# Electronic Supplementary Material (ESI) for Polymer Chemistry.
# This journal is © The Royal Society of Chemistry 2020

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_1
_database_code_depnum_ccdc_archive 'CCDC 1585233'
loop_
_audit_author_name
_audit_author_address
'Guillermo Ahumada'
;UNIST
South Korea
;
_audit_update_record             
;
2020-05-19 deposited with the CCDC.	2020-07-15 downloaded from the CCDC.
;
_audit_creation_date             2020-04-16
_audit_creation_method           
;
Olex2 1.3
(compiled 2020.02.04 svn.rd84adfe8 for OlexSys, GUI svn.r6032)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        
;
 ?
;
_chemical_formula_moiety         'C16 H16 Cl2 Rh2'
_chemical_formula_sum            'C16 H16 Cl2 Rh2'
_chemical_formula_weight         485.01
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Rh Rh 0.0927 3.6045 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_H-M_alt        'P 1 21/c 1'
_space_group_name_Hall           '-P 2ybc'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'

_cell_length_a                   10.747(3)
_cell_length_b                   11.263(3)
_cell_length_c                   12.692(4)
_cell_angle_alpha                90
_cell_angle_beta                 102.758(12)
_cell_angle_gamma                90
_cell_volume                     1498.4(7)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    1023
_cell_measurement_temperature    123
_cell_measurement_theta_max      68.1
_cell_measurement_theta_min      25.3
_shelx_estimated_absorpt_T_max   0.420
_shelx_estimated_absorpt_T_min   0.102
_exptl_absorpt_coefficient_mu    20.964
_exptl_absorpt_correction_T_max  0.591
_exptl_absorpt_correction_T_min  0.227
_exptl_absorpt_correction_type   numerical
_exptl_absorpt_process_details   
'Abscor. T. Higashi (2001). The Rigaku Corporation, Tokyo, Japan'
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            'metallic light yellow'
_exptl_crystal_colour_lustre     metallic
_exptl_crystal_colour_modifier   light
_exptl_crystal_colour_primary    yellow
_exptl_crystal_density_diffrn    2.150
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       Prism
_exptl_crystal_F_000             944
_exptl_crystal_recrystallization_method 
'The material was recrystallised from DCM by slow evaporation'
_exptl_crystal_size_max          0.2
_exptl_crystal_size_mid          0.06
_exptl_crystal_size_min          0.05
_exptl_special_details           
;
 ?
;
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0392
_diffrn_reflns_av_unetI/netI     0.0408
_diffrn_reflns_Laue_measured_fraction_full 0.936
_diffrn_reflns_Laue_measured_fraction_max 0.936
_diffrn_reflns_limit_h_max       4
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       15
_diffrn_reflns_limit_l_min       -14
_diffrn_reflns_number            7893
_diffrn_reflns_point_group_measured_fraction_full 0.936
_diffrn_reflns_point_group_measured_fraction_max 0.936
_diffrn_reflns_theta_full        67.687
_diffrn_reflns_theta_max         68.283
_diffrn_reflns_theta_min         7.266
_diffrn_ambient_temperature      123.0
_diffrn_detector_area_resol_mean ?
_diffrn_detector_type            'Rigaku Pilatus 200K'
_diffrn_measured_fraction_theta_full 0.982
_diffrn_measured_fraction_theta_max 0.982
_diffrn_measurement_device       'AFC12 (Right): Kappa 3 circle'
_diffrn_measurement_device_type  'Rigaku Xtalab P200'
_diffrn_measurement_method       'profile data from ω-scans'
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54187
_diffrn_source                   ?
_diffrn_source_current           0.6
_diffrn_source_power             0.03
_diffrn_source_voltage           50.0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                2263
_reflns_number_total             2574
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       ?
_computing_data_collection       ?
_computing_data_reduction        ?
_computing_molecular_graphics    'Olex2 1.3 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.3 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2018/3 (Sheldrick, 2015)'
_computing_structure_solution    'SHELXT 2018/2 (Sheldrick, 2018)'
_refine_diff_density_max         1.844
_refine_diff_density_min         -0.787
_refine_diff_density_rms         0.153
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.969
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     181
_refine_ls_number_reflns         2574
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0353
_refine_ls_R_factor_gt           0.0330
_refine_ls_restrained_S_all      0.969
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0536P)²] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0803
_refine_ls_wR_factor_ref         0.0812
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups
2.a Ternary CH refined with riding coordinates:
 C2A(H2A), C3A(H3A), C1A(H1A), C4A(H4A), C5(H5), C5A(H5A), C6(H6), C6A(H6A)
2.b Aromatic/amide H refined with riding coordinates:
 C3(H3), C4(H4), C1(H1), C2(H2), C7A(H7A), C8A(H8A), C7(H7), C8(H8)
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Rh1A Rh 0.83426(3) 0.39095(3) 0.65374(2) 0.01871(12) Uani 1 1 d . . . . .
Cl1 Cl 0.91065(9) 0.57093(9) 0.58944(8) 0.0222(2) Uani 1 1 d . . . . .
Cl2 Cl 0.90306(9) 0.47008(9) 0.83229(8) 0.0239(2) Uani 1 1 d . . . . .
C3 C 0.6839(4) 0.7597(4) 0.6381(3) 0.0216(9) Uani 1 1 d . . . . .
H3 H 0.670117 0.721202 0.569880 0.026 Uiso 1 1 calc R U . A 1
C2A C 0.8256(4) 0.2058(4) 0.6791(4) 0.0232(9) Uani 1 1 d . . . . .
H2A H 0.882806 0.166506 0.742362 0.028 Uiso 1 1 calc R U . . .
C4 C 0.7935(4) 0.8227(4) 0.6826(4) 0.0257(10) Uani 1 1 d . . . . .
H4 H 0.862407 0.833133 0.647726 0.031 Uiso 1 1 calc R U . B 1
C3A C 0.6915(4) 0.3440(4) 0.5208(3) 0.0222(9) Uani 1 1 d . . . . .
H3A H 0.649019 0.405239 0.467853 0.027 Uiso 1 1 calc R U . . .
C1 C 0.6700(4) 0.6942(4) 0.8079(3) 0.0242(9) Uani 1 1 d . . . . .
H1 H 0.648264 0.619937 0.834437 0.029 Uiso 1 1 calc R U . C 1
C1A C 0.7106(4) 0.2603(4) 0.6887(3) 0.0219(9) Uani 1 1 d . . . . .
H1A H 0.682316 0.260155 0.758600 0.026 Uiso 1 1 calc R U . . .
C2 C 0.7801(4) 0.7568(4) 0.8528(4) 0.0277(10) Uani 1 1 d . . . . .
H2 H 0.841948 0.729983 0.913614 0.033 Uiso 1 1 calc R U . D 1
C4A C 0.8063(4) 0.2903(4) 0.5106(4) 0.0243(9) Uani 1 1 d . . . . .
H4A H 0.848794 0.312155 0.450695 0.029 Uiso 1 1 calc R U . . .
C5 C 0.5871(4) 0.7584(4) 0.7105(4) 0.0229(9) Uani 1 1 d . . . . .
H5 H 0.506591 0.715056 0.677987 0.028 Uiso 1 1 calc R U . . .
C5A C 0.6139(4) 0.2648(4) 0.5798(4) 0.0226(9) Uani 1 1 d . . . . .
H5A H 0.530536 0.300840 0.585190 0.027 Uiso 1 1 calc R U . . .
C6 C 0.7916(5) 0.8738(4) 0.7938(4) 0.0298(11) Uani 1 1 d . . . . .
H6 H 0.870189 0.919851 0.826454 0.036 Uiso 1 1 calc R U . . .
C6A C 0.8251(4) 0.1681(4) 0.5641(4) 0.0262(10) Uani 1 1 d . . . . .
H6A H 0.906342 0.128934 0.557106 0.031 Uiso 1 1 calc R U . . .
C7A C 0.5999(4) 0.1425(4) 0.5303(4) 0.0251(10) Uani 1 1 d . . . . .
H7A H 0.519397 0.104728 0.507255 0.030 Uiso 1 1 calc R U . . .
C8A C 0.7077(5) 0.0919(4) 0.5214(4) 0.0281(10) Uani 1 1 d . . . . .
H8A H 0.711769 0.015160 0.491235 0.034 Uiso 1 1 calc R U . . .
C7 C 0.5649(5) 0.8854(4) 0.7419(4) 0.0276(10) Uani 1 1 d . . . . .
H7 H 0.482165 0.919212 0.731931 0.033 Uiso 1 1 calc R U . . .
C8 C 0.6695(5) 0.9450(4) 0.7840(4) 0.0316(11) Uani 1 1 d . . . . .
H8 H 0.668678 1.025457 0.806253 0.038 Uiso 1 1 calc R U . . .
Rh1 Rh 0.81688(3) 0.64316(3) 0.73056(2) 0.01913(12) Uani 1 1 d . . . E 2


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Rh1A Cl1 2.3969(11) . ?
Rh1A Cl2 2.3950(12) . ?
Rh1A C2A 2.115(5) . ?
Rh1A C3A 2.082(4) . ?
Rh1A C1A 2.095(4) . ?
Rh1A C4A 2.106(4) . ?
Cl1 Rh1 2.3839(11) . ?
Cl2 Rh1 2.4077(12) . ?
C3 H3 0.9500 . ?
C3 C4 1.385(6) . ?
C3 C5 1.532(6) . ?
C3 Rh1 2.098(4) . ?
C2A H2A 1.0000 . ?
C2A C1A 1.409(6) . ?
C2A C6A 1.519(6) . ?
C4 H4 0.9500 . ?
C4 C6 1.529(7) . ?
C4 Rh1 2.111(5) . ?
C3A H3A 1.0000 . ?
C3A C4A 1.405(6) . ?
C3A C5A 1.526(6) . ?
C1 H1 0.9500 . ?
C1 C2 1.387(7) . ?
C1 C5 1.536(6) . ?
C1 Rh1 2.114(4) . ?
C1A H1A 1.0000 . ?
C1A C5A 1.535(6) . ?
C2 H2 0.9500 . ?
C2 C6 1.534(7) . ?
C2 Rh1 2.114(4) . ?
C4A H4A 1.0000 . ?
C4A C6A 1.528(7) . ?
C5 H5 1.0000 . ?
C5 C7 1.517(6) . ?
C5A H5A 1.0000 . ?
C5A C7A 1.508(6) . ?
C6 H6 1.0000 . ?
C6 C8 1.519(7) . ?
C6A H6A 1.0000 . ?
C6A C8A 1.524(7) . ?
C7A H7A 0.9500 . ?
C7A C8A 1.318(7) . ?
C8A H8A 0.9500 . ?
C7 H7 0.9500 . ?
C7 C8 1.317(7) . ?
C8 H8 0.9500 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Cl2 Rh1A Cl1 87.14(4) . . ?
C2A Rh1A Cl1 156.27(12) . . ?
C2A Rh1A Cl2 103.74(13) . . ?
C3A Rh1A Cl1 100.67(13) . . ?
C3A Rh1A Cl2 151.57(12) . . ?
C3A Rh1A C2A 79.86(18) . . ?
C3A Rh1A C1A 66.73(17) . . ?
C3A Rh1A C4A 39.20(18) . . ?
C1A Rh1A Cl1 161.30(12) . . ?
C1A Rh1A Cl2 97.99(12) . . ?
C1A Rh1A C2A 39.10(17) . . ?
C1A Rh1A C4A 80.11(17) . . ?
C4A Rh1A Cl1 98.95(13) . . ?
C4A Rh1A Cl2 166.41(13) . . ?
C4A Rh1A C2A 66.31(18) . . ?
Rh1 Cl1 Rh1A 78.42(3) . . ?
Rh1A Cl2 Rh1 78.00(4) . . ?
C4 C3 H3 123.5 . . ?
C4 C3 C5 112.9(4) . . ?
C4 C3 Rh1 71.3(3) . . ?
C5 C3 H3 123.5 . . ?
C5 C3 Rh1 97.3(3) . . ?
Rh1A C2A H2A 121.3 . . ?
C1A C2A Rh1A 69.7(3) . . ?
C1A C2A H2A 121.3 . . ?
C1A C2A C6A 112.8(4) . . ?
C6A C2A Rh1A 96.9(3) . . ?
C6A C2A H2A 121.3 . . ?
C3 C4 H4 123.7 . . ?
C3 C4 C6 112.7(4) . . ?
C3 C4 Rh1 70.3(3) . . ?
C6 C4 H4 123.7 . . ?
C6 C4 Rh1 96.8(3) . . ?
Rh1A C3A H3A 121.0 . . ?
C4A C3A Rh1A 71.3(2) . . ?
C4A C3A H3A 121.0 . . ?
C4A C3A C5A 112.3(4) . . ?
C5A C3A Rh1A 97.8(3) . . ?
C5A C3A H3A 121.0 . . ?
C2 C1 H1 123.8 . . ?
C2 C1 C5 112.4(4) . . ?
C2 C1 Rh1 70.8(2) . . ?
C5 C1 H1 123.8 . . ?
C5 C1 Rh1 96.6(3) . . ?
Rh1A C1A H1A 121.4 . . ?
C2A C1A Rh1A 71.2(2) . . ?
C2A C1A H1A 121.4 . . ?
C2A C1A C5A 111.7(4) . . ?
C5A C1A Rh1A 97.0(3) . . ?
C5A C1A H1A 121.4 . . ?
C1 C2 H2 123.5 . . ?
C1 C2 C6 112.9(4) . . ?
C1 C2 Rh1 70.9(3) . . ?
C6 C2 H2 123.5 . . ?
C6 C2 Rh1 96.6(3) . . ?
Rh1A C4A H4A 121.4 . . ?
C3A C4A Rh1A 69.5(2) . . ?
C3A C4A H4A 121.4 . . ?
C3A C4A C6A 112.3(4) . . ?
C6A C4A Rh1A 97.0(3) . . ?
C6A C4A H4A 121.4 . . ?
C3 C5 C1 97.9(3) . . ?
C3 C5 H5 113.4 . . ?
C1 C5 H5 113.4 . . ?
C7 C5 C3 108.4(3) . . ?
C7 C5 C1 109.2(4) . . ?
C7 C5 H5 113.4 . . ?
C3A C5A C1A 97.2(3) . . ?
C3A C5A H5A 113.0 . . ?
C1A C5A H5A 113.0 . . ?
C7A C5A C3A 110.2(4) . . ?
C7A C5A C1A 109.3(4) . . ?
C7A C5A H5A 113.0 . . ?
C4 C6 C2 98.4(4) . . ?
C4 C6 H6 113.3 . . ?
C2 C6 H6 113.3 . . ?
C8 C6 C4 108.1(4) . . ?
C8 C6 C2 109.4(4) . . ?
C8 C6 H6 113.3 . . ?
C2A C6A C4A 98.5(4) . . ?
C2A C6A H6A 113.0 . . ?
C2A C6A C8A 109.1(4) . . ?
C4A C6A H6A 113.0 . . ?
C8A C6A C4A 109.4(4) . . ?
C8A C6A H6A 113.0 . . ?
C5A C7A H7A 122.5 . . ?
C8A C7A C5A 114.9(4) . . ?
C8A C7A H7A 122.5 . . ?
C6A C8A H8A 123.2 . . ?
C7A C8A C6A 113.6(4) . . ?
C7A C8A H8A 123.2 . . ?
C5 C7 H7 122.7 . . ?
C8 C7 C5 114.7(4) . . ?
C8 C7 H7 122.7 . . ?
C6 C8 H8 122.9 . . ?
C7 C8 C6 114.1(4) . . ?
C7 C8 H8 122.9 . . ?
Cl1 Rh1 Cl2 87.15(4) . . ?
C3 Rh1 Cl1 98.16(12) . . ?
C3 Rh1 Cl2 160.10(12) . . ?
C3 Rh1 C4 38.41(18) . . ?
C3 Rh1 C1 66.63(17) . . ?
C3 Rh1 C2 79.47(18) . . ?
C4 Rh1 Cl1 98.82(12) . . ?
C4 Rh1 Cl2 159.65(14) . . ?
C4 Rh1 C1 79.63(17) . . ?
C4 Rh1 C2 66.56(18) . . ?
C1 Rh1 Cl1 157.59(13) . . ?
C1 Rh1 Cl2 102.09(13) . . ?
C2 Rh1 Cl1 159.43(13) . . ?
C2 Rh1 Cl2 102.05(14) . . ?
C2 Rh1 C1 38.30(18) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Rh1A C2A C1A C5A 90.2(3) . . . . ?
Rh1A C2A C6A C4A -9.9(3) . . . . ?
Rh1A C2A C6A C8A -123.9(3) . . . . ?
Rh1A C3A C4A C6A 89.3(3) . . . . ?
Rh1A C3A C5A C1A -9.6(3) . . . . ?
Rh1A C3A C5A C7A -123.3(3) . . . . ?
Rh1A C1A C5A C3A 9.6(3) . . . . ?
Rh1A C1A C5A C7A 124.0(3) . . . . ?
Rh1A C4A C6A C2A 9.9(3) . . . . ?
Rh1A C4A C6A C8A 123.7(3) . . . . ?
C3 C4 C6 C2 60.4(5) . . . . ?
C3 C4 C6 C8 -53.3(5) . . . . ?
C3 C5 C7 C8 -52.5(5) . . . . ?
C2A C1A C5A C3A -63.0(4) . . . . ?
C2A C1A C5A C7A 51.4(5) . . . . ?
C2A C6A C8A C7A 53.4(5) . . . . ?
C4 C3 C5 C1 -61.9(4) . . . . ?
C4 C3 C5 C7 51.5(5) . . . . ?
C4 C6 C8 C7 54.1(5) . . . . ?
C3A C4A C6A C2A -60.7(4) . . . . ?
C3A C4A C6A C8A 53.0(5) . . . . ?
C3A C5A C7A C8A 52.3(5) . . . . ?
C1 C2 C6 C4 -60.9(5) . . . . ?
C1 C2 C6 C8 51.7(5) . . . . ?
C1 C5 C7 C8 53.1(5) . . . . ?
C1A C2A C6A C4A 60.9(4) . . . . ?
C1A C2A C6A C8A -53.1(5) . . . . ?
C1A C5A C7A C8A -53.4(5) . . . . ?
C2 C1 C5 C3 61.2(4) . . . . ?
C2 C1 C5 C7 -51.5(5) . . . . ?
C2 C6 C8 C7 -52.1(5) . . . . ?
C4A C3A C5A C1A 63.3(4) . . . . ?
C4A C3A C5A C7A -50.4(5) . . . . ?
C4A C6A C8A C7A -53.3(5) . . . . ?
C5 C3 C4 C6 0.9(6) . . . . ?
C5 C3 C4 Rh1 90.2(3) . . . . ?
C5 C1 C2 C6 -0.2(5) . . . . ?
C5 C1 C2 Rh1 -89.3(3) . . . . ?
C5 C7 C8 C6 -0.7(6) . . . . ?
C5A C3A C4A Rh1A -90.9(3) . . . . ?
C5A C3A C4A C6A -1.6(5) . . . . ?
C5A C7A C8A C6A 0.3(6) . . . . ?
C6A C2A C1A Rh1A -89.1(3) . . . . ?
C6A C2A C1A C5A 1.1(5) . . . . ?
Rh1 C3 C4 C6 -89.3(4) . . . . ?
Rh1 C3 C5 C1 10.9(3) . . . . ?
Rh1 C3 C5 C7 124.2(3) . . . . ?
Rh1 C4 C6 C2 -11.1(3) . . . . ?
Rh1 C4 C6 C8 -124.8(3) . . . . ?
Rh1 C1 C2 C6 89.1(3) . . . . ?
Rh1 C1 C5 C3 -10.8(3) . . . . ?
Rh1 C1 C5 C7 -123.5(3) . . . . ?
Rh1 C2 C6 C4 11.0(4) . . . . ?
Rh1 C2 C6 C8 123.7(3) . . . . ?

_olex2_diffrn_ambient_temperature_device 
'Rigaku Low-Temperature Gas Spray Cooler low-temperature'
_olex2_submission_special_instructions 'No special instructions were received'
