data_BA2PR2GE4O13_publ

_pd_block_id
  2021-05-26T14:29|BA2PR2GE4O13|Chufarov|Stadi-P

_audit_creation_method  "from EXP file using GSAS2CIF"
_audit_creation_date                   2021-05-26T14:29
_audit_author_name                     Chufarov
_audit_update_record
; 2021-05-26T14:29  Initial CIF as created by GSAS2CIF
;

#=============================================================================
# this information describes the project, paper etc. for the CIF             #
# Acta Cryst. Section C papers and editorial correspondence is generated     #
# from the information in this section                                       #
#                                                                            #
#   (from)   CIF submission form for Rietveld refinements (Acta Cryst. C)    #
#                                                 Version 14 December 1998   #
#=============================================================================
# 1. SUBMISSION DETAILS

_publ_contact_author_name            'Lipina, Olga Andreevna'
_publ_contact_author_address            
'Inst. of Solid State Chemistry UB RAS 91, Pervomaiskaya, Ekaterinburg Russia'
_publ_contact_author_email           'LipinaOlgaA@yandex.ru'
_publ_contact_author_fax             ?
_publ_contact_author_phone           '+7 952 143 0282'

_publ_contact_letter
; ?
;

_publ_requested_journal              'Dalton Transactions'
_publ_requested_coeditor_name        ?
_publ_requested_category             ?   # Acta C: one of CI/CM/CO/FI/FM/FO

#==============================================================================

# 2. PROCESSING SUMMARY (IUCr Office Use Only)

_journal_data_validation_number      ?

_journal_date_recd_electronic        ?
_journal_date_to_coeditor            ?
_journal_date_from_coeditor          ?
_journal_date_accepted               ?
_journal_date_printers_first         ?
_journal_date_printers_final         ?
_journal_date_proofs_out             ?
_journal_date_proofs_in              ?
_journal_coeditor_name               ?
_journal_coeditor_code               ?
_journal_coeditor_notes
; ?
;
_journal_techeditor_code             ?
_journal_techeditor_notes
; ?
;
_journal_coden_ASTM                  ?
_journal_name_full                   'Dalton Transactions'
_journal_year                        2021
_journal_volume                      ?
_journal_issue                       ?
_journal_page_first                  ?
_journal_page_last                   ?
_journal_paper_category              ?
_journal_suppl_publ_number           ?
_journal_suppl_publ_pages            ?

#==============================================================================

# 3. TITLE AND AUTHOR LIST

_publ_section_title   
;
Structural and spectroscopic characterization of new Ba2RE2Ge4O13 (RE = Pr, Nd, Gd, Dy) and Ba2Gd2-xEuxGe4O13 tetragermanates
;

_publ_section_title_footnote
; ?
;

# The loop structure below should contain the names and addresses of all
# authors, in the required order of publication. Repeat as necessary.

loop_
	_publ_author_name
	_publ_author_footnote
	_publ_author_address

'Lipina, Olga A.'
','
'Inst. of Solid State Chemistry, UB RAS, Pervomaiskaya 91, Ekaterinburg, Russia'

'Surat, Ludmila L.'
','
'Inst. of Solid State Chemistry, UB RAS, Pervomaiskaya 91, Ekaterinburg, Russia'

'Chufarov, Alexander Yu.'
','
'Inst. of Solid State Chemistry, UB RAS, Pervomaiskaya 91, Ekaterinburg, Russia'

'Tyutyunnik, Alexander P.'
','
'Inst. of Solid State Chemistry, UB RAS, Pervomaiskaya 91, Ekaterinburg, Russia'

'Enyashin, Andrey N.'
','
'Inst. of Solid State Chemistry, UB RAS, Pervomaiskaya 91, Ekaterinburg, Russia'

'Baklanova, Yana V.'
','
'Inst. of Solid State Chemistry, UB RAS, Pervomaiskaya 91, Ekaterinburg, Russia'

'Chvanova, Anastasia V.'
','
'Inst. of Solid State Chemistry, UB RAS, Pervomaiskaya 91, Ekaterinburg, Russia'

'Mironov, Leonid Yu.'
','
'ITMO University, Kronverksky Pr. 49, bldg. A, St. Petersburg, Russia'

'Belova, Ksenia G.'
','
;
Inst. of High Temperature Electrochemistry, Akademicheskaya 20, UB RAS,
Ekaterinburg, Russia
Inst. of Natural Sciences and Mathematics, Ural Federal University, 
48 Kuybisheva, Ekaterinburg, Russia
;

'Zubkov, Vladimir G.'
','
'Inst. of Solid State Chemistry, UB RAS, Pervomaiskaya 91, Ekaterinburg, Russia'

#==============================================================================

# 4. TEXT

_publ_section_synopsis
;  ?
;
_publ_section_abstract
; ?
;
_publ_section_comment
; ?
;
_publ_section_exptl_prep      # Details of the preparation of the sample(s)
                              # should be given here.
; ?
;
_publ_section_exptl_refinement
; ?
;
_publ_section_references
; ?
;
_publ_section_figure_captions
; ?
;
_publ_section_acknowledgements
; This work was supported by the Russian Science Foundation (Grant 19-73-00219)
;


#=============================================================================
# 5. OVERALL REFINEMENT & COMPUTING DETAILS

_refine_special_details
; ?
;
_pd_proc_ls_special_details
; ?
;

# The following items are used to identify the programs used.
_computing_molecular_graphics     'VESTA Ver. 3.4.4'
_computing_publication_material   ?

_refine_ls_weighting_scheme       ?
_refine_ls_weighting_details      ?
_refine_ls_hydrogen_treatment     ?
_refine_ls_extinction_method      ?
_refine_ls_extinction_coef        ?
_refine_ls_number_constraints     ?

_refine_ls_restrained_S_all       ?
_refine_ls_restrained_S_obs       ?

#==============================================================================
# 6. SAMPLE PREPARATION DATA

# (In the unusual case where multiple samples are used in a single
#  Rietveld study, this information should be moved into the phase
#  blocks)

# The following three fields describe the preparation of the material.
# The cooling rate is in K/min.  The pressure at which the sample was
# prepared is in kPa.  The temperature of preparation is in K.

_pd_prep_cool_rate                ?
_pd_prep_pressure                 ?
_pd_prep_temperature              ?

_pd_char_colour                   white       # use ICDD colour descriptions

_refine_ls_shift/su_max                0.04
_refine_ls_shift/su_mean               0.00
_computing_structure_refinement        GSAS
_refine_ls_number_parameters           69
_refine_ls_goodness_of_fit_all         1.29
_refine_ls_number_restraints           0
_refine_ls_matrix_type                 full
#==============================================================================
# 7. CHEMICAL, STRUCTURAL AND CRYSTAL DATA

_pd_char_particle_morphology      ?

_chemical_name_systematic         "Dibarium dipraseodymium(III) tetragermanate"
_chemical_name_common             "Barium Praseodymium Germanate"
_chemical_formula_moiety          ?
_chemical_formula_structural      "Ba2 Pr2 Ge4 O13"
_chemical_formula_analytical      ?
_chemical_melting_point           ?
_chemical_compound_source         ?       # for minerals and
                                          # natural products
_symmetry_space_group_name_Hall   "-C 2yc"

_exptl_crystal_F_000               ?
_exptl_crystal_density_diffrn      5.592
_exptl_crystal_density_meas        ?
_exptl_crystal_density_method      "not measured"

_cell_measurement_temperature     298(2)

_cell_special_details
; ?
;

_geom_special_details             ?

# The following item identifies the program(s) used (if appropriate).
_computing_structure_solution     
"GSAS (A.C. Larson and R.B. Von Dreele, 2004), EXPGUI (Toby, B.H., 2001)"

#==============================================================================

# 8. Phase information from GSAS




_pd_phase_name                         "BA2PR2GE4O13"
_cell_length_a                         13.28238(16)
_cell_length_b                         5.42142(7)
_cell_length_c                         18.05076(26)
_cell_angle_alpha                      90.0
_cell_angle_beta                       105.4404(7)
_cell_angle_gamma                      90.0
_cell_volume                           1252.91(4)
_symmetry_cell_setting                 monoclinic
_symmetry_space_group_name_H-M         "C 1 2/c 1"
loop_ _symmetry_equiv_pos_site_id _symmetry_equiv_pos_as_xyz
       1 +x,+y,+z 
       2 -x,+y,-z+1/2 
      -1 -x,-y,-z 
      -2 +x,-y,+z+1/2 
     101 +x+1/2,+y+1/2,+z 
     102 -x+1/2,+y+1/2,-z+1/2 
    -101 -x+1/2,-y+1/2,-z 
    -102 +x+1/2,-y+1/2,+z+1/2 

# ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS


loop_
      _atom_site_type_symbol
      _atom_site_label
      _atom_site_fract_x
      _atom_site_fract_y
      _atom_site_fract_z
      _atom_site_occupancy
      _atom_site_thermal_displace_type
      _atom_site_U_iso_or_equiv
      _atom_site_symmetry_multiplicity
Ba
Ba      0.15698(10)  0.5035(5)    0.33231(7)   1.0        Uiso   0.0263(6)     8
Pr
Pr      0.11713(10)  0.5112(4)    0.08758(7)   1.0        Uiso   0.0249(6)     8
Ge
Ge1     0.06606(18)  0.0463(7)    0.18570(15)  1.0        Uiso   0.0243(10)    8
Ge
Ge2    -0.11945(22) -0.0312(8)    0.04059(15)  1.0        Uiso   0.0233(9)     8
O 
O1      0.0752(11)  -0.2727(25)   0.1921(9)    1.0        Uiso   0.022(5)      8
O 
O2      0.1749(11)   0.2338(21)   0.1990(8)    1.0        Uiso   0.017(5)      8
O 
O3      0.0          0.1803(33)   0.25         1.0        Uiso   0.018(6)      4
O 
O4     -0.0178(11)   0.1732(22)   0.0951(7)    1.0        Uiso   0.014(4)      8
O 
O5     -0.1620(10)   0.1023(23)  -0.0482(8)    1.0        Uiso   0.027(5)      8
O 
O6     -0.2037(8)   -0.0428(34)   0.0983(6)    1.0        Uiso   0.028(5)      8
O 
O7     -0.0669(9)   -0.3419(24)   0.0346(7)    1.0        Uiso   0.022(5)      8
 
# If you change Z, be sure to change all 3 of the following
_chemical_formula_sum                  "Ba2 Ge4 O13 Pr2"
_chemical_formula_weight               1054.82
_cell_formula_units_Z                  4

# MOLECULAR GEOMETRY

loop_
      _geom_bond_atom_site_label_1
      _geom_bond_atom_site_label_2
      _geom_bond_distance
      _geom_bond_site_symmetry_1
      _geom_bond_site_symmetry_2
      _geom_bond_publ_flag
  Ba        O1               2.756(14)  .      1_565  N
  Ba        O1               3.233(14)  .      2_565  N
  Ba        O2               2.880(14)  .      1_555  N
  Ba        O2               2.745(13)  .    102_555  N
  Ba        O3               2.824(11)  .      1_555  N
  Ba        O4               3.103(13)  .      2_555  N
  Ba        O5               2.828(13)  .   -102_555  N
  Ba        O6               3.211(18)  .      2_555  N
  Ba        O6               2.755(17)  .      2_565  N
  Ba        O7               3.071(12)  .      2_565  N
  Pr        O1               2.409(14)  .      1_565  N
  Pr        O2               2.464(13)  .      1_555  N
  Pr        O4               2.592(14)  .      1_555  N
  Pr        O5               2.340(12)  .     -1_565  N
  Pr        O6               2.354(10)  .    101_555  N
  Pr        O7               2.506(13)  .      1_565  N
  Pr        O7               2.317(12)  .     -1_555  N
  Ge1       Ge2             3.1100(34)  .      1_555  N
  Ge1       O1               1.735(14)  .      1_555  N
  Ge1       O2               1.732(13)  .      1_555  N
  Ge1       O3                1.785(7)  .      1_555  N
  Ge1       O4               1.848(12)  .      1_555  N
  Ge2       Ge1             3.1100(34)  .      1_555  N
  Ge2       O4               1.820(13)  .      1_555  N
  Ge2       O5               1.712(13)  .      1_555  N
  Ge2       O6               1.722(10)  .      1_555  N
  Ge2       O7               1.838(13)  .      1_555  N

loop_
      _geom_angle_atom_site_label_1
      _geom_angle_atom_site_label_2
      _geom_angle_atom_site_label_3
      _geom_angle
      _geom_angle_site_symmetry_1
      _geom_angle_site_symmetry_2
      _geom_angle_site_symmetry_3
      _geom_angle_publ_flag
  O1        Ba        O2               63.65(33)      1_565  .      1_555  N
  O1        Ba        O2                 75.8(4)      1_565  .    102_555  N
  O1        Ba        O3                 74.6(4)      1_565  .      1_555  N
  O1        Ba        O4                120.5(4)      1_565  .      2_555  N
  O1        Ba        O5                146.8(4)      1_565  .   -102_555  N
  O1        Ba        O6                 90.6(4)      1_565  .      2_565  N
  O1        Ba        O7              117.22(34)      1_565  .      2_565  N
  O2        Ba        O2               78.82(29)      1_555  .    102_555  N
  O2        Ba        O3               57.26(29)      1_555  .      1_555  N
  O2        Ba        O4                104.5(4)      1_555  .      2_555  N
  O2        Ba        O5                106.9(4)      1_555  .   -102_555  N
  O2        Ba        O6              140.75(34)      1_555  .      2_565  N
  O2        Ba        O7                158.2(4)      1_555  .      2_565  N
  O2        Ba        O3              134.51(29)    102_555  .      1_555  N
  O2        Ba        O4              163.34(35)    102_555  .      2_555  N
  O2        Ba        O5                 71.1(4)    102_555  .   -102_555  N
  O2        Ba        O6               65.80(34)    102_555  .      2_565  N
  O2        Ba        O7                123.0(4)    102_555  .      2_565  N
  O3        Ba        O4               54.87(26)      1_555  .      2_555  N
  O3        Ba        O5                129.4(4)      1_555  .   -102_555  N
  O3        Ba        O6              146.99(34)      1_555  .      2_565  N
  O3        Ba        O7              101.18(26)      1_555  .      2_565  N
  O4        Ba        O5               92.43(30)      2_555  .   -102_555  N
  O4        Ba        O6              114.26(32)      2_555  .      2_565  N
  O4        Ba        O7               55.08(34)      2_555  .      2_565  N
  O5        Ba        O6                 78.0(4)   -102_555  .      2_565  N
  O5        Ba        O7               83.58(35)   -102_555  .      2_565  N
  O6        Ba        O7               59.23(32)      2_565  .      2_565  N
  O1        Pr        O2                 75.2(4)      1_565  .      1_555  N
  O1        Pr        O4                 89.7(4)      1_565  .      1_555  N
  O1        Pr        O5                 86.1(5)      1_565  .     -1_565  N
  O1        Pr        O6                115.8(5)      1_565  .    101_555  N
  O1        Pr        O7                 74.8(4)      1_565  .      1_565  N
  O1        Pr        O7                150.5(5)      1_565  .     -1_555  N
  O2        Pr        O4                 66.1(4)      1_555  .      1_555  N
  O2        Pr        O5                138.1(5)      1_555  .     -1_565  N
  O2        Pr        O6                 76.6(5)      1_555  .    101_555  N
  O2        Pr        O7                124.4(4)      1_555  .      1_565  N
  O2        Pr        O7                118.9(5)      1_555  .     -1_555  N
  O4        Pr        O5                152.2(4)      1_555  .     -1_565  N
  O4        Pr        O6                127.3(5)      1_555  .    101_555  N
  O4        Pr        O7                 68.1(4)      1_555  .      1_565  N
  O4        Pr        O7                 75.1(4)      1_555  .     -1_555  N
  O5        Pr        O6                 78.6(6)     -1_565  .    101_555  N
  O5        Pr        O7                 84.3(5)     -1_565  .      1_565  N
  O5        Pr        O7                 95.6(5)     -1_565  .     -1_555  N
  O6        Pr        O7                158.9(4)    101_555  .      1_565  N
  O6        Pr        O7                 93.3(4)    101_555  .     -1_555  N
  O7        Pr        O7                 76.0(5)      1_565  .     -1_555  N
  O1        Ge1       O2                122.3(8)      1_555  .      1_555  N
  O1        Ge1       O3                113.6(8)      1_555  .      1_555  N
  O1        Ge1       O4                116.4(7)      1_555  .      1_555  N
  O2        Ge1       O3                102.0(6)      1_555  .      1_555  N
  O2        Ge1       O4                100.8(7)      1_555  .      1_555  N
  O3        Ge1       O4                 98.0(5)      1_555  .      1_555  N
  O4        Ge2       O5                105.2(6)      1_555  .      1_555  N
  O4        Ge2       O6                101.7(6)      1_555  .      1_555  N
  O4        Ge2       O7                110.6(6)      1_555  .      1_555  N
  O5        Ge2       O6                118.5(6)      1_555  .      1_555  N
  O5        Ge2       O7                111.6(7)      1_555  .      1_555  N
  O6        Ge2       O7                108.7(7)      1_555  .      1_555  N
  Ge1       O3        Ge1              132.0(11)      1_555  .      2_555  N
  Ge1       O4        Ge2               115.9(7)      1_555  .      1_555  N

# Powder diffraction data for histogram  1
#==============================================================================
# 9. INSTRUMENT CHARACTERIZATION

_exptl_special_details
; ?
;

# if regions of the data are excluded, the reason(s) are supplied here:
_pd_proc_info_excluded_regions
; ?
;

# The following item is used to identify the equipment used to record
# the powder pattern when the diffractogram was measured at a laboratory
# other than the authors' home institution, e.g. when neutron or synchrotron
# radiation is used.

_pd_instr_location
; ?
;
_pd_calibration_special_details           # description of the method used
                                          # to calibrate the instrument
"external Si standard"

_diffrn_ambient_temperature       298
_diffrn_source                    "sealed X-ray tube"
_diffrn_source_target             Cu
_diffrn_source_type               "PHILIPS PW 2283/20"
_diffrn_measurement_device_type   "transmission diffractometer Stadi-P (STOE)"
_diffrn_detector                  "position sensitive detector"
_diffrn_detector_type             "linear mini-PSD (STOE)"
       # make or model of detector

_pd_meas_scan_method              step       # options are 'step', 'cont',
                                          # 'tof', 'fixed' or
                                          # 'disp' (= dispersive)
_pd_meas_special_details
;  ?
;

# The following two items identify the program(s) used (if appropriate).
_computing_data_collection        
"STOE Powder Software Package (STOE, Germany)"
_computing_data_reduction         
"STOE Powder Software Package (STOE, Germany)"

# Describe any processing performed on the data, prior to refinement.
# For example: a manual Lp correction or a precomputed absorption correction
_pd_proc_info_data_reduction      ?

# The following item is used for angular dispersive measurements only.

_diffrn_radiation_monochromator   "Primary, curved Ge 111"

# The following items are used to define the size of the instrument.
# Not all distances are appropriate for all instrument types.

_pd_instr_dist_src/mono           260
_pd_instr_dist_mono/spec          130
_pd_instr_dist_src/spec           ?
_pd_instr_dist_spec/anal          ?
_pd_instr_dist_anal/detc          ?
_pd_instr_dist_spec/detc          220

# 10. Specimen size and mounting information

# The next three fields give the specimen dimensions in mm.  The equatorial
# plane contains the incident and diffracted beam.

_pd_spec_size_axial               7       # perpendicular to
                                          # equatorial plane

_pd_spec_size_equat               0.1       # parallel to
                                          # scattering vector
                                          # in transmission

_pd_spec_size_thick               ?       # parallel to
                                          # scattering vector
                                          # in reflection

_pd_spec_mounting                         # This field should be
                                          # used to give details of the
                                          # container.
"powder on Mylar film"

_pd_spec_mount_mode               transmission       # options are 'reflection'
                                          # or 'transmission'

_pd_spec_shape                    flat_sheet       # options are 'cylinder'
                                          # 'flat_sheet' or 'irregular'







loop_ _atom_type_symbol
      _atom_type_number_in_cell
      _atom_type_scat_dispersion_real
      _atom_type_scat_dispersion_imag
      _atom_type_scat_Cromer_Mann_a1
      _atom_type_scat_Cromer_Mann_a2
      _atom_type_scat_Cromer_Mann_a3
      _atom_type_scat_Cromer_Mann_a4
      _atom_type_scat_Cromer_Mann_b1
      _atom_type_scat_Cromer_Mann_b2
      _atom_type_scat_Cromer_Mann_b3
      _atom_type_scat_Cromer_Mann_b4
      _atom_type_scat_Cromer_Mann_c
      _atom_type_scat_source
  Ba         8.0    0.000    0.000
 20.3361 3.21600 19.2970 0.27560 10.8880 20.2073 2.69590 167.202 2.77310 
  International_Tables_Vol_C
  Pr         8.0    0.000    0.000
 22.0440 2.77393 19.6697 0.22209 12.3856 16.7669 2.82428 143.644 2.05830 
  International_Tables_Vol_C
  Ge        16.0    0.000    0.000
 16.0816 2.85090 6.37470 0.25160 3.70680 11.4468 3.68300 54.7625 2.13130 
  International_Tables_Vol_C
  O         52.0    0.000    0.000
 3.04850 13.2771 2.28680 5.70110 1.54630 0.32390 0.86700 32.9089 0.25080 
  International_Tables_Vol_C
_diffrn_radiation_probe                x-ray
_diffrn_radiation_polarisn_ratio       0.8
_diffrn_radiation_wavelength           1.54056
_diffrn_radiation_type                 'Cu K\a~1~'
_pd_proc_ls_prof_R_factor              0.0155
_pd_proc_ls_prof_wR_factor             0.0198
_pd_proc_ls_prof_wR_expected           0.0155
_refine_ls_R_Fsqd_factor               0.02024

_pd_proc_ls_background_function
;   GSAS Background function number 1 with 16 terms.
 Shifted Chebyshev function of 1st kind
      1:    3879.15     2:   -2826.74     3:    1156.04     4:   -738.216    
      5:    209.786     6:   -22.3072     7:   -19.9144     8:    1.21828    
      9:    13.6987    10:   -30.5536    11:    38.3649    12:   -22.5625    
     13:    6.98545    14:   0.847730    15:    1.05683    16:   -5.89515    
;

_exptl_absorpt_process_details
;   GSAS Absorption/surface roughness correction: function number 4
 Flat plate transmission absorption correction
Terms =    -0.22028         0.0000    
Correction is not refined.
;
_exptl_absorpt_correction_T_min        1.40592
_exptl_absorpt_correction_T_max        2.09072
# Extinction correction
_gsas_exptl_extinct_corr_T_min         1.00000
_gsas_exptl_extinct_corr_T_max         1.00000

_pd_proc_ls_profile_function
;
 CW Profile function number 3 with  19 terms
 Pseudovoigt profile coefficients as parameterized in
 P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83.
 Asymmetry correction of L.W. Finger, D.E. Cox & A. P. Jephcoat (1994).
 J. Appl. Cryst.,27,892-900.
 #1(GU)   =   75.579 #2(GV)   =    0.000 #3(GW)   =   21.566
 #4(GP)   =    0.000 #5(LX)   =    2.578 #6(LY)   =    8.732
 #7(S/L)  =   0.0230 #8(H/L)  =   0.0230
 #9(trns) =     0.00 #10(shft)=   0.0000
 #11(stec)=     9.70 #12(ptec)=    -2.13 #13(sfec)=     0.00
 #14(L11) =    0.033 #15(L22) =    0.142 #16(L33) =    0.014
 #17(L12) =   -0.048 #18(L13) =    0.026 #19(L23) =   -0.037
 Peak tails are ignored  where the intensity is below 0.0010 times the peak
   Aniso. broadening axis   0.0   0.0   1.0
;
_pd_proc_ls_peak_cutoff 0.00100
_pd_proc_info_datetime                 2021-05-26T14:29:33
_pd_calc_method                        "Rietveld Refinement"

#---- raw/calc data loop -----
_pd_meas_2theta_range_min              5.0
_pd_meas_2theta_range_max              119.98
_pd_meas_2theta_range_inc              0.02
_pd_proc_2theta_range_min              4.98308
_pd_proc_2theta_range_max              119.96308
_pd_proc_2theta_range_inc              0.02

loop_
      _pd_meas_counts_total
      _pd_proc_ls_weight
      _pd_proc_intensity_bkg_calc
      _pd_calc_intensity_total
  8868.0     0.0001128   8929.37598   8929.37305
  8729.0     0.0001146   8919.12598   8919.12207
  8783.0     0.0001139   8908.93652   8908.93359
  9054.0     0.0001104   8898.80762   8898.80469
  9093.0     0.0001100   8888.73828   8888.73535
  8901.0     0.0001123   8878.72852   8878.72559
  8962.0     0.0001116   8868.77832   8868.77539
  8751.0     0.0001143   8858.88574   8858.88281
  8692.0     0.0001150   8849.05078   8849.04785
  8907.0     0.0001123   8839.27344   8839.27148
  9052.0     0.0001105   8829.55273   8829.55078
  8874.0     0.0001127   8819.88965   8819.88672
  8895.0     0.0001124   8810.28125   8810.27832
  8833.0     0.0001132   8800.72754   8800.72559
  8842.0     0.0001131   8791.23047   8791.22852
  8967.0     0.0001115   8781.78711   8781.78516
  8665.0     0.0001154   8772.39844   8772.39648
  8661.0     0.0001155   8763.06250   8763.06152
  8759.0     0.0001142   8753.78027   8753.77832
  8832.0     0.0001132   8744.55078   8744.54980
  8848.0     0.0001130   8735.37402   8735.37207
  8609.0     0.0001162   8726.24805   8726.24707
  8740.0     0.0001144   8717.17383   8717.17188
  8641.0     0.0001157   8708.15137   8708.14941
  8641.0     0.0001157   8699.17773   8699.17676
  8662.0     0.0001154   8690.25488   8690.25391
  8546.0     0.0001170   8681.38184   8681.38086
  8612.0     0.0001161   8672.55762   8672.55664
  8705.0     0.0001149   8663.78320   8663.78125
  8566.0     0.0001167   8655.05566   8655.05469
  8618.0     0.0001160   8646.37695   8646.37598
  8582.0     0.0001165   8637.74512   8637.74414
  8625.0     0.0001159   8629.16113   8629.16016
  8555.0     0.0001169   8620.62305   8620.62207
  8633.0     0.0001158   8612.13184   8612.13086
  8579.0     0.0001166   8603.68652   8603.68555
  8470.0     0.0001181   8595.28613   8595.28613
  8465.0     0.0001181   8586.93164   8586.93066
  8676.0     0.0001153   8578.62109   8578.62109
  8501.0     0.0001176   8570.35547   8570.35449
  8474.0     0.0001180   8562.13379   8562.13281
  8494.0     0.0001177   8553.95508   8553.95410
  8483.0     0.0001179   8545.81934   8545.81836
  8500.0     0.0001176   8537.72754   8537.72656
  8417.0     0.0001188   8529.67676   8529.67578
  8482.0     0.0001179   8521.66895   8521.66797
  8395.0     0.0001191   8513.70215   8513.70117
  8500.0     0.0001176   8505.77734   8505.77637
  8505.0     0.0001176   8497.89258   8497.89258
  8443.0     0.0001184   8490.04883   8490.04785
  8553.0     0.0001169   8482.24512   8482.24512
  8246.0     0.0001213   8474.48145   8474.48145
  8552.0     0.0001169   8466.75781   8466.75781
  8573.0     0.0001166   8459.07227   8459.07227
  8519.0     0.0001174   8451.42578   8451.42578
  8416.0     0.0001188   8443.81836   8443.81836
  8492.0     0.0001178   8436.24805   8436.24805
  8391.0     0.0001192   8428.71680   8428.71680
  8553.0     0.0001169   8421.22168   8421.22168
  8610.0     0.0001161   8413.76465   8413.76465
  8466.0     0.0001181   8406.34375   8406.34375
  8270.0     0.0001209   8398.95996   8398.95898
  8353.0     0.0001197   8391.61133   8391.61133
  8522.0     0.0001173   8384.29883   8384.29883
  8233.0     0.0001215   8377.02148   8377.02148
  8412.0     0.0001189   8369.78027   8369.78027
  8263.0     0.0001210   8362.57227   8362.57227
  8243.0     0.0001213   8355.40039   8355.40039
  8541.0     0.0001171   8348.26172   8348.26172
  8469.0     0.0001181   8341.15723   8341.15723
  8460.0     0.0001182   8334.08691   8334.08691
  8283.0     0.0001207   8327.04883   8327.04883
  8287.0     0.0001207   8320.04395   8320.04395
  8451.0     0.0001183   8313.07129   8313.07129
  8346.0     0.0001198   8306.13184   8306.13281
  8249.0     0.0001212   8299.22461   8299.22461
  8251.0     0.0001212   8292.34863   8292.34863
  8133.0     0.0001230   8285.50391   8285.50391
  8293.0     0.0001206   8278.69043   8278.69043
  8341.0     0.0001199   8271.90820   8271.90820
  8329.0     0.0001201   8265.15625   8265.15625
  8214.0     0.0001217   8258.43457   8258.43555
  8100.0     0.0001235   8251.74316   8251.74414
  8270.0     0.0001209   8245.08203   8245.08203
  8322.0     0.0001202   8238.45020   8238.45020
  8322.0     0.0001202   8231.84668   8231.84668
  8223.0     0.0001216   8225.27246   8225.27344
  8197.0     0.0001220   8218.72754   8218.72754
  8259.0     0.0001211   8212.21094   8212.21094
  8376.0     0.0001194   8205.72168   8205.72168
  8231.0     0.0001215   8199.26074   8199.26074
  8228.0     0.0001215   8192.82715   8192.82715
  8133.0     0.0001230   8186.42139   8186.42139
  8281.0     0.0001208   8180.04248   8180.04248
  8398.0     0.0001191   8173.69043   8173.69043
  8136.0     0.0001229   8167.36523   8167.36572
  8202.0     0.0001219   8161.06592   8161.06592
  8064.0     0.0001240   8154.79297   8154.79297
  8062.0     0.0001240   8148.54590   8148.54590
  8215.0     0.0001217   8142.32422   8142.32422
  8365.0     0.0001195   8136.12842   8136.12842
  8155.0     0.0001226   8129.95703   8129.95703
  7984.0     0.0001253   8123.81055   8123.81055
  8008.0     0.0001249   8117.68945   8117.68945
  8357.0     0.0001197   8111.59180   8111.59229
  8241.0     0.0001213   8105.51953   8105.51953
  8080.0     0.0001238   8099.47021   8099.47021
  8162.0     0.0001225   8093.44482   8093.44482
  8197.0     0.0001220   8087.44287   8087.44287
  8209.0     0.0001218   8081.46387   8081.46436
  8042.0     0.0001243   8075.50879   8075.50879
  8199.0     0.0001220   8069.57568   8069.57568
  8027.0     0.0001246   8063.66602   8063.66602
  8111.0     0.0001233   8057.77783   8057.77783
  8106.0     0.0001234   8051.91162   8051.91211
  8073.0     0.0001239   8046.06836   8046.06836
  8026.0     0.0001246   8040.24609   8040.24609
  8121.0     0.0001231   8034.44629   8034.44629
  8172.0     0.0001224   8028.66650   8028.66650
  8156.0     0.0001226   8022.90820   8022.90820
  7989.0     0.0001252   8017.17139   8017.17139
  7907.0     0.0001265   8011.45459   8011.45459
  7720.0     0.0001295   8005.75879   8005.75879
  8051.0     0.0001242   8000.08301   8000.08301
  8005.0     0.0001249   7994.42725   7994.42725
  7942.0     0.0001259   7988.79150   7988.79150
  7854.0     0.0001273   7983.17529   7983.17529
  7724.0     0.0001295   7977.57861   7977.57861
  8012.0     0.0001248   7972.00098   7972.00098
  8113.0     0.0001233   7966.44287   7966.44287
  7993.0     0.0001251   7960.90381   7960.90332
  8017.0     0.0001247   7955.38330   7955.38281
  7750.0     0.0001290   7949.88086   7949.88086
  8029.0     0.0001245   7944.39697   7944.39697
  8059.0     0.0001241   7938.93164   7938.93164
  7871.0     0.0001270   7933.48389   7933.48389
  7745.0     0.0001291   7928.05420   7928.05420
  8096.0     0.0001235   7922.64209   7922.64160
  7905.0     0.0001265   7917.24707   7917.24658
  8020.0     0.0001247   7911.86963   7911.86963
  7978.0     0.0001253   7906.50928   7906.50928
  7834.0     0.0001276   7901.16602   7901.16602
  7768.0     0.0001287   7895.83936   7895.83887
  8039.0     0.0001244   7890.52930   7890.52881
  7981.0     0.0001253   7885.23535   7885.23535
  7866.0     0.0001271   7879.95801   7879.95752
  7739.0     0.0001292   7874.69678   7874.69678
  7746.0     0.0001291   7869.45117   7869.45117
  7862.0     0.0001272   7864.22217   7864.22168
  7886.0     0.0001268   7859.00781   7859.00732
  7841.0     0.0001275   7853.80908   7853.80859
  7683.0     0.0001302   7848.62549   7848.62549
  7845.0     0.0001275   7843.45752   7843.45703
  7823.0     0.0001278   7838.30420   7838.30371
  7915.0     0.0001263   7833.16553   7833.16504
  7793.0     0.0001283   7828.04150   7828.04102
  7786.0     0.0001284   7822.93262   7822.93213
  7722.0     0.0001295   7817.83691   7817.83643
  7894.0     0.0001267   7812.75684   7812.75635
  7822.0     0.0001278   7807.68945   7807.68896
  7820.0     0.0001279   7802.63721   7802.63672
  7816.0     0.0001279   7797.59766   7797.59717
  7820.0     0.0001279   7792.57227   7792.57178
  7850.0     0.0001274   7787.56055   7787.55957
  7900.0     0.0001266   7782.56152   7782.56104
  7789.0     0.0001284   7777.57617   7777.57568
  7797.0     0.0001283   7772.60352   7772.60303
  7684.0     0.0001301   7767.64404   7767.64307
  7770.0     0.0001287   7762.69727   7762.69678
  7754.0     0.0001290   7757.76270   7757.76221
  7802.0     0.0001282   7752.84131   7752.84082
  7681.0     0.0001302   7747.93213   7747.93115
  7660.0     0.0001305   7743.03516   7743.03467
  7741.0     0.0001292   7738.14990   7738.14941
  7864.0     0.0001272   7733.27734   7733.27637
  7731.0     0.0001293   7728.41602   7728.41553
  7694.0     0.0001300   7723.56641   7723.56543
  7744.0     0.0001291   7718.72900   7718.72803
  7671.0     0.0001304   7713.90234   7713.90137
  7690.0     0.0001300   7709.08740   7709.08691
  7628.0     0.0001311   7704.28320   7704.28271
  7661.0     0.0001305   7699.49072   7699.48975
  7688.0     0.0001301   7694.70898   7694.70850
  7772.0     0.0001287   7689.93799   7689.93750
  7788.0     0.0001284   7685.17773   7685.17725
  7476.0     0.0001338   7680.42871   7680.42773
  7626.0     0.0001311   7675.68945   7675.68848
  7518.0     0.0001330   7670.96094   7670.96045
  7753.0     0.0001290   7666.24268   7666.24170
  7609.0     0.0001314   7661.53467   7661.53369
  7581.0     0.0001319   7656.83643   7656.83545
  7726.0     0.0001294   7652.14844   7652.14746
  7661.0     0.0001305   7647.46973   7647.46875
  7731.0     0.0001293   7642.80078   7642.79980
  7675.0     0.0001303   7638.14209   7638.14111
  7662.0     0.0001305   7633.49268   7633.49170
  7652.0     0.0001307   7628.85254   7628.85156
  7588.0     0.0001318   7624.22168   7624.22070
  7767.0     0.0001287   7619.59961   7619.59863
  7616.0     0.0001313   7614.98730   7614.98633
  7672.0     0.0001303   7610.38379   7610.38232
  7660.0     0.0001305   7605.78906   7606.14062
  7670.0     0.0001304   7601.20312   7601.56787
  7631.0     0.0001310   7596.62549   7597.00439
  7603.0     0.0001315   7592.05713   7592.45117
  7718.0     0.0001296   7587.49658   7587.90625
  7579.0     0.0001319   7582.94531   7583.37207
  7521.0     0.0001330   7578.40137   7578.84619
  7575.0     0.0001320   7573.86670   7574.33008
  7644.0     0.0001308   7569.33936   7569.82275
  7588.0     0.0001318   7564.81982   7565.32520
  7582.0     0.0001319   7560.30859   7560.83789
  7403.0     0.0001351   7555.80518   7556.35840
  7632.0     0.0001310   7551.30957   7551.88965
  7567.0     0.0001322   7546.82129   7547.43066
  7472.0     0.0001338   7542.34082   7542.98047
  7543.0     0.0001326   7537.86768   7538.54102
  7618.0     0.0001313   7533.40186   7534.11133
  7614.0     0.0001313   7528.94385   7529.69238
  7682.0     0.0001302   7524.49268   7525.28320
  7482.0     0.0001337   7520.04883   7520.88574
  7419.0     0.0001348   7515.61182   7516.49854
  7521.0     0.0001330   7511.18164   7512.12354
  7617.0     0.0001313   7506.75879   7507.76074
  7553.0     0.0001324   7502.34229   7503.41064
  7451.0     0.0001342   7497.93262   7499.07471
  7512.0     0.0001331   7493.52930   7494.75342
  7441.0     0.0001344   7489.13281   7490.44727
  7627.0     0.0001311   7484.74316   7486.15918
  7609.0     0.0001314   7480.35938   7481.89014
  7547.0     0.0001325   7475.98242   7477.64209
  7326.0     0.0001365   7471.61133   7473.41797
  7283.0     0.0001373   7467.24658   7469.22168
  7420.0     0.0001348   7462.88818   7465.05957
  7484.0     0.0001336   7458.53516   7460.93945
  7561.0     0.0001323   7454.18848   7456.88086
  7396.0     0.0001352   7449.84766   7452.91943
  7607.0     0.0001315   7445.51318   7449.12793
  7285.0     0.0001373   7441.18359   7445.63037
  7303.0     0.0001369   7436.86035   7442.62549
  7462.0     0.0001340   7432.54199   7440.37402
  7266.0     0.0001376   7428.22949   7439.17529
  7579.0     0.0001319   7423.92236   7439.29883
  7348.0     0.0001361   7419.62109   7440.92725
  7511.0     0.0001331   7415.32471   7444.13721
  7390.0     0.0001353   7411.03369   7448.95508
  7418.0     0.0001348   7406.74756   7455.43311
  7406.0     0.0001350   7402.46729   7463.72949
  7437.0     0.0001345   7398.19141   7474.17676
  7641.0     0.0001309   7393.92139   7487.37939
  7573.0     0.0001320   7389.65527   7504.33350
  7323.0     0.0001366   7385.39453   7526.56299
  7520.0     0.0001330   7381.13916   7556.05811
  7571.0     0.0001321   7376.88770   7594.65039
  7663.0     0.0001305   7372.64111   7642.41162
  7624.0     0.0001312   7368.39941   7695.29004
  7720.0     0.0001295   7364.16260   7743.32471
  7618.0     0.0001313   7359.92969   7771.51953
  7742.0     0.0001292   7355.70117   7764.74316
  7766.0     0.0001288   7351.47754   7716.67676
  7672.0     0.0001303   7347.25830   7637.77441
  7447.0     0.0001343   7343.04346   7549.82520
  7420.0     0.0001348   7338.83203   7471.84619
  7468.0     0.0001339   7334.62549   7413.27393
  7478.0     0.0001337   7330.42334   7374.62012
  7364.0     0.0001358   7326.22461   7351.23389
  7279.0     0.0001374   7322.03027   7337.33350
  7321.0     0.0001366   7317.83984   7328.40723
  7538.0     0.0001327   7313.65381   7321.77783
  7399.0     0.0001352   7309.47070   7316.14307
  7364.0     0.0001358   7305.29199   7310.95898
  7270.0     0.0001376   7301.11719   7306.01709
  7275.0     0.0001375   7296.94580   7301.23047
  7208.0     0.0001387   7292.77832   7296.55859
  7369.0     0.0001357   7288.61426   7291.97461
  7275.0     0.0001375   7284.45361   7287.45996
  7175.0     0.0001394   7280.29688   7283.00244
  7236.0     0.0001382   7276.14355   7278.59131
  7210.0     0.0001387   7271.99414   7274.21924
  7409.0     0.0001350   7267.84717   7269.87939
  7098.0     0.0001409   7263.70410   7265.56641
  7197.0     0.0001389   7259.56445   7261.27832
  7262.0     0.0001377   7255.42773   7257.00977
  7131.0     0.0001402   7251.29492   7252.75977
  7179.0     0.0001393   7247.16455   7248.52490
  7097.0     0.0001409   7243.03760   7244.30469
  7262.0     0.0001377   7238.91357   7240.09619
  7171.0     0.0001395   7234.79297   7235.89893
  7359.0     0.0001359   7230.67529   7231.71240
  7229.0     0.0001383   7226.56006   7227.53467
  7364.0     0.0001358   7222.44873   7223.36572
  7133.0     0.0001402   7218.33936   7219.20459
  7287.0     0.0001372   7214.23291   7215.05029
  7209.0     0.0001387   7210.13037   7210.90332
  7246.0     0.0001380   7206.02930   7206.76172
  7237.0     0.0001382   7201.93213   7202.62695
  7218.0     0.0001385   7197.83643   7198.49707
  6960.0     0.0001437   7193.74463   7194.37256
  7219.0     0.0001385   7189.65479   7190.25293
  7177.0     0.0001393   7185.56787   7186.13818
  7099.0     0.0001409   7181.48291   7182.02734
  7021.0     0.0001424   7177.40039   7177.92090
  7071.0     0.0001414   7173.32129   7173.81934
  7208.0     0.0001387   7169.24365   7169.72070
  7260.0     0.0001377   7165.16943   7165.62646
  7146.0     0.0001399   7161.09717   7161.53516
  7078.0     0.0001413   7157.02686   7157.44775
  7013.0     0.0001426   7152.95947   7153.36377
  7215.0     0.0001386   7148.89404   7149.28271
  7087.0     0.0001411   7144.83057   7145.20459
  7156.0     0.0001397   7140.77002   7141.13037
  6939.0     0.0001441   7136.71143   7137.05811
  7054.0     0.0001418   7132.65527   7132.98975
  7111.0     0.0001406   7128.60059   7128.92383
  7347.0     0.0001361   7124.54883   7124.54736
  7066.0     0.0001415   7120.49854   7120.49658
  7009.0     0.0001427   7116.45068   7116.44873
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  2202.0     0.000454    2010.88562   2222.51416
  2136.0     0.000468    2010.23328   2215.05786
  2237.0     0.000447    2009.57971   2207.95776
  2263.0     0.000442    2008.92529   2201.11426
  2178.0     0.000459    2008.26990   2194.49365
  2182.0     0.000458    2007.61389   2188.11011
  2196.0     0.000455    2006.95654   2182.03345
  2172.0     0.000460    2006.29858   2176.35913
  2206.0     0.000453    2005.63953   2171.20264
  2107.0     0.000475    2004.97974   2166.68457
  2214.0     0.000452    2004.31897   2162.90894
  2109.0     0.000474    2003.65710   2159.96094
  2195.0     0.000456    2002.99463   2157.70923
  2150.0     0.000465    2002.33093   2156.58032
  2194.0     0.000456    2001.66663   2156.38794
  2176.0     0.000460    2001.00122   2157.11035
  2145.0     0.000466    2000.33496   2158.69849
  2181.0     0.000459    1999.66760   2161.15210
  2239.0     0.000447    1998.99963   2164.20581
  2170.0     0.000461    1998.33069   2167.79077
  2198.0     0.000455    1997.66064   2171.73242
  2139.0     0.000468    1996.98987   2175.82520
  2189.0     0.000457    1996.31799   2179.84619
  2232.0     0.000448    1995.64539   2183.57153
  2286.0     0.000437    1994.97156   2186.78174
  2249.0     0.000445    1994.29724   2189.33301
  2200.0     0.000455    1993.62195   2191.09399
  2204.0     0.000454    1992.94543   2192.07080
  2159.0     0.000463    1992.26843   2192.33130
  2210.0     0.000452    1991.59009   2192.02051
  2226.0     0.000449    1990.91113   2191.32178
  2227.0     0.000449    1990.23096   2190.43506
  2180.0     0.000459    1989.55029   2189.55371
  2191.0     0.000456    1988.86841   2188.84351
  2222.0     0.000450    1988.18579   2188.43555
  2153.0     0.000464    1987.50232   2188.42261
  2206.0     0.000453    1986.81775   2188.86060
  2258.0     0.000443    1986.13245   2189.76978
  2321.0     0.000431    1985.44592   2191.18896
  2132.0     0.000469    1984.75903   2193.04443
  2130.0     0.000469    1984.07080   2195.30542
  2072.0     0.000483    1983.38184   2197.94409
  2236.0     0.000447    1982.69189   2200.90698
  2265.0     0.000442    1982.00122   2204.12354
  2106.0     0.000475    1981.30969   2207.57959
  2168.0     0.000461    1980.61707   2211.01978
  2185.0     0.000458    1979.92371   2214.38232
  2195.0     0.000456    1979.22925   2217.51660
  2198.0     0.000455    1978.53430   2220.25513
  2185.0     0.000458    1977.83801   2222.43457
  2232.0     0.000448    1977.14111   2223.90967
  2170.0     0.000461    1976.44336   2224.57520
  2180.0     0.000459    1975.74463   2224.38623
  2255.0     0.000443    1975.04517   2223.37476
  2198.0     0.000455    1974.34448   2221.62549
  2124.0     0.000471    1973.64331   2219.32739
  2225.0     0.000449    1972.94092   2216.60938
  2252.0     0.000444    1972.23804   2213.72119
  2213.0     0.000452    1971.53394   2210.80493
  2203.0     0.000454    1970.82935   2208.03271
  2175.0     0.000460    1970.12366   2205.50000
  2181.0     0.000459    1969.41699   2203.25220
  2224.0     0.000450    1968.70984   2201.30176
  2167.0     0.000461    1968.00146   2199.55811
  2257.0     0.000443    1967.29248   2197.94897
  2189.0     0.000457    1966.58240   2196.36206
  2169.0     0.000461    1965.87183   2194.68433
  2147.0     0.000466    1965.16003   2192.76807
  2221.0     0.000450    1964.44763   2190.51025
  2235.0     0.000447    1963.73462   2187.79614
  2117.0     0.000472    1963.02026   2184.53491
  2122.0     0.000471    1962.30542   2180.64966
  2106.0     0.000475    1961.58960   2176.07983
  2231.0     0.000448    1960.87305   2170.79565
  2234.0     0.000448    1960.15552   2164.80615
  2125.0     0.000471    1959.43738   2158.15698
  2180.0     0.000459    1958.71851   2150.93970
  2091.0     0.000478    1957.99841   2143.27441
  2187.0     0.000457    1957.27783   2135.30981
  2048.0     0.000488    1956.55627   2127.20630
  2104.0     0.000475    1955.83411   2119.12085
  2068.0     0.000484    1955.11084   2111.20605
  2072.0     0.000483    1954.38721   2103.58936
  2082.0     0.000480    1953.66235   2096.38354
  2132.0     0.000469    1952.93689   2089.67822
  2035.0     0.000491    1952.21094   2083.53540
  2048.0     0.000488    1951.48376   2078.00317
  2110.0     0.000474    1950.75598   2073.10620
  2105.0     0.000475    1950.02722   2068.85278
  2015.0     0.000496    1949.29810   2065.24390
  2075.0     0.000482    1948.56775   2062.26270
  2073.0     0.000482    1947.83704   2059.88916
  2040.0     0.000490    1947.10522   2058.10132
  2079.0     0.000481    1946.37305   2056.87354
  2081.0     0.000481    1945.63989   2056.19043
  2080.0     0.000481    1944.90588   2056.06860
  2021.0     0.000495    1944.17151   2056.43555
  2024.0     0.000494    1943.43591   2057.32544
  2060.0     0.000485    1942.69995   2058.74121
  2091.0     0.000478    1941.96289   2060.68921
  2034.0     0.000492    1941.22559   2063.17725
  2065.0     0.000484    1940.48730   2066.21094
  2083.0     0.000480    1939.74817   2069.79980
  2104.0     0.000475    1939.00867   2073.95630
  2091.0     0.000478    1938.26819   2078.69800
  2039.0     0.000490    1937.52710   2084.04370
  2121.0     0.000471    1936.78528   2089.56104
  2105.0     0.000475    1936.04285   2096.16602
  2171.0     0.000461    1935.29944   2103.41162
  2090.0     0.000478    1934.55579   2111.29321
  2119.0     0.000472    1933.81140   2119.77393
  2120.0     0.000472    1933.06592   2128.80225
  2162.0     0.000463    1932.32019   2138.29102
  2230.0     0.000448    1931.57361   2148.11060
  2247.0     0.000445    1930.82642   2158.12769
  2218.0     0.000451    1930.07849   2168.06812
  2209.0     0.000453    1929.33020   2177.71753
  2237.0     0.000447    1928.58081   2186.79443
  2175.0     0.000460    1927.83118   2195.00757
  2217.0     0.000451    1927.08093   2202.06250
  2178.0     0.000459    1926.32971   2207.70117
  2200.0     0.000455    1925.57812   2211.71240
  2241.0     0.000446    1924.82568   2213.96216
  2224.0     0.000450    1924.07300   2214.39673
  2194.0     0.000456    1923.31946   2213.04077
  2146.0     0.000466    1922.56543   2210.01270
  2106.0     0.000475    1921.81091   2205.45972
  2222.0     0.000450    1921.05554   2199.61621
  2165.0     0.000462    1920.29980   2192.73340
  2142.0     0.000467    1919.54321   2185.17651
  2065.0     0.000484    1918.78638   2177.04272
  2196.0     0.000455    1918.02869   2168.68530
  2138.0     0.000468    1917.27063   2160.33862
  2142.0     0.000467    1916.51196   2152.21631
  2203.0     0.000454    1915.75293   2144.44116
  2156.0     0.000464    1914.99316   2137.14453
  2175.0     0.000460    1914.23279   2130.36719
  2160.0     0.000463    1913.47217   2124.13623
  2184.0     0.000458    1912.71069   2118.39233
  2192.0     0.000456    1911.94897   2113.06836
  2051.0     0.000488    1911.18665   2108.05127
  2081.0     0.000481    1910.42383   2103.20874
  2048.0     0.000488    1909.66040   2098.41162
  2112.0     0.000473    1908.89673   2093.50415
  2028.0     0.000493    1908.13257   2088.39966
  2079.0     0.000481    1907.36755   2083.07446
  2035.0     0.000491    1906.60254   2077.47290
  2046.0     0.000489    1905.83667   2071.72119
  2076.0     0.000482    1905.07068   2065.79810
  1995.0     0.000501    1904.30383   2059.86230
  2035.0     0.000491    1903.53699   2054.02173
  2079.0     0.000481    1902.76965   2048.38037
  2075.0     0.000482    1902.00159   2043.02307
  2079.0     0.000481    1901.23340   2038.01892
  1994.0     0.000502    1900.46448   2033.41113
  1957.0     0.000511    1899.69543   2029.22302
  2062.0     0.000485    1898.92578   2025.45776
  2097.0     0.000477    1898.15601   2022.10376
  2023.0     0.000494    1897.38550   2019.12268
  2019.0     0.000495    1896.61487   2016.47205
  2008.0     0.000498    1895.84399   2014.09741
  2012.0     0.000497    1895.07239   2011.93347
  2048.0     0.000488    1894.30078   2009.91870
  2007.0     0.000498    1893.52844   2007.98694
  2024.0     0.000494    1892.75610   2006.08142
  2089.0     0.000479    1891.98315   2004.15417
  1984.0     0.000504    1891.21008   2002.16797
  2111.0     0.000474    1890.43652   2000.17871
  2073.0     0.000482    1889.66284   1998.00916
  2092.0     0.000478    1888.88879   1995.75769
  2017.0     0.000496    1888.11438   1993.46228
  2041.0     0.000490    1887.33984   1991.02673
  1965.0     0.000509    1886.56458   1988.53833
  2041.0     0.000490    1885.78955   1986.02039
  1905.0     0.000525    1885.01392   1983.49780
  1919.0     0.000521    1884.23828   1980.99426
  1968.0     0.000508    1883.46228   1978.52954
  1961.0     0.000510    1882.68591   1976.12854
  2009.0     0.000498    1881.90955   1973.80920
  2014.0     0.000497    1881.13269   1971.72620
  1899.0     0.000527    1880.35583   1969.64917
  1856.0     0.000539    1879.57849   1967.74207
  1855.0     0.000539    1878.80127   1966.10449
  2031.0     0.000492    1878.02344   1964.66528
  1891.0     0.000529    1877.24585   1963.53284
  1998.0     0.000501    1876.46802   1962.75671
  1978.0     0.000506    1875.68970   1962.38696
  1965.0     0.000509    1874.91162   1962.47449
  1982.0     0.000505    1874.13293   1963.06165
  2010.0     0.000498    1873.35437   1964.19604
  1956.0     0.000511    1872.57544   1965.89880
  1895.0     0.000528    1871.79675   1968.20496
  2012.0     0.000497    1871.01758   1971.13550
  2018.0     0.000496    1870.23853   1974.70471
  1980.0     0.000505    1869.45935   1978.91711
  1979.0     0.000505    1868.67981   1983.76819
  2039.0     0.000490    1867.90051   1989.24829
  1998.0     0.000501    1867.12085   1995.33533
  2022.0     0.000495    1866.34131   2002.00281
  1998.0     0.000501    1865.56140   2009.25867
  2034.0     0.000492    1864.78162   2016.97168
  2042.0     0.000490    1864.00195   2025.12891
  2076.0     0.000482    1863.22192   2033.68469
  2097.0     0.000477    1862.44202   2042.44922
  2040.0     0.000490    1861.66199   2051.40747
  2054.0     0.000487    1860.88208   2060.35864
  2093.0     0.000478    1860.10193   2068.98193
  2108.0     0.000474    1859.32202   2077.61304
  2182.0     0.000458    1858.54187   2085.92139
  2063.0     0.000485    1857.76184   2093.82764
  2078.0     0.000481    1856.98206   2101.28516
  2037.0     0.000491    1856.20190   2108.26758
  2205.0     0.000454    1855.42200   2114.75830
  2124.0     0.000471    1854.64185   2120.74609
  2198.0     0.000455    1853.86218   2126.19995
  2034.0     0.000492    1853.08215   2131.15698
  2177.0     0.000459    1852.30237   2135.41626
  2189.0     0.000457    1851.52246   2138.99634
  2179.0     0.000459    1850.74304   2141.82983
  2142.0     0.000467    1849.96350   2143.85059
  2091.0     0.000478    1849.18384   2144.96582
  2137.0     0.000468    1848.40466   2145.07788
  2136.0     0.000468    1847.62524   2144.07031
  2154.0     0.000464    1846.84619   2141.84253
  2125.0     0.000471    1846.06689   2138.39771
  2136.0     0.000468    1845.28821   2133.33032
  2146.0     0.000466    1844.50952   2126.78516
  2132.0     0.000469    1843.73071   2118.80176
  2091.0     0.000478    1842.95239   2109.49341
  2108.0     0.000474    1842.17383   2099.04712
  2091.0     0.000478    1841.39575   2087.69922
  2028.0     0.000493    1840.61768   2075.70850
  2017.0     0.000496    1839.83997   2063.34741
  2065.0     0.000484    1839.06213   2050.86963
  2061.0     0.000485    1838.28491   2038.50061
  1978.0     0.000506    1837.50769   2026.43835
  1988.0     0.000503    1836.73047   2014.84070
  2036.0     0.000491    1835.95386   2003.83386
  2016.0     0.000496    1835.17712   1993.50598
  1924.0     0.000520    1834.40076   1983.92676
  2003.0     0.000499    1833.62451   1975.12976
  1902.0     0.000526    1832.84875   1967.13574
  1991.0     0.000502    1832.07300   1959.94275
  1985.0     0.000504    1831.29761   1953.53760
  1883.0     0.000531    1830.52271   1947.88782
  1923.0     0.000520    1829.74768   1943.29846
  1846.0     0.000542    1828.97314   1939.03845
  1959.0     0.000510    1828.19873   1935.40491
  1968.0     0.000508    1827.42493   1932.33252
  1985.0     0.000504    1826.65100   1929.83862
  1911.0     0.000523    1825.87769   1927.75732
  1943.0     0.000515    1825.10474   1926.10645
  1916.0     0.000522    1824.33179   1924.76135
  1915.0     0.000522    1823.55933   1923.96826
  1916.0     0.000522    1822.78699   1923.49622
  1942.0     0.000515    1822.01538   1923.41626
  1912.0     0.000523    1821.24377   1923.74976
  1922.0     0.000520    1820.47266   1924.53040
  1909.0     0.000524    1819.70178   1925.79822
  1969.0     0.000508    1818.93140   1927.60828
  1952.0     0.000512    1818.16150   1930.01331
  1904.0     0.000525    1817.39172   1933.07312
  1953.0     0.000512    1816.62244   1936.83911
  2027.0     0.000493    1815.85327   1941.36157
  1865.0     0.000536    1815.08472   1946.68250
  2032.0     0.000492    1814.31641   1952.85376
  1921.0     0.000521    1813.54871   1959.84912
  2058.0     0.000486    1812.78113   1967.69275
  1987.0     0.000503    1812.01428   1976.36426
  2006.0     0.000499    1811.24768   1985.82751
  2034.0     0.000492    1810.48132   1996.01782
  1969.0     0.000508    1809.71570   2006.84644
  2072.0     0.000483    1808.95020   2018.18884
  2068.0     0.000484    1808.18530   2029.88660
  2084.0     0.000480    1807.42053   2041.74414
  2085.0     0.000480    1806.65662   2053.53271
  2104.0     0.000475    1805.89294   2064.97925
  2093.0     0.000478    1805.12952   2075.79297
  2121.0     0.000471    1804.36694   2085.66455
  2153.0     0.000464    1803.60437   2094.32422
  2119.0     0.000472    1802.84253   2101.43652
  2029.0     0.000493    1802.08081   2106.81982
  2138.0     0.000468    1801.32007   2110.33472
  2055.0     0.000487    1800.55933   2111.93799
  2066.0     0.000484    1799.79919   2111.68872
  2084.0     0.000480    1799.03979   2109.66406
  2027.0     0.000493    1798.28040   2106.03687
  2042.0     0.000490    1797.52161   2100.99219
  2123.0     0.000471    1796.76318   2094.70361
  2029.0     0.000493    1796.00562   2087.33203
  2052.0     0.000487    1795.24805   2078.81421
  2001.0     0.000500    1794.49121   2069.68799
  2083.0     0.000480    1793.73474   2059.81909
  2059.0     0.000486    1792.97888   2049.35059
  2043.0     0.000489    1792.22339   2038.41223
  1982.0     0.000505    1791.46838   2027.15234
  2072.0     0.000483    1790.71387   2015.73376
  1978.0     0.000506    1789.95959   2004.32568
  1965.0     0.000509    1789.20630   1993.09741
  1994.0     0.000502    1788.45288   1982.20654
  2000.0     0.000500    1787.70032   1971.79614
  1996.0     0.000501    1786.94824   1961.98804
  1973.0     0.000507    1786.19641   1952.88354
  1918.0     0.000521    1785.44531   1944.56067
  1930.0     0.000518    1784.69434   1937.08081
  1916.0     0.000522    1783.94421   1930.48413
  2037.0     0.000491    1783.19409   1924.80078
  1919.0     0.000521    1782.44482   1920.04333
  1876.0     0.000533    1781.69568   1916.22290
  1941.0     0.000515    1780.94739   1913.33362
  1873.0     0.000534    1780.19946   1911.36670
  1930.0     0.000518    1779.45178   1910.30676
  1916.0     0.000522    1778.70483   1910.13452
  1928.0     0.000519    1777.95801   1910.86682
  1952.0     0.000512    1777.21179   1912.38550
  1891.0     0.000529    1776.46582   1914.69507
  1924.0     0.000520    1775.72070   1917.75171
  1913.0     0.000523    1774.97546   1921.50623
  2047.0     0.000489    1774.23108   1925.89893
  1948.0     0.000513    1773.48718   1930.86365
  1898.0     0.000527    1772.74341   1936.32349
  2075.0     0.000482    1772.00012   1942.19275
  1942.0     0.000515    1771.25720   1948.37268
  2002.0     0.000500    1770.51489   1954.75269
  1917.0     0.000522    1769.77258   1961.24207
  1948.0     0.000513    1769.03101   1967.65515
  1974.0     0.000507    1768.28992   1973.88757
  1889.0     0.000529    1767.54883   1979.80518
  1968.0     0.000508    1766.80823   1985.28271
  2021.0     0.000495    1766.06799   1990.20703
  2022.0     0.000495    1765.32812   1994.47900
  2023.0     0.000494    1764.58850   1998.02515
  2016.0     0.000496    1763.84949   2000.80591
  2005.0     0.000499    1763.11035   2002.81934
  2014.0     0.000497    1762.37195   2004.12891
  1956.0     0.000511    1761.63379   2004.74866
  1998.0     0.000501    1760.89563   2004.82690
  1945.0     0.000514    1760.15808   2004.50757
  2007.0     0.000498    1759.42041   2003.94702
  1968.0     0.000508    1758.68347   2003.30737
  1952.0     0.000512    1757.94641   2002.74146
  1994.0     0.000502    1757.20984   2002.37378
  1992.0     0.000502    1756.47314   2002.30688
  2053.0     0.000487    1755.73706   2002.62354
  2032.0     0.000492    1755.00110   2003.37598
  2019.0     0.000495    1754.26514   2004.59558
  1929.0     0.000518    1753.52954   2006.29517
  2054.0     0.000487    1752.79382   2008.46326
  2001.0     0.000500    1752.05859   2011.08264
  1981.0     0.000505    1751.32324   2014.10938
  1917.0     0.000522    1750.58813   2017.51086
  2025.0     0.000494    1749.85315   2021.07629
  2007.0     0.000498    1749.11804   2024.96545
  2069.0     0.000483    1748.38330   2028.96545
  2010.0     0.000498    1747.64832   2032.97827
  2025.0     0.000494    1746.91357   2036.86194
  2060.0     0.000485    1746.17871   2040.38220
  2033.0     0.000492    1745.44385   2043.40356
  1978.0     0.000506    1744.70886   2045.73230
  2050.0     0.000488    1743.97412   2047.16980
  2066.0     0.000484    1743.23926   2047.52441
  2102.0     0.000476    1742.50403   2046.63477
  2089.0     0.000479    1741.76917   2044.39026
  2098.0     0.000477    1741.03369   2040.74109
  1988.0     0.000503    1740.29834   2035.71167
  2010.0     0.000498    1739.56250   2029.39929
  2037.0     0.000491    1738.82690   2021.96509
  1994.0     0.000502    1738.09082   2013.61877
  2065.0     0.000484    1737.35461   2004.58899
  2076.0     0.000482    1736.61829   1995.11548
  1995.0     0.000501    1735.88135   1985.46863
  1974.0     0.000507    1735.14429   1975.75244
  2084.0     0.000480    1734.40674   1966.18640
  1907.0     0.000524    1733.66907   1956.91028
  2043.0     0.000489    1732.93066   1948.00391
  1935.0     0.000517    1732.19214   1939.53967
  1974.0     0.000507    1731.45325   1931.54700
  1927.0     0.000519    1730.71362   1924.02808
  1886.0     0.000530    1729.97363   1916.97534
  1887.0     0.000530    1729.23291   1910.31824
  1883.0     0.000531    1728.49194   1904.09460
  1886.0     0.000530    1727.75000   1898.07678
  1907.0     0.000524    1727.00781   1892.29626
  1939.0     0.000516    1726.26465   1886.68542
  1887.0     0.000530    1725.52112   1881.22839
  1806.0     0.000554    1724.77673   1875.89771
  1899.0     0.000527    1724.03149   1870.70337
  1830.0     0.000546    1723.28564   1865.64453
  1814.0     0.000551    1722.53857   1860.75574
  1801.0     0.000555    1721.79102   1856.06982
  1824.0     0.000548    1721.04248   1851.62097
  1855.0     0.000539    1720.29297   1847.43250
  1845.0     0.000542    1719.54236   1843.52832
  1791.0     0.000558    1718.79114   1839.92578
  1806.0     0.000554    1718.03870   1836.61584
  1875.0     0.000533    1717.28491   1833.60400
  1853.0     0.000540    1716.53040   1830.88379
  1827.0     0.000547    1715.77429   1828.44739
  1892.0     0.000529    1715.01733   1826.24731
  1848.0     0.000541    1714.25879   1824.35742
  1864.0     0.000536    1713.49927   1822.74353
  1740.0     0.000575    1712.73840   1821.41541
  1853.0     0.000540    1711.97583   1820.38916
  1774.0     0.000564    1711.21228   1819.69641
  1753.0     0.000570    1710.44678   1819.45129
  1785.0     0.000560    1709.68005   1819.52820
  1843.0     0.000543    1708.91150   1820.05078
  1780.0     0.000562    1708.14172   1821.05969
  1830.0     0.000546    1707.36987   1822.59424
  1867.0     0.000536    1706.59656   1824.68701
  1815.0     0.000551    1705.82166   1827.36719
  1864.0     0.000536    1705.04443   1830.65295
  1841.0     0.000543    1704.26575   1834.56140
  1843.0     0.000543    1703.48474   1839.04797
  1794.0     0.000557    1702.70227   1844.20862
  1880.0     0.000532    1701.91736   1849.99268
  1852.0     0.000540    1701.13049   1856.36145
  1890.0     0.000529    1700.34143   1863.29175
  1813.0     0.000552    1699.55042   1870.73682
  1900.0     0.000526    1698.75696   1878.63391
  1907.0     0.000524    1697.96118   1886.89905
  1920.0     0.000521    1697.16309   1895.44800
  1969.0     0.000508    1696.36230   1904.12341
  1901.0     0.000526    1695.55945   1912.79822
  1944.0     0.000514    1694.75354   1921.30225
  1883.0     0.000531    1693.94531   1929.52539
  1914.0     0.000522    1693.13452   1937.09351
  1919.0     0.000521    1692.32068   1943.85986
  1952.0     0.000512    1691.50415   1949.59900
  1996.0     0.000501    1690.68457   1954.09619
  1968.0     0.000508    1689.86230   1957.17700
  1971.0     0.000507    1689.03674   1958.71936
  1961.0     0.000510    1688.20825   1958.67798
  2020.0     0.000495    1687.37634   1957.08093
  1994.0     0.000502    1686.54163   1954.02942
  1921.0     0.000521    1685.70349   1949.68323
  1956.0     0.000511    1684.86157   1944.23853
  1937.0     0.000516    1684.01672   1937.91846
  1908.0     0.000524    1683.16785   1930.94434
  1901.0     0.000526    1682.31567   1923.52991
  1818.0     0.000550    1681.45947   1915.87646
  1895.0     0.000528    1680.59998   1908.16162
  1848.0     0.000541    1679.73621   1900.54993
  1898.0     0.000527    1678.86865   1893.18799
  1910.0     0.000524    1677.99731   1886.20142
  1794.0     0.000557    1677.12146   1879.69385
  1866.0     0.000536    1676.24170   1873.75549
  1846.0     0.000542    1675.35754   1868.44800
  1871.0     0.000534    1674.46912   1863.81128
  1884.0     0.000531    1673.57593   1859.86011
  1893.0     0.000528    1672.67871   1856.58618
  1834.0     0.000545    1671.77661   1853.95435
  1862.0     0.000537    1670.86963   1851.91052
  1811.0     0.000552    1669.95801   1850.38135
  1864.0     0.000536    1669.04138   1849.27490
  1811.0     0.000552    1668.11987   1848.48853
  1872.0     0.000534    1667.19299   1847.91516
  1805.0     0.000554    1666.26123   1847.44995
  1798.0     0.000556    1665.32385   1846.99292
  1856.0     0.000539    1664.38135   1846.46558
  1785.0     0.000560    1663.43347   1845.80981
  1780.0     0.000562    1662.47949   1844.98987
  1830.0     0.000546    1661.52026   1843.99438
  1863.0     0.000537    1660.55469   1842.82739
  1818.0     0.000550    1659.58386   1841.50269
  1815.0     0.000551    1658.60632   1840.03125
  1806.0     0.000554    1657.62317   1838.41772
  1831.0     0.000546    1656.63330   1836.65808
  1856.0     0.000539    1655.63757   1834.74023
  1931.0     0.000518    1654.63525   1832.64453
  1865.0     0.000536    1653.62598   1830.35559
  1833.0     0.000546    1652.61047   1827.87231
  1834.0     0.000545    1651.58752   1825.20593
  1810.0     0.000552    1650.55811   1822.39453
  1854.0     0.000539    1649.52148   1819.50037
  1870.0     0.000535    1648.47778   1816.60291
  1828.0     0.000547    1647.42676   1813.80017
  1799.0     0.000556    1646.36792   1811.19397
  1802.0     0.000555    1645.30200   1808.88367
  1804.0     0.000554    1644.22791   1806.96582
  1884.0     0.000531    1643.14636   1805.52380
  1842.0     0.000543    1642.05664   1804.62329
  1849.0     0.000541    1640.95898   1804.32263
  1799.0    .            .            .
_pd_meas_number_of_points              5750
_pd_proc_number_of_points              5750

_reflns_number_total                   923
_reflns_limit_h_min                    0
_reflns_limit_h_max                    15
_reflns_limit_k_min                    0
_reflns_limit_k_max                    6
_reflns_limit_l_min                    -20
_reflns_limit_l_max                    20
_reflns_d_resolution_high              0.890
_reflns_d_resolution_low               8.700
#--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--#
