11 -148.7(5) . . . . ?
Cl4_11 B5_11 B8_11 Cl8_11 0.4(9) . . . . ?
B6_11 B5_11 B8_11 Cl8_11 109.6(6) . . . . ?
B9_11 B5_11 B8_11 Cl8_11 -111.4(6) . . . . ?
B1_11 B5_11 B8_11 B7_11 -0.2(8) . . . . ?
B4_11 B5_11 B8_11 B7_11 64.1(7) . . . . ?
Cl4_11 B5_11 B8_11 B7_11 -146.9(6) . . . . ?
B6_11 B5_11 B8_11 B7_11 -37.7(5) . . . . ?
B9_11 B5_11 B8_11 B7_11 101.3(6) . . . . ?
Cl7_11 B7_11 B8_11 B12_11 -111.6(7) . . . . ?
B11_11 B7_11 B8_11 B12_11 37.9(5) . . . . ?
B2_11 B7_11 B8_11 B12_11 100.7(6) . . . . ?
B6_11 B7_11 B8_11 B12_11 138.3(6) . . . . ?
Cl7_11 B7_11 B8_11 B6_11 110.1(7) . . . . ?
B11_11 B7_11 B8_11 B6_11 -100.5(6) . . . . ?
B12_11 B7_11 B8_11 B6_11 -138.3(6) . . . . ?
B2_11 B7_11 B8_11 B6_11 -37.6(5) . . . . ?
Cl7_11 B7_11 B8_11 B9_11 -149.2(6) . . . . ?
B11_11 B7_11 B8_11 B9_11 0.3(8) . . . . ?
B12_11 B7_11 B8_11 B9_11 -37.6(5) . . . . ?
B2_11 B7_11 B8_11 B9_11 63.1(7) . . . . ?
B6_11 B7_11 B8_11 B9_11 100.7(6) . . . . ?
Cl7_11 B7_11 B8_11 Cl8_11 -1.4(9) . . . . ?
B11_11 B7_11 B8_11 Cl8_11 148.0(5) . . . . ?
B12_11 B7_11 B8_11 Cl8_11 110.2(6) . . . . ?
B2_11 B7_11 B8_11 Cl8_11 -149.1(5) . . . . ?
B6_11 B7_11 B8_11 Cl8_11 -111.5(6) . . . . ?
Cl7_11 B7_11 B8_11 B5_11 147.4(6) . . . . ?
B11_11 B7_11 B8_11 B5_11 -63.2(7) . . . . ?
B12_11 B7_11 B8_11 B5_11 -101.0(6) . . . . ?
B2_11 B7_11 B8_11 B5_11 -0.3(7) . . . . ?
B6_11 B7_11 B8_11 B5_11 37.3(5) . . . . ?
B5_11 B4_11 B9_11 B10_11 -138.1(6) . . . . ?
Cl3_11 B4_11 B9_11 B10_11 109.9(7) . . . . ?
B1_11 B4_11 B9_11 B10_11 -100.8(6) . . . . ?
B3_11 B4_11 B9_11 B10_11 -37.1(5) . . . . ?
B10_11 B4_11 B9_11 B5_11 138.1(6) . . . . ?
Cl3_11 B4_11 B9_11 B5_11 -112.0(7) . . . . ?
B1_11 B4_11 B9_11 B5_11 37.3(6) . . . . ?
B3_11 B4_11 B9_11 B5_11 100.9(6) . . . . ?
B5_11 B4_11 B9_11 B8_11 -37.4(6) . . . . ?
B10_11 B4_11 B9_11 B8_11 100.7(6) . . . . ?
Cl3_11 B4_11 B9_11 B8_11 -149.5(6) . . . . ?
B1_11 B4_11 B9_11 B8_11 -0.1(8) . . . . ?
B3_11 B4_11 B9_11 B8_11 63.5(7) . . . . ?
B5_11 B4_11 B9_11 Cl9_11 111.4(7) . . . . ?
B10_11 B4_11 B9_11 Cl9_11 -110.5(7) . . . . ?
Cl3_11 B4_11 B9_11 Cl9_11 -0.6(10) . . . . ?
B1_11 B4_11 B9_11 Cl9_11 148.7(6) . . . . ?
B3_11 B4_11 B9_11 Cl9_11 -147.7(6) . . . . ?
B5_11 B4_11 B9_11 B12_11 -100.0(6) . . . . ?
B10_11 B4_11 B9_11 B12_11 38.0(5) . . . . ?
Cl3_11 B4_11 B9_11 B12_11 147.9(6) . . . . ?
B1_11 B4_11 B9_11 B12_11 -62.7(7) . . . . ?
B3_11 B4_11 B9_11 B12_11 0.9(8) . . . . ?
B1_11 B5_11 B9_11 B10_11 -0.8(8) . . . . ?
B4_11 B5_11 B9_11 B10_11 37.5(5) . . . . ?
Cl4_11 B5_11 B9_11 B10_11 149.2(6) . . . . ?
B6_11 B5_11 B9_11 B10_11 -64.0(7) . . . . ?
B8_11 B5_11 B9_11 B10_11 -100.7(6) . . . . ?
B1_11 B5_11 B9_11 B4_11 -38.2(6) . . . . ?
Cl4_11 B5_11 B9_11 B4_11 111.7(7) . . . . ?
B6_11 B5_11 B9_11 B4_11 -101.5(6) . . . . ?
B8_11 B5_11 B9_11 B4_11 -138.2(6) . . . . ?
B1_11 B5_11 B9_11 B8_11 100.0(6) . . . . ?
B4_11 B5_11 B9_11 B8_11 138.2(6) . . . . ?
Cl4_11 B5_11 B9_11 B8_11 -110.1(7) . . . . ?
B6_11 B5_11 B9_11 B8_11 36.7(6) . . . . ?
B1_11 B5_11 B9_11 Cl9_11 -149.4(6) . . . . ?
B4_11 B5_11 B9_11 Cl9_11 -111.2(7) . . . . ?
Cl4_11 B5_11 B9_11 Cl9_11 0.5(9) . . . . ?
B6_11 B5_11 B9_11 Cl9_11 147.3(6) . . . . ?
B8_11 B5_11 B9_11 Cl9_11 110.6(7) . . . . ?
B1_11 B5_11 B9_11 B12_11 63.0(7) . . . . ?
B4_11 B5_11 B9_11 B12_11 101.2(6) . . . . ?
Cl4_11 B5_11 B9_11 B12_11 -147.1(6) . . . . ?
B6_11 B5_11 B9_11 B12_11 -0.3(8) . . . . ?
B8_11 B5_11 B9_11 B12_11 -37.0(5) . . . . ?
B12_11 B8_11 B9_11 B10_11 -37.3(5) . . . . ?
B6_11 B8_11 B9_11 B10_11 64.2(7) . . . . ?
Cl8_11 B8_11 B9_11 B10_11 -146.6(6) . . . . ?
B5_11 B8_11 B9_11 B10_11 100.7(6) . . . . ?
B7_11 B8_11 B9_11 B10_11 0.0(8) . . . . ?
B12_11 B8_11 B9_11 B4_11 -100.8(6) . . . . ?
B6_11 B8_11 B9_11 B4_11 0.6(8) . . . . ?
Cl8_11 B8_11 B9_11 B4_11 149.9(6) . . . . ?
B5_11 B8_11 B9_11 B4_11 37.2(6) . . . . ?
B7_11 B8_11 B9_11 B4_11 -63.5(7) . . . . ?
B12_11 B8_11 B9_11 B5_11 -138.0(6) . . . . ?
B6_11 B8_11 B9_11 B5_11 -36.6(5) . . . . ?
Cl8_11 B8_11 B9_11 B5_11 112.7(7) . . . . ?
B7_11 B8_11 B9_11 B5_11 -100.7(6) . . . . ?
B12_11 B8_11 B9_11 Cl9_11 110.1(7) . . . . ?
B6_11 B8_11 B9_11 Cl9_11 -148.4(6) . . . . ?
Cl8_11 B8_11 B9_11 Cl9_11 0.9(9) . . . . ?
B5_11 B8_11 B9_11 Cl9_11 -111.9(7) . . . . ?
B7_11 B8_11 B9_11 Cl9_11 147.4(6) . . . . ?
B6_11 B8_11 B9_11 B12_11 101.5(6) . . . . ?
Cl8_11 B8_11 B9_11 B12_11 -109.2(7) . . . . ?
B5_11 B8_11 B9_11 B12_11 138.0(6) . . . . ?
B7_11 B8_11 B9_11 B12_11 37.3(5) . . . . ?
B5_11 B9_11 B10_11 B4_11 -37.3(5) . . . . ?
B8_11 B9_11 B10_11 B4_11 -100.9(6) . . . . ?
Cl9_11 B9_11 B10_11 B4_11 111.7(7) . . . . ?
B12_11 B9_11 B10_11 B4_11 -137.7(6) . . . . ?
B4_11 B9_11 B10_11 B11_11 100.6(6) . . . . ?
B5_11 B9_11 B10_11 B11_11 63.3(7) . . . . ?
B8_11 B9_11 B10_11 B11_11 -0.3(8) . . . . ?
Cl9_11 B9_11 B10_11 B11_11 -147.7(6) . . . . ?
B12_11 B9_11 B10_11 B11_11 -37.1(5) . . . . ?
B4_11 B9_11 B10_11 B3_11 37.6(5) . . . . ?
B5_11 B9_11 B10_11 B3_11 0.3(8) . . . . ?
B8_11 B9_11 B10_11 B3_11 -63.3(7) . . . . ?
Cl9_11 B9_11 B10_11 B3_11 149.3(6) . . . . ?
B12_11 B9_11 B10_11 B3_11 -100.1(6) . . . . ?
B4_11 B9_11 B10_11 Cl10_11 -114.3(7) . . . . ?
B5_11 B9_11 B10_11 Cl10_11 -151.6(6) . . . . ?
B8_11 B9_11 B10_11 Cl10_11 144.8(6) . . . . ?
Cl9_11 B9_11 B10_11 Cl10_11 -2.6(9) . . . . ?
B12_11 B9_11 B10_11 Cl10_11 108.0(6) . . . . ?
B4_11 B9_11 B10_11 B12_11 137.7(6) . . . . ?
B5_11 B9_11 B10_11 B12_11 100.4(6) . . . . ?
B8_11 B9_11 B10_11 B12_11 36.8(5) . . . . ?
Cl9_11 B9_11 B10_11 B12_11 -110.6(7) . . . . ?
B5_11 B4_11 B10_11 B9_11 37.7(5) . . . . ?
Cl3_11 B4_11 B10_11 B9_11 -110.5(7) . . . . ?
B1_11 B4_11 B10_11 B9_11 100.3(6) . . . . ?
B3_11 B4_11 B10_11 B9_11 138.3(6) . . . . ?
B5_11 B4_11 B10_11 B11_11 -63.2(7) . . . . ?
B9_11 B4_11 B10_11 B11_11 -100.9(6) . . . . ?
Cl3_11 B4_11 B10_11 B11_11 148.6(6) . . . . ?
B1_11 B4_11 B10_11 B11_11 -0.5(8) . . . . ?
B3_11 B4_11 B10_11 B11_11 37.5(6) . . . . ?
B5_11 B4_11 B10_11 B3_11 -100.7(6) . . . . ?
B9_11 B4_11 B10_11 B3_11 -138.3(6) . . . . ?
Cl3_11 B4_11 B10_11 B3_11 111.1(7) . . . . ?
B1_11 B4_11 B10_11 B3_11 -38.0(6) . . . . ?
B5_11 B4_11 B10_11 Cl10_11 146.5(6) . . . . ?
B9_11 B4_11 B10_11 Cl10_11 108.8(7) . . . . ?
Cl3_11 B4_11 B10_11 Cl10_11 -1.7(10) . . . . ?
B1_11 B4_11 B10_11 Cl10_11 -150.8(6) . . . . ?
B3_11 B4_11 B10_11 Cl10_11 -112.8(7) . . . . ?
B5_11 B4_11 B10_11 B12_11 -0.3(7) . . . . ?
B9_11 B4_11 B10_11 B12_11 -38.0(5) . . . . ?
Cl3_11 B4_11 B10_11 B12_11 -148.5(5) . . . . ?
B1_11 B4_11 B10_11 B12_11 62.4(7) . . . . ?
B3_11 B4_11 B10_11 B12_11 100.4(6) . . . . ?
B11_11 B3_11 B10_11 B9_11 100.4(6) . . . . ?
B2_11 B3_11 B10_11 B9_11 62.8(7) . . . . ?
Cl2_11 B3_11 B10_11 B9_11 -147.6(6) . . . . ?
B4_11 B3_11 B10_11 B9_11 -37.4(5) . . . . ?
B1_11 B3_11 B10_11 B9_11 0.3(8) . . . . ?
B11_11 B3_11 B10_11 B4_11 137.8(6) . . . . ?
B2_11 B3_11 B10_11 B4_11 100.2(6) . . . . ?
Cl2_11 B3_11 B10_11 B4_11 -110.2(7) . . . . ?
B1_11 B3_11 B10_11 B4_11 37.6(5) . . . . ?
B2_11 B3_11 B10_11 B11_11 -37.6(6) . . . . ?
Cl2_11 B3_11 B10_11 B11_11 112.0(7) . . . . ?
B4_11 B3_11 B10_11 B11_11 -137.8(6) . . . . ?
B1_11 B3_11 B10_11 B11_11 -100.1(6) . . . . ?
B11_11 B3_11 B10_11 Cl10_11 -108.7(7) . . . . ?
B2_11 B3_11 B10_11 Cl10_11 -146.3(6) . . . . ?
Cl2_11 B3_11 B10_11 Cl10_11 3.3(10) . . . . ?
B4_11 B3_11 B10_11 Cl10_11 113.5(7) . . . . ?
B1_11 B3_11 B10_11 Cl10_11 151.2(6) . . . . ?
B11_11 B3_11 B10_11 B12_11 36.6(5) . . . . ?
B2_11 B3_11 B10_11 B12_11 -1.0(8) . . . . ?
Cl2_11 B3_11 B10_11 B12_11 148.6(6) . . . . ?
B4_11 B3_11 B10_11 B12_11 -101.1(6) . . . . ?
B1_11 B3_11 B10_11 B12_11 -63.5(7) . . . . ?
B2_11 B3_11 B11_11 B12_11 100.8(6) . . . . ?
B10_11 B3_11 B11_11 B12_11 -37.5(6) . . . . ?
Cl2_11 B3_11 B11_11 B12_11 -149.8(5) . . . . ?
B4_11 B3_11 B11_11 B12_11 0.0(8) . . . . ?
B1_11 B3_11 B11_11 B12_11 63.0(7) . . . . ?
B2_11 B3_11 B11_11 B10_11 138.3(6) . . . . ?
Cl2_11 B3_11 B11_11 B10_11 -112.3(7) . . . . ?
B4_11 B3_11 B11_11 B10_11 37.5(5) . . . . ?
B1_11 B3_11 B11_11 B10_11 100.4(6) . . . . ?
B2_11 B3_11 B11_11 B7_11 36.8(6) . . . . ?
B10_11 B3_11 B11_11 B7_11 -101.5(6) . . . . ?
Cl2_11 B3_11 B11_11 B7_11 146.2(6) . . . . ?
B4_11 B3_11 B11_11 B7_11 -64.0(7) . . . . ?
B1_11 B3_11 B11_11 B7_11 -1.1(8) . . . . ?
B10_11 B3_11 B11_11 B2_11 -138.3(6) . . . . ?
Cl2_11 B3_11 B11_11 B2_11 109.4(6) . . . . ?
B4_11 B3_11 B11_11 B2_11 -100.8(6) . . . . ?
B1_11 B3_11 B11_11 B2_11 -37.8(5) . . . . ?
B2_11 B3_11 B11_11 Cl11_11 -113.5(7) . . . . ?
B10_11 B3_11 B11_11 Cl11_11 108.2(7) . . . . ?
Cl2_11 B3_11 B11_11 Cl11_11 -4.1(9) . . . . ?
B4_11 B3_11 B11_11 Cl11_11 145.7(6) . . . . ?
B1_11 B3_11 B11_11 Cl11_11 -151.3(6) . . . . ?
B9_11 B10_11 B11_11 B3_11 -101.3(6) . . . . ?
B4_11 B10_11 B11_11 B3_11 -37.9(6) . . . . ?
Cl10_11 B10_11 B11_11 B3_11 113.6(7) . . . . ?
B12_11 B10_11 B11_11 B3_11 -138.7(6) . . . . ?
B9_11 B10_11 B11_11 B12_11 37.4(6) . . . . ?
B4_11 B10_11 B11_11 B12_11 100.8(6) . . . . ?
B3_11 B10_11 B11_11 B12_11 138.7(6) . . . . ?
Cl10_11 B10_11 B11_11 B12_11 -107.7(6) . . . . ?
B9_11 B10_11 B11_11 B7_11 0.4(8) . . . . ?
B4_11 B10_11 B11_11 B7_11 63.8(7) . . . . ?
B3_11 B10_11 B11_11 B7_11 101.7(7) . . . . ?
Cl10_11 B10_11 B11_11 B7_11 -144.7(6) . . . . ?
B12_11 B10_11 B11_11 B7_11 -37.0(6) . . . . ?
B9_11 B10_11 B11_11 B2_11 -63.8(7) . . . . ?
B4_11 B10_11 B11_11 B2_11 -0.4(8) . . . . ?
B3_11 B10_11 B11_11 B2_11 37.5(6) . . . . ?
Cl10_11 B10_11 B11_11 B2_11 151.1(6) . . . . ?
B12_11 B10_11 B11_11 B2_11 -101.2(6) . . . . ?
B9_11 B10_11 B11_11 Cl11_11 146.8(6) . . . . ?
B4_11 B10_11 B11_11 Cl11_11 -149.8(6) . . . . ?
B3_11 B10_11 B11_11 Cl11_11 -111.9(7) . . . . ?
Cl10_11 B10_11 B11_11 Cl11_11 1.7(9) . . . . ?
B12_11 B10_11 B11_11 Cl11_11 109.4(7) . . . . ?
Cl7_11 B7_11 B11_11 B3_11 -147.1(6) . . . . ?
B12_11 B7_11 B11_11 B3_11 101.3(6) . . . . ?
B2_11 B7_11 B11_11 B3_11 -36.6(6) . . . . ?
B8_11 B7_11 B11_11 B3_11 63.7(7) . . . . ?
B6_11 B7_11 B11_11 B3_11 1.5(8) . . . . ?
Cl7_11 B7_11 B11_11 B12_11 111.6(7) . . . . ?
B2_11 B7_11 B11_11 B12_11 -137.9(6) . . . . ?
B8_11 B7_11 B11_11 B12_11 -37.6(5) . . . . ?
B6_11 B7_11 B11_11 B12_11 -99.8(6) . . . . ?
Cl7_11 B7_11 B11_11 B10_11 148.7(6) . . . . ?
B12_11 B7_11 B11_11 B10_11 37.2(6) . . . . ?
B2_11 B7_11 B11_11 B10_11 -100.8(6) . . . . ?
B8_11 B7_11 B11_11 B10_11 -0.4(8) . . . . ?
B6_11 B7_11 B11_11 B10_11 -62.7(7) . . . . ?
Cl7_11 B7_11 B11_11 B2_11 -110.5(7) . . . . ?
B12_11 B7_11 B11_11 B2_11 137.9(6) . . . . ?
B8_11 B7_11 B11_11 B2_11 100.3(6) . . . . ?
B6_11 B7_11 B11_11 B2_11 38.1(5) . . . . ?
Cl7_11 B7_11 B11_11 Cl11_11 3.2(10) . . . . ?
B12_11 B7_11 B11_11 Cl11_11 -108.4(7) . . . . ?
B2_11 B7_11 B11_11 Cl11_11 113.7(7) . . . . ?
B8_11 B7_11 B11_11 Cl11_11 -146.0(6) . . . . ?
B6_11 B7_11 B11_11 Cl11_11 151.8(6) . . . . ?
B1_11 B2_11 B11_11 B3_11 38.7(6) . . . . ?
Cl6_11 B2_11 B11_11 B3_11 -111.0(7) . . . . ?
B6_11 B2_11 B11_11 B3_11 101.2(6) . . . . ?
B7_11 B2_11 B11_11 B3_11 139.5(6) . . . . ?
B1_11 B2_11 B11_11 B12_11 -63.0(7) . . . . ?
B3_11 B2_11 B11_11 B12_11 -101.7(6) . . . . ?
Cl6_11 B2_11 B11_11 B12_11 147.2(6) . . . . ?
B6_11 B2_11 B11_11 B12_11 -0.6(8) . . . . ?
B7_11 B2_11 B11_11 B12_11 37.8(5) . . . . ?
B1_11 B2_11 B11_11 B10_11 1.3(8) . . . . ?
B3_11 B2_11 B11_11 B10_11 -37.5(6) . . . . ?
Cl6_11 B2_11 B11_11 B10_11 -148.5(6) . . . . ?
B6_11 B2_11 B11_11 B10_11 63.7(7) . . . . ?
B7_11 B2_11 B11_11 B10_11 102.0(6) . . . . ?
B1_11 B2_11 B11_11 B7_11 -100.8(6) . . . . ?
B3_11 B2_11 B11_11 B7_11 -139.5(6) . . . . ?
Cl6_11 B2_11 B11_11 B7_11 109.5(7) . . . . ?
B6_11 B2_11 B11_11 B7_11 -38.3(5) . . . . ?
B1_11 B2_11 B11_11 Cl11_11 149.0(6) . . . . ?
B3_11 B2_11 B11_11 Cl11_11 110.2(7) . . . . ?
Cl6_11 B2_11 B11_11 Cl11_11 -0.8(10) . . . . ?
B6_11 B2_11 B11_11 Cl11_11 -148.6(6) . . . . ?
B7_11 B2_11 B11_11 Cl11_11 -110.3(7) . . . . ?
B6_11 B8_11 B12_11 B11_11 -0.8(8) . . . . ?
B9_11 B8_11 B12_11 B11_11 100.0(6) . . . . ?
Cl8_11 B8_11 B12_11 B11_11 -147.2(5) . . . . ?
B5_11 B8_11 B12_11 B11_11 62.5(7) . . . . ?
B7_11 B8_11 B12_11 B11_11 -38.4(5) . . . . ?
B6_11 B8_11 B12_11 B7_11 37.6(6) . . . . ?
B9_11 B8_11 B12_11 B7_11 138.4(6) . . . . ?
Cl8_11 B8_11 B12_11 B7_11 -108.8(6) . . . . ?
B5_11 B8_11 B12_11 B7_11 100.9(6) . . . . ?
B6_11 B8_11 B12_11 B9_11 -100.8(6) . . . . ?
Cl8_11 B8_11 B12_11 B9_11 112.8(6) . . . . ?
B5_11 B8_11 B12_11 B9_11 -37.5(5) . . . . ?
B7_11 B8_11 B12_11 B9_11 -138.4(6) . . . . ?
B6_11 B8_11 B12_11 Cl12_11 149.0(6) . . . . ?
B9_11 B8_11 B12_11 Cl12_11 -110.2(6) . . . . ?
Cl8_11 B8_11 B12_11 Cl12_11 2.6(9) . . . . ?
B5_11 B8_11 B12_11 Cl12_11 -147.8(5) . . . . ?
B7_11 B8_11 B12_11 Cl12_11 111.4(6) . . . . ?
B6_11 B8_11 B12_11 B10_11 -64.0(7) . . . . ?
B9_11 B8_11 B12_11 B10_11 36.8(5) . . . . ?
Cl8_11 B8_11 B12_11 B10_11 149.6(5) . . . . ?
B5_11 B8_11 B12_11 B10_11 -0.7(7) . . . . ?
B7_11 B8_11 B12_11 B10_11 -101.6(6) . . . . ?
B3_11 B11_11 B12_11 B8_11 -63.0(7) . . . . ?
B10_11 B11_11 B12_11 B8_11 -100.3(6) . . . . ?
B7_11 B11_11 B12_11 B8_11 38.7(6) . . . . ?
B2_11 B11_11 B12_11 B8_11 0.8(7) . . . . ?
Cl11_11 B11_11 B12_11 B8_11 150.4(6) . . . . ?
B3_11 B11_11 B12_11 B7_11 -101.8(6) . . . . ?
B10_11 B11_11 B12_11 B7_11 -139.1(6) . . . . ?
B2_11 B11_11 B12_11 B7_11 -37.9(6) . . . . ?
Cl11_11 B11_11 B12_11 B7_11 111.7(7) . . . . ?
B3_11 B11_11 B12_11 B9_11 0.5(8) . . . . ?
B10_11 B11_11 B12_11 B9_11 -36.8(5) . . . . ?
B7_11 B11_11 B12_11 B9_11 102.3(6) . . . . ?
B2_11 B11_11 B12_11 B9_11 64.4(7) . . . . ?
Cl11_11 B11_11 B12_11 B9_11 -146.0(6) . . . . ?
B3_11 B11_11 B12_11 Cl12_11 146.8(5) . . . . ?
B10_11 B11_11 B12_11 Cl12_11 109.5(6) . . . . ?
B7_11 B11_11 B12_11 Cl12_11 -111.4(6) . . . . ?
B2_11 B11_11 B12_11 Cl12_11 -149.3(5) . . . . ?
Cl11_11 B11_11 B12_11 Cl12_11 0.3(9) . . . . ?
B3_11 B11_11 B12_11 B10_11 37.3(5) . . . . ?
B7_11 B11_11 B12_11 B10_11 139.1(6) . . . . ?
B2_11 B11_11 B12_11 B10_11 101.2(6) . . . . ?
Cl11_11 B11_11 B12_11 B10_11 -109.3(7) . . . . ?
Cl7_11 B7_11 B12_11 B8_11 110.9(7) . . . . ?
B11_11 B7_11 B12_11 B8_11 -137.1(6) . . . . ?
B2_11 B7_11 B12_11 B8_11 -99.6(6) . . . . ?
B6_11 B7_11 B12_11 B8_11 -36.7(6) . . . . ?
Cl7_11 B7_11 B12_11 B11_11 -112.0(7) . . . . ?
B2_11 B7_11 B12_11 B11_11 37.4(5) . . . . ?
B8_11 B7_11 B12_11 B11_11 137.1(6) . . . . ?
B6_11 B7_11 B12_11 B11_11 100.4(6) . . . . ?
Cl7_11 B7_11 B12_11 B9_11 148.4(6) . . . . ?
B11_11 B7_11 B12_11 B9_11 -99.6(6) . . . . ?
B2_11 B7_11 B12_11 B9_11 -62.1(7) . . . . ?
B8_11 B7_11 B12_11 B9_11 37.5(5) . . . . ?
B6_11 B7_11 B12_11 B9_11 0.9(8) . . . . ?
Cl7_11 B7_11 B12_11 Cl12_11 -1.4(10) . . . . ?
B11_11 B7_11 B12_11 Cl12_11 110.6(7) . . . . ?
B2_11 B7_11 B12_11 Cl12_11 148.1(6) . . . . ?
B8_11 B7_11 B12_11 Cl12_11 -112.3(7) . . . . ?
B6_11 B7_11 B12_11 Cl12_11 -149.0(6) . . . . ?
Cl7_11 B7_11 B12_11 B10_11 -148.7(6) . . . . ?
B11_11 B7_11 B12_11 B10_11 -36.7(6) . . . . ?
B2_11 B7_11 B12_11 B10_11 0.8(8) . . . . ?
B8_11 B7_11 B12_11 B10_11 100.4(6) . . . . ?
B6_11 B7_11 B12_11 B10_11 63.8(7) . . . . ?
B10_11 B9_11 B12_11 B8_11 138.4(6) . . . . ?
B4_11 B9_11 B12_11 B8_11 100.5(6) . . . . ?
B5_11 B9_11 B12_11 B8_11 37.5(5) . . . . ?
Cl9_11 B9_11 B12_11 B8_11 -110.6(7) . . . . ?
B10_11 B9_11 B12_11 B11_11 37.0(5) . . . . ?
B4_11 B9_11 B12_11 B11_11 -0.9(7) . . . . ?
B5_11 B9_11 B12_11 B11_11 -63.9(7) . . . . ?
B8_11 B9_11 B12_11 B11_11 -101.4(6) . . . . ?
Cl9_11 B9_11 B12_11 B11_11 148.1(6) . . . . ?
B10_11 B9_11 B12_11 B7_11 100.6(6) . . . . ?
B4_11 B9_11 B12_11 B7_11 62.7(7) . . . . ?
B5_11 B9_11 B12_11 B7_11 -0.4(8) . . . . ?
B8_11 B9_11 B12_11 B7_11 -37.8(6) . . . . ?
Cl9_11 B9_11 B12_11 B7_11 -148.4(6) . . . . ?
B10_11 B9_11 B12_11 Cl12_11 -109.3(6) . . . . ?
B4_11 B9_11 B12_11 Cl12_11 -147.3(6) . . . . ?
B5_11 B9_11 B12_11 Cl12_11 149.7(6) . . . . ?
B8_11 B9_11 B12_11 Cl12_11 112.2(7) . . . . ?
Cl9_11 B9_11 B12_11 Cl12_11 1.7(9) . . . . ?
B4_11 B9_11 B12_11 B10_11 -37.9(5) . . . . ?
B5_11 B9_11 B12_11 B10_11 -100.9(6) . . . . ?
B8_11 B9_11 B12_11 B10_11 -138.4(6) . . . . ?
Cl9_11 B9_11 B12_11 B10_11 111.0(7) . . . . ?
B9_11 B10_11 B12_11 B8_11 -37.2(5) . . . . ?
B4_11 B10_11 B12_11 B8_11 0.6(7) . . . . ?
B11_11 B10_11 B12_11 B8_11 101.1(6) . . . . ?
B3_11 B10_11 B12_11 B8_11 64.5(7) . . . . ?
Cl10_11 B10_11 B12_11 B8_11 -148.2(5) . . . . ?
B9_11 B10_11 B12_11 B11_11 -138.3(6) . . . . ?
B4_11 B10_11 B12_11 B11_11 -100.5(6) . . . . ?
B3_11 B10_11 B12_11 B11_11 -36.6(6) . . . . ?
Cl10_11 B10_11 B12_11 B11_11 110.7(6) . . . . ?
B9_11 B10_11 B12_11 B7_11 -101.6(6) . . . . ?
B4_11 B10_11 B12_11 B7_11 -63.7(7) . . . . ?
B11_11 B10_11 B12_11 B7_11 36.8(6) . . . . ?
B3_11 B10_11 B12_11 B7_11 0.1(8) . . . . ?
Cl10_11 B10_11 B12_11 B7_11 147.4(5) . . . . ?
B4_11 B10_11 B12_11 B9_11 37.8(5) . . . . ?
B11_11 B10_11 B12_11 B9_11 138.3(6) . . . . ?
B3_11 B10_11 B12_11 B9_11 101.7(6) . . . . ?
Cl10_11 B10_11 B12_11 B9_11 -111.0(6) . . . . ?
B9_11 B10_11 B12_11 Cl12_11 110.6(6) . . . . ?
B4_11 B10_11 B12_11 Cl12_11 148.4(5) . . . . ?
B11_11 B10_11 B12_11 Cl12_11 -111.1(6) . . . . ?
B3_11 B10_11 B12_11 Cl12_11 -147.7(5) . . . . ?
Cl10_11 B10_11 B12_11 Cl12_11 -0.4(8) . . . . ?
B4_12 B1_12 B2_12 B3_12 137.6(6) . . . . ?
B5_12 B1_12 B2_12 B3_12 37.3(6) . . . . ?
Cl1_12 B1_12 B2_12 B3_12 -112.0(7) . . . . ?
B6_12 B1_12 B2_12 B3_12 100.7(7) . . . . ?
B3_12 B1_12 B2_12 B4_12 -137.6(6) . . . . ?
B5_12 B1_12 B2_12 B4_12 -100.3(6) . . . . ?
Cl1_12 B1_12 B2_12 B4_12 110.4(7) . . . . ?
B6_12 B1_12 B2_12 B4_12 -36.9(6) . . . . ?
B3_12 B1_12 B2_12 B11_12 -37.3(6) . . . . ?
B4_12 B1_12 B2_12 B11_12 100.4(7) . . . . ?
B5_12 B1_12 B2_12 B11_12 0.0(8) . . . . ?
Cl1_12 B1_12 B2_12 B11_12 -149.3(6) . . . . ?
B6_12 B1_12 B2_12 B11_12 63.5(8) . . . . ?
B3_12 B1_12 B2_12 Cl2_12 111.1(7) . . . . ?
B4_12 B1_12 B2_12 Cl2_12 -111.2(7) . . . . ?
B5_12 B1_12 B2_12 Cl2_12 148.4(6) . . . . ?
Cl1_12 B1_12 B2_12 Cl2_12 -0.9(10) . . . . ?
B6_12 B1_12 B2_12 Cl2_12 -148.1(6) . . . . ?
B3_12 B1_12 B2_12 B10_12 -99.8(7) . . . . ?
B4_12 B1_12 B2_12 B10_12 37.8(6) . . . . ?
B5_12 B1_12 B2_12 B10_12 -62.5(8) . . . . ?
Cl1_12 B1_12 B2_12 B10_12 148.2(6) . . . . ?
B6_12 B1_12 B2_12 B10_12 1.0(8) . . . . ?
B2_12 B1_12 B3_12 B5_12 138.3(6) . . . . ?
B4_12 B1_12 B3_12 B5_12 99.9(7) . . . . ?
Cl1_12 B1_12 B3_12 B5_12 -110.0(8) . . . . ?
B6_12 B1_12 B3_12 B5_12 37.1(6) . . . . ?
B2_12 B1_12 B3_12 B11_12 37.5(6) . . . . ?
B4_12 B1_12 B3_12 B11_12 -1.0(9) . . . . ?
B5_12 B1_12 B3_12 B11_12 -100.8(7) . . . . ?
Cl1_12 B1_12 B3_12 B11_12 149.2(6) . . . . ?
B6_12 B1_12 B3_12 B11_12 -63.8(8) . . . . ?
B4_12 B1_12 B3_12 B2_12 -38.4(6) . . . . ?
B5_12 B1_12 B3_12 B2_12 -138.3(6) . . . . ?
Cl1_12 B1_12 B3_12 B2_12 111.7(8) . . . . ?
B6_12 B1_12 B3_12 B2_12 -101.3(6) . . . . ?
B2_12 B1_12 B3_12 Cl3_12 -109.9(7) . . . . ?
B4_12 B1_12 B3_12 Cl3_12 -148.3(6) . . . . ?
B5_12 B1_12 B3_12 Cl3_12 111.8(7) . . . . ?
Cl1_12 B1_12 B3_12 Cl3_12 1.8(11) . . . . ?
B6_12 B1_12 B3_12 Cl3_12 148.8(6) . . . . ?
B2_12 B1_12 B3_12 B9_12 101.0(7) . . . . ?
B4_12 B1_12 B3_12 B9_12 62.5(8) . . . . ?
B5_12 B1_12 B3_12 B9_12 -37.4(6) . . . . ?
Cl1_12 B1_12 B3_12 B9_12 -147.3(7) . . . . ?
B6_12 B1_12 B3_12 B9_12 -0.3(8) . . . . ?
B4_12 B2_12 B3_12 B1_12 38.3(6) . . . . ?
B11_12 B2_12 B3_12 B1_12 138.2(7) . . . . ?
Cl2_12 B2_12 B3_12 B1_12 -109.3(7) . . . . ?
B10_12 B2_12 B3_12 B1_12 102.0(7) . . . . ?
B1_12 B2_12 B3_12 B5_12 -37.6(6) . . . . ?
B4_12 B2_12 B3_12 B5_12 0.8(8) . . . . ?
B11_12 B2_12 B3_12 B5_12 100.6(7) . . . . ?
Cl2_12 B2_12 B3_12 B5_12 -146.9(6) . . . . ?
B10_12 B2_12 B3_12 B5_12 64.4(8) . . . . ?
B1_12 B2_12 B3_12 B11_12 -138.2(7) . . . . ?
B4_12 B2_12 B3_12 B11_12 -99.9(7) . . . . ?
Cl2_12 B2_12 B3_12 B11_12 112.5(7) . . . . ?
B10_12 B2_12 B3_12 B11_12 -36.2(6) . . . . ?
B1_12 B2_12 B3_12 Cl3_12 109.9(7) . . . . ?
B4_12 B2_12 B3_12 Cl3_12 148.2(6) . . . . ?
B11_12 B2_12 B3_12 Cl3_12 -111.9(7) . . . . ?
Cl2_12 B2_12 B3_12 Cl3_12 0.6(10) . . . . ?
B10_12 B2_12 B3_12 Cl3_12 -148.1(6) . . . . ?
B1_12 B2_12 B3_12 B9_12 -101.3(6) . . . . ?
B4_12 B2_12 B3_12 B9_12 -62.9(7) . . . . ?
B11_12 B2_12 B3_12 B9_12 36.9(6) . . . . ?
Cl2_12 B2_12 B3_12 B9_12 149.4(6) . . . . ?
B10_12 B2_12 B3_12 B9_12 0.7(8) . . . . ?
B1_12 B2_12 B4_12 B6_12 37.8(6) . . . . ?
B3_12 B2_12 B4_12 B6_12 -0.4(8) . . . . ?
B11_12 B2_12 B4_12 B6_12 -63.5(8) . . . . ?
Cl2_12 B2_12 B4_12 B6_12 147.3(6) . . . . ?
B10_12 B2_12 B4_12 B6_12 -100.2(6) . . . . ?
B1_12 B2_12 B4_12 B8_12 100.8(7) . . . . ?
B3_12 B2_12 B4_12 B8_12 62.6(8) . . . . ?
B11_12 B2_12 B4_12 B8_12 -0.5(8) . . . . ?
Cl2_12 B2_12 B4_12 B8_12 -149.7(6) . . . . ?
B10_12 B2_12 B4_12 B8_12 -37.2(6) . . . . ?
B3_12 B2_12 B4_12 B1_12 -38.2(6) . . . . ?
B11_12 B2_12 B4_12 B1_12 -101.3(7) . . . . ?
Cl2_12 B2_12 B4_12 B1_12 109.5(7) . . . . ?
B10_12 B2_12 B4_12 B1_12 -138.0(6) . . . . ?
B1_12 B2_12 B4_12 B10_12 138.0(6) . . . . ?
B3_12 B2_12 B4_12 B10_12 99.8(7) . . . . ?
B11_12 B2_12 B4_12 B10_12 36.7(6) . . . . ?
Cl2_12 B2_12 B4_12 B10_12 -112.5(7) . . . . ?
B1_12 B2_12 B4_12 Cl4_12 -110.9(7) . . . . ?
B3_12 B2_12 B4_12 Cl4_12 -149.0(6) . . . . ?
B11_12 B2_12 B4_12 Cl4_12 147.9(6) . . . . ?
Cl2_12 B2_12 B4_12 Cl4_12 -1.4(9) . . . . ?
B10_12 B2_12 B4_12 Cl4_12 111.1(7) . . . . ?
B2_12 B1_12 B4_12 B6_12 -138.5(6) . . . . ?
B3_12 B1_12 B4_12 B6_12 -99.9(7) . . . . ?
B5_12 B1_12 B4_12 B6_12 -36.7(6) . . . . ?
Cl1_12 B1_12 B4_12 B6_12 109.5(8) . . . . ?
B2_12 B1_12 B4_12 B8_12 -101.1(7) . . . . ?
B3_12 B1_12 B4_12 B8_12 -62.6(9) . . . . ?
B5_12 B1_12 B4_12 B8_12 0.6(9) . . . . ?
Cl1_12 B1_12 B4_12 B8_12 146.8(6) . . . . ?
B6_12 B1_12 B4_12 B8_12 37.3(6) . . . . ?
B3_12 B1_12 B4_12 B2_12 38.5(6) . . . . ?
B5_12 B1_12 B4_12 B2_12 101.8(7) . . . . ?
Cl1_12 B1_12 B4_12 B2_12 -112.1(8) . . . . ?
B6_12 B1_12 B4_12 B2_12 138.5(6) . . . . ?
B2_12 B1_12 B4_12 B10_12 -37.9(6) . . . . ?
B3_12 B1_12 B4_12 B10_12 0.7(9) . . . . ?
B5_12 B1_12 B4_12 B10_12 63.9(8) . . . . ?
Cl1_12 B1_12 B4_12 B10_12 -149.9(6) . . . . ?
B6_12 B1_12 B4_12 B10_12 100.6(7) . . . . ?
B2_12 B1_12 B4_12 Cl4_12 110.0(8) . . . . ?
B3_12 B1_12 B4_12 Cl4_12 148.5(6) . . . . ?
B5_12 B1_12 B4_12 Cl4_12 -148.2(6) . . . . ?
Cl1_12 B1_12 B4_12 Cl4_12 -2.1(11) . . . . ?
B6_12 B1_12 B4_12 Cl4_12 -111.5(8) . . . . ?
B1_12 B3_12 B5_12 Cl5_12 110.3(8) . . . . ?
B11_12 B3_12 B5_12 Cl5_12 -149.1(7) . . . . ?
B2_12 B3_12 B5_12 Cl5_12 147.0(6) . . . . ?
Cl3_12 B3_12 B5_12 Cl5_12 -0.2(11) . . . . ?
B9_12 B3_12 B5_12 Cl5_12 -111.1(8) . . . . ?
B1_12 B3_12 B5_12 B9_12 -138.6(6) . . . . ?
B11_12 B3_12 B5_12 B9_12 -38.0(6) . . . . ?
B2_12 B3_12 B5_12 B9_12 -101.9(7) . . . . ?
Cl3_12 B3_12 B5_12 B9_12 110.9(8) . . . . ?
B11_12 B3_12 B5_12 B1_12 100.6(7) . . . . ?
B2_12 B3_12 B5_12 B1_12 36.7(6) . . . . ?
Cl3_12 B3_12 B5_12 B1_12 -110.5(7) . . . . ?
B9_12 B3_12 B5_12 B1_12 138.6(6) . . . . ?
B1_12 B3_12 B5_12 B6_12 -37.5(6) . . . . ?
B11_12 B3_12 B5_12 B6_12 63.1(8) . . . . ?
B2_12 B3_12 B5_12 B6_12 -0.8(9) . . . . ?
Cl3_12 B3_12 B5_12 B6_12 -148.0(6) . . . . ?
B9_12 B3_12 B5_12 B6_12 101.1(7) . . . . ?
B1_12 B3_12 B5_12 B7_12 -100.2(6) . . . . ?
B11_12 B3_12 B5_12 B7_12 0.3(9) . . . . ?
B2_12 B3_12 B5_12 B7_12 -63.6(8) . . . . ?
Cl3_12 B3_12 B5_12 B7_12 149.3(6) . . . . ?
B9_12 B3_12 B5_12 B7_12 38.3(6) . . . . ?
B2_12 B1_12 B5_12 B3_12 -37.8(6) . . . . ?
B4_12 B1_12 B5_12 B3_12 -102.0(7) . . . . ?
Cl1_12 B1_12 B5_12 B3_12 111.9(7) . . . . ?
B6_12 B1_12 B5_12 B3_12 -138.5(6) . . . . ?
B2_12 B1_12 B5_12 Cl5_12 -149.4(6) . . . . ?
B3_12 B1_12 B5_12 Cl5_12 -111.6(7) . . . . ?
B4_12 B1_12 B5_12 Cl5_12 146.4(6) . . . . ?
Cl1_12 B1_12 B5_12 Cl5_12 0.3(10) . . . . ?
B6_12 B1_12 B5_12 Cl5_12 109.9(7) . . . . ?
B2_12 B1_12 B5_12 B9_12 -0.3(8) . . . . ?
B3_12 B1_12 B5_12 B9_12 37.5(6) . . . . ?
B4_12 B1_12 B5_12 B9_12 -64.6(8) . . . . ?
Cl1_12 B1_12 B5_12 B9_12 149.3(6) . . . . ?
B6_12 B1_12 B5_12 B9_12 -101.0(7) . . . . ?
B2_12 B1_12 B5_12 B6_12 100.7(7) . . . . ?
B3_12 B1_12 B5_12 B6_12 138.5(6) . . . . ?
B4_12 B1_12 B5_12 B6_12 36.4(6) . . . . ?
Cl1_12 B1_12 B5_12 B6_12 -109.7(7) . . . . ?
B2_12 B1_12 B5_12 B7_12 63.5(8) . . . . ?
B3_12 B1_12 B5_12 B7_12 101.3(7) . . . . ?
B4_12 B1_12 B5_12 B7_12 -0.7(8) . . . . ?
Cl1_12 B1_12 B5_12 B7_12 -146.8(6) . . . . ?
B6_12 B1_12 B5_12 B7_12 -37.2(6) . . . . ?
B2_12 B4_12 B6_12 B8_12 101.6(6) . . . . ?
B1_12 B4_12 B6_12 B8_12 138.1(6) . . . . ?
B10_12 B4_12 B6_12 B8_12 37.2(6) . . . . ?
Cl4_12 B4_12 B6_12 B8_12 -109.8(7) . . . . ?
B8_12 B4_12 B6_12 B7_12 -37.9(6) . . . . ?
B2_12 B4_12 B6_12 B7_12 63.7(8) . . . . ?
B1_12 B4_12 B6_12 B7_12 100.2(7) . . . . ?
B10_12 B4_12 B6_12 B7_12 -0.7(8) . . . . ?
Cl4_12 B4_12 B6_12 B7_12 -147.8(6) . . . . ?
B8_12 B4_12 B6_12 Cl6_12 112.0(7) . . . . ?
B2_12 B4_12 B6_12 Cl6_12 -146.4(6) . . . . ?
B1_12 B4_12 B6_12 Cl6_12 -109.9(7) . . . . ?
B10_12 B4_12 B6_12 Cl6_12 149.2(6) . . . . ?
Cl4_12 B4_12 B6_12 Cl6_12 2.1(9) . . . . ?
B8_12 B4_12 B6_12 B5_12 -101.7(7) . . . . ?
B2_12 B4_12 B6_12 B5_12 -0.1(8) . . . . ?
B1_12 B4_12 B6_12 B5_12 36.4(6) . . . . ?
B10_12 B4_12 B6_12 B5_12 -64.5(8) . . . . ?
Cl4_12 B4_12 B6_12 B5_12 148.4(6) . . . . ?
B8_12 B4_12 B6_12 B1_12 -138.1(6) . . . . ?
B2_12 B4_12 B6_12 B1_12 -36.5(6) . . . . ?
B10_12 B4_12 B6_12 B1_12 -100.9(7) . . . . ?
Cl4_12 B4_12 B6_12 B1_12 112.0(7) . . . . ?
B3_12 B5_12 B6_12 B8_12 -63.1(8) . . . . ?
Cl5_12 B5_12 B6_12 B8_12 148.4(7) . . . . ?
B9_12 B5_12 B6_12 B8_12 1.2(9) . . . . ?
B1_12 B5_12 B6_12 B8_12 -100.1(7) . . . . ?
B7_12 B5_12 B6_12 B8_12 37.9(6) . . . . ?
B3_12 B5_12 B6_12 B4_12 0.6(9) . . . . ?
Cl5_12 B5_12 B6_12 B4_12 -147.9(6) . . . . ?
B9_12 B5_12 B6_12 B4_12 64.9(8) . . . . ?
B1_12 B5_12 B6_12 B4_12 -36.4(6) . . . . ?
B7_12 B5_12 B6_12 B4_12 101.6(7) . . . . ?
B3_12 B5_12 B6_12 B7_12 -101.0(7) . . . . ?
Cl5_12 B5_12 B6_12 B7_12 110.5(8) . . . . ?
B9_12 B5_12 B6_12 B7_12 -36.7(6) . . . . ?
B1_12 B5_12 B6_12 B7_12 -138.0(7) . . . . ?
B3_12 B5_12 B6_12 Cl6_12 145.0(7) . . . . ?
Cl5_12 B5_12 B6_12 Cl6_12 -3.5(11) . . . . ?
B9_12 B5_12 B6_12 Cl6_12 -150.7(6) . . . . ?
B1_12 B5_12 B6_12 Cl6_12 108.1(8) . . . . ?
B7_12 B5_12 B6_12 Cl6_12 -113.9(8) . . . . ?
B3_12 B5_12 B6_12 B1_12 36.9(6) . . . . ?
Cl5_12 B5_12 B6_12 B1_12 -111.6(8) . . . . ?
B9_12 B5_12 B6_12 B1_12 101.3(7) . . . . ?
B7_12 B5_12 B6_12 B1_12 138.0(7) . . . . ?
B2_12 B1_12 B6_12 B8_12 0.0(8) . . . . ?
B3_12 B1_12 B6_12 B8_12 64.4(8) . . . . ?
B4_12 B1_12 B6_12 B8_12 -37.5(6) . . . . ?
B5_12 B1_12 B6_12 B8_12 101.4(7) . . . . ?
Cl1_12 B1_12 B6_12 B8_12 -147.9(6) . . . . ?
B2_12 B1_12 B6_12 B4_12 37.5(6) . . . . ?
B3_12 B1_12 B6_12 B4_12 101.9(7) . . . . ?
B5_12 B1_12 B6_12 B4_12 138.8(6) . . . . ?
Cl1_12 B1_12 B6_12 B4_12 -110.4(7) . . . . ?
B2_12 B1_12 B6_12 B7_12 -63.7(8) . . . . ?
B3_12 B1_12 B6_12 B7_12 0.7(8) . . . . ?
B4_12 B1_12 B6_12 B7_12 -101.2(7) . . . . ?
B5_12 B1_12 B6_12 B7_12 37.7(6) . . . . ?
Cl1_12 B1_12 B6_12 B7_12 148.5(6) . . . . ?
B2_12 B1_12 B6_12 Cl6_12 145.3(6) . . . . ?
B3_12 B1_12 B6_12 Cl6_12 -150.3(6) . . . . ?
B4_12 B1_12 B6_12 Cl6_12 107.8(7) . . . . ?
B5_12 B1_12 B6_12 Cl6_12 -113.3(7) . . . . ?
Cl1_12 B1_12 B6_12 Cl6_12 -2.5(10) . . . . ?
B2_12 B1_12 B6_12 B5_12 -101.4(7) . . . . ?
B3_12 B1_12 B6_12 B5_12 -37.0(6) . . . . ?
B4_12 B1_12 B6_12 B5_12 -138.8(6) . . . . ?
Cl1_12 B1_12 B6_12 B5_12 110.8(7) . . . . ?
B4_12 B6_12 B7_12 B8_12 37.9(6) . . . . ?
Cl6_12 B6_12 B7_12 B8_12 -109.9(8) . . . . ?
B5_12 B6_12 B7_12 B8_12 137.9(7) . . . . ?
B1_12 B6_12 B7_12 B8_12 100.7(7) . . . . ?
B8_12 B6_12 B7_12 B12_12 -37.9(6) . . . . ?
B4_12 B6_12 B7_12 B12_12 0.0(9) . . . . ?
Cl6_12 B6_12 B7_12 B12_12 -147.8(6) . . . . ?
B5_12 B6_12 B7_12 B12_12 100.0(7) . . . . ?
B1_12 B6_12 B7_12 B12_12 62.7(8) . . . . ?
B8_12 B6_12 B7_12 Cl7_12 112.4(8) . . . . ?
B4_12 B6_12 B7_12 Cl7_12 150.4(6) . . . . ?
Cl6_12 B6_12 B7_12 Cl7_12 2.5(11) . . . . ?
B5_12 B6_12 B7_12 Cl7_12 -109.7(8) . . . . ?
B1_12 B6_12 B7_12 Cl7_12 -146.9(6) . . . . ?
B8_12 B6_12 B7_12 B5_12 -137.9(7) . . . . ?
B4_12 B6_12 B7_12 B5_12 -100.0(7) . . . . ?
Cl6_12 B6_12 B7_12 B5_12 112.2(8) . . . . ?
B1_12 B6_12 B7_12 B5_12 -37.2(6) . . . . ?
B8_12 B6_12 B7_12 B9_12 -101.5(7) . . . . ?
B4_12 B6_12 B7_12 B9_12 -63.6(8) . . . . ?
Cl6_12 B6_12 B7_12 B9_12 148.6(6) . . . . ?
B5_12 B6_12 B7_12 B9_12 36.4(6) . . . . ?
B1_12 B6_12 B7_12 B9_12 -0.9(9) . . . . ?
B3_12 B5_12 B7_12 B8_12 63.4(8) . . . . ?
Cl5_12 B5_12 B7_12 B8_12 -146.7(6) . . . . ?
B9_12 B5_12 B7_12 B8_12 102.0(7) . . . . ?
B1_12 B5_12 B7_12 B8_12 0.6(8) . . . . ?
B6_12 B5_12 B7_12 B8_12 -37.3(6) . . . . ?
B3_12 B5_12 B7_12 B6_12 100.7(7) . . . . ?
Cl5_12 B5_12 B7_12 B6_12 -109.4(7) . . . . ?
B9_12 B5_12 B7_12 B6_12 139.2(7) . . . . ?
B1_12 B5_12 B7_12 B6_12 37.8(6) . . . . ?
B3_12 B5_12 B7_12 B12_12 -1.4(9) . . . . ?
Cl5_12 B5_12 B7_12 B12_12 148.5(6) . . . . ?
B9_12 B5_12 B7_12 B12_12 37.1(6) . . . . ?
B1_12 B5_12 B7_12 B12_12 -64.2(8) . . . . ?
B6_12 B5_12 B7_12 B12_12 -102.1(7) . . . . ?
B3_12 B5_12 B7_12 Cl7_12 -148.5(6) . . . . ?
Cl5_12 B5_12 B7_12 Cl7_12 1.3(10) . . . . ?
B9_12 B5_12 B7_12 Cl7_12 -110.0(7) . . . . ?
B1_12 B5_12 B7_12 Cl7_12 148.6(6) . . . . ?
B6_12 B5_12 B7_12 Cl7_12 110.8(8) . . . . ?
B3_12 B5_12 B7_12 B9_12 -38.5(6) . . . . ?
Cl5_12 B5_12 B7_12 B9_12 111.4(7) . . . . ?
B1_12 B5_12 B7_12 B9_12 -101.4(7) . . . . ?
B6_12 B5_12 B7_12 B9_12 -139.2(7) . . . . ?
B7_12 B6_12 B8_12 B4_12 137.8(7) . . . . ?
Cl6_12 B6_12 B8_12 B4_12 -107.7(7) . . . . ?
B5_12 B6_12 B8_12 B4_12 99.9(7) . . . . ?
B1_12 B6_12 B8_12 B4_12 37.0(6) . . . . ?
B4_12 B6_12 B8_12 B7_12 -137.8(7) . . . . ?
Cl6_12 B6_12 B8_12 B7_12 114.5(8) . . . . ?
B5_12 B6_12 B8_12 B7_12 -37.9(6) . . . . ?
B1_12 B6_12 B8_12 B7_12 -100.7(7) . . . . ?
B4_12 B6_12 B8_12 Cl8_12 110.6(7) . . . . ?
B7_12 B6_12 B8_12 Cl8_12 -111.6(7) . . . . ?
Cl6_12 B6_12 B8_12 Cl8_12 2.9(10) . . . . ?
B5_12 B6_12 B8_12 Cl8_12 -149.5(6) . . . . ?
B1_12 B6_12 B8_12 Cl8_12 147.6(6) . . . . ?
B4_12 B6_12 B8_12 B10_12 -38.0(6) . . . . ?
B7_12 B6_12 B8_12 B10_12 99.8(7) . . . . ?
Cl6_12 B6_12 B8_12 B10_12 -145.7(6) . . . . ?
B5_12 B6_12 B8_12 B10_12 61.9(8) . . . . ?
B1_12 B6_12 B8_12 B10_12 -1.0(8) . . . . ?
B4_12 B6_12 B8_12 B12_12 -101.0(7) . . . . ?
B7_12 B6_12 B8_12 B12_12 36.8(6) . . . . ?
Cl6_12 B6_12 B8_12 B12_12 151.3(6) . . . . ?
B5_12 B6_12 B8_12 B12_12 -1.2(9) . . . . ?
B1_12 B6_12 B8_12 B12_12 -64.0(8) . . . . ?
B2_12 B4_12 B8_12 B6_12 -100.4(7) . . . . ?
B1_12 B4_12 B8_12 B6_12 -38.2(6) . . . . ?
B10_12 B4_12 B8_12 B6_12 -138.1(6) . . . . ?
Cl4_12 B4_12 B8_12 B6_12 111.1(7) . . . . ?
B6_12 B4_12 B8_12 B7_12 37.9(6) . . . . ?
B2_12 B4_12 B8_12 B7_12 -62.5(8) . . . . ?
B1_12 B4_12 B8_12 B7_12 -0.3(9) . . . . ?
B10_12 B4_12 B8_12 B7_12 -100.2(7) . . . . ?
Cl4_12 B4_12 B8_12 B7_12 149.0(6) . . . . ?
B6_12 B4_12 B8_12 Cl8_12 -111.0(7) . . . . ?
B2_12 B4_12 B8_12 Cl8_12 148.6(6) . . . . ?
B1_12 B4_12 B8_12 Cl8_12 -149.2(6) . . . . ?
B10_12 B4_12 B8_12 Cl8_12 110.9(7) . . . . ?
Cl4_12 B4_12 B8_12 Cl8_12 0.0(10) . . . . ?
B6_12 B4_12 B8_12 B10_12 138.1(6) . . . . ?
B2_12 B4_12 B8_12 B10_12 37.7(6) . . . . ?
B1_12 B4_12 B8_12 B10_12 99.9(7) . . . . ?
Cl4_12 B4_12 B8_12 B10_12 -110.9(7) . . . . ?
B6_12 B4_12 B8_12 B12_12 100.7(7) . . . . ?
B2_12 B4_12 B8_12 B12_12 0.3(8) . . . . ?
B1_12 B4_12 B8_12 B12_12 62.5(8) . . . . ?
B10_12 B4_12 B8_12 B12_12 -37.4(6) . . . . ?
Cl4_12 B4_12 B8_12 B12_12 -148.2(6) . . . . ?
B12_12 B7_12 B8_12 B6_12 138.5(7) . . . . ?
Cl7_12 B7_12 B8_12 B6_12 -109.3(8) . . . . ?
B5_12 B7_12 B8_12 B6_12 37.7(6) . . . . ?
B9_12 B7_12 B8_12 B6_12 100.7(7) . . . . ?
B6_12 B7_12 B8_12 B4_12 -37.9(6) . . . . ?
B12_12 B7_12 B8_12 B4_12 100.6(7) . . . . ?
Cl7_12 B7_12 B8_12 B4_12 -147.2(7) . . . . ?
B5_12 B7_12 B8_12 B4_12 -0.2(9) . . . . ?
B9_12 B7_12 B8_12 B4_12 62.8(8) . . . . ?
B6_12 B7_12 B8_12 Cl8_12 110.8(8) . . . . ?
B12_12 B7_12 B8_12 Cl8_12 -110.7(7) . . . . ?
Cl7_12 B7_12 B8_12 Cl8_12 1.4(11) . . . . ?
B5_12 B7_12 B8_12 Cl8_12 148.5(6) . . . . ?
B9_12 B7_12 B8_12 Cl8_12 -148.6(6) . . . . ?
B6_12 B7_12 B8_12 B10_12 -102.1(7) . . . . ?
B12_12 B7_12 B8_12 B10_12 36.4(6) . . . . ?
Cl7_12 B7_12 B8_12 B10_12 148.6(6) . . . . ?
B5_12 B7_12 B8_12 B10_12 -64.4(8) . . . . ?
B9_12 B7_12 B8_12 B10_12 -1.4(8) . . . . ?
B6_12 B7_12 B8_12 B12_12 -138.5(7) . . . . ?
Cl7_12 B7_12 B8_12 B12_12 112.1(8) . . . . ?
B5_12 B7_12 B8_12 B12_12 -100.8(7) . . . . ?
B9_12 B7_12 B8_12 B12_12 -37.9(6) . . . . ?
B3_12 B5_12 B9_12 Cl11_12 -112.7(7) . . . . ?
Cl5_12 B5_12 B9_12 Cl11_12 -0.6(10) . . . . ?
B1_12 B5_12 B9_12 Cl11_12 -149.6(6) . . . . ?
B6_12 B5_12 B9_12 Cl11_12 146.1(6) . . . . ?
B7_12 B5_12 B9_12 Cl11_12 109.9(7) . . . . ?
B3_12 B5_12 B9_12 B11_12 37.4(6) . . . . ?
Cl5_12 B5_12 B9_12 B11_12 149.5(6) . . . . ?
B1_12 B5_12 B9_12 B11_12 0.5(8) . . . . ?
B6_12 B5_12 B9_12 B11_12 -63.7(8) . . . . ?
B7_12 B5_12 B9_12 B11_12 -100.0(7) . . . . ?
B3_12 B5_12 B9_12 B12_12 100.5(7) . . . . ?
Cl5_12 B5_12 B9_12 B12_12 -147.4(6) . . . . ?
B1_12 B5_12 B9_12 B12_12 63.6(8) . . . . ?
B6_12 B5_12 B9_12 B12_12 -0.7(9) . . . . ?
B7_12 B5_12 B9_12 B12_12 -36.9(6) . . . . ?
Cl5_12 B5_12 B9_12 B3_12 112.1(7) . . . . ?
B1_12 B5_12 B9_12 B3_12 -36.9(6) . . . . ?
B6_12 B5_12 B9_12 B3_12 -101.2(7) . . . . ?
B7_12 B5_12 B9_12 B3_12 -137.4(7) . . . . ?
B3_12 B5_12 B9_12 B7_12 137.4(7) . . . . ?
Cl5_12 B5_12 B9_12 B7_12 -110.5(8) . . . . ?
B1_12 B5_12 B9_12 B7_12 100.5(7) . . . . ?
B6_12 B5_12 B9_12 B7_12 36.2(6) . . . . ?
B1_12 B3_12 B9_12 Cl11_12 147.3(6) . . . . ?
B5_12 B3_12 B9_12 Cl11_12 109.6(8) . . . . ?
B11_12 B3_12 B9_12 Cl11_12 -113.1(8) . . . . ?
B2_12 B3_12 B9_12 Cl11_12 -150.2(6) . . . . ?
Cl3_12 B3_12 B9_12 Cl11_12 -1.6(10) . . . . ?
B1_12 B3_12 B9_12 B11_12 -99.7(7) . . . . ?
B5_12 B3_12 B9_12 B11_12 -137.3(6) . . . . ?
B2_12 B3_12 B9_12 B11_12 -37.2(6) . . . . ?
Cl3_12 B3_12 B9_12 B11_12 111.4(7) . . . . ?
B1_12 B3_12 B9_12 B5_12 37.7(6) . . . . ?
B11_12 B3_12 B9_12 B5_12 137.3(6) . . . . ?
B2_12 B3_12 B9_12 B5_12 100.2(7) . . . . ?
Cl3_12 B3_12 B9_12 B5_12 -111.2(7) . . . . ?
B1_12 B3_12 B9_12 B12_12 -62.7(8) . . . . ?
B5_12 B3_12 B9_12 B12_12 -100.4(7) . . . . ?
B11_12 B3_12 B9_12 B12_12 36.9(6) . . . . ?
B2_12 B3_12 B9_12 B12_12 -0.2(8) . . . . ?
Cl3_12 B3_12 B9_12 B12_12 148.3(6) . . . . ?
B1_12 B3_12 B9_12 B7_12 -0.2(9) . . . . ?
B5_12 B3_12 B9_12 B7_12 -37.9(6) . . . . ?
B11_12 B3_12 B9_12 B7_12 99.4(7) . . . . ?
B2_12 B3_12 B9_12 B7_12 62.3(8) . . . . ?
Cl3_12 B3_12 B9_12 B7_12 -149.1(6) . . . . ?
B8_12 B7_12 B9_12 Cl11_12 149.1(6) . . . . ?
B6_12 B7_12 B9_12 Cl11_12 -147.9(7) . . . . ?
B12_12 B7_12 B9_12 Cl11_12 110.6(7) . . . . ?
Cl7_12 B7_12 B9_12 Cl11_12 -1.7(11) . . . . ?
B5_12 B7_12 B9_12 Cl11_12 -111.1(8) . . . . ?
B8_12 B7_12 B9_12 B11_12 -0.1(8) . . . . ?
B6_12 B7_12 B9_12 B11_12 62.9(8) . . . . ?
B12_12 B7_12 B9_12 B11_12 -38.6(6) . . . . ?
Cl7_12 B7_12 B9_12 B11_12 -150.9(6) . . . . ?
B5_12 B7_12 B9_12 B11_12 99.7(7) . . . . ?
B8_12 B7_12 B9_12 B5_12 -99.8(7) . . . . ?
B6_12 B7_12 B9_12 B5_12 -36.8(6) . . . . ?
B12_12 B7_12 B9_12 B5_12 -138.3(6) . . . . ?
Cl7_12 B7_12 B9_12 B5_12 109.4(8) . . . . ?
B8_12 B7_12 B9_12 B12_12 38.5(6) . . . . ?
B6_12 B7_12 B9_12 B12_12 101.5(7) . . . . ?
Cl7_12 B7_12 B9_12 B12_12 -112.3(8) . . . . ?
B5_12 B7_12 B9_12 B12_12 138.3(6) . . . . ?
B8_12 B7_12 B9_12 B3_12 -62.4(8) . . . . ?
B6_12 B7_12 B9_12 B3_12 0.7(9) . . . . ?
B12_12 B7_12 B9_12 B3_12 -100.9(7) . . . . ?
Cl7_12 B7_12 B9_12 B3_12 146.9(6) . . . . ?
B5_12 B7_12 B9_12 B3_12 37.4(6) . . . . ?
B6_12 B8_12 B10_12 B11_12 -61.4(8) . . . . ?
B4_12 B8_12 B10_12 B11_12 -99.2(7) . . . . ?
B7_12 B8_12 B10_12 B11_12 2.4(8) . . . . ?
Cl8_12 B8_12 B10_12 B11_12 149.9(6) . . . . ?
B12_12 B8_12 B10_12 B11_12 38.7(6) . . . . ?
B6_12 B8_12 B10_12 Cl9_12 147.9(6) . . . . ?
B4_12 B8_12 B10_12 Cl9_12 110.1(7) . . . . ?
B7_12 B8_12 B10_12 Cl9_12 -148.3(6) . . . . ?
Cl8_12 B8_12 B10_12 Cl9_12 -0.8(10) . . . . ?
B12_12 B8_12 B10_12 Cl9_12 -111.9(7) . . . . ?
B6_12 B8_12 B10_12 B12_12 -100.2(7) . . . . ?
B4_12 B8_12 B10_12 B12_12 -137.9(6) . . . . ?
B7_12 B8_12 B10_12 B12_12 -36.4(6) . . . . ?
Cl8_12 B8_12 B10_12 B12_12 111.1(7) . . . . ?
B6_12 B8_12 B10_12 B4_12 37.8(6) . . . . ?
B7_12 B8_12 B10_12 B4_12 101.6(7) . . . . ?
Cl8_12 B8_12 B10_12 B4_12 -110.9(7) . . . . ?
B12_12 B8_12 B10_12 B4_12 137.9(6) . . . . ?
B6_12 B8_12 B10_12 B2_12 1.5(8) . . . . ?
B4_12 B8_12 B10_12 B2_12 -36.2(6) . . . . ?
B7_12 B8_12 B10_12 B2_12 65.3(8) . . . . ?
Cl8_12 B8_12 B10_12 B2_12 -147.2(6) . . . . ?
B12_12 B8_12 B10_12 B2_12 101.7(7) . . . . ?
B6_12 B4_12 B10_12 B11_12 64.6(8) . . . . ?
B8_12 B4_12 B10_12 B11_12 101.6(7) . . . . ?
B2_12 B4_12 B10_12 B11_12 -36.9(6) . . . . ?
B1_12 B4_12 B10_12 B11_12 -0.1(8) . . . . ?
Cl4_12 B4_12 B10_12 B11_12 -148.2(6) . . . . ?
B6_12 B4_12 B10_12 Cl9_12 -149.1(6) . . . . ?
B8_12 B4_12 B10_12 Cl9_12 -112.0(7) . . . . ?
B2_12 B4_12 B10_12 Cl9_12 109.4(7) . . . . ?
B1_12 B4_12 B10_12 Cl9_12 146.2(6) . . . . ?
Cl4_12 B4_12 B10_12 Cl9_12 -1.9(10) . . . . ?
B6_12 B4_12 B10_12 B8_12 -37.1(6) . . . . ?
B2_12 B4_12 B10_12 B8_12 -138.5(6) . . . . ?
B1_12 B4_12 B10_12 B8_12 -101.8(7) . . . . ?
Cl4_12 B4_12 B10_12 B8_12 110.1(7) . . . . ?
B6_12 B4_12 B10_12 B12_12 1.1(8) . . . . ?
B8_12 B4_12 B10_12 B12_12 38.2(6) . . . . ?
B2_12 B4_12 B10_12 B12_12 -100.4(7) . . . . ?
B1_12 B4_12 B10_12 B12_12 -63.6(8) . . . . ?
Cl4_12 B4_12 B10_12 B12_12 148.3(6) . . . . ?
B6_12 B4_12 B10_12 B2_12 101.5(7) . . . . ?
B8_12 B4_12 B10_12 B2_12 138.5(6) . . . . ?
B1_12 B4_12 B10_12 B2_12 36.8(6) . . . . ?
Cl4_12 B4_12 B10_12 B2_12 -111.3(7) . . . . ?
B1_12 B2_12 B10_12 B11_12 100.3(7) . . . . ?
B3_12 B2_12 B10_12 B11_12 36.5(6) . . . . ?
B4_12 B2_12 B10_12 B11_12 138.3(7) . . . . ?
Cl2_12 B2_12 B10_12 B11_12 -111.6(8) . . . . ?
B1_12 B2_12 B10_12 Cl9_12 -148.7(6) . . . . ?
B3_12 B2_12 B10_12 Cl9_12 147.5(6) . . . . ?
B4_12 B2_12 B10_12 Cl9_12 -110.7(7) . . . . ?
B11_12 B2_12 B10_12 Cl9_12 111.0(7) . . . . ?
Cl2_12 B2_12 B10_12 Cl9_12 -0.6(10) . . . . ?
B1_12 B2_12 B10_12 B8_12 -1.5(8) . . . . ?
B3_12 B2_12 B10_12 B8_12 -65.3(8) . . . . ?
B4_12 B2_12 B10_12 B8_12 36.5(6) . . . . ?
B11_12 B2_12 B10_12 B8_12 -101.8(7) . . . . ?
Cl2_12 B2_12 B10_12 B8_12 146.5(6) . . . . ?
B1_12 B2_12 B10_12 B12_12 62.8(8) . . . . ?
B3_12 B2_12 B10_12 B12_12 -0.9(8) . . . . ?
B4_12 B2_12 B10_12 B12_12 100.9(7) . . . . ?
B11_12 B2_12 B10_12 B12_12 -37.4(6) . . . . ?
Cl2_12 B2_12 B10_12 B12_12 -149.1(6) . . . . ?
B1_12 B2_12 B10_12 B4_12 -38.0(6) . . . . ?
B3_12 B2_12 B10_12 B4_12 -101.8(7) . . . . ?
B11_12 B2_12 B10_12 B4_12 -138.3(7) . . . . ?
Cl2_12 B2_12 B10_12 B4_12 110.0(8) . . . . ?
B1_12 B3_12 B11_12 B10_12 0.9(9) . . . . ?
B5_12 B3_12 B11_12 B10_12 -63.3(8) . . . . ?
B2_12 B3_12 B11_12 B10_12 37.6(6) . . . . ?
Cl3_12 B3_12 B11_12 B10_12 147.9(6) . . . . ?
B9_12 B3_12 B11_12 B10_12 -101.4(7) . . . . ?
B1_12 B3_12 B11_12 B9_12 102.2(7) . . . . ?
B5_12 B3_12 B11_12 B9_12 38.1(6) . . . . ?
B2_12 B3_12 B11_12 B9_12 138.9(6) . . . . ?
Cl3_12 B3_12 B11_12 B9_12 -110.8(7) . . . . ?
B1_12 B3_12 B11_12 B2_12 -36.7(6) . . . . ?
B5_12 B3_12 B11_12 B2_12 -100.9(7) . . . . ?
Cl3_12 B3_12 B11_12 B2_12 110.3(7) . . . . ?
B9_12 B3_12 B11_12 B2_12 -138.9(6) . . . . ?
B1_12 B3_12 B11_12 B12_12 65.0(8) . . . . ?
B5_12 B3_12 B11_12 B12_12 0.8(9) . . . . ?
B2_12 B3_12 B11_12 B12_12 101.7(7) . . . . ?
Cl3_12 B3_12 B11_12 B12_12 -148.1(6) . . . . ?
B9_12 B3_12 B11_12 B12_12 -37.3(6) . . . . ?
B1_12 B3_12 B11_12 Cl10_12 -147.4(6) . . . . ?
B5_12 B3_12 B11_12 Cl10_12 148.4(6) . . . . ?
B2_12 B3_12 B11_12 Cl10_12 -110.7(8) . . . . ?
Cl3_12 B3_12 B11_12 Cl10_12 -0.5(11) . . . . ?
B9_12 B3_12 B11_12 Cl10_12 110.3(8) . . . . ?
Cl9_12 B10_12 B11_12 B3_12 -146.8(6) . . . . ?
B8_12 B10_12 B11_12 B3_12 62.1(8) . . . . ?
B12_12 B10_12 B11_12 B3_12 101.3(7) . . . . ?
B4_12 B10_12 B11_12 B3_12 -0.5(8) . . . . ?
B2_12 B10_12 B11_12 B3_12 -37.0(6) . . . . ?
Cl9_12 B10_12 B11_12 B9_12 148.6(6) . . . . ?
B8_12 B10_12 B11_12 B9_12 -2.5(8) . . . . ?
B12_12 B10_12 B11_12 B9_12 36.7(6) . . . . ?
B4_12 B10_12 B11_12 B9_12 -65.1(8) . . . . ?
B2_12 B10_12 B11_12 B9_12 -101.5(7) . . . . ?
Cl9_12 B10_12 B11_12 B2_12 -109.8(7) . . . . ?
B8_12 B10_12 B11_12 B2_12 99.1(7) . . . . ?
B12_12 B10_12 B11_12 B2_12 138.2(7) . . . . ?
B4_12 B10_12 B11_12 B2_12 36.5(6) . . . . ?
Cl9_12 B10_12 B11_12 B12_12 111.9(7) . . . . ?
B8_12 B10_12 B11_12 B12_12 -39.2(6) . . . . ?
B4_12 B10_12 B11_12 B12_12 -101.8(7) . . . . ?
B2_12 B10_12 B11_12 B12_12 -138.2(7) . . . . ?
Cl9_12 B10_12 B11_12 Cl10_12 2.6(10) . . . . ?
B8_12 B10_12 B11_12 Cl10_12 -148.5(6) . . . . ?
B12_12 B10_12 B11_12 Cl10_12 -109.3(7) . . . . ?
B4_12 B10_12 B11_12 Cl10_12 148.9(6) . . . . ?
B2_12 B10_12 B11_12 Cl10_12 112.5(7) . . . . ?
Cl11_12 B9_12 B11_12 B3_12 111.8(8) . . . . ?
B5_12 B9_12 B11_12 B3_12 -37.3(6) . . . . ?
B12_12 B9_12 B11_12 B3_12 -138.6(6) . . . . ?
B7_12 B9_12 B11_12 B3_12 -100.3(7) . . . . ?
Cl11_12 B9_12 B11_12 B10_12 -146.3(7) . . . . ?
B5_12 B9_12 B11_12 B10_12 64.6(8) . . . . ?
B12_12 B9_12 B11_12 B10_12 -36.8(6) . . . . ?
B3_12 B9_12 B11_12 B10_12 101.9(7) . . . . ?
B7_12 B9_12 B11_12 B10_12 1.6(8) . . . . ?
Cl11_12 B9_12 B11_12 B2_12 148.6(7) . . . . ?
B5_12 B9_12 B11_12 B2_12 -0.5(9) . . . . ?
B12_12 B9_12 B11_12 B2_12 -101.8(7) . . . . ?
B3_12 B9_12 B11_12 B2_12 36.8(6) . . . . ?
B7_12 B9_12 B11_12 B2_12 -63.5(8) . . . . ?
Cl11_12 B9_12 B11_12 B12_12 -109.6(8) . . . . ?
B5_12 B9_12 B11_12 B12_12 101.3(6) . . . . ?
B3_12 B9_12 B11_12 B12_12 138.6(6) . . . . ?
B7_12 B9_12 B11_12 B12_12 38.3(6) . . . . ?
Cl11_12 B9_12 B11_12 Cl10_12 -0.9(11) . . . . ?
B5_12 B9_12 B11_12 Cl10_12 -150.0(6) . . . . ?
B12_12 B9_12 B11_12 Cl10_12 108.7(7) . . . . ?
B3_12 B9_12 B11_12 Cl10_12 -112.7(8) . . . . ?
B7_12 B9_12 B11_12 Cl10_12 147.0(6) . . . . ?
B1_12 B2_12 B11_12 B3_12 37.5(6) . . . . ?
B4_12 B2_12 B11_12 B3_12 101.6(7) . . . . ?
Cl2_12 B2_12 B11_12 B3_12 -109.8(7) . . . . ?
B10_12 B2_12 B11_12 B3_12 138.9(6) . . . . ?
B1_12 B2_12 B11_12 B10_12 -101.4(7) . . . . ?
B3_12 B2_12 B11_12 B10_12 -138.9(6) . . . . ?
B4_12 B2_12 B11_12 B10_12 -37.3(6) . . . . ?
Cl2_12 B2_12 B11_12 B10_12 111.3(7) . . . . ?
B1_12 B2_12 B11_12 B9_12 0.3(9) . . . . ?
B3_12 B2_12 B11_12 B9_12 -37.2(6) . . . . ?
B4_12 B2_12 B11_12 B9_12 64.4(8) . . . . ?
Cl2_12 B2_12 B11_12 B9_12 -147.0(6) . . . . ?
B10_12 B2_12 B11_12 B9_12 101.7(7) . . . . ?
B1_12 B2_12 B11_12 B12_12 -63.6(8) . . . . ?
B3_12 B2_12 B11_12 B12_12 -101.2(7) . . . . ?
B4_12 B2_12 B11_12 B12_12 0.5(9) . . . . ?
Cl2_12 B2_12 B11_12 B12_12 149.1(6) . . . . ?
B10_12 B2_12 B11_12 B12_12 37.7(6) . . . . ?
B1_12 B2_12 B11_12 Cl10_12 149.6(6) . . . . ?
B3_12 B2_12 B11_12 Cl10_12 112.0(8) . . . . ?
B4_12 B2_12 B11_12 Cl10_12 -146.3(6) . . . . ?
Cl2_12 B2_12 B11_12 Cl10_12 2.3(11) . . . . ?
B10_12 B2_12 B11_12 Cl10_12 -109.1(8) . . . . ?
B8_12 B7_12 B12_12 Cl12_12 111.6(8) . . . . ?
B6_12 B7_12 B12_12 Cl12_12 148.6(7) . . . . ?
Cl7_12 B7_12 B12_12 Cl12_12 -1.2(11) . . . . ?
B5_12 B7_12 B12_12 Cl12_12 -147.5(7) . . . . ?
B9_12 B7_12 B12_12 Cl12_12 -110.5(8) . . . . ?
B8_12 B7_12 B12_12 B10_12 -36.4(6) . . . . ?
B6_12 B7_12 B12_12 B10_12 0.7(9) . . . . ?
Cl7_12 B7_12 B12_12 B10_12 -149.1(6) . . . . ?
B5_12 B7_12 B12_12 B10_12 64.6(8) . . . . ?
B9_12 B7_12 B12_12 B10_12 101.5(7) . . . . ?
B8_12 B7_12 B12_12 B11_12 -99.1(6) . . . . ?
B6_12 B7_12 B12_12 B11_12 -62.1(8) . . . . ?
Cl7_12 B7_12 B12_12 B11_12 148.1(7) . . . . ?
B5_12 B7_12 B12_12 B11_12 1.8(8) . . . . ?
B9_12 B7_12 B12_12 B11_12 38.8(6) . . . . ?
B8_12 B7_12 B12_12 B9_12 -137.9(6) . . . . ?
B6_12 B7_12 B12_12 B9_12 -100.9(7) . . . . ?
Cl7_12 B7_12 B12_12 B9_12 109.3(8) . . . . ?
B5_12 B7_12 B12_12 B9_12 -36.9(6) . . . . ?
B6_12 B7_12 B12_12 B8_12 37.0(6) . . . . ?
Cl7_12 B7_12 B12_12 B8_12 -112.8(8) . . . . ?
B5_12 B7_12 B12_12 B8_12 100.9(7) . . . . ?
B9_12 B7_12 B12_12 B8_12 137.9(6) . . . . ?
B11_12 B10_12 B12_12 Cl12_12 110.5(7) . . . . ?
Cl9_12 B10_12 B12_12 Cl12_12 -0.2(10) . . . . ?
B8_12 B10_12 B12_12 Cl12_12 -112.8(7) . . . . ?
B4_12 B10_12 B12_12 Cl12_12 -150.1(6) . . . . ?
B2_12 B10_12 B12_12 Cl12_12 147.7(6) . . . . ?
B11_12 B10_12 B12_12 B7_12 -100.5(7) . . . . ?
Cl9_12 B10_12 B12_12 B7_12 148.9(6) . . . . ?
B8_12 B10_12 B12_12 B7_12 36.3(6) . . . . ?
B4_12 B10_12 B12_12 B7_12 -1.1(8) . . . . ?
B2_12 B10_12 B12_12 B7_12 -63.3(8) . . . . ?
Cl9_12 B10_12 B12_12 B11_12 -110.7(8) . . . . ?
B8_12 B10_12 B12_12 B11_12 136.8(6) . . . . ?
B4_12 B10_12 B12_12 B11_12 99.4(7) . . . . ?
B2_12 B10_12 B12_12 B11_12 37.2(6) . . . . ?
B11_12 B10_12 B12_12 B9_12 -36.4(6) . . . . ?
Cl9_12 B10_12 B12_12 B9_12 -147.1(6) . . . . ?
B8_12 B10_12 B12_12 B9_12 100.4(7) . . . . ?
B4_12 B10_12 B12_12 B9_12 63.0(8) . . . . ?
B2_12 B10_12 B12_12 B9_12 0.8(8) . . . . ?
B11_12 B10_12 B12_12 B8_12 -136.8(6) . . . . ?
Cl9_12 B10_12 B12_12 B8_12 112.5(7) . . . . ?
B4_12 B10_12 B12_12 B8_12 -37.4(6) . . . . ?
B2_12 B10_12 B12_12 B8_12 -99.6(7) . . . . ?
B3_12 B11_12 B12_12 Cl12_12 148.6(6) . . . . ?
B10_12 B11_12 B12_12 Cl12_12 -109.7(8) . . . . ?
B9_12 B11_12 B12_12 Cl12_12 111.1(7) . . . . ?
B2_12 B11_12 B12_12 Cl12_12 -147.9(6) . . . . ?
Cl10_12 B11_12 B12_12 Cl12_12 -0.2(11) . . . . ?
B3_12 B11_12 B12_12 B7_12 -1.7(8) . . . . ?
B10_12 B11_12 B12_12 B7_12 100.1(7) . . . . ?
B9_12 B11_12 B12_12 B7_12 -39.2(6) . . . . ?
B2_12 B11_12 B12_12 B7_12 61.9(8) . . . . ?
Cl10_12 B11_12 B12_12 B7_12 -150.4(6) . . . . ?
B3_12 B11_12 B12_12 B10_12 -101.8(7) . . . . ?
B9_12 B11_12 B12_12 B10_12 -139.3(6) . . . . ?
B2_12 B11_12 B12_12 B10_12 -38.2(6) . . . . ?
Cl10_12 B11_12 B12_12 B10_12 109.5(7) . . . . ?
B3_12 B11_12 B12_12 B9_12 37.5(6) . . . . ?
B10_12 B11_12 B12_12 B9_12 139.3(6) . . . . ?
B2_12 B11_12 B12_12 B9_12 101.1(7) . . . . ?
Cl10_12 B11_12 B12_12 B9_12 -111.3(7) . . . . ?
B3_12 B11_12 B12_12 B8_12 -63.9(8) . . . . ?
B10_12 B11_12 B12_12 B8_12 37.9(6) . . . . ?
B9_12 B11_12 B12_12 B8_12 -101.4(7) . . . . ?
B2_12 B11_12 B12_12 B8_12 -0.3(9) . . . . ?
Cl10_12 B11_12 B12_12 B8_12 147.4(6) . . . . ?
Cl11_12 B9_12 B12_12 Cl12_12 3.9(11) . . . . ?
B11_12 B9_12 B12_12 Cl12_12 -110.2(8) . . . . ?
B5_12 B9_12 B12_12 Cl12_12 150.8(6) . . . . ?
B3_12 B9_12 B12_12 Cl12_12 -146.8(6) . . . . ?
B7_12 B9_12 B12_12 Cl12_12 113.5(8) . . . . ?
Cl11_12 B9_12 B12_12 B7_12 -109.6(7) . . . . ?
B11_12 B9_12 B12_12 B7_12 136.3(6) . . . . ?
B5_12 B9_12 B12_12 B7_12 37.3(6) . . . . ?
B3_12 B9_12 B12_12 B7_12 99.7(7) . . . . ?
Cl11_12 B9_12 B12_12 B10_12 150.4(6) . . . . ?
B11_12 B9_12 B12_12 B10_12 36.3(6) . . . . ?
B5_12 B9_12 B12_12 B10_12 -62.7(8) . . . . ?
B3_12 B9_12 B12_12 B10_12 -0.3(8) . . . . ?
B7_12 B9_12 B12_12 B10_12 -100.0(7) . . . . ?
Cl11_12 B9_12 B12_12 B11_12 114.1(7) . . . . ?
B5_12 B9_12 B12_12 B11_12 -99.0(7) . . . . ?
B3_12 B9_12 B12_12 B11_12 -36.6(6) . . . . ?
B7_12 B9_12 B12_12 B11_12 -136.3(6) . . . . ?
Cl11_12 B9_12 B12_12 B8_12 -146.9(6) . . . . ?
B11_12 B9_12 B12_12 B8_12 99.0(6) . . . . ?
B5_12 B9_12 B12_12 B8_12 0.0(8) . . . . ?
B3_12 B9_12 B12_12 B8_12 62.4(8) . . . . ?
B7_12 B9_12 B12_12 B8_12 -37.3(6) . . . . ?
B6_12 B8_12 B12_12 Cl12_12 -149.5(7) . . . . ?
B4_12 B8_12 B12_12 Cl12_12 146.8(6) . . . . ?
B7_12 B8_12 B12_12 Cl12_12 -112.3(8) . . . . ?
Cl8_12 B8_12 B12_12 Cl12_12 -1.3(11) . . . . ?
B10_12 B8_12 B12_12 Cl12_12 108.8(8) . . . . ?
B6_12 B8_12 B12_12 B7_12 -37.2(6) . . . . ?
B4_12 B8_12 B12_12 B7_12 -100.9(7) . . . . ?
Cl8_12 B8_12 B12_12 B7_12 111.1(7) . . . . ?
B10_12 B8_12 B12_12 B7_12 -138.9(6) . . . . ?
B6_12 B8_12 B12_12 B10_12 101.7(7) . . . . ?
B4_12 B8_12 B12_12 B10_12 38.0(6) . . . . ?
B7_12 B8_12 B12_12 B10_12 138.9(7) . . . . ?
Cl8_12 B8_12 B12_12 B10_12 -110.1(7) . . . . ?
B6_12 B8_12 B12_12 B11_12 63.7(8) . . . . ?
B4_12 B8_12 B12_12 B11_12 0.0(8) . . . . ?
B7_12 B8_12 B12_12 B11_12 100.9(7) . . . . ?
Cl8_12 B8_12 B12_12 B11_12 -148.1(6) . . . . ?
B10_12 B8_12 B12_12 B11_12 -38.0(6) . . . . ?
B6_12 B8_12 B12_12 B9_12 0.7(9) . . . . ?
B4_12 B8_12 B12_12 B9_12 -63.0(8) . . . . ?
B7_12 B8_12 B12_12 B9_12 37.9(6) . . . . ?
Cl8_12 B8_12 B12_12 B9_12 149.0(6) . . . . ?
B10_12 B8_12 B12_12 B9_12 -100.9(7) . . . . ?
B4_13 B1_13 B2_13 B3_13 -38.5(5) . . . . ?
B5_13 B1_13 B2_13 B3_13 -101.9(6) . . . . ?
Cl1_13 B1_13 B2_13 B3_13 111.9(6) . . . . ?
B6_13 B1_13 B2_13 B3_13 -139.2(6) . . . . ?
B3_13 B1_13 B2_13 B6_13 139.2(6) . . . . ?
B4_13 B1_13 B2_13 B6_13 100.7(6) . . . . ?
B5_13 B1_13 B2_13 B6_13 37.3(5) . . . . ?
Cl1_13 B1_13 B2_13 B6_13 -108.8(6) . . . . ?
B3_13 B1_13 B2_13 B12_13 101.8(6) . . . . ?
B4_13 B1_13 B2_13 B12_13 63.3(7) . . . . ?
B5_13 B1_13 B2_13 B12_13 -0.1(8) . . . . ?
Cl1_13 B1_13 B2_13 B12_13 -146.3(5) . . . . ?
B6_13 B1_13 B2_13 B12_13 -37.5(5) . . . . ?
B3_13 B1_13 B2_13 B11_13 37.0(5) . . . . ?
B4_13 B1_13 B2_13 B11_13 -1.5(7) . . . . ?
B5_13 B1_13 B2_13 B11_13 -64.9(7) . . . . ?
Cl1_13 B1_13 B2_13 B11_13 149.0(5) . . . . ?
B6_13 B1_13 B2_13 B11_13 -102.2(6) . . . . ?
B3_13 B1_13 B2_13 Cl6_13 -110.1(7) . . . . ?
B4_13 B1_13 B2_13 Cl6_13 -148.6(5) . . . . ?
B5_13 B1_13 B2_13 Cl6_13 148.0(6) . . . . ?
Cl1_13 B1_13 B2_13 Cl6_13 1.8(9) . . . . ?
B6_13 B1_13 B2_13 Cl6_13 110.7(7) . . . . ?
B6_13 B2_13 B3_13 B1_13 -37.6(5) . . . . ?
B12_13 B2_13 B3_13 B1_13 -101.9(6) . . . . ?
B11_13 B2_13 B3_13 B1_13 -138.9(6) . . . . ?
Cl6_13 B2_13 B3_13 B1_13 110.6(6) . . . . ?
B6_13 B2_13 B3_13 B11_13 101.4(6) . . . . ?
B1_13 B2_13 B3_13 B11_13 138.9(6) . . . . ?
B12_13 B2_13 B3_13 B11_13 37.0(5) . . . . ?
Cl6_13 B2_13 B3_13 B11_13 -110.4(6) . . . . ?
B6_13 B2_13 B3_13 Cl5_13 -146.4(5) . . . . ?
B1_13 B2_13 B3_13 Cl5_13 -108.8(6) . . . . ?
B12_13 B2_13 B3_13 Cl5_13 149.2(5) . . . . ?
B11_13 B2_13 B3_13 Cl5_13 112.2(6) . . . . ?
Cl6_13 B2_13 B3_13 Cl5_13 1.8(9) . . . . ?
B6_13 B2_13 B3_13 B4_13 0.4(7) . . . . ?
B1_13 B2_13 B3_13 B4_13 38.0(5) . . . . ?
B12_13 B2_13 B3_13 B4_13 -63.9(7) . . . . ?
B11_13 B2_13 B3_13 B4_13 -100.9(6) . . . . ?
Cl6_13 B2_13 B3_13 B4_13 148.6(5) . . . . ?
B6_13 B2_13 B3_13 B10_13 63.2(7) . . . . ?
B1_13 B2_13 B3_13 B10_13 100.7(6) . . . . ?
B12_13 B2_13 B3_13 B10_13 -1.2(7) . . . . ?
B11_13 B2_13 B3_13 B10_13 -38.2(5) . . . . ?
Cl6_13 B2_13 B3_13 B10_13 -148.6(5) . . . . ?
B4_13 B1_13 B3_13 B2_13 137.4(6) . . . . ?
B5_13 B1_13 B3_13 B2_13 99.9(6) . . . . ?
Cl1_13 B1_13 B3_13 B2_13 -107.5(7) . . . . ?
B6_13 B1_13 B3_13 B2_13 35.8(5) . . . . ?
B2_13 B1_13 B3_13 B11_13 -37.7(6) . . . . ?
B4_13 B1_13 B3_13 B11_13 99.7(6) . . . . ?
B5_13 B1_13 B3_13 B11_13 62.2(7) . . . . ?
Cl1_13 B1_13 B3_13 B11_13 -145.2(6) . . . . ?
B6_13 B1_13 B3_13 B11_13 -1.9(8) . . . . ?
B2_13 B1_13 B3_13 Cl5_13 111.2(7) . . . . ?
B4_13 B1_13 B3_13 Cl5_13 -111.4(6) . . . . ?
B5_13 B1_13 B3_13 Cl5_13 -148.9(5) . . . . ?
Cl1_13 B1_13 B3_13 Cl5_13 3.7(9) . . . . ?
B6_13 B1_13 B3_13 Cl5_13 147.0(5) . . . . ?
B2_13 B1_13 B3_13 B4_13 -137.4(6) . . . . ?
B5_13 B1_13 B3_13 B4_13 -37.5(5) . . . . ?
Cl1_13 B1_13 B3_13 B4_13 115.1(7) . . . . ?
B6_13 B1_13 B3_13 B4_13 -101.6(6) . . . . ?
B2_13 B1_13 B3_13 B10_13 -101.2(6) . . . . ?
B4_13 B1_13 B3_13 B10_13 36.2(5) . . . . ?
B5_13 B1_13 B3_13 B10_13 -1.3(7) . . . . ?
Cl1_13 B1_13 B3_13 B10_13 151.3(5) . . . . ?
B6_13 B1_13 B3_13 B10_13 -65.4(7) . . . . ?
B3_13 B1_13 B4_13 B8_13 -100.2(6) . . . . ?
B2_13 B1_13 B4_13 B8_13 -62.5(7) . . . . ?
B5_13 B1_13 B4_13 B8_13 38.2(5) . . . . ?
Cl1_13 B1_13 B4_13 B8_13 149.1(6) . . . . ?
B6_13 B1_13 B4_13 B8_13 -0.3(7) . . . . ?
B3_13 B1_13 B4_13 B10_13 -36.7(5) . . . . ?
B2_13 B1_13 B4_13 B10_13 1.0(7) . . . . ?
B5_13 B1_13 B4_13 B10_13 101.7(6) . . . . ?
Cl1_13 B1_13 B4_13 B10_13 -147.4(6) . . . . ?
B6_13 B1_13 B4_13 B10_13 63.2(7) . . . . ?
B3_13 B1_13 B4_13 B5_13 -138.4(6) . . . . ?
B2_13 B1_13 B4_13 B5_13 -100.6(6) . . . . ?
Cl1_13 B1_13 B4_13 B5_13 111.0(7) . . . . ?
B6_13 B1_13 B4_13 B5_13 -38.4(5) . . . . ?
B3_13 B1_13 B4_13 Cl4_13 110.7(6) . . . . ?
B2_13 B1_13 B4_13 Cl4_13 148.5(6) . . . . ?
B5_13 B1_13 B4_13 Cl4_13 -110.9(6) . . . . ?
Cl1_13 B1_13 B4_13 Cl4_13 0.1(10) . . . . ?
B6_13 B1_13 B4_13 Cl4_13 -149.3(5) . . . . ?
B2_13 B1_13 B4_13 B3_13 37.7(5) . . . . ?
B5_13 B1_13 B4_13 B3_13 138.4(6) . . . . ?
Cl1_13 B1_13 B4_13 B3_13 -110.7(7) . . . . ?
B6_13 B1_13 B4_13 B3_13 99.9(6) . . . . ?
B2_13 B3_13 B4_13 B8_13 63.2(7) . . . . ?
B1_13 B3_13 B4_13 B8_13 101.5(6) . . . . ?
B11_13 B3_13 B4_13 B8_13 -1.4(7) . . . . ?
Cl5_13 B3_13 B4_13 B8_13 -150.1(5) . . . . ?
B10_13 B3_13 B4_13 B8_13 -37.7(5) . . . . ?
B2_13 B3_13 B4_13 B1_13 -38.3(5) . . . . ?
B11_13 B3_13 B4_13 B1_13 -103.0(6) . . . . ?
Cl5_13 B3_13 B4_13 B1_13 108.4(6) . . . . ?
B10_13 B3_13 B4_13 B1_13 -139.2(6) . . . . ?
B2_13 B3_13 B4_13 B10_13 100.9(6) . . . . ?
B1_13 B3_13 B4_13 B10_13 139.2(6) . . . . ?
B11_13 B3_13 B4_13 B10_13 36.2(5) . . . . ?
Cl5_13 B3_13 B4_13 B10_13 -112.4(6) . . . . ?
B2_13 B3_13 B4_13 B5_13 -1.1(7) . . . . ?
B1_13 B3_13 B4_13 B5_13 37.2(5) . . . . ?
B11_13 B3_13 B4_13 B5_13 -65.8(7) . . . . ?
Cl5_13 B3_13 B4_13 B5_13 145.6(5) . . . . ?
B10_13 B3_13 B4_13 B5_13 -102.0(6) . . . . ?
B2_13 B3_13 B4_13 Cl4_13 -149.1(5) . . . . ?
B1_13 B3_13 B4_13 Cl4_13 -110.8(6) . . . . ?
B11_13 B3_13 B4_13 Cl4_13 146.3(5) . . . . ?
Cl5_13 B3_13 B4_13 Cl4_13 -2.4(8) . . . . ?
B10_13 B3_13 B4_13 Cl4_13 110.0(6) . . . . ?
B8_13 B4_13 B5_13 Cl3_13 111.6(7) . . . . ?
B1_13 B4_13 B5_13 Cl3_13 -110.4(7) . . . . ?
B10_13 B4_13 B5_13 Cl3_13 149.0(6) . . . . ?
Cl4_13 B4_13 B5_13 Cl3_13 1.0(9) . . . . ?
B3_13 B4_13 B5_13 Cl3_13 -147.1(6) . . . . ?
B8_13 B4_13 B5_13 B1_13 -138.0(6) . . . . ?
B10_13 B4_13 B5_13 B1_13 -100.6(6) . . . . ?
Cl4_13 B4_13 B5_13 B1_13 111.4(6) . . . . ?
B3_13 B4_13 B5_13 B1_13 -36.7(5) . . . . ?
B1_13 B4_13 B5_13 B8_13 138.0(6) . . . . ?
B10_13 B4_13 B5_13 B8_13 37.4(5) . . . . ?
Cl4_13 B4_13 B5_13 B8_13 -110.6(6) . . . . ?
B3_13 B4_13 B5_13 B8_13 101.3(6) . . . . ?
B8_13 B4_13 B5_13 B7_13 -37.3(5) . . . . ?
B1_13 B4_13 B5_13 B7_13 100.7(6) . . . . ?
B10_13 B4_13 B5_13 B7_13 0.2(7) . . . . ?
Cl4_13 B4_13 B5_13 B7_13 -147.9(5) . . . . ?
B3_13 B4_13 B5_13 B7_13 64.0(7) . . . . ?
B8_13 B4_13 B5_13 B6_13 -99.9(6) . . . . ?
B1_13 B4_13 B5_13 B6_13 38.1(5) . . . . ?
B10_13 B4_13 B5_13 B6_13 -62.5(7) . . . . ?
Cl4_13 B4_13 B5_13 B6_13 149.5(5) . . . . ?
B3_13 B4_13 B5_13 B6_13 1.4(7) . . . . ?
B3_13 B1_13 B5_13 Cl3_13 149.6(5) . . . . ?
B2_13 B1_13 B5_13 Cl3_13 -147.5(5) . . . . ?
B4_13 B1_13 B5_13 Cl3_13 111.7(6) . . . . ?
Cl1_13 B1_13 B5_13 Cl3_13 -2.7(9) . . . . ?
B6_13 B1_13 B5_13 Cl3_13 -111.0(6) . . . . ?
B3_13 B1_13 B5_13 B4_13 37.9(5) . . . . ?
B2_13 B1_13 B5_13 B4_13 100.8(6) . . . . ?
Cl1_13 B1_13 B5_13 B4_13 -114.4(7) . . . . ?
B6_13 B1_13 B5_13 B4_13 137.3(6) . . . . ?
B3_13 B1_13 B5_13 B8_13 0.8(7) . . . . ?
B2_13 B1_13 B5_13 B8_13 63.7(7) . . . . ?
B4_13 B1_13 B5_13 B8_13 -37.1(5) . . . . ?
Cl1_13 B1_13 B5_13 B8_13 -151.5(5) . . . . ?
B6_13 B1_13 B5_13 B8_13 100.2(6) . . . . ?
B3_13 B1_13 B5_13 B7_13 -61.9(7) . . . . ?
B2_13 B1_13 B5_13 B7_13 1.0(7) . . . . ?
B4_13 B1_13 B5_13 B7_13 -99.8(6) . . . . ?
Cl1_13 B1_13 B5_13 B7_13 145.7(6) . . . . ?
B6_13 B1_13 B5_13 B7_13 37.5(5) . . . . ?
B3_13 B1_13 B5_13 B6_13 -99.4(6) . . . . ?
B2_13 B1_13 B5_13 B6_13 -36.5(5) . . . . ?
B4_13 B1_13 B5_13 B6_13 -137.3(6) . . . . ?
Cl1_13 B1_13 B5_13 B6_13 108.2(6) . . . . ?
B3_13 B2_13 B6_13 B12_13 -101.8(6) . . . . ?
B1_13 B2_13 B6_13 B12_13 -138.7(6) . . . . ?
B11_13 B2_13 B6_13 B12_13 -37.3(5) . . . . ?
Cl6_13 B2_13 B6_13 B12_13 110.0(6) . . . . ?
B3_13 B2_13 B6_13 Cl2_13 147.3(6) . . . . ?
B1_13 B2_13 B6_13 Cl2_13 110.4(7) . . . . ?
B12_13 B2_13 B6_13 Cl2_13 -110.9(7) . . . . ?
B11_13 B2_13 B6_13 Cl2_13 -148.3(6) . . . . ?
Cl6_13 B2_13 B6_13 Cl2_13 -0.9(9) . . . . ?
B3_13 B2_13 B6_13 B7_13 -63.1(7) . . . . ?
B1_13 B2_13 B6_13 B7_13 -100.0(6) . . . . ?
B12_13 B2_13 B6_13 B7_13 38.7(5) . . . . ?
B11_13 B2_13 B6_13 B7_13 1.3(8) . . . . ?
Cl6_13 B2_13 B6_13 B7_13 148.7(5) . . . . ?
B3_13 B2_13 B6_13 B1_13 37.0(5) . . . . ?
B12_13 B2_13 B6_13 B1_13 138.7(6) . . . . ?
B11_13 B2_13 B6_13 B1_13 101.4(6) . . . . ?
Cl6_13 B2_13 B6_13 B1_13 -111.3(6) . . . . ?
B3_13 B2_13 B6_13 B5_13 0.4(8) . . . . ?
B1_13 B2_13 B6_13 B5_13 -36.5(5) . . . . ?
B12_13 B2_13 B6_13 B5_13 102.2(6) . . . . ?
B11_13 B2_13 B6_13 B5_13 64.8(7) . . . . ?
Cl6_13 B2_13 B6_13 B5_13 -147.8(5) . . . . ?
B3_13 B1_13 B6_13 B2_13 -36.0(6) . . . . ?
B4_13 B1_13 B6_13 B2_13 -100.4(6) . . . . ?
B5_13 B1_13 B6_13 B2_13 -138.5(6) . . . . ?
Cl1_13 B1_13 B6_13 B2_13 108.3(7) . . . . ?
B3_13 B1_13 B6_13 B12_13 1.3(8) . . . . ?
B2_13 B1_13 B6_13 B12_13 37.3(5) . . . . ?
B4_13 B1_13 B6_13 B12_13 -63.1(7) . . . . ?
B5_13 B1_13 B6_13 B12_13 -101.3(6) . . . . ?
Cl1_13 B1_13 B6_13 B12_13 145.6(6) . . . . ?
B3_13 B1_13 B6_13 Cl2_13 -148.3(6) . . . . ?
B2_13 B1_13 B6_13 Cl2_13 -112.3(7) . . . . ?
B4_13 B1_13 B6_13 Cl2_13 147.3(5) . . . . ?
B5_13 B1_13 B6_13 Cl2_13 109.1(6) . . . . ?
Cl1_13 B1_13 B6_13 Cl2_13 -4.0(9) . . . . ?
B3_13 B1_13 B6_13 B7_13 64.8(7) . . . . ?
B2_13 B1_13 B6_13 B7_13 100.8(6) . . . . ?
B4_13 B1_13 B6_13 B7_13 0.4(7) . . . . ?
B5_13 B1_13 B6_13 B7_13 -37.7(5) . . . . ?
Cl1_13 B1_13 B6_13 B7_13 -150.9(6) . . . . ?
B3_13 B1_13 B6_13 B5_13 102.6(6) . . . . ?
B2_13 B1_13 B6_13 B5_13 138.5(6) . . . . ?
B4_13 B1_13 B6_13 B5_13 38.2(5) . . . . ?
Cl1_13 B1_13 B6_13 B5_13 -113.1(7) . . . . ?
Cl3_13 B5_13 B6_13 B2_13 147.6(6) . . . . ?
B4_13 B5_13 B6_13 B2_13 -1.1(7) . . . . ?
B1_13 B5_13 B6_13 B2_13 36.8(5) . . . . ?
B8_13 B5_13 B6_13 B2_13 -63.6(7) . . . . ?
B7_13 B5_13 B6_13 B2_13 -100.9(6) . . . . ?
Cl3_13 B5_13 B6_13 B12_13 -148.4(6) . . . . ?
B4_13 B5_13 B6_13 B12_13 62.9(7) . . . . ?
B1_13 B5_13 B6_13 B12_13 100.7(6) . . . . ?
B8_13 B5_13 B6_13 B12_13 0.4(7) . . . . ?
B7_13 B5_13 B6_13 B12_13 -37.0(5) . . . . ?
Cl3_13 B5_13 B6_13 Cl2_13 -0.2(9) . . . . ?
B4_13 B5_13 B6_13 Cl2_13 -149.0(5) . . . . ?
B1_13 B5_13 B6_13 Cl2_13 -111.1(6) . . . . ?
B8_13 B5_13 B6_13 Cl2_13 148.5(5) . . . . ?
B7_13 B5_13 B6_13 Cl2_13 111.2(6) . . . . ?
Cl3_13 B5_13 B6_13 B7_13 -111.4(7) . . . . ?
B4_13 B5_13 B6_13 B7_13 99.8(6) . . . . ?
B1_13 B5_13 B6_13 B7_13 137.7(6) . . . . ?
B8_13 B5_13 B6_13 B7_13 37.3(5) . . . . ?
Cl3_13 B5_13 B6_13 B1_13 110.9(7) . . . . ?
B4_13 B5_13 B6_13 B1_13 -37.9(5) . . . . ?
B8_13 B5_13 B6_13 B1_13 -100.4(6) . . . . ?
B7_13 B5_13 B6_13 B1_13 -137.7(6) . . . . ?
B2_13 B6_13 B7_13 Cl12_13 -149.9(6) . . . . ?
B12_13 B6_13 B7_13 Cl12_13 -111.1(7) . . . . ?
Cl2_13 B6_13 B7_13 Cl12_13 0.2(9) . . . . ?
B1_13 B6_13 B7_13 Cl12_13 147.2(6) . . . . ?
B5_13 B6_13 B7_13 Cl12_13 109.9(7) . . . . ?
B2_13 B6_13 B7_13 B9_13 -1.0(8) . . . . ?
B12_13 B6_13 B7_13 B9_13 37.9(5) . . . . ?
Cl2_13 B6_13 B7_13 B9_13 149.2(5) . . . . ?
B1_13 B6_13 B7_13 B9_13 -63.8(7) . . . . ?
B5_13 B6_13 B7_13 B9_13 -101.1(6) . . . . ?
B2_13 B6_13 B7_13 B12_13 -38.8(5) . . . . ?
Cl2_13 B6_13 B7_13 B12_13 111.3(6) . . . . ?
B1_13 B6_13 B7_13 B12_13 -101.7(6) . . . . ?
B5_13 B6_13 B7_13 B12_13 -139.0(6) . . . . ?
B2_13 B6_13 B7_13 B8_13 62.5(7) . . . . ?
B12_13 B6_13 B7_13 B8_13 101.3(6) . . . . ?
Cl2_13 B6_13 B7_13 B8_13 -147.4(5) . . . . ?
B1_13 B6_13 B7_13 B8_13 -0.4(7) . . . . ?
B5_13 B6_13 B7_13 B8_13 -37.7(5) . . . . ?
B2_13 B6_13 B7_13 B5_13 100.2(6) . . . . ?
B12_13 B6_13 B7_13 B5_13 139.0(6) . . . . ?
Cl2_13 B6_13 B7_13 B5_13 -109.7(6) . . . . ?
B1_13 B6_13 B7_13 B5_13 37.3(5) . . . . ?
Cl3_13 B5_13 B7_13 Cl12_13 -1.3(9) . . . . ?
B4_13 B5_13 B7_13 Cl12_13 147.7(5) . . . . ?
B1_13 B5_13 B7_13 Cl12_13 -149.5(5) . . . . ?
B8_13 B5_13 B7_13 Cl12_13 110.5(7) . . . . ?
B6_13 B5_13 B7_13 Cl12_13 -111.7(6) . . . . ?
Cl3_13 B5_13 B7_13 B9_13 -148.7(6) . . . . ?
B4_13 B5_13 B7_13 B9_13 0.2(7) . . . . ?
B1_13 B5_13 B7_13 B9_13 63.1(7) . . . . ?
B8_13 B5_13 B7_13 B9_13 -36.9(5) . . . . ?
B6_13 B5_13 B7_13 B9_13 100.8(6) . . . . ?
Cl3_13 B5_13 B7_13 B12_13 146.8(5) . . . . ?
B4_13 B5_13 B7_13 B12_13 -64.3(7) . . . . ?
B1_13 B5_13 B7_13 B12_13 -1.5(7) . . . . ?
B8_13 B5_13 B7_13 B12_13 -101.5(6) . . . . ?
B6_13 B5_13 B7_13 B12_13 36.3(5) . . . . ?
Cl3_13 B5_13 B7_13 B8_13 -111.8(7) . . . . ?
B4_13 B5_13 B7_13 B8_13 37.2(5) . . . . ?
B1_13 B5_13 B7_13 B8_13 100.0(6) . . . . ?
B6_13 B5_13 B7_13 B8_13 137.8(6) . . . . ?
Cl3_13 B5_13 B7_13 B6_13 110.5(6) . . . . ?
B4_13 B5_13 B7_13 B6_13 -100.6(6) . . . . ?
B1_13 B5_13 B7_13 B6_13 -37.8(5) . . . . ?
B8_13 B5_13 B7_13 B6_13 -137.8(6) . . . . ?
B1_13 B4_13 B8_13 B10_13 100.5(6) . . . . ?
B5_13 B4_13 B8_13 B10_13 138.3(6) . . . . ?
Cl4_13 B4_13 B8_13 B10_13 -110.1(6) . . . . ?
B3_13 B4_13 B8_13 B10_13 37.9(5) . . . . ?
B1_13 B4_13 B8_13 Cl11_13 -149.7(6) . . . . ?
B10_13 B4_13 B8_13 Cl11_13 109.8(7) . . . . ?
B5_13 B4_13 B8_13 Cl11_13 -111.9(6) . . . . ?
Cl4_13 B4_13 B8_13 Cl11_13 -0.3(9) . . . . ?
B3_13 B4_13 B8_13 Cl11_13 147.7(5) . . . . ?
B1_13 B4_13 B8_13 B9_13 63.1(7) . . . . ?
B10_13 B4_13 B8_13 B9_13 -37.4(5) . . . . ?
B5_13 B4_13 B8_13 B9_13 100.9(6) . . . . ?
Cl4_13 B4_13 B8_13 B9_13 -147.5(5) . . . . ?
B3_13 B4_13 B8_13 B9_13 0.5(7) . . . . ?
B1_13 B4_13 B8_13 B7_13 0.0(7) . . . . ?
B10_13 B4_13 B8_13 B7_13 -100.5(6) . . . . ?
B5_13 B4_13 B8_13 B7_13 37.9(5) . . . . ?
Cl4_13 B4_13 B8_13 B7_13 149.4(5) . . . . ?
B3_13 B4_13 B8_13 B7_13 -62.6(7) . . . . ?
B1_13 B4_13 B8_13 B5_13 -37.9(5) . . . . ?
B10_13 B4_13 B8_13 B5_13 -138.3(6) . . . . ?
Cl4_13 B4_13 B8_13 B5_13 111.5(6) . . . . ?
B3_13 B4_13 B8_13 B5_13 -100.4(6) . . . . ?
Cl12_13 B7_13 B8_13 B4_13 -147.7(6) . . . . ?
B9_13 B7_13 B8_13 B4_13 101.2(6) . . . . ?
B12_13 B7_13 B8_13 B4_13 62.9(7) . . . . ?
B6_13 B7_13 B8_13 B4_13 0.3(7) . . . . ?
B5_13 B7_13 B8_13 B4_13 -37.5(5) . . . . ?
Cl12_13 B7_13 B8_13 B10_13 148.8(6) . . . . ?
B9_13 B7_13 B8_13 B10_13 37.8(5) . . . . ?
B12_13 B7_13 B8_13 B10_13 -0.6(7) . . . . ?
B6_13 B7_13 B8_13 B10_13 -63.2(7) . . . . ?
B5_13 B7_13 B8_13 B10_13 -101.0(6) . . . . ?
Cl12_13 B7_13 B8_13 Cl11_13 2.2(9) . . . . ?
B9_13 B7_13 B8_13 Cl11_13 -108.9(6) . . . . ?
B12_13 B7_13 B8_13 Cl11_13 -147.2(5) . . . . ?
B6_13 B7_13 B8_13 Cl11_13 150.2(5) . . . . ?
B5_13 B7_13 B8_13 Cl11_13 112.4(6) . . . . ?
Cl12_13 B7_13 B8_13 B9_13 111.1(7) . . . . ?
B12_13 B7_13 B8_13 B9_13 -38.4(5) . . . . ?
B6_13 B7_13 B8_13 B9_13 -101.0(6) . . . . ?
B5_13 B7_13 B8_13 B9_13 -138.8(6) . . . . ?
Cl12_13 B7_13 B8_13 B5_13 -110.2(7) . . . . ?
B9_13 B7_13 B8_13 B5_13 138.8(6) . . . . ?
B12_13 B7_13 B8_13 B5_13 100.4(6) . . . . ?
B6_13 B7_13 B8_13 B5_13 37.8(5) . . . . ?
Cl3_13 B5_13 B8_13 B4_13 -111.1(7) . . . . ?
B1_13 B5_13 B8_13 B4_13 37.2(5) . . . . ?
B7_13 B5_13 B8_13 B4_13 137.8(6) . . . . ?
B6_13 B5_13 B8_13 B4_13 100.5(6) . . . . ?
Cl3_13 B5_13 B8_13 B10_13 -148.4(5) . . . . ?
B4_13 B5_13 B8_13 B10_13 -37.3(5) . . . . ?
B1_13 B5_13 B8_13 B10_13 -0.1(7) . . . . ?
B7_13 B5_13 B8_13 B10_13 100.5(6) . . . . ?
B6_13 B5_13 B8_13 B10_13 63.2(7) . . . . ?
Cl3_13 B5_13 B8_13 Cl11_13 0.1(9) . . . . ?
B4_13 B5_13 B8_13 Cl11_13 111.2(7) . . . . ?
B1_13 B5_13 B8_13 Cl11_13 148.4(6) . . . . ?
B7_13 B5_13 B8_13 Cl11_13 -111.0(7) . . . . ?
B6_13 B5_13 B8_13 Cl11_13 -148.3(5) . . . . ?
Cl3_13 B5_13 B8_13 B9_13 147.8(5) . . . . ?
B4_13 B5_13 B8_13 B9_13 -101.0(6) . . . . ?
B1_13 B5_13 B8_13 B9_13 -63.8(7) . . . . ?
B7_13 B5_13 B8_13 B9_13 36.8(5) . . . . ?
B6_13 B5_13 B8_13 B9_13 -0.5(7) . . . . ?
Cl3_13 B5_13 B8_13 B7_13 111.0(7) . . . . ?
B4_13 B5_13 B8_13 B7_13 -137.8(6) . . . . ?
B1_13 B5_13 B8_13 B7_13 -100.6(6) . . . . ?
B6_13 B5_13 B8_13 B7_13 -37.3(5) . . . . ?
Cl12_13 B7_13 B9_13 Cl10_13 0.8(9) . . . . ?
B12_13 B7_13 B9_13 Cl10_13 -111.3(6) . . . . ?
B8_13 B7_13 B9_13 Cl10_13 111.0(6) . . . . ?
B6_13 B7_13 B9_13 Cl10_13 -148.3(5) . . . . ?
B5_13 B7_13 B9_13 Cl10_13 148.0(5) . . . . ?
Cl12_13 B7_13 B9_13 B8_13 -110.2(7) . . . . ?
B12_13 B7_13 B9_13 B8_13 137.7(6) . . . . ?
B6_13 B7_13 B9_13 B8_13 100.6(6) . . . . ?
B5_13 B7_13 B9_13 B8_13 36.9(5) . . . . ?
Cl12_13 B7_13 B9_13 B10_13 -147.7(6) . . . . ?
B12_13 B7_13 B9_13 B10_13 100.3(6) . . . . ?
B8_13 B7_13 B9_13 B10_13 -37.4(5) . . . . ?
B6_13 B7_13 B9_13 B10_13 63.2(7) . . . . ?
B5_13 B7_13 B9_13 B10_13 -0.5(7) . . . . ?
Cl12_13 B7_13 B9_13 B11_13 149.4(6) . . . . ?
B12_13 B7_13 B9_13 B11_13 37.3(5) . . . . ?
B8_13 B7_13 B9_13 B11_13 -100.4(6) . . . . ?
B6_13 B7_13 B9_13 B11_13 0.2(7) . . . . ?
B5_13 B7_13 B9_13 B11_13 -63.5(7) . . . . ?
Cl12_13 B7_13 B9_13 B12_13 112.1(7) . . . . ?
B8_13 B7_13 B9_13 B12_13 -137.7(6) . . . . ?
B6_13 B7_13 B9_13 B12_13 -37.1(5) . . . . ?
B5_13 B7_13 B9_13 B12_13 -100.8(6) . . . . ?
B4_13 B8_13 B9_13 B7_13 -100.5(6) . . . . ?
B10_13 B8_13 B9_13 B7_13 -137.8(6) . . . . ?
Cl11_13 B8_13 B9_13 B7_13 111.6(7) . . . . ?
B5_13 B8_13 B9_13 B7_13 -37.2(5) . . . . ?
B4_13 B8_13 B9_13 Cl10_13 148.1(5) . . . . ?
B10_13 B8_13 B9_13 Cl10_13 110.8(6) . . . . ?
Cl11_13 B8_13 B9_13 Cl10_13 0.1(9) . . . . ?
B7_13 B8_13 B9_13 Cl10_13 -111.4(7) . . . . ?
B5_13 B8_13 B9_13 Cl10_13 -148.6(5) . . . . ?
B4_13 B8_13 B9_13 B10_13 37.3(5) . . . . ?
Cl11_13 B8_13 B9_13 B10_13 -110.7(6) . . . . ?
B7_13 B8_13 B9_13 B10_13 137.8(6) . . . . ?
B5_13 B8_13 B9_13 B10_13 100.6(6) . . . . ?
B4_13 B8_13 B9_13 B11_13 0.6(7) . . . . ?
B10_13 B8_13 B9_13 B11_13 -36.7(5) . . . . ?
Cl11_13 B8_13 B9_13 B11_13 -147.4(5) . . . . ?
B7_13 B8_13 B9_13 B11_13 101.0(6) . . . . ?
B5_13 B8_13 B9_13 B11_13 63.9(7) . . . . ?
B4_13 B8_13 B9_13 B12_13 -62.8(7) . . . . ?
B10_13 B8_13 B9_13 B12_13 -100.1(6) . . . . ?
Cl11_13 B8_13 B9_13 B12_13 149.2(5) . . . . ?
B7_13 B8_13 B9_13 B12_13 37.7(5) . . . . ?
B5_13 B8_13 B9_13 B12_13 0.5(7) . . . . ?
Cl11_13 B8_13 B10_13 B4_13 -112.0(6) . . . . ?
B9_13 B8_13 B10_13 B4_13 138.4(6) . . . . ?
B7_13 B8_13 B10_13 B4_13 101.0(6) . . . . ?
B5_13 B8_13 B10_13 B4_13 37.1(5) . . . . ?
B4_13 B8_13 B10_13 B11_13 -101.1(6) . . . . ?
Cl11_13 B8_13 B10_13 B11_13 146.9(5) . . . . ?
B9_13 B8_13 B10_13 B11_13 37.4(5) . . . . ?
B7_13 B8_13 B10_13 B11_13 -0.1(7) . . . . ?
B5_13 B8_13 B10_13 B11_13 -63.9(7) . . . . ?
B4_13 B8_13 B10_13 B9_13 -138.4(6) . . . . ?
Cl11_13 B8_13 B10_13 B9_13 109.5(6) . . . . ?
B7_13 B8_13 B10_13 B9_13 -37.5(5) . . . . ?
B5_13 B8_13 B10_13 B9_13 -101.3(6) . . . . ?
B4_13 B8_13 B10_13 B3_13 -37.9(5) . . . . ?
Cl11_13 B8_13 B10_13 B3_13 -149.9(5) . . . . ?
B9_13 B8_13 B10_13 B3_13 100.6(6) . . . . ?
B7_13 B8_13 B10_13 B3_13 63.1(7) . . . . ?
B5_13 B8_13 B10_13 B3_13 -0.7(7) . . . . ?
B4_13 B8_13 B10_13 Cl9_13 111.8(6) . . . . ?
Cl11_13 B8_13 B10_13 Cl9_13 -0.3(9) . . . . ?
B9_13 B8_13 B10_13 Cl9_13 -109.8(6) . . . . ?
B7_13 B8_13 B10_13 Cl9_13 -147.3(5) . . . . ?
B5_13 B8_13 B10_13 Cl9_13 148.9(5) . . . . ?
B1_13 B4_13 B10_13 B8_13 -101.7(6) . . . . ?
B5_13 B4_13 B10_13 B8_13 -37.8(5) . . . . ?
Cl4_13 B4_13 B10_13 B8_13 110.5(6) . . . . ?
B3_13 B4_13 B10_13 B8_13 -137.8(6) . . . . ?
B8_13 B4_13 B10_13 B11_13 101.4(6) . . . . ?
B1_13 B4_13 B10_13 B11_13 -0.2(7) . . . . ?
B5_13 B4_13 B10_13 B11_13 63.6(7) . . . . ?
Cl4_13 B4_13 B10_13 B11_13 -148.1(5) . . . . ?
B3_13 B4_13 B10_13 B11_13 -36.4(5) . . . . ?
B8_13 B4_13 B10_13 B9_13 37.4(5) . . . . ?
B1_13 B4_13 B10_13 B9_13 -64.3(7) . . . . ?
B5_13 B4_13 B10_13 B9_13 -0.5(7) . . . . ?
Cl4_13 B4_13 B10_13 B9_13 147.8(5) . . . . ?
B3_13 B4_13 B10_13 B9_13 -100.4(6) . . . . ?
B8_13 B4_13 B10_13 B3_13 137.8(6) . . . . ?
B1_13 B4_13 B10_13 B3_13 36.1(5) . . . . ?
B5_13 B4_13 B10_13 B3_13 99.9(6) . . . . ?
Cl4_13 B4_13 B10_13 B3_13 -111.7(6) . . . . ?
B8_13 B4_13 B10_13 Cl9_13 -109.2(6) . . . . ?
B1_13 B4_13 B10_13 Cl9_13 149.2(5) . . . . ?
B5_13 B4_13 B10_13 Cl9_13 -147.0(6) . . . . ?
Cl4_13 B4_13 B10_13 Cl9_13 1.3(9) . . . . ?
B3_13 B4_13 B10_13 Cl9_13 113.0(6) . . . . ?
B7_13 B9_13 B10_13 B8_13 37.8(5) . . . . ?
Cl10_13 B9_13 B10_13 B8_13 -110.7(6) . . . . ?
B11_13 B9_13 B10_13 B8_13 138.6(6) . . . . ?
B12_13 B9_13 B10_13 B8_13 100.8(6) . . . . ?
B7_13 B9_13 B10_13 B4_13 0.6(7) . . . . ?
Cl10_13 B9_13 B10_13 B4_13 -147.9(6) . . . . ?
B8_13 B9_13 B10_13 B4_13 -37.2(5) . . . . ?
B11_13 B9_13 B10_13 B4_13 101.4(6) . . . . ?
B12_13 B9_13 B10_13 B4_13 63.6(7) . . . . ?
B7_13 B9_13 B10_13 B11_13 -100.8(6) . . . . ?
Cl10_13 B9_13 B10_13 B11_13 110.7(6) . . . . ?
B8_13 B9_13 B10_13 B11_13 -138.6(6) . . . . ?
B12_13 B9_13 B10_13 B11_13 -37.8(5) . . . . ?
B7_13 B9_13 B10_13 B3_13 -63.2(7) . . . . ?
Cl10_13 B9_13 B10_13 B3_13 148.3(5) . . . . ?
B8_13 B9_13 B10_13 B3_13 -101.0(6) . . . . ?
B11_13 B9_13 B10_13 B3_13 37.6(5) . . . . ?
B12_13 B9_13 B10_13 B3_13 -0.2(7) . . . . ?
B7_13 B9_13 B10_13 Cl9_13 147.8(6) . . . . ?
Cl10_13 B9_13 B10_13 Cl9_13 -0.7(9) . . . . ?
B8_13 B9_13 B10_13 Cl9_13 110.0(6) . . . . ?
B11_13 B9_13 B10_13 Cl9_13 -111.4(6) . . . . ?
B12_13 B9_13 B10_13 Cl9_13 -149.2(5) . . . . ?
B2_13 B3_13 B10_13 B8_13 -62.8(7) . . . . ?
B1_13 B3_13 B10_13 B8_13 1.3(7) . . . . ?
B11_13 B3_13 B10_13 B8_13 -101.7(6) . . . . ?
Cl5_13 B3_13 B10_13 B8_13 147.5(5) . . . . ?
B4_13 B3_13 B10_13 B8_13 37.7(5) . . . . ?
B2_13 B3_13 B10_13 B4_13 -100.5(6) . . . . ?
B1_13 B3_13 B10_13 B4_13 -36.4(5) . . . . ?
B11_13 B3_13 B10_13 B4_13 -139.4(6) . . . . ?
Cl5_13 B3_13 B10_13 B4_13 109.8(7) . . . . ?
B2_13 B3_13 B10_13 B11_13 38.8(5) . . . . ?
B1_13 B3_13 B10_13 B11_13 102.9(6) . . . . ?
Cl5_13 B3_13 B10_13 B11_13 -110.9(6) . . . . ?
B4_13 B3_13 B10_13 B11_13 139.4(6) . . . . ?
B2_13 B3_13 B10_13 B9_13 0.8(7) . . . . ?
B1_13 B3_13 B10_13 B9_13 64.9(7) . . . . ?
B11_13 B3_13 B10_13 B9_13 -38.0(5) . . . . ?
Cl5_13 B3_13 B10_13 B9_13 -148.9(6) . . . . ?
B4_13 B3_13 B10_13 B9_13 101.4(6) . . . . ?
B2_13 B3_13 B10_13 Cl9_13 148.6(6) . . . . ?
B1_13 B3_13 B10_13 Cl9_13 -147.3(6) . . . . ?
B11_13 B3_13 B10_13 Cl9_13 109.8(7) . . . . ?
Cl5_13 B3_13 B10_13 Cl9_13 -1.1(9) . . . . ?
B4_13 B3_13 B10_13 Cl9_13 -110.8(6) . . . . ?
B2_13 B3_13 B11_13 Cl7_13 111.3(7) . . . . ?
B1_13 B3_13 B11_13 Cl7_13 148.8(6) . . . . ?
Cl5_13 B3_13 B11_13 Cl7_13 0.8(9) . . . . ?
B4_13 B3_13 B11_13 Cl7_13 -147.6(5) . . . . ?
B10_13 B3_13 B11_13 Cl7_13 -111.5(6) . . . . ?
B2_13 B3_13 B11_13 B10_13 -137.1(6) . . . . ?
B1_13 B3_13 B11_13 B10_13 -99.7(6) . . . . ?
Cl5_13 B3_13 B11_13 B10_13 112.4(6) . . . . ?
B4_13 B3_13 B11_13 B10_13 -36.0(5) . . . . ?
B1_13 B3_13 B11_13 B2_13 37.5(6) . . . . ?
Cl5_13 B3_13 B11_13 B2_13 -110.5(7) . . . . ?
B4_13 B3_13 B11_13 B2_13 101.1(6) . . . . ?
B10_13 B3_13 B11_13 B2_13 137.1(6) . . . . ?
B2_13 B3_13 B11_13 B9_13 -99.3(6) . . . . ?
B1_13 B3_13 B11_13 B9_13 -61.8(7) . . . . ?
Cl5_13 B3_13 B11_13 B9_13 150.2(5) . . . . ?
B4_13 B3_13 B11_13 B9_13 1.8(7) . . . . ?
B10_13 B3_13 B11_13 B9_13 37.9(5) . . . . ?
B2_13 B3_13 B11_13 B12_13 -35.6(5) . . . . ?
B1_13 B3_13 B11_13 B12_13 1.8(8) . . . . ?
Cl5_13 B3_13 B11_13 B12_13 -146.1(5) . . . . ?
B4_13 B3_13 B11_13 B12_13 65.5(7) . . . . ?
B10_13 B3_13 B11_13 B12_13 101.5(6) . . . . ?
B8_13 B10_13 B11_13 Cl7_13 -147.4(5) . . . . ?
B4_13 B10_13 B11_13 Cl7_13 148.9(5) . . . . ?
B9_13 B10_13 B11_13 Cl7_13 -110.1(6) . . . . ?
B3_13 B10_13 B11_13 Cl7_13 112.3(6) . . . . ?
Cl9_13 B10_13 B11_13 Cl7_13 -0.7(9) . . . . ?
B8_13 B10_13 B11_13 B3_13 100.3(6) . . . . ?
B4_13 B10_13 B11_13 B3_13 36.6(5) . . . . ?
B9_13 B10_13 B11_13 B3_13 137.6(6) . . . . ?
Cl9_13 B10_13 B11_13 B3_13 -112.9(6) . . . . ?
B8_13 B10_13 B11_13 B2_13 63.0(7) . . . . ?
B4_13 B10_13 B11_13 B2_13 -0.6(7) . . . . ?
B9_13 B10_13 B11_13 B2_13 100.3(6) . . . . ?
B3_13 B10_13 B11_13 B2_13 -37.3(5) . . . . ?
Cl9_13 B10_13 B11_13 B2_13 -150.2(5) . . . . ?
B8_13 B10_13 B11_13 B9_13 -37.3(5) . . . . ?
B4_13 B10_13 B11_13 B9_13 -101.0(6) . . . . ?
B3_13 B10_13 B11_13 B9_13 -137.6(6) . . . . ?
Cl9_13 B10_13 B11_13 B9_13 109.4(6) . . . . ?
B8_13 B10_13 B11_13 B12_13 0.8(7) . . . . ?
B4_13 B10_13 B11_13 B12_13 -62.9(7) . . . . ?
B9_13 B10_13 B11_13 B12_13 38.1(5) . . . . ?
B3_13 B10_13 B11_13 B12_13 -99.5(6) . . . . ?
Cl9_13 B10_13 B11_13 B12_13 147.5(5) . . . . ?
B3_13 B2_13 B11_13 Cl7_13 -111.1(6) . . . . ?
B6_13 B2_13 B11_13 Cl7_13 146.5(5) . . . . ?
B1_13 B2_13 B11_13 Cl7_13 -148.0(6) . . . . ?
B12_13 B2_13 B11_13 Cl7_13 109.4(6) . . . . ?
Cl6_13 B2_13 B11_13 Cl7_13 -0.8(9) . . . . ?
B6_13 B2_13 B11_13 B3_13 -102.4(6) . . . . ?
B1_13 B2_13 B11_13 B3_13 -36.9(5) . . . . ?
B12_13 B2_13 B11_13 B3_13 -139.5(6) . . . . ?
Cl6_13 B2_13 B11_13 B3_13 110.3(7) . . . . ?
B3_13 B2_13 B11_13 B10_13 38.2(5) . . . . ?
B6_13 B2_13 B11_13 B10_13 -64.1(7) . . . . ?
B1_13 B2_13 B11_13 B10_13 1.3(7) . . . . ?
B12_13 B2_13 B11_13 B10_13 -101.2(6) . . . . ?
Cl6_13 B2_13 B11_13 B10_13 148.6(6) . . . . ?
B3_13 B2_13 B11_13 B9_13 101.2(6) . . . . ?
B6_13 B2_13 B11_13 B9_13 -1.2(7) . . . . ?
B1_13 B2_13 B11_13 B9_13 64.2(7) . . . . ?
B12_13 B2_13 B11_13 B9_13 -38.3(5) . . . . ?
Cl6_13 B2_13 B11_13 B9_13 -148.5(5) . . . . ?
B3_13 B2_13 B11_13 B12_13 139.5(6) . . . . ?
B6_13 B2_13 B11_13 B12_13 37.1(5) . . . . ?
B1_13 B2_13 B11_13 B12_13 102.5(6) . . . . ?
Cl6_13 B2_13 B11_13 B12_13 -110.2(7) . . . . ?
B7_13 B9_13 B11_13 Cl7_13 -147.8(5) . . . . ?
Cl10_13 B9_13 B11_13 Cl7_13 0.9(9) . . . . ?
B8_13 B9_13 B11_13 Cl7_13 148.4(5) . . . . ?
B10_13 B9_13 B11_13 Cl7_13 111.8(6) . . . . ?
B12_13 B9_13 B11_13 Cl7_13 -110.7(6) . . . . ?
B7_13 B9_13 B11_13 B3_13 62.3(7) . . . . ?
Cl10_13 B9_13 B11_13 B3_13 -149.1(5) . . . . ?
B8_13 B9_13 B11_13 B3_13 -1.5(7) . . . . ?
B10_13 B9_13 B11_13 B3_13 -38.2(5) . . . . ?
B12_13 B9_13 B11_13 B3_13 99.4(6) . . . . ?
B7_13 B9_13 B11_13 B10_13 100.4(6) . . . . ?
Cl10_13 B9_13 B11_13 B10_13 -110.9(6) . . . . ?
B8_13 B9_13 B11_13 B10_13 36.7(5) . . . . ?
B12_13 B9_13 B11_13 B10_13 137.6(6) . . . . ?
B7_13 B9_13 B11_13 B2_13 0.6(7) . . . . ?
Cl10_13 B9_13 B11_13 B2_13 149.3(5) . . . . ?
B8_13 B9_13 B11_13 B2_13 -63.2(7) . . . . ?
B10_13 B9_13 B11_13 B2_13 -99.8(6) . . . . ?
B12_13 B9_13 B11_13 B2_13 37.7(5) . . . . ?
B7_13 B9_13 B11_13 B12_13 -37.1(5) . . . . ?
Cl10_13 B9_13 B11_13 B12_13 111.5(6) . . . . ?
B8_13 B9_13 B11_13 B12_13 -100.9(6) . . . . ?
B10_13 B9_13 B11_13 B12_13 -137.6(6) . . . . ?
B2_13 B6_13 B12_13 Cl8_13 -111.1(7) . . . . ?
Cl2_13 B6_13 B12_13 Cl8_13 1.5(9) . . . . ?
B7_13 B6_13 B12_13 Cl8_13 112.2(6) . . . . ?
B1_13 B6_13 B12_13 Cl8_13 -148.0(6) . . . . ?
B5_13 B6_13 B12_13 Cl8_13 149.2(5) . . . . ?
Cl2_13 B6_13 B12_13 B2_13 112.7(7) . . . . ?
B7_13 B6_13 B12_13 B2_13 -136.7(6) . . . . ?
B1_13 B6_13 B12_13 B2_13 -36.9(5) . . . . ?
B5_13 B6_13 B12_13 B2_13 -99.7(6) . . . . ?
B2_13 B6_13 B12_13 B7_13 136.7(6) . . . . ?
Cl2_13 B6_13 B12_13 B7_13 -110.7(7) . . . . ?
B1_13 B6_13 B12_13 B7_13 99.8(6) . . . . ?
B5_13 B6_13 B12_13 B7_13 37.0(5) . . . . ?
B2_13 B6_13 B12_13 B11_13 36.7(5) . . . . ?
Cl2_13 B6_13 B12_13 B11_13 149.4(5) . . . . ?
B7_13 B6_13 B12_13 B11_13 -99.9(6) . . . . ?
B1_13 B6_13 B12_13 B11_13 -0.2(7) . . . . ?
B5_13 B6_13 B12_13 B11_13 -63.0(7) . . . . ?
B2_13 B6_13 B12_13 B9_13 99.6(6) . . . . ?
Cl2_13 B6_13 B12_13 B9_13 -147.7(5) . . . . ?
B7_13 B6_13 B12_13 B9_13 -37.1(5) . . . . ?
B1_13 B6_13 B12_13 B9_13 62.7(7) . . . . ?
B5_13 B6_13 B12_13 B9_13 -0.1(7) . . . . ?
B3_13 B2_13 B12_13 Cl8_13 -146.5(6) . . . . ?
B6_13 B2_13 B12_13 Cl8_13 111.3(7) . . . . ?
B1_13 B2_13 B12_13 Cl8_13 149.3(5) . . . . ?
B11_13 B2_13 B12_13 Cl8_13 -109.7(7) . . . . ?
Cl6_13 B2_13 B12_13 Cl8_13 1.0(9) . . . . ?
B3_13 B2_13 B12_13 B6_13 102.2(6) . . . . ?
B1_13 B2_13 B12_13 B6_13 38.0(5) . . . . ?
B11_13 B2_13 B12_13 B6_13 139.0(6) . . . . ?
Cl6_13 B2_13 B12_13 B6_13 -110.3(7) . . . . ?
B3_13 B2_13 B12_13 B7_13 63.4(7) . . . . ?
B6_13 B2_13 B12_13 B7_13 -38.8(5) . . . . ?
B1_13 B2_13 B12_13 B7_13 -0.8(8) . . . . ?
B11_13 B2_13 B12_13 B7_13 100.2(6) . . . . ?
Cl6_13 B2_13 B12_13 B7_13 -149.1(5) . . . . ?
B3_13 B2_13 B12_13 B11_13 -36.8(5) . . . . ?
B6_13 B2_13 B12_13 B11_13 -139.0(6) . . . . ?
B1_13 B2_13 B12_13 B11_13 -101.0(6) . . . . ?
Cl6_13 B2_13 B12_13 B11_13 110.7(6) . . . . ?
B3_13 B2_13 B12_13 B9_13 1.1(8) . . . . ?
B6_13 B2_13 B12_13 B9_13 -101.1(6) . . . . ?
B1_13 B2_13 B12_13 B9_13 -63.1(7) . . . . ?
B11_13 B2_13 B12_13 B9_13 37.9(5) . . . . ?
Cl6_13 B2_13 B12_13 B9_13 148.6(5) . . . . ?
Cl12_13 B7_13 B12_13 Cl8_13 -1.1(9) . . . . ?
B9_13 B7_13 B12_13 Cl8_13 110.0(7) . . . . ?
B8_13 B7_13 B12_13 Cl8_13 147.9(5) . . . . ?
B6_13 B7_13 B12_13 Cl8_13 -111.9(7) . . . . ?
B5_13 B7_13 B12_13 Cl8_13 -148.6(5) . . . . ?
Cl12_13 B7_13 B12_13 B6_13 110.8(7) . . . . ?
B9_13 B7_13 B12_13 B6_13 -138.1(6) . . . . ?
B8_13 B7_13 B12_13 B6_13 -100.2(6) . . . . ?
B5_13 B7_13 B12_13 B6_13 -36.8(5) . . . . ?
Cl12_13 B7_13 B12_13 B2_13 148.9(6) . . . . ?
B9_13 B7_13 B12_13 B2_13 -100.0(6) . . . . ?
B8_13 B7_13 B12_13 B2_13 -62.1(7) . . . . ?
B6_13 B7_13 B12_13 B2_13 38.1(5) . . . . ?
B5_13 B7_13 B12_13 B2_13 1.4(7) . . . . ?
Cl12_13 B7_13 B12_13 B11_13 -147.9(5) . . . . ?
B9_13 B7_13 B12_13 B11_13 -36.8(5) . . . . ?
B8_13 B7_13 B12_13 B11_13 1.1(7) . . . . ?
B6_13 B7_13 B12_13 B11_13 101.3(6) . . . . ?
B5_13 B7_13 B12_13 B11_13 64.6(7) . . . . ?
Cl12_13 B7_13 B12_13 B9_13 -111.1(7) . . . . ?
B8_13 B7_13 B12_13 B9_13 37.9(5) . . . . ?
B6_13 B7_13 B12_13 B9_13 138.1(6) . . . . ?
B5_13 B7_13 B12_13 B9_13 101.4(6) . . . . ?
Cl7_13 B11_13 B12_13 Cl8_13 -0.1(9) . . . . ?
B3_13 B11_13 B12_13 Cl8_13 147.5(5) . . . . ?
B10_13 B11_13 B12_13 Cl8_13 -148.7(5) . . . . ?
B2_13 B11_13 B12_13 Cl8_13 112.1(6) . . . . ?
B9_13 B11_13 B12_13 Cl8_13 -110.8(6) . . . . ?
Cl7_13 B11_13 B12_13 B6_13 -148.6(5) . . . . ?
B3_13 B11_13 B12_13 B6_13 -1.0(7) . . . . ?
B10_13 B11_13 B12_13 B6_13 62.8(7) . . . . ?
B2_13 B11_13 B12_13 B6_13 -36.4(5) . . . . ?
B9_13 B11_13 B12_13 B6_13 100.7(6) . . . . ?
Cl7_13 B11_13 B12_13 B2_13 -112.2(6) . . . . ?
B3_13 B11_13 B12_13 B2_13 35.4(5) . . . . ?
B10_13 B11_13 B12_13 B2_13 99.2(6) . . . . ?
B9_13 B11_13 B12_13 B2_13 137.0(6) . . . . ?
Cl7_13 B11_13 B12_13 B7_13 147.5(6) . . . . ?
B3_13 B11_13 B12_13 B7_13 -64.9(7) . . . . ?
B10_13 B11_13 B12_13 B7_13 -1.1(7) . . . . ?
B2_13 B11_13 B12_13 B7_13 -100.3(6) . . . . ?
B9_13 B11_13 B12_13 B7_13 36.7(5) . . . . ?
Cl7_13 B11_13 B12_13 B9_13 110.7(6) . . . . ?
B3_13 B11_13 B12_13 B9_13 -101.7(6) . . . . ?
B10_13 B11_13 B12_13 B9_13 -37.9(5) . . . . ?
B2_13 B11_13 B12_13 B9_13 -137.0(6) . . . . ?
B7_13 B9_13 B12_13 Cl8_13 -111.9(6) . . . . ?
Cl10_13 B9_13 B12_13 Cl8_13 -1.0(9) . . . . ?
B8_13 B9_13 B12_13 Cl8_13 -149.9(5) . . . . ?
B10_13 B9_13 B12_13 Cl8_13 147.4(5) . . . . ?
B11_13 B9_13 B12_13 Cl8_13 109.8(6) . . . . ?
B7_13 B9_13 B12_13 B6_13 37.7(5) . . . . ?
Cl10_13 B9_13 B12_13 B6_13 148.6(6) . . . . ?
B8_13 B9_13 B12_13 B6_13 -0.3(7) . . . . ?
B10_13 B9_13 B12_13 B6_13 -63.0(7) . . . . ?
B11_13 B9_13 B12_13 B6_13 -100.6(6) . . . . ?
B7_13 B9_13 B12_13 B2_13 100.1(6) . . . . ?
Cl10_13 B9_13 B12_13 B2_13 -148.9(6) . . . . ?
B8_13 B9_13 B12_13 B2_13 62.2(7) . . . . ?
B10_13 B9_13 B12_13 B2_13 -0.6(7) . . . . ?
B11_13 B9_13 B12_13 B2_13 -38.2(5) . . . . ?
Cl10_13 B9_13 B12_13 B7_13 111.0(7) . . . . ?
B8_13 B9_13 B12_13 B7_13 -38.0(5) . . . . ?
B10_13 B9_13 B12_13 B7_13 -100.7(6) . . . . ?
B11_13 B9_13 B12_13 B7_13 -138.3(6) . . . . ?
B7_13 B9_13 B12_13 B11_13 138.3(6) . . . . ?
Cl10_13 B9_13 B12_13 B11_13 -110.7(7) . . . . ?
B8_13 B9_13 B12_13 B11_13 100.4(6) . . . . ?
B10_13 B9_13 B12_13 B11_13 37.6(5) . . . . ?

_refine_diff_density_max         2.522
_refine_diff_density_min         -0.895
_refine_diff_density_rms         0.125



