# Electronic Supplementary Material (ESI) for Nanoscale.
# This journal is © The Royal Society of Chemistry 2021

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_1
_database_code_depnum_ccdc_archive 'CCDC 1985876'
loop_
_audit_author_name
_audit_author_address
'Chen-Wei Chiu'
;Department of Chemistry, National Dong Hwa University
Taiwan
;
_audit_update_record             
;
2020-02-24 deposited with the CCDC.	2021-06-25 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2018/3
_shelx_SHELXL_version_number     2018/3
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C72 H168 Ag20 O24 P12 Pt Se24'
_chemical_formula_weight         6037.22

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Se Se -0.0929 2.2259 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      monoclinic
_space_group_IT_number           4
_space_group_name_H-M_alt        'P 21'
_space_group_name_Hall           'P 2yb'

_shelx_space_group_comment       
; 
The symmetry employed for this shelxl refinement is uniquely defined 
by the following loop, which should always be used as a source of 
symmetry information in preference to the above space-group names. 
They are only intended as comments. 
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z'

_cell_length_a                   15.9963(6)
_cell_length_b                   29.4039(11)
_cell_length_c                   16.5323(6)
_cell_angle_alpha                90
_cell_angle_beta                 107.5256(8)
_cell_angle_gamma                90
_cell_volume                     7415.1(5)
_cell_formula_units_Z            2
_cell_measurement_temperature    150(2)
_cell_measurement_reflns_used    9655
_cell_measurement_theta_min      2.45
_cell_measurement_theta_max      27.12

_exptl_crystal_description       plate
_exptl_crystal_colour            red
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    2.704
_exptl_crystal_F_000             5612
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          0.300
_exptl_crystal_size_mid          0.180
_exptl_crystal_size_min          0.040
_exptl_absorpt_coefficient_mu    9.582
_shelx_estimated_absorpt_T_min   0.161
_shelx_estimated_absorpt_T_max   0.700
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_correction_T_min  0.3423
_exptl_absorpt_correction_T_max  0.7455
_exptl_absorpt_process_details   SADABS
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      150(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_source                   ?
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            42098
_diffrn_reflns_av_unetI/netI     0.0548
_diffrn_reflns_av_R_equivalents  0.0340
_diffrn_reflns_limit_h_min       -19
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_k_min       -34
_diffrn_reflns_limit_k_max       23
_diffrn_reflns_limit_l_min       -19
_diffrn_reflns_limit_l_max       19
_diffrn_reflns_theta_min         1.335
_diffrn_reflns_theta_max         25.000
_diffrn_reflns_theta_full        25.000
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measured_fraction_theta_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.999
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.745
_diffrn_reflns_point_group_measured_fraction_full 0.745
_reflns_number_total             19437
_reflns_number_gt                18097
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.459
_reflns_Friedel_fraction_max     0.479
_reflns_Friedel_fraction_full    0.479

_reflns_special_details          
; 
 Reflections were merged by SHELXL according to the crystal 
 class for the calculation of statistics and refinement. 
  
 _reflns_Friedel_fraction is defined as the number of unique 
 Friedel pairs measured divided by the number that would be 
 possible theoretically, ignoring centric projections and 
 systematic absences. Completness statistics refer to single and 
 composite reflections containing twin component 1 only. 
;

_computing_data_collection       'Bruker APEX2'
_computing_cell_refinement       'Bruker SAINT'
_computing_data_reduction        'Bruker SAINT'
_computing_structure_solution    'SHELXS-97 (Sheldrick 2008)'
_computing_structure_refinement  'SHELXL-2018/3 (Sheldrick, 2018)'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_refine_special_details          
; 
 Refined as a 2-component inversion twin. 
;
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0546P)²+22.1413P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_abs_structure_details 
; 
 Refined as an inversion twin. 
;
_refine_ls_abs_structure_Flack   0.139(8)
_chemical_absolute_configuration ?
_refine_ls_number_reflns         19437
_refine_ls_number_parameters     1394
_refine_ls_number_restraints     462
_refine_ls_R_factor_all          0.0428
_refine_ls_R_factor_gt           0.0380
_refine_ls_wR_factor_ref         0.0989
_refine_ls_wR_factor_gt          0.0957
_refine_ls_goodness_of_fit_ref   1.053
_refine_ls_restrained_S_all      1.246
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt1 Pt 0.19483(4) 0.33645(2) 0.39237(4) 0.01171(11) Uani 1 1 d . . . . .
Ag1 Ag 0.21312(7) 0.41081(4) 0.29676(7) 0.0182(2) Uani 1 1 d . . . . .
Ag2 Ag 0.29591(7) 0.40966(4) 0.47585(7) 0.0201(2) Uani 1 1 d . . . . .
Ag3 Ag 0.35406(7) 0.34747(4) 0.36421(7) 0.0188(2) Uani 1 1 d . . . . .
Ag4 Ag 0.18914(8) 0.35620(4) 0.55310(7) 0.0202(2) Uani 1 1 d . . . . .
Ag5 Ag 0.33875(7) 0.31454(4) 0.52697(7) 0.0192(2) Uani 1 1 d . . . . .
Ag6 Ag 0.28599(7) 0.25926(4) 0.37688(7) 0.0193(2) Uani 1 1 d . . . . .
Ag7 Ag 0.20167(7) 0.31832(4) 0.23034(7) 0.0193(2) Uani 1 1 d . . . . .
Ag8 Ag 0.05038(7) 0.35785(4) 0.25812(7) 0.0199(2) Uani 1 1 d . . . . .
Ag9 Ag 0.10575(7) 0.41393(4) 0.41190(7) 0.0199(2) Uani 1 1 d . . . . .
Ag10 Ag 0.03379(7) 0.32611(4) 0.41987(7) 0.0208(2) Uani 1 1 d . . . . .
Ag11 Ag 0.09541(7) 0.26399(4) 0.31117(7) 0.0198(2) Uani 1 1 d . . . . .
Ag12 Ag 0.17768(7) 0.26246(4) 0.48908(7) 0.0195(2) Uani 1 1 d . . . . .
Ag13 Ag 0.48322(7) 0.37741(4) 0.52582(8) 0.0225(3) Uani 1 1 d . . . . .
Ag14 Ag 0.19399(8) 0.45565(4) 0.57756(8) 0.0260(3) Uani 1 1 d . . . . .
Ag15 Ag 0.34684(8) 0.21482(4) 0.54465(8) 0.0248(3) Uani 1 1 d . . . . .
Ag16 Ag 0.06573(8) 0.29174(4) 0.59618(8) 0.0253(3) Uani 1 1 d . . . . .
Ag17 Ag 0.32357(7) 0.38371(4) 0.19162(8) 0.0219(3) Uani 1 1 d . . . . .
Ag18 Ag 0.04203(8) 0.45851(4) 0.24529(8) 0.0232(3) Uani 1 1 d . . . . .
Ag19 Ag 0.19778(8) 0.21810(4) 0.21012(8) 0.0255(3) Uani 1 1 d . . . . .
Ag20 Ag -0.08798(8) 0.29308(4) 0.26203(8) 0.0261(3) Uani 1 1 d . . . . .
C1 C 0.1803(13) 0.2220(7) 0.8126(11) 0.037(4) Uani 1 1 d . . . . .
H1A H 0.233916 0.218241 0.861288 0.044 Uiso 1 1 calc R U . . .
H1B H 0.183719 0.251752 0.785627 0.044 Uiso 1 1 calc R U . . .
C2 C 0.1026(13) 0.2208(7) 0.8422(11) 0.043(4) Uani 1 1 d . . . . .
H2A H 0.110753 0.242566 0.889629 0.052 Uiso 1 1 calc R U . . .
H2B H 0.096995 0.189997 0.864221 0.052 Uiso 1 1 calc R U . . .
C3 C 0.0184(13) 0.2325(7) 0.7730(13) 0.045(4) Uani 1 1 d . . . . .
H3A H 0.023680 0.262789 0.750447 0.068 Uiso 1 1 calc R U . . .
H3B H -0.030842 0.232141 0.796757 0.068 Uiso 1 1 calc R U . . .
H3C H 0.008071 0.209996 0.727288 0.068 Uiso 1 1 calc R U . . .
C4 C 0.2893(15) 0.1120(7) 0.6904(15) 0.054(6) Uani 1 1 d . . . . .
H4A H 0.291931 0.110492 0.750931 0.065 Uiso 1 1 calc R U . . .
H4B H 0.342876 0.127576 0.686812 0.065 Uiso 1 1 calc R U . . .
C5 C 0.2877(16) 0.0664(7) 0.6578(18) 0.064(7) Uani 1 1 d . . . . .
H5A H 0.282176 0.068004 0.596629 0.077 Uiso 1 1 calc R U . . .
H5B H 0.235128 0.050516 0.663533 0.077 Uiso 1 1 calc R U . . .
C6 C 0.3661(15) 0.0394(8) 0.7011(17) 0.063(7) Uani 1 1 d . . . . .
H6A H 0.416626 0.051054 0.685749 0.095 Uiso 1 1 calc R U . . .
H6B H 0.356083 0.007471 0.683636 0.095 Uiso 1 1 calc R U . . .
H6C H 0.377549 0.041620 0.762617 0.095 Uiso 1 1 calc R U . . .
C7 C -0.206(3) 0.1951(10) 0.509(2) 0.17(2) Uani 1 1 d D . . . .
H7A H -0.190205 0.178453 0.463828 0.207 Uiso 1 1 calc R U . . .
H7B H -0.269469 0.201316 0.488868 0.207 Uiso 1 1 calc R U . . .
C8 C -0.188(3) 0.1644(11) 0.586(2) 0.135(15) Uani 1 1 d D . . . .
H8A H -0.220862 0.135817 0.569070 0.162 Uiso 1 1 calc R U . . .
H8B H -0.124476 0.156597 0.604560 0.162 Uiso 1 1 calc R U . . .
C9 C -0.211(2) 0.1841(15) 0.660(2) 0.129(14) Uani 1 1 d D . . . .
H9A H -0.196780 0.162000 0.706747 0.193 Uiso 1 1 calc R U . . .
H9B H -0.176808 0.211977 0.678954 0.193 Uiso 1 1 calc R U . . .
H9C H -0.273404 0.191152 0.643386 0.193 Uiso 1 1 calc R U . . .
C10 C -0.3023(15) 0.2748(9) 0.3209(13) 0.078(7) Uani 1 1 d D U . . .
H10A H -0.264813 0.271404 0.283294 0.093 Uiso 1 1 calc R U . . .
H10B H -0.341591 0.301017 0.299353 0.093 Uiso 1 1 calc R U . . .
C11 C -0.359(2) 0.2329(12) 0.311(2) 0.128(10) Uani 1 1 d D U . . .
H11A H -0.399832 0.235157 0.344813 0.153 Uiso 1 1 calc R U . . .
H11B H -0.322408 0.205250 0.327664 0.153 Uiso 1 1 calc R U . . .
C12 C -0.408(2) 0.2322(12) 0.216(2) 0.107(10) Uani 1 1 d D U . . .
H12A H -0.465564 0.217796 0.206882 0.161 Uiso 1 1 calc R U . . .
H12B H -0.374431 0.214852 0.185762 0.161 Uiso 1 1 calc R U . . .
H12C H -0.416358 0.263384 0.194111 0.161 Uiso 1 1 calc R U . . .
C13 C -0.0511(15) 0.1933(8) -0.0223(11) 0.057(5) Uani 1 1 d D . . . .
H13A H -0.019605 0.175037 -0.054164 0.069 Uiso 1 1 calc R U . . .
H13B H -0.027078 0.224577 -0.018022 0.069 Uiso 1 1 calc R U . . .
C14 C -0.1431(18) 0.1954(9) -0.073(2) 0.089(9) Uani 1 1 d D . . . .
H14A H -0.148330 0.210461 -0.127912 0.107 Uiso 1 1 calc R U . . .
H14B H -0.176539 0.213558 -0.042821 0.107 Uiso 1 1 calc R U . . .
C15 C -0.1801(18) 0.1480(9) -0.088(2) 0.099(11) Uani 1 1 d D . . . .
H15A H -0.141805 0.128952 -0.110586 0.149 Uiso 1 1 calc R U . . .
H15B H -0.238782 0.149056 -0.129591 0.149 Uiso 1 1 calc R U . . .
H15C H -0.183933 0.135137 -0.034893 0.149 Uiso 1 1 calc R U . . .
C16 C -0.1485(19) 0.1401(9) 0.174(3) 0.128(14) Uani 1 1 d D . . . .
H16A H -0.107400 0.131144 0.229821 0.153 Uiso 1 1 calc R U . . .
H16B H -0.140815 0.118466 0.131262 0.153 Uiso 1 1 calc R U . . .
C17 C -0.2412(17) 0.1362(11) 0.179(2) 0.105(11) Uani 1 1 d D . . . .
H17A H -0.250742 0.159825 0.217797 0.126 Uiso 1 1 calc R U . . .
H17B H -0.248678 0.106168 0.202608 0.126 Uiso 1 1 calc R U . . .
C18 C -0.310(3) 0.142(2) 0.093(3) 0.18(2) Uani 1 1 d D . . . .
H18A H -0.368348 0.138813 0.099903 0.277 Uiso 1 1 calc R U . . .
H18B H -0.303670 0.171631 0.069736 0.277 Uiso 1 1 calc R U . . .
H18C H -0.301605 0.117945 0.054539 0.277 Uiso 1 1 calc R U . . .
C19 C 0.4582(15) 0.0979(10) 0.4976(19) 0.088(9) Uani 1 1 d D . . . .
H19A H 0.439745 0.066350 0.480224 0.106 Uiso 1 1 calc R U . . .
H19B H 0.428081 0.108206 0.538567 0.106 Uiso 1 1 calc R U . . .
C20 C 0.5574(15) 0.1004(9) 0.5371(16) 0.085(8) Uani 1 1 d D . . . .
H20A H 0.586574 0.086878 0.497811 0.102 Uiso 1 1 calc R U . . .
H20B H 0.575801 0.132607 0.546484 0.102 Uiso 1 1 calc R U . . .
C21 C 0.585(2) 0.0753(10) 0.6201(15) 0.085(9) Uani 1 1 d D . . . .
H21A H 0.649104 0.077284 0.644579 0.127 Uiso 1 1 calc R U . . .
H21B H 0.557074 0.089009 0.659301 0.127 Uiso 1 1 calc R U . . .
H21C H 0.567831 0.043348 0.610700 0.127 Uiso 1 1 calc R U . . .
C22 C 0.285(4) 0.0561(9) 0.306(3) 0.27(5) Uani 1 1 d D . . . .
H22A H 0.253730 0.048381 0.347919 0.328 Uiso 1 1 calc R U . . .
H22B H 0.339666 0.037900 0.319341 0.328 Uiso 1 1 calc R U . . .
C23 C 0.227(3) 0.0477(11) 0.2160(18) 0.144(17) Uani 1 1 d D . . . .
H23A H 0.262121 0.042578 0.176409 0.173 Uiso 1 1 calc R U . . .
H23B H 0.184773 0.072578 0.194726 0.173 Uiso 1 1 calc R U . . .
C24 C 0.183(3) 0.0042(12) 0.233(3) 0.18(2) Uani 1 1 d D . . . .
H24A H 0.142084 -0.006822 0.180317 0.274 Uiso 1 1 calc R U . . .
H24B H 0.228087 -0.019085 0.256346 0.274 Uiso 1 1 calc R U . . .
H24C H 0.151706 0.010540 0.274434 0.274 Uiso 1 1 calc R U . . .
C25 C 0.335(2) 0.1989(9) 0.0677(16) 0.073(6) Uani 1 1 d D U . . .
H25A H 0.303154 0.192828 0.109084 0.088 Uiso 1 1 calc R U . . .
H25B H 0.397195 0.205561 0.099988 0.088 Uiso 1 1 calc R U . . .
C26 C 0.332(2) 0.1571(11) 0.014(2) 0.120(10) Uani 1 1 d D U . . .
H26A H 0.327511 0.165331 -0.045530 0.143 Uiso 1 1 calc R U . . .
H26B H 0.282781 0.137053 0.014254 0.143 Uiso 1 1 calc R U . . .
C27 C 0.420(3) 0.135(2) 0.058(4) 0.22(2) Uani 1 1 d D U . . .
H27A H 0.425782 0.106652 0.027882 0.335 Uiso 1 1 calc R U . . .
H27B H 0.467858 0.155564 0.057326 0.335 Uiso 1 1 calc R U . . .
H27C H 0.423517 0.127531 0.116591 0.335 Uiso 1 1 calc R U . . .
C28 C 0.3208(10) 0.3394(6) -0.0468(10) 0.027(3) Uani 1 1 d . . . . .
H28A H 0.358431 0.355998 0.003041 0.032 Uiso 1 1 calc R U . . .
H28B H 0.291922 0.362336 -0.090140 0.032 Uiso 1 1 calc R U . . .
C29 C 0.3769(13) 0.3103(7) -0.0814(14) 0.043(5) Uani 1 1 d . . . . .
H29A H 0.339106 0.289547 -0.124098 0.052 Uiso 1 1 calc R U . . .
H29B H 0.414460 0.291479 -0.034999 0.052 Uiso 1 1 calc R U . . .
C30 C 0.4351(13) 0.3370(8) -0.1225(13) 0.048(5) Uani 1 1 d . . . . .
H30A H 0.399831 0.359983 -0.160861 0.072 Uiso 1 1 calc R U . . .
H30B H 0.460852 0.316192 -0.154661 0.072 Uiso 1 1 calc R U . . .
H30C H 0.481944 0.352058 -0.078356 0.072 Uiso 1 1 calc R U . . .
C31 C 0.5810(18) 0.2002(9) 0.7435(16) 0.072(6) Uani 1 1 d D U . . .
H31A H 0.645532 0.203927 0.763152 0.086 Uiso 1 1 calc R U . . .
H31B H 0.565502 0.181960 0.690707 0.086 Uiso 1 1 calc R U . . .
C32 C 0.552(2) 0.1753(10) 0.8105(18) 0.101(9) Uani 1 1 d D U . . .
H32A H 0.490973 0.164839 0.784345 0.122 Uiso 1 1 calc R U . . .
H32B H 0.588979 0.147812 0.827225 0.122 Uiso 1 1 calc R U . . .
C33 C 0.555(3) 0.2011(13) 0.890(2) 0.136(13) Uani 1 1 d D U . . .
H33A H 0.535018 0.181518 0.927948 0.205 Uiso 1 1 calc R U . . .
H33B H 0.615629 0.210823 0.917940 0.205 Uiso 1 1 calc R U . . .
H33C H 0.517250 0.227915 0.874896 0.205 Uiso 1 1 calc R U . . .
C34 C 0.6904(13) 0.2988(9) 0.6121(15) 0.066(6) Uani 1 1 d D . . . .
H34A H 0.649420 0.318406 0.569552 0.079 Uiso 1 1 calc R U . . .
H34B H 0.709348 0.273646 0.581857 0.079 Uiso 1 1 calc R U . . .
C35 C 0.7695(15) 0.3263(11) 0.662(2) 0.102(11) Uani 1 1 d D . . . .
H35A H 0.801650 0.309383 0.713824 0.122 Uiso 1 1 calc R U . . .
H35B H 0.809529 0.330683 0.627216 0.122 Uiso 1 1 calc R U . . .
C36 C 0.742(2) 0.3721(11) 0.687(3) 0.133(16) Uani 1 1 d D . . . .
H36A H 0.693283 0.384035 0.640118 0.199 Uiso 1 1 calc R U . . .
H36B H 0.791597 0.393259 0.698303 0.199 Uiso 1 1 calc R U . . .
H36C H 0.723217 0.368872 0.737611 0.199 Uiso 1 1 calc R U . . .
C37 C 0.0632(12) 0.3572(7) 0.8438(11) 0.036(4) Uani 1 1 d . . . . .
H37A H 0.108129 0.374727 0.886716 0.044 Uiso 1 1 calc R U . . .
H37B H 0.088078 0.326999 0.837667 0.044 Uiso 1 1 calc R U . . .
C38 C -0.0167(13) 0.3514(9) 0.8724(13) 0.053(5) Uani 1 1 d . . . . .
H38A H -0.000852 0.334377 0.926599 0.064 Uiso 1 1 calc R U . . .
H38B H -0.061074 0.333355 0.829688 0.064 Uiso 1 1 calc R U . . .
C39 C -0.0563(14) 0.3979(10) 0.8845(14) 0.060(6) Uani 1 1 d . . . . .
H39A H -0.012429 0.415808 0.926668 0.090 Uiso 1 1 calc R U . . .
H39B H -0.107651 0.393155 0.904224 0.090 Uiso 1 1 calc R U . . .
H39C H -0.074018 0.414305 0.830403 0.090 Uiso 1 1 calc R U . . .
C40 C 0.1574(13) 0.4652(6) 0.8253(13) 0.044(5) Uani 1 1 d D . . . .
H40A H 0.146440 0.459767 0.880394 0.053 Uiso 1 1 calc R U . . .
H40B H 0.103063 0.477411 0.784892 0.053 Uiso 1 1 calc R U . . .
C41 C 0.2321(14) 0.4986(7) 0.8363(18) 0.077(7) Uani 1 1 d D . . . .
H41A H 0.237209 0.506117 0.779595 0.092 Uiso 1 1 calc R U . . .
H41B H 0.217460 0.527002 0.861159 0.092 Uiso 1 1 calc R U . . .
C42 C 0.3199(16) 0.4818(11) 0.8915(15) 0.093(10) Uani 1 1 d D . . . .
H42A H 0.320085 0.481099 0.950824 0.140 Uiso 1 1 calc R U . . .
H42B H 0.366210 0.502207 0.885844 0.140 Uiso 1 1 calc R U . . .
H42C H 0.330459 0.451048 0.873710 0.140 Uiso 1 1 calc R U . . .
C43 C -0.2940(18) 0.3375(11) 0.065(2) 0.102(11) Uani 1 1 d D . . . .
H43A H -0.341169 0.360278 0.044671 0.122 Uiso 1 1 calc R U . . .
H43B H -0.297706 0.324684 0.119669 0.122 Uiso 1 1 calc R U . . .
C44 C -0.301(3) 0.3002(15) 0.000(3) 0.18(2) Uani 1 1 d D . . . .
H44A H -0.257703 0.276454 0.027520 0.217 Uiso 1 1 calc R U . . .
H44B H -0.359672 0.286308 -0.011154 0.217 Uiso 1 1 calc R U . . .
C45 C -0.288(3) 0.3103(19) -0.085(3) 0.20(2) Uani 1 1 d D . . . .
H45A H -0.294864 0.282237 -0.118692 0.293 Uiso 1 1 calc R U . . .
H45B H -0.331771 0.332609 -0.115867 0.293 Uiso 1 1 calc R U . . .
H45C H -0.229081 0.322685 -0.076920 0.293 Uiso 1 1 calc R U . . .
C46 C -0.2139(12) 0.4772(6) 0.1609(14) 0.041(4) Uani 1 1 d . . . . .
H46A H -0.150319 0.483644 0.182635 0.049 Uiso 1 1 calc R U . . .
H46B H -0.236831 0.474774 0.210102 0.049 Uiso 1 1 calc R U . . .
C47 C -0.2574(16) 0.5140(7) 0.1070(17) 0.064(6) Uani 1 1 d . . . . .
H47A H -0.254865 0.541860 0.141460 0.076 Uiso 1 1 calc R U . . .
H47B H -0.319841 0.506216 0.080153 0.076 Uiso 1 1 calc R U . . .
C48 C -0.211(2) 0.5234(10) 0.0352(19) 0.089(8) Uani 1 1 d . . . . .
H48A H -0.225362 0.554139 0.012535 0.133 Uiso 1 1 calc R U . . .
H48B H -0.231911 0.501157 -0.010680 0.133 Uiso 1 1 calc R U . . .
H48C H -0.147328 0.520472 0.059786 0.133 Uiso 1 1 calc R U . . .
C49 C 0.0555(15) 0.5864(7) 0.5480(16) 0.057(6) Uani 1 1 d D . . . .
H49A H 0.062426 0.611507 0.510588 0.068 Uiso 1 1 calc R U . . .
H49B H 0.113415 0.579875 0.589220 0.068 Uiso 1 1 calc R U . . .
C50 C -0.0090(18) 0.5996(7) 0.5938(16) 0.070(7) Uani 1 1 d D . . . .
H50A H -0.065540 0.607509 0.551453 0.084 Uiso 1 1 calc R U . . .
H50B H 0.012831 0.627128 0.628204 0.084 Uiso 1 1 calc R U . . .
C51 C -0.025(2) 0.5627(8) 0.6511(16) 0.080(9) Uani 1 1 d D . . . .
H51A H -0.043226 0.534797 0.618227 0.121 Uiso 1 1 calc R U . . .
H51B H -0.070645 0.572462 0.675375 0.121 Uiso 1 1 calc R U . . .
H51C H 0.029576 0.556950 0.696935 0.121 Uiso 1 1 calc R U . . .
C52 C -0.0324(12) 0.5939(7) 0.3266(10) 0.038(4) Uani 1 1 d D . . . .
H52A H -0.027042 0.626986 0.338511 0.045 Uiso 1 1 calc R U . . .
H52B H -0.075699 0.581156 0.352389 0.045 Uiso 1 1 calc R U . . .
C53 C -0.0616(12) 0.5856(7) 0.2322(10) 0.049(5) Uani 1 1 d D . . . .
H53A H -0.118860 0.600659 0.206766 0.058 Uiso 1 1 calc R U . . .
H53B H -0.069784 0.552572 0.221571 0.058 Uiso 1 1 calc R U . . .
C54 C 0.0034(14) 0.6033(7) 0.1894(14) 0.057(6) Uani 1 1 d D . . . .
H54A H 0.006711 0.636496 0.194008 0.086 Uiso 1 1 calc R U . . .
H54B H -0.015836 0.594544 0.129386 0.086 Uiso 1 1 calc R U . . .
H54C H 0.061326 0.590197 0.216998 0.086 Uiso 1 1 calc R U . . .
C55 C 0.3266(17) 0.5428(11) 0.142(2) 0.092(9) Uani 1 1 d D . . . .
H55A H 0.322861 0.548272 0.200403 0.110 Uiso 1 1 calc R U . . .
H55B H 0.291852 0.566627 0.104666 0.110 Uiso 1 1 calc R U . . .
C56 C 0.4216(18) 0.5458(18) 0.143(3) 0.17(2) Uani 1 1 d D . . . .
H56A H 0.454307 0.567338 0.187495 0.207 Uiso 1 1 calc R U . . .
H56B H 0.449931 0.515579 0.155130 0.207 Uiso 1 1 calc R U . . .
C57 C 0.421(4) 0.562(2) 0.057(3) 0.24(3) Uani 1 1 d D . . . .
H57A H 0.481304 0.564592 0.054492 0.367 Uiso 1 1 calc R U . . .
H57B H 0.388349 0.540587 0.013570 0.367 Uiso 1 1 calc R U . . .
H57C H 0.392705 0.592107 0.045787 0.367 Uiso 1 1 calc R U . . .
C58 C 0.0413(13) 0.5137(8) 0.0340(14) 0.048(5) Uani 1 1 d . . . . .
H58A H 0.024664 0.517830 0.086583 0.057 Uiso 1 1 calc R U . . .
H58B H 0.019698 0.483712 0.009404 0.057 Uiso 1 1 calc R U . . .
C59 C 0.0019(15) 0.5508(8) -0.0280(14) 0.055(5) Uani 1 1 d . . . . .
H59A H -0.062581 0.549671 -0.040612 0.066 Uiso 1 1 calc R U . . .
H59B H 0.022129 0.580438 -0.000857 0.066 Uiso 1 1 calc R U . . .
C60 C 0.0225(18) 0.5486(10) -0.1064(15) 0.073(7) Uani 1 1 d . . . . .
H60A H 0.085494 0.543211 -0.094774 0.109 Uiso 1 1 calc R U . . .
H60B H 0.006516 0.577374 -0.136978 0.109 Uiso 1 1 calc R U . . .
H60C H -0.010385 0.523661 -0.141020 0.109 Uiso 1 1 calc R U . . .
C61 C 0.7015(10) 0.4075(6) 0.4242(13) 0.039(4) Uani 1 1 d D . . . .
H61A H 0.717150 0.387273 0.382976 0.047 Uiso 1 1 calc R U . . .
H61B H 0.700672 0.389076 0.474070 0.047 Uiso 1 1 calc R U . . .
C62 C 0.7682(12) 0.4455(7) 0.4511(16) 0.067(7) Uani 1 1 d D . . . .
H62A H 0.827408 0.432059 0.473692 0.080 Uiso 1 1 calc R U . . .
H62B H 0.767359 0.463818 0.400560 0.080 Uiso 1 1 calc R U . . .
C63 C 0.7516(19) 0.4765(9) 0.5174(17) 0.089(9) Uani 1 1 d D . . . .
H63A H 0.689001 0.483739 0.502181 0.133 Uiso 1 1 calc R U . . .
H63B H 0.785280 0.504656 0.520492 0.133 Uiso 1 1 calc R U . . .
H63C H 0.769879 0.461274 0.572706 0.133 Uiso 1 1 calc R U . . .
C64 C 0.5832(12) 0.4101(7) 0.1963(11) 0.037(4) Uani 1 1 d . . . . .
H64A H 0.576233 0.441613 0.214386 0.044 Uiso 1 1 calc R U . . .
H64B H 0.644060 0.406571 0.194168 0.044 Uiso 1 1 calc R U . . .
C65 C 0.5221(17) 0.4021(11) 0.1122(13) 0.072(8) Uani 1 1 d . . . . .
H65A H 0.461335 0.404956 0.115080 0.086 Uiso 1 1 calc R U . . .
H65B H 0.529871 0.370734 0.094200 0.086 Uiso 1 1 calc R U . . .
C66 C 0.536(2) 0.4374(13) 0.043(2) 0.101(12) Uani 1 1 d . . . . .
H66A H 0.528909 0.468570 0.060555 0.151 Uiso 1 1 calc R U . . .
H66B H 0.492336 0.431408 -0.012255 0.151 Uiso 1 1 calc R U . . .
H66C H 0.594944 0.433619 0.037441 0.151 Uiso 1 1 calc R U . . .
C67 C 0.5697(19) 0.4471(8) 0.7453(16) 0.093(9) Uani 1 1 d D . . . .
H67A H 0.616083 0.440076 0.718934 0.111 Uiso 1 1 calc R U . . .
H67B H 0.532374 0.419850 0.741119 0.111 Uiso 1 1 calc R U . . .
C68 C 0.611(3) 0.4600(12) 0.8378(18) 0.143(17) Uani 1 1 d D . . . .
H68A H 0.641701 0.489363 0.840710 0.172 Uiso 1 1 calc R U . . .
H68B H 0.563659 0.464219 0.864559 0.172 Uiso 1 1 calc R U . . .
C69 C 0.675(3) 0.4248(16) 0.888(4) 0.23(3) Uani 1 1 d D . . . .
H69A H 0.675833 0.398582 0.851483 0.348 Uiso 1 1 calc R U . . .
H69B H 0.656766 0.414802 0.936639 0.348 Uiso 1 1 calc R U . . .
H69C H 0.733700 0.438136 0.907974 0.348 Uiso 1 1 calc R U . . .
C70 C 0.363(2) 0.5532(8) 0.683(2) 0.090(10) Uani 1 1 d D . . . .
H70A H 0.388994 0.542010 0.741212 0.107 Uiso 1 1 calc R U . . .
H70B H 0.298452 0.548533 0.666668 0.107 Uiso 1 1 calc R U . . .
C71 C 0.383(3) 0.6032(8) 0.677(3) 0.19(2) Uani 1 1 d D . . . .
H71A H 0.343434 0.623497 0.697009 0.225 Uiso 1 1 calc R U . . .
H71B H 0.385869 0.612746 0.620965 0.225 Uiso 1 1 calc R U . . .
C72 C 0.472(3) 0.597(2) 0.742(5) 0.32(5) Uani 1 1 d D . . . .
H72A H 0.502744 0.626409 0.752462 0.477 Uiso 1 1 calc R U . . .
H72B H 0.464764 0.585790 0.795461 0.477 Uiso 1 1 calc R U . . .
H72C H 0.506439 0.575231 0.720776 0.477 Uiso 1 1 calc R U . . .
O1 O 0.1742(7) 0.1848(4) 0.7505(7) 0.028(2) Uani 1 1 d . . . . .
O2 O 0.2151(7) 0.1377(4) 0.6456(7) 0.028(2) Uani 1 1 d . . . . .
O3 O -0.1606(11) 0.2373(5) 0.5223(10) 0.061(4) Uani 1 1 d D . . . .
O4 O -0.2467(8) 0.2866(6) 0.4030(10) 0.058(4) Uani 1 1 d D . . . .
O5 O -0.0299(10) 0.1752(5) 0.0616(9) 0.059(4) Uani 1 1 d D . . . .
O6 O -0.1261(9) 0.1842(6) 0.1538(13) 0.080(6) Uani 1 1 d D . . . .
O7 O 0.4371(10) 0.1282(6) 0.4231(10) 0.061(5) Uani 1 1 d . . . . .
O8 O 0.3035(18) 0.1032(6) 0.3078(14) 0.107(8) Uani 1 1 d D . . . .
O9 O 0.2992(8) 0.2368(4) 0.0194(7) 0.034(3) Uani 1 1 d . . . . .
O10 O 0.2541(7) 0.3152(4) -0.0217(7) 0.028(3) Uani 1 1 d . . . . .
O11 O 0.5415(8) 0.2426(5) 0.7268(8) 0.039(3) Uani 1 1 d . . . . .
O12 O 0.6470(8) 0.2806(5) 0.6697(9) 0.047(3) Uani 1 1 d . . . . .
O13 O 0.0396(7) 0.3810(4) 0.7629(7) 0.030(3) Uani 1 1 d . . . . .
O14 O 0.1829(7) 0.4233(4) 0.7932(7) 0.025(2) Uani 1 1 d . . . . .
O15 O -0.2119(8) 0.3568(5) 0.0756(10) 0.048(4) Uani 1 1 d . . . . .
O16 O -0.2275(8) 0.4354(4) 0.1157(9) 0.039(3) Uani 1 1 d . . . . .
O17 O 0.0219(8) 0.5465(4) 0.4984(8) 0.036(3) Uani 1 1 d . . . . .
O18 O 0.0509(7) 0.5721(4) 0.3612(8) 0.030(3) Uani 1 1 d . . . . .
O19 O 0.2922(9) 0.5003(5) 0.1144(9) 0.046(3) Uani 1 1 d . . . . .
O20 O 0.1357(8) 0.5161(5) 0.0529(8) 0.042(3) Uani 1 1 d . . . . .
O21 O 0.6174(7) 0.4274(4) 0.3861(7) 0.026(2) Uani 1 1 d . . . . .
O22 O 0.5671(7) 0.3777(4) 0.2584(7) 0.029(3) Uani 1 1 d . . . . .
O23 O 0.5184(11) 0.4842(7) 0.7027(11) 0.074(5) Uani 1 1 d D . . . .
O24 O 0.3968(13) 0.5298(5) 0.6278(12) 0.070(5) Uani 1 1 d . . . . .
P1 P 0.2003(3) 0.18983(14) 0.6653(3) 0.0237(9) Uani 1 1 d . . . . .
P2 P -0.1507(3) 0.26871(16) 0.4485(3) 0.0300(10) Uani 1 1 d . . . . .
P3 P -0.0404(3) 0.20149(17) 0.1422(3) 0.0331(11) Uani 1 1 d . . . . .
P4 P 0.3390(4) 0.14264(16) 0.3722(3) 0.0375(12) Uani 1 1 d . . . . .
P5 P 0.2760(3) 0.28246(14) 0.0585(3) 0.0222(9) Uani 1 1 d . . . . .
P6 P 0.5451(3) 0.27088(16) 0.6477(3) 0.0278(9) Uani 1 1 d . . . . .
P7 P 0.1131(3) 0.39489(14) 0.7207(3) 0.0238(9) Uani 1 1 d . . . . .
P8 P -0.1636(3) 0.39266(15) 0.1453(3) 0.0261(9) Uani 1 1 d . . . . .
P9 P 0.0621(3) 0.53078(14) 0.4268(3) 0.0228(9) Uani 1 1 d . . . . .
P10 P 0.1975(3) 0.48218(16) 0.1188(3) 0.0288(10) Uani 1 1 d . . . . .
P11 P 0.5380(2) 0.39717(15) 0.3330(3) 0.0224(9) Uani 1 1 d . . . . .
P12 P 0.4287(3) 0.47648(19) 0.6375(3) 0.0421(13) Uani 1 1 d . . . . .
Se1 Se 0.08750(11) 0.20689(5) 0.55930(10) 0.0256(3) Uani 1 1 d . . . . .
Se2 Se 0.31525(12) 0.23123(6) 0.68822(11) 0.0299(4) Uani 1 1 d . . . . .
Se3 Se -0.08144(11) 0.32881(6) 0.50749(12) 0.0309(4) Uani 1 1 d . . . . .
Se4 Se -0.09502(11) 0.22888(6) 0.36877(12) 0.0323(4) Uani 1 1 d . . . . .
Se5 Se -0.05918(13) 0.27204(7) 0.11875(12) 0.0382(4) Uani 1 1 d . . . . .
Se6 Se 0.06798(12) 0.17928(6) 0.24936(12) 0.0333(4) Uani 1 1 d . . . . .
Se7 Se 0.25400(13) 0.15102(6) 0.44868(12) 0.0374(4) Uani 1 1 d . . . . .
Se8 Se 0.36051(12) 0.20023(6) 0.29932(11) 0.0329(4) Uani 1 1 d . . . . .
Se9 Se 0.15091(11) 0.27496(6) 0.08208(10) 0.0269(4) Uani 1 1 d . . . . .
Se10 Se 0.38387(10) 0.30448(6) 0.16307(11) 0.0280(4) Uani 1 1 d . . . . .
Se11 Se 0.50114(11) 0.23437(6) 0.53059(12) 0.0336(4) Uani 1 1 d . . . . .
Se12 Se 0.47525(10) 0.33231(6) 0.65977(10) 0.0265(3) Uani 1 1 d . . . . .
Se13 Se 0.18968(11) 0.33594(6) 0.70787(10) 0.0266(3) Uani 1 1 d . . . . .
Se14 Se 0.04917(12) 0.43309(6) 0.61015(12) 0.0336(4) Uani 1 1 d . . . . .
Se15 Se -0.15873(11) 0.37265(6) 0.27030(13) 0.0342(4) Uani 1 1 d . . . . .
Se16 Se -0.03931(11) 0.40440(6) 0.12076(10) 0.0270(4) Uani 1 1 d . . . . .
Se17 Se 0.20083(11) 0.51964(6) 0.47109(11) 0.0289(4) Uani 1 1 d . . . . .
Se18 Se -0.02276(10) 0.47440(5) 0.37059(11) 0.0238(3) Uani 1 1 d . . . . .
Se19 Se 0.18983(11) 0.49704(5) 0.24567(11) 0.0266(4) Uani 1 1 d . . . . .
Se20 Se 0.18184(12) 0.41315(7) 0.07735(11) 0.0324(4) Uani 1 1 d . . . . .
Se21 Se 0.42843(10) 0.44197(6) 0.29402(11) 0.0279(4) Uani 1 1 d . . . . .
Se22 Se 0.52547(10) 0.33615(6) 0.40268(11) 0.0252(3) Uani 1 1 d . . . . .
Se23 Se 0.43913(11) 0.46303(6) 0.51304(12) 0.0300(4) Uani 1 1 d . . . . .
Se24 Se 0.34517(13) 0.43300(7) 0.68367(12) 0.0372(4) Uani 1 1 d . . . . .


_geom_special_details            
; 
 All esds (except the esd in the dihedral angle between two l.s. planes) 
 are estimated using the full covariance matrix.  The cell esds are taken 
 into account individually in the estimation of esds in distances, angles 
 and torsion angles; correlations between esds in cell parameters are only 
 used when they are defined by crystal symmetry.  An approximate (isotropic) 
 treatment of cell esds is used for estimating esds involving l.s. planes. 
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt1 Ag3 2.7428(12) . ?
Pt1 Ag4 2.7480(12) . ?
Pt1 Ag6 2.7510(13) . ?
Pt1 Ag8 2.7518(13) . ?
Pt1 Ag5 2.7534(13) . ?
Pt1 Ag11 2.7542(13) . ?
Pt1 Ag9 2.7571(13) . ?
Pt1 Ag12 2.7622(13) . ?
Pt1 Ag10 2.7642(12) . ?
Pt1 Ag1 2.7646(13) . ?
Pt1 Ag7 2.7655(12) . ?
Pt1 Ag2 2.7945(13) . ?
Ag1 Se19 2.663(2) . ?
Ag1 Ag2 2.8565(16) . ?
Ag1 Ag3 2.8776(15) . ?
Ag1 Ag7 2.9180(16) . ?
Ag1 Ag9 2.9240(15) . ?
Ag1 Ag8 2.9340(15) . ?
Ag1 Ag17 2.9374(16) . ?
Ag1 Ag18 2.9629(16) . ?
Ag2 Se23 2.691(2) . ?
Ag2 Ag4 2.8867(16) . ?
Ag2 Ag9 2.9067(16) . ?
Ag2 Ag3 2.9411(16) . ?
Ag2 Ag5 2.9424(17) . ?
Ag2 Ag14 2.9940(16) . ?
Ag2 Ag13 3.0115(16) . ?
Ag3 Se22 2.6427(18) . ?
Ag3 Ag6 2.8449(16) . ?
Ag3 Ag7 2.8855(16) . ?
Ag3 Ag5 2.9385(16) . ?
Ag3 Ag17 2.9455(16) . ?
Ag3 Ag13 2.9762(16) . ?
Ag4 Se13 2.6246(19) . ?
Ag4 Ag5 2.8349(16) . ?
Ag4 Ag9 2.8697(17) . ?
Ag4 Ag10 2.9177(17) . ?
Ag4 Ag12 2.9384(16) . ?
Ag4 Ag14 2.9501(17) . ?
Ag4 Ag16 2.9738(16) . ?
Ag5 Se12 2.641(2) . ?
Ag5 Ag6 2.8723(16) . ?
Ag5 Ag12 2.8991(16) . ?
Ag5 Ag15 2.9458(17) . ?
Ag5 Ag13 2.9639(16) . ?
Ag6 Se8 2.6455(19) . ?
Ag6 Ag12 2.8961(15) . ?
Ag6 Ag11 2.9153(16) . ?
Ag6 Ag19 2.9520(17) . ?
Ag6 Ag15 2.9534(17) . ?
Ag6 Ag7 2.9556(16) . ?
Ag7 Se9 2.663(2) . ?
Ag7 Ag8 2.8439(15) . ?
Ag7 Ag11 2.9317(15) . ?
Ag7 Ag17 2.9429(16) . ?
Ag7 Ag19 2.9643(17) . ?
Ag8 Se16 2.670(2) . ?
Ag8 Ag10 2.9188(16) . ?
Ag8 Ag11 2.9196(17) . ?
Ag8 Ag9 2.9344(16) . ?
Ag8 Ag20 2.9352(16) . ?
Ag8 Ag18 2.9677(17) . ?
Ag9 Se18 2.6473(19) . ?
Ag9 Ag10 2.8464(16) . ?
Ag9 Ag18 2.9416(17) . ?
Ag9 Ag14 2.9445(17) . ?
Ag10 Se3 2.6665(18) . ?
Ag10 Ag20 2.9130(18) . ?
Ag10 Ag12 2.9195(16) . ?
Ag10 Ag11 2.9332(16) . ?
Ag10 Ag16 2.9802(17) . ?
Ag11 Se6 2.678(2) . ?
Ag11 Ag12 2.8378(17) . ?
Ag11 Ag20 2.9262(16) . ?
Ag11 Ag19 2.9902(16) . ?
Ag12 Se1 2.6658(19) . ?
Ag12 Ag15 2.9379(17) . ?
Ag12 Ag16 2.9988(16) . ?
Ag13 Se23 2.606(2) . ?
Ag13 Se12 2.617(2) . ?
Ag13 Se22 2.627(2) . ?
Ag14 Se17 2.601(2) . ?
Ag14 Se24 2.610(2) . ?
Ag14 Se14 2.617(2) . ?
Ag15 Se11 2.612(2) . ?
Ag15 Se7 2.612(2) . ?
Ag15 Se2 2.616(2) . ?
Ag16 Se3 2.608(2) . ?
Ag16 Se13 2.613(2) . ?
Ag16 Se1 2.616(2) . ?
Ag17 Se10 2.618(2) . ?
Ag17 Se20 2.623(2) . ?
Ag17 Se21 2.628(2) . ?
Ag18 Se16 2.617(2) . ?
Ag18 Se19 2.620(2) . ?
Ag18 Se18 2.6222(19) . ?
Ag19 Se6 2.617(2) . ?
Ag19 Se9 2.623(2) . ?
Ag19 Se8 2.630(2) . ?
Ag20 Se4 2.610(2) . ?
Ag20 Se5 2.620(2) . ?
Ag20 Se15 2.620(2) . ?
C1 C2 1.47(3) . ?
C1 O1 1.48(2) . ?
C2 C3 1.52(3) . ?
C4 O2 1.41(2) . ?
C4 C5 1.44(3) . ?
C5 C6 1.47(3) . ?
C7 O3 1.420(12) . ?
C7 C8 1.512(12) . ?
C8 C9 1.497(12) . ?
C10 O4 1.423(12) . ?
C10 C11 1.508(12) . ?
C11 C12 1.528(12) . ?
C13 O5 1.428(12) . ?
C13 C14 1.46(3) . ?
C14 C15 1.507(12) . ?
C16 O6 1.413(12) . ?
C16 C17 1.511(12) . ?
C17 C18 1.515(9) . ?
C19 O7 1.47(3) . ?
C19 C20 1.525(12) . ?
C20 C21 1.502(12) . ?
C22 O8 1.414(12) . ?
C22 C23 1.522(12) . ?
C23 C24 1.528(13) . ?
C25 O9 1.39(3) . ?
C25 C26 1.511(12) . ?
C26 C27 1.524(12) . ?
C28 O10 1.444(19) . ?
C28 C29 1.47(2) . ?
C29 C30 1.52(2) . ?
C31 O11 1.39(3) . ?
C31 C32 1.513(12) . ?
C32 C33 1.501(12) . ?
C34 O12 1.44(3) . ?
C34 C35 1.520(12) . ?
C35 C36 1.512(12) . ?
C37 O13 1.46(2) . ?
C37 C38 1.50(3) . ?
C38 C39 1.55(4) . ?
C40 O14 1.45(2) . ?
C40 C41 1.515(12) . ?
C41 C42 1.510(12) . ?
C43 O15 1.39(3) . ?
C43 C44 1.520(12) . ?
C44 C45 1.519(13) . ?
C46 O16 1.42(2) . ?
C46 C47 1.44(3) . ?
C47 C48 1.60(4) . ?
C49 O17 1.44(2) . ?
C49 C50 1.504(12) . ?
C50 C51 1.510(9) . ?
C52 O18 1.43(2) . ?
C52 C53 1.508(12) . ?
C53 C54 1.514(12) . ?
C55 O19 1.39(3) . ?
C55 C56 1.518(9) . ?
C56 C57 1.507(13) . ?
C58 O20 1.45(2) . ?
C58 C59 1.50(3) . ?
C59 C60 1.43(3) . ?
C61 O21 1.43(2) . ?
C61 C62 1.517(9) . ?
C62 C63 1.510(12) . ?
C64 C65 1.46(3) . ?
C64 O22 1.48(2) . ?
C65 C66 1.61(3) . ?
C67 O23 1.416(12) . ?
C67 C68 1.519(12) . ?
C68 C69 1.516(9) . ?
C70 O24 1.37(3) . ?
C70 C71 1.514(12) . ?
C71 C72 1.515(13) . ?
O1 P1 1.593(12) . ?
O2 P1 1.600(12) . ?
O3 P2 1.574(15) . ?
O4 P2 1.583(14) . ?
O5 P3 1.593(14) . ?
O6 P3 1.528(14) . ?
O7 P4 1.598(15) . ?
O8 P4 1.563(18) . ?
O9 P5 1.583(13) . ?
O10 P5 1.590(12) . ?
O11 P6 1.566(13) . ?
O12 P6 1.586(13) . ?
O13 P7 1.592(12) . ?
O14 P7 1.604(12) . ?
O15 P8 1.581(14) . ?
O16 P8 1.601(12) . ?
O17 P9 1.577(12) . ?
O18 P9 1.603(12) . ?
O19 P10 1.628(14) . ?
O20 P10 1.583(12) . ?
O21 P11 1.583(11) . ?
O22 P11 1.555(12) . ?
O23 P12 1.529(17) . ?
O24 P12 1.642(17) . ?
P1 Se2 2.142(5) . ?
P1 Se1 2.161(5) . ?
P2 Se4 2.148(5) . ?
P2 Se3 2.157(5) . ?
P3 Se5 2.115(6) . ?
P3 Se6 2.173(6) . ?
P4 Se7 2.131(6) . ?
P4 Se8 2.166(5) . ?
P5 Se10 2.142(5) . ?
P5 Se9 2.163(4) . ?
P6 Se11 2.139(5) . ?
P6 Se12 2.165(5) . ?
P7 Se14 2.127(5) . ?
P7 Se13 2.169(5) . ?
P8 Se15 2.128(5) . ?
P8 Se16 2.174(5) . ?
P9 Se17 2.142(4) . ?
P9 Se18 2.167(5) . ?
P10 Se20 2.132(5) . ?
P10 Se19 2.182(5) . ?
P11 Se21 2.131(5) . ?
P11 Se22 2.173(5) . ?
P12 Se24 2.149(6) . ?
P12 Se23 2.151(5) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Ag3 Pt1 Ag4 116.23(4) . . ?
Ag3 Pt1 Ag6 62.38(4) . . ?
Ag4 Pt1 Ag6 115.92(4) . . ?
Ag3 Pt1 Ag8 115.67(4) . . ?
Ag4 Pt1 Ag8 117.86(4) . . ?
Ag6 Pt1 Ag8 116.96(4) . . ?
Ag3 Pt1 Ag5 64.64(4) . . ?
Ag4 Pt1 Ag5 62.04(4) . . ?
Ag6 Pt1 Ag5 62.91(4) . . ?
Ag8 Pt1 Ag5 179.60(5) . . ?
Ag3 Pt1 Ag11 115.99(4) . . ?
Ag4 Pt1 Ag11 116.89(4) . . ?
Ag6 Pt1 Ag11 63.95(4) . . ?
Ag8 Pt1 Ag11 64.05(4) . . ?
Ag5 Pt1 Ag11 115.62(4) . . ?
Ag3 Pt1 Ag9 117.47(4) . . ?
Ag4 Pt1 Ag9 62.84(4) . . ?
Ag6 Pt1 Ag9 178.64(4) . . ?
Ag8 Pt1 Ag9 64.37(4) . . ?
Ag5 Pt1 Ag9 115.75(4) . . ?
Ag11 Pt1 Ag9 116.96(4) . . ?
Ag3 Pt1 Ag12 116.78(4) . . ?
Ag4 Pt1 Ag12 64.45(4) . . ?
Ag6 Pt1 Ag12 63.38(4) . . ?
Ag8 Pt1 Ag12 116.19(4) . . ?
Ag5 Pt1 Ag12 63.42(4) . . ?
Ag11 Pt1 Ag12 61.92(4) . . ?
Ag9 Pt1 Ag12 115.99(4) . . ?
Ag3 Pt1 Ag10 179.44(5) . . ?
Ag4 Pt1 Ag10 63.92(4) . . ?
Ag6 Pt1 Ag10 118.09(4) . . ?
Ag8 Pt1 Ag10 63.90(4) . . ?
Ag5 Pt1 Ag10 115.80(4) . . ?
Ag11 Pt1 Ag10 64.22(4) . . ?
Ag9 Pt1 Ag10 62.07(4) . . ?
Ag12 Pt1 Ag10 63.78(4) . . ?
Ag3 Pt1 Ag1 63.00(3) . . ?
Ag4 Pt1 Ag1 115.20(4) . . ?
Ag6 Pt1 Ag1 116.68(4) . . ?
Ag8 Pt1 Ag1 64.26(4) . . ?
Ag5 Pt1 Ag1 116.13(4) . . ?
Ag11 Pt1 Ag1 118.57(4) . . ?
Ag9 Pt1 Ag1 63.95(4) . . ?
Ag12 Pt1 Ag1 179.51(5) . . ?
Ag10 Pt1 Ag1 116.44(4) . . ?
Ag3 Pt1 Ag7 63.18(4) . . ?
Ag4 Pt1 Ag7 178.87(5) . . ?
Ag6 Pt1 Ag7 64.79(4) . . ?
Ag8 Pt1 Ag7 62.05(4) . . ?
Ag5 Pt1 Ag7 118.06(4) . . ?
Ag11 Pt1 Ag7 64.17(4) . . ?
Ag9 Pt1 Ag7 116.44(4) . . ?
Ag12 Pt1 Ag7 116.65(4) . . ?
Ag10 Pt1 Ag7 116.66(4) . . ?
Ag1 Pt1 Ag7 63.69(4) . . ?
Ag3 Pt1 Ag2 64.16(4) . . ?
Ag4 Pt1 Ag2 62.77(4) . . ?
Ag6 Pt1 Ag2 115.94(4) . . ?
Ag8 Pt1 Ag2 116.27(4) . . ?
Ag5 Pt1 Ag2 64.06(4) . . ?
Ag11 Pt1 Ag2 179.60(4) . . ?
Ag9 Pt1 Ag2 63.14(4) . . ?
Ag12 Pt1 Ag2 117.68(4) . . ?
Ag10 Pt1 Ag2 115.64(4) . . ?
Ag1 Pt1 Ag2 61.84(4) . . ?
Ag7 Pt1 Ag2 116.18(4) . . ?
Se19 Ag1 Pt1 154.91(6) . . ?
Se19 Ag1 Ag2 108.48(6) . . ?
Pt1 Ag1 Ag2 59.60(3) . . ?
Se19 Ag1 Ag3 139.25(6) . . ?
Pt1 Ag1 Ag3 58.13(3) . . ?
Ag2 Ag1 Ag3 61.71(4) . . ?
Se19 Ag1 Ag7 141.36(6) . . ?
Pt1 Ag1 Ag7 58.17(3) . . ?
Ag2 Ag1 Ag7 109.63(5) . . ?
Ag3 Ag1 Ag7 59.71(4) . . ?
Se19 Ag1 Ag9 97.08(5) . . ?
Pt1 Ag1 Ag9 57.90(3) . . ?
Ag2 Ag1 Ag9 60.36(4) . . ?
Ag3 Ag1 Ag9 108.25(5) . . ?
Ag7 Ag1 Ag9 106.95(5) . . ?
Se19 Ag1 Ag8 113.96(6) . . ?
Pt1 Ag1 Ag8 57.66(3) . . ?
Ag2 Ag1 Ag8 108.87(5) . . ?
Ag3 Ag1 Ag8 106.32(5) . . ?
Ag7 Ag1 Ag8 58.15(4) . . ?
Ag9 Ag1 Ag8 60.12(4) . . ?
Se19 Ag1 Ag17 97.02(5) . . ?
Pt1 Ag1 Ag17 108.05(4) . . ?
Ag2 Ag1 Ag17 115.87(5) . . ?
Ag3 Ag1 Ag17 60.86(4) . . ?
Ag7 Ag1 Ag17 60.34(4) . . ?
Ag9 Ag1 Ag17 165.83(5) . . ?
Ag8 Ag1 Ag17 112.30(5) . . ?
Se19 Ag1 Ag18 55.20(5) . . ?
Pt1 Ag1 Ag18 106.92(4) . . ?
Ag2 Ag1 Ag18 113.77(5) . . ?
Ag3 Ag1 Ag18 164.97(5) . . ?
Ag7 Ag1 Ag18 112.66(5) . . ?
Ag9 Ag1 Ag18 59.96(4) . . ?
Ag8 Ag1 Ag18 60.43(4) . . ?
Ag17 Ag1 Ag18 128.81(5) . . ?
Se23 Ag2 Pt1 152.65(6) . . ?
Se23 Ag2 Ag1 109.09(6) . . ?
Pt1 Ag2 Ag1 58.57(3) . . ?
Se23 Ag2 Ag4 142.47(6) . . ?
Pt1 Ag2 Ag4 57.83(3) . . ?
Ag1 Ag2 Ag4 108.27(5) . . ?
Se23 Ag2 Ag9 141.60(6) . . ?
Pt1 Ag2 Ag9 57.80(3) . . ?
Ag1 Ag2 Ag9 60.97(4) . . ?
Ag4 Ag2 Ag9 59.38(4) . . ?
Se23 Ag2 Ag3 95.60(5) . . ?
Pt1 Ag2 Ag3 57.07(3) . . ?
Ag1 Ag2 Ag3 59.50(4) . . ?
Ag4 Ag2 Ag3 106.26(5) . . ?
Ag9 Ag2 Ag3 107.02(5) . . ?
Se23 Ag2 Ag5 112.34(6) . . ?
Pt1 Ag2 Ag5 57.29(3) . . ?
Ag1 Ag2 Ag5 107.71(5) . . ?
Ag4 Ag2 Ag5 58.19(4) . . ?
Ag9 Ag2 Ag5 105.85(5) . . ?
Ag3 Ag2 Ag5 59.93(4) . . ?
Se23 Ag2 Ag14 100.28(6) . . ?
Pt1 Ag2 Ag14 107.06(4) . . ?
Ag1 Ag2 Ag14 114.57(5) . . ?
Ag4 Ag2 Ag14 60.19(4) . . ?
Ag9 Ag2 Ag14 59.85(4) . . ?
Ag3 Ag2 Ag14 164.12(5) . . ?
Ag5 Ag2 Ag14 112.78(5) . . ?
Se23 Ag2 Ag13 54.03(5) . . ?
Pt1 Ag2 Ag13 105.83(4) . . ?
Ag1 Ag2 Ag13 113.61(5) . . ?
Ag4 Ag2 Ag13 112.30(5) . . ?
Ag9 Ag2 Ag13 163.56(5) . . ?
Ag3 Ag2 Ag13 59.98(4) . . ?
Ag5 Ag2 Ag13 59.70(4) . . ?
Ag14 Ag2 Ag13 130.78(5) . . ?
Se22 Ag3 Pt1 153.32(6) . . ?
Se22 Ag3 Ag6 105.06(6) . . ?
Pt1 Ag3 Ag6 58.95(3) . . ?
Se22 Ag3 Ag1 144.08(6) . . ?
Pt1 Ag3 Ag1 58.87(3) . . ?
Ag6 Ag3 Ag1 110.24(5) . . ?
Se22 Ag3 Ag7 136.29(6) . . ?
Pt1 Ag3 Ag7 58.79(3) . . ?
Ag6 Ag3 Ag7 62.09(4) . . ?
Ag1 Ag3 Ag7 60.84(4) . . ?
Se22 Ag3 Ag5 96.01(5) . . ?
Pt1 Ag3 Ag5 57.86(3) . . ?
Ag6 Ag3 Ag5 59.53(4) . . ?
Ag1 Ag3 Ag5 107.25(4) . . ?
Ag7 Ag3 Ag5 108.68(5) . . ?
Se22 Ag3 Ag2 115.38(6) . . ?
Pt1 Ag3 Ag2 58.77(3) . . ?
Ag6 Ag3 Ag2 108.68(5) . . ?
Ag1 Ag3 Ag2 58.79(4) . . ?
Ag7 Ag3 Ag2 108.19(5) . . ?
Ag5 Ag3 Ag2 60.06(4) . . ?
Se22 Ag3 Ag17 97.81(5) . . ?
Pt1 Ag3 Ag17 108.41(4) . . ?
Ag6 Ag3 Ag17 116.47(5) . . ?
Ag1 Ag3 Ag17 60.57(4) . . ?
Ag7 Ag3 Ag17 60.61(4) . . ?
Ag5 Ag3 Ag17 166.19(5) . . ?
Ag2 Ag3 Ag17 113.06(5) . . ?
Se22 Ag3 Ag13 55.37(5) . . ?
Pt1 Ag3 Ag13 108.16(4) . . ?
Ag6 Ag3 Ag13 112.41(5) . . ?
Ag1 Ag3 Ag13 114.05(5) . . ?
Ag7 Ag3 Ag13 166.95(5) . . ?
Ag5 Ag3 Ag13 60.14(4) . . ?
Ag2 Ag3 Ag13 61.18(4) . . ?
Ag17 Ag3 Ag13 129.07(5) . . ?
Se13 Ag4 Pt1 154.61(6) . . ?
Se13 Ag4 Ag5 107.18(6) . . ?
Pt1 Ag4 Ag5 59.08(3) . . ?
Se13 Ag4 Ag9 142.33(6) . . ?
Pt1 Ag4 Ag9 58.74(3) . . ?
Ag5 Ag4 Ag9 109.79(5) . . ?
Se13 Ag4 Ag2 136.57(6) . . ?
Pt1 Ag4 Ag2 59.40(3) . . ?
Ag5 Ag4 Ag2 61.89(4) . . ?
Ag9 Ag4 Ag2 60.66(4) . . ?
Se13 Ag4 Ag10 114.78(6) . . ?
Pt1 Ag4 Ag10 58.31(3) . . ?
Ag5 Ag4 Ag10 108.67(5) . . ?
Ag9 Ag4 Ag10 58.91(4) . . ?
Ag2 Ag4 Ag10 108.30(5) . . ?
Se13 Ag4 Ag12 96.88(6) . . ?
Pt1 Ag4 Ag12 58.01(3) . . ?
Ag5 Ag4 Ag12 60.25(4) . . ?
Ag9 Ag4 Ag12 107.37(5) . . ?
Ag2 Ag4 Ag12 109.43(5) . . ?
Ag10 Ag4 Ag12 59.81(4) . . ?
Se13 Ag4 Ag14 95.69(6) . . ?
Pt1 Ag4 Ag14 109.56(5) . . ?
Ag5 Ag4 Ag14 117.42(5) . . ?
Ag9 Ag4 Ag14 60.77(4) . . ?
Ag2 Ag4 Ag14 61.71(4) . . ?
Ag10 Ag4 Ag14 112.66(5) . . ?
Ag12 Ag4 Ag14 167.28(5) . . ?
Se13 Ag4 Ag16 55.21(5) . . ?
Pt1 Ag4 Ag16 108.34(5) . . ?
Ag5 Ag4 Ag16 114.39(5) . . ?
Ag9 Ag4 Ag16 113.10(5) . . ?
Ag2 Ag4 Ag16 167.67(6) . . ?
Ag10 Ag4 Ag16 60.77(4) . . ?
Ag12 Ag4 Ag16 60.95(4) . . ?
Ag14 Ag4 Ag16 126.23(5) . . ?
Se12 Ag5 Pt1 155.01(6) . . ?
Se12 Ag5 Ag4 108.21(6) . . ?
Pt1 Ag5 Ag4 58.89(3) . . ?
Se12 Ag5 Ag6 141.67(6) . . ?
Pt1 Ag5 Ag6 58.51(3) . . ?
Ag4 Ag5 Ag6 109.52(5) . . ?
Se12 Ag5 Ag12 137.96(6) . . ?
Pt1 Ag5 Ag12 58.44(3) . . ?
Ag4 Ag5 Ag12 61.64(4) . . ?
Ag6 Ag5 Ag12 60.24(4) . . ?
Se12 Ag5 Ag3 114.84(6) . . ?
Pt1 Ag5 Ag3 57.51(3) . . ?
Ag4 Ag5 Ag3 107.71(5) . . ?
Ag6 Ag5 Ag3 58.62(4) . . ?
Ag12 Ag5 Ag3 106.85(5) . . ?
Se12 Ag5 Ag2 96.51(6) . . ?
Pt1 Ag5 Ag2 58.65(3) . . ?
Ag4 Ag5 Ag2 59.92(4) . . ?
Ag6 Ag5 Ag2 107.90(5) . . ?
Ag12 Ag5 Ag2 108.97(5) . . ?
Ag3 Ag5 Ag2 60.01(4) . . ?
Se12 Ag5 Ag15 96.54(6) . . ?
Pt1 Ag5 Ag15 108.31(5) . . ?
Ag4 Ag5 Ag15 115.39(5) . . ?
Ag6 Ag5 Ag15 60.99(4) . . ?
Ag12 Ag5 Ag15 60.34(4) . . ?
Ag3 Ag5 Ag15 113.93(5) . . ?
Ag2 Ag5 Ag15 166.95(5) . . ?
Se12 Ag5 Ag13 55.31(5) . . ?
Pt1 Ag5 Ag13 108.22(5) . . ?
Ag4 Ag5 Ag13 115.29(5) . . ?
Ag6 Ag5 Ag13 111.98(5) . . ?
Ag12 Ag5 Ag13 166.42(5) . . ?
Ag3 Ag5 Ag13 60.56(4) . . ?
Ag2 Ag5 Ag13 61.31(4) . . ?
Ag15 Ag5 Ag13 127.62(5) . . ?
Se8 Ag6 Pt1 156.25(6) . . ?
Se8 Ag6 Ag3 108.92(6) . . ?
Pt1 Ag6 Ag3 58.67(3) . . ?
Se8 Ag6 Ag5 137.05(6) . . ?
Pt1 Ag6 Ag5 58.59(3) . . ?
Ag3 Ag6 Ag5 61.85(4) . . ?
Se8 Ag6 Ag12 140.85(7) . . ?
Pt1 Ag6 Ag12 58.50(3) . . ?
Ag3 Ag6 Ag12 109.49(5) . . ?
Ag5 Ag6 Ag12 60.34(4) . . ?
Se8 Ag6 Ag11 115.08(6) . . ?
Pt1 Ag6 Ag11 58.08(3) . . ?
Ag3 Ag6 Ag11 108.03(5) . . ?
Ag5 Ag6 Ag11 107.29(5) . . ?
Ag12 Ag6 Ag11 58.46(4) . . ?
Se8 Ag6 Ag19 55.72(5) . . ?
Pt1 Ag6 Ag19 107.91(5) . . ?
Ag3 Ag6 Ag19 113.01(5) . . ?
Ag5 Ag6 Ag19 166.49(5) . . ?
Ag12 Ag6 Ag19 113.67(5) . . ?
Ag11 Ag6 Ag19 61.27(4) . . ?
Se8 Ag6 Ag15 95.49(6) . . ?
Pt1 Ag6 Ag15 108.16(4) . . ?
Ag3 Ag6 Ag15 116.57(5) . . ?
Ag5 Ag6 Ag15 60.73(4) . . ?
Ag12 Ag6 Ag15 60.29(4) . . ?
Ag11 Ag6 Ag15 112.52(5) . . ?
Ag19 Ag6 Ag15 128.71(5) . . ?
Se8 Ag6 Ag7 98.59(6) . . ?
Pt1 Ag6 Ag7 57.84(3) . . ?
Ag3 Ag6 Ag7 59.63(4) . . ?
Ag5 Ag6 Ag7 108.57(5) . . ?
Ag12 Ag6 Ag7 107.01(5) . . ?
Ag11 Ag6 Ag7 59.91(4) . . ?
Ag19 Ag6 Ag7 60.24(4) . . ?
Ag15 Ag6 Ag7 165.87(5) . . ?
Se9 Ag7 Pt1 153.34(6) . . ?
Se9 Ag7 Ag8 107.81(6) . . ?
Pt1 Ag7 Ag8 58.74(3) . . ?
Se9 Ag7 Ag3 143.23(6) . . ?
Pt1 Ag7 Ag3 58.03(3) . . ?
Ag8 Ag7 Ag3 108.55(5) . . ?
Se9 Ag7 Ag1 139.43(6) . . ?
Pt1 Ag7 Ag1 58.14(3) . . ?
Ag8 Ag7 Ag1 61.21(4) . . ?
Ag3 Ag7 Ag1 59.45(4) . . ?
Se9 Ag7 Ag11 95.78(5) . . ?
Pt1 Ag7 Ag11 57.73(3) . . ?
Ag8 Ag7 Ag11 60.71(4) . . ?
Ag3 Ag7 Ag11 106.51(5) . . ?
Ag1 Ag7 Ag11 108.40(5) . . ?
Se9 Ag7 Ag17 98.68(5) . . ?
Pt1 Ag7 Ag17 107.87(5) . . ?
Ag8 Ag7 Ag17 114.83(5) . . ?
Ag3 Ag7 Ag17 60.70(4) . . ?
Ag1 Ag7 Ag17 60.16(4) . . ?
Ag11 Ag7 Ag17 165.52(5) . . ?
Se9 Ag7 Ag6 114.23(6) . . ?
Pt1 Ag7 Ag6 57.37(3) . . ?
Ag8 Ag7 Ag6 107.96(5) . . ?
Ag3 Ag7 Ag6 58.28(4) . . ?
Ag1 Ag7 Ag6 106.12(5) . . ?
Ag11 Ag7 Ag6 59.36(4) . . ?
Ag17 Ag7 Ag6 113.16(5) . . ?
Se9 Ag7 Ag19 55.26(5) . . ?
Pt1 Ag7 Ag19 107.18(5) . . ?
Ag8 Ag7 Ag19 115.75(5) . . ?
Ag3 Ag7 Ag19 111.47(5) . . ?
Ag1 Ag7 Ag19 164.97(5) . . ?
Ag11 Ag7 Ag19 60.95(4) . . ?
Ag17 Ag7 Ag19 128.15(5) . . ?
Ag6 Ag7 Ag19 59.82(4) . . ?
Se16 Ag8 Pt1 155.36(6) . . ?
Se16 Ag8 Ag7 109.73(6) . . ?
Pt1 Ag8 Ag7 59.21(3) . . ?
Se16 Ag8 Ag10 140.30(6) . . ?
Pt1 Ag8 Ag10 58.26(3) . . ?
Ag7 Ag8 Ag10 109.50(5) . . ?
Se16 Ag8 Ag11 139.56(6) . . ?
Pt1 Ag8 Ag11 58.02(3) . . ?
Ag7 Ag8 Ag11 61.13(4) . . ?
Ag10 Ag8 Ag11 60.32(4) . . ?
Se16 Ag8 Ag1 97.31(5) . . ?
Pt1 Ag8 Ag1 58.08(3) . . ?
Ag7 Ag8 Ag1 60.64(4) . . ?
Ag10 Ag8 Ag1 106.84(5) . . ?
Ag11 Ag8 Ag1 108.29(5) . . ?
Se16 Ag8 Ag9 113.17(6) . . ?
Pt1 Ag8 Ag9 57.90(3) . . ?
Ag7 Ag8 Ag9 108.66(5) . . ?
Ag10 Ag8 Ag9 58.19(4) . . ?
Ag11 Ag8 Ag9 106.74(5) . . ?
Ag1 Ag8 Ag9 59.77(4) . . ?
Se16 Ag8 Ag20 97.80(6) . . ?
Pt1 Ag8 Ag20 106.83(5) . . ?
Ag7 Ag8 Ag20 114.99(5) . . ?
Ag10 Ag8 Ag20 59.68(4) . . ?
Ag11 Ag8 Ag20 59.97(4) . . ?
Ag1 Ag8 Ag20 164.81(6) . . ?
Ag9 Ag8 Ag20 112.24(5) . . ?
Se16 Ag8 Ag18 55.02(5) . . ?
Pt1 Ag8 Ag18 107.12(5) . . ?
Ag7 Ag8 Ag18 114.72(5) . . ?
Ag10 Ag8 Ag18 111.70(5) . . ?
Ag11 Ag8 Ag18 165.01(6) . . ?
Ag1 Ag8 Ag18 60.27(4) . . ?
Ag9 Ag8 Ag18 59.79(4) . . ?
Ag20 Ag8 Ag18 129.10(5) . . ?
Se18 Ag9 Pt1 155.97(6) . . ?
Se18 Ag9 Ag10 109.13(6) . . ?
Pt1 Ag9 Ag10 59.09(3) . . ?
Se18 Ag9 Ag4 137.88(6) . . ?
Pt1 Ag9 Ag4 58.43(3) . . ?
Ag10 Ag9 Ag4 61.38(4) . . ?
Se18 Ag9 Ag2 140.27(6) . . ?
Pt1 Ag9 Ag2 59.06(3) . . ?
Ag10 Ag9 Ag2 109.73(5) . . ?
Ag4 Ag9 Ag2 59.96(4) . . ?
Se18 Ag9 Ag1 114.57(6) . . ?
Pt1 Ag9 Ag1 58.15(3) . . ?
Ag10 Ag9 Ag1 109.07(5) . . ?
Ag4 Ag9 Ag1 106.90(5) . . ?
Ag2 Ag9 Ag1 58.67(4) . . ?
Se18 Ag9 Ag8 98.37(6) . . ?
Pt1 Ag9 Ag8 57.73(3) . . ?
Ag10 Ag9 Ag8 60.63(4) . . ?
Ag4 Ag9 Ag8 108.51(5) . . ?
Ag2 Ag9 Ag8 107.50(5) . . ?
Ag1 Ag9 Ag8 60.11(4) . . ?
Se18 Ag9 Ag18 55.66(5) . . ?
Pt1 Ag9 Ag18 107.71(4) . . ?
Ag10 Ag9 Ag18 114.63(5) . . ?
Ag4 Ag9 Ag18 166.03(5) . . ?
Ag2 Ag9 Ag18 112.92(5) . . ?
Ag1 Ag9 Ag18 60.68(4) . . ?
Ag8 Ag9 Ag18 60.67(4) . . ?
Se18 Ag9 Ag14 94.45(5) . . ?
Pt1 Ag9 Ag14 109.47(5) . . ?
Ag10 Ag9 Ag14 114.98(5) . . ?
Ag4 Ag9 Ag14 60.97(4) . . ?
Ag2 Ag9 Ag14 61.55(4) . . ?
Ag1 Ag9 Ag14 114.05(5) . . ?
Ag8 Ag9 Ag14 167.18(5) . . ?
Ag18 Ag9 Ag14 128.25(5) . . ?
Se3 Ag10 Pt1 156.49(6) . . ?
Se3 Ag10 Ag9 110.70(6) . . ?
Pt1 Ag10 Ag9 58.84(3) . . ?
Se3 Ag10 Ag20 96.40(6) . . ?
Pt1 Ag10 Ag20 107.11(4) . . ?
Ag9 Ag10 Ag20 115.57(5) . . ?
Se3 Ag10 Ag4 98.73(6) . . ?
Pt1 Ag10 Ag4 57.77(3) . . ?
Ag9 Ag10 Ag4 59.70(4) . . ?
Ag20 Ag10 Ag4 164.82(5) . . ?
Se3 Ag10 Ag8 139.16(6) . . ?
Pt1 Ag10 Ag8 57.85(3) . . ?
Ag9 Ag10 Ag8 61.18(4) . . ?
Ag20 Ag10 Ag8 60.44(4) . . ?
Ag4 Ag10 Ag8 107.63(5) . . ?
Se3 Ag10 Ag12 113.49(6) . . ?
Pt1 Ag10 Ag12 58.08(3) . . ?
Ag9 Ag10 Ag12 108.52(5) . . ?
Ag20 Ag10 Ag12 111.90(5) . . ?
Ag4 Ag10 Ag12 60.45(4) . . ?
Ag8 Ag10 Ag12 106.59(5) . . ?
Se3 Ag10 Ag11 140.01(6) . . ?
Pt1 Ag10 Ag11 57.72(3) . . ?
Ag9 Ag10 Ag11 108.74(5) . . ?
Ag20 Ag10 Ag11 60.07(4) . . ?
Ag4 Ag10 Ag11 106.52(5) . . ?
Ag8 Ag10 Ag11 59.85(4) . . ?
Ag12 Ag10 Ag11 58.01(4) . . ?
Se3 Ag10 Ag16 54.68(5) . . ?
Pt1 Ag10 Ag16 107.72(5) . . ?
Ag9 Ag10 Ag16 113.60(5) . . ?
Ag20 Ag10 Ag16 129.39(5) . . ?
Ag4 Ag10 Ag16 60.55(4) . . ?
Ag8 Ag10 Ag16 165.55(5) . . ?
Ag12 Ag10 Ag16 61.09(4) . . ?
Ag11 Ag10 Ag16 113.44(5) . . ?
Se6 Ag11 Pt1 155.47(6) . . ?
Se6 Ag11 Ag12 110.63(6) . . ?
Pt1 Ag11 Ag12 59.18(3) . . ?
Se6 Ag11 Ag6 97.51(6) . . ?
Pt1 Ag11 Ag6 57.97(3) . . ?
Ag12 Ag11 Ag6 60.43(4) . . ?
Se6 Ag11 Ag8 140.12(6) . . ?
Pt1 Ag11 Ag8 57.94(3) . . ?
Ag12 Ag11 Ag8 108.77(5) . . ?
Ag6 Ag11 Ag8 107.02(5) . . ?
Se6 Ag11 Ag20 97.51(6) . . ?
Pt1 Ag11 Ag20 107.02(5) . . ?
Ag12 Ag11 Ag20 113.93(5) . . ?
Ag6 Ag11 Ag20 164.99(6) . . ?
Ag8 Ag11 Ag20 60.28(4) . . ?
Se6 Ag11 Ag7 112.57(6) . . ?
Pt1 Ag11 Ag7 58.11(3) . . ?
Ag12 Ag11 Ag7 109.24(5) . . ?
Ag6 Ag11 Ag7 60.73(4) . . ?
Ag8 Ag11 Ag7 58.16(4) . . ?
Ag20 Ag11 Ag7 112.61(5) . . ?
Se6 Ag11 Ag10 140.03(6) . . ?
Pt1 Ag11 Ag10 58.06(3) . . ?
Ag12 Ag11 Ag10 60.76(4) . . ?
Ag6 Ag11 Ag10 107.94(5) . . ?
Ag8 Ag11 Ag10 59.83(4) . . ?
Ag20 Ag11 Ag10 59.62(4) . . ?
Ag7 Ag11 Ag10 106.73(5) . . ?
Se6 Ag11 Ag19 54.65(5) . . ?
Pt1 Ag11 Ag19 106.76(4) . . ?
Ag12 Ag11 Ag19 114.26(5) . . ?
Ag6 Ag11 Ag19 59.97(4) . . ?
Ag8 Ag11 Ag19 112.69(5) . . ?
Ag20 Ag11 Ag19 130.44(5) . . ?
Ag7 Ag11 Ag19 60.07(4) . . ?
Ag10 Ag11 Ag19 164.77(5) . . ?
Se1 Ag12 Pt1 153.63(6) . . ?
Se1 Ag12 Ag11 108.55(6) . . ?
Pt1 Ag12 Ag11 58.90(3) . . ?
Se1 Ag12 Ag6 139.96(6) . . ?
Pt1 Ag12 Ag6 58.12(3) . . ?
Ag11 Ag12 Ag6 61.11(4) . . ?
Se1 Ag12 Ag5 142.37(6) . . ?
Pt1 Ag12 Ag5 58.14(3) . . ?
Ag11 Ag12 Ag5 108.67(5) . . ?
Ag6 Ag12 Ag5 59.42(4) . . ?
Se1 Ag12 Ag10 95.59(5) . . ?
Pt1 Ag12 Ag10 58.14(3) . . ?
Ag11 Ag12 Ag10 61.24(4) . . ?
Ag6 Ag12 Ag10 108.84(5) . . ?
Ag5 Ag12 Ag10 106.89(5) . . ?
Se1 Ag12 Ag15 98.04(6) . . ?
Pt1 Ag12 Ag15 108.29(4) . . ?
Ag11 Ag12 Ag15 115.32(5) . . ?
Ag6 Ag12 Ag15 60.82(4) . . ?
Ag5 Ag12 Ag15 60.62(4) . . ?
Ag10 Ag12 Ag15 166.27(5) . . ?
Se1 Ag12 Ag4 113.66(6) . . ?
Pt1 Ag12 Ag4 57.54(3) . . ?
Ag11 Ag12 Ag4 108.52(5) . . ?
Ag6 Ag12 Ag4 106.06(5) . . ?
Ag5 Ag12 Ag4 58.10(4) . . ?
Ag10 Ag12 Ag4 59.74(4) . . ?
Ag15 Ag12 Ag4 112.52(5) . . ?
Se1 Ag12 Ag16 54.63(5) . . ?
Pt1 Ag12 Ag16 107.26(4) . . ?
Ag11 Ag12 Ag16 115.75(5) . . ?
Ag6 Ag12 Ag16 165.08(5) . . ?
Ag5 Ag12 Ag16 111.76(5) . . ?
Ag10 Ag12 Ag16 60.45(4) . . ?
Ag15 Ag12 Ag16 127.58(5) . . ?
Ag4 Ag12 Ag16 60.11(4) . . ?
Se23 Ag13 Se12 118.50(7) . . ?
Se23 Ag13 Se22 120.65(7) . . ?
Se12 Ag13 Se22 120.74(7) . . ?
Se23 Ag13 Ag5 114.24(6) . . ?
Se12 Ag13 Ag5 56.07(5) . . ?
Se22 Ag13 Ag5 95.73(5) . . ?
Se23 Ag13 Ag3 96.61(6) . . ?
Se12 Ag13 Ag3 114.34(6) . . ?
Se22 Ag13 Ag3 55.86(5) . . ?
Ag5 Ag13 Ag3 59.30(4) . . ?
Se23 Ag13 Ag2 56.69(5) . . ?
Se12 Ag13 Ag2 95.38(5) . . ?
Se22 Ag13 Ag2 113.56(6) . . ?
Ag5 Ag13 Ag2 58.99(4) . . ?
Ag3 Ag13 Ag2 58.83(4) . . ?
Se17 Ag14 Se24 114.85(7) . . ?
Se17 Ag14 Se14 122.88(7) . . ?
Se24 Ag14 Se14 119.69(7) . . ?
Se17 Ag14 Ag9 77.18(6) . . ?
Se24 Ag14 Ag9 127.33(7) . . ?
Se14 Ag14 Ag9 83.09(6) . . ?
Se17 Ag14 Ag4 128.98(6) . . ?
Se24 Ag14 Ag4 79.63(6) . . ?
Se14 Ag14 Ag4 77.79(6) . . ?
Ag9 Ag14 Ag4 58.26(4) . . ?
Se17 Ag14 Ag2 78.80(5) . . ?
Se24 Ag14 Ag2 73.22(6) . . ?
Se14 Ag14 Ag2 131.80(7) . . ?
Ag9 Ag14 Ag2 58.60(4) . . ?
Ag4 Ag14 Ag2 58.10(4) . . ?
Se11 Ag15 Se7 118.93(7) . . ?
Se11 Ag15 Se2 119.08(7) . . ?
Se7 Ag15 Se2 116.98(7) . . ?
Se11 Ag15 Ag12 132.32(7) . . ?
Se7 Ag15 Ag12 81.42(6) . . ?
Se2 Ag15 Ag12 77.55(6) . . ?
Se11 Ag15 Ag5 77.67(6) . . ?
Se7 Ag15 Ag5 130.90(7) . . ?
Se2 Ag15 Ag5 83.78(6) . . ?
Ag12 Ag15 Ag5 59.04(4) . . ?
Se11 Ag15 Ag6 82.65(6) . . ?
Se7 Ag15 Ag6 77.35(6) . . ?
Se2 Ag15 Ag6 132.17(6) . . ?
Ag12 Ag15 Ag6 58.89(4) . . ?
Ag5 Ag15 Ag6 58.27(4) . . ?
Se3 Ag16 Se13 123.63(7) . . ?
Se3 Ag16 Se1 115.38(7) . . ?
Se13 Ag16 Se1 120.88(7) . . ?
Se3 Ag16 Ag4 98.68(6) . . ?
Se13 Ag16 Ag4 55.59(5) . . ?
Se1 Ag16 Ag4 114.04(6) . . ?
Se3 Ag16 Ag10 56.53(5) . . ?
Se13 Ag16 Ag10 113.12(6) . . ?
Se1 Ag16 Ag10 95.23(6) . . ?
Ag4 Ag16 Ag10 58.69(4) . . ?
Se3 Ag16 Ag12 112.74(6) . . ?
Se13 Ag16 Ag12 95.69(5) . . ?
Se1 Ag16 Ag12 56.19(5) . . ?
Ag4 Ag16 Ag12 58.94(4) . . ?
Ag10 Ag16 Ag12 58.46(4) . . ?
Se10 Ag17 Se20 116.70(7) . . ?
Se10 Ag17 Se21 119.86(7) . . ?
Se20 Ag17 Se21 119.63(7) . . ?
Se10 Ag17 Ag1 131.92(6) . . ?
Se20 Ag17 Ag1 78.06(5) . . ?
Se21 Ag17 Ag1 79.80(5) . . ?
Se10 Ag17 Ag7 76.24(5) . . ?
Se20 Ag17 Ag7 83.49(6) . . ?
Se21 Ag17 Ag7 128.47(6) . . ?
Ag1 Ag17 Ag7 59.50(4) . . ?
Se10 Ag17 Ag3 83.70(5) . . ?
Se20 Ag17 Ag3 132.24(6) . . ?
Se21 Ag17 Ag3 74.00(5) . . ?
Ag1 Ag17 Ag3 58.57(4) . . ?
Ag7 Ag17 Ag3 58.69(4) . . ?
Se16 Ag18 Se19 119.94(7) . . ?
Se16 Ag18 Se18 120.57(7) . . ?
Se19 Ag18 Se18 119.48(7) . . ?
Se16 Ag18 Ag9 114.56(6) . . ?
Se19 Ag18 Ag9 97.61(6) . . ?
Se18 Ag18 Ag9 56.47(5) . . ?
Se16 Ag18 Ag1 97.79(6) . . ?
Se19 Ag18 Ag1 56.57(5) . . ?
Se18 Ag18 Ag1 114.08(6) . . ?
Ag9 Ag18 Ag1 59.37(4) . . ?
Se16 Ag18 Ag8 56.70(5) . . ?
Se19 Ag18 Ag8 114.20(6) . . ?
Se18 Ag18 Ag8 98.12(6) . . ?
Ag9 Ag18 Ag8 59.55(4) . . ?
Ag1 Ag18 Ag8 59.30(4) . . ?
Se6 Ag19 Se9 115.01(7) . . ?
Se6 Ag19 Se8 119.94(8) . . ?
Se9 Ag19 Se8 125.03(7) . . ?
Se6 Ag19 Ag6 98.00(6) . . ?
Se9 Ag19 Ag6 115.62(6) . . ?
Se8 Ag19 Ag6 56.23(5) . . ?
Se6 Ag19 Ag7 113.39(6) . . ?
Se9 Ag19 Ag7 56.54(5) . . ?
Se8 Ag19 Ag7 98.73(6) . . ?
Ag6 Ag19 Ag7 59.94(4) . . ?
Se6 Ag19 Ag11 56.59(5) . . ?
Se9 Ag19 Ag11 95.26(6) . . ?
Se8 Ag19 Ag11 113.14(6) . . ?
Ag6 Ag19 Ag11 58.76(4) . . ?
Ag7 Ag19 Ag11 58.99(4) . . ?
Se4 Ag20 Se5 119.72(8) . . ?
Se4 Ag20 Se15 120.22(7) . . ?
Se5 Ag20 Se15 117.02(8) . . ?
Se4 Ag20 Ag10 77.80(6) . . ?
Se5 Ag20 Ag10 129.53(6) . . ?
Se15 Ag20 Ag10 80.70(6) . . ?
Se4 Ag20 Ag11 81.06(6) . . ?
Se5 Ag20 Ag11 75.37(6) . . ?
Se15 Ag20 Ag11 131.24(7) . . ?
Ag10 Ag20 Ag11 60.31(4) . . ?
Se4 Ag20 Ag8 132.11(7) . . ?
Se5 Ag20 Ag8 78.12(6) . . ?
Se15 Ag20 Ag8 76.25(5) . . ?
Ag10 Ag20 Ag8 59.88(4) . . ?
Ag11 Ag20 Ag8 59.75(4) . . ?
C2 C1 O1 109.0(14) . . ?
C1 C2 C3 113.0(16) . . ?
O2 C4 C5 112.6(18) . . ?
C4 C5 C6 114(2) . . ?
O3 C7 C8 116(3) . . ?
C9 C8 C7 115(3) . . ?
O4 C10 C11 119(2) . . ?
C10 C11 C12 104(2) . . ?
O5 C13 C14 118(2) . . ?
C13 C14 C15 110(2) . . ?
O6 C16 C17 114(2) . . ?
C16 C17 C18 113(3) . . ?
O7 C19 C20 106.1(19) . . ?
C21 C20 C19 111(2) . . ?
O8 C22 C23 104(2) . . ?
C22 C23 C24 97.4(10) . . ?
O9 C25 C26 112(2) . . ?
C25 C26 C27 102(3) . . ?
O10 C28 C29 114.4(15) . . ?
C28 C29 C30 113.5(18) . . ?
O11 C31 C32 111(2) . . ?
C33 C32 C31 117(3) . . ?
O12 C34 C35 109(2) . . ?
C36 C35 C34 111(2) . . ?
O13 C37 C38 109.5(16) . . ?
C37 C38 C39 111.2(19) . . ?
O14 C40 C41 107.1(16) . . ?
C42 C41 C40 115(2) . . ?
O15 C43 C44 104(3) . . ?
C45 C44 C43 121(4) . . ?
O16 C46 C47 110.8(18) . . ?
C46 C47 C48 110(2) . . ?
O17 C49 C50 107.6(17) . . ?
C49 C50 C51 113.5(19) . . ?
O18 C52 C53 107.5(14) . . ?
C52 C53 C54 112.8(16) . . ?
O19 C55 C56 110(3) . . ?
C57 C56 C55 107(3) . . ?
O20 C58 C59 108.0(18) . . ?
C60 C59 C58 115(2) . . ?
O21 C61 C62 108.1(15) . . ?
C63 C62 C61 113.4(18) . . ?
C65 C64 O22 110.5(15) . . ?
C64 C65 C66 112(2) . . ?
O23 C67 C68 109(2) . . ?
C69 C68 C67 113(3) . . ?
O24 C70 C71 108(2) . . ?
C70 C71 C72 91.0(8) . . ?
C1 O1 P1 124.4(10) . . ?
C4 O2 P1 124.0(12) . . ?
C7 O3 P2 124.1(18) . . ?
C10 O4 P2 127.7(14) . . ?
C13 O5 P3 125.3(13) . . ?
C16 O6 P3 129.6(16) . . ?
C19 O7 P4 122.8(15) . . ?
C22 O8 P4 140(2) . . ?
C25 O9 P5 123.6(13) . . ?
C28 O10 P5 122.8(10) . . ?
C31 O11 P6 120.9(13) . . ?
C34 O12 P6 125.6(12) . . ?
C37 O13 P7 120.3(10) . . ?
C40 O14 P7 120.5(11) . . ?
C43 O15 P8 126.5(17) . . ?
C46 O16 P8 122.4(12) . . ?
C49 O17 P9 119.9(10) . . ?
C52 O18 P9 120.7(11) . . ?
C55 O19 P10 124.0(15) . . ?
C58 O20 P10 120.9(12) . . ?
C61 O21 P11 120.3(10) . . ?
C64 O22 P11 118.0(11) . . ?
C67 O23 P12 121.1(17) . . ?
C70 O24 P12 125.9(17) . . ?
O1 P1 O2 100.7(6) . . ?
O1 P1 Se2 109.6(5) . . ?
O2 P1 Se2 114.1(5) . . ?
O1 P1 Se1 111.2(5) . . ?
O2 P1 Se1 101.4(5) . . ?
Se2 P1 Se1 118.31(19) . . ?
O3 P2 O4 104.7(9) . . ?
O3 P2 Se4 108.2(6) . . ?
O4 P2 Se4 114.3(6) . . ?
O3 P2 Se3 106.7(6) . . ?
O4 P2 Se3 103.6(6) . . ?
Se4 P2 Se3 118.2(2) . . ?
O6 P3 O5 105.5(9) . . ?
O6 P3 Se5 105.4(8) . . ?
O5 P3 Se5 111.6(6) . . ?
O6 P3 Se6 108.9(9) . . ?
O5 P3 Se6 106.1(6) . . ?
Se5 P3 Se6 118.6(2) . . ?
O8 P4 O7 105.0(12) . . ?
O8 P4 Se7 109.0(10) . . ?
O7 P4 Se7 114.8(6) . . ?
O8 P4 Se8 106.7(9) . . ?
O7 P4 Se8 101.8(7) . . ?
Se7 P4 Se8 118.5(2) . . ?
O9 P5 O10 101.2(7) . . ?
O9 P5 Se10 110.8(5) . . ?
O10 P5 Se10 114.3(5) . . ?
O9 P5 Se9 109.3(5) . . ?
O10 P5 Se9 103.2(4) . . ?
Se10 P5 Se9 116.72(19) . . ?
O11 P6 O12 101.4(7) . . ?
O11 P6 Se11 113.9(6) . . ?
O12 P6 Se11 109.4(6) . . ?
O11 P6 Se12 102.5(5) . . ?
O12 P6 Se12 110.6(6) . . ?
Se11 P6 Se12 117.7(2) . . ?
O13 P7 O14 104.3(6) . . ?
O13 P7 Se14 106.5(5) . . ?
O14 P7 Se14 114.4(5) . . ?
O13 P7 Se13 110.6(5) . . ?
O14 P7 Se13 101.7(4) . . ?
Se14 P7 Se13 118.5(2) . . ?
O15 P8 O16 100.0(7) . . ?
O15 P8 Se15 113.0(6) . . ?
O16 P8 Se15 110.4(6) . . ?
O15 P8 Se16 104.1(6) . . ?
O16 P8 Se16 110.7(5) . . ?
Se15 P8 Se16 117.2(2) . . ?
O17 P9 O18 107.3(7) . . ?
O17 P9 Se17 113.8(5) . . ?
O18 P9 Se17 103.9(5) . . ?
O17 P9 Se18 101.6(5) . . ?
O18 P9 Se18 111.2(5) . . ?
Se17 P9 Se18 118.71(19) . . ?
O20 P10 O19 99.3(7) . . ?
O20 P10 Se20 112.9(6) . . ?
O19 P10 Se20 108.5(6) . . ?
O20 P10 Se19 109.3(6) . . ?
O19 P10 Se19 107.4(6) . . ?
Se20 P10 Se19 117.7(2) . . ?
O22 P11 O21 105.4(6) . . ?
O22 P11 Se21 113.8(5) . . ?
O21 P11 Se21 105.6(5) . . ?
O22 P11 Se22 102.3(5) . . ?
O21 P11 Se22 110.9(5) . . ?
Se21 P11 Se22 118.18(18) . . ?
O23 P12 O24 97.2(10) . . ?
O23 P12 Se24 112.9(8) . . ?
O24 P12 Se24 113.3(6) . . ?
O23 P12 Se23 112.0(7) . . ?
O24 P12 Se23 101.1(7) . . ?
Se24 P12 Se23 117.8(2) . . ?
P1 Se1 Ag16 99.77(13) . . ?
P1 Se1 Ag12 93.79(12) . . ?
Ag16 Se1 Ag12 69.18(5) . . ?
P1 Se2 Ag15 97.15(13) . . ?
P2 Se3 Ag16 99.53(14) . . ?
P2 Se3 Ag10 94.32(13) . . ?
Ag16 Se3 Ag10 68.80(5) . . ?
P2 Se4 Ag20 97.53(14) . . ?
P3 Se5 Ag20 96.89(15) . . ?
P3 Se6 Ag19 99.46(15) . . ?
P3 Se6 Ag11 91.74(14) . . ?
Ag19 Se6 Ag11 68.76(5) . . ?
P4 Se7 Ag15 95.49(16) . . ?
P4 Se8 Ag19 99.90(17) . . ?
P4 Se8 Ag6 94.18(14) . . ?
Ag19 Se8 Ag6 68.05(6) . . ?
P5 Se9 Ag19 98.93(13) . . ?
P5 Se9 Ag7 94.29(13) . . ?
Ag19 Se9 Ag7 68.20(5) . . ?
P5 Se10 Ag17 99.42(13) . . ?
P6 Se11 Ag15 95.26(14) . . ?
P6 Se12 Ag13 100.76(14) . . ?
P6 Se12 Ag5 94.50(13) . . ?
Ag13 Se12 Ag5 68.63(5) . . ?
P7 Se13 Ag16 97.82(13) . . ?
P7 Se13 Ag4 94.46(13) . . ?
Ag16 Se13 Ag4 69.20(5) . . ?
P7 Se14 Ag14 94.83(14) . . ?
P8 Se15 Ag20 94.96(14) . . ?
P8 Se16 Ag18 102.46(14) . . ?
P8 Se16 Ag8 92.72(13) . . ?
Ag18 Se16 Ag8 68.29(5) . . ?
P9 Se17 Ag14 95.26(13) . . ?
P9 Se18 Ag18 97.44(12) . . ?
P9 Se18 Ag9 93.77(12) . . ?
Ag18 Se18 Ag9 67.87(5) . . ?
P10 Se19 Ag18 102.89(14) . . ?
P10 Se19 Ag1 94.09(13) . . ?
Ag18 Se19 Ag1 68.22(5) . . ?
P10 Se20 Ag17 95.19(14) . . ?
P11 Se21 Ag17 95.69(13) . . ?
P11 Se22 Ag13 96.63(13) . . ?
P11 Se22 Ag3 91.31(12) . . ?
Ag13 Se22 Ag3 68.77(5) . . ?
P12 Se23 Ag13 101.37(18) . . ?
P12 Se23 Ag2 91.14(15) . . ?
Ag13 Se23 Ag2 69.28(5) . . ?
P12 Se24 Ag14 99.14(18) . . ?

_refine_diff_density_max         2.391
_refine_diff_density_min         -1.609
_refine_diff_density_rms         0.221

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_1b
_database_code_depnum_ccdc_archive 'CCDC 2069764'
loop_
_audit_author_name
_audit_author_address
'Chen-Wei Liu'
;Department of Chemistry, National Dong Hwa University
Taiwan
;
_audit_update_record             
;
2021-03-11 deposited with the CCDC.	2021-06-25 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2018/3
_shelx_SHELXL_version_number     2018/3
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C81 H186 Ag20 O27 P12 Pt Se24'
_chemical_formula_weight         6211.46

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Se Se -0.0929 2.2259 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      monoclinic
_space_group_IT_number           7
_space_group_name_H-M_alt        'P n'
_space_group_name_Hall           'P -2yac'

_shelx_space_group_comment       
; 
The symmetry employed for this shelxl refinement is uniquely defined 
by the following loop, which should always be used as a source of 
symmetry information in preference to the above space-group names. 
They are only intended as comments. 
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'x+1/2, -y, z+1/2'

_cell_length_a                   17.9783(12)
_cell_length_b                   26.4928(18)
_cell_length_c                   18.7771(13)
_cell_angle_alpha                90
_cell_angle_beta                 112.7096(12)
_cell_angle_gamma                90
_cell_volume                     8250.1(10)
_cell_formula_units_Z            2
_cell_measurement_temperature    100(2)
_cell_measurement_reflns_used    9929
_cell_measurement_theta_min      2.32
_cell_measurement_theta_max      26.37

_exptl_crystal_description       plate
_exptl_crystal_colour            red
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    2.500
_exptl_crystal_F_000             5804
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          0.100
_exptl_crystal_size_mid          0.060
_exptl_crystal_size_min          0.040
_exptl_absorpt_coefficient_mu    8.618
_shelx_estimated_absorpt_T_min   0.479
_shelx_estimated_absorpt_T_max   0.724
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_correction_T_min  0.5307
_exptl_absorpt_correction_T_max  0.7454
_exptl_absorpt_process_details   SADABS
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      100(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_source                   ?
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            58143
_diffrn_reflns_av_unetI/netI     0.0461
_diffrn_reflns_av_R_equivalents  0.0309
_diffrn_reflns_limit_h_min       -21
_diffrn_reflns_limit_h_max       21
_diffrn_reflns_limit_k_min       -31
_diffrn_reflns_limit_k_max       31
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_limit_l_max       22
_diffrn_reflns_theta_min         1.449
_diffrn_reflns_theta_max         25.000
_diffrn_reflns_theta_full        25.000
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measured_fraction_theta_full 0.996
_diffrn_reflns_Laue_measured_fraction_max 0.996
_diffrn_reflns_Laue_measured_fraction_full 0.996
_diffrn_reflns_point_group_measured_fraction_max 0.932
_diffrn_reflns_point_group_measured_fraction_full 0.932
_reflns_number_total             27116
_reflns_number_gt                24794
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.870
_reflns_Friedel_fraction_max     0.868
_reflns_Friedel_fraction_full    0.868

_reflns_special_details          
; 
 Reflections were merged by SHELXL according to the crystal 
 class for the calculation of statistics and refinement. 
  
 _reflns_Friedel_fraction is defined as the number of unique 
 Friedel pairs measured divided by the number that would be 
 possible theoretically, ignoring centric projections and 
 systematic absences. Completness statistics refer to single and 
 composite reflections containing twin component 1 only. 
;

_computing_data_collection       'Bruker APEX2'
_computing_cell_refinement       'Bruker SAINT'
_computing_data_reduction        'Bruker SAINT'
_computing_structure_solution    'SHELXS-97 (Sheldrick 2008)'
_computing_structure_refinement  'SHELXL-2018/3 (Sheldrick, 2018)'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_refine_special_details          
; 
 Refined as a 2-component inversion twin. 
;
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0477P)²+65.8507P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_abs_structure_details 
; 
 Refined as an inversion twin. 
;
_refine_ls_abs_structure_Flack   0.293(7)
_chemical_absolute_configuration ?
_refine_ls_number_reflns         27116
_refine_ls_number_parameters     1576
_refine_ls_number_restraints     495
_refine_ls_R_factor_all          0.0432
_refine_ls_R_factor_gt           0.0367
_refine_ls_wR_factor_ref         0.0981
_refine_ls_wR_factor_gt          0.0943
_refine_ls_goodness_of_fit_ref   1.039
_refine_ls_restrained_S_all      1.032
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt1 Pt 0.12136(4) 0.75463(2) 0.69311(4) 0.01244(12) Uani 1 1 d . . . . .
Ag1 Ag 0.04996(7) 0.80851(4) 0.55701(8) 0.0158(3) Uani 0.95 1 d . . P A 1
Ag2 Ag 0.20043(8) 0.84103(4) 0.67714(8) 0.0154(3) Uani 0.95 1 d . . P A 1
Ag3 Ag 0.04775(7) 0.84563(4) 0.69864(8) 0.0154(3) Uani 0.95 1 d . . P A 1
Ag4 Ag -0.04501(8) 0.75571(4) 0.63093(8) 0.0158(3) Uani 0.95 1 d . . P A 1
Ag5 Ag 0.04714(8) 0.69697(4) 0.56228(8) 0.0163(3) Uani 0.95 1 d . . P A 1
Ag6 Ag 0.19340(8) 0.74967(4) 0.58799(8) 0.0151(3) Uani 0.95 1 d . . P A 1
Ag7 Ag 0.28754(8) 0.75469(4) 0.75528(8) 0.0158(3) Uani 0.95 1 d . . P A 1
Ag8 Ag 0.19486(7) 0.81060(4) 0.82553(8) 0.0151(3) Uani 0.95 1 d . . P A 1
Ag9 Ag 0.04655(8) 0.76051(4) 0.79587(8) 0.0156(3) Uani 0.95 1 d . . P A 1
Ag10 Ag 0.04245(7) 0.66871(4) 0.70901(8) 0.0162(3) Uani 0.95 1 d . . P A 1
Ag11 Ag 0.19329(8) 0.66379(4) 0.68591(8) 0.0164(3) Uani 0.95 1 d . . P A 1
Ag12 Ag 0.19479(7) 0.70088(4) 0.82825(8) 0.0152(3) Uani 0.95 1 d . . P A 1
Ag1B Ag 0.1249(14) 0.6552(8) 0.7476(15) 0.0158(3) Uani 0.05 1 d . . P A 2
Ag2B Ag 0.2475(14) 0.8127(8) 0.7903(15) 0.0154(3) Uani 0.05 1 d . . P A 2
Ag3B Ag 0.1245(14) 0.8479(8) 0.6431(15) 0.0154(3) Uani 0.05 1 d . . P A 2
Ag4B Ag -0.0212(14) 0.7989(9) 0.6191(15) 0.0158(3) Uani 0.05 1 d . . P A 2
Ag5B Ag -0.0019(14) 0.6892(8) 0.6028(15) 0.0163(3) Uani 0.05 1 d . . P A 2
Ag6B Ag 0.1609(14) 0.6746(8) 0.6130(15) 0.0151(3) Uani 0.05 1 d . . P A 2
Ag7B Ag 0.1677(14) 0.7395(9) 0.8512(15) 0.0158(3) Uani 0.05 1 d . . P A 2
Ag8B Ag 0.0029(14) 0.7268(8) 0.7483(14) 0.0151(3) Uani 0.05 1 d . . P A 2
Ag9B Ag 0.2683(14) 0.7036(8) 0.7755(15) 0.0156(3) Uani 0.05 1 d . . P A 2
Ag0X Ag 0.0801(14) 0.7641(9) 0.5384(15) 0.0162(3) Uani 0.05 1 d . . P A 2
Ag1X Ag 0.2476(14) 0.7749(8) 0.6478(15) 0.0164(3) Uani 0.05 1 d . . P A 2
Ag2X Ag 0.0766(14) 0.8266(8) 0.7738(15) 0.0152(3) Uani 0.05 1 d . . P A 2
Ag13 Ag -0.09815(8) 0.75302(4) 0.46136(8) 0.0196(3) Uani 1 1 d . . . . .
Ag14 Ag -0.09984(7) 0.82197(4) 0.72549(8) 0.0177(3) Uani 1 1 d . . . . .
Ag15 Ag 0.17854(7) 0.91757(4) 0.78104(8) 0.0176(3) Uani 1 1 d . . . . .
Ag16 Ag 0.18329(8) 0.84834(4) 0.51705(8) 0.0200(3) Uani 1 1 d . . . . .
Ag17 Ag 0.34026(7) 0.68794(4) 0.65737(8) 0.0204(3) Uani 1 1 d . . . . .
Ag18 Ag 0.33866(8) 0.75567(4) 0.92398(8) 0.0183(3) Uani 1 1 d . . . . .
Ag19 Ag 0.06883(8) 0.66077(4) 0.87619(8) 0.0203(3) Uani 1 1 d . . . . .
Ag20 Ag 0.06482(8) 0.58877(4) 0.61083(8) 0.0216(3) Uani 1 1 d . . . . .
Se1 Se 0.14348(10) 0.59346(6) 0.52000(11) 0.0240(4) Uani 1 1 d . . . . .
Se2 Se 0.31492(10) 0.59932(6) 0.70882(11) 0.0232(4) Uani 1 1 d . . . . .
Se3 Se 0.12755(12) 0.54603(7) 0.74631(12) 0.0294(4) Uani 1 1 d . . . . .
Se4 Se -0.04465(10) 0.61224(7) 0.76645(11) 0.0257(4) Uani 1 1 d . . . . .
Se5 Se -0.08994(11) 0.60552(6) 0.55529(12) 0.0268(4) Uani 1 1 d . . . . .
Se6 Se -0.03577(11) 0.67804(6) 0.41284(11) 0.0246(4) Uani 1 1 d . . . . .
Se7 Se -0.07590(10) 0.84798(6) 0.44062(10) 0.0219(4) Uani 1 1 d . . . . .
Se8 Se 0.09160(10) 0.79670(7) 0.39591(10) 0.0242(4) Uani 1 1 d . . . . .
Se9 Se 0.26349(10) 0.70042(6) 0.50676(10) 0.0207(4) Uani 1 1 d . . . . .
Se10 Se 0.33931(10) 0.82931(6) 0.56811(11) 0.0228(4) Uani 1 1 d . . . . .
Se11 Se 0.43269(10) 0.75865(6) 0.74802(10) 0.0216(4) Uani 1 1 d . . . . .
Se12 Se 0.41077(10) 0.67558(6) 0.89639(10) 0.0222(4) Uani 1 1 d . . . . .
Se13 Se 0.21379(10) 0.62307(6) 0.92499(11) 0.0223(4) Uani 1 1 d . . . . .
Se14 Se 0.25888(11) 0.74874(6) 1.01549(11) 0.0239(4) Uani 1 1 d . . . . .
Se15 Se -0.15423(10) 0.73440(6) 0.74795(10) 0.0202(4) Uani 1 1 d . . . . .
Se16 Se 0.02919(10) 0.74405(6) 0.92835(10) 0.0183(3) Uani 1 1 d . . . . .
Se17 Se -0.19243(9) 0.72677(6) 0.53343(10) 0.0191(3) Uani 1 1 d . . . . .
Se18 Se -0.16182(10) 0.86189(6) 0.58805(10) 0.0201(4) Uani 1 1 d . . . . .
Se19 Se -0.02336(10) 0.88353(6) 0.83786(10) 0.0241(4) Uani 1 1 d . . . . .
Se20 Se 0.03217(9) 0.94636(6) 0.69084(10) 0.0190(3) Uani 1 1 d . . . . .
Se21 Se 0.13519(10) 0.93531(6) 0.55012(10) 0.0242(4) Uani 1 1 d . . . . .
Se22 Se 0.30120(9) 0.91858(6) 0.73791(10) 0.0185(3) Uani 1 1 d . . . . .
Se23 Se 0.20113(11) 0.88653(6) 0.92057(10) 0.0228(4) Uani 1 1 d . . . . .
Se24 Se 0.39383(10) 0.84566(6) 0.91471(11) 0.0264(4) Uani 1 1 d . . . . .
P1 P 0.2525(3) 0.56015(16) 0.5996(3) 0.0244(10) Uani 1 1 d . . . . .
P2 P 0.0197(3) 0.54149(17) 0.7683(3) 0.0285(11) Uani 1 1 d . . . . .
P3 P -0.1033(3) 0.61654(16) 0.4374(3) 0.0270(11) Uani 1 1 d . . . . .
P4 P -0.0148(3) 0.84313(16) 0.3611(3) 0.0226(10) Uani 1 1 d . . . . .
P5 P 0.3311(3) 0.76612(16) 0.4944(3) 0.0206(9) Uani 1 1 d . . . . .
P6 P 0.4898(3) 0.71736(17) 0.8560(3) 0.0221(10) Uani 1 1 d . . . . .
P7 P 0.2700(3) 0.66831(17) 1.0284(3) 0.0244(10) Uani 1 1 d . . . . .
P8 P -0.1012(3) 0.73587(16) 0.8718(3) 0.0195(9) Uani 1 1 d . . . . .
P9 P -0.2435(3) 0.80158(15) 0.5331(3) 0.0194(9) Uani 1 1 d . . . . .
P10 P -0.0311(3) 0.94975(16) 0.7687(3) 0.0225(10) Uani 1 1 d . . . . .
P11 P 0.2496(3) 0.96117(16) 0.6308(3) 0.0223(10) Uani 1 1 d . . . . .
P12 P 0.3320(3) 0.88527(16) 0.9759(3) 0.0257(10) Uani 1 1 d . . . . .
O1 O 0.3071(9) 0.5529(7) 0.5500(9) 0.053(4) Uani 1 1 d . . . . .
O2 O 0.2377(8) 0.5055(4) 0.6265(9) 0.036(3) Uani 1 1 d . . . . .
O3 O -0.0390(9) 0.5039(5) 0.7086(9) 0.042(3) Uani 1 1 d . . . . .
O4 O 0.0363(9) 0.5188(5) 0.8510(9) 0.045(4) Uani 1 1 d . . . . .
O5 O -0.0779(8) 0.5689(5) 0.4019(8) 0.035(3) Uani 1 1 d . . . . .
O6 O -0.1983(8) 0.6234(5) 0.3938(9) 0.044(4) Uani 1 1 d . . . . .
O7 O -0.0766(8) 0.8265(5) 0.2771(7) 0.030(3) Uani 1 1 d . . . . .
O8 O 0.0002(7) 0.9009(4) 0.3473(7) 0.025(3) Uani 1 1 d . . . . .
O9 O 0.2884(7) 0.7801(4) 0.4053(7) 0.025(3) Uani 1 1 d . . . . .
O10 O 0.4217(7) 0.7495(4) 0.5096(8) 0.027(3) Uani 1 1 d . . . . .
O11 O 0.5600(7) 0.6825(5) 0.8517(8) 0.029(3) Uani 1 1 d . . . . .
O12 O 0.5430(7) 0.7592(4) 0.9156(7) 0.025(3) Uani 1 1 d . . . . .
O13 O 0.3606(7) 0.6492(5) 1.0609(8) 0.031(3) Uani 1 1 d . . . . .
O14 O 0.2436(8) 0.6491(5) 1.0942(8) 0.034(3) Uani 1 1 d . . . . .
O15 O -0.1290(7) 0.6849(4) 0.8962(7) 0.024(3) Uani 1 1 d . . . . .
O16 O -0.1330(6) 0.7797(4) 0.9091(7) 0.021(2) Uani 1 1 d . . . . .
O17 O -0.3077(7) 0.7921(4) 0.5697(7) 0.022(3) Uani 1 1 d . . . . .
O18 O -0.2895(7) 0.8214(4) 0.4470(7) 0.026(3) Uani 1 1 d . . . . .
O19 O -0.1198(7) 0.9640(4) 0.7138(8) 0.029(3) Uani 1 1 d . . . . .
O20 O -0.0073(8) 0.9988(5) 0.8211(8) 0.032(3) Uani 1 1 d . . . . .
O21 O 0.3175(7) 0.9618(5) 0.5974(7) 0.027(3) Uani 1 1 d . . . . .
O22 O 0.2468(8) 1.0200(4) 0.6475(8) 0.035(3) Uani 1 1 d . . . . .
O23 O 0.3467(9) 0.8624(5) 1.0590(8) 0.044(4) Uani 1 1 d . . . . .
O24 O 0.3679(9) 0.9405(4) 1.0000(8) 0.039(3) Uani 1 1 d . . . . .
O25 O 0.6437(9) 0.9216(7) 0.7891(11) 0.063(5) Uani 1 1 d . . . . .
O26 O 0.6392(12) 0.5574(9) 0.6406(14) 0.092(7) Uani 1 1 d . . . . .
O27 O 0.1159(12) 0.9165(7) 0.1527(10) 0.066(5) Uani 1 1 d . . . . .
C1 C 0.3935(14) 0.5613(8) 0.5778(14) 0.053(5) Uani 1 1 d D . . . .
H1 H 0.408354 0.594829 0.603991 0.063 Uiso 1 1 calc R U . . .
C2 C 0.440(2) 0.5193(11) 0.630(2) 0.089(9) Uani 1 1 d . . . . .
H2A H 0.497087 0.522464 0.640164 0.133 Uiso 1 1 calc R U . . .
H2B H 0.419601 0.486693 0.605797 0.133 Uiso 1 1 calc R U . . .
H2C H 0.432283 0.521395 0.679340 0.133 Uiso 1 1 calc R U . . .
C3 C 0.413(2) 0.5593(11) 0.5062(17) 0.087(9) Uani 1 1 d D . . . .
H3A H 0.379224 0.583647 0.468117 0.130 Uiso 1 1 calc R U . . .
H3B H 0.402532 0.525268 0.484189 0.130 Uiso 1 1 calc R U . . .
H3C H 0.469980 0.567771 0.520015 0.130 Uiso 1 1 calc R U . . .
C4 C 0.1949(13) 0.4673(7) 0.5668(13) 0.039(5) Uani 1 1 d . . . . .
H4 H 0.174986 0.483832 0.514848 0.047 Uiso 1 1 calc R U . . .
C5 C 0.1236(14) 0.4508(8) 0.5842(14) 0.047(5) Uani 1 1 d . . . . .
H5A H 0.099706 0.480248 0.599011 0.071 Uiso 1 1 calc R U . . .
H5B H 0.141254 0.426441 0.626770 0.071 Uiso 1 1 calc R U . . .
H5C H 0.083326 0.435054 0.538288 0.071 Uiso 1 1 calc R U . . .
C6 C 0.2522(16) 0.4254(8) 0.5683(16) 0.056(6) Uani 1 1 d . . . . .
H6A H 0.278416 0.412567 0.621079 0.084 Uiso 1 1 calc R U . . .
H6B H 0.293205 0.438394 0.550616 0.084 Uiso 1 1 calc R U . . .
H6C H 0.222221 0.398061 0.534114 0.084 Uiso 1 1 calc R U . . .
C7 C -0.1256(13) 0.5009(8) 0.6837(13) 0.042(5) Uani 1 1 d . . . . .
H7 H -0.148172 0.535899 0.675013 0.051 Uiso 1 1 calc R U . . .
C8 C -0.1496(14) 0.4761(11) 0.7414(17) 0.068(8) Uani 1 1 d . . . . .
H8A H -0.116692 0.489053 0.792823 0.103 Uiso 1 1 calc R U . . .
H8B H -0.141656 0.439601 0.739898 0.103 Uiso 1 1 calc R U . . .
H8C H -0.206640 0.483142 0.729863 0.103 Uiso 1 1 calc R U . . .
C9 C -0.1546(16) 0.4736(9) 0.6073(15) 0.064(7) Uani 1 1 d . . . . .
H9A H -0.143986 0.437346 0.616211 0.096 Uiso 1 1 calc R U . . .
H9B H -0.126033 0.486530 0.575978 0.096 Uiso 1 1 calc R U . . .
H9C H -0.212687 0.479057 0.579932 0.096 Uiso 1 1 calc R U . . .
C10 C 0.0910(15) 0.4758(9) 0.8853(14) 0.050(5) Uani 1 1 d . . . . .
H10 H 0.124970 0.471400 0.854284 0.060 Uiso 1 1 calc R U . . .
C11 C 0.145(2) 0.4889(12) 0.9632(18) 0.098(12) Uani 1 1 d . . . . .
H11A H 0.114575 0.504464 0.990586 0.148 Uiso 1 1 calc R U . . .
H11B H 0.186039 0.512691 0.960921 0.148 Uiso 1 1 calc R U . . .
H11C H 0.171929 0.458276 0.990549 0.148 Uiso 1 1 calc R U . . .
C12 C 0.0444(17) 0.4274(9) 0.8778(16) 0.064(7) Uani 1 1 d . . . . .
H12A H 0.020811 0.417197 0.823417 0.095 Uiso 1 1 calc R U . . .
H12B H 0.001260 0.432711 0.896728 0.095 Uiso 1 1 calc R U . . .
H12C H 0.080763 0.400897 0.908276 0.095 Uiso 1 1 calc R U . . .
C13 C -0.0858(13) 0.5158(7) 0.4208(14) 0.043(5) Uani 1 1 d . . . . .
H13 H -0.067577 0.512161 0.478020 0.052 Uiso 1 1 calc R U . . .
C14 C -0.0322(13) 0.4857(7) 0.3935(14) 0.044(5) Uani 1 1 d . . . . .
H14A H -0.042008 0.494904 0.340116 0.066 Uiso 1 1 calc R U . . .
H14B H -0.043448 0.449658 0.396035 0.066 Uiso 1 1 calc R U . . .
H14C H 0.024234 0.492541 0.426486 0.066 Uiso 1 1 calc R U . . .
C15 C -0.1745(13) 0.5021(10) 0.3828(17) 0.058(7) Uani 1 1 d . . . . .
H15A H -0.182508 0.467548 0.396977 0.087 Uiso 1 1 calc R U . . .
H15B H -0.192108 0.504570 0.326619 0.087 Uiso 1 1 calc R U . . .
H15C H -0.206232 0.525461 0.400389 0.087 Uiso 1 1 calc R U . . .
C16 C -0.2411(13) 0.6532(8) 0.3253(13) 0.050(5) Uani 1 1 d . . . . .
H16 H -0.220352 0.688597 0.332570 0.060 Uiso 1 1 calc R U . . .
C17 C -0.2273(18) 0.6294(10) 0.2619(15) 0.072(7) Uani 1 1 d . . . . .
H17A H -0.248419 0.594858 0.255016 0.108 Uiso 1 1 calc R U . . .
H17B H -0.169254 0.628545 0.273512 0.108 Uiso 1 1 calc R U . . .
H17C H -0.254743 0.648708 0.214466 0.108 Uiso 1 1 calc R U . . .
C18 C -0.3236(15) 0.6522(9) 0.3195(19) 0.069(7) Uani 1 1 d . . . . .
H18A H -0.348104 0.619624 0.298297 0.103 Uiso 1 1 calc R U . . .
H18B H -0.354043 0.679444 0.285484 0.103 Uiso 1 1 calc R U . . .
H18C H -0.324662 0.656740 0.370938 0.103 Uiso 1 1 calc R U . . .
C19 C -0.0780(12) 0.7769(7) 0.2426(13) 0.037(4) Uani 1 1 d . . . . .
H19 H -0.045367 0.752388 0.283077 0.044 Uiso 1 1 calc R U . . .
C20 C -0.0416(16) 0.7824(11) 0.1789(16) 0.066(7) Uani 1 1 d . . . . .
H20A H 0.016433 0.788880 0.203742 0.098 Uiso 1 1 calc R U . . .
H20B H -0.067884 0.810543 0.144581 0.098 Uiso 1 1 calc R U . . .
H20C H -0.050744 0.751115 0.148836 0.098 Uiso 1 1 calc R U . . .
C21 C -0.1665(14) 0.7606(10) 0.2089(16) 0.060(7) Uani 1 1 d . . . . .
H21A H -0.194268 0.777148 0.158912 0.089 Uiso 1 1 calc R U . . .
H21B H -0.192259 0.770292 0.244313 0.089 Uiso 1 1 calc R U . . .
H21C H -0.169700 0.723889 0.201853 0.089 Uiso 1 1 calc R U . . .
C22 C 0.0334(12) 0.9170(7) 0.2908(11) 0.033(4) Uani 1 1 d . . . . .
H22 H 0.045328 0.886529 0.265639 0.040 Uiso 1 1 calc R U . . .
C23 C 0.1111(14) 0.9446(9) 0.3350(12) 0.046(5) Uani 1 1 d . . . . .
H23A H 0.148559 0.921844 0.373360 0.069 Uiso 1 1 calc R U . . .
H23B H 0.099965 0.973870 0.361200 0.069 Uiso 1 1 calc R U . . .
H23C H 0.135326 0.955955 0.299108 0.069 Uiso 1 1 calc R U . . .
C24 C -0.0326(15) 0.9472(10) 0.2314(14) 0.057(7) Uani 1 1 d . . . . .
H24A H -0.053818 0.971979 0.257420 0.086 Uiso 1 1 calc R U . . .
H24B H -0.076059 0.924434 0.200434 0.086 Uiso 1 1 calc R U . . .
H24C H -0.010862 0.964694 0.197676 0.086 Uiso 1 1 calc R U . . .
C25 C 0.2888(11) 0.8272(7) 0.3701(12) 0.033(4) Uani 1 1 d . . . . .
H25 H 0.267465 0.853310 0.395784 0.039 Uiso 1 1 calc R U . . .
C26 C 0.2343(12) 0.8243(10) 0.2889(13) 0.046(5) Uani 1 1 d . . . . .
H26A H 0.179474 0.817316 0.285336 0.068 Uiso 1 1 calc R U . . .
H26B H 0.251960 0.797125 0.263618 0.068 Uiso 1 1 calc R U . . .
H26C H 0.235086 0.856446 0.263429 0.068 Uiso 1 1 calc R U . . .
C27 C 0.3758(12) 0.8427(8) 0.3803(13) 0.040(5) Uani 1 1 d . . . . .
H27A H 0.395907 0.819384 0.351346 0.060 Uiso 1 1 calc R U . . .
H27B H 0.411145 0.841509 0.435133 0.060 Uiso 1 1 calc R U . . .
H27C H 0.375165 0.877122 0.360766 0.060 Uiso 1 1 calc R U . . .
C28 C 0.4399(11) 0.6995(7) 0.4844(13) 0.032(4) Uani 1 1 d . . . . .
H28 H 0.410871 0.673130 0.501804 0.038 Uiso 1 1 calc R U . . .
C29 C 0.4143(13) 0.6954(8) 0.4008(13) 0.042(5) Uani 1 1 d . . . . .
H29A H 0.442343 0.720959 0.382624 0.063 Uiso 1 1 calc R U . . .
H29B H 0.355992 0.700914 0.376144 0.063 Uiso 1 1 calc R U . . .
H29C H 0.427466 0.661739 0.387610 0.063 Uiso 1 1 calc R U . . .
C30 C 0.5300(12) 0.6930(7) 0.5300(15) 0.043(5) Uani 1 1 d . . . . .
H30A H 0.555166 0.726217 0.544976 0.064 Uiso 1 1 calc R U . . .
H30B H 0.553989 0.675609 0.498019 0.064 Uiso 1 1 calc R U . . .
H30C H 0.538729 0.672975 0.576451 0.064 Uiso 1 1 calc R U . . .
C31 C 0.5467(13) 0.6377(8) 0.8035(13) 0.041(4) Uani 1 1 d . . . . .
H31 H 0.489954 0.625871 0.789280 0.049 Uiso 1 1 calc R U . . .
C32 C 0.5599(14) 0.6475(9) 0.7363(13) 0.049(6) Uani 1 1 d . . . . .
H32A H 0.608983 0.667647 0.748935 0.073 Uiso 1 1 calc R U . . .
H32B H 0.513820 0.666110 0.699812 0.073 Uiso 1 1 calc R U . . .
H32C H 0.566000 0.615489 0.712871 0.073 Uiso 1 1 calc R U . . .
C33 C 0.6061(14) 0.5976(8) 0.8587(15) 0.050(6) Uani 1 1 d . . . . .
H33A H 0.657310 0.614040 0.889552 0.075 Uiso 1 1 calc R U . . .
H33B H 0.615806 0.570580 0.827734 0.075 Uiso 1 1 calc R U . . .
H33C H 0.582106 0.583382 0.893069 0.075 Uiso 1 1 calc R U . . .
C34 C 0.5740(11) 0.7536(7) 1.0002(11) 0.027(4) Uani 1 1 d . . . . .
H34 H 0.527821 0.746823 1.016080 0.033 Uiso 1 1 calc R U . . .
C35 C 0.6109(13) 0.8036(7) 1.0325(12) 0.037(5) Uani 1 1 d . . . . .
H35A H 0.626887 0.821145 0.994598 0.056 Uiso 1 1 calc R U . . .
H35B H 0.658547 0.798225 1.080030 0.056 Uiso 1 1 calc R U . . .
H35C H 0.571535 0.824182 1.043818 0.056 Uiso 1 1 calc R U . . .
C36 C 0.6333(12) 0.7106(8) 1.0268(12) 0.036(5) Uani 1 1 d . . . . .
H36A H 0.679893 0.717859 1.013626 0.054 Uiso 1 1 calc R U . . .
H36B H 0.607331 0.679391 1.001319 0.054 Uiso 1 1 calc R U . . .
H36C H 0.651253 0.706739 1.082900 0.054 Uiso 1 1 calc R U . . .
C37 C 0.4302(12) 0.6761(8) 1.1171(13) 0.042(4) Uani 1 1 d . . . . .
H37 H 0.432335 0.711137 1.098165 0.050 Uiso 1 1 calc R U . . .
C38 C 0.4249(14) 0.6784(10) 1.1910(14) 0.052(6) Uani 1 1 d . . . . .
H38A H 0.467934 0.700107 1.225378 0.079 Uiso 1 1 calc R U . . .
H38B H 0.430682 0.644392 1.212952 0.079 Uiso 1 1 calc R U . . .
H38C H 0.372389 0.692338 1.185340 0.079 Uiso 1 1 calc R U . . .
C39 C 0.4994(12) 0.6478(11) 1.1179(14) 0.055(6) Uani 1 1 d . . . . .
H39A H 0.503430 0.650676 1.067515 0.083 Uiso 1 1 calc R U . . .
H39B H 0.493075 0.612184 1.128732 0.083 Uiso 1 1 calc R U . . .
H39C H 0.548437 0.661260 1.158048 0.083 Uiso 1 1 calc R U . . .
C40 C 0.1634(13) 0.6596(8) 1.0961(13) 0.040(5) Uani 1 1 d . . . . .
H40 H 0.124856 0.671098 1.044194 0.048 Uiso 1 1 calc R U . . .
C41 C 0.171(2) 0.6985(10) 1.1554(17) 0.076(9) Uani 1 1 d . . . . .
H41A H 0.213538 0.722447 1.158353 0.114 Uiso 1 1 calc R U . . .
H41B H 0.184397 0.682208 1.205703 0.114 Uiso 1 1 calc R U . . .
H41C H 0.119610 0.716613 1.141344 0.114 Uiso 1 1 calc R U . . .
C42 C 0.1369(16) 0.6074(9) 1.1166(19) 0.066(8) Uani 1 1 d . . . . .
H42A H 0.173943 0.597214 1.168279 0.099 Uiso 1 1 calc R U . . .
H42B H 0.137981 0.582175 1.078797 0.099 Uiso 1 1 calc R U . . .
H42C H 0.082075 0.609978 1.115463 0.099 Uiso 1 1 calc R U . . .
C43 C -0.0978(12) 0.6639(7) 0.9734(12) 0.033(4) Uani 1 1 d . . . . .
H43 H -0.041727 0.676611 1.002187 0.040 Uiso 1 1 calc R U . . .
C44 C -0.1494(13) 0.6788(8) 1.0144(12) 0.039(5) Uani 1 1 d . . . . .
H44A H -0.204236 0.666255 0.986253 0.059 Uiso 1 1 calc R U . . .
H44B H -0.150365 0.715673 1.017926 0.059 Uiso 1 1 calc R U . . .
H44C H -0.127872 0.664332 1.066512 0.059 Uiso 1 1 calc R U . . .
C45 C -0.0964(16) 0.6067(8) 0.9666(16) 0.054(6) Uani 1 1 d . . . . .
H45A H -0.058915 0.597036 0.942496 0.080 Uiso 1 1 calc R U . . .
H45B H -0.150630 0.594513 0.934848 0.080 Uiso 1 1 calc R U . . .
H45C H -0.078824 0.591578 1.018175 0.080 Uiso 1 1 calc R U . . .
C46 C -0.2113(11) 0.8061(7) 0.8707(13) 0.033(4) Uani 1 1 d . . . . .
H46 H -0.220373 0.814412 0.816059 0.039 Uiso 1 1 calc R U . . .
C47 C -0.2050(13) 0.8535(7) 0.9163(14) 0.040(5) Uani 1 1 d . . . . .
H47A H -0.166445 0.876558 0.907978 0.061 Uiso 1 1 calc R U . . .
H47B H -0.186466 0.845240 0.971279 0.061 Uiso 1 1 calc R U . . .
H47C H -0.257995 0.869812 0.899335 0.061 Uiso 1 1 calc R U . . .
C48 C -0.2795(12) 0.7737(8) 0.8737(13) 0.040(5) Uani 1 1 d . . . . .
H48A H -0.329492 0.793390 0.855789 0.061 Uiso 1 1 calc R U . . .
H48B H -0.266675 0.762551 0.926888 0.061 Uiso 1 1 calc R U . . .
H48C H -0.286323 0.744172 0.840314 0.061 Uiso 1 1 calc R U . . .
C49 C -0.3378(11) 0.8294(7) 0.6093(13) 0.033(4) Uani 1 1 d . . . . .
H49 H -0.291586 0.850043 0.644205 0.040 Uiso 1 1 calc R U . . .
C50 C -0.3738(12) 0.8008(7) 0.6573(12) 0.034(4) Uani 1 1 d . . . . .
H50A H -0.337779 0.773008 0.683977 0.051 Uiso 1 1 calc R U . . .
H50B H -0.426317 0.787072 0.623774 0.051 Uiso 1 1 calc R U . . .
H50C H -0.380743 0.823521 0.695381 0.051 Uiso 1 1 calc R U . . .
C51 C -0.3964(13) 0.8636(8) 0.5484(14) 0.046(6) Uani 1 1 d . . . . .
H51A H -0.449201 0.847096 0.525947 0.070 Uiso 1 1 calc R U . . .
H51B H -0.376099 0.870120 0.507805 0.070 Uiso 1 1 calc R U . . .
H51C H -0.401680 0.895555 0.572278 0.070 Uiso 1 1 calc R U . . .
C52 C -0.3329(12) 0.7897(7) 0.3819(11) 0.034(4) Uani 1 1 d . . . . .
H52 H -0.309577 0.754942 0.392012 0.041 Uiso 1 1 calc R U . . .
C53 C -0.4208(12) 0.7874(9) 0.3713(13) 0.046(5) Uani 1 1 d . . . . .
H53A H -0.453705 0.805396 0.323958 0.069 Uiso 1 1 calc R U . . .
H53B H -0.427392 0.803225 0.415625 0.069 Uiso 1 1 calc R U . . .
H53C H -0.438078 0.752075 0.367332 0.069 Uiso 1 1 calc R U . . .
C54 C -0.3193(13) 0.8114(9) 0.3153(13) 0.042(5) Uani 1 1 d . . . . .
H54A H -0.263301 0.822969 0.332143 0.063 Uiso 1 1 calc R U . . .
H54B H -0.355781 0.840045 0.294551 0.063 Uiso 1 1 calc R U . . .
H54C H -0.329710 0.785629 0.275223 0.063 Uiso 1 1 calc R U . . .
C55 C -0.1936(11) 0.9589(7) 0.7296(12) 0.033(4) Uani 1 1 d . . . . .
H55 H -0.200167 0.922781 0.741285 0.040 Uiso 1 1 calc R U . . .
C56 C -0.1879(12) 0.9902(8) 0.7969(13) 0.039(5) Uani 1 1 d . . . . .
H56A H -0.184608 1.025901 0.784843 0.058 Uiso 1 1 calc R U . . .
H56B H -0.139542 0.980663 0.841570 0.058 Uiso 1 1 calc R U . . .
H56C H -0.235775 0.984659 0.808772 0.058 Uiso 1 1 calc R U . . .
C57 C -0.2615(11) 0.9733(7) 0.6561(13) 0.039(5) Uani 1 1 d . . . . .
H57A H -0.257290 0.954227 0.613123 0.058 Uiso 1 1 calc R U . . .
H57B H -0.258722 1.009529 0.646860 0.058 Uiso 1 1 calc R U . . .
H57C H -0.313002 0.965574 0.660252 0.058 Uiso 1 1 calc R U . . .
C58 C 0.0739(12) 1.0086(7) 0.8788(12) 0.034(4) Uani 1 1 d . . . . .
H58 H 0.112371 0.983407 0.872659 0.040 Uiso 1 1 calc R U . . .
C59 C 0.0701(15) 1.0022(10) 0.9579(14) 0.053(6) Uani 1 1 d . . . . .
H59A H 0.064082 0.966321 0.967262 0.079 Uiso 1 1 calc R U . . .
H59B H 0.023863 1.020991 0.959622 0.079 Uiso 1 1 calc R U . . .
H59C H 0.119855 1.015118 0.997729 0.079 Uiso 1 1 calc R U . . .
C60 C 0.0982(14) 1.0600(7) 0.8652(13) 0.042(5) Uani 1 1 d . . . . .
H60A H 0.057988 1.084457 0.866783 0.063 Uiso 1 1 calc R U . . .
H60B H 0.101709 1.061202 0.814415 0.063 Uiso 1 1 calc R U . . .
H60C H 0.150805 1.068204 0.905267 0.063 Uiso 1 1 calc R U . . .
C61 C 0.3034(12) 0.9720(7) 0.5159(11) 0.033(4) Uani 1 1 d . . . . .
H61 H 0.263167 0.947856 0.480681 0.040 Uiso 1 1 calc R U . . .
C62 C 0.2761(17) 1.0256(8) 0.4965(13) 0.053(6) Uani 1 1 d . . . . .
H62A H 0.315896 1.048395 0.532439 0.079 Uiso 1 1 calc R U . . .
H62B H 0.223921 1.030208 0.500909 0.079 Uiso 1 1 calc R U . . .
H62C H 0.270529 1.033077 0.443620 0.079 Uiso 1 1 calc R U . . .
C63 C 0.3880(14) 0.9645(8) 0.5123(14) 0.046(5) Uani 1 1 d . . . . .
H63A H 0.410174 0.931806 0.535153 0.070 Uiso 1 1 calc R U . . .
H63B H 0.424172 0.991571 0.541198 0.070 Uiso 1 1 calc R U . . .
H63C H 0.382634 0.965349 0.458397 0.070 Uiso 1 1 calc R U . . .
C64 C 0.2065(12) 1.0413(7) 0.6933(13) 0.037(4) Uani 1 1 d . . . . .
H64 H 0.181128 1.013521 0.712047 0.044 Uiso 1 1 calc R U . . .
C65 C 0.2635(14) 1.0666(10) 0.7577(15) 0.057(6) Uani 1 1 d . . . . .
H65A H 0.274393 1.100116 0.741964 0.085 Uiso 1 1 calc R U . . .
H65B H 0.313585 1.047035 0.777823 0.085 Uiso 1 1 calc R U . . .
H65C H 0.241797 1.070092 0.798036 0.085 Uiso 1 1 calc R U . . .
C66 C 0.1409(16) 1.0759(9) 0.6412(17) 0.070(8) Uani 1 1 d . . . . .
H66A H 0.096122 1.055567 0.606341 0.105 Uiso 1 1 calc R U . . .
H66B H 0.162675 1.096908 0.610786 0.105 Uiso 1 1 calc R U . . .
H66C H 0.121586 1.097583 0.672708 0.105 Uiso 1 1 calc R U . . .
C67 C 0.4188(16) 0.8711(9) 1.1254(13) 0.054(6) Uani 1 1 d . . . . .
H67 H 0.458819 0.886996 1.107274 0.065 Uiso 1 1 calc R U . . .
C68 C 0.449(2) 0.8200(11) 1.155(2) 0.099(11) Uani 1 1 d . U . . .
H68A H 0.454506 0.799912 1.113034 0.149 Uiso 1 1 calc R U . . .
H68B H 0.502175 0.822897 1.197284 0.149 Uiso 1 1 calc R U . . .
H68C H 0.411502 0.803362 1.173280 0.149 Uiso 1 1 calc R U . . .
C69 C 0.409(2) 0.9040(13) 1.1801(17) 0.102(12) Uani 1 1 d . . . . .
H69A H 0.461406 0.916046 1.215720 0.153 Uiso 1 1 calc R U . . .
H69B H 0.381864 0.885935 1.209198 0.153 Uiso 1 1 calc R U . . .
H69C H 0.375400 0.932829 1.153389 0.153 Uiso 1 1 calc R U . . .
C70 C 0.3604(12) 0.9823(7) 0.9460(11) 0.034(4) Uani 1 1 d . . . . .
H70 H 0.324082 0.972156 0.892490 0.040 Uiso 1 1 calc R U . . .
C71 C 0.4403(15) 0.9945(9) 0.9480(17) 0.060(7) Uani 1 1 d . . . . .
H71A H 0.472592 1.010051 0.997700 0.090 Uiso 1 1 calc R U . . .
H71B H 0.435187 1.018031 0.906120 0.090 Uiso 1 1 calc R U . . .
H71C H 0.466839 0.963493 0.941509 0.090 Uiso 1 1 calc R U . . .
C72 C 0.3232(15) 1.0237(8) 0.9732(15) 0.053(6) Uani 1 1 d . . . . .
H72A H 0.284876 1.041879 0.928712 0.080 Uiso 1 1 calc R U . . .
H72B H 0.365296 1.047013 1.004980 0.080 Uiso 1 1 calc R U . . .
H72C H 0.294847 1.009765 1.004045 0.080 Uiso 1 1 calc R U . . .
C73 C 0.5101(14) 0.9100(10) 0.7061(15) 0.062(7) Uani 1 1 d . . . . .
H73A H 0.528924 0.922610 0.666868 0.093 Uiso 1 1 calc R U . . .
H73B H 0.466205 0.931532 0.707220 0.093 Uiso 1 1 calc R U . . .
H73C H 0.490421 0.875338 0.693366 0.093 Uiso 1 1 calc R U . . .
C74 C 0.5766(11) 0.9109(7) 0.7817(13) 0.035(4) Uani 1 1 d . . . . .
C75 C 0.5621(16) 0.8940(10) 0.8517(16) 0.061(7) Uani 1 1 d . . . . .
H75A H 0.539614 0.922011 0.870987 0.091 Uiso 1 1 calc R U . . .
H75B H 0.613172 0.883168 0.891897 0.091 Uiso 1 1 calc R U . . .
H75C H 0.523986 0.865676 0.837722 0.091 Uiso 1 1 calc R U . . .
C76 C 0.7417(14) 0.5896(11) 0.7516(16) 0.063(7) Uani 1 1 d . . . . .
H76A H 0.710925 0.572026 0.777162 0.094 Uiso 1 1 calc R U . . .
H76B H 0.749519 0.624947 0.768481 0.094 Uiso 1 1 calc R U . . .
H76C H 0.794379 0.573340 0.765262 0.094 Uiso 1 1 calc R U . . .
C77 C 0.6974(13) 0.5876(10) 0.6676(16) 0.052(5) Uani 1 1 d . . . . .
C78 C 0.7230(12) 0.6261(8) 0.6176(14) 0.044(5) Uani 1 1 d . . . . .
H78A H 0.685568 0.623688 0.563523 0.066 Uiso 1 1 calc R U . . .
H78B H 0.777758 0.618301 0.621601 0.066 Uiso 1 1 calc R U . . .
H78C H 0.721660 0.660475 0.636476 0.066 Uiso 1 1 calc R U . . .
C79 C 0.1433(17) 0.8515(11) 0.0843(15) 0.062(7) Uani 1 1 d . . . . .
H79A H 0.192345 0.868921 0.086865 0.093 Uiso 1 1 calc R U . . .
H79B H 0.114866 0.837979 0.032244 0.093 Uiso 1 1 calc R U . . .
H79C H 0.157684 0.823831 0.121794 0.093 Uiso 1 1 calc R U . . .
C80 C 0.0909(15) 0.8872(9) 0.1023(13) 0.048(5) Uani 1 1 d . . . . .
C81 C 0.0010(16) 0.8815(13) 0.0539(13) 0.072(8) Uani 1 1 d . . . . .
H81A H -0.024560 0.862811 0.083388 0.108 Uiso 1 1 calc R U . . .
H81B H -0.006470 0.863155 0.006359 0.108 Uiso 1 1 calc R U . . .
H81C H -0.023674 0.915042 0.040908 0.108 Uiso 1 1 calc R U . . .


_geom_special_details            
; 
 All esds (except the esd in the dihedral angle between two l.s. planes) 
 are estimated using the full covariance matrix.  The cell esds are taken 
 into account individually in the estimation of esds in distances, angles 
 and torsion angles; correlations between esds in cell parameters are only 
 used when they are defined by crystal symmetry.  An approximate (isotropic) 
 treatment of cell esds is used for estimating esds involving l.s. planes. 
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt1 Ag3B 2.65(2) . ?
Pt1 Ag4B 2.67(2) . ?
Pt1 Ag0X 2.72(3) . ?
Pt1 Ag2X 2.74(2) . ?
Pt1 Ag9 2.7494(15) . ?
Pt1 Ag6 2.7504(15) . ?
Pt1 Ag8 2.7550(14) . ?
Pt1 Ag7 2.7561(14) . ?
Pt1 Ag10 2.7587(13) . ?
Pt1 Ag4 2.7593(14) . ?
Pt1 Ag11 2.7598(13) . ?
Pt1 Ag5 2.7601(14) . ?
Ag1 Se7 2.678(2) . ?
Ag1 Ag3 2.8501(19) . ?
Ag1 Ag6 2.8740(18) . ?
Ag1 Ag2 2.9046(18) . ?
Ag1 Ag4 2.9374(18) . ?
Ag1 Ag5 2.9576(17) . ?
Ag1 Ag13 2.9639(18) . ?
Ag1 Ag16 2.9684(18) . ?
Ag2 Se22 2.6850(19) . ?
Ag2 Ag7 2.8395(17) . ?
Ag2 Ag16 2.9073(19) . ?
Ag2 Ag6 2.9176(17) . ?
Ag2 Ag3 2.9272(17) . ?
Ag2 Ag8 2.9393(19) . ?
Ag2 Ag15 2.9438(18) . ?
Ag3 Se20 2.6815(19) . ?
Ag3 Ag4 2.9044(17) . ?
Ag3 Ag9 2.9067(18) . ?
Ag3 Ag8 2.9440(18) . ?
Ag3 Ag14 2.9530(17) . ?
Ag3 Ag15 2.9573(17) . ?
Ag4 Se17 2.687(2) . ?
Ag4 Ag10 2.8556(18) . ?
Ag4 Ag9 2.895(2) . ?
Ag4 Ag5 2.9115(18) . ?
Ag4 Ag14 2.9252(18) . ?
Ag4 Ag13 2.951(2) . ?
Ag5 Se6 2.668(2) . ?
Ag5 Ag6 2.8489(18) . ?
Ag5 Ag10 2.8875(19) . ?
Ag5 Ag11 2.8906(19) . ?
Ag5 Ag13 2.9660(18) . ?
Ag5 Ag20 2.9875(17) . ?
Ag6 Se9 2.665(2) . ?
Ag6 Ag16 2.9077(17) . ?
Ag6 Ag11 2.9256(18) . ?
Ag6 Ag7 2.940(2) . ?
Ag6 Ag17 2.9473(18) . ?
Ag7 Se11 2.667(2) . ?
Ag7 Ag8 2.8997(18) . ?
Ag7 Ag12 2.9078(18) . ?
Ag7 Ag18 2.938(2) . ?
Ag7 Ag11 2.9433(18) . ?
Ag7 Ag17 2.9582(18) . ?
Ag8 Se23 2.662(2) . ?
Ag8 Ag9 2.8344(17) . ?
Ag8 Ag12 2.9073(17) . ?
Ag8 Ag18 2.9204(18) . ?
Ag8 Ag15 2.9369(16) . ?
Ag9 Se16 2.660(2) . ?
Ag9 Ag10 2.9133(18) . ?
Ag9 Ag14 2.9391(17) . ?
Ag9 Ag12 2.9524(17) . ?
Ag9 Ag19 2.9917(17) . ?
Ag10 Se4 2.675(2) . ?
Ag10 Ag11 2.9099(17) . ?
Ag10 Ag12 2.9164(18) . ?
Ag10 Ag20 2.9356(18) . ?
Ag10 Ag19 2.9956(19) . ?
Ag11 Se2 2.675(2) . ?
Ag11 Ag12 2.8378(19) . ?
Ag11 Ag20 2.9595(18) . ?
Ag11 Ag17 2.9617(18) . ?
Ag12 Se13 2.681(2) . ?
Ag12 Ag18 2.9050(18) . ?
Ag12 Ag19 2.9396(18) . ?
Ag1B Ag9B 2.74(3) . ?
Ag1B Ag7B 2.87(3) . ?
Ag1B Ag6B 2.89(4) . ?
Ag1B Se3 2.89(2) . ?
Ag1B Ag8B 2.90(3) . ?
Ag1B Ag5B 2.94(3) . ?
Ag1B Ag20 2.95(2) . ?
Ag1B Ag19 2.96(3) . ?
Ag2B Ag18 2.85(2) . ?
Ag2B Ag1X 2.86(4) . ?
Ag2B Ag7B 2.90(3) . ?
Ag2B Se24 2.90(2) . ?
Ag2B Ag9B 2.94(3) . ?
Ag2B Ag3B 2.95(4) . ?
Ag2B Ag2X 2.99(3) . ?
Ag2B Ag15 3.02(2) . ?
Ag3B Ag4B 2.80(3) . ?
Ag3B Ag0X 2.87(3) . ?
Ag3B Ag1X 2.92(3) . ?
Ag3B Ag16 2.94(3) . ?
Ag3B Ag2X 2.95(4) . ?
Ag3B Se21 2.95(2) . ?
Ag3B Ag15 3.02(2) . ?
Ag4B Ag2X 2.85(4) . ?
Ag4B Se18 2.90(2) . ?
Ag4B Ag14 2.92(2) . ?
Ag4B Ag0X 2.93(3) . ?
Ag4B Ag5B 2.95(3) . ?
Ag4B Ag8B 2.98(3) . ?
Ag4B Ag13 3.00(2) . ?
Ag5B Se5 2.67(2) . ?
Ag5B Ag8B 2.88(3) . ?
Ag5B Ag6B 2.89(3) . ?
Ag5B Ag20 2.90(2) . ?
Ag5B Ag0X 2.99(3) . ?
Ag5B Ag13 3.06(2) . ?
Ag6B Se1 2.71(2) . ?
Ag6B Ag20 2.85(2) . ?
Ag6B Ag0X 2.85(3) . ?
Ag6B Ag9B 3.01(4) . ?
Ag6B Ag1X 3.02(3) . ?
Ag6B Ag17 3.02(2) . ?
Ag7B Ag9B 2.86(3) . ?
Ag7B Ag8B 2.86(3) . ?
Ag7B Ag18 2.87(2) . ?
Ag7B Ag2X 2.88(3) . ?
Ag7B Se14 2.89(3) . ?
Ag7B Ag19 2.89(2) . ?
Ag8B Se15 2.83(2) . ?
Ag8B Ag19 2.83(2) . ?
Ag8B Ag2X 2.91(3) . ?
Ag8B Ag14 3.06(2) . ?
Ag9B Se12 2.79(2) . ?
Ag9B Ag18 2.92(2) . ?
Ag9B Ag1X 2.96(3) . ?
Ag9B Ag17 3.00(2) . ?
Ag0X Se8 2.89(3) . ?
Ag0X Ag1X 2.93(3) . ?
Ag0X Ag13 2.98(2) . ?
Ag0X Ag16 3.03(2) . ?
Ag1X Ag17 2.81(2) . ?
Ag1X Se10 2.99(2) . ?
Ag1X Ag16 2.99(2) . ?
Ag2X Se19 2.94(2) . ?
Ag2X Ag14 2.95(2) . ?
Ag2X Ag15 3.00(2) . ?
Ag13 Se7 2.600(2) . ?
Ag13 Se6 2.612(2) . ?
Ag13 Se17 2.638(2) . ?
Ag14 Se19 2.600(2) . ?
Ag14 Se18 2.608(2) . ?
Ag14 Se15 2.6144(19) . ?
Ag15 Se23 2.624(2) . ?
Ag15 Se22 2.626(2) . ?
Ag15 Se20 2.633(2) . ?
Ag16 Se21 2.618(2) . ?
Ag16 Se8 2.621(2) . ?
Ag16 Se10 2.639(2) . ?
Ag17 Se11 2.643(2) . ?
Ag17 Se2 2.644(2) . ?
Ag17 Se9 2.645(2) . ?
Ag18 Se24 2.613(2) . ?
Ag18 Se14 2.636(2) . ?
Ag18 Se12 2.640(2) . ?
Ag19 Se13 2.605(2) . ?
Ag19 Se4 2.611(2) . ?
Ag19 Se16 2.622(2) . ?
Ag20 Se5 2.605(2) . ?
Ag20 Se1 2.605(2) . ?
Ag20 Se3 2.610(2) . ?
Se1 P1 2.144(5) . ?
Se2 P1 2.182(5) . ?
Se3 P2 2.137(5) . ?
Se4 P2 2.196(5) . ?
Se5 P3 2.152(6) . ?
Se6 P3 2.185(5) . ?
Se7 P4 2.173(5) . ?
Se8 P4 2.153(5) . ?
Se9 P5 2.187(5) . ?
Se10 P5 2.141(5) . ?
Se11 P6 2.180(5) . ?
Se12 P6 2.156(5) . ?
Se13 P7 2.171(5) . ?
Se14 P7 2.145(5) . ?
Se15 P8 2.147(5) . ?
Se16 P8 2.180(5) . ?
Se17 P9 2.183(4) . ?
Se18 P9 2.146(5) . ?
Se19 P10 2.155(5) . ?
Se20 P10 2.173(5) . ?
Se21 P11 2.143(5) . ?
Se22 P11 2.176(5) . ?
Se23 P12 2.174(5) . ?
Se24 P12 2.155(5) . ?
P1 O2 1.590(13) . ?
P1 O1 1.604(16) . ?
P2 O3 1.565(15) . ?
P2 O4 1.582(15) . ?
P3 O5 1.575(13) . ?
P3 O6 1.594(15) . ?
P4 O8 1.594(12) . ?
P4 O7 1.601(13) . ?
P5 O9 1.592(13) . ?
P5 O10 1.602(12) . ?
P6 O11 1.592(13) . ?
P6 O12 1.603(13) . ?
P7 O14 1.569(14) . ?
P7 O13 1.586(13) . ?
P8 O15 1.569(12) . ?
P8 O16 1.572(12) . ?
P9 O17 1.574(13) . ?
P9 O18 1.594(13) . ?
P10 O19 1.575(13) . ?
P10 O20 1.586(13) . ?
P11 O21 1.572(13) . ?
P11 O22 1.595(12) . ?
P12 O24 1.592(12) . ?
P12 O23 1.598(15) . ?
O1 C1 1.45(3) . ?
O2 C4 1.48(2) . ?
O3 C7 1.45(3) . ?
O4 C10 1.48(3) . ?
O5 C13 1.47(2) . ?
O6 C16 1.45(3) . ?
O7 C19 1.46(2) . ?
O8 C22 1.47(2) . ?
O9 C25 1.41(2) . ?
O10 C28 1.48(2) . ?
O11 C31 1.45(2) . ?
O12 C34 1.48(2) . ?
O13 C37 1.47(2) . ?
O14 C40 1.48(2) . ?
O15 C43 1.45(2) . ?
O16 C46 1.49(2) . ?
O17 C49 1.46(2) . ?
O18 C52 1.44(2) . ?
O19 C55 1.47(2) . ?
O20 C58 1.47(2) . ?
O21 C61 1.48(2) . ?
O22 C64 1.44(2) . ?
O23 C67 1.43(3) . ?
O24 C70 1.47(2) . ?
O25 C74 1.19(2) . ?
O26 C77 1.26(3) . ?
O27 C80 1.17(3) . ?
C1 C2 1.51(4) . ?
C1 C3 1.515(14) . ?
C4 C5 1.51(3) . ?
C4 C6 1.51(3) . ?
C7 C8 1.47(3) . ?
C7 C9 1.51(3) . ?
C10 C11 1.45(4) . ?
C10 C12 1.51(3) . ?
C13 C14 1.49(3) . ?
C13 C15 1.52(3) . ?
C16 C18 1.44(4) . ?
C16 C17 1.45(4) . ?
C19 C21 1.53(3) . ?
C19 C20 1.58(3) . ?
C22 C24 1.51(3) . ?
C22 C23 1.51(3) . ?
C25 C26 1.46(3) . ?
C25 C27 1.56(3) . ?
C28 C29 1.46(3) . ?
C28 C30 1.52(3) . ?
C31 C32 1.40(3) . ?
C31 C33 1.58(3) . ?
C34 C35 1.50(3) . ?
C34 C36 1.51(2) . ?
C37 C38 1.43(3) . ?
C37 C39 1.45(3) . ?
C40 C41 1.49(3) . ?
C40 C42 1.56(3) . ?
C43 C44 1.47(3) . ?
C43 C45 1.52(3) . ?
C46 C47 1.50(3) . ?
C46 C48 1.51(3) . ?
C49 C50 1.50(3) . ?
C49 C51 1.52(3) . ?
C52 C54 1.48(3) . ?
C52 C53 1.52(3) . ?
C55 C56 1.48(3) . ?
C55 C57 1.50(3) . ?
C58 C60 1.48(3) . ?
C58 C59 1.52(3) . ?
C61 C62 1.50(3) . ?
C61 C63 1.56(3) . ?
C64 C65 1.41(3) . ?
C64 C66 1.52(3) . ?
C67 C69 1.41(4) . ?
C67 C68 1.48(4) . ?
C70 C71 1.46(3) . ?
C70 C72 1.48(3) . ?
C73 C74 1.46(3) . ?
C74 C75 1.50(3) . ?
C76 C77 1.47(4) . ?
C77 C78 1.57(4) . ?
C79 C80 1.46(3) . ?
C80 C81 1.52(3) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Ag3B Pt1 Ag4B 63.5(7) . . ?
Ag3B Pt1 Ag0X 64.5(7) . . ?
Ag4B Pt1 Ag0X 65.9(7) . . ?
Ag3B Pt1 Ag2X 66.3(7) . . ?
Ag4B Pt1 Ag2X 63.6(7) . . ?
Ag0X Pt1 Ag2X 120.6(7) . . ?
Ag9 Pt1 Ag6 178.80(5) . . ?
Ag9 Pt1 Ag8 61.98(4) . . ?
Ag6 Pt1 Ag8 118.60(4) . . ?
Ag9 Pt1 Ag7 116.54(5) . . ?
Ag6 Pt1 Ag7 64.54(4) . . ?
Ag8 Pt1 Ag7 63.49(4) . . ?
Ag9 Pt1 Ag10 63.86(4) . . ?
Ag6 Pt1 Ag10 116.27(4) . . ?
Ag8 Pt1 Ag10 115.72(5) . . ?
Ag7 Pt1 Ag10 118.25(4) . . ?
Ag9 Pt1 Ag4 63.41(4) . . ?
Ag6 Pt1 Ag4 115.51(5) . . ?
Ag8 Pt1 Ag4 116.11(4) . . ?
Ag7 Pt1 Ag4 179.37(4) . . ?
Ag10 Pt1 Ag4 62.33(4) . . ?
Ag9 Pt1 Ag11 116.69(4) . . ?
Ag6 Pt1 Ag11 64.14(4) . . ?
Ag8 Pt1 Ag11 116.29(5) . . ?
Ag7 Pt1 Ag11 64.50(4) . . ?
Ag10 Pt1 Ag11 63.65(4) . . ?
Ag4 Pt1 Ag11 116.12(4) . . ?
Ag9 Pt1 Ag5 117.17(4) . . ?
Ag6 Pt1 Ag5 62.26(4) . . ?
Ag8 Pt1 Ag5 178.80(5) . . ?
Ag7 Pt1 Ag5 116.73(4) . . ?
Ag10 Pt1 Ag5 63.10(4) . . ?
Ag4 Pt1 Ag5 63.67(4) . . ?
Ag11 Pt1 Ag5 63.16(4) . . ?
Se7 Ag1 Pt1 153.91(7) . . ?
Se7 Ag1 Ag3 108.36(6) . . ?
Pt1 Ag1 Ag3 59.05(4) . . ?
Se7 Ag1 Ag6 141.85(7) . . ?
Pt1 Ag1 Ag6 58.27(4) . . ?
Ag3 Ag1 Ag6 109.45(6) . . ?
Se7 Ag1 Ag2 139.30(6) . . ?
Pt1 Ag1 Ag2 58.39(4) . . ?
Ag3 Ag1 Ag2 61.14(4) . . ?
Ag6 Ag1 Ag2 60.65(4) . . ?
Se7 Ag1 Ag4 96.28(6) . . ?
Pt1 Ag1 Ag4 57.72(4) . . ?
Ag3 Ag1 Ag4 60.22(4) . . ?
Ag6 Ag1 Ag4 106.61(5) . . ?
Ag2 Ag1 Ag4 108.14(6) . . ?
Se7 Ag1 Ag5 113.42(6) . . ?
Pt1 Ag1 Ag5 57.49(4) . . ?
Ag3 Ag1 Ag5 107.87(5) . . ?
Ag6 Ag1 Ag5 58.47(4) . . ?
Ag2 Ag1 Ag5 107.05(5) . . ?
Ag4 Ag1 Ag5 59.19(4) . . ?
Se7 Ag1 Ag13 54.60(5) . . ?
Pt1 Ag1 Ag13 106.93(5) . . ?
Ag3 Ag1 Ag13 113.81(6) . . ?
Ag6 Ag1 Ag13 112.31(5) . . ?
Ag2 Ag1 Ag13 165.29(6) . . ?
Ag4 Ag1 Ag13 60.00(4) . . ?
Ag5 Ag1 Ag13 60.12(4) . . ?
Se7 Ag1 Ag16 99.51(6) . . ?
Pt1 Ag1 Ag16 106.53(5) . . ?
Ag3 Ag1 Ag16 114.63(5) . . ?
Ag6 Ag1 Ag16 59.67(4) . . ?
Ag2 Ag1 Ag16 59.33(4) . . ?
Ag4 Ag1 Ag16 164.19(6) . . ?
Ag5 Ag1 Ag16 112.93(5) . . ?
Ag13 Ag1 Ag16 130.35(6) . . ?
Se22 Ag2 Pt1 151.19(7) . . ?
Se22 Ag2 Ag7 104.46(6) . . ?
Pt1 Ag2 Ag7 58.83(4) . . ?
Se22 Ag2 Ag1 146.13(6) . . ?
Pt1 Ag2 Ag1 58.41(4) . . ?
Ag7 Ag2 Ag1 108.96(5) . . ?
Se22 Ag2 Ag16 99.97(6) . . ?
Pt1 Ag2 Ag16 108.24(5) . . ?
Ag7 Ag2 Ag16 113.90(6) . . ?
Ag1 Ag2 Ag16 61.43(5) . . ?
Se22 Ag2 Ag6 138.70(7) . . ?
Pt1 Ag2 Ag6 57.76(4) . . ?
Ag7 Ag2 Ag6 61.40(4) . . ?
Ag1 Ag2 Ag6 59.16(4) . . ?
Ag16 Ag2 Ag6 59.89(4) . . ?
Se22 Ag2 Ag3 115.10(6) . . ?
Pt1 Ag2 Ag3 58.12(4) . . ?
Ag7 Ag2 Ag3 108.77(5) . . ?
Ag1 Ag2 Ag3 58.51(4) . . ?
Ag16 Ag2 Ag3 114.15(5) . . ?
Ag6 Ag2 Ag3 106.17(5) . . ?
Se22 Ag2 Ag8 94.09(6) . . ?
Pt1 Ag2 Ag8 57.60(4) . . ?
Ag7 Ag2 Ag8 60.21(4) . . ?
Ag1 Ag2 Ag8 107.00(5) . . ?
Ag16 Ag2 Ag8 165.84(6) . . ?
Ag6 Ag2 Ag8 107.85(5) . . ?
Ag3 Ag2 Ag8 60.24(4) . . ?
Se22 Ag2 Ag15 55.40(5) . . ?
Pt1 Ag2 Ag15 106.96(5) . . ?
Ag7 Ag2 Ag15 113.61(6) . . ?
Ag1 Ag2 Ag15 113.34(5) . . ?
Ag16 Ag2 Ag15 130.64(6) . . ?
Ag6 Ag2 Ag15 164.66(6) . . ?
Ag3 Ag2 Ag15 60.49(4) . . ?
Ag8 Ag2 Ag15 59.90(4) . . ?
Se20 Ag3 Pt1 154.83(6) . . ?
Se20 Ag3 Ag1 109.34(6) . . ?
Pt1 Ag3 Ag1 59.07(4) . . ?
Se20 Ag3 Ag4 139.66(6) . . ?
Pt1 Ag3 Ag4 58.12(4) . . ?
Ag1 Ag3 Ag4 61.38(4) . . ?
Se20 Ag3 Ag9 141.31(7) . . ?
Pt1 Ag3 Ag9 57.86(4) . . ?
Ag1 Ag3 Ag9 108.93(5) . . ?
Ag4 Ag3 Ag9 59.76(4) . . ?
Se20 Ag3 Ag2 96.76(6) . . ?
Pt1 Ag3 Ag2 58.12(4) . . ?
Ag1 Ag3 Ag2 60.35(4) . . ?
Ag4 Ag3 Ag2 108.42(5) . . ?
Ag9 Ag3 Ag2 106.80(5) . . ?
Se20 Ag3 Ag8 113.59(6) . . ?
Pt1 Ag3 Ag8 57.54(4) . . ?
Ag1 Ag3 Ag8 108.34(5) . . ?
Ag4 Ag3 Ag8 106.28(5) . . ?
Ag9 Ag3 Ag8 57.95(4) . . ?
Ag2 Ag3 Ag8 60.08(4) . . ?
Se20 Ag3 Ag14 97.98(5) . . ?
Pt1 Ag3 Ag14 107.17(5) . . ?
Ag1 Ag3 Ag14 115.04(5) . . ?
Ag4 Ag3 Ag14 59.91(4) . . ?
Ag9 Ag3 Ag14 60.20(4) . . ?
Ag2 Ag3 Ag14 165.23(6) . . ?
Ag8 Ag3 Ag14 112.37(6) . . ?
Se20 Ag3 Ag15 55.42(5) . . ?
Pt1 Ag3 Ag15 106.59(5) . . ?
Ag1 Ag3 Ag15 114.57(6) . . ?
Ag4 Ag3 Ag15 164.53(6) . . ?
Ag9 Ag3 Ag15 111.63(6) . . ?
Ag2 Ag3 Ag15 60.03(4) . . ?
Ag8 Ag3 Ag15 59.69(4) . . ?
Ag14 Ag3 Ag15 129.26(6) . . ?
Se17 Ag4 Pt1 155.29(6) . . ?
Se17 Ag4 Ag10 108.80(6) . . ?
Pt1 Ag4 Ag10 58.82(4) . . ?
Se17 Ag4 Ag9 138.20(7) . . ?
Pt1 Ag4 Ag9 58.13(4) . . ?
Ag10 Ag4 Ag9 60.87(4) . . ?
Se17 Ag4 Ag3 141.36(6) . . ?
Pt1 Ag4 Ag3 58.52(4) . . ?
Ag10 Ag4 Ag3 109.15(6) . . ?
Ag9 Ag4 Ag3 60.16(4) . . ?
Se17 Ag4 Ag5 97.24(6) . . ?
Pt1 Ag4 Ag5 58.17(4) . . ?
Ag10 Ag4 Ag5 60.08(4) . . ?
Ag9 Ag4 Ag5 108.14(5) . . ?
Ag3 Ag4 Ag5 107.67(5) . . ?
Se17 Ag4 Ag14 96.31(6) . . ?
Pt1 Ag4 Ag14 108.28(5) . . ?
Ag10 Ag4 Ag14 114.87(6) . . ?
Ag9 Ag4 Ag14 60.66(4) . . ?
Ag3 Ag4 Ag14 60.87(4) . . ?
Ag5 Ag4 Ag14 166.45(6) . . ?
Se17 Ag4 Ag1 114.48(7) . . ?
Pt1 Ag4 Ag1 58.13(4) . . ?
Ag10 Ag4 Ag1 108.76(5) . . ?
Ag9 Ag4 Ag1 106.88(5) . . ?
Ag3 Ag4 Ag1 58.40(4) . . ?
Ag5 Ag4 Ag1 60.75(4) . . ?
Ag14 Ag4 Ag1 113.24(5) . . ?
Se17 Ag4 Ag13 55.56(5) . . ?
Pt1 Ag4 Ag13 107.63(5) . . ?
Ag10 Ag4 Ag13 114.78(5) . . ?
Ag9 Ag4 Ag13 165.68(6) . . ?
Ag3 Ag4 Ag13 112.59(5) . . ?
Ag5 Ag4 Ag13 60.78(5) . . ?
Ag14 Ag4 Ag13 128.67(6) . . ?
Ag1 Ag4 Ag13 60.44(5) . . ?
Se6 Ag5 Pt1 157.22(6) . . ?
Se6 Ag5 Ag6 112.00(7) . . ?
Pt1 Ag5 Ag6 58.70(4) . . ?
Se6 Ag5 Ag10 138.12(7) . . ?
Pt1 Ag5 Ag10 58.43(4) . . ?
Ag6 Ag5 Ag10 109.29(6) . . ?
Se6 Ag5 Ag11 138.86(7) . . ?
Pt1 Ag5 Ag11 58.42(4) . . ?
Ag6 Ag5 Ag11 61.29(4) . . ?
Ag10 Ag5 Ag11 60.48(4) . . ?
Se6 Ag5 Ag4 112.57(6) . . ?
Pt1 Ag5 Ag4 58.15(4) . . ?
Ag6 Ag5 Ag4 107.99(5) . . ?
Ag10 Ag5 Ag4 59.00(4) . . ?
Ag11 Ag5 Ag4 107.65(6) . . ?
Se6 Ag5 Ag1 99.35(6) . . ?
Pt1 Ag5 Ag1 57.87(4) . . ?
Ag6 Ag5 Ag1 59.30(4) . . ?
Ag10 Ag5 Ag1 107.35(5) . . ?
Ag11 Ag5 Ag1 107.98(5) . . ?
Ag4 Ag5 Ag1 60.06(4) . . ?
Se6 Ag5 Ag13 54.93(5) . . ?
Pt1 Ag5 Ag13 107.19(5) . . ?
Ag6 Ag5 Ag13 112.99(5) . . ?
Ag10 Ag5 Ag13 113.36(6) . . ?
Ag11 Ag5 Ag13 165.60(6) . . ?
Ag4 Ag5 Ag13 60.27(5) . . ?
Ag1 Ag5 Ag13 60.05(4) . . ?
Se6 Ag5 Ag20 95.22(6) . . ?
Pt1 Ag5 Ag20 107.55(5) . . ?
Ag6 Ag5 Ag20 115.85(5) . . ?
Ag10 Ag5 Ag20 59.93(4) . . ?
Ag11 Ag5 Ag20 60.43(4) . . ?
Ag4 Ag5 Ag20 112.92(6) . . ?
Ag1 Ag5 Ag20 165.38(6) . . ?
Ag13 Ag5 Ag20 129.72(6) . . ?
Se9 Ag6 Pt1 153.12(6) . . ?
Se9 Ag6 Ag5 105.82(6) . . ?
Pt1 Ag6 Ag5 59.03(4) . . ?
Se9 Ag6 Ag1 137.33(7) . . ?
Pt1 Ag6 Ag1 59.00(4) . . ?
Ag5 Ag6 Ag1 62.23(4) . . ?
Se9 Ag6 Ag16 97.91(6) . . ?
Pt1 Ag6 Ag16 108.80(5) . . ?
Ag5 Ag6 Ag16 118.20(6) . . ?
Ag1 Ag6 Ag16 61.78(4) . . ?
Se9 Ag6 Ag2 144.02(7) . . ?
Pt1 Ag6 Ag2 58.45(4) . . ?
Ag5 Ag6 Ag2 109.66(5) . . ?
Ag1 Ag6 Ag2 60.19(4) . . ?
Ag16 Ag6 Ag2 59.88(4) . . ?
Se9 Ag6 Ag11 95.41(6) . . ?
Pt1 Ag6 Ag11 58.09(4) . . ?
Ag5 Ag6 Ag11 60.06(4) . . ?
Ag1 Ag6 Ag11 109.31(5) . . ?
Ag16 Ag6 Ag11 166.40(6) . . ?
Ag2 Ag6 Ag11 107.15(6) . . ?
Se9 Ag6 Ag7 115.43(6) . . ?
Pt1 Ag6 Ag7 57.82(4) . . ?
Ag5 Ag6 Ag7 108.44(6) . . ?
Ag1 Ag6 Ag7 107.05(5) . . ?
Ag16 Ag6 Ag7 110.92(5) . . ?
Ag2 Ag6 Ag7 57.99(4) . . ?
Ag11 Ag6 Ag7 60.24(4) . . ?
Se9 Ag6 Ag17 55.98(5) . . ?
Pt1 Ag6 Ag17 107.40(5) . . ?
Ag5 Ag6 Ag17 114.44(5) . . ?
Ag1 Ag6 Ag17 166.19(7) . . ?
Ag16 Ag6 Ag17 126.03(6) . . ?
Ag2 Ag6 Ag17 111.94(6) . . ?
Ag11 Ag6 Ag17 60.57(4) . . ?
Ag7 Ag6 Ag17 60.33(5) . . ?
Se11 Ag7 Pt1 154.21(7) . . ?
Se11 Ag7 Ag2 107.29(6) . . ?
Pt1 Ag7 Ag2 59.35(4) . . ?
Se11 Ag7 Ag8 138.47(6) . . ?
Pt1 Ag7 Ag8 58.24(4) . . ?
Ag2 Ag7 Ag8 61.60(4) . . ?
Se11 Ag7 Ag12 142.54(7) . . ?
Pt1 Ag7 Ag12 58.27(4) . . ?
Ag2 Ag7 Ag12 109.64(5) . . ?
Ag8 Ag7 Ag12 60.08(4) . . ?
Se11 Ag7 Ag18 98.61(6) . . ?
Pt1 Ag7 Ag18 107.06(5) . . ?
Ag2 Ag7 Ag18 115.50(5) . . ?
Ag8 Ag7 Ag18 60.03(4) . . ?
Ag12 Ag7 Ag18 59.59(4) . . ?
Se11 Ag7 Ag6 96.79(6) . . ?
Pt1 Ag7 Ag6 57.64(4) . . ?
Ag2 Ag7 Ag6 60.61(4) . . ?
Ag8 Ag7 Ag6 108.32(5) . . ?
Ag12 Ag7 Ag6 106.43(5) . . ?
Ag18 Ag7 Ag6 164.52(6) . . ?
Se11 Ag7 Ag11 114.65(6) . . ?
Pt1 Ag7 Ag11 57.81(4) . . ?
Ag2 Ag7 Ag11 108.78(6) . . ?
Ag8 Ag7 Ag11 106.59(5) . . ?
Ag12 Ag7 Ag11 58.02(4) . . ?
Ag18 Ag7 Ag11 111.80(5) . . ?
Ag6 Ag7 Ag11 59.64(4) . . ?
Se11 Ag7 Ag17 55.75(5) . . ?
Pt1 Ag7 Ag17 106.95(5) . . ?
Ag2 Ag7 Ag17 113.93(6) . . ?
Ag8 Ag7 Ag17 165.10(6) . . ?
Ag12 Ag7 Ag17 112.29(5) . . ?
Ag18 Ag7 Ag17 129.30(6) . . ?
Ag6 Ag7 Ag17 59.96(4) . . ?
Ag11 Ag7 Ag17 60.25(4) . . ?
Se23 Ag8 Pt1 153.26(7) . . ?
Se23 Ag8 Ag9 106.18(6) . . ?
Pt1 Ag8 Ag9 58.91(4) . . ?
Se23 Ag8 Ag7 143.88(7) . . ?
Pt1 Ag8 Ag7 58.27(4) . . ?
Ag9 Ag8 Ag7 109.49(5) . . ?
Se23 Ag8 Ag12 138.06(7) . . ?
Pt1 Ag8 Ag12 58.29(4) . . ?
Ag9 Ag8 Ag12 61.87(4) . . ?
Ag7 Ag8 Ag12 60.10(4) . . ?
Se23 Ag8 Ag18 98.87(6) . . ?
Pt1 Ag8 Ag18 107.58(5) . . ?
Ag9 Ag8 Ag18 115.27(5) . . ?
Ag7 Ag8 Ag18 60.64(5) . . ?
Ag12 Ag8 Ag18 59.80(4) . . ?
Se23 Ag8 Ag15 55.62(5) . . ?
Pt1 Ag8 Ag15 107.59(5) . . ?
Ag9 Ag8 Ag15 114.38(5) . . ?
Ag7 Ag8 Ag15 112.04(6) . . ?
Ag12 Ag8 Ag15 165.71(6) . . ?
Ag18 Ag8 Ag15 128.88(5) . . ?
Se23 Ag8 Ag2 114.84(6) . . ?
Pt1 Ag8 Ag2 58.13(4) . . ?
Ag9 Ag8 Ag2 108.41(6) . . ?
Ag7 Ag8 Ag2 58.19(4) . . ?
Ag12 Ag8 Ag2 106.93(5) . . ?
Ag18 Ag8 Ag2 113.01(5) . . ?
Ag15 Ag8 Ag2 60.13(4) . . ?
Se23 Ag8 Ag3 95.55(6) . . ?
Pt1 Ag8 Ag3 58.08(4) . . ?
Ag9 Ag8 Ag3 60.37(4) . . ?
Ag7 Ag8 Ag3 106.70(6) . . ?
Ag12 Ag8 Ag3 108.85(5) . . ?
Ag18 Ag8 Ag3 165.58(6) . . ?
Ag15 Ag8 Ag3 60.38(4) . . ?
Ag2 Ag8 Ag3 59.68(4) . . ?
Se16 Ag9 Pt1 155.90(6) . . ?
Se16 Ag9 Ag8 109.52(6) . . ?
Pt1 Ag9 Ag8 59.10(4) . . ?
Se16 Ag9 Ag4 140.33(7) . . ?
Pt1 Ag9 Ag4 58.46(4) . . ?
Ag8 Ag9 Ag4 109.51(6) . . ?
Se16 Ag9 Ag3 138.29(6) . . ?
Pt1 Ag9 Ag3 58.60(4) . . ?
Ag8 Ag9 Ag3 61.68(4) . . ?
Ag4 Ag9 Ag3 60.08(4) . . ?
Se16 Ag9 Ag10 113.57(6) . . ?
Pt1 Ag9 Ag10 58.22(4) . . ?
Ag8 Ag9 Ag10 108.63(5) . . ?
Ag4 Ag9 Ag10 58.90(4) . . ?
Ag3 Ag9 Ag10 107.50(6) . . ?
Se16 Ag9 Ag14 95.93(6) . . ?
Pt1 Ag9 Ag14 108.15(5) . . ?
Ag8 Ag9 Ag14 116.11(5) . . ?
Ag4 Ag9 Ag14 60.18(4) . . ?
Ag3 Ag9 Ag14 60.68(4) . . ?
Ag10 Ag9 Ag14 112.71(6) . . ?
Se16 Ag9 Ag12 98.18(6) . . ?
Pt1 Ag9 Ag12 57.79(4) . . ?
Ag8 Ag9 Ag12 60.28(4) . . ?
Ag4 Ag9 Ag12 106.98(5) . . ?
Ag3 Ag9 Ag12 108.63(5) . . ?
Ag10 Ag9 Ag12 59.63(4) . . ?
Ag14 Ag9 Ag12 165.79(6) . . ?
Se16 Ag9 Ag19 54.90(5) . . ?
Pt1 Ag9 Ag19 107.29(5) . . ?
Ag8 Ag9 Ag19 112.44(5) . . ?
Ag4 Ag9 Ag19 114.25(5) . . ?
Ag3 Ag9 Ag19 165.89(6) . . ?
Ag10 Ag9 Ag19 60.95(4) . . ?
Ag14 Ag9 Ag19 129.67(6) . . ?
Ag12 Ag9 Ag19 59.28(4) . . ?
Se4 Ag10 Pt1 155.58(7) . . ?
Se4 Ag10 Ag4 111.49(6) . . ?
Pt1 Ag10 Ag4 58.85(4) . . ?
Se4 Ag10 Ag5 140.08(7) . . ?
Pt1 Ag10 Ag5 58.47(4) . . ?
Ag4 Ag10 Ag5 60.92(4) . . ?
Se4 Ag10 Ag11 139.40(7) . . ?
Pt1 Ag10 Ag11 58.20(4) . . ?
Ag4 Ag10 Ag11 108.65(5) . . ?
Ag5 Ag10 Ag11 59.81(4) . . ?
Se4 Ag10 Ag9 97.67(6) . . ?
Pt1 Ag10 Ag9 57.91(4) . . ?
Ag4 Ag10 Ag9 60.23(4) . . ?
Ag5 Ag10 Ag9 108.30(5) . . ?
Ag11 Ag10 Ag9 107.29(5) . . ?
Se4 Ag10 Ag12 112.10(7) . . ?
Pt1 Ag10 Ag12 58.14(4) . . ?
Ag4 Ag10 Ag12 109.03(5) . . ?
Ag5 Ag10 Ag12 106.98(5) . . ?
Ag11 Ag10 Ag12 58.30(4) . . ?
Ag9 Ag10 Ag12 60.85(4) . . ?
Se4 Ag10 Ag20 95.35(6) . . ?
Pt1 Ag10 Ag20 109.05(5) . . ?
Ag4 Ag10 Ag20 116.21(6) . . ?
Ag5 Ag10 Ag20 61.73(4) . . ?
Ag11 Ag10 Ag20 60.83(4) . . ?
Ag9 Ag10 Ag20 166.86(6) . . ?
Ag12 Ag10 Ag20 112.16(5) . . ?
Se4 Ag10 Ag19 54.47(5) . . ?
Pt1 Ag10 Ag19 106.94(5) . . ?
Ag4 Ag10 Ag19 115.32(5) . . ?
Ag5 Ag10 Ag19 165.22(6) . . ?
Ag11 Ag10 Ag19 111.92(5) . . ?
Ag9 Ag10 Ag19 60.82(4) . . ?
Ag12 Ag10 Ag19 59.62(4) . . ?
Ag20 Ag10 Ag19 127.07(5) . . ?
Se2 Ag11 Pt1 156.66(7) . . ?
Se2 Ag11 Ag12 111.08(7) . . ?
Pt1 Ag11 Ag12 59.08(4) . . ?
Se2 Ag11 Ag5 139.14(7) . . ?
Pt1 Ag11 Ag5 58.42(4) . . ?
Ag12 Ag11 Ag5 109.04(5) . . ?
Se2 Ag11 Ag10 139.07(7) . . ?
Pt1 Ag11 Ag10 58.16(4) . . ?
Ag12 Ag11 Ag10 60.97(4) . . ?
Ag5 Ag11 Ag10 59.71(4) . . ?
Se2 Ag11 Ag6 113.49(6) . . ?
Pt1 Ag11 Ag6 57.77(4) . . ?
Ag12 Ag11 Ag6 108.70(5) . . ?
Ag5 Ag11 Ag6 58.65(4) . . ?
Ag10 Ag11 Ag6 106.60(5) . . ?
Se2 Ag11 Ag7 98.97(6) . . ?
Pt1 Ag11 Ag7 57.69(4) . . ?
Ag12 Ag11 Ag7 60.36(4) . . ?
Ag5 Ag11 Ag7 107.22(5) . . ?
Ag10 Ag11 Ag7 107.93(5) . . ?
Ag6 Ag11 Ag7 60.12(4) . . ?
Se2 Ag11 Ag20 94.99(6) . . ?
Pt1 Ag11 Ag20 108.34(5) . . ?
Ag12 Ag11 Ag20 113.77(6) . . ?
Ag5 Ag11 Ag20 61.40(4) . . ?
Ag10 Ag11 Ag20 60.01(4) . . ?
Ag6 Ag11 Ag20 114.37(6) . . ?
Ag7 Ag11 Ag20 166.03(6) . . ?
Se2 Ag11 Ag17 55.67(5) . . ?
Pt1 Ag11 Ag17 106.75(5) . . ?
Ag12 Ag11 Ag17 114.26(6) . . ?
Ag5 Ag11 Ag17 112.76(6) . . ?
Ag10 Ag11 Ag17 164.84(6) . . ?
Ag6 Ag11 Ag17 60.08(4) . . ?
Ag7 Ag11 Ag17 60.13(4) . . ?
Ag20 Ag11 Ag17 130.21(6) . . ?
Se13 Ag12 Pt1 155.51(6) . . ?
Se13 Ag12 Ag11 108.93(6) . . ?
Pt1 Ag12 Ag11 59.05(4) . . ?
Se13 Ag12 Ag18 96.59(6) . . ?
Pt1 Ag12 Ag18 107.85(5) . . ?
Ag11 Ag12 Ag18 115.99(6) . . ?
Se13 Ag12 Ag8 141.25(7) . . ?
Pt1 Ag12 Ag8 58.10(4) . . ?
Ag11 Ag12 Ag8 109.24(5) . . ?
Ag18 Ag12 Ag8 60.32(4) . . ?
Se13 Ag12 Ag7 138.60(6) . . ?
Pt1 Ag12 Ag7 58.11(4) . . ?
Ag11 Ag12 Ag7 61.62(4) . . ?
Ag18 Ag12 Ag7 60.72(5) . . ?
Ag8 Ag12 Ag7 59.82(4) . . ?
Se13 Ag12 Ag10 97.57(6) . . ?
Pt1 Ag12 Ag10 58.07(4) . . ?
Ag11 Ag12 Ag10 60.74(4) . . ?
Ag18 Ag12 Ag10 165.70(6) . . ?
Ag8 Ag12 Ag10 106.58(5) . . ?
Ag7 Ag12 Ag10 108.72(6) . . ?
Se13 Ag12 Ag19 54.99(5) . . ?
Pt1 Ag12 Ag19 108.44(5) . . ?
Ag11 Ag12 Ag19 115.78(5) . . ?
Ag18 Ag12 Ag19 126.75(6) . . ?
Ag8 Ag12 Ag19 111.86(5) . . ?
Ag7 Ag12 Ag19 166.23(6) . . ?
Ag10 Ag12 Ag19 61.53(4) . . ?
Se13 Ag12 Ag9 114.82(6) . . ?
Pt1 Ag12 Ag9 57.42(4) . . ?
Ag11 Ag12 Ag9 108.16(6) . . ?
Ag18 Ag12 Ag9 112.17(5) . . ?
Ag8 Ag12 Ag9 57.85(4) . . ?
Ag7 Ag12 Ag9 106.08(5) . . ?
Ag10 Ag12 Ag9 59.52(4) . . ?
Ag19 Ag12 Ag9 61.03(4) . . ?
Ag9B Ag1B Pt1 61.3(7) . . ?
Ag9B Ag1B Ag7B 61.3(8) . . ?
Pt1 Ag1B Ag7B 58.7(7) . . ?
Ag9B Ag1B Ag6B 64.6(9) . . ?
Pt1 Ag1B Ag6B 59.8(7) . . ?
Ag7B Ag1B Ag6B 111.3(10) . . ?
Ag9B Ag1B Se3 116.9(9) . . ?
Pt1 Ag1B Se3 158.4(10) . . ?
Ag7B Ag1B Se3 141.6(11) . . ?
Ag6B Ag1B Se3 99.2(9) . . ?
Ag9B Ag1B Ag8B 110.4(10) . . ?
Pt1 Ag1B Ag8B 58.6(6) . . ?
Ag7B Ag1B Ag8B 59.5(8) . . ?
Ag6B Ag1B Ag8B 108.2(10) . . ?
Se3 Ag1B Ag8B 132.0(10) . . ?
Ag9B Ag1B Ag5B 111.7(10) . . ?
Pt1 Ag1B Ag5B 58.4(6) . . ?
Ag7B Ag1B Ag5B 107.3(10) . . ?
Ag6B Ag1B Ag5B 59.4(8) . . ?
Se3 Ag1B Ag5B 108.0(9) . . ?
Ag8B Ag1B Ag5B 59.0(8) . . ?
Ag9B Ag1B Ag20 116.5(10) . . ?
Pt1 Ag1B Ag20 107.0(8) . . ?
Ag7B Ag1B Ag20 165.3(11) . . ?
Ag6B Ag1B Ag20 58.3(7) . . ?
Se3 Ag1B Ag20 53.0(4) . . ?
Ag8B Ag1B Ag20 111.7(9) . . ?
Ag5B Ag1B Ag20 59.0(7) . . ?
Ag9B Ag1B Ag19 114.3(10) . . ?
Pt1 Ag1B Ag19 106.4(7) . . ?
Ag7B Ag1B Ag19 59.6(7) . . ?
Ag6B Ag1B Ag19 165.5(10) . . ?
Se3 Ag1B Ag19 94.0(7) . . ?
Ag8B Ag1B Ag19 57.8(7) . . ?
Ag5B Ag1B Ag19 110.7(9) . . ?
Ag20 Ag1B Ag19 127.9(8) . . ?
Pt1 Ag2B Ag18 109.5(7) . . ?
Pt1 Ag2B Ag1X 58.9(7) . . ?
Ag18 Ag2B Ag1X 115.6(9) . . ?
Pt1 Ag2B Ag7B 58.9(7) . . ?
Ag18 Ag2B Ag7B 60.1(7) . . ?
Ag1X Ag2B Ag7B 108.3(10) . . ?
Pt1 Ag2B Se24 163.3(9) . . ?
Ag18 Ag2B Se24 54.1(5) . . ?
Ag1X Ag2B Se24 122.1(9) . . ?
Ag7B Ag2B Se24 108.5(9) . . ?
Pt1 Ag2B Ag9B 59.5(6) . . ?
Ag18 Ag2B Ag9B 60.7(7) . . ?
Ag1X Ag2B Ag9B 61.4(8) . . ?
Ag7B Ag2B Ag9B 58.7(8) . . ?
Se24 Ag2B Ag9B 105.2(9) . . ?
Pt1 Ag2B Ag3B 55.2(6) . . ?
Ag18 Ag2B Ag3B 164.6(10) . . ?
Ag1X Ag2B Ag3B 60.3(8) . . ?
Ag7B Ag2B Ag3B 106.0(10) . . ?
Se24 Ag2B Ag3B 141.3(9) . . ?
Ag9B Ag2B Ag3B 107.4(10) . . ?
Pt1 Ag2B Ag2X 56.8(6) . . ?
Ag18 Ag2B Ag2X 112.1(9) . . ?
Ag1X Ag2B Ag2X 108.6(10) . . ?
Ag7B Ag2B Ag2X 58.5(8) . . ?
Se24 Ag2B Ag2X 128.5(10) . . ?
Ag9B Ag2B Ag2X 106.0(9) . . ?
Ag3B Ag2B Ag2X 59.6(8) . . ?
Pt1 Ag2B Ag15 105.1(8) . . ?
Ag18 Ag2B Ag15 128.5(9) . . ?
Ag1X Ag2B Ag15 114.7(9) . . ?
Ag7B Ag2B Ag15 112.6(9) . . ?
Se24 Ag2B Ag15 89.6(6) . . ?
Ag9B Ag2B Ag15 164.4(10) . . ?
Ag3B Ag2B Ag15 60.8(6) . . ?
Ag2X Ag2B Ag15 59.9(6) . . ?
Pt1 Ag3B Ag4B 58.6(7) . . ?
Pt1 Ag3B Ag0X 58.9(7) . . ?
Ag4B Ag3B Ag0X 62.3(8) . . ?
Pt1 Ag3B Ag1X 59.4(6) . . ?
Ag4B Ag3B Ag1X 110.4(10) . . ?
Ag0X Ag3B Ag1X 60.9(8) . . ?
Pt1 Ag3B Ag16 110.6(8) . . ?
Ag4B Ag3B Ag16 118.5(10) . . ?
Ag0X Ag3B Ag16 62.8(7) . . ?
Ag1X Ag3B Ag16 61.5(7) . . ?
Pt1 Ag3B Ag2B 58.9(7) . . ?
Ag4B Ag3B Ag2B 108.7(10) . . ?
Ag0X Ag3B Ag2B 107.9(10) . . ?
Ag1X Ag3B Ag2B 58.4(8) . . ?
Ag16 Ag3B Ag2B 112.5(9) . . ?
Pt1 Ag3B Ag2X 58.3(6) . . ?
Ag4B Ag3B Ag2X 59.4(8) . . ?
Ag0X Ag3B Ag2X 109.3(10) . . ?
Ag1X Ag3B Ag2X 108.1(10) . . ?
Ag16 Ag3B Ag2X 168.7(9) . . ?
Ag2B Ag3B Ag2X 60.9(8) . . ?
Pt1 Ag3B Se21 162.9(10) . . ?
Ag4B Ag3B Se21 122.7(10) . . ?
Ag0X Ag3B Se21 105.4(10) . . ?
Ag1X Ag3B Se21 108.4(9) . . ?
Ag16 Ag3B Se21 52.8(4) . . ?
Ag2B Ag3B Se21 127.3(9) . . ?
Ag2X Ag3B Se21 138.4(9) . . ?
Pt1 Ag3B Ag15 108.1(8) . . ?
Ag4B Ag3B Ag15 113.2(9) . . ?
Ag0X Ag3B Ag15 166.9(10) . . ?
Ag1X Ag3B Ag15 113.0(9) . . ?
Ag16 Ag3B Ag15 126.2(8) . . ?
Ag2B Ag3B Ag15 60.8(7) . . ?
Ag2X Ag3B Ag15 60.3(7) . . ?
Se21 Ag3B Ag15 87.4(6) . . ?
Pt1 Ag4B Ag3B 57.9(7) . . ?
Pt1 Ag4B Ag2X 59.5(7) . . ?
Ag3B Ag4B Ag2X 63.0(9) . . ?
Pt1 Ag4B Se18 161.2(10) . . ?
Ag3B Ag4B Se18 117.0(9) . . ?
Ag2X Ag4B Se18 101.8(9) . . ?
Pt1 Ag4B Ag14 110.9(9) . . ?
Ag3B Ag4B Ag14 117.5(10) . . ?
Ag2X Ag4B Ag14 61.4(7) . . ?
Se18 Ag4B Ag14 53.3(4) . . ?
Pt1 Ag4B Ag0X 57.9(7) . . ?
Ag3B Ag4B Ag0X 60.0(8) . . ?
Ag2X Ag4B Ag0X 110.2(10) . . ?
Se18 Ag4B Ag0X 138.2(11) . . ?
Ag14 Ag4B Ag0X 168.6(11) . . ?
Pt1 Ag4B Ag5B 59.7(7) . . ?
Ag3B Ag4B Ag5B 109.4(10) . . ?
Ag2X Ag4B Ag5B 108.0(10) . . ?
Se18 Ag4B Ag5B 132.4(10) . . ?
Ag14 Ag4B Ag5B 112.6(9) . . ?
Ag0X Ag4B Ag5B 61.1(8) . . ?
Pt1 Ag4B Ag8B 59.2(7) . . ?
Ag3B Ag4B Ag8B 109.4(10) . . ?
Ag2X Ag4B Ag8B 59.9(8) . . ?
Se18 Ag4B Ag8B 112.0(9) . . ?
Ag14 Ag4B Ag8B 62.3(7) . . ?
Ag0X Ag4B Ag8B 107.2(10) . . ?
Ag5B Ag4B Ag8B 58.0(8) . . ?
Pt1 Ag4B Ag13 108.7(8) . . ?
Ag3B Ag4B Ag13 113.1(10) . . ?
Ag2X Ag4B Ag13 168.1(10) . . ?
Se18 Ag4B Ag13 90.0(7) . . ?
Ag14 Ag4B Ag13 126.8(8) . . ?
Ag0X Ag4B Ag13 60.3(7) . . ?
Ag5B Ag4B Ag13 61.8(7) . . ?
Ag8B Ag4B Ag13 114.3(9) . . ?
Se5 Ag5B Pt1 160.4(10) . . ?
Se5 Ag5B Ag8B 113.7(10) . . ?
Pt1 Ag5B Ag8B 59.1(7) . . ?
Se5 Ag5B Ag6B 111.4(9) . . ?
Pt1 Ag5B Ag6B 59.9(7) . . ?
Ag8B Ag5B Ag6B 109.0(10) . . ?
Se5 Ag5B Ag20 55.6(4) . . ?
Pt1 Ag5B Ag20 108.7(8) . . ?
Ag8B Ag5B Ag20 114.1(9) . . ?
Ag6B Ag5B Ag20 58.9(6) . . ?
Se5 Ag5B Ag1B 101.6(9) . . ?
Pt1 Ag5B Ag1B 58.7(7) . . ?
Ag8B Ag5B Ag1B 59.9(8) . . ?
Ag6B Ag5B Ag1B 59.5(8) . . ?
Ag20 Ag5B Ag1B 60.8(7) . . ?
Se5 Ag5B Ag4B 140.6(10) . . ?
Pt1 Ag5B Ag4B 55.1(6) . . ?
Ag8B Ag5B Ag4B 61.5(8) . . ?
Ag6B Ag5B Ag4B 106.4(10) . . ?
Ag20 Ag5B Ag4B 163.7(10) . . ?
Ag1B Ag5B Ag4B 106.6(10) . . ?
Se5 Ag5B Ag0X 137.5(11) . . ?
Pt1 Ag5B Ag0X 55.8(7) . . ?
Ag8B Ag5B Ag0X 108.4(10) . . ?
Ag6B Ag5B Ag0X 58.0(8) . . ?
Ag20 Ag5B Ag0X 111.8(9) . . ?
Ag1B Ag5B Ag0X 104.5(10) . . ?
Ag4B Ag5B Ag0X 59.1(8) . . ?
Se5 Ag5B Ag13 96.0(7) . . ?
Pt1 Ag5B Ag13 103.5(7) . . ?
Ag8B Ag5B Ag13 115.7(9) . . ?
Ag6B Ag5B Ag13 110.6(9) . . ?
Ag20 Ag5B Ag13 129.5(9) . . ?
Ag1B Ag5B Ag13 162.0(10) . . ?
Ag4B Ag5B Ag13 59.8(7) . . ?
Ag0X Ag5B Ag13 59.0(7) . . ?
Se1 Ag6B Pt1 160.3(9) . . ?
Se1 Ag6B Ag20 55.9(4) . . ?
Pt1 Ag6B Ag20 109.2(8) . . ?
Se1 Ag6B Ag0X 115.7(10) . . ?
Pt1 Ag6B Ag0X 57.0(7) . . ?
Ag20 Ag6B Ag0X 117.8(9) . . ?
Se1 Ag6B Ag5B 101.7(9) . . ?
Pt1 Ag6B Ag5B 58.7(6) . . ?
Ag20 Ag6B Ag5B 60.8(6) . . ?
Ag0X Ag6B Ag5B 62.9(8) . . ?
Se1 Ag6B Ag1B 114.4(9) . . ?
Pt1 Ag6B Ag1B 58.9(6) . . ?
Ag20 Ag6B Ag1B 62.0(7) . . ?
Ag0X Ag6B Ag1B 109.5(10) . . ?
Ag5B Ag6B Ag1B 61.1(8) . . ?
Se1 Ag6B Ag9B 136.4(10) . . ?
Pt1 Ag6B Ag9B 57.8(6) . . ?
Ag20 Ag6B Ag9B 111.5(9) . . ?
Ag0X Ag6B Ag9B 106.9(10) . . ?
Ag5B Ag6B Ag9B 105.7(10) . . ?
Ag1B Ag6B Ag9B 55.4(8) . . ?
Se1 Ag6B Ag1X 139.3(10) . . ?
Pt1 Ag6B Ag1X 56.2(6) . . ?
Ag20 Ag6B Ag1X 164.8(10) . . ?
Ag0X Ag6B Ag1X 59.8(8) . . ?
Ag5B Ag6B Ag1X 108.7(9) . . ?
Ag1B Ag6B Ag1X 103.8(10) . . ?
Ag9B Ag6B Ag1X 58.7(8) . . ?
Se1 Ag6B Ag17 96.7(7) . . ?
Pt1 Ag6B Ag17 103.0(7) . . ?
Ag20 Ag6B Ag17 132.4(8) . . ?
Ag0X Ag6B Ag17 108.9(8) . . ?
Ag5B Ag6B Ag17 161.7(10) . . ?
Ag1B Ag6B Ag17 110.8(9) . . ?
Ag9B Ag6B Ag17 59.5(6) . . ?
Ag1X Ag6B Ag17 55.3(6) . . ?
Pt1 Ag7B Ag9B 60.3(7) . . ?
Pt1 Ag7B Ag8B 59.5(7) . . ?
Ag9B Ag7B Ag8B 108.3(11) . . ?
Pt1 Ag7B Ag1B 59.8(7) . . ?
Ag9B Ag7B Ag1B 57.3(8) . . ?
Ag8B Ag7B Ag1B 60.9(8) . . ?
Pt1 Ag7B Ag18 108.1(8) . . ?
Ag9B Ag7B Ag18 61.3(7) . . ?
Ag8B Ag7B Ag18 167.6(11) . . ?
Ag1B Ag7B Ag18 113.4(9) . . ?
Pt1 Ag7B Ag2X 57.9(7) . . ?
Ag9B Ag7B Ag2X 111.2(11) . . ?
Ag8B Ag7B Ag2X 61.0(8) . . ?
Ag1B Ag7B Ag2X 109.4(11) . . ?
Ag18 Ag7B Ag2X 114.6(9) . . ?
Pt1 Ag7B Se14 159.7(9) . . ?
Ag9B Ag7B Se14 110.6(9) . . ?
Ag8B Ag7B Se14 137.9(10) . . ?
Ag1B Ag7B Se14 133.1(10) . . ?
Ag18 Ag7B Se14 54.4(4) . . ?
Ag2X Ag7B Se14 116.6(9) . . ?
Pt1 Ag7B Ag19 109.1(8) . . ?
Ag9B Ag7B Ag19 112.8(9) . . ?
Ag8B Ag7B Ag19 59.0(6) . . ?
Ag1B Ag7B Ag19 61.8(7) . . ?
Ag18 Ag7B Ag19 129.9(9) . . ?
Ag2X Ag7B Ag19 113.2(9) . . ?
Se14 Ag7B Ag19 91.1(7) . . ?
Pt1 Ag7B Ag2B 58.2(7) . . ?
Ag9B Ag7B Ag2B 61.4(8) . . ?
Ag8B Ag7B Ag2B 110.7(11) . . ?
Ag1B Ag7B Ag2B 107.4(11) . . ?
Ag18 Ag7B Ag2B 59.1(7) . . ?
Ag2X Ag7B Ag2B 62.3(8) . . ?
Se14 Ag7B Ag2B 101.6(9) . . ?
Ag19 Ag7B Ag2B 167.2(11) . . ?
Pt1 Ag8B Se15 151.8(9) . . ?
Pt1 Ag8B Ag19 110.3(8) . . ?
Se15 Ag8B Ag19 97.8(7) . . ?
Pt1 Ag8B Ag7B 58.8(7) . . ?
Se15 Ag8B Ag7B 139.9(11) . . ?
Ag19 Ag8B Ag7B 61.0(7) . . ?
Pt1 Ag8B Ag5B 59.2(7) . . ?
Se15 Ag8B Ag5B 111.0(9) . . ?
Ag19 Ag8B Ag5B 116.1(9) . . ?
Ag7B Ag8B Ag5B 109.0(10) . . ?
Pt1 Ag8B Ag1B 59.2(7) . . ?
Se15 Ag8B Ag1B 143.2(9) . . ?
Ag19 Ag8B Ag1B 62.0(7) . . ?
Ag7B Ag8B Ag1B 59.6(8) . . ?
Ag5B Ag8B Ag1B 61.0(8) . . ?
Pt1 Ag8B Ag2X 57.3(7) . . ?
Se15 Ag8B Ag2X 109.1(8) . . ?
Ag19 Ag8B Ag2X 114.0(9) . . ?
Ag7B Ag8B Ag2X 59.8(8) . . ?
Ag5B Ag8B Ag2X 108.4(10) . . ?
Ag1B Ag8B Ag2X 107.3(10) . . ?
Pt1 Ag8B Ag4B 54.8(6) . . ?
Se15 Ag8B Ag4B 97.0(8) . . ?
Ag19 Ag8B Ag4B 164.9(10) . . ?
Ag7B Ag8B Ag4B 105.1(10) . . ?
Ag5B Ag8B Ag4B 60.5(8) . . ?
Ag1B Ag8B Ag4B 106.7(10) . . ?
Ag2X Ag8B Ag4B 57.8(8) . . ?
Pt1 Ag8B Ag14 103.6(7) . . ?
Se15 Ag8B Ag14 52.6(4) . . ?
Ag19 Ag8B Ag14 131.3(9) . . ?
Ag7B Ag8B Ag14 114.2(9) . . ?
Ag5B Ag8B Ag14 110.9(9) . . ?
Ag1B Ag8B Ag14 162.8(10) . . ?
Ag2X Ag8B Ag14 59.1(6) . . ?
Ag4B Ag8B Ag14 57.9(6) . . ?
Ag1B Ag9B Se12 122.1(10) . . ?
Ag1B Ag9B Pt1 60.6(7) . . ?
Se12 Ag9B Pt1 160.1(10) . . ?
Ag1B Ag9B Ag7B 61.4(8) . . ?
Se12 Ag9B Ag7B 104.0(10) . . ?
Pt1 Ag9B Ag7B 58.5(7) . . ?
Ag1B Ag9B Ag18 115.5(10) . . ?
Se12 Ag9B Ag18 55.0(5) . . ?
Pt1 Ag9B Ag18 105.3(7) . . ?
Ag7B Ag9B Ag18 59.6(7) . . ?
Ag1B Ag9B Ag2B 109.4(10) . . ?
Se12 Ag9B Ag2B 107.2(9) . . ?
Pt1 Ag9B Ag2B 57.1(6) . . ?
Ag7B Ag9B Ag2B 59.9(8) . . ?
Ag18 Ag9B Ag2B 58.0(7) . . ?
Ag1B Ag9B Ag1X 109.2(11) . . ?
Se12 Ag9B Ag1X 128.2(10) . . ?
Pt1 Ag9B Ag1X 57.0(6) . . ?
Ag7B Ag9B Ag1X 106.5(10) . . ?
Ag18 Ag9B Ag1X 110.2(9) . . ?
Ag2B Ag9B Ag1X 57.9(8) . . ?
Ag1B Ag9B Ag17 115.9(10) . . ?
Se12 Ag9B Ag17 92.4(7) . . ?
Pt1 Ag9B Ag17 103.9(8) . . ?
Ag7B Ag9B Ag17 161.9(11) . . ?
Ag18 Ag9B Ag17 128.3(8) . . ?
Ag2B Ag9B Ag17 108.3(9) . . ?
Ag1X Ag9B Ag17 56.2(6) . . ?
Ag1B Ag9B Ag6B 60.0(8) . . ?
Se12 Ag9B Ag6B 141.7(10) . . ?
Pt1 Ag9B Ag6B 58.1(6) . . ?
Ag7B Ag9B Ag6B 107.9(10) . . ?
Ag18 Ag9B Ag6B 163.3(10) . . ?
Ag2B Ag9B Ag6B 106.9(10) . . ?
Ag1X Ag9B Ag6B 60.8(8) . . ?
Ag17 Ag9B Ag6B 60.4(7) . . ?
Pt1 Ag0X Ag6B 61.4(7) . . ?
Pt1 Ag0X Ag3B 56.6(7) . . ?
Ag6B Ag0X Ag3B 110.7(11) . . ?
Pt1 Ag0X Se8 158.2(9) . . ?
Ag6B Ag0X Se8 119.8(10) . . ?
Ag3B Ag0X Se8 107.7(9) . . ?
Pt1 Ag0X Ag1X 58.5(7) . . ?
Ag6B Ag0X Ag1X 63.0(8) . . ?
Ag3B Ag0X Ag1X 60.4(8) . . ?
Se8 Ag0X Ag1X 101.4(9) . . ?
Pt1 Ag0X Ag4B 56.2(7) . . ?
Ag6B Ag0X Ag4B 107.9(10) . . ?
Ag3B Ag0X Ag4B 57.7(8) . . ?
Se8 Ag0X Ag4B 131.7(10) . . ?
Ag1X Ag0X Ag4B 106.4(10) . . ?
Pt1 Ag0X Ag13 108.0(8) . . ?
Ag6B Ag0X Ag13 113.9(9) . . ?
Ag3B Ag0X Ag13 111.8(9) . . ?
Se8 Ag0X Ag13 91.6(7) . . ?
Ag1X Ag0X Ag13 166.3(11) . . ?
Ag4B Ag0X Ag13 61.0(7) . . ?
Pt1 Ag0X Ag5B 58.7(7) . . ?
Ag6B Ag0X Ag5B 59.1(8) . . ?
Ag3B Ag0X Ag5B 106.6(11) . . ?
Se8 Ag0X Ag5B 142.5(10) . . ?
Ag1X Ag0X Ag5B 108.3(10) . . ?
Ag4B Ag0X Ag5B 59.8(8) . . ?
Ag13 Ag0X Ag5B 61.6(7) . . ?
Pt1 Ag0X Ag16 106.4(8) . . ?
Ag6B Ag0X Ag16 117.2(9) . . ?
Ag3B Ag0X Ag16 59.8(7) . . ?
Se8 Ag0X Ag16 52.5(4) . . ?
Ag1X Ag0X Ag16 60.3(6) . . ?
Ag4B Ag0X Ag16 111.9(9) . . ?
Ag13 Ag0X Ag16 127.5(8) . . ?
Ag5B Ag0X Ag16 164.9(11) . . ?
Pt1 Ag1X Ag17 111.0(8) . . ?
Pt1 Ag1X Ag2B 58.8(7) . . ?
Ag17 Ag1X Ag2B 116.3(10) . . ?
Pt1 Ag1X Ag3B 55.5(6) . . ?
Ag17 Ag1X Ag3B 166.2(10) . . ?
Ag2B Ag1X Ag3B 61.3(8) . . ?
Pt1 Ag1X Ag0X 56.9(7) . . ?
Ag17 Ag1X Ag0X 112.9(9) . . ?
Ag2B Ag1X Ag0X 108.5(10) . . ?
Ag3B Ag1X Ag0X 58.7(8) . . ?
Pt1 Ag1X Ag9B 59.3(7) . . ?
Ag17 Ag1X Ag9B 62.5(7) . . ?
Ag2B Ag1X Ag9B 60.7(8) . . ?
Ag3B Ag1X Ag9B 107.7(10) . . ?
Ag0X Ag1X Ag9B 106.3(10) . . ?
Pt1 Ag1X Se10 157.5(9) . . ?
Ag17 Ag1X Se10 90.0(7) . . ?
Ag2B Ag1X Se10 119.9(9) . . ?
Ag3B Ag1X Se10 102.9(8) . . ?
Ag0X Ag1X Se10 108.2(9) . . ?
Ag9B Ag1X Se10 142.3(10) . . ?
Pt1 Ag1X Ag16 106.0(7) . . ?
Ag17 Ag1X Ag16 128.2(9) . . ?
Ag2B Ag1X Ag16 113.6(8) . . ?
Ag3B Ag1X Ag16 59.7(7) . . ?
Ag0X Ag1X Ag16 61.4(7) . . ?
Ag9B Ag1X Ag16 165.2(10) . . ?
Se10 Ag1X Ag16 52.3(4) . . ?
Pt1 Ag1X Ag6B 58.7(6) . . ?
Ag17 Ag1X Ag6B 62.4(6) . . ?
Ag2B Ag1X Ag6B 108.9(10) . . ?
Ag3B Ag1X Ag6B 104.8(9) . . ?
Ag0X Ag1X Ag6B 57.2(8) . . ?
Ag9B Ag1X Ag6B 60.5(8) . . ?
Se10 Ag1X Ag6B 130.8(10) . . ?
Ag16 Ag1X Ag6B 113.0(9) . . ?
Pt1 Ag2X Ag4B 57.0(7) . . ?
Pt1 Ag2X Ag7B 59.3(7) . . ?
Ag4B Ag2X Ag7B 108.3(10) . . ?
Pt1 Ag2X Ag8B 59.3(7) . . ?
Ag4B Ag2X Ag8B 62.3(8) . . ?
Ag7B Ag2X Ag8B 59.3(8) . . ?
Pt1 Ag2X Se19 160.1(9) . . ?
Ag4B Ag2X Se19 108.4(9) . . ?
Ag7B Ag2X Se19 121.6(10) . . ?
Ag8B Ag2X Se19 102.8(8) . . ?
Pt1 Ag2X Ag14 108.1(8) . . ?
Ag4B Ag2X Ag14 60.5(7) . . ?
Ag7B Ag2X Ag14 117.2(9) . . ?
Ag8B Ag2X Ag14 62.9(6) . . ?
Se19 Ag2X Ag14 52.5(4) . . ?
Pt1 Ag2X Ag3B 55.3(6) . . ?
Ag4B Ag2X Ag3B 57.7(8) . . ?
Ag7B Ag2X Ag3B 106.3(10) . . ?
Ag8B Ag2X Ag3B 107.3(10) . . ?
Se19 Ag2X Ag3B 131.6(9) . . ?
Ag14 Ag2X Ag3B 112.1(9) . . ?
Pt1 Ag2X Ag2B 57.5(6) . . ?
Ag4B Ag2X Ag2B 106.2(10) . . ?
Ag7B Ag2X Ag2B 59.1(8) . . ?
Ag8B Ag2X Ag2B 106.8(9) . . ?
Se19 Ag2X Ag2B 142.0(10) . . ?
Ag14 Ag2X Ag2B 165.5(10) . . ?
Ag3B Ag2X Ag2B 59.5(8) . . ?
Pt1 Ag2X Ag15 106.2(8) . . ?
Ag4B Ag2X Ag15 112.3(9) . . ?
Ag7B Ag2X Ag15 113.8(9) . . ?
Ag8B Ag2X Ag15 165.5(10) . . ?
Se19 Ag2X Ag15 91.7(6) . . ?
Ag14 Ag2X Ag15 127.9(8) . . ?
Ag3B Ag2X Ag15 61.0(6) . . ?
Ag2B Ag2X Ag15 60.6(6) . . ?
Se7 Ag13 Se6 124.89(8) . . ?
Se7 Ag13 Se17 119.89(7) . . ?
Se6 Ag13 Se17 115.21(7) . . ?
Se7 Ag13 Ag4 97.69(6) . . ?
Se6 Ag13 Ag4 113.02(7) . . ?
Se17 Ag13 Ag4 57.13(5) . . ?
Se7 Ag13 Ag1 57.09(5) . . ?
Se6 Ag13 Ag1 100.50(6) . . ?
Se17 Ag13 Ag1 115.13(7) . . ?
Ag4 Ag13 Ag1 59.55(4) . . ?
Se7 Ag13 Ag5 115.57(6) . . ?
Se6 Ag13 Ag5 56.72(5) . . ?
Se17 Ag13 Ag5 97.01(6) . . ?
Ag4 Ag13 Ag5 58.95(4) . . ?
Ag1 Ag13 Ag5 59.84(4) . . ?
Se7 Ag13 Ag0X 77.2(4) . . ?
Se6 Ag13 Ag0X 73.6(5) . . ?
Se17 Ag13 Ag0X 124.1(5) . . ?
Se7 Ag13 Ag4B 73.6(5) . . ?
Se6 Ag13 Ag4B 123.8(4) . . ?
Se17 Ag13 Ag4B 75.1(5) . . ?
Ag0X Ag13 Ag4B 58.7(7) . . ?
Se7 Ag13 Ag5B 126.6(4) . . ?
Se6 Ag13 Ag5B 73.0(5) . . ?
Se17 Ag13 Ag5B 70.7(5) . . ?
Ag0X Ag13 Ag5B 59.4(6) . . ?
Ag4B Ag13 Ag5B 58.4(6) . . ?
Se19 Ag14 Se18 116.02(7) . . ?
Se19 Ag14 Se15 122.63(8) . . ?
Se18 Ag14 Se15 118.42(7) . . ?
Se19 Ag14 Ag4B 116.2(5) . . ?
Se18 Ag14 Ag4B 62.8(5) . . ?
Se15 Ag14 Ag4B 103.5(4) . . ?
Se19 Ag14 Ag4 132.25(6) . . ?
Se18 Ag14 Ag4 76.00(6) . . ?
Se15 Ag14 Ag4 78.47(5) . . ?
Se19 Ag14 Ag9 83.19(6) . . ?
Se18 Ag14 Ag9 129.50(7) . . ?
Se15 Ag14 Ag9 76.21(5) . . ?
Ag4 Ag14 Ag9 59.16(4) . . ?
Se19 Ag14 Ag2X 63.6(5) . . ?
Se18 Ag14 Ag2X 106.6(5) . . ?
Se15 Ag14 Ag2X 114.4(4) . . ?
Ag4B Ag14 Ag2X 58.1(7) . . ?
Se19 Ag14 Ag3 77.11(6) . . ?
Se18 Ag14 Ag3 79.27(6) . . ?
Se15 Ag14 Ag3 129.24(6) . . ?
Ag4 Ag14 Ag3 59.22(4) . . ?
Ag9 Ag14 Ag3 59.12(4) . . ?
Se19 Ag14 Ag8B 107.6(5) . . ?
Se18 Ag14 Ag8B 118.5(5) . . ?
Se15 Ag14 Ag8B 59.3(4) . . ?
Ag4B Ag14 Ag8B 59.8(7) . . ?
Ag2X Ag14 Ag8B 58.0(6) . . ?
Se23 Ag15 Se22 119.10(7) . . ?
Se23 Ag15 Se20 117.65(7) . . ?
Se22 Ag15 Se20 123.25(7) . . ?
Se23 Ag15 Ag8 56.88(5) . . ?
Se22 Ag15 Ag8 95.40(5) . . ?
Se20 Ag15 Ag8 115.33(6) . . ?
Se23 Ag15 Ag2 115.92(6) . . ?
Se22 Ag15 Ag2 57.30(5) . . ?
Se20 Ag15 Ag2 97.44(6) . . ?
Ag8 Ag15 Ag2 59.98(4) . . ?
Se23 Ag15 Ag3 96.07(6) . . ?
Se22 Ag15 Ag3 115.97(6) . . ?
Se20 Ag15 Ag3 56.97(5) . . ?
Ag8 Ag15 Ag3 59.93(4) . . ?
Ag2 Ag15 Ag3 59.48(4) . . ?
Se23 Ag15 Ag2X 69.5(5) . . ?
Se22 Ag15 Ag2X 124.4(5) . . ?
Se20 Ag15 Ag2X 76.2(5) . . ?
Se23 Ag15 Ag3B 122.6(5) . . ?
Se22 Ag15 Ag3B 76.8(5) . . ?
Se20 Ag15 Ag3B 73.4(4) . . ?
Ag2X Ag15 Ag3B 58.7(7) . . ?
Se23 Ag15 Ag2B 75.7(5) . . ?
Se22 Ag15 Ag2B 69.7(4) . . ?
Se20 Ag15 Ag2B 126.1(5) . . ?
Ag2X Ag15 Ag2B 59.5(6) . . ?
Ag3B Ag15 Ag2B 58.4(6) . . ?
Se21 Ag16 Se8 120.70(7) . . ?
Se21 Ag16 Se10 118.95(7) . . ?
Se8 Ag16 Se10 116.08(7) . . ?
Se21 Ag16 Ag2 74.12(6) . . ?
Se8 Ag16 Ag2 129.99(7) . . ?
Se10 Ag16 Ag2 86.45(6) . . ?
Se21 Ag16 Ag6 130.57(7) . . ?
Se8 Ag16 Ag6 80.52(6) . . ?
Se10 Ag16 Ag6 78.00(6) . . ?
Ag2 Ag16 Ag6 60.23(4) . . ?
Se21 Ag16 Ag3B 63.8(4) . . ?
Se8 Ag16 Ag3B 113.3(5) . . ?
Se10 Ag16 Ag3B 111.6(5) . . ?
Se21 Ag16 Ag1 83.11(6) . . ?
Se8 Ag16 Ag1 74.64(6) . . ?
Se10 Ag16 Ag1 133.55(7) . . ?
Ag2 Ag16 Ag1 59.24(4) . . ?
Ag6 Ag16 Ag1 58.55(4) . . ?
Se21 Ag16 Ag1X 115.9(5) . . ?
Se8 Ag16 Ag1X 106.7(5) . . ?
Se10 Ag16 Ag1X 63.8(4) . . ?
Ag3B Ag16 Ag1X 58.8(6) . . ?
Se21 Ag16 Ag0X 110.0(5) . . ?
Se8 Ag16 Ag0X 61.2(5) . . ?
Se10 Ag16 Ag0X 115.5(5) . . ?
Ag3B Ag16 Ag0X 57.4(7) . . ?
Ag1X Ag16 Ag0X 58.3(6) . . ?
Se11 Ag17 Se2 123.24(8) . . ?
Se11 Ag17 Se9 122.60(7) . . ?
Se2 Ag17 Se9 114.15(7) . . ?
Se11 Ag17 Ag1X 70.7(5) . . ?
Se2 Ag17 Ag1X 124.8(5) . . ?
Se9 Ag17 Ag1X 77.1(5) . . ?
Se11 Ag17 Ag6 97.16(6) . . ?
Se2 Ag17 Ag6 113.75(6) . . ?
Se9 Ag17 Ag6 56.60(5) . . ?
Se11 Ag17 Ag7 56.54(5) . . ?
Se2 Ag17 Ag7 99.32(6) . . ?
Se9 Ag17 Ag7 115.43(6) . . ?
Ag6 Ag17 Ag7 59.71(4) . . ?
Se11 Ag17 Ag11 114.81(6) . . ?
Se2 Ag17 Ag11 56.67(5) . . ?
Se9 Ag17 Ag11 94.97(6) . . ?
Ag6 Ag17 Ag11 59.35(4) . . ?
Ag7 Ag17 Ag11 59.63(4) . . ?
Se11 Ag17 Ag9B 76.6(5) . . ?
Se2 Ag17 Ag9B 70.6(4) . . ?
Se9 Ag17 Ag9B 125.3(5) . . ?
Ag1X Ag17 Ag9B 61.2(7) . . ?
Se11 Ag17 Ag6B 126.8(4) . . ?
Se2 Ag17 Ag6B 71.4(4) . . ?
Se9 Ag17 Ag6B 70.1(5) . . ?
Ag1X Ag17 Ag6B 62.3(6) . . ?
Ag9B Ag17 Ag6B 60.1(7) . . ?
Se24 Ag18 Se14 115.03(7) . . ?
Se24 Ag18 Se12 119.49(7) . . ?
Se14 Ag18 Se12 120.26(7) . . ?
Se24 Ag18 Ag2B 64.0(5) . . ?
Se14 Ag18 Ag2B 109.8(5) . . ?
Se12 Ag18 Ag2B 114.4(5) . . ?
Se24 Ag18 Ag7B 117.9(5) . . ?
Se14 Ag18 Ag7B 63.2(5) . . ?
Se12 Ag18 Ag7B 107.6(5) . . ?
Ag2B Ag18 Ag7B 60.9(7) . . ?
Se24 Ag18 Ag12 133.21(7) . . ?
Se14 Ag18 Ag12 77.87(6) . . ?
Se12 Ag18 Ag12 82.20(6) . . ?
Se24 Ag18 Ag8 76.66(5) . . ?
Se14 Ag18 Ag8 82.87(6) . . ?
Se12 Ag18 Ag8 131.15(7) . . ?
Ag12 Ag18 Ag8 59.88(4) . . ?
Se24 Ag18 Ag9B 113.7(5) . . ?
Se14 Ag18 Ag9B 116.4(5) . . ?
Se12 Ag18 Ag9B 59.9(5) . . ?
Ag2B Ag18 Ag9B 61.3(7) . . ?
Ag7B Ag18 Ag9B 59.1(7) . . ?
Se24 Ag18 Ag7 84.55(6) . . ?
Se14 Ag18 Ag7 132.83(7) . . ?
Se12 Ag18 Ag7 75.77(6) . . ?
Ag12 Ag18 Ag7 59.68(4) . . ?
Ag8 Ag18 Ag7 59.33(4) . . ?
Se13 Ag19 Se4 117.36(7) . . ?
Se13 Ag19 Se16 124.79(7) . . ?
Se4 Ag19 Se16 117.84(7) . . ?
Se13 Ag19 Ag8B 124.7(5) . . ?
Se4 Ag19 Ag8B 72.0(5) . . ?
Se16 Ag19 Ag8B 73.3(5) . . ?
Se13 Ag19 Ag7B 74.9(5) . . ?
Se4 Ag19 Ag7B 124.6(5) . . ?
Se16 Ag19 Ag7B 74.2(5) . . ?
Ag8B Ag19 Ag7B 60.0(7) . . ?
Se13 Ag19 Ag12 57.45(5) . . ?
Se4 Ag19 Ag12 113.33(7) . . ?
Se16 Ag19 Ag12 99.38(6) . . ?
Se13 Ag19 Ag1B 70.0(5) . . ?
Se4 Ag19 Ag1B 74.9(5) . . ?
Se16 Ag19 Ag1B 125.1(4) . . ?
Ag8B Ag19 Ag1B 60.2(7) . . ?
Ag7B Ag19 Ag1B 58.6(7) . . ?
Se13 Ag19 Ag9 115.92(6) . . ?
Se4 Ag19 Ag9 97.20(6) . . ?
Se16 Ag19 Ag9 56.11(5) . . ?
Ag12 Ag19 Ag9 59.70(4) . . ?
Se13 Ag19 Ag10 97.34(6) . . ?
Se4 Ag19 Ag10 56.50(5) . . ?
Se16 Ag19 Ag10 112.12(6) . . ?
Ag12 Ag19 Ag10 58.85(4) . . ?
Ag9 Ag19 Ag10 58.23(4) . . ?
Se5 Ag20 Se1 119.71(8) . . ?
Se5 Ag20 Se3 117.20(8) . . ?
Se1 Ag20 Se3 121.29(7) . . ?
Se5 Ag20 Ag6B 114.7(5) . . ?
Se1 Ag20 Ag6B 59.4(5) . . ?
Se3 Ag20 Ag6B 107.5(5) . . ?
Se5 Ag20 Ag5B 57.7(5) . . ?
Se1 Ag20 Ag5B 103.9(5) . . ?
Se3 Ag20 Ag5B 117.6(5) . . ?
Ag6B Ag20 Ag5B 60.3(7) . . ?
Se5 Ag20 Ag10 75.19(6) . . ?
Se1 Ag20 Ag10 128.12(6) . . ?
Se3 Ag20 Ag10 79.24(6) . . ?
Se5 Ag20 Ag1B 102.8(5) . . ?
Se1 Ag20 Ag1B 115.6(5) . . ?
Se3 Ag20 Ag1B 62.3(5) . . ?
Ag6B Ag20 Ag1B 59.7(7) . . ?
Ag5B Ag20 Ag1B 60.2(7) . . ?
Se5 Ag20 Ag11 126.36(6) . . ?
Se1 Ag20 Ag11 76.04(6) . . ?
Se3 Ag20 Ag11 82.12(6) . . ?
Ag10 Ag20 Ag11 59.16(4) . . ?
Se5 Ag20 Ag5 75.11(5) . . ?
Se1 Ag20 Ag5 77.01(6) . . ?
Se3 Ag20 Ag5 131.98(7) . . ?
Ag10 Ag20 Ag5 58.35(4) . . ?
Ag11 Ag20 Ag5 58.16(4) . . ?
P1 Se1 Ag20 96.04(15) . . ?
P1 Se1 Ag6B 91.7(5) . . ?
Ag20 Se1 Ag6B 64.7(5) . . ?
P1 Se2 Ag17 100.23(14) . . ?
P1 Se2 Ag11 93.49(13) . . ?
Ag17 Se2 Ag11 67.66(5) . . ?
P2 Se3 Ag20 97.46(16) . . ?
P2 Se3 Ag1B 92.0(5) . . ?
Ag20 Se3 Ag1B 64.7(5) . . ?
P2 Se4 Ag19 99.31(15) . . ?
P2 Se4 Ag10 95.57(14) . . ?
Ag19 Se4 Ag10 69.03(6) . . ?
P3 Se5 Ag20 96.46(14) . . ?
P3 Se5 Ag5B 92.7(6) . . ?
Ag20 Se5 Ag5B 66.7(5) . . ?
P3 Se6 Ag13 98.34(14) . . ?
P3 Se6 Ag5 92.77(15) . . ?
Ag13 Se6 Ag5 68.35(6) . . ?
P4 Se7 Ag13 101.16(13) . . ?
P4 Se7 Ag1 92.63(13) . . ?
Ag13 Se7 Ag1 68.31(6) . . ?
P4 Se8 Ag16 98.79(14) . . ?
P4 Se8 Ag0X 94.5(5) . . ?
Ag16 Se8 Ag0X 66.3(5) . . ?
P5 Se9 Ag17 97.53(14) . . ?
P5 Se9 Ag6 94.39(13) . . ?
Ag17 Se9 Ag6 67.43(6) . . ?
P5 Se10 Ag16 96.69(14) . . ?
P5 Se10 Ag1X 91.9(5) . . ?
Ag16 Se10 Ag1X 63.9(5) . . ?
P6 Se11 Ag17 101.33(14) . . ?
P6 Se11 Ag7 92.94(13) . . ?
Ag17 Se11 Ag7 67.71(5) . . ?
P6 Se12 Ag18 95.54(13) . . ?
P6 Se12 Ag9B 95.7(5) . . ?
Ag18 Se12 Ag9B 65.1(5) . . ?
P7 Se13 Ag19 99.20(14) . . ?
P7 Se13 Ag12 94.30(13) . . ?
Ag19 Se13 Ag12 67.56(5) . . ?
P7 Se14 Ag18 95.30(15) . . ?
P7 Se14 Ag7B 91.5(5) . . ?
Ag18 Se14 Ag7B 62.4(5) . . ?
P8 Se15 Ag14 96.98(13) . . ?
P8 Se15 Ag8B 88.5(5) . . ?
Ag14 Se15 Ag8B 68.2(4) . . ?
P8 Se16 Ag19 97.52(13) . . ?
P8 Se16 Ag9 93.06(14) . . ?
Ag19 Se16 Ag9 69.00(6) . . ?
P9 Se17 Ag13 96.44(13) . . ?
P9 Se17 Ag4 92.63(13) . . ?
Ag13 Se17 Ag4 67.31(6) . . ?
P9 Se18 Ag14 97.20(14) . . ?
P9 Se18 Ag4B 92.9(5) . . ?
Ag14 Se18 Ag4B 63.9(5) . . ?
P10 Se19 Ag14 97.50(14) . . ?
P10 Se19 Ag2X 94.5(5) . . ?
Ag14 Se19 Ag2X 64.0(5) . . ?
P10 Se20 Ag15 103.41(14) . . ?
P10 Se20 Ag3 94.31(13) . . ?
Ag15 Se20 Ag3 67.61(5) . . ?
P11 Se21 Ag16 97.71(13) . . ?
P11 Se21 Ag3B 95.5(5) . . ?
Ag16 Se21 Ag3B 63.4(5) . . ?
P11 Se22 Ag15 100.45(14) . . ?
P11 Se22 Ag2 91.56(13) . . ?
Ag15 Se22 Ag2 67.30(5) . . ?
P12 Se23 Ag15 101.74(15) . . ?
P12 Se23 Ag8 93.82(13) . . ?
Ag15 Se23 Ag8 67.50(6) . . ?
P12 Se24 Ag18 96.98(14) . . ?
P12 Se24 Ag2B 94.7(5) . . ?
Ag18 Se24 Ag2B 61.9(5) . . ?
O2 P1 O1 106.9(8) . . ?
O2 P1 Se1 112.1(5) . . ?
O1 P1 Se1 104.1(7) . . ?
O2 P1 Se2 102.9(6) . . ?
O1 P1 Se2 113.3(6) . . ?
Se1 P1 Se2 117.3(2) . . ?
O3 P2 O4 106.3(8) . . ?
O3 P2 Se3 107.9(6) . . ?
O4 P2 Se3 111.7(6) . . ?
O3 P2 Se4 109.1(6) . . ?
O4 P2 Se4 103.8(6) . . ?
Se3 P2 Se4 117.4(2) . . ?
O5 P3 O6 107.6(7) . . ?
O5 P3 Se5 113.0(6) . . ?
O6 P3 Se5 102.5(7) . . ?
O5 P3 Se6 103.5(6) . . ?
O6 P3 Se6 112.2(6) . . ?
Se5 P3 Se6 117.9(2) . . ?
O8 P4 O7 101.6(7) . . ?
O8 P4 Se8 114.3(5) . . ?
O7 P4 Se8 109.9(5) . . ?
O8 P4 Se7 102.6(5) . . ?
O7 P4 Se7 110.5(5) . . ?
Se8 P4 Se7 116.8(2) . . ?
O9 P5 O10 107.2(7) . . ?
O9 P5 Se10 112.5(5) . . ?
O10 P5 Se10 106.7(5) . . ?
O9 P5 Se9 103.5(5) . . ?
O10 P5 Se9 109.3(5) . . ?
Se10 P5 Se9 117.1(2) . . ?
O11 P6 O12 99.6(7) . . ?
O11 P6 Se12 111.3(5) . . ?
O12 P6 Se12 114.0(5) . . ?
O11 P6 Se11 110.0(5) . . ?
O12 P6 Se11 104.0(5) . . ?
Se12 P6 Se11 116.6(2) . . ?
O14 P7 O13 99.9(7) . . ?
O14 P7 Se14 111.6(6) . . ?
O13 P7 Se14 113.4(5) . . ?
O14 P7 Se13 110.3(6) . . ?
O13 P7 Se13 102.8(6) . . ?
Se14 P7 Se13 117.2(2) . . ?
O15 P8 O16 107.1(7) . . ?
O15 P8 Se15 104.0(5) . . ?
O16 P8 Se15 114.2(5) . . ?
O15 P8 Se16 110.3(5) . . ?
O16 P8 Se16 102.5(5) . . ?
Se15 P8 Se16 118.3(2) . . ?
O17 P9 O18 108.3(7) . . ?
O17 P9 Se18 112.9(5) . . ?
O18 P9 Se18 103.4(4) . . ?
O17 P9 Se17 103.5(5) . . ?
O18 P9 Se17 110.8(5) . . ?
Se18 P9 Se17 117.8(2) . . ?
O19 P10 O20 99.9(7) . . ?
O19 P10 Se19 113.8(5) . . ?
O20 P10 Se19 110.7(6) . . ?
O19 P10 Se20 103.3(5) . . ?
O20 P10 Se20 111.5(5) . . ?
Se19 P10 Se20 116.3(2) . . ?
O21 P11 O22 99.0(7) . . ?
O21 P11 Se21 113.7(5) . . ?
O22 P11 Se21 110.9(5) . . ?
O21 P11 Se22 104.8(5) . . ?
O22 P11 Se22 111.1(5) . . ?
Se21 P11 Se22 116.0(2) . . ?
O24 P12 O23 100.0(7) . . ?
O24 P12 Se24 111.3(6) . . ?
O23 P12 Se24 114.2(6) . . ?
O24 P12 Se23 111.5(6) . . ?
O23 P12 Se23 102.3(6) . . ?
Se24 P12 Se23 116.0(2) . . ?
C1 O1 P1 125.6(14) . . ?
C4 O2 P1 118.8(13) . . ?
C7 O3 P2 127.6(14) . . ?
C10 O4 P2 124.1(14) . . ?
C13 O5 P3 126.4(14) . . ?
C16 O6 P3 127.9(15) . . ?
C19 O7 P4 124.8(12) . . ?
C22 O8 P4 122.6(11) . . ?
C25 O9 P5 127.5(12) . . ?
C28 O10 P5 121.4(11) . . ?
C31 O11 P6 124.2(12) . . ?
C34 O12 P6 123.9(11) . . ?
C37 O13 P7 125.7(13) . . ?
C40 O14 P7 123.4(13) . . ?
C43 O15 P8 125.3(11) . . ?
C46 O16 P8 124.8(11) . . ?
C49 O17 P9 126.5(11) . . ?
C52 O18 P9 124.6(11) . . ?
C55 O19 P10 127.6(12) . . ?
C58 O20 P10 123.8(11) . . ?
C61 O21 P11 124.6(11) . . ?
C64 O22 P11 124.3(12) . . ?
C67 O23 P12 123.0(15) . . ?
C70 O24 P12 125.1(12) . . ?
O1 C1 C2 111(2) . . ?
O1 C1 C3 105(2) . . ?
C2 C1 C3 107(2) . . ?
O2 C4 C5 105.6(17) . . ?
O2 C4 C6 109.6(18) . . ?
C5 C4 C6 114.5(18) . . ?
O3 C7 C8 112.0(19) . . ?
O3 C7 C9 105.5(19) . . ?
C8 C7 C9 113(2) . . ?
C11 C10 O4 109(2) . . ?
C11 C10 C12 115(2) . . ?
O4 C10 C12 111(2) . . ?
O5 C13 C14 107.2(18) . . ?
O5 C13 C15 107.3(18) . . ?
C14 C13 C15 114.4(18) . . ?
C18 C16 C17 115(2) . . ?
C18 C16 O6 104(2) . . ?
C17 C16 O6 106.9(19) . . ?
O7 C19 C21 105.9(18) . . ?
O7 C19 C20 108.2(17) . . ?
C21 C19 C20 112(2) . . ?
O8 C22 C24 105.4(16) . . ?
O8 C22 C23 107.0(15) . . ?
C24 C22 C23 116.6(19) . . ?
O9 C25 C26 108.5(17) . . ?
O9 C25 C27 111.2(16) . . ?
C26 C25 C27 112.3(17) . . ?
C29 C28 O10 113.1(16) . . ?
C29 C28 C30 115.0(17) . . ?
O10 C28 C30 103.8(15) . . ?
C32 C31 O11 111.5(19) . . ?
C32 C31 C33 114.3(19) . . ?
O11 C31 C33 103.5(17) . . ?
O12 C34 C35 105.6(15) . . ?
O12 C34 C36 111.0(15) . . ?
C35 C34 C36 112.7(17) . . ?
C38 C37 C39 113(2) . . ?
C38 C37 O13 111.2(18) . . ?
C39 C37 O13 104.1(18) . . ?
O14 C40 C41 110(2) . . ?
O14 C40 C42 103.4(16) . . ?
C41 C40 C42 112(2) . . ?
O15 C43 C44 110.1(16) . . ?
O15 C43 C45 108.1(17) . . ?
C44 C43 C45 110.1(16) . . ?
O16 C46 C47 105.6(16) . . ?
O16 C46 C48 110.1(16) . . ?
C47 C46 C48 109.8(18) . . ?
O17 C49 C50 107.2(15) . . ?
O17 C49 C51 107.8(17) . . ?
C50 C49 C51 114.8(16) . . ?
O18 C52 C54 106.2(16) . . ?
O18 C52 C53 109.3(17) . . ?
C54 C52 C53 114.1(18) . . ?
O19 C55 C56 110.5(16) . . ?
O19 C55 C57 105.6(16) . . ?
C56 C55 C57 114.1(17) . . ?
O20 C58 C60 108.1(16) . . ?
O20 C58 C59 107.1(17) . . ?
C60 C58 C59 113.5(18) . . ?
O21 C61 C62 109.4(17) . . ?
O21 C61 C63 104.0(16) . . ?
C62 C61 C63 110.1(18) . . ?
C65 C64 O22 109.4(17) . . ?
C65 C64 C66 113.1(19) . . ?
O22 C64 C66 107.3(18) . . ?
C69 C67 O23 114(3) . . ?
C69 C67 C68 115(3) . . ?
O23 C67 C68 105(2) . . ?
C71 C70 O24 108.7(18) . . ?
C71 C70 C72 113.6(19) . . ?
O24 C70 C72 104.7(18) . . ?
O25 C74 C73 122(2) . . ?
O25 C74 C75 118(2) . . ?
C73 C74 C75 119(2) . . ?
O26 C77 C76 119(3) . . ?
O26 C77 C78 124(3) . . ?
C76 C77 C78 117(2) . . ?
O27 C80 C79 122(2) . . ?
O27 C80 C81 122(2) . . ?
C79 C80 C81 115(2) . . ?

_refine_diff_density_max         2.517
_refine_diff_density_min         -1.146
_refine_diff_density_rms         0.213


_chemical_properties_physical    Light-sensitive
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_2
_database_code_depnum_ccdc_archive 'CCDC 2069767'
loop_
_audit_author_name
_audit_author_address
'Chen-Wei Liu'
;Department of Chemistry, National Dong Hwa University
Taiwan
;
_audit_update_record             
;
2021-03-11 deposited with the CCDC.	2021-06-25 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2014/7
_shelx_SHELXL_version_number     2014/7
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C192 H216 Ag20 P12 Pt Se24'
_chemical_formula_weight         7142.81

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Se Se -0.0929 2.2259 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'

_shelx_space_group_comment       
; 
The symmetry employed for this shelxl refinement is uniquely defined 
by the following loop, which should always be used as a source of 
symmetry information in preference to the above space-group names. 
They are only intended as comments. 
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   18.4077(12)
_cell_length_b                   18.8892(13)
_cell_length_c                   33.160(2)
_cell_angle_alpha                78.1000(10)
_cell_angle_beta                 84.0500(10)
_cell_angle_gamma                83.2810(10)
_cell_volume                     11167.1(13)
_cell_formula_units_Z            2
_cell_measurement_temperature    150(2)
_cell_measurement_reflns_used    9969
_cell_measurement_theta_min      2.21
_cell_measurement_theta_max      24.73

_exptl_crystal_description       plate
_exptl_crystal_colour            red
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    2.124
_exptl_crystal_F_000             6764
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          0.100
_exptl_crystal_size_mid          0.070
_exptl_crystal_size_min          0.030
_exptl_absorpt_coefficient_mu    6.374
_shelx_estimated_absorpt_T_min   0.568
_shelx_estimated_absorpt_T_max   0.832
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_correction_T_min  0.5984
_exptl_absorpt_correction_T_max  0.7452
_exptl_absorpt_process_details   SADABS
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      150(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_source                   ?
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            64121
_diffrn_reflns_av_unetI/netI     0.1094
_diffrn_reflns_av_R_equivalents  0.0483
_diffrn_reflns_limit_h_min       -21
_diffrn_reflns_limit_h_max       21
_diffrn_reflns_limit_k_min       -22
_diffrn_reflns_limit_k_max       22
_diffrn_reflns_limit_l_min       -39
_diffrn_reflns_limit_l_max       32
_diffrn_reflns_theta_min         1.237
_diffrn_reflns_theta_max         24.999
_diffrn_reflns_theta_full        24.999
_diffrn_measured_fraction_theta_max 0.986
_diffrn_measured_fraction_theta_full 0.986
_diffrn_reflns_Laue_measured_fraction_max 0.986
_diffrn_reflns_Laue_measured_fraction_full 0.986
_diffrn_reflns_point_group_measured_fraction_max 0.986
_diffrn_reflns_point_group_measured_fraction_full 0.986
_reflns_number_total             38771
_reflns_number_gt                20897
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
; 
 Reflections were merged by SHELXL according to the crystal 
 class for the calculation of statistics and refinement. 
  
 _reflns_Friedel_fraction is defined as the number of unique 
 Friedel pairs measured divided by the number that would be 
 possible theoretically, ignoring centric projections and 
 systematic absences. 

Squeeze program was used to mask the electron densities of 
potential solvent molecules, which the attempt to model solvent
molecules from residual densities was unsuccessful.

# SQUEEZE RESULTS (Version =  41016)
# Note: Data are Listed for all Voids in the P1 Unit Cell
# i.e. Centre of Gravity, Solvent Accessible Volume,
# Recovered number of Electrons in the Void and
# Details about the Squeezed Material
loop_
  _platon_squeeze_void_nr
  _platon_squeeze_void_average_x
  _platon_squeeze_void_average_y
  _platon_squeeze_void_average_z
  _platon_squeeze_void_volume
  _platon_squeeze_void_count_electrons
  _platon_squeeze_void_content
   1  0.212  0.342  0.760        86        27 ' '
   2  0.494  0.596  0.527        20         9 ' '
   3  0.506  0.404  0.473        20         9 ' '
   4  0.788  0.658  0.240        88        25 ' '
_platon_squeeze_void_probe_radius                  1.20
_platon_squeeze_details                           ?


TITL 1_a.res in P-1
CELL   18.4077   18.8892   33.1600     78.10     84.05     83.28
SPGR P-1
# Solvent Accessible Volume =       216
# Electrons Found in S.A.V. =        70
# Note: Atoms in Void as Cxxx and Qxxx all others
Q101 0.702 0.722 0.257 !       6.40 eA-3
Q102 0.826 0.668 0.209 !       6.21 eA-3
Q103 0.514 0.260 0.251 !       5.99 eA-3
Q104 0.852 0.452 0.022 !       4.81 eA-3
Q105 0.894 0.456 0.243 !       4.10 eA-3
Q106 0.962 0.419 0.268 !       3.67 eA-3
Q107 0.047 0.609 0.407 !       3.59 eA-3
Q108 0.830 0.527 0.029 !       3.38 eA-3
Q109 0.146 0.856 0.398 !       2.98 eA-3
C110 0.780 0.656 0.256 !       2.83 eA-3
Q111 0.874 0.374 0.013 !       2.72 eA-3
Q112 0.112 0.642 0.367 !       2.70 eA-3
Q113 0.506 0.158 0.109 !       2.62 eA-3
Q114 0.489 0.612 0.491 !       2.44 eA-3
Q115 0.076 0.812 0.399 !       2.39 eA-3
Q116 0.253 0.616 0.434 !       2.39 eA-3
Q117 0.470 0.490 0.468 !       2.32 eA-3
Q118 0.958 0.827 0.297 !       2.30 eA-3
Q119 0.159 0.615 0.340 !       2.28 eA-3
Q120 0.416 0.501 0.493 !       2.26 eA-3
Q121 0.862 0.653 0.258 !       2.23 eA-3
Q122 0.776 0.419 0.047 !       2.19 eA-3
Q123 0.031 0.453 0.248 !       2.12 eA-3
Q124 0.062 0.578 0.366 !       2.09 eA-3
Q125 0.943 0.984 0.299 !       2.07 eA-3
Q126 0.928 0.468 0.007 !       2.06 eA-3
Q127 0.076 0.861 0.016 !       2.04 eA-3
Q128 0.535 0.577 0.475 !       2.03 eA-3
Q129 0.782 0.626 0.283 !       2.00 eA-3
Q130 0.560 0.425 0.485 !       2.00 eA-3
Q131 0.108 0.483 0.437 !       1.99 eA-3
Q132 0.369 0.612 0.366 !       1.98 eA-3
Q133 0.200 0.785 0.407 !       1.96 eA-3
Q134 0.906 0.640 0.335 !       1.96 eA-3
Q135 0.030 0.327 0.050 !       1.93 eA-3
Q136 0.946 0.090 0.038 !       1.91 eA-3
Q137 0.114 0.670 0.331 !       1.86 eA-3
Q138 0.160 1.002 0.072 !       1.85 eA-3
Q139 0.908 0.669 0.289 !       1.83 eA-3
Q140 0.624 0.717 0.217 !       1.83 eA-3
Q141 0.893 0.374 0.470 !       1.82 eA-3
Q142 0.906 0.563 0.335 !       1.81 eA-3
Q143 0.169 0.847 0.006 !       1.77 eA-3
Q144 0.879 0.419 0.073 !       1.77 eA-3
Q145 0.773 0.637 0.296 !       1.75 eA-3
Q146 0.123 0.684 0.384 !       1.75 eA-3
Q147 0.938 0.862 0.111 !       1.75 eA-3
Q148 0.091 0.533 0.012 !       1.74 eA-3
Q149 0.893 0.061 0.063 !       1.74 eA-3
Q150 0.279 0.641 0.055 !       1.73 eA-3
Q151 0.893 0.293 0.427 !       1.72 eA-3
Q152 0.966 0.140-0.002 !       1.72 eA-3
Q153 0.165 0.996 0.040 !       1.72 eA-3
Q154 0.953 0.778 0.020 !       1.71 eA-3
Q155 0.018 0.848 0.017 !       1.71 eA-3
Q156 0.937 0.560 0.439 !       1.71 eA-3
Q157 0.872 0.827 0.264 !       1.70 eA-3
Q158 0.218 0.041 0.099 !       1.69 eA-3
Q159 0.127 0.860 0.448 !       1.66 eA-3
Q160 0.834 0.127 0.023 !       1.66 eA-3
Q161 0.941 0.409 0.447 !       1.64 eA-3
Q162 0.222 0.690 0.071 !       1.63 eA-3
Q163 0.916 0.016 0.118 !       1.63 eA-3
Q164 0.980 0.027 0.008 !       1.62 eA-3
Q165 0.013 0.623 0.439 !       1.62 eA-3
Q166 0.193 0.530 0.012 !       1.62 eA-3
Q167 0.142 0.893 0.430 !       1.60 eA-3
Q168 0.220 0.907 0.227 !       1.60 eA-3
Q169 0.059 0.046 0.057 !       1.60 eA-3
Q170 0.019 0.347 0.320 !       1.59 eA-3
Q171 0.923 0.869 0.010 !       1.58 eA-3
Q172 0.958 0.612 0.461 !       1.58 eA-3
Q173 0.533 0.377 0.484 !       1.57 eA-3
Q174 0.932 0.687 0.233 !       1.57 eA-3
Q175 0.999 0.951 0.029 !       1.57 eA-3
Q176 0.019 0.581 0.345 !       1.57 eA-3
Q177 0.124 0.814 0.180 !       1.56 eA-3
Q178 0.049 0.201 0.013 !       1.56 eA-3
Q179 0.967 0.642 0.236 !       1.55 eA-3
Q180 0.527 0.530 0.459 !       1.55 eA-3
Q181 0.017 0.535 0.439 !       1.55 eA-3
Q182 0.941 0.642 0.431 !       1.55 eA-3
Q183 0.016 0.255 0.057 !       1.54 eA-3
Q184 0.049 0.572 0.482 !       1.54 eA-3
Q185 0.139 0.605 0.412 !       1.53 eA-3
Q186 0.091 0.940 0.178 !       1.53 eA-3
Q187 0.033 0.450 0.481 !       1.53 eA-3
Q188 0.979 0.611 0.374 !       1.51 eA-3
Q189 0.149 0.255 0.056 !       1.51 eA-3
Q190 0.074 0.967 0.014 !       1.51 eA-3
Q191 0.468 0.107 0.124 !       1.51 eA-3
Q192 0.249 0.064 0.071 !       1.50 eA-3
C193 0.709 0.623 0.247 !       1.50 eA-3
Q194 0.845 0.674 0.359 !       1.50 eA-3
Q195 0.452 0.425 0.477 !       1.50 eA-3
Q196 0.972 0.964 0.163 !       1.50 eA-3
Q197 0.099 1.004 0.043 !       1.49 eA-3
Q198 0.074 0.485 0.486 !       1.49 eA-3
Q199 0.885 0.096 0.033 !       1.49 eA-3

;

_computing_data_collection       'Bruker APEX2'
_computing_cell_refinement       'Bruker SAINT'
_computing_data_reduction        'Bruker SAINT'
_computing_structure_solution    'SHELXS-97 (Sheldrick 2008)'
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_refine_special_details          SQUEEZE
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.1267P)²] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_number_reflns         38771
_refine_ls_number_parameters     1567
_refine_ls_number_restraints     2007
_refine_ls_R_factor_all          0.1390
_refine_ls_R_factor_gt           0.0770
_refine_ls_wR_factor_ref         0.2383
_refine_ls_wR_factor_gt          0.2120
_refine_ls_goodness_of_fit_ref   1.034
_refine_ls_restrained_S_all      1.019
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.41757(6) 0.28850(6) 0.18499(4) 0.0412(3) Uani 1 1 d . . . . .
Ag2 Ag 0.39216(9) 0.37411(8) 0.24870(5) 0.0660(5) Uani 1 1 d . . . . .
Ag3 Ag 0.52251(7) 0.39471(7) 0.18403(4) 0.0465(3) Uani 1 1 d . . . . .
Ag4 Ag 0.56991(7) 0.25136(6) 0.16582(4) 0.0398(3) Uani 1 1 d . . . . .
Ag5 Ag 0.48297(7) 0.14506(6) 0.22086(5) 0.0456(3) Uani 1 1 d . . . . .
Ag6 Ag 0.37676(7) 0.22197(7) 0.27361(4) 0.0475(3) Uani 1 1 d . . . . .
Ag7 Ag 0.55440(8) 0.39140(8) 0.27038(5) 0.0578(4) Uani 1 1 d . . . . .
Ag8 Ag 0.65542(7) 0.31093(7) 0.21936(4) 0.0458(3) Uani 1 1 d . . . . .
Ag9 Ag 0.62861(6) 0.16125(6) 0.23879(4) 0.0407(3) Uani 1 1 d . . . . .
Ag10 Ag 0.50754(6) 0.14201(7) 0.30496(4) 0.0441(3) Uani 1 1 d . . . . .
Ag11 Ag 0.45964(7) 0.28314(7) 0.32493(4) 0.0456(3) Uani 1 1 d . . . . .
Ag12 Ag 0.61358(7) 0.24347(7) 0.30651(4) 0.0450(3) Uani 1 1 d . . . . .
Ag13 Ag 0.37226(8) 0.44790(7) 0.16191(5) 0.0511(4) Uani 1 1 d . . . . .
Ag14 Ag 0.65742(7) 0.37663(7) 0.12761(4) 0.0452(3) Uani 1 1 d . . . . .
Ag15 Ag 0.60732(8) 0.09374(7) 0.16740(5) 0.0541(4) Uani 1 1 d . . . . .
Ag16 Ag 0.32605(6) 0.16389(7) 0.20628(5) 0.0457(3) Uani 1 1 d . . . . .
Ag17 Ag 0.41965(7) 0.44177(7) 0.31947(4) 0.0453(3) Uani 1 1 d . . . . .
Ag18 Ag 0.70786(7) 0.36114(7) 0.29213(5) 0.0541(4) Uani 1 1 d . . . . .
Ag19 Ag 0.37653(7) 0.15786(7) 0.36429(5) 0.0519(4) Uani 1 1 d . . . . .
Ag20 Ag 0.66153(6) 0.08813(7) 0.32286(4) 0.0401(3) Uani 1 1 d . . . . .
C1 C 0.2467(11) 0.5869(11) 0.2073(7) 0.092(6) Uani 1 1 d D U . . .
H1A H 0.2582 0.6312 0.1870 0.110 Uiso 1 1 calc R U . . .
H1B H 0.2433 0.5484 0.1915 0.110 Uiso 1 1 calc R U . . .
C2 C 0.1719(10) 0.6026(15) 0.2289(6) 0.125(8) Uani 1 1 d D U . . .
H2A H 0.1581 0.5582 0.2485 0.151 Uiso 1 1 calc R U . . .
H2B H 0.1739 0.6409 0.2450 0.151 Uiso 1 1 calc R U . . .
C3 C 0.1150(11) 0.6268(11) 0.1988(6) 0.162(6) Uani 1 1 d DG U . . .
C4 C 0.0800(12) 0.6970(10) 0.1930(7) 0.162(6) Uani 1 1 d G U . . .
H4 H 0.0915 0.7302 0.2089 0.194 Uiso 1 1 calc R U . . .
C5 C 0.0282(11) 0.7187(8) 0.1641(7) 0.162(6) Uani 1 1 d G U . . .
H5 H 0.0043 0.7667 0.1602 0.194 Uiso 1 1 calc R U . . .
C6 C 0.0114(10) 0.6701(11) 0.1410(6) 0.162(6) Uani 1 1 d G U . . .
H6 H -0.0240 0.6849 0.1212 0.194 Uiso 1 1 calc R U . . .
C7 C 0.0464(12) 0.5999(10) 0.1468(7) 0.162(6) Uani 1 1 d G U . . .
H7 H 0.0349 0.5667 0.1309 0.194 Uiso 1 1 calc R U . . .
C8 C 0.0982(11) 0.5782(8) 0.1757(7) 0.162(6) Uani 1 1 d DG U . . .
H8 H 0.1221 0.5302 0.1796 0.194 Uiso 1 1 calc R U . . .
C9 C 0.3318(13) 0.6316(9) 0.2669(6) 0.074(6) Uani 1 1 d . U . . .
H9A H 0.2837 0.6432 0.2817 0.089 Uiso 1 1 calc R U . . .
H9B H 0.3674 0.6131 0.2879 0.089 Uiso 1 1 calc R U . . .
C10 C 0.3578(17) 0.7053(11) 0.2385(8) 0.125(8) Uani 1 1 d D U . . .
H10A H 0.3892 0.6915 0.2147 0.150 Uiso 1 1 calc R U . . .
H10B H 0.3134 0.7342 0.2273 0.150 Uiso 1 1 calc R U . . .
C11 C 0.3982(13) 0.7551(9) 0.2556(6) 0.131(8) Uani 1 1 d DG U . . .
C12 C 0.3561(10) 0.8071(11) 0.2745(7) 0.153(10) Uani 1 1 d G U . . .
H12 H 0.3044 0.8139 0.2730 0.184 Uiso 1 1 calc R U . . .
C13 C 0.3896(14) 0.8491(9) 0.2956(6) 0.157(11) Uani 1 1 d G U . . .
H13 H 0.3608 0.8846 0.3085 0.188 Uiso 1 1 calc R U . . .
C14 C 0.4652(14) 0.8391(11) 0.2978(7) 0.174(13) Uani 1 1 d G U . . .
H14 H 0.4881 0.8678 0.3122 0.209 Uiso 1 1 calc R U . . .
C15 C 0.5073(10) 0.7871(13) 0.2789(8) 0.194(17) Uani 1 1 d G U . . .
H15 H 0.5590 0.7803 0.2804 0.233 Uiso 1 1 calc R U . . .
C16 C 0.4738(13) 0.7451(11) 0.2578(7) 0.208(19) Uani 1 1 d G U . . .
H16 H 0.5026 0.7096 0.2449 0.249 Uiso 1 1 calc R U . . .
C17 C 0.2249(9) 0.3874(11) 0.0957(6) 0.058(4) Uani 1 1 d . U . . .
H17A H 0.1767 0.4158 0.0993 0.070 Uiso 1 1 calc R U . . .
H17B H 0.2626 0.4223 0.0895 0.070 Uiso 1 1 calc R U . . .
C18 C 0.2246(11) 0.3537(12) 0.0598(6) 0.071(5) Uani 1 1 d . U . . .
H18A H 0.2735 0.3270 0.0559 0.085 Uiso 1 1 calc R U . . .
H18B H 0.2194 0.3934 0.0353 0.085 Uiso 1 1 calc R U . . .
C19 C 0.1697(9) 0.3039(10) 0.0594(5) 0.091(6) Uani 1 1 d G U . . .
C20 C 0.0956(10) 0.3290(9) 0.0616(5) 0.125(8) Uani 1 1 d G U . . .
H20 H 0.0810 0.3786 0.0625 0.151 Uiso 1 1 calc R U . . .
C21 C 0.0429(7) 0.2815(13) 0.0626(6) 0.160(11) Uani 1 1 d G U . . .
H21 H -0.0077 0.2986 0.0641 0.192 Uiso 1 1 calc R U . . .
C22 C 0.0643(11) 0.2089(12) 0.0612(5) 0.144(9) Uani 1 1 d G U . . .
H22 H 0.0283 0.1764 0.0618 0.173 Uiso 1 1 calc R U . . .
C23 C 0.1384(12) 0.1838(9) 0.0590(5) 0.147(10) Uani 1 1 d G U . . .
H23 H 0.1530 0.1342 0.0580 0.177 Uiso 1 1 calc R U . . .
C24 C 0.1911(8) 0.2313(11) 0.0580(5) 0.111(7) Uani 1 1 d G U . . .
H24 H 0.2417 0.2141 0.0565 0.133 Uiso 1 1 calc R U . . .
C25 C 0.1655(8) 0.2730(10) 0.1604(6) 0.051(4) Uani 1 1 d . U . . .
H25A H 0.1568 0.2515 0.1367 0.061 Uiso 1 1 calc R U . . .
H25B H 0.1804 0.2323 0.1829 0.061 Uiso 1 1 calc R U . . .
C26 C 0.0927(9) 0.3102(12) 0.1752(6) 0.067(5) Uani 1 1 d . U . . .
H26A H 0.1010 0.3365 0.1970 0.080 Uiso 1 1 calc R U . . .
H26B H 0.0729 0.3463 0.1519 0.080 Uiso 1 1 calc R U . . .
C27 C 0.0369(6) 0.2560(7) 0.1923(4) 0.064(4) Uani 1 1 d G U . . .
C28 C -0.0194(7) 0.2490(7) 0.1689(4) 0.074(5) Uani 1 1 d G U . . .
H28 H -0.0249 0.2804 0.1428 0.089 Uiso 1 1 calc R U . . .
C29 C -0.0674(6) 0.1963(8) 0.1837(5) 0.083(6) Uani 1 1 d G U . . .
H29 H -0.1059 0.1915 0.1677 0.099 Uiso 1 1 calc R U . . .
C30 C -0.0593(7) 0.1504(8) 0.2219(5) 0.118(9) Uani 1 1 d G U . . .
H30 H -0.0921 0.1143 0.2320 0.142 Uiso 1 1 calc R U . . .
C31 C -0.0030(9) 0.1573(10) 0.2453(4) 0.150(12) Uani 1 1 d G U . . .
H31 H 0.0025 0.1260 0.2714 0.179 Uiso 1 1 calc R U . . .
C32 C 0.0450(7) 0.2101(10) 0.2305(4) 0.124(10) Uani 1 1 d G U . . .
H32 H 0.0835 0.2149 0.2465 0.149 Uiso 1 1 calc R U . . .
C33 C 0.2105(11) 0.0294(10) 0.2910(7) 0.081(5) Uani 1 1 d D U . . .
H33A H 0.1631 0.0495 0.2796 0.097 Uiso 1 1 calc R U . . .
H33B H 0.2450 0.0157 0.2682 0.097 Uiso 1 1 calc R U . . .
C34 C 0.1994(17) -0.0373(11) 0.3249(7) 0.137(8) Uani 1 1 d D U . . .
H34A H 0.1460 -0.0368 0.3233 0.164 Uiso 1 1 calc R U . A 1
H34B H 0.2209 -0.0740 0.3084 0.164 Uiso 1 1 calc R U . A 1
C35 C 0.2031(15) -0.0855(17) 0.3657(8) 0.139(6) Uani 0.5 1 d DG U P B 1
C36 C 0.2466(16) -0.1513(18) 0.3739(10) 0.139(6) Uani 0.5 1 d DG U P B 1
H36 H 0.2903 -0.1593 0.3568 0.167 Uiso 0.5 1 calc R U P B 1
C37 C 0.226(2) -0.2053(15) 0.4071(12) 0.139(6) Uani 0.5 1 d G U P B 1
H37 H 0.2559 -0.2502 0.4127 0.167 Uiso 0.5 1 calc R U P B 1
C38 C 0.162(2) -0.1935(18) 0.4320(10) 0.139(6) Uani 0.5 1 d G U P B 1
H38 H 0.1483 -0.2304 0.4547 0.167 Uiso 0.5 1 calc R U P B 1
C39 C 0.1188(19) -0.128(2) 0.4239(9) 0.139(6) Uani 0.5 1 d G U P B 1
H39 H 0.0751 -0.1196 0.4409 0.167 Uiso 0.5 1 calc R U P B 1
C40 C 0.1392(17) -0.0737(17) 0.3907(9) 0.139(6) Uani 0.5 1 d DG U P B 1
H40 H 0.1095 -0.0287 0.3851 0.167 Uiso 0.5 1 calc R U P B 1
C35B C 0.181(2) -0.1024(18) 0.3113(15) 0.139(6) Uani 0.5 1 d DG U P B 2
C36B C 0.163(2) -0.0992(16) 0.2713(13) 0.139(6) Uani 0.5 1 d G U P B 2
H36B H 0.1644 -0.0550 0.2516 0.167 Uiso 0.5 1 calc R U P B 2
C37B C 0.143(2) -0.161(2) 0.2602(10) 0.139(6) Uani 0.5 1 d G U P B 2
H37B H 0.1303 -0.1585 0.2329 0.167 Uiso 0.5 1 calc R U P B 2
C38B C 0.141(2) -0.2254(17) 0.2891(14) 0.139(6) Uani 0.5 1 d G U P B 2
H38B H 0.1269 -0.2674 0.2815 0.167 Uiso 0.5 1 calc R U P B 2
C39B C 0.159(2) -0.2286(17) 0.3291(13) 0.139(6) Uani 0.5 1 d G U P B 2
H39B H 0.1577 -0.2728 0.3488 0.167 Uiso 0.5 1 calc R U P B 2
C40B C 0.179(2) -0.167(2) 0.3402(10) 0.139(6) Uani 0.5 1 d G U P B 2
H40B H 0.1918 -0.1692 0.3676 0.167 Uiso 0.5 1 calc R U P B 2
C41 C 0.1873(10) 0.1035(11) 0.3565(6) 0.066(5) Uani 1 1 d . U . . .
H41A H 0.1918 0.0567 0.3765 0.080 Uiso 1 1 calc R U . . .
H41B H 0.2056 0.1404 0.3691 0.080 Uiso 1 1 calc R U . . .
C42 C 0.1049(10) 0.1256(11) 0.3505(6) 0.063(4) Uani 1 1 d . U . . .
H42A H 0.0995 0.1721 0.3304 0.075 Uiso 1 1 calc R U . . .
H42B H 0.0852 0.0882 0.3389 0.075 Uiso 1 1 calc R U . . .
C43 C 0.0602(8) 0.1340(8) 0.3912(4) 0.087(3) Uani 1 1 d G U . . .
C44 C 0.0577(8) 0.1984(7) 0.4056(4) 0.087(3) Uani 1 1 d G U . . .
H44 H 0.0814 0.2381 0.3895 0.104 Uiso 1 1 calc R U . . .
C45 C 0.0206(9) 0.2047(7) 0.4436(4) 0.087(3) Uani 1 1 d G U . . .
H45 H 0.0188 0.2487 0.4534 0.104 Uiso 1 1 calc R U . . .
C46 C -0.0141(8) 0.1465(8) 0.4672(3) 0.087(3) Uani 1 1 d G U . . .
H46 H -0.0395 0.1508 0.4931 0.104 Uiso 1 1 calc R U . . .
C47 C -0.0116(8) 0.0821(7) 0.4528(4) 0.087(3) Uani 1 1 d G U . . .
H47 H -0.0353 0.0424 0.4689 0.104 Uiso 1 1 calc R U . . .
C48 C 0.0255(9) 0.0758(7) 0.4148(4) 0.087(3) Uani 1 1 d G U . . .
H48 H 0.0273 0.0318 0.4050 0.104 Uiso 1 1 calc R U . . .
C49 C 0.3158(11) 0.2695(11) 0.4548(6) 0.087(6) Uani 1 1 d D U . . .
H49A H 0.2654 0.2546 0.4614 0.104 Uiso 1 1 calc R U . . .
H49B H 0.3498 0.2249 0.4549 0.104 Uiso 1 1 calc R U . . .
C50 C 0.3339(11) 0.3066(13) 0.4887(5) 0.107(5) Uani 1 1 d D U . . .
H50A H 0.3781 0.3310 0.4765 0.129 Uiso 1 1 calc R U . C 1
H50B H 0.2938 0.3463 0.4891 0.129 Uiso 1 1 calc R U . C 1
C51 C 0.3478(17) 0.2818(16) 0.5334(6) 0.093(4) Uani 0.5 1 d DG U P D 1
C52 C 0.2979(14) 0.2321(17) 0.5513(9) 0.093(4) Uani 0.5 1 d G U P D 1
H52 H 0.2600 0.2240 0.5360 0.112 Uiso 0.5 1 calc R U P D 1
C53 C 0.3037(15) 0.1944(14) 0.5917(9) 0.093(4) Uani 0.5 1 d G U P D 1
H53 H 0.2696 0.1605 0.6040 0.112 Uiso 0.5 1 calc R U P D 1
C54 C 0.3593(17) 0.2062(15) 0.6142(6) 0.093(4) Uani 0.5 1 d G U P D 1
H54 H 0.3632 0.1804 0.6418 0.112 Uiso 0.5 1 calc R U P D 1
C55 C 0.4091(14) 0.2559(16) 0.5962(8) 0.093(4) Uani 0.5 1 d G U P D 1
H55 H 0.4471 0.2640 0.6116 0.112 Uiso 0.5 1 calc R U P D 1
C56 C 0.4034(15) 0.2936(14) 0.5558(8) 0.093(4) Uani 0.5 1 d G U P D 1
H56 H 0.4374 0.3275 0.5436 0.112 Uiso 0.5 1 calc R U P D 1
C51B C 0.2585(13) 0.3300(16) 0.5067(9) 0.093(4) Uani 0.5 1 d DG U P D 2
C52B C 0.2650(13) 0.4006(17) 0.5111(9) 0.093(4) Uani 0.5 1 d G U P D 2
H52B H 0.3091 0.4223 0.5013 0.112 Uiso 0.5 1 calc R U P D 2
C53B C 0.2068(17) 0.4394(13) 0.5297(9) 0.093(4) Uani 0.5 1 d G U P D 2
H53B H 0.2112 0.4876 0.5327 0.112 Uiso 0.5 1 calc R U P D 2
C54B C 0.1421(14) 0.4076(16) 0.5439(9) 0.093(4) Uani 0.5 1 d G U P D 2
H54B H 0.1024 0.4341 0.5567 0.112 Uiso 0.5 1 calc R U P D 2
C55B C 0.1357(12) 0.3370(17) 0.5395(9) 0.093(4) Uani 0.5 1 d G U P D 2
H55B H 0.0915 0.3153 0.5493 0.112 Uiso 0.5 1 calc R U P D 2
C56B C 0.1939(15) 0.2983(13) 0.5209(9) 0.093(4) Uani 0.5 1 d G U P D 2
H56B H 0.1895 0.2500 0.5179 0.112 Uiso 0.5 1 calc R U P D 2
C57 C 0.2716(10) 0.4136(11) 0.4035(7) 0.072(5) Uani 1 1 d . U . . .
H57A H 0.2866 0.4341 0.4261 0.087 Uiso 1 1 calc R U . . .
H57B H 0.2830 0.4472 0.3770 0.087 Uiso 1 1 calc R U . . .
C58 C 0.1828(10) 0.4058(10) 0.4101(5) 0.073(4) Uani 1 1 d D U . . .
H58A H 0.1562 0.4517 0.3964 0.088 Uiso 1 1 calc R U . E 1
H58B H 0.1719 0.3664 0.3967 0.088 Uiso 1 1 calc R U . E 1
C59 C 0.1558(12) 0.3897(10) 0.4544(5) 0.067(3) Uani 0.5 1 d DG U P F 1
C60 C 0.1526(12) 0.4315(10) 0.4846(6) 0.067(3) Uani 0.5 1 d G U P F 1
H60 H 0.1693 0.4785 0.4779 0.081 Uiso 0.5 1 calc R U P F 1
C61 C 0.1250(13) 0.4043(13) 0.5248(6) 0.067(3) Uani 0.5 1 d G U P F 1
H61 H 0.1228 0.4329 0.5454 0.081 Uiso 0.5 1 calc R U P F 1
C62 C 0.1006(13) 0.3355(13) 0.5347(5) 0.067(3) Uani 0.5 1 d G U P F 1
H62 H 0.0817 0.3169 0.5621 0.081 Uiso 0.5 1 calc R U P F 1
C63 C 0.1038(12) 0.2937(10) 0.5045(6) 0.067(3) Uani 0.5 1 d G U P F 1
H63 H 0.0871 0.2466 0.5113 0.081 Uiso 0.5 1 calc R U P F 1
C64 C 0.1314(12) 0.3209(9) 0.4643(6) 0.067(3) Uani 0.5 1 d DG U P F 1
H64 H 0.1336 0.2923 0.4437 0.081 Uiso 0.5 1 calc R U P F 1
C59B C 0.1313(14) 0.4768(9) 0.3998(8) 0.067(3) Uani 0.5 1 d G U P F 2
C60B C 0.1311(13) 0.5154(12) 0.3593(7) 0.067(3) Uani 0.5 1 d G U P F 2
H60B H 0.1519 0.4926 0.3371 0.081 Uiso 0.5 1 calc R U P F 2
C61B C 0.1006(14) 0.5872(12) 0.3511(6) 0.067(3) Uani 0.5 1 d G U P F 2
H61B H 0.1006 0.6136 0.3234 0.081 Uiso 0.5 1 calc R U P F 2
C62B C 0.0703(13) 0.6205(9) 0.3835(8) 0.067(3) Uani 0.5 1 d G U P F 2
H62B H 0.0494 0.6696 0.3779 0.081 Uiso 0.5 1 calc R U P F 2
C63B C 0.0704(13) 0.5820(12) 0.4240(7) 0.067(3) Uani 0.5 1 d G U P F 2
H63B H 0.0496 0.6047 0.4461 0.081 Uiso 0.5 1 calc R U P F 2
C64B C 0.1009(14) 0.5101(12) 0.4321(6) 0.067(3) Uani 0.5 1 d G U P F 2
H64B H 0.1010 0.4838 0.4598 0.081 Uiso 0.5 1 calc R U P F 2
C65 C 0.4610(10) 0.6026(9) 0.0851(5) 0.051(4) Uani 1 1 d . U . . .
H65A H 0.4324 0.6003 0.1123 0.061 Uiso 1 1 calc R U . . .
H65B H 0.4941 0.6414 0.0819 0.061 Uiso 1 1 calc R U . . .
C66 C 0.4091(11) 0.6230(12) 0.0520(6) 0.072(5) Uani 1 1 d . U . . .
H66A H 0.4344 0.6473 0.0258 0.086 Uiso 1 1 calc R U . . .
H66B H 0.3895 0.5792 0.0470 0.086 Uiso 1 1 calc R U . . .
C67 C 0.3489(10) 0.6731(11) 0.0665(6) 0.137(5) Uani 1 1 d G U . . .
C68 C 0.3637(8) 0.7407(12) 0.0722(7) 0.137(5) Uani 1 1 d G U . . .
H68 H 0.4114 0.7561 0.0648 0.165 Uiso 1 1 calc R U . . .
C69 C 0.3086(11) 0.7858(9) 0.0888(7) 0.137(5) Uani 1 1 d G U . . .
H69 H 0.3187 0.8320 0.0928 0.165 Uiso 1 1 calc R U . . .
C70 C 0.2388(9) 0.7634(11) 0.0997(6) 0.137(5) Uani 1 1 d G U . . .
H70 H 0.2011 0.7942 0.1111 0.165 Uiso 1 1 calc R U . . .
C71 C 0.2240(8) 0.6958(12) 0.0940(6) 0.137(5) Uani 1 1 d G U . . .
H71 H 0.1762 0.6804 0.1014 0.165 Uiso 1 1 calc R U . . .
C72 C 0.2790(11) 0.6507(9) 0.0774(6) 0.137(5) Uani 1 1 d G U . . .
H72 H 0.2689 0.6045 0.0735 0.165 Uiso 1 1 calc R U . . .
C73 C 0.5743(11) 0.5124(11) 0.0365(6) 0.066(5) Uani 1 1 d . U . . .
H73A H 0.5962 0.4618 0.0368 0.080 Uiso 1 1 calc R U . . .
H73B H 0.5421 0.5259 0.0134 0.080 Uiso 1 1 calc R U . . .
C74 C 0.6342(11) 0.5608(10) 0.0280(6) 0.066(4) Uani 1 1 d . U . . .
H74A H 0.6656 0.5457 0.0514 0.079 Uiso 1 1 calc R U . . .
H74B H 0.6642 0.5492 0.0032 0.079 Uiso 1 1 calc R U . . .
C75 C 0.6208(7) 0.6405(5) 0.0212(4) 0.054(4) Uani 1 1 d G U . . .
C76 C 0.5777(7) 0.6754(7) -0.0105(4) 0.059(4) Uani 1 1 d G U . . .
H76 H 0.5609 0.6482 -0.0282 0.070 Uiso 1 1 calc R U . . .
C77 C 0.5590(7) 0.7501(7) -0.0162(4) 0.082(6) Uani 1 1 d G U . . .
H77 H 0.5296 0.7739 -0.0379 0.098 Uiso 1 1 calc R U . . .
C78 C 0.5835(8) 0.7899(5) 0.0097(5) 0.100(7) Uani 1 1 d G U . . .
H78 H 0.5707 0.8409 0.0058 0.120 Uiso 1 1 calc R U . . .
C79 C 0.6266(8) 0.7550(8) 0.0414(5) 0.104(7) Uani 1 1 d G U . . .
H79 H 0.6433 0.7822 0.0591 0.125 Uiso 1 1 calc R U . . .
C80 C 0.6452(7) 0.6803(8) 0.0472(4) 0.080(6) Uani 1 1 d G U . . .
H80 H 0.6747 0.6565 0.0688 0.096 Uiso 1 1 calc R U . . .
C81 C 0.4782(14) -0.0684(13) 0.1680(8) 0.115(8) Uani 1 1 d D U . . .
H81A H 0.5228 -0.0700 0.1826 0.138 Uiso 1 1 calc R U . . .
H81B H 0.4441 -0.1000 0.1864 0.138 Uiso 1 1 calc R U . . .
C82 C 0.4991(18) -0.0981(10) 0.1290(8) 0.153(9) Uani 1 1 d D U . . .
H82A H 0.4542 -0.0979 0.1150 0.184 Uiso 1 1 calc R U . . .
H82B H 0.5316 -0.0653 0.1102 0.184 Uiso 1 1 calc R U . . .
C83 C 0.5364(10) -0.1717(8) 0.1360(7) 0.148(5) Uani 1 1 d DG U . . .
C84 C 0.5055(8) -0.2375(10) 0.1457(7) 0.148(5) Uani 1 1 d G U . . .
H84 H 0.4542 -0.2382 0.1445 0.177 Uiso 1 1 calc R U . . .
C85 C 0.5495(10) -0.3021(8) 0.1571(7) 0.148(5) Uani 1 1 d G U . . .
H85 H 0.5284 -0.3470 0.1637 0.177 Uiso 1 1 calc R U . . .
C86 C 0.6245(10) -0.3010(8) 0.1588(7) 0.148(5) Uani 1 1 d G U . . .
H86 H 0.6546 -0.3452 0.1666 0.177 Uiso 1 1 calc R U . . .
C87 C 0.6554(8) -0.2353(10) 0.1491(7) 0.148(5) Uani 1 1 d G U . . .
H87 H 0.7067 -0.2345 0.1502 0.177 Uiso 1 1 calc R U . . .
C88 C 0.6114(11) -0.1706(8) 0.1377(7) 0.148(5) Uani 1 1 d G U . . .
H88 H 0.6325 -0.1257 0.1310 0.177 Uiso 1 1 calc R U . . .
C89 C 0.3457(14) 0.0229(16) 0.1329(9) 0.135(9) Uani 1 1 d D U . . .
H89A H 0.3216 0.0730 0.1253 0.162 Uiso 1 1 calc R U . . .
H89B H 0.3579 0.0035 0.1072 0.162 Uiso 1 1 calc R U . . .
C90 C 0.2925(10) -0.0246(19) 0.1621(10) 0.170(9) Uani 1 1 d D U . . .
H90A H 0.3125 -0.0758 0.1629 0.204 Uiso 1 1 calc R U . . .
H90B H 0.2948 -0.0149 0.1901 0.204 Uiso 1 1 calc R U . . .
C91 C 0.2146(10) -0.0198(16) 0.1550(9) 0.205(8) Uani 1 1 d DG U . . .
C92 C 0.1722(14) 0.0451(14) 0.1579(9) 0.205(8) Uani 1 1 d G U . . .
H92 H 0.1916 0.0812 0.1687 0.245 Uiso 1 1 calc R U . . .
C93 C 0.1015(13) 0.0573(12) 0.1451(9) 0.205(8) Uani 1 1 d G U . . .
H93 H 0.0726 0.1017 0.1471 0.245 Uiso 1 1 calc R U . . .
C94 C 0.0732(10) 0.0045(16) 0.1294(9) 0.205(8) Uani 1 1 d G U . . .
H94 H 0.0249 0.0128 0.1206 0.245 Uiso 1 1 calc R U . . .
C95 C 0.1156(14) -0.0604(14) 0.1264(9) 0.205(8) Uani 1 1 d G U . . .
H95 H 0.0962 -0.0965 0.1156 0.245 Uiso 1 1 calc R U . . .
C96 C 0.1863(13) -0.0726(12) 0.1392(9) 0.205(8) Uani 1 1 d G U . . .
H96 H 0.2153 -0.1170 0.1372 0.245 Uiso 1 1 calc R U . . .
C97 C 0.4558(9) -0.0395(9) 0.4264(6) 0.048(4) Uani 1 1 d . U . . .
H97A H 0.4475 -0.0366 0.4560 0.057 Uiso 1 1 calc R U . . .
H97B H 0.4089 -0.0227 0.4136 0.057 Uiso 1 1 calc R U . . .
C98 C 0.4782(12) -0.1192(9) 0.4227(6) 0.067(5) Uani 1 1 d . U . . .
H98A H 0.4694 -0.1261 0.3949 0.081 Uiso 1 1 calc R U . . .
H98B H 0.5311 -0.1317 0.4265 0.081 Uiso 1 1 calc R U . . .
C99 C 0.4346(8) -0.1667(7) 0.4545(4) 0.064(5) Uani 1 1 d G U . . .
C100 C 0.4562(6) -0.1896(7) 0.4944(4) 0.062(5) Uani 1 1 d G U . . .
H100 H 0.4983 -0.1723 0.5020 0.075 Uiso 1 1 calc R U . . .
C101 C 0.4163(8) -0.2377(8) 0.5233(3) 0.081(6) Uani 1 1 d G U . . .
H101 H 0.4311 -0.2533 0.5506 0.098 Uiso 1 1 calc R U . . .
C102 C 0.3547(8) -0.2629(8) 0.5122(5) 0.108(9) Uani 1 1 d G U . . .
H102 H 0.3275 -0.2958 0.5319 0.130 Uiso 1 1 calc R U . . .
C103 C 0.3331(8) -0.2401(10) 0.4723(5) 0.146(14) Uani 1 1 d G U . . .
H103 H 0.2910 -0.2573 0.4647 0.176 Uiso 1 1 calc R U . . .
C104 C 0.3730(9) -0.1920(10) 0.4434(4) 0.149(15) Uani 1 1 d G U . . .
H104 H 0.3582 -0.1763 0.4161 0.178 Uiso 1 1 calc R U . . .
C105 C 0.6087(8) -0.0063(8) 0.4276(5) 0.038(3) Uani 1 1 d . U . . .
H10C H 0.6248 -0.0576 0.4260 0.046 Uiso 1 1 calc R U . . .
H10D H 0.6478 0.0235 0.4130 0.046 Uiso 1 1 calc R U . . .
C106 C 0.5999(9) 0.0006(10) 0.4733(5) 0.047(4) Uani 1 1 d . U . . .
H10E H 0.5765 0.0495 0.4759 0.056 Uiso 1 1 calc R U . . .
H10F H 0.5681 -0.0359 0.4895 0.056 Uiso 1 1 calc R U . . .
C107 C 0.6741(6) -0.0115(8) 0.4897(4) 0.058(4) Uani 1 1 d G U . . .
C108 C 0.7093(7) 0.0497(6) 0.4897(5) 0.088(7) Uani 1 1 d G U . . .
H108 H 0.6874 0.0966 0.4784 0.105 Uiso 1 1 calc R U . . .
C109 C 0.7767(8) 0.0421(8) 0.5064(5) 0.103(8) Uani 1 1 d G U . . .
H109 H 0.8008 0.0839 0.5064 0.124 Uiso 1 1 calc R U . . .
C110 C 0.8089(6) -0.0266(9) 0.5230(4) 0.086(6) Uani 1 1 d G U . . .
H110 H 0.8549 -0.0318 0.5344 0.104 Uiso 1 1 calc R U . . .
C111 C 0.7737(8) -0.0878(7) 0.5229(5) 0.105(8) Uani 1 1 d G U . . .
H111 H 0.7956 -0.1348 0.5343 0.126 Uiso 1 1 calc R U . . .
C112 C 0.7063(8) -0.0802(6) 0.5063(5) 0.098(8) Uani 1 1 d G U . . .
H112 H 0.6822 -0.1221 0.5062 0.118 Uiso 1 1 calc R U . . .
C113 C 0.5320(12) 0.5128(12) 0.3903(7) 0.088(6) Uani 1 1 d D U . . .
H11A H 0.4954 0.4768 0.3981 0.105 Uiso 1 1 calc R U . . .
H11B H 0.5641 0.5051 0.4132 0.105 Uiso 1 1 calc R U . . .
C114 C 0.4910(11) 0.5879(12) 0.3872(10) 0.146(9) Uani 1 1 d D U . . .
H11C H 0.5181 0.6179 0.4006 0.175 Uiso 1 1 calc R U . . .
H11D H 0.4890 0.6115 0.3578 0.175 Uiso 1 1 calc R U . . .
C115 C 0.4156(9) 0.5854(13) 0.4072(9) 0.174(7) Uani 1 1 d DG U . . .
C116 C 0.3555(15) 0.6047(13) 0.3836(6) 0.174(7) Uani 1 1 d DG U . . .
H116 H 0.3627 0.6139 0.3542 0.209 Uiso 1 1 calc R U . . .
C117 C 0.2850(11) 0.6106(13) 0.4029(8) 0.174(7) Uani 1 1 d G U . . .
H117 H 0.2440 0.6238 0.3868 0.209 Uiso 1 1 calc R U . . .
C118 C 0.2745(9) 0.5972(13) 0.4458(9) 0.174(7) Uani 1 1 d G U . . .
H118 H 0.2263 0.6012 0.4590 0.209 Uiso 1 1 calc R U . . .
C119 C 0.3345(15) 0.5778(13) 0.4694(6) 0.174(7) Uani 1 1 d G U . . .
H119 H 0.3273 0.5687 0.4987 0.209 Uiso 1 1 calc R U . . .
C120 C 0.4050(11) 0.5720(13) 0.4501(9) 0.174(7) Uani 1 1 d G U . . .
H120 H 0.4460 0.5587 0.4662 0.209 Uiso 1 1 calc R U . . .
C121 C 0.6696(13) 0.5444(14) 0.3339(8) 0.108(7) Uani 1 1 d D U . . .
H12A H 0.6946 0.5389 0.3066 0.129 Uiso 1 1 calc R U . . .
H12B H 0.6508 0.5963 0.3316 0.129 Uiso 1 1 calc R U . . .
C122 C 0.7274(16) 0.527(2) 0.3653(11) 0.204(11) Uani 1 1 d D U . . .
H12C H 0.7016 0.5318 0.3925 0.245 Uiso 1 1 calc R U . . .
H12D H 0.7461 0.4755 0.3672 0.245 Uiso 1 1 calc R U . . .
C123 C 0.7922(17) 0.5690(17) 0.3598(10) 0.225(8) Uani 1 1 d DG U . . .
C124 C 0.8567(19) 0.5582(10) 0.3351(10) 0.225(8) Uani 1 1 d G U . . .
H124 H 0.8686 0.5135 0.3259 0.270 Uiso 1 1 calc R U . . .
C125 C 0.9038(13) 0.6126(13) 0.3239(7) 0.225(8) Uani 1 1 d DG U . . .
H125 H 0.9478 0.6052 0.3070 0.270 Uiso 1 1 calc R U . . .
C126 C 0.8864(14) 0.6780(11) 0.3374(8) 0.225(8) Uani 1 1 d G U . . .
H126 H 0.9185 0.7152 0.3297 0.270 Uiso 1 1 calc R U . . .
C127 C 0.8219(16) 0.6889(15) 0.3621(8) 0.225(8) Uani 1 1 d G U . . .
H127 H 0.8100 0.7336 0.3713 0.270 Uiso 1 1 calc R U . . .
C128 C 0.7748(12) 0.634(2) 0.3733(8) 0.225(8) Uani 1 1 d DG U . . .
H128 H 0.7308 0.6419 0.3902 0.270 Uiso 1 1 calc R U . . .
C129 C 0.8770(9) 0.4103(11) 0.2130(6) 0.075(5) Uani 1 1 d D U . . .
H12E H 0.9029 0.3678 0.2026 0.090 Uiso 1 1 calc R U . . .
H12F H 0.9062 0.4518 0.2017 0.090 Uiso 1 1 calc R U . . .
C130 C 0.8805(14) 0.3940(14) 0.2596(7) 0.208(10) Uani 1 1 d D U . . .
H13A H 0.8432 0.4290 0.2704 0.249 Uiso 1 1 calc R U . . .
H13B H 0.8629 0.3454 0.2696 0.249 Uiso 1 1 calc R U . . .
C131 C 0.9484(12) 0.3936(10) 0.2816(7) 0.222(8) Uani 1 1 d DG U . . .
C132 C 1.0064(14) 0.3403(10) 0.2905(9) 0.222(8) Uani 1 1 d DG U . . .
H132 H 0.9994 0.2905 0.2930 0.267 Uiso 1 1 calc R U . . .
C133 C 1.0748(12) 0.3599(13) 0.2958(7) 0.222(8) Uani 1 1 d G U . . .
H133 H 1.1144 0.3235 0.3020 0.267 Uiso 1 1 calc R U . . .
C134 C 1.0851(11) 0.4327(14) 0.2922(7) 0.222(8) Uani 1 1 d G U . . .
H134 H 1.1318 0.4461 0.2959 0.267 Uiso 1 1 calc R U . . .
C135 C 1.0271(12) 0.4860(12) 0.2832(8) 0.222(8) Uani 1 1 d G U . . .
H135 H 1.0342 0.5358 0.2808 0.267 Uiso 1 1 calc R U . . .
C136 C 0.9588(10) 0.4664(10) 0.2779(6) 0.222(8) Uani 1 1 d DG U . . .
H136 H 0.9191 0.5029 0.2718 0.267 Uiso 1 1 calc R U . . .
C137 C 0.8059(10) 0.5085(9) 0.1464(6) 0.061(4) Uani 1 1 d D U . . .
H13C H 0.7634 0.5193 0.1294 0.073 Uiso 1 1 calc R U . G 1
H13D H 0.8125 0.5526 0.1569 0.073 Uiso 1 1 calc R U . G 1
C138 C 0.875(2) 0.485(2) 0.1212(13) 0.076(11) Uani 0.5 1 d D U P H 1
H13E H 0.8678 0.4461 0.1065 0.091 Uiso 0.5 1 calc R U P H 1
H13F H 0.9179 0.4711 0.1377 0.091 Uiso 0.5 1 calc R U P H 1
C139 C 0.8770(14) 0.5638(12) 0.0911(8) 0.052(6) Uani 0.5 1 d G U P H 1
C140 C 0.9442(12) 0.5700(13) 0.0679(9) 0.069(9) Uani 0.5 1 d G U P H 1
H140 H 0.9794 0.5288 0.0688 0.083 Uiso 0.5 1 calc R U P H 1
C141 C 0.9597(13) 0.6364(16) 0.0433(9) 0.086(13) Uani 0.5 1 d G U P H 1
H141 H 1.0056 0.6406 0.0275 0.103 Uiso 0.5 1 calc R U P H 1
C142 C 0.9082(17) 0.6966(13) 0.0420(11) 0.104(19) Uani 0.5 1 d G U P H 1
H142 H 0.9188 0.7420 0.0252 0.124 Uiso 0.5 1 calc R U P H 1
C143 C 0.8411(16) 0.6905(13) 0.0652(13) 0.12(3) Uani 0.5 1 d G U P H 1
H143 H 0.8058 0.7316 0.0643 0.149 Uiso 0.5 1 calc R U P H 1
C144 C 0.8255(13) 0.6241(16) 0.0897(11) 0.12(2) Uani 0.5 1 d G U P H 1
H144 H 0.7796 0.6199 0.1056 0.139 Uiso 0.5 1 calc R U P H 1
C1D8 C 0.819(2) 0.5815(13) 0.1556(8) 0.063(9) Uani 0.5 1 d D U P H 2
H1D1 H 0.7805 0.5939 0.1768 0.076 Uiso 0.5 1 calc R U P H 2
H1D2 H 0.8666 0.5750 0.1683 0.076 Uiso 0.5 1 calc R U P H 2
C1D9 C 0.8213(18) 0.6444(11) 0.1211(6) 0.073(10) Uani 0.5 1 d DG U P H 2
C1E0 C 0.8567(19) 0.6372(10) 0.0828(7) 0.070(11) Uani 0.5 1 d G U P H 2
H1E0 H 0.8762 0.5906 0.0780 0.084 Uiso 0.5 1 calc R U P H 2
C1E1 C 0.8634(18) 0.6983(14) 0.0516(6) 0.068(11) Uani 0.5 1 d G U P H 2
H1E1 H 0.8876 0.6934 0.0254 0.081 Uiso 0.5 1 calc R U P H 2
C1E2 C 0.8348(19) 0.7665(11) 0.0586(7) 0.103(17) Uani 0.5 1 d G U P H 2
H1E2 H 0.8394 0.8082 0.0373 0.123 Uiso 0.5 1 calc R U P H 2
C1E3 C 0.7994(17) 0.7736(10) 0.0969(8) 0.087(13) Uani 0.5 1 d G U P H 2
H1E3 H 0.7798 0.8203 0.1017 0.105 Uiso 0.5 1 calc R U P H 2
C1E4 C 0.7926(15) 0.7126(14) 0.1281(6) 0.068(9) Uani 0.5 1 d G U P H 2
H1E4 H 0.7684 0.7175 0.1543 0.081 Uiso 0.5 1 calc R U P H 2
C145 C 0.7826(9) 0.2665(9) 0.0617(6) 0.058(4) Uani 1 1 d D U . . .
H14A H 0.7796 0.2810 0.0314 0.070 Uiso 1 1 calc R U . I 1
H14B H 0.7835 0.3107 0.0731 0.070 Uiso 1 1 calc R U . I 1
C146 C 0.8515(15) 0.2140(16) 0.0715(8) 0.064(6) Uani 0.5 1 d D U P J 1
H14C H 0.8923 0.2422 0.0740 0.077 Uiso 0.5 1 calc R U P J 1
H14D H 0.8418 0.1810 0.0984 0.077 Uiso 0.5 1 calc R U P J 1
C147 C 0.8736(13) 0.1705(12) 0.0395(7) 0.063(3) Uani 0.5 1 d DG U P J 1
C148 C 0.8948(13) 0.2072(9) 0.0000(8) 0.063(3) Uani 0.5 1 d G U P J 1
H148 H 0.8882 0.2588 -0.0065 0.075 Uiso 0.5 1 calc R U P J 1
C149 C 0.9255(13) 0.1684(12) -0.0300(6) 0.063(3) Uani 0.5 1 d G U P J 1
H149 H 0.9399 0.1935 -0.0570 0.075 Uiso 0.5 1 calc R U P J 1
C150 C 0.9351(13) 0.0929(12) -0.0204(7) 0.063(3) Uani 0.5 1 d G U P J 1
H150 H 0.9560 0.0664 -0.0409 0.075 Uiso 0.5 1 calc R U P J 1
C151 C 0.9139(13) 0.0562(9) 0.0191(8) 0.063(3) Uani 0.5 1 d G U P J 1
H151 H 0.9205 0.0046 0.0256 0.075 Uiso 0.5 1 calc R U P J 1
C152 C 0.8832(13) 0.0950(12) 0.0491(6) 0.063(3) Uani 0.5 1 d G U P J 1
H152 H 0.8688 0.0699 0.0761 0.075 Uiso 0.5 1 calc R U P J 1
C1E6 C 0.7790(17) 0.3227(17) 0.0207(9) 0.067(7) Uani 0.5 1 d D U P J 2
H1E5 H 0.7794 0.2948 -0.0016 0.081 Uiso 0.5 1 calc R U P J 2
H1E6 H 0.7301 0.3508 0.0219 0.081 Uiso 0.5 1 calc R U P J 2
C1E7 C 0.8333(11) 0.3767(12) 0.0063(8) 0.063(3) Uani 0.5 1 d DG U P J 2
C1E8 C 0.8777(13) 0.3534(10) -0.0259(8) 0.063(3) Uani 0.5 1 d G U P J 2
H1E8 H 0.8698 0.3097 -0.0341 0.075 Uiso 0.5 1 calc R U P J 2
C1E9 C 0.9338(12) 0.3939(13) -0.0462(7) 0.063(3) Uani 0.5 1 d G U P J 2
H1E9 H 0.9642 0.3780 -0.0682 0.075 Uiso 0.5 1 calc R U P J 2
C1F0 C 0.9454(11) 0.4578(12) -0.0342(7) 0.063(3) Uani 0.5 1 d G U P J 2
H1F0 H 0.9837 0.4855 -0.0481 0.075 Uiso 0.5 1 calc R U P J 2
C1F1 C 0.9009(13) 0.4811(10) -0.0020(8) 0.063(3) Uani 0.5 1 d G U P J 2
H1F1 H 0.9088 0.5248 0.0061 0.075 Uiso 0.5 1 calc R U P J 2
C1F2 C 0.8448(12) 0.4406(12) 0.0182(7) 0.063(3) Uani 0.5 1 d G U P J 2
H1F2 H 0.8144 0.4565 0.0402 0.075 Uiso 0.5 1 calc R U P J 2
C153 C 0.6929(12) 0.1500(11) 0.0562(7) 0.075(5) Uani 1 1 d D U . . .
H15A H 0.7414 0.1214 0.0551 0.091 Uiso 1 1 calc R U . K 1
H15B H 0.6591 0.1167 0.0735 0.091 Uiso 1 1 calc R U . K 1
C154 C 0.668(3) 0.1622(13) 0.0126(9) 0.085(8) Uani 0.5 1 d D U P L 1
H15C H 0.6192 0.1898 0.0120 0.102 Uiso 0.5 1 calc R U P L 1
H15D H 0.7027 0.1925 -0.0065 0.102 Uiso 0.5 1 calc R U P L 1
C155 C 0.665(2) 0.0950(15) -0.0028(12) 0.116(5) Uani 0.5 1 d DG U P L 1
C156 C 0.6057(17) 0.0534(18) 0.0076(11) 0.116(5) Uani 0.5 1 d DG U P L 1
H156 H 0.5653 0.0679 0.0254 0.139 Uiso 0.5 1 calc R U P L 1
C157 C 0.6056(17) -0.0095(17) -0.0080(12) 0.116(5) Uani 0.5 1 d G U P L 1
H157 H 0.5652 -0.0380 -0.0009 0.139 Uiso 0.5 1 calc R U P L 1
C158 C 0.665(2) -0.0308(15) -0.0340(11) 0.116(5) Uani 0.5 1 d G U P L 1
H158 H 0.6645 -0.0738 -0.0447 0.139 Uiso 0.5 1 calc R U P L 1
C159 C 0.7237(17) 0.0108(18) -0.0445(10) 0.116(5) Uani 0.5 1 d G U P L 1
H159 H 0.7640 -0.0037 -0.0622 0.139 Uiso 0.5 1 calc R U P L 1
C160 C 0.7238(18) 0.0737(17) -0.0289(12) 0.116(5) Uani 0.5 1 d DG U P L 1
H160 H 0.7642 0.1022 -0.0360 0.139 Uiso 0.5 1 calc R U P L 1
C1F4 C 0.7649(16) 0.1018(18) 0.0503(18) 0.107(10) Uani 0.5 1 d D U P L 2
H1F3 H 0.7967 0.1309 0.0288 0.128 Uiso 0.5 1 calc R U P L 2
H1F4 H 0.7891 0.0939 0.0764 0.128 Uiso 0.5 1 calc R U P L 2
C1F5 C 0.766(2) 0.0304(16) 0.0391(11) 0.116(5) Uani 0.5 1 d DG U P L 2
C1F6 C 0.7207(19) -0.0230(18) 0.0578(9) 0.116(5) Uani 0.5 1 d DG U P L 2
H1F6 H 0.6957 -0.0212 0.0841 0.139 Uiso 0.5 1 calc R U P L 2
C1F7 C 0.7118(18) -0.0789(16) 0.0378(11) 0.116(5) Uani 0.5 1 d G U P L 2
H1F7 H 0.6807 -0.1154 0.0505 0.139 Uiso 0.5 1 calc R U P L 2
C1F8 C 0.748(2) -0.0815(16) -0.0008(11) 0.116(5) Uani 0.5 1 d G U P L 2
H1F8 H 0.7424 -0.1197 -0.0144 0.139 Uiso 0.5 1 calc R U P L 2
C1F9 C 0.7939(19) -0.0281(19) -0.0194(9) 0.116(5) Uani 0.5 1 d G U P L 2
H1F9 H 0.8190 -0.0299 -0.0458 0.139 Uiso 0.5 1 calc R U P L 2
C1G0 C 0.8028(18) 0.0278(16) 0.0006(12) 0.116(5) Uani 0.5 1 d G U P L 2
H1G0 H 0.8339 0.0643 -0.0122 0.139 Uiso 0.5 1 calc R U P L 2
C161 C 0.7717(10) -0.0383(10) 0.1979(6) 0.056(4) Uani 1 1 d D U . . .
H16A H 0.7669 0.0052 0.1755 0.068 Uiso 1 1 calc R U . M 1
H16B H 0.8240 -0.0475 0.2038 0.068 Uiso 1 1 calc R U . M 1
C162 C 0.7508(19) -0.1025(16) 0.1826(8) 0.069(5) Uani 0.5 1 d D U P N 1
H16C H 0.7661 -0.1479 0.2020 0.082 Uiso 0.5 1 calc R U P N 1
H16D H 0.6967 -0.0989 0.1823 0.082 Uiso 0.5 1 calc R U P N 1
C163 C 0.7849(19) -0.1064(19) 0.1408(7) 0.098(4) Uani 0.5 1 d DG U P N 1
C164 C 0.8482(18) -0.1516(17) 0.1338(8) 0.098(4) Uani 0.5 1 d DG U P N 1
H164 H 0.8717 -0.1810 0.1565 0.118 Uiso 0.5 1 calc R U P N 1
C165 C 0.8770(15) -0.1537(17) 0.0936(10) 0.098(4) Uani 0.5 1 d G U P N 1
H165 H 0.9202 -0.1846 0.0888 0.118 Uiso 0.5 1 calc R U P N 1
C166 C 0.8426(18) -0.1107(18) 0.0604(7) 0.098(4) Uani 0.5 1 d G U P N 1
H166 H 0.8623 -0.1121 0.0329 0.118 Uiso 0.5 1 calc R U P N 1
C167 C 0.7793(18) -0.0654(17) 0.0674(8) 0.098(4) Uani 0.5 1 d G U P N 1
H167 H 0.7558 -0.0360 0.0447 0.118 Uiso 0.5 1 calc R U P N 1
C168 C 0.7505(15) -0.0633(17) 0.1076(10) 0.098(4) Uani 0.5 1 d DG U P N 1
H168 H 0.7073 -0.0324 0.1124 0.118 Uiso 0.5 1 calc R U P N 1
C1G2 C 0.860(2) -0.043(2) 0.1998(8) 0.069(5) Uani 0.5 1 d D U P N 2
H1G1 H 0.8729 -0.0034 0.2128 0.082 Uiso 0.5 1 calc R U P N 2
H1G2 H 0.8786 -0.0900 0.2165 0.082 Uiso 0.5 1 calc R U P N 2
C1G3 C 0.8948(18) -0.0347(18) 0.1572(7) 0.098(4) Uani 0.5 1 d DG U P N 2
C1G4 C 0.9173(18) 0.0318(15) 0.1364(9) 0.098(4) Uani 0.5 1 d G U P N 2
H1G4 H 0.9102 0.0725 0.1496 0.118 Uiso 0.5 1 calc R U P N 2
C1G5 C 0.9503(18) 0.0388(14) 0.0963(9) 0.098(4) Uani 0.5 1 d G U P N 2
H1G5 H 0.9657 0.0843 0.0821 0.118 Uiso 0.5 1 calc R U P N 2
C1G6 C 0.9607(17) -0.0208(18) 0.0770(7) 0.098(4) Uani 0.5 1 d G U P N 2
H1G6 H 0.9832 -0.0160 0.0496 0.118 Uiso 0.5 1 calc R U P N 2
C1G7 C 0.9381(18) -0.0873(15) 0.0978(9) 0.098(4) Uani 0.5 1 d G U P N 2
H1G7 H 0.9453 -0.1280 0.0846 0.118 Uiso 0.5 1 calc R U P N 2
C1G8 C 0.9052(18) -0.0942(14) 0.1379(9) 0.098(4) Uani 0.5 1 d G U P N 2
H1G8 H 0.8898 -0.1397 0.1521 0.118 Uiso 0.5 1 calc R U P N 2
C169 C 0.7311(9) -0.0908(9) 0.2883(5) 0.060(4) Uani 1 1 d D U . . .
H16E H 0.6967 -0.0801 0.3117 0.071 Uiso 1 1 calc R U . O 1
H16F H 0.7190 -0.1366 0.2816 0.071 Uiso 1 1 calc R U . O 1
C170 C 0.8095(10) -0.1020(18) 0.3017(8) 0.061(6) Uani 0.5 1 d D U P P 1
H17C H 0.8172 -0.0558 0.3094 0.074 Uiso 0.5 1 calc R U P P 1
H17D H 0.8077 -0.1386 0.3278 0.074 Uiso 0.5 1 calc R U P P 1
C171 C 0.8787(14) -0.1232(13) 0.2784(9) 0.101(5) Uani 0.5 1 d DG U P P 1
C172 C 0.8960(11) -0.1886(11) 0.2649(10) 0.101(5) Uani 0.5 1 d DG U P P 1
H172 H 0.8675 -0.2281 0.2756 0.121 Uiso 0.5 1 calc R U P P 1
C173 C 0.9549(13) -0.1961(13) 0.2358(10) 0.101(5) Uani 0.5 1 d G U P P 1
H173 H 0.9667 -0.2408 0.2266 0.121 Uiso 0.5 1 calc R U P P 1
C174 C 0.9966(14) -0.1382(16) 0.2202(9) 0.101(5) Uani 0.5 1 d G U P P 1
H174 H 1.0369 -0.1434 0.2003 0.121 Uiso 0.5 1 calc R U P P 1
C175 C 0.9794(16) -0.0729(14) 0.2336(10) 0.101(5) Uani 0.5 1 d G U P P 1
H175 H 1.0079 -0.0333 0.2230 0.121 Uiso 0.5 1 calc R U P P 1
C176 C 0.9204(18) -0.0654(12) 0.2627(10) 0.101(5) Uani 0.5 1 d DG U P P 1
H176 H 0.9086 -0.0207 0.2720 0.121 Uiso 0.5 1 calc R U P P 1
C1H0 C 0.723(2) -0.1669(13) 0.2804(10) 0.080(7) Uani 0.5 1 d D U P P 2
H1H1 H 0.6992 -0.1619 0.2543 0.096 Uiso 0.5 1 calc R U P P 2
H1H2 H 0.7717 -0.1938 0.2774 0.096 Uiso 0.5 1 calc R U P P 2
C1H1 C 0.6777(18) -0.2085(16) 0.3146(9) 0.101(5) Uani 0.5 1 d DG U P P 2
C1H2 C 0.6018(18) -0.2076(16) 0.3178(9) 0.101(5) Uani 0.5 1 d G U P P 2
H1H3 H 0.5746 -0.1825 0.2954 0.121 Uiso 0.5 1 calc R U P P 2
C1H3 C 0.5655(13) -0.2433(17) 0.3538(11) 0.101(5) Uani 0.5 1 d G U P P 2
H1H4 H 0.5136 -0.2427 0.3560 0.121 Uiso 0.5 1 calc R U P P 2
C1H4 C 0.6053(18) -0.2800(16) 0.3866(8) 0.101(5) Uani 0.5 1 d G U P P 2
H1H5 H 0.5805 -0.3045 0.4112 0.121 Uiso 0.5 1 calc R U P P 2
C1H5 C 0.6812(18) -0.2810(16) 0.3834(9) 0.101(5) Uani 0.5 1 d G U P P 2
H1H6 H 0.7084 -0.3060 0.4058 0.121 Uiso 0.5 1 calc R U P P 2
C1H6 C 0.7175(13) -0.2452(17) 0.3474(11) 0.101(5) Uani 0.5 1 d G U P P 2
H1H7 H 0.7694 -0.2458 0.3452 0.121 Uiso 0.5 1 calc R U P P 2
C177 C 0.8451(10) 0.1075(10) 0.3516(7) 0.090(6) Uani 1 1 d D U . . .
H17E H 0.8302 0.0862 0.3292 0.108 Uiso 1 1 calc R U . . .
H17F H 0.8968 0.1178 0.3441 0.108 Uiso 1 1 calc R U . . .
C178 C 0.8442(18) 0.0485(11) 0.3906(8) 0.174(12) Uani 1 1 d D U . . .
H17G H 0.8679 0.0643 0.4123 0.208 Uiso 1 1 calc R U . . .
H17H H 0.7929 0.0406 0.4010 0.208 Uiso 1 1 calc R U . . .
C179 C 0.8841(17) -0.0206(10) 0.3817(10) 0.253(10) Uani 1 1 d DG U . . .
C180 C 0.9378(17) -0.0351(12) 0.3510(9) 0.253(10) Uani 1 1 d G U . . .
H180 H 0.9532 0.0034 0.3297 0.304 Uiso 1 1 calc R U . . .
C181 C 0.9689(15) -0.1060(15) 0.3514(8) 0.253(10) Uani 1 1 d G U . . .
H181 H 1.0056 -0.1159 0.3304 0.304 Uiso 1 1 calc R U . . .
C182 C 0.9462(16) -0.1623(10) 0.3825(10) 0.253(10) Uani 1 1 d G U . . .
H182 H 0.9675 -0.2107 0.3828 0.304 Uiso 1 1 calc R U . . .
C183 C 0.8925(16) -0.1478(12) 0.4132(9) 0.253(10) Uani 1 1 d G U . . .
H183 H 0.8771 -0.1863 0.4345 0.304 Uiso 1 1 calc R U . . .
C184 C 0.8614(15) -0.0770(15) 0.4128(8) 0.253(10) Uani 1 1 d G U . . .
H184 H 0.8247 -0.0671 0.4338 0.304 Uiso 1 1 calc R U . . .
C185 C 0.8339(14) 0.2346(11) 0.3862(9) 0.113(8) Uani 1 1 d D U . . .
H18C H 0.8192 0.2092 0.4146 0.135 Uiso 1 1 calc R U . . .
H18D H 0.8877 0.2243 0.3816 0.135 Uiso 1 1 calc R U . . .
C186 C 0.8172(14) 0.3151(11) 0.3846(9) 0.141(8) Uani 1 1 d D U . . .
H18E H 0.8260 0.3428 0.3561 0.170 Uiso 1 1 calc R U . . .
H18F H 0.7656 0.3269 0.3948 0.170 Uiso 1 1 calc R U . . .
C187 C 0.8685(11) 0.3314(11) 0.4121(8) 0.178(7) Uani 1 1 d DG U . . .
C188 C 0.8549(10) 0.3160(11) 0.4548(8) 0.178(7) Uani 1 1 d G U . . .
H188 H 0.8225 0.2807 0.4675 0.214 Uiso 1 1 calc R U . . .
C189 C 0.8887(12) 0.3522(13) 0.4791(6) 0.178(7) Uani 1 1 d G U . . .
H189 H 0.8795 0.3417 0.5083 0.214 Uiso 1 1 calc R U . . .
C190 C 0.9362(11) 0.4038(12) 0.4605(8) 0.178(7) Uani 1 1 d G U . . .
H190 H 0.9593 0.4286 0.4771 0.214 Uiso 1 1 calc R U . . .
C191 C 0.9498(10) 0.4193(11) 0.4178(8) 0.178(7) Uani 1 1 d G U . . .
H191 H 0.9822 0.4545 0.4051 0.214 Uiso 1 1 calc R U . . .
C192 C 0.9159(12) 0.3830(13) 0.3935(6) 0.178(7) Uani 1 1 d DG U . . .
H192 H 0.9252 0.3936 0.3643 0.214 Uiso 1 1 calc R U . . .
P1 P 0.3230(3) 0.5589(2) 0.23870(16) 0.0561(14) Uani 1 1 d . U . . .
P2 P 0.2422(2) 0.3265(2) 0.14471(16) 0.0460(11) Uani 1 1 d . U . . .
P3 P 0.2455(2) 0.0937(3) 0.31168(17) 0.0527(13) Uani 1 1 d D U . . .
P4 P 0.3217(3) 0.3259(3) 0.40291(17) 0.0623(15) Uani 1 1 d . U . . .
P5 P 0.5176(3) 0.5147(2) 0.08522(15) 0.0472(11) Uani 1 1 d . U . . .
P6 P 0.4343(4) 0.0256(3) 0.1581(3) 0.100(3) Uani 1 1 d . U . . .
P7 P 0.5261(2) 0.0216(2) 0.40103(14) 0.0390(10) Uani 1 1 d . U . . .
P8 P 0.5902(3) 0.4908(3) 0.34335(18) 0.0609(14) Uani 1 1 d . U . . .
P9 P 0.7913(2) 0.4309(3) 0.18999(16) 0.0504(12) Uani 1 1 d . U . . .
P10 P 0.7024(3) 0.2159(2) 0.08626(15) 0.0468(11) Uani 1 1 d . U . . .
P11 P 0.7176(2) -0.0182(2) 0.24392(14) 0.0372(10) Uani 1 1 d . U . . .
P12 P 0.7914(3) 0.1937(3) 0.3500(2) 0.0717(18) Uani 1 1 d . U . . .
Pt1 Pt 0.51455(3) 0.26977(3) 0.24543(2) 0.03245(15) Uani 1 1 d . . . . .
Se1 Se 0.29618(9) 0.46187(9) 0.28470(6) 0.0463(4) Uani 1 1 d . . . . .
Se2 Se 0.42084(12) 0.54188(9) 0.19864(6) 0.0570(5) Uani 1 1 d . . . . .
Se3 Se 0.25311(10) 0.38792(10) 0.19232(7) 0.0557(5) Uani 1 1 d . . . . .
Se4 Se 0.33778(9) 0.24998(9) 0.13320(6) 0.0435(4) Uani 1 1 d . . . . .
Se5 Se 0.23847(8) 0.19929(9) 0.26871(6) 0.0446(4) Uani 1 1 d . . . . .
Se6 Se 0.35609(10) 0.05302(10) 0.32826(7) 0.0605(6) Uani 1 1 d . . . . .
Se7 Se 0.28134(10) 0.27205(10) 0.35980(9) 0.0726(7) Uani 1 1 d . . . . .
Se8 Se 0.43698(10) 0.34801(10) 0.38901(6) 0.0474(4) Uani 1 1 d . . . . .
Se9 Se 0.44489(12) 0.43007(10) 0.09303(6) 0.0602(5) Uani 1 1 d . . . . .
Se10 Se 0.59003(10) 0.50264(8) 0.13508(6) 0.0435(4) Uani 1 1 d . . . . .
Se11 Se 0.40308(10) 0.03787(10) 0.22069(9) 0.0808(8) Uani 1 1 d . . . . .
Se12 Se 0.49877(15) 0.10958(17) 0.12117(8) 0.0985(10) Uani 1 1 d . . . . .
Se13 Se 0.48886(9) 0.13288(9) 0.40815(6) 0.0454(4) Uani 1 1 d . . . . .
Se14 Se 0.55285(8) 0.00566(8) 0.33771(5) 0.0378(4) Uani 1 1 d . . . . .
Se15 Se 0.52711(10) 0.52184(9) 0.28896(6) 0.0506(5) Uani 1 1 d . . . . .
Se16 Se 0.62672(10) 0.37609(11) 0.35979(7) 0.0567(5) Uani 1 1 d . . . . .
Se17 Se 0.77369(9) 0.33249(9) 0.16774(6) 0.0442(4) Uani 1 1 d . . . . .
Se18 Se 0.69996(10) 0.46962(10) 0.22967(7) 0.0549(5) Uani 1 1 d . . . . .
Se19 Se 0.72677(11) 0.16014(10) 0.14800(6) 0.0583(5) Uani 1 1 d . . . . .
Se20 Se 0.60481(9) 0.29479(9) 0.08481(5) 0.0429(4) Uani 1 1 d . . . . .
Se21 Se 0.75294(8) 0.08048(9) 0.25781(5) 0.0391(4) Uani 1 1 d . . . . .
Se22 Se 0.60269(9) -0.00983(9) 0.23297(6) 0.0455(4) Uani 1 1 d . . . . .
Se23 Se 0.80296(10) 0.25124(11) 0.28753(9) 0.0739(7) Uani 1 1 d . . . . .
Se24 Se 0.67839(11) 0.17398(10) 0.37378(6) 0.0543(5) Uani 1 1 d . . . . .


_geom_special_details            
; 
 All esds (except the esd in the dihedral angle between two l.s. planes) 
 are estimated using the full covariance matrix.  The cell esds are taken 
 into account individually in the estimation of esds in distances, angles 
 and torsion angles; correlations between esds in cell parameters are only 
 used when they are defined by crystal symmetry.  An approximate (isotropic) 
 treatment of cell esds is used for estimating esds involving l.s. planes. 
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 Se4 2.631(2) . ?
Ag1 Pt1 2.7626(13) . ?
Ag1 Ag4 2.8484(17) . ?
Ag1 Ag2 2.885(2) . ?
Ag1 Ag5 2.8999(17) . ?
Ag1 Ag3 2.9370(17) . ?
Ag1 Ag16 2.9786(17) . ?
Ag1 Ag13 2.9903(17) . ?
Ag1 Ag6 3.0033(19) . ?
Ag2 Se1 2.644(2) . ?
Ag2 Pt1 2.8232(15) . ?
Ag2 Ag6 2.861(2) . ?
Ag2 Ag13 2.967(2) . ?
Ag2 Ag17 3.005(2) . ?
Ag2 Ag11 3.041(2) . ?
Ag2 Ag3 3.052(2) . ?
Ag2 Ag7 3.212(2) . ?
Ag3 Se10 2.673(2) . ?
Ag3 Pt1 2.7882(14) . ?
Ag3 Ag4 2.9104(17) . ?
Ag3 Ag13 2.9434(18) . ?
Ag3 Ag8 2.9643(18) . ?
Ag3 Ag7 2.969(2) . ?
Ag3 Ag14 2.9809(19) . ?
Ag4 Se20 2.676(2) . ?
Ag4 Pt1 2.8046(14) . ?
Ag4 Ag9 2.8865(17) . ?
Ag4 Ag5 2.9255(18) . ?
Ag4 Ag8 2.9519(18) . ?
Ag4 Ag15 2.9672(17) . ?
Ag4 Ag14 3.0052(17) . ?
Ag5 Se11 2.639(2) . ?
Ag5 Pt1 2.7859(14) . ?
Ag5 Ag10 2.859(2) . ?
Ag5 Ag9 2.8689(17) . ?
Ag5 Ag6 2.944(2) . ?
Ag5 Ag15 2.945(2) . ?
Ag5 Ag16 2.9466(17) . ?
Ag6 Se5 2.6570(19) . ?
Ag6 Pt1 2.7962(13) . ?
Ag6 Ag10 2.8597(17) . ?
Ag6 Ag11 2.8846(19) . ?
Ag6 Ag16 2.9566(19) . ?
Ag6 Ag19 3.001(2) . ?
Ag7 Se15 2.641(2) . ?
Ag7 Pt1 2.7937(15) . ?
Ag7 Ag8 2.894(2) . ?
Ag7 Ag12 2.9337(19) . ?
Ag7 Ag18 2.9497(19) . ?
Ag7 Ag17 2.993(2) . ?
Ag7 Ag11 3.025(2) . ?
Ag8 Se17 2.643(2) . ?
Ag8 Pt1 2.7938(13) . ?
Ag8 Ag9 2.8569(18) . ?
Ag8 Ag12 2.969(2) . ?
Ag8 Ag14 3.038(2) . ?
Ag8 Ag18 3.049(2) . ?
Ag9 Se21 2.6550(19) . ?
Ag9 Pt1 2.7824(13) . ?
Ag9 Ag20 2.9350(18) . ?
Ag9 Ag12 2.9565(19) . ?
Ag9 Ag10 2.9597(18) . ?
Ag9 Ag15 2.9895(19) . ?
Ag10 Se14 2.6534(19) . ?
Ag10 Pt1 2.7915(14) . ?
Ag10 Ag11 2.8948(18) . ?
Ag10 Ag12 2.9021(17) . ?
Ag10 Ag20 2.9745(16) . ?
Ag10 Ag19 2.9777(19) . ?
Ag11 Se8 2.638(2) . ?
Ag11 Pt1 2.7744(15) . ?
Ag11 Ag12 2.8805(18) . ?
Ag11 Ag19 2.9670(18) . ?
Ag11 Ag17 2.9733(18) . ?
Ag12 Se24 2.665(2) . ?
Ag12 Pt1 2.7946(14) . ?
Ag12 Ag18 2.9109(18) . ?
Ag12 Ag20 2.9189(17) . ?
Ag13 Se9 2.588(3) . ?
Ag13 Se3 2.601(2) . ?
Ag13 Se2 2.631(2) . ?
Ag14 Se10 2.599(2) . ?
Ag14 Se17 2.601(2) . ?
Ag14 Se20 2.623(2) . ?
Ag15 Se12 2.596(3) . ?
Ag15 Se22 2.609(2) . ?
Ag15 Se19 2.616(3) . ?
Ag16 Se11 2.605(2) . ?
Ag16 Se4 2.629(2) . ?
Ag16 Se5 2.638(2) . ?
Ag17 Se1 2.608(2) . ?
Ag17 Se15 2.623(2) . ?
Ag17 Se8 2.625(2) . ?
Ag18 Se23 2.573(2) . ?
Ag18 Se18 2.599(3) . ?
Ag18 Se16 2.610(3) . ?
Ag19 Se13 2.594(2) . ?
Ag19 Se6 2.595(3) . ?
Ag19 Se7 2.604(2) . ?
Ag20 Se21 2.612(2) . ?
Ag20 Se14 2.6230(19) . ?
Ag20 Se24 2.633(2) . ?
C1 C2 1.512(10) . ?
C1 P1 1.799(18) . ?
C2 C3 1.489(10) . ?
C3 C4 1.3900 . ?
C3 C8 1.3900 . ?
C4 C5 1.3900 . ?
C5 C6 1.3900 . ?
C6 C7 1.3900 . ?
C7 C8 1.3900 . ?
C9 C10 1.60(3) . ?
C9 P1 1.844(16) . ?
C10 C11 1.493(10) . ?
C11 C12 1.3900 . ?
C11 C16 1.3900 . ?
C12 C13 1.3900 . ?
C13 C14 1.3900 . ?
C14 C15 1.3900 . ?
C15 C16 1.3900 . ?
C17 C18 1.46(3) . ?
C17 P2 1.820(19) . ?
C18 C19 1.46(2) . ?
C19 C20 1.3900 . ?
C19 C24 1.3900 . ?
C20 C21 1.3900 . ?
C21 C22 1.3900 . ?
C22 C23 1.3900 . ?
C23 C24 1.3900 . ?
C25 C26 1.52(2) . ?
C25 P2 1.802(17) . ?
C26 C27 1.52(2) . ?
C27 C28 1.3900 . ?
C27 C32 1.3900 . ?
C28 C29 1.3900 . ?
C29 C30 1.3900 . ?
C30 C31 1.3900 . ?
C31 C32 1.3900 . ?
C33 C34 1.524(10) . ?
C33 P3 1.73(2) . ?
C34 C35 1.470(10) . ?
C34 C35B 1.475(10) . ?
C35 C36 1.3900 . ?
C35 C40 1.3900 . ?
C36 C37 1.3900 . ?
C37 C38 1.3900 . ?
C38 C39 1.3900 . ?
C39 C40 1.3900 . ?
C35B C36B 1.3900 . ?
C35B C40B 1.3900 . ?
C36B C37B 1.3900 . ?
C37B C38B 1.3900 . ?
C38B C39B 1.3900 . ?
C39B C40B 1.3900 . ?
C41 C42 1.55(2) . ?
C41 P3 1.77(2) . ?
C42 C43 1.54(2) . ?
C43 C44 1.3900 . ?
C43 C48 1.3900 . ?
C44 C45 1.3900 . ?
C45 C46 1.3900 . ?
C46 C47 1.3900 . ?
C47 C48 1.3900 . ?
C49 C50 1.524(10) . ?
C49 P4 1.83(2) . ?
C50 C51 1.498(9) . ?
C50 C51B 1.506(13) . ?
C51 C52 1.3900 . ?
C51 C56 1.3900 . ?
C52 C53 1.3900 . ?
C53 C54 1.3900 . ?
C54 C55 1.3900 . ?
C55 C56 1.3900 . ?
C51B C52B 1.3900 . ?
C51B C56B 1.3900 . ?
C52B C53B 1.3900 . ?
C53B C54B 1.3900 . ?
C54B C55B 1.3900 . ?
C55B C56B 1.3900 . ?
C57 C58 1.65(3) . ?
C57 P4 1.801(18) . ?
C58 C59 1.482(9) . ?
C58 C59B 1.55(2) . ?
C59 C60 1.3900 . ?
C59 C64 1.3900 . ?
C60 C61 1.3900 . ?
C61 C62 1.3900 . ?
C62 C63 1.3900 . ?
C63 C64 1.3900 . ?
C59B C60B 1.3900 . ?
C59B C64B 1.3900 . ?
C60B C61B 1.3900 . ?
C61B C62B 1.3900 . ?
C62B C63B 1.3900 . ?
C63B C64B 1.3900 . ?
C65 C66 1.49(2) . ?
C65 P5 1.854(17) . ?
C66 C67 1.48(2) . ?
C67 C68 1.3900 . ?
C67 C72 1.3900 . ?
C68 C69 1.3900 . ?
C69 C70 1.3900 . ?
C70 C71 1.3900 . ?
C71 C72 1.3900 . ?
C73 C74 1.48(3) . ?
C73 P5 1.84(2) . ?
C74 C75 1.47(2) . ?
C75 C76 1.3900 . ?
C75 C80 1.3900 . ?
C76 C77 1.3900 . ?
C77 C78 1.3900 . ?
C78 C79 1.3900 . ?
C79 C80 1.3900 . ?
C81 C82 1.509(10) . ?
C81 P6 1.84(2) . ?
C82 C83 1.461(10) . ?
C83 C84 1.3900 . ?
C83 C88 1.3900 . ?
C84 C85 1.3900 . ?
C85 C86 1.3900 . ?
C86 C87 1.3900 . ?
C87 C88 1.3900 . ?
C89 C90 1.534(10) . ?
C89 P6 1.92(2) . ?
C90 C91 1.466(10) . ?
C91 C92 1.3900 . ?
C91 C96 1.3900 . ?
C92 C93 1.3900 . ?
C93 C94 1.3900 . ?
C94 C95 1.3900 . ?
C95 C96 1.3900 . ?
C97 C98 1.54(2) . ?
C97 P7 1.856(17) . ?
C98 C99 1.47(2) . ?
C99 C100 1.3900 . ?
C99 C104 1.3900 . ?
C100 C101 1.3900 . ?
C101 C102 1.3900 . ?
C102 C103 1.3900 . ?
C103 C104 1.3900 . ?
C105 C106 1.54(2) . ?
C105 P7 1.805(15) . ?
C106 C107 1.498(18) . ?
C107 C108 1.3900 . ?
C107 C112 1.3900 . ?
C108 C109 1.3900 . ?
C109 C110 1.3900 . ?
C110 C111 1.3900 . ?
C111 C112 1.3900 . ?
C113 C114 1.517(10) . ?
C113 P8 1.89(2) . ?
C114 C115 1.476(10) . ?
C115 C116 1.3900 . ?
C115 C120 1.3900 . ?
C116 C117 1.3900 . ?
C117 C118 1.3900 . ?
C118 C119 1.3900 . ?
C119 C120 1.3900 . ?
C121 C122 1.527(10) . ?
C121 P8 1.84(2) . ?
C122 C123 1.482(10) . ?
C123 C124 1.3900 . ?
C123 C128 1.3900 . ?
C124 C125 1.3900 . ?
C125 C126 1.3900 . ?
C126 C127 1.3900 . ?
C127 C128 1.3900 . ?
C129 C130 1.520(10) . ?
C129 P9 1.790(17) . ?
C130 C131 1.509(10) . ?
C131 C132 1.3900 . ?
C131 C136 1.3900 . ?
C132 C133 1.3900 . ?
C133 C134 1.3900 . ?
C134 C135 1.3900 . ?
C135 C136 1.3900 . ?
C137 C138 1.52(3) . ?
C137 C1D8 1.52(3) . ?
C137 P9 1.856(19) . ?
C138 C139 1.61(5) . ?
C139 C140 1.3900 . ?
C139 C144 1.3900 . ?
C140 C141 1.3900 . ?
C141 C142 1.3900 . ?
C142 C143 1.3900 . ?
C143 C144 1.3900 . ?
C1D8 C1D9 1.471(10) . ?
C1D9 C1E0 1.3900 . ?
C1D9 C1E4 1.3900 . ?
C1E0 C1E1 1.3900 . ?
C1E1 C1E2 1.3900 . ?
C1E2 C1E3 1.3900 . ?
C1E3 C1E4 1.3900 . ?
C145 C146 1.535(10) . ?
C145 C1E6 1.545(13) . ?
C145 P10 1.874(18) . ?
C146 C147 1.467(10) . ?
C147 C148 1.3900 . ?
C147 C152 1.3900 . ?
C148 C149 1.3900 . ?
C149 C150 1.3900 . ?
C150 C151 1.3900 . ?
C151 C152 1.3900 . ?
C1E6 C1E7 1.484(10) . ?
C1E7 C1E8 1.3900 . ?
C1E7 C1F2 1.3900 . ?
C1E8 C1E9 1.3900 . ?
C1E9 C1F0 1.3900 . ?
C1F0 C1F1 1.3900 . ?
C1F1 C1F2 1.3900 . ?
C153 C154 1.525(10) . ?
C153 C1F4 1.536(14) . ?
C153 P10 1.782(19) . ?
C154 C155 1.474(10) . ?
C155 C156 1.3900 . ?
C155 C160 1.3900 . ?
C156 C157 1.3900 . ?
C157 C158 1.3900 . ?
C158 C159 1.3900 . ?
C159 C160 1.3900 . ?
C1F4 C1F5 1.468(10) . ?
C1F5 C1F6 1.3900 . ?
C1F5 C1G0 1.3900 . ?
C1F6 C1F7 1.3900 . ?
C1F7 C1F8 1.3900 . ?
C1F8 C1F9 1.3900 . ?
C1F9 C1G0 1.3900 . ?
C161 C162 1.511(10) . ?
C161 C1G2 1.63(4) . ?
C161 P11 1.816(18) . ?
C162 C163 1.474(10) . ?
C163 C164 1.3900 . ?
C163 C168 1.3900 . ?
C164 C165 1.3900 . ?
C165 C166 1.3900 . ?
C166 C167 1.3900 . ?
C167 C168 1.3900 . ?
C1G2 C1G3 1.471(10) . ?
C1G3 C1G4 1.3900 . ?
C1G3 C1G8 1.3900 . ?
C1G4 C1G5 1.3900 . ?
C1G5 C1G6 1.3900 . ?
C1G6 C1G7 1.3900 . ?
C1G7 C1G8 1.3900 . ?
C169 C170 1.531(9) . ?
C169 C1H0 1.540(13) . ?
C169 P11 1.808(17) . ?
C170 C171 1.478(10) . ?
C171 C172 1.3900 . ?
C171 C176 1.3900 . ?
C172 C173 1.3900 . ?
C173 C174 1.3900 . ?
C174 C175 1.3900 . ?
C175 C176 1.3900 . ?
C1H0 C1H1 1.475(10) . ?
C1H1 C1H2 1.3900 . ?
C1H1 C1H6 1.3900 . ?
C1H2 C1H3 1.3900 . ?
C1H3 C1H4 1.3900 . ?
C1H4 C1H5 1.3900 . ?
C1H5 C1H6 1.3900 . ?
C177 C178 1.524(10) . ?
C177 P12 1.798(19) . ?
C178 C179 1.491(10) . ?
C179 C180 1.3900 . ?
C179 C184 1.3900 . ?
C180 C181 1.3900 . ?
C181 C182 1.3900 . ?
C182 C183 1.3900 . ?
C183 C184 1.3900 . ?
C185 C186 1.506(10) . ?
C185 P12 1.833(17) . ?
C186 C187 1.476(10) . ?
C187 C188 1.3900 . ?
C187 C192 1.3900 . ?
C188 C189 1.3900 . ?
C189 C190 1.3900 . ?
C190 C191 1.3900 . ?
C191 C192 1.3900 . ?
P1 Se2 2.158(6) . ?
P1 Se1 2.198(6) . ?
P2 Se3 2.180(5) . ?
P2 Se4 2.197(5) . ?
P3 Se6 2.175(5) . ?
P3 Se5 2.197(5) . ?
P4 Se7 2.152(7) . ?
P4 Se8 2.194(6) . ?
P5 Se9 2.161(5) . ?
P5 Se10 2.190(5) . ?
P6 Se11 2.148(9) . ?
P6 Se12 2.182(9) . ?
P7 Se14 2.181(5) . ?
P7 Se13 2.185(4) . ?
P8 Se16 2.167(6) . ?
P8 Se15 2.187(6) . ?
P9 Se18 2.178(5) . ?
P9 Se17 2.205(5) . ?
P10 Se19 2.166(5) . ?
P10 Se20 2.194(5) . ?
P11 Se22 2.166(4) . ?
P11 Se21 2.193(4) . ?
P12 Se23 2.134(8) . ?
P12 Se24 2.192(6) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Se4 Ag1 Pt1 157.11(6) . . ?
Se4 Ag1 Ag4 111.07(6) . . ?
Pt1 Ag1 Ag4 59.96(4) . . ?
Se4 Ag1 Ag2 136.24(7) . . ?
Pt1 Ag1 Ag2 59.94(4) . . ?
Ag4 Ag1 Ag2 112.10(6) . . ?
Se4 Ag1 Ag5 98.22(6) . . ?
Pt1 Ag1 Ag5 58.88(4) . . ?
Ag4 Ag1 Ag5 61.18(4) . . ?
Ag2 Ag1 Ag5 108.34(6) . . ?
Se4 Ag1 Ag3 138.59(7) . . ?
Pt1 Ag1 Ag3 58.48(4) . . ?
Ag4 Ag1 Ag3 60.38(4) . . ?
Ag2 Ag1 Ag3 63.22(5) . . ?
Ag5 Ag1 Ag3 108.72(5) . . ?
Se4 Ag1 Ag16 55.48(5) . . ?
Pt1 Ag1 Ag16 107.14(5) . . ?
Ag4 Ag1 Ag16 115.36(5) . . ?
Ag2 Ag1 Ag16 109.79(6) . . ?
Ag5 Ag1 Ag16 60.15(4) . . ?
Ag3 Ag1 Ag16 165.56(6) . . ?
Se4 Ag1 Ag13 95.72(6) . . ?
Pt1 Ag1 Ag13 107.17(5) . . ?
Ag4 Ag1 Ag13 113.23(5) . . ?
Ag2 Ag1 Ag13 60.63(5) . . ?
Ag5 Ag1 Ag13 166.06(6) . . ?
Ag3 Ag1 Ag13 59.54(4) . . ?
Ag16 Ag1 Ag13 129.82(5) . . ?
Se4 Ag1 Ag6 112.77(6) . . ?
Pt1 Ag1 Ag6 57.84(4) . . ?
Ag4 Ag1 Ag6 109.10(5) . . ?
Ag2 Ag1 Ag6 58.09(5) . . ?
Ag5 Ag1 Ag6 59.80(5) . . ?
Ag3 Ag1 Ag6 107.90(5) . . ?
Ag16 Ag1 Ag6 59.24(4) . . ?
Ag13 Ag1 Ag6 114.47(6) . . ?
Se1 Ag2 Pt1 154.86(8) . . ?
Se1 Ag2 Ag6 116.29(8) . . ?
Pt1 Ag2 Ag6 58.93(4) . . ?
Se1 Ag2 Ag1 145.42(8) . . ?
Pt1 Ag2 Ag1 57.87(4) . . ?
Ag6 Ag2 Ag1 63.02(5) . . ?
Se1 Ag2 Ag13 97.30(7) . . ?
Pt1 Ag2 Ag13 106.21(6) . . ?
Ag6 Ag2 Ag13 119.70(7) . . ?
Ag1 Ag2 Ag13 61.43(5) . . ?
Se1 Ag2 Ag17 54.53(5) . . ?
Pt1 Ag2 Ag17 102.61(6) . . ?
Ag6 Ag2 Ag17 112.49(6) . . ?
Ag1 Ag2 Ag17 160.05(7) . . ?
Ag13 Ag2 Ag17 127.71(6) . . ?
Se1 Ag2 Ag11 99.29(7) . . ?
Pt1 Ag2 Ag11 56.33(4) . . ?
Ag6 Ag2 Ag11 58.43(5) . . ?
Ag1 Ag2 Ag11 106.92(5) . . ?
Ag13 Ag2 Ag11 161.76(7) . . ?
Ag17 Ag2 Ag11 58.91(5) . . ?
Se1 Ag2 Ag3 135.12(8) . . ?
Pt1 Ag2 Ag3 56.50(4) . . ?
Ag6 Ag2 Ag3 108.60(6) . . ?
Ag1 Ag2 Ag3 59.22(5) . . ?
Ag13 Ag2 Ag3 58.53(5) . . ?
Ag17 Ag2 Ag3 108.06(7) . . ?
Ag11 Ag2 Ag3 103.84(6) . . ?
Se1 Ag2 Ag7 109.26(7) . . ?
Pt1 Ag2 Ag7 54.70(4) . . ?
Ag6 Ag2 Ag7 104.77(6) . . ?
Ag1 Ag2 Ag7 103.73(6) . . ?
Ag13 Ag2 Ag7 109.24(7) . . ?
Ag17 Ag2 Ag7 57.44(5) . . ?
Ag11 Ag2 Ag7 57.79(5) . . ?
Ag3 Ag2 Ag7 56.52(5) . . ?
Se10 Ag3 Pt1 154.79(7) . . ?
Se10 Ag3 Ag4 114.40(7) . . ?
Pt1 Ag3 Ag4 58.92(4) . . ?
Se10 Ag3 Ag1 143.14(7) . . ?
Pt1 Ag3 Ag1 57.63(4) . . ?
Ag4 Ag3 Ag1 58.30(4) . . ?
Se10 Ag3 Ag13 97.20(6) . . ?
Pt1 Ag3 Ag13 107.79(5) . . ?
Ag4 Ag3 Ag13 112.81(6) . . ?
Ag1 Ag3 Ag13 61.13(4) . . ?
Se10 Ag3 Ag8 97.05(6) . . ?
Pt1 Ag3 Ag8 58.02(4) . . ?
Ag4 Ag3 Ag8 60.32(4) . . ?
Ag1 Ag3 Ag8 106.36(5) . . ?
Ag13 Ag3 Ag8 165.75(6) . . ?
Se10 Ag3 Ag7 107.75(6) . . ?
Pt1 Ag3 Ag7 57.96(4) . . ?
Ag4 Ag3 Ag7 107.57(5) . . ?
Ag1 Ag3 Ag7 108.72(6) . . ?
Ag13 Ag3 Ag7 116.96(6) . . ?
Ag8 Ag3 Ag7 58.40(5) . . ?
Se10 Ag3 Ag14 54.40(5) . . ?
Pt1 Ag3 Ag14 109.15(5) . . ?
Ag4 Ag3 Ag14 61.33(4) . . ?
Ag1 Ag3 Ag14 113.72(6) . . ?
Ag13 Ag3 Ag14 128.19(6) . . ?
Ag8 Ag3 Ag14 61.46(4) . . ?
Ag7 Ag3 Ag14 113.11(6) . . ?
Se10 Ag3 Ag2 139.18(7) . . ?
Pt1 Ag3 Ag2 57.60(4) . . ?
Ag4 Ag3 Ag2 105.80(5) . . ?
Ag1 Ag3 Ag2 57.56(5) . . ?
Ag13 Ag3 Ag2 59.30(5) . . ?
Ag8 Ag3 Ag2 109.04(6) . . ?
Ag7 Ag3 Ag2 64.45(5) . . ?
Ag14 Ag3 Ag2 166.28(6) . . ?
Se20 Ag4 Pt1 155.33(6) . . ?
Se20 Ag4 Ag1 110.01(6) . . ?
Pt1 Ag4 Ag1 58.50(4) . . ?
Se20 Ag4 Ag9 141.14(6) . . ?
Pt1 Ag4 Ag9 58.52(4) . . ?
Ag1 Ag4 Ag9 108.03(5) . . ?
Se20 Ag4 Ag3 97.06(6) . . ?
Pt1 Ag4 Ag3 58.37(4) . . ?
Ag1 Ag4 Ag3 61.32(4) . . ?
Ag9 Ag4 Ag3 107.94(5) . . ?
Se20 Ag4 Ag5 138.85(7) . . ?
Pt1 Ag4 Ag5 58.13(4) . . ?
Ag1 Ag4 Ag5 60.28(4) . . ?
Ag9 Ag4 Ag5 59.15(4) . . ?
Ag3 Ag4 Ag5 108.75(5) . . ?
Se20 Ag4 Ag8 114.24(6) . . ?
Pt1 Ag4 Ag8 58.00(4) . . ?
Ag1 Ag4 Ag8 109.05(5) . . ?
Ag9 Ag4 Ag8 58.58(4) . . ?
Ag3 Ag4 Ag8 60.75(4) . . ?
Ag5 Ag4 Ag8 106.32(5) . . ?
Se20 Ag4 Ag15 95.99(6) . . ?
Pt1 Ag4 Ag15 108.57(5) . . ?
Ag1 Ag4 Ag15 113.02(6) . . ?
Ag9 Ag4 Ag15 61.40(4) . . ?
Ag3 Ag4 Ag15 166.93(6) . . ?
Ag5 Ag4 Ag15 59.95(5) . . ?
Ag8 Ag4 Ag15 114.08(5) . . ?
Se20 Ag4 Ag14 54.63(5) . . ?
Pt1 Ag4 Ag14 108.03(5) . . ?
Ag1 Ag4 Ag14 115.65(5) . . ?
Ag9 Ag4 Ag14 113.70(5) . . ?
Ag3 Ag4 Ag14 60.49(4) . . ?
Ag5 Ag4 Ag14 166.06(6) . . ?
Ag8 Ag4 Ag14 61.31(4) . . ?
Ag15 Ag4 Ag14 129.32(6) . . ?
Se11 Ag5 Pt1 154.57(8) . . ?
Se11 Ag5 Ag10 107.36(8) . . ?
Pt1 Ag5 Ag10 59.26(4) . . ?
Se11 Ag5 Ag9 137.62(7) . . ?
Pt1 Ag5 Ag9 58.93(4) . . ?
Ag10 Ag5 Ag9 62.22(4) . . ?
Se11 Ag5 Ag1 114.83(6) . . ?
Pt1 Ag5 Ag1 58.10(4) . . ?
Ag10 Ag5 Ag1 109.00(6) . . ?
Ag9 Ag5 Ag1 107.11(5) . . ?
Se11 Ag5 Ag4 142.14(9) . . ?
Pt1 Ag5 Ag4 58.76(4) . . ?
Ag10 Ag5 Ag4 109.80(5) . . ?
Ag9 Ag5 Ag4 59.75(4) . . ?
Ag1 Ag5 Ag4 58.54(4) . . ?
Se11 Ag5 Ag6 96.36(7) . . ?
Pt1 Ag5 Ag6 58.34(4) . . ?
Ag10 Ag5 Ag6 59.03(5) . . ?
Ag9 Ag5 Ag6 108.77(6) . . ?
Ag1 Ag5 Ag6 61.85(5) . . ?
Ag4 Ag5 Ag6 108.65(5) . . ?
Se11 Ag5 Ag15 95.60(7) . . ?
Pt1 Ag5 Ag15 109.73(5) . . ?
Ag10 Ag5 Ag15 117.42(5) . . ?
Ag9 Ag5 Ag15 61.88(5) . . ?
Ag1 Ag5 Ag15 112.19(6) . . ?
Ag4 Ag5 Ag15 60.73(5) . . ?
Ag6 Ag5 Ag15 168.03(6) . . ?
Se11 Ag5 Ag16 55.27(5) . . ?
Pt1 Ag5 Ag16 107.41(5) . . ?
Ag10 Ag5 Ag16 112.95(6) . . ?
Ag9 Ag5 Ag16 166.31(6) . . ?
Ag1 Ag5 Ag16 61.25(4) . . ?
Ag4 Ag5 Ag16 114.00(5) . . ?
Ag6 Ag5 Ag16 60.26(4) . . ?
Ag15 Ag5 Ag16 127.60(6) . . ?
Se5 Ag6 Pt1 156.86(7) . . ?
Se5 Ag6 Ag10 138.34(7) . . ?
Pt1 Ag6 Ag10 59.14(4) . . ?
Se5 Ag6 Ag2 109.19(7) . . ?
Pt1 Ag6 Ag2 59.86(4) . . ?
Ag10 Ag6 Ag2 111.96(6) . . ?
Se5 Ag6 Ag11 138.50(7) . . ?
Pt1 Ag6 Ag11 58.44(4) . . ?
Ag10 Ag6 Ag11 60.52(5) . . ?
Ag2 Ag6 Ag11 63.91(5) . . ?
Se5 Ag6 Ag5 113.38(7) . . ?
Pt1 Ag6 Ag5 58.00(4) . . ?
Ag10 Ag6 Ag5 59.00(5) . . ?
Ag2 Ag6 Ag5 107.80(6) . . ?
Ag11 Ag6 Ag5 107.30(5) . . ?
Se5 Ag6 Ag16 55.75(5) . . ?
Pt1 Ag6 Ag16 106.86(5) . . ?
Ag10 Ag6 Ag16 112.63(6) . . ?
Ag2 Ag6 Ag16 111.10(6) . . ?
Ag11 Ag6 Ag16 165.27(6) . . ?
Ag5 Ag6 Ag16 59.92(4) . . ?
Se5 Ag6 Ag19 94.44(6) . . ?
Pt1 Ag6 Ag19 108.69(5) . . ?
Ag10 Ag6 Ag19 61.02(4) . . ?
Ag2 Ag6 Ag19 117.24(6) . . ?
Ag11 Ag6 Ag19 60.51(5) . . ?
Ag5 Ag6 Ag19 114.32(6) . . ?
Ag16 Ag6 Ag19 129.64(6) . . ?
Se5 Ag6 Ag1 100.14(6) . . ?
Pt1 Ag6 Ag1 56.76(4) . . ?
Ag10 Ag6 Ag1 106.16(5) . . ?
Ag2 Ag6 Ag1 58.89(5) . . ?
Ag11 Ag6 Ag1 107.94(5) . . ?
Ag5 Ag6 Ag1 58.36(4) . . ?
Ag16 Ag6 Ag1 59.96(4) . . ?
Ag19 Ag6 Ag1 165.37(6) . . ?
Se15 Ag7 Pt1 153.34(7) . . ?
Se15 Ag7 Ag8 141.01(8) . . ?
Pt1 Ag7 Ag8 58.80(4) . . ?
Se15 Ag7 Ag12 140.23(8) . . ?
Pt1 Ag7 Ag12 58.35(4) . . ?
Ag8 Ag7 Ag12 61.26(5) . . ?
Se15 Ag7 Ag18 98.11(6) . . ?
Pt1 Ag7 Ag18 108.44(5) . . ?
Ag8 Ag7 Ag18 62.88(5) . . ?
Ag12 Ag7 Ag18 59.31(5) . . ?
Se15 Ag7 Ag3 111.10(7) . . ?
Pt1 Ag7 Ag3 57.78(4) . . ?
Ag8 Ag7 Ag3 60.72(5) . . ?
Ag12 Ag7 Ag3 108.58(6) . . ?
Ag18 Ag7 Ag3 118.92(6) . . ?
Se15 Ag7 Ag17 55.06(5) . . ?
Pt1 Ag7 Ag17 103.65(5) . . ?
Ag8 Ag7 Ag17 162.42(6) . . ?
Ag12 Ag7 Ag17 112.12(6) . . ?
Ag18 Ag7 Ag17 129.84(7) . . ?
Ag3 Ag7 Ag17 110.64(6) . . ?
Se15 Ag7 Ag11 111.88(7) . . ?
Pt1 Ag7 Ag11 56.79(4) . . ?
Ag8 Ag7 Ag11 106.79(6) . . ?
Ag12 Ag7 Ag11 57.79(5) . . ?
Ag18 Ag7 Ag11 110.55(6) . . ?
Ag3 Ag7 Ag11 106.28(5) . . ?
Ag17 Ag7 Ag11 59.21(4) . . ?
Se15 Ag7 Ag2 97.78(6) . . ?
Pt1 Ag7 Ag2 55.56(4) . . ?
Ag8 Ag7 Ag2 106.60(6) . . ?
Ag12 Ag7 Ag2 104.67(5) . . ?
Ag18 Ag7 Ag2 163.32(6) . . ?
Ag3 Ag7 Ag2 59.03(5) . . ?
Ag17 Ag7 Ag2 57.81(4) . . ?
Ag11 Ag7 Ag2 58.27(4) . . ?
Se17 Ag8 Pt1 156.32(7) . . ?
Se17 Ag8 Ag9 111.67(6) . . ?
Pt1 Ag8 Ag9 58.98(4) . . ?
Se17 Ag8 Ag7 138.28(7) . . ?
Pt1 Ag8 Ag7 58.80(4) . . ?
Ag9 Ag8 Ag7 109.48(6) . . ?
Se17 Ag8 Ag4 97.97(6) . . ?
Pt1 Ag8 Ag4 58.36(4) . . ?
Ag9 Ag8 Ag4 59.57(4) . . ?
Ag7 Ag8 Ag4 108.46(5) . . ?
Se17 Ag8 Ag3 111.55(7) . . ?
Pt1 Ag8 Ag3 57.83(4) . . ?
Ag9 Ag8 Ag3 107.27(5) . . ?
Ag7 Ag8 Ag3 60.88(5) . . ?
Ag4 Ag8 Ag3 58.94(4) . . ?
Se17 Ag8 Ag12 140.13(7) . . ?
Pt1 Ag8 Ag12 57.92(4) . . ?
Ag9 Ag8 Ag12 60.95(4) . . ?
Ag7 Ag8 Ag12 60.03(5) . . ?
Ag4 Ag8 Ag12 107.82(5) . . ?
Ag3 Ag8 Ag12 107.75(5) . . ?
Se17 Ag8 Ag14 53.95(5) . . ?
Pt1 Ag8 Ag14 107.41(5) . . ?
Ag9 Ag8 Ag14 113.59(6) . . ?
Ag7 Ag8 Ag14 113.61(6) . . ?
Ag4 Ag8 Ag14 60.21(4) . . ?
Ag3 Ag8 Ag14 59.54(4) . . ?
Ag12 Ag8 Ag14 165.32(6) . . ?
Se17 Ag8 Ag18 97.94(6) . . ?
Pt1 Ag8 Ag18 105.74(5) . . ?
Ag9 Ag8 Ag18 112.39(6) . . ?
Ag7 Ag8 Ag18 59.45(5) . . ?
Ag4 Ag8 Ag18 164.00(6) . . ?
Ag3 Ag8 Ag18 115.93(6) . . ?
Ag12 Ag8 Ag18 57.84(4) . . ?
Ag14 Ag8 Ag18 132.50(6) . . ?
Se21 Ag9 Pt1 156.17(7) . . ?
Se21 Ag9 Ag8 109.01(6) . . ?
Pt1 Ag9 Ag8 59.38(4) . . ?
Se21 Ag9 Ag5 139.79(6) . . ?
Pt1 Ag9 Ag5 59.05(4) . . ?
Ag8 Ag9 Ag5 110.47(5) . . ?
Se21 Ag9 Ag4 137.05(7) . . ?
Pt1 Ag9 Ag4 59.27(4) . . ?
Ag8 Ag9 Ag4 61.85(4) . . ?
Ag5 Ag9 Ag4 61.10(4) . . ?
Se21 Ag9 Ag20 55.45(5) . . ?
Pt1 Ag9 Ag20 107.69(5) . . ?
Ag8 Ag9 Ag20 113.70(6) . . ?
Ag5 Ag9 Ag20 112.83(6) . . ?
Ag4 Ag9 Ag20 166.94(6) . . ?
Se21 Ag9 Ag12 98.13(6) . . ?
Pt1 Ag9 Ag12 58.19(4) . . ?
Ag8 Ag9 Ag12 61.40(5) . . ?
Ag5 Ag9 Ag12 107.03(5) . . ?
Ag4 Ag9 Ag12 109.94(5) . . ?
Ag20 Ag9 Ag12 59.40(4) . . ?
Se21 Ag9 Ag10 114.22(6) . . ?
Pt1 Ag9 Ag10 58.08(4) . . ?
Ag8 Ag9 Ag10 108.69(5) . . ?
Ag5 Ag9 Ag10 58.72(5) . . ?
Ag4 Ag9 Ag10 108.09(5) . . ?
Ag20 Ag9 Ag10 60.61(4) . . ?
Ag12 Ag9 Ag10 58.75(4) . . ?
Se21 Ag9 Ag15 95.24(6) . . ?
Pt1 Ag9 Ag15 108.55(5) . . ?
Ag8 Ag9 Ag15 116.29(6) . . ?
Ag5 Ag9 Ag15 60.30(5) . . ?
Ag4 Ag9 Ag15 60.63(4) . . ?
Ag20 Ag9 Ag15 128.18(5) . . ?
Ag12 Ag9 Ag15 166.38(6) . . ?
Ag10 Ag9 Ag15 112.95(6) . . ?
Se14 Ag10 Pt1 153.40(7) . . ?
Se14 Ag10 Ag5 106.94(6) . . ?
Pt1 Ag10 Ag5 59.07(4) . . ?
Se14 Ag10 Ag6 137.84(6) . . ?
Pt1 Ag10 Ag6 59.30(4) . . ?
Ag5 Ag10 Ag6 61.97(5) . . ?
Se14 Ag10 Ag11 143.23(7) . . ?
Pt1 Ag10 Ag11 58.37(4) . . ?
Ag5 Ag10 Ag11 109.35(5) . . ?
Ag6 Ag10 Ag11 60.17(4) . . ?
Se14 Ag10 Ag12 113.15(6) . . ?
Pt1 Ag10 Ag12 58.75(4) . . ?
Ag5 Ag10 Ag12 108.79(6) . . ?
Ag6 Ag10 Ag12 108.77(5) . . ?
Ag11 Ag10 Ag12 59.59(4) . . ?
Se14 Ag10 Ag9 95.76(6) . . ?
Pt1 Ag10 Ag9 57.78(4) . . ?
Ag5 Ag10 Ag9 59.05(4) . . ?
Ag6 Ag10 Ag9 108.58(5) . . ?
Ag11 Ag10 Ag9 107.63(5) . . ?
Ag12 Ag10 Ag9 60.57(4) . . ?
Se14 Ag10 Ag20 55.20(5) . . ?
Pt1 Ag10 Ag20 106.37(5) . . ?
Ag5 Ag10 Ag20 111.95(6) . . ?
Ag6 Ag10 Ag20 165.66(6) . . ?
Ag11 Ag10 Ag20 114.00(5) . . ?
Ag12 Ag10 Ag20 59.55(4) . . ?
Ag9 Ag10 Ag20 59.28(4) . . ?
Se14 Ag10 Ag19 97.04(6) . . ?
Pt1 Ag10 Ag19 109.48(5) . . ?
Ag5 Ag10 Ag19 117.68(5) . . ?
Ag6 Ag10 Ag19 61.83(5) . . ?
Ag11 Ag10 Ag19 60.68(5) . . ?
Ag12 Ag10 Ag19 112.73(6) . . ?
Ag9 Ag10 Ag19 167.14(6) . . ?
Ag20 Ag10 Ag19 128.66(6) . . ?
Se8 Ag11 Pt1 154.66(7) . . ?
Se8 Ag11 Ag12 111.52(6) . . ?
Pt1 Ag11 Ag12 59.20(4) . . ?
Se8 Ag11 Ag6 139.15(7) . . ?
Pt1 Ag11 Ag6 59.18(4) . . ?
Ag12 Ag11 Ag6 108.68(6) . . ?
Se8 Ag11 Ag10 140.55(7) . . ?
Pt1 Ag11 Ag10 58.95(4) . . ?
Ag12 Ag11 Ag10 60.33(4) . . ?
Ag6 Ag11 Ag10 59.32(4) . . ?
Se8 Ag11 Ag19 95.08(7) . . ?
Pt1 Ag11 Ag19 110.26(5) . . ?
Ag12 Ag11 Ag19 113.68(6) . . ?
Ag6 Ag11 Ag19 61.68(5) . . ?
Ag10 Ag11 Ag19 61.04(5) . . ?
Se8 Ag11 Ag17 55.40(5) . . ?
Pt1 Ag11 Ag17 104.63(5) . . ?
Ag12 Ag11 Ag17 114.26(5) . . ?
Ag6 Ag11 Ag17 112.74(6) . . ?
Ag10 Ag11 Ag17 163.53(6) . . ?
Ag19 Ag11 Ag17 130.33(6) . . ?
Se8 Ag11 Ag7 97.30(6) . . ?
Pt1 Ag11 Ag7 57.40(4) . . ?
Ag12 Ag11 Ag7 59.51(4) . . ?
Ag6 Ag11 Ag7 109.10(6) . . ?
Ag10 Ag11 Ag7 107.40(5) . . ?
Ag19 Ag11 Ag7 167.46(6) . . ?
Ag17 Ag11 Ag7 59.85(4) . . ?
Se8 Ag11 Ag2 112.42(6) . . ?
Pt1 Ag11 Ag2 57.87(4) . . ?
Ag12 Ag11 Ag2 110.55(6) . . ?
Ag6 Ag11 Ag2 57.66(5) . . ?
Ag10 Ag11 Ag2 106.01(6) . . ?
Ag19 Ag11 Ag2 112.82(6) . . ?
Ag17 Ag11 Ag2 59.95(5) . . ?
Ag7 Ag11 Ag2 63.94(5) . . ?
Se24 Ag12 Pt1 157.72(7) . . ?
Se24 Ag12 Ag11 111.89(7) . . ?
Pt1 Ag12 Ag11 58.51(4) . . ?
Se24 Ag12 Ag10 99.08(7) . . ?
Pt1 Ag12 Ag10 58.65(4) . . ?
Ag11 Ag12 Ag10 60.08(4) . . ?
Se24 Ag12 Ag18 92.76(7) . . ?
Pt1 Ag12 Ag18 109.52(5) . . ?
Ag11 Ag12 Ag18 115.97(6) . . ?
Ag10 Ag12 Ag18 168.14(6) . . ?
Se24 Ag12 Ag20 56.05(5) . . ?
Pt1 Ag12 Ag20 107.81(5) . . ?
Ag11 Ag12 Ag20 116.16(6) . . ?
Ag10 Ag12 Ag20 61.46(4) . . ?
Ag18 Ag12 Ag20 126.25(6) . . ?
Se24 Ag12 Ag7 138.70(7) . . ?
Pt1 Ag12 Ag7 58.32(4) . . ?
Ag11 Ag12 Ag7 62.70(5) . . ?
Ag10 Ag12 Ag7 109.69(5) . . ?
Ag18 Ag12 Ag7 60.62(5) . . ?
Ag20 Ag12 Ag7 165.25(6) . . ?
Se24 Ag12 Ag9 114.13(6) . . ?
Pt1 Ag12 Ag9 57.79(4) . . ?
Ag11 Ag12 Ag9 108.10(5) . . ?
Ag10 Ag12 Ag9 60.68(4) . . ?
Ag18 Ag12 Ag9 113.55(6) . . ?
Ag20 Ag12 Ag9 59.93(4) . . ?
Ag7 Ag12 Ag9 105.75(6) . . ?
Se24 Ag12 Ag8 138.78(7) . . ?
Pt1 Ag12 Ag8 57.89(4) . . ?
Ag11 Ag12 Ag8 108.66(5) . . ?
Ag10 Ag12 Ag8 107.22(5) . . ?
Ag18 Ag12 Ag8 62.45(5) . . ?
Ag20 Ag12 Ag8 110.88(6) . . ?
Ag7 Ag12 Ag8 58.72(5) . . ?
Ag9 Ag12 Ag8 57.65(4) . . ?
Se9 Ag13 Se3 124.61(8) . . ?
Se9 Ag13 Se2 115.25(8) . . ?
Se3 Ag13 Se2 119.96(8) . . ?
Se9 Ag13 Ag3 75.06(6) . . ?
Se3 Ag13 Ag3 126.51(7) . . ?
Se2 Ag13 Ag3 71.28(6) . . ?
Se9 Ag13 Ag2 131.40(7) . . ?
Se3 Ag13 Ag2 71.81(7) . . ?
Se2 Ag13 Ag2 72.83(6) . . ?
Ag3 Ag13 Ag2 62.17(5) . . ?
Se9 Ag13 Ag1 81.45(6) . . ?
Se3 Ag13 Ag1 74.15(6) . . ?
Se2 Ag13 Ag1 121.48(7) . . ?
Ag3 Ag13 Ag1 59.33(4) . . ?
Ag2 Ag13 Ag1 57.93(4) . . ?
Se10 Ag14 Se17 117.28(7) . . ?
Se10 Ag14 Se20 120.82(7) . . ?
Se17 Ag14 Se20 121.79(7) . . ?
Se10 Ag14 Ag3 56.76(5) . . ?
Se17 Ag14 Ag3 112.27(7) . . ?
Se20 Ag14 Ag3 96.51(6) . . ?
Se10 Ag14 Ag4 113.61(6) . . ?
Se17 Ag14 Ag4 97.59(6) . . ?
Se20 Ag14 Ag4 56.28(5) . . ?
Ag3 Ag14 Ag4 58.18(4) . . ?
Se10 Ag14 Ag8 96.89(6) . . ?
Se17 Ag14 Ag8 55.24(5) . . ?
Se20 Ag14 Ag8 113.08(6) . . ?
Ag3 Ag14 Ag8 59.00(4) . . ?
Ag4 Ag14 Ag8 58.48(4) . . ?
Se12 Ag15 Se22 116.09(10) . . ?
Se12 Ag15 Se19 125.07(10) . . ?
Se22 Ag15 Se19 118.27(7) . . ?
Se12 Ag15 Ag5 77.62(7) . . ?
Se22 Ag15 Ag5 76.03(6) . . ?
Se19 Ag15 Ag5 122.67(7) . . ?
Se12 Ag15 Ag4 84.02(8) . . ?
Se22 Ag15 Ag4 126.00(7) . . ?
Se19 Ag15 Ag4 70.87(6) . . ?
Ag5 Ag15 Ag4 59.32(4) . . ?
Se12 Ag15 Ag9 131.33(8) . . ?
Se22 Ag15 Ag9 73.61(6) . . ?
Se19 Ag15 Ag9 73.05(6) . . ?
Ag5 Ag15 Ag9 57.82(4) . . ?
Ag4 Ag15 Ag9 57.97(4) . . ?
Se11 Ag16 Se4 120.82(9) . . ?
Se11 Ag16 Se5 116.39(9) . . ?
Se4 Ag16 Se5 122.79(7) . . ?
Se11 Ag16 Ag5 56.37(5) . . ?
Se4 Ag16 Ag5 97.12(6) . . ?
Se5 Ag16 Ag5 113.88(7) . . ?
Se11 Ag16 Ag6 96.81(7) . . ?
Se4 Ag16 Ag6 114.34(6) . . ?
Se5 Ag16 Ag6 56.36(5) . . ?
Ag5 Ag16 Ag6 59.83(4) . . ?
Se11 Ag16 Ag1 113.32(6) . . ?
Se4 Ag16 Ag1 55.54(5) . . ?
Se5 Ag16 Ag1 101.22(6) . . ?
Ag5 Ag16 Ag1 58.60(4) . . ?
Ag6 Ag16 Ag1 60.80(4) . . ?
Se1 Ag17 Se15 120.84(8) . . ?
Se1 Ag17 Se8 121.24(8) . . ?
Se15 Ag17 Se8 117.75(7) . . ?
Se1 Ag17 Ag11 101.86(6) . . ?
Se15 Ag17 Ag11 114.07(6) . . ?
Se8 Ag17 Ag11 55.81(5) . . ?
Se1 Ag17 Ag7 117.25(7) . . ?
Se15 Ag17 Ag7 55.64(5) . . ?
Se8 Ag17 Ag7 98.38(6) . . ?
Ag11 Ag17 Ag7 60.93(5) . . ?
Se1 Ag17 Ag2 55.65(5) . . ?
Se15 Ag17 Ag2 103.49(7) . . ?
Se8 Ag17 Ag2 113.94(7) . . ?
Ag11 Ag17 Ag2 61.14(5) . . ?
Ag7 Ag17 Ag2 64.75(5) . . ?
Se23 Ag18 Se18 119.47(9) . . ?
Se23 Ag18 Se16 123.03(10) . . ?
Se18 Ag18 Se16 117.19(8) . . ?
Se23 Ag18 Ag12 78.85(6) . . ?
Se18 Ag18 Ag12 123.29(7) . . ?
Se16 Ag18 Ag12 75.61(6) . . ?
Se23 Ag18 Ag7 131.34(7) . . ?
Se18 Ag18 Ag7 71.30(6) . . ?
Se16 Ag18 Ag7 73.03(6) . . ?
Ag12 Ag18 Ag7 60.07(4) . . ?
Se23 Ag18 Ag8 80.26(7) . . ?
Se18 Ag18 Ag8 70.78(6) . . ?
Se16 Ag18 Ag8 124.75(6) . . ?
Ag12 Ag18 Ag8 59.72(4) . . ?
Ag7 Ag18 Ag8 57.67(4) . . ?
Se13 Ag19 Se6 114.87(7) . . ?
Se13 Ag19 Se7 125.00(9) . . ?
Se6 Ag19 Se7 119.92(8) . . ?
Se13 Ag19 Ag11 79.33(6) . . ?
Se6 Ag19 Ag11 124.40(8) . . ?
Se7 Ag19 Ag11 74.39(6) . . ?
Se13 Ag19 Ag10 74.19(6) . . ?
Se6 Ag19 Ag10 73.88(6) . . ?
Se7 Ag19 Ag10 125.06(7) . . ?
Ag11 Ag19 Ag10 58.28(4) . . ?
Se13 Ag19 Ag6 126.52(7) . . ?
Se6 Ag19 Ag6 73.71(7) . . ?
Se7 Ag19 Ag6 75.35(7) . . ?
Ag11 Ag19 Ag6 57.81(4) . . ?
Ag10 Ag19 Ag6 57.15(4) . . ?
Se21 Ag20 Se14 118.45(7) . . ?
Se21 Ag20 Se24 121.43(7) . . ?
Se14 Ag20 Se24 120.10(8) . . ?
Se21 Ag20 Ag12 100.07(6) . . ?
Se14 Ag20 Ag12 113.55(6) . . ?
Se24 Ag20 Ag12 57.09(5) . . ?
Se21 Ag20 Ag9 56.83(5) . . ?
Se14 Ag20 Ag9 97.03(6) . . ?
Se24 Ag20 Ag9 115.84(6) . . ?
Ag12 Ag20 Ag9 60.67(4) . . ?
Se21 Ag20 Ag10 115.07(6) . . ?
Se14 Ag20 Ag10 56.17(5) . . ?
Se24 Ag20 Ag10 98.02(6) . . ?
Ag12 Ag20 Ag10 58.99(4) . . ?
Ag9 Ag20 Ag10 60.11(4) . . ?
C2 C1 P1 117.9(13) . . ?
C3 C2 C1 111.5(17) . . ?
C4 C3 C8 120.0 . . ?
C4 C3 C2 121.2(17) . . ?
C8 C3 C2 118.8(17) . . ?
C5 C4 C3 120.0 . . ?
C4 C5 C6 120.0 . . ?
C7 C6 C5 120.0 . . ?
C8 C7 C6 120.0 . . ?
C7 C8 C3 120.0 . . ?
C10 C9 P1 114.9(15) . . ?
C11 C10 C9 121.2(19) . . ?
C12 C11 C16 120.0 . . ?
C12 C11 C10 117(2) . . ?
C16 C11 C10 122(2) . . ?
C13 C12 C11 120.0 . . ?
C12 C13 C14 120.0 . . ?
C15 C14 C13 120.0 . . ?
C16 C15 C14 120.0 . . ?
C15 C16 C11 120.0 . . ?
C18 C17 P2 116.7(15) . . ?
C17 C18 C19 119.6(17) . . ?
C20 C19 C24 120.0 . . ?
C20 C19 C18 119.6(16) . . ?
C24 C19 C18 120.4(16) . . ?
C19 C20 C21 120.0 . . ?
C22 C21 C20 120.0 . . ?
C21 C22 C23 120.0 . . ?
C22 C23 C24 120.0 . . ?
C23 C24 C19 120.0 . . ?
C26 C25 P2 118.5(14) . . ?
C27 C26 C25 111.9(17) . . ?
C28 C27 C32 120.0 . . ?
C28 C27 C26 120.3(12) . . ?
C32 C27 C26 119.5(12) . . ?
C29 C28 C27 120.0 . . ?
C28 C29 C30 120.0 . . ?
C29 C30 C31 120.0 . . ?
C30 C31 C32 120.0 . . ?
C31 C32 C27 120.0 . . ?
C34 C33 P3 108.8(16) . . ?
C35 C34 C33 158(3) . . ?
C35B C34 C33 116(3) . . ?
C36 C35 C40 120.0 . . ?
C36 C35 C34 125.0(13) . . ?
C40 C35 C34 110.4(8) . . ?
C37 C36 C35 120.0 . . ?
C36 C37 C38 120.0 . . ?
C39 C38 C37 120.0 . . ?
C38 C39 C40 120.0 . . ?
C39 C40 C35 120.0 . . ?
C36B C35B C40B 120.0 . . ?
C36B C35B C34 122(3) . . ?
C40B C35B C34 118(3) . . ?
C35B C36B C37B 120.0 . . ?
C38B C37B C36B 120.0 . . ?
C37B C38B C39B 120.0 . . ?
C38B C39B C40B 120.0 . . ?
C39B C40B C35B 120.0 . . ?
C42 C41 P3 116.7(14) . . ?
C43 C42 C41 112.0(16) . . ?
C44 C43 C48 120.0 . . ?
C44 C43 C42 120.0(12) . . ?
C48 C43 C42 120.0(12) . . ?
C45 C44 C43 120.0 . . ?
C46 C45 C44 120.0 . . ?
C45 C46 C47 120.0 . . ?
C48 C47 C46 120.0 . . ?
C47 C48 C43 120.0 . . ?
C50 C49 P4 114.4(15) . . ?
C51 C50 C49 135(2) . . ?
C51B C50 C49 101.8(18) . . ?
C52 C51 C56 120.0 . . ?
C52 C51 C50 108(2) . . ?
C56 C51 C50 132(2) . . ?
C53 C52 C51 120.0 . . ?
C52 C53 C54 120.0 . . ?
C53 C54 C55 120.0 . . ?
C54 C55 C56 120.0 . . ?
C55 C56 C51 120.0 . . ?
C52B C51B C56B 120.0 . . ?
C52B C51B C50 103(2) . . ?
C56B C51B C50 137(2) . . ?
C53B C52B C51B 120.0 . . ?
C52B C53B C54B 120.0 . . ?
C55B C54B C53B 120.0 . . ?
C54B C55B C56B 120.0 . . ?
C55B C56B C51B 120.0 . . ?
C58 C57 P4 110.1(14) . . ?
C59 C58 C57 112.4(17) . . ?
C59B C58 C57 116.7(18) . . ?
C60 C59 C64 120.0 . . ?
C60 C59 C58 130.3(8) . . ?
C64 C59 C58 109.7(8) . . ?
C61 C60 C59 120.0 . . ?
C60 C61 C62 120.0 . . ?
C61 C62 C63 120.0 . . ?
C64 C63 C62 120.0 . . ?
C63 C64 C59 120.0 . . ?
C60B C59B C64B 120.0 . . ?
C60B C59B C58 119.8(16) . . ?
C64B C59B C58 118.1(16) . . ?
C59B C60B C61B 120.0 . . ?
C60B C61B C62B 120.0 . . ?
C63B C62B C61B 120.0 . . ?
C62B C63B C64B 120.0 . . ?
C63B C64B C59B 120.0 . . ?
C66 C65 P5 114.6(14) . . ?
C67 C66 C65 106.9(17) . . ?
C68 C67 C72 120.0 . . ?
C68 C67 C66 119.7(18) . . ?
C72 C67 C66 120.1(18) . . ?
C69 C68 C67 120.0 . . ?
C70 C69 C68 120.0 . . ?
C71 C70 C69 120.0 . . ?
C70 C71 C72 120.0 . . ?
C71 C72 C67 120.0 . . ?
C74 C73 P5 115.1(15) . . ?
C75 C74 C73 123.0(17) . . ?
C76 C75 C80 120.0 . . ?
C76 C75 C74 117.8(12) . . ?
C80 C75 C74 122.0(12) . . ?
C77 C76 C75 120.0 . . ?
C78 C77 C76 120.0 . . ?
C77 C78 C79 120.0 . . ?
C78 C79 C80 120.0 . . ?
C79 C80 C75 120.0 . . ?
C82 C81 P6 113.1(15) . . ?
C83 C82 C81 114.2(19) . . ?
C84 C83 C88 120.0 . . ?
C84 C83 C82 128.4(19) . . ?
C88 C83 C82 111.1(19) . . ?
C85 C84 C83 120.0 . . ?
C86 C85 C84 120.0 . . ?
C85 C86 C87 120.0 . . ?
C88 C87 C86 120.0 . . ?
C87 C88 C83 120.0 . . ?
C90 C89 P6 111.5(16) . . ?
C91 C90 C89 122(3) . . ?
C92 C91 C96 120.0 . . ?
C92 C91 C90 117(2) . . ?
C96 C91 C90 122(2) . . ?
C93 C92 C91 120.0 . . ?
C94 C93 C92 120.0 . . ?
C95 C94 C93 120.0 . . ?
C94 C95 C96 120.0 . . ?
C95 C96 C91 120.0 . . ?
C98 C97 P7 112.5(12) . . ?
C99 C98 C97 109.0(15) . . ?
C100 C99 C104 120.0 . . ?
C100 C99 C98 121.1(13) . . ?
C104 C99 C98 118.8(13) . . ?
C99 C100 C101 120.0 . . ?
C102 C101 C100 120.0 . . ?
C101 C102 C103 120.0 . . ?
C104 C103 C102 120.0 . . ?
C103 C104 C99 120.0 . . ?
C106 C105 P7 114.1(11) . . ?
C107 C106 C105 108.9(13) . . ?
C108 C107 C112 120.0 . . ?
C108 C107 C106 117.4(11) . . ?
C112 C107 C106 122.6(11) . . ?
C107 C108 C109 120.0 . . ?
C110 C109 C108 120.0 . . ?
C109 C110 C111 120.0 . . ?
C112 C111 C110 120.0 . . ?
C111 C112 C107 120.0 . . ?
C114 C113 P8 118.4(17) . . ?
C115 C114 C113 112.1(18) . . ?
C116 C115 C120 120.0 . . ?
C116 C115 C114 120(2) . . ?
C120 C115 C114 119(2) . . ?
C115 C116 C117 120.0 . . ?
C118 C117 C116 120.0 . . ?
C117 C118 C119 120.0 . . ?
C120 C119 C118 120.0 . . ?
C119 C120 C115 120.0 . . ?
C122 C121 P8 118.3(18) . . ?
C123 C122 C121 121(3) . . ?
C124 C123 C128 120.0 . . ?
C124 C123 C122 127(3) . . ?
C128 C123 C122 111(3) . . ?
C123 C124 C125 120.0 . . ?
C124 C125 C126 120.0 . . ?
C125 C126 C127 120.0 . . ?
C128 C127 C126 120.0 . . ?
C127 C128 C123 120.0 . . ?
C130 C129 P9 121.7(14) . . ?
C131 C130 C129 125.2(17) . . ?
C132 C131 C136 120.0 . . ?
C132 C131 C130 131.1(10) . . ?
C136 C131 C130 105.1(8) . . ?
C133 C132 C131 120.0 . . ?
C132 C133 C134 120.0 . . ?
C135 C134 C133 120.0 . . ?
C136 C135 C134 120.0 . . ?
C135 C136 C131 120.0 . . ?
C138 C137 P9 105.8(19) . . ?
C1D8 C137 P9 119.3(14) . . ?
C137 C138 C139 93(2) . . ?
C140 C139 C144 120.0 . . ?
C140 C139 C138 111(2) . . ?
C144 C139 C138 128(2) . . ?
C139 C140 C141 120.0 . . ?
C142 C141 C140 120.0 . . ?
C143 C142 C141 120.0 . . ?
C142 C143 C144 120.0 . . ?
C143 C144 C139 120.0 . . ?
C1D9 C1D8 C137 118(2) . . ?
C1E0 C1D9 C1E4 120.0 . . ?
C1E0 C1D9 C1D8 121(2) . . ?
C1E4 C1D9 C1D8 119(2) . . ?
C1D9 C1E0 C1E1 120.0 . . ?
C1E2 C1E1 C1E0 120.0 . . ?
C1E1 C1E2 C1E3 120.0 . . ?
C1E4 C1E3 C1E2 120.0 . . ?
C1E3 C1E4 C1D9 120.0 . . ?
C146 C145 P10 106.2(18) . . ?
C1E6 C145 P10 122.4(13) . . ?
C147 C146 C145 112.3(18) . . ?
C148 C147 C152 120.0 . . ?
C148 C147 C146 118(2) . . ?
C152 C147 C146 122(2) . . ?
C147 C148 C149 120.0 . . ?
C150 C149 C148 120.0 . . ?
C151 C150 C149 120.0 . . ?
C150 C151 C152 120.0 . . ?
C151 C152 C147 120.0 . . ?
C1E7 C1E6 C145 123(2) . . ?
C1E8 C1E7 C1F2 120.0 . . ?
C1E8 C1E7 C1E6 107(2) . . ?
C1F2 C1E7 C1E6 133(2) . . ?
C1E7 C1E8 C1E9 120.0 . . ?
C1F0 C1E9 C1E8 120.0 . . ?
C1F1 C1F0 C1E9 120.0 . . ?
C1F0 C1F1 C1F2 120.0 . . ?
C1F1 C1F2 C1E7 120.0 . . ?
C154 C153 P10 128.5(15) . . ?
C1F4 C153 P10 112.0(16) . . ?
C155 C154 C153 114(2) . . ?
C156 C155 C160 120.0 . . ?
C156 C155 C154 123(3) . . ?
C160 C155 C154 117(3) . . ?
C157 C156 C155 120.0 . . ?
C156 C157 C158 120.0 . . ?
C159 C158 C157 120.0 . . ?
C158 C159 C160 120.0 . . ?
C159 C160 C155 120.0 . . ?
C1F5 C1F4 C153 122(3) . . ?
C1F6 C1F5 C1G0 120.0 . . ?
C1F6 C1F5 C1F4 125(3) . . ?
C1G0 C1F5 C1F4 112(3) . . ?
C1F7 C1F6 C1F5 120.0 . . ?
C1F6 C1F7 C1F8 120.0 . . ?
C1F9 C1F8 C1F7 120.0 . . ?
C1G0 C1F9 C1F8 120.0 . . ?
C1F9 C1G0 C1F5 120.0 . . ?
C162 C161 P11 115.0(13) . . ?
C1G2 C161 P11 114.9(14) . . ?
C163 C162 C161 112(2) . . ?
C164 C163 C168 120.0 . . ?
C164 C163 C162 123(3) . . ?
C168 C163 C162 117(3) . . ?
C163 C164 C165 120.0 . . ?
C166 C165 C164 120.0 . . ?
C165 C166 C167 120.0 . . ?
C168 C167 C166 120.0 . . ?
C167 C168 C163 120.0 . . ?
C1G3 C1G2 C161 108(3) . . ?
C1G4 C1G3 C1G8 120.0 . . ?
C1G4 C1G3 C1G2 120(3) . . ?
C1G8 C1G3 C1G2 120(3) . . ?
C1G3 C1G4 C1G5 120.0 . . ?
C1G6 C1G5 C1G4 120.0 . . ?
C1G5 C1G6 C1G7 120.0 . . ?
C1G6 C1G7 C1G8 120.0 . . ?
C1G7 C1G8 C1G3 120.0 . . ?
C170 C169 P11 113.5(16) . . ?
C1H0 C169 P11 114.2(18) . . ?
C171 C170 C169 129(2) . . ?
C172 C171 C176 120.0 . . ?
C172 C171 C170 126(2) . . ?
C176 C171 C170 113(2) . . ?
C173 C172 C171 120.0 . . ?
C172 C173 C174 120.0 . . ?
C175 C174 C173 120.0 . . ?
C176 C175 C174 120.0 . . ?
C175 C176 C171 120.0 . . ?
C1H1 C1H0 C169 111(2) . . ?
C1H2 C1H1 C1H6 120.0 . . ?
C1H2 C1H1 C1H0 126(3) . . ?
C1H6 C1H1 C1H0 114(3) . . ?
C1H1 C1H2 C1H3 120.0 . . ?
C1H2 C1H3 C1H4 120.0 . . ?
C1H5 C1H4 C1H3 120.0 . . ?
C1H4 C1H5 C1H6 120.0 . . ?
C1H5 C1H6 C1H1 120.0 . . ?
C178 C177 P12 121.4(15) . . ?
C179 C178 C177 110.2(19) . . ?
C180 C179 C184 120.0 . . ?
C180 C179 C178 132(2) . . ?
C184 C179 C178 108(2) . . ?
C181 C180 C179 120.0 . . ?
C180 C181 C182 120.0 . . ?
C181 C182 C183 120.0 . . ?
C184 C183 C182 120.0 . . ?
C183 C184 C179 120.0 . . ?
C186 C185 P12 118.3(15) . . ?
C187 C186 C185 104.0(9) . . ?
C188 C187 C192 120.0 . . ?
C188 C187 C186 122(2) . . ?
C192 C187 C186 115(2) . . ?
C187 C188 C189 120.0 . . ?
C190 C189 C188 120.0 . . ?
C191 C190 C189 120.0 . . ?
C190 C191 C192 120.0 . . ?
C191 C192 C187 120.0 . . ?
C1 P1 C9 108.2(9) . . ?
C1 P1 Se2 108.5(7) . . ?
C9 P1 Se2 110.5(8) . . ?
C1 P1 Se1 107.7(8) . . ?
C9 P1 Se1 107.7(7) . . ?
Se2 P1 Se1 114.2(2) . . ?
C25 P2 C17 108.3(8) . . ?
C25 P2 Se3 108.9(6) . . ?
C17 P2 Se3 110.8(7) . . ?
C25 P2 Se4 106.3(6) . . ?
C17 P2 Se4 107.5(7) . . ?
Se3 P2 Se4 114.70(19) . . ?
C33 P3 C41 105.9(10) . . ?
C33 P3 Se6 108.6(8) . . ?
C41 P3 Se6 110.2(7) . . ?
C33 P3 Se5 110.3(7) . . ?
C41 P3 Se5 107.5(7) . . ?
Se6 P3 Se5 114.1(2) . . ?
C57 P4 C49 109.9(10) . . ?
C57 P4 Se7 111.4(8) . . ?
C49 P4 Se7 110.1(8) . . ?
C57 P4 Se8 104.9(8) . . ?
C49 P4 Se8 106.0(7) . . ?
Se7 P4 Se8 114.2(2) . . ?
C73 P5 C65 112.9(9) . . ?
C73 P5 Se9 106.9(7) . . ?
C65 P5 Se9 108.4(6) . . ?
C73 P5 Se10 108.7(7) . . ?
C65 P5 Se10 105.7(6) . . ?
Se9 P5 Se10 114.4(2) . . ?
C81 P6 C89 106.3(12) . . ?
C81 P6 Se11 99.3(9) . . ?
C89 P6 Se11 107.1(10) . . ?
C81 P6 Se12 117.6(10) . . ?
C89 P6 Se12 110.4(9) . . ?
Se11 P6 Se12 115.0(3) . . ?
C105 P7 C97 107.9(7) . . ?
C105 P7 Se14 106.8(5) . . ?
C97 P7 Se14 108.8(6) . . ?
C105 P7 Se13 107.7(6) . . ?
C97 P7 Se13 109.4(5) . . ?
Se14 P7 Se13 116.0(2) . . ?
C121 P8 C113 108.9(11) . . ?
C121 P8 Se16 109.9(9) . . ?
C113 P8 Se16 105.1(7) . . ?
C121 P8 Se15 107.7(9) . . ?
C113 P8 Se15 109.9(7) . . ?
Se16 P8 Se15 115.1(2) . . ?
C129 P9 C137 105.0(9) . . ?
C129 P9 Se18 114.7(7) . . ?
C137 P9 Se18 105.4(6) . . ?
C129 P9 Se17 105.5(7) . . ?
C137 P9 Se17 111.5(6) . . ?
Se18 P9 Se17 114.4(2) . . ?
C153 P10 C145 107.3(10) . . ?
C153 P10 Se19 108.8(7) . . ?
C145 P10 Se19 108.6(6) . . ?
C153 P10 Se20 110.5(7) . . ?
C145 P10 Se20 107.7(5) . . ?
Se19 P10 Se20 113.8(2) . . ?
C169 P11 C161 111.7(8) . . ?
C169 P11 Se22 106.5(6) . . ?
C161 P11 Se22 108.1(6) . . ?
C169 P11 Se21 108.0(6) . . ?
C161 P11 Se21 108.4(6) . . ?
Se22 P11 Se21 114.21(18) . . ?
C177 P12 C185 103.1(10) . . ?
C177 P12 Se23 106.4(8) . . ?
C185 P12 Se23 113.5(9) . . ?
C177 P12 Se24 108.6(7) . . ?
C185 P12 Se24 109.7(10) . . ?
Se23 P12 Se24 114.7(2) . . ?
Ag1 Pt1 Ag11 118.65(4) . . ?
Ag1 Pt1 Ag9 113.63(4) . . ?
Ag11 Pt1 Ag9 116.51(4) . . ?
Ag1 Pt1 Ag5 63.02(4) . . ?
Ag11 Pt1 Ag5 115.19(5) . . ?
Ag9 Pt1 Ag5 62.03(4) . . ?
Ag1 Pt1 Ag3 63.89(4) . . ?
Ag11 Pt1 Ag3 119.12(4) . . ?
Ag9 Pt1 Ag3 114.61(4) . . ?
Ag5 Pt1 Ag3 116.65(5) . . ?
Ag1 Pt1 Ag10 115.15(4) . . ?
Ag11 Pt1 Ag10 62.68(4) . . ?
Ag9 Pt1 Ag10 64.14(4) . . ?
Ag5 Pt1 Ag10 61.67(4) . . ?
Ag3 Pt1 Ag10 178.17(5) . . ?
Ag1 Pt1 Ag7 119.50(5) . . ?
Ag11 Pt1 Ag7 65.81(4) . . ?
Ag9 Pt1 Ag7 114.75(4) . . ?
Ag5 Pt1 Ag7 176.77(4) . . ?
Ag3 Pt1 Ag7 64.26(5) . . ?
Ag10 Pt1 Ag7 117.37(5) . . ?
Ag1 Pt1 Ag8 116.47(5) . . ?
Ag11 Pt1 Ag8 117.19(4) . . ?
Ag9 Pt1 Ag8 61.64(4) . . ?
Ag5 Pt1 Ag8 114.92(4) . . ?
Ag3 Pt1 Ag8 64.15(4) . . ?
Ag10 Pt1 Ag8 115.62(4) . . ?
Ag7 Pt1 Ag8 62.40(4) . . ?
Ag1 Pt1 Ag12 177.16(4) . . ?
Ag11 Pt1 Ag12 62.29(4) . . ?
Ag9 Pt1 Ag12 64.03(4) . . ?
Ag5 Pt1 Ag12 114.14(4) . . ?
Ag3 Pt1 Ag12 118.30(4) . . ?
Ag10 Pt1 Ag12 62.60(4) . . ?
Ag7 Pt1 Ag12 63.33(4) . . ?
Ag8 Pt1 Ag12 64.19(4) . . ?
Ag1 Pt1 Ag6 65.40(4) . . ?
Ag11 Pt1 Ag6 62.37(4) . . ?
Ag9 Pt1 Ag6 115.80(4) . . ?
Ag5 Pt1 Ag6 63.66(4) . . ?
Ag3 Pt1 Ag6 118.64(4) . . ?
Ag10 Pt1 Ag6 61.57(4) . . ?
Ag7 Pt1 Ag6 118.93(5) . . ?
Ag8 Pt1 Ag6 177.15(5) . . ?
Ag12 Pt1 Ag6 113.83(5) . . ?
Ag1 Pt1 Ag4 61.54(4) . . ?
Ag11 Pt1 Ag4 178.14(4) . . ?
Ag9 Pt1 Ag4 62.21(4) . . ?
Ag5 Pt1 Ag4 63.11(4) . . ?
Ag3 Pt1 Ag4 62.71(4) . . ?
Ag10 Pt1 Ag4 115.49(4) . . ?
Ag7 Pt1 Ag4 115.84(5) . . ?
Ag8 Pt1 Ag4 63.64(4) . . ?
Ag12 Pt1 Ag4 117.42(4) . . ?
Ag6 Pt1 Ag4 116.70(4) . . ?
Ag1 Pt1 Ag2 62.19(4) . . ?
Ag11 Pt1 Ag2 65.80(4) . . ?
Ag9 Pt1 Ag2 175.39(5) . . ?
Ag5 Pt1 Ag2 113.48(5) . . ?
Ag3 Pt1 Ag2 65.90(4) . . ?
Ag10 Pt1 Ag2 115.23(5) . . ?
Ag7 Pt1 Ag2 69.75(5) . . ?
Ag8 Pt1 Ag2 121.44(5) . . ?
Ag12 Pt1 Ag2 120.09(5) . . ?
Ag6 Pt1 Ag2 61.20(5) . . ?
Ag4 Pt1 Ag2 115.37(5) . . ?
P1 Se1 Ag17 96.14(15) . . ?
P1 Se1 Ag2 93.27(15) . . ?
Ag17 Se1 Ag2 69.82(6) . . ?
P1 Se2 Ag13 97.07(14) . . ?
P2 Se3 Ag13 99.68(15) . . ?
P2 Se4 Ag16 96.00(15) . . ?
P2 Se4 Ag1 94.61(13) . . ?
Ag16 Se4 Ag1 68.98(6) . . ?
P3 Se5 Ag16 99.23(16) . . ?
P3 Se5 Ag6 94.35(13) . . ?
Ag16 Se5 Ag6 67.89(6) . . ?
P3 Se6 Ag19 96.57(16) . . ?
P4 Se7 Ag19 100.20(15) . . ?
P4 Se8 Ag17 96.88(15) . . ?
P4 Se8 Ag11 95.12(18) . . ?
Ag17 Se8 Ag11 68.79(6) . . ?
P5 Se9 Ag13 99.80(15) . . ?
P5 Se10 Ag14 97.68(14) . . ?
P5 Se10 Ag3 94.36(13) . . ?
Ag14 Se10 Ag3 68.85(6) . . ?
P6 Se11 Ag16 99.19(19) . . ?
P6 Se11 Ag5 97.3(2) . . ?
Ag16 Se11 Ag5 68.36(6) . . ?
P6 Se12 Ag15 98.77(19) . . ?
P7 Se13 Ag19 99.82(14) . . ?
P7 Se14 Ag20 94.63(13) . . ?
P7 Se14 Ag10 93.46(12) . . ?
Ag20 Se14 Ag10 68.63(5) . . ?
P8 Se15 Ag17 95.89(17) . . ?
P8 Se15 Ag7 92.74(15) . . ?
Ag17 Se15 Ag7 69.30(6) . . ?
P8 Se16 Ag18 99.07(18) . . ?
P9 Se17 Ag14 101.57(15) . . ?
P9 Se17 Ag8 91.99(14) . . ?
Ag14 Se17 Ag8 70.81(6) . . ?
P9 Se18 Ag18 98.26(16) . . ?
P10 Se19 Ag15 97.63(15) . . ?
P10 Se20 Ag14 94.88(14) . . ?
P10 Se20 Ag4 91.95(14) . . ?
Ag14 Se20 Ag4 69.09(6) . . ?
P11 Se21 Ag20 97.24(13) . . ?
P11 Se21 Ag9 94.27(12) . . ?
Ag20 Se21 Ag9 67.72(5) . . ?
P11 Se22 Ag15 97.03(13) . . ?
P12 Se23 Ag18 99.65(17) . . ?
P12 Se24 Ag20 95.32(16) . . ?
P12 Se24 Ag12 97.24(19) . . ?
Ag20 Se24 Ag12 66.87(6) . . ?

_refine_diff_density_max         3.973
_refine_diff_density_min         -2.658
_refine_diff_density_rms         0.251

