# Electronic Supplementary Material (ESI) for Materials Advances.
# This journal is © The Royal Society of Chemistry 2020

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_dy6
_database_code_depnum_ccdc_archive 'CCDC 1571865'
_audit_update_record             
;
2017-08-31 deposited with the CCDC.	2020-10-26 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-97
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'Dy6 N8 O47'
_chemical_melting_point          ?

_exptl_crystal_description       Block
_exptl_crystal_colour            Colorless
_chemical_formula_weight         1839.08

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_H-M   'P 21/n'
_symmetry_int_tables_number      14
_chemical_absolute_configuration ?

loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'

_cell_length_a                   12.5852(3)
_cell_length_b                   10.2029(3)
_cell_length_c                   15.6621(4)
_cell_angle_alpha                90
_cell_angle_beta                 97.381(3)
_cell_angle_gamma                90
_cell_volume                     1994.44(9)
_cell_formula_units_Z            2
_cell_measurement_temperature    293(2)
_cell_measurement_reflns_used    999
_cell_measurement_theta_min      2.17
_cell_measurement_theta_max      26.50
_exptl_crystal_size_max          0.28
_exptl_crystal_size_mid          0.20
_exptl_crystal_size_min          0.15
_exptl_crystal_density_meas      ?
_exptl_crystal_density_diffrn    3.062
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             1656
_exptl_absorpt_coefficient_mu    11.240
_exptl_absorpt_correction_type   Multi-Scan
_exptl_absorpt_correction_T_min  0.1449
_exptl_absorpt_correction_T_max  0.2834
_exptl_absorpt_process_details   Sadabs

_exptl_special_details           
;
 ?
;
_diffrn_radiation_probe          X-ray
_diffrn_ambient_temperature      293
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_monochromator  graphite
_diffrn_measurement_device_type  'BRUKER SMART APEX'
_diffrn_measurement_method       /w-scans
_diffrn_detector_area_resol_mean ?
_diffrn_standards_number         ?
_diffrn_standards_interval_count ?
_diffrn_standards_interval_time  ?
_diffrn_standards_decay_%        ?
_diffrn_reflns_number            7356
_diffrn_reflns_av_R_equivalents  0.0316
_diffrn_reflns_av_sigmaI/netI    0.0487
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_k_min       -7
_diffrn_reflns_limit_k_max       12
_diffrn_reflns_limit_l_min       -10
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_theta_min         2.99
_diffrn_reflns_theta_max         25.00
_reflns_number_total             3505
_reflns_number_gt                3026
_reflns_threshold_expression     >2sigma(I)

_computing_data_collection       'SMART 5.628 (Bruker, 2003)'
_computing_cell_refinement       'SAINT 6.45 ( Bruker, 2003)'
_computing_data_reduction        'SAINT 6.45 ( Bruker, 2003)'
_computing_structure_solution    SIR-97
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_molecular_graphics    'DIAMOND 2.1e'
_computing_publication_material  ?

_refine_special_details          
;
 Refinement of F² against ALL reflections.  The weighted R-factor wR and
 goodness of fit S are based on F², conventional R-factors R are based
 on F, with F set to zero for negative F². The threshold expression of
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is
 not relevant to the choice of reflections for refinement.  R-factors based
 on F² are statistically about twice as large as those based on F, and R-
 factors based on ALL data will be even larger.
;

_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'calc w=1/[σ²(Fo²)+(0.0938P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_atom_sites_solution_hydrogens   ?
_refine_ls_hydrogen_treatment    ?
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       ?
_refine_ls_number_reflns         3505
_refine_ls_number_parameters     277
_refine_ls_number_restraints     74
_refine_ls_R_factor_all          0.0508
_refine_ls_R_factor_gt           0.0431
_refine_ls_wR_factor_ref         0.1432
_refine_ls_wR_factor_gt          0.1314
_refine_ls_goodness_of_fit_ref   1.091
_refine_ls_restrained_S_all      1.090
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Dy1 Dy 0.80864(4) 0.95090(5) 0.01670(3) 0.0248(2) Uani 1 1 d . . .
Dy2 Dy 1.01919(4) 1.11851(5) 0.13938(3) 0.0235(2) Uani 1 1 d . . .
Dy3 Dy 1.05541(4) 0.79197(5) 0.07806(3) 0.02295(19) Uani 1 1 d . . .
N1 N 0.6002(9) 0.9359(14) -0.0909(7) 0.048(3) Uani 1 1 d U . .
N2 N 1.1179(8) 1.3678(10) 0.2118(7) 0.035(2) Uani 1 1 d U . .
N3 N 1.1958(8) 0.5612(10) 0.0633(7) 0.036(2) Uani 1 1 d U . .
N4 N 0.680(2) 1.371(2) 0.1497(15) 0.141(10) Uani 1 1 d DU . .
O1 O 1.0000 1.0000 0.0000 0.022(2) Uani 1 2 d S . .
O2 O 0.9295(6) 0.9163(8) 0.1405(5) 0.0262(16) Uani 1 1 d . . .
O1W O 0.7316(8) 0.7486(12) 0.0766(8) 0.069(3) Uani 1 1 d . . .
O3 O 0.9057(6) 0.7733(7) -0.0272(5) 0.0252(16) Uani 1 1 d . . .
O2W O 0.7064(8) 1.0151(13) 0.1324(7) 0.062(3) Uani 1 1 d . . .
O4 O 1.1611(6) 0.9747(7) 0.1197(5) 0.0269(17) Uani 1 1 d . . .
O3W O 0.8912(9) 1.1740(11) 0.2378(7) 0.062(3) Uani 1 1 d . . .
O5 O 0.8638(6) 1.1678(8) 0.0459(5) 0.0274(17) Uani 1 1 d . . .
O4W O 1.0815(7) 1.0396(9) 0.2844(6) 0.045(2) Uani 1 1 d . . .
O6 O 0.6670(8) 0.8494(10) -0.0903(7) 0.051(2) Uani 1 1 d U . .
O5W O 1.1095(7) 0.7629(9) 0.2315(6) 0.039(2) Uani 1 1 d . . .
O7 O 0.6244(8) 1.0340(11) -0.0445(7) 0.060(3) Uani 1 1 d U . .
O6W O 0.9417(7) 0.6247(9) 0.1349(7) 0.047(2) Uani 1 1 d . . .
O8 O 0.5143(9) 0.9303(16) -0.1401(8) 0.087(4) Uani 1 1 d U . .
O7W O 0.5204(10) 0.7354(14) 0.0856(9) 0.085(4) Uani 1 1 d . . .
O9 O 1.0250(6) 1.3670(8) 0.1732(6) 0.043(2) Uani 1 1 d U . .
O10 O 1.1659(7) 1.2571(8) 0.2154(6) 0.038(2) Uani 1 1 d U . .
O11 O 1.1618(8) 1.4676(8) 0.2413(6) 0.045(2) Uani 1 1 d U . .
O12 O 1.2326(7) 0.6644(8) 0.1030(6) 0.042(2) Uani 1 1 d U . .
O13 O 1.1027(7) 0.5681(9) 0.0268(7) 0.049(3) Uani 1 1 d U . .
O14 O 1.2475(8) 0.4586(8) 0.0630(7) 0.050(3) Uani 1 1 d U . .
O15 O 0.582(2) 1.386(3) 0.156(2) 0.31(2) Uani 1 1 d DU . .
O16 O 0.6998(14) 1.3398(19) 0.0867(10) 0.127(7) Uani 1 1 d U . .
O17 O 0.723(3) 1.345(3) 0.2284(19) 0.274(17) Uani 1 1 d DU . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Dy1 O2 2.332(7) . ?
Dy1 O3 2.337(8) . ?
Dy1 O4 2.344(7) 3_775 ?
Dy1 O5 2.346(8) . ?
Dy1 O2W 2.443(11) . ?
Dy1 O1 2.5062(5) . ?
Dy1 O6 2.508(9) . ?
Dy1 O1W 2.512(11) . ?
Dy1 O7 2.538(9) . ?
Dy1 N1 2.934(10) . ?
Dy1 Dy2 3.5114(7) . ?
Dy1 Dy3 3.5258(7) . ?
Dy2 O5 2.343(7) . ?
Dy2 O2 2.353(8) . ?
Dy2 O4 2.362(8) . ?
Dy2 O3 2.372(7) 3_775 ?
Dy2 O3W 2.436(11) . ?
Dy2 O4W 2.443(8) . ?
Dy2 O1 2.4799(5) . ?
Dy2 O10 2.503(8) . ?
Dy2 O9 2.590(8) . ?
Dy2 Dy3 3.5132(7) . ?
Dy2 Dy3 3.5344(7) 3_775 ?
Dy3 O4 2.334(7) . ?
Dy3 O2 2.340(7) . ?
Dy3 O5 2.340(8) 3_775 ?
Dy3 O3 2.346(7) . ?
Dy3 O5W 2.431(9) . ?
Dy3 O6W 2.466(9) . ?
Dy3 O1 2.5034(5) . ?
Dy3 O13 2.517(9) . ?
Dy3 O12 2.568(9) . ?
Dy3 Dy2 3.5344(7) 3_775 ?
N1 O6 1.218(15) . ?
N1 O8 1.245(14) . ?
N1 O7 1.251(15) . ?
N2 O11 1.220(12) . ?
N2 O9 1.245(12) . ?
N2 O10 1.279(12) . ?
N3 O14 1.233(12) . ?
N3 O13 1.238(13) . ?
N3 O12 1.279(13) . ?
N4 O16 1.09(2) . ?
N4 O15 1.27(3) . ?
N4 O17 1.306(18) . ?
O1 Dy2 2.4799(5) 3_775 ?
O1 Dy3 2.5034(5) 3_775 ?
O1 Dy1 2.5062(5) 3_775 ?
O3 Dy2 2.372(7) 3_775 ?
O4 Dy1 2.344(7) 3_775 ?
O5 Dy3 2.340(8) 3_775 ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O2 Dy1 O3 79.5(3) . . ?
O2 Dy1 O4 129.9(3) . 3_775 ?
O3 Dy1 O4 80.3(3) . 3_775 ?
O2 Dy1 O5 80.6(3) . . ?
O3 Dy1 O5 129.5(3) . . ?
O4 Dy1 O5 78.1(3) 3_775 . ?
O2 Dy1 O2W 76.9(3) . . ?
O3 Dy1 O2W 140.4(3) . . ?
O4 Dy1 O2W 138.8(3) 3_775 . ?
O5 Dy1 O2W 76.9(3) . . ?
O2 Dy1 O1 65.44(19) . . ?
O3 Dy1 O1 65.09(17) . . ?
O4 Dy1 O1 64.50(18) 3_775 . ?
O5 Dy1 O1 64.38(18) . . ?
O2W Dy1 O1 128.9(3) . . ?
O2 Dy1 O6 145.5(3) . . ?
O3 Dy1 O6 80.6(3) . . ?
O4 Dy1 O6 73.1(3) 3_775 . ?
O5 Dy1 O6 133.4(3) . . ?
O2W Dy1 O6 102.1(4) . . ?
O1 Dy1 O6 128.5(3) . . ?
O2 Dy1 O1W 78.9(3) . . ?
O3 Dy1 O1W 73.4(4) . . ?
O4 Dy1 O1W 136.2(4) 3_775 . ?
O5 Dy1 O1W 145.2(4) . . ?
O2W Dy1 O1W 71.2(4) . . ?
O1 Dy1 O1W 128.7(3) . . ?
O6 Dy1 O1W 68.6(4) . . ?
O2 Dy1 O7 146.2(3) . . ?
O3 Dy1 O7 129.4(3) . . ?
O4 Dy1 O7 78.2(3) 3_775 . ?
O5 Dy1 O7 89.5(3) . . ?
O2W Dy1 O7 69.4(3) . . ?
O1 Dy1 O7 137.5(3) . . ?
O6 Dy1 O7 49.4(3) . . ?
O1W Dy1 O7 92.1(4) . . ?
O2 Dy1 N1 155.4(3) . . ?
O3 Dy1 N1 104.7(3) . . ?
O4 Dy1 N1 74.4(3) 3_775 . ?
O5 Dy1 N1 112.4(3) . . ?
O2W Dy1 N1 85.6(3) . . ?
O1 Dy1 N1 138.6(2) . . ?
O6 Dy1 N1 24.3(3) . . ?
O1W Dy1 N1 79.2(4) . . ?
O7 Dy1 N1 25.1(3) . . ?
O2 Dy1 Dy2 41.7(2) . . ?
O3 Dy1 Dy2 98.76(17) . . ?
O4 Dy1 Dy2 98.14(17) 3_775 . ?
O5 Dy1 Dy2 41.47(17) . . ?
O2W Dy1 Dy2 84.0(2) . . ?
O1 Dy1 Dy2 44.930(11) . . ?
O6 Dy1 Dy2 171.2(2) . . ?
O1W Dy1 Dy2 119.7(3) . . ?
O7 Dy1 Dy2 129.2(3) . . ?
N1 Dy1 Dy2 153.6(3) . . ?
O2 Dy1 Dy3 41.08(18) . . ?
O3 Dy1 Dy3 41.26(17) . . ?
O4 Dy1 Dy3 99.03(18) 3_775 . ?
O5 Dy1 Dy3 98.78(17) . . ?
O2W Dy1 Dy3 116.8(2) . . ?
O1 Dy1 Dy3 45.235(11) . . ?
O6 Dy1 Dy3 121.2(2) . . ?
O1W Dy1 Dy3 83.6(3) . . ?
O7 Dy1 Dy3 170.6(2) . . ?
N1 Dy1 Dy3 145.5(3) . . ?
Dy2 Dy1 Dy3 59.898(14) . . ?
O5 Dy2 O2 80.2(3) . . ?
O5 Dy2 O4 129.5(3) . . ?
O2 Dy2 O4 80.1(3) . . ?
O5 Dy2 O3 79.5(3) . 3_775 ?
O2 Dy2 O3 130.6(3) . 3_775 ?
O4 Dy2 O3 79.2(3) . 3_775 ?
O5 Dy2 O3W 77.2(3) . . ?
O2 Dy2 O3W 80.9(3) . . ?
O4 Dy2 O3W 143.1(3) . . ?
O3 Dy2 O3W 136.0(3) 3_775 . ?
O5 Dy2 O4W 142.6(3) . . ?
O2 Dy2 O4W 78.5(3) . . ?
O4 Dy2 O4W 76.0(3) . . ?
O3 Dy2 O4W 137.0(3) 3_775 . ?
O3W Dy2 O4W 69.4(3) . . ?
O5 Dy2 O1 64.86(19) . . ?
O2 Dy2 O1 65.57(18) . . ?
O4 Dy2 O1 64.67(17) . . ?
O3 Dy2 O1 65.03(18) 3_775 . ?
O3W Dy2 O1 132.3(3) . . ?
O4W Dy2 O1 129.9(2) . . ?
O5 Dy2 O10 133.0(3) . . ?
O2 Dy2 O10 144.8(3) . . ?
O4 Dy2 O10 83.6(3) . . ?
O3 Dy2 O10 75.5(3) 3_775 . ?
O3W Dy2 O10 94.3(4) . . ?
O4W Dy2 O10 67.3(3) . . ?
O1 Dy2 O10 132.6(2) . . ?
O5 Dy2 O9 85.3(3) . . ?
O2 Dy2 O9 149.1(3) . . ?
O4 Dy2 O9 129.3(2) . . ?
O3 Dy2 O9 72.1(3) 3_775 . ?
O3W Dy2 O9 69.3(3) . . ?
O4W Dy2 O9 97.8(3) . . ?
O1 Dy2 O9 130.9(2) . . ?
O10 Dy2 O9 49.4(3) . . ?
O5 Dy2 Dy1 41.55(19) . . ?
O2 Dy2 Dy1 41.23(17) . . ?
O4 Dy2 Dy1 98.99(17) . . ?
O3 Dy2 Dy1 99.54(17) 3_775 . ?
O3W Dy2 Dy1 86.9(3) . . ?
O4W Dy2 Dy1 118.6(2) . . ?
O1 Dy2 Dy1 45.539(12) . . ?
O10 Dy2 Dy1 173.94(19) . . ?
O9 Dy2 Dy1 126.05(17) . . ?
O5 Dy2 Dy3 99.20(19) . . ?
O2 Dy2 Dy3 41.39(18) . . ?
O4 Dy2 Dy3 41.27(17) . . ?
O3 Dy2 Dy3 99.25(19) 3_775 . ?
O3W Dy2 Dy3 120.9(3) . . ?
O4W Dy2 Dy3 84.5(2) . . ?
O1 Dy2 Dy3 45.445(11) . . ?
O10 Dy2 Dy3 123.53(19) . . ?
O9 Dy2 Dy3 169.5(2) . . ?
Dy1 Dy2 Dy3 60.256(14) . . ?
O5 Dy2 Dy3 40.97(19) . 3_775 ?
O2 Dy2 Dy3 99.52(18) . 3_775 ?
O4 Dy2 Dy3 98.43(17) . 3_775 ?
O3 Dy2 Dy3 41.22(17) 3_775 3_775 ?
O3W Dy2 Dy3 115.8(2) . 3_775 ?
O4W Dy2 Dy3 174.3(2) . 3_775 ?
O1 Dy2 Dy3 45.096(11) . 3_775 ?
O10 Dy2 Dy3 113.6(2) . 3_775 ?
O9 Dy2 Dy3 86.6(2) . 3_775 ?
Dy1 Dy2 Dy3 60.675(14) . 3_775 ?
Dy3 Dy2 Dy3 90.540(16) . 3_775 ?
O4 Dy3 O2 81.0(3) . . ?
O4 Dy3 O5 78.4(3) . 3_775 ?
O2 Dy3 O5 129.9(3) . 3_775 ?
O4 Dy3 O3 129.7(3) . . ?
O2 Dy3 O3 79.1(3) . . ?
O5 Dy3 O3 80.0(3) 3_775 . ?
O4 Dy3 O5W 75.2(3) . . ?
O2 Dy3 O5W 76.8(3) . . ?
O5 Dy3 O5W 138.2(3) 3_775 . ?
O3 Dy3 O5W 141.5(3) . . ?
O4 Dy3 O6W 142.0(3) . . ?
O2 Dy3 O6W 76.6(3) . . ?
O5 Dy3 O6W 139.0(3) 3_775 . ?
O3 Dy3 O6W 75.3(3) . . ?
O5W Dy3 O6W 70.2(3) . . ?
O4 Dy3 O1 64.68(17) . . ?
O2 Dy3 O1 65.38(19) . . ?
O5 Dy3 O1 64.51(18) 3_775 . ?
O3 Dy3 O1 65.01(18) . . ?
O5W Dy3 O1 127.7(2) . . ?
O6W Dy3 O1 128.7(2) . . ?
O4 Dy3 O13 131.6(3) . . ?
O2 Dy3 O13 145.7(3) . . ?
O5 Dy3 O13 75.4(3) 3_775 . ?
O3 Dy3 O13 84.5(3) . . ?
O5W Dy3 O13 99.0(3) . . ?
O6W Dy3 O13 70.1(3) . . ?
O1 Dy3 O13 132.5(2) . . ?
O4 Dy3 O12 84.8(3) . . ?
O2 Dy3 O12 146.4(3) . . ?
O5 Dy3 O12 75.8(3) 3_775 . ?
O3 Dy3 O12 132.0(3) . . ?
O5W Dy3 O12 70.1(3) . . ?
O6W Dy3 O12 97.3(3) . . ?
O1 Dy3 O12 133.3(2) . . ?
O13 Dy3 O12 49.7(3) . . ?
O4 Dy3 Dy2 41.88(19) . . ?
O2 Dy3 Dy2 41.68(19) . . ?
O5 Dy3 Dy2 98.38(19) 3_775 . ?
O3 Dy3 Dy2 98.53(19) . . ?
O5W Dy3 Dy2 82.8(2) . . ?
O6W Dy3 Dy2 117.1(2) . . ?
O1 Dy3 Dy2 44.901(11) . . ?
O13 Dy3 Dy2 172.7(2) . . ?
O12 Dy3 Dy2 125.43(18) . . ?
O4 Dy3 Dy1 99.17(18) . . ?
O2 Dy3 Dy1 40.92(17) . . ?
O5 Dy3 Dy1 98.90(17) 3_775 . ?
O3 Dy3 Dy1 41.07(19) . . ?
O5W Dy3 Dy1 116.8(2) . . ?
O6W Dy3 Dy1 83.4(2) . . ?
O1 Dy3 Dy1 45.299(11) . . ?
O13 Dy3 Dy1 124.5(2) . . ?
O12 Dy3 Dy1 172.6(2) . . ?
Dy2 Dy3 Dy1 59.847(14) . . ?
O4 Dy3 Dy2 97.71(17) . 3_775 ?
O2 Dy3 Dy2 98.75(18) . 3_775 ?
O5 Dy3 Dy2 41.02(17) 3_775 3_775 ?
O3 Dy3 Dy2 41.77(18) . 3_775 ?
O5W Dy3 Dy2 172.0(2) . 3_775 ?
O6W Dy3 Dy2 115.6(2) . 3_775 ?
O1 Dy3 Dy2 44.559(11) . 3_775 ?
O13 Dy3 Dy2 88.4(2) . 3_775 ?
O12 Dy3 Dy2 113.3(2) . 3_775 ?
Dy2 Dy3 Dy2 89.460(15) . 3_775 ?
Dy1 Dy3 Dy2 60.189(14) . 3_775 ?
O6 N1 O8 121.0(14) . . ?
O6 N1 O7 117.3(10) . . ?
O8 N1 O7 121.5(14) . . ?
O6 N1 Dy1 57.9(6) . . ?
O8 N1 Dy1 176.9(10) . . ?
O7 N1 Dy1 59.4(6) . . ?
O11 N2 O9 122.7(10) . . ?
O11 N2 O10 122.2(10) . . ?
O9 N2 O10 115.1(10) . . ?
O14 N3 O13 121.1(11) . . ?
O14 N3 O12 122.9(10) . . ?
O13 N3 O12 116.0(10) . . ?
O16 N4 O15 116(3) . . ?
O16 N4 O17 133(3) . . ?
O15 N4 O17 104(2) . . ?
Dy2 O1 Dy2 180.000(11) 3_775 . ?
Dy2 O1 Dy3 90.346(16) 3_775 . ?
Dy2 O1 Dy3 89.654(16) . . ?
Dy2 O1 Dy3 89.654(16) 3_775 3_775 ?
Dy2 O1 Dy3 90.346(16) . 3_775 ?
Dy3 O1 Dy3 180.0 . 3_775 ?
Dy2 O1 Dy1 90.469(16) 3_775 . ?
Dy2 O1 Dy1 89.531(16) . . ?
Dy3 O1 Dy1 89.466(16) . . ?
Dy3 O1 Dy1 90.534(16) 3_775 . ?
Dy2 O1 Dy1 89.531(16) 3_775 3_775 ?
Dy2 O1 Dy1 90.469(16) . 3_775 ?
Dy3 O1 Dy1 90.534(16) . 3_775 ?
Dy3 O1 Dy1 89.466(16) 3_775 3_775 ?
Dy1 O1 Dy1 180.0 . 3_775 ?
Dy1 O2 Dy3 98.0(3) . . ?
Dy1 O2 Dy2 97.1(3) . . ?
Dy3 O2 Dy2 96.9(3) . . ?
Dy1 O3 Dy3 97.7(3) . . ?
Dy1 O3 Dy2 97.5(3) . 3_775 ?
Dy3 O3 Dy2 97.0(3) . 3_775 ?
Dy3 O4 Dy1 99.1(3) . 3_775 ?
Dy3 O4 Dy2 96.8(3) . . ?
Dy1 O4 Dy2 97.6(3) 3_775 . ?
Dy3 O5 Dy2 98.0(3) 3_775 . ?
Dy3 O5 Dy1 98.8(3) 3_775 . ?
Dy2 O5 Dy1 97.0(3) . . ?
N1 O6 Dy1 97.9(8) . . ?
N1 O7 Dy1 95.4(8) . . ?
N2 O9 Dy2 96.1(6) . . ?
N2 O10 Dy2 99.4(6) . . ?
N3 O12 Dy3 95.2(6) . . ?
N3 O13 Dy3 98.8(7) . . ?

_diffrn_measured_fraction_theta_max 0.998
_diffrn_reflns_theta_full        25.00
_diffrn_measured_fraction_theta_full 0.998
_refine_diff_density_max         2.339
_refine_diff_density_min         -1.957
_refine_diff_density_rms         0.377

