# Electronic Supplementary Material (ESI) for Chemical Communications.
# This journal is © The Royal Society of Chemistry 2022

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_mo_202015d_0m_a
_audit_block_doi                 10.5517/ccdc.csd.cc24dh35
_database_code_depnum_ccdc_archive 'CCDC 1978206'
loop_
_audit_author_name
_audit_author_address
'Xueli Chen'
;Zhongyuan University of Technology
China
;
_audit_update_record             
;
2020-01-16 deposited with the CCDC.	2022-01-06 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-97
_chemical_name_systematic        
; 
 ? 
;
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C24 H20 Cl6 Cu4 N4 O5'
_chemical_formula_weight         911.30

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_symmetry_cell_setting           ?
_symmetry_space_group_name_H-M   ?

loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z'

_cell_length_a                   12.709(9)
_cell_length_b                   12.889(9)
_cell_length_c                   13.598(8)
_cell_angle_alpha                90.00
_cell_angle_beta                 91.23(2)
_cell_angle_gamma                90.00
_cell_volume                     2227(2)
_cell_formula_units_Z            2
_cell_measurement_temperature    293(2)
_cell_measurement_reflns_used    ?
_cell_measurement_theta_min      ?
_cell_measurement_theta_max      ?

_exptl_crystal_description       ?
_exptl_crystal_colour            ?
_exptl_crystal_size_max          ?
_exptl_crystal_size_mid          ?
_exptl_crystal_size_min          ?
_exptl_crystal_density_meas      ?
_exptl_crystal_density_diffrn    1.359
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             900
_exptl_absorpt_coefficient_mu    2.274
_exptl_absorpt_correction_type   ?
_exptl_absorpt_correction_T_min  ?
_exptl_absorpt_correction_T_max  ?
_exptl_absorpt_process_details   ?

_exptl_special_details           
; 
 ? 
;

_diffrn_ambient_temperature      293(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_monochromator  graphite
_diffrn_measurement_device_type  ?
_diffrn_measurement_method       ?
_diffrn_detector_area_resol_mean ?
_diffrn_standards_number         ?
_diffrn_standards_interval_count ?
_diffrn_standards_interval_time  ?
_diffrn_standards_decay_%        ?
_diffrn_reflns_number            49719
_diffrn_reflns_av_R_equivalents  0.0275
_diffrn_reflns_av_sigmaI/netI    0.0251
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_k_min       -15
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_l_min       -16
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_theta_min         2.18
_diffrn_reflns_theta_max         25.50
_reflns_number_total             8286
_reflns_number_gt                7831
_reflns_threshold_expression     >2sigma(I)

_computing_data_collection       ?
_computing_cell_refinement       ?
_computing_data_reduction        ?
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_molecular_graphics    ?
_computing_publication_material  ?

_refine_special_details          
; 
 Refinement of F² against ALL reflections.  The weighted R-factor wR and 
 goodness of fit S are based on F², conventional R-factors R are based 
 on F, with F set to zero for negative F². The threshold expression of 
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is 
 not relevant to the choice of reflections for refinement.  R-factors based 
 on F² are statistically about twice as large as those based on F, and R- 
 factors based on ALL data will be even larger. 
;

_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'calc w=1/[σ²(Fo²)+(0.1760P)²+1.8224P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    mixed
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       ?
_refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881'
_refine_ls_abs_structure_Flack   0.03(2)
_refine_ls_number_reflns         8286
_refine_ls_number_parameters     388
_refine_ls_number_restraints     602
_refine_ls_R_factor_all          0.0699
_refine_ls_R_factor_gt           0.0674
_refine_ls_wR_factor_ref         0.2245
_refine_ls_wR_factor_gt          0.2186
_refine_ls_goodness_of_fit_ref   1.109
_refine_ls_restrained_S_all      1.134
_refine_ls_shift/su_max          0.097
_refine_ls_shift/su_mean         0.003

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Cu1 Cu 0.33168(7) 0.34613(7) 0.34242(7) 0.0440(2) Uani 1 1 d U . .
Cu2 Cu 0.34672(7) 0.48377(7) 0.15246(7) 0.0453(3) Uani 1 1 d U . .
Cu3 Cu 0.16338(7) 0.32647(7) 0.17461(7) 0.0448(3) Uani 1 1 d U . .
Cu4 Cu 0.17116(7) 0.52486(7) 0.30454(7) 0.0446(2) Uani 1 1 d U . .
Cl1 Cl 0.24690(19) 0.46301(18) 0.45529(15) 0.0601(5) Uani 1 1 d U . .
Cl2 Cl 0.02408(16) 0.4399(2) 0.22798(19) 0.0614(6) Uani 1 1 d U . .
Cl3 Cl 0.26871(18) 0.36648(19) 0.03495(15) 0.0584(5) Uani 1 1 d U . .
Cl4 Cl 0.48432(15) 0.4047(2) 0.25645(17) 0.0599(5) Uani 1 1 d U . .
Cl5 Cl 0.22680(19) 0.20043(16) 0.29445(19) 0.0604(5) Uani 1 1 d U . .
Cl6A Cl 0.2674(2) 0.64190(16) 0.19901(19) 0.0653(6) Uani 1 1 d U . .
O1 O 0.2537(3) 0.4200(4) 0.2438(4) 0.0384(9) Uani 1 1 d U . .
O2 O 0.2764(8) 0.8755(8) 0.4584(8) 0.095(2) Uani 1 1 d DU . .
O3 O 0.2785(10) 0.1878(14) 0.7010(10) 0.131(4) Uani 1 1 d DU . .
O4 O 0.7160(11) 0.3874(13) -0.0031(11) 0.139(4) Uani 1 1 d DU . .
O5A O -0.0939(15) 0.0183(19) 0.2704(14) 0.184(6) Uani 1 1 d U . .
N1 N 0.4409(6) 0.5460(7) 0.0546(6) 0.0608(16) Uani 1 1 d U . .
N2 N 0.4123(6) 0.2664(6) 0.4442(6) 0.0562(15) Uani 1 1 d U . .
N4 N 0.0671(7) 0.2278(7) 0.1049(7) 0.0653(17) Uani 1 1 d U . .
N3C N 0.0950(6) 0.6359(6) 0.3752(6) 0.0582(15) Uani 1 1 d U . .
C1 C 0.4164(11) 0.6321(10) 0.0034(9) 0.080(2) Uani 1 1 d U . .
H1 H 0.3527 0.6659 0.0128 0.096 Uiso 1 1 calc R . .
C8 C 0.5577(10) 0.1572(11) 0.4834(11) 0.086(3) Uani 1 1 d U . .
H8 H 0.6179 0.1220 0.4644 0.103 Uiso 1 1 calc R . .
C12 C 0.3739(13) 0.1796(14) 0.7076(12) 0.104(3) Uani 1 1 d DU . .
H12 H 0.4102 0.1648 0.7660 0.125 Uiso 1 1 calc R . .
C13 C 0.1504(8) 0.7218(8) 0.4026(8) 0.0647(19) Uani 1 1 d U . .
H13 H 0.2174 0.7314 0.3780 0.078 Uiso 1 1 calc R . .
C17 C 0.0008(9) 0.6223(10) 0.4120(9) 0.074(2) Uani 1 1 d U . .
H17 H -0.0340 0.5605 0.3980 0.088 Uiso 1 1 calc R . .
C19 C 0.0035(9) 0.1724(10) 0.1554(10) 0.080(2) Uani 1 1 d U . .
H19 H 0.0051 0.1813 0.2233 0.096 Uiso 1 1 calc R . .
C21 C -0.0748(12) 0.0961(13) 0.0088(12) 0.099(3) Uani 1 1 d U . .
H21 H -0.1259 0.0582 -0.0255 0.119 Uiso 1 1 calc R . .
C23 C 0.0655(10) 0.2161(11) 0.0097(10) 0.084(3) Uani 1 1 d U . .
H23 H 0.1125 0.2534 -0.0281 0.101 Uiso 1 1 calc R . .
C24 C -0.1310(15) 0.0335(18) 0.1840(16) 0.122(4) Uani 1 1 d U . .
H24 H -0.1951 0.0048 0.1641 0.147 Uiso 1 1 calc R . .
C22B C -0.0043(12) 0.1499(13) -0.0356(11) 0.099(3) Uani 1 1 d U . .
H22B H -0.0008 0.1430 -0.1035 0.118 Uiso 1 1 calc R . .
C20K C -0.0692(11) 0.0984(12) 0.1156(12) 0.092(3) Uani 1 1 d U . .
C7M C 0.5030(9) 0.2173(10) 0.4202(10) 0.075(2) Uani 1 1 d U . .
H7M H 0.5283 0.2259 0.3571 0.090 Uiso 1 1 calc R . .
C9N C 0.5182(9) 0.1492(11) 0.5850(10) 0.080(2) Uani 1 1 d U . .
H9N H 0.5548 0.1116 0.6331 0.096 Uiso 1 1 calc R . .
C4O C 0.6021(11) 0.5339(13) -0.0315(10) 0.090(2) Uani 1 1 d U . .
C14P C 0.1118(9) 0.7931(10) 0.4639(9) 0.074(2) Uani 1 1 d U . .
C10Q C 0.4294(10) 0.1971(10) 0.6050(9) 0.079(2) Uani 1 1 d U . .
C5R C 0.5311(9) 0.4969(10) 0.0335(9) 0.077(2) Uani 1 1 d U . .
H5R H 0.5458 0.4343 0.0650 0.092 Uiso 1 1 calc R . .
C3T C 0.5766(12) 0.6241(13) -0.0786(11) 0.096(3) Uani 1 1 d U . .
H3T H 0.6229 0.6541 -0.1224 0.115 Uiso 1 1 calc R . .
C15U C 0.0161(11) 0.7826(11) 0.5000(11) 0.087(2) Uani 1 1 d U . .
H15U H -0.0100 0.8311 0.5439 0.105 Uiso 1 1 calc R . .
C2V C 0.4851(13) 0.6683(13) -0.0612(12) 0.097(3) Uani 1 1 d U . .
H2V H 0.4674 0.7282 -0.0959 0.117 Uiso 1 1 calc R . .
C6W C 0.7047(14) 0.4678(15) -0.0449(14) 0.119(4) Uani 1 1 d DU . .
H6W H 0.7570 0.4918 -0.0859 0.143 Uiso 1 1 calc R . .
C16X C -0.0480(10) 0.6922(12) 0.4686(11) 0.086(3) Uani 1 1 d U . .
H16X H -0.1176 0.6842 0.4869 0.104 Uiso 1 1 calc R . .
C18Y C 0.1853(10) 0.8946(10) 0.4830(10) 0.085(3) Uani 1 1 d DU . .
H18Y H 0.1624 0.9574 0.5085 0.102 Uiso 1 1 calc R . .
C11Z C 0.3708(9) 0.2520(9) 0.5346(7) 0.066(2) Uani 1 1 d U . .
H11Z H 0.3048 0.2782 0.5492 0.080 Uiso 1 1 calc R . .


_geom_special_details            
; 
 All esds (except the esd in the dihedral angle between two l.s. planes) 
 are estimated using the full covariance matrix.  The cell esds are taken 
 into account individually in the estimation of esds in distances, angles 
 and torsion angles; correlations between esds in cell parameters are only 
 used when they are defined by crystal symmetry.  An approximate (isotropic) 
 treatment of cell esds is used for estimating esds involving l.s. planes. 
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Cu1 O1 1.905(5) . ?
Cu1 N2 1.990(7) . ?
Cu1 Cl5 2.386(3) . ?
Cu1 Cl4 2.408(3) . ?
Cu1 Cl1 2.420(2) . ?
Cu2 O1 1.918(5) . ?
Cu2 N1 1.979(7) . ?
Cu2 Cl6A 2.366(3) . ?
Cu2 Cl3 2.399(2) . ?
Cu2 Cl4 2.448(3) . ?
Cu3 O1 1.900(5) . ?
Cu3 N4 1.991(8) . ?
Cu3 Cl3 2.403(3) . ?
Cu3 Cl2 2.419(3) . ?
Cu3 Cl5 2.427(2) . ?
Cu4 O1 1.910(5) . ?
Cu4 N3C 1.987(8) . ?
Cu4 Cl1 2.383(3) . ?
Cu4 Cl2 2.386(3) . ?
Cu4 Cl6A 2.430(3) . ?
O2 C18Y 1.236(13) . ?
O3 C12 1.218(14) . ?
O4 C6W 1.189(16) . ?
O5A C24 1.27(2) . ?
N1 C1 1.343(15) . ?
N1 C5R 1.345(15) . ?
N2 C11Z 1.361(14) . ?
N2 C7M 1.361(14) . ?
N4 C23 1.303(16) . ?
N4 C19 1.288(16) . ?
N3C C17 1.319(14) . ?
N3C C13 1.360(13) . ?
C1 C2V 1.336(18) . ?
C1 H1 0.9300 . ?
C8 C7M 1.340(16) . ?
C8 C9N 1.484(19) . ?
C8 H8 0.9300 . ?
C12 C10Q 1.59(2) . ?
C12 H12 0.9300 . ?
C13 C14P 1.340(15) . ?
C13 H13 0.9300 . ?
C17 C16X 1.345(17) . ?
C17 H17 0.9300 . ?
C19 C20K 1.425(17) . ?
C19 H19 0.9300 . ?
C21 C22B 1.29(2) . ?
C21 C20K 1.45(2) . ?
C21 H21 0.9300 . ?
C23 C22B 1.368(17) . ?
C23 H23 0.9300 . ?
C24 C20K 1.49(2) . ?
C24 H24 0.9300 . ?
C22B H22B 0.9300 . ?
C7M H7M 0.9300 . ?
C9N C10Q 1.320(18) . ?
C9N H9N 0.9300 . ?
C4O C5R 1.363(16) . ?
C4O C3T 1.36(2) . ?
C4O C6W 1.57(2) . ?
C14P C15U 1.328(18) . ?
C14P C18Y 1.625(18) . ?
C10Q C11Z 1.392(14) . ?
C5R H5R 0.9300 . ?
C3T C2V 1.32(2) . ?
C3T H3T 0.9300 . ?
C15U C16X 1.48(2) . ?
C15U H15U 0.9300 . ?
C2V H2V 0.9300 . ?
C6W H6W 0.9300 . ?
C16X H16X 0.9300 . ?
C18Y H18Y 0.9300 . ?
C11Z H11Z 0.9300 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O1 Cu1 N2 178.9(3) . . ?
O1 Cu1 Cl5 85.51(17) . . ?
N2 Cu1 Cl5 93.4(2) . . ?
O1 Cu1 Cl4 85.07(16) . . ?
N2 Cu1 Cl4 95.2(2) . . ?
Cl5 Cu1 Cl4 124.41(10) . . ?
O1 Cu1 Cl1 84.46(17) . . ?
N2 Cu1 Cl1 96.3(3) . . ?
Cl5 Cu1 Cl1 114.18(10) . . ?
Cl4 Cu1 Cl1 119.16(10) . . ?
O1 Cu2 N1 177.9(3) . . ?
O1 Cu2 Cl6A 85.65(18) . . ?
N1 Cu2 Cl6A 95.6(3) . . ?
O1 Cu2 Cl3 84.81(17) . . ?
N1 Cu2 Cl3 93.1(3) . . ?
Cl6A Cu2 Cl3 123.29(11) . . ?
O1 Cu2 Cl4 83.68(15) . . ?
N1 Cu2 Cl4 97.0(3) . . ?
Cl6A Cu2 Cl4 120.49(11) . . ?
Cl3 Cu2 Cl4 113.72(10) . . ?
O1 Cu3 N4 178.7(3) . . ?
O1 Cu3 Cl3 85.09(16) . . ?
N4 Cu3 Cl3 96.2(3) . . ?
O1 Cu3 Cl2 84.63(16) . . ?
N4 Cu3 Cl2 94.7(3) . . ?
Cl3 Cu3 Cl2 122.08(10) . . ?
O1 Cu3 Cl5 84.47(17) . . ?
N4 Cu3 Cl5 94.8(3) . . ?
Cl3 Cu3 Cl5 119.45(10) . . ?
Cl2 Cu3 Cl5 115.96(11) . . ?
O1 Cu4 N3C 175.4(3) . . ?
O1 Cu4 Cl1 85.40(16) . . ?
N3C Cu4 Cl1 91.0(3) . . ?
O1 Cu4 Cl2 85.35(16) . . ?
N3C Cu4 Cl2 99.0(2) . . ?
Cl1 Cu4 Cl2 121.33(10) . . ?
O1 Cu4 Cl6A 84.02(17) . . ?
N3C Cu4 Cl6A 95.4(3) . . ?
Cl1 Cu4 Cl6A 121.08(10) . . ?
Cl2 Cu4 Cl6A 115.27(11) . . ?
Cu4 Cl1 Cu1 80.78(8) . . ?
Cu4 Cl2 Cu3 80.61(8) . . ?
Cu2 Cl3 Cu3 80.68(8) . . ?
Cu1 Cl4 Cu2 80.67(8) . . ?
Cu1 Cl5 Cu3 80.34(8) . . ?
Cu2 Cl6A Cu4 81.14(8) . . ?
Cu3 O1 Cu1 109.4(3) . . ?
Cu3 O1 Cu4 109.4(2) . . ?
Cu1 O1 Cu4 109.4(2) . . ?
Cu3 O1 Cu2 109.0(2) . . ?
Cu1 O1 Cu2 110.6(2) . . ?
Cu4 O1 Cu2 109.2(3) . . ?
C1 N1 C5R 117.9(9) . . ?
C1 N1 Cu2 123.1(8) . . ?
C5R N1 Cu2 118.9(7) . . ?
C11Z N2 C7M 119.9(8) . . ?
C11Z N2 Cu1 119.7(6) . . ?
C7M N2 Cu1 120.0(7) . . ?
C23 N4 C19 118.0(10) . . ?
C23 N4 Cu3 122.9(8) . . ?
C19 N4 Cu3 119.1(8) . . ?
C17 N3C C13 118.2(9) . . ?
C17 N3C Cu4 122.9(8) . . ?
C13 N3C Cu4 117.6(6) . . ?
C2V C1 N1 118.8(13) . . ?
C2V C1 H1 120.6 . . ?
N1 C1 H1 120.6 . . ?
C7M C8 C9N 117.1(11) . . ?
C7M C8 H8 121.4 . . ?
C9N C8 H8 121.4 . . ?
O3 C12 C10Q 112.5(13) . . ?
O3 C12 H12 123.8 . . ?
C10Q C12 H12 123.8 . . ?
C14P C13 N3C 122.3(11) . . ?
C14P C13 H13 118.9 . . ?
N3C C13 H13 118.9 . . ?
N3C C17 C16X 124.1(13) . . ?
N3C C17 H17 117.9 . . ?
C16X C17 H17 117.9 . . ?
N4 C19 C20K 125.3(13) . . ?
N4 C19 H19 117.4 . . ?
C20K C19 H19 117.4 . . ?
C22B C21 C20K 115.8(12) . . ?
C22B C21 H21 122.1 . . ?
C20K C21 H21 122.1 . . ?
N4 C23 C22B 121.0(14) . . ?
N4 C23 H23 119.5 . . ?
C22B C23 H23 119.5 . . ?
O5A C24 C20K 118.3(17) . . ?
O5A C24 H24 120.8 . . ?
C20K C24 H24 120.9 . . ?
C21 C22B C23 125.0(15) . . ?
C21 C22B H22B 117.5 . . ?
C23 C22B H22B 117.5 . . ?
C19 C20K C21 114.3(13) . . ?
C19 C20K C24 119.0(15) . . ?
C21 C20K C24 126.7(14) . . ?
C8 C7M N2 123.1(12) . . ?
C8 C7M H7M 118.5 . . ?
N2 C7M H7M 118.5 . . ?
C10Q C9N C8 117.8(10) . . ?
C10Q C9N H9N 121.1 . . ?
C8 C9N H9N 121.1 . . ?
C5R C4O C3T 116.7(13) . . ?
C5R C4O C6W 116.6(13) . . ?
C3T C4O C6W 126.7(12) . . ?
C15U C14P C13 120.7(12) . . ?
C15U C14P C18Y 123.4(11) . . ?
C13 C14P C18Y 115.7(11) . . ?
C9N C10Q C11Z 122.9(12) . . ?
C9N C10Q C12 120.7(11) . . ?
C11Z C10Q C12 115.7(11) . . ?
C4O C5R N1 123.5(12) . . ?
C4O C5R H5R 118.2 . . ?
N1 C5R H5R 118.2 . . ?
C2V C3T C4O 119.0(12) . . ?
C2V C3T H3T 120.5 . . ?
C4O C3T H3T 120.5 . . ?
C14P C15U C16X 118.4(11) . . ?
C14P C15U H15U 120.8 . . ?
C16X C15U H15U 120.8 . . ?
C1 C2V C3T 123.9(14) . . ?
C1 C2V H2V 118.1 . . ?
C3T C2V H2V 118.1 . . ?
O4 C6W C4O 120.6(15) . . ?
O4 C6W H6W 119.7 . . ?
C4O C6W H6W 119.7 . . ?
C17 C16X C15U 115.8(12) . . ?
C17 C16X H16X 122.1 . . ?
C15U C16X H16X 122.1 . . ?
O2 C18Y C14P 109.6(10) . . ?
O2 C18Y H18Y 125.2 . . ?
C14P C18Y H18Y 125.2 . . ?
N2 C11Z C10Q 118.6(10) . . ?
N2 C11Z H11Z 120.7 . . ?
C10Q C11Z H11Z 120.7 . . ?

_diffrn_measured_fraction_theta_max 0.999
_diffrn_reflns_theta_full        25.50
_diffrn_measured_fraction_theta_full 0.999
_refine_diff_density_max         2.646
_refine_diff_density_min         -0.596
_refine_diff_density_rms         0.204
