# Electronic Supplementary Material (ESI) for New Journal of Chemistry.
# This journal is © The Royal Society of Chemistry and the Centre National de la Recherche Scientifique 2021

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
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data_4444
_database_code_depnum_ccdc_archive 'CCDC 2102195'
loop_
_audit_author_name
_audit_author_address
'Yuchen Yan'
;xinjiang University
China
;
_audit_update_record             
;
2021-08-09 deposited with the CCDC.	2021-09-06 downloaded from the CCDC.
;
_audit_creation_date             2021-04-25
_audit_creation_method           
;
Olex2 1.3
(compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6272)
;
_shelx_SHELXL_version_number     2016/6
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'Cs Li5 O12 S3'
_chemical_formula_sum            'Cs Li5 O12 S3'
_chemical_formula_weight         455.79
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cs Cs -0.3680 2.1192 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Li Li -0.0003 0.0001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_H-M_alt        'P 1 21/c 1'
_space_group_name_Hall           '-P 2ybc'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'

_cell_length_a                   4.9300(15)
_cell_length_b                   15.558(5)
_cell_length_c                   14.566(5)
_cell_angle_alpha                90
_cell_angle_beta                 91.349(4)
_cell_angle_gamma                90
_cell_volume                     1116.9(6)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    1401
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      23.29
_cell_measurement_theta_min      2.62
_shelx_estimated_absorpt_T_max   0.7456
_shelx_estimated_absorpt_T_min   0.6736
_exptl_absorpt_coefficient_mu    3.931
_exptl_absorpt_correction_T_max  ?
_exptl_absorpt_correction_T_min  ?
_exptl_absorpt_correction_type   ?
_exptl_absorpt_process_details   ?
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            colourless
_exptl_crystal_colour_primary    colourless
_exptl_crystal_density_diffrn    2.711
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             856
_exptl_crystal_size_max          0.165
_exptl_crystal_size_mid          0.142
_exptl_crystal_size_min          0.123
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0412
_diffrn_reflns_av_unetI/netI     0.0542
_diffrn_reflns_Laue_measured_fraction_full 0.997
_diffrn_reflns_Laue_measured_fraction_max 0.991
_diffrn_reflns_limit_h_max       2
_diffrn_reflns_limit_h_min       -6
_diffrn_reflns_limit_k_max       20
_diffrn_reflns_limit_k_min       -19
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_limit_l_min       -18
_diffrn_reflns_number            6860
_diffrn_reflns_point_group_measured_fraction_full 0.997
_diffrn_reflns_point_group_measured_fraction_max 0.991
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         27.405
_diffrn_reflns_theta_min         1.915
_diffrn_ambient_temperature      296(2)
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.991
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       ?
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                1865
_reflns_number_total             2528
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       ?
_computing_data_collection       ?
_computing_data_reduction        ?
_computing_molecular_graphics    'Olex2 1.3 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.3 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL-2016/6 (Sheldrick, 2016)'
_computing_structure_solution    ?
_refine_diff_density_max         0.783
_refine_diff_density_min         -0.786
_refine_diff_density_rms         0.137
_refine_ls_extinction_coef       0.0019(3)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     'SHELXL-2016/6 (Sheldrick 2016)'
_refine_ls_goodness_of_fit_ref   1.053
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     200
_refine_ls_number_reflns         2528
_refine_ls_number_restraints     6
_refine_ls_R_factor_all          0.0585
_refine_ls_R_factor_gt           0.0384
_refine_ls_restrained_S_all      1.131
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0339P)²] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0780
_refine_ls_wR_factor_ref         0.0864
_refine_special_details          ?
_olex2_refinement_description    
;
1. Uiso/Uaniso restraints and constraints
O12 \\sim S2: within 3.8A with sigma of 0.005 and sigma for terminal atoms of
0.005 within 3.8A
2. Others
 Fixed Sof: O9A(0.5) O9B(0.5)
;
_atom_sites_solution_hydrogens   .
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Cs1 Cs 0.25262(7) 0.56622(2) 0.23421(3) 0.04245(16) Uani 1 1 d . . . . .
Li1 Li 0.3044(18) 0.7392(6) 0.4340(6) 0.034(2) Uani 1 1 d . . . . .
Li2 Li -0.2201(17) 0.4323(5) 0.0631(6) 0.0272(18) Uani 1 1 d . . . . .
Li3 Li 0.1893(16) 0.2863(5) 0.1569(5) 0.0249(18) Uani 1 1 d . . . . .
Li4 Li -0.2900(15) 0.4165(5) 0.4412(5) 0.0202(16) Uani 1 1 d . . . . .
Li5 Li -0.1998(16) 0.8067(5) 0.1333(5) 0.0268(18) Uani 1 1 d . . . . .
S1 S -0.2152(2) 0.61639(7) 0.44416(7) 0.0135(2) Uani 1 1 d . . . . .
S2 S -0.2687(3) 0.63545(8) 0.02754(8) 0.0263(3) Uani 1 1 d . U . . .
S3 S 0.6991(2) 0.34517(7) 0.24742(7) 0.0162(2) Uani 1 1 d . . . . .
O1 O -0.3433(6) 0.6801(2) 0.3835(2) 0.0288(8) Uani 1 1 d . . . . .
O2 O -0.2498(7) 0.5320(2) 0.4038(2) 0.0313(8) Uani 1 1 d . . . . .
O3 O -0.3440(6) 0.6203(2) 0.5343(2) 0.0304(8) Uani 1 1 d . . . . .
O4 O 0.0765(6) 0.63643(19) 0.4563(2) 0.0201(7) Uani 1 1 d . . . . .
O5 O 0.8141(6) 0.27200(19) 0.19628(19) 0.0193(7) Uani 1 1 d . . . . .
O6 O 0.4047(6) 0.3323(2) 0.25621(19) 0.0223(7) Uani 1 1 d . . . . .
O7 O 0.8274(6) 0.3480(2) 0.33923(19) 0.0206(7) Uani 1 1 d . . . . .
O8 O 0.7482(7) 0.4248(2) 0.1983(2) 0.0290(8) Uani 1 1 d . . . . .
O9A O -0.182(3) 0.5459(8) 0.0373(9) 0.068(4) Uani 0.5 1 d . . P . .
O9B O -0.299(3) 0.5519(8) 0.0683(10) 0.062(4) Uani 0.5 1 d . . P . .
O10 O -0.5437(8) 0.6559(2) -0.0056(3) 0.0466(10) Uani 1 1 d . . . . .
O11 O -0.1971(8) 0.6873(3) 0.1052(3) 0.0519(12) Uani 1 1 d . . . . .
O12 O -0.0892(9) 0.6504(3) -0.0481(3) 0.0669(12) Uani 1 1 d . U . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Cs1 O1 3.411(3) 1_655 ?
Cs1 O2 3.579(4) . ?
Cs1 O2 3.481(3) 1_655 ?
Cs1 O4 3.542(3) . ?
Cs1 O5 3.376(3) 2_655 ?
Cs1 O6 3.728(4) . ?
Cs1 O8 3.339(4) . ?
Cs1 O8 3.352(3) 1_455 ?
Cs1 O9A 3.554(14) . ?
Cs1 O9B 3.604(18) . ?
Cs1 O9B 3.320(10) 1_655 ?
Cs1 O11 3.435(4) . ?
Li1 Li2 3.033(12) 2 ?
Li1 Li3 2.946(12) 2_655 ?
Li1 Li3 2.840(11) 2 ?
Li1 Li4 3.030(11) 3_566 ?
Li1 S1 3.044(9) 1_655 ?
Li1 O1 2.113(10) 1_655 ?
Li1 O4 1.985(9) . ?
Li1 O5 2.038(9) 2_655 ?
Li1 O10 1.991(10) 4_676 ?
Li1 O12 2.608(11) 4_576 ?
Li2 Li3 3.313(11) . ?
Li2 S2 2.968(9) 3_565 ?
Li2 S2 3.008(9) 3_465 ?
Li2 S3 3.043(8) 1_455 ?
Li2 O8 1.983(9) 1_455 ?
Li2 O9A 1.817(15) . ?
Li2 O9A 2.514(17) 3_565 ?
Li2 O9B 1.903(15) . ?
Li2 O10 1.973(9) 3_465 ?
Li2 O12 2.011(9) 3_565 ?
Li3 Li5 3.071(11) 2_545 ?
Li3 S1 3.029(8) 2_545 ?
Li3 S2 2.984(8) 3_565 ?
Li3 S3 2.956(8) . ?
Li3 S3 2.927(8) 1_455 ?
Li3 O1 1.916(8) 2_545 ?
Li3 O5 1.962(9) 1_455 ?
Li3 O6 1.913(8) . ?
Li3 O12 1.920(9) 3_565 ?
Li4 Li5 3.208(11) 2_445 ?
Li4 Li5 3.170(11) 2_545 ?
Li4 S1 3.032(8) 3_466 ?
Li4 S1 3.010(8) 3_566 ?
Li4 S3 3.032(8) 1_455 ?
Li4 O2 1.889(8) . ?
Li4 O3 1.934(8) 3_466 ?
Li4 O4 1.985(8) 3_566 ?
Li4 O7 1.928(8) 1_455 ?
Li5 S1 3.004(8) 4_575 ?
Li5 S3 3.044(8) 2_655 ?
Li5 O3 1.956(9) 4_575 ?
Li5 O6 1.960(8) 2 ?
Li5 O7 1.977(9) 2_655 ?
Li5 O11 1.902(9) . ?
S1 O1 1.461(3) . ?
S1 O2 1.447(3) . ?
S1 O3 1.474(3) . ?
S1 O4 1.478(3) . ?
S2 O9A 1.464(11) . ?
S2 O9B 1.438(13) . ?
S2 O10 1.463(4) . ?
S2 O11 1.428(4) . ?
S2 O12 1.449(4) . ?
S3 O5 1.481(3) . ?
S3 O6 1.474(3) . ?
S3 O7 1.466(3) . ?
S3 O8 1.453(3) . ?
O9A O9B 0.748(15) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O1 Cs1 O2 40.16(7) 1_655 1_655 ?
O1 Cs1 O2 92.31(8) 1_655 . ?
O1 Cs1 O4 53.80(8) 1_655 . ?
O1 Cs1 O6 109.82(7) 1_655 . ?
O1 Cs1 O9A 153.2(2) 1_655 . ?
O1 Cs1 O9B 151.7(2) 1_655 . ?
O1 Cs1 O11 115.06(9) 1_655 . ?
O2 Cs1 O2 88.56(8) 1_655 . ?
O2 Cs1 O4 65.34(7) 1_655 . ?
O2 Cs1 O6 69.68(7) 1_655 . ?
O2 Cs1 O6 86.36(7) . . ?
O2 Cs1 O9A 163.86(19) 1_655 . ?
O2 Cs1 O9B 167.1(2) 1_655 . ?
O2 Cs1 O9B 85.97(18) . . ?
O4 Cs1 O2 39.37(7) . . ?
O4 Cs1 O6 106.00(7) . . ?
O4 Cs1 O9A 127.5(2) . . ?
O4 Cs1 O9B 115.73(17) . . ?
O5 Cs1 O1 51.37(7) 2_655 1_655 ?
O5 Cs1 O2 81.96(7) 2_655 . ?
O5 Cs1 O2 90.24(7) 2_655 1_655 ?
O5 Cs1 O4 53.56(7) 2_655 . ?
O5 Cs1 O6 157.04(6) 2_655 . ?
O5 Cs1 O9A 105.39(19) 2_655 . ?
O5 Cs1 O9B 100.5(2) 2_655 . ?
O5 Cs1 O11 65.02(8) 2_655 . ?
O8 Cs1 O1 149.36(8) 1_455 1_655 ?
O8 Cs1 O1 91.36(8) . 1_655 ?
O8 Cs1 O2 121.20(8) 1_455 1_655 ?
O8 Cs1 O2 60.28(8) . 1_655 ?
O8 Cs1 O2 122.08(8) . . ?
O8 Cs1 O2 59.15(8) 1_455 . ?
O8 Cs1 O4 98.52(8) 1_455 . ?
O8 Cs1 O4 122.84(7) . . ?
O8 Cs1 O5 126.30(8) 1_455 2_655 ?
O8 Cs1 O5 138.49(8) . 2_655 ?
O8 Cs1 O6 39.07(7) . . ?
O8 Cs1 O6 61.29(7) 1_455 . ?
O8 Cs1 O8 94.93(8) . 1_455 ?
O8 Cs1 O9A 52.0(2) 1_455 . ?
O8 Cs1 O9A 104.2(2) . . ?
O8 Cs1 O9B 113.46(19) . . ?
O8 Cs1 O9B 46.3(2) 1_455 . ?
O8 Cs1 O11 78.93(9) 1_455 . ?
O8 Cs1 O11 137.83(9) . . ?
O9A Cs1 O2 97.5(3) . . ?
O9A Cs1 O6 95.66(19) . . ?
O9A Cs1 O9B 12.0(2) . . ?
O9B Cs1 O1 96.3(3) 1_655 1_655 ?
O9B Cs1 O2 167.3(2) 1_655 . ?
O9B Cs1 O2 92.1(3) 1_655 1_655 ?
O9B Cs1 O4 150.1(3) 1_655 . ?
O9B Cs1 O5 110.7(2) 1_655 2_655 ?
O9B Cs1 O6 82.0(2) 1_655 . ?
O9B Cs1 O6 98.3(2) . . ?
O9B Cs1 O8 110.3(3) 1_655 1_455 ?
O9B Cs1 O8 48.7(2) 1_655 . ?
O9B Cs1 O9A 78.8(4) 1_655 . ?
O9B Cs1 O9B 90.7(4) 1_655 . ?
O9B Cs1 O11 94.0(3) 1_655 . ?
O11 Cs1 O2 155.09(8) . 1_655 ?
O11 Cs1 O2 90.62(9) . . ?
O11 Cs1 O4 99.29(8) . . ?
O11 Cs1 O6 135.11(8) . . ?
O11 Cs1 O9A 40.39(19) . . ?
O11 Cs1 O9B 36.8(2) . . ?
Li2 Li1 Cs1 132.5(3) 2 . ?
Li2 Li1 S1 136.7(3) 2 1_655 ?
Li3 Li1 Cs1 83.1(3) 2_655 . ?
Li3 Li1 Cs1 78.0(3) 2 . ?
Li3 Li1 Li2 83.0(3) 2_655 2 ?
Li3 Li1 Li2 68.6(3) 2 2 ?
Li3 Li1 Li3 116.9(4) 2 2_655 ?
Li3 Li1 Li4 117.0(4) 2 3_566 ?
Li3 Li1 Li4 120.0(4) 2_655 3_566 ?
Li3 Li1 S1 147.3(4) 2 1_655 ?
Li3 Li1 S1 60.7(2) 2_655 1_655 ?
Li4 Li1 Cs1 84.0(2) 3_566 . ?
Li4 Li1 Li2 141.1(4) 3_566 2 ?
Li4 Li1 S1 59.9(2) 3_566 1_655 ?
S1 Li1 Cs1 69.28(19) 1_655 . ?
O1 Li1 Cs1 59.2(2) 1_655 . ?
O1 Li1 Li2 123.4(4) 1_655 2 ?
O1 Li1 Li3 40.5(2) 1_655 2_655 ?
O1 Li1 Li3 130.7(4) 1_655 2 ?
O1 Li1 Li4 83.8(3) 1_655 3_566 ?
O1 Li1 S1 25.66(14) 1_655 1_655 ?
O1 Li1 O12 160.2(4) 1_655 4_576 ?
O4 Li1 Cs1 63.0(3) . . ?
O4 Li1 Li2 135.8(5) . 2 ?
O4 Li1 Li3 78.6(3) . 2 ?
O4 Li1 Li3 139.7(5) . 2_655 ?
O4 Li1 Li4 40.2(2) . 3_566 ?
O4 Li1 S1 85.9(3) . 1_655 ?
O4 Li1 O1 100.3(4) . 1_655 ?
O4 Li1 O5 101.7(4) . 2_655 ?
O4 Li1 O10 142.7(5) . 4_676 ?
O4 Li1 O12 95.1(4) . 4_576 ?
O5 Li1 Cs1 58.3(2) 2_655 . ?
O5 Li1 Li2 74.3(3) 2_655 2 ?
O5 Li1 Li3 43.7(2) 2_655 2 ?
O5 Li1 Li3 75.3(3) 2_655 2_655 ?
O5 Li1 Li4 138.5(4) 2_655 3_566 ?
O5 Li1 S1 114.1(4) 2_655 1_655 ?
O5 Li1 O1 90.3(4) 2_655 1_655 ?
O5 Li1 O12 74.4(3) 2_655 4_576 ?
O10 Li1 Cs1 153.7(4) 4_676 . ?
O10 Li1 Li2 39.9(3) 4_676 2 ?
O10 Li1 Li3 71.4(3) 4_676 2_655 ?
O10 Li1 Li3 107.7(4) 4_676 2 ?
O10 Li1 Li4 113.8(4) 4_676 3_566 ?
O10 Li1 S1 102.1(3) 4_676 1_655 ?
O10 Li1 O1 101.9(4) 4_676 1_655 ?
O10 Li1 O5 107.6(4) 4_676 2_655 ?
O10 Li1 O12 71.9(3) 4_676 4_576 ?
O12 Li1 Cs1 119.0(3) 4_576 . ?
O12 Li1 Li2 40.9(2) 4_576 2 ?
O12 Li1 Li3 121.4(3) 4_576 2_655 ?
O12 Li1 Li3 41.0(2) 4_576 2 ?
O12 Li1 Li4 116.0(4) 4_576 3_566 ?
O12 Li1 S1 171.2(4) 4_576 1_655 ?
Li1 Li2 Cs1 126.2(3) 2_545 . ?
Li1 Li2 Li3 52.9(2) 2_545 . ?
Li1 Li2 S3 61.7(2) 2_545 1_455 ?
Li3 Li2 Cs1 76.0(2) . . ?
S2 Li2 Cs1 89.7(2) 3_565 . ?
S2 Li2 Cs1 159.1(3) 3_465 . ?
S2 Li2 Li1 76.5(3) 3_565 2_545 ?
S2 Li2 Li1 63.0(2) 3_465 2_545 ?
S2 Li2 Li3 115.9(3) 3_465 . ?
S2 Li2 Li3 56.4(2) 3_565 . ?
S2 Li2 S2 111.2(3) 3_565 3_465 ?
S2 Li2 S3 96.1(2) 3_465 1_455 ?
S2 Li2 S3 111.0(3) 3_565 1_455 ?
S3 Li2 Cs1 76.48(17) 1_455 . ?
S3 Li2 Li3 54.65(19) 1_455 . ?
O8 Li2 Cs1 57.7(2) 1_455 . ?
O8 Li2 Li1 85.1(3) 1_455 2_545 ?
O8 Li2 Li3 67.1(3) 1_455 . ?
O8 Li2 S2 120.3(4) 1_455 3_565 ?
O8 Li2 S2 109.3(3) 1_455 3_465 ?
O8 Li2 S3 23.38(14) 1_455 1_455 ?
O8 Li2 O9A 131.8(5) 1_455 3_565 ?
O8 Li2 O12 98.5(4) 1_455 3_565 ?
O9A Li2 Cs1 80.5(4) 3_565 . ?
O9A Li2 Cs1 63.7(5) . . ?
O9A Li2 Li1 104.6(4) 3_565 2_545 ?
O9A Li2 Li1 168.8(6) . 2_545 ?
O9A Li2 Li3 133.4(6) . . ?
O9A Li2 Li3 81.5(4) 3_565 . ?
O9A Li2 S2 109.9(6) . 3_465 ?
O9A Li2 S2 29.5(3) 3_565 3_565 ?
O9A Li2 S2 99.5(6) . 3_565 ?
O9A Li2 S2 117.1(4) 3_565 3_465 ?
O9A Li2 S3 134.0(4) 3_565 1_455 ?
O9A Li2 S3 129.2(6) . 1_455 ?
O9A Li2 O8 105.9(6) . 1_455 ?
O9A Li2 O9A 70.2(6) . 3_565 ?
O9A Li2 O9B 23.0(5) . . ?
O9A Li2 O10 130.6(6) . 3_465 ?
O9A Li2 O12 121.2(7) . 3_565 ?
O9B Li2 Cs1 65.1(6) . . ?
O9B Li2 Li1 160.0(6) . 2_545 ?
O9B Li2 Li3 141.0(7) . . ?
O9B Li2 S2 100.9(6) . 3_465 ?
O9B Li2 S2 122.3(5) . 3_565 ?
O9B Li2 S3 111.7(5) . 1_455 ?
O9B Li2 O8 89.8(5) . 1_455 ?
O9B Li2 O9A 93.2(6) . 3_565 ?
O9B Li2 O10 125.3(7) . 3_465 ?
O9B Li2 O12 141.9(7) . 3_565 ?
O10 Li2 Cs1 164.7(4) 3_465 . ?
O10 Li2 Li1 40.3(2) 3_465 2_545 ?
O10 Li2 Li3 92.6(3) 3_465 . ?
O10 Li2 S2 24.53(17) 3_465 3_465 ?
O10 Li2 S2 92.4(3) 3_465 3_565 ?
O10 Li2 S3 88.7(3) 3_465 1_455 ?
O10 Li2 O8 108.7(4) 3_465 1_455 ?
O10 Li2 O9A 108.2(5) 3_465 3_565 ?
O10 Li2 O12 87.2(4) 3_465 3_565 ?
O12 Li2 Cs1 88.2(3) 3_565 . ?
O12 Li2 Li1 58.1(3) 3_565 2_545 ?
O12 Li2 Li3 31.7(2) 3_565 . ?
O12 Li2 S2 111.0(3) 3_565 3_465 ?
O12 Li2 S2 25.72(17) 3_565 3_565 ?
O12 Li2 S3 85.7(3) 3_565 1_455 ?
O12 Li2 O9A 54.1(4) 3_565 3_565 ?
Li1 Li3 Li1 116.9(4) 2_545 2_645 ?
Li1 Li3 Li2 58.5(3) 2_545 . ?
Li1 Li3 Li2 120.0(3) 2_645 . ?
Li1 Li3 Li5 119.0(4) 2_545 2_545 ?
Li1 Li3 Li5 118.6(3) 2_645 2_545 ?
Li1 Li3 S1 61.2(2) 2_645 2_545 ?
Li1 Li3 S1 66.0(2) 2_545 2_545 ?
Li1 Li3 S2 64.3(2) 2_645 3_565 ?
Li1 Li3 S2 79.3(3) 2_545 3_565 ?
Li1 Li3 S3 176.8(4) 2_545 . ?
Li1 Li3 S3 65.4(2) 2_545 1_455 ?
Li1 Li3 S3 63.7(2) 2_645 . ?
Li5 Li3 Li2 109.6(3) 2_545 . ?
S1 Li3 Li2 115.5(3) 2_545 . ?
S1 Li3 Li5 125.0(3) 2_545 2_545 ?
S2 Li3 Li2 56.0(2) 3_565 . ?
S2 Li3 Li5 148.6(3) 3_565 2_545 ?
S2 Li3 S1 84.9(2) 3_565 2_545 ?
S3 Li3 Li1 176.1(3) 1_455 2_645 ?
S3 Li3 Li2 118.3(3) . . ?
S3 Li3 Li2 58.0(2) 1_455 . ?
S3 Li3 Li5 62.0(2) . 2_545 ?
S3 Li3 Li5 60.9(2) 1_455 2_545 ?
S3 Li3 S1 122.5(3) 1_455 2_545 ?
S3 Li3 S1 116.2(3) . 2_545 ?
S3 Li3 S2 113.9(3) 1_455 3_565 ?
S3 Li3 S2 98.4(2) . 3_565 ?
S3 Li3 S3 113.9(2) 1_455 . ?
O1 Li3 Li1 88.6(3) 2_545 2_545 ?
O1 Li3 Li1 45.7(3) 2_545 2_645 ?
O1 Li3 Li2 134.9(4) 2_545 . ?
O1 Li3 Li5 113.4(4) 2_545 2_545 ?
O1 Li3 S1 22.66(14) 2_545 2_545 ?
O1 Li3 S2 90.8(3) 2_545 3_565 ?
O1 Li3 S3 138.2(4) 2_545 1_455 ?
O1 Li3 S3 93.7(3) 2_545 . ?
O1 Li3 O5 112.1(4) 2_545 1_455 ?
O1 Li3 O12 106.5(4) 2_545 3_565 ?
O5 Li3 Li1 156.6(4) 1_455 2_645 ?
O5 Li3 Li1 45.9(3) 1_455 2_545 ?
O5 Li3 Li2 68.2(3) 1_455 . ?
O5 Li3 Li5 73.4(3) 1_455 2_545 ?
O5 Li3 S1 95.4(3) 1_455 2_545 ?
O5 Li3 S2 117.0(3) 1_455 3_565 ?
O5 Li3 S3 134.6(4) 1_455 . ?
O5 Li3 S3 27.09(14) 1_455 1_455 ?
O6 Li3 Li1 88.4(3) . 2_645 ?
O6 Li3 Li1 154.6(4) . 2_545 ?
O6 Li3 Li2 112.2(4) . . ?
O6 Li3 Li5 38.1(2) . 2_545 ?
O6 Li3 S1 131.7(4) . 2_545 ?
O6 Li3 S2 116.5(4) . 3_565 ?
O6 Li3 S3 25.29(15) . . ?
O6 Li3 S3 89.5(3) . 1_455 ?
O6 Li3 O1 109.8(4) . 2_545 ?
O6 Li3 O5 109.4(4) . 1_455 ?
O6 Li3 O12 124.0(5) . 3_565 ?
O12 Li3 Li1 63.0(3) 3_565 2_545 ?
O12 Li3 Li1 87.7(4) 3_565 2_645 ?
O12 Li3 Li2 33.4(2) 3_565 . ?
O12 Li3 Li5 140.0(4) 3_565 2_545 ?
O12 Li3 S1 93.4(3) 3_565 2_545 ?
O12 Li3 S2 23.70(17) 3_565 3_565 ?
O12 Li3 S3 90.7(3) 3_565 1_455 ?
O12 Li3 S3 114.1(4) 3_565 . ?
O12 Li3 O5 94.2(4) 3_565 1_455 ?
Li1 Li4 Cs1 144.8(3) 3_566 1_455 ?
Li1 Li4 Li5 75.4(3) 3_566 2_445 ?
Li1 Li4 Li5 78.7(3) 3_566 2_545 ?
Li1 Li4 S1 60.3(2) 3_566 3_466 ?
Li1 Li4 S3 105.4(3) 3_566 1_455 ?
Li5 Li4 Cs1 115.7(2) 2_545 1_455 ?
Li5 Li4 Cs1 70.4(2) 2_445 1_455 ?
Li5 Li4 Li5 101.2(3) 2_545 2_445 ?
S1 Li4 Cs1 151.2(2) 3_566 1_455 ?
S1 Li4 Cs1 93.50(18) 3_466 1_455 ?
S1 Li4 Li1 64.0(2) 3_566 3_566 ?
S1 Li4 Li5 58.09(19) 3_566 2_545 ?
S1 Li4 Li5 57.5(2) 3_466 2_445 ?
S1 Li4 Li5 136.6(3) 3_466 2_545 ?
S1 Li4 Li5 136.8(3) 3_566 2_445 ?
S1 Li4 S1 109.4(2) 3_566 3_466 ?
S1 Li4 S3 116.8(2) 3_566 1_455 ?
S1 Li4 S3 117.0(2) 3_466 1_455 ?
S3 Li4 Cs1 63.73(13) 1_455 1_455 ?
S3 Li4 Li5 58.73(19) 1_455 2_545 ?
S3 Li4 Li5 59.6(2) 1_455 2_445 ?
O2 Li4 Cs1 49.7(2) . 1_455 ?
O2 Li4 Li1 159.6(4) . 3_566 ?
O2 Li4 Li5 109.1(4) . 2_545 ?
O2 Li4 Li5 119.7(4) . 2_445 ?
O2 Li4 S1 114.2(3) . 3_466 ?
O2 Li4 S1 103.3(3) . 3_566 ?
O2 Li4 S3 94.6(3) . 1_455 ?
O2 Li4 O3 116.1(4) . 3_466 ?
O2 Li4 O4 123.6(4) . 3_566 ?
O2 Li4 O7 105.6(4) . 1_455 ?
O3 Li4 Cs1 79.5(2) 3_466 1_455 ?
O3 Li4 Li1 67.5(3) 3_466 3_566 ?
O3 Li4 Li5 128.7(4) 3_466 2_545 ?
O3 Li4 Li5 34.7(2) 3_466 2_445 ?
O3 Li4 S1 23.42(14) 3_466 3_466 ?
O3 Li4 S1 127.7(3) 3_466 3_566 ?
O3 Li4 S3 93.9(3) 3_466 1_455 ?
O3 Li4 O4 102.7(4) 3_466 3_566 ?
O4 Li4 Cs1 172.3(3) 3_566 1_455 ?
O4 Li4 Li1 40.3(2) 3_566 3_566 ?
O4 Li4 Li5 115.6(3) 3_566 2_445 ?
O4 Li4 Li5 68.9(3) 3_566 2_545 ?
O4 Li4 S1 25.17(14) 3_566 3_566 ?
O4 Li4 S1 86.3(3) 3_566 3_466 ?
O4 Li4 S3 123.1(3) 3_566 1_455 ?
O7 Li4 Cs1 85.6(2) 1_455 1_455 ?
O7 Li4 Li1 91.8(3) 1_455 3_566 ?
O7 Li4 Li5 36.2(2) 1_455 2_545 ?
O7 Li4 Li5 72.1(3) 1_455 2_445 ?
O7 Li4 S1 126.2(3) 1_455 3_466 ?
O7 Li4 S1 94.2(3) 1_455 3_566 ?
O7 Li4 S3 23.02(14) 1_455 1_455 ?
O7 Li4 O3 106.1(4) 1_455 3_466 ?
O7 Li4 O4 100.7(3) 1_455 3_566 ?
Cs1 Li5 Cs1 129.07(17) 2 . ?
Li3 Li5 Cs1 70.4(2) 2 2 ?
Li3 Li5 Cs1 66.4(2) 2 . ?
Li3 Li5 Li4 113.7(3) 2 2 ?
Li3 Li5 Li4 112.7(3) 2 2_455 ?
Li4 Li5 Cs1 73.4(2) 2 2 ?
Li4 Li5 Cs1 67.3(2) 2_455 2 ?
Li4 Li5 Cs1 156.3(3) 2_455 . ?
Li4 Li5 Cs1 100.4(2) 2 . ?
Li4 Li5 Li4 101.2(3) 2 2_455 ?
S1 Li5 Cs1 128.4(2) 4_575 . ?
S1 Li5 Cs1 92.0(2) 4_575 2 ?
S1 Li5 Li3 162.5(3) 4_575 2 ?
S1 Li5 Li4 58.3(2) 4_575 2_455 ?
S1 Li5 Li4 58.3(2) 4_575 2 ?
S1 Li5 S3 116.6(3) 4_575 2_655 ?
S3 Li5 Cs1 66.13(15) 2_655 . ?
S3 Li5 Cs1 68.42(15) 2_655 2 ?
S3 Li5 Li3 57.2(2) 2_655 2 ?
S3 Li5 Li4 58.4(2) 2_655 2 ?
S3 Li5 Li4 135.0(3) 2_655 2_455 ?
O3 Li5 Cs1 151.2(3) 4_575 . ?
O3 Li5 Cs1 76.7(3) 4_575 2 ?
O3 Li5 Li3 142.3(4) 4_575 2 ?
O3 Li5 Li4 34.2(2) 4_575 2_455 ?
O3 Li5 Li4 72.6(3) 4_575 2 ?
O3 Li5 S1 24.69(14) 4_575 4_575 ?
O3 Li5 S3 125.6(4) 4_575 2_655 ?
O3 Li5 O6 107.6(4) 4_575 2 ?
O3 Li5 O7 106.3(4) 4_575 2_655 ?
O6 Li5 Cs1 99.2(3) 2 . ?
O6 Li5 Cs1 55.1(2) 2 2 ?
O6 Li5 Li3 37.0(2) 2 2 ?
O6 Li5 Li4 125.7(4) 2 2 ?
O6 Li5 Li4 75.8(3) 2 2_455 ?
O6 Li5 S1 132.0(4) 2 4_575 ?
O6 Li5 S3 85.3(3) 2 2_655 ?
O6 Li5 O7 105.2(4) 2 2_655 ?
O7 Li5 Cs1 76.0(3) 2_655 . ?
O7 Li5 Cs1 71.6(3) 2_655 2 ?
O7 Li5 Li3 80.7(3) 2_655 2 ?
O7 Li5 Li4 127.8(4) 2_655 2_455 ?
O7 Li5 Li4 35.2(2) 2_655 2 ?
O7 Li5 S1 93.4(3) 2_655 4_575 ?
O7 Li5 S3 23.66(13) 2_655 2_655 ?
O11 Li5 Cs1 42.7(2) . . ?
O11 Li5 Cs1 166.5(4) . 2 ?
O11 Li5 Li3 96.5(4) . 2 ?
O11 Li5 Li4 117.1(4) . 2_455 ?
O11 Li5 Li4 116.3(4) . 2 ?
O11 Li5 S1 101.0(3) . 4_575 ?
O11 Li5 S3 107.8(3) . 2_655 ?
O11 Li5 O3 114.4(4) . 4_575 ?
O11 Li5 O6 112.4(4) . 2 ?
O11 Li5 O7 110.5(4) . 2_655 ?
Cs1 S1 Cs1 75.97(3) . 1_455 ?
Li1 S1 Cs1 123.66(16) 1_455 . ?
Li1 S1 Cs1 66.16(17) 1_455 1_455 ?
Li3 S1 Cs1 80.53(15) 2 1_455 ?
Li3 S1 Cs1 76.36(16) 2 . ?
Li3 S1 Li1 58.0(2) 2 1_455 ?
Li3 S1 Li4 117.3(2) 2 3_466 ?
Li4 S1 Cs1 82.44(15) 3_466 1_455 ?
Li4 S1 Cs1 153.81(14) 3_566 1_455 ?
Li4 S1 Cs1 152.23(15) 3_466 . ?
Li4 S1 Cs1 84.56(15) 3_566 . ?
Li4 S1 Li1 140.0(2) 3_566 1_455 ?
Li4 S1 Li1 59.8(2) 3_466 1_455 ?
Li4 S1 Li3 112.0(2) 3_566 2 ?
Li4 S1 Li4 109.4(2) 3_566 3_466 ?
Li5 S1 Cs1 141.82(16) 4_576 . ?
Li5 S1 Cs1 140.36(16) 4_576 1_455 ?
Li5 S1 Li1 78.3(2) 4_576 1_455 ?
Li5 S1 Li3 95.6(2) 4_576 2 ?
Li5 S1 Li4 63.6(2) 4_576 3_566 ?
Li5 S1 Li4 64.2(2) 4_576 3_466 ?
O1 S1 Cs1 85.30(14) . . ?
O1 S1 Cs1 54.01(14) . 1_455 ?
O1 S1 Li1 38.8(2) . 1_455 ?
O1 S1 Li3 30.4(2) . 2 ?
O1 S1 Li4 142.3(2) . 3_566 ?
O1 S1 Li4 96.1(2) . 3_466 ?
O1 S1 Li5 106.6(2) . 4_576 ?
O1 S1 O3 108.8(2) . . ?
O1 S1 O4 109.57(18) . . ?
O2 S1 Cs1 56.74(14) . 1_455 ?
O2 S1 Cs1 64.65(15) . . ?
O2 S1 Li1 117.8(2) . 1_455 ?
O2 S1 Li3 126.9(2) . 2 ?
O2 S1 Li4 89.0(2) . 3_466 ?
O2 S1 Li4 99.2(2) . 3_566 ?
O2 S1 Li5 137.2(2) . 4_576 ?
O2 S1 O1 109.0(2) . . ?
O2 S1 O3 110.5(2) . . ?
O2 S1 O4 110.2(2) . . ?
O3 S1 Cs1 165.83(15) . . ?
O3 S1 Cs1 113.28(13) . 1_455 ?
O3 S1 Li1 70.5(2) . 1_455 ?
O3 S1 Li3 114.9(2) . 2 ?
O3 S1 Li4 31.44(19) . 3_466 ?
O3 S1 Li4 83.1(2) . 3_566 ?
O3 S1 Li5 33.7(2) . 4_576 ?
O3 S1 O4 108.83(17) . . ?
O4 S1 Cs1 137.81(12) . 1_455 ?
O4 S1 Cs1 63.29(12) . . ?
O4 S1 Li1 128.8(2) . 1_455 ?
O4 S1 Li3 79.77(19) . 2 ?
O4 S1 Li4 139.69(19) . 3_466 ?
O4 S1 Li4 34.82(18) . 3_566 ?
O4 S1 Li5 78.6(2) . 4_576 ?
Cs1 S2 Cs1 75.27(3) 1_455 . ?
Li2 S2 Cs1 74.57(16) 3_465 1_455 ?
Li2 S2 Cs1 74.27(16) 3_565 . ?
Li2 S2 Cs1 137.37(16) 3_565 1_455 ?
Li2 S2 Cs1 137.91(16) 3_465 . ?
Li2 S2 Li2 111.2(3) 3_565 3_465 ?
Li2 S2 Li3 67.6(2) 3_565 3_565 ?
Li3 S2 Cs1 133.01(16) 3_565 . ?
Li3 S2 Cs1 151.20(16) 3_565 1_455 ?
Li3 S2 Li2 82.8(2) 3_565 3_465 ?
O9A S2 Cs1 81.2(6) . 1_455 ?
O9A S2 Cs1 59.8(5) . . ?
O9A S2 Li2 87.0(6) . 3_465 ?
O9A S2 Li2 57.8(6) . 3_565 ?
O9A S2 Li3 115.6(6) . 3_565 ?
O9B S2 Cs1 61.6(7) . . ?
O9B S2 Cs1 51.6(4) . 1_455 ?
O9B S2 Li2 76.7(7) . 3_465 ?
O9B S2 Li2 87.5(5) . 3_565 ?
O9B S2 Li3 139.3(6) . 3_565 ?
O9B S2 O9A 29.8(6) . . ?
O9B S2 O10 103.1(7) . . ?
O9B S2 O12 122.1(4) . . ?
O10 S2 Cs1 150.23(17) . . ?
O10 S2 Cs1 75.47(17) . 1_455 ?
O10 S2 Li2 133.3(2) . 3_565 ?
O10 S2 Li2 34.1(2) . 3_465 ?
O10 S2 Li3 75.8(2) . 3_565 ?
O10 S2 O9A 120.3(6) . . ?
O11 S2 Cs1 72.31(19) . 1_455 ?
O11 S2 Cs1 54.66(17) . . ?
O11 S2 Li2 137.3(2) . 3_465 ?
O11 S2 Li2 111.4(2) . 3_565 ?
O11 S2 Li3 116.6(2) . 3_565 ?
O11 S2 O9A 113.3(6) . . ?
O11 S2 O9B 102.1(7) . . ?
O11 S2 O10 110.4(2) . . ?
O11 S2 O12 111.6(3) . . ?
O12 S2 Cs1 173.7(2) . 1_455 ?
O12 S2 Cs1 102.69(17) . . ?
O12 S2 Li2 37.0(2) . 3_565 ?
O12 S2 Li2 104.1(3) . 3_465 ?
O12 S2 Li3 32.2(2) . 3_565 ?
O12 S2 O9A 92.6(6) . . ?
O12 S2 O10 107.0(2) . . ?
Li2 S3 Cs1 70.43(16) 1_655 . ?
Li2 S3 Li5 118.0(2) 1_655 2_645 ?
Li3 S3 Cs1 77.79(15) . . ?
Li3 S3 Cs1 133.79(16) 1_655 . ?
Li3 S3 Li2 82.6(2) . 1_655 ?
Li3 S3 Li2 67.4(2) 1_655 1_655 ?
Li3 S3 Li3 113.9(2) 1_655 . ?
Li3 S3 Li4 122.5(2) 1_655 1_655 ?
Li3 S3 Li4 121.6(2) . 1_655 ?
Li3 S3 Li5 149.7(2) . 2_645 ?
Li3 S3 Li5 61.9(2) 1_655 2_645 ?
Li4 S3 Cs1 74.54(14) 1_655 . ?
Li4 S3 Li2 131.2(2) 1_655 1_655 ?
Li4 S3 Li5 62.9(2) 1_655 2_645 ?
Li5 S3 Cs1 128.40(16) 2_645 . ?
O5 S3 Cs1 146.70(12) . . ?
O5 S3 Li2 80.7(2) . 1_655 ?
O5 S3 Li3 82.47(19) . . ?
O5 S3 Li3 37.13(19) . 1_655 ?
O5 S3 Li4 138.69(19) . 1_655 ?
O5 S3 Li5 79.69(19) . 2_645 ?
O6 S3 Cs1 65.66(14) . . ?
O6 S3 Li2 106.7(2) . 1_655 ?
O6 S3 Li3 33.68(19) . . ?
O6 S3 Li3 145.3(2) . 1_655 ?
O6 S3 Li4 87.97(19) . 1_655 ?
O6 S3 Li5 135.3(2) . 2_645 ?
O6 S3 O5 109.19(18) . . ?
O7 S3 Cs1 103.77(13) . . ?
O7 S3 Li2 136.8(2) . 1_655 ?
O7 S3 Li3 139.4(2) . . ?
O7 S3 Li3 94.4(2) . 1_655 ?
O7 S3 Li4 30.95(18) . 1_655 ?
O7 S3 Li5 32.76(19) . 2_645 ?
O7 S3 O5 108.65(17) . . ?
O7 S3 O6 109.21(18) . . ?
O8 S3 Cs1 49.86(14) . . ?
O8 S3 Li2 32.8(2) . 1_655 ?
O8 S3 Li3 101.2(2) . . ?
O8 S3 Li3 84.0(2) . 1_655 ?
O8 S3 Li4 98.44(19) . 1_655 ?
O8 S3 Li5 107.8(2) . 2_645 ?
O8 S3 O5 109.72(19) . . ?
O8 S3 O6 109.5(2) . . ?
O8 S3 O7 110.50(19) . . ?
Li1 O1 Cs1 88.6(3) 1_455 1_455 ?
Li3 O1 Cs1 118.8(3) 2 1_455 ?
Li3 O1 Li1 93.8(4) 2 1_455 ?
S1 O1 Cs1 105.70(16) . 1_455 ?
S1 O1 Li1 115.6(3) . 1_455 ?
S1 O1 Li3 127.0(3) . 2 ?
Cs1 O2 Cs1 88.56(8) 1_455 . ?
Li4 O2 Cs1 114.8(3) . . ?
Li4 O2 Cs1 105.8(3) . 1_455 ?
S1 O2 Cs1 93.93(16) . . ?
S1 O2 Cs1 102.93(16) . 1_455 ?
S1 O2 Li4 139.3(3) . . ?
Li4 O3 Li5 111.1(4) 3_466 4_576 ?
S1 O3 Li4 125.1(3) . 3_466 ?
S1 O3 Li5 121.6(3) . 4_576 ?
Li1 O4 Cs1 87.0(3) . . ?
Li4 O4 Cs1 115.0(2) 3_566 . ?
Li4 O4 Li1 99.5(3) 3_566 . ?
S1 O4 Cs1 94.82(13) . . ?
S1 O4 Li1 134.7(3) . . ?
S1 O4 Li4 120.0(3) . 3_566 ?
Li1 O5 Cs1 90.8(3) 2_645 2_645 ?
Li3 O5 Cs1 107.1(3) 1_655 2_645 ?
Li3 O5 Li1 90.4(4) 1_655 2_645 ?
S3 O5 Cs1 122.48(16) . 2_645 ?
S3 O5 Li1 123.8(3) . 2_645 ?
S3 O5 Li3 115.8(3) . 1_655 ?
Li3 O6 Cs1 101.2(3) . . ?
Li3 O6 Li5 104.9(4) . 2_545 ?
Li5 O6 Cs1 99.3(3) 2_545 . ?
S3 O6 Cs1 93.22(15) . . ?
S3 O6 Li3 121.0(3) . . ?
S3 O6 Li5 128.8(3) . 2_545 ?
Li4 O7 Li5 108.5(3) 1_655 2_645 ?
S3 O7 Li4 126.0(3) . 1_655 ?
S3 O7 Li5 123.6(3) . 2_645 ?
Cs1 O8 Cs1 94.93(8) . 1_655 ?
Li2 O8 Cs1 92.3(3) 1_655 1_655 ?
Li2 O8 Cs1 101.1(3) 1_655 . ?
S3 O8 Cs1 127.89(18) . 1_655 ?
S3 O8 Cs1 110.70(18) . . ?
S3 O8 Li2 123.8(3) . 1_655 ?
Li2 O9A Cs1 89.3(5) 3_565 . ?
Li2 O9A Cs1 89.0(5) . . ?
Li2 O9A Li2 109.8(6) . 3_565 ?
S2 O9A Cs1 99.4(6) . . ?
S2 O9A Li2 92.7(7) . 3_565 ?
S2 O9A Li2 156.2(11) . . ?
O9B O9A Cs1 88(2) . . ?
O9B O9A Li2 85.0(19) . . ?
O9B O9A Li2 165(2) . 3_565 ?
O9B O9A S2 73.2(16) . . ?
Cs1 O9B Cs1 90.7(4) 1_455 . ?
Li2 O9B Cs1 86.3(6) . . ?
Li2 O9B Cs1 103.6(5) . 1_455 ?
S2 O9B Cs1 108.5(5) . 1_455 ?
S2 O9B Cs1 97.8(8) . . ?
S2 O9B Li2 147.5(7) . . ?
O9A O9B Cs1 80(2) . . ?
O9A O9B Cs1 170(2) . 1_455 ?
O9A O9B Li2 72.0(17) . . ?
O9A O9B S2 76.9(17) . . ?
Li2 O10 Li1 99.8(4) 3_465 4_475 ?
S2 O10 Li1 131.3(4) . 4_475 ?
S2 O10 Li2 121.4(3) . 3_465 ?
Li5 O11 Cs1 115.2(3) . . ?
S2 O11 Cs1 105.5(2) . . ?
S2 O11 Li5 136.1(4) . . ?
Li2 O12 Li1 80.9(3) 3_565 4_575 ?
Li3 O12 Li1 76.0(3) 3_565 4_575 ?
Li3 O12 Li2 114.8(4) 3_565 3_565 ?
S2 O12 Li1 130.6(3) . 4_575 ?
S2 O12 Li2 117.2(3) . 3_565 ?
S2 O12 Li3 124.1(4) . 3_565 ?

_olex2_submission_special_instructions 'No special instructions were received'
