#=============================================================================== data_SRX-PTSA-MeOH #=============================================================================== _audit_creation_method 'SHELXL-2014/7' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C7 H7 O3 S, C23 H24 Cl N6 O2, C H4 O' _chemical_formula_sum 'C31 H35 Cl N6 O6 S' _chemical_formula_weight 655.16 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cl' 'Cl' 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'S' 'S' 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 4 _space_group_name_H-M_alt 'P 21' _space_group_name_Hall 'P 2yb' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' _cell_length_a 14.5891(8) _cell_length_b 7.5159(3) _cell_length_c 15.6522(9) _cell_angle_alpha 90 _cell_angle_beta 113.725(7) _cell_angle_gamma 90 _cell_volume 1571.22(15) _cell_formula_units_Z 2 _cell_measurement_temperature 120(2) _cell_measurement_reflns_used 900 _cell_measurement_theta_min 2.6 _cell_measurement_theta_max 29.1 _exptl_crystal_description Needle _exptl_crystal_colour colourless _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.385 _exptl_crystal_F_000 688 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.400 _exptl_crystal_size_mid 0.020 _exptl_crystal_size_min 0.010 _exptl_absorpt_coefficient_mu 0.242 _shelx_estimated_absorpt_T_min 0.909 _shelx_estimated_absorpt_T_max 0.998 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.994 _exptl_absorpt_correction_T_max 0.998 _exptl_absorpt_process_details SADABS _diffrn_ambient_temperature 120(2) _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'Mova (Mo) X-ray Source' _diffrn_measurement_device_type 'Mova (Mo) X-ray Source' _diffrn_measurement_method ? _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 6669 _diffrn_reflns_av_unetI/netI 0.0760 _diffrn_reflns_av_R_equivalents 0.0292 _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_h_max 17 _diffrn_reflns_limit_k_min -8 _diffrn_reflns_limit_k_max 9 _diffrn_reflns_limit_l_min -19 _diffrn_reflns_limit_l_max 18 _diffrn_reflns_theta_min 2.630 _diffrn_reflns_theta_max 25.998 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measured_fraction_theta_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.855 _diffrn_reflns_point_group_measured_fraction_full 0.869 _reflns_number_total 5283 _reflns_number_gt 4571 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.583 _reflns_Friedel_fraction_max 0.685 _reflns_Friedel_fraction_full 0.716 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_cell_refinement 'CrysAlisPro 1.171.38.41 (Rigaku OD, 2015)' _computing_data_collection 'CrysAlisPro 1.171.38.41 (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.38.41 (Rigaku OD, 2015)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0318P)^2^+0.1245P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens mixed _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_abs_structure_details ; Flack x determined using 1398 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack -0.04(7) _chemical_absolute_configuration rm _refine_ls_number_reflns 5283 _refine_ls_number_parameters 418 _refine_ls_number_restraints 1 _refine_ls_R_factor_all 0.0616 _refine_ls_R_factor_gt 0.0509 _refine_ls_wR_factor_ref 0.1059 _refine_ls_wR_factor_gt 0.0961 _refine_ls_goodness_of_fit_ref 1.045 _refine_ls_restrained_S_all 1.045 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group S1 S -0.22322(8) 0.15396(17) -0.22235(8) 0.0228(3) Uani 1 1 d . . . . . Cl1 Cl -0.29277(9) -0.33412(19) -0.55247(8) 0.0337(3) Uani 1 1 d . . . . . N5 N -0.2120(3) -0.8520(6) 0.2638(2) 0.0190(8) Uani 1 1 d . . . . . O2 O -0.3733(2) -0.8284(4) 0.0310(2) 0.0210(7) Uani 1 1 d . . . . . O1 O -0.4282(2) -0.4749(4) -0.2565(2) 0.0211(7) Uani 1 1 d . . . . . O3 O -0.1884(2) 0.0056(4) -0.1551(2) 0.0245(8) Uani 1 1 d . . . . . C20 C -0.1578(3) -0.8576(7) 0.2051(3) 0.0185(9) Uani 1 1 d . . . . . C24 C -0.1458(3) 0.1511(7) -0.2852(3) 0.0206(9) Uani 1 1 d . . . . . N2 N -0.3723(3) -0.3462(6) -0.1112(2) 0.0202(8) Uani 1 1 d . . . . . O6 O -0.4804(3) -0.0439(5) -0.2733(3) 0.0272(8) Uani 1 1 d . . . . . N1 N -0.3013(3) -0.2850(5) -0.2218(3) 0.0189(9) Uani 1 1 d . . . . . N3 N -0.3186(3) -0.5426(5) 0.0604(3) 0.0171(8) Uani 1 1 d . . . . . O5 O -0.2095(3) 0.3258(4) -0.1770(3) 0.0306(9) Uani 1 1 d . . . . . O4 O -0.3244(2) 0.1243(4) -0.2925(2) 0.0287(8) Uani 1 1 d . . . . . C7 C -0.3647(3) -0.3643(6) -0.1916(3) 0.0188(10) Uani 1 1 d . . . . . C14 C -0.3043(3) -0.7210(6) 0.0672(3) 0.0163(10) Uani 1 1 d . . . . . C23 C 0.0187(3) -0.8634(7) 0.0405(3) 0.0269(11) Uani 1 1 d . . . . . H23A H -0.0248 -0.8788 -0.0257 0.040 Uiso 1 1 calc R U . . . H23B H 0.0676 -0.9604 0.0609 0.040 Uiso 1 1 calc R U . . . H23C H 0.0539 -0.7493 0.0494 0.040 Uiso 1 1 calc R U . . . C3 C -0.3372(3) -0.3768(6) -0.4661(3) 0.0234(11) Uani 1 1 d . . . . . N6 N -0.1861(3) -0.9515(6) 0.3403(3) 0.0305(10) Uani 1 1 d . . . . . C26 C -0.0057(4) 0.0373(7) -0.3128(4) 0.0308(13) Uani 1 1 d . . . . . H26 H 0.0495 -0.0418 -0.2962 0.037 Uiso 1 1 calc R U . . . C9 C -0.4203(3) -0.4759(6) 0.0104(3) 0.0196(10) Uani 1 1 d . . . . . H9A H -0.4267 -0.3595 0.0371 0.024 Uiso 1 1 calc R U . . . H9B H -0.4679 -0.5593 0.0197 0.024 Uiso 1 1 calc R U . . . C29 C -0.1689(4) 0.2623(6) -0.3618(3) 0.0248(11) Uani 1 1 d . . . . . H29 H -0.2255 0.3385 -0.3796 0.030 Uiso 1 1 calc R U . . . C17 C -0.0439(3) -0.8657(6) 0.0972(3) 0.0208(10) Uani 1 1 d . . . . . N4 N -0.2912(3) -0.7454(6) 0.2464(3) 0.0314(11) Uani 1 1 d . . . . . C1 C -0.3285(3) -0.3389(7) -0.3150(3) 0.0201(9) Uani 1 1 d . . . . . C8 C -0.4481(3) -0.4539(6) -0.0931(3) 0.0208(11) Uani 1 1 d . . . . . H8A H -0.4536 -0.5726 -0.1222 0.025 Uiso 1 1 calc R U . . . H8B H -0.5142 -0.3949 -0.1221 0.025 Uiso 1 1 calc R U . . . C2 C -0.2910(4) -0.2946(6) -0.3803(3) 0.0238(11) Uani 1 1 d . . . . . H2 H -0.2372 -0.2132 -0.3672 0.029 Uiso 1 1 calc R U . . . C27 C -0.0270(3) 0.1513(8) -0.3890(3) 0.0271(11) Uani 1 1 d . . . . . C19 C -0.0622(3) -0.9319(6) 0.2415(3) 0.0212(11) Uani 1 1 d . . . . . H19 H -0.0352 -0.9798 0.3029 0.025 Uiso 1 1 calc R U . . . C16 C -0.1404(3) -0.7949(6) 0.0621(3) 0.0199(10) Uani 1 1 d . . . . . H16 H -0.1676 -0.7488 0.0004 0.024 Uiso 1 1 calc R U . . . C12 C -0.3092(4) -0.2150(6) -0.0420(3) 0.0213(11) Uani 1 1 d . . . . . H12A H -0.3499 -0.1563 -0.0125 0.026 Uiso 1 1 calc R U . . . H12B H -0.2872 -0.1223 -0.0745 0.026 Uiso 1 1 calc R U . . . C4 C -0.4166(4) -0.4973(7) -0.4877(3) 0.0268(12) Uani 1 1 d . . . . . H4 H -0.4457 -0.5496 -0.5480 0.032 Uiso 1 1 calc R U . . . C6 C -0.4063(3) -0.4579(6) -0.3350(3) 0.0209(11) Uani 1 1 d . . . . . C11 C -0.2175(3) -0.2989(6) 0.0338(3) 0.0199(11) Uani 1 1 d . . . . . H11A H -0.1700 -0.2028 0.0668 0.024 Uiso 1 1 calc R U . . . H11B H -0.1841 -0.3756 0.0034 0.024 Uiso 1 1 calc R U . . . C13 C -0.2591(4) -0.2967(6) 0.1776(3) 0.0254(11) Uani 1 1 d . . . . . H13A H -0.3126 -0.2115 0.1448 0.038 Uiso 1 1 calc R U . . . H13B H -0.1983 -0.2320 0.2166 0.038 Uiso 1 1 calc R U . . . H13C H -0.2799 -0.3739 0.2170 0.038 Uiso 1 1 calc R U . . . C18 C -0.0069(3) -0.9351(6) 0.1872(3) 0.0240(11) Uani 1 1 d . . . . . H18 H 0.0582 -0.9862 0.2123 0.029 Uiso 1 1 calc R U . . . C30 C 0.0367(4) 0.1523(8) -0.4446(3) 0.0367(13) Uani 1 1 d . . . . . H30A H -0.0056 0.1293 -0.5105 0.055 Uiso 1 1 calc R U . . . H30B H 0.0880 0.0596 -0.4210 0.055 Uiso 1 1 calc R U . . . H30C H 0.0690 0.2687 -0.4386 0.055 Uiso 1 1 calc R U . . . C28 C -0.1103(4) 0.2634(6) -0.4124(4) 0.0253(12) Uani 1 1 d . . . . . H28 H -0.1267 0.3415 -0.4642 0.030 Uiso 1 1 calc R U . . . C25 C -0.0638(4) 0.0373(6) -0.2607(3) 0.0268(12) Uani 1 1 d . . . . . H25 H -0.0476 -0.0400 -0.2086 0.032 Uiso 1 1 calc R U . . . C10 C -0.2380(3) -0.4103(6) 0.1061(3) 0.0192(10) Uani 1 1 d . . . . . H10 H -0.1755 -0.4793 0.1416 0.023 Uiso 1 1 calc R U . . . C15 C -0.1983(3) -0.7893(6) 0.1143(3) 0.0184(10) Uani 1 1 d . . . . . C22 C -0.2536(4) -0.9063(6) 0.3740(3) 0.0296(13) Uani 1 1 d . . . . . H22 H -0.2568 -0.9534 0.4291 0.036 Uiso 1 1 calc R U . . . C5 C -0.4524(4) -0.5397(6) -0.4204(3) 0.0265(11) Uani 1 1 d . . . . . H5 H -0.5060 -0.6211 -0.4326 0.032 Uiso 1 1 calc R U . . . C21 C -0.3184(4) -0.7799(7) 0.3162(4) 0.0300(12) Uani 1 1 d . . . . . H21 H -0.3731 -0.7269 0.3251 0.036 Uiso 1 1 calc R U . . . C31 C -0.5055(4) 0.0658(7) -0.2112(4) 0.0331(13) Uani 1 1 d . . . . . H31A H -0.4448 0.0925 -0.1557 0.050 Uiso 1 1 calc R U . . . H31B H -0.5535 0.0031 -0.1926 0.050 Uiso 1 1 calc R U . . . H31C H -0.5355 0.1770 -0.2428 0.050 Uiso 1 1 calc R U . . . H1 H -0.257(4) -0.204(7) -0.187(4) 0.035(16) Uiso 1 1 d . . . . . H02 H -0.437(4) -0.004(8) -0.283(4) 0.05(2) Uiso 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 S1 0.0250(6) 0.0183(6) 0.0254(6) 0.0018(6) 0.0105(5) -0.0031(6) Cl1 0.0452(7) 0.0368(7) 0.0258(6) -0.0007(7) 0.0211(6) -0.0025(7) N5 0.022(2) 0.0157(18) 0.0192(19) 0.002(2) 0.0075(16) -0.001(2) O2 0.0130(15) 0.0186(16) 0.0295(17) -0.0010(17) 0.0065(13) -0.0027(15) O1 0.0243(18) 0.0211(18) 0.0192(17) -0.0029(15) 0.0102(15) -0.0054(14) O3 0.0289(19) 0.0217(18) 0.0210(19) 0.0038(16) 0.0081(16) -0.0048(15) C20 0.016(2) 0.016(2) 0.022(2) -0.005(2) 0.0058(18) -0.004(2) C24 0.022(2) 0.014(2) 0.024(2) -0.004(2) 0.0071(19) -0.002(2) N2 0.026(2) 0.0183(19) 0.0199(19) 0.003(2) 0.0134(16) -0.003(2) O6 0.025(2) 0.027(2) 0.033(2) -0.0030(17) 0.0147(18) -0.0047(17) N1 0.020(2) 0.016(2) 0.022(2) -0.0030(18) 0.0090(18) -0.0053(17) N3 0.014(2) 0.015(2) 0.022(2) 0.0004(18) 0.0066(17) 0.0009(16) O5 0.044(2) 0.0173(18) 0.036(2) -0.0010(17) 0.022(2) -0.0018(17) O4 0.0232(17) 0.031(2) 0.0302(18) 0.0056(18) 0.0091(15) -0.0025(16) C7 0.022(2) 0.014(2) 0.022(2) 0.002(2) 0.0101(19) 0.002(2) C14 0.018(2) 0.017(2) 0.017(2) 0.003(2) 0.011(2) 0.000(2) C23 0.020(2) 0.026(3) 0.037(3) -0.005(3) 0.014(2) 0.001(2) C3 0.030(3) 0.023(3) 0.020(2) 0.003(2) 0.013(2) 0.003(2) N6 0.040(3) 0.027(2) 0.027(2) 0.006(2) 0.016(2) 0.006(2) C26 0.026(3) 0.026(3) 0.037(3) -0.001(3) 0.009(2) 0.006(2) C9 0.014(2) 0.020(3) 0.024(3) 0.001(2) 0.007(2) 0.001(2) C29 0.027(3) 0.020(3) 0.024(3) 0.002(2) 0.007(2) 0.004(2) C17 0.019(2) 0.016(2) 0.027(2) -0.004(2) 0.0078(19) -0.002(2) N4 0.031(3) 0.038(3) 0.031(3) 0.009(2) 0.019(2) 0.013(2) C1 0.023(2) 0.016(2) 0.019(2) -0.001(2) 0.0072(19) 0.002(2) C8 0.018(2) 0.023(3) 0.022(2) 0.005(2) 0.008(2) 0.001(2) C2 0.025(3) 0.019(3) 0.028(3) 0.002(2) 0.011(2) 0.001(2) C27 0.024(2) 0.027(3) 0.030(3) -0.010(3) 0.010(2) -0.008(3) C19 0.020(3) 0.015(2) 0.023(3) 0.005(2) 0.003(2) 0.001(2) C16 0.019(2) 0.015(3) 0.024(2) 0.000(2) 0.007(2) -0.0034(19) C12 0.032(3) 0.014(2) 0.024(3) 0.001(2) 0.018(2) -0.002(2) C4 0.028(3) 0.027(3) 0.021(3) -0.002(2) 0.006(2) -0.002(2) C6 0.027(3) 0.018(3) 0.020(2) 0.002(2) 0.012(2) 0.002(2) C11 0.022(2) 0.018(3) 0.024(2) -0.001(2) 0.013(2) -0.004(2) C13 0.028(3) 0.021(3) 0.025(3) 0.001(2) 0.009(2) -0.003(2) C18 0.017(3) 0.018(2) 0.032(3) 0.000(2) 0.005(2) 0.003(2) C30 0.037(3) 0.039(3) 0.040(3) -0.012(3) 0.022(3) -0.009(3) C28 0.028(3) 0.023(3) 0.026(3) 0.001(2) 0.013(2) 0.001(2) C25 0.030(3) 0.021(3) 0.026(3) 0.002(2) 0.009(2) 0.002(2) C10 0.015(2) 0.016(2) 0.025(2) -0.001(2) 0.007(2) -0.0029(18) C15 0.018(2) 0.012(2) 0.022(2) 0.002(2) 0.004(2) -0.0018(19) C22 0.043(3) 0.029(3) 0.021(3) 0.001(2) 0.017(3) 0.000(2) C5 0.034(3) 0.017(3) 0.027(3) -0.004(2) 0.011(2) -0.003(2) C21 0.037(3) 0.033(3) 0.030(3) 0.001(3) 0.023(3) 0.001(2) C31 0.041(3) 0.034(3) 0.026(3) -0.006(3) 0.015(3) -0.003(3) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag S1 O5 1.448(3) . ? S1 O4 1.460(3) . ? S1 O3 1.476(3) . ? S1 C24 1.771(4) . ? Cl1 C3 1.747(4) . ? N5 N6 1.332(5) . ? N5 N4 1.340(5) . ? N5 C20 1.434(5) . ? O2 C14 1.236(5) . ? O1 C7 1.350(5) . ? O1 C6 1.394(5) . ? C20 C19 1.393(6) . ? C20 C15 1.399(6) . ? C24 C29 1.388(6) . ? C24 C25 1.393(6) . ? N2 C7 1.314(5) . ? N2 C12 1.480(6) . ? N2 C8 1.487(5) . ? O6 C31 1.430(6) . ? O6 H02 0.77(5) . ? N1 C7 1.336(5) . ? N1 C1 1.409(5) . ? N1 H1 0.89(5) . ? N3 C14 1.354(5) . ? N3 C9 1.460(5) . ? N3 C10 1.485(5) . ? C14 C15 1.510(6) . ? C23 C17 1.508(6) . ? C23 H23A 0.9800 . ? C23 H23B 0.9800 . ? C23 H23C 0.9800 . ? C3 C2 1.383(6) . ? C3 C4 1.400(6) . ? N6 C22 1.334(6) . ? C26 C25 1.393(6) . ? C26 C27 1.398(7) . ? C26 H26 0.9500 . ? C9 C8 1.512(6) . ? C9 H9A 0.9900 . ? C9 H9B 0.9900 . ? C29 C28 1.380(6) . ? C29 H29 0.9500 . ? C17 C18 1.392(6) . ? C17 C16 1.395(6) . ? N4 C21 1.330(6) . ? C1 C6 1.378(6) . ? C1 C2 1.380(6) . ? C8 H8A 0.9900 . ? C8 H8B 0.9900 . ? C2 H2 0.9500 . ? C27 C28 1.401(7) . ? C27 C30 1.507(6) . ? C19 C18 1.388(6) . ? C19 H19 0.9500 . ? C16 C15 1.391(6) . ? C16 H16 0.9500 . ? C12 C11 1.522(6) . ? C12 H12A 0.9900 . ? C12 H12B 0.9900 . ? C4 C5 1.388(6) . ? C4 H4 0.9500 . ? C6 C5 1.376(6) . ? C11 C10 1.532(6) . ? C11 H11A 0.9900 . ? C11 H11B 0.9900 . ? C13 C10 1.535(6) . ? C13 H13A 0.9800 . ? C13 H13B 0.9800 . ? C13 H13C 0.9800 . ? C18 H18 0.9500 . ? C30 H30A 0.9800 . ? C30 H30B 0.9800 . ? C30 H30C 0.9800 . ? C28 H28 0.9500 . ? C25 H25 0.9500 . ? C10 H10 1.0000 . ? C22 C21 1.388(7) . ? C22 H22 0.9500 . ? C5 H5 0.9500 . ? C21 H21 0.9500 . ? C31 H31A 0.9800 . ? C31 H31B 0.9800 . ? C31 H31C 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O5 S1 O4 113.8(2) . . ? O5 S1 O3 112.59(19) . . ? O4 S1 O3 112.00(19) . . ? O5 S1 C24 106.8(2) . . ? O4 S1 C24 104.93(19) . . ? O3 S1 C24 105.9(2) . . ? N6 N5 N4 115.3(4) . . ? N6 N5 C20 122.0(4) . . ? N4 N5 C20 122.7(4) . . ? C7 O1 C6 106.0(3) . . ? C19 C20 C15 120.5(4) . . ? C19 C20 N5 118.0(4) . . ? C15 C20 N5 121.5(4) . . ? C29 C24 C25 119.4(4) . . ? C29 C24 S1 119.1(4) . . ? C25 C24 S1 121.5(4) . . ? C7 N2 C12 120.2(4) . . ? C7 N2 C8 118.8(4) . . ? C12 N2 C8 120.9(3) . . ? C31 O6 H02 112(5) . . ? C7 N1 C1 106.9(4) . . ? C7 N1 H1 121(3) . . ? C1 N1 H1 131(3) . . ? C14 N3 C9 118.3(4) . . ? C14 N3 C10 123.9(4) . . ? C9 N3 C10 117.7(3) . . ? N2 C7 N1 129.0(4) . . ? N2 C7 O1 119.2(4) . . ? N1 C7 O1 111.8(4) . . ? O2 C14 N3 122.6(4) . . ? O2 C14 C15 119.2(4) . . ? N3 C14 C15 118.0(4) . . ? C17 C23 H23A 109.5 . . ? C17 C23 H23B 109.5 . . ? H23A C23 H23B 109.5 . . ? C17 C23 H23C 109.5 . . ? H23A C23 H23C 109.5 . . ? H23B C23 H23C 109.5 . . ? C2 C3 C4 123.7(4) . . ? C2 C3 Cl1 118.8(4) . . ? C4 C3 Cl1 117.4(4) . . ? N5 N6 C22 103.0(4) . . ? C25 C26 C27 121.4(5) . . ? C25 C26 H26 119.3 . . ? C27 C26 H26 119.3 . . ? N3 C9 C8 112.9(4) . . ? N3 C9 H9A 109.0 . . ? C8 C9 H9A 109.0 . . ? N3 C9 H9B 109.0 . . ? C8 C9 H9B 109.0 . . ? H9A C9 H9B 107.8 . . ? C28 C29 C24 120.6(4) . . ? C28 C29 H29 119.7 . . ? C24 C29 H29 119.7 . . ? C18 C17 C16 117.4(4) . . ? C18 C17 C23 121.3(4) . . ? C16 C17 C23 121.2(4) . . ? C21 N4 N5 103.6(4) . . ? C6 C1 C2 121.6(4) . . ? C6 C1 N1 106.6(4) . . ? C2 C1 N1 131.8(4) . . ? N2 C8 C9 111.3(4) . . ? N2 C8 H8A 109.4 . . ? C9 C8 H8A 109.4 . . ? N2 C8 H8B 109.4 . . ? C9 C8 H8B 109.4 . . ? H8A C8 H8B 108.0 . . ? C1 C2 C3 115.4(4) . . ? C1 C2 H2 122.3 . . ? C3 C2 H2 122.3 . . ? C26 C27 C28 117.6(4) . . ? C26 C27 C30 121.3(5) . . ? C28 C27 C30 121.2(5) . . ? C18 C19 C20 119.3(4) . . ? C18 C19 H19 120.4 . . ? C20 C19 H19 120.4 . . ? C15 C16 C17 122.4(4) . . ? C15 C16 H16 118.8 . . ? C17 C16 H16 118.8 . . ? N2 C12 C11 112.8(4) . . ? N2 C12 H12A 109.0 . . ? C11 C12 H12A 109.0 . . ? N2 C12 H12B 109.0 . . ? C11 C12 H12B 109.0 . . ? H12A C12 H12B 107.8 . . ? C5 C4 C3 119.5(5) . . ? C5 C4 H4 120.2 . . ? C3 C4 H4 120.2 . . ? C5 C6 C1 123.1(4) . . ? C5 C6 O1 128.3(4) . . ? C1 C6 O1 108.6(4) . . ? C12 C11 C10 115.5(4) . . ? C12 C11 H11A 108.4 . . ? C10 C11 H11A 108.4 . . ? C12 C11 H11B 108.4 . . ? C10 C11 H11B 108.4 . . ? H11A C11 H11B 107.5 . . ? C10 C13 H13A 109.5 . . ? C10 C13 H13B 109.5 . . ? H13A C13 H13B 109.5 . . ? C10 C13 H13C 109.5 . . ? H13A C13 H13C 109.5 . . ? H13B C13 H13C 109.5 . . ? C19 C18 C17 121.9(4) . . ? C19 C18 H18 119.0 . . ? C17 C18 H18 119.0 . . ? C27 C30 H30A 109.5 . . ? C27 C30 H30B 109.5 . . ? H30A C30 H30B 109.5 . . ? C27 C30 H30C 109.5 . . ? H30A C30 H30C 109.5 . . ? H30B C30 H30C 109.5 . . ? C29 C28 C27 121.3(5) . . ? C29 C28 H28 119.4 . . ? C27 C28 H28 119.4 . . ? C26 C25 C24 119.7(5) . . ? C26 C25 H25 120.1 . . ? C24 C25 H25 120.1 . . ? N3 C10 C11 111.2(4) . . ? N3 C10 C13 111.8(4) . . ? C11 C10 C13 113.0(4) . . ? N3 C10 H10 106.8 . . ? C11 C10 H10 106.8 . . ? C13 C10 H10 106.8 . . ? C16 C15 C20 118.5(4) . . ? C16 C15 C14 117.9(4) . . ? C20 C15 C14 123.5(4) . . ? N6 C22 C21 109.6(4) . . ? N6 C22 H22 125.2 . . ? C21 C22 H22 125.2 . . ? C6 C5 C4 116.7(5) . . ? C6 C5 H5 121.7 . . ? C4 C5 H5 121.7 . . ? N4 C21 C22 108.5(4) . . ? N4 C21 H21 125.7 . . ? C22 C21 H21 125.7 . . ? O6 C31 H31A 109.5 . . ? O6 C31 H31B 109.5 . . ? H31A C31 H31B 109.5 . . ? O6 C31 H31C 109.5 . . ? H31A C31 H31C 109.5 . . ? H31B C31 H31C 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag N6 N5 C20 C19 -16.9(7) . . . . ? N4 N5 C20 C19 162.2(4) . . . . ? N6 N5 C20 C15 163.8(4) . . . . ? N4 N5 C20 C15 -17.1(7) . . . . ? O5 S1 C24 C29 -67.8(4) . . . . ? O4 S1 C24 C29 53.4(4) . . . . ? O3 S1 C24 C29 172.0(4) . . . . ? O5 S1 C24 C25 113.6(4) . . . . ? O4 S1 C24 C25 -125.2(4) . . . . ? O3 S1 C24 C25 -6.6(5) . . . . ? C12 N2 C7 N1 4.2(7) . . . . ? C8 N2 C7 N1 -178.4(4) . . . . ? C12 N2 C7 O1 -175.0(4) . . . . ? C8 N2 C7 O1 2.3(6) . . . . ? C1 N1 C7 N2 -175.6(5) . . . . ? C1 N1 C7 O1 3.7(5) . . . . ? C6 O1 C7 N2 176.4(4) . . . . ? C6 O1 C7 N1 -2.9(5) . . . . ? C9 N3 C14 O2 1.7(6) . . . . ? C10 N3 C14 O2 177.6(4) . . . . ? C9 N3 C14 C15 176.6(4) . . . . ? C10 N3 C14 C15 -7.5(6) . . . . ? N4 N5 N6 C22 0.3(6) . . . . ? C20 N5 N6 C22 179.5(4) . . . . ? C14 N3 C9 C8 -88.2(5) . . . . ? C10 N3 C9 C8 95.7(5) . . . . ? C25 C24 C29 C28 -1.3(7) . . . . ? S1 C24 C29 C28 -179.9(4) . . . . ? N6 N5 N4 C21 -0.5(6) . . . . ? C20 N5 N4 C21 -179.7(4) . . . . ? C7 N1 C1 C6 -2.9(5) . . . . ? C7 N1 C1 C2 177.9(5) . . . . ? C7 N2 C8 C9 156.7(4) . . . . ? C12 N2 C8 C9 -26.0(6) . . . . ? N3 C9 C8 N2 -52.2(5) . . . . ? C6 C1 C2 C3 0.3(7) . . . . ? N1 C1 C2 C3 179.4(5) . . . . ? C4 C3 C2 C1 0.0(7) . . . . ? Cl1 C3 C2 C1 -178.2(3) . . . . ? C25 C26 C27 C28 -1.3(8) . . . . ? C25 C26 C27 C30 179.4(5) . . . . ? C15 C20 C19 C18 0.9(7) . . . . ? N5 C20 C19 C18 -178.4(4) . . . . ? C18 C17 C16 C15 1.2(7) . . . . ? C23 C17 C16 C15 -177.5(4) . . . . ? C7 N2 C12 C11 -98.8(5) . . . . ? C8 N2 C12 C11 83.9(5) . . . . ? C2 C3 C4 C5 -0.3(7) . . . . ? Cl1 C3 C4 C5 178.0(4) . . . . ? C2 C1 C6 C5 -0.4(7) . . . . ? N1 C1 C6 C5 -179.7(4) . . . . ? C2 C1 C6 O1 -179.6(4) . . . . ? N1 C1 C6 O1 1.1(5) . . . . ? C7 O1 C6 C5 -178.1(5) . . . . ? C7 O1 C6 C1 1.0(5) . . . . ? N2 C12 C11 C10 -73.4(5) . . . . ? C20 C19 C18 C17 0.2(7) . . . . ? C16 C17 C18 C19 -1.2(7) . . . . ? C23 C17 C18 C19 177.5(4) . . . . ? C24 C29 C28 C27 0.8(8) . . . . ? C26 C27 C28 C29 0.5(8) . . . . ? C30 C27 C28 C29 179.8(5) . . . . ? C27 C26 C25 C24 0.9(7) . . . . ? C29 C24 C25 C26 0.4(7) . . . . ? S1 C24 C25 C26 179.0(4) . . . . ? C14 N3 C10 C11 115.0(4) . . . . ? C9 N3 C10 C11 -69.0(5) . . . . ? C14 N3 C10 C13 -117.6(4) . . . . ? C9 N3 C10 C13 58.3(5) . . . . ? C12 C11 C10 N3 50.8(5) . . . . ? C12 C11 C10 C13 -75.9(5) . . . . ? C17 C16 C15 C20 -0.1(7) . . . . ? C17 C16 C15 C14 -176.0(4) . . . . ? C19 C20 C15 C16 -1.0(7) . . . . ? N5 C20 C15 C16 178.3(4) . . . . ? C19 C20 C15 C14 174.7(4) . . . . ? N5 C20 C15 C14 -6.0(7) . . . . ? O2 C14 C15 C16 94.3(5) . . . . ? N3 C14 C15 C16 -80.8(5) . . . . ? O2 C14 C15 C20 -81.4(6) . . . . ? N3 C14 C15 C20 103.5(5) . . . . ? N5 N6 C22 C21 0.0(5) . . . . ? C1 C6 C5 C4 0.2(7) . . . . ? O1 C6 C5 C4 179.1(4) . . . . ? C3 C4 C5 C6 0.2(7) . . . . ? N5 N4 C21 C22 0.4(5) . . . . ? N6 C22 C21 N4 -0.2(6) . . . . ? _refine_diff_density_max 0.343 _refine_diff_density_min -0.308 _refine_diff_density_rms 0.059 _shelx_res_file ; shelx.res created by SHELXL-2014/7 TITL ST1_120K_ in P21 #4 CELL 0.71073 14.589079 7.515905 15.652224 90 113.7253 90 ZERR 2 0.000805 0.000288 0.000866 0 0.0066 0 LATT -1 SYMM -X,0.5+Y,-Z SFAC C H CL N O S UNIT 62 70 2 12 12 2 ACTA BOND $H L.S. 12 PLAN 5 MORE -1 BOND $H OMIT 0 52 SIZE 0.02 0.01 0.4 TEMP -153 CONF fmap 2 53 WGHT 0.031800 0.124500 FVAR 4.25557 S1 6 -0.223222 0.153960 -0.222349 11.00000 0.02495 0.01833 = 0.02539 0.00178 0.01048 -0.00309 CL1 3 -0.292765 -0.334121 -0.552468 11.00000 0.04518 0.03677 = 0.02583 -0.00066 0.02115 -0.00252 N5 4 -0.212032 -0.851959 0.263753 11.00000 0.02155 0.01568 = 0.01922 0.00250 0.00754 -0.00065 O2 5 -0.373313 -0.828353 0.031018 11.00000 0.01304 0.01861 = 0.02947 -0.00095 0.00652 -0.00269 O1 5 -0.428165 -0.474947 -0.256532 11.00000 0.02431 0.02110 = 0.01924 -0.00285 0.01024 -0.00544 O3 5 -0.188421 0.005557 -0.155144 11.00000 0.02892 0.02170 = 0.02101 0.00384 0.00808 -0.00479 C20 1 -0.157757 -0.857601 0.205109 11.00000 0.01597 0.01609 = 0.02180 -0.00535 0.00576 -0.00397 C24 1 -0.145849 0.151138 -0.285182 11.00000 0.02165 0.01374 = 0.02427 -0.00363 0.00712 -0.00219 N2 4 -0.372277 -0.346212 -0.111247 11.00000 0.02626 0.01829 = 0.01986 0.00261 0.01337 -0.00298 O6 5 -0.480409 -0.043895 -0.273297 11.00000 0.02484 0.02712 = 0.03263 -0.00301 0.01472 -0.00466 N1 4 -0.301269 -0.284994 -0.221765 11.00000 0.01955 0.01626 = 0.02155 -0.00297 0.00901 -0.00527 N3 4 -0.318587 -0.542622 0.060441 11.00000 0.01427 0.01456 = 0.02191 0.00039 0.00664 0.00088 O5 5 -0.209485 0.325765 -0.176960 11.00000 0.04377 0.01732 = 0.03620 -0.00100 0.02183 -0.00179 O4 5 -0.324395 0.124273 -0.292544 11.00000 0.02317 0.03125 = 0.03020 0.00563 0.00906 -0.00251 C7 1 -0.364708 -0.364283 -0.191639 11.00000 0.02179 0.01364 = 0.02220 0.00199 0.01010 0.00151 C14 1 -0.304259 -0.720987 0.067235 11.00000 0.01798 0.01738 = 0.01721 0.00293 0.01082 0.00007 C23 1 0.018678 -0.863360 0.040513 11.00000 0.01970 0.02620 = 0.03706 -0.00522 0.01369 0.00067 AFIX 137 H23A 2 -0.024794 -0.878801 -0.025682 11.00000 -1.50000 H23B 2 0.067603 -0.960437 0.060939 11.00000 -1.50000 H23C 2 0.053900 -0.749325 0.049429 11.00000 -1.50000 AFIX 0 C3 1 -0.337162 -0.376817 -0.466135 11.00000 0.03043 0.02266 = 0.02029 0.00277 0.01349 0.00293 N6 4 -0.186149 -0.951495 0.340324 11.00000 0.04006 0.02692 = 0.02663 0.00591 0.01560 0.00585 C26 1 -0.005724 0.037328 -0.312800 11.00000 0.02561 0.02634 = 0.03714 -0.00060 0.00913 0.00626 AFIX 43 H26 2 0.049524 -0.041815 -0.296214 11.00000 -1.20000 AFIX 0 C9 1 -0.420261 -0.475854 0.010372 11.00000 0.01406 0.01982 = 0.02430 0.00132 0.00712 0.00132 AFIX 23 H9A 2 -0.426695 -0.359479 0.037074 11.00000 -1.20000 H9B 2 -0.467936 -0.559263 0.019721 11.00000 -1.20000 AFIX 0 C29 1 -0.168865 0.262346 -0.361799 11.00000 0.02652 0.02026 = 0.02417 0.00185 0.00665 0.00397 AFIX 43 H29 2 -0.225490 0.338495 -0.379561 11.00000 -1.20000 AFIX 0 C17 1 -0.043910 -0.865696 0.097217 11.00000 0.01859 0.01584 = 0.02658 -0.00446 0.00780 -0.00185 N4 4 -0.291181 -0.745373 0.246388 11.00000 0.03137 0.03770 = 0.03089 0.00913 0.01864 0.01327 C1 1 -0.328523 -0.338857 -0.315037 11.00000 0.02331 0.01633 = 0.01934 -0.00117 0.00720 0.00181 C8 1 -0.448102 -0.453895 -0.093106 11.00000 0.01752 0.02268 = 0.02194 0.00535 0.00753 0.00071 AFIX 23 H8A 2 -0.453615 -0.572581 -0.122201 11.00000 -1.20000 H8B 2 -0.514208 -0.394943 -0.122055 11.00000 -1.20000 AFIX 0 C2 1 -0.291025 -0.294559 -0.380337 11.00000 0.02491 0.01922 = 0.02797 0.00175 0.01126 0.00093 AFIX 43 H2 2 -0.237235 -0.213179 -0.367237 11.00000 -1.20000 AFIX 0 C27 1 -0.026959 0.151340 -0.389003 11.00000 0.02363 0.02668 = 0.03006 -0.01012 0.00994 -0.00800 C19 1 -0.062235 -0.931858 0.241523 11.00000 0.02022 0.01468 = 0.02342 0.00526 0.00333 0.00116 AFIX 43 H19 2 -0.035238 -0.979799 0.302865 11.00000 -1.20000 AFIX 0 C16 1 -0.140433 -0.794888 0.062131 11.00000 0.01893 0.01463 = 0.02432 0.00049 0.00673 -0.00336 AFIX 43 H16 2 -0.167647 -0.748838 0.000393 11.00000 -1.20000 AFIX 0 C12 1 -0.309248 -0.215029 -0.041968 11.00000 0.03238 0.01394 = 0.02411 0.00148 0.01810 -0.00179 AFIX 23 H12A 2 -0.349927 -0.156299 -0.012498 11.00000 -1.20000 H12B 2 -0.287221 -0.122349 -0.074533 11.00000 -1.20000 AFIX 0 C4 1 -0.416558 -0.497278 -0.487704 11.00000 0.02839 0.02658 = 0.02147 -0.00168 0.00590 -0.00182 AFIX 43 H4 2 -0.445722 -0.549600 -0.547969 11.00000 -1.20000 AFIX 0 C6 1 -0.406291 -0.457904 -0.335019 11.00000 0.02738 0.01777 = 0.01968 0.00209 0.01177 0.00241 C11 1 -0.217473 -0.298885 0.033756 11.00000 0.02172 0.01769 = 0.02428 -0.00131 0.01335 -0.00435 AFIX 23 H11A 2 -0.170031 -0.202799 0.066811 11.00000 -1.20000 H11B 2 -0.184115 -0.375578 0.003439 11.00000 -1.20000 AFIX 0 C13 1 -0.259110 -0.296687 0.177613 11.00000 0.02845 0.02066 = 0.02495 0.00086 0.00859 -0.00295 AFIX 137 H13A 2 -0.312638 -0.211530 0.144820 11.00000 -1.50000 H13B 2 -0.198297 -0.232017 0.216638 11.00000 -1.50000 H13C 2 -0.279905 -0.373927 0.217033 11.00000 -1.50000 AFIX 0 C18 1 -0.006893 -0.935082 0.187242 11.00000 0.01709 0.01807 = 0.03242 0.00009 0.00536 0.00270 AFIX 43 H18 2 0.058167 -0.986153 0.212277 11.00000 -1.20000 AFIX 0 C30 1 0.036703 0.152302 -0.444633 11.00000 0.03717 0.03862 = 0.04031 -0.01215 0.02180 -0.00906 AFIX 137 H30A 2 -0.005556 0.129316 -0.510461 11.00000 -1.50000 H30B 2 0.088022 0.059559 -0.421002 11.00000 -1.50000 H30C 2 0.069037 0.268658 -0.438607 11.00000 -1.50000 AFIX 0 C28 1 -0.110264 0.263353 -0.412432 11.00000 0.02837 0.02327 = 0.02622 0.00139 0.01293 0.00064 AFIX 43 H28 2 -0.126745 0.341536 -0.464183 11.00000 -1.20000 AFIX 0 C25 1 -0.063842 0.037299 -0.260676 11.00000 0.03006 0.02114 = 0.02647 0.00205 0.00859 0.00180 AFIX 43 H25 2 -0.047617 -0.040044 -0.208626 11.00000 -1.20000 AFIX 0 C10 1 -0.237955 -0.410344 0.106130 11.00000 0.01530 0.01579 = 0.02545 -0.00145 0.00696 -0.00293 AFIX 13 H10 2 -0.175494 -0.479265 0.141628 11.00000 -1.20000 AFIX 0 C15 1 -0.198294 -0.789277 0.114307 11.00000 0.01751 0.01172 = 0.02244 0.00170 0.00429 -0.00179 C22 1 -0.253619 -0.906273 0.373992 11.00000 0.04295 0.02882 = 0.02118 0.00067 0.01709 -0.00018 AFIX 43 H22 2 -0.256809 -0.953360 0.429056 11.00000 -1.20000 AFIX 0 C5 1 -0.452351 -0.539701 -0.420377 11.00000 0.03434 0.01729 = 0.02663 -0.00390 0.01093 -0.00302 AFIX 43 H5 2 -0.505967 -0.621140 -0.432647 11.00000 -1.20000 AFIX 0 C21 1 -0.318439 -0.779875 0.316229 11.00000 0.03652 0.03297 = 0.02973 0.00076 0.02280 0.00074 AFIX 43 H21 2 -0.373098 -0.726884 0.325074 11.00000 -1.20000 AFIX 0 C31 1 -0.505531 0.065819 -0.211213 11.00000 0.04115 0.03430 = 0.02552 -0.00551 0.01527 -0.00311 AFIX 137 H31A 2 -0.444830 0.092489 -0.155688 11.00000 -1.50000 H31B 2 -0.553489 0.003103 -0.192612 11.00000 -1.50000 H31C 2 -0.535490 0.177047 -0.242795 11.00000 -1.50000 AFIX 0 H1 2 -0.257364 -0.204406 -0.187319 11.00000 0.03484 H02 2 -0.437208 -0.004023 -0.283294 11.00000 0.05470 HKLF 4 REM ST1_120K_ in P21 #4 REM R1 = 0.0509 for 4571 Fo > 4sig(Fo) and 0.0616 for all 5283 data REM 418 parameters refined using 1 restraints END WGHT 0.0331 0.1107 REM Highest difference peak 0.343, deepest hole -0.308, 1-sigma level 0.059 Q1 1 -0.1768 0.1546 -0.2577 11.00000 0.05 0.27 Q2 1 -0.5429 -0.0232 -0.3553 11.00000 0.05 0.25 Q3 1 -0.0545 0.2189 -0.3661 11.00000 0.05 0.25 Q4 1 -0.0983 0.1513 -0.2565 11.00000 0.05 0.24 Q5 1 -0.0844 -0.3573 0.0427 11.00000 0.05 0.24 ; _shelx_res_checksum 4317 _shelx_hkl_file ; 0 -7 0 452.395 166.430 4 0 -7 -1 3806.87 448.879 4 0 -7 1 3483.81 431.744 3 0 -7 -2 5250.90 560.479 4 0 -7 -3 589.830 219.769 4 0 -7 -4 18740.2 1147.92 4 0 -7 -5 1961.24 386.477 4 0 -7 -6 55.5525 97.8857 4 0 -7 -7 2723.13 494.603 4 0 -7 -8 993.286 284.615 4 0 -7 -9 11.9535 169.251 4 0 -7 -10 1135.43 387.386 4 0 -7 -11 382.170 235.991 4 0 -7 -12 1803.42 502.023 4 0 -7 -13 3015.93 722.092 4 0 -7 -14 5106.78 937.648 4 0 -6 0 34159.6 1298.96 3 0 -6 0 32615.2 1317.40 4 0 -6 -1 261.138 128.412 3 0 -6 -1 209.866 110.602 4 0 -6 -2 835.156 174.517 3 0 -6 -2 1003.62 233.451 4 0 -6 -3 5336.20 556.990 4 0 -6 -3 4970.35 437.216 3 0 -6 -4 8485.52 725.638 4 0 -6 -5 399.390 172.328 4 0 -6 -6 5081.68 618.095 4 0 -6 -7 2932.13 483.721 4 0 -6 -8 3040.54 522.672 4 0 -6 -9 2249.48 490.212 4 0 -6 -10 59.4343 163.201 4 0 -6 -11-208.159 181.388 4 0 -6 -12 3930.12 762.540 4 0 -6 -13 648.492 330.056 4 0 -6 -14 1053.49 393.256 4 0 -6 -15-243.727 224.279 4 0 -5 0 257.695 123.486 3 0 -5 -1 21079.8 890.226 3 0 -5 -1 21456.1 990.268 4 0 -5 -2 2574.01 287.440 3 0 -5 -2 2947.16 367.164 4 0 -5 -3 5510.75 509.606 4 0 -5 -3 5671.72 437.205 3 0 -5 -4 3399.89 322.838 1 0 -5 -4 4149.63 469.745 4 0 -5 -5 12573.5 870.697 4 0 -5 -5 12381.9 602.055 1 0 -5 -6 494.159 199.138 4 0 -5 -7 5423.59 636.010 4 0 -5 -8 4658.09 622.983 4 0 -5 -9 981.024 321.255 4 0 -5 -10 991.952 343.407 4 0 -5 -11 5578.27 808.143 4 0 -5 -12 1177.58 387.905 4 0 -5 -13 4236.09 777.966 4 0 -5 -14 3717.64 767.263 4 0 -5 -15 248.295 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957.143 2 2 3 2 53241.9 1430.54 4 2 3 2 52561.0 1114.12 3 2 3 3 7248.48 498.732 4 2 3 3 8236.40 388.636 3 2 3 4 7555.97 431.325 3 2 3 6 11853.6 699.649 1 2 3 7 11420.3 715.638 1 2 3 8 2495.20 341.063 1 2 3 9 6500.48 589.830 1 2 3 10 882.097 218.814 1 2 3 11 255.677 149.184 1 2 3 12 9111.87 801.493 1 2 3 13 7719.65 767.262 1 2 3 14 1994.63 404.141 1 -2 4 5 6365.95 718.064 2 -2 4 4 20443.4 1268.49 2 -2 4 3 1927.70 371.405 2 2 4 -3 2198.79 423.300 2 2 4 -2 6620.91 713.079 2 -2 4 2 7523.73 735.709 2 -2 4 1 1444.64 328.433 2 2 4 -1 1796.99 384.177 2 -2 4 0 31653.9 1532.02 2 2 4 0 31367.6 1629.55 2 2 4 1 27196.1 1535.58 2 2 4 2 29805.8 1625.15 2 2 4 3 4333.63 406.493 4 2 4 3 3064.12 507.592 2 2 4 4 36318.3 1069.57 3 2 4 5 8024.66 500.364 3 2 4 6 484.463 146.878 3 2 4 11 2582.88 403.039 1 2 4 12 349.682 179.272 1 -2 5 7 5021.25 731.476 2 -2 5 6 272.976 178.502 2 -2 5 5 4194.00 647.711 2 -2 5 4 3893.78 617.124 2 2 5 -3 7692.67 851.346 2 -2 5 3 8256.76 882.291 2 -2 5 2 222.901 107.707 2 2 5 -2 262.731 233.235 2 -2 5 1 5101.76 675.629 2 2 5 -1 6520.11 795.916 2 -2 5 0 7759.23 827.321 2 2 5 0 6984.28 842.069 2 2 5 1 6145.52 813.142 2 2 5 2 901.574 309.771 2 2 5 3 14074.0 1232.95 2 2 5 4 2676.92 550.695 2 2 5 5 12577.3 643.821 3 2 5 5 12754.1 1215.85 2 -2 6 10 1304.94 524.746 2 -2 6 9 836.225 348.262 2 -2 6 8 8960.04 1106.52 2 -2 6 7 1466.52 459.225 2 -2 6 6 6701.09 926.596 2 -2 6 5 1377.77 391.151 2 -2 6 4 8811.13 1031.35 2 -2 6 3 10567.8 1096.72 2 2 6 -3 9566.90 1043.88 2 -2 6 2 12511.4 1180.69 2 2 6 -2 10381.1 1097.88 2 2 6 -1-28.0177 166.129 2 -2 6 1 97.4127 166.905 2 -2 6 0 6336.49 822.714 2 2 6 0 5849.52 873.614 2 2 6 1 993.376 366.424 2 2 6 2 5105.37 796.712 2 2 6 3 8986.22 1081.12 2 2 6 4 9898.69 1152.38 2 2 6 5 6918.74 991.910 2 2 6 6 1092.04 413.904 2 2 6 7 5578.81 935.657 2 2 6 8 3248.27 727.460 2 -2 7 13 2980.10 763.610 2 -2 7 12 3499.48 797.225 2 -2 7 11 1426.94 532.923 2 -2 7 10 5695.95 988.669 2 -2 7 9 3277.57 743.828 2 -2 7 8 3874.65 782.833 2 -2 7 7 935.843 381.371 2 -2 7 6 472.161 283.183 2 -2 7 5-63.0758 146.225 2 -2 7 4 2928.16 624.415 2 -2 7 3 4427.57 777.841 2 -2 7 2 4084.01 741.450 2 2 7 -2 2697.38 618.249 2 -2 7 1 1693.62 488.382 2 2 7 -1 1139.68 385.934 2 -2 7 0 10117.7 1129.79 2 2 7 0 6628.91 967.056 2 2 7 1 7222.75 1032.55 2 2 7 2 7351.48 1045.18 2 2 7 3 1150.41 422.106 2 2 7 4 10434.2 1290.53 2 2 7 5 5104.84 913.156 2 2 7 6 397.607 403.472 2 2 7 7 2216.42 639.987 2 2 7 8 3381.73 767.451 2 2 7 9 146.847 314.147 2 2 7 10 588.271 363.494 2 2 7 11 987.687 442.486 2 -2 8 11 1625.35 553.355 2 -2 8 10 2343.26 672.058 2 -2 8 9 310.881 279.560 2 -2 8 8 2164.36 634.571 2 -2 8 7 1425.30 527.452 2 -2 8 6 2805.87 700.587 2 -2 8 5 1698.06 530.700 2 -2 8 4 7168.40 1069.44 2 -2 8 3 1626.31 497.646 2 2 8 -2 1694.62 513.488 2 -2 8 2 3598.83 734.566 2 2 8 -1 1748.32 533.297 2 -2 8 1 1636.48 499.659 2 2 8 0-5.50841 155.769 2 2 8 1 906.651 418.096 2 2 8 2 9596.39 1290.11 2 2 8 3-10.4179 237.315 2 2 8 4 3401.61 781.310 2 2 8 5 4790.31 945.030 2 2 8 6 22.8735 187.781 2 2 8 7 1311.31 515.202 2 2 8 8 53.0743 231.024 2 -2 9 7 1269.26 527.201 2 -2 9 6 936.500 425.760 2 -2 9 5-95.4330 186.223 2 -2 9 4 2949.87 761.632 2 -2 9 3 1348.03 532.699 2 -2 9 2 2547.80 647.877 2 2 9 -1 540.327 314.954 2 -2 9 1 416.130 306.418 2 2 9 0 3334.85 780.811 2 2 9 1 958.588 442.889 2 2 9 2 2050.89 632.799 2 2 9 3 1066.74 468.699 2 2 9 4 1101.84 510.156 2 3 -8 -13 260.645 282.562 4 3 -8 -12 177.046 145.936 4 3 -8 -11 189.359 158.506 4 3 -8 -10 3558.12 654.960 4 3 -8 -9 345.372 250.691 4 3 -8 -8 393.859 224.390 4 3 -8 -7 1219.06 364.701 4 3 -8 -6 2659.05 501.248 4 3 -8 -5 1183.11 326.993 4 3 -8 -4 70.7100 79.3700 4 3 -8 -3 828.889 276.805 4 3 -8 -2 1228.60 321.164 4 3 -8 1 7.34450 75.9746 3 3 -7 -14 844.273 366.786 4 3 -7 -13 538.364 297.385 4 3 -7 -12 3645.72 702.943 4 3 -7 -11 1193.04 415.954 4 3 -7 -10 163.452 195.757 4 3 -7 -9 2870.68 557.863 4 3 -7 -8 1878.06 442.344 4 3 -7 -7 4258.70 637.580 4 3 -7 -6 1956.00 427.096 4 3 -7 -6 2573.45 423.336 3 3 -7 -5 1456.11 343.119 4 3 -7 -5 1377.85 321.276 3 3 -7 -4 778.070 266.742 4 3 -7 -4 517.218 175.223 3 3 -7 -3 9495.07 805.495 3 3 -7 -3 9335.68 859.024 4 3 -7 -2 22802.9 1287.54 3 3 -7 -1 3648.27 514.079 3 3 -7 0 7710.08 772.916 3 3 -6 -15 2778.49 684.058 4 3 -6 -14 2975.39 665.502 4 3 -6 -13 2007.36 526.770 4 3 -6 -12 1634.80 468.023 4 3 -6 -11 163.613 184.670 4 3 -6 -10 4331.70 691.015 4 3 -6 -9 7297.72 845.287 4 3 -6 -8 318.874 192.533 4 3 -6 -7 3742.73 576.335 4 3 -6 -6 7377.30 695.401 3 3 -6 -6 7222.24 766.187 4 3 -6 -5 2270.65 413.388 4 3 -6 -5 1676.49 318.639 3 3 -6 -4 4925.65 554.574 3 3 -6 -4 6641.17 696.317 4 3 -6 -3 4042.10 505.424 3 3 -6 -2 12015.3 881.423 3 -3 -6 1 10223.6 478.818 4 3 -6 -1 10236.5 826.298 3 -3 -6 0 1846.22 225.419 4 -3 -6 -1 9799.53 596.301 4 -3 -6 -2 39595.1 1433.52 4 -3 -6 -3 2003.45 332.325 4 -3 -6 -4 2305.51 374.146 4 -3 -6 -5 5848.34 651.164 4 -3 -6 -6 4802.79 613.160 4 -3 -6 -7 368.028 199.840 4 -3 -6 -8 5583.85 752.678 4 -3 -6 -9 845.792 347.233 4 -3 -6 -10 1359.33 417.901 4 -3 -6 -11 1212.75 402.823 4 3 -6 11 1342.17 431.734 1 -3 -6 -12 1584.09 487.372 4 3 -6 12 1615.85 474.084 1 3 -5 -16 512.451 235.734 4 3 -5 -15 4691.47 854.503 4 3 -5 -14 1251.95 448.101 4 3 -5 -13 4827.36 795.599 4 3 -5 -12 5483.86 787.547 4 3 -5 -11 15576.0 1294.65 4 3 -5 -10 271.868 180.806 4 3 -5 -9 1033.03 348.652 4 3 -5 -8 1222.23 312.764 4 3 -5 -7 1359.81 330.329 4 3 -5 -6-77.7010 131.981 4 -3 -5 6 118.886 66.1867 4 -3 -5 5 15026.4 584.153 4 3 -5 -5 15471.6 1023.05 4 3 -5 -5 16566.4 965.715 3 -3 -5 4 3847.73 244.362 4 3 -5 -4 3758.04 450.954 3 3 -5 -4 3823.37 489.860 4 3 -5 -3 3552.59 440.372 3 -3 -5 3 3460.54 212.848 4 3 -5 -2 21973.7 1144.65 3 -3 -5 2 22386.9 626.673 4 -3 -5 1 72.8048 36.7750 3 3 -5 -1 100.808 117.899 3 -3 -5 1 122.519 49.5002 4 -3 -5 0 234.611 76.0475 4 -3 -5 -1 128.992 58.7500 4 -3 -5 -2 3370.29 374.174 4 -3 -5 -3 21850.2 1070.60 4 -3 -5 -4 12206.9 851.011 4 -3 -5 -5 10795.4 846.036 4 -3 -5 -6 4705.55 598.134 4 -3 -5 -7 602.728 252.285 4 -3 -5 -8 6953.18 828.765 4 -3 -5 -9 3223.30 581.078 4 -3 -5 -10 4704.12 750.660 4 3 -5 11 232.765 187.125 1 -3 -5 -11 487.458 255.221 4 3 -5 12 523.018 280.882 1 3 -5 13 1441.75 423.742 1 3 -4 -17-77.9692 183.245 4 3 -4 -16 148.971 208.886 4 3 -4 -15 5708.45 928.581 4 3 -4 -14 492.344 278.685 4 3 -4 -13 5551.68 809.054 4 3 -4 -12 2263.11 503.905 4 3 -4 -11 8073.64 883.644 4 3 -4 -10 5103.36 672.834 4 3 -4 -9 2548.20 450.221 4 3 -4 -8 2603.69 445.629 4 -3 -4 7 17680.3 803.212 4 3 -4 -7 18474.4 1150.74 4 3 -4 -6 887.791 247.742 4 -3 -4 6 817.932 152.976 4 3 -4 -6 606.358 177.952 3 3 -4 -5 13571.6 839.766 3 -3 -4 5 15063.5 584.847 4 3 -4 -5 15395.5 967.566 4 -3 -4 4 36739.8 886.937 4 3 -4 -4 37837.2 1542.13 4 3 -4 -4 37825.3 848.974 1 3 -4 -4 35408.4 1410.12 3 3 -4 -3 2699.02 356.689 3 3 -4 -2 17681.3 957.407 3 -3 -4 1 21616.2 600.928 4 -3 -4 0 17605.2 639.877 4 -3 -4 -1 2267.27 249.482 4 -3 -4 -2 14634.0 750.472 4 -3 -4 -3 7551.00 593.433 4 -3 -4 -4 5314.88 540.354 4 -3 -4 -5 2014.68 367.576 4 -3 -4 -6 10602.0 875.565 4 -3 -4 -7 6718.93 737.724 4 -3 -4 -8 10859.4 996.265 4 -3 -4 -9 3132.88 576.168 4 -3 -4 -10 267.837 245.765 4 3 -4 10 388.289 196.287 1 3 -4 11 836.661 333.201 1 -3 -4 -11 756.995 314.640 4 3 -4 12 3945.76 690.205 1 3 -4 13 1141.22 397.306 1 3 -4 14 1928.44 516.000 1 3 -3 -18 501.333 316.433 4 3 -3 -17 646.157 363.857 4 3 -3 -16 816.444 402.257 4 3 -3 -15 301.520 176.879 4 3 -3 -14 2219.08 530.805 4 3 -3 -13 2679.02 574.309 4 3 -3 -12 467.894 226.558 4 3 -3 -11 20648.3 1387.69 4 3 -3 -10 5468.47 667.418 4 3 -3 -9 1775.36 371.922 4 3 -3 -8 14227.4 983.118 4 -3 -3 7 5023.68 414.070 4 3 -3 -7 6144.43 613.619 4 -3 -3 6 32477.0 1029.33 4 3 -3 -6 30596.3 1370.44 4 3 -3 -5 9459.10 706.312 4 3 -3 -5 9465.38 659.527 3 -3 -3 5 10407.4 462.751 4 3 -3 -4 35876.3 1324.56 3 -3 -3 4 34658.2 824.609 4 3 -3 -3 619.817 171.964 3 3 -3 -3 521.639 78.0323 1 3 -3 -2 52447.2 1245.28 1 3 -3 -2 56054.0 1808.06 2 3 -3 -2 50950.9 1656.62 3 3 -3 -1 6542.14 574.915 2 -3 -3 0 40342.4 1004.09 4 3 -3 0 40875.1 1541.93 2 -3 -3 -1 12334.9 572.681 4 -3 -3 -2 48810.1 1510.28 1 -3 -3 -2 46498.9 1412.54 4 -3 -3 -3 16915.8 873.491 4 -3 -3 -3 17452.7 839.789 1 -3 -3 -4 36651.6 1446.90 4 -3 -3 -5 4965.68 543.013 4 -3 -3 -6 1484.04 343.083 4 -3 -3 -7 3593.87 534.853 4 -3 -3 -8 2016.84 422.358 4 3 -3 8 2633.11 477.217 1 3 -3 9 2281.27 452.407 1 -3 -3 -9 2726.58 530.334 4 3 -3 10 8299.45 904.773 1 3 -3 11 271.043 205.562 1 3 -3 12 6853.93 881.811 1 3 -3 13 1631.52 465.202 1 3 -3 14 491.314 298.097 1 3 -3 15 1267.90 405.191 1 -3 -2 20 335.029 224.295 1 -3 -2 19 2212.05 528.411 1 3 -2 -18 5726.07 989.867 4 3 -2 -17 1903.92 584.611 4 3 -2 -16 4535.67 825.408 4 3 -2 -15 15761.2 1467.45 4 3 -2 -14 12734.1 1237.55 4 3 -2 -13 2066.29 462.484 4 3 -2 -12 5820.53 756.102 4 3 -2 -11 2980.21 515.252 4 3 -2 -10 8169.57 785.729 4 3 -2 -9 1322.28 313.841 4 3 -2 -8 7957.53 692.223 4 3 -2 -7 41510.0 1616.11 4 -3 -2 7 45164.5 1407.31 4 3 -2 -6 7687.64 624.049 4 -3 -2 6 7596.34 470.380 4 3 -2 -5 12527.0 721.508 3 -3 -2 5 12696.4 547.398 4 3 -2 -5 11677.3 731.081 4 -3 -2 4 2748.21 198.810 4 3 -2 -4 2985.07 331.861 3 -3 -2 4 3189.20 368.518 2 3 -2 -4 2723.38 333.739 4 3 -2 -3 11024.4 331.502 1 3 -2 -3 10908.7 629.581 3 -3 -2 3 11054.0 695.942 2 3 -2 -2 5350.14 265.988 1 -3 -2 2 5447.68 475.164 2 3 -2 -2 5624.84 415.198 2 3 -2 -2 5441.17 442.419 3 3 -2 -1 32202.3 1105.55 2 -3 -2 1 31533.8 1211.18 2 3 -2 -1 31017.8 878.444 1 3 -2 0 94253.6 2234.32 2 3 -2 0 93853.2 2056.54 1 3 -2 1 61062.6 1626.36 1 -3 -2 -1 60436.4 1625.85 1 3 -2 2 13245.1 713.795 1 -3 -2 -2 14370.5 692.817 1 3 -2 3 13724.3 785.998 1 -3 -2 -3 14075.6 782.334 4 -3 -2 -3 14356.5 707.709 1 3 -2 4 5866.55 547.085 1 -3 -2 -4 7273.78 518.833 1 -3 -2 -4 7054.52 600.956 4 -3 -2 -5 2793.74 408.455 4 3 -2 5 4299.06 495.173 1 -3 -2 -6 19958.4 1170.63 4 3 -2 6 18392.2 1109.24 1 3 -2 7 5832.21 645.493 1 3 -2 8 9472.59 862.769 1 3 -2 9 1489.68 362.601 1 3 -2 10 8512.74 876.443 1 3 -2 11 3698.52 593.937 1 3 -2 12 9459.68 1003.76 1 3 -2 13 697.111 299.447 1 3 -2 14 3378.57 646.770 1 3 -2 15 1027.55 360.854 1 3 -2 16 239.514 203.176 1 -3 -1 20 1411.20 417.138 1 -3 -1 19 867.790 343.335 1 3 -1 -19 952.696 471.442 4 -3 -1 18 643.680 341.870 1 3 -1 -18 1301.49 500.333 4 3 -1 -17 718.242 371.882 4 3 -1 -16 4800.01 813.422 4 3 -1 -15 828.955 374.842 4 3 -1 -14 765.302 287.266 4 3 -1 -13 1795.03 439.768 4 3 -1 -12 9887.81 962.991 4 3 -1 -11 17607.1 1221.86 4 3 -1 -10 2700.92 444.931 4 3 -1 -9 202.334 120.781 4 3 -1 -8 9912.84 741.395 4 3 -1 -7 20603.9 1025.89 4 -3 -1 7 20946.2 940.365 4 3 -1 -6 64295.2 1900.45 4 -3 -1 6 66306.7 1729.67 4 3 -1 -5 14495.4 764.170 4 -3 -1 5 15810.1 664.487 4 3 -1 -4 14027.7 695.917 3 3 -1 -4 14903.2 726.454 4 -3 -1 4 14210.7 560.731 4 -3 -1 3 27832.7 914.948 2 -3 -1 3 29827.2 868.638 3 3 -1 -3 27595.8 961.840 3 3 -1 -2 139456. 2501.68 1 -3 -1 2 143115. 2789.65 2 3 -1 -2 138281. 2848.06 3 -3 -1 2 140570. 2569.89 3 3 -1 -1 52307.0 1191.66 1 3 -1 -1 51856.7 1150.74 2 -3 -1 0 30826.3 961.141 1 3 -1 0 29276.4 884.662 1 -3 -1 -1 65743.3 1608.43 1 3 -1 1 65012.5 1603.90 1 3 -1 2 34127.0 1144.33 1 -3 -1 -2 34574.3 1093.89 1 3 -1 3 12287.0 694.052 1 -3 -1 -3 12122.8 632.356 1 -3 -1 -4 14410.5 737.697 1 3 -1 4 15394.7 839.836 1 3 -1 5 801.955 208.056 1 3 -1 6 35332.9 1474.10 1 3 -1 7 1286.41 295.082 1 3 -1 8 3492.99 490.966 1 3 -1 9 5573.22 651.551 1 3 -1 10 3662.77 554.439 1 3 -1 11 980.288 320.397 1 3 -1 12 2013.89 444.858 1 3 -1 13 1579.62 422.239 1 3 -1 14 2942.97 572.184 1 3 -1 15 2285.52 526.781 1 3 -1 16 2344.93 563.380 1 3 -1 17 519.404 264.558 1 -3 0 19 3319.17 587.009 1 -3 0 18 1044.89 327.137 1 3 0 -17 97.9770 188.671 4 -3 0 17 32.6348 96.0227 1 3 0 -16 18646.6 1599.07 4 -3 0 16 15065.6 1151.60 1 3 0 -15 12522.5 1240.27 4 3 0 -14 44060.9 2295.92 4 3 0 -13 18639.7 1378.91 4 3 0 -12 1422.44 374.557 4 3 0 -11 9440.03 878.732 4 3 0 -10 11229.4 903.331 4 3 0 -9 3681.09 478.324 4 3 0 -8 27449.7 1245.03 4 3 0 -7 11387.8 708.660 4 -3 0 6 61131.3 1763.23 4 3 0 -6 61512.7 1725.42 4 3 0 -5 568.646 133.317 4 -3 0 5 661.318 139.789 4 -3 0 4 37094.5 1137.72 3 3 0 -4 36986.4 1093.01 4 3 0 -3 93558.0 2044.87 3 -3 0 3 97754.3 2062.78 3 -3 0 2 11779.7 504.872 3 3 0 -2 9535.54 463.731 3 -3 0 1 18799.4 640.637 1 3 0 -1 17736.7 655.412 3 3 0 -1 19042.1 650.945 1 3 0 0 44294.7 1159.09 1 -3 0 0 44536.4 1144.95 1 3 0 1 72021.3 1687.75 1 -3 0 -1 70970.7 1674.66 1 -3 0 -2 108314. 2356.18 1 3 0 2 106467. 2368.90 1 3 0 3 550.321 155.571 1 -3 0 -3 487.991 137.393 1 3 0 4-76.5659 114.782 1 3 0 5 18001.5 918.924 1 3 0 6 34913.9 1406.94 1 3 0 7 3412.91 447.219 1 3 0 8 22934.1 1243.86 1 3 0 9 288.484 183.245 1 3 0 10 3133.20 484.772 1 3 0 11 1083.59 310.925 1 3 0 12 20871.9 1396.18 1 3 0 13 186.935 177.159 1 3 0 14 47.9140 121.700 1 3 0 15 2677.88 553.181 1 3 0 16 3549.71 661.887 1 3 0 17 916.959 322.514 1 3 0 18 638.571 302.518 1 -3 1 17 463.392 216.207 1 -3 1 16 4450.75 574.714 1 -3 1 15 574.994 209.437 1 3 1 -15 478.681 270.367 4 -3 1 14 1427.73 314.687 1 3 1 -14 1204.63 376.328 4 -3 1 13 1651.93 310.146 1 3 1 -13 2204.58 466.921 4 3 1 -12 10106.9 943.864 4 3 1 -11 18815.7 1225.44 4 3 1 -10 2528.32 415.167 4 3 1 -9 57.2327 108.144 4 3 1 -8 9016.22 686.870 4 3 1 -7 21061.8 976.586 4 -3 1 6 67471.7 1905.88 3 3 1 -6 62029.7 1707.92 4 3 1 -5 13711.3 610.294 4 -3 1 5 14235.0 732.210 3 3 1 -4 14042.7 542.427 4 -3 1 4 14613.7 704.476 3 -3 1 3 27732.5 676.265 1 3 1 -3 27033.4 713.832 4 -3 1 3 27652.5 973.079 3 -3 1 2 138660. 2517.30 2 3 1 -2 142357. 2753.85 2 -3 1 2 139289. 2488.19 1 -3 1 2 140395. 2880.26 3 3 1 -1 50995.5 1092.10 3 3 1 -1 51507.9 1346.14 2 -3 1 1 52438.4 1188.63 1 -3 1 0 29019.9 874.926 1 3 1 1 64925.2 1633.54 1 -3 1 -1 66145.3 1640.08 1 3 1 2 35870.4 1177.27 4 3 1 2 34244.3 1120.94 1 3 1 3 12045.2 706.680 4 3 1 3 11345.1 628.669 1 3 1 4 15458.5 782.209 1 3 1 5 634.199 173.214 1 3 1 6 31093.8 1296.85 1 3 1 7 1036.31 248.841 1 3 1 8 3961.70 492.847 1 3 1 9 7170.17 699.579 1 3 1 10 3628.44 520.048 1 3 1 11 1910.36 402.390 1 3 1 12 1677.31 377.446 1 3 1 13 1521.85 400.046 1 3 1 14 2149.69 480.983 1 3 1 15 1435.38 403.754 1 3 1 16 1426.21 423.160 1 3 1 17 624.521 286.105 1 -3 2 15 16236.7 985.619 1 -3 2 14 12028.9 802.058 1 -3 2 13 2357.32 326.961 1 -3 2 12 6216.46 508.196 1 -3 2 11 3296.05 343.218 1 -3 2 10 8192.11 500.390 1 3 2 -10 9489.55 788.738 4 3 2 -9 984.146 249.275 4 -3 2 9 1004.57 157.533 1 -3 2 8 8085.98 397.723 1 3 2 -8 7653.09 614.527 4 3 2 -7 41460.9 1416.13 4 -3 2 7 43532.8 984.288 1 -3 2 6 7165.35 251.367 1 3 2 -6 8192.70 511.573 4 3 2 -5 12700.7 567.606 4 -3 2 5 12342.9 717.318 3 -3 2 4 3275.10 351.414 3 3 2 -4 3264.36 224.631 4 3 2 -3 10611.4 665.541 2 -3 2 3 11955.0 660.160 3 -3 2 3 10350.7 599.293 2 -3 2 2 5506.89 421.096 2 3 2 -2 5471.10 479.912 2 -3 2 1 32435.5 1078.96 2 3 2 -1 31251.2 1233.86 2 3 2 0 91880.7 2405.88 2 3 2 0 91633.7 1762.50 4 3 2 1 61128.9 1458.32 4 3 2 2 14182.7 666.872 4 3 2 3 14233.3 732.650 4 3 2 3 13577.0 715.579 1 3 2 4 7423.25 543.473 1 3 2 5 3734.73 396.452 1 3 2 6 22037.1 1057.64 1 3 2 7 4710.86 496.031 1 3 2 8 10620.3 785.009 1 3 2 9 1669.23 324.019 1 3 2 10 9343.99 808.134 1 3 2 11 4529.80 582.432 1 3 2 12 10242.4 918.342 1 3 2 13 343.283 193.265 1 3 2 14 3647.75 593.992 1 3 2 15 1156.88 350.019 1 3 2 16 645.094 272.027 1 -3 3 12 447.421 117.321 1 -3 3 11 17724.6 693.476 1 -3 3 10 4765.09 300.165 1 -3 3 9 1476.82 133.844 1 -3 3 4 36519.9 1480.75 2 -3 3 4 35865.9 1368.20 3 -3 3 3 585.667 194.454 2 3 3 -3 573.509 193.302 2 3 3 -2 50070.6 1875.97 2 -3 3 2 47954.3 1699.60 2 -3 3 1 7014.83 587.449 2 3 3 -1 6919.40 663.132 2 3 3 0 39151.3 960.354 4 3 3 0 38859.8 1648.92 2 3 3 1 13291.5 931.044 2 3 3 1 11679.1 526.223 4 3 3 2 49030.8 1364.81 4 3 3 2 47206.6 983.818 3 3 3 3 18959.0 851.273 4 3 3 6 2092.69 318.937 1 3 3 7 3614.94 431.899 1 3 3 8 1877.68 321.736 1 3 3 9 2898.68 423.863 1 3 3 10 8426.89 755.851 1 3 3 11 334.171 154.221 1 3 3 12 6227.79 700.336 1 3 3 13 1374.12 341.419 1 -3 4 6 1114.23 316.023 2 -3 4 5 13535.2 1015.35 2 -3 4 4 36962.2 1722.10 2 -3 4 3 3566.78 497.084 2 3 4 -3 2828.03 472.262 2 -3 4 2 18372.6 1150.17 2 3 4 -2 18233.4 1220.96 2 3 4 -1 21731.7 1358.34 2 -3 4 1 23345.0 1283.80 2 -3 4 0 16267.9 1053.26 2 3 4 0 16157.5 1166.06 2 3 4 1 1359.56 348.319 2 3 4 2 16371.2 756.772 4 3 4 2 14307.8 1126.93 2 3 4 3 6758.14 511.196 4 3 4 3 7148.00 805.242 2 3 4 3 6895.78 327.806 3 3 4 4 6404.94 381.034 3 3 4 5 1997.69 241.189 3 3 4 6 9691.65 598.466 3 3 4 10 608.687 225.654 1 3 4 11 970.661 259.578 1 -3 5 8 943.006 360.207 2 -3 5 7 1570.47 444.088 2 -3 5 6-86.8533 175.835 2 -3 5 5 15068.7 1219.80 2 -3 5 4 4841.33 670.810 2 3 5 -3 3934.21 614.153 2 -3 5 3 3646.95 575.507 2 3 5 -2 21371.3 1488.54 2 -3 5 2 23026.5 1449.53 2 -3 5 1 153.167 210.131 2 3 5 -1-25.5405 136.678 2 3 5 0 103.530 173.032 2 -3 5 0 127.692 153.647 2 3 5 1 27.2892 133.691 2 3 5 2 3471.98 635.113 2 3 5 3 21728.1 1585.94 2 3 5 4 14355.3 1300.15 2 3 5 5 12450.7 1224.87 2 -3 6 11-361.828 250.512 2 -3 6 10 2970.01 672.692 2 -3 6 9 6829.24 969.927 2 -3 6 8-6.46250 177.808 2 -3 6 7 4802.79 776.045 2 -3 6 6 7849.78 969.974 2 -3 6 5 2281.31 532.764 2 -3 6 4 4639.42 722.692 2 -3 6 3 4284.55 701.050 2 3 6 -3 4462.29 730.965 2 -3 6 2 12123.8 1154.79 2 3 6 -2 10283.1 1107.66 2 -3 6 1 11009.0 1069.63 2 3 6 -1 10989.2 1150.32 2 3 6 0 1110.21 361.457 2 3 6 1 10739.2 1177.92 2 3 6 2 38156.4 2281.57 2 3 6 3 2229.14 570.059 2 3 6 4 2117.53 540.286 2 3 6 5 5172.95 861.845 2 3 6 6 5412.59 906.108 2 3 6 7 138.192 179.811 2 -3 7 14 419.705 304.224 2 -3 7 13 77.9524 217.624 2 -3 7 12 3353.58 780.748 2 -3 7 11 1062.88 445.351 2 -3 7 10 319.455 278.621 2 -3 7 9 3113.44 703.415 2 -3 7 8 1727.72 512.402 2 -3 7 7 3841.58 753.944 2 -3 7 6 2991.18 646.928 2 -3 7 5 1961.37 528.565 2 -3 7 4 250.647 129.562 2 -3 7 3 8944.68 1092.56 2 3 7 -3 10412.9 1206.67 2 -3 7 2 22040.1 1698.19 2 3 7 -2 24930.0 1896.44 2 3 7 -1 2500.03 576.939 2 -3 7 1 3996.58 705.339 2 3 7 0 7476.86 1047.27 2 3 7 1 4137.41 786.672 2 3 7 2 561.706 352.545 2 3 7 3 1962.76 551.689 2 3 7 4 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7 3337.83 863.768 2 -4 9 9 3156.71 803.529 2 -4 9 8 5456.23 1038.14 2 -4 9 7 350.637 218.843 2 -4 9 6 1612.02 536.438 2 -4 9 5 119.423 171.883 2 -4 9 4 1959.06 589.716 2 -4 9 3 1801.36 555.786 2 4 9 -2 768.233 333.662 2 4 9 -1 515.698 365.441 2 4 9 0 524.047 380.937 2 4 9 1 4621.22 957.068 2 4 9 2 1212.60 556.755 2 5 -8 -12 1075.05 383.362 4 5 -8 -11 351.143 234.507 4 5 -8 -10 1629.04 471.079 4 5 -8 -9 1818.10 473.966 4 5 -8 -8 264.255 147.246 4 5 -8 -7 5410.15 764.873 4 5 -8 -6 3508.47 621.471 4 5 -8 -5 795.311 294.318 4 5 -8 -4 3.39156 128.703 4 5 -8 -4 351.793 227.344 3 5 -8 -3 2616.64 485.874 3 5 -8 -2 2244.50 466.860 3 5 -8 -1 2009.58 453.238 3 5 -8 0 3606.32 608.703 3 5 -8 1 858.739 344.132 3 5 -8 3 3915.22 604.378 1 5 -8 4 3123.23 559.582 1 5 -8 5 430.105 228.652 1 5 -8 6 2237.45 507.382 1 5 -8 7 132.148 150.400 1 5 -8 8 2922.42 633.481 1 5 -7 -14 1176.95 400.816 4 5 -7 -13 697.874 365.836 4 5 -7 -12 4963.55 812.177 4 5 -7 -11 5870.18 862.219 4 5 -7 -10 1153.27 355.042 4 5 -7 -9 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717.178 1 5 0 5 729.369 210.215 1 5 0 6 1745.00 351.243 1 5 0 7-101.084 124.752 1 5 0 8 10070.3 889.231 1 5 0 9 480.452 173.532 1 5 0 10 57.8640 132.963 1 5 0 11 60.3853 129.821 1 5 0 12 9286.18 1008.53 1 5 0 13 1982.32 479.034 1 5 0 14-54.1827 144.872 1 5 0 15 1925.84 506.188 1 5 0 16 3460.93 695.589 1 5 1 -18 401.771 240.857 4 -5 1 17 203.950 147.660 1 5 1 -17-35.4259 110.896 4 5 1 -16 3235.36 637.579 4 5 1 -15 345.966 238.259 4 5 1 -14 16878.9 1307.35 4 5 1 -13 2006.44 438.480 4 5 1 -12 36401.3 1765.35 4 5 1 -11 2038.44 376.964 4 5 1 -10 10251.6 790.231 4 5 1 -9 2584.35 364.233 4 5 1 -8 22003.5 1013.80 4 5 1 -7 1229.00 220.232 4 5 1 -6 83725.3 2029.71 4 5 1 -5 17053.0 715.000 4 -5 1 4 16353.8 645.407 1 -5 1 4 16948.6 871.940 3 -5 1 3 2310.66 233.381 1 5 1 -3 2072.57 229.732 2 5 1 -3 2172.28 239.602 3 -5 1 2 35474.9 1079.09 1 5 1 -2 33338.8 1033.70 3 5 1 -2 35114.3 1096.56 2 -5 1 1 28591.7 1002.01 1 5 1 -1 27391.4 923.227 3 -5 1 0 13218.6 680.394 1 5 1 0 11760.6 701.309 1 5 1 1 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348.405 3 7 -3 -3 4804.95 415.395 1 7 -3 -3 4830.70 451.257 2 7 -3 -3 4226.54 547.418 3 7 -3 -2 1001.14 201.842 1 7 -3 -2 1001.18 217.929 2 7 -3 -1 1434.23 268.786 2 7 -3 -1 1182.94 248.510 1 7 -3 0 5253.62 524.653 1 7 -3 1 17732.5 1043.69 1 7 -3 2 717.530 220.171 1 7 -3 3 1901.71 370.589 1 7 -3 4 7671.89 768.301 1 7 -3 5 2022.73 412.322 1 7 -3 6 30701.0 1718.27 1 7 -3 7 754.398 292.025 1 7 -3 8 2359.11 496.304 1 7 -3 9 1866.88 455.701 1 7 -3 10 81.2214 164.733 1 7 -3 11 1537.24 481.840 1 7 -3 12 5319.16 867.506 1 7 -2 -19 3370.43 764.483 4 7 -2 -18 2336.96 589.201 4 7 -2 -17 514.961 305.338 4 7 -2 -16 1456.08 445.505 4 7 -2 -15 166.322 258.363 4 7 -2 -14 88.1665 131.527 4 7 -2 -13 2603.95 512.197 4 7 -2 -12 5566.64 697.022 4 7 -2 -11 22905.3 1403.76 4 7 -2 -10 20211.9 1280.08 4 7 -2 -9 3010.77 470.780 4 7 -2 -8 2437.08 420.809 4 7 -2 -8 2326.04 411.700 3 7 -2 -7 16617.5 1085.90 3 7 -2 -6 10849.3 829.694 3 -7 -2 6 12813.4 829.513 2 7 -2 -5 543.370 212.095 3 -7 -2 5 543.937 153.869 3 -7 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730.875 217.130 4 7 0 -8 14113.1 870.418 4 7 0 -7 267.004 120.347 4 7 0 -6 201.470 136.699 3 -7 0 5 1902.28 150.902 2 7 0 -5 2510.94 347.222 3 7 0 -4 2214.28 316.784 3 7 0 -3 5428.77 505.814 3 7 0 -2 17814.1 944.679 3 7 0 -1 9364.22 683.504 1 7 0 0 3269.53 419.716 1 7 0 1 24088.3 1190.66 1 7 0 2 23420.0 1218.59 1 7 0 3 6092.52 631.874 1 7 0 4 2329.68 410.313 1 7 0 5 217.180 162.420 1 7 0 6 52.6203 98.1234 1 7 0 7 77.8514 134.469 1 7 0 8 29223.6 1707.80 1 7 0 9 5202.93 733.625 1 7 0 10 666.378 297.449 1 7 0 11 462.197 254.537 1 7 0 12-40.9683 116.919 1 7 0 13 333.718 221.073 1 7 0 14-372.356 246.441 1 7 1 -20 691.410 319.483 4 7 1 -19 1267.77 480.381 4 7 1 -18 1990.24 523.484 4 7 1 -17 2315.19 539.694 4 7 1 -16 1463.82 418.215 4 7 1 -15 11865.1 1116.18 4 7 1 -14 4195.46 641.677 4 7 1 -13 2853.21 487.147 4 7 1 -12 6047.45 667.929 4 7 1 -11 2467.01 400.133 4 7 1 -10 11518.8 813.342 4 7 1 -9 3679.86 427.385 4 7 1 -8 1807.63 286.212 4 7 1 -7 2699.35 331.670 4 -7 1 6 117207. 2662.49 1 7 1 -6 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17741.1 783.070 4 7 2 -6 11505.7 580.898 4 -7 2 6 10860.5 577.731 2 -7 2 6 12280.9 586.575 1 -7 2 5 684.542 130.031 2 7 2 -5 604.552 124.967 4 -7 2 5 785.084 150.111 1 7 2 -4 7374.57 588.913 2 -7 2 4 8198.55 519.913 1 7 2 -3 5803.94 540.676 2 -7 2 3 5555.62 449.456 1 7 2 -3 6401.81 438.387 3 7 2 -2 4604.55 492.704 2 7 2 -2 3946.98 335.055 3 7 2 -1 17067.8 983.958 2 7 2 -1 16584.9 732.686 3 7 2 2 5065.90 581.730 1 7 2 3 589.897 201.786 1 7 2 4 16523.4 1111.94 1 7 2 5 527.562 195.288 1 7 2 6 19858.9 1301.71 1 7 2 7 6723.98 770.983 1 7 2 8 15061.7 1202.50 1 7 2 9 5335.98 731.929 1 7 2 10 2757.74 542.887 1 7 2 11 1158.93 366.678 1 7 2 12 495.258 242.616 1 7 2 13 739.200 332.799 1 7 2 14 1195.08 398.319 1 7 2 15 448.883 275.970 1 7 3 -14 100.939 94.9719 4 7 3 -13 10837.7 903.814 4 7 3 -12 24056.1 1290.63 4 7 3 -11 4995.48 530.798 4 7 3 -10 46580.4 1560.50 4 -7 3 10 32581.8 741.246 1 7 3 -9 5009.46 445.872 4 -7 3 9 3563.72 192.197 1 7 3 -8 8174.69 516.250 4 -7 3 8 7733.83 329.302 1 -7 3 7 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652.585 2 -8 7 10 8826.87 1102.28 2 -8 7 9 1659.61 473.591 2 -8 7 8 1624.47 470.327 2 -8 7 7 110.018 147.104 2 -8 7 6 239.374 228.946 2 8 7 -5 1880.06 536.101 2 8 7 -4 10818.8 1289.19 2 8 7 -3 5766.69 947.629 2 8 7 -2 457.375 252.838 2 8 7 -1 656.688 382.413 2 8 7 0 7240.95 1104.22 2 8 7 1 2324.68 640.929 2 8 7 2 881.501 407.806 2 8 7 3 346.171 244.463 2 8 7 4 1182.48 484.625 2 8 7 5 1545.66 576.459 2 8 7 6 1574.40 577.857 2 -8 8 9 1026.29 388.079 2 -8 8 8 4114.24 775.067 2 -8 8 7 171.352 111.771 2 -8 8 6 2023.14 553.988 2 8 8 -4 2361.60 618.505 2 8 8 -3 850.959 428.387 2 8 8 -2 2442.59 653.327 2 8 8 -1 1613.54 527.407 2 8 8 0 461.098 309.293 2 8 8 1 1304.09 508.522 2 8 8 2 592.121 368.841 2 9 -9 -5 40.8631 121.792 4 9 -9 -3 330.198 261.919 3 9 -9 -2 894.446 362.947 3 9 -9 -1 352.513 289.602 3 9 -8 -10 248.799 243.491 4 9 -8 -10 288.075 164.044 3 9 -8 -9 476.331 269.780 4 9 -8 -9 96.4191 94.7445 3 9 -8 -8 708.125 286.603 4 9 -8 -8 707.087 322.693 3 9 -8 -7 1977.03 499.879 4 9 -8 -7 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539.971 1 9 -4 2 7144.96 775.890 1 9 -4 3 811.451 286.745 1 9 -4 4 8305.46 903.428 1 9 -4 5 34.9395 102.224 1 9 -4 6 1209.90 385.874 1 9 -4 7 1746.02 476.378 1 9 -4 8 472.658 241.785 1 9 -4 9 2010.09 515.372 1 9 -3 -18 5898.32 944.835 4 9 -3 -17 110.285 150.160 4 9 -3 -16 5656.91 872.295 4 9 -3 -15 12078.7 1235.04 4 9 -3 -14 1876.35 470.425 4 9 -3 -13 10105.3 1055.83 4 9 -3 -12 2078.02 484.769 4 9 -3 -11 4773.66 690.410 4 9 -3 -10 7413.67 860.029 4 9 -3 -10 7683.04 844.392 3 9 -3 -9 507.183 238.298 4 9 -3 -9 1248.17 376.458 3 9 -3 -8 4098.71 605.424 3 9 -3 -7 10062.6 940.963 3 9 -3 -6 18134.6 1266.87 3 9 -3 -5 9590.18 907.731 3 9 -3 -4 6778.16 568.864 1 9 -3 -4 7016.40 789.883 3 9 -3 -3 1620.69 389.277 3 9 -3 -3 1566.87 287.882 1 9 -3 -3 1854.33 270.892 2 9 -3 -2 5076.96 533.375 1 9 -3 -2 3754.72 413.461 2 9 -3 -2 4184.44 621.037 3 9 -3 -1 8490.34 720.038 1 9 -3 -1 8470.11 660.378 2 9 -3 0 664.068 217.286 1 9 -3 1 1110.79 280.326 1 9 -3 2 7787.17 792.834 1 9 -3 3 2096.04 426.339 1 9 -3 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367.604 1 9 3 -17-7.24926 62.5253 4 9 3 -16 4983.21 700.775 4 9 3 -15 12518.4 1059.86 4 9 3 -14 1256.51 337.219 4 9 3 -13 9763.43 828.051 4 9 3 -12 2181.74 362.733 4 9 3 -11 4687.07 502.650 4 9 3 -10 7648.47 587.465 4 -9 3 9 922.264 153.299 1 9 3 -9 882.293 187.070 4 -9 3 9 696.607 193.124 2 9 3 -8 3240.91 317.115 4 -9 3 8 3227.57 372.480 2 -9 3 8 3737.77 328.336 1 -9 3 7 10938.3 647.497 2 9 3 -7 12421.5 589.026 4 -9 3 7 10822.9 612.462 1 9 3 -6 18381.4 711.060 4 -9 3 6 17641.5 844.935 1 9 3 -5 7583.28 723.155 2 9 3 -4 9337.87 816.409 2 9 3 -3 2153.97 405.311 2 9 3 -3 2086.08 253.217 3 9 3 -2 4162.75 568.006 2 9 3 -2 5111.56 398.045 3 9 3 -1 7770.63 585.357 4 9 3 -1 9392.12 878.528 2 9 3 -1 8585.45 529.679 3 9 3 0 630.976 157.768 3 9 3 0 641.821 235.770 2 9 3 1 1511.30 242.122 3 9 3 7 4723.00 728.858 1 9 3 8 1783.15 456.607 1 9 3 9-64.9585 82.3051 1 9 3 10 1367.19 453.166 1 9 3 11 1048.31 382.871 1 9 3 12 649.938 311.302 1 -9 4 11 10380.2 908.314 2 -9 4 10 4404.42 575.935 2 -9 4 9 1962.99 355.848 2 -9 4 8 6996.92 656.381 2 -9 4 7 7495.06 657.431 2 -9 4 6 9948.75 723.056 2 9 4 -5 1504.36 357.884 2 9 4 -4 1775.06 411.206 2 9 4 -3 2678.58 506.584 2 9 4 -2 11761.2 1082.46 2 9 4 -1 3043.51 570.040 2 9 4 0 1407.56 138.722 3 9 4 0 1345.76 382.972 2 9 4 1 3200.05 594.812 2 9 4 2 6004.36 838.889 2 -9 5 14 230.970 214.875 2 -9 5 13 2413.89 522.572 2 -9 5 12 425.226 227.315 2 -9 5 11 2961.25 555.642 2 -9 5 10 448.787 178.501 2 -9 5 9 824.026 275.964 2 -9 5 8 3116.97 505.152 2 -9 5 7 4125.38 550.334 2 -9 5 6 31114.9 1546.40 2 9 5 -5 399.492 217.365 2 9 5 -4 2799.97 570.431 2 9 5 -3 4637.58 730.299 2 9 5 -2 12765.6 1240.28 2 9 5 -1 4350.70 740.928 2 9 5 0 5147.68 806.108 2 9 5 1 1660.79 487.965 2 9 5 2 9870.30 1176.41 2 9 5 3 916.861 381.638 2 9 5 4 3954.69 789.620 2 -9 6 11 3972.68 669.062 2 -9 6 10 7753.68 926.582 2 -9 6 9 276.461 137.119 2 -9 6 8 881.438 280.763 2 -9 6 7 8304.54 884.148 2 -9 6 6 689.929 259.096 2 9 6 -5 8661.55 1084.44 2 9 6 -4 1784.20 493.880 2 9 6 -3 2384.81 548.458 2 9 6 -2 11932.9 1313.33 2 9 6 -1 815.593 400.979 2 9 6 0 2100.68 560.482 2 9 6 1 5312.08 912.794 2 9 6 2 2561.57 657.718 2 9 6 3-52.1710 242.312 2 9 6 4 2945.76 720.207 2 9 6 5 788.047 362.187 2 9 6 6 3322.34 816.640 2 9 6 7 679.013 412.851 2 -9 7 8 1802.66 491.099 2 9 7 -5 1385.80 467.393 2 9 7 -4 3246.09 716.628 2 9 7 -3 2775.88 680.174 2 9 7 -2 1939.08 571.403 2 9 7 -1 1682.88 535.496 2 9 7 0 2048.95 587.747 2 9 7 1 373.112 255.652 2 9 7 2 2032.15 622.078 2 9 7 3 517.102 329.373 2 9 7 4 1788.54 548.158 2 9 7 5 205.733 337.902 2 9 8 -4 706.467 357.903 2 9 8 -3 560.513 357.758 2 9 8 -2 3210.31 762.195 2 9 8 -1 756.924 402.492 2 9 8 0 149.122 160.541 2 9 8 1 806.034 432.183 2 10 -8 -10 1024.32 372.889 3 10 -8 -9 152.010 108.051 3 10 -8 -8 2007.68 541.963 4 10 -8 -8 2556.43 586.217 3 10 -8 -7 339.739 169.555 4 10 -8 -7 269.510 159.383 3 10 -8 -6 2908.02 632.966 3 10 -8 -5 4110.79 770.956 3 10 -8 -4 212.722 217.288 3 10 -8 -3 243.356 200.497 3 10 -8 -2 582.825 304.995 3 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892.843 1 10 -3 -18 3613.86 730.390 4 10 -3 -17 325.285 202.194 4 10 -3 -16 1543.95 453.079 4 10 -3 -15 2272.33 540.833 4 10 -3 -14 2978.18 593.914 4 10 -3 -13 4716.16 733.462 4 10 -3 -12 346.262 215.411 4 10 -3 -11 2564.64 519.126 4 10 -3 -11 2162.88 488.542 3 10 -3 -10 609.052 304.038 4 10 -3 -10 255.922 168.416 3 10 -3 -9 2524.00 503.383 3 10 -3 -8 27067.6 1628.57 3 10 -3 -7 6076.82 755.196 3 10 -3 -6 9541.49 948.788 3 10 -3 -5 4387.17 637.390 3 10 -3 -4 3304.02 431.328 1 10 -3 -4 3363.62 569.190 3 10 -3 -3 6411.53 622.401 1 10 -3 -3 5550.82 741.672 3 10 -3 -2 7653.64 709.436 1 10 -3 -2 8024.26 912.935 3 10 -3 -1 1278.04 304.607 1 10 -3 0 18401.9 1185.52 1 10 -3 1 6330.28 716.290 1 10 -3 2 10283.1 944.498 1 10 -3 3 204.232 181.157 1 10 -3 4 1362.65 368.598 1 10 -3 5 1213.76 360.761 1 10 -3 6 1219.85 424.854 1 10 -3 7 774.809 292.144 1 10 -3 8 2706.07 619.976 1 10 -3 9-1.19830 242.353 1 10 -2 -19 922.039 382.361 4 10 -2 -18 2409.17 583.900 4 10 -2 -17 7794.42 1024.86 4 10 -2 -16 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4819.45 769.381 4 10 0 -16 222.755 167.292 4 10 0 -15 1203.14 373.943 4 10 0 -14 2263.72 466.334 4 10 0 -13 474.796 233.152 4 10 0 -12 6611.60 738.788 4 10 0 -11 996.250 304.132 4 10 0 -10 244.222 158.435 4 -10 0 9 2459.85 265.431 2 10 0 -9 2592.60 436.768 4 -10 0 8 7602.14 360.848 2 10 0 -8 10152.3 856.754 3 10 0 -7 3650.14 495.868 3 10 0 -6 9719.75 815.638 3 10 0 -5 13606.7 968.328 3 10 0 -4 967.354 270.621 3 10 0 -3 5628.47 330.651 2 10 0 -3 6714.41 676.455 3 10 0 -2 7546.31 732.947 3 10 0 -1 5408.79 648.662 1 10 0 0 10481.5 902.738 1 10 0 1 8772.28 850.548 1 10 0 2 2251.31 441.496 1 10 0 3 5017.00 688.336 1 10 0 4 7253.66 846.758 1 10 0 5 1152.08 355.623 1 10 0 6 79.7461 278.572 1 10 0 7 175.810 176.088 1 10 0 8 26.1658 106.330 1 10 0 9 358.516 259.050 1 10 0 10 8641.82 1114.19 1 10 0 11 2683.01 624.905 1 10 1 -21 1005.33 409.291 4 10 1 -20 1417.01 468.796 4 10 1 -19 612.817 312.120 4 10 1 -18 7900.40 1015.33 4 10 1 -17 867.628 335.106 4 10 1 -16 560.275 217.784 4 10 1 -15 1266.46 355.794 4 10 1 -14 811.981 279.390 4 10 1 -13 9364.59 860.927 4 10 1 -12 3392.58 499.606 4 10 1 -11 436.659 179.701 4 10 1 -10 9161.10 763.441 4 10 1 -9 6210.60 615.854 4 10 1 -8 808.097 238.331 4 10 1 -7 6495.50 649.377 3 10 1 -6 2463.44 382.836 3 10 1 -5 643.329 198.713 3 10 1 -4 5017.33 393.213 2 10 1 -4 5108.90 539.031 3 10 1 -3 26860.7 1075.61 2 10 1 -3 26918.0 1296.46 3 10 1 -2 11259.2 712.436 2 10 1 -2 10946.9 808.745 3 10 1 -1 3237.16 447.271 3 10 1 1 2061.74 416.918 1 10 1 2 7714.98 836.320 1 10 1 3 921.574 320.046 1 10 1 4 5593.79 748.324 1 10 1 5 5796.30 774.927 1 10 1 6 2314.90 516.961 1 10 1 7 930.109 360.557 1 10 1 8 2742.47 593.215 1 10 1 9 325.051 222.926 1 10 1 10 4722.94 815.651 1 10 1 11-38.2585 146.450 1 10 2 -20 288.526 246.794 4 10 2 -19 375.259 235.075 4 10 2 -18 2172.99 544.105 4 10 2 -17 7819.47 948.415 4 10 2 -16 303.476 168.314 4 10 2 -15 1920.84 433.070 4 10 2 -14 4328.10 606.602 4 10 2 -13 3633.47 512.977 4 10 2 -12 8006.17 734.218 4 10 2 -11 170.332 133.711 4 10 2 -10 5.98523 81.4740 4 10 2 -9 8758.61 663.272 4 -10 2 9 6988.25 432.739 2 10 2 -8 7750.14 604.640 4 10 2 -7 5721.65 511.302 4 10 2 -5 18967.3 994.470 2 10 2 -5 19193.2 1011.27 3 10 2 -4 1981.73 326.356 2 10 2 -4 2150.98 325.921 3 10 2 -3 2148.04 352.880 2 10 2 -3 2074.39 314.815 3 10 2 -2 7985.68 707.413 2 10 2 -2 6720.01 580.164 3 10 2 -1 1134.30 248.285 3 10 2 -1 1340.34 305.318 2 10 2 0 3020.28 412.948 3 10 2 3 3010.93 543.276 1 10 2 4 2594.05 524.693 1 10 2 5 1537.97 407.898 1 10 2 6 10219.4 1090.53 1 10 2 7-121.070 122.805 1 10 2 8-66.3622 149.648 1 10 2 9 1920.86 515.043 1 10 2 10 3108.11 655.697 1 10 2 11 213.241 176.202 1 10 3 -14 2523.05 440.946 4 10 3 -13 5082.27 582.771 4 10 3 -12 99.1643 84.3512 4 10 3 -11 2115.96 328.601 4 -10 3 11 1636.63 306.933 2 10 3 -10 294.061 112.450 4 -10 3 10 575.952 186.767 2 10 3 -9 2469.68 302.132 4 -10 3 9 2194.54 297.834 2 -10 3 8 24973.8 968.130 2 10 3 -8 30082.9 1066.56 4 10 3 -7 7232.09 476.668 4 10 3 -6 8769.39 526.860 4 10 3 -5 4218.29 543.261 2 10 3 -4 2730.89 450.839 2 10 3 -3 6310.15 708.140 2 10 3 -3 6431.24 497.690 3 10 3 -2 9704.54 895.603 2 10 3 -2 9559.42 607.826 3 10 3 -1 1670.07 381.350 2 10 3 -1 1752.04 264.551 3 10 3 0 18341.7 1310.15 2 10 3 0 19214.5 928.332 3 10 3 1 5665.99 508.121 3 10 3 8 1445.15 464.042 1 10 3 9 409.097 249.844 1 10 3 10-185.944 182.154 1 10 3 11 1188.75 424.647 1 -10 4 10 448.472 182.876 2 -10 4 9 1495.45 296.668 2 -10 4 8 3224.22 412.317 2 10 4 -5 3401.18 562.304 2 10 4 -4 3108.60 571.794 2 10 4 -3 150.261 149.011 2 10 4 -2 1661.61 409.523 2 10 4 -1 2309.59 493.946 2 10 4 0 6281.75 837.566 2 10 4 1 4864.33 758.539 2 10 4 2 575.651 274.041 2 -10 5 9 2443.49 449.065 2 10 5 -5 2935.00 565.753 2 10 5 -4 9373.36 1058.83 2 10 5 -3 5757.46 825.169 2 10 5 -2 7827.38 983.457 2 10 5 -1 2662.55 591.776 2 10 5 0 5516.90 853.480 2 10 5 1 2635.28 606.396 2 10 5 2 3669.36 719.858 2 10 5 3 493.290 315.404 2 10 5 4 375.466 267.349 2 10 5 5 2013.86 583.639 2 10 6 -5 841.344 359.824 2 10 6 -4 952.306 349.534 2 10 6 -3 1317.72 437.066 2 10 6 -2 719.222 353.266 2 10 6 -1 2050.75 547.671 2 10 6 0 2200.83 576.919 2 10 6 1 4361.39 856.912 2 10 6 2 965.315 430.983 2 10 6 3 374.252 285.752 2 10 6 4 790.905 410.191 2 10 6 5 1557.69 544.272 2 10 6 6 2480.22 726.743 2 10 7 -5 2066.84 586.047 2 10 7 -4 4710.07 864.026 2 10 7 -3 2880.23 682.103 2 10 7 -2 4147.28 855.511 2 10 7 -1 544.352 304.988 2 10 7 0 804.432 367.256 2 10 7 1 918.800 524.555 2 10 7 2 870.262 411.017 2 10 7 3 795.873 360.681 2 10 7 4 2331.84 702.660 2 10 8 -4 300.191 338.783 2 10 8 -3 193.135 218.315 2 10 8 -2 413.970 261.804 2 10 8 -1 1050.75 480.205 2 10 8 0 834.257 415.906 2 11 -8 -9 941.384 426.189 3 11 -8 -8 14.7427 92.9363 3 11 -8 -7 266.178 223.078 3 11 -8 -6 1683.01 521.666 3 11 -8 -5 3954.42 759.454 3 11 -8 -4 446.667 243.102 3 11 -8 -3 1090.38 411.998 3 11 -7 -11 602.103 314.068 4 11 -7 -11 812.519 352.965 3 11 -7 -10 2189.78 569.294 4 11 -7 -10 2570.61 604.547 3 11 -7 -9 875.813 347.751 4 11 -7 -9 1540.54 486.787 3 11 -7 -8 1576.86 515.850 4 11 -7 -8 793.958 390.762 3 11 -7 -7 3388.55 687.325 3 11 -7 -6 6635.41 964.875 3 11 -7 -5 2210.98 574.424 3 11 -7 -4 822.576 371.748 3 11 -7 -3 2681.21 621.059 3 11 -7 -2 740.075 374.911 3 11 -7 -1 1414.03 491.931 3 11 -7 0 351.365 316.606 3 11 -7 3 4166.02 711.470 1 11 -7 4 1121.28 398.070 1 11 -6 -13-219.737 207.453 4 11 -6 -12 5343.39 883.432 4 11 -6 -11 248.774 179.189 4 11 -6 -11 455.868 280.726 3 11 -6 -10 551.797 297.600 4 11 -6 -10 1001.12 430.963 3 11 -6 -9 902.849 331.434 4 11 -6 -9 1155.18 451.229 3 11 -6 -8 1148.73 402.835 3 11 -6 -7 1020.12 364.846 3 11 -6 -6 5758.19 871.195 3 11 -6 -5 8827.06 1088.85 3 11 -6 -4 2021.68 527.393 3 11 -6 -3 280.885 236.731 3 11 -6 -2 8020.27 1069.68 3 11 -6 -1 461.115 281.771 3 11 -6 -1 607.572 252.035 1 11 -6 0 1563.59 394.732 1 11 -6 1 1596.75 391.467 1 11 -6 2 7.29511 105.895 1 11 -6 3 113.544 199.273 1 11 -6 4 330.412 217.073 1 11 -6 5 1040.07 396.067 1 11 -5 -15 473.656 304.165 4 11 -5 -14 6.05496 176.638 4 11 -5 -13 2257.01 543.456 4 11 -5 -12 3031.18 636.778 4 11 -5 -11 401.127 277.357 4 11 -5 -11 54.3025 182.840 3 11 -5 -10 3108.58 623.475 4 11 -5 -10 3830.11 690.019 3 11 -5 -9 4329.27 722.287 3 11 -5 -8 6607.18 896.896 3 11 -5 -7-44.5501 95.4261 3 11 -5 -6 8212.52 989.771 3 11 -5 -5 4666.19 762.030 3 11 -5 -4 1224.50 289.409 1 11 -5 -4 594.710 286.951 3 11 -5 -3 1890.13 494.841 3 11 -5 -3 2750.12 439.160 1 11 -5 -2 2844.82 641.859 3 11 -5 -2 2655.10 450.334 1 11 -5 -1 3988.90 741.781 3 11 -5 -1 4105.78 578.644 1 11 -5 0 302.422 147.671 1 11 -5 1 6490.66 798.139 1 11 -5 2 1586.36 380.097 1 11 -5 3 1287.98 382.781 1 11 -5 4 1.99538 146.532 1 11 -5 5 1839.10 495.974 1 11 -5 6 1171.59 397.995 1 11 -4 -17 1075.59 442.637 4 11 -4 -16 407.307 262.061 4 11 -4 -15 1847.52 496.521 4 11 -4 -14 12267.9 1298.79 4 11 -4 -13 1971.56 531.242 4 11 -4 -12 674.906 322.780 4 11 -4 -11 1195.92 419.838 4 11 -4 -11 1053.42 365.379 3 11 -4 -10 2852.95 579.280 4 11 -4 -10 2022.55 516.385 3 11 -4 -9 895.028 332.450 3 11 -4 -8 3658.23 633.870 3 11 -4 -7 7495.49 908.157 3 11 -4 -6 16594.8 1367.35 3 11 -4 -5-126.632 105.755 3 11 -4 -5 141.986 96.0625 1 11 -4 -4 2239.52 508.544 3 11 -4 -4 1876.22 355.373 1 11 -4 -3 5740.85 628.105 1 11 -4 -3 5113.85 776.603 3 11 -4 -2 15714.3 1102.83 1 11 -4 -2 18369.7 1499.06 3 11 -4 -1 2812.74 479.640 1 11 -4 0 3509.55 552.085 1 11 -4 1-106.041 144.746 1 11 -4 2 1484.91 403.105 1 11 -4 3 2263.33 504.673 1 11 -4 4 168.724 185.259 1 11 -4 5 813.164 316.843 1 11 -4 6 1268.89 396.186 1 11 -4 7 3696.16 717.347 1 11 -3 -18 2403.48 641.005 4 11 -3 -17 839.174 358.682 4 11 -3 -16 4527.59 811.501 4 11 -3 -15 1977.35 509.507 4 11 -3 -14 55.3212 139.439 4 11 -3 -13 1986.10 489.800 4 11 -3 -12 98.6325 144.530 4 11 -3 -11 1095.43 381.341 4 11 -3 -11 1062.56 335.338 3 11 -3 -10 7332.15 880.695 4 11 -3 -10 6573.22 837.928 3 11 -3 -9 660.761 235.369 3 11 -3 -8 2885.68 564.149 3 11 -3 -7 553.242 237.154 3 11 -3 -6 6304.95 801.381 3 11 -3 -5-14.9448 187.049 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1 11 -2 -2 12850.8 1136.94 3 11 -2 -1 173.331 161.790 1 11 -2 0 3456.00 537.778 1 11 -2 1 1720.82 402.838 1 11 -2 2 1203.44 339.393 1 11 -2 3 897.463 324.920 1 11 -2 4 3244.27 596.744 1 11 -2 5 3631.06 654.507 1 11 -2 6 1346.44 426.624 1 11 -2 7 2164.74 546.886 1 11 -2 8 1541.65 469.274 1 11 -2 9 1025.56 380.462 1 11 -1 -20 4155.93 825.760 4 11 -1 -19 2632.97 642.144 4 11 -1 -18 622.375 325.313 4 11 -1 -17 620.391 315.706 4 11 -1 -16 2649.96 554.098 4 11 -1 -15 7862.46 939.356 4 11 -1 -14 457.102 232.458 4 11 -1 -13 4151.83 640.104 4 11 -1 -12 29888.4 1714.53 4 11 -1 -11 6871.40 789.826 4 11 -1 -10 10728.0 961.388 4 11 -1 -10 10579.4 985.572 3 11 -1 -9 4243.20 618.584 3 11 -1 -8 2056.43 425.561 3 11 -1 -7 543.661 242.775 3 11 -1 -6 9197.05 872.635 3 11 -1 -5 247.423 132.468 3 11 -1 -4 5211.56 665.214 3 11 -1 -3 5990.74 728.766 3 11 -1 -2 317.147 134.676 3 11 -1 -2 325.375 195.315 1 11 -1 -1 12343.0 1000.32 1 11 -1 0 1368.00 346.881 1 11 -1 1 401.027 187.262 1 11 -1 2 4656.57 667.180 1 11 -1 3 562.326 273.790 1 11 -1 4 1284.45 383.610 1 11 -1 5 3907.92 669.587 1 11 -1 6 1715.59 482.434 1 11 -1 7 1235.06 405.382 1 11 -1 8 1696.56 482.944 1 11 -1 9 504.400 214.749 1 11 0 -20 818.955 367.177 4 11 0 -19 796.888 392.971 4 11 0 -18 6902.34 973.927 4 11 0 -17 1445.46 424.635 4 11 0 -16 1290.87 389.728 4 11 0 -15 1140.27 354.003 4 11 0 -14 4166.24 634.894 4 11 0 -13 1273.52 349.646 4 11 0 -12-50.9614 111.197 4 11 0 -11 22050.4 1362.13 4 11 0 -10 199.473 115.815 4 11 0 -9 5642.72 643.118 4 11 0 -9 5689.23 682.143 3 11 0 -8 4403.00 591.634 3 11 0 -7 935.362 290.758 3 11 0 -6 51399.5 2080.40 3 11 0 -5 3625.66 515.528 3 11 0 -4 30727.6 1553.68 3 11 0 -3 2884.03 474.020 3 11 0 -3 2394.66 225.325 2 11 0 -2 10606.3 915.140 3 11 0 -1 154.179 149.626 1 11 0 0 9898.22 944.250 1 11 0 1 843.855 297.525 1 11 0 2 346.439 237.897 1 11 0 3 731.451 280.502 1 11 0 4 4318.09 678.886 1 11 0 5 10049.7 1074.90 1 11 0 6 1984.36 522.730 1 11 0 7 4677.75 798.876 1 11 0 8 250.778 230.586 1 11 0 9 287.405 226.948 1 11 1 -21 532.969 303.333 4 11 1 -20 5187.29 875.774 4 11 1 -19 2975.90 667.419 4 11 1 -18 468.264 312.368 4 11 1 -17 38.1187 172.790 4 11 1 -16 1964.24 456.528 4 11 1 -15 7077.10 820.569 4 11 1 -14 972.603 286.861 4 11 1 -13 4451.09 595.504 4 11 1 -12 27088.2 1475.33 4 11 1 -11 6767.68 685.721 4 11 1 -10 11308.3 872.637 4 11 1 -9 3870.51 497.050 4 11 1 -8 1989.68 381.140 3 11 1 -7 344.716 175.818 3 11 1 -6 7988.08 732.774 3 11 1 -5 496.346 162.807 3 11 1 -4 5686.43 432.507 2 11 1 -4 5589.75 605.428 3 11 1 -3 4616.68 433.020 2 11 1 -3 3601.06 482.492 3 11 1 -2 444.012 210.603 3 11 1 -2 467.828 164.713 2 11 1 -1 13523.7 994.644 3 11 1 1 617.785 264.608 1 11 1 2 3561.70 596.533 1 11 1 3 250.042 185.253 1 11 1 4 1087.54 355.727 1 11 1 5 4706.39 747.875 1 11 1 6 1877.64 504.499 1 11 1 7 1703.66 474.045 1 11 1 8 1049.60 378.506 1 11 1 9 478.190 307.813 1 11 1 10 84.0141 257.843 1 11 2 -18 2119.12 505.550 4 11 2 -17 535.947 257.972 4 11 2 -16 16.0905 139.664 4 11 2 -15 3855.21 593.958 4 11 2 -14 6393.58 717.534 4 11 2 -13 3192.22 485.967 4 11 2 -12 3189.92 454.385 4 11 2 -11 10956.9 820.726 4 11 2 -10 285.385 139.586 4 11 2 -9 6685.62 598.831 4 11 2 -8 8282.93 668.720 4 11 2 -6 44219.3 1719.95 3 11 2 -5 3498.65 420.575 2 11 2 -5 3436.13 442.016 3 11 2 -4 2860.15 405.133 2 11 2 -4 3445.85 430.129 3 11 2 -3 605.386 193.910 2 11 2 -3 824.004 224.790 3 11 2 -2 13254.9 942.847 2 11 2 -2 14267.6 902.734 3 11 2 -1 327.353 163.137 3 11 2 -1 421.092 209.321 2 11 2 0 4180.72 513.162 3 11 2 4 3700.53 658.556 1 11 2 5 3323.36 633.157 1 11 2 6 2247.97 534.440 1 11 2 7 1844.85 495.208 1 11 2 8 1619.76 462.687 1 11 2 9 1257.76 434.593 1 11 2 10 1037.65 402.144 1 11 3 -13 286.129 171.505 4 11 3 -11 1034.45 226.524 4 11 3 -10 7144.32 562.179 4 11 3 -9 1518.13 253.663 4 11 3 -8 3690.46 377.339 4 11 3 -7 936.940 185.635 4 11 3 -5 614.321 230.694 2 11 3 -4 1871.15 390.996 2 11 3 -4 1773.81 282.786 3 11 3 -3 442.336 206.123 2 11 3 -3 67.3349 81.3076 3 11 3 -2 2343.30 453.885 2 11 3 -2 2164.37 311.443 3 11 3 -1 6338.30 764.515 2 11 3 -1 7011.37 568.689 3 11 3 0 5842.06 751.305 2 11 3 0 7301.53 596.047 3 11 3 1 3085.25 400.606 3 11 3 1 2802.21 525.211 2 11 4 -5 493.195 261.956 2 11 4 -4 1056.74 301.377 2 11 4 -3 6608.10 818.996 2 11 4 -2 14093.2 1239.11 2 11 4 -1 2091.23 482.576 2 11 4 0 2260.82 512.107 2 11 4 1 125.276 119.727 2 11 4 2 1018.35 352.770 2 11 4 3 1063.04 381.998 2 11 5 -5 4404.07 711.474 2 11 5 -4 801.644 295.969 2 11 5 -3 3434.12 652.947 2 11 5 -2 3044.50 616.469 2 11 5 -1 3133.80 640.110 2 11 5 0 59.6757 119.074 2 11 5 1 5774.54 914.597 2 11 5 2 2238.93 584.071 2 11 5 3 724.722 334.444 2 11 5 4 491.024 323.866 2 11 5 5 926.005 410.548 2 11 6 -5 9944.41 1170.89 2 11 6 -4 2903.47 644.885 2 11 6 -3 299.640 247.936 2 11 6 -2 5871.63 940.890 2 11 6 -1 750.274 330.743 2 11 6 0 1716.68 539.058 2 11 6 1 1681.45 547.031 2 11 6 2 293.960 234.112 2 11 6 3 312.527 266.033 2 11 6 4 327.670 248.211 2 11 6 5 1184.95 497.522 2 11 7 -5 2854.42 692.338 2 11 7 -4 1057.28 419.723 2 11 7 -3 2189.90 623.227 2 11 7 -2 477.498 341.927 2 11 7 -1 778.063 348.772 2 11 7 0-67.2298 162.873 2 11 7 1 2004.38 622.727 2 11 7 2 1702.38 608.913 2 11 7 3 3518.15 866.878 2 11 8 -4 1165.96 444.459 2 11 8 -3 1228.02 454.011 2 11 8 -2 1435.91 536.618 2 12 -7 -11 1672.02 507.640 3 12 -7 -10 454.686 301.880 3 12 -7 -9 2075.69 571.798 4 12 -7 -9 3684.31 743.210 3 12 -7 -8 2474.63 611.715 3 12 -7 -7 2111.88 570.344 3 12 -7 -6 667.223 323.123 3 12 -7 -5-132.846 167.164 3 12 -7 -4 8019.78 1130.67 3 12 -7 -3 453.464 279.100 3 12 -7 -2 22.1586 204.881 3 12 -7 -1 170.161 308.657 3 12 -6 -12 6252.78 964.243 4 12 -6 -12 7350.57 1036.80 3 12 -6 -11 4059.08 791.959 4 12 -6 -11 3584.72 720.791 3 12 -6 -10-90.3533 181.468 4 12 -6 -10 462.859 283.279 3 12 -6 -9 1512.29 456.576 3 12 -6 -8 3350.54 701.204 3 12 -6 -7 277.187 254.147 3 12 -6 -6 176.022 209.456 3 12 -6 -5 6349.23 946.748 3 12 -6 -4 2195.88 574.646 3 12 -6 -3 6576.50 993.014 3 12 -6 -2 2628.48 642.664 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12 -4 -12 6145.73 914.005 4 12 -4 -12 6475.07 918.902 3 12 -4 -11 814.480 287.199 4 12 -4 -11 1612.98 460.922 3 12 -4 -10-49.5218 197.063 4 12 -4 -10 19.0861 142.161 3 12 -4 -9 4321.75 726.563 3 12 -4 -8 698.228 276.525 3 12 -4 -7 2330.97 536.576 3 12 -4 -6 3379.36 653.148 3 12 -4 -5 3332.52 646.368 3 12 -4 -5 3406.67 494.668 1 12 -4 -4 437.439 273.420 3 12 -4 -4 1289.90 300.754 1 12 -4 -3 2561.57 452.973 1 12 -4 -3 3132.00 657.976 3 12 -4 -2 3261.77 660.496 3 12 -4 -2 2299.76 444.484 1 12 -4 -1 1485.04 378.162 1 12 -4 0 13285.9 1138.60 1 12 -4 1 2906.55 555.092 1 12 -4 2 226.490 179.369 1 12 -4 3 3410.19 633.540 1 12 -4 4 2074.31 529.152 1 12 -4 5 245.410 184.008 1 12 -4 6 169.620 249.510 1 12 -3 -17 1918.83 532.488 4 12 -3 -16 9025.25 1131.35 4 12 -3 -15-42.3944 121.007 4 12 -3 -14 964.821 363.097 4 12 -3 -13 9934.14 1106.54 4 12 -3 -12 22.7252 184.024 4 12 -3 -11 692.155 260.022 4 12 -3 -11 518.480 263.088 3 12 -3 -10 3831.25 656.339 4 12 -3 -10 4104.18 678.335 3 12 -3 -9 2653.31 543.992 3 12 -3 -8 1982.16 488.729 3 12 -3 -7 9494.01 1015.92 3 12 -3 -6 12891.7 1226.30 3 12 -3 -5 1538.49 440.011 3 12 -3 -4 9694.57 1039.00 3 12 -3 -4 8654.14 804.477 1 12 -3 -3 3563.79 661.841 3 12 -3 -3 3147.02 497.790 1 12 -3 -2 653.750 235.168 1 12 -3 -2 699.230 289.995 3 12 -3 -1 1376.95 359.051 1 12 -3 0 4742.26 673.121 1 12 -3 1 1897.54 439.319 1 12 -3 2 8007.52 920.214 1 12 -3 3 68.4166 144.172 1 12 -3 4 282.234 306.766 1 12 -3 5 2773.45 596.685 1 12 -3 6 1009.97 386.618 1 12 -3 7 463.513 322.676 1 12 -2 -18 8635.93 1123.52 4 12 -2 -17 4558.69 796.209 4 12 -2 -16 1006.51 376.531 4 12 -2 -15 293.089 249.372 4 12 -2 -14 327.045 210.298 4 12 -2 -13 1987.32 493.677 4 12 -2 -12 8551.33 978.469 4 12 -2 -11 103.777 104.917 4 12 -2 -11 289.000 243.563 3 12 -2 -10 861.229 326.881 4 12 -2 -10 844.984 308.396 3 12 -2 -9 2743.53 530.294 3 12 -2 -8 293.162 202.804 3 12 -2 -7 1915.46 442.134 3 12 -2 -6 6502.79 816.048 3 12 -2 -5 1542.39 412.488 3 12 -2 -4 832.292 316.472 3 12 -2 -3 4492.60 693.938 3 12 -2 -3 4167.08 583.370 1 12 -2 -2 6031.48 707.637 1 12 -2 -2 6358.03 843.334 3 12 -2 -1 2905.67 508.704 1 12 -2 0 18361.8 1333.95 1 12 -2 1 184.329 165.806 1 12 -2 2 4748.11 705.605 1 12 -2 3 253.364 168.134 1 12 -2 4 6029.68 839.286 1 12 -2 5 323.692 182.699 1 12 -2 6 3409.55 679.907 1 12 -2 7 805.608 351.193 1 12 -1 -19 105.293 296.707 4 12 -1 -18 671.201 330.682 4 12 -1 -17 2009.11 522.792 4 12 -1 -16 3051.54 603.113 4 12 -1 -15 1782.55 455.280 4 12 -1 -14 60.4718 186.731 4 12 -1 -13 6140.60 788.616 4 12 -1 -12 207.980 167.800 4 12 -1 -11 4232.48 671.404 4 12 -1 -10 739.850 257.952 4 12 -1 -10 498.217 253.711 3 12 -1 -9 2885.02 513.061 3 12 -1 -8 7883.50 851.282 3 12 -1 -7 19640.7 1351.48 3 12 -1 -6 8231.74 869.110 3 12 -1 -5 998.884 328.064 3 12 -1 -4 56852.9 2448.41 3 12 -1 -3 532.496 218.142 3 12 -1 -2 133.795 186.739 3 12 -1 -2 155.317 125.022 1 12 -1 -1 3341.49 557.056 1 12 -1 0 4749.78 672.627 1 12 -1 1 249.006 212.899 1 12 -1 2 18122.6 1390.91 1 12 -1 3 1056.11 337.868 1 12 -1 4 847.680 318.145 1 12 -1 5 727.307 328.295 1 12 -1 6 1980.83 508.171 1 12 -1 7 1810.26 527.525 1 12 -1 8 970.174 380.723 1 12 0 -20-14.6767 278.805 4 12 0 -19 331.796 275.326 4 12 0 -18 5955.25 886.166 4 12 0 -17 8650.75 1022.17 4 12 0 -16 2076.43 507.842 4 12 0 -15-96.4805 164.899 4 12 0 -14 1017.79 331.539 4 12 0 -13 2889.79 525.515 4 12 0 -12 336.222 219.544 4 12 0 -11 3844.45 563.380 4 12 0 -10 405.235 193.115 4 12 0 -9 6566.41 762.349 3 12 0 -8 2462.34 464.669 3 12 0 -7 704.783 265.842 3 12 0 -6 24198.1 1428.49 3 12 0 -5 1159.87 307.261 3 12 0 -4 775.116 256.183 3 12 0 -3 35855.1 1825.70 3 12 0 -2-16.8578 106.922 3 12 0 -1 3543.02 569.494 3 12 0 -1 2339.37 472.750 1 12 0 0 5437.75 735.653 1 12 0 1 34.4215 163.756 1 12 0 2 4958.99 726.506 1 12 0 3 2664.50 548.079 1 12 0 4 44.6442 177.319 1 12 0 5 1670.52 490.129 1 12 0 6 6522.58 936.063 1 12 0 7 96.4996 139.555 1 12 0 8 370.421 186.931 1 12 1 -20 115.858 159.674 4 12 1 -19-413.298 251.556 4 12 1 -18 937.695 350.175 4 12 1 -17 1242.49 395.069 4 12 1 -16 2787.50 533.481 4 12 1 -15 1363.35 384.994 4 12 1 -14 229.995 123.761 4 12 1 -13 6055.42 707.473 4 12 1 -12 262.042 171.543 4 12 1 -11 3909.80 546.230 4 12 1 -10 807.711 245.461 4 12 1 -9 2520.24 424.847 4 12 1 -8 7754.46 779.717 3 12 1 -7 21969.3 1305.84 3 12 1 -6 8578.60 788.802 3 12 1 -5 774.243 238.852 3 12 1 -4 53208.5 1545.66 2 12 1 -4 58245.5 2186.29 3 12 1 -3 1152.08 303.335 3 12 1 -3 911.185 208.255 2 12 1 -2 184.492 115.969 3 12 1 -2 262.342 137.022 2 12 1 -1 2656.24 452.551 3 12 1 0 4230.69 585.268 3 12 1 2 18828.2 1461.34 1 12 1 3 327.236 176.501 1 12 1 4 1972.89 495.179 1 12 1 5 320.992 254.744 1 12 1 6 3249.38 670.055 1 12 1 7 1137.12 386.743 1 12 1 8 888.367 386.724 1 12 2 -17 4089.96 667.292 4 12 2 -16 1357.47 380.456 4 12 2 -15 574.628 216.184 4 12 2 -14 757.801 273.384 4 12 2 -13 2316.06 417.460 4 12 2 -12 8936.55 784.199 4 12 2 -11 12.4264 67.9385 4 12 2 -10 536.880 192.656 4 12 2 -9 3508.04 466.899 4 12 2 -8 209.196 131.508 4 12 2 -6 6864.40 671.862 3 12 2 -5 878.568 215.138 2 12 2 -5 1164.21 278.143 3 12 2 -4 574.210 186.152 2 12 2 -4 483.086 178.268 3 12 2 -3 4035.14 504.879 2 12 2 -3 5876.20 606.929 3 12 2 -2 6374.35 669.443 2 12 2 -2 5560.79 598.169 3 12 2 -1 3300.69 464.025 3 12 2 -1 2202.98 408.852 2 12 2 0 17503.8 1124.94 3 12 2 1-3.02481 97.5250 3 12 2 5-182.119 183.469 1 12 2 6 2880.33 627.745 1 12 2 7 85.0315 123.435 1 12 2 8 1834.65 541.961 1 12 3 -8 2312.53 313.728 4 12 3 -7 8748.61 617.214 4 12 3 -5 1932.09 373.874 2 12 3 -4 10058.5 894.572 2 12 3 -4 8700.59 676.150 3 12 3 -3 3977.04 575.381 2 12 3 -3 3238.28 405.326 3 12 3 -2 913.277 286.628 2 12 3 -2 1086.02 239.674 3 12 3 -1 1189.29 249.298 3 12 3 -1 1375.51 356.597 2 12 3 0 5796.79 764.311 2 12 3 1 2472.44 519.605 2 12 4 -5 3679.87 621.924 2 12 4 -4 931.266 322.658 2 12 4 -3 2636.58 529.796 2 12 4 -2 2104.21 489.984 2 12 4 -1 995.229 368.031 2 12 4 0 12382.2 1235.15 2 12 4 1 2147.08 548.343 2 12 4 2 109.465 158.019 2 12 4 3 2606.15 599.402 2 12 5 -5 315.035 240.791 2 12 5 -4 5321.95 803.363 2 12 5 -3 29.7264 154.255 2 12 5 -2 1326.97 434.377 2 12 5 -1 519.020 243.722 2 12 5 0 3372.10 700.045 2 12 5 1 31.3493 154.861 2 12 5 2 3932.15 789.852 2 12 5 3 551.218 316.157 2 12 5 4 1047.61 435.421 2 12 5 5 2358.02 651.291 2 12 5 6 1297.42 521.840 2 12 6 -5 7060.87 993.741 2 12 6 -4 1031.26 379.425 2 12 6 -3 5136.09 869.659 2 12 6 -2 1722.43 501.849 2 12 6 -1 111.578 244.656 2 12 6 0 3345.77 737.641 2 12 6 1 1226.18 463.558 2 12 6 2 180.685 268.558 2 12 6 3 475.563 319.337 2 12 6 4 471.047 298.461 2 12 7 -5-8.24430 110.475 2 12 7 -4 6980.94 1065.71 2 12 7 -3 480.631 323.551 2 12 7 -2-31.5534 260.048 2 12 7 -1 207.535 146.112 2 12 7 0 1991.20 615.854 2 12 7 1 2667.76 733.827 2 12 7 2 460.557 329.807 2 12 8 -4 291.909 261.462 2 13 -6 -12 765.807 328.319 3 13 -6 -11 782.118 368.161 4 13 -6 -11 615.473 359.730 3 13 -6 -10 2823.19 687.432 4 13 -6 -10 4166.39 795.466 3 13 -6 -9 2114.74 562.038 3 13 -6 -8 995.098 435.511 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