# Electronic Supplementary Material (ESI) for Dalton Transactions.
# This journal is © The Royal Society of Chemistry 2020

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_shelx
_database_code_depnum_ccdc_archive 'CCDC 1994941'
loop_
_audit_author_name
_audit_author_address
'Oleg Siidra'
;Saint Petersburg State University
Russia
;
_audit_update_record             
;
2020-04-05 deposited with the CCDC.	2020-05-11 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2018/3
_shelx_SHELXL_version_number     2018/3
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'Cl0.67 H Cu0.33 Li0.67 O2.17 Se0.67'
_chemical_formula_weight         137.75

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Li Li -0.0003 0.0001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Se Se -0.0929 2.2259 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      monoclinic
_space_group_IT_number           15
_space_group_name_H-M_alt        'C 2/c'
_space_group_name_Hall           '-C 2yc'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'

_cell_length_a                   13.075(14)
_cell_length_b                   7.672(8)
_cell_length_c                   17.79(2)
_cell_angle_alpha                90
_cell_angle_beta                 98.93(3)
_cell_angle_gamma                90
_cell_volume                     1763(3)
_cell_formula_units_Z            24
_cell_measurement_temperature    296(2)
_cell_measurement_reflns_used    891
_cell_measurement_theta_min      2.317
_cell_measurement_theta_max      24.045

_exptl_crystal_description       prism
_exptl_crystal_colour            ?
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    3.114
_exptl_crystal_F_000             1536
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          ?
_exptl_crystal_size_mid          ?
_exptl_crystal_size_min          ?
_exptl_absorpt_coefficient_mu    11.332
_shelx_estimated_absorpt_T_min   ?
_shelx_estimated_absorpt_T_max   ?
_exptl_absorpt_correction_type   ?
_exptl_absorpt_correction_T_min  ?
_exptl_absorpt_correction_T_max  ?
_exptl_absorpt_process_details   ?
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      296(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_source                   ?
_diffrn_measurement_device_type  'Bruker APEX 2 Duo'
_diffrn_measurement_method       ?
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            9531
_diffrn_reflns_av_unetI/netI     0.0633
_diffrn_reflns_av_R_equivalents  0.1138
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_k_min       -8
_diffrn_reflns_limit_k_max       8
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_theta_min         2.317
_diffrn_reflns_theta_max         24.045
_diffrn_reflns_theta_full        24.046
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measured_fraction_theta_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.999
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.999
_diffrn_reflns_point_group_measured_fraction_full 0.999
_reflns_number_total             1396
_reflns_number_gt                1096
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       ?
_computing_cell_refinement       ?
_computing_data_reduction        ?
_computing_structure_solution    ?
_computing_structure_refinement  'SHELXL-2018/3 (Sheldrick, 2018)'
_computing_molecular_graphics    ?
_computing_publication_material  ?
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0183P)²+5.9458P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   difmap
_refine_ls_hydrogen_treatment    refall
_refine_ls_extinction_method     'SHELXL-2018/3 (Sheldrick 2018)'
_refine_ls_extinction_coef       0.00039(9)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_number_reflns         1396
_refine_ls_number_parameters     139
_refine_ls_number_restraints     2
_refine_ls_R_factor_all          0.0527
_refine_ls_R_factor_gt           0.0329
_refine_ls_wR_factor_ref         0.0733
_refine_ls_wR_factor_gt          0.0655
_refine_ls_goodness_of_fit_ref   1.015
_refine_ls_restrained_S_all      1.014
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Se1 Se 0.42851(5) 0.10261(10) 0.40056(4) 0.0141(2) Uani 1 1 d . . . . .
Se2 Se 0.26270(6) -0.34361(10) 0.61174(4) 0.0151(2) Uani 1 1 d . . . . .
Cu1 Cu 0.12684(7) 0.08471(12) 0.49663(5) 0.0182(3) Uani 1 1 d . . . . .
Cl1 Cl 0.29958(14) 0.0431(3) 0.54029(11) 0.0221(5) Uani 1 1 d . . . . .
Cl2 Cl 0.46826(14) -0.3130(3) 0.43650(11) 0.0220(5) Uani 1 1 d . . . . .
O1 O 0.3932(4) 0.3118(6) 0.4076(3) 0.0190(12) Uani 1 1 d . . . . .
O2 O 0.4843(4) 0.1217(7) 0.3235(3) 0.0213(13) Uani 1 1 d . . . . .
O3 O 0.3689(4) -0.4545(7) 0.5964(3) 0.0223(13) Uani 1 1 d . . . . .
O4 O 0.3011(4) -0.2571(7) 0.6950(3) 0.0236(14) Uani 1 1 d . . . . .
O5 O 0.3070(4) 0.0233(6) 0.3528(3) 0.0175(12) Uani 1 1 d . . . . .
OW1 O 0.500000 -0.4360(11) 0.250000 0.0251(19) Uani 1 2 d DS T P . .
OW2 O 0.3467(5) 0.1792(7) 0.7114(3) 0.0238(13) Uani 1 1 d D . . . .
Li1 Li 0.3938(11) -0.0665(19) 0.7220(8) 0.030(4) Uani 1 1 d . . . . .
Li2 Li 0.4908(11) -0.570(2) 0.3454(9) 0.039(4) Uani 1 1 d . . . . .
H1 H 0.550(6) -0.389(12) 0.285(5) 0.07(4) Uiso 1 1 d D . . . .
H2 H 0.291(7) 0.206(11) 0.732(5) 0.03(3) Uiso 1 1 d . . . . .
H3 H 0.323(8) 0.220(12) 0.665(2) 0.07(4) Uiso 1 1 d D . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Se1 O2 1.656(5) . ?
Se1 O1 1.680(5) . ?
Se1 O5 1.788(5) . ?
Se1 Li2 2.859(16) 1_565 ?
Se1 Li1 3.151(14) 6 ?
Se1 Li1 3.436(15) 5_656 ?
Se2 O4 1.630(5) . ?
Se2 O3 1.686(5) . ?
Se2 O5 1.818(5) 7_546 ?
Se2 Li1 3.203(14) . ?
Se2 Li2 3.262(15) 5_646 ?
Cu1 O1 1.934(5) 7_556 ?
Cu1 O3 1.942(5) 7_546 ?
Cu1 Cl1 2.294(3) . ?
Cu1 Cl2 2.318(3) 3_455 ?
Cu1 Li2 3.214(15) 3_455 ?
Cu1 Li2 3.409(18) 7_546 ?
Cl1 Li1 3.382(15) . ?
Cl2 Li2 2.599(17) . ?
O1 Li2 2.027(17) 1_565 ?
O2 Li1 1.943(15) 5_656 ?
O2 Li1 2.044(15) 6 ?
O2 Li2 2.395(17) 1_565 ?
O3 Li2 1.970(15) 5_646 ?
O4 Li1 1.912(15) . ?
O5 Li1 2.764(15) 6 ?
OW1 Li2 2.005(17) 2_655 ?
OW1 Li2 2.005(17) . ?
OW2 Li1 1.983(16) . ?
Li1 Li1 2.80(3) 2_656 ?
Li1 Li2 3.47(2) 5_646 ?
Li1 Li2 3.65(2) 6_546 ?
Li2 Li2 3.44(3) 2_655 ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O2 Se1 O1 98.0(3) . . ?
O2 Se1 O5 96.3(2) . . ?
O1 Se1 O5 97.3(2) . . ?
O2 Se1 Li2 56.8(4) . 1_565 ?
O1 Se1 Li2 44.2(4) . 1_565 ?
O5 Se1 Li2 114.5(3) . 1_565 ?
O2 Se1 Li1 35.5(3) . 6 ?
O1 Se1 Li1 99.3(3) . 6 ?
O5 Se1 Li1 60.9(3) . 6 ?
Li2 Se1 Li1 74.7(4) 1_565 6 ?
O2 Se1 Li1 18.8(3) . 5_656 ?
O1 Se1 Li1 110.2(3) . 5_656 ?
O5 Se1 Li1 108.0(3) . 5_656 ?
Li2 Se1 Li1 66.2(4) 1_565 5_656 ?
Li1 Se1 Li1 50.1(4) 6 5_656 ?
O4 Se2 O3 101.9(3) . . ?
O4 Se2 O5 95.4(3) . 7_546 ?
O3 Se2 O5 98.2(3) . 7_546 ?
O4 Se2 Li1 27.5(3) . . ?
O3 Se2 Li1 93.3(3) . . ?
O5 Se2 Li1 122.7(3) 7_546 . ?
O4 Se2 Li2 73.5(4) . 5_646 ?
O3 Se2 Li2 29.2(3) . 5_646 ?
O5 Se2 Li2 107.2(3) 7_546 5_646 ?
Li1 Se2 Li2 64.9(4) . 5_646 ?
O1 Cu1 O3 171.1(2) 7_556 7_546 ?
O1 Cu1 Cl1 91.15(17) 7_556 . ?
O3 Cu1 Cl1 93.43(16) 7_546 . ?
O1 Cu1 Cl2 91.92(17) 7_556 3_455 ?
O3 Cu1 Cl2 85.57(16) 7_546 3_455 ?
Cl1 Cu1 Cl2 165.19(9) . 3_455 ?
O1 Cu1 Li2 139.1(3) 7_556 3_455 ?
O3 Cu1 Li2 35.1(3) 7_546 3_455 ?
Cl1 Cu1 Li2 128.3(3) . 3_455 ?
Cl2 Cu1 Li2 53.1(3) 3_455 3_455 ?
O1 Cu1 Li2 31.4(3) 7_556 7_546 ?
O3 Cu1 Li2 139.7(3) 7_546 7_546 ?
Cl1 Cu1 Li2 105.2(2) . 7_546 ?
Cl2 Cu1 Li2 84.6(2) 3_455 7_546 ?
Li2 Cu1 Li2 114.6(3) 3_455 7_546 ?
Cu1 Cl1 Li1 123.5(3) . . ?
Cu1 Cl2 Li2 81.4(3) 3_545 . ?
Se1 O1 Cu1 122.3(3) . 7_556 ?
Se1 O1 Li2 100.5(5) . 1_565 ?
Cu1 O1 Li2 118.7(5) 7_556 1_565 ?
Se1 O2 Li1 145.2(5) . 5_656 ?
Se1 O2 Li1 116.4(5) . 6 ?
Li1 O2 Li1 89.2(6) 5_656 6 ?
Se1 O2 Li2 87.8(5) . 1_565 ?
Li1 O2 Li2 105.8(6) 5_656 1_565 ?
Li1 O2 Li2 110.4(6) 6 1_565 ?
Se2 O3 Cu1 122.0(3) . 7_546 ?
Se2 O3 Li2 126.1(6) . 5_646 ?
Cu1 O3 Li2 110.4(6) 7_546 5_646 ?
Se2 O4 Li1 129.3(5) . . ?
Se1 O5 Se2 123.4(3) . 7_546 ?
Se1 O5 Li1 84.7(3) . 6 ?
Se2 O5 Li1 132.6(4) 7_546 6 ?
Li2 OW1 Li2 118.2(10) 2_655 . ?
O4 Li1 O2 104.9(7) . 5_656 ?
O4 Li1 OW2 121.8(8) . . ?
O2 Li1 OW2 115.5(8) 5_656 . ?
O4 Li1 O2 108.7(7) . 6_556 ?
O2 Li1 O2 85.6(6) 5_656 6_556 ?
OW2 Li1 O2 114.2(7) . 6_556 ?
O4 Li1 O5 88.6(6) . 6_556 ?
O2 Li1 O5 148.0(7) 5_656 6_556 ?
OW2 Li1 O5 78.7(5) . 6_556 ?
O2 Li1 O5 62.4(4) 6_556 6_556 ?
O4 Li1 Li1 130.1(5) . 2_656 ?
O2 Li1 Li1 46.9(5) 5_656 2_656 ?
OW2 Li1 Li1 108.1(4) . 2_656 ?
O2 Li1 Li1 43.9(4) 6_556 2_656 ?
O5 Li1 Li1 102.4(7) 6_556 2_656 ?
O4 Li1 Se1 99.9(6) . 6_556 ?
O2 Li1 Se1 113.7(6) 5_656 6_556 ?
OW2 Li1 Se1 100.0(5) . 6_556 ?
O2 Li1 Se1 28.1(3) 6_556 6_556 ?
O5 Li1 Se1 34.4(2) 6_556 6_556 ?
Li1 Li1 Se1 70.2(5) 2_656 6_556 ?
O4 Li1 Se2 23.2(3) . . ?
O2 Li1 Se2 89.8(5) 5_656 . ?
OW2 Li1 Se2 116.3(6) . . ?
O2 Li1 Se2 125.8(6) 6_556 . ?
O5 Li1 Se2 110.2(5) 6_556 . ?
Li1 Li1 Se2 128.6(5) 2_656 . ?
Se1 Li1 Se2 122.6(5) 6_556 . ?
O4 Li1 Cl1 80.1(5) . . ?
O2 Li1 Cl1 81.7(5) 5_656 . ?
OW2 Li1 Cl1 67.1(4) . . ?
O2 Li1 Cl1 166.2(7) 6_556 . ?
O5 Li1 Cl1 129.7(5) 6_556 . ?
Li1 Li1 Cl1 122.3(7) 2_656 . ?
Se1 Li1 Cl1 163.7(5) 6_556 . ?
Se2 Li1 Cl1 59.9(2) . . ?
O4 Li1 Se1 104.1(5) . 5_656 ?
O2 Li1 Se1 16.0(3) 5_656 5_656 ?
OW2 Li1 Se1 104.3(6) . 5_656 ?
O2 Li1 Se1 100.9(5) 6_556 5_656 ?
O5 Li1 Se1 162.0(5) 6_556 5_656 ?
Li1 Li1 Se1 59.7(5) 2_656 5_656 ?
Se1 Li1 Se1 128.8(4) 6_556 5_656 ?
Se2 Li1 Se1 84.7(3) . 5_656 ?
Cl1 Li1 Se1 66.1(3) . 5_656 ?
O4 Li1 Li2 65.9(5) . 5_646 ?
O2 Li1 Li2 41.6(4) 5_656 5_646 ?
OW2 Li1 Li2 151.1(7) . 5_646 ?
O2 Li1 Li2 85.2(5) 6_556 5_646 ?
O5 Li1 Li2 130.2(6) 6_556 5_646 ?
Li1 Li1 Li2 70.3(4) 2_656 5_646 ?
Se1 Li1 Li2 106.0(5) 6_556 5_646 ?
Se2 Li1 Li2 58.4(3) . 5_646 ?
Cl1 Li1 Li2 89.0(4) . 5_646 ?
Se1 Li1 Li2 48.9(3) 5_656 5_646 ?
O4 Li1 Li2 73.4(5) . 6_546 ?
O2 Li1 Li2 81.6(5) 5_656 6_546 ?
OW2 Li1 Li2 148.9(7) . 6_546 ?
O2 Li1 Li2 37.9(4) 6_556 6_546 ?
O5 Li1 Li2 74.6(4) 6_556 6_546 ?
Li1 Li1 Li2 63.5(4) 2_656 6_546 ?
Se1 Li1 Li2 49.0(3) 6_556 6_546 ?
Se2 Li1 Li2 88.0(4) . 6_546 ?
Cl1 Li1 Li2 143.7(5) . 6_546 ?
Se1 Li1 Li2 96.6(4) 5_656 6_546 ?
Li2 Li1 Li2 57.7(6) 5_646 6_546 ?
O3 Li2 OW1 102.8(7) 5_646 . ?
O3 Li2 O1 111.7(8) 5_646 1_545 ?
OW1 Li2 O1 144.8(8) . 1_545 ?
O3 Li2 O2 100.8(6) 5_646 1_545 ?
OW1 Li2 O2 112.0(8) . 1_545 ?
O1 Li2 O2 68.8(5) 1_545 1_545 ?
O3 Li2 Cl2 77.7(5) 5_646 . ?
OW1 Li2 Cl2 99.5(7) . . ?
O1 Li2 Cl2 81.8(6) 1_545 . ?
O2 Li2 Cl2 147.8(7) 1_545 . ?
O3 Li2 Se1 101.3(6) 5_646 1_545 ?
OW1 Li2 Se1 143.0(8) . 1_545 ?
O1 Li2 Se1 35.3(3) 1_545 1_545 ?
O2 Li2 Se1 35.4(3) 1_545 1_545 ?
Cl2 Li2 Se1 112.8(6) . 1_545 ?
O3 Li2 Cu1 34.5(3) 5_646 3_545 ?
OW1 Li2 Cu1 114.9(6) . 3_545 ?
O1 Li2 Cu1 91.2(6) 1_545 3_545 ?
O2 Li2 Cu1 120.2(5) 1_545 3_545 ?
Cl2 Li2 Cu1 45.5(3) . 3_545 ?
Se1 Li2 Cu1 100.8(5) 1_545 3_545 ?
O3 Li2 Se2 24.7(3) 5_646 5_646 ?
OW1 Li2 Se2 96.6(6) . 5_646 ?
O1 Li2 Se2 117.7(6) 1_545 5_646 ?
O2 Li2 Se2 81.2(4) 1_545 5_646 ?
Cl2 Li2 Se2 102.2(4) . 5_646 ?
Se1 Li2 Se2 93.8(4) 1_545 5_646 ?
Cu1 Li2 Se2 58.7(2) 3_545 5_646 ?
O3 Li2 Cu1 94.2(6) 5_646 7_546 ?
OW1 Li2 Cu1 144.0(7) . 7_546 ?
O1 Li2 Cu1 29.8(3) 1_545 7_546 ?
O2 Li2 Cu1 95.3(5) 1_545 7_546 ?
Cl2 Li2 Cu1 53.2(3) . 7_546 ?
Se1 Li2 Cu1 60.0(3) 1_545 7_546 ?
Cu1 Li2 Cu1 65.4(3) 3_545 7_546 ?
Se2 Li2 Cu1 110.9(4) 5_646 7_546 ?
O3 Li2 Li2 108.4(8) 5_646 2_655 ?
OW1 Li2 Li2 30.9(5) . 2_655 ?
O1 Li2 Li2 133.2(7) 1_545 2_655 ?
O2 Li2 Li2 81.1(4) 1_545 2_655 ?
Cl2 Li2 Li2 130.3(3) . 2_655 ?
Se1 Li2 Li2 113.9(4) 1_545 2_655 ?
Cu1 Li2 Li2 135.4(6) 3_545 2_655 ?
Se2 Li2 Li2 90.7(6) 5_646 2_655 ?
Cu1 Li2 Li2 157.4(7) 7_546 2_655 ?
O3 Li2 Li1 80.8(6) 5_646 5_646 ?
OW1 Li2 Li1 91.9(7) . 5_646 ?
O1 Li2 Li1 100.0(6) 1_545 5_646 ?
O2 Li2 Li1 32.6(3) 1_545 5_646 ?
Cl2 Li2 Li1 157.3(6) . 5_646 ?
Se1 Li2 Li1 64.9(4) 1_545 5_646 ?
Cu1 Li2 Li1 111.9(5) 3_545 5_646 ?
Se2 Li2 Li1 56.7(3) 5_646 5_646 ?
Cu1 Li2 Li1 122.3(5) 7_546 5_646 ?
Li2 Li2 Li1 63.8(4) 2_655 5_646 ?
O3 Li2 Li1 126.7(7) 5_646 6_545 ?
OW1 Li2 Li1 86.8(6) . 6_545 ?
O1 Li2 Li1 78.4(5) 1_545 6_545 ?
O2 Li2 Li1 31.6(3) 1_545 6_545 ?
Cl2 Li2 Li1 153.1(6) . 6_545 ?
Se1 Li2 Li1 56.3(4) 1_545 6_545 ?
Cu1 Li2 Li1 151.8(5) 3_545 6_545 ?
Se2 Li2 Li1 103.0(5) 5_646 6_545 ?
Cu1 Li2 Li1 108.2(5) 7_546 6_545 ?
Li2 Li2 Li1 58.5(3) 2_655 6_545 ?
Li1 Li2 Li1 46.2(5) 5_646 6_545 ?

_refine_diff_density_max         0.695
_refine_diff_density_min         -0.705
_refine_diff_density_rms         0.173

