data_BA2ND2GE4O13_publ

_pd_block_id
  2021-05-26T17:10|BA2ND2GE4O13|Chufarov|Overall

_audit_creation_method  "from EXP file using GSAS2CIF"
_audit_creation_date                   2021-05-26T17:10
_audit_author_name                     Chufarov
_audit_update_record
; 2021-05-26T17:10  Initial CIF as created by GSAS2CIF
;

#=============================================================================
# this information describes the project, paper etc. for the CIF             #
# Acta Cryst. Section C papers and editorial correspondence is generated     #
# from the information in this section                                       #
#                                                                            #
#   (from)   CIF submission form for Rietveld refinements (Acta Cryst. C)    #
#                                                 Version 14 December 1998   #
#=============================================================================
# 1. SUBMISSION DETAILS

_publ_contact_author_name            'Lipina, Olga Andreevna'
_publ_contact_author_address            
'Inst. of Solid State Chemistry UB RAS 91, Pervomaiskaya, Ekaterinburg Russia'
_publ_contact_author_email           'LipinaOlgaA@yandex.ru'
_publ_contact_author_fax             ?
_publ_contact_author_phone           '+7 952 143 0282'

_publ_contact_letter
; ?
;

_publ_requested_journal              'Dalton Transactions'
_publ_requested_coeditor_name        ?
_publ_requested_category             ?   # Acta C: one of CI/CM/CO/FI/FM/FO

#==============================================================================

# 2. PROCESSING SUMMARY (IUCr Office Use Only)

_journal_data_validation_number      ?

_journal_date_recd_electronic        ?
_journal_date_to_coeditor            ?
_journal_date_from_coeditor          ?
_journal_date_accepted               ?
_journal_date_printers_first         ?
_journal_date_printers_final         ?
_journal_date_proofs_out             ?
_journal_date_proofs_in              ?
_journal_coeditor_name               ?
_journal_coeditor_code               ?
_journal_coeditor_notes
; ?
;
_journal_techeditor_code             ?
_journal_techeditor_notes
; ?
;
_journal_coden_ASTM                  ?
_journal_name_full                   'Dalton Transactions'
_journal_year                        2021
_journal_volume                      ?
_journal_issue                       ?
_journal_page_first                  ?
_journal_page_last                   ?
_journal_paper_category              ?
_journal_suppl_publ_number           ?
_journal_suppl_publ_pages            ?

#==============================================================================

# 3. TITLE AND AUTHOR LIST

_publ_section_title   
;
Structural and spectroscopic characterization of new Ba2RE2Ge4O13 (RE = Pr, Nd, Gd, Dy) and Ba2Gd2-xEuxGe4O13 tetragermanates
;

_publ_section_title_footnote
; ?
;

# The loop structure below should contain the names and addresses of all
# authors, in the required order of publication. Repeat as necessary.

loop_
	_publ_author_name
	_publ_author_footnote
	_publ_author_address

'Lipina, Olga A.'
','
'Inst. of Solid State Chemistry, UB RAS, Pervomaiskaya 91, Ekaterinburg, Russia'

'Surat, Ludmila L.'
','
'Inst. of Solid State Chemistry, UB RAS, Pervomaiskaya 91, Ekaterinburg, Russia'

'Chufarov, Alexander Yu.'
','
'Inst. of Solid State Chemistry, UB RAS, Pervomaiskaya 91, Ekaterinburg, Russia'

'Tyutyunnik, Alexander P.'
','
'Inst. of Solid State Chemistry, UB RAS, Pervomaiskaya 91, Ekaterinburg, Russia'

'Enyashin, Andrey N.'
','
'Inst. of Solid State Chemistry, UB RAS, Pervomaiskaya 91, Ekaterinburg, Russia'

'Baklanova, Yana V.'
','
'Inst. of Solid State Chemistry, UB RAS, Pervomaiskaya 91, Ekaterinburg, Russia'

'Chvanova, Anastasia V.'
','
'Inst. of Solid State Chemistry, UB RAS, Pervomaiskaya 91, Ekaterinburg, Russia'

'Mironov, Leonid Yu.'
','
'ITMO University, Kronverksky Pr. 49, bldg. A, St. Petersburg, Russia'

'Belova, Ksenia G.'
','
;
Inst. of High Temperature Electrochemistry, Akademicheskaya 20, UB RAS,
Ekaterinburg, Russia
Inst. of Natural Sciences and Mathematics, Ural Federal University, 
48 Kuybisheva, Ekaterinburg, Russia
;

'Zubkov, Vladimir G.'
','
'Inst. of Solid State Chemistry, UB RAS, Pervomaiskaya 91, Ekaterinburg, Russia'

#==============================================================================

# 4. TEXT

_publ_section_synopsis
;  ?
;
_publ_section_abstract
; ?
;
_publ_section_comment
; ?
;
_publ_section_exptl_prep      # Details of the preparation of the sample(s)
                              # should be given here.
; ?
;
_publ_section_exptl_refinement
; ?
;
_publ_section_references
; ?
;
_publ_section_figure_captions
; ?
;
_publ_section_acknowledgements
; This work was supported by the Russian Science Foundation (Grant 19-73-00219)
;


#=============================================================================
# 5. OVERALL REFINEMENT & COMPUTING DETAILS

_refine_special_details
; ?
;
_pd_proc_ls_special_details
; ?
;

# The following items are used to identify the programs used.
_computing_molecular_graphics     'VESTA Ver. 3.4.4'
_computing_publication_material   ?

_refine_ls_weighting_scheme       ?
_refine_ls_weighting_details      ?
_refine_ls_hydrogen_treatment     ?
_refine_ls_extinction_method      ?
_refine_ls_extinction_coef        ?
_refine_ls_number_constraints     ?

_refine_ls_restrained_S_all       ?
_refine_ls_restrained_S_obs       ?

#==============================================================================
# 6. SAMPLE PREPARATION DATA

# (In the unusual case where multiple samples are used in a single
#  Rietveld study, this information should be moved into the phase
#  blocks)

# The following three fields describe the preparation of the material.
# The cooling rate is in K/min.  The pressure at which the sample was
# prepared is in kPa.  The temperature of preparation is in K.

_pd_prep_cool_rate                ?
_pd_prep_pressure                 ?
_pd_prep_temperature              ?

_pd_char_colour                   white       # use ICDD colour descriptions


_refine_ls_shift/su_max                0.04
_refine_ls_shift/su_mean               0.01
_computing_structure_refinement        GSAS
_refine_ls_number_parameters           68
_refine_ls_goodness_of_fit_all         1.35
_refine_ls_number_restraints           0
_refine_ls_matrix_type                 full

#==============================================================================
# 7. CHEMICAL, STRUCTURAL AND CRYSTAL DATA

_pd_char_particle_morphology      ?

_chemical_name_systematic         "Dibarium dineodymium(III) tetragermanate"
_chemical_name_common             "Barium Neodymium Germanate"
_chemical_formula_moiety          ?
_chemical_formula_structural      "Ba2 Nd2 Ge4 O13"
_chemical_formula_analytical      ?
_chemical_melting_point           ?
_chemical_compound_source         ?       # for minerals and
                                          # natural products
_symmetry_space_group_name_Hall   "-C 2yc"

_exptl_crystal_F_000               ?
_exptl_crystal_density_diffrn      5.655
_exptl_crystal_density_meas        ?
_exptl_crystal_density_method      "not measured"

_cell_measurement_temperature     298(2)

_cell_special_details
; ?
;

_geom_special_details             ?

# The following item identifies the program(s) used (if appropriate).
_computing_structure_solution     
"GSAS (A.C. Larson and R.B. Von Dreele, 2004), EXPGUI (Toby, B.H., 2001)"

#==============================================================================

# 8. Phase information from GSAS




_pd_phase_name                        "Ba2Nd2Ge4O13"
_cell_length_a                         13.23863(10)
_cell_length_b                         5.41200(4)
_cell_length_c                         18.04514(16)
_cell_angle_alpha                      90.0
_cell_angle_beta                       105.3650(4)
_cell_angle_gamma                      90.0
_cell_volume                           1246.678(23)
_symmetry_cell_setting                 monoclinic
_symmetry_space_group_name_H-M         "C 1 2/c 1"
loop_ _symmetry_equiv_pos_site_id _symmetry_equiv_pos_as_xyz
       1 +x,+y,+z 
       2 -x,+y,-z+1/2 
      -1 -x,-y,-z 
      -2 +x,-y,+z+1/2 
     101 +x+1/2,+y+1/2,+z 
     102 -x+1/2,+y+1/2,-z+1/2 
    -101 -x+1/2,-y+1/2,-z 
    -102 +x+1/2,-y+1/2,+z+1/2 

# ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS


loop_
      _atom_site_type_symbol
      _atom_site_label
      _atom_site_fract_x
      _atom_site_fract_y
      _atom_site_fract_z
      _atom_site_occupancy
      _atom_site_thermal_displace_type
      _atom_site_U_iso_or_equiv
      _atom_site_symmetry_multiplicity
Ba
Ba      0.15676(8)   0.5031(4)    0.33256(5)   1.0        Uiso   0.0249(9)     8
Nd
Nd      0.11615(8)   0.51062(32)  0.08719(5)   1.0        Uiso   0.0230(9)     8
Ge
Ge1     0.06640(14)  0.0457(5)    0.18567(11)  1.0        Uiso   0.0232(11)    8
Ge
Ge2    -0.11998(17) -0.0307(6)    0.04035(12)  1.0        Uiso   0.0263(10)    8
O 
O1      0.0756(8)   -0.2726(18)   0.1899(6)    1.0        Uiso   0.013(4)      8
O 
O2      0.1726(8)    0.2300(16)   0.1978(6)    1.0        Uiso   0.0156(34)    8
O 
O3      0.0          0.1725(26)   0.25         1.0        Uiso   0.024(5)      4
O 
O4     -0.0175(8)    0.1652(17)   0.0965(6)    1.0        Uiso   0.016(4)      8
O 
O5     -0.1635(7)    0.1019(17)  -0.0507(6)    1.0        Uiso   0.019(4)      8
O 
O6     -0.2053(6)   -0.0485(22)   0.0986(4)    1.0        Uiso   0.014(4)      8
O 
O7     -0.0694(7)   -0.3391(20)   0.0354(6)    1.0        Uiso   0.026(4)      8

# If you change Z, be sure to change all 3 of the following
_chemical_formula_sum                  "Ba2 Ge4 Nd2 O13"
_chemical_formula_weight               1061.49
_cell_formula_units_Z                  4

# MOLECULAR GEOMETRY

loop_
      _geom_bond_atom_site_label_1
      _geom_bond_atom_site_label_2
      _geom_bond_distance
      _geom_bond_site_symmetry_1
      _geom_bond_site_symmetry_2
      _geom_bond_publ_flag
  Ba        O1               2.792(10)  .      1_565  N
  Ba        O1               3.231(10)  .      2_565  N
  Ba        O2               2.900(10)  .      1_555  N
  Ba        O2               2.751(10)  .    102_555  N
  Ba        O3                2.844(9)  .      1_555  N
  Ba        O4               3.104(10)  .      2_555  N
  Ba        O5               2.786(10)  .   -102_555  N
  Ba        O6               3.232(12)  .      2_555  N
  Ba        O6               2.725(11)  .      2_565  N
  Ba        O7               3.033(10)  .      2_565  N
  Nd        O1               2.372(11)  .      1_565  N
  Nd        O2               2.462(10)  .      1_555  N
  Nd        O4               2.609(10)  .      1_555  N
  Nd        O5                2.333(9)  .     -1_565  N
  Nd        O6                2.340(7)  .    101_555  N
  Nd        O7               2.520(10)  .      1_565  N
  Nd        O7                2.327(9)  .     -1_555  N
  Ge1       Ge1             3.2625(34)  .      2_555  N
  Ge1       Ge2             3.1157(26)  .      1_555  N
  Ge1       O1               1.727(10)  .      1_555  N
  Ge1       O2               1.690(10)  .      1_555  N
  Ge1       O3                1.770(5)  .      1_555  N
  Ge1       O4                1.815(9)  .      1_555  N
  Ge2       O4               1.807(10)  .      1_555  N
  Ge2       O5                1.746(9)  .      1_555  N
  Ge2       O6                1.737(7)  .      1_555  N
  Ge2       O7               1.809(11)  .      1_555  N

loop_
      _geom_angle_atom_site_label_1
      _geom_angle_atom_site_label_2
      _geom_angle_atom_site_label_3
      _geom_angle
      _geom_angle_site_symmetry_1
      _geom_angle_site_symmetry_2
      _geom_angle_site_symmetry_3
      _geom_angle_publ_flag
  O1        Ba        O2               62.87(24)      1_565  .      1_555  N
  O1        Ba        O2               75.99(33)      1_565  .    102_555  N
  O1        Ba        O3               75.00(27)      1_565  .      1_555  N
  O1        Ba        O4              120.73(28)      1_565  .      2_555  N
  O1        Ba        O5              145.98(28)      1_565  .   -102_555  N
  O1        Ba        O6               91.14(28)      1_565  .      2_565  N
  O1        Ba        O7              117.91(27)      1_565  .      2_565  N
  O2        Ba        O2               79.33(22)      1_555  .    102_555  N
  O2        Ba        O3               56.29(22)      1_555  .      1_555  N
  O2        Ba        O4              103.20(27)      1_555  .      2_555  N
  O2        Ba        O5              107.03(29)      1_555  .   -102_555  N
  O2        Ba        O6              140.87(26)      1_555  .      2_565  N
  O2        Ba        O7              158.30(30)      1_555  .      2_565  N
  O2        Ba        O3              134.43(22)    102_555  .      1_555  N
  O2        Ba        O4              162.58(27)    102_555  .      2_555  N
  O2        Ba        O5               70.11(27)    102_555  .   -102_555  N
  O2        Ba        O6               65.59(25)    102_555  .      2_565  N
  O2        Ba        O7              122.34(30)    102_555  .      2_565  N
  O3        Ba        O4               54.18(20)      1_555  .      2_555  N
  O3        Ba        O5              128.77(33)      1_555  .   -102_555  N
  O3        Ba        O6              148.24(26)      1_555  .      2_565  N
  O3        Ba        O7              102.20(21)      1_555  .      2_565  N
  O4        Ba        O5               92.86(23)      2_555  .   -102_555  N
  O4        Ba        O6              115.50(24)      2_555  .      2_565  N
  O4        Ba        O7               56.64(26)      2_555  .      2_565  N
  O5        Ba        O6               77.65(27)   -102_555  .      2_565  N
  O5        Ba        O7               83.74(27)   -102_555  .      2_565  N
  O6        Ba        O7               58.93(25)      2_565  .      2_565  N
  O1        Nd        O2               75.79(29)      1_565  .      1_555  N
  O1        Nd        O4               90.36(34)      1_565  .      1_555  N
  O1        Nd        O5               84.78(33)      1_565  .     -1_565  N
  O1        Nd        O6              115.58(33)      1_565  .    101_555  N
  O1        Nd        O7               74.31(31)      1_565  .      1_565  N
  O1        Nd        O7                151.9(4)      1_565  .     -1_555  N
  O2        Nd        O4               64.60(33)      1_555  .      1_555  N
  O2        Nd        O5              137.46(34)      1_555  .     -1_565  N
  O2        Nd        O6                 76.2(4)      1_555  .    101_555  N
  O2        Nd        O7              123.79(34)      1_555  .      1_565  N
  O2        Nd        O7                118.2(4)      1_555  .     -1_555  N
  O4        Nd        O5              154.10(33)      1_555  .     -1_565  N
  O4        Nd        O6              125.64(35)      1_555  .    101_555  N
  O4        Nd        O7               69.16(34)      1_555  .      1_565  N
  O4        Nd        O7               76.19(31)      1_555  .     -1_555  N
  O5        Nd        O6                 78.9(4)     -1_565  .    101_555  N
  O5        Nd        O7               85.06(35)     -1_565  .      1_565  N
  O5        Nd        O7                 96.6(4)     -1_565  .     -1_555  N
  O6        Nd        O7              159.95(33)    101_555  .      1_565  N
  O6        Nd        O7               92.12(32)    101_555  .     -1_555  N
  O7        Nd        O7                 77.8(4)      1_565  .     -1_555  N
  Ge1       Ge1       Ge2               98.22(9)      2_555  .      1_555  N
  O1        Ge1       O2                122.5(6)      1_555  .      1_555  N
  O1        Ge1       O3                113.5(6)      1_555  .      1_555  N
  O1        Ge1       O4                114.4(5)      1_555  .      1_555  N
  O2        Ge1       O3                103.1(5)      1_555  .      1_555  N
  O2        Ge1       O4                101.4(5)      1_555  .      1_555  N
  O3        Ge1       O4                 98.6(4)      1_555  .      1_555  N
  O4        Ge2       O5                107.4(4)      1_555  .      1_555  N
  O4        Ge2       O6                101.9(4)      1_555  .      1_555  N
  O4        Ge2       O7                109.6(5)      1_555  .      1_555  N
  O5        Ge2       O6                119.1(4)      1_555  .      1_555  N
  O5        Ge2       O7                111.6(5)      1_555  .      1_555  N
  O6        Ge2       O7                106.7(5)      1_555  .      1_555  N

#==============================================================================
# 9. INSTRUMENT CHARACTERIZATION

_exptl_special_details
; ?
;

# if regions of the data are excluded, the reason(s) are supplied here:
_pd_proc_info_excluded_regions
; ?
;

# The following item is used to identify the equipment used to record
# the powder pattern when the diffractogram was measured at a laboratory
# other than the authors' home institution, e.g. when neutron or synchrotron
# radiation is used.

_pd_instr_location
; ?
;
_pd_calibration_special_details           # description of the method used
                                          # to calibrate the instrument
"external Si standard"

_diffrn_ambient_temperature       298
_diffrn_source                    "sealed X-ray tube"
_diffrn_source_target             Cu
_diffrn_source_type               "PHILIPS PW 2283/20"
_diffrn_measurement_device_type   "transmission diffractometer Stadi-P (STOE)"
_diffrn_detector                  "position sensitive detector"
_diffrn_detector_type             "linear mini-PSD (STOE)"
       # make or model of detector

_pd_meas_scan_method              step       # options are 'step', 'cont',
                                          # 'tof', 'fixed' or
                                          # 'disp' (= dispersive)
_pd_meas_special_details
;  ?
;

# The following two items identify the program(s) used (if appropriate).
_computing_data_collection        
"STOE Powder Software Package (STOE, Germany)"
_computing_data_reduction         
"STOE Powder Software Package (STOE, Germany)"

# Describe any processing performed on the data, prior to refinement.
# For example: a manual Lp correction or a precomputed absorption correction
_pd_proc_info_data_reduction      ?

# The following item is used for angular dispersive measurements only.

_diffrn_radiation_monochromator   "Primary, curved Ge 111"

# The following items are used to define the size of the instrument.
# Not all distances are appropriate for all instrument types.

_pd_instr_dist_src/mono           260
_pd_instr_dist_mono/spec          130
_pd_instr_dist_src/spec           ?
_pd_instr_dist_spec/anal          ?
_pd_instr_dist_anal/detc          ?
_pd_instr_dist_spec/detc          220

# 10. Specimen size and mounting information

# The next three fields give the specimen dimensions in mm.  The equatorial
# plane contains the incident and diffracted beam.

_pd_spec_size_axial               7       # perpendicular to
                                          # equatorial plane

_pd_spec_size_equat               0.1       # parallel to
                                          # scattering vector
                                          # in transmission

_pd_spec_size_thick               ?       # parallel to
                                          # scattering vector
                                          # in reflection

_pd_spec_mounting                         # This field should be
                                          # used to give details of the
                                          # container.
"powder on Mylar film"

_pd_spec_mount_mode               transmission       # options are 'reflection'
                                          # or 'transmission'

_pd_spec_shape                    flat_sheet       # options are 'cylinder'
                                          # 'flat_sheet' or 'irregular'






# phase table
loop_     _pd_phase_id
          _pd_phase_block_id
          _pd_phase_mass_%
          _pd_proc_ls_profile_function
          _pd_proc_ls_peak_cutoff
  1  2021-05-26T17:10|BA2ND2GE4O13_phase1|Chufarov||
           98.64(8)
;
 CW Profile function number 3 with  19 terms
 Pseudovoigt profile coefficients as parameterized in
 P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83.
 Asymmetry correction of L.W. Finger, D.E. Cox & A. P. Jephcoat (1994).
 J. Appl. Cryst.,27,892-900.
 #1(GU)   =   50.867 #2(GV)   =  -16.803 #3(GW)   =   26.215
 #4(GP)   =    0.000 #5(LX)   =    0.500 #6(LY)   =   15.550
 #7(S/L)  =   0.0230 #8(H/L)  =   0.0230
 #9(trns) =     0.00 #10(shft)=   0.0000
 #11(stec)=    -0.41 #12(ptec)=    -0.24 #13(sfec)=     0.00
 #14(L11) =   -0.025 #15(L22) =   -0.210 #16(L33) =   -0.010
 #17(L12) =   -0.032 #18(L13) =    0.013 #19(L23) =   -0.028
 Peak tails are ignored  where the intensity is below 0.0010 times the peak
   Aniso. broadening axis   0.0   0.0   1.0
;
           0.00100

loop_ _atom_type_symbol
      _atom_type_number_in_cell
      _atom_type_scat_dispersion_real
      _atom_type_scat_dispersion_imag
      _atom_type_scat_Cromer_Mann_a1
      _atom_type_scat_Cromer_Mann_a2
      _atom_type_scat_Cromer_Mann_a3
      _atom_type_scat_Cromer_Mann_a4
      _atom_type_scat_Cromer_Mann_b1
      _atom_type_scat_Cromer_Mann_b2
      _atom_type_scat_Cromer_Mann_b3
      _atom_type_scat_Cromer_Mann_b4
      _atom_type_scat_Cromer_Mann_c
      _atom_type_scat_source
  Ba     8.0        0.000    0.000
 20.3361 3.21600 19.2970 0.27560 10.8880 20.2073 2.69590 167.202 2.77310 
  International_Tables_Vol_C
  Nd     8.0        0.000    0.000
 22.6845 2.66248 19.6847 0.21063 12.7740 15.8850 2.85137 137.903 1.98486 
  International_Tables_Vol_C
  Ge    16.0        0.000    0.000
 16.0816 2.85090 6.37470 0.25160 3.70680 11.4468 3.68300 54.7625 2.13130 
  International_Tables_Vol_C
  O     52.0        0.000    0.000
 3.04850 13.2771 2.28680 5.70110 1.54630 0.32390 0.86700 32.9089 0.25080 
  International_Tables_Vol_C
_diffrn_radiation_probe                x-ray
_diffrn_radiation_polarisn_ratio       0.8
_diffrn_radiation_wavelength           1.54056
_diffrn_radiation_type                 'Cu K\a~1~'
_pd_proc_ls_prof_R_factor              0.0123
_pd_proc_ls_prof_wR_factor             0.0162
_pd_proc_ls_prof_wR_expected           0.0121
_refine_ls_R_Fsqd_factor               0.02454

_pd_proc_ls_background_function
;   GSAS Background function number 1 with 13 terms.
 Shifted Chebyshev function of 1st kind
      1:    6428.84     2:   -4193.25     3:    1685.71     4:   -1082.56    
      5:    289.211     6:   -32.1029     7:   -49.0405     8:    37.4261    
      9:   -6.55106    10:   -25.1037    11:    35.8955    12:   -17.0418    
     13:   -2.47824    
;

_exptl_absorpt_process_details
;   GSAS Absorption/surface roughness correction: function number 4
 Flat plate transmission absorption correction
Terms =    -0.21554         0.0000    
Correction is refined.
;
_exptl_absorpt_correction_T_min        1.39430
_exptl_absorpt_correction_T_max        2.08455
# Extinction correction
_gsas_exptl_extinct_corr_T_min         1.00000
_gsas_exptl_extinct_corr_T_max         1.00000
_pd_proc_info_datetime                 2021-05-26T17:10:14
_pd_calc_method                        "Rietveld Refinement"

#---- raw/calc data loop -----
_pd_meas_2theta_range_min              5.0
_pd_meas_2theta_range_max              119.98
_pd_meas_2theta_range_inc              0.02
_pd_proc_2theta_range_min              4.9683
_pd_proc_2theta_range_max              119.9483
_pd_proc_2theta_range_inc              0.02

loop_
      _pd_meas_counts_total
      _pd_proc_ls_weight
      _pd_proc_intensity_bkg_calc
      _pd_calc_intensity_total
  13624.0    0.0000734   13694.21875   13694.22461
  13654.0    0.0000732   13683.99707   13684.00098
  13550.0    0.0000738   13673.80469   13673.80957
  13486.0    0.0000742   13663.64160   13663.64551
  13447.0    0.0000744   13653.50684   13653.51172
  13511.0    0.0000740   13643.40039   13643.40527
  13556.0    0.0000738   13633.32324   13633.32812
  13693.0    0.0000730   13623.27344   13623.27832
  13516.0    0.0000740   13613.25098   13613.25586
  13545.0    0.0000738   13603.25781   13603.26367
  13407.0    0.0000746   13593.29199   13593.29688
  13568.0    0.0000737   13583.35352   13583.35938
  13223.0    0.0000756   13573.44238   13573.44727
  13519.0    0.0000740   13563.55762   13563.56348
  13550.0    0.0000738   13553.70215   13553.70703
  13640.0    0.0000733   13543.87109   13543.87695
  13397.0    0.0000746   13534.06836   13534.07422
  13648.0    0.0000733   13524.29199   13524.29785
  13292.0    0.0000752   13514.54102   13514.54688
  13553.0    0.0000738   13504.81738   13504.82324
  13645.0    0.0000733   13495.12012   13495.12598
  13719.0    0.0000729   13485.44824   13485.45410
  13535.0    0.0000739   13475.80176   13475.80762
  13565.0    0.0000737   13466.18164   13466.18750
  13307.0    0.0000751   13456.58594   13456.59180
  13403.0    0.0000746   13447.01562   13447.02148
  13603.0    0.0000735   13437.47070   13437.47754
  13429.0    0.0000745   13427.95117   13427.95703
  13509.0    0.0000740   13418.45605   13418.46289
  13486.0    0.0000742   13408.98535   13408.99219
  13323.0    0.0000751   13399.54004   13399.54688
  13546.0    0.0000738   13390.11816   13390.12500
  13256.0    0.0000754   13380.72070   13380.72754
  13328.0    0.0000750   13371.34766   13371.35449
  13370.0    0.0000748   13361.99805   13362.00488
  13224.0    0.0000756   13352.67285   13352.67969
  13345.0    0.0000749   13343.37012   13343.37793
  13251.0    0.0000755   13334.09180   13334.09863
  13352.0    0.0000749   13324.83691   13324.84375
  13355.0    0.0000749   13315.60449   13315.61133
  13521.0    0.0000740   13306.39551   13306.40332
  13144.0    0.0000761   13297.20898   13297.21680
  13465.0    0.0000743   13288.04590   13288.05273
  13190.0    0.0000758   13278.90527   13278.91211
  13166.0    0.0000760   13269.78613   13269.79395
  13410.0    0.0000746   13260.69043   13260.69824
  13090.0    0.0000764   13251.61621   13251.62402
  13317.0    0.0000751   13242.56543   13242.57227
  13166.0    0.0000760   13233.53516   13233.54199
  13070.0    0.0000765   13224.52637   13224.53320
  13100.0    0.0000763   13215.54004   13215.54688
  13325.0    0.0000750   13206.57422   13206.58203
  13155.0    0.0000760   13197.63086   13197.63867
  13171.0    0.0000759   13188.70801   13188.71582
  13334.0    0.0000750   13179.80566   13179.81348
  13150.0    0.0000760   13170.92578   13170.93359
  12940.0    0.0000773   13162.06543   13162.07324
  13012.0    0.0000769   13153.22656   13153.23438
  13277.0    0.0000753   13144.40723   13144.41504
  13312.0    0.0000751   13135.60938   13135.61719
  12935.0    0.0000773   13126.83105   13126.83887
  13257.0    0.0000754   13118.07227   13118.08105
  13042.0    0.0000767   13109.33496   13109.34277
  13037.0    0.0000767   13100.61621   13100.62500
  13159.0    0.0000760   13091.91797   13091.92676
  13061.0    0.0000766   13083.23926   13083.24805
  12928.0    0.0000774   13074.58008   13074.58789
  13189.0    0.0000758   13065.94043   13065.94922
  13112.0    0.0000763   13057.31934   13057.32812
  12885.0    0.0000776   13048.71777   13048.72656
  13053.0    0.0000766   13040.13574   13040.14355
  13214.0    0.0000757   13031.57227   13031.58008
  13049.0    0.0000766   13023.02637   13023.03516
  12875.0    0.0000777   13014.50000   13014.50879
  12964.0    0.0000771   13005.99316   13006.00098
  13052.0    0.0000766   12997.50293   12997.51074
  12980.0    0.0000770   12989.03223   12989.04004
  13053.0    0.0000766   12980.57812   12980.58691
  12880.0    0.0000776   12972.14355   12972.15137
  12942.0    0.0000773   12963.72656   12963.73438
  12879.0    0.0000776   12955.32617   12955.33496
  13022.0    0.0000768   12946.94531   12946.95312
  13094.0    0.0000764   12938.58105   12938.58984
  12920.0    0.0000774   12930.23438   12930.24414
  13061.0    0.0000766   12921.90430   12921.91406
  12835.0    0.0000779   12913.59180   12913.60156
  13120.0    0.0000762   12905.29688   12905.30762
  12939.0    0.0000773   12897.01855   12897.02832
  12902.0    0.0000775   12888.75684   12888.76758
  12992.0    0.0000770   12880.51172   12880.52246
  12966.0    0.0000771   12872.28418   12872.29590
  12723.0    0.0000786   12864.07227   12864.08398
  12882.0    0.0000776   12855.87695   12855.88965
  12796.0    0.0000781   12847.69824   12847.71094
  12893.0    0.0000776   12839.53516   12839.54883
  12991.0    0.0000770   12831.38965   12831.40430
  12733.0    0.0000785   12823.25879   12823.27441
  12876.0    0.0000777   12815.14355   12815.16016
  12772.0    0.0000783   12807.04492   12807.06250
  12959.0    0.0000772   12798.96094   12798.98047
  12860.0    0.0000778   12790.89355   12790.91602
  12810.0    0.0000781   12782.84082   12782.86523
  12718.0    0.0000786   12774.80371   12774.83105
  12964.0    0.0000771   12766.78223   12766.81055
  12904.0    0.0000775   12758.77539   12758.80273
  12744.0    0.0000785   12750.78418   12750.80762
  12756.0    0.0000784   12742.80664   12742.82617
  12893.0    0.0000776   12734.84473   12734.86133
  12758.0    0.0000784   12726.89746   12726.91016
  12829.0    0.0000779   12718.96484   12718.97559
  12780.0    0.0000782   12711.04688   12711.05664
  12759.0    0.0000784   12703.14258   12703.15234
  12709.0    0.0000787   12695.25391   12695.26270
  12738.0    0.0000785   12687.37793   12687.38672
  12817.0    0.0000780   12679.51660   12679.52539
  12566.0    0.0000796   12671.66992   12671.67871
  12726.0    0.0000786   12663.83691   12663.84570
  12694.0    0.0000788   12656.01758   12656.02637
  12904.0    0.0000775   12648.21191   12648.22070
  12633.0    0.0000792   12640.41992   12640.42871
  12668.0    0.0000789   12632.64160   12632.65039
  12699.0    0.0000787   12624.87695   12624.88574
  12600.0    0.0000794   12617.12500   12617.13379
  12494.0    0.0000800   12609.38672   12609.39551
  12754.0    0.0000784   12601.66211   12601.67090
  12546.0    0.0000797   12593.94922   12593.95801
  12492.0    0.0000801   12586.25000   12586.25879
  12516.0    0.0000799   12578.56445   12578.57324
  12786.0    0.0000782   12570.89062   12570.89941
  12579.0    0.0000795   12563.23047   12563.23926
  12491.0    0.0000801   12555.58203   12555.59082
  12454.0    0.0000803   12547.94727   12547.95605
  12367.0    0.0000809   12540.32324   12540.33203
  12490.0    0.0000801   12532.71289   12532.72168
  12567.0    0.0000796   12525.11426   12525.12305
  12584.0    0.0000795   12517.52832   12517.53711
  12573.0    0.0000795   12509.95410   12509.96289
  12449.0    0.0000803   12502.39160   12502.40039
  12387.0    0.0000807   12494.84180   12494.85059
  12213.0    0.0000819   12487.30371   12487.31250
  12523.0    0.0000799   12479.77637   12479.78516
  12436.0    0.0000804   12472.26270   12472.27148
  12485.0    0.0000801   12464.75879   12464.76758
  12489.0    0.0000801   12457.26660   12457.27539
  12478.0    0.0000801   12449.78613   12449.79492
  12380.0    0.0000808   12442.31738   12442.32617
  12418.0    0.0000805   12434.86035   12434.86816
  12585.0    0.0000795   12427.41309   12427.42188
  12489.0    0.0000801   12419.97852   12419.98730
  12234.0    0.0000817   12412.55371   12412.56250
  12573.0    0.0000795   12405.13965   12405.14844
  12190.0    0.0000820   12397.73730   12397.74609
  12449.0    0.0000803   12390.34570   12390.35449
  12397.0    0.0000807   12382.96484   12382.97363
  12231.0    0.0000818   12375.59375   12375.60254
  12294.0    0.0000813   12368.23438   12368.24219
  12367.0    0.0000809   12360.88477   12360.89355
  12425.0    0.0000805   12353.54590   12353.55371
  12348.0    0.0000810   12346.21777   12346.22559
  12214.0    0.0000819   12338.89844   12338.90723
  12345.0    0.0000810   12331.59082   12331.59961
  12561.0    0.0000796   12324.29297   12324.30078
  12288.0    0.0000814   12317.00391   12317.01270
  12390.0    0.0000807   12309.72656   12309.73535
  12449.0    0.0000803   12302.45801   12302.46680
  12212.0    0.0000819   12295.20020   12295.20801
  12220.0    0.0000818   12287.95117   12287.95996
  12269.0    0.0000815   12280.71191   12280.72070
  12466.0    0.0000802   12273.48340   12273.49121
  12373.0    0.0000808   12266.26270   12266.27148
  12465.0    0.0000802   12259.05273   12259.06152
  12241.0    0.0000817   12251.85156   12251.86035
  12339.0    0.0000810   12244.66113   12244.66895
  12246.0    0.0000817   12237.47852   12237.48633
  12137.0    0.0000824   12230.30566   12230.31348
  12208.0    0.0000819   12223.14062   12223.14941
  12264.0    0.0000815   12215.98535   12215.99414
  12461.0    0.0000803   12208.83984   12208.84863
  12136.0    0.0000824   12201.70312   12201.71191
  12290.0    0.0000814   12194.57520   12194.58398
  12334.0    0.0000811   12187.45508   12187.46387
  12083.0    0.0000828   12180.34473   12180.35352
  12067.0    0.0000829   12173.24316   12173.25195
  12171.0    0.0000822   12166.14941   12166.15820
  12196.0    0.0000820   12159.06445   12159.07324
  12063.0    0.0000829   12151.98828   12151.99707
  12256.0    0.0000816   12144.91992   12144.92871
  12092.0    0.0000827   12137.86035   12137.86914
  12193.0    0.0000820   12130.80859   12130.81738
  12212.0    0.0000819   12123.76660   12123.77539
  11984.0    0.0000834   12116.73145   12116.74023
  12135.0    0.0000824   12109.70508   12109.71289
  12339.0    0.0000810   12102.68555   12102.69434
  12188.0    0.0000820   12095.67480   12095.68359
  12113.0    0.0000826   12088.67188   12088.68066
  12269.0    0.0000815   12081.67676   12081.68652
  12199.0    0.0000820   12074.68945   12074.69922
  11928.0    0.0000838   12067.70996   12067.71973
  12065.0    0.0000829   12060.73828   12060.74707
  12057.0    0.0000829   12053.77441   12053.78516
  12048.0    0.0000830   12046.81738   12046.82812
  11918.0    0.0000839   12039.86914   12039.87988
  11837.0    0.0000845   12032.92676   12032.94043
  12087.0    0.0000827   12025.99219   12026.00879
  12055.0    0.0000830   12019.06641   12019.08496
  11897.0    0.0000841   12012.14648   12012.17090
  11983.0    0.0000835   12005.23438   12005.26562
  12077.0    0.0000828   11998.32910   11998.36816
  12072.0    0.0000828   11991.43164   11991.47949
  11887.0    0.0000841   11984.54004   11984.59863
  12081.0    0.0000828   11977.65625   11977.72754
  11967.0    0.0000836   11970.77930   11970.86426
  12100.0    0.0000826   11963.90918   11964.01074
  12057.0    0.0000829   11957.04590   11957.69727
  12059.0    0.0000829   11950.18945   11950.88965
  12038.0    0.0000831   11943.33984   11944.09668
  12073.0    0.0000828   11936.49707   11937.32520
  11894.0    0.0000841   11929.66113   11930.57129
  12123.0    0.0000825   11922.83203   11923.84180
  12028.0    0.0000831   11916.00879   11917.12402
  11920.0    0.0000839   11909.19238   11910.40430
  11805.0    0.0000847   11902.38281   11903.65820
  11938.0    0.0000838   11895.57812   11896.86816
  11991.0    0.0000834   11888.78125   11890.04102
  12005.0    0.0000833   11881.99023   11883.20410
  11844.0    0.0000844   11875.20605   11876.39062
  11863.0    0.0000843   11868.42773   11869.61426
  11729.0    0.0000853   11861.65527   11862.87891
  11884.0    0.0000841   11854.88867   11856.18066
  12047.0    0.0000830   11848.12891   11849.50977
  11797.0    0.0000848   11841.37500   11842.86328
  11808.0    0.0000847   11834.62695   11836.23828
  11874.0    0.0000842   11827.88477   11829.63770
  11855.0    0.0000844   11821.14941   11823.06641
  12002.0    0.0000833   11814.41797   11816.53027
  11670.0    0.0000857   11807.69434   11810.04590
  11831.0    0.0000845   11800.97559   11803.64355
  11645.0    0.0000859   11794.26270   11797.40234
  11854.0    0.0000844   11787.55469   11791.46191
  12032.0    0.0000831   11780.85449   11786.08008
  12138.0    0.0000824   11774.15723   11781.63281
  11817.0    0.0000846   11767.46680   11778.60645
  11784.0    0.0000849   11760.78223   11777.51074
  11740.0    0.0000852   11754.10254   11778.78027
  11895.0    0.0000841   11747.42773   11782.67969
  11701.0    0.0000855   11740.75977   11789.31543
  11712.0    0.0000854   11734.09570   11798.73730
  11848.0    0.0000844   11727.43848   11811.07715
  11890.0    0.0000841   11720.78516   11826.69238
  12055.0    0.0000830   11714.13867   11846.31641
  11734.0    0.0000852   11707.49512   11871.24316
  11885.0    0.0000841   11700.85840   11903.59961
  12012.0    0.0000833   11694.22656   11946.52734
  11951.0    0.0000837   11687.59961   12003.83594
  12222.0    0.0000818   11680.97754   12078.32031
  12218.0    0.0000818   11674.36035   12168.23242
  12168.0    0.0000822   11667.74902   12262.98926
  12211.0    0.0000819   11661.14062   12341.35156
  12259.0    0.0000816   11654.53906   12375.86523
  12467.0    0.0000802   11647.94141   12344.37402
  12311.0    0.0000812   11641.34863   12244.69434
  12247.0    0.0000817   11634.76172   12100.78418
  12026.0    0.0000832   11628.17773   11949.26172
  12011.0    0.0000833   11621.59961   11819.76953
  11743.0    0.0000852   11615.02637   11725.80371
  11706.0    0.0000854   11608.45703   11666.05469
  11507.0    0.0000869   11601.89258   11631.32617
  11449.0    0.0000873   11595.33301   11611.44922
  11541.0    0.0000866   11588.77832   11598.98633
  11565.0    0.0000865   11582.22656   11589.73535
  11422.0    0.0000876   11575.68066   11581.75781
  11746.0    0.0000851   11569.13867   11574.29004
  11438.0    0.0000874   11562.60059   11567.06152
  11511.0    0.0000869   11556.06738   11559.97852
  11651.0    0.0000858   11549.53906   11552.99609
  11779.0    0.0000849   11543.01367   11546.09277
  11597.0    0.0000862   11536.49414   11539.25488
  11329.0    0.0000883   11529.97754   11532.46582
  11517.0    0.0000868   11523.46582   11525.72168
  11647.0    0.0000859   11516.95898   11519.01270
  11526.0    0.0000868   11510.45508   11512.33301
  11591.0    0.0000863   11503.95605   11505.67969
  11475.0    0.0000871   11497.45996   11499.04785
  11393.0    0.0000878   11490.96973   11492.43750
  11552.0    0.0000866   11484.48145   11485.84180
  11538.0    0.0000867   11477.99902   11479.26367
  11418.0    0.0000876   11471.51953   11472.69824
  11362.0    0.0000880   11465.04395   11466.14551
  11402.0    0.0000877   11458.57324   11459.60449
  11491.0    0.0000870   11452.10547   11453.07324
  11465.0    0.0000872   11445.64258   11446.55176
  11541.0    0.0000866   11439.18262   11440.03906
  11467.0    0.0000872   11432.72559   11433.53516
  11527.0    0.0000868   11426.27441   11427.04004
  11617.0    0.0000861   11419.82520   11420.54980
  11466.0    0.0000872   11413.38086   11414.06836
  11397.0    0.0000877   11406.93945   11407.59180
  11331.0    0.0000883   11400.50293   11401.12402
  11369.0    0.0000880   11394.06934   11394.65918
  11273.0    0.0000887   11387.63965   11388.20215
  11492.0    0.0000870   11381.21289   11381.75000
  11409.0    0.0000877   11374.78906   11375.30273
  11228.0    0.0000891   11368.37012   11368.86133
  11366.0    0.0000880   11361.95410   11362.42383
  11624.0    0.0000860   11355.54199   11355.54688
  11207.0    0.0000892   11349.13379   11349.13770
  11338.0    0.0000882   11342.72754   11342.73145
  11344.0    0.0000882   11336.32617   11336.33008
  11235.0    0.0000890   11329.92676   11329.93164
  11380.0    0.0000879   11323.53125   11323.53516
  11299.0    0.0000885   11317.14062   11317.14453
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  3717.0     0.0002690   3244.08276    3657.37305
  3684.0     0.0002714   3242.83057    3673.19385
  3669.0     0.0002726   3241.57642    3691.85278
  3681.0     0.0002717   3240.32129    3712.58057
  3795.0     0.0002635   3239.06470    3735.34863
  3714.0     0.0002693   3237.80640    3759.49023
  3751.0     0.0002666   3236.54712    3784.04590
  3812.0     0.0002623   3235.28564    3807.85718
  3893.0     0.0002569   3234.02319    3829.63672
  3706.0     0.0002698   3232.75903    3848.30420
  3828.0     0.0002612   3231.49365    3862.36694
  3712.0     0.0002694   3230.22632    3871.09766
  3886.0     0.0002573   3228.95776    3873.84277
  3957.0     0.0002527   3227.68774    3870.15747
  3985.0     0.0002509   3226.41577    3859.86499
  3936.0     0.0002541   3225.14233    3842.82031
  3847.0     0.0002599   3223.86694    3819.40796
  3875.0     0.0002581   3222.59082    3790.33301
  3809.0     0.0002625   3221.31201    3756.68066
  3729.0     0.0002682   3220.03223    3719.81689
  3802.0     0.0002630   3218.75098    3681.22217
  3737.0     0.0002676   3217.46729    3642.31885
  3691.0     0.0002709   3216.18237    3604.36426
  3569.0     0.0002802   3214.89526    3568.38306
  3622.0     0.0002761   3213.60693    3535.17114
  3509.0     0.0002850   3212.31641    3505.30176
  3610.0     0.0002770   3211.02441    3479.23828
  3433.0     0.0002913   3209.73047    3456.97095
  3458.0     0.0002892   3208.43481    3438.62085
  3345.0     0.0002990   3207.13745    3424.22290
  3420.0     0.0002924   3205.83789    3413.25928
  3379.0     0.0002959   3204.53662    3405.45728
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  3443.0     0.0002904   3201.92822    3397.88525
  3423.0     0.0002921   3200.62109    3396.95386
  3377.0     0.0002961   3199.31201    3397.08740
  3328.0     0.0003005   3198.00098    3397.61084
  3427.0     0.0002918   3196.68823    3397.84668
  3412.0     0.0002931   3195.37354    3397.29688
  3334.0     0.0002999   3194.05615    3395.20825
  3378.0     0.0002960   3192.73730    3391.55347
  3449.0     0.0002899   3191.41602    3386.06128
  3512.0     0.0002847   3190.09277    3378.93726
  3425.0     0.0002920   3188.76733    3370.53540
  3475.0     0.0002878   3187.44019    3361.24316
  3292.0     0.0003038   3186.11060    3351.45410
  3424.0     0.0002921   3184.77856    3341.52856
  3271.0     0.0003057   3183.44482    3331.77734
  3324.0     0.0003008   3182.10840    3322.45850
  3332.0     0.0003001   3180.77002    3313.76636
  3308.0     0.0003023   3179.42896    3305.84106
  3403.0     0.0002939   3178.08643    3298.78638
  3377.0     0.0002961   3176.74072    3292.67505
  3305.0     0.0003026   3175.39331    3287.51001
  3358.0     0.0002978   3174.04370    3283.29834
  3228.0     0.0003098   3172.69092    3280.29565
  3282.0     0.0003047   3171.33643    3277.97437
  3304.0     0.0003027   3169.97876    3276.58521
  3233.0     0.0003093   3168.61963    3276.13257
  3265.0     0.0003063   3167.25708    3276.60620
  3249.0     0.0003078   3165.89282    3277.99463
  3369.0     0.0002968   3164.52563    3280.28003
  3211.0     0.0003114   3163.15601    3283.42456
  3277.0     0.0003052   3161.78418    3287.31836
  3306.0     0.0003025   3160.40918    3291.99805
  3314.0     0.0003018   3159.03198    3297.31250
  3231.0     0.0003095   3157.65161    3303.14136
  3303.0     0.0003028   3156.26929    3309.59399
  3360.0     0.0002976   3154.88354    3316.07080
  3264.0     0.0003064   3153.49561    3322.68579
  3368.0     0.0002969   3152.10522    3329.33252
  3327.0     0.0003006   3150.71118    3335.91431
  3309.0     0.0003022   3149.31494    3342.32788
  3428.0     0.0002917   3147.91553    3348.46558
  3367.0     0.0002970   3146.51367    3354.10815
  3454.0     0.0002895   3145.10840    3359.13525
  3317.0     0.0003015   3143.70093    3363.32568
  3315.0     0.0003017   3142.28979    3366.84546
  3434.0     0.0002912   3140.87646    3369.65186
  3370.0     0.0002967   3139.45996    3371.87231
  3370.0     0.0002967   3138.04004    3373.73462
  3339.0     0.0002995   3136.61768    3375.50366
  3340.0     0.0002994   3135.19141    3377.34692
  3311.0     0.0003020   3133.76270    3379.51611
  3362.0     0.0002974   3132.33057    3382.20215
  3416.0     0.0002927   3130.89575    3385.58789
  3320.0     0.0003012   3129.45703    3389.79199
  3508.0     0.0002851   3128.01562    3394.91968
  3296.0     0.0003034   3126.57129    3400.99097
  3345.0     0.0002990   3125.12280    3408.12231
  3332.0     0.0003001   3123.67163    3415.80103
  3331.0     0.0003002   3122.21680    3423.98926
  3401.0     0.0002940   3120.75903    3432.45361
  3531.0     0.0002832   3119.29736    3441.00928
  3440.0     0.0002907   3117.83276    3449.51855
  3419.0     0.0002925   3116.36475    3457.94482
  3399.0     0.0002942   3114.89258    3466.25000
  3445.0     0.0002903   3113.41748    3474.41577
  3586.0     0.0002789   3111.93848    3482.36475
  3395.0     0.0002946   3110.45630    3490.00488
  3353.0     0.0002982   3108.96997    3497.17822
  3423.0     0.0002921   3107.48071    3503.85620
  3595.0     0.0002782   3105.98682    3509.59497
  3588.0     0.0002787   3104.48999    3514.13403
  3484.0     0.0002870   3102.98975    3517.00000
  3603.0     0.0002775   3101.48462    3517.72363
  3536.0     0.0002828   3099.97656    3515.85449
  3427.0     0.0002918   3098.46387    3511.29395
  3575.0     0.0002797   3096.94824    3504.10205
  3524.0     0.0002838   3095.42773    3494.57178
  3487.0     0.0002868   3093.90405    3483.23828
  3603.0     0.0002775   3092.37573    3470.75977
  3427.0     0.0002918   3090.84424    3457.78735
  3449.0     0.0002899   3089.30835    3444.90869
  3445.0     0.0002903   3087.76782    3432.53589
  3513.0     0.0002847   3086.22388    3421.01880
  3476.0     0.0002877   3084.67529    3410.26953
  3431.0     0.0002915   3083.12280    3400.29663
  3389.0     0.0002951   3081.56567    3390.81934
  3460.0     0.0002890   3080.00488    3381.50488
  3332.0     0.0003001   3078.43945    3371.99878
  3393.0     0.0002947   3076.86938    3362.03491
  3297.0     0.0003033   3075.29565    3351.52515
  3356.0     0.0002980   3073.71655    3340.57202
  3339.0     0.0002995   3072.13379    3329.50366
  3266.0     0.0003062   3070.54614    3318.64478
  3242.0     0.0003085   3068.95410    3308.50879
  3328.0    .            .             .
_pd_meas_number_of_points              5750
_pd_proc_number_of_points              5750

_reflns_number_total                   916
_reflns_limit_h_min                    0
_reflns_limit_h_max                    14
_reflns_limit_k_min                    0
_reflns_limit_k_max                    6
_reflns_limit_l_min                    -20
_reflns_limit_l_max                    18
_reflns_d_resolution_high              0.890
_reflns_d_resolution_low               12.518
#--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--#
