# Electronic Supplementary Material (ESI) for CrystEngComm.
# This journal is © The Royal Society of Chemistry 2021

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_P
_database_code_depnum_ccdc_archive 'CCDC 2102323'
loop_
_audit_author_name
_audit_author_address
'Kuan-Guan Liu'
;Ningxia University
China
;
_audit_update_record             
;
2021-08-10 deposited with the CCDC.	2021-10-11 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2018/3
_shelx_SHELXL_version_number     2018/3
_chemical_name_systematic        ?
_chemical_name_common            (TeO6)Ag36(CCtBu)18(tfa)8(F5PhCO2)4
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C152 H162 Ag36 F44 O30 Te'
_chemical_formula_weight         7315.73

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Te Te -0.5308 1.6751 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   17.5326(11)
_cell_length_b                   18.5686(11)
_cell_length_c                   19.6507(11)
_cell_angle_alpha                65.240(2)
_cell_angle_beta                 66.895(2)
_cell_angle_gamma                69.537(2)
_cell_volume                     5210.2(5)
_cell_formula_units_Z            1
_cell_measurement_temperature    100(2)
_cell_measurement_reflns_used    9183
_cell_measurement_theta_min      2.65
_cell_measurement_theta_max      30.51

_exptl_crystal_description       block
_exptl_crystal_colour            yellow
_exptl_crystal_density_meas      'not measured'
_exptl_crystal_density_method    'not measured'
_exptl_crystal_density_diffrn    2.332
_exptl_crystal_F_000             3454
_exptl_transmission_factor_min   0.513
_exptl_transmission_factor_max   0.754
_exptl_crystal_size_max          0.240
_exptl_crystal_size_mid          0.160
_exptl_crystal_size_min          0.080
_exptl_absorpt_coefficient_mu    3.524
_shelx_estimated_absorpt_T_min   0.485
_shelx_estimated_absorpt_T_max   0.766
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_correction_T_min  ?
_exptl_absorpt_correction_T_max  ?
_exptl_absorpt_process_details   
;
CrysAlisPro 1.171.39.33c (Rigaku Oxford Diffraction, 2017)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      100(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_source                   'fine-focus sealed tube'
_diffrn_measurement_device_type  'Bruker APEX-III CMOS'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            106968
_diffrn_reflns_av_unetI/netI     0.0293
_diffrn_reflns_av_R_equivalents  0.0280
_diffrn_reflns_limit_h_min       -24
_diffrn_reflns_limit_h_max       25
_diffrn_reflns_limit_k_min       -26
_diffrn_reflns_limit_k_max       26
_diffrn_reflns_limit_l_min       -28
_diffrn_reflns_limit_l_max       27
_diffrn_reflns_theta_min         2.528
_diffrn_reflns_theta_max         30.525
_diffrn_reflns_theta_full        25.242
_diffrn_measured_fraction_theta_max 0.984
_diffrn_measured_fraction_theta_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.984
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.984
_diffrn_reflns_point_group_measured_fraction_full 0.999
_reflns_number_total             31325
_reflns_number_gt                26520
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       'Bruker APEX3'
_computing_cell_refinement       'Bruker SAINT'
_computing_data_reduction        'Bruker SAINT'
_computing_structure_solution    'SHELXS-97 (Sheldrick 2008)'
_computing_structure_refinement  'SHELXL-2018/3 (Sheldrick, 2018)'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_refine_special_details          
;
;

_exptl_special_details           
;
;

loop_
_platon_squeeze_void_nr
_platon_squeeze_void_average_x
_platon_squeeze_void_average_y
_platon_squeeze_void_average_z
_platon_squeeze_void_volume
_platon_squeeze_void_count_electrons
_platon_squeeze_void_content
1 0.000 0.500 0.000 786 80 ' '
2 0.143 -0.001 0.171 17 1 ' '
3 0.857 0.001 0.829 18 1 ' '
_platon_squeeze_details          
;
;


_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0520P)²+43.2558P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_number_reflns         31325
_refine_ls_number_parameters     1223
_refine_ls_number_restraints     1175
_refine_ls_R_factor_all          0.0578
_refine_ls_R_factor_gt           0.0483
_refine_ls_wR_factor_ref         0.1281
_refine_ls_wR_factor_gt          0.1227
_refine_ls_goodness_of_fit_ref   1.042
_refine_ls_restrained_S_all      1.059
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.66956(4) -0.27293(3) 0.71100(3) 0.04090(11) Uani 1 1 d . . . . .
Ag2 Ag 0.51893(3) -0.13884(2) 0.67385(2) 0.02391(8) Uani 1 1 d . . . . .
Ag3 Ag 0.56012(3) 0.17251(2) 0.46895(2) 0.02588(8) Uani 1 1 d . . . . .
Ag4 Ag 0.35500(2) 0.00439(2) 0.67675(2) 0.02362(8) Uani 1 1 d . . . . .
Ag5 Ag 0.53774(3) 0.03367(2) 0.64580(2) 0.02445(8) Uani 1 1 d . . . . .
Ag6 Ag 0.66701(3) 0.18812(2) 0.30994(2) 0.02847(8) Uani 1 1 d . . . . .
Ag7 Ag 0.28998(2) 0.02280(2) 0.54718(3) 0.02529(8) Uani 1 1 d . . . . .
Ag8 Ag 0.19684(3) 0.16500(3) 0.60037(3) 0.03137(9) Uani 1 1 d . . . . .
Ag9 Ag 0.56236(3) -0.16879(3) 0.81334(3) 0.03355(10) Uani 1 1 d . . . . .
Ag10 Ag 0.36467(3) 0.17343(2) 0.50192(3) 0.03202(9) Uani 1 1 d . . . . .
Ag11 Ag 0.33999(3) -0.13951(3) 0.81598(3) 0.03315(9) Uani 1 1 d . . . . .
Ag12 Ag 0.31892(4) 0.17032(3) 0.66802(3) 0.03860(11) Uani 1 1 d . . . . .
Ag13 Ag 0.53442(3) -0.29764(3) 0.65738(3) 0.03595(10) Uani 1 1 d . . . . .
Ag14 Ag 0.25666(3) 0.31993(3) 0.43323(3) 0.04146(11) Uani 1 1 d . . . . .
Ag15 Ag 0.17241(3) -0.00124(3) 0.70939(3) 0.03489(10) Uani 1 1 d . . . . .
Ag16 Ag 0.68779(3) -0.09426(3) 0.66737(3) 0.03686(10) Uani 1 1 d . . . . .
Ag17 Ag 0.42984(3) -0.01645(3) 0.79866(3) 0.03299(9) Uani 1 1 d . . . . .
Ag18 Ag 0.18931(3) 0.16323(3) 0.45677(3) 0.03641(10) Uani 1 1 d . . . . .
Te1 Te 0.500000 0.000000 0.500000 0.01487(7) Uani 1 2 d S . P . .
O1 O 0.4176(2) 0.07824(19) 0.4455(2) 0.0189(6) Uani 1 1 d . . . . .
O2 O 0.4837(2) 0.0765(2) 0.5495(2) 0.0184(6) Uani 1 1 d . . . . .
O3 O 0.5902(2) 0.0474(2) 0.41442(19) 0.0187(6) Uani 1 1 d . . . . .
O11 O 0.3255(2) -0.0630(2) 0.4714(2) 0.0264(8) Uani 1 1 d . . . . .
C11 C 0.7307(4) 0.0673(4) 0.5517(4) 0.0334(11) Uani 1 1 d . U . . .
O12 O 0.7654(3) 0.0122(3) 0.6003(3) 0.0428(11) Uani 1 1 d . . . . .
C12 C 0.7555(4) 0.1485(4) 0.5161(4) 0.0376(11) Uani 1 1 d . U . . .
C13 C 0.7859(4) 0.1824(4) 0.4360(5) 0.0425(12) Uani 1 1 d . U . . .
C14 C 0.8054(5) 0.2583(5) 0.4019(5) 0.0519(15) Uani 1 1 d . U . . .
C15 C 0.7955(5) 0.3011(5) 0.4467(6) 0.0537(16) Uani 1 1 d . U . . .
C16 C 0.7671(5) 0.2696(5) 0.5265(6) 0.0521(15) Uani 1 1 d . U . . .
C17 C 0.7470(4) 0.1923(5) 0.5608(5) 0.0452(13) Uani 1 1 d . U . . .
O21 O 0.3156(3) -0.1510(3) 0.9426(3) 0.0449(11) Uani 1 1 d . . . . .
C21 C 0.3708(5) -0.1454(5) 0.9638(4) 0.0446(14) Uani 1 1 d . U . . .
O22 O 0.4301(3) -0.1083(3) 0.9223(3) 0.0448(11) Uani 1 1 d . . . . .
C22 C 0.3682(6) -0.1904(5) 1.0506(4) 0.0509(14) Uani 1 1 d . U . . .
C23 C 0.2986(6) -0.1803(6) 1.1077(5) 0.0562(16) Uani 1 1 d . U . . .
C24 C 0.2967(6) -0.2239(6) 1.1856(5) 0.0612(17) Uani 1 1 d . U . . .
C25 C 0.3664(7) -0.2802(6) 1.2032(5) 0.0608(17) Uani 1 1 d . U . . .
C26 C 0.4391(7) -0.2905(6) 1.1452(5) 0.065(2) Uani 1 1 d . U . . .
C27 C 0.4362(6) -0.2436(6) 1.0685(5) 0.0623(19) Uani 1 1 d . U . . .
O31 O 0.6465(4) -0.2605(3) 0.8882(4) 0.0581(15) Uani 1 1 d . . . . .
C31 C 0.6677(5) -0.3320(4) 0.8899(5) 0.0450(16) Uani 1 1 d . U . . .
O32 O 0.6712(3) -0.3588(3) 0.8418(3) 0.0464(12) Uani 1 1 d . . . . .
C32 C 0.6923(6) -0.3959(5) 0.9637(5) 0.058(2) Uani 1 1 d . U . . .
O41 O 0.0612(3) 0.0845(3) 0.7716(3) 0.0498(13) Uani 1 1 d . . . . .
C41 C 0.0562(5) 0.1583(5) 0.7547(5) 0.0496(18) Uani 1 1 d . U . . .
O42 O 0.1044(4) 0.2016(4) 0.7051(3) 0.0553(14) Uani 1 1 d . . . . .
C42 C -0.0275(6) 0.2002(6) 0.8055(5) 0.065(2) Uani 1 1 d . U . . .
O51 O 0.0816(3) 0.2543(3) 0.5224(3) 0.0485(12) Uani 1 1 d . . . . .
C51 C 0.0678(5) 0.3282(5) 0.5032(6) 0.0532(17) Uani 1 1 d . U . . .
O52 O 0.1158(4) 0.3750(3) 0.4636(4) 0.0567(15) Uani 1 1 d . . . . .
C52 C -0.0265(7) 0.3657(6) 0.5413(7) 0.089(3) Uani 1 1 d D U . . .
O61 O 0.5341(4) 0.1892(4) 0.5979(4) 0.0644(17) Uani 1 1 d . . . . .
C61 C 0.4844(5) 0.2202(4) 0.6461(4) 0.0410(14) Uani 1 1 d . U . . .
O62 O 0.4130(5) 0.2089(6) 0.6906(4) 0.086(2) Uani 1 1 d . . . . .
C62 C 0.5121(6) 0.2762(5) 0.6666(5) 0.0556(19) Uani 1 1 d . U . . .
C101 C 0.4814(4) -0.2219(3) 0.7853(3) 0.0295(10) Uani 1 1 d . U . . .
C102 C 0.4544(4) -0.2817(3) 0.8340(3) 0.0315(11) Uani 1 1 d . U . . .
C103 C 0.4248(4) -0.3571(4) 0.8906(4) 0.0368(13) Uani 1 1 d . U . . .
C104 C 0.3459(5) -0.3584(5) 0.8767(5) 0.0559(19) Uani 1 1 d . U . . .
H10A H 0.298163 -0.316355 0.893474 0.084 Uiso 1 1 calc R U . . .
H10B H 0.331870 -0.411830 0.906773 0.084 Uiso 1 1 calc R U . . .
H10C H 0.356799 -0.347736 0.820814 0.084 Uiso 1 1 calc R U . . .
C105 C 0.4966(5) -0.4305(4) 0.8760(5) 0.0489(17) Uani 1 1 d . U . . .
H10D H 0.508577 -0.429492 0.822566 0.073 Uiso 1 1 calc R U . . .
H10E H 0.478962 -0.480928 0.913440 0.073 Uiso 1 1 calc R U . . .
H10F H 0.547890 -0.427790 0.882750 0.073 Uiso 1 1 calc R U . . .
C106 C 0.4062(6) -0.3594(5) 0.9742(4) 0.059(2) Uani 1 1 d . U . . .
H10G H 0.458496 -0.360366 0.982032 0.089 Uiso 1 1 calc R U . . .
H10H H 0.385195 -0.408225 1.011419 0.089 Uiso 1 1 calc R U . . .
H10I H 0.363061 -0.310923 0.982738 0.089 Uiso 1 1 calc R U . . .
C111 C 0.1578(3) 0.0697(3) 0.5823(3) 0.0274(10) Uani 1 1 d . U . . .
C112 C 0.0854(4) 0.0678(3) 0.5930(3) 0.0289(10) Uani 1 1 d . U . . .
C113 C -0.0028(4) 0.0660(4) 0.6039(4) 0.0382(12) Uani 1 1 d . U . . .
C114 C -0.0103(5) -0.0232(5) 0.6391(6) 0.0554(18) Uani 1 1 d . U . . .
H11A H 0.036137 -0.054687 0.607759 0.083 Uiso 1 1 calc R U . . .
H11B H -0.064960 -0.026249 0.639089 0.083 Uiso 1 1 calc R U . . .
H11C H -0.006887 -0.045483 0.692983 0.083 Uiso 1 1 calc R U . . .
C115 C -0.0658(4) 0.1142(6) 0.6577(5) 0.0513(17) Uani 1 1 d . U . . .
H11D H -0.054615 0.089975 0.708739 0.077 Uiso 1 1 calc R U . . .
H11E H -0.123862 0.113105 0.664589 0.077 Uiso 1 1 calc R U . . .
H11F H -0.059364 0.170677 0.634400 0.077 Uiso 1 1 calc R U . . .
C116 C -0.0153(5) 0.1040(6) 0.5216(5) 0.0529(18) Uani 1 1 d . U . . .
H11G H -0.008371 0.160215 0.498885 0.079 Uiso 1 1 calc R U . . .
H11H H -0.072449 0.103274 0.525406 0.079 Uiso 1 1 calc R U . . .
H11I H 0.027141 0.072503 0.488125 0.079 Uiso 1 1 calc R U . . .
C121 C 0.7645(4) 0.1328(3) 0.2315(3) 0.0298(11) Uani 1 1 d . . . . .
C122 C 0.1748(4) -0.1242(4) 0.8248(4) 0.0394(13) Uani 1 1 d . U . . .
C123 C 0.1023(5) -0.1281(5) 0.8986(4) 0.0547(19) Uani 1 1 d . U . . .
C124 C 0.1165(7) -0.2132(6) 0.9569(5) 0.067(2) Uani 1 1 d . U . . .
H12A H 0.120213 -0.252782 0.934190 0.100 Uiso 1 1 calc R U . . .
H12B H 0.068861 -0.216892 1.004926 0.100 Uiso 1 1 calc R U . . .
H12C H 0.169528 -0.224993 0.969154 0.100 Uiso 1 1 calc R U . . .
C125 C 0.0190(6) -0.1068(7) 0.8775(6) 0.070(3) Uani 1 1 d . U . . .
H12D H 0.008928 -0.050026 0.843527 0.105 Uiso 1 1 calc R U . . .
H12E H -0.028690 -0.114271 0.925545 0.105 Uiso 1 1 calc R U . . .
H12F H 0.023883 -0.142538 0.850157 0.105 Uiso 1 1 calc R U . . .
C126 C 0.0996(6) -0.0652(5) 0.9332(5) 0.059(2) Uani 1 1 d . U . . .
H12G H 0.154170 -0.076689 0.942721 0.088 Uiso 1 1 calc R U . . .
H12H H 0.053922 -0.069090 0.982540 0.088 Uiso 1 1 calc R U . . .
H12I H 0.089042 -0.010184 0.895935 0.088 Uiso 1 1 calc R U . . .
C131 C 0.3038(4) 0.0495(4) 0.7690(4) 0.0344(12) Uani 1 1 d . U . . .
C132 C 0.2764(5) 0.0782(4) 0.8221(4) 0.0419(14) Uani 1 1 d . U . . .
C133 C 0.2393(5) 0.1141(5) 0.8862(5) 0.0508(16) Uani 1 1 d . U . . .
C134 C 0.2375(7) 0.0454(6) 0.9660(5) 0.064(2) Uani 1 1 d . U . . .
H13A H 0.203334 0.008925 0.974136 0.096 Uiso 1 1 calc R U . . .
H13B H 0.212281 0.069292 1.008159 0.096 Uiso 1 1 calc R U . . .
H13C H 0.295589 0.014587 0.966312 0.096 Uiso 1 1 calc R U . . .
C135 C 0.1471(6) 0.1581(6) 0.8888(6) 0.066(2) Uani 1 1 d . U . . .
H13D H 0.145221 0.200402 0.838192 0.099 Uiso 1 1 calc R U . . .
H13E H 0.122394 0.183022 0.930102 0.099 Uiso 1 1 calc R U . . .
H13F H 0.114537 0.119041 0.899694 0.099 Uiso 1 1 calc R U . . .
C136 C 0.2904(7) 0.1703(7) 0.8759(6) 0.067(2) Uani 1 1 d . U . . .
H13G H 0.346236 0.138581 0.883195 0.101 Uiso 1 1 calc R U . . .
H13H H 0.260419 0.198510 0.914716 0.101 Uiso 1 1 calc R U . . .
H13I H 0.297956 0.210251 0.823142 0.101 Uiso 1 1 calc R U . . .
C141 C 0.2805(5) 0.2602(4) 0.5565(4) 0.0406(13) Uani 1 1 d . U . . .
C142 C 0.2509(5) 0.3159(4) 0.5835(5) 0.0489(15) Uani 1 1 d . U . . .
C143 C 0.2080(6) 0.3857(5) 0.6137(5) 0.0655(19) Uani 1 1 d D U . . .
C144 C 0.2247(10) 0.3648(9) 0.6886(8) 0.122(4) Uani 1 1 d D U . . .
H14A H 0.201181 0.317714 0.726974 0.183 Uiso 1 1 calc R U . . .
H14B H 0.197795 0.411236 0.707989 0.183 Uiso 1 1 calc R U . . .
H14C H 0.286169 0.351749 0.680359 0.183 Uiso 1 1 calc R U . . .
C145 C 0.1126(8) 0.4034(8) 0.6289(8) 0.115(4) Uani 1 1 d D U . . .
H14D H 0.100323 0.410928 0.581498 0.172 Uiso 1 1 calc R U . . .
H14E H 0.085701 0.453046 0.643260 0.172 Uiso 1 1 calc R U . . .
H14F H 0.089997 0.357735 0.671782 0.172 Uiso 1 1 calc R U . . .
C146 C 0.2396(9) 0.4562(8) 0.5517(9) 0.127(4) Uani 1 1 d D U . . .
H14G H 0.301237 0.445695 0.541078 0.190 Uiso 1 1 calc R U . . .
H14H H 0.212006 0.504266 0.568551 0.190 Uiso 1 1 calc R U . . .
H14I H 0.226579 0.465728 0.504059 0.190 Uiso 1 1 calc R U . . .
C151 C 0.2249(4) 0.2114(4) 0.3298(4) 0.0397(13) Uani 1 1 d . U . . .
C152 C 0.1611(5) 0.2450(4) 0.3095(5) 0.0464(15) Uani 1 1 d . U . . .
C153 C 0.0867(5) 0.2876(5) 0.2802(5) 0.0561(18) Uani 1 1 d . U . . .
C154 C 0.0223(6) 0.3419(6) 0.3290(6) 0.072(3) Uani 1 1 d . U . . .
H15A H -0.001121 0.307548 0.382423 0.107 Uiso 1 1 calc R U . . .
H15B H -0.023822 0.374798 0.305171 0.107 Uiso 1 1 calc R U . . .
H15C H 0.051028 0.377707 0.330585 0.107 Uiso 1 1 calc R U . . .
C155 C 0.0454(6) 0.2253(6) 0.2859(7) 0.072(3) Uani 1 1 d . U . . .
H15D H 0.087878 0.187484 0.259138 0.108 Uiso 1 1 calc R U . . .
H15E H -0.000629 0.252970 0.261078 0.108 Uiso 1 1 calc R U . . .
H15F H 0.022106 0.195112 0.341057 0.108 Uiso 1 1 calc R U . . .
C156 C 0.1168(6) 0.3405(6) 0.1944(6) 0.071(3) Uani 1 1 d . U . . .
H15G H 0.147821 0.377352 0.190985 0.107 Uiso 1 1 calc R U . . .
H15H H 0.067397 0.372477 0.174852 0.107 Uiso 1 1 calc R U . . .
H15I H 0.154295 0.305559 0.162778 0.107 Uiso 1 1 calc R U . . .
C161 C 0.5751(4) -0.0255(4) 0.7491(4) 0.0330(11) Uani 1 1 d . U . . .
C162 C 0.6092(5) -0.0371(4) 0.7973(4) 0.0435(14) Uani 1 1 d . U . . .
C163 C 0.6516(6) -0.0416(5) 0.8509(5) 0.0588(17) Uani 1 1 d D U . . .
C164 C 0.6092(8) -0.0876(7) 0.9352(5) 0.083(3) Uani 1 1 d D U . . .
H16A H 0.547602 -0.065635 0.947568 0.125 Uiso 1 1 calc R U . . .
H16B H 0.631498 -0.081434 0.970516 0.125 Uiso 1 1 calc R U . . .
H16C H 0.621150 -0.145395 0.941648 0.125 Uiso 1 1 calc R U . . .
C165 C 0.7428(8) -0.0925(8) 0.8308(7) 0.101(3) Uani 1 1 d D U . . .
H16D H 0.740971 -0.147842 0.839271 0.152 Uiso 1 1 calc R U . . .
H16E H 0.773021 -0.094530 0.864520 0.152 Uiso 1 1 calc R U . . .
H16F H 0.772603 -0.067576 0.775892 0.152 Uiso 1 1 calc R U . . .
C166 C 0.6541(9) 0.0411(7) 0.8392(7) 0.099(3) Uani 1 1 d D U . . .
H16G H 0.674150 0.069960 0.783042 0.149 Uiso 1 1 calc R U . . .
H16H H 0.692807 0.038276 0.865491 0.149 Uiso 1 1 calc R U . . .
H16I H 0.596866 0.070138 0.861159 0.149 Uiso 1 1 calc R U . . .
C171 C 0.5885(4) 0.2754(3) 0.3671(3) 0.0306(11) Uani 1 1 d . U . . .
C172 C 0.4316(5) -0.3453(4) 0.6342(5) 0.0449(15) Uani 1 1 d . U . . .
C173 C 0.4515(6) -0.4292(5) 0.6322(5) 0.065(2) Uani 1 1 d D U . . .
C174 C 0.4650(8) -0.4887(6) 0.7075(7) 0.090(3) Uani 1 1 d D U . . .
H17A H 0.410385 -0.489064 0.748464 0.136 Uiso 1 1 calc R U . . .
H17B H 0.503578 -0.473300 0.721497 0.136 Uiso 1 1 calc R U . . .
H17C H 0.490057 -0.542973 0.702416 0.136 Uiso 1 1 calc R U . . .
C175 C 0.5387(8) -0.4409(7) 0.5679(7) 0.099(3) Uani 1 1 d D U . . .
H17D H 0.558568 -0.498201 0.571066 0.149 Uiso 1 1 calc R U . . .
H17E H 0.580629 -0.424467 0.576510 0.149 Uiso 1 1 calc R U . . .
H17F H 0.531230 -0.407282 0.516036 0.149 Uiso 1 1 calc R U . . .
C176 C 0.3866(8) -0.4375(6) 0.6072(7) 0.088(3) Uani 1 1 d D U . . .
H17G H 0.330339 -0.425628 0.643588 0.133 Uiso 1 1 calc R U . . .
H17H H 0.399156 -0.493152 0.607008 0.133 Uiso 1 1 calc R U . . .
H17I H 0.387417 -0.399178 0.554386 0.133 Uiso 1 1 calc R U . . .
C181 C 0.6499(4) -0.3706(4) 0.6814(4) 0.0375(13) Uani 1 1 d . U . . .
C182 C 0.3019(4) 0.4354(4) 0.2979(4) 0.0401(13) Uani 1 1 d . U . . .
C183 C 0.2501(5) 0.5177(5) 0.2675(4) 0.0524(18) Uani 1 1 d D U . . .
C184 C 0.2380(7) 0.5669(6) 0.3183(6) 0.080(3) Uani 1 1 d D U . . .
H18A H 0.198748 0.546573 0.370054 0.120 Uiso 1 1 calc R U . . .
H18B H 0.214505 0.624377 0.293434 0.120 Uiso 1 1 calc R U . . .
H18C H 0.293012 0.561396 0.324120 0.120 Uiso 1 1 calc R U . . .
C185 C 0.2970(6) 0.5568(5) 0.1830(5) 0.067(3) Uani 1 1 d D U . . .
H18D H 0.352170 0.561529 0.180203 0.101 Uiso 1 1 calc R U . . .
H18E H 0.263297 0.611063 0.162022 0.101 Uiso 1 1 calc R U . . .
H18F H 0.305845 0.523161 0.152041 0.101 Uiso 1 1 calc R U . . .
C186 C 0.1635(6) 0.5098(6) 0.2740(6) 0.080(3) Uani 1 1 d D U . . .
H18G H 0.171565 0.472159 0.247399 0.120 Uiso 1 1 calc R U . . .
H18H H 0.131102 0.563223 0.249507 0.120 Uiso 1 1 calc R U . . .
H18I H 0.132353 0.488813 0.329347 0.120 Uiso 1 1 calc R U . . .
F1 F 0.5734(4) 0.3095(4) 0.6096(4) 0.0853(19) Uani 1 1 d . . . . .
F2 F 0.4542(5) 0.3344(5) 0.6854(6) 0.128(3) Uani 1 1 d . . . . .
F3 F 0.5424(6) 0.2312(5) 0.7302(4) 0.109(3) Uani 1 1 d . . . . .
F4 F 0.7280(5) -0.3677(4) 0.9916(4) 0.095(2) Uani 1 1 d . U . . .
F5 F 0.6256(4) -0.4180(4) 1.0200(3) 0.0826(19) Uani 1 1 d . . . . .
F6 F 0.7452(5) -0.4629(4) 0.9515(4) 0.109(3) Uani 1 1 d . . . . .
F7 F -0.0558(5) 0.1546(5) 0.8735(4) 0.112(3) Uani 1 1 d . . . . .
F8 F -0.0141(5) 0.2657(5) 0.8105(5) 0.103(2) Uani 1 1 d . . . . .
F9 F -0.0884(4) 0.2291(5) 0.7724(4) 0.101(2) Uani 1 1 d . U . . .
F10 F -0.0425(5) 0.4354(5) 0.5424(7) 0.098(3) Uani 0.731(15) 1 d D U P A 1
F20 F -0.0474(16) 0.4277(16) 0.4784(15) 0.106(5) Uani 0.269(15) 1 d D U P A 2
F11 F -0.0776(4) 0.3504(5) 0.5191(6) 0.120(3) Uani 1 1 d D U . . .
F12 F -0.0532(7) 0.3256(7) 0.6191(6) 0.176(4) Uani 1 1 d D U . . .
F21 F 0.5126(4) -0.2577(5) 1.0127(4) 0.101(2) Uani 1 1 d . . . . .
F22 F 0.5094(5) -0.3462(5) 1.1622(4) 0.111(3) Uani 1 1 d . . . . .
F23 F 0.3652(5) -0.3256(5) 1.2790(4) 0.097(2) Uani 1 1 d . . . . .
F24 F 0.2253(5) -0.2127(5) 1.2462(4) 0.101(2) Uani 1 1 d . . . . .
F25 F 0.2290(4) -0.1263(4) 1.0947(4) 0.0855(19) Uani 1 1 d . . . . .
F31 F 0.7984(3) 0.1419(3) 0.3892(3) 0.0478(10) Uani 1 1 d . . . . .
F32 F 0.8338(4) 0.2901(4) 0.3242(4) 0.0768(17) Uani 1 1 d . . . . .
F33 F 0.8137(4) 0.3746(4) 0.4138(5) 0.091(2) Uani 1 1 d . . . . .
F34 F 0.7554(4) 0.3113(4) 0.5725(5) 0.090(2) Uani 1 1 d . . . . .
F35 F 0.7166(3) 0.1628(4) 0.6393(3) 0.0633(13) Uani 1 1 d . . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 C151 2.217(7) 2_656 ?
Ag1 C181 2.286(7) . ?
Ag1 O32 2.396(5) . ?
Ag1 Ag14 2.9787(8) 2_656 ?
Ag1 Ag9 3.0110(7) . ?
Ag1 Ag2 3.0166(7) . ?
Ag1 Ag16 3.1604(7) . ?
Ag1 Ag13 3.1715(7) . ?
Ag2 C101 2.087(6) . ?
Ag2 O1 2.149(3) 2_656 ?
Ag2 Ag9 2.9100(6) . ?
Ag2 Ag13 3.0071(6) . ?
Ag2 Ag5 3.1290(6) . ?
Ag2 Ag4 3.1609(6) . ?
Ag2 Ag11 3.2809(6) . ?
Ag2 Ag16 3.2857(7) . ?
Ag3 C171 2.140(6) . ?
Ag3 O2 2.263(3) . ?
Ag3 O61 2.526(6) . ?
Ag3 O11 2.555(4) 2_656 ?
Ag3 Ag6 2.8957(6) . ?
Ag3 Ag13 3.1645(7) 2_656 ?
Ag3 Ag10 3.2233(7) . ?
Ag3 Ag5 3.3181(6) . ?
Ag4 C131 2.065(6) . ?
Ag4 O3 2.122(3) 2_656 ?
Ag4 Ag12 2.8639(6) . ?
Ag4 Ag11 2.9150(6) . ?
Ag4 Ag17 2.9910(6) . ?
Ag4 Ag7 3.0294(6) . ?
Ag4 Ag15 3.0392(6) . ?
Ag4 Ag5 3.2158(6) . ?
Ag5 C161 2.104(6) . ?
Ag5 O2 2.175(3) . ?
Ag5 Ag17 2.8102(6) . ?
Ag5 Ag16 2.8993(6) . ?
Ag6 C121 2.093(6) . ?
Ag6 C171 2.130(6) . ?
Ag6 Ag11 3.0230(6) 2_656 ?
Ag6 Ag13 3.3635(7) 2_656 ?
Ag7 C111 2.107(5) . ?
Ag7 O3 2.278(3) 2_656 ?
Ag7 O11 2.390(4) . ?
Ag7 O1 2.537(4) . ?
Ag7 Ag18 2.9041(6) . ?
Ag7 Ag8 2.9478(6) . ?
Ag7 Ag15 2.9839(6) . ?
Ag7 Ag10 3.1452(6) . ?
Ag8 O42 2.260(5) . ?
Ag8 C111 2.300(5) . ?
Ag8 C141 2.358(7) . ?
Ag8 Ag10 2.8330(6) . ?
Ag8 Ag18 2.8905(7) . ?
Ag8 Ag12 2.9747(7) . ?
Ag8 Ag15 2.9944(7) . ?
Ag9 O31 2.256(5) . ?
Ag9 C101 2.312(6) . ?
Ag9 C161 2.470(6) . ?
Ag9 C162 2.703(7) . ?
Ag9 Ag17 2.9547(7) . ?
Ag9 Ag16 2.9718(7) . ?
Ag10 C141 2.113(7) . ?
Ag10 O1 2.214(3) . ?
Ag10 O2 2.442(3) . ?
Ag10 Ag14 2.8525(7) . ?
Ag10 Ag12 3.0200(7) . ?
Ag10 Te1 3.2696(4) . ?
Ag10 Ag13 3.2723(7) 2_656 ?
Ag11 O21 2.282(5) . ?
Ag11 C121 2.309(6) 2_656 ?
Ag11 C101 2.408(6) . ?
Ag11 C102 2.682(6) . ?
Ag11 Ag17 3.0438(7) . ?
Ag12 O62 2.258(6) . ?
Ag12 C131 2.306(7) . ?
Ag12 C141 2.314(7) . ?
Ag12 C142 2.651(7) . ?
Ag13 C181 2.111(7) . ?
Ag13 C171 2.252(6) 2_656 ?
Ag13 C172 2.518(7) . ?
Ag13 Ag14 3.3462(8) 2_656 ?
Ag14 C181 2.246(7) 2_656 ?
Ag14 O52 2.256(5) . ?
Ag14 C141 2.343(7) . ?
Ag14 C182 2.656(7) . ?
Ag14 Ag18 3.3047(8) . ?
Ag15 C121 2.298(6) 2_656 ?
Ag15 O41 2.328(5) . ?
Ag15 C111 2.355(6) . ?
Ag15 C122 2.455(6) . ?
Ag16 C151 2.171(7) 2_656 ?
Ag16 C161 2.362(7) . ?
Ag16 O12 2.406(5) . ?
Ag16 Ag18 2.9658(7) 2_656 ?
Ag17 C131 2.289(6) . ?
Ag17 O22 2.311(5) . ?
Ag17 C161 2.313(7) . ?
Ag17 C132 2.633(7) . ?
Ag18 C151 2.171(7) . ?
Ag18 C111 2.328(6) . ?
Ag18 O51 2.402(5) . ?
Te1 O2 1.924(3) 2_656 ?
Te1 O2 1.924(3) . ?
Te1 O3 1.936(3) . ?
Te1 O3 1.936(3) 2_656 ?
Te1 O1 1.947(3) . ?
Te1 O1 1.947(3) 2_656 ?
O11 C11 1.273(6) 2_656 ?
C11 O12 1.238(8) . ?
C11 C12 1.512(9) . ?
C12 C17 1.368(9) . ?
C12 C13 1.380(11) . ?
C13 F31 1.328(9) . ?
C13 C14 1.385(10) . ?
C14 F32 1.334(11) . ?
C14 C15 1.345(12) . ?
C15 F33 1.335(9) . ?
C15 C16 1.369(13) . ?
C16 F34 1.337(9) . ?
C16 C17 1.411(11) . ?
C17 F35 1.346(10) . ?
O21 C21 1.242(9) . ?
C21 O22 1.258(9) . ?
C21 C22 1.543(10) . ?
C22 C23 1.314(12) . ?
C22 C27 1.318(12) . ?
C23 F25 1.316(11) . ?
C23 C24 1.394(12) . ?
C24 C25 1.358(14) . ?
C24 F24 1.371(11) . ?
C25 C26 1.353(13) . ?
C25 F23 1.366(10) . ?
C26 F22 1.358(12) . ?
C26 C27 1.401(12) . ?
C27 F21 1.381(11) . ?
O31 C31 1.236(9) . ?
C31 O32 1.213(9) . ?
C31 C32 1.547(10) . ?
C32 F5 1.303(11) . ?
C32 F4 1.307(11) . ?
C32 F6 1.317(12) . ?
O41 C41 1.246(10) . ?
C41 O42 1.218(11) . ?
C41 C42 1.567(10) . ?
C42 F7 1.254(12) . ?
C42 F9 1.305(11) . ?
C42 F8 1.365(13) . ?
O51 C51 1.220(9) . ?
C51 O52 1.225(10) . ?
C51 C52 1.562(14) . ?
C52 F10 1.233(11) . ?
C52 F11 1.289(10) . ?
C52 F12 1.357(12) . ?
C52 F20 1.362(16) . ?
O61 C61 1.203(9) . ?
C61 O62 1.244(10) . ?
C61 C62 1.527(10) . ?
C62 F2 1.269(11) . ?
C62 F1 1.316(10) . ?
C62 F3 1.371(12) . ?
C101 C102 1.223(8) . ?
C102 C103 1.489(8) . ?
C103 C104 1.521(11) . ?
C103 C106 1.530(10) . ?
C103 C105 1.538(10) . ?
C111 C112 1.215(8) . ?
C112 C113 1.485(8) . ?
C113 C115 1.525(10) . ?
C113 C114 1.536(11) . ?
C113 C116 1.542(10) . ?
C121 C122 1.220(9) 2_656 ?
C122 C123 1.501(10) . ?
C123 C124 1.519(12) . ?
C123 C125 1.549(14) . ?
C123 C126 1.558(13) . ?
C131 C132 1.222(9) . ?
C132 C133 1.488(9) . ?
C133 C136 1.507(13) . ?
C133 C135 1.526(12) . ?
C133 C134 1.549(12) . ?
C141 C142 1.221(9) . ?
C142 C143 1.487(10) . ?
C143 C146 1.464(13) . ?
C143 C144 1.477(12) . ?
C143 C145 1.517(13) . ?
C151 C152 1.206(10) . ?
C152 C153 1.466(11) . ?
C153 C155 1.513(13) . ?
C153 C156 1.536(12) . ?
C153 C154 1.540(14) . ?
C161 C162 1.220(8) . ?
C162 C163 1.471(9) . ?
C163 C166 1.468(11) . ?
C163 C164 1.522(11) . ?
C163 C165 1.539(12) . ?
C171 C172 1.213(9) 2_656 ?
C172 C173 1.487(10) . ?
C173 C176 1.477(11) . ?
C173 C174 1.479(11) . ?
C173 C175 1.569(12) . ?
C181 C182 1.215(10) 2_656 ?
C182 C183 1.487(10) . ?
C183 C185 1.515(10) . ?
C183 C186 1.526(10) . ?
C183 C184 1.531(10) . ?
F20 F11 1.49(3) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C151 Ag1 C181 134.2(3) 2_656 . ?
C151 Ag1 O32 103.4(2) 2_656 . ?
C181 Ag1 O32 93.7(2) . . ?
C151 Ag1 Ag14 89.20(19) 2_656 2_656 ?
C181 Ag1 Ag14 48.34(17) . 2_656 ?
O32 Ag1 Ag14 127.63(13) . 2_656 ?
C151 Ag1 Ag9 90.13(18) 2_656 . ?
C181 Ag1 Ag9 135.55(17) . . ?
O32 Ag1 Ag9 74.22(13) . . ?
Ag14 Ag1 Ag9 157.56(2) 2_656 . ?
C151 Ag1 Ag2 105.47(17) 2_656 . ?
C181 Ag1 Ag2 99.66(17) . . ?
O32 Ag1 Ag2 122.93(13) . . ?
Ag14 Ag1 Ag2 100.97(2) 2_656 . ?
Ag9 Ag1 Ag2 57.734(15) . . ?
C151 Ag1 Ag16 43.35(17) 2_656 . ?
C181 Ag1 Ag16 151.43(17) . . ?
O32 Ag1 Ag16 114.80(13) . . ?
Ag14 Ag1 Ag16 109.00(2) 2_656 . ?
Ag9 Ag1 Ag16 57.511(16) . . ?
Ag2 Ag1 Ag16 64.221(15) . . ?
C151 Ag1 Ag13 143.80(18) 2_656 . ?
C181 Ag1 Ag13 41.68(17) . . ?
O32 Ag1 Ag13 112.57(13) . . ?
Ag14 Ag1 Ag13 65.835(18) 2_656 . ?
Ag9 Ag1 Ag13 103.23(2) . . ?
Ag2 Ag1 Ag13 58.083(15) . . ?
Ag16 Ag1 Ag13 118.67(2) . . ?
C101 Ag2 O1 165.97(18) . 2_656 ?
C101 Ag2 Ag9 51.98(16) . . ?
O1 Ag2 Ag9 127.26(9) 2_656 . ?
C101 Ag2 Ag13 71.27(16) . . ?
O1 Ag2 Ag13 98.42(9) 2_656 . ?
Ag9 Ag2 Ag13 109.997(17) . . ?
C101 Ag2 Ag1 69.79(17) . . ?
O1 Ag2 Ag1 97.31(9) 2_656 . ?
Ag9 Ag2 Ag1 61.037(16) . . ?
Ag13 Ag2 Ag1 63.539(16) . . ?
C101 Ag2 Ag5 123.04(16) . . ?
O1 Ag2 Ag5 66.42(9) 2_656 . ?
Ag9 Ag2 Ag5 78.960(15) . . ?
Ag13 Ag2 Ag5 164.501(19) . . ?
Ag1 Ag2 Ag5 113.470(18) . . ?
C101 Ag2 Ag4 100.75(17) . . ?
O1 Ag2 Ag4 92.97(9) 2_656 . ?
Ag9 Ag2 Ag4 104.341(17) . . ?
Ag13 Ag2 Ag4 125.251(18) . . ?
Ag1 Ag2 Ag4 165.322(19) . . ?
Ag5 Ag2 Ag4 61.493(13) . . ?
C101 Ag2 Ag11 47.10(17) . . ?
O1 Ag2 Ag11 146.18(9) 2_656 . ?
Ag9 Ag2 Ag11 73.724(16) . . ?
Ag13 Ag2 Ag11 97.206(17) . . ?
Ag1 Ag2 Ag11 116.502(18) . . ?
Ag5 Ag2 Ag11 97.492(16) . . ?
Ag4 Ag2 Ag11 53.771(13) . . ?
C101 Ag2 Ag16 105.86(17) . . ?
O1 Ag2 Ag16 70.47(9) 2_656 . ?
Ag9 Ag2 Ag16 56.938(15) . . ?
Ag13 Ag2 Ag16 119.820(18) . . ?
Ag1 Ag2 Ag16 60.013(15) . . ?
Ag5 Ag2 Ag16 53.673(13) . . ?
Ag4 Ag2 Ag16 114.491(16) . . ?
Ag11 Ag2 Ag16 125.136(17) . . ?
C171 Ag3 O2 153.18(18) . . ?
C171 Ag3 O61 115.6(2) . . ?
O2 Ag3 O61 80.85(19) . . ?
C171 Ag3 O11 122.67(18) . 2_656 ?
O2 Ag3 O11 81.02(12) . 2_656 ?
O61 Ag3 O11 74.27(17) . 2_656 ?
C171 Ag3 Ag6 47.15(17) . . ?
O2 Ag3 Ag6 127.03(8) . . ?
O61 Ag3 Ag6 148.00(17) . . ?
O11 Ag3 Ag6 93.24(9) 2_656 . ?
C171 Ag3 Ag13 45.32(16) . 2_656 ?
O2 Ag3 Ag13 108.20(8) . 2_656 ?
O61 Ag3 Ag13 123.64(14) . 2_656 ?
O11 Ag3 Ag13 160.33(9) 2_656 2_656 ?
Ag6 Ag3 Ag13 67.254(16) . 2_656 ?
C171 Ag3 Ag10 106.26(16) . . ?
O2 Ag3 Ag10 49.13(8) . . ?
O61 Ag3 Ag10 94.13(17) . . ?
O11 Ag3 Ag10 130.14(9) 2_656 . ?
Ag6 Ag3 Ag10 115.666(18) . . ?
Ag13 Ag3 Ag10 61.623(15) 2_656 . ?
C171 Ag3 Ag5 164.89(16) . . ?
O2 Ag3 Ag5 40.60(8) . . ?
O61 Ag3 Ag5 51.13(15) . . ?
O11 Ag3 Ag5 51.04(9) 2_656 . ?
Ag6 Ag3 Ag5 138.875(18) . . ?
Ag13 Ag3 Ag5 145.057(18) 2_656 . ?
Ag10 Ag3 Ag5 83.605(15) . . ?
C131 Ag4 O3 177.3(2) . 2_656 ?
C131 Ag4 Ag12 52.80(18) . . ?
O3 Ag4 Ag12 129.64(9) 2_656 . ?
C131 Ag4 Ag11 75.57(18) . . ?
O3 Ag4 Ag11 101.89(9) 2_656 . ?
Ag12 Ag4 Ag11 128.24(2) . . ?
C131 Ag4 Ag17 49.81(17) . . ?
O3 Ag4 Ag17 128.19(9) 2_656 . ?
Ag12 Ag4 Ag17 79.905(16) . . ?
Ag11 Ag4 Ag17 62.029(16) . . ?
C131 Ag4 Ag7 133.40(17) . . ?
O3 Ag4 Ag7 48.66(9) 2_656 . ?
Ag12 Ag4 Ag7 101.258(17) . . ?
Ag11 Ag4 Ag7 118.884(18) . . ?
Ag17 Ag4 Ag7 176.551(19) . . ?
C131 Ag4 Ag15 83.74(18) . . ?
O3 Ag4 Ag15 96.86(9) 2_656 . ?
Ag12 Ag4 Ag15 96.202(18) . . ?
Ag11 Ag4 Ag15 80.017(17) . . ?
Ag17 Ag4 Ag15 124.331(18) . . ?
Ag7 Ag4 Ag15 58.904(14) . . ?
C131 Ag4 Ag2 119.44(17) . . ?
O3 Ag4 Ag2 58.17(9) 2_656 . ?
Ag12 Ag4 Ag2 134.820(19) . . ?
Ag11 Ag4 Ag2 65.220(14) . . ?
Ag17 Ag4 Ag2 71.065(14) . . ?
Ag7 Ag4 Ag2 106.095(15) . . ?
Ag15 Ag4 Ag2 128.687(18) . . ?
C131 Ag4 Ag5 90.52(19) . . ?
O3 Ag4 Ag5 89.11(9) 2_656 . ?
Ag12 Ag4 Ag5 76.214(16) . . ?
Ag11 Ag4 Ag5 103.554(16) . . ?
Ag17 Ag4 Ag5 53.694(14) . . ?
Ag7 Ag4 Ag5 123.294(16) . . ?
Ag15 Ag4 Ag5 172.309(18) . . ?
Ag2 Ag4 Ag5 58.766(13) . . ?
C161 Ag5 O2 168.39(19) . . ?
C161 Ag5 Ag17 53.87(19) . . ?
O2 Ag5 Ag17 117.51(9) . . ?
C161 Ag5 Ag16 53.51(18) . . ?
O2 Ag5 Ag16 126.53(9) . . ?
Ag17 Ag5 Ag16 98.078(18) . . ?
C161 Ag5 Ag2 83.73(16) . . ?
O2 Ag5 Ag2 86.19(9) . . ?
Ag17 Ag5 Ag2 73.867(15) . . ?
Ag16 Ag5 Ag2 65.927(16) . . ?
C161 Ag5 Ag4 109.84(18) . . ?
O2 Ag5 Ag4 59.71(9) . . ?
Ag17 Ag5 Ag4 59.060(14) . . ?
Ag16 Ag5 Ag4 124.831(18) . . ?
Ag2 Ag5 Ag4 59.741(12) . . ?
C161 Ag5 Ag3 148.92(17) . . ?
O2 Ag5 Ag3 42.63(9) . . ?
Ag17 Ag5 Ag3 146.472(19) . . ?
Ag16 Ag5 Ag3 115.401(19) . . ?
Ag2 Ag5 Ag3 120.362(15) . . ?
Ag4 Ag5 Ag3 99.844(14) . . ?
C121 Ag6 C171 161.6(2) . . ?
C121 Ag6 Ag3 148.14(16) . . ?
C171 Ag6 Ag3 47.45(15) . . ?
C121 Ag6 Ag11 49.68(16) . 2_656 ?
C171 Ag6 Ag11 134.73(16) . 2_656 ?
Ag3 Ag6 Ag11 131.92(2) . 2_656 ?
C121 Ag6 Ag13 143.44(16) . 2_656 ?
C171 Ag6 Ag13 41.21(16) . 2_656 ?
Ag3 Ag6 Ag13 60.188(15) . 2_656 ?
Ag11 Ag6 Ag13 95.170(18) 2_656 2_656 ?
C111 Ag7 O3 146.56(18) . 2_656 ?
C111 Ag7 O11 111.66(17) . . ?
O3 Ag7 O11 89.25(12) 2_656 . ?
C111 Ag7 O1 135.72(17) . . ?
O3 Ag7 O1 69.56(11) 2_656 . ?
O11 Ag7 O1 84.29(12) . . ?
C111 Ag7 Ag18 52.48(16) . . ?
O3 Ag7 Ag18 153.53(8) 2_656 . ?
O11 Ag7 Ag18 97.46(9) . . ?
O1 Ag7 Ag18 85.58(7) . . ?
C111 Ag7 Ag8 50.88(15) . . ?
O3 Ag7 Ag8 114.24(9) 2_656 . ?
O11 Ag7 Ag8 155.92(9) . . ?
O1 Ag7 Ag8 98.52(8) . . ?
Ag18 Ag7 Ag8 59.193(16) . . ?
C111 Ag7 Ag15 51.69(16) . . ?
O3 Ag7 Ag15 95.02(9) 2_656 . ?
O11 Ag7 Ag15 125.44(10) . . ?
O1 Ag7 Ag15 147.28(8) . . ?
Ag18 Ag7 Ag15 101.650(18) . . ?
Ag8 Ag7 Ag15 60.634(16) . . ?
C111 Ag7 Ag4 105.77(15) . . ?
O3 Ag7 Ag4 44.38(9) 2_656 . ?
O11 Ag7 Ag4 131.30(9) . . ?
O1 Ag7 Ag4 90.17(8) . . ?
Ag18 Ag7 Ag4 130.382(18) . . ?
Ag8 Ag7 Ag4 72.753(15) . . ?
Ag15 Ag7 Ag4 60.712(15) . . ?
C111 Ag7 Ag10 102.48(15) . . ?
O3 Ag7 Ag10 82.64(8) 2_656 . ?
O11 Ag7 Ag10 127.45(10) . . ?
O1 Ag7 Ag10 44.28(8) . . ?
Ag18 Ag7 Ag10 72.929(17) . . ?
Ag8 Ag7 Ag10 55.300(14) . . ?
Ag15 Ag7 Ag10 107.001(18) . . ?
Ag4 Ag7 Ag10 70.046(14) . . ?
O42 Ag8 C111 111.9(2) . . ?
O42 Ag8 C141 96.4(2) . . ?
C111 Ag8 C141 151.1(2) . . ?
O42 Ag8 Ag10 139.13(17) . . ?
C111 Ag8 Ag10 107.32(14) . . ?
C141 Ag8 Ag10 46.93(17) . . ?
O42 Ag8 Ag18 136.93(16) . . ?
C111 Ag8 Ag18 51.78(15) . . ?
C141 Ag8 Ag18 103.33(18) . . ?
Ag10 Ag8 Ag18 77.956(19) . . ?
O42 Ag8 Ag7 142.70(16) . . ?
C111 Ag8 Ag7 45.29(13) . . ?
C141 Ag8 Ag7 112.75(17) . . ?
Ag10 Ag8 Ag7 65.888(15) . . ?
Ag18 Ag8 Ag7 59.649(15) . . ?
O42 Ag8 Ag12 80.29(17) . . ?
C111 Ag8 Ag12 138.37(14) . . ?
C141 Ag8 Ag12 49.79(16) . . ?
Ag10 Ag8 Ag12 62.608(18) . . ?
Ag18 Ag8 Ag12 140.56(2) . . ?
Ag7 Ag8 Ag12 100.608(18) . . ?
O42 Ag8 Ag15 82.44(16) . . ?
C111 Ag8 Ag15 50.78(14) . . ?
C141 Ag8 Ag15 143.82(16) . . ?
Ag10 Ag8 Ag15 115.455(19) . . ?
Ag18 Ag8 Ag15 101.719(19) . . ?
Ag7 Ag8 Ag15 60.279(16) . . ?
Ag12 Ag8 Ag15 94.844(19) . . ?
O31 Ag9 C101 115.5(2) . . ?
O31 Ag9 C161 121.2(2) . . ?
C101 Ag9 C161 122.63(19) . . ?
O31 Ag9 C162 95.9(2) . . ?
C101 Ag9 C162 148.7(2) . . ?
C161 Ag9 C162 26.80(18) . . ?
O31 Ag9 Ag2 140.85(15) . . ?
C101 Ag9 Ag2 45.35(14) . . ?
C161 Ag9 Ag2 82.84(13) . . ?
C162 Ag9 Ag2 109.03(14) . . ?
O31 Ag9 Ag17 143.93(16) . . ?
C101 Ag9 Ag17 88.38(14) . . ?
C161 Ag9 Ag17 49.49(16) . . ?
C162 Ag9 Ag17 64.41(17) . . ?
Ag2 Ag9 Ag17 75.185(16) . . ?
O31 Ag9 Ag16 102.25(18) . . ?
C101 Ag9 Ag16 110.12(14) . . ?
C161 Ag9 Ag16 50.41(16) . . ?
C162 Ag9 Ag16 59.70(17) . . ?
Ag2 Ag9 Ag16 67.911(17) . . ?
Ag17 Ag9 Ag16 93.367(18) . . ?
O31 Ag9 Ag1 80.20(16) . . ?
C101 Ag9 Ag1 67.60(15) . . ?
C161 Ag9 Ag1 113.07(15) . . ?
C162 Ag9 Ag1 120.94(18) . . ?
Ag2 Ag9 Ag1 61.230(16) . . ?
Ag17 Ag9 Ag1 135.59(2) . . ?
Ag16 Ag9 Ag1 63.770(18) . . ?
C141 Ag10 O1 163.2(2) . . ?
C141 Ag10 O2 121.71(19) . . ?
O1 Ag10 O2 70.77(11) . . ?
C141 Ag10 Ag8 54.6(2) . . ?
O1 Ag10 Ag8 110.59(9) . . ?
O2 Ag10 Ag8 118.74(8) . . ?
C141 Ag10 Ag14 53.84(18) . . ?
O1 Ag10 Ag14 117.81(9) . . ?
O2 Ag10 Ag14 162.69(8) . . ?
Ag8 Ag10 Ag14 73.807(18) . . ?
C141 Ag10 Ag12 49.83(18) . . ?
O1 Ag10 Ag12 133.92(9) . . ?
O2 Ag10 Ag12 75.54(8) . . ?
Ag8 Ag10 Ag12 60.994(17) . . ?
Ag14 Ag10 Ag12 103.545(19) . . ?
C141 Ag10 Ag7 113.4(2) . . ?
O1 Ag10 Ag7 53.12(9) . . ?
O2 Ag10 Ag7 87.03(8) . . ?
Ag8 Ag10 Ag7 58.812(14) . . ?
Ag14 Ag10 Ag7 110.19(2) . . ?
Ag12 Ag10 Ag7 95.300(18) . . ?
C141 Ag10 Ag3 111.25(19) . . ?
O1 Ag10 Ag3 85.47(9) . . ?
O2 Ag10 Ag3 44.48(8) . . ?
Ag8 Ag10 Ag3 152.85(2) . . ?
Ag14 Ag10 Ag3 118.964(19) . . ?
Ag12 Ag10 Ag3 92.007(18) . . ?
Ag7 Ag10 Ag3 126.835(16) . . ?
C141 Ag10 Te1 153.51(19) . . ?
O1 Ag10 Te1 35.40(8) . . ?
O2 Ag10 Te1 35.81(7) . . ?
Ag8 Ag10 Te1 116.479(17) . . ?
Ag14 Ag10 Te1 152.40(2) . . ?
Ag12 Ag10 Te1 103.683(16) . . ?
Ag7 Ag10 Te1 62.724(11) . . ?
Ag3 Ag10 Te1 64.373(11) . . ?
C141 Ag10 Ag13 98.0(2) . 2_656 ?
O1 Ag10 Ag13 89.78(9) . 2_656 ?
O2 Ag10 Ag13 100.59(8) . 2_656 ?
Ag8 Ag10 Ag13 139.61(2) . 2_656 ?
Ag14 Ag10 Ag13 65.815(17) . 2_656 ?
Ag12 Ag10 Ag13 127.18(2) . 2_656 ?
Ag7 Ag10 Ag13 137.48(2) . 2_656 ?
Ag3 Ag10 Ag13 58.304(14) . 2_656 ?
Te1 Ag10 Ag13 100.476(15) . 2_656 ?
O21 Ag11 C121 123.0(2) . 2_656 ?
O21 Ag11 C101 102.73(19) . . ?
C121 Ag11 C101 122.5(2) 2_656 . ?
O21 Ag11 C102 90.48(18) . . ?
C121 Ag11 C102 113.8(2) 2_656 . ?
C101 Ag11 C102 27.12(19) . . ?
O21 Ag11 Ag4 128.76(14) . . ?
C121 Ag11 Ag4 78.10(14) 2_656 . ?
C101 Ag11 Ag4 100.31(13) . . ?
C102 Ag11 Ag4 125.70(13) . . ?
O21 Ag11 Ag6 153.89(14) . 2_656 ?
C121 Ag11 Ag6 43.73(15) 2_656 2_656 ?
C101 Ag11 Ag6 79.80(13) . 2_656 ?
C102 Ag11 Ag6 80.23(13) . 2_656 ?
Ag4 Ag11 Ag6 75.079(15) . 2_656 ?
O21 Ag11 Ag17 77.17(14) . . ?
C121 Ag11 Ag17 134.48(14) 2_656 . ?
C101 Ag11 Ag17 84.61(14) . . ?
C102 Ag11 Ag17 105.47(14) . . ?
Ag4 Ag11 Ag17 60.211(15) . . ?
Ag6 Ag11 Ag17 128.769(19) 2_656 . ?
O21 Ag11 Ag2 129.24(14) . . ?
C121 Ag11 Ag2 107.70(15) 2_656 . ?
C101 Ag11 Ag2 39.42(13) . . ?
C102 Ag11 Ag2 65.05(13) . . ?
Ag4 Ag11 Ag2 61.009(14) . . ?
Ag6 Ag11 Ag2 68.374(15) 2_656 . ?
Ag17 Ag11 Ag2 68.784(15) . . ?
O62 Ag12 C131 102.2(3) . . ?
O62 Ag12 C141 112.3(3) . . ?
C131 Ag12 C141 145.4(2) . . ?
O62 Ag12 C142 97.6(3) . . ?
C131 Ag12 C142 150.3(3) . . ?
C141 Ag12 C142 27.4(2) . . ?
O62 Ag12 Ag4 117.7(3) . . ?
C131 Ag12 Ag4 45.52(15) . . ?
C141 Ag12 Ag4 112.06(15) . . ?
C142 Ag12 Ag4 137.99(15) . . ?
O62 Ag12 Ag8 163.4(2) . . ?
C131 Ag12 Ag8 94.40(16) . . ?
C141 Ag12 Ag8 51.12(18) . . ?
C142 Ag12 Ag8 66.92(16) . . ?
Ag4 Ag12 Ag8 74.758(16) . . ?
O62 Ag12 Ag10 114.2(2) . . ?
C131 Ag12 Ag10 119.01(15) . . ?
C141 Ag12 Ag10 44.25(16) . . ?
C142 Ag12 Ag10 70.87(17) . . ?
Ag4 Ag12 Ag10 74.040(16) . . ?
Ag8 Ag12 Ag10 56.398(15) . . ?
C181 Ag13 C171 153.8(2) . 2_656 ?
C181 Ag13 C172 125.0(2) . . ?
C171 Ag13 C172 28.8(2) 2_656 . ?
C181 Ag13 Ag2 104.34(18) . . ?
C171 Ag13 Ag2 101.71(15) 2_656 . ?
C172 Ag13 Ag2 130.38(16) . . ?
C181 Ag13 Ag3 147.88(18) . 2_656 ?
C171 Ag13 Ag3 42.52(14) 2_656 2_656 ?
C172 Ag13 Ag3 62.81(16) . 2_656 ?
Ag2 Ag13 Ag3 78.658(15) . 2_656 ?
C181 Ag13 Ag1 46.08(18) . . ?
C171 Ag13 Ag1 159.18(16) 2_656 . ?
C172 Ag13 Ag1 168.57(16) . . ?
Ag2 Ag13 Ag1 58.377(15) . . ?
Ag3 Ag13 Ag1 128.619(19) 2_656 . ?
C181 Ag13 Ag10 91.26(18) . 2_656 ?
C171 Ag13 Ag10 101.96(14) 2_656 2_656 ?
C172 Ag13 Ag10 112.76(18) . 2_656 ?
Ag2 Ag13 Ag10 66.542(15) . 2_656 ?
Ag3 Ag13 Ag10 60.073(15) 2_656 2_656 ?
Ag1 Ag13 Ag10 76.724(17) . 2_656 ?
C181 Ag13 Ag14 41.34(18) . 2_656 ?
C171 Ag13 Ag14 140.05(16) 2_656 2_656 ?
C172 Ag13 Ag14 126.01(18) . 2_656 ?
Ag2 Ag13 Ag14 93.286(17) . 2_656 ?
Ag3 Ag13 Ag14 107.081(19) 2_656 2_656 ?
Ag1 Ag13 Ag14 54.310(17) . 2_656 ?
Ag10 Ag13 Ag14 51.046(14) 2_656 2_656 ?
C181 Ag13 Ag6 158.35(19) . 2_656 ?
C171 Ag13 Ag6 38.54(16) 2_656 2_656 ?
C172 Ag13 Ag6 64.58(17) . 2_656 ?
Ag2 Ag13 Ag6 67.433(15) . 2_656 ?
Ag3 Ag13 Ag6 52.559(13) 2_656 2_656 ?
Ag1 Ag13 Ag6 120.93(2) . 2_656 ?
Ag10 Ag13 Ag6 102.701(16) 2_656 2_656 ?
Ag14 Ag13 Ag6 153.171(19) 2_656 2_656 ?
C181 Ag14 O52 123.8(2) 2_656 . ?
C181 Ag14 C141 126.4(3) 2_656 . ?
O52 Ag14 C141 102.0(2) . . ?
C181 Ag14 C182 27.1(2) 2_656 . ?
O52 Ag14 C182 97.3(2) . . ?
C141 Ag14 C182 139.8(2) . . ?
C181 Ag14 Ag10 100.26(17) 2_656 . ?
O52 Ag14 Ag10 135.53(16) . . ?
C141 Ag14 Ag10 46.72(16) . . ?
C182 Ag14 Ag10 127.10(15) . . ?
C181 Ag14 Ag1 49.50(17) 2_656 2_656 ?
O52 Ag14 Ag1 115.99(17) . 2_656 ?
C141 Ag14 Ag1 133.31(16) . 2_656 ?
C182 Ag14 Ag1 62.82(15) . 2_656 ?
Ag10 Ag14 Ag1 86.59(2) . 2_656 ?
C181 Ag14 Ag18 118.14(17) 2_656 . ?
O52 Ag14 Ag18 81.87(15) . . ?
C141 Ag14 Ag18 92.40(16) . . ?
C182 Ag14 Ag18 125.24(15) . . ?
Ag10 Ag14 Ag18 71.141(17) . . ?
Ag1 Ag14 Ag18 68.683(18) 2_656 . ?
C181 Ag14 Ag13 38.36(17) 2_656 2_656 ?
O52 Ag14 Ag13 161.24(16) . 2_656 ?
C141 Ag14 Ag13 91.51(19) . 2_656 ?
C182 Ag14 Ag13 64.20(15) . 2_656 ?
Ag10 Ag14 Ag13 63.139(16) . 2_656 ?
Ag1 Ag14 Ag13 59.856(17) 2_656 2_656 ?
Ag18 Ag14 Ag13 110.761(19) . 2_656 ?
C121 Ag15 O41 126.5(2) 2_656 . ?
C121 Ag15 C111 132.8(2) 2_656 . ?
O41 Ag15 C111 97.33(19) . . ?
C121 Ag15 C122 29.5(2) 2_656 . ?
O41 Ag15 C122 97.4(2) . . ?
C111 Ag15 C122 151.6(2) . . ?
C121 Ag15 Ag7 98.94(15) 2_656 . ?
O41 Ag15 Ag7 134.05(14) . . ?
C111 Ag15 Ag7 44.58(13) . . ?
C122 Ag15 Ag7 128.36(16) . . ?
C121 Ag15 Ag8 146.97(15) 2_656 . ?
O41 Ag15 Ag8 76.79(14) . . ?
C111 Ag15 Ag8 49.17(14) . . ?
C122 Ag15 Ag8 158.88(18) . . ?
Ag7 Ag15 Ag8 59.087(15) . . ?
C121 Ag15 Ag4 75.64(15) 2_656 . ?
O41 Ag15 Ag4 119.62(16) . . ?
C111 Ag15 Ag4 99.25(13) . . ?
C122 Ag15 Ag4 94.31(16) . . ?
Ag7 Ag15 Ag4 60.384(14) . . ?
Ag8 Ag15 Ag4 71.976(16) . . ?
C151 Ag16 C161 142.0(2) 2_656 . ?
C151 Ag16 O12 109.9(2) 2_656 . ?
C161 Ag16 O12 95.4(2) . . ?
C151 Ag16 Ag5 157.50(19) 2_656 . ?
C161 Ag16 Ag5 45.74(14) . . ?
O12 Ag16 Ag5 86.25(11) . . ?
C151 Ag16 Ag18 46.92(19) 2_656 2_656 ?
C161 Ag16 Ag18 169.21(14) . 2_656 ?
O12 Ag16 Ag18 83.83(13) . 2_656 ?
Ag5 Ag16 Ag18 123.53(2) . 2_656 ?
C151 Ag16 Ag9 92.08(19) 2_656 . ?
C161 Ag16 Ag9 53.72(15) . . ?
O12 Ag16 Ag9 145.33(13) . . ?
Ag5 Ag16 Ag9 81.775(18) . . ?
Ag18 Ag16 Ag9 129.58(2) 2_656 . ?
C151 Ag16 Ag1 44.52(19) 2_656 . ?
C161 Ag16 Ag1 111.35(15) . . ?
O12 Ag16 Ag1 152.72(13) . . ?
Ag5 Ag16 Ag1 115.94(2) . . ?
Ag18 Ag16 Ag1 70.858(18) 2_656 . ?
Ag9 Ag16 Ag1 58.720(17) . . ?
C151 Ag16 Ag2 98.36(19) 2_656 . ?
C161 Ag16 Ag2 76.61(14) . . ?
O12 Ag16 Ag2 140.65(11) . . ?
Ag5 Ag16 Ag2 60.400(15) . . ?
Ag18 Ag16 Ag2 97.122(19) 2_656 . ?
Ag9 Ag16 Ag2 55.151(14) . . ?
Ag1 Ag16 Ag2 55.766(15) . . ?
C131 Ag17 O22 119.9(2) . . ?
C131 Ag17 C161 143.2(2) . . ?
O22 Ag17 C161 96.9(2) . . ?
C131 Ag17 C132 27.6(2) . . ?
O22 Ag17 C132 103.2(2) . . ?
C161 Ag17 C132 147.4(2) . . ?
C131 Ag17 Ag5 97.10(16) . . ?
O22 Ag17 Ag5 141.91(14) . . ?
C161 Ag17 Ag5 47.27(14) . . ?
C132 Ag17 Ag5 114.49(16) . . ?
C131 Ag17 Ag9 144.83(16) . . ?
O22 Ag17 Ag9 61.32(13) . . ?
C161 Ag17 Ag9 54.29(15) . . ?
C132 Ag17 Ag9 158.05(18) . . ?
Ag5 Ag17 Ag9 83.585(18) . . ?
C131 Ag17 Ag4 43.58(15) . . ?
O22 Ag17 Ag4 134.55(14) . . ?
C161 Ag17 Ag4 111.46(14) . . ?
C132 Ag17 Ag4 71.18(14) . . ?
Ag5 Ag17 Ag4 67.245(15) . . ?
Ag9 Ag17 Ag4 107.585(19) . . ?
C131 Ag17 Ag11 70.11(17) . . ?
O22 Ag17 Ag11 76.97(14) . . ?
C161 Ag17 Ag11 125.10(14) . . ?
C132 Ag17 Ag11 84.80(17) . . ?
Ag5 Ag17 Ag11 110.784(19) . . ?
Ag9 Ag17 Ag11 76.780(18) . . ?
Ag4 Ag17 Ag11 57.760(14) . . ?
C151 Ag18 C111 159.1(2) . . ?
C151 Ag18 O51 115.3(2) . . ?
C111 Ag18 O51 81.68(19) . . ?
C151 Ag18 Ag8 147.55(19) . . ?
C111 Ag18 Ag8 50.92(14) . . ?
O51 Ag18 Ag8 59.78(13) . . ?
C151 Ag18 Ag7 124.62(18) . . ?
C111 Ag18 Ag7 45.88(13) . . ?
O51 Ag18 Ag7 117.84(13) . . ?
Ag8 Ag18 Ag7 61.157(15) . . ?
C151 Ag18 Ag16 46.92(17) . 2_656 ?
C111 Ag18 Ag16 115.54(14) . 2_656 ?
O51 Ag18 Ag16 162.18(13) . 2_656 ?
Ag8 Ag18 Ag16 134.08(2) . 2_656 ?
Ag7 Ag18 Ag16 79.439(17) . 2_656 ?
C151 Ag18 Ag14 81.87(19) . . ?
C111 Ag18 Ag14 117.40(14) . . ?
O51 Ag18 Ag14 67.37(14) . . ?
Ag8 Ag18 Ag14 66.491(17) . . ?
Ag7 Ag18 Ag14 104.69(2) . . ?
Ag16 Ag18 Ag14 105.61(2) 2_656 . ?
O2 Te1 O2 180.0 2_656 . ?
O2 Te1 O3 90.13(14) 2_656 . ?
O2 Te1 O3 89.87(14) . . ?
O2 Te1 O3 89.87(14) 2_656 2_656 ?
O2 Te1 O3 90.13(14) . 2_656 ?
O3 Te1 O3 180.0(2) . 2_656 ?
O2 Te1 O1 91.44(14) 2_656 . ?
O2 Te1 O1 88.56(14) . . ?
O3 Te1 O1 89.63(14) . . ?
O3 Te1 O1 90.37(14) 2_656 . ?
O2 Te1 O1 88.56(14) 2_656 2_656 ?
O2 Te1 O1 91.44(14) . 2_656 ?
O3 Te1 O1 90.37(14) . 2_656 ?
O3 Te1 O1 89.63(14) 2_656 2_656 ?
O1 Te1 O1 180.0 . 2_656 ?
O2 Te1 Ag10 47.95(10) 2_656 2_656 ?
O2 Te1 Ag10 132.05(10) . 2_656 ?
O3 Te1 Ag10 84.58(10) . 2_656 ?
O3 Te1 Ag10 95.42(10) 2_656 2_656 ?
O1 Te1 Ag10 138.79(10) . 2_656 ?
O1 Te1 Ag10 41.21(10) 2_656 2_656 ?
O2 Te1 Ag10 132.05(10) 2_656 . ?
O2 Te1 Ag10 47.95(10) . . ?
O3 Te1 Ag10 95.42(10) . . ?
O3 Te1 Ag10 84.58(10) 2_656 . ?
O1 Te1 Ag10 41.21(10) . . ?
O1 Te1 Ag10 138.79(10) 2_656 . ?
Ag10 Te1 Ag10 180.0 2_656 . ?
Te1 O1 Ag2 110.49(16) . 2_656 ?
Te1 O1 Ag10 103.38(15) . . ?
Ag2 O1 Ag10 104.56(14) 2_656 . ?
Te1 O1 Ag7 95.40(13) . . ?
Ag2 O1 Ag7 150.19(15) 2_656 . ?
Ag10 O1 Ag7 82.60(11) . . ?
Te1 O2 Ag5 117.64(16) . . ?
Te1 O2 Ag3 111.12(15) . . ?
Ag5 O2 Ag3 96.77(13) . . ?
Te1 O2 Ag10 96.24(13) . . ?
Ag5 O2 Ag10 141.60(15) . . ?
Ag3 O2 Ag10 86.39(11) . . ?
Te1 O3 Ag4 114.78(16) . 2_656 ?
Te1 O3 Ag7 104.58(14) . 2_656 ?
Ag4 O3 Ag7 86.96(12) 2_656 2_656 ?
C11 O11 Ag7 120.4(4) 2_656 . ?
C11 O11 Ag3 131.7(4) 2_656 2_656 ?
Ag7 O11 Ag3 97.36(13) . 2_656 ?
O12 C11 O11 126.2(6) . 2_656 ?
O12 C11 C12 118.1(5) . . ?
O11 C11 C12 115.7(5) 2_656 . ?
C11 O12 Ag16 109.0(4) . . ?
C17 C12 C13 117.2(6) . . ?
C17 C12 C11 122.1(7) . . ?
C13 C12 C11 120.7(6) . . ?
F31 C13 C12 120.3(6) . . ?
F31 C13 C14 118.0(7) . . ?
C12 C13 C14 121.7(7) . . ?
F32 C14 C15 119.1(8) . . ?
F32 C14 C13 120.6(8) . . ?
C15 C14 C13 120.4(8) . . ?
F33 C15 C14 120.4(9) . . ?
F33 C15 C16 119.4(8) . . ?
C14 C15 C16 120.2(7) . . ?
F34 C16 C15 121.5(8) . . ?
F34 C16 C17 119.3(8) . . ?
C15 C16 C17 119.1(7) . . ?
F35 C17 C12 119.8(7) . . ?
F35 C17 C16 118.8(7) . . ?
C12 C17 C16 121.4(8) . . ?
C21 O21 Ag11 120.9(5) . . ?
O21 C21 O22 127.6(6) . . ?
O21 C21 C22 116.7(7) . . ?
O22 C21 C22 115.7(7) . . ?
C21 O22 Ag17 121.0(5) . . ?
C23 C22 C27 118.5(8) . . ?
C23 C22 C21 121.9(8) . . ?
C27 C22 C21 119.5(7) . . ?
C22 C23 F25 122.0(8) . . ?
C22 C23 C24 121.0(9) . . ?
F25 C23 C24 116.9(8) . . ?
C25 C24 F24 118.2(8) . . ?
C25 C24 C23 119.9(9) . . ?
F24 C24 C23 121.9(9) . . ?
C26 C25 C24 119.8(9) . . ?
C26 C25 F23 119.2(9) . . ?
C24 C25 F23 121.0(9) . . ?
C25 C26 F22 120.3(8) . . ?
C25 C26 C27 116.8(9) . . ?
F22 C26 C27 122.9(9) . . ?
C22 C27 F21 122.8(7) . . ?
C22 C27 C26 124.0(9) . . ?
F21 C27 C26 113.3(8) . . ?
C31 O31 Ag9 118.8(5) . . ?
O32 C31 O31 128.9(6) . . ?
O32 C31 C32 115.6(7) . . ?
O31 C31 C32 115.5(7) . . ?
C31 O32 Ag1 121.6(4) . . ?
F5 C32 F4 106.2(9) . . ?
F5 C32 F6 106.5(8) . . ?
F4 C32 F6 106.9(8) . . ?
F5 C32 C31 111.4(7) . . ?
F4 C32 C31 112.0(7) . . ?
F6 C32 C31 113.4(8) . . ?
C41 O41 Ag15 124.8(5) . . ?
O42 C41 O41 130.4(7) . . ?
O42 C41 C42 116.8(8) . . ?
O41 C41 C42 112.8(8) . . ?
C41 O42 Ag8 119.7(5) . . ?
F7 C42 F9 106.8(10) . . ?
F7 C42 F8 108.6(8) . . ?
F9 C42 F8 105.7(8) . . ?
F7 C42 C41 114.7(8) . . ?
F9 C42 C41 111.2(7) . . ?
F8 C42 C41 109.5(9) . . ?
C51 O51 Ag18 129.7(6) . . ?
O51 C51 O52 130.8(8) . . ?
O51 C51 C52 112.1(8) . . ?
O52 C51 C52 117.0(7) . . ?
C51 O52 Ag14 117.3(5) . . ?
F10 C52 F11 116.2(10) . . ?
F10 C52 F12 100.0(10) . . ?
F11 C52 F12 98.5(9) . . ?
F11 C52 F20 68.3(14) . . ?
F12 C52 F20 146.4(15) . . ?
F10 C52 C51 117.2(9) . . ?
F11 C52 C51 110.5(9) . . ?
F12 C52 C51 112.2(9) . . ?
F20 C52 C51 101.4(14) . . ?
C61 O61 Ag3 145.0(5) . . ?
O61 C61 O62 130.6(7) . . ?
O61 C61 C62 119.0(8) . . ?
O62 C61 C62 110.0(7) . . ?
C61 O62 Ag12 127.0(6) . . ?
F2 C62 F1 105.9(8) . . ?
F2 C62 F3 105.6(9) . . ?
F1 C62 F3 107.2(8) . . ?
F2 C62 C61 116.0(8) . . ?
F1 C62 C61 113.0(7) . . ?
F3 C62 C61 108.6(7) . . ?
C102 C101 Ag2 156.6(5) . . ?
C102 C101 Ag9 119.3(5) . . ?
Ag2 C101 Ag9 82.7(2) . . ?
C102 C101 Ag11 89.0(4) . . ?
Ag2 C101 Ag11 93.5(2) . . ?
Ag9 C101 Ag11 104.2(2) . . ?
C101 C102 C103 176.9(7) . . ?
C101 C102 Ag11 63.9(4) . . ?
C103 C102 Ag11 118.6(4) . . ?
C102 C103 C104 108.8(5) . . ?
C102 C103 C106 109.5(6) . . ?
C104 C103 C106 111.2(7) . . ?
C102 C103 C105 108.0(5) . . ?
C104 C103 C105 110.1(6) . . ?
C106 C103 C105 109.1(6) . . ?
C112 C111 Ag7 150.7(5) . . ?
C112 C111 Ag8 125.5(4) . . ?
Ag7 C111 Ag8 83.83(19) . . ?
C112 C111 Ag18 102.2(4) . . ?
Ag7 C111 Ag18 81.64(19) . . ?
Ag8 C111 Ag18 77.29(18) . . ?
C112 C111 Ag15 101.0(4) . . ?
Ag7 C111 Ag15 83.73(19) . . ?
Ag8 C111 Ag15 80.05(17) . . ?
Ag18 C111 Ag15 154.2(3) . . ?
C111 C112 C113 178.5(6) . . ?
C112 C113 C115 109.7(6) . . ?
C112 C113 C114 108.2(6) . . ?
C115 C113 C114 110.9(6) . . ?
C112 C113 C116 106.2(6) . . ?
C115 C113 C116 111.5(6) . . ?
C114 C113 C116 110.1(6) . . ?
C122 C121 Ag6 160.3(5) 2_656 . ?
C122 C121 Ag15 82.4(4) 2_656 2_656 ?
Ag6 C121 Ag15 113.8(3) . 2_656 ?
C122 C121 Ag11 97.7(5) 2_656 2_656 ?
Ag6 C121 Ag11 86.6(2) . 2_656 ?
Ag15 C121 Ag11 112.4(2) 2_656 2_656 ?
C121 C122 C123 170.9(7) 2_656 . ?
C121 C122 Ag15 68.1(4) 2_656 . ?
C123 C122 Ag15 120.1(5) . . ?
C122 C123 C124 108.7(7) . . ?
C122 C123 C125 108.0(7) . . ?
C124 C123 C125 111.3(8) . . ?
C122 C123 C126 109.1(7) . . ?
C124 C123 C126 109.7(7) . . ?
C125 C123 C126 110.0(8) . . ?
C132 C131 Ag4 177.1(7) . . ?
C132 C131 Ag17 92.1(5) . . ?
Ag4 C131 Ag17 86.6(2) . . ?
C132 C131 Ag12 96.3(5) . . ?
Ag4 C131 Ag12 81.7(2) . . ?
Ag17 C131 Ag12 109.9(3) . . ?
C131 C132 C133 177.5(7) . . ?
C131 C132 Ag17 60.3(4) . . ?
C133 C132 Ag17 122.2(5) . . ?
C132 C133 C136 111.4(7) . . ?
C132 C133 C135 108.8(6) . . ?
C136 C133 C135 111.5(8) . . ?
C132 C133 C134 109.8(7) . . ?
C136 C133 C134 108.5(7) . . ?
C135 C133 C134 106.9(8) . . ?
C142 C141 Ag10 163.5(7) . . ?
C142 C141 Ag12 91.9(5) . . ?
Ag10 C141 Ag12 85.9(2) . . ?
C142 C141 Ag14 103.6(5) . . ?
Ag10 C141 Ag14 79.4(2) . . ?
Ag12 C141 Ag14 164.6(3) . . ?
C142 C141 Ag8 117.3(7) . . ?
Ag10 C141 Ag8 78.4(2) . . ?
Ag12 C141 Ag8 79.1(2) . . ?
Ag14 C141 Ag8 93.1(2) . . ?
C141 C142 C143 174.7(8) . . ?
C141 C142 Ag12 60.7(4) . . ?
C143 C142 Ag12 123.0(5) . . ?
C146 C143 C144 114.4(9) . . ?
C146 C143 C142 106.4(9) . . ?
C144 C143 C142 109.2(9) . . ?
C146 C143 C145 108.4(8) . . ?
C144 C143 C145 108.1(9) . . ?
C142 C143 C145 110.3(8) . . ?
C152 C151 Ag16 133.3(6) . 2_656 ?
C152 C151 Ag18 108.6(6) . . ?
Ag16 C151 Ag18 86.2(2) 2_656 . ?
C152 C151 Ag1 122.0(5) . 2_656 ?
Ag16 C151 Ag1 92.1(3) 2_656 2_656 ?
Ag18 C151 Ag1 108.2(3) . 2_656 ?
C151 C152 C153 176.6(9) . . ?
C152 C153 C155 108.8(7) . . ?
C152 C153 C156 108.3(7) . . ?
C155 C153 C156 110.3(9) . . ?
C152 C153 C154 110.2(8) . . ?
C155 C153 C154 109.6(8) . . ?
C156 C153 C154 109.7(8) . . ?
C162 C161 Ag5 157.7(6) . . ?
C162 C161 Ag17 114.0(6) . . ?
Ag5 C161 Ag17 78.9(2) . . ?
C162 C161 Ag16 99.7(5) . . ?
Ag5 C161 Ag16 80.8(2) . . ?
Ag17 C161 Ag16 134.6(2) . . ?
C162 C161 Ag9 87.3(5) . . ?
Ag5 C161 Ag9 114.1(2) . . ?
Ag17 C161 Ag9 76.21(19) . . ?
Ag16 C161 Ag9 75.87(18) . . ?
C161 C162 C163 173.5(7) . . ?
C161 C162 Ag9 65.9(4) . . ?
C163 C162 Ag9 120.6(5) . . ?
C166 C163 C162 108.8(7) . . ?
C166 C163 C164 113.6(8) . . ?
C162 C163 C164 111.0(7) . . ?
C166 C163 C165 109.7(8) . . ?
C162 C163 C165 108.1(8) . . ?
C164 C163 C165 105.5(7) . . ?
C172 C171 Ag6 147.9(6) 2_656 . ?
C172 C171 Ag3 125.6(6) 2_656 . ?
Ag6 C171 Ag3 85.4(2) . . ?
C172 C171 Ag13 87.9(5) 2_656 2_656 ?
Ag6 C171 Ag13 100.2(2) . 2_656 ?
Ag3 C171 Ag13 92.2(2) . 2_656 ?
C171 C172 C173 175.5(8) 2_656 . ?
C171 C172 Ag13 63.3(4) 2_656 . ?
C173 C172 Ag13 120.8(5) . . ?
C176 C173 C174 116.5(8) . . ?
C176 C173 C172 109.6(7) . . ?
C174 C173 C172 109.4(7) . . ?
C176 C173 C175 107.2(8) . . ?
C174 C173 C175 106.4(8) . . ?
C172 C173 C175 107.3(8) . . ?
C182 C181 Ag13 153.4(6) 2_656 . ?
C182 C181 Ag14 95.6(5) 2_656 2_656 ?
Ag13 C181 Ag14 100.3(3) . 2_656 ?
C182 C181 Ag1 111.1(5) 2_656 . ?
Ag13 C181 Ag1 92.2(3) . . ?
Ag14 C181 Ag1 82.2(2) 2_656 . ?
C181 C182 C183 174.6(8) 2_656 . ?
C181 C182 Ag14 57.3(4) 2_656 . ?
C183 C182 Ag14 127.7(5) . . ?
C182 C183 C185 108.6(6) . . ?
C182 C183 C186 109.1(7) . . ?
C185 C183 C186 110.9(7) . . ?
C182 C183 C184 107.7(7) . . ?
C185 C183 C184 111.0(7) . . ?
C186 C183 C184 109.4(7) . . ?
C52 F20 F11 53.5(9) . . ?
C52 F11 F20 58.2(9) . . ?

_refine_diff_density_max         5.723
_refine_diff_density_min         -2.152
_refine_diff_density_rms         0.193

