#=============================================================================== data_SRX-BSA #=============================================================================== _audit_creation_method SHELXL-2013 _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C23 H24 Cl N6 O2, C6 H5 O3 S' _chemical_formula_sum 'C29 H29 Cl N6 O5 S' _chemical_formula_weight 609.09 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'S' 'S' 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cl' 'Cl' 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 7 _space_group_name_H-M_alt 'P c' _space_group_name_Hall 'P -2yc' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' 'x, -y, z+1/2' _cell_length_a 15.4711(18) _cell_length_b 7.0655(6) _cell_length_c 13.0349(12) _cell_angle_alpha 90 _cell_angle_beta 104.993(11) _cell_angle_gamma 90 _cell_volume 1376.4(2) _cell_formula_units_Z 2 _cell_measurement_temperature 120(2) _cell_measurement_reflns_used 1000 _cell_measurement_theta_min 2.7 _cell_measurement_theta_max 26.0 _exptl_crystal_description plate _exptl_crystal_colour colourless _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.470 _exptl_crystal_F_000 636 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.1 _exptl_crystal_size_mid 0.1 _exptl_crystal_size_min 0.05 _exptl_absorpt_coefficient_mu 0.268 _exptl_absorpt_correction_T_max 0.96 _exptl_absorpt_correction_T_min 0.94 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details SADABS _exptl_special_details ; ? ; _diffrn_ambient_temperature 120(2) _diffrn_measurement_device 'three-circle diffractometer' _diffrn_measurement_device_type 'Xcalibur, Eos, Nova' _diffrn_measurement_method '\w and \f scans' _diffrn_radiation_monochromator 'mirror optics' _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_source 'microfocus sealed X-ray tube' _diffrn_source_type 'Incoatec I\ms' _diffrn_reflns_number 11028 _diffrn_reflns_av_unetI/netI 0.1269 _diffrn_reflns_av_R_equivalents 0.0906 _diffrn_reflns_limit_h_min -19 _diffrn_reflns_limit_h_max 15 _diffrn_reflns_limit_k_min -8 _diffrn_reflns_limit_k_max 8 _diffrn_reflns_limit_l_min -15 _diffrn_reflns_limit_l_max 16 _diffrn_reflns_theta_min 2.726 _diffrn_reflns_theta_max 26.000 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measured_fraction_theta_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 1.000 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.841 _diffrn_reflns_point_group_measured_fraction_full 0.846 _reflns_number_total 4538 _reflns_number_gt 3300 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.681 _reflns_Friedel_fraction_max 0.683 _reflns_Friedel_fraction_full 0.691 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection ? _computing_cell_refinement ? _computing_data_reduction ? _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ; ? ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0279P)^2^] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens mixed _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_abs_structure_details ; Flack x determined using 912 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons and Flack (2004), Acta Cryst. A60, s61). ; _refine_ls_abs_structure_Flack -0.02(10) _refine_ls_number_reflns 4538 _refine_ls_number_parameters 385 _refine_ls_number_restraints 2 _refine_ls_R_factor_all 0.1000 _refine_ls_R_factor_gt 0.0689 _refine_ls_wR_factor_ref 0.1229 _refine_ls_wR_factor_gt 0.1092 _refine_ls_goodness_of_fit_ref 1.017 _refine_ls_restrained_S_all 1.017 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C3 C 0.1108(5) -0.1161(10) -0.1146(6) 0.027(2) Uani 1 1 d . . . . . C2 C 0.0234(5) -0.1755(10) -0.1312(6) 0.0244(19) Uani 1 1 d . . . . . H2 H 0.0041 -0.2528 -0.0818 0.029 Uiso 1 1 calc R U . . . C1 C -0.0346(5) -0.1141(10) -0.2256(6) 0.0210(18) Uani 1 1 d . . . . . C6 C -0.0058(5) 0.0028(10) -0.2952(6) 0.0209(18) Uani 1 1 d . . . . . C5 C 0.0813(5) 0.0614(10) -0.2778(6) 0.027(2) Uani 1 1 d . . . . . H5 H 0.0998 0.1397 -0.3273 0.033 Uiso 1 1 calc R U . . . C4 C 0.1410(6) 0.0018(10) -0.1851(6) 0.027(2) Uani 1 1 d . . . . . H4 H 0.2018 0.0403 -0.1691 0.033 Uiso 1 1 calc R U . . . C7 C -0.1483(5) -0.0508(10) -0.3625(6) 0.0241(19) Uani 1 1 d . . . . . C8 C -0.3045(5) -0.1476(10) -0.4196(6) 0.028(2) Uani 1 1 d . . . . . H8A H -0.2841 -0.2434 -0.3630 0.033 Uiso 1 1 calc R U . . . H8B H -0.3306 -0.2161 -0.4867 0.033 Uiso 1 1 calc R U . . . C9 C -0.3771(6) -0.0277(10) -0.3925(6) 0.028(2) Uani 1 1 d . . . . . H9A H -0.4127 -0.1079 -0.3563 0.034 Uiso 1 1 calc R U . . . H9B H -0.3488 0.0735 -0.3425 0.034 Uiso 1 1 calc R U . . . C12 C -0.2328(5) 0.0925(10) -0.5228(6) 0.0269(19) Uani 1 1 d . . . . . H12A H -0.1926 0.0472 -0.5656 0.032 Uiso 1 1 calc R U . . . H12B H -0.2116 0.2191 -0.4948 0.032 Uiso 1 1 calc R U . . . C11 C -0.3278(5) 0.1117(11) -0.5956(6) 0.029(2) Uani 1 1 d . . . . . H11A H -0.3246 0.1894 -0.6577 0.035 Uiso 1 1 calc R U . . . H11B H -0.3488 -0.0158 -0.6224 0.035 Uiso 1 1 calc R U . . . C10 C -0.3983(5) 0.1991(11) -0.5463(6) 0.0259(19) Uani 1 1 d . . . . . H10 H -0.4486 0.2402 -0.6072 0.031 Uiso 1 1 calc R U . . . C13 C -0.3658(6) 0.3763(11) -0.4826(7) 0.040(2) Uani 1 1 d . . . . . H13A H -0.3241 0.3413 -0.4149 0.060 Uiso 1 1 calc R U . . . H13B H -0.4169 0.4440 -0.4690 0.060 Uiso 1 1 calc R U . . . H13C H -0.3351 0.4581 -0.5228 0.060 Uiso 1 1 calc R U . . . C14 C -0.5156(5) -0.0266(11) -0.5281(6) 0.028(2) Uani 1 1 d . . . . . C20 C -0.6002(5) -0.0074(10) -0.7252(6) 0.0224(18) Uani 1 1 d . . . . . C22 C -0.4639(6) -0.3905(11) -0.7441(6) 0.033(2) Uani 1 1 d . . . . . H22 H -0.4113 -0.4659 -0.7262 0.039 Uiso 1 1 calc R U . . . C21 C -0.5400(6) -0.4287(11) -0.8239(6) 0.031(2) Uani 1 1 d . . . . . H21 H -0.5474 -0.5342 -0.8706 0.037 Uiso 1 1 calc R U . . . C19 C -0.6573(5) 0.0888(11) -0.8086(6) 0.0288(19) Uani 1 1 d . . . . . H19 H -0.6699 0.0402 -0.8789 0.035 Uiso 1 1 calc R U . . . C18 C -0.6955(6) 0.2569(12) -0.7875(7) 0.036(2) Uani 1 1 d . . . . . H18 H -0.7352 0.3213 -0.8447 0.043 Uiso 1 1 calc R U . . . C17 C -0.6784(6) 0.3346(10) -0.6876(6) 0.0274(19) Uani 1 1 d . . . . . C16 C -0.6207(5) 0.2396(10) -0.6078(6) 0.0268(19) Uani 1 1 d . . . . . H16 H -0.6075 0.2915 -0.5382 0.032 Uiso 1 1 calc R U . . . C15 C -0.5794(5) 0.0676(11) -0.6234(6) 0.0253(19) Uani 1 1 d . . . . . C24 C -0.0897(5) -0.3892(9) -0.5680(6) 0.0203(18) Uani 1 1 d . . . . . C25 C -0.0979(5) -0.4555(9) -0.4694(6) 0.0220(18) Uani 1 1 d . . . . . H25 H -0.1546 -0.4918 -0.4604 0.026 Uiso 1 1 calc R U . . . C26 C -0.0220(6) -0.4669(10) -0.3856(6) 0.027(2) Uani 1 1 d . . . . . H26 H -0.0265 -0.5174 -0.3196 0.033 Uiso 1 1 calc R U . . . C27 C 0.0600(5) -0.4064(10) -0.3961(6) 0.027(2) Uani 1 1 d . . . . . H27 H 0.1114 -0.4126 -0.3375 0.033 Uiso 1 1 calc R U . . . C28 C 0.0667(5) -0.3364(11) -0.4930(7) 0.030(2) Uani 1 1 d . . . . . H28 H 0.1228 -0.2928 -0.5006 0.036 Uiso 1 1 calc R U . . . C29 C -0.0078(5) -0.3297(10) -0.5791(6) 0.025(2) Uani 1 1 d . . . . . H29 H -0.0024 -0.2840 -0.6457 0.030 Uiso 1 1 calc R U . . . C23 C -0.7210(6) 0.5178(11) -0.6669(7) 0.037(2) Uani 1 1 d . . . . . H23A H -0.7395 0.5903 -0.7330 0.055 Uiso 1 1 calc R U . . . H23B H -0.6777 0.5918 -0.6138 0.055 Uiso 1 1 calc R U . . . H23C H -0.7734 0.4904 -0.6404 0.055 Uiso 1 1 calc R U . . . N6 N -0.4767(5) -0.2307(9) -0.6966(5) 0.0316(18) Uani 1 1 d . . . . . N4 N -0.5591(4) -0.1787(9) -0.7478(5) 0.0265(16) Uani 1 1 d . . . . . N5 N -0.6019(5) -0.2950(9) -0.8258(5) 0.0306(17) Uani 1 1 d . . . . . N3 N -0.4370(4) 0.0585(9) -0.4864(5) 0.0263(16) Uani 1 1 d . . . . . N2 N -0.2260(4) -0.0396(8) -0.4315(5) 0.0209(15) Uani 1 1 d . . . . . N1 N -0.1254(5) -0.1448(9) -0.2702(5) 0.0235(16) Uani 1 1 d . . . . . O5 O -0.1583(4) -0.3103(7) -0.7658(4) 0.0340(15) Uani 1 1 d . . . . . O3 O -0.2117(3) -0.5895(6) -0.6943(4) 0.0249(13) Uani 1 1 d . . . . . O4 O -0.2536(4) -0.2814(8) -0.6454(5) 0.0381(15) Uani 1 1 d . . . . . O2 O -0.5431(4) -0.1678(8) -0.4879(4) 0.0342(15) Uani 1 1 d . . . . . O1 O -0.0783(3) 0.0408(6) -0.3810(4) 0.0241(13) Uani 1 1 d . . . . . S1 S -0.18577(13) -0.3885(3) -0.67738(14) 0.0222(4) Uani 1 1 d . . . . . Cl1 Cl 0.18890(13) -0.1887(3) 0.00007(16) 0.0337(5) Uani 1 1 d . . . . . H1 H -0.158(4) -0.226(8) -0.247(5) 0.005(18) Uiso 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C3 0.033(5) 0.020(4) 0.026(5) -0.010(4) 0.004(4) -0.004(4) C2 0.027(5) 0.024(4) 0.022(4) -0.004(3) 0.007(4) -0.005(4) C1 0.021(5) 0.012(4) 0.030(5) -0.007(3) 0.007(4) -0.002(3) C6 0.022(5) 0.012(4) 0.028(4) -0.005(3) 0.004(4) 0.003(3) C5 0.031(5) 0.025(5) 0.030(5) -0.001(4) 0.013(4) -0.003(4) C4 0.029(5) 0.026(5) 0.027(5) -0.009(4) 0.009(4) -0.011(4) C7 0.025(5) 0.017(4) 0.029(5) -0.009(4) 0.004(4) -0.005(4) C8 0.026(5) 0.019(4) 0.029(5) 0.003(4) -0.007(4) -0.004(4) C9 0.037(5) 0.024(4) 0.024(5) -0.002(4) 0.007(4) -0.013(4) C12 0.028(5) 0.024(4) 0.030(5) 0.006(4) 0.010(4) 0.004(4) C11 0.035(5) 0.020(4) 0.034(5) 0.000(4) 0.010(4) -0.007(4) C10 0.023(5) 0.028(4) 0.029(5) -0.001(4) 0.010(4) -0.006(4) C13 0.046(6) 0.033(5) 0.043(6) -0.001(4) 0.013(5) -0.002(5) C14 0.030(5) 0.026(5) 0.032(5) -0.008(4) 0.014(4) 0.001(4) C20 0.020(4) 0.021(4) 0.027(5) -0.001(4) 0.007(4) 0.001(3) C22 0.040(6) 0.026(5) 0.033(5) -0.004(4) 0.014(4) 0.003(4) C21 0.045(6) 0.025(5) 0.025(5) -0.006(4) 0.013(4) -0.009(4) C19 0.023(5) 0.035(5) 0.027(5) -0.006(4) 0.004(4) -0.006(4) C18 0.033(5) 0.040(5) 0.032(5) 0.002(4) 0.005(4) 0.003(4) C17 0.028(5) 0.025(4) 0.031(5) 0.008(4) 0.011(4) 0.005(4) C16 0.021(5) 0.030(5) 0.031(5) -0.004(4) 0.010(4) -0.001(4) C15 0.020(5) 0.036(5) 0.019(4) 0.001(4) 0.005(4) -0.005(4) C24 0.026(5) 0.007(4) 0.027(4) -0.003(3) 0.005(4) -0.001(3) C25 0.024(5) 0.012(4) 0.031(5) -0.002(3) 0.009(4) -0.002(3) C26 0.038(5) 0.016(4) 0.029(5) 0.000(4) 0.009(4) -0.004(4) C27 0.026(5) 0.021(4) 0.030(5) -0.004(4) -0.002(4) -0.002(4) C28 0.022(5) 0.027(5) 0.040(5) 0.004(4) 0.006(4) -0.006(4) C29 0.033(5) 0.017(4) 0.023(5) 0.000(3) 0.002(4) -0.003(4) C23 0.031(5) 0.029(5) 0.046(6) 0.002(4) 0.000(4) 0.008(4) N6 0.032(4) 0.032(4) 0.025(4) -0.003(3) -0.002(3) -0.001(3) N4 0.025(4) 0.029(4) 0.026(4) -0.004(3) 0.005(3) -0.006(3) N5 0.033(4) 0.028(4) 0.028(4) -0.010(3) 0.003(3) -0.010(3) N3 0.024(4) 0.029(4) 0.023(4) 0.003(3) 0.001(3) -0.004(3) N2 0.023(4) 0.017(3) 0.022(4) 0.001(3) 0.003(3) -0.003(3) N1 0.032(4) 0.018(4) 0.020(4) -0.001(3) 0.005(3) -0.007(3) O5 0.034(4) 0.037(3) 0.026(3) 0.008(3) 0.000(3) -0.008(3) O3 0.027(3) 0.018(3) 0.029(3) -0.003(2) 0.006(3) -0.003(2) O4 0.027(3) 0.036(4) 0.046(4) -0.021(3) 0.002(3) 0.009(3) O2 0.035(4) 0.038(4) 0.027(3) 0.007(3) 0.003(3) -0.014(3) O1 0.026(3) 0.019(3) 0.032(3) 0.001(2) 0.016(3) 0.000(2) S1 0.0229(11) 0.0170(10) 0.0253(11) -0.0024(9) 0.0040(9) 0.0004(9) Cl1 0.0284(12) 0.0391(12) 0.0309(12) -0.0047(10) 0.0030(10) -0.0035(10) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag C3 C2 1.378(11) . ? C3 C4 1.407(10) . ? C3 Cl1 1.739(8) . ? C2 C1 1.391(10) . ? C1 C6 1.384(10) . ? C1 N1 1.392(10) . ? C6 C5 1.370(10) . ? C6 O1 1.390(8) . ? C5 C4 1.383(10) . ? C7 N2 1.305(9) . ? C7 O1 1.336(9) . ? C7 N1 1.339(9) . ? C8 N2 1.476(9) . ? C8 C9 1.521(11) . ? C9 N3 1.463(9) . ? C12 N2 1.495(9) . ? C12 C11 1.535(10) . ? C11 C10 1.532(11) . ? C10 N3 1.483(9) . ? C10 C13 1.514(10) . ? C14 O2 1.251(9) . ? C14 N3 1.339(9) . ? C14 C15 1.525(10) . ? C20 C15 1.387(10) . ? C20 C19 1.388(10) . ? C20 N4 1.432(9) . ? C22 N6 1.327(9) . ? C22 C21 1.381(11) . ? C21 N5 1.341(10) . ? C19 C18 1.386(11) . ? C18 C17 1.375(11) . ? C17 C16 1.359(10) . ? C17 C23 1.508(10) . ? C16 C15 1.411(10) . ? C24 C29 1.377(11) . ? C24 C25 1.405(10) . ? C24 S1 1.773(7) . ? C25 C26 1.383(10) . ? C26 C27 1.380(11) . ? C27 C28 1.385(10) . ? C28 C29 1.386(10) . ? N6 N4 1.329(8) . ? N4 N5 1.341(8) . ? O5 S1 1.438(5) . ? O3 S1 1.477(5) . ? O4 S1 1.440(6) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C2 C3 C4 123.7(8) . . ? C2 C3 Cl1 118.8(6) . . ? C4 C3 Cl1 117.5(6) . . ? C3 C2 C1 115.2(7) . . ? C6 C1 C2 121.5(7) . . ? C6 C1 N1 106.3(7) . . ? C2 C1 N1 132.2(7) . . ? C5 C6 C1 122.8(8) . . ? C5 C6 O1 129.0(7) . . ? C1 C6 O1 108.2(6) . . ? C6 C5 C4 117.3(8) . . ? C5 C4 C3 119.4(8) . . ? N2 C7 O1 119.4(7) . . ? N2 C7 N1 129.2(8) . . ? O1 C7 N1 111.4(7) . . ? N2 C8 C9 114.5(6) . . ? N3 C9 C8 112.5(6) . . ? N2 C12 C11 114.0(6) . . ? C10 C11 C12 116.6(6) . . ? N3 C10 C13 112.8(7) . . ? N3 C10 C11 112.3(6) . . ? C13 C10 C11 113.0(7) . . ? O2 C14 N3 124.0(8) . . ? O2 C14 C15 118.1(7) . . ? N3 C14 C15 117.6(7) . . ? C15 C20 C19 120.3(7) . . ? C15 C20 N4 121.0(7) . . ? C19 C20 N4 118.6(7) . . ? N6 C22 C21 108.5(8) . . ? N5 C21 C22 110.0(7) . . ? C18 C19 C20 118.8(8) . . ? C17 C18 C19 122.8(8) . . ? C16 C17 C18 117.1(7) . . ? C16 C17 C23 121.2(7) . . ? C18 C17 C23 121.7(7) . . ? C17 C16 C15 123.2(7) . . ? C20 C15 C16 117.7(7) . . ? C20 C15 C14 123.6(7) . . ? C16 C15 C14 118.7(7) . . ? C29 C24 C25 120.1(7) . . ? C29 C24 S1 121.2(6) . . ? C25 C24 S1 118.8(6) . . ? C26 C25 C24 118.9(7) . . ? C27 C26 C25 121.2(8) . . ? C26 C27 C28 119.3(7) . . ? C27 C28 C29 120.5(8) . . ? C24 C29 C28 120.0(7) . . ? C22 N6 N4 103.9(7) . . ? N6 N4 N5 115.6(6) . . ? N6 N4 C20 123.3(6) . . ? N5 N4 C20 121.1(7) . . ? N4 N5 C21 102.0(6) . . ? C14 N3 C9 117.7(7) . . ? C14 N3 C10 122.3(6) . . ? C9 N3 C10 117.7(6) . . ? C7 N2 C8 122.2(6) . . ? C7 N2 C12 116.7(7) . . ? C8 N2 C12 121.1(6) . . ? C7 N1 C1 107.5(7) . . ? C7 O1 C6 106.5(6) . . ? O5 S1 O4 114.8(4) . . ? O5 S1 O3 112.0(3) . . ? O4 S1 O3 111.0(3) . . ? O5 S1 C24 106.6(3) . . ? O4 S1 C24 106.9(3) . . ? O3 S1 C24 104.9(3) . . ? _refine_diff_density_max 0.318 _refine_diff_density_min -0.314 _refine_diff_density_rms 0.069 _shelxl_version_number 2013-4 _shelx_res_file ; TITL ST1 in Pc CELL 0.71073 15.471143 7.065511 13.034911 90 104.993 90 ZERR 2 0.001782 0.000559 0.0012 0 0.0108 0 LATT -1 SYMM +X,-Y,0.5+Z SFAC C H N O S Cl UNIT 58 58 12 10 2 2 L.S. 12 PLAN 5 TEMP -153.15 fmap 2 acta MERG 2 OMIT 0 52 WGHT 0.027900 FVAR 1.69848 C3 1 0.110781 -0.116120 -0.114588 11.00000 0.03299 0.02006 = 0.02645 -0.00995 0.00356 -0.00424 C2 1 0.023364 -0.175473 -0.131250 11.00000 0.02749 0.02351 = 0.02243 -0.00415 0.00701 -0.00505 AFIX 43 H2 2 0.004083 -0.252781 -0.081789 11.00000 -1.20000 AFIX 0 C1 1 -0.034592 -0.114148 -0.225600 11.00000 0.02125 0.01215 = 0.02989 -0.00742 0.00709 -0.00218 C6 1 -0.005757 0.002835 -0.295238 11.00000 0.02223 0.01190 = 0.02752 -0.00524 0.00446 0.00266 C5 1 0.081255 0.061402 -0.277777 11.00000 0.03088 0.02474 = 0.02962 -0.00111 0.01287 -0.00336 AFIX 43 H5 2 0.099835 0.139747 -0.327340 11.00000 -1.20000 AFIX 0 C4 1 0.140962 0.001850 -0.185066 11.00000 0.02904 0.02610 = 0.02723 -0.00863 0.00854 -0.01129 AFIX 43 H4 2 0.201831 0.040290 -0.169124 11.00000 -1.20000 AFIX 0 C7 1 -0.148277 -0.050836 -0.362455 11.00000 0.02488 0.01693 = 0.02887 -0.00943 0.00391 -0.00550 C8 1 -0.304471 -0.147610 -0.419577 11.00000 0.02642 0.01873 = 0.02940 0.00292 -0.00731 -0.00378 AFIX 23 H8A 2 -0.284104 -0.243355 -0.363027 11.00000 -1.20000 H8B 2 -0.330649 -0.216140 -0.486672 11.00000 -1.20000 AFIX 0 C9 1 -0.377141 -0.027687 -0.392465 11.00000 0.03732 0.02367 = 0.02367 -0.00157 0.00744 -0.01304 AFIX 23 H9A 2 -0.412710 -0.107900 -0.356323 11.00000 -1.20000 H9B 2 -0.348792 0.073485 -0.342474 11.00000 -1.20000 AFIX 0 C12 1 -0.232831 0.092477 -0.522819 11.00000 0.02802 0.02423 = 0.02996 0.00616 0.01016 0.00378 AFIX 23 H12A 2 -0.192583 0.047197 -0.565567 11.00000 -1.20000 H12B 2 -0.211605 0.219115 -0.494756 11.00000 -1.20000 AFIX 0 C11 1 -0.327828 0.111668 -0.595623 11.00000 0.03487 0.01981 = 0.03386 0.00023 0.01034 -0.00741 AFIX 23 H11A 2 -0.324582 0.189392 -0.657710 11.00000 -1.20000 H11B 2 -0.348782 -0.015842 -0.622410 11.00000 -1.20000 AFIX 0 C10 1 -0.398316 0.199129 -0.546318 11.00000 0.02264 0.02759 = 0.02917 -0.00064 0.00959 -0.00583 AFIX 13 H10 2 -0.448594 0.240157 -0.607234 11.00000 -1.20000 AFIX 0 C13 1 -0.365768 0.376251 -0.482645 11.00000 0.04589 0.03288 = 0.04283 -0.00133 0.01256 -0.00239 AFIX 137 H13A 2 -0.324143 0.341316 -0.414943 11.00000 -1.50000 H13B 2 -0.416948 0.443996 -0.469018 11.00000 -1.50000 H13C 2 -0.335146 0.458088 -0.522761 11.00000 -1.50000 AFIX 0 C14 1 -0.515607 -0.026607 -0.528069 11.00000 0.02952 0.02598 = 0.03195 -0.00785 0.01397 0.00107 C20 1 -0.600154 -0.007393 -0.725173 11.00000 0.01966 0.02117 = 0.02715 -0.00139 0.00721 0.00101 C22 1 -0.463940 -0.390483 -0.744086 11.00000 0.04032 0.02638 = 0.03317 -0.00360 0.01360 0.00258 AFIX 43 H22 2 -0.411331 -0.465887 -0.726200 11.00000 -1.20000 AFIX 0 C21 1 -0.539986 -0.428706 -0.823905 11.00000 0.04481 0.02540 = 0.02463 -0.00618 0.01349 -0.00926 AFIX 43 H21 2 -0.547366 -0.534151 -0.870592 11.00000 -1.20000 AFIX 0 C19 1 -0.657255 0.088816 -0.808588 11.00000 0.02269 0.03493 = 0.02717 -0.00606 0.00380 -0.00607 AFIX 43 H19 2 -0.669895 0.040230 -0.878863 11.00000 -1.20000 AFIX 0 C18 1 -0.695482 0.256939 -0.787540 11.00000 0.03333 0.03991 = 0.03158 0.00202 0.00469 0.00275 AFIX 43 H18 2 -0.735220 0.321347 -0.844655 11.00000 -1.20000 AFIX 0 C17 1 -0.678392 0.334599 -0.687560 11.00000 0.02827 0.02505 = 0.03100 0.00794 0.01146 0.00532 C16 1 -0.620686 0.239598 -0.607816 11.00000 0.02141 0.02965 = 0.03100 -0.00421 0.00966 -0.00107 AFIX 43 H16 2 -0.607490 0.291471 -0.538249 11.00000 -1.20000 AFIX 0 C15 1 -0.579432 0.067628 -0.623379 11.00000 0.02046 0.03644 = 0.01887 0.00086 0.00478 -0.00545 C24 1 -0.089683 -0.389204 -0.568037 11.00000 0.02617 0.00658 = 0.02715 -0.00289 0.00493 -0.00136 C25 1 -0.097884 -0.455465 -0.469372 11.00000 0.02433 0.01207 = 0.03065 -0.00221 0.00890 -0.00214 AFIX 43 H25 2 -0.154580 -0.491801 -0.460352 11.00000 -1.20000 AFIX 0 C26 1 -0.022047 -0.466920 -0.385593 11.00000 0.03760 0.01585 = 0.02881 0.00025 0.00858 -0.00425 AFIX 43 H26 2 -0.026538 -0.517368 -0.319612 11.00000 -1.20000 AFIX 0 C27 1 0.060014 -0.406399 -0.396116 11.00000 0.02601 0.02087 = 0.02984 -0.00393 -0.00193 -0.00190 AFIX 43 H27 2 0.111364 -0.412635 -0.337520 11.00000 -1.20000 AFIX 0 C28 1 0.066734 -0.336448 -0.493028 11.00000 0.02175 0.02744 = 0.03967 0.00396 0.00646 -0.00622 AFIX 43 H28 2 0.122844 -0.292775 -0.500556 11.00000 -1.20000 AFIX 0 C29 1 -0.007789 -0.329697 -0.579092 11.00000 0.03263 0.01677 = 0.02317 0.00007 0.00228 -0.00304 AFIX 43 H29 2 -0.002389 -0.284031 -0.645702 11.00000 -1.20000 AFIX 0 C23 1 -0.720998 0.517812 -0.666888 11.00000 0.03110 0.02877 = 0.04561 0.00177 0.00029 0.00788 AFIX 137 H23A 2 -0.739516 0.590331 -0.733043 11.00000 -1.50000 H23B 2 -0.677715 0.591758 -0.613806 11.00000 -1.50000 H23C 2 -0.773446 0.490394 -0.640382 11.00000 -1.50000 AFIX 0 N6 3 -0.476712 -0.230701 -0.696568 11.00000 0.03221 0.03229 = 0.02525 -0.00252 -0.00188 -0.00125 N4 3 -0.559129 -0.178714 -0.747811 11.00000 0.02453 0.02864 = 0.02572 -0.00355 0.00548 -0.00564 N5 3 -0.601890 -0.294992 -0.825787 11.00000 0.03348 0.02801 = 0.02760 -0.00970 0.00323 -0.01016 N3 3 -0.436988 0.058476 -0.486371 11.00000 0.02425 0.02925 = 0.02266 0.00277 0.00140 -0.00397 N2 3 -0.226013 -0.039575 -0.431482 11.00000 0.02260 0.01713 = 0.02186 0.00124 0.00348 -0.00261 N1 3 -0.125434 -0.144837 -0.270214 11.00000 0.03172 0.01800 = 0.02008 -0.00069 0.00538 -0.00693 O5 4 -0.158301 -0.310323 -0.765779 11.00000 0.03437 0.03724 = 0.02592 0.00764 -0.00011 -0.00815 O3 4 -0.211707 -0.589531 -0.694305 11.00000 0.02727 0.01813 = 0.02855 -0.00275 0.00586 -0.00314 O4 4 -0.253589 -0.281432 -0.645354 11.00000 0.02745 0.03642 = 0.04607 -0.02052 0.00185 0.00857 O2 4 -0.543059 -0.167847 -0.487899 11.00000 0.03519 0.03772 = 0.02680 0.00715 0.00285 -0.01415 O1 4 -0.078275 0.040783 -0.380980 11.00000 0.02567 0.01949 = 0.03181 0.00052 0.01574 -0.00028 S1 5 -0.185774 -0.388544 -0.677378 11.00000 0.02293 0.01701 = 0.02526 -0.00238 0.00396 0.00039 CL1 6 0.188901 -0.188673 0.000073 11.00000 0.02841 0.03910 = 0.03095 -0.00472 0.00296 -0.00346 H1 2 -0.157614 -0.225748 -0.246969 11.00000 0.00486 HKLF 4 REM ST1 in Pc REM R1 = 0.0689 for 3300 Fo > 4sig(Fo) and 0.1000 for all 4538 data REM 385 parameters refined using 2 restraints END WGHT 0.0279 0.0000 REM Highest difference peak 0.318, deepest hole -0.314, 1-sigma level 0.069 Q1 1 -0.3035 0.2474 -0.4985 11.00000 0.05 0.32 Q2 1 -0.4974 0.1059 -0.6476 11.00000 0.05 0.30 Q3 1 -0.0792 -0.2713 -0.4544 11.00000 0.05 0.29 Q4 1 0.2395 -0.0779 -0.0061 11.00000 0.05 0.26 Q5 1 -0.2209 -0.2475 -0.2853 11.00000 0.05 0.25 ; _shelx_res_checksum 56713 _shelx_hkl_file ; -20 0 -1 20.8522 73.8223 8 -20 0 0 4.90617 95.8737 8 -20 0 1-67.8653 99.4962 8 -20 0 2 161.797 130.824 8 -20 -1 -1 89.6838 129.645 8 -20 1 0 232.434 171.981 8 -20 1 1-143.762 127.177 8 -20 1 2 28.4112 141.330 8 -20 1 3 75.2698 177.009 8 -20 2 0 34.4066 110.456 8 -20 2 1 212.173 169.848 8 -19 0 -2 12.3592 60.7890 8 -19 0 -1-11.0834 63.9755 8 -19 0 0 466.369 208.137 8 -19 0 0 200.478 129.503 3 -19 0 1 7.26848 73.0631 8 -19 0 2 514.136 222.966 8 -19 0 3 77.0924 101.306 8 -19 0 4 155.212 155.347 8 -19 0 5 104.695 220.045 8 -19 0 6 533.154 255.028 8 -19 0 7 96.4893 154.799 8 -19 -1 -2 103.542 125.313 8 -19 -1 -1 406.661 184.659 8 -19 1 -1 369.352 177.186 8 -19 -1 0 254.278 172.561 8 -19 1 0 324.755 182.676 8 -19 1 1-215.670 143.730 8 -19 -1 1-36.2846 80.8326 8 -19 -1 2-31.0959 79.6402 8 -19 1 2 62.1520 70.7967 8 -19 1 3 460.876 209.520 8 -19 -1 3 471.117 230.939 8 -19 1 4 1014.81 312.856 8 -19 -1 4 983.302 340.557 8 -19 -1 5 180.286 151.405 8 -19 1 5 397.514 206.038 8 -19 1 6-36.5148 83.8178 8 -19 -1 6-47.9879 129.953 8 -19 1 7 152.016 160.165 8 -19 -2 -3 328.148 262.257 8 -19 -2 -2 31.8154 111.744 8 -19 -2 -1 339.983 195.929 8 -19 2 -1-78.7446 94.0074 8 -19 -2 0 1.30802 120.382 8 -19 2 0 47.7659 117.105 8 -19 -2 1 189.014 180.634 8 -19 2 1 203.249 160.076 8 -19 2 2 336.513 190.488 8 -19 -2 2 199.412 154.980 8 -19 -2 3 285.816 196.910 8 -19 2 3 113.693 132.900 8 -19 2 4 398.611 200.646 8 -19 -2 4 103.868 149.770 8 -19 2 5 582.604 261.403 8 -19 2 6 15.6470 68.0741 8 -19 3 0 208.862 194.336 8 -19 3 1 14.0309 82.0417 8 -19 3 2 88.4154 128.875 8 -19 3 3 196.655 74.7784 8 -19 3 4 500.012 262.825 8 -19 4 1-239.988 162.913 8 -18 0 -3 5.94222 105.074 3 -18 0 -2 692.026 293.718 3 -18 0 -2 76.8711 56.7278 8 -18 0 -1 140.660 162.808 8 -18 0 -1 204.484 218.636 3 -18 0 0 458.415 216.486 8 -18 0 1 125.066 108.298 8 -18 0 2 588.882 274.207 8 -18 0 3-122.355 118.712 8 -18 0 4 694.774 243.473 8 -18 0 5 83.3133 113.822 8 -18 0 6 151.833 155.941 8 -18 0 7 290.668 176.670 8 -18 0 8 305.028 189.426 8 -18 0 9 262.443 171.113 8 -18 0 10 637.714 249.974 8 -18 1 -4 503.520 224.946 3 -18 -1 -3 207.391 133.320 8 -18 1 -3 667.451 293.454 3 -18 -1 -2 125.094 117.117 8 -18 -1 -2 452.964 251.532 3 -18 1 -2 294.951 157.012 8 -18 1 -2 98.4067 76.9478 3 -18 -1 -1 50.6389 69.8589 3 -18 1 -1 45.4259 71.8737 8 -18 -1 -1 248.038 153.098 8 -18 -1 0 89.4478 102.314 3 -18 -1 0 72.7698 109.016 8 -18 1 0-6.87989 104.521 8 -18 1 1-0.34929 86.4353 8 -18 -1 1 163.881 148.280 3 -18 -1 1 392.002 190.154 8 -18 -1 2 125.881 132.309 8 -18 1 2 40.1243 76.1894 8 -18 -1 3 287.394 185.175 8 -18 1 3 282.724 171.891 8 -18 1 4 642.892 236.910 8 -18 -1 4 401.222 205.472 8 -18 -1 5 105.012 154.389 8 -18 1 5 280.864 181.001 8 -18 -1 6 486.982 216.066 8 -18 1 6 213.956 147.040 8 -18 1 7 270.589 148.988 8 -18 -1 7 404.205 217.230 8 -18 1 8 268.801 187.135 8 -18 -1 8 356.376 201.565 8 -18 -1 9 434.357 223.419 8 -18 1 9 259.280 174.535 8 -18 2 -4 821.625 241.903 2 -18 2 -4 61.2675 93.5613 3 -18 -2 -3 185.631 157.129 8 -18 2 -3 437.138 246.330 3 -18 -2 -2 0.39557 151.285 8 -18 -2 -1 127.722 118.543 8 -18 -2 -1 255.916 166.835 3 -18 2 -1 263.226 161.988 8 -18 2 0 13.7825 74.3061 8 -18 -2 0 43.4083 67.9578 8 -18 -2 0 123.158 154.052 3 -18 2 1 316.295 157.336 8 -18 -2 1 307.571 195.951 8 -18 -2 1 288.593 227.002 3 -18 2 2 21.2356 112.016 8 -18 -2 2 73.5994 128.797 8 -18 -2 2-73.0819 146.585 3 -18 -2 3 624.680 252.946 8 -18 2 3 518.993 225.163 8 -18 -2 4 263.491 165.890 8 -18 2 4 409.083 209.824 8 -18 2 5 139.400 161.521 8 -18 -2 5-52.9067 94.2779 8 -18 -2 6 753.655 272.600 8 -18 2 6 360.468 226.094 8 -18 2 7 38.6984 143.086 8 -18 -2 7 81.3572 101.250 8 -18 2 8 556.731 258.560 8 -18 -2 8 88.7938 109.996 8 -18 3 -3-199.841 153.241 3 -18 -3 -3 128.153 151.491 8 -18 -3 -2 240.132 187.993 8 -18 3 -1 210.006 192.857 8 -18 -3 -1 447.975 225.648 8 -18 -3 0-102.381 86.2862 8 -18 3 0 225.708 194.066 8 -18 -3 1 348.924 226.973 3 -18 3 1 423.633 215.954 8 -18 -3 1 336.547 201.882 8 -18 -3 2 658.299 302.493 3 -18 3 2 699.560 255.393 8 -18 -3 2 671.163 335.844 8 -18 3 3 50.9567 113.173 8 -18 -3 3 254.139 217.225 8 -18 -3 3-55.6049 109.052 3 -18 3 4 2.89740 62.6462 8 -18 -3 4 87.0758 142.343 8 -18 -3 4 114.284 161.878 3 -18 3 5 111.653 161.908 8 -18 -3 5 332.443 209.877 8 -18 -3 5 739.761 281.685 3 -18 -3 6 586.602 239.273 8 -18 3 6 290.328 174.302 8 -18 4 0-163.998 133.979 8 -18 4 1 250.526 169.010 8 -18 4 2 69.4809 169.584 8 -18 4 3 436.528 232.873 8 -18 4 4 555.348 237.701 8 -18 -4 4 306.919 215.019 3 -18 -4 5 139.652 123.866 3 -18 -4 6 13.1175 110.494 3 -18 -4 7 776.844 298.290 3 -18 -4 8 45.4055 111.611 3 -17 0 -5-30.0999 73.9379 3 -17 0 -4 631.868 267.129 3 -17 0 -3 99.4954 80.3203 8 -17 0 -3-26.0475 70.7914 3 -17 0 -2 630.504 220.787 8 -17 0 -2 749.951 288.632 3 -17 0 -1 291.993 177.948 3 -17 0 -1-96.6638 75.7828 8 -17 0 0-11.6855 67.1285 8 -17 0 1 18.9329 126.649 8 -17 0 2 633.421 228.225 8 -17 0 3-15.2747 61.8015 8 -17 0 4 1026.81 278.024 8 -17 0 5 156.024 160.991 8 -17 0 6 422.195 182.990 8 -17 0 7 221.003 159.160 8 -17 0 8 938.277 285.190 8 -17 0 9-138.224 124.111 8 -17 0 10 139.384 139.815 8 -17 0 11 56.1618 136.555 8 -17 0 12 264.273 239.735 8 -17 1 -6 306.834 203.609 3 -17 1 -5-63.8085 105.361 3 -17 -1 -4 303.705 198.453 3 -17 1 -4 286.026 184.706 3 -17 1 -3 463.099 220.394 3 -17 -1 -3 409.793 200.819 3 -17 -1 -3 164.228 149.346 8 -17 -1 -2 535.006 219.173 8 -17 1 -2 350.554 174.370 8 -17 -1 -2 548.528 250.145 3 -17 1 -2 597.604 270.263 3 -17 -1 -1 501.979 193.357 8 -17 1 -1 899.093 257.229 8 -17 -1 -1 540.145 250.573 3 -17 -1 0 203.102 174.982 3 -17 1 0 215.455 145.137 8 -17 -1 0 301.233 165.963 8 -17 -1 1 785.304 251.197 8 -17 1 1 601.321 210.516 8 -17 1 2 308.032 164.432 8 -17 -1 2 212.179 125.242 8 -17 1 3 100.522 114.673 8 -17 -1 3 29.9148 64.0235 8 -17 1 4 173.408 110.289 8 -17 -1 4 37.3663 68.4796 8 -17 -1 5 480.033 188.488 8 -17 1 5 858.545 291.202 8 -17 1 6 43.7573 115.724 8 -17 -1 6 177.274 189.144 8 -17 -1 7 60.8377 83.5745 8 -17 1 7 468.461 219.597 8 -17 1 8 441.713 216.054 8 -17 -1 8 240.978 151.665 8 -17 1 9 403.136 207.447 8 -17 -1 9 160.293 137.764 8 -17 -1 10-136.996 124.280 8 -17 1 10 217.565 199.336 8 -17 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333.967 144.577 8 -11 1 1 159.936 90.1906 8 -11 1 2 10.7321 79.9525 8 -11 -1 2 74.1620 72.8818 8 -11 1 3 831.606 193.324 8 -11 -1 3 773.233 195.191 8 -11 -1 4 866.789 212.555 8 -11 -1 4 902.586 117.299 5 -11 1 4 694.209 195.294 8 -11 -1 5 179.666 130.793 8 -11 1 5 68.3573 90.8819 8 -11 -1 5 89.7823 48.5138 5 -11 -1 6 880.946 221.273 8 -11 -1 6 799.670 134.615 5 -11 1 6 833.659 208.990 8 -11 -1 7 607.468 196.212 8 -11 1 7 639.060 198.985 8 -11 -1 8 2336.05 352.624 8 -11 1 8 2546.12 378.983 8 -11 -1 9 2075.79 338.929 8 -11 1 9 2009.76 343.479 8 -11 1 10 1283.47 283.499 8 -11 -1 10 1184.24 276.268 8 -11 -1 11 999.898 250.642 8 -11 1 11 824.049 234.446 8 -11 1 12 466.810 188.419 8 -11 -1 12 518.684 178.713 8 -11 -1 13 146.694 102.327 8 -11 1 13 84.2416 129.387 8 -11 -1 14 281.453 164.685 8 -11 -1 14 74.1218 73.8607 7 -11 1 14 73.2717 98.9375 8 -11 1 14 31.9819 86.4465 7 -11 -1 15 401.014 175.824 7 -11 1 15 568.507 238.389 8 -11 1 15 154.639 144.178 7 -11 -2 -11 318.913 229.469 3 -11 -2 -10 288.257 208.883 3 -11 2 -10-10.4545 114.023 2 -11 2 -9 357.107 166.632 2 -11 -2 -9 432.426 226.046 3 -11 2 -8 788.916 233.306 3 -11 -2 -8 781.686 275.766 3 -11 2 -8 1247.83 301.219 2 -11 2 -7 722.517 211.294 2 -11 -2 -7 934.097 300.122 3 -11 2 -7 446.555 154.953 1 -11 2 -7 568.268 183.028 3 -11 -2 -7 530.542 169.651 8 -11 2 -6 690.541 211.573 3 -11 2 -6 882.157 238.525 2 -11 2 -6 540.646 192.632 1 -11 -2 -6 746.399 268.436 3 -11 -2 -6 929.545 228.043 8 -11 2 -5 469.492 147.853 8 -11 2 -5 484.527 160.295 2 -11 -2 -5 500.762 186.596 8 -11 -2 -5 356.905 168.335 3 -11 2 -5 331.702 141.727 3 -11 -2 -4 278.732 152.372 8 -11 -2 -4 214.905 147.006 3 -11 2 -4 462.905 155.713 8 -11 2 -4 263.653 119.570 2 -11 2 -4 277.809 148.830 3 -11 -2 -3 210.101 152.835 3 -11 2 -3 382.707 140.183 2 -11 2 -3 463.702 152.425 8 -11 -2 -3 387.998 193.388 8 -11 2 -2 829.499 171.645 2 -11 2 -2 1117.05 225.940 8 -11 -2 -2 1011.34 246.299 8 -11 -2 -2 799.582 239.639 3 -11 -2 -1 1018.74 258.882 8 -11 2 -1 914.940 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107.811 8 -11 -3 0 290.928 162.551 8 -11 3 1 852.087 154.396 2 -11 3 1 927.437 229.382 8 -11 -3 1 666.815 227.979 3 -11 -3 1 681.296 242.154 8 -11 -3 2 251.969 115.201 8 -11 3 2 332.509 158.965 8 -11 -3 2 181.936 141.314 3 -11 -3 3 100.237 72.0349 8 -11 3 3 173.279 107.525 8 -11 -3 3 418.887 199.966 3 -11 -3 4 1524.44 296.124 8 -11 3 4 1068.17 248.986 8 -11 -3 5 210.267 150.151 8 -11 3 5 173.978 99.0724 8 -11 3 5 166.809 48.4484 5 -11 3 6 2027.86 369.007 8 -11 3 6 1972.10 176.127 5 -11 -3 6 1935.06 340.282 8 -11 3 7 20.8640 35.4565 5 -11 -3 7 78.4475 76.1181 8 -11 3 7 121.554 106.794 8 -11 3 8 675.223 211.095 8 -11 -3 8 507.643 179.679 8 -11 -3 9 138.209 121.526 8 -11 3 9 195.384 112.691 8 -11 3 10 1365.07 318.634 8 -11 -3 10 1044.25 261.600 8 -11 3 11 153.817 147.469 8 -11 -3 11 351.531 162.561 8 -11 3 12 286.253 144.605 8 -11 -3 12 299.273 152.054 8 -11 3 13 549.184 184.459 7 -11 -3 13 431.281 168.105 8 -11 -3 13 398.431 170.205 7 -11 3 14 133.892 105.200 7 -11 -3 14 25.9506 151.173 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14 833.999 249.043 7 -4 -2 14 190.865 121.699 7 -4 2 15 424.694 202.899 7 -4 -2 15 545.299 215.064 7 -4 2 16-104.421 108.787 7 -4 -3 -14 500.661 315.613 3 -4 3 -14 11.2292 98.6720 4 -4 3 -13 315.646 185.700 2 -4 -3 -13 361.457 247.064 3 -4 3 -13 169.954 164.535 4 -4 3 -12 406.203 192.704 2 -4 -3 -12 658.565 259.540 3 -4 3 -12 249.655 168.297 4 -4 3 -11 216.817 153.512 2 -4 -3 -11 358.606 224.680 3 -4 3 -11 207.570 142.373 4 -4 3 -10 795.089 223.265 2 -4 -3 -10 839.529 279.785 3 -4 3 -10 946.447 284.595 4 -4 3 -10 712.045 203.256 1 -4 3 -9 810.721 234.898 2 -4 3 -9 690.142 185.108 1 -4 -3 -9 495.462 211.373 3 -4 3 -9 482.170 197.697 4 -4 3 -8 428.431 145.495 1 -4 3 -8 452.201 156.441 4 -4 3 -8 265.882 123.579 2 -4 -3 -8 613.291 218.938 3 -4 3 -8 293.179 75.3443 3 -4 3 -7 312.345 132.112 2 -4 3 -7 210.286 64.7336 3 -4 -3 -7 555.351 195.641 3 -4 3 -7 137.591 107.073 4 -4 -3 -7 270.129 70.9732 1 -4 3 -7 179.739 82.5884 1 -4 -3 -6 3165.98 445.025 3 -4 3 -6 2440.44 304.247 1 -4 3 -6 2815.64 390.320 4 -4 -3 -6 2057.53 213.927 1 -4 3 -6 2646.18 210.275 3 -4 3 -6 2402.22 316.344 2 -4 -3 -6 2711.46 432.617 6 -4 3 -5 736.455 108.017 3 -4 3 -5 874.330 194.035 2 -4 -3 -5 676.548 213.367 3 -4 3 -5 818.917 170.119 1 -4 3 -5 720.788 202.677 4 -4 -3 -5 783.935 153.838 1 -4 -3 -5 772.447 228.907 6 -4 3 -4 1052.79 195.595 2 -4 -3 -4 1500.35 290.445 3 -4 3 -4 1484.58 225.628 1 -4 3 -4 1222.47 237.623 4 -4 -3 -4 986.906 252.412 6 -4 -3 -3 1627.99 272.690 3 -4 3 -3 2476.43 280.931 1 -4 3 -3 2446.26 313.654 4 -4 -3 -3 2216.22 332.214 6 -4 3 -2 65.5980 62.2109 1 -4 -3 -2 114.654 93.5732 3 -4 3 -2 61.5970 44.3652 7 -4 -3 -2 100.563 78.3678 6 -4 -3 -1 49.5099 94.5844 6 -4 -3 -1 156.699 109.890 3 -4 3 -1 163.780 96.3519 1 -4 3 0 7373.41 401.681 5 -4 3 0 7835.79 470.107 1 -4 -3 0 8555.82 556.228 3 -4 -3 0 7615.32 504.409 6 -4 -3 1 1481.88 208.323 6 -4 3 1 1576.78 174.888 5 -4 3 1 1741.93 227.077 1 -4 -3 1 2109.16 263.944 3 -4 3 2 3335.42 260.168 5 -4 -3 2 3247.10 309.757 3 -4 3 2 3757.80 328.440 1 -4 -3 2 3239.38 298.435 6 -4 3 3 8783.68 435.851 5 -4 3 3 9577.26 493.010 1 -4 -3 3 9497.39 492.569 3 -4 -3 3 9163.51 487.284 6 -4 3 4 13892.9 595.029 1 -4 -3 4 13008.9 558.601 3 -4 3 5 4058.06 312.436 1 -4 3 6 359.489 97.6438 1 -4 3 6 259.680 91.4287 7 -4 -3 7 61.6379 63.0506 8 -4 3 7 199.275 82.0117 7 -4 -3 7 12.2011 66.9261 7 -4 3 7 95.5690 60.7082 1 -4 -3 8 1125.76 186.941 8 -4 3 8 1686.05 184.423 1 -4 3 8 1554.72 227.514 7 -4 -3 8 999.092 138.546 3 -4 -3 8 907.245 204.404 7 -4 -3 9 161.406 84.1786 8 -4 3 9 241.621 72.6053 1 -4 3 9 91.9260 81.9357 7 -4 -3 9 169.723 114.438 7 -4 3 10 832.586 126.768 1 -4 -3 10 985.583 170.025 8 -4 3 10 941.997 207.398 7 -4 -3 10 1020.14 241.660 7 -4 3 11 209.708 129.934 7 -4 -3 11 35.7073 90.3849 7 -4 3 12 2288.78 355.664 7 -4 -3 12 2124.49 373.160 7 -4 3 13 129.561 116.191 7 -4 -3 13 226.980 149.094 7 -4 3 14 188.842 118.170 7 -4 -3 14 141.714 113.259 7 -4 -3 15 474.009 217.188 7 -4 3 15 550.829 204.885 7 -4 3 16 90.9763 88.6971 7 -4 4 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240.008 3 -4 -4 -3 3267.45 257.188 7 -4 -4 -2 413.208 140.558 6 -4 -4 -2 623.557 170.073 3 -4 4 -2 351.603 121.656 1 -4 4 -2 405.648 104.632 3 -4 4 -2 456.091 96.7726 7 -4 -4 -1 217.576 120.812 6 -4 -4 -1 294.585 133.958 3 -4 4 -1 224.649 110.082 1 -4 4 -1 284.296 88.4089 3 -4 4 -1 225.357 61.6441 7 -4 -4 0 1002.82 211.684 6 -4 -4 0 1272.81 234.430 3 -4 4 0 1014.48 194.634 1 -4 4 0 1067.20 179.444 5 -4 4 0 1133.59 121.603 7 -4 -4 1 328.277 128.454 6 -4 4 1 358.516 115.403 1 -4 -4 1 193.441 81.5607 3 -4 4 1 278.712 109.796 5 -4 4 2 956.862 177.259 5 -4 -4 2 685.509 160.756 6 -4 4 2 984.870 173.644 1 -4 -4 2 1086.79 197.735 3 -4 -4 3 196.713 117.255 6 -4 -4 3 381.142 123.227 3 -4 4 3 392.621 120.811 1 -4 4 3 256.138 88.6039 5 -4 4 4 1858.40 234.913 5 -4 4 4 2156.49 256.400 1 -4 -4 4 1877.61 224.972 3 -4 4 5 5613.33 413.122 5 -4 4 5 5696.56 416.160 1 -4 4 5 5328.26 318.940 7 -4 -4 5 6078.78 375.688 3 -4 4 6 4933.01 336.691 7 -4 4 6 6114.52 425.648 1 -4 -4 6 4933.29 424.992 7 -4 -4 6 5075.41 312.286 3 -4 -4 7 444.682 84.4525 3 -4 4 7 517.603 132.851 1 -4 4 7 839.140 148.655 7 -4 -4 7 834.755 192.066 7 -4 4 8 998.582 180.068 1 -4 -4 8 587.628 165.148 8 -4 4 8 739.689 147.851 7 -4 -4 8 588.664 162.398 7 -4 -4 9 170.540 85.2010 8 -4 4 9 388.247 113.570 1 -4 -4 9 310.460 131.117 7 -4 4 9 209.235 73.8759 7 -4 -4 10 652.886 161.681 8 -4 4 10 620.454 158.176 7 -4 -4 10 391.547 157.070 7 -4 4 10 351.050 113.657 1 -4 -4 11 128.321 111.201 7 -4 4 11 19.7654 58.0502 7 -4 4 12-8.97478 54.9868 7 -4 -4 12-45.2284 97.0288 7 -4 4 13 635.983 197.660 7 -4 -4 13 557.615 216.312 7 -4 -4 14 485.697 197.148 7 -4 4 14 461.847 184.585 7 -4 4 15 168.825 115.559 7 -4 -4 15 205.849 129.632 7 -4 5 -12 579.001 257.132 4 -4 -5 -11 122.407 178.073 3 -4 5 -11 148.819 143.994 4 -4 5 -10 116.666 100.299 1 -4 -5 -10 259.421 188.578 3 -4 5 -10 123.370 148.411 4 -4 -5 -9 813.666 284.237 3 -4 5 -9 489.681 212.358 4 -4 -5 -9 663.565 284.438 6 -4 5 -9 498.949 198.893 1 -4 -5 -8 716.667 263.659 3 -4 5 -8 294.651 160.761 4 -4 5 -8 571.757 203.307 1 -4 -5 -8 863.256 331.180 6 -4 5 -7 657.452 220.034 1 -4 5 -7 504.757 208.224 4 -4 -5 -7 770.938 267.370 3 -4 -5 -7 781.976 281.026 6 -4 5 -6 814.632 223.799 1 -4 -5 -6 634.862 233.388 3 -4 5 -6 553.510 204.840 4 -4 -5 -6 441.600 211.857 6 -4 -5 -5 190.937 91.0723 3 -4 -5 -5 168.785 121.082 6 -4 5 -5 195.235 154.734 1 -4 5 -4 3362.89 411.926 1 -4 -5 -4 4134.75 540.236 3 -4 -5 -4 2419.20 420.901 6 -4 -5 -3 1686.76 331.686 6 -4 -5 -3 1955.36 360.949 3 -4 5 -3 1488.85 282.320 1 -4 5 -3 1180.84 161.007 3 -4 5 -2 122.020 108.807 1 -4 -5 -2-74.1255 98.7141 3 -4 5 -2 158.788 67.5808 3 -4 5 -2 113.139 35.4894 7 -4 -5 -1 182.101 91.4353 6 -4 -5 -1 398.438 171.574 3 -4 5 -1 239.713 125.333 1 -4 5 -1 133.566 52.0497 7 -4 -5 0 48.6383 93.2968 6 -4 5 0 3.09570 82.0017 5 -4 -5 0 131.229 120.178 3 -4 5 0 21.4023 93.5261 1 -4 5 0 10.2879 27.0942 7 -4 -5 1 39.0585 67.2551 6 -4 5 1 176.308 88.8630 5 -4 -5 1 214.222 112.781 3 -4 5 1 306.087 123.845 1 -4 5 1 117.702 28.0561 7 -4 5 2 3573.31 372.711 5 -4 5 2 3257.69 366.647 1 -4 -5 2 3906.74 401.244 3 -4 -5 2 3746.38 441.048 6 -4 -5 3 520.598 172.325 6 -4 -5 3 490.560 136.134 3 -4 5 3 523.749 156.907 1 -4 5 3 532.296 147.400 5 -4 5 4 2961.69 342.875 5 -4 5 4 1977.82 123.242 7 -4 5 4 3205.03 359.153 1 -4 -5 4 2742.24 276.553 7 -4 -5 4 2393.85 273.460 3 -4 -5 4 2568.71 354.288 6 -4 5 5 2043.49 285.599 5 -4 -5 5 1837.25 248.095 7 -4 5 5 1682.45 256.335 1 -4 5 5 1479.99 130.628 7 -4 -5 5 1524.77 194.979 3 -4 5 6 1279.98 225.905 5 -4 5 6 1314.08 235.789 1 -4 5 6 1187.43 136.916 7 -4 -5 6 1444.42 227.201 7 -4 5 7 27.8838 43.0710 7 -4 5 7-63.0631 69.7364 5 -4 -5 7 135.269 95.1930 7 -4 5 7 37.1604 65.7732 1 -4 5 8 747.441 136.835 7 -4 -5 8 953.472 210.028 7 -4 5 8 1200.32 224.646 1 -4 5 9 128.075 85.2929 1 -4 -5 9 103.583 93.0977 7 -4 5 9 94.9135 53.4462 7 -4 -5 9 139.552 102.734 8 -4 5 10 220.924 96.7260 7 -4 -5 10 85.8056 95.5128 7 -4 -5 11 38.2251 65.2018 7 -4 -5 12 207.313 158.511 7 -4 -5 13-55.0450 99.2971 7 -4 -5 14 429.678 199.615 7 -4 6 -11 206.641 163.211 4 -4 6 -10 153.675 154.984 1 -4 6 -10 446.190 233.918 4 -4 -6 -10 701.541 296.009 3 -4 6 -9 124.980 160.761 1 -4 6 -9 71.6482 94.9611 4 -4 -6 -9 293.878 240.179 3 -4 -6 -9 10.6572 121.542 6 -4 6 -8 414.359 187.112 1 -4 -6 -8 420.621 234.251 3 -4 -6 -8 43.2474 91.7978 6 -4 -6 -7 397.611 229.881 3 -4 6 -7 732.654 259.117 1 -4 -6 -7 663.249 287.022 6 -4 6 -6 220.262 142.355 1 -4 -6 -6 277.904 223.243 3 -4 -6 -6 596.050 265.757 6 -4 -6 -5 33.1373 88.8251 3 -4 6 -5 38.6548 80.9298 1 -4 -6 -5 76.5220 127.322 6 -4 6 -4 1563.70 321.786 1 -4 -6 -4 1849.36 399.898 3 -4 -6 -4 1138.79 327.048 6 -4 -6 -3 31.8795 128.973 6 -4 6 -3 96.2963 101.597 1 -4 -6 -3 43.8351 79.3046 3 -4 6 -2 1016.77 254.366 1 -4 -6 -2 397.108 207.669 6 -4 -6 -2 524.234 201.816 3 -4 -6 -1 703.727 249.063 6 -4 -6 -1 728.540 231.605 3 -4 6 -1 461.970 182.321 1 -4 -6 0 1710.94 335.848 6 -4 6 0 1690.42 290.809 5 -4 -6 0 1844.47 341.145 3 -4 6 0 1549.70 290.676 1 -4 -6 1 537.857 217.899 6 -4 6 1 611.035 174.140 5 -4 -6 1 578.555 179.945 3 -4 6 1 431.182 164.283 1 -4 -6 2 369.721 165.134 6 -4 6 2 65.4314 69.2342 5 -4 -6 2 259.270 146.160 3 -4 6 2 71.2621 79.1424 1 -4 6 3 3077.97 378.514 5 -4 -6 3 2810.99 418.613 6 -4 -6 3 2989.00 351.128 3 -4 6 3 1861.42 314.841 1 -4 -6 4 1189.38 281.263 6 -4 6 4 1437.46 266.419 5 -4 6 4 1060.05 235.766 1 -4 -6 5 1807.19 334.057 6 -4 -6 5 1314.20 200.116 7 -4 6 5 1469.79 266.638 5 -4 6 5 1591.13 289.380 1 -4 6 6 1163.28 247.581 1 -4 6 6 1155.75 246.502 5 -4 -6 6 933.180 174.806 7 -4 6 7 1137.18 246.599 1 -4 -6 7 1716.85 257.870 7 -4 6 7 1344.54 261.200 5 -4 -6 8 335.434 146.036 7 -4 6 8 72.7964 84.8555 1 -4 6 8 321.133 142.092 5 -4 6 9 64.1981 95.9298 5 -4 -6 9 176.479 115.242 7 -4 6 10 244.227 119.627 5 -4 -6 10 15.9676 66.0027 7 -4 -6 11 180.733 117.863 7 -4 -6 12 261.959 140.076 7 -4 -6 13 67.7526 90.1922 7 -4 -6 14-92.5660 100.571 7 -4 7 -10 156.352 195.858 1 -4 7 -9 28.1254 137.654 1 -4 -7 -8 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159.994 5 -4 7 4 47.3802 59.0165 1 -4 -7 5 97.0320 145.752 6 -4 7 5 135.492 116.956 5 -4 7 5 321.462 165.611 1 -4 -7 6 160.420 119.812 6 -4 7 6 249.529 161.819 5 -4 7 6 133.089 119.236 1 -4 7 7 1057.59 250.219 5 -4 7 7 283.451 157.713 1 -4 7 8 322.372 143.024 5 -4 7 8 172.856 161.389 1 -4 7 9 11.6503 113.463 5 -4 7 10 63.1940 106.503 5 -4 7 11 224.082 177.152 5 -4 -8 -6 758.139 314.582 3 -4 8 -5-27.6124 118.947 1 -4 -8 -5 184.256 186.809 3 -4 -8 -5-45.7031 150.552 6 -4 8 -4 175.041 172.724 1 -4 -8 -4-165.210 78.1059 3 -4 -8 -4 26.0236 180.326 6 -4 -8 -3 28.2617 151.508 6 -4 -8 -3 78.8503 101.672 3 -4 8 -3 294.146 186.847 1 -4 -8 -2 325.936 232.616 6 -4 -8 -2-7.40675 71.6474 3 -4 8 -2 76.1484 118.895 1 -4 -8 -1 275.711 213.747 6 -4 -8 -1 39.6442 80.8346 3 -4 8 -1 301.129 181.349 1 -4 -8 0 87.3453 96.0066 6 -4 8 0-66.0568 98.4327 1 -4 -8 1 190.936 181.780 6 -4 8 1 146.029 124.853 5 -4 8 1-76.1151 135.055 1 -4 -8 2 320.021 193.697 6 -4 8 2 349.170 184.719 1 -4 8 2 405.789 181.713 5 -4 -8 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204.365 1 0 3 1 1410.14 199.091 3 0 -3 1 1503.86 174.815 3 0 3 2 2742.49 257.521 5 0 3 2 3139.38 295.570 1 0 -3 2 2963.67 188.454 7 0 -3 2 2970.06 205.181 3 0 3 3 464.036 118.581 1 0 -3 3 559.317 102.564 7 0 3 4 1020.50 188.474 1 0 -3 4 1265.57 167.427 7 0 3 5 281.545 99.0470 1 0 3 5 434.288 94.4405 7 0 -3 5 423.748 112.948 7 0 3 6 669.815 128.642 7 0 -3 6 578.825 136.648 7 0 3 7 702.634 149.396 7 0 -3 7 479.505 125.746 7 0 -3 8 1650.87 149.642 8 0 3 8 1899.38 248.269 7 0 -3 8 1748.72 271.687 7 0 3 9 787.004 180.666 7 0 -3 9 514.336 169.855 7 0 3 10 337.096 112.558 7 0 -3 10 325.158 137.827 7 0 3 11 659.873 182.148 7 0 -3 11 612.890 183.782 7 0 3 12 170.909 108.314 7 0 -3 12 73.7995 71.3288 7 0 -3 13 86.9318 60.7950 7 0 -3 14 166.355 128.387 7 0 -3 15 418.760 202.748 7 0 4 -14 73.2334 104.005 4 0 4 -13 395.407 211.436 4 0 4 -12 774.045 266.533 4 0 -4 -12 975.742 307.197 3 0 4 -11 7.40415 71.0881 4 0 -4 -11 239.245 210.133 3 0 4 -10 66.2681 105.350 4 0 -4 -10 200.239 177.046 3 0 -4 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579.831 161.275 5 0 -4 0 536.965 138.964 3 0 4 0 274.145 123.632 1 0 -4 1 112.924 73.3391 3 0 4 1 216.315 91.4824 5 0 4 1-5.04200 77.3003 1 0 4 2 1406.59 212.073 5 0 -4 2 1322.57 123.591 7 0 4 2 981.371 200.250 1 0 4 3 1079.40 211.537 1 0 4 3 1211.14 212.314 5 0 -4 3 949.590 127.823 7 0 4 4 330.342 127.412 1 0 4 4 436.174 138.306 5 0 -4 4 278.623 76.0337 7 0 -4 5 228.753 83.9473 7 0 4 5 7.31959 48.7961 1 0 4 6-57.9576 56.0776 1 0 -4 6 54.4373 71.6116 7 0 -4 7 491.987 140.873 7 0 -4 8 72.4893 86.5049 7 0 -4 9 304.909 138.569 7 0 -4 10-32.3390 108.767 7 0 -4 11 463.204 177.806 7 0 -4 12 871.737 234.354 7 0 -4 13 135.058 102.943 7 0 -4 14 31.0837 114.802 7 0 5 -13 128.309 145.595 4 0 5 -12 363.584 218.973 4 0 -5 -12 240.634 198.552 3 0 5 -11 368.317 203.123 4 0 -5 -11 418.609 232.044 3 0 -5 -11 56.8616 106.589 6 0 5 -10 648.195 269.974 4 0 -5 -10 801.299 299.246 3 0 -5 -10 684.946 317.702 6 0 5 -9 427.263 218.343 4 0 -5 -9 188.716 154.827 3 0 -5 -9-2.98019 101.962 6 0 5 -8 312.201 182.121 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131.626 5 0 5 3 558.521 179.719 1 0 5 4 2520.94 330.861 5 0 5 4 2896.61 390.379 1 0 -5 4 2341.74 229.187 7 0 5 5 122.232 78.9670 5 0 5 5 211.522 118.331 1 0 -5 5-50.1623 41.5338 7 0 5 6 2323.03 326.298 5 0 -5 6 1616.94 231.759 7 0 -5 7 84.0369 87.6174 7 0 -5 8 74.4751 70.2538 7 0 -5 9 118.520 103.743 7 0 -5 10 492.885 178.708 7 0 -5 11 89.0226 94.1521 7 0 -5 12 505.952 215.808 7 0 -5 13 140.937 130.204 7 0 -5 14 38.2259 79.0062 7 0 6 -11 347.813 185.412 4 0 -6 -11 139.123 146.731 6 0 6 -10 94.4077 147.510 4 0 -6 -10 364.076 205.983 3 0 -6 -10-189.339 193.347 6 0 6 -9 122.142 151.099 4 0 -6 -9 174.671 172.737 6 0 6 -8 619.372 289.211 4 0 -6 -8 783.700 313.828 3 0 -6 -8 514.018 271.942 6 0 6 -7 1083.26 329.820 4 0 -6 -7 1148.44 338.633 3 0 -6 -7 429.755 242.166 6 0 -6 -6 123.890 166.647 6 0 6 -6 25.4190 150.317 1 0 -6 -6-14.7380 88.5574 3 0 -6 -5 541.779 228.155 6 0 -6 -5 115.268 132.294 3 0 6 -5 236.593 152.301 1 0 -6 -4 654.753 224.260 6 0 6 -4 675.284 246.501 1 0 -6 -4 600.494 201.130 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0 -7 -5 961.084 284.814 6 0 7 -5 583.843 252.926 1 0 -7 -5 835.717 270.568 3 0 -7 -4 51.4587 135.644 6 0 7 -4-150.455 109.301 1 0 -7 -4 120.334 171.490 3 0 -7 -3 908.980 290.571 6 0 7 -3 214.848 203.433 1 0 -7 -3 823.484 252.605 3 0 -7 -2 745.408 275.246 6 0 7 -2 562.954 256.067 1 0 7 -1 77.4256 109.993 1 0 -7 -1-109.130 93.4004 6 0 7 -1 129.301 77.9418 5 0 7 0 0.35032 113.419 1 0 -7 0-89.2409 114.930 6 0 7 0-86.6633 102.497 5 0 -7 1 245.607 157.997 6 0 7 1 164.724 171.691 1 0 7 1 373.427 170.896 5 0 -7 2 854.578 274.506 6 0 7 2 728.283 223.479 5 0 7 2 922.822 294.687 1 0 7 3 382.192 232.062 1 0 7 3 934.259 257.516 5 0 7 4 90.6163 117.356 5 0 7 5 831.921 247.370 5 0 7 6 320.808 168.858 5 0 7 7 424.065 211.985 5 0 7 8 79.7009 63.7976 5 0 7 9 135.257 135.497 5 0 7 10 119.504 132.597 5 0 -8 -6 393.500 250.910 6 0 -8 -5 309.311 244.570 6 0 -8 -4 409.857 229.127 6 0 -8 -3 96.3221 151.364 6 0 -8 -2 1235.98 353.912 6 0 -8 -1 417.364 223.063 6 0 8 -1 629.196 232.476 5 0 -8 0 6.29336 128.785 6 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0 -2 2351.19 121.541 8 1 0 -2 2213.31 107.443 2 1 0 2 59.2776 46.4490 3 1 0 2 52.7230 45.3378 7 1 0 3 72.7968 48.7414 3 1 0 3 25.9874 46.0653 7 1 0 4 1847.52 196.076 7 1 0 4 1933.49 200.893 3 1 0 5-36.5074 57.8235 3 1 0 5 118.062 77.7794 7 1 0 6 5985.98 417.803 7 1 0 6 5816.09 417.320 3 1 0 7 30.5586 81.1170 7 1 0 8 291.829 110.147 7 1 0 9 81.0704 106.254 7 1 0 10 7855.30 634.609 7 1 0 11-3.03220 88.4065 7 1 0 12 766.620 213.054 7 1 0 13-77.9728 74.2049 7 1 0 14 1093.10 304.254 7 1 0 15 32.0534 108.114 7 1 1 -17 246.464 162.816 2 1 -1 -16 98.7378 91.3517 2 1 1 -16 49.8294 89.8836 2 1 1 -15 318.191 164.651 2 1 -1 -15 93.5302 145.707 2 1 1 -14 520.375 200.895 2 1 -1 -14 377.035 149.406 2 1 1 -13 137.810 124.780 2 1 -1 -13 227.101 131.325 2 1 1 -12 414.454 158.698 2 1 -1 -12 259.782 130.762 2 1 1 -11 1024.96 215.895 2 1 1 -10 447.843 137.344 2 1 1 -9 1358.80 218.184 2 1 -1 -9 885.569 156.679 8 1 -1 -9 954.655 235.159 3 1 1 -8 158.418 76.7570 2 1 -1 -8 217.395 81.0988 8 1 -1 -8-12.7794 84.0028 3 1 1 -7 735.587 158.148 2 1 -1 -7 697.182 133.099 8 1 -1 -7 609.029 174.403 3 1 1 -6 717.342 143.666 2 1 -1 -6 924.537 137.412 8 1 -1 -6 680.606 163.794 3 1 -1 -5 5152.17 320.295 8 1 1 -5 4453.70 302.406 2 1 -1 -5 4508.29 374.836 6 1 -1 -5 5446.30 413.271 3 1 -1 -4 7580.08 377.137 8 1 1 -4 6937.93 361.287 2 1 -1 -4 7434.35 433.890 6 1 -1 -4 8014.89 463.393 3 1 -1 -3 9779.80 411.327 8 1 -1 -3 9207.84 428.876 6 1 -1 -3 10109.9 479.124 3 1 -1 -2 47485.8 997.406 8 1 1 -2 46201.7 1061.26 4 1 -1 -2 46217.2 1020.91 6 1 -1 -2 45728.1 1074.70 3 1 1 -1 17917.5 465.445 5 1 -1 -1 17094.0 498.056 8 1 1 -1 17828.2 527.094 4 1 -1 -1 18518.9 516.537 6 1 -1 0 2789.81 142.287 5 1 1 0 2652.54 150.445 5 1 -1 0 2893.19 159.571 1 1 1 0 2639.27 164.043 3 1 1 0 2519.96 166.453 6 1 1 1 680.576 99.8588 6 1 1 1 619.654 98.6370 3 1 -1 1 657.571 104.039 4 1 -1 1 673.356 84.1925 2 1 -1 1 591.981 86.1067 1 1 1 2 862.437 127.599 6 1 1 2 970.070 137.007 3 1 -1 2 1200.46 117.636 1 1 -1 2 991.782 112.581 7 1 -1 2 884.451 105.874 2 1 1 3 464.302 119.836 3 1 1 3 400.050 80.1702 7 1 -1 3 475.075 94.7574 7 1 -1 3 457.139 82.9900 1 1 -1 3 640.316 77.6889 3 1 1 3 766.872 138.193 6 1 -1 4 1829.84 156.867 1 1 1 4 1368.26 157.869 7 1 -1 4 1733.69 189.007 7 1 -1 4 1589.97 139.336 3 1 1 4 1392.28 197.354 3 1 1 4 1223.81 184.114 6 1 -1 5-53.7517 48.6698 3 1 -1 5 16.2067 23.1156 1 1 -1 5-26.9465 51.5559 7 1 1 6 3679.39 310.656 7 1 -1 6 3543.08 326.642 7 1 -1 6 3197.02 261.202 3 1 -1 7 1728.24 245.820 7 1 1 7 1342.87 207.916 7 1 -1 7 1829.50 214.099 3 1 -1 8 354.805 105.658 3 1 1 8 453.186 130.822 7 1 -1 8 464.264 137.737 7 1 1 9 1734.44 275.945 7 1 -1 9 1813.58 291.934 7 1 1 10 865.161 216.529 7 1 -1 10 591.158 185.468 7 1 1 11 713.608 202.176 7 1 -1 11 774.391 215.638 7 1 1 12 100.227 77.8724 7 1 -1 12 14.5011 84.8824 7 1 1 13 82.9191 134.308 7 1 -1 13 181.328 144.708 7 1 1 14 162.205 114.266 7 1 -1 14 348.896 168.972 7 1 -1 15 239.216 157.724 7 1 -2 -15 129.862 78.4635 2 1 2 -13 314.431 150.782 2 1 2 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1 2 0 5708.82 311.982 5 1 -2 0 5940.84 289.395 5 1 -2 0 5110.31 306.251 1 1 2 0 5975.19 362.189 1 1 2 0 5878.94 318.987 3 1 -2 1 1727.46 162.538 5 1 2 1 1773.16 171.553 5 1 -2 1 1568.55 168.545 1 1 -2 1 1694.26 202.457 4 1 2 1 1630.14 189.429 1 1 2 1 1745.97 197.604 3 1 2 1 2162.50 219.855 6 1 -2 2 1736.02 174.324 5 1 -2 2 1801.68 187.885 1 1 -2 2 1789.58 217.997 4 1 2 2 1146.69 172.110 1 1 -2 2 1554.66 140.897 7 1 2 2 1587.79 200.693 3 1 -2 2 1644.52 175.700 2 1 2 2 1656.07 212.155 6 1 -2 3 5494.26 340.450 1 1 -2 3 5067.95 296.703 7 1 -2 3 5053.92 334.087 2 1 2 3 6128.56 430.627 3 1 2 3 5395.06 405.388 6 1 -2 4 1140.93 153.016 1 1 -2 4 956.664 146.901 7 1 2 5 669.707 122.945 7 1 -2 5 777.992 152.993 7 1 -2 5 694.765 124.086 1 1 -2 6 698.548 67.7603 8 1 -2 6 1070.29 159.915 1 1 -2 6 1001.49 73.6090 8 1 2 6 1005.66 167.316 7 1 -2 6 972.052 173.642 7 1 2 7 185.158 96.3180 7 1 -2 7-16.3115 78.3127 7 1 2 8 126.521 92.7696 7 1 -2 8 114.426 81.0805 7 1 -2 8 250.547 75.3096 3 1 2 9 2498.77 320.768 7 1 -2 9 1867.88 305.872 7 1 -2 9 2061.13 226.885 3 1 2 10 334.363 132.532 7 1 -2 10 135.148 108.172 7 1 -2 11 2409.58 374.514 7 1 2 11 1794.53 314.747 7 1 2 12 808.905 233.059 7 1 -2 12 390.432 184.572 7 1 -2 13 1347.42 331.186 7 1 -2 14 293.631 190.387 7 1 -2 15 24.2109 80.3930 7 1 3 -15 0.53377 94.8090 4 1 3 -14 100.175 123.898 4 1 3 -13 203.953 172.781 4 1 3 -12 180.613 204.422 4 1 -3 -11 230.182 117.048 3 1 3 -11 340.975 208.785 4 1 -3 -10 1540.57 337.028 3 1 3 -10 1635.19 344.520 4 1 -3 -9 180.101 184.919 3 1 3 -9-2.03933 98.7978 4 1 -3 -9 166.653 168.379 6 1 -3 -8 633.991 215.345 3 1 3 -8 439.355 173.714 4 1 -3 -8 1147.17 310.271 6 1 -3 -7 1837.65 322.731 3 1 3 -7 1474.52 300.157 4 1 -3 -7 1768.18 306.139 6 1 -3 -6 809.346 224.888 3 1 3 -6 727.799 209.710 4 1 -3 -6 629.005 190.174 6 1 -3 -5 317.894 130.993 6 1 -3 -5 366.533 147.099 3 1 3 -5 286.430 119.409 4 1 3 -5 175.512 118.733 1 1 -3 -4 415.701 162.334 6 1 3 -4 516.305 163.997 4 1 -3 -4 347.983 131.878 3 1 -3 -4 330.801 93.1579 1 1 3 -4 272.389 135.098 1 1 -3 -3 194.514 83.2232 6 1 3 -3 212.603 98.2547 1 1 3 -3 460.051 146.067 4 1 -3 -3 143.654 101.859 3 1 -3 -3 184.279 77.3277 1 1 3 -2 345.442 115.166 1 1 -3 -2 566.471 155.948 6 1 3 -2 667.562 147.189 5 1 3 -2 358.756 134.279 4 1 -3 -2 451.066 129.211 3 1 -3 -2 480.291 111.479 1 1 3 -2 495.834 83.2221 3 1 3 -1 333.714 89.9922 3 1 -3 -1 311.306 106.076 6 1 3 -1 374.479 112.216 5 1 -3 -1 447.830 119.551 3 1 3 -1 342.797 126.372 1 1 3 0 2953.81 277.089 5 1 -3 0 3212.73 255.898 5 1 3 0 2737.91 314.120 1 1 3 0 2674.28 251.911 3 1 3 1 4065.19 313.901 5 1 3 1 3526.02 347.811 1 1 3 1 4017.64 342.411 3 1 3 2 929.906 159.374 5 1 3 2 925.321 169.941 1 1 -3 2 978.764 113.499 7 1 -3 3 675.030 109.779 7 1 3 3 379.371 121.680 1 1 -3 4 511.185 105.582 7 1 -3 5 2871.49 279.493 7 1 -3 6 773.983 164.656 7 1 -3 7 334.393 125.850 7 1 -3 8 1535.96 106.023 8 1 -3 8 2282.77 313.458 7 1 -3 9 1976.12 314.301 7 1 -3 10 626.831 184.927 7 1 -3 11 756.687 231.047 7 1 -3 12 616.734 214.177 7 1 -3 13 105.266 117.508 7 1 -3 14 241.908 194.264 7 1 4 -14 249.757 186.078 4 1 4 -13 396.380 208.620 4 1 4 -12 241.519 179.447 4 1 4 -11 788.553 277.594 4 1 -4 -11 985.190 308.078 3 1 -4 -11 1162.60 344.572 6 1 4 -10 267.131 189.603 4 1 -4 -10 87.5553 100.022 3 1 -4 -10 89.0742 118.885 6 1 4 -9 805.728 251.872 4 1 -4 -9 697.655 263.258 3 1 -4 -9 514.991 229.756 6 1 4 -8 898.375 246.129 4 1 -4 -8 985.715 292.969 3 1 -4 -8 917.782 285.025 6 1 4 -7 1217.81 283.418 4 1 -4 -7 1291.47 300.511 3 1 -4 -7 1081.10 256.479 6 1 -4 -6-57.7763 78.0015 6 1 4 -6 136.097 127.673 4 1 -4 -6 198.309 146.540 3 1 -4 -5 1418.59 294.433 6 1 4 -5 1357.42 286.280 1 1 4 -5 988.142 245.158 4 1 -4 -5 1395.85 287.452 3 1 -4 -4 1032.51 262.160 6 1 4 -4 818.190 228.413 4 1 -4 -4 750.938 204.777 3 1 4 -4 606.990 205.651 1 1 -4 -3 1022.41 239.559 6 1 4 -3 753.751 213.977 1 1 -4 -3 1190.32 249.188 3 1 4 -2 7308.81 510.208 5 1 4 -2 6840.05 568.592 1 1 4 -2 6615.94 382.215 3 1 -4 -2 6747.38 570.157 6 1 -4 -2 7292.95 550.752 3 1 4 -1 8059.06 522.949 5 1 4 -1 7767.68 586.648 1 1 4 -1 7910.41 468.228 3 1 -4 -1 7272.86 570.483 6 1 -4 -1 7974.37 545.229 3 1 4 0 3623.84 346.244 5 1 4 0 3206.53 380.608 1 1 4 0 3561.48 335.783 3 1 4 1 1653.67 243.366 5 1 4 1 1277.60 243.070 1 1 4 2 2752.10 304.993 5 1 4 2 2803.07 358.800 1 1 4 3 4337.97 391.529 5 1 4 3 3977.21 428.487 1 1 4 4 452.276 141.233 5 1 -4 4 319.840 80.3871 7 1 -4 5 1182.83 185.623 7 1 -4 6 1216.62 210.118 7 1 -4 7 3071.39 344.964 7 1 -4 8 899.673 203.872 7 1 -4 9 637.282 203.688 7 1 -4 10 654.985 195.926 7 1 -4 11 147.257 113.041 7 1 -4 12 978.703 269.932 7 1 -4 13 673.332 214.117 7 1 5 -13-9.54828 102.337 4 1 5 -12 172.109 172.610 4 1 -5 -12 645.421 279.344 6 1 5 -11 277.116 212.038 4 1 -5 -11 399.186 239.424 6 1 5 -10-80.0780 92.5918 4 1 -5 -10 173.049 110.920 3 1 -5 -10 185.141 192.963 6 1 5 -9-9.04559 117.770 4 1 -5 -9 188.329 195.283 3 1 -5 -9 73.7047 162.480 6 1 5 -8 2918.72 487.922 4 1 -5 -8 3594.76 546.473 6 1 -5 -8 4376.69 606.009 3 1 -5 -7 2195.20 426.391 6 1 5 -7 1851.73 358.532 4 1 -5 -7 1781.56 371.158 3 1 -5 -6 2204.58 404.643 6 1 5 -6 1609.70 354.801 4 1 -5 -6 1654.22 337.392 3 1 -5 -5 348.626 165.282 6 1 5 -5 762.755 247.457 4 1 -5 -5 360.524 169.533 3 1 5 -5 163.534 152.402 1 1 5 -4 3000.69 461.428 1 1 -5 -4 3638.22 491.156 6 1 -5 -4 4266.45 499.968 3 1 -5 -3 666.852 236.306 6 1 5 -3 391.768 165.587 1 1 -5 -3 920.233 243.510 3 1 -5 -2 848.942 222.794 6 1 5 -2 1079.80 234.524 5 1 -5 -2 1220.96 241.481 3 1 5 -2 850.526 239.819 1 1 5 -2 868.325 162.025 3 1 -5 -1 136.849 113.316 6 1 5 -1-3.22965 58.5377 5 1 5 -1 24.9629 120.874 1 1 -5 0 278.386 149.636 6 1 5 0 153.873 69.5860 5 1 5 0 69.6411 125.267 1 1 5 1 552.617 161.803 5 1 5 1 553.391 178.248 1 1 5 2 1020.03 213.902 5 1 5 2 731.595 212.390 1 1 5 3 325.480 132.643 5 1 5 3 318.782 151.272 1 1 5 4 877.583 208.972 5 1 5 5 955.416 209.144 5 1 5 6 217.357 118.659 5 1 -5 7 2613.67 325.927 7 1 -5 8 1827.67 287.572 7 1 -5 9 107.936 99.6032 7 1 -5 10 960.337 246.233 7 1 -6 -12 451.057 287.275 6 1 6 -11 188.723 180.374 4 1 -6 -11 399.586 251.154 6 1 6 -10 472.820 227.892 4 1 -6 -10 712.092 334.329 6 1 6 -9 393.258 222.378 4 1 -6 -9 634.926 272.645 6 1 6 -8-14.0156 84.2710 4 1 -6 -8 239.672 164.221 3 1 -6 -8 180.067 218.744 6 1 -6 -7 66.6482 92.1627 6 1 6 -7 115.371 104.082 4 1 -6 -7 128.024 181.650 3 1 -6 -6 551.609 265.784 6 1 -6 -6 928.525 290.113 3 1 -6 -5 693.683 244.349 6 1 -6 -5 758.624 254.961 3 1 -6 -4 1497.36 342.642 6 1 6 -4 1542.42 368.443 1 1 -6 -4 1892.62 363.770 3 1 -6 -3 462.021 223.211 6 1 6 -3 132.108 126.293 1 1 -6 -2 1338.86 329.525 6 1 6 -2 1069.35 242.132 5 1 6 -2 1062.19 307.826 1 1 -6 -1 23.7596 81.1047 6 1 6 -1 147.238 120.416 5 1 6 -1-1.20317 89.0576 1 1 -6 0 1304.92 312.464 6 1 6 0 1034.00 236.741 5 1 6 0 886.718 273.271 1 1 6 1 1165.59 252.501 5 1 6 1 1294.05 313.176 1 1 6 2 1034.13 255.765 5 1 6 3 46.2443 94.7218 5 1 6 4 1131.51 256.446 5 1 6 5 115.317 60.7816 5 1 6 6 4991.79 536.795 5 1 6 7 332.143 159.725 5 1 6 8-20.6576 80.0511 5 1 6 9-32.3711 61.2321 5 1 -7 -10 282.530 215.232 6 1 -7 -9 323.701 236.488 6 1 -7 -8 68.0493 133.422 6 1 -7 -7 1001.78 346.175 6 1 -7 -6 458.455 275.422 6 1 -7 -5-40.3018 144.364 6 1 -7 -4 526.564 225.756 6 1 -7 -3 650.147 253.778 6 1 -7 -2 316.958 185.217 6 1 -7 -1 1151.79 322.188 6 1 7 -1 1223.87 284.969 5 1 -7 0 249.913 166.647 6 1 7 0 132.032 121.198 5 1 -7 1 379.754 203.459 6 1 7 1 296.862 145.493 5 1 -7 2 214.086 153.707 6 1 7 2 176.091 136.550 5 1 7 3 520.245 206.955 5 1 7 4 172.348 125.108 5 1 7 5 49.1957 66.1970 5 1 7 6 387.007 184.304 5 1 7 7-9.25749 59.2818 5 1 7 8 157.130 119.710 5 1 7 9 385.067 170.594 5 1 -8 -7 277.690 256.760 6 1 -8 -6 103.607 107.388 6 1 -8 -5 120.074 132.002 6 1 -8 -4-5.88591 102.016 6 1 -8 -3 192.688 208.367 6 1 -8 -2 118.935 234.138 6 1 -8 -1 172.089 158.595 6 1 8 -1 315.569 174.978 5 1 -8 0 333.771 182.189 6 1 8 0 279.411 155.994 5 1 -8 1 345.809 218.873 6 1 8 1 267.988 167.843 5 1 -8 2 186.761 180.761 6 1 8 2 469.420 180.876 5 1 -8 3 613.938 266.487 6 1 8 3 120.351 89.2098 5 1 8 4 268.592 216.520 5 1 8 5 210.694 170.186 5 1 8 6 72.7137 130.297 5 2 0 -16 51.3976 70.6741 2 2 0 -15 13.4051 54.7322 2 2 0 -14 463.922 187.977 2 2 0 -13-37.2173 67.3250 2 2 0 -12 1213.93 231.418 2 2 0 -11-49.3877 52.0646 2 2 0 -10 1863.49 197.837 8 2 0 -10 1780.43 247.078 2 2 0 -9-2.25684 24.5188 8 2 0 -9-8.10100 47.2040 2 2 0 -8 2102.50 200.963 8 2 0 -8 1727.91 209.806 2 2 0 -7 138.481 57.9239 8 2 0 -7 42.8797 41.1917 2 2 0 -6 3886.15 246.316 8 2 0 -6 3306.73 242.926 2 2 0 -5-33.5602 30.1201 8 2 0 -5-8.97933 34.1557 2 2 0 -4 11734.2 399.346 8 2 0 -4 11286.4 367.717 2 2 0 -3 18.4630 30.9828 2 2 0 -3 38.6141 37.7798 8 2 0 -2 14177.5 400.108 8 2 0 -1-2.52144 23.0401 8 2 0 0 11715.6 327.540 8 2 0 2 47377.2 1028.87 3 2 0 3 32.1746 54.6661 3 2 0 4 4657.76 318.449 7 2 0 4 4430.47 318.193 3 2 0 5 56.1151 63.6747 3 2 0 5 68.4596 63.2681 7 2 0 6 3312.07 319.665 7 2 0 6 3438.02 329.366 3 2 0 7-25.9540 50.4734 7 2 0 8 7583.38 561.727 7 2 0 9-74.9668 89.0083 7 2 0 10 532.533 168.912 7 2 0 11 70.8724 81.1788 7 2 0 12 3176.68 461.410 7 2 1 -16 142.344 158.688 2 2 -1 -15 216.155 147.826 2 2 1 -15 37.4157 94.1712 2 2 1 -14 507.430 180.351 2 2 -1 -14 639.713 195.305 2 2 1 -13 604.749 201.257 2 2 -1 -13 586.142 169.319 2 2 1 -12 1250.39 254.024 2 2 -1 -12 1577.80 261.356 2 2 1 -11 263.918 114.003 2 2 -1 -11-61.7219 69.5058 2 2 1 -10 946.235 187.263 2 2 1 -9 2280.06 275.359 2 2 -1 -8 982.243 159.729 8 2 1 -8 1318.89 198.258 2 2 1 -7 117.550 76.8050 2 2 -1 -7 64.4531 57.7893 8 2 -1 -6 4521.46 322.619 8 2 1 -6 3707.05 296.345 2 2 -1 -6 4519.57 390.477 6 2 -1 -5 1869.23 197.661 8 2 -1 -5 1674.13 218.230 6 2 -1 -4 5970.18 344.049 8 2 -1 -4 5785.76 361.198 6 2 -1 -3 27898.3 765.669 8 2 -1 -3 26911.7 769.821 6 2 -1 -2 38936.9 909.309 8 2 1 -2 37558.1 929.957 4 2 -1 -2 38414.0 896.314 6 2 1 -1 3516.05 189.850 5 2 -1 -1 4285.79 242.288 8 2 1 -1 3794.48 228.036 4 2 -1 0 5175.47 192.213 5 2 1 0 5933.22 238.047 5 2 -1 0 5478.84 255.653 8 2 1 0 5866.21 287.378 3 2 -1 0 5386.08 211.427 2 2 1 0 5806.94 264.448 6 2 -1 1 8527.94 298.790 8 2 -1 1 8856.91 360.328 4 2 1 1 7929.61 377.210 3 2 1 1 8278.38 366.504 6 2 -1 2 6620.08 226.691 8 2 1 2 6558.62 381.634 3 2 1 2 7140.24 384.094 6 2 1 3 4126.26 327.303 3 2 1 3 3829.52 324.431 6 2 1 4 550.508 134.042 3 2 -1 4 936.401 151.537 7 2 1 4 566.539 151.538 6 2 -1 5 7156.44 445.209 7 2 -1 5 7801.85 401.815 3 2 1 6 1803.10 233.766 7 2 -1 6 2084.39 259.467 7 2 -1 6 1855.59 210.260 3 2 1 7 330.553 107.227 7 2 -1 7 409.615 142.708 7 2 -1 7 474.205 120.057 3 2 1 8 2853.91 338.999 7 2 -1 8 2041.47 291.790 7 2 1 9 1262.88 238.376 7 2 -1 9 1698.25 283.956 7 2 1 10 2061.36 324.770 7 2 -1 10 1496.38 291.312 7 2 -1 11 2245.84 369.128 7 2 -1 12 363.317 181.803 7 2 -1 13-7.69831 97.7266 7 2 -2 -14 121.390 107.904 2 2 -2 -8 1223.16 279.047 6 2 -2 -7 498.320 173.368 3 2 -2 -7 457.713 171.370 6 2 -2 -6 3742.36 384.246 6 2 -2 -6 3760.46 416.757 3 2 2 -5 5357.38 458.819 4 2 -2 -5 5913.19 457.409 6 2 -2 -5 5600.92 469.763 3 2 -2 -4 2585.96 269.474 8 2 2 -4 2289.79 279.858 4 2 -2 -4 2753.68 295.026 6 2 -2 -3 7656.26 449.909 8 2 2 -3 7348.13 475.037 4 2 -2 -3 7366.76 456.838 6 2 2 -2 16153.2 601.649 5 2 -2 -2 18161.8 682.067 8 2 2 -2 16889.5 699.612 4 2 -2 -2 15985.3 659.938 6 2 2 -1 4888.04 301.200 5 2 -2 -1 5504.89 347.256 8 2 2 -1 4845.15 275.591 3 2 -2 0 2258.27 174.100 5 2 2 0 1920.38 180.830 5 2 -2 0 2398.56 214.612 1 2 -2 0 2474.47 219.438 8 2 2 0 2096.75 203.753 3 2 2 0 2202.40 211.749 6 2 -2 1 3722.04 241.117 5 2 2 1 4015.74 263.726 5 2 -2 1 4403.71 301.239 1 2 -2 1 4031.88 273.429 8 2 -2 1 4015.84 305.740 4 2 2 1 3969.62 306.986 3 2 -2 1 4112.44 262.784 2 2 2 1 4254.46 314.200 6 2 -2 2 42.2889 36.7737 2 2 2 2 63.1744 48.7149 6 2 2 2 80.1946 82.1321 3 2 -2 2 140.325 59.8247 8 2 -2 2 186.268 70.8894 1 2 -2 2 196.377 87.8951 4 2 -2 3 751.221 100.964 8 2 -2 3 829.004 137.089 1 2 -2 4 2228.11 226.824 1 2 -2 4 2368.85 165.171 8 2 -2 4 2140.26 227.573 7 2 -2 5 2985.09 266.992 1 2 -2 5 2799.08 149.280 8 2 -2 5 3107.81 296.973 7 2 -2 6 215.788 81.5288 7 2 -2 7 4263.07 402.725 7 2 -2 8 2826.44 352.481 7 2 -2 9 1519.57 277.261 7 2 -2 10-53.8258 112.794 7 2 -2 11 134.582 108.055 7 2 -2 12 860.748 253.726 7 2 3 -15 58.4058 94.0484 4 2 3 -14 564.576 289.013 4 2 3 -13-138.863 141.971 4 2 3 -12 982.146 300.559 4 2 3 -11 205.859 140.622 4 2 3 -10 899.608 263.681 4 2 -3 -10 573.908 203.184 6 2 3 -9 1365.20 306.174 4 2 -3 -9 1022.86 289.520 6 2 3 -8 274.540 153.332 4 2 -3 -8 480.236 190.964 3 2 -3 -8 646.820 250.053 6 2 3 -7 400.518 166.732 4 2 -3 -7 290.600 154.772 3 2 -3 -7 439.183 168.428 6 2 -3 -6 939.418 217.841 6 2 3 -6 851.853 205.556 4 2 -3 -6 845.468 226.548 3 2 3 -5 3316.57 401.725 4 2 -3 -5 3358.81 392.871 6 2 -3 -5 3524.13 416.815 3 2 3 -4 7468.64 570.811 4 2 -3 -4 7517.80 560.485 6 2 -3 -4 8241.44 593.507 3 2 3 -3 5671.41 477.811 4 2 -3 -3 5125.76 452.555 6 2 3 -2 4707.19 362.128 5 2 -3 -2 5087.15 432.184 6 2 -3 -1 1491.96 168.527 5 2 3 -1 1092.56 172.016 5 2 3 -1 1068.06 156.794 3 2 -3 0 2186.75 204.619 5 2 3 0 1558.64 195.082 5 2 3 0 1902.10 232.855 3 2 -3 1 1980.79 210.855 5 2 3 1 1404.58 190.545 5 2 3 1 1486.72 213.519 3 2 3 2 902.800 150.753 5 2 -3 5 2344.61 215.345 8 2 -3 5 2042.83 242.382 7 2 -3 6 713.730 110.212 8 2 -3 6 390.802 128.742 7 2 -3 7 88.5091 33.3433 8 2 -3 7 291.438 126.120 7 2 -3 8 63.9104 79.7820 7 2 -3 9 711.104 188.979 7 2 -3 10 247.212 151.545 7 2 -3 11 262.597 137.477 7 2 4 -14 155.795 208.217 4 2 4 -13 17.5884 81.3193 4 2 4 -12 875.614 279.228 4 2 4 -11 386.965 206.050 4 2 -4 -11 256.682 156.434 6 2 4 -10 2072.04 396.223 4 2 -4 -10 1986.21 428.717 6 2 4 -9 1132.20 303.469 4 2 -4 -9 838.985 267.655 6 2 4 -8 2912.76 454.286 4 2 -4 -8 2640.29 429.376 6 2 -4 -7 2160.58 378.047 6 2 4 -7 1934.47 359.411 4 2 -4 -7 2341.66 395.740 3 2 4 -6 2123.87 354.134 4 2 -4 -6 2339.87 383.501 3 2 -4 -6 2506.70 403.015 6 2 -4 -5 642.859 233.273 6 2 4 -5 886.885 239.658 4 2 -4 -5 860.441 231.729 3 2 -4 -4 319.548 160.892 6 2 4 -4 164.331 117.041 4 2 -4 -3 3803.49 426.122 6 2 4 -2 2387.01 295.393 5 2 4 -2 2427.21 242.457 3 2 -4 -2 2174.26 320.021 6 2 4 -1 4265.86 387.140 5 2 4 -1 4670.85 368.654 3 2 4 0 234.984 110.119 5 2 4 1 1915.61 266.867 5 2 4 2 1751.96 250.915 5 2 4 3 728.483 170.736 5 2 4 4 986.699 189.632 5 2 -4 6 1303.46 187.997 8 2 5 -13 252.980 130.422 4 2 5 -12 212.679 179.742 4 2 -5 -12 289.194 236.342 6 2 5 -11 450.626 222.549 4 2 -5 -11 607.280 268.013 6 2 5 -10 782.313 256.756 4 2 -5 -10 1229.37 372.139 6 2 5 -9 124.324 119.740 4 2 -5 -9 74.0218 104.457 6 2 5 -8 771.092 244.798 4 2 -5 -8 535.218 234.323 6 2 -5 -7 1249.79 337.120 6 2 5 -7 845.537 260.200 4 2 -5 -6 238.937 166.416 6 2 5 -6 316.656 174.451 4 2 -5 -5 573.836 214.530 6 2 5 -5 382.048 193.936 4 2 -5 -4 3165.77 457.690 6 2 -5 -3 538.423 180.697 6 2 -5 -2 512.543 199.642 6 2 5 -2 388.823 140.259 5 2 5 -2 559.759 139.111 3 2 -5 -1 2358.11 359.999 6 2 5 -1 2412.56 323.363 5 2 5 0 54.2789 66.4536 5 2 5 1 221.166 124.439 5 2 5 2 2147.73 305.016 5 2 5 3 43.4133 94.5026 5 2 5 4 82.5113 87.2056 5 2 5 5 340.349 144.108 5 2 5 6 1276.24 259.342 5 2 6 -12 408.236 255.572 4 2 -6 -12 153.307 188.186 6 2 6 -11 324.339 261.705 4 2 -6 -11-127.220 100.063 6 2 6 -10-8.28712 75.8419 4 2 -6 -10-116.840 183.452 6 2 6 -9 933.924 319.052 4 2 -6 -9 1122.84 348.174 6 2 6 -8 36.4584 109.841 4 2 -6 -8 196.807 150.275 6 2 -6 -7 648.119 231.213 6 2 6 -7 521.359 210.274 4 2 -6 -6 486.621 199.727 6 2 -6 -5 769.870 260.192 6 2 -6 -4-49.1556 113.485 6 2 -6 -3 310.514 155.431 6 2 -6 -2 951.581 251.070 6 2 6 -2 722.442 202.120 5 2 -6 -1 5.57980 124.199 6 2 6 -1-119.691 117.566 5 2 -6 0 553.340 181.926 6 2 6 0 401.744 176.076 5 2 6 1 1014.88 234.460 5 2 6 2 53.8736 63.3870 5 2 6 3 175.939 94.3369 5 2 6 4 515.587 177.167 5 2 6 5 2584.12 394.487 5 2 6 6 810.200 224.276 5 2 6 7 258.036 156.406 5 2 6 8 258.454 144.374 5 2 6 9 188.031 148.085 5 2 7 -10 338.955 246.542 4 2 -7 -10 383.282 235.703 6 2 -7 -9 483.579 278.849 6 2 -7 -8 232.919 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70.0965 2 3 0 -14 88.9737 94.5642 2 3 0 -13 124.492 81.9414 2 3 0 -12 3896.35 399.285 2 3 0 -11 54.3675 84.0407 2 3 0 -10 2696.99 261.273 8 3 0 -10 2917.46 303.423 2 3 0 -9 14.6724 52.8524 2 3 0 -9 100.267 61.7900 8 3 0 -8 669.089 130.621 2 3 0 -8 851.856 136.284 8 3 0 -7-30.5305 50.7971 2 3 0 -7 22.8387 32.0870 8 3 0 -6 1227.59 148.791 8 3 0 -6 1055.67 128.929 2 3 0 -5-53.0940 48.2756 2 3 0 -5 4.51596 30.2159 8 3 0 -4 13099.1 475.343 8 3 0 -3-7.07494 52.1323 8 3 0 -3-18.7523 27.9213 6 3 0 -2 8575.40 346.349 8 3 0 -1 7.53841 33.7579 8 3 0 0 7414.40 299.413 8 3 0 3 27.7576 43.5149 3 3 0 4 25555.6 870.090 3 3 0 5 49.2216 68.9938 3 3 -1 -15 674.942 207.470 2 3 -1 -14 212.767 115.318 2 3 1 -14 333.705 148.508 2 3 -1 -13 649.241 173.540 2 3 1 -13 351.219 144.612 2 3 1 -12 335.026 145.454 2 3 -1 -12 237.450 121.788 2 3 1 -11 878.637 200.137 2 3 -1 -11 897.430 180.857 2 3 1 -10 671.560 159.711 2 3 -1 -10 545.680 131.656 2 3 1 -9 883.622 190.184 2 3 -1 -9 801.881 151.942 2 3 1 -8 916.422 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528.687 141.799 5 8 3 3 105.056 106.309 5 8 4 -14 386.997 224.107 4 8 4 -13 484.343 247.401 4 8 -4 -13 289.469 150.717 6 8 4 -12 109.364 106.393 4 8 -4 -12 162.342 104.635 6 8 4 -11 489.005 223.407 4 8 -4 -11 361.520 162.283 6 8 4 -10-6.12216 73.3347 4 8 -4 -10-24.8468 82.9388 6 8 -4 -9 355.728 188.916 6 8 4 -9 240.284 124.827 4 8 -4 -8 784.718 257.186 6 8 4 -8 252.197 138.057 4 8 -4 -7 614.952 191.514 6 8 4 -7 665.125 214.169 4 8 -4 -6 1917.90 334.205 6 8 4 -6 1854.47 338.689 4 8 -4 -5 81.3351 90.1116 6 8 4 -5 175.900 104.634 4 8 -4 -4 1222.62 282.342 6 8 4 -3 679.125 175.415 5 8 4 -2 154.385 92.9729 5 8 4 -1 45.1015 67.4361 5 8 4 0 2839.19 347.192 5 8 4 1 1536.55 253.696 5 8 4 2 1316.31 245.354 5 8 4 3 1700.05 277.225 5 8 4 4 2194.04 321.315 5 8 4 5 3005.91 380.252 5 8 -5 -14 495.696 298.750 6 8 5 -13 71.5516 78.2416 4 8 -5 -13-44.1819 141.388 6 8 5 -12 429.891 248.544 4 8 -5 -12 538.861 252.518 6 8 5 -11-10.8486 68.9780 4 8 -5 -11 150.882 177.585 6 8 -5 -10 510.118 230.622 6 8 5 -10 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168.761 114.369 5 9 5 0 1058.88 237.935 5 9 5 1 465.030 160.633 5 9 5 2 121.462 76.9477 5 9 5 3 570.820 191.534 5 9 5 4 886.356 233.161 5 9 5 5 289.547 124.720 5 9 5 6 387.284 166.392 5 9 5 7 557.887 206.950 5 9 5 8 418.644 178.844 5 9 -6 -13-75.4819 121.438 6 9 -6 -12 300.840 189.571 6 9 6 -11 203.068 172.390 4 9 -6 -11 778.471 277.121 6 9 -6 -10 297.207 155.691 6 9 6 -10 300.188 194.881 4 9 -6 -9 40.8638 76.4773 6 9 6 -9 374.569 210.793 4 9 -6 -8 274.029 226.421 6 9 -6 -7 203.832 179.384 6 9 -6 -6 235.368 179.012 6 9 -6 -5 570.140 239.635 6 9 -6 -4 151.882 143.491 6 9 6 -3 317.634 167.400 5 9 6 -2 61.8284 143.260 5 9 6 -1 777.186 223.591 5 9 6 0 12.7683 72.9160 5 9 6 1 122.593 149.182 5 9 6 2-1.82151 87.9038 5 9 6 3 1743.65 356.437 5 9 6 4 871.627 259.162 5 9 6 5 775.488 246.693 5 9 6 6 213.275 143.635 5 9 6 7 567.198 226.573 5 9 -7 -10-37.9173 101.853 6 9 -7 -9 313.188 254.850 6 9 -7 -8 247.353 209.326 6 9 -7 -7 200.355 208.003 6 9 -7 -6 88.6830 86.5097 6 9 -7 -5-50.8771 91.0600 6 9 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182.130 4 10 2 -5 1684.97 251.738 4 10 2 -4 1176.69 197.426 4 10 2 -3 152.226 65.3656 6 10 2 -2 1836.59 214.556 5 10 2 -2 1866.55 224.564 6 10 2 -1 312.206 103.164 5 10 -2 -1 251.100 75.3050 4 10 2 0 240.612 84.3734 5 10 -2 0 88.7453 24.0475 5 10 -2 0 133.896 54.5596 4 10 -2 1 1379.87 130.353 5 10 2 1 1724.34 215.450 5 10 2 2 461.145 120.999 5 10 3 -15 161.980 149.963 4 10 3 -14 9.76849 99.7978 4 10 3 -13-102.913 138.499 4 10 3 -12 110.374 173.853 4 10 -3 -12 25.4852 103.378 6 10 3 -11 699.663 255.961 4 10 -3 -11 828.280 224.574 6 10 3 -10 996.580 275.039 4 10 -3 -10 1048.65 263.835 6 10 -3 -9 476.799 162.591 6 10 3 -9 372.410 166.028 4 10 -3 -8 532.339 165.274 6 10 3 -8 817.887 229.119 4 10 -3 -7 575.066 172.473 6 10 3 -7 94.7632 108.841 4 10 -3 -6 1350.65 254.540 6 10 3 -6 1256.24 249.797 4 10 -3 -5 1297.18 259.862 6 10 3 -5 1009.65 215.985 4 10 3 -4 204.768 115.821 4 10 3 -3 247.922 90.1146 5 10 3 -2 1050.93 194.862 5 10 3 -1 472.178 133.532 5 10 3 0 1673.62 243.304 5 10 3 1 2335.54 294.331 5 10 3 2 570.986 145.301 5 10 3 3 382.998 128.282 5 10 3 4 380.528 145.393 5 10 4 -14 272.846 195.811 4 10 4 -13 402.935 241.069 4 10 4 -12 943.053 311.689 4 10 -4 -12 320.133 190.938 6 10 4 -11 705.864 252.810 4 10 -4 -11 796.471 258.223 6 10 -4 -10 264.488 167.168 6 10 4 -10 402.449 187.808 4 10 -4 -9 149.022 163.952 6 10 4 -9 218.530 172.590 4 10 -4 -8 635.841 223.960 6 10 4 -8 480.352 195.797 4 10 -4 -7 131.011 138.726 6 10 4 -7 86.8594 81.0502 4 10 -4 -6 733.827 223.072 6 10 4 -6 637.084 223.900 4 10 -4 -5 177.399 115.202 6 10 4 -3 1046.77 219.873 5 10 4 -2 1009.81 205.155 5 10 4 -1 723.455 171.404 5 10 4 0 282.482 141.291 5 10 4 1 660.401 192.748 5 10 4 2 1176.82 236.963 5 10 4 3 1562.07 275.548 5 10 4 4 1171.49 245.110 5 10 4 5 391.406 136.269 5 10 4 6 101.698 110.101 5 10 5 -13 295.368 231.724 4 10 5 -12-8.43957 98.2085 4 10 -5 -12 211.770 140.713 6 10 5 -11 48.1717 99.3727 4 10 -5 -11 44.5552 103.353 6 10 -5 -10 951.815 300.463 6 10 5 -10 598.909 230.439 4 10 -5 -9 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126.330 5 10 6 3 362.955 178.479 5 10 6 4 257.264 154.247 5 10 6 5 349.715 165.517 5 10 6 6-20.7731 88.3421 5 10 6 7 323.374 192.679 5 10 -7 -10 173.752 201.482 6 10 -7 -9 185.640 99.7012 6 10 -7 -8-215.392 166.384 6 10 -7 -7-5.78749 127.621 6 10 -7 -6-156.118 146.955 6 10 -7 -5 289.648 162.022 6 10 -7 -4 93.4074 117.148 6 10 -7 -3 553.514 292.646 6 10 7 -2 97.9029 124.774 5 10 7 -1 532.507 251.212 5 10 7 0-29.5485 105.697 5 10 7 1 1059.44 292.749 5 10 7 2 418.826 208.652 5 10 7 3 298.736 182.093 5 10 7 4 196.767 155.935 5 11 0 -3 43.7657 32.7686 4 11 0 0 1196.86 110.468 5 11 -1 -9 2256.07 244.070 6 11 -1 -8 2470.41 239.112 6 11 -1 -7 568.270 113.478 6 11 -1 -6 992.379 156.528 6 11 1 -5 43.3650 56.0425 4 11 1 -4 427.493 70.8703 6 11 1 -4 965.480 148.914 4 11 1 -3 683.427 102.005 4 11 1 -3 859.929 134.738 6 11 -1 -2 13.0738 18.0818 4 11 1 -2 21.5645 47.2936 6 11 1 -1 372.938 82.0512 5 11 1 0 2287.41 205.955 5 11 1 1 4844.19 318.023 5 11 2 -10 827.226 247.079 4 11 2 -9 599.076 193.395 4 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