# Electronic Supplementary Material (ESI) for Dalton Transactions.
# This journal is © The Royal Society of Chemistry 2021

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_rbpbocl
_database_code_depnum_ccdc_archive 'CCDC 2101780'
loop_
_audit_author_name
_audit_author_address
'zhongxu Fan' 'Xinjiang University'
_audit_update_record             
;
2021-08-06 deposited with the CCDC.	2021-09-01 downloaded from the CCDC.
;
_audit_creation_date             2021-08-06
_audit_creation_method           
;
Olex2 1.2
(compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506)
;
_shelx_SHELXL_version_number     2016/6
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         '0.5(Cl18 O8 Pb16 Rb2)'
_chemical_formula_sum            'Cl9 O4 Pb8 Rb'
_chemical_formula_weight         2126.04
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pb Pb -3.3944 10.1111 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Rb Rb -0.9393 2.9676 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      tetragonal
_space_group_IT_number           85
_space_group_name_H-M_alt        'P 4/n'
_space_group_name_Hall           '-P 4a'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, -y+1/2, z'
'-y+1/2, x, z'
'y, -x+1/2, z'
'-x, -y, -z'
'x-1/2, y-1/2, -z'
'y-1/2, -x, -z'
'-y, x-1/2, -z'

_cell_length_a                   11.9557(3)
_cell_length_b                   11.9557(3)
_cell_length_c                   7.9620(4)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_volume                     1138.08(8)
_cell_formula_units_Z            2
_cell_measurement_reflns_used    3776
_cell_measurement_temperature    293
_cell_measurement_theta_max      32.19
_cell_measurement_theta_min      2.56
_shelx_estimated_absorpt_T_max   0.213
_shelx_estimated_absorpt_T_min   0.046
_exptl_absorpt_coefficient_mu    62.128
_exptl_absorpt_correction_T_max  0.0393
_exptl_absorpt_correction_T_min  0.0049
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
'SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1458 before and 0.0898 after correction. The Ratio of minimum to maximum transmission is 0.1247. The λ/2 correction factor is Not present.'
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            'clear light colourless'
_exptl_crystal_colour_lustre     clear
_exptl_crystal_colour_modifier   light
_exptl_crystal_colour_primary    colourless
_exptl_crystal_density_diffrn    6.204
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             1756
loop_
_exptl_crystal_face_index_h
_exptl_crystal_face_index_k
_exptl_crystal_face_index_l
_exptl_crystal_face_perp_dist
-1.00 0.00 1.00 0.0460
0.00 1.00 2.00 0.0620
2.00 -1.00 -1.00 0.0650
2.00 1.00 1.00 0.0480
0.00 -2.00 -1.00 0.0410
0.00 2.00 1.00 0.0400
0.00 -1.00 0.00 0.0180
1.00 0.00 -2.00 0.0500
1.00 0.00 0.00 0.0650

_exptl_crystal_preparation       ?
_exptl_crystal_size_max          0.129
_exptl_crystal_size_mid          0.111
_exptl_crystal_size_min          0.036
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0784
_diffrn_reflns_av_unetI/netI     0.0555
_diffrn_reflns_Laue_measured_fraction_full 0.986
_diffrn_reflns_Laue_measured_fraction_max 0.986
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_k_min       -12
_diffrn_reflns_limit_l_max       9
_diffrn_reflns_limit_l_min       -9
_diffrn_reflns_number            6638
_diffrn_reflns_point_group_measured_fraction_full 0.986
_diffrn_reflns_point_group_measured_fraction_max 0.986
_diffrn_reflns_theta_full        25.014
_diffrn_reflns_theta_max         25.014
_diffrn_reflns_theta_min         2.409
_diffrn_ambient_temperature      293
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.986
_diffrn_measured_fraction_theta_max 0.986
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_diffrn_standards_number         0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                874
_reflns_number_total             1001
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT V8.38A (?, 2016)'
_computing_data_collection       ?
_computing_data_reduction        'SAINT V8.38A (?, 2016)'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'XL (Sheldrick, 2008)'
_computing_structure_solution    'SHELXT 2018/2 (Sheldrick, 2018)'
_refine_diff_density_max         1.696
_refine_diff_density_min         -1.461
_refine_diff_density_rms         0.427
_refine_ls_extinction_coef       0.00111(12)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     'SHELXL-2016/6 (Sheldrick 2016)'
_refine_ls_goodness_of_fit_ref   1.096
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     56
_refine_ls_number_reflns         1001
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0381
_refine_ls_R_factor_gt           0.0325
_refine_ls_restrained_S_all      1.096
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0342P)²] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0756
_refine_ls_wR_factor_ref         0.0825
_refine_special_details          ?
_olex2_refinement_description    
;
1. Others
 Sof(Rb2)=0.25*(1-FVAR(2))
 Sof(Rb1)=0.25*FVAR(2)
;
_atom_sites_solution_hydrogens   .
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Pb1 Pb 0.10726(4) 0.69214(4) 0.65116(5) 0.0186(2) Uani 1 1 d . . . . .
Pb2 Pb 0.01233(4) 0.66602(4) 0.17031(6) 0.0221(2) Uani 1 1 d . . . . .
Rb1 Rb 0.250000 0.250000 0.3327(8) 0.0217(14) Uani 0.819(16) 4 d S T P A 1
Cl1 Cl -0.1283(3) 0.5688(3) 0.3996(4) 0.0321(8) Uani 1 1 d . . . . .
Cl2 Cl 0.1273(3) 0.4649(3) 0.1195(4) 0.0303(8) Uani 1 1 d . . . . .
Cl3 Cl 0.250000 0.750000 0.000000 0.0325(15) Uani 1 4 d S T P . .
O1 O 0.1387(7) 0.7021(7) 0.3699(9) 0.0159(17) Uani 1 1 d . . . . .
Rb2 Rb 0.250000 0.250000 0.223(3) 0.005(5) Uani 0.181(16) 4 d S T P A 2


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pb1 Pb1 3.5462(7) 7_566 ?
Pb1 Pb1 3.6828(9) 2_565 ?
Pb1 Pb1 3.5463(7) 8_666 ?
Pb1 Rb1 4.3289(5) 5_566 ?
Pb1 O1 2.325(8) 7_566 ?
Pb1 O1 2.373(8) 8_666 ?
Pb1 O1 2.274(7) . ?
Pb1 Rb2 4.441(5) 5_566 ?
Pb2 Cl1 2.740(3) . ?
Pb2 Cl2 2.800(3) . ?
Pb2 Cl3 3.3046(5) . ?
Pb2 O1 2.234(8) . ?
Pb2 Rb2 4.547(15) 5_565 ?
Rb1 Cl1 3.370(5) 8_666 ?
Rb1 Cl1 3.370(5) 6_656 ?
Rb1 Cl1 3.370(5) 5_566 ?
Rb1 Cl1 3.370(5) 7_556 ?
Rb1 Cl2 3.410(5) . ?
Rb1 Cl2 3.410(5) 2 ?
Rb1 Cl2 3.410(5) 4 ?
Rb1 Cl2 3.410(5) 3 ?
Cl2 Rb2 3.071(7) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Pb1 Pb1 Pb1 62.565(14) 7_566 8_666 ?
Pb1 Pb1 Pb1 58.718(7) 7_566 2_565 ?
Pb1 Pb1 Pb1 58.717(7) 8_666 2_565 ?
Pb1 Pb1 Rb1 137.16(8) 8_666 5_566 ?
Pb1 Pb1 Rb1 148.69(2) 2_565 5_566 ?
Pb1 Pb1 Rb1 101.21(6) 7_566 5_566 ?
Pb1 Pb1 Rb2 108.82(18) 7_566 5_566 ?
Pb1 Pb1 Rb2 146.39(10) 2_565 5_566 ?
Pb1 Pb1 Rb2 148.0(3) 8_666 5_566 ?
Rb1 Pb1 Rb2 11.3(2) 5_566 5_566 ?
O1 Pb1 Pb1 41.3(2) . 7_566 ?
O1 Pb1 Pb1 39.24(18) 8_666 8_666 ?
O1 Pb1 Pb1 80.1(2) . 2_565 ?
O1 Pb1 Pb1 37.9(2) 8_666 2_565 ?
O1 Pb1 Pb1 40.1(2) . 8_666 ?
O1 Pb1 Pb1 39.03(18) 7_566 7_566 ?
O1 Pb1 Pb1 82.5(2) 7_566 8_666 ?
O1 Pb1 Pb1 38.9(2) 7_566 2_565 ?
O1 Pb1 Pb1 81.9(2) 8_666 7_566 ?
O1 Pb1 Rb1 173.1(2) 8_666 5_566 ?
O1 Pb1 Rb1 110.1(2) 7_566 5_566 ?
O1 Pb1 Rb1 100.6(2) . 5_566 ?
O1 Pb1 O1 78.6(3) . 7_566 ?
O1 Pb1 O1 76.2(3) 7_566 8_666 ?
O1 Pb1 O1 77.6(3) . 8_666 ?
O1 Pb1 Rb2 169.0(3) 8_666 5_566 ?
O1 Pb1 Rb2 110.5(2) 7_566 5_566 ?
O1 Pb1 Rb2 111.9(3) . 5_566 ?
Cl1 Pb2 Cl2 91.90(11) . . ?
Cl1 Pb2 Cl3 158.39(8) . . ?
Cl1 Pb2 Rb2 97.45(18) . 5_565 ?
Cl2 Pb2 Cl3 77.26(8) . . ?
Cl2 Pb2 Rb2 115.40(15) . 5_565 ?
Cl3 Pb2 Rb2 104.07(16) . 5_565 ?
O1 Pb2 Cl1 91.3(2) . . ?
O1 Pb2 Cl2 86.4(2) . . ?
O1 Pb2 Cl3 69.6(2) . . ?
O1 Pb2 Rb2 156.1(2) . 5_565 ?
Pb1 Rb1 Pb1 89.949(5) 7_556 6_656 ?
Pb1 Rb1 Pb1 89.949(5) 7_556 5_566 ?
Pb1 Rb1 Pb1 89.949(5) 8_666 6_656 ?
Pb1 Rb1 Pb1 176.59(17) 6_656 5_566 ?
Pb1 Rb1 Pb1 176.59(17) 8_666 7_556 ?
Pb1 Rb1 Pb1 89.949(5) 8_666 5_566 ?
Cl1 Rb1 Pb1 54.26(6) 5_566 8_666 ?
Cl1 Rb1 Pb1 120.67(12) 8_666 7_556 ?
Cl1 Rb1 Pb1 56.79(6) 7_556 7_556 ?
Cl1 Rb1 Pb1 54.26(6) 8_666 6_656 ?
Cl1 Rb1 Pb1 123.13(13) 5_566 7_556 ?
Cl1 Rb1 Pb1 123.13(12) 8_666 5_566 ?
Cl1 Rb1 Pb1 120.67(12) 5_566 6_656 ?
Cl1 Rb1 Pb1 56.79(6) 8_666 8_666 ?
Cl1 Rb1 Pb1 56.79(6) 6_656 6_656 ?
Cl1 Rb1 Pb1 120.67(12) 7_556 8_666 ?
Cl1 Rb1 Pb1 56.79(6) 5_566 5_566 ?
Cl1 Rb1 Pb1 54.26(6) 7_556 5_566 ?
Cl1 Rb1 Pb1 54.26(6) 6_656 7_556 ?
Cl1 Rb1 Pb1 123.13(12) 6_656 8_666 ?
Cl1 Rb1 Pb1 120.67(12) 6_656 5_566 ?
Cl1 Rb1 Pb1 123.13(13) 7_556 6_656 ?
Cl1 Rb1 Cl1 66.41(11) 7_556 6_656 ?
Cl1 Rb1 Cl1 66.41(11) 8_666 6_656 ?
Cl1 Rb1 Cl1 66.41(11) 8_666 5_566 ?
Cl1 Rb1 Cl1 101.5(2) 8_666 7_556 ?
Cl1 Rb1 Cl1 101.5(2) 5_566 6_656 ?
Cl1 Rb1 Cl1 66.41(11) 5_566 7_556 ?
Cl1 Rb1 Cl2 105.43(8) 8_666 . ?
Cl1 Rb1 Cl2 169.99(18) 8_666 3 ?
Cl1 Rb1 Cl2 111.32(8) 7_556 . ?
Cl1 Rb1 Cl2 69.20(8) 8_666 4 ?
Cl1 Rb1 Cl2 169.99(18) 7_556 4 ?
Cl1 Rb1 Cl2 105.43(8) 5_566 3 ?
Cl1 Rb1 Cl2 105.43(8) 6_656 4 ?
Cl1 Rb1 Cl2 69.20(8) 7_556 3 ?
Cl1 Rb1 Cl2 169.99(18) 5_566 2 ?
Cl1 Rb1 Cl2 169.99(18) 6_656 . ?
Cl1 Rb1 Cl2 105.43(8) 7_556 2 ?
Cl1 Rb1 Cl2 69.20(8) 6_656 2 ?
Cl1 Rb1 Cl2 111.33(8) 5_566 4 ?
Cl1 Rb1 Cl2 111.33(8) 6_656 3 ?
Cl1 Rb1 Cl2 69.20(8) 5_566 . ?
Cl1 Rb1 Cl2 111.33(8) 8_666 2 ?
Cl2 Rb1 Pb1 133.58(11) 3 6_656 ?
Cl2 Rb1 Pb1 124.02(10) 4 7_556 ?
Cl2 Rb1 Pb1 124.02(10) 3 8_666 ?
Cl2 Rb1 Pb1 58.00(6) . 5_566 ?
Cl2 Rb1 Pb1 48.72(5) . 8_666 ?
Cl2 Rb1 Pb1 58.00(6) 4 8_666 ?
Cl2 Rb1 Pb1 58.00(6) 2 6_656 ?
Cl2 Rb1 Pb1 48.72(5) 4 6_656 ?
Cl2 Rb1 Pb1 133.58(11) 4 5_566 ?
Cl2 Rb1 Pb1 124.02(10) 2 5_566 ?
Cl2 Rb1 Pb1 133.58(11) . 7_556 ?
Cl2 Rb1 Pb1 58.00(6) 3 7_556 ?
Cl2 Rb1 Pb1 133.58(11) 2 8_666 ?
Cl2 Rb1 Pb1 124.02(10) . 6_656 ?
Cl2 Rb1 Pb1 48.72(5) 3 5_566 ?
Cl2 Rb1 Pb1 48.72(5) 2 7_556 ?
Cl2 Rb1 Cl2 120.3(2) . 2 ?
Cl2 Rb1 Cl2 75.66(9) . 3 ?
Cl2 Rb1 Cl2 75.66(9) 3 2 ?
Cl2 Rb1 Cl2 75.66(9) 2 4 ?
Cl2 Rb1 Cl2 120.3(2) 3 4 ?
Cl2 Rb1 Cl2 75.66(9) . 4 ?
Pb2 Cl1 Rb1 114.44(12) . 5_566 ?
Pb2 Cl2 Rb1 141.86(15) . . ?
Pb2 Cl2 Rb2 156.1(4) . . ?
Pb1 O1 Pb1 103.2(3) 8_666 7_566 ?
Pb1 O1 Pb1 99.4(3) . 7_566 ?
Pb1 O1 Pb1 100.9(3) . 8_666 ?
Pb2 O1 Pb1 108.5(3) . 7_566 ?
Pb2 O1 Pb1 125.4(4) . . ?
Pb2 O1 Pb1 116.3(3) . 8_666 ?
Pb1 Rb2 Pb1 87.10(12) 6_656 7_556 ?
Pb1 Rb2 Pb1 154.0(5) 6_656 5_566 ?
Pb1 Rb2 Pb1 87.10(12) 8_666 6_656 ?
Pb1 Rb2 Pb1 87.10(12) 7_556 5_566 ?
Pb1 Rb2 Pb1 154.0(5) 8_666 7_556 ?
Pb1 Rb2 Pb1 87.10(12) 8_666 5_566 ?
Pb1 Rb2 Pb2 148.5(4) 8_666 7 ?
Pb1 Rb2 Pb2 92.87(14) 7_556 6_655 ?
Pb1 Rb2 Pb2 57.12(7) 5_566 5_565 ?
Pb1 Rb2 Pb2 57.12(7) 6_656 6_655 ?
Pb1 Rb2 Pb2 105.07(17) 7_556 5_565 ?
Pb1 Rb2 Pb2 92.87(14) 6_656 8_665 ?
Pb1 Rb2 Pb2 92.87(14) 5_566 7 ?
Pb1 Rb2 Pb2 105.07(17) 6_656 7 ?
Pb1 Rb2 Pb2 148.5(4) 6_656 5_565 ?
Pb1 Rb2 Pb2 148.5(4) 5_566 6_655 ?
Pb1 Rb2 Pb2 148.5(4) 7_556 8_665 ?
Pb1 Rb2 Pb2 57.12(7) 7_556 7 ?
Pb1 Rb2 Pb2 105.07(17) 8_666 6_655 ?
Pb1 Rb2 Pb2 105.07(17) 5_566 8_665 ?
Pb1 Rb2 Pb2 92.87(14) 8_666 5_565 ?
Pb1 Rb2 Pb2 57.12(7) 8_666 8_665 ?
Pb2 Rb2 Pb2 61.6(2) 5_565 8_665 ?
Pb2 Rb2 Pb2 61.6(2) 7 5_565 ?
Pb2 Rb2 Pb2 61.6(2) 7 6_655 ?
Pb2 Rb2 Pb2 92.8(4) 7 8_665 ?
Pb2 Rb2 Pb2 92.8(4) 5_565 6_655 ?
Pb2 Rb2 Pb2 61.6(2) 6_655 8_665 ?
Cl2 Rb2 Pb1 142.24(7) 2 8_666 ?
Cl2 Rb2 Pb1 130.55(7) 2 5_566 ?
Cl2 Rb2 Pb1 130.55(7) 3 8_666 ?
Cl2 Rb2 Pb1 58.06(8) 3 7_556 ?
Cl2 Rb2 Pb1 130.55(7) 4 7_556 ?
Cl2 Rb2 Pb1 47.97(9) 2 7_556 ?
Cl2 Rb2 Pb1 142.24(7) . 7_556 ?
Cl2 Rb2 Pb1 130.55(7) . 6_656 ?
Cl2 Rb2 Pb1 47.97(9) 3 5_566 ?
Cl2 Rb2 Pb1 47.97(9) . 8_666 ?
Cl2 Rb2 Pb1 58.06(8) 2 6_656 ?
Cl2 Rb2 Pb1 142.24(7) 3 6_656 ?
Cl2 Rb2 Pb1 142.24(7) 4 5_566 ?
Cl2 Rb2 Pb1 58.06(8) 4 8_666 ?
Cl2 Rb2 Pb1 58.06(8) . 5_566 ?
Cl2 Rb2 Pb1 47.97(9) 4 6_656 ?
Cl2 Rb2 Pb2 109.2(5) . 6_655 ?
Cl2 Rb2 Pb2 45.6(2) . 5_565 ?
Cl2 Rb2 Pb2 48.9(2) 2 7 ?
Cl2 Rb2 Pb2 109.2(5) 3 8_665 ?
Cl2 Rb2 Pb2 48.9(2) 3 5_565 ?
Cl2 Rb2 Pb2 106.6(5) 3 6_655 ?
Cl2 Rb2 Pb2 106.6(5) 4 5_565 ?
Cl2 Rb2 Pb2 106.6(5) 2 8_665 ?
Cl2 Rb2 Pb2 109.2(5) 2 5_565 ?
Cl2 Rb2 Pb2 48.9(2) 4 6_655 ?
Cl2 Rb2 Pb2 45.6(2) 3 7 ?
Cl2 Rb2 Pb2 109.2(5) 4 7 ?
Cl2 Rb2 Pb2 48.9(2) . 8_665 ?
Cl2 Rb2 Pb2 45.6(2) 2 6_655 ?
Cl2 Rb2 Pb2 45.6(2) 4 8_665 ?
Cl2 Rb2 Pb2 106.6(5) . 7 ?
Cl2 Rb2 Cl2 148.8(8) 3 4 ?
Cl2 Rb2 Cl2 85.8(2) 4 2 ?
Cl2 Rb2 Cl2 85.8(2) . 3 ?
Cl2 Rb2 Cl2 85.8(2) 3 2 ?
Cl2 Rb2 Cl2 85.8(2) . 4 ?
Cl2 Rb2 Cl2 148.8(8) . 2 ?

_olex2_submission_special_instructions 'No special instructions were received'
