# Electronic Supplementary Material (ESI) for Inorganic Chemistry Frontiers.
# This journal is © the Partner Organisations 2021

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_dy
_database_code_depnum_ccdc_archive 'CCDC 2058342'
loop_
_audit_author_name
_audit_author_address
'Hai-Ling Wang'
;Guangxi Normal University
China
;
_audit_update_record             
;
2021-01-24 deposited with the CCDC.	2021-02-19 downloaded from the CCDC.
;
_audit_creation_date             2020-02-05
_audit_creation_method           
;
Olex2 1.2
(compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C84 H93 Dy16 N29 O80'
_chemical_formula_sum            'C84 H93 Dy16 N29 O80'
_chemical_formula_weight         5388.87
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_H-M_alt        'P 1 21/n 1'
_space_group_name_Hall           '-P 2yn'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'

_cell_length_a                   22.7736(8)
_cell_length_b                   34.9804(5)
_cell_length_c                   24.2097(10)
_cell_angle_alpha                90
_cell_angle_beta                 109.462(4)
_cell_angle_gamma                90
_cell_volume                     18184.2(11)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    ?
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      30.4910
_cell_measurement_theta_min      1.7710
_shelx_estimated_absorpt_T_max   ?
_shelx_estimated_absorpt_T_min   ?
_exptl_absorpt_coefficient_mu    6.568
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.72145
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   ?
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.968
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             9984
_exptl_crystal_size_max          0.06
_exptl_crystal_size_mid          0.03
_exptl_crystal_size_min          0.02
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0797
_diffrn_reflns_av_unetI/netI     0.0771
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.780
_diffrn_reflns_limit_h_max       29
_diffrn_reflns_limit_h_min       -31
_diffrn_reflns_limit_k_max       48
_diffrn_reflns_limit_k_min       -42
_diffrn_reflns_limit_l_max       33
_diffrn_reflns_limit_l_min       -25
_diffrn_reflns_number            171635
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.780
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         30.354
_diffrn_reflns_theta_min         1.612
_diffrn_ambient_temperature      293(2)
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.780
_diffrn_measurement_device_type  'multiwire proportional'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                21088
_reflns_number_total             42726
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'CrysAlisPro 1.171.40.53 (Rigaku OD, 2019)'
_computing_data_collection       'CrysAlisPro 1.171.40.53 (Rigaku OD, 2019)'
_computing_data_reduction        'CrysAlisPro 1.171.40.53 (Rigaku OD, 2019)'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    'ShelXS-1997 (Sheldrick, 2008)'
_refine_diff_density_max         4.988
_refine_diff_density_min         -2.605
_refine_diff_density_rms         0.319
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.024
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1739
_refine_ls_number_reflns         42726
_refine_ls_number_restraints     709
_refine_ls_R_factor_all          0.1706
_refine_ls_R_factor_gt           0.0976
_refine_ls_restrained_S_all      1.033
_refine_ls_shift/su_max          0.188
_refine_ls_shift/su_mean         0.006
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.1575P)²+299.8119P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2577
_refine_ls_wR_factor_ref         0.3245
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups
 At 1.5 times of:
  All O(H) groups, All O(H,H) groups
2. Restrained distances
 O53-O54
 2 with sigma of 0.01
 O71-O72
 2 with sigma of 0.01
 O65-O67
 2 with sigma of 0.01
 O67-O66
 2 with sigma of 0.01
 O66-O67
 2 with sigma of 0.01
 O65-N25 = O66-N25 = O67-N25
 1.3 with sigma of 0.01
 O58-O56
 2 with sigma of 0.01
 O66-N25 = O67-N25 = O75-N29 = O76-N29 = O74-N29 = O79-N28 = O78-N28 = O77-N28
 = O61-N27 = O59-N27 = O60-N27 = O58-N24 = O56-N24 = O57-N24 = O53-N26 = O54-
 N26 = O55-N26
 1.3 with sigma of 0.01
 O67-O65 \\sim O65-O66
 with sigma of 0.01
 O66-O67 \\sim O67-O65
 with sigma of 0.01
 O58-O57 \\sim O57-O56
 with sigma of 0.01
3. Restrained planarity
 O53, O54, O55, N26
 with sigma of 0.01
 O65, O66, O67, N25
 with sigma of 0.01
 O56, O57, O58, N24
 with sigma of 0.01
4. Uiso/Uaniso restraints and constraints
C4 \\sim C5: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02
O50 \\sim N20 \\sim O52 \\sim O51: within 2A with sigma of 0.01 and sigma for
terminal atoms of 0.02
O71 \\sim N23 \\sim O73 \\sim O72: within 2A with sigma of 0.01 and sigma for
terminal atoms of 0.02
O70 \\sim O68 \\sim N21 \\sim O69: within 2A with sigma of 0.01 and sigma for
terminal atoms of 0.02
N27 \\sim O59: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02
O76 \\sim N29 \\sim O74 \\sim O75: within 2A with sigma of 0.01 and sigma for
terminal atoms of 0.02
O75 \\sim N29 \\sim O76 \\sim O74: within 2A with sigma of 0.01 and sigma for
terminal atoms of 0.02
O57 \\sim N24 \\sim O56 \\sim O58 \\sim Dy2: within 2A with sigma of 0.01 and
sigma for terminal atoms of 0.02
Uanis(O39) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(C5) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(C3) \\sim Ueq, Uanis(C2) \\sim Ueq, Uanis(C1) \\sim Ueq, Uanis(C6) \\sim
Ueq, Uanis(C7) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of
0.02
Uanis(O51) \\sim Ueq, Uanis(N20) \\sim Ueq, Uanis(O50) \\sim Ueq, Uanis(O52)
\\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(O71) \\sim Ueq, Uanis(N23) \\sim Ueq, Uanis(O73) \\sim Ueq, Uanis(O72)
\\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(O70) \\sim Ueq, Uanis(O68) \\sim Ueq, Uanis(N21) \\sim Ueq, Uanis(O69)
\\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(N25) \\sim Ueq, Uanis(O67) \\sim Ueq, Uanis(O66) \\sim Ueq, Uanis(O65)
\\sim Ueq, Uanis(Dy11) \\sim Ueq: with sigma of 0.01 and sigma for terminal
atoms of 0.02
Uanis(O48) \\sim Ueq, Uanis(N19) \\sim Ueq, Uanis(O49) \\sim Ueq, Uanis(O47)
\\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(N27) \\sim Ueq, Uanis(O59) \\sim Ueq: with sigma of 0.01 and sigma for
terminal atoms of 0.02
Uanis(O53) \\sim Ueq, Uanis(N26) \\sim Ueq, Uanis(O54) \\sim Ueq, Uanis(O55)
\\sim Ueq, Uanis(O77) \\sim Ueq, Uanis(N28) \\sim Ueq, Uanis(O78) \\sim Ueq,
Uanis(O79) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(O76) \\sim Ueq, Uanis(N29) \\sim Ueq, Uanis(O74) \\sim Ueq, Uanis(O75)
\\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(O76) \\sim Ueq, Uanis(N29) \\sim Ueq, Uanis(O75) \\sim Ueq, Uanis(O74)
\\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(C18) \\sim Ueq, Uanis(C15) \\sim Ueq, Uanis(C16) \\sim Ueq, Uanis(N4)
\\sim Ueq, Uanis(C20) \\sim Ueq, Uanis(C19) \\sim Ueq: with sigma of 0.01 and
sigma for terminal atoms of 0.02
Uanis(C14) \\sim Ueq, Uanis(C13) \\sim Ueq, Uanis(C12) \\sim Ueq, Uanis(C17)
\\sim Ueq, Uanis(C9) \\sim Ueq, Uanis(C10) \\sim Ueq, Uanis(C11) \\sim Ueq,
Uanis(N3) \\sim Ueq, Uanis(C8) \\sim Ueq: with sigma of 0.01 and sigma for
terminal atoms of 0.02
Uanis(C83) \\sim Ueq, Uanis(C82) \\sim Ueq, Uanis(C81) \\sim Ueq, Uanis(C79)
\\sim Ueq, Uanis(C84) \\sim Ueq, Uanis(C80) \\sim Ueq: with sigma of 0.01 and
sigma for terminal atoms of 0.02
Uanis(O57) \\sim Ueq, Uanis(N24) \\sim Ueq, Uanis(O56) \\sim Ueq, Uanis(O58)
\\sim Ueq, Uanis(Dy2) \\sim Ueq: with sigma of 0.01 and sigma for terminal
atoms of 0.02
Uanis(O58) \\sim Ueq, Uanis(N24) \\sim Ueq, Uanis(O57) \\sim Ueq, Uanis(O56)
\\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
5. Rigid body (RIGU) restrains
 O50, N20, O52, O51
 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01
 O72, N23, O73, O71
 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01
 O70, N21, O68, O69
 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01
 Dy11, O65, N25, O67, O66
 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01
 C2, C3, C5, C4, C6, C1
 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01
 C74, C75
 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01
 N1, C7
 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01
 O75, N29, O76, O74
 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01
 O57, N24, O56, O58, Dy2
 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.02
 O58, N24, O57, O56
 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01
6. Others
 Sof(Dy7)=Sof(O39)=Sof(H39A)=Sof(H39B)=1-FVAR(1)
 Sof(Dy7A)=Sof(O40)=Sof(H40A)=Sof(H40B)=FVAR(1)
 Fixed U11: O20(0.148474) O25(0.148474) O30(0.148474) O45(0.086989)
 O48(0.171999) O53(0.081713) O54(0.081713) O55(0.198287) O65(0.105459)
 O66(0.105459) O68(0.105459) O70(0.105459) O75(0.105459) O77(0.150687)
 N21(0.105459) N24(0.147856) N25(0.105459) N26(0.130454) N28(0.141874)
 N29(0.105459) C82(0.17018)
 Fixed U12: O20(-0.016492) O25(-0.016492) O30(-0.016492) O45(0.013566) O48(-
 0.006428) O53(0.014185) O54(0.014185) O55(0.014185) O65(0.014185)
 O66(0.014185) O68(0.014185) O70(0.014185) O75(0.014185) O77(0.011675)
 N21(0.014185) N24(0.017485) N25(0.014185) N26(0.014185) N28(-0.023601)
 N29(0.014185) C82(-0.002881)
 Fixed U13: O20(0.073994) O25(0.073994) O30(0.073994) O45(0.025244)
 O48(0.017964) O53(0.02567) O54(0.02567) O55(-0.005027) O65(0.022137)
 O66(0.022137) O68(0.022137) O70(0.022137) O75(0.022137) O77(-0.00123)
 N21(0.022137) N24(-0.000147) N25(0.022137) N26(0.015069) N28(0.011091)
 N29(0.022137) C82(0.028634)
 Fixed U22: O20(0.04684) O25(0.04684) O30(0.04684) O45(0.08028) O48(0.18156)
 O53(0.09032) O54(0.09032) O55(0.19803) O65(0.12032) O66(0.12032) O68(0.12032)
 O70(0.12032) O75(0.12032) O77(0.10831) N21(0.12032) N24(0.12511) N25(0.12032)
 N26(0.14032) N28(0.1324) N29(0.12032) C82(0.18986)
 Fixed U23: O20(-0.02284) O25(-0.02284) O30(-0.02284) O45(0.04673)
 O48(0.01864) O53(0.01079) O54(0.01079) O55(0.01079) O65(0.01079) O66(0.01079)
 O68(0.01079) O70(0.01079) O75(0.01079) O77(-0.01503) N21(0.01079) N24(0.01472)
 N25(0.01079) N26(0.01079) N28(0.00484) N29(0.01079) C82(0.00257)
 Fixed U33: O20(0.12835) O25(0.12835) O30(0.12835) O45(0.18626) O48(0.18258)
 O53(0.11125) O54(0.11125) O55(0.19812) O65(0.12125) O66(0.12125) O68(0.12125)
 O70(0.12125) O75(0.12125) O77(0.13092) N21(0.12125) N24(0.18296) N25(0.12125)
 N26(0.14125) N28(0.1351) N29(0.12125) C82(0.18576)
7.a Riding coordinates:
 O13(H13), O14(H14), O15(H15), O16(H16), O17(H17), O18(H18), O19(H19),
 O20(H20), O21(H21), O22(H22), O23(H23), O24(H24), O25(H25), O26(H26), O27(H27),
  O28(H28), O29(H29), O30(H30), O31(H31), O32(H32), O33(H33), O34(H34),
 O35(H35A,H35B), O36(H36A,H36B), O37(H37A,H37B), O38(H38A,H38B), O39(H39A,H39B),
  O40(H40A,H40B), O41(H41A,H41B), O42(H42A,H42B), O43(H43A,H43B), O44(H44A,
 H44B), O45(H45), O46(H46A,H46B), O80(H80), O81(H81)
7.b Aromatic/amide H refined with riding coordinates:
 C4(H4), C5(H5), C3(H3), C2(H2), C7(H7), C10(H10), C11(H11), C13(H13A),
 C14(H14A), C18(H18A), C19(H19A), C22(H22A), C24(H24A), C25(H25A), C26(H26A),
 C27(H27A), C30(H30A), C31(H31A), C32(H32A), C33(H33A), C35(H35), C38(H38),
 C39(H39), C41(H41), C42(H42), C46(H46), C47(H47), C50(H50), C52(H52), C53(H53),
  C54(H54), C55(H55), C58(H58), C62(H62), C60(H60), C59(H59), C63(H63),
 C66(H66), C67(H67), C70(H70), C71(H71), C74(H74), C75(H75), C78(H78), C83(H83),
  C82(H82), C80(H80A), C81(H81A)
7.c Fitted hexagon refined as free rotating group:
 C1(C6,C4,C5,C3,C2), C58(C57,C61,C62,C60,C59), C79(C84,C83,C82,C80,C81)
;
_atom_sites_solution_hydrogens   mixed
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Dy1 Dy 0.24682(6) 0.35493(3) 0.85501(6) 0.0808(4) Uani 1 1 d . . . . .
Dy2 Dy 0.31449(6) 0.41158(3) 0.74730(7) 0.0996(5) Uani 1 1 d . U . . .
Dy3 Dy 0.46615(6) 0.38878(3) 0.74683(6) 0.0845(4) Uani 1 1 d . . . . .
Dy4 Dy 0.38882(6) 0.32466(2) 0.82037(7) 0.0911(4) Uani 1 1 d . . . . .
Dy5 Dy 0.35192(5) 0.26605(2) 0.92281(6) 0.0761(3) Uani 1 1 d . . . . .
Dy6 Dy 0.38211(5) 0.22367(2) 0.80251(5) 0.0646(3) Uani 1 1 d . . . . .
Dy7 Dy 0.51594(14) 0.28318(6) 0.77764(15) 0.0785(12) Uani 0.421(3) 1 d . . P .
.
Dy7A Dy 0.45776(8) 0.28561(4) 0.71644(8) 0.0572(6) Uani 0.579(3) 1 d . . P . .
Dy8 Dy 0.57435(6) 0.33842(3) 0.67069(6) 0.0777(4) Uani 1 1 d . . . . .
Dy9 Dy 0.64915(6) 0.42393(3) 0.74141(6) 0.0895(4) Uani 1 1 d . . . . .
Dy10 Dy 0.72118(6) 0.36998(3) 0.63824(6) 0.0796(4) Uani 1 1 d . . . . .
Dy11 Dy 0.62293(6) 0.27948(3) 0.57237(6) 0.0825(4) Uani 1 1 d . U . . .
Dy12 Dy 0.59520(5) 0.23394(2) 0.68964(5) 0.0657(3) Uani 1 1 d . . . . .
Dy13 Dy 0.49169(4) 0.18440(2) 0.74434(5) 0.0617(3) Uani 1 1 d . . . . .
Dy14 Dy 0.34622(5) 0.13838(2) 0.71626(5) 0.0703(3) Uani 1 1 d . . . . .
Dy15 Dy 0.50194(5) 0.08028(2) 0.74666(5) 0.0704(3) Uani 1 1 d . . . . .
Dy16 Dy 0.64541(5) 0.14937(3) 0.77722(6) 0.0728(3) Uani 1 1 d . . . . .
O1 O 0.6111(9) 0.4629(4) 0.7932(10) 0.112(7) Uani 1 1 d . . . . .
O2 O 0.7045(9) 0.4294(4) 0.6758(9) 0.102(6) Uani 1 1 d . . . . .
O3 O 0.7218(8) 0.3077(4) 0.6005(10) 0.108(7) Uani 1 1 d . . . . .
O4 O 0.6043(8) 0.2175(4) 0.5969(7) 0.082(5) Uani 1 1 d . . . . .
O5 O 0.6849(7) 0.1956(4) 0.7294(8) 0.084(5) Uani 1 1 d . . . . .
O6 O 0.5979(7) 0.0907(3) 0.7362(8) 0.083(5) Uani 1 1 d . . . . .
O7 O 0.4056(8) 0.0832(3) 0.7596(8) 0.088(5) Uani 1 1 d . . . . .
O8 O 0.2978(7) 0.1803(4) 0.7623(7) 0.078(4) Uani 1 1 d . . . . .
O9 O 0.2523(8) 0.2945(4) 0.8983(9) 0.095(5) Uani 1 1 d . . . . .
O10 O 0.2697(8) 0.4149(4) 0.8229(8) 0.089(5) Uani 1 1 d . . . . .
O11 O 0.3991(9) 0.4477(5) 0.7452(11) 0.124(8) Uani 1 1 d . . . . .
O12 O 0.3684(7) 0.2053(3) 0.8927(8) 0.083(5) Uani 1 1 d . . . . .
O13 O 0.6769(7) 0.3633(3) 0.7149(7) 0.077(4) Uani 1 1 d . . . . .
H13 H 0.701233 0.353987 0.742821 0.116 Uiso 1 1 d R . . . .
O14 O 0.5732(8) 0.4081(5) 0.6531(10) 0.110(6) Uani 1 1 d . . . . .
H14 H 0.573177 0.418410 0.623413 0.165 Uiso 1 1 d R . . . .
O15 O 0.5725(8) 0.3811(4) 0.7511(7) 0.088(5) Uani 1 1 d . . . . .
H15 H 0.589540 0.375319 0.782423 0.132 Uiso 1 1 d R . . . .
O16 O 0.6193(8) 0.3456(4) 0.5967(7) 0.084(5) Uani 1 1 d . . . . .
H16 H 0.594143 0.354750 0.569836 0.126 Uiso 1 1 d R . . . .
O17 O 0.6570(7) 0.2822(4) 0.6732(7) 0.076(4) Uani 1 1 d . . . . .
H17 H 0.690920 0.283361 0.698232 0.114 Uiso 1 1 d R . . . .
O18 O 0.5444(7) 0.2817(3) 0.6174(6) 0.068(4) Uani 1 1 d . . . . .
H18 H 0.502556 0.281502 0.589891 0.102 Uiso 1 1 d R . . . .
O19 O 0.5788(11) 0.2902(4) 0.7408(8) 0.108(7) Uani 1 1 d . . . . .
H19 H 0.614311 0.294252 0.767629 0.162 Uiso 1 1 d R . . . .
O20 O 0.4769(10) 0.3381(4) 0.6828(8) 0.108 Uani 1 1 d . . . . .
H20 H 0.452119 0.342841 0.650247 0.162 Uiso 1 1 d R . . . .
O21 O 0.3696(9) 0.3688(6) 0.7122(9) 0.113(6) Uani 1 1 d . . . . .
H21 H 0.352968 0.363274 0.677619 0.170 Uiso 1 1 d R . . . .
O22 O 0.4041(8) 0.3900(4) 0.8180(8) 0.088(5) Uani 1 1 d . . . . .
H22 H 0.416623 0.399023 0.847398 0.133 Uiso 1 1 d R . . . .
O23 O 0.2907(7) 0.3491(4) 0.7796(7) 0.075(4) Uani 1 1 d . . . . .
H23 H 0.268137 0.336360 0.750975 0.112 Uiso 1 1 d R . . . .
O24 O 0.3498(7) 0.3328(3) 0.8980(7) 0.078(4) Uani 1 1 d . . . . .
H24 H 0.372273 0.340460 0.933034 0.117 Uiso 1 1 d R . . . .
O25 O 0.3857(10) 0.2810(4) 0.7485(8) 0.108 Uani 1 1 d . . . . .
H25 H 0.360250 0.283472 0.719374 0.162 Uiso 1 1 d R . . . .
O26 O 0.4819(8) 0.3322(4) 0.8011(9) 0.097(6) Uani 1 1 d . . . . .
H26 H 0.512967 0.331015 0.831423 0.145 Uiso 1 1 d R . . . .
O27 O 0.4903(8) 0.2358(4) 0.6854(8) 0.096(6) Uani 1 1 d . . . . .
H27 H 0.470937 0.233324 0.649362 0.144 Uiso 1 1 d R . . . .
O28 O 0.5965(6) 0.2094(3) 0.7802(7) 0.069(4) Uani 1 1 d . . . . .
H28 H 0.609820 0.222760 0.807965 0.103 Uiso 1 1 d R . . . .
O29 O 0.5620(6) 0.1687(3) 0.6934(6) 0.058(3) Uani 1 1 d . . . . .
H29 H 0.545174 0.156950 0.662950 0.086 Uiso 1 1 d R . . . .
O30 O 0.4823(10) 0.2357(4) 0.7981(8) 0.108 Uani 1 1 d . . . . .
H30 H 0.507020 0.225545 0.830884 0.162 Uiso 1 1 d R . . . .
O31 O 0.5518(6) 0.1352(3) 0.7966(7) 0.071(4) Uani 1 1 d . . . . .
H31 H 0.559517 0.136305 0.830329 0.107 Uiso 1 1 d R . . . .
O32 O 0.4410(7) 0.1306(4) 0.6928(7) 0.075(4) Uani 1 1 d . . . . .
H32 H 0.435498 0.131549 0.656776 0.113 Uiso 1 1 d R . . . .
O33 O 0.4278(6) 0.1626(3) 0.7990(6) 0.062(3) Uani 1 1 d . . . . .
H33 H 0.439870 0.150331 0.826649 0.093 Uiso 1 1 d R . . . .
O34 O 0.3839(6) 0.2009(3) 0.7107(6) 0.063(3) Uani 1 1 d . . . . .
H34 H 0.366832 0.213096 0.681364 0.094 Uiso 1 1 d R . . . .
O35 O 0.6380(9) 0.2967(5) 0.4811(8) 0.100(6) Uani 1 1 d . . . . .
H35A H 0.665776 0.319111 0.486732 0.150 Uiso 1 1 d R . . . .
H35B H 0.606176 0.315661 0.474242 0.150 Uiso 1 1 d R . . . .
O36 O 0.4614(17) 0.4173(10) 0.6588(15) 0.25(2) Uani 1 1 d . . . . .
H36A H 0.442927 0.400069 0.626931 0.374 Uiso 1 1 d R . . . .
H36B H 0.436727 0.440149 0.653511 0.374 Uiso 1 1 d R . . . .
O37 O 0.5300(9) 0.4225(4) 0.8275(8) 0.094(5) Uani 1 1 d . . . . .
H37A H 0.505392 0.440175 0.840729 0.142 Uiso 1 1 d R . . . .
H37B H 0.549383 0.404475 0.858119 0.142 Uiso 1 1 d R . . . .
O38 O 0.4871(13) 0.3443(7) 0.9211(10) 0.153(9) Uani 1 1 d . . . . .
H38A H 0.484573 0.370988 0.929424 0.229 Uiso 1 1 d R . . . .
H38B H 0.484113 0.329358 0.953354 0.229 Uiso 1 1 d R . . . .
O39 O 0.599(3) 0.2715(17) 0.880(3) 0.15(2) Uani 0.421(3) 1 d . U P . .
H39A H 0.591778 0.246269 0.892305 0.218 Uiso 0.421(3) 1 d R . P . .
H39B H 0.592828 0.289839 0.907455 0.218 Uiso 0.421(3) 1 d R . P . .
O40 O 0.3715(15) 0.2801(9) 0.6200(14) 0.104(10) Uani 0.579(3) 1 d . . P . .
H40A H 0.388133 0.269446 0.591876 0.156 Uiso 0.579(3) 1 d R . P . .
H40B H 0.353323 0.304586 0.606586 0.156 Uiso 0.579(3) 1 d R . P . .
O41 O 0.6725(14) 0.1683(9) 0.8778(12) 0.195(14) Uani 1 1 d . . . . .
H41A H 0.706924 0.185786 0.887261 0.292 Uiso 1 1 d R . . . .
H41B H 0.684094 0.146046 0.902191 0.292 Uiso 1 1 d R . . . .
O42 O 0.3066(18) 0.1587(7) 0.6133(12) 0.227(19) Uani 1 1 d . . . . .
H42A H 0.263033 0.164687 0.600476 0.341 Uiso 1 1 d R . . . .
H42B H 0.313913 0.138477 0.589576 0.341 Uiso 1 1 d R . . . .
O43 O 0.3388(9) 0.2800(4) 1.0157(8) 0.099(6) Uani 1 1 d . . . . .
H43A H 0.378645 0.267458 1.025814 0.148 Uiso 1 1 d R . . . .
H43B H 0.344955 0.306818 1.023784 0.148 Uiso 1 1 d R . . . .
O44 O 0.2871(9) 0.3799(5) 0.9556(9) 0.115(7) Uani 1 1 d . . . . .
H44A H 0.326210 0.392493 0.961773 0.172 Uiso 1 1 d R . . . .
H44B H 0.257370 0.397972 0.960363 0.172 Uiso 1 1 d R . . . .
O45 O 0.2795(9) 0.4479(5) 0.6586(10) 0.118 Uani 1 1 d . . . . .
H45 H 0.284376 0.474575 0.668150 0.177 Uiso 1 1 d R . . . .
O46 O 0.4867(9) 0.3566(5) 0.5776(10) 0.121(7) Uani 1 1 d . . . . .
H46A H 0.495509 0.346184 0.544471 0.181 Uiso 1 1 d R . . . .
H46B H 0.483699 0.383944 0.573991 0.181 Uiso 1 1 d R . . . .
O47 O 0.6960(11) 0.3927(6) 0.8324(10) 0.124(7) Uani 1 1 d . U . . .
O48 O 0.8012(16) 0.4041(9) 0.8920(14) 0.179 Uani 1 1 d . U . . .
O49 O 0.7530(10) 0.4352(6) 0.8094(9) 0.117(6) Uani 1 1 d . U . . .
O50 O 0.7876(11) 0.3200(7) 0.7092(11) 0.135(6) Uani 1 1 d . U . . .
O51 O 0.8137(10) 0.3753(7) 0.7276(10) 0.120(5) Uani 1 1 d . U . . .
O52 O 0.8728(13) 0.3350(7) 0.7913(12) 0.146(7) Uani 1 1 d . U . . .
O53 O 0.6596(8) 0.4180(4) 0.5640(8) 0.094 Uani 1 1 d D U . . .
O54 O 0.7003(8) 0.3755(4) 0.5346(8) 0.094 Uani 1 1 d D U . . .
O55 O 0.6471(14) 0.4236(8) 0.4660(10) 0.198 Uani 1 1 d D U . . .
O56 O 0.1544(11) 0.4029(8) 0.6197(10) 0.210(9) Uani 1 1 d D U . . .
O57 O 0.2106(12) 0.4216(7) 0.7147(10) 0.175(5) Uani 1 1 d D U . . .
O58 O 0.2359(11) 0.3759(7) 0.6566(11) 0.170(5) Uani 1 1 d D U . . .
O59 O 0.1028(10) 0.3188(7) 0.7038(10) 0.143(7) Uani 1 1 d D U . . .
O60 O 0.1524(8) 0.3633(5) 0.7652(8) 0.095(5) Uani 1 1 d D . . . .
O61 O 0.1858(9) 0.3046(5) 0.7870(10) 0.114(7) Uani 1 1 d D . . . .
O62 O 0.4497(9) 0.2953(5) 0.9962(8) 0.096(5) Uani 1 1 d . . . . .
O63 O 0.4409(10) 0.2368(6) 0.9986(10) 0.107(6) Uani 1 1 d . . . . .
O64 O 0.5239(17) 0.2663(9) 1.0666(17) 0.186(13) Uani 1 1 d . . . . .
O65 O 0.5202(9) 0.3095(4) 0.4968(8) 0.116 Uani 1 1 d D U . . .
O66 O 0.5363(9) 0.2494(4) 0.4955(8) 0.116 Uani 1 1 d D U . . .
O67 O 0.4623(12) 0.2743(7) 0.4314(11) 0.257(15) Uani 1 1 d D U . . .
O68 O 0.7596(10) 0.1454(6) 0.8271(9) 0.116 Uani 1 1 d . U . . .
O69 O 0.8051(14) 0.0910(9) 0.8793(14) 0.182(8) Uani 1 1 d . U . . .
O70 O 0.6942(10) 0.0962(6) 0.8431(9) 0.116 Uani 1 1 d . U . . .
O71 O 0.5534(11) 0.0605(6) 0.8443(10) 0.123(6) Uani 1 1 d D U . . .
O72 O 0.5207(14) 0.1019(8) 0.8832(12) 0.175(8) Uani 1 1 d D U . . .
O73 O 0.5468(14) 0.0534(8) 0.9318(12) 0.159(7) Uani 1 1 d . U . . .
O74 O 0.4479(14) 0.0510(8) 0.5611(10) 0.167(7) Uani 1 1 d D U . . .
O75 O 0.5075(10) 0.0844(6) 0.6429(9) 0.116 Uani 1 1 d D U . . .
O76 O 0.4375(11) 0.0525(6) 0.6539(10) 0.130(4) Uani 1 1 d D U . . .
O77 O 0.2318(11) 0.1267(6) 0.6627(10) 0.130 Uani 1 1 d D U . . .
O78 O 0.2040(17) 0.0745(11) 0.6087(16) 0.247(17) Uani 1 1 d D U . . .
O79 O 0.3068(10) 0.0840(6) 0.6523(10) 0.129(7) Uani 1 1 d D U . A 2
O80 O 0.3149(7) 0.2693(3) 0.8206(7) 0.072(4) Uani 1 1 d . . . . .
H80 H 0.282990 0.263328 0.798786 0.108 Uiso 1 1 d R . . . .
O81 O 0.4285(6) 0.2709(3) 0.8757(6) 0.060(3) Uani 1 1 d . . . . .
H81 H 0.464666 0.264046 0.894101 0.090 Uiso 1 1 d R . . . .
N1 N 0.6778(11) 0.4907(5) 0.7231(9) 0.095(7) Uani 1 1 d . U . . .
N2 N 0.7167(10) 0.4944(5) 0.6875(10) 0.091(6) Uani 1 1 d . . . . .
N3 N 0.7898(9) 0.4243(5) 0.6294(8) 0.073(5) Uani 1 1 d . U . . .
N4 N 0.8122(9) 0.3525(5) 0.6059(8) 0.072(4) Uani 1 1 d . U . . .
N5 N 0.7689(10) 0.2578(5) 0.5711(9) 0.086(6) Uani 1 1 d . . . . .
N6 N 0.7116(9) 0.2387(5) 0.5702(8) 0.074(5) Uani 1 1 d . . . . .
N7 N 0.6900(8) 0.1144(4) 0.7112(9) 0.076(5) Uani 1 1 d . . . . .
N8 N 0.6748(9) 0.0735(4) 0.6982(9) 0.080(6) Uani 1 1 d . . . . .
N9 N 0.5596(8) 0.0228(4) 0.7341(8) 0.065(4) Uani 1 1 d . . . . .
N10 N 0.4567(9) 0.0189(4) 0.7629(9) 0.079(5) Uani 1 1 d . . . . .
N11 N 0.3300(10) 0.0605(4) 0.7950(10) 0.087(6) Uani 1 1 d . . . . .
N12 N 0.3073(9) 0.0991(4) 0.7823(10) 0.084(6) Uani 1 1 d . . . . .
N13 N 0.2643(9) 0.2232(4) 0.9273(9) 0.082(6) Uani 1 1 d . . . . .
N14 N 0.2070(9) 0.2419(4) 0.9254(9) 0.082(6) Uani 1 1 d . . . . .
N15 N 0.1595(9) 0.3377(5) 0.8901(9) 0.077(5) Uani 1 1 d . . . . .
N16 N 0.1790(10) 0.4083(6) 0.8656(9) 0.089(6) Uani 1 1 d . . . . .
N17 N 0.2593(13) 0.4798(6) 0.8133(12) 0.112(8) Uani 1 1 d . . . . .
N18 N 0.3033(11) 0.4753(5) 0.7871(11) 0.098(7) Uani 1 1 d . . . . .
N19 N 0.7485(17) 0.4076(10) 0.8481(15) 0.141(10) Uani 1 1 d . U . . .
N20 N 0.8265(15) 0.3440(9) 0.7500(14) 0.127(5) Uani 1 1 d . U . . .
N21 N 0.7541(13) 0.1081(8) 0.8435(12) 0.116 Uani 1 1 d . U . . .
N22 N 0.4712(17) 0.2621(8) 1.0211(13) 0.111(9) Uani 1 1 d . . . . .
N23 N 0.5386(15) 0.0702(9) 0.8822(14) 0.131(6) Uani 1 1 d . U . . .
N24 N 0.2014(8) 0.4019(5) 0.6681(8) 0.152 Uani 1 1 d D U . . .
N25 N 0.5080(7) 0.2789(5) 0.4765(6) 0.116 Uani 1 1 d D U . . .
N26 N 0.6682(6) 0.4061(4) 0.5166(7) 0.137 Uani 1 1 d D U . . .
N27 N 0.1450(10) 0.3275(5) 0.7531(9) 0.111(7) Uani 1 1 d D U . . .
N28 N 0.2494(11) 0.0943(7) 0.6452(13) 0.136 Uani 1 1 d D U . . .
N29 N 0.4593(11) 0.0640(7) 0.6141(10) 0.116 Uani 1 1 d D U . . .
C1 C 0.6155(10) 0.5011(4) 0.8113(9) 0.111(8) Uani 1 1 d . U . . .
C6 C 0.6325(9) 0.5305(6) 0.7809(8) 0.095(7) Uani 1 1 d G U . . .
C4 C 0.6262(11) 0.5684(5) 0.7954(10) 0.144(8) Uani 1 1 d G U . . .
H4 H 0.637551 0.587990 0.775139 0.172 Uiso 1 1 calc R . . . .
C5 C 0.6028(12) 0.5769(5) 0.8402(11) 0.150(9) Uani 1 1 d G U . . .
H5 H 0.598553 0.602217 0.849889 0.180 Uiso 1 1 calc R . . . .
C3 C 0.5858(11) 0.5475(7) 0.8705(9) 0.152(11) Uani 1 1 d G U . . .
H3 H 0.570140 0.553239 0.900482 0.182 Uiso 1 1 calc R . . . .
C2 C 0.5921(10) 0.5097(6) 0.8560(9) 0.113(8) Uani 1 1 d G U . . .
H2 H 0.580727 0.490033 0.876327 0.136 Uiso 1 1 calc R . . . .
C7 C 0.6700(13) 0.5224(7) 0.7440(12) 0.094(7) Uani 1 1 d . U . . .
H7 H 0.690658 0.543136 0.734825 0.112 Uiso 1 1 calc R . . . .
C8 C 0.7281(10) 0.4613(6) 0.6703(9) 0.067(5) Uani 1 1 d . U . . .
C9 C 0.7791(10) 0.4590(6) 0.6425(10) 0.072(5) Uani 1 1 d . U . . .
C10 C 0.8162(12) 0.4898(7) 0.6361(10) 0.081(6) Uani 1 1 d . U . . .
H10 H 0.806176 0.514382 0.644549 0.098 Uiso 1 1 calc R . . . .
C11 C 0.8640(12) 0.4850(7) 0.6188(11) 0.085(7) Uani 1 1 d . U . . .
H11 H 0.887249 0.505734 0.613659 0.102 Uiso 1 1 calc R . . . .
C12 C 0.8788(13) 0.4486(7) 0.6086(12) 0.092(7) Uani 1 1 d . U . . .
C13 C 0.9357(11) 0.4374(8) 0.5981(11) 0.086(7) Uani 1 1 d . U . . .
H13A H 0.963260 0.456796 0.597147 0.103 Uiso 1 1 calc R . . . .
C14 C 0.9523(14) 0.4007(8) 0.5893(12) 0.100(8) Uani 1 1 d . U . . .
H14A H 0.989147 0.395267 0.582214 0.120 Uiso 1 1 calc R . . . .
C15 C 0.9102(11) 0.3718(7) 0.5918(10) 0.076(6) Uani 1 1 d . U . . .
C16 C 0.8569(12) 0.3813(7) 0.6045(11) 0.084(7) Uani 1 1 d . U . . .
C17 C 0.8405(13) 0.4182(8) 0.6135(12) 0.093(7) Uani 1 1 d . U . . .
C18 C 0.9191(11) 0.3324(7) 0.5780(11) 0.084(6) Uani 1 1 d . U . . .
H18A H 0.953724 0.325211 0.568333 0.101 Uiso 1 1 calc R . . . .
C19 C 0.8757(11) 0.3061(7) 0.5796(11) 0.086(6) Uani 1 1 d . U . . .
H19A H 0.882554 0.280570 0.573232 0.103 Uiso 1 1 calc R . . . .
C20 C 0.8187(11) 0.3165(7) 0.5909(11) 0.081(6) Uani 1 1 d . U . . .
C21 C 0.7657(10) 0.2927(6) 0.5825(11) 0.073(6) Uani 1 1 d . . . . .
C22 C 0.7164(13) 0.2025(7) 0.5619(13) 0.100(9) Uani 1 1 d . . . . .
H22A H 0.752982 0.193496 0.557394 0.120 Uiso 1 1 calc R . . . .
C23 C 0.6655(10) 0.1739(6) 0.5593(10) 0.075(6) Uani 1 1 d . . . . .
C24 C 0.6724(13) 0.1376(6) 0.5410(11) 0.091(9) Uani 1 1 d . . . . .
H24A H 0.705228 0.132363 0.527435 0.109 Uiso 1 1 calc R . . . .
C25 C 0.6327(13) 0.1093(6) 0.5423(12) 0.095(9) Uani 1 1 d . . . . .
H25A H 0.642789 0.084049 0.537648 0.114 Uiso 1 1 calc R . . . .
C26 C 0.5777(11) 0.1180(6) 0.5505(11) 0.076(6) Uani 1 1 d . . . . .
H26A H 0.546368 0.099656 0.542951 0.091 Uiso 1 1 calc R . . . .
C27 C 0.5683(12) 0.1544(5) 0.5701(10) 0.078(7) Uani 1 1 d . . . . .
H27A H 0.532223 0.159481 0.578721 0.094 Uiso 1 1 calc R . . . .
C28 C 0.6136(11) 0.1836(6) 0.5771(9) 0.071(6) Uani 1 1 d . . . . .
C29 C 0.7410(9) 0.1939(5) 0.7193(9) 0.061(5) Uani 1 1 d . . . . .
C30 C 0.7795(12) 0.2283(6) 0.7290(15) 0.110(10) Uani 1 1 d . . . . .
H30A H 0.770085 0.249177 0.748388 0.132 Uiso 1 1 calc R . . . .
C31 C 0.8301(12) 0.2299(9) 0.7090(18) 0.135(14) Uani 1 1 d . . . . .
H31A H 0.852702 0.252462 0.712431 0.162 Uiso 1 1 calc R . . . .
C32 C 0.8463(13) 0.1991(8) 0.685(2) 0.149(16) Uani 1 1 d . . . . .
H32A H 0.881144 0.199998 0.673286 0.179 Uiso 1 1 calc R . . . .
C33 C 0.8116(12) 0.1655(7) 0.6777(16) 0.118(12) Uani 1 1 d . . . . .
H33A H 0.822941 0.144912 0.659128 0.141 Uiso 1 1 calc R . . . .
C34 C 0.7615(10) 0.1616(6) 0.6966(13) 0.091(8) Uani 1 1 d . . . . .
C35 C 0.7314(13) 0.1251(6) 0.6872(13) 0.097(9) Uani 1 1 d . . . . .
H35 H 0.741760 0.107905 0.662648 0.116 Uiso 1 1 calc R . . . .
C36 C 0.6293(11) 0.0665(5) 0.7176(12) 0.079(7) Uani 1 1 d . . . . .
C37 C 0.6115(14) 0.0252(5) 0.7217(13) 0.096(9) Uani 1 1 d . . . . .
C38 C 0.6424(10) -0.0072(5) 0.7097(10) 0.069(6) Uani 1 1 d . . . . .
H38 H 0.676564 -0.004177 0.697187 0.082 Uiso 1 1 calc R . . . .
C39 C 0.6225(13) -0.0415(5) 0.7165(12) 0.090(8) Uani 1 1 d . . . . .
H39 H 0.643822 -0.063009 0.710910 0.108 Uiso 1 1 calc R . . . .
C40 C 0.5672(12) -0.0456(6) 0.7329(12) 0.085(7) Uani 1 1 d . . . . .
C41 C 0.5440(16) -0.0818(7) 0.7425(16) 0.123(12) Uani 1 1 d . . . . .
H41 H 0.562991 -0.103877 0.735208 0.148 Uiso 1 1 calc R . . . .
C42 C 0.4957(12) -0.0849(5) 0.7616(11) 0.085(7) Uani 1 1 d . . . . .
H42 H 0.482983 -0.108910 0.769640 0.102 Uiso 1 1 calc R . . . .
C43 C 0.4614(11) -0.0496(5) 0.7702(10) 0.072(6) Uani 1 1 d . . . . .
C44 C 0.4861(12) -0.0146(5) 0.7620(10) 0.075(6) Uani 1 1 d . . . . .
C45 C 0.5408(10) -0.0127(5) 0.7432(10) 0.070(6) Uani 1 1 d . . . . .
C46 C 0.4086(14) -0.0496(5) 0.7851(15) 0.110(10) Uani 1 1 d . . . . .
H46 H 0.390823 -0.072952 0.789018 0.132 Uiso 1 1 calc R . . . .
C47 C 0.3808(11) -0.0165(6) 0.7944(10) 0.077(6) Uani 1 1 d . . . . .
H47 H 0.347466 -0.016575 0.808442 0.093 Uiso 1 1 calc R . . . .
C48 C 0.4067(9) 0.0177(5) 0.7811(9) 0.061(5) Uani 1 1 d . . . . .
C49 C 0.3794(11) 0.0572(5) 0.7784(11) 0.075(6) Uani 1 1 d . . . . .
C50 C 0.2642(10) 0.1071(5) 0.8049(11) 0.079(7) Uani 1 1 d . . . . .
H50 H 0.255608 0.088870 0.829044 0.095 Uiso 1 1 calc R . . . .
C51 C 0.2285(10) 0.1424(6) 0.7952(13) 0.084(7) Uani 1 1 d . . . . .
C52 C 0.1769(12) 0.1412(7) 0.8128(13) 0.094(8) Uani 1 1 d . . . . .
H52 H 0.167736 0.119050 0.829552 0.112 Uiso 1 1 calc R . . . .
C53 C 0.1388(14) 0.1727(7) 0.8058(15) 0.112(10) Uani 1 1 d . . . . .
H53 H 0.102726 0.170856 0.815491 0.135 Uiso 1 1 calc R . . . .
C54 C 0.1527(16) 0.2069(8) 0.7848(16) 0.125(12) Uani 1 1 d . . . . .
H54 H 0.128686 0.228703 0.782795 0.150 Uiso 1 1 calc R . . . .
C55 C 0.2034(10) 0.2070(7) 0.7671(14) 0.096(9) Uani 1 1 d . . . . .
H55 H 0.210236 0.228867 0.748147 0.116 Uiso 1 1 calc R . . . .
C56 C 0.2457(8) 0.1775(5) 0.7748(8) 0.054(4) Uani 1 1 d . . . . .
C58 C 0.4092(6) 0.1438(3) 0.9213(7) 0.071(6) Uani 1 1 d . . . . .
H58 H 0.444337 0.150443 0.911922 0.085 Uiso 1 1 calc R . . . .
C57 C 0.3632(6) 0.1708(2) 0.9171(6) 0.061(5) Uani 1 1 d G . . . .
C61 C 0.3108(5) 0.1608(3) 0.9311(7) 0.074(6) Uani 1 1 d G . . . .
C62 C 0.3043(6) 0.1238(3) 0.9492(8) 0.094(8) Uani 1 1 d G . . . .
H62 H 0.269258 0.117095 0.958529 0.113 Uiso 1 1 calc R . . . .
C60 C 0.3504(7) 0.0968(2) 0.9533(8) 0.094(9) Uani 1 1 d G . . . .
H60 H 0.346087 0.072000 0.965451 0.112 Uiso 1 1 calc R . . . .
C59 C 0.4028(6) 0.1068(3) 0.9394(7) 0.091(8) Uani 1 1 d G . . . .
H59 H 0.433627 0.088674 0.942147 0.110 Uiso 1 1 calc R . . . .
C63 C 0.2609(12) 0.1864(5) 0.9299(10) 0.080(7) Uani 1 1 d . . . . .
H63 H 0.223847 0.175802 0.931087 0.096 Uiso 1 1 calc R . . . .
C64 C 0.2069(11) 0.2773(6) 0.9100(11) 0.079(7) Uani 1 1 d . . . . .
C65 C 0.1512(13) 0.3012(6) 0.9049(12) 0.089(8) Uani 1 1 d . . . . .
C66 C 0.0982(10) 0.2902(8) 0.9149(12) 0.095(8) Uani 1 1 d . . . . .
H66 H 0.092447 0.264661 0.922217 0.114 Uiso 1 1 calc R . . . .
C67 C 0.0528(12) 0.3167(8) 0.9142(13) 0.095(8) Uani 1 1 d . . . . .
H67 H 0.016282 0.308615 0.919940 0.114 Uiso 1 1 calc R . . . .
C68 C 0.0609(14) 0.3536(9) 0.9055(12) 0.103(9) Uani 1 1 d . . . . .
C69 C 0.1140(13) 0.3640(8) 0.8912(13) 0.100(9) Uani 1 1 d . . . . .
C70 C 0.0191(16) 0.3839(9) 0.9072(15) 0.123(12) Uani 1 1 d . . . . .
H70 H -0.018467 0.378551 0.912919 0.148 Uiso 1 1 calc R . . . .
C71 C 0.0357(13) 0.4210(10) 0.9002(14) 0.120(11) Uani 1 1 d . . . . .
H71 H 0.010710 0.440568 0.906154 0.144 Uiso 1 1 calc R . . . .
C72 C 0.0877(17) 0.4313(8) 0.8847(12) 0.112(11) Uani 1 1 d . . . . .
C73 C 0.1298(13) 0.4022(6) 0.8830(12) 0.091(8) Uani 1 1 d . . . . .
C74 C 0.1042(14) 0.4680(7) 0.8769(11) 0.101(9) Uani 1 1 d . U . . .
H74 H 0.079436 0.487929 0.882039 0.122 Uiso 1 1 calc R . . . .
C75 C 0.1560(14) 0.4768(7) 0.8616(11) 0.096(9) Uani 1 1 d . U . . .
H75 H 0.167991 0.501877 0.858355 0.115 Uiso 1 1 calc R . . . .
C76 C 0.1894(11) 0.4453(7) 0.8514(12) 0.083(7) Uani 1 1 d . . . . .
C77 C 0.2443(15) 0.4459(7) 0.8297(14) 0.105(9) Uani 1 1 d . . . . .
C78 C 0.3261(13) 0.5080(9) 0.7787(13) 0.104(9) Uani 1 1 d . . . . .
H78 H 0.310777 0.529944 0.790842 0.125 Uiso 1 1 calc R . . . .
C79 C 0.3726(10) 0.5125(8) 0.7522(11) 0.126(11) Uani 1 1 d . U . . .
C84 C 0.4107(13) 0.4855(6) 0.7391(11) 0.131(11) Uani 1 1 d G U . . .
C83 C 0.4616(12) 0.4972(8) 0.7239(11) 0.150(13) Uani 1 1 d G U . . .
H83 H 0.487134 0.479119 0.715086 0.181 Uiso 1 1 calc R . . . .
C82 C 0.4745(11) 0.5359(9) 0.7218(12) 0.182 Uani 1 1 d G U . . .
H82 H 0.508540 0.543749 0.711680 0.218 Uiso 1 1 calc R . . . .
C80 C 0.4364(14) 0.5629(6) 0.7350(12) 0.190(19) Uani 1 1 d G U . . .
H80A H 0.444941 0.588856 0.733624 0.228 Uiso 1 1 calc R . . . .
C81 C 0.3854(12) 0.5513(7) 0.7502(11) 0.149(13) Uani 1 1 d G U . . .
H81A H 0.359935 0.569332 0.758974 0.179 Uiso 1 1 calc R . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Dy1 Dy4 3.7539(13) . ?
Dy1 Dy5 3.9334(14) . ?
Dy1 O9 2.344(15) . ?
Dy1 O10 2.357(14) . ?
Dy1 O23 2.363(13) . ?
Dy1 O24 2.358(14) . ?
Dy1 O44 2.46(2) . ?
Dy1 O60 2.514(19) . ?
Dy1 O61 2.49(2) . ?
Dy1 N15 2.482(18) . ?
Dy1 N16 2.491(16) . ?
Dy1 N27 2.93(2) . ?
Dy2 Dy3 3.5484(16) . ?
Dy2 Dy4 3.6392(15) . ?
Dy2 O10 2.376(15) . ?
Dy2 O11 2.319(19) . ?
Dy2 O21 2.289(16) . ?
Dy2 O22 2.310(18) . ?
Dy2 O23 2.442(13) . ?
Dy2 O45 2.391(19) . ?
Dy2 O57 2.26(3) . ?
Dy2 O58 2.64(3) . ?
Dy2 N18 2.47(2) . ?
Dy2 N24 2.671(19) . ?
Dy3 Dy4 3.6593(13) . ?
Dy3 Dy7 3.863(2) . ?
Dy3 Dy7A 3.6752(16) . ?
Dy3 O11 2.558(17) . ?
Dy3 O15 2.404(17) . ?
Dy3 O20 2.421(15) . ?
Dy3 O21 2.19(2) . ?
Dy3 O22 2.567(15) . ?
Dy3 O26 2.337(14) . ?
Dy3 O36 2.32(3) . ?
Dy3 O37 2.329(18) . ?
Dy4 Dy5 3.5283(14) . ?
Dy4 Dy6 3.5562(12) . ?
Dy4 Dy7A 3.6459(17) . ?
Dy4 O22 2.315(12) . ?
Dy4 O23 2.287(15) . ?
Dy4 O24 2.348(14) . ?
Dy4 O25 2.297(16) . ?
Dy4 O26 2.332(15) . ?
Dy4 O38 2.79(3) . ?
Dy4 O80 2.568(13) . ?
Dy4 O81 2.312(12) . ?
Dy5 Dy6 3.5337(13) . ?
Dy5 O9 2.366(16) . ?
Dy5 O12 2.318(11) . ?
Dy5 O24 2.408(11) . ?
Dy5 O43 2.414(15) . ?
Dy5 O62 2.555(19) . ?
Dy5 O63 2.46(2) . ?
Dy5 O80 2.335(16) . ?
Dy5 O81 2.386(11) . ?
Dy5 N13 2.526(18) . ?
Dy6 Dy13 3.5270(11) . ?
Dy6 Dy14 3.5764(13) . ?
Dy6 O8 2.386(14) . ?
Dy6 O12 2.395(14) . ?
Dy6 O25 2.411(15) . ?
Dy6 O30 2.36(2) . ?
Dy6 O33 2.391(11) . ?
Dy6 O34 2.375(13) . ?
Dy6 O80 2.351(12) . ?
Dy6 O81 2.395(13) . ?
Dy7 Dy7A 1.628(4) . ?
Dy7 Dy8 3.808(3) . ?
Dy7 Dy12 3.651(2) . ?
Dy7 Dy13 3.549(2) . ?
Dy7 O19 1.939(17) . ?
Dy7 O20 2.897(17) . ?
Dy7 O25 2.81(2) . ?
Dy7 O26 2.038(15) . ?
Dy7 O27 2.68(2) . ?
Dy7 O30 1.960(15) . ?
Dy7 O39 2.60(6) . ?
Dy7A Dy8 3.6944(16) . ?
Dy7A Dy13 3.6389(15) . ?
Dy7A O19 2.63(2) . ?
Dy7A O20 2.112(14) . ?
Dy7A O25 2.042(18) . ?
Dy7A O26 2.530(19) . ?
Dy7A O27 2.124(15) . ?
Dy7A O30 2.555(17) . ?
Dy7A O40 2.51(3) . ?
Dy8 Dy9 3.5827(14) . ?
Dy8 Dy11 3.5909(13) . ?
Dy8 O13 2.386(15) . ?
Dy8 O14 2.475(17) . ?
Dy8 O15 2.466(14) . ?
Dy8 O16 2.353(14) . ?
Dy8 O17 2.709(15) . ?
Dy8 O18 2.343(12) . ?
Dy8 O19 2.370(16) . ?
Dy8 O20 2.333(19) . ?
Dy8 O46 2.54(2) . ?
Dy9 Dy10 3.9012(14) . ?
Dy9 O1 2.215(15) . ?
Dy9 O2 2.341(14) . ?
Dy9 O13 2.362(12) . ?
Dy9 O14 2.32(2) . ?
Dy9 O15 2.370(16) . ?
Dy9 O47 2.37(2) . ?
Dy9 O49 2.42(2) . ?
Dy9 N1 2.505(18) . ?
Dy9 N19 2.87(4) . ?
Dy10 Dy11 3.8978(14) . ?
Dy10 O2 2.349(14) . ?
Dy10 O3 2.365(13) . ?
Dy10 O13 2.400(13) . ?
Dy10 O16 2.360(16) . ?
Dy10 O50 2.56(2) . ?
Dy10 O51 2.47(2) . ?
Dy10 O53 2.516(16) . ?
Dy10 O54 2.401(17) . ?
Dy10 N3 2.514(17) . ?
Dy10 N4 2.523(17) . ?
Dy11 Dy12 3.4916(14) . ?
Dy11 O3 2.342(15) . ?
Dy11 O4 2.325(12) . ?
Dy11 O16 2.395(14) . ?
Dy11 O17 2.304(15) . ?
Dy11 O18 2.385(12) . ?
Dy11 O35 2.423(14) . ?
Dy11 O65 2.660(18) . ?
Dy11 O66 2.45(2) . ?
Dy11 N6 2.486(18) . ?
Dy11 N25 2.862(15) . ?
Dy12 Dy13 3.5204(11) . ?
Dy12 Dy16 3.5972(15) . ?
Dy12 O4 2.393(14) . ?
Dy12 O5 2.363(14) . ?
Dy12 O17 2.315(13) . ?
Dy12 O18 2.416(15) . ?
Dy12 O19 2.419(14) . ?
Dy12 O27 2.359(14) . ?
Dy12 O28 2.345(15) . ?
Dy12 O29 2.416(11) . ?
Dy13 Dy14 3.5393(13) . ?
Dy13 Dy16 3.5403(14) . ?
Dy13 O27 2.290(14) . ?
Dy13 O28 2.416(13) . ?
Dy13 O29 2.389(11) . ?
Dy13 O30 2.269(15) . ?
Dy13 O31 2.298(14) . ?
Dy13 O32 2.338(13) . ?
Dy13 O33 2.395(12) . ?
Dy13 O34 2.385(13) . ?
Dy14 O7 2.389(13) . ?
Dy14 O8 2.329(13) . ?
Dy14 O32 2.424(13) . ?
Dy14 O33 2.387(14) . ?
Dy14 O34 2.369(11) . ?
Dy14 O42 2.46(3) . ?
Dy14 O77 2.53(2) . ?
Dy14 O79 2.43(2) . ?
Dy14 N12 2.486(17) . ?
Dy14 N28 2.77(3) . ?
Dy15 Dy16 3.9310(13) . ?
Dy15 O6 2.310(14) . ?
Dy15 O7 2.320(14) . ?
Dy15 O31 2.351(13) . ?
Dy15 O32 2.349(15) . ?
Dy15 O71 2.37(2) . ?
Dy15 O75 2.56(2) . ?
Dy15 O76 2.44(2) . ?
Dy15 N9 2.476(14) . ?
Dy15 N10 2.469(16) . ?
Dy16 O5 2.337(15) . ?
Dy16 O6 2.378(13) . ?
Dy16 O28 2.391(12) . ?
Dy16 O29 2.369(14) . ?
Dy16 O31 2.384(13) . ?
Dy16 O41 2.40(3) . ?
Dy16 O68 2.48(2) . ?
Dy16 O70 2.46(2) . ?
Dy16 N7 2.482(15) . ?
Dy16 N21 2.85(3) . ?
O1 C1 1.40(2) . ?
O2 C8 1.27(2) . ?
O3 C21 1.33(2) . ?
O4 C28 1.32(2) . ?
O5 C29 1.38(2) . ?
O6 C36 1.28(2) . ?
O7 C49 1.26(2) . ?
O8 C56 1.32(2) . ?
O9 C64 1.30(2) . ?
O10 C77 1.26(2) . ?
O11 C84 1.37(2) . ?
O12 C57 1.366(13) . ?
O47 N19 1.24(4) . ?
O48 N19 1.32(4) . ?
O49 N19 1.37(4) . ?
O50 N20 1.37(3) . ?
O51 N20 1.21(3) . ?
O52 N20 1.23(3) . ?
O53 N26 1.296(10) . ?
O54 N26 1.287(10) . ?
O55 N26 1.309(10) . ?
O56 N24 1.299(10) . ?
O57 N24 1.279(10) . ?
O58 N24 1.289(10) . ?
O59 N27 1.295(10) . ?
O60 N27 1.286(10) . ?
O61 N27 1.291(10) . ?
O62 N22 1.33(3) . ?
O63 N22 1.14(3) . ?
O64 N22 1.34(4) . ?
O65 N25 1.172(8) . ?
O66 N25 1.223(7) . ?
O67 N25 1.243(7) . ?
O68 N21 1.38(3) . ?
O69 N21 1.34(3) . ?
O70 N21 1.42(3) . ?
O71 N23 1.13(3) . ?
O72 N23 1.18(3) . ?
O73 N23 1.29(3) . ?
O74 N29 1.304(10) . ?
O75 N29 1.300(10) . ?
O76 N29 1.287(10) . ?
O77 N28 1.317(10) . ?
O78 N28 1.311(10) . ?
O79 N28 1.312(10) . ?
N1 N2 1.43(3) . ?
N1 C7 1.26(3) . ?
N2 C8 1.28(3) . ?
N3 C9 1.30(3) . ?
N3 C17 1.35(3) . ?
N4 C16 1.44(3) . ?
N4 C20 1.33(3) . ?
N5 N6 1.46(2) . ?
N5 C21 1.26(3) . ?
N6 C22 1.29(3) . ?
N7 N8 1.48(2) . ?
N7 C35 1.32(3) . ?
N8 C36 1.30(2) . ?
N9 C37 1.32(3) . ?
N9 C45 1.35(2) . ?
N10 C44 1.35(3) . ?
N10 C48 1.35(2) . ?
N11 N12 1.44(2) . ?
N11 C49 1.32(3) . ?
N12 C50 1.30(2) . ?
N13 N14 1.45(2) . ?
N13 C63 1.29(2) . ?
N14 C64 1.29(2) . ?
N15 C65 1.36(3) . ?
N15 C69 1.39(3) . ?
N16 C73 1.34(3) . ?
N16 C76 1.38(3) . ?
N17 N18 1.36(3) . ?
N17 C77 1.33(3) . ?
N18 C78 1.30(3) . ?
C1 C6 1.3900 . ?
C1 C2 1.3900 . ?
C6 C4 1.3900 . ?
C6 C7 1.46(3) . ?
C4 C5 1.3900 . ?
C5 C3 1.3900 . ?
C3 C2 1.3900 . ?
C8 C9 1.53(3) . ?
C9 C10 1.41(3) . ?
C10 C11 1.30(3) . ?
C11 C12 1.36(3) . ?
C12 C13 1.46(4) . ?
C12 C17 1.40(3) . ?
C13 C14 1.37(4) . ?
C14 C15 1.41(3) . ?
C15 C16 1.39(3) . ?
C15 C18 1.45(3) . ?
C16 C17 1.38(3) . ?
C18 C19 1.36(3) . ?
C19 C20 1.46(3) . ?
C20 C21 1.42(3) . ?
C22 C23 1.52(3) . ?
C23 C24 1.37(3) . ?
C23 C28 1.43(3) . ?
C24 C25 1.35(3) . ?
C25 C26 1.37(3) . ?
C26 C27 1.40(3) . ?
C27 C28 1.42(3) . ?
C29 C30 1.46(3) . ?
C29 C34 1.40(3) . ?
C30 C31 1.39(4) . ?
C31 C32 1.33(4) . ?
C32 C33 1.39(4) . ?
C33 C34 1.37(3) . ?
C34 C35 1.43(3) . ?
C36 C37 1.51(3) . ?
C37 C38 1.41(3) . ?
C38 C39 1.31(3) . ?
C39 C40 1.45(3) . ?
C40 C41 1.42(3) . ?
C40 C45 1.36(3) . ?
C41 C42 1.33(4) . ?
C42 C43 1.51(3) . ?
C43 C44 1.39(2) . ?
C43 C46 1.36(3) . ?
C44 C45 1.46(3) . ?
C46 C47 1.37(3) . ?
C47 C48 1.42(3) . ?
C48 C49 1.51(3) . ?
C50 C51 1.45(3) . ?
C51 C52 1.38(3) . ?
C51 C56 1.43(3) . ?
C52 C53 1.38(3) . ?
C53 C54 1.38(4) . ?
C54 C55 1.36(4) . ?
C55 C56 1.38(3) . ?
C58 C57 1.3900 . ?
C58 C59 1.3900 . ?
C57 C61 1.3900 . ?
C61 C62 1.3900 . ?
C61 C63 1.44(2) . ?
C62 C60 1.3900 . ?
C60 C59 1.3900 . ?
C64 C65 1.49(3) . ?
C65 C66 1.36(3) . ?
C66 C67 1.38(3) . ?
C67 C68 1.33(4) . ?
C68 C69 1.41(4) . ?
C68 C70 1.43(3) . ?
C69 C73 1.42(4) . ?
C70 C71 1.38(4) . ?
C71 C72 1.40(4) . ?
C72 C73 1.41(3) . ?
C72 C74 1.37(4) . ?
C74 C75 1.38(4) . ?
C75 C76 1.41(3) . ?
C76 C77 1.51(4) . ?
C78 C79 1.42(3) . ?
C79 C84 1.3900 . ?
C79 C81 1.3900 . ?
C84 C83 1.3900 . ?
C83 C82 1.3900 . ?
C82 C80 1.3900 . ?
C80 C81 1.3900 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Dy4 Dy1 Dy5 54.58(2) . . ?
O9 Dy1 Dy4 85.7(3) . . ?
O9 Dy1 Dy5 33.6(4) . . ?
O9 Dy1 O10 165.1(6) . . ?
O9 Dy1 O23 107.2(5) . . ?
O9 Dy1 O24 67.1(5) . . ?
O9 Dy1 O44 86.0(6) . . ?
O9 Dy1 O60 113.2(6) . . ?
O9 Dy1 O61 66.0(7) . . ?
O9 Dy1 N15 63.7(5) . . ?
O9 Dy1 N16 124.9(6) . . ?
O9 Dy1 N27 89.4(6) . . ?
O10 Dy1 Dy4 82.8(3) . . ?
O10 Dy1 Dy5 132.1(4) . . ?
O10 Dy1 O23 67.9(5) . . ?
O10 Dy1 O24 98.1(5) . . ?
O10 Dy1 O44 87.7(6) . . ?
O10 Dy1 O60 80.2(6) . . ?
O10 Dy1 O61 123.2(6) . . ?
O10 Dy1 N15 128.3(5) . . ?
O10 Dy1 N16 65.1(6) . . ?
O10 Dy1 N27 102.4(6) . . ?
O23 Dy1 Dy4 35.5(4) . . ?
O23 Dy1 Dy5 84.2(3) . . ?
O23 Dy1 O44 132.9(6) . . ?
O23 Dy1 O60 78.6(5) . . ?
O23 Dy1 O61 73.5(6) . . ?
O23 Dy1 N15 146.7(6) . . ?
O23 Dy1 N16 125.5(6) . . ?
O23 Dy1 N27 75.0(6) . . ?
O24 Dy1 Dy4 37.0(4) . . ?
O24 Dy1 Dy5 34.8(3) . . ?
O24 Dy1 O23 72.4(5) . . ?
O24 Dy1 O44 72.0(6) . . ?
O24 Dy1 O60 149.1(5) . . ?
O24 Dy1 O61 108.3(5) . . ?
O24 Dy1 N15 124.2(6) . . ?
O24 Dy1 N16 139.5(6) . . ?
O24 Dy1 N27 131.0(5) . . ?
O44 Dy1 Dy4 104.9(4) . . ?
O44 Dy1 Dy5 83.9(4) . . ?
O44 Dy1 O60 138.1(5) . . ?
O44 Dy1 O61 147.9(6) . . ?
O44 Dy1 N15 79.9(6) . . ?
O44 Dy1 N16 70.8(6) . . ?
O44 Dy1 N27 151.7(6) . . ?
O60 Dy1 Dy4 113.1(4) . . ?
O60 Dy1 Dy5 132.8(4) . . ?
O60 Dy1 N27 25.9(3) . . ?
O61 Dy1 Dy4 89.2(4) . . ?
O61 Dy1 Dy5 81.1(4) . . ?
O61 Dy1 O60 51.9(5) . . ?
O61 Dy1 N27 26.0(3) . . ?
N15 Dy1 Dy4 148.8(4) . . ?
N15 Dy1 Dy5 96.4(4) . . ?
N15 Dy1 O60 76.9(6) . . ?
N15 Dy1 O61 73.8(6) . . ?
N15 Dy1 N16 63.4(6) . . ?
N15 Dy1 N27 73.0(6) . . ?
N16 Dy1 Dy4 147.6(5) . . ?
N16 Dy1 Dy5 149.5(5) . . ?
N16 Dy1 O60 67.7(6) . . ?
N16 Dy1 O61 111.7(7) . . ?
N16 Dy1 N27 89.4(7) . . ?
N27 Dy1 Dy4 102.6(4) . . ?
N27 Dy1 Dy5 107.0(4) . . ?
Dy3 Dy2 Dy4 61.19(3) . . ?
O10 Dy2 Dy3 133.0(4) . . ?
O10 Dy2 Dy4 85.2(3) . . ?
O10 Dy2 O23 66.4(4) . . ?
O10 Dy2 O45 124.4(6) . . ?
O10 Dy2 O58 108.5(7) . . ?
O10 Dy2 N18 61.9(6) . . ?
O10 Dy2 N24 90.0(6) . . ?
O11 Dy2 Dy3 46.0(4) . . ?
O11 Dy2 Dy4 102.2(4) . . ?
O11 Dy2 O10 124.2(7) . . ?
O11 Dy2 O23 140.3(5) . . ?
O11 Dy2 O45 73.9(7) . . ?
O11 Dy2 O58 125.3(9) . . ?
O11 Dy2 N18 73.2(7) . . ?
O11 Dy2 N24 131.6(6) . . ?
O21 Dy2 Dy3 36.7(5) . . ?
O21 Dy2 Dy4 53.9(5) . . ?
O21 Dy2 O10 138.3(6) . . ?
O21 Dy2 O11 77.7(7) . . ?
O21 Dy2 O22 66.6(7) . . ?
O21 Dy2 O23 75.1(6) . . ?
O21 Dy2 O45 94.2(7) . . ?
O21 Dy2 O58 71.7(7) . . ?
O21 Dy2 N18 150.8(7) . . ?
O21 Dy2 N24 99.6(7) . . ?
O22 Dy2 Dy3 46.2(4) . . ?
O22 Dy2 Dy4 38.2(3) . . ?
O22 Dy2 O10 86.9(6) . . ?
O22 Dy2 O11 70.1(6) . . ?
O22 Dy2 O23 72.9(5) . . ?
O22 Dy2 O45 141.9(6) . . ?
O22 Dy2 O58 130.5(6) . . ?
O22 Dy2 N18 100.7(7) . . ?
O22 Dy2 N24 153.2(5) . . ?
O23 Dy2 Dy3 96.9(3) . . ?
O23 Dy2 Dy4 38.2(4) . . ?
O23 Dy2 O58 71.5(7) . . ?
O23 Dy2 N18 128.2(6) . . ?
O23 Dy2 N24 81.5(5) . . ?
O45 Dy2 Dy3 98.6(4) . . ?
O45 Dy2 Dy4 147.4(5) . . ?
O45 Dy2 O23 136.0(7) . . ?
O45 Dy2 O58 64.7(8) . . ?
O45 Dy2 N18 79.9(7) . . ?
O45 Dy2 N24 58.0(6) . . ?
O57 Dy2 Dy3 160.3(6) . . ?
O57 Dy2 Dy4 124.2(7) . . ?
O57 Dy2 O10 66.0(7) . . ?
O57 Dy2 O11 133.6(8) . . ?
O57 Dy2 O21 127.7(8) . . ?
O57 Dy2 O22 150.9(7) . . ?
O57 Dy2 O23 86.1(8) . . ?
O57 Dy2 O45 66.9(8) . . ?
O57 Dy2 O58 56.0(5) . . ?
O57 Dy2 N18 76.4(8) . . ?
O57 Dy2 N24 28.6(3) . . ?
O58 Dy2 Dy3 106.4(4) . . ?
O58 Dy2 Dy4 94.9(5) . . ?
O58 Dy2 N24 28.1(3) . . ?
N18 Dy2 Dy3 115.5(5) . . ?
N18 Dy2 Dy4 130.9(6) . . ?
N18 Dy2 O58 128.3(7) . . ?
N18 Dy2 N24 101.2(7) . . ?
N24 Dy2 Dy3 132.5(4) . . ?
N24 Dy2 Dy4 115.1(3) . . ?
Dy2 Dy3 Dy4 60.63(3) . . ?
Dy2 Dy3 Dy7 115.96(5) . . ?
Dy2 Dy3 Dy7A 103.63(4) . . ?
Dy4 Dy3 Dy7 58.52(4) . . ?
Dy4 Dy3 Dy7A 59.62(3) . . ?
Dy7A Dy3 Dy7 24.78(6) . . ?
O11 Dy3 Dy2 40.7(4) . . ?
O11 Dy3 Dy4 96.9(4) . . ?
O11 Dy3 Dy7 155.3(4) . . ?
O11 Dy3 Dy7A 142.9(5) . . ?
O11 Dy3 O22 62.5(5) . . ?
O15 Dy3 Dy2 172.9(3) . . ?
O15 Dy3 Dy4 123.5(4) . . ?
O15 Dy3 Dy7 70.1(4) . . ?
O15 Dy3 Dy7A 83.3(3) . . ?
O15 Dy3 O11 132.7(5) . . ?
O15 Dy3 O20 68.3(6) . . ?
O15 Dy3 O22 138.2(6) . . ?
O20 Dy3 Dy2 118.2(5) . . ?
O20 Dy3 Dy4 91.7(4) . . ?
O20 Dy3 Dy7 48.5(4) . . ?
O20 Dy3 Dy7A 33.1(4) . . ?
O20 Dy3 O11 140.2(8) . . ?
O20 Dy3 O22 129.6(5) . . ?
O21 Dy3 Dy2 38.6(4) . . ?
O21 Dy3 Dy4 53.6(5) . . ?
O21 Dy3 Dy7 87.8(5) . . ?
O21 Dy3 Dy7A 68.4(5) . . ?
O21 Dy3 O11 74.5(7) . . ?
O21 Dy3 O15 148.2(6) . . ?
O21 Dy3 O20 79.9(7) . . ?
O21 Dy3 O22 63.5(6) . . ?
O21 Dy3 O26 83.8(7) . . ?
O21 Dy3 O36 93.0(12) . . ?
O21 Dy3 O37 138.5(6) . . ?
O22 Dy3 Dy2 40.5(4) . . ?
O22 Dy3 Dy4 38.9(3) . . ?
O22 Dy3 Dy7 94.5(3) . . ?
O22 Dy3 Dy7A 98.5(3) . . ?
O26 Dy3 Dy2 99.0(4) . . ?
O26 Dy3 Dy4 38.3(4) . . ?
O26 Dy3 Dy7 26.0(4) . . ?
O26 Dy3 Dy7A 43.0(5) . . ?
O26 Dy3 O11 132.1(6) . . ?
O26 Dy3 O15 85.3(5) . . ?
O26 Dy3 O20 73.1(6) . . ?
O26 Dy3 O22 69.7(5) . . ?
O36 Dy3 Dy2 99.1(7) . . ?
O36 Dy3 Dy4 145.8(11) . . ?
O36 Dy3 Dy7 120.6(8) . . ?
O36 Dy3 Dy7A 104.8(10) . . ?
O36 Dy3 O11 78.1(8) . . ?
O36 Dy3 O15 79.9(9) . . ?
O36 Dy3 O20 73.2(10) . . ?
O36 Dy3 O22 137.8(7) . . ?
O36 Dy3 O26 146.3(10) . . ?
O36 Dy3 O37 112.1(13) . . ?
O37 Dy3 Dy2 102.7(4) . . ?
O37 Dy3 Dy4 99.8(4) . . ?
O37 Dy3 Dy7 105.1(4) . . ?
O37 Dy3 Dy7A 129.9(4) . . ?
O37 Dy3 O11 78.9(7) . . ?
O37 Dy3 O15 71.4(6) . . ?
O37 Dy3 O20 137.7(7) . . ?
O37 Dy3 O22 76.1(5) . . ?
O37 Dy3 O26 91.2(6) . . ?
Dy2 Dy4 Dy7A 102.42(4) . . ?
Dy5 Dy4 Dy2 130.24(4) . . ?
Dy5 Dy4 Dy6 59.84(3) . . ?
Dy5 Dy4 Dy7A 121.71(3) . . ?
Dy6 Dy4 Dy2 140.96(6) . . ?
Dy6 Dy4 Dy7A 63.57(3) . . ?
O22 Dy4 Dy2 38.1(4) . . ?
O22 Dy4 Dy5 131.6(4) . . ?
O22 Dy4 Dy6 168.0(4) . . ?
O22 Dy4 Dy7A 104.5(4) . . ?
O22 Dy4 O24 90.0(5) . . ?
O22 Dy4 O26 74.3(5) . . ?
O22 Dy4 O38 72.3(7) . . ?
O22 Dy4 O80 148.1(5) . . ?
O23 Dy4 Dy2 41.3(3) . . ?
O23 Dy4 Dy5 95.3(3) . . ?
O23 Dy4 Dy6 108.9(4) . . ?
O23 Dy4 Dy7A 115.2(4) . . ?
O23 Dy4 O22 75.7(5) . . ?
O23 Dy4 O24 74.0(5) . . ?
O23 Dy4 O25 98.2(7) . . ?
O23 Dy4 O26 134.0(5) . . ?
O23 Dy4 O38 131.9(6) . . ?
O23 Dy4 O80 74.7(5) . . ?
O23 Dy4 O81 133.7(5) . . ?
O24 Dy4 Dy2 92.8(3) . . ?
O24 Dy4 Dy5 42.8(3) . . ?
O24 Dy4 Dy6 101.9(3) . . ?
O24 Dy4 Dy7A 164.2(3) . . ?
O24 Dy4 O38 71.2(6) . . ?
O24 Dy4 O80 70.5(5) . . ?
O25 Dy4 Dy2 107.2(5) . . ?
O25 Dy4 Dy5 101.0(4) . . ?
O25 Dy4 Dy6 42.2(4) . . ?
O25 Dy4 Dy7A 30.7(5) . . ?
O25 Dy4 O22 127.2(6) . . ?
O25 Dy4 O24 139.7(5) . . ?
O25 Dy4 O26 74.0(7) . . ?
O25 Dy4 O38 129.7(8) . . ?
O25 Dy4 O80 69.3(5) . . ?
O25 Dy4 O81 78.8(5) . . ?
O26 Dy4 Dy2 96.6(3) . . ?
O26 Dy4 Dy5 130.7(4) . . ?
O26 Dy4 Dy6 95.3(3) . . ?
O26 Dy4 Dy7A 43.5(5) . . ?
O26 Dy4 O24 139.3(7) . . ?
O26 Dy4 O38 68.3(7) . . ?
O26 Dy4 O80 136.5(4) . . ?
O38 Dy4 Dy2 109.1(5) . . ?
O38 Dy4 Dy5 80.7(5) . . ?
O38 Dy4 Dy6 109.9(5) . . ?
O38 Dy4 Dy7A 106.9(5) . . ?
O80 Dy4 Dy2 115.6(3) . . ?
O80 Dy4 Dy5 41.4(3) . . ?
O80 Dy4 Dy6 41.3(3) . . ?
O80 Dy4 Dy7A 98.8(3) . . ?
O80 Dy4 O38 121.2(6) . . ?
O81 Dy4 Dy2 172.0(3) . . ?
O81 Dy4 Dy5 42.1(3) . . ?
O81 Dy4 Dy6 41.8(3) . . ?
O81 Dy4 Dy7A 85.4(3) . . ?
O81 Dy4 O22 141.7(6) . . ?
O81 Dy4 O24 79.3(4) . . ?
O81 Dy4 O26 90.1(5) . . ?
O81 Dy4 O38 69.5(6) . . ?
O81 Dy4 O80 60.9(5) . . ?
Dy4 Dy5 Dy1 60.12(3) . . ?
Dy4 Dy5 Dy6 60.47(3) . . ?
Dy6 Dy5 Dy1 104.25(4) . . ?
O9 Dy5 Dy1 33.2(4) . . ?
O9 Dy5 Dy4 90.7(4) . . ?
O9 Dy5 Dy6 113.8(5) . . ?
O9 Dy5 O24 65.9(5) . . ?
O9 Dy5 O43 75.1(6) . . ?
O9 Dy5 O62 123.1(6) . . ?
O9 Dy5 O63 147.7(6) . . ?
O9 Dy5 O81 130.0(5) . . ?
O9 Dy5 N13 63.6(5) . . ?
O12 Dy5 Dy1 137.2(5) . . ?
O12 Dy5 Dy4 102.2(3) . . ?
O12 Dy5 Dy6 42.3(3) . . ?
O12 Dy5 O9 123.3(6) . . ?
O12 Dy5 O24 143.4(5) . . ?
O12 Dy5 O43 124.1(5) . . ?
O12 Dy5 O62 113.0(6) . . ?
O12 Dy5 O63 70.9(7) . . ?
O12 Dy5 O80 75.5(5) . . ?
O12 Dy5 O81 72.2(4) . . ?
O12 Dy5 N13 71.5(4) . . ?
O24 Dy5 Dy1 34.0(4) . . ?
O24 Dy5 Dy4 41.5(3) . . ?
O24 Dy5 Dy6 101.2(4) . . ?
O24 Dy5 O43 92.2(5) . . ?
O24 Dy5 O62 74.1(6) . . ?
O24 Dy5 O63 122.2(7) . . ?
O24 Dy5 N13 129.5(5) . . ?
O43 Dy5 Dy1 89.0(4) . . ?
O43 Dy5 Dy4 132.0(4) . . ?
O43 Dy5 Dy6 166.1(4) . . ?
O43 Dy5 O62 67.7(6) . . ?
O43 Dy5 O63 73.5(6) . . ?
O43 Dy5 N13 74.7(6) . . ?
O62 Dy5 Dy1 104.0(4) . . ?
O62 Dy5 Dy4 84.2(4) . . ?
O62 Dy5 Dy6 112.2(3) . . ?
O63 Dy5 Dy1 151.2(5) . . ?
O63 Dy5 Dy4 115.9(5) . . ?
O63 Dy5 Dy6 95.8(4) . . ?
O63 Dy5 O62 48.5(7) . . ?
O63 Dy5 N13 100.8(7) . . ?
O80 Dy5 Dy1 64.2(3) . . ?
O80 Dy5 Dy4 46.7(3) . . ?
O80 Dy5 Dy6 41.2(3) . . ?
O80 Dy5 O9 74.7(6) . . ?
O80 Dy5 O24 73.7(5) . . ?
O80 Dy5 O43 149.8(5) . . ?
O80 Dy5 O62 129.9(5) . . ?
O80 Dy5 O63 136.7(5) . . ?
O80 Dy5 O81 63.5(5) . . ?
O80 Dy5 N13 93.6(6) . . ?
O81 Dy5 Dy1 100.6(3) . . ?
O81 Dy5 Dy4 40.5(3) . . ?
O81 Dy5 Dy6 42.4(3) . . ?
O81 Dy5 O24 76.6(4) . . ?
O81 Dy5 O43 140.1(6) . . ?
O81 Dy5 O62 72.4(5) . . ?
O81 Dy5 O63 80.5(5) . . ?
O81 Dy5 N13 140.9(5) . . ?
N13 Dy5 Dy1 96.1(4) . . ?
N13 Dy5 Dy4 138.7(5) . . ?
N13 Dy5 Dy6 99.2(4) . . ?
N13 Dy5 O62 136.5(6) . . ?
Dy4 Dy6 Dy14 153.10(5) . . ?
Dy5 Dy6 Dy4 59.69(3) . . ?
Dy5 Dy6 Dy14 139.63(3) . . ?
Dy13 Dy6 Dy4 115.34(3) . . ?
Dy13 Dy6 Dy5 148.25(5) . . ?
Dy13 Dy6 Dy14 59.76(3) . . ?
O8 Dy6 Dy4 132.7(3) . . ?
O8 Dy6 Dy5 104.6(3) . . ?
O8 Dy6 Dy13 99.8(3) . . ?
O8 Dy6 Dy14 40.1(3) . . ?
O8 Dy6 O12 82.5(5) . . ?
O8 Dy6 O25 118.5(7) . . ?
O8 Dy6 O33 73.6(4) . . ?
O8 Dy6 O81 146.8(4) . . ?
O12 Dy6 Dy4 99.8(3) . . ?
O12 Dy6 Dy5 40.6(3) . . ?
O12 Dy6 Dy13 125.7(3) . . ?
O12 Dy6 Dy14 103.6(3) . . ?
O12 Dy6 O25 139.1(4) . . ?
O12 Dy6 O81 70.7(4) . . ?
O25 Dy6 Dy4 39.8(4) . . ?
O25 Dy6 Dy5 98.5(4) . . ?
O25 Dy6 Dy13 87.2(4) . . ?
O25 Dy6 Dy14 114.9(4) . . ?
O30 Dy6 Dy4 79.9(3) . . ?
O30 Dy6 Dy5 114.8(4) . . ?
O30 Dy6 Dy13 39.4(4) . . ?
O30 Dy6 Dy14 99.2(4) . . ?
O30 Dy6 O8 139.0(5) . . ?
O30 Dy6 O12 120.8(6) . . ?
O30 Dy6 O25 67.5(7) . . ?
O30 Dy6 O33 73.7(5) . . ?
O30 Dy6 O34 72.5(5) . . ?
O30 Dy6 O81 73.5(5) . . ?
O33 Dy6 Dy4 153.0(3) . . ?
O33 Dy6 Dy5 127.6(3) . . ?
O33 Dy6 Dy13 42.6(3) . . ?
O33 Dy6 Dy14 41.5(3) . . ?
O33 Dy6 O12 89.0(4) . . ?
O33 Dy6 O25 129.1(5) . . ?
O33 Dy6 O81 123.6(5) . . ?
O34 Dy6 Dy4 115.7(3) . . ?
O34 Dy6 Dy5 168.9(3) . . ?
O34 Dy6 Dy13 42.3(3) . . ?
O34 Dy6 Dy14 41.0(3) . . ?
O34 Dy6 O8 70.6(5) . . ?
O34 Dy6 O12 144.3(4) . . ?
O34 Dy6 O25 76.0(5) . . ?
O34 Dy6 O33 61.5(4) . . ?
O34 Dy6 O81 141.5(4) . . ?
O80 Dy6 Dy4 46.2(3) . . ?
O80 Dy6 Dy5 40.9(4) . . ?
O80 Dy6 Dy13 158.4(3) . . ?
O80 Dy6 Dy14 129.7(4) . . ?
O80 Dy6 O8 91.3(5) . . ?
O80 Dy6 O12 73.8(4) . . ?
O80 Dy6 O25 71.2(5) . . ?
O80 Dy6 O30 125.9(5) . . ?
O80 Dy6 O33 158.6(4) . . ?
O80 Dy6 O34 128.2(5) . . ?
O80 Dy6 O81 63.1(5) . . ?
O81 Dy6 Dy4 40.1(3) . . ?
O81 Dy6 Dy5 42.2(3) . . ?
O81 Dy6 Dy13 111.6(3) . . ?
O81 Dy6 Dy14 165.0(3) . . ?
O81 Dy6 O25 75.0(5) . . ?
Dy4 Dy7 Dy8 118.46(7) . . ?
Dy7A Dy7 Dy4 75.96(10) . . ?
Dy7A Dy7 Dy8 73.58(10) . . ?
Dy7A Dy7 Dy12 84.51(11) . . ?
Dy7A Dy7 Dy13 80.00(10) . . ?
Dy7A Dy7 O19 94.4(7) . . ?
Dy7A Dy7 O20 45.7(4) . . ?
Dy7A Dy7 O25 45.8(4) . . ?
Dy7A Dy7 O26 86.5(6) . . ?
Dy7A Dy7 O27 52.4(4) . . ?
Dy7A Dy7 O30 90.3(7) . . ?
Dy7A Dy7 O39 171.2(14) . . ?
Dy12 Dy7 Dy4 159.72(11) . . ?
Dy12 Dy7 Dy8 59.33(4) . . ?
Dy13 Dy7 Dy4 111.73(6) . . ?
Dy13 Dy7 Dy8 113.75(7) . . ?
Dy13 Dy7 Dy12 58.52(4) . . ?
O19 Dy7 Dy4 148.2(5) . . ?
O19 Dy7 Dy8 31.1(6) . . ?
O19 Dy7 Dy12 37.5(4) . . ?
O19 Dy7 Dy13 95.8(4) . . ?
O19 Dy7 O20 68.3(7) . . ?
O19 Dy7 O25 140.1(7) . . ?
O19 Dy7 O26 115.4(6) . . ?
O19 Dy7 O27 71.6(6) . . ?
O19 Dy7 O30 129.4(6) . . ?
O19 Dy7 O39 92.8(15) . . ?
O20 Dy7 Dy4 84.2(3) . . ?
O20 Dy7 Dy8 37.7(4) . . ?
O20 Dy7 Dy12 86.0(3) . . ?
O20 Dy7 Dy13 118.8(3) . . ?
O25 Dy7 Dy4 38.6(3) . . ?
O25 Dy7 Dy8 114.9(3) . . ?
O25 Dy7 Dy12 121.8(3) . . ?
O25 Dy7 Dy13 81.1(3) . . ?
O25 Dy7 O20 78.4(5) . . ?
O26 Dy7 Dy4 35.2(4) . . ?
O26 Dy7 Dy8 90.8(4) . . ?
O26 Dy7 Dy12 150.1(4) . . ?
O26 Dy7 Dy13 146.8(4) . . ?
O26 Dy7 O20 67.6(6) . . ?
O26 Dy7 O25 68.0(6) . . ?
O26 Dy7 O27 138.8(7) . . ?
O26 Dy7 O39 95.0(14) . . ?
O27 Dy7 Dy4 120.2(3) . . ?
O27 Dy7 Dy8 77.1(3) . . ?
O27 Dy7 Dy12 40.2(3) . . ?
O27 Dy7 Dy13 40.2(3) . . ?
O27 Dy7 O20 79.9(5) . . ?
O27 Dy7 O25 81.7(5) . . ?
O30 Dy7 Dy4 81.5(5) . . ?
O30 Dy7 Dy8 148.9(5) . . ?
O30 Dy7 Dy12 93.4(5) . . ?
O30 Dy7 Dy13 35.8(4) . . ?
O30 Dy7 O20 136.0(8) . . ?
O30 Dy7 O25 64.7(7) . . ?
O30 Dy7 O26 115.1(6) . . ?
O30 Dy7 O27 72.1(6) . . ?
O30 Dy7 O39 81.1(15) . . ?
O39 Dy7 Dy4 100.4(13) . . ?
O39 Dy7 Dy8 115.0(14) . . ?
O39 Dy7 Dy12 98.2(13) . . ?
O39 Dy7 Dy13 94.2(13) . . ?
O39 Dy7 O20 142.6(14) . . ?
O39 Dy7 O25 127.0(14) . . ?
O39 Dy7 O27 125.9(13) . . ?
Dy3 Dy7A Dy8 64.81(3) . . ?
Dy4 Dy7A Dy3 59.98(3) . . ?
Dy4 Dy7A Dy8 122.50(4) . . ?
Dy7 Dy7A Dy3 84.08(9) . . ?
Dy7 Dy7A Dy4 78.38(10) . . ?
Dy7 Dy7A Dy8 81.41(10) . . ?
Dy7 Dy7A Dy13 73.86(8) . . ?
Dy7 Dy7A O19 47.4(4) . . ?
Dy7 Dy7A O20 100.8(6) . . ?
Dy7 Dy7A O25 99.4(6) . . ?
Dy7 Dy7A O26 53.5(4) . . ?
Dy7 Dy7A O27 90.3(6) . . ?
Dy7 Dy7A O30 50.1(5) . . ?
Dy7 Dy7A O40 172.2(8) . . ?
Dy13 Dy7A Dy3 157.60(7) . . ?
Dy13 Dy7A Dy4 110.49(4) . . ?
Dy13 Dy7A Dy8 114.38(4) . . ?
O19 Dy7A Dy3 85.1(3) . . ?
O19 Dy7A Dy4 118.9(3) . . ?
O19 Dy7A Dy8 39.7(4) . . ?
O19 Dy7A Dy13 82.9(3) . . ?
O20 Dy7A Dy3 38.8(4) . . ?
O20 Dy7A Dy4 97.6(4) . . ?
O20 Dy7A Dy8 35.7(5) . . ?
O20 Dy7A Dy13 149.2(5) . . ?
O20 Dy7A O19 72.4(7) . . ?
O20 Dy7A O26 74.7(6) . . ?
O20 Dy7A O27 115.8(5) . . ?
O20 Dy7A O30 150.7(8) . . ?
O20 Dy7A O40 84.6(9) . . ?
O25 Dy7A Dy3 89.8(4) . . ?
O25 Dy7A Dy4 35.1(5) . . ?
O25 Dy7A Dy8 154.4(4) . . ?
O25 Dy7A Dy13 90.0(4) . . ?
O25 Dy7A O19 146.7(7) . . ?
O25 Dy7A O20 120.7(6) . . ?
O25 Dy7A O26 74.2(6) . . ?
O25 Dy7A O27 119.3(5) . . ?
O25 Dy7A O30 69.4(7) . . ?
O25 Dy7A O40 82.4(9) . . ?
O26 Dy7A Dy3 39.0(3) . . ?
O26 Dy7A Dy4 39.4(4) . . ?
O26 Dy7A Dy8 86.4(3) . . ?
O26 Dy7A Dy13 120.0(3) . . ?
O26 Dy7A O19 81.4(5) . . ?
O26 Dy7A O30 83.1(5) . . ?
O27 Dy7A Dy3 151.0(3) . . ?
O27 Dy7A Dy4 146.3(4) . . ?
O27 Dy7A Dy8 86.2(3) . . ?
O27 Dy7A Dy13 36.0(4) . . ?
O27 Dy7A O19 70.5(5) . . ?
O27 Dy7A O26 143.8(7) . . ?
O27 Dy7A O30 72.6(6) . . ?
O27 Dy7A O40 82.3(9) . . ?
O30 Dy7A Dy3 122.2(4) . . ?
O30 Dy7A Dy4 75.8(4) . . ?
O30 Dy7A Dy8 125.4(5) . . ?
O30 Dy7A Dy13 38.2(3) . . ?
O30 Dy7A O19 85.7(6) . . ?
O40 Dy7A Dy3 103.5(7) . . ?
O40 Dy7A Dy4 106.7(7) . . ?
O40 Dy7A Dy8 100.3(7) . . ?
O40 Dy7A Dy13 98.6(7) . . ?
O40 Dy7A O19 130.7(8) . . ?
O40 Dy7A O26 134.0(8) . . ?
O40 Dy7A O30 124.7(9) . . ?
Dy9 Dy8 Dy7A 123.30(4) . . ?
Dy9 Dy8 Dy11 126.41(4) . . ?
Dy11 Dy8 Dy7A 108.82(4) . . ?
O13 Dy8 Dy7A 137.9(4) . . ?
O13 Dy8 Dy9 40.8(3) . . ?
O13 Dy8 Dy11 92.0(3) . . ?
O13 Dy8 O14 70.7(5) . . ?
O13 Dy8 O15 72.3(5) . . ?
O13 Dy8 O17 71.7(4) . . ?
O13 Dy8 O46 131.9(6) . . ?
O14 Dy8 Dy7A 125.3(4) . . ?
O14 Dy8 Dy9 40.1(5) . . ?
O14 Dy8 Dy11 116.1(5) . . ?
O14 Dy8 O17 133.4(5) . . ?
O14 Dy8 O46 68.9(6) . . ?
O15 Dy8 Dy7A 82.1(4) . . ?
O15 Dy8 Dy9 41.2(4) . . ?
O15 Dy8 Dy11 164.0(4) . . ?
O15 Dy8 O14 62.4(6) . . ?
O15 Dy8 O17 128.1(5) . . ?
O15 Dy8 O46 109.5(6) . . ?
O16 Dy8 Dy7A 145.0(4) . . ?
O16 Dy8 Dy9 91.0(4) . . ?
O16 Dy8 Dy11 41.3(3) . . ?
O16 Dy8 O13 72.2(5) . . ?
O16 Dy8 O14 75.3(6) . . ?
O16 Dy8 O15 131.5(5) . . ?
O16 Dy8 O17 67.6(5) . . ?
O16 Dy8 O19 134.0(6) . . ?
O16 Dy8 O46 73.1(7) . . ?
O17 Dy8 Dy7A 101.2(3) . . ?
O17 Dy8 Dy9 112.3(3) . . ?
O17 Dy8 Dy11 39.9(3) . . ?
O18 Dy8 Dy7A 68.6(3) . . ?
O18 Dy8 Dy9 167.3(3) . . ?
O18 Dy8 Dy11 41.0(3) . . ?
O18 Dy8 O13 128.2(4) . . ?
O18 Dy8 O14 139.1(6) . . ?
O18 Dy8 O15 150.5(5) . . ?
O18 Dy8 O16 78.0(4) . . ?
O18 Dy8 O17 57.9(5) . . ?
O18 Dy8 O19 74.1(5) . . ?
O18 Dy8 O46 74.0(6) . . ?
O19 Dy8 Dy7A 45.1(5) . . ?
O19 Dy8 Dy9 110.6(4) . . ?
O19 Dy8 Dy11 96.7(3) . . ?
O19 Dy8 O13 97.8(6) . . ?
O19 Dy8 O14 145.1(6) . . ?
O19 Dy8 O15 82.8(5) . . ?
O19 Dy8 O17 66.6(5) . . ?
O19 Dy8 O46 130.3(7) . . ?
O20 Dy8 Dy7A 31.9(4) . . ?
O20 Dy8 Dy9 105.4(4) . . ?
O20 Dy8 Dy11 126.6(4) . . ?
O20 Dy8 O13 140.9(5) . . ?
O20 Dy8 O14 94.1(5) . . ?
O20 Dy8 O15 68.7(6) . . ?
O20 Dy8 O16 140.2(7) . . ?
O20 Dy8 O17 132.6(4) . . ?
O20 Dy8 O18 87.2(5) . . ?
O20 Dy8 O19 73.9(7) . . ?
O20 Dy8 O46 67.3(7) . . ?
O46 Dy8 Dy7A 87.8(5) . . ?
O46 Dy8 Dy9 108.8(4) . . ?
O46 Dy8 Dy11 83.1(5) . . ?
O46 Dy8 O17 122.4(6) . . ?
Dy8 Dy9 Dy10 61.62(3) . . ?
O1 Dy9 Dy8 124.8(5) . . ?
O1 Dy9 Dy10 170.9(4) . . ?
O1 Dy9 O2 137.3(5) . . ?
O1 Dy9 O13 153.8(5) . . ?
O1 Dy9 O14 110.9(7) . . ?
O1 Dy9 O15 83.8(5) . . ?
O1 Dy9 O47 84.1(8) . . ?
O1 Dy9 O49 89.6(8) . . ?
O1 Dy9 N1 72.6(6) . . ?
O1 Dy9 N19 87.3(9) . . ?
O2 Dy9 Dy8 91.2(4) . . ?
O2 Dy9 Dy10 33.8(3) . . ?
O2 Dy9 O13 68.6(4) . . ?
O2 Dy9 O15 134.4(5) . . ?
O2 Dy9 O47 119.4(8) . . ?
O2 Dy9 O49 79.8(7) . . ?
O2 Dy9 N1 64.7(5) . . ?
O2 Dy9 N19 100.7(9) . . ?
O13 Dy9 Dy8 41.3(4) . . ?
O13 Dy9 Dy10 35.3(3) . . ?
O13 Dy9 O15 74.5(4) . . ?
O13 Dy9 O47 76.2(6) . . ?
O13 Dy9 O49 92.4(7) . . ?
O13 Dy9 N1 132.9(5) . . ?
O13 Dy9 N19 82.2(8) . . ?
O14 Dy9 Dy8 43.3(4) . . ?
O14 Dy9 Dy10 68.8(5) . . ?
O14 Dy9 O2 78.4(7) . . ?
O14 Dy9 O13 73.8(6) . . ?
O14 Dy9 O15 66.1(6) . . ?
O14 Dy9 O47 135.4(7) . . ?
O14 Dy9 O49 157.3(7) . . ?
O14 Dy9 N1 102.5(7) . . ?
O14 Dy9 N19 154.6(8) . . ?
O15 Dy9 Dy8 43.2(3) . . ?
O15 Dy9 Dy10 103.8(3) . . ?
O15 Dy9 O47 74.6(7) . . ?
O15 Dy9 O49 128.4(7) . . ?
O15 Dy9 N1 148.2(7) . . ?
O15 Dy9 N19 99.8(8) . . ?
O47 Dy9 Dy8 93.1(5) . . ?
O47 Dy9 Dy10 102.6(5) . . ?
O47 Dy9 O49 53.7(7) . . ?
O47 Dy9 N1 122.1(8) . . ?
O47 Dy9 N19 25.2(8) . . ?
O49 Dy9 Dy8 131.4(5) . . ?
O49 Dy9 Dy10 89.4(5) . . ?
O49 Dy9 N1 73.5(8) . . ?
O49 Dy9 N19 28.6(8) . . ?
N1 Dy9 Dy8 143.6(5) . . ?
N1 Dy9 Dy10 98.5(4) . . ?
N1 Dy9 N19 99.9(9) . . ?
N19 Dy9 Dy8 111.8(7) . . ?
N19 Dy9 Dy10 96.1(7) . . ?
Dy8 Dy10 Dy11 55.27(2) . . ?
O2 Dy10 Dy8 84.9(3) . . ?
O2 Dy10 Dy11 137.0(4) . . ?
O2 Dy10 O3 170.8(5) . . ?
O2 Dy10 O13 67.8(4) . . ?
O2 Dy10 O16 102.8(6) . . ?
O2 Dy10 O50 118.7(8) . . ?
O2 Dy10 O51 78.2(7) . . ?
O2 Dy10 O53 64.1(6) . . ?
O2 Dy10 O54 109.4(6) . . ?
O2 Dy10 N3 63.2(5) . . ?
O2 Dy10 N4 126.2(5) . . ?
O3 Dy10 Dy8 86.1(3) . . ?
O3 Dy10 Dy11 33.9(4) . . ?
O3 Dy10 O13 105.5(5) . . ?
O3 Dy10 O50 63.3(8) . . ?
O3 Dy10 O51 107.1(8) . . ?
O3 Dy10 O53 114.3(7) . . ?
O3 Dy10 O54 72.2(6) . . ?
O3 Dy10 N3 125.5(5) . . ?
O3 Dy10 N4 63.0(5) . . ?
O13 Dy10 Dy8 36.5(4) . . ?
O13 Dy10 Dy11 84.6(3) . . ?
O13 Dy10 O50 73.8(6) . . ?
O13 Dy10 O51 77.6(6) . . ?
O13 Dy10 O53 109.9(5) . . ?
O13 Dy10 O54 145.9(6) . . ?
O13 Dy10 N3 124.9(5) . . ?
O13 Dy10 N4 144.7(6) . . ?
O16 Dy10 Dy8 35.3(4) . . ?
O16 Dy10 Dy11 35.2(4) . . ?
O16 Dy10 O3 68.5(5) . . ?
O16 Dy10 O13 71.8(5) . . ?
O16 Dy10 O50 108.4(7) . . ?
O16 Dy10 O51 146.1(6) . . ?
O16 Dy10 O53 72.7(6) . . ?
O16 Dy10 O54 76.1(6) . . ?
O16 Dy10 N3 142.0(6) . . ?
O16 Dy10 N4 125.0(5) . . ?
O50 Dy10 Dy8 91.5(5) . . ?
O50 Dy10 Dy11 81.4(6) . . ?
O51 Dy10 Dy8 112.9(5) . . ?
O51 Dy10 Dy11 128.6(5) . . ?
O51 Dy10 O50 47.5(8) . . ?
O51 Dy10 O53 133.2(7) . . ?
O51 Dy10 N3 69.2(7) . . ?
O51 Dy10 N4 75.0(7) . . ?
O53 Dy10 Dy8 91.3(4) . . ?
O53 Dy10 Dy11 98.2(4) . . ?
O53 Dy10 O50 176.2(6) . . ?
O53 Dy10 N4 105.1(5) . . ?
O54 Dy10 Dy8 110.7(4) . . ?
O54 Dy10 Dy11 75.5(4) . . ?
O54 Dy10 O50 128.5(6) . . ?
O54 Dy10 O51 136.3(7) . . ?
O54 Dy10 O53 48.0(3) . . ?
O54 Dy10 N3 76.3(6) . . ?
O54 Dy10 N4 66.0(6) . . ?
N3 Dy10 Dy8 147.4(4) . . ?
N3 Dy10 Dy11 150.2(4) . . ?
N3 Dy10 O50 109.2(7) . . ?
N3 Dy10 O53 69.4(6) . . ?
N3 Dy10 N4 63.9(6) . . ?
N4 Dy10 Dy8 148.7(4) . . ?
N4 Dy10 Dy11 95.4(4) . . ?
N4 Dy10 O50 71.3(7) . . ?
Dy12 Dy11 Dy8 62.86(3) . . ?
O3 Dy11 Dy8 92.5(4) . . ?
O3 Dy11 Dy12 111.9(5) . . ?
O3 Dy11 O16 68.3(5) . . ?
O3 Dy11 O18 130.4(5) . . ?
O3 Dy11 O35 75.3(7) . . ?
O3 Dy11 O65 125.0(6) . . ?
O3 Dy11 O66 148.6(6) . . ?
O3 Dy11 N6 62.5(5) . . ?
O3 Dy11 N25 140.4(6) . . ?
O4 Dy11 Dy8 104.1(3) . . ?
O4 Dy11 Dy12 43.0(3) . . ?
O4 Dy11 O3 123.9(6) . . ?
O4 Dy11 O16 144.5(5) . . ?
O4 Dy11 O18 71.6(4) . . ?
O4 Dy11 O35 123.9(5) . . ?
O4 Dy11 O65 110.5(6) . . ?
O4 Dy11 O66 67.9(6) . . ?
O4 Dy11 N6 71.9(5) . . ?
O4 Dy11 N25 90.3(5) . . ?
O16 Dy11 Dy8 40.4(3) . . ?
O16 Dy11 Dy12 102.1(3) . . ?
O16 Dy11 O35 90.7(5) . . ?
O16 Dy11 O65 72.1(6) . . ?
O16 Dy11 O66 121.1(6) . . ?
O16 Dy11 N6 130.8(5) . . ?
O16 Dy11 N25 96.3(5) . . ?
O17 Dy11 Dy8 49.0(4) . . ?
O17 Dy11 Dy12 41.0(3) . . ?
O17 Dy11 O3 73.9(6) . . ?
O17 Dy11 O4 78.1(5) . . ?
O17 Dy11 O16 74.1(5) . . ?
O17 Dy11 O18 63.5(5) . . ?
O17 Dy11 O35 148.9(6) . . ?
O17 Dy11 O65 128.4(5) . . ?
O17 Dy11 O66 136.3(6) . . ?
O17 Dy11 N6 93.3(6) . . ?
O17 Dy11 N25 138.9(5) . . ?
O18 Dy11 Dy8 40.1(3) . . ?
O18 Dy11 Dy12 43.7(4) . . ?
O18 Dy11 O16 76.3(4) . . ?
O18 Dy11 O35 139.8(6) . . ?
O18 Dy11 O65 71.3(6) . . ?
O18 Dy11 O66 79.9(6) . . ?
O18 Dy11 N6 140.0(5) . . ?
O18 Dy11 N25 75.4(5) . . ?
O35 Dy11 Dy8 129.1(4) . . ?
O35 Dy11 Dy12 166.9(4) . . ?
O35 Dy11 O65 68.5(6) . . ?
O35 Dy11 O66 74.8(6) . . ?
O35 Dy11 N6 76.1(6) . . ?
O35 Dy11 N25 68.4(5) . . ?
O65 Dy11 Dy8 80.5(4) . . ?
O65 Dy11 Dy12 112.5(4) . . ?
O65 Dy11 N25 24.2(2) . . ?
O66 Dy11 Dy8 113.7(4) . . ?
O66 Dy11 Dy12 95.9(4) . . ?
O66 Dy11 O65 49.2(3) . . ?
O66 Dy11 N6 101.0(5) . . ?
O66 Dy11 N25 25.1(2) . . ?
N6 Dy11 Dy8 140.8(4) . . ?
N6 Dy11 Dy12 97.1(4) . . ?
N6 Dy11 O65 138.3(6) . . ?
N6 Dy11 N25 120.6(5) . . ?
N25 Dy11 Dy8 98.1(3) . . ?
N25 Dy11 Dy12 106.9(3) . . ?
Dy11 Dy12 Dy7 121.18(5) . . ?
Dy11 Dy12 Dy13 148.83(5) . . ?
Dy11 Dy12 Dy16 138.28(4) . . ?
Dy13 Dy12 Dy7 59.30(4) . . ?
Dy13 Dy12 Dy16 59.65(3) . . ?
Dy16 Dy12 Dy7 99.55(5) . . ?
O4 Dy12 Dy7 151.1(4) . . ?
O4 Dy12 Dy11 41.5(3) . . ?
O4 Dy12 Dy13 120.9(3) . . ?
O4 Dy12 Dy16 104.2(4) . . ?
O4 Dy12 O18 69.9(5) . . ?
O4 Dy12 O19 138.8(5) . . ?
O4 Dy12 O29 86.2(4) . . ?
O5 Dy12 Dy7 124.0(4) . . ?
O5 Dy12 Dy11 102.9(4) . . ?
O5 Dy12 Dy13 99.4(4) . . ?
O5 Dy12 Dy16 39.8(4) . . ?
O5 Dy12 O4 84.9(6) . . ?
O5 Dy12 O18 145.8(5) . . ?
O5 Dy12 O19 120.9(7) . . ?
O5 Dy12 O29 71.8(4) . . ?
O17 Dy12 Dy7 101.7(3) . . ?
O17 Dy12 Dy11 40.8(4) . . ?
O17 Dy12 Dy13 160.9(3) . . ?
O17 Dy12 Dy16 127.5(4) . . ?
O17 Dy12 O4 76.5(4) . . ?
O17 Dy12 O5 89.5(5) . . ?
O17 Dy12 O18 62.8(5) . . ?
O17 Dy12 O19 72.6(5) . . ?
O17 Dy12 O27 129.6(5) . . ?
O17 Dy12 O28 127.5(5) . . ?
O17 Dy12 O29 155.6(4) . . ?
O18 Dy12 Dy7 83.5(3) . . ?
O18 Dy12 Dy11 43.0(3) . . ?
O18 Dy12 Dy13 113.2(3) . . ?
O18 Dy12 Dy16 167.6(3) . . ?
O18 Dy12 O19 72.0(6) . . ?
O18 Dy12 O29 126.9(5) . . ?
O19 Dy12 Dy7 29.2(4) . . ?
O19 Dy12 Dy11 98.4(4) . . ?
O19 Dy12 Dy13 88.4(4) . . ?
O19 Dy12 Dy16 116.1(4) . . ?
O27 Dy12 Dy7 47.2(5) . . ?
O27 Dy12 Dy11 114.0(4) . . ?
O27 Dy12 Dy13 40.0(3) . . ?
O27 Dy12 Dy16 99.6(3) . . ?
O27 Dy12 O4 111.7(6) . . ?
O27 Dy12 O5 139.4(5) . . ?
O27 Dy12 O18 73.5(5) . . ?
O27 Dy12 O19 70.9(7) . . ?
O27 Dy12 O29 72.8(5) . . ?
O28 Dy12 Dy7 58.8(3) . . ?
O28 Dy12 Dy11 167.8(3) . . ?
O28 Dy12 Dy13 43.1(3) . . ?
O28 Dy12 Dy16 41.0(3) . . ?
O28 Dy12 O4 144.2(4) . . ?
O28 Dy12 O5 70.9(5) . . ?
O28 Dy12 O18 141.6(4) . . ?
O28 Dy12 O19 77.0(5) . . ?
O28 Dy12 O27 75.4(5) . . ?
O28 Dy12 O29 61.7(4) . . ?
O29 Dy12 Dy7 101.7(3) . . ?
O29 Dy12 Dy11 127.2(3) . . ?
O29 Dy12 Dy13 42.6(3) . . ?
O29 Dy12 Dy16 40.8(3) . . ?
O29 Dy12 O19 130.3(5) . . ?
Dy6 Dy13 Dy14 60.81(3) . . ?
Dy6 Dy13 Dy16 145.41(4) . . ?
Dy12 Dy13 Dy6 127.59(3) . . ?
Dy12 Dy13 Dy14 148.52(4) . . ?
Dy12 Dy13 Dy16 61.26(3) . . ?
Dy14 Dy13 Dy16 132.68(3) . . ?
O27 Dy13 Dy6 94.4(3) . . ?
O27 Dy13 Dy12 41.5(4) . . ?
O27 Dy13 Dy14 114.8(5) . . ?
O27 Dy13 Dy16 102.7(4) . . ?
O27 Dy13 O28 75.3(6) . . ?
O27 Dy13 O29 74.5(4) . . ?
O27 Dy13 O31 144.5(5) . . ?
O27 Dy13 O32 113.5(6) . . ?
O27 Dy13 O33 135.2(4) . . ?
O27 Dy13 O34 78.3(5) . . ?
O28 Dy13 Dy6 117.5(3) . . ?
O28 Dy13 Dy12 41.5(4) . . ?
O28 Dy13 Dy14 169.5(3) . . ?
O28 Dy13 Dy16 42.3(3) . . ?
O29 Dy13 Dy6 168.9(3) . . ?
O29 Dy13 Dy12 43.2(3) . . ?
O29 Dy13 Dy14 122.8(3) . . ?
O29 Dy13 Dy16 41.7(3) . . ?
O29 Dy13 O28 61.1(4) . . ?
O29 Dy13 O33 147.9(4) . . ?
O30 Dy13 Dy6 41.3(5) . . ?
O30 Dy13 Dy12 91.7(4) . . ?
O30 Dy13 Dy14 102.0(5) . . ?
O30 Dy13 Dy16 114.9(6) . . ?
O30 Dy13 O27 75.6(6) . . ?
O30 Dy13 O28 77.2(6) . . ?
O30 Dy13 O29 133.3(5) . . ?
O30 Dy13 O31 115.4(6) . . ?
O30 Dy13 O32 144.9(6) . . ?
O30 Dy13 O33 75.2(5) . . ?
O30 Dy13 O34 73.8(7) . . ?
O31 Dy13 Dy6 116.2(3) . . ?
O31 Dy13 Dy12 103.0(3) . . ?
O31 Dy13 Dy14 96.5(3) . . ?
O31 Dy13 Dy16 41.8(3) . . ?
O31 Dy13 O28 74.8(5) . . ?
O31 Dy13 O29 74.5(5) . . ?
O31 Dy13 O32 77.8(6) . . ?
O31 Dy13 O33 79.4(4) . . ?
O31 Dy13 O34 136.5(4) . . ?
O32 Dy13 Dy6 103.7(3) . . ?
O32 Dy13 Dy12 117.9(3) . . ?
O32 Dy13 Dy14 42.9(3) . . ?
O32 Dy13 Dy16 96.7(3) . . ?
O32 Dy13 O28 137.4(4) . . ?
O32 Dy13 O29 80.5(4) . . ?
O32 Dy13 O33 75.9(5) . . ?
O32 Dy13 O34 75.1(5) . . ?
O33 Dy13 Dy6 42.5(3) . . ?
O33 Dy13 Dy12 166.2(3) . . ?
O33 Dy13 Dy14 42.2(3) . . ?
O33 Dy13 Dy16 120.2(3) . . ?
O33 Dy13 O28 128.8(5) . . ?
O34 Dy13 Dy6 42.1(3) . . ?
O34 Dy13 Dy12 119.6(3) . . ?
O34 Dy13 Dy14 41.7(3) . . ?
O34 Dy13 Dy16 171.3(3) . . ?
O34 Dy13 O28 144.7(4) . . ?
O34 Dy13 O29 132.1(5) . . ?
O34 Dy13 O33 61.3(4) . . ?
Dy13 Dy14 Dy6 59.42(2) . . ?
O7 Dy14 Dy6 115.5(4) . . ?
O7 Dy14 Dy13 85.8(4) . . ?
O7 Dy14 O32 66.1(5) . . ?
O7 Dy14 O42 130.0(10) . . ?
O7 Dy14 O77 115.5(6) . . ?
O7 Dy14 O79 71.5(7) . . ?
O7 Dy14 N12 62.7(5) . . ?
O7 Dy14 N28 92.3(7) . . ?
O8 Dy14 Dy6 41.3(4) . . ?
O8 Dy14 Dy13 100.6(3) . . ?
O8 Dy14 O7 125.9(5) . . ?
O8 Dy14 O32 141.6(5) . . ?
O8 Dy14 O33 74.7(5) . . ?
O8 Dy14 O34 71.7(4) . . ?
O8 Dy14 O42 103.4(10) . . ?
O8 Dy14 O77 77.0(6) . . ?
O8 Dy14 O79 131.7(6) . . ?
O8 Dy14 N12 73.3(5) . . ?
O8 Dy14 N28 104.0(6) . . ?
O32 Dy14 Dy6 100.5(3) . . ?
O32 Dy14 Dy13 41.1(3) . . ?
O32 Dy14 O42 81.3(11) . . ?
O32 Dy14 O77 135.1(6) . . ?
O32 Dy14 O79 86.1(6) . . ?
O32 Dy14 N12 128.7(6) . . ?
O32 Dy14 N28 112.3(6) . . ?
O33 Dy14 Dy6 41.6(3) . . ?
O33 Dy14 Dy13 42.3(3) . . ?
O33 Dy14 O7 75.5(5) . . ?
O33 Dy14 O32 74.4(5) . . ?
O33 Dy14 O42 132.0(6) . . ?
O33 Dy14 O77 150.3(6) . . ?
O33 Dy14 O79 146.3(6) . . ?
O33 Dy14 N12 90.0(6) . . ?
O33 Dy14 N28 162.6(7) . . ?
O34 Dy14 Dy6 41.1(3) . . ?
O34 Dy14 Dy13 42.0(3) . . ?
O34 Dy14 O7 127.4(5) . . ?
O34 Dy14 O32 73.8(4) . . ?
O34 Dy14 O33 61.7(4) . . ?
O34 Dy14 O42 72.1(6) . . ?
O34 Dy14 O77 116.8(6) . . ?
O34 Dy14 O79 138.6(7) . . ?
O34 Dy14 N12 139.6(5) . . ?
O34 Dy14 N28 135.0(7) . . ?
O42 Dy14 Dy6 106.6(6) . . ?
O42 Dy14 Dy13 93.8(7) . . ?
O42 Dy14 O77 63.8(10) . . ?
O42 Dy14 N12 136.4(9) . . ?
O42 Dy14 N28 65.4(8) . . ?
O77 Dy14 Dy6 115.5(5) . . ?
O77 Dy14 Dy13 155.7(5) . . ?
O77 Dy14 N28 28.3(3) . . ?
O79 Dy14 Dy6 171.8(5) . . ?
O79 Dy14 Dy13 127.0(5) . . ?
O79 Dy14 O42 69.3(8) . . ?
O79 Dy14 O77 56.4(6) . . ?
O79 Dy14 N12 80.9(7) . . ?
O79 Dy14 N28 28.3(4) . . ?
N12 Dy14 Dy6 98.5(4) . . ?
N12 Dy14 Dy13 129.8(5) . . ?
N12 Dy14 O77 73.3(7) . . ?
N12 Dy14 N28 73.2(8) . . ?
N28 Dy14 Dy6 143.8(4) . . ?
N28 Dy14 Dy13 150.8(5) . . ?
Dy13 Dy15 Dy14 55.46(2) . . ?
Dy13 Dy15 Dy16 55.54(2) . . ?
Dy16 Dy15 Dy14 110.98(3) . . ?
O6 Dy15 Dy13 84.2(3) . . ?
O6 Dy15 Dy14 136.3(3) . . ?
O6 Dy15 Dy16 33.6(3) . . ?
O6 Dy15 O7 168.3(4) . . ?
O6 Dy15 O31 67.4(5) . . ?
O6 Dy15 O32 103.1(5) . . ?
O6 Dy15 O71 89.1(7) . . ?
O6 Dy15 O75 61.7(6) . . ?
O6 Dy15 O76 105.3(7) . . ?
O6 Dy15 N9 63.6(5) . . ?
O6 Dy15 N10 127.9(5) . . ?
O7 Dy15 Dy13 84.2(3) . . ?
O7 Dy15 Dy14 33.8(3) . . ?
O7 Dy15 Dy16 135.3(3) . . ?
O7 Dy15 O31 102.1(5) . . ?
O7 Dy15 O32 68.4(5) . . ?
O7 Dy15 O71 93.1(7) . . ?
O7 Dy15 O75 119.2(7) . . ?
O7 Dy15 O76 80.6(7) . . ?
O7 Dy15 N9 128.1(5) . . ?
O7 Dy15 N10 63.5(5) . . ?
O31 Dy15 Dy13 37.8(4) . . ?
O31 Dy15 Dy14 85.7(3) . . ?
O31 Dy15 Dy16 34.2(3) . . ?
O31 Dy15 O71 74.4(6) . . ?
O31 Dy15 O75 106.6(6) . . ?
O31 Dy15 O76 147.0(6) . . ?
O31 Dy15 N9 122.8(5) . . ?
O31 Dy15 N10 141.6(6) . . ?
O32 Dy15 Dy13 38.8(3) . . ?
O32 Dy15 Dy14 35.0(3) . . ?
O32 Dy15 Dy16 86.8(3) . . ?
O32 Dy15 O31 76.5(5) . . ?
O32 Dy15 O71 141.1(6) . . ?
O32 Dy15 O75 68.1(6) . . ?
O32 Dy15 O76 74.0(6) . . ?
O32 Dy15 N9 141.3(5) . . ?
O32 Dy15 N10 122.7(6) . . ?
O71 Dy15 Dy13 108.4(5) . . ?
O71 Dy15 Dy14 116.9(5) . . ?
O71 Dy15 Dy16 83.6(6) . . ?
O71 Dy15 O75 145.8(7) . . ?
O71 Dy15 O76 138.6(8) . . ?
O71 Dy15 N9 77.2(6) . . ?
O71 Dy15 N10 71.3(7) . . ?
O75 Dy15 Dy13 87.3(5) . . ?
O75 Dy15 Dy14 97.1(5) . . ?
O75 Dy15 Dy16 80.8(5) . . ?
O76 Dy15 Dy13 111.6(5) . . ?
O76 Dy15 Dy14 78.8(5) . . ?
O76 Dy15 Dy16 128.8(5) . . ?
O76 Dy15 O75 48.0(6) . . ?
O76 Dy15 N9 75.2(7) . . ?
O76 Dy15 N10 69.2(7) . . ?
N9 Dy15 Dy13 147.5(4) . . ?
N9 Dy15 Dy14 151.4(4) . . ?
N9 Dy15 Dy16 94.7(4) . . ?
N9 Dy15 O75 74.0(6) . . ?
N10 Dy15 Dy13 147.4(4) . . ?
N10 Dy15 Dy14 94.6(4) . . ?
N10 Dy15 Dy16 150.4(5) . . ?
N10 Dy15 O75 111.4(7) . . ?
N10 Dy15 N9 65.1(5) . . ?
Dy13 Dy16 Dy12 59.10(3) . . ?
O5 Dy16 Dy12 40.3(3) . . ?
O5 Dy16 Dy13 99.4(3) . . ?
O5 Dy16 O6 126.0(6) . . ?
O5 Dy16 O28 70.5(4) . . ?
O5 Dy16 O29 73.1(5) . . ?
O5 Dy16 O31 139.3(5) . . ?
O5 Dy16 O41 107.5(10) . . ?
O5 Dy16 O68 76.5(6) . . ?
O5 Dy16 O70 132.8(6) . . ?
O5 Dy16 N7 73.4(5) . . ?
O5 Dy16 N21 103.0(6) . . ?
O6 Dy16 Dy12 116.9(4) . . ?
O6 Dy16 Dy13 85.8(4) . . ?
O6 Dy16 O28 128.3(5) . . ?
O6 Dy16 O31 65.8(5) . . ?
O6 Dy16 O41 126.1(10) . . ?
O6 Dy16 O68 114.4(6) . . ?
O6 Dy16 O70 70.3(7) . . ?
O6 Dy16 N7 62.2(5) . . ?
O6 Dy16 N21 89.2(7) . . ?
O28 Dy16 Dy12 40.1(3) . . ?
O28 Dy16 Dy13 42.8(3) . . ?
O28 Dy16 O41 72.0(7) . . ?
O28 Dy16 O68 117.3(6) . . ?
O28 Dy16 O70 139.4(6) . . ?
O28 Dy16 N7 138.3(6) . . ?
O28 Dy16 N21 138.9(7) . . ?
O29 Dy16 Dy12 41.8(3) . . ?
O29 Dy16 Dy13 42.1(3) . . ?
O29 Dy16 O6 76.4(5) . . ?
O29 Dy16 O28 61.8(5) . . ?
O29 Dy16 O31 73.4(5) . . ?
O29 Dy16 O41 130.8(7) . . ?
O29 Dy16 O68 147.6(5) . . ?
O29 Dy16 O70 146.2(6) . . ?
O29 Dy16 N7 88.4(6) . . ?
O29 Dy16 N21 157.4(6) . . ?
O31 Dy16 Dy12 99.1(3) . . ?
O31 Dy16 Dy13 40.0(3) . . ?
O31 Dy16 O28 73.8(4) . . ?
O31 Dy16 O41 78.5(9) . . ?
O31 Dy16 O68 139.0(6) . . ?
O31 Dy16 O70 87.4(6) . . ?
O31 Dy16 N7 127.5(5) . . ?
O31 Dy16 N21 116.7(6) . . ?
O41 Dy16 Dy12 107.2(7) . . ?
O41 Dy16 Dy13 91.9(7) . . ?
O41 Dy16 O68 69.4(8) . . ?
O41 Dy16 O70 69.0(8) . . ?
O41 Dy16 N7 140.2(8) . . ?
O41 Dy16 N21 71.8(8) . . ?
O68 Dy16 Dy12 114.1(5) . . ?
O68 Dy16 Dy13 158.0(5) . . ?
O68 Dy16 N7 72.4(7) . . ?
O68 Dy16 N21 29.0(7) . . ?
O70 Dy16 Dy12 171.8(5) . . ?
O70 Dy16 Dy13 127.3(5) . . ?
O70 Dy16 O68 57.9(7) . . ?
O70 Dy16 N7 81.5(7) . . ?
O70 Dy16 N21 29.9(7) . . ?
N7 Dy16 Dy12 98.3(4) . . ?
N7 Dy16 Dy13 127.7(5) . . ?
N7 Dy16 N21 69.4(7) . . ?
N21 Dy16 Dy12 142.5(5) . . ?
N21 Dy16 Dy13 155.4(5) . . ?
C1 O1 Dy9 139.8(13) . . ?
Dy9 O2 Dy10 112.6(5) . . ?
C8 O2 Dy9 119.0(13) . . ?
C8 O2 Dy10 127.7(13) . . ?
Dy11 O3 Dy10 111.8(6) . . ?
C21 O3 Dy10 126.4(11) . . ?
C21 O3 Dy11 119.8(12) . . ?
Dy11 O4 Dy12 95.5(4) . . ?
C28 O4 Dy11 132.8(11) . . ?
C28 O4 Dy12 129.1(13) . . ?
Dy16 O5 Dy12 99.9(5) . . ?
C29 O5 Dy12 132.7(13) . . ?
C29 O5 Dy16 126.1(12) . . ?
Dy15 O6 Dy16 114.0(5) . . ?
C36 O6 Dy15 126.4(12) . . ?
C36 O6 Dy16 119.1(13) . . ?
Dy15 O7 Dy14 113.5(5) . . ?
C49 O7 Dy14 118.5(14) . . ?
C49 O7 Dy15 127.1(13) . . ?
Dy14 O8 Dy6 98.7(5) . . ?
C56 O8 Dy6 127.9(12) . . ?
C56 O8 Dy14 131.9(12) . . ?
Dy1 O9 Dy5 113.2(6) . . ?
C64 O9 Dy1 125.9(14) . . ?
C64 O9 Dy5 120.9(14) . . ?
Dy1 O10 Dy2 114.1(5) . . ?
C77 O10 Dy1 124.0(16) . . ?
C77 O10 Dy2 118.4(16) . . ?
Dy2 O11 Dy3 93.2(6) . . ?
C84 O11 Dy2 136.2(16) . . ?
C84 O11 Dy3 130.2(16) . . ?
Dy5 O12 Dy6 97.1(4) . . ?
C57 O12 Dy5 128.9(10) . . ?
C57 O12 Dy6 133.5(10) . . ?
Dy8 O13 Dy10 106.8(6) . . ?
Dy9 O13 Dy8 98.0(5) . . ?
Dy9 O13 Dy10 110.0(5) . . ?
Dy9 O14 Dy8 96.5(7) . . ?
Dy3 O15 Dy8 108.4(6) . . ?
Dy9 O15 Dy3 133.7(7) . . ?
Dy9 O15 Dy8 95.6(5) . . ?
Dy8 O16 Dy10 109.3(7) . . ?
Dy8 O16 Dy11 98.3(5) . . ?
Dy10 O16 Dy11 110.1(7) . . ?
Dy11 O17 Dy8 91.2(6) . . ?
Dy11 O17 Dy12 98.2(6) . . ?
Dy12 O17 Dy8 94.3(5) . . ?
Dy8 O18 Dy11 98.9(4) . . ?
Dy8 O18 Dy12 101.8(6) . . ?
Dy11 O18 Dy12 93.3(5) . . ?
Dy7 O19 Dy7A 38.2(4) . . ?
Dy7 O19 Dy8 123.9(10) . . ?
Dy7 O19 Dy12 113.3(7) . . ?
Dy8 O19 Dy7A 95.2(8) . . ?
Dy8 O19 Dy12 101.0(6) . . ?
Dy12 O19 Dy7A 99.5(6) . . ?
Dy3 O20 Dy7 92.7(6) . . ?
Dy7A O20 Dy3 108.1(6) . . ?
Dy7A O20 Dy7 33.5(3) . . ?
Dy7A O20 Dy8 112.3(8) . . ?
Dy8 O20 Dy3 112.3(8) . . ?
Dy8 O20 Dy7 92.8(7) . . ?
Dy3 O21 Dy2 104.7(8) . . ?
Dy2 O22 Dy3 93.2(6) . . ?
Dy2 O22 Dy4 103.8(7) . . ?
Dy4 O22 Dy3 97.0(5) . . ?
Dy1 O23 Dy2 111.5(5) . . ?
Dy4 O23 Dy1 107.6(6) . . ?
Dy4 O23 Dy2 100.6(6) . . ?
Dy1 O24 Dy5 111.2(6) . . ?
Dy4 O24 Dy1 105.8(7) . . ?
Dy4 O24 Dy5 95.8(4) . . ?
Dy4 O25 Dy6 98.1(6) . . ?
Dy4 O25 Dy7 91.7(7) . . ?
Dy6 O25 Dy7 96.3(7) . . ?
Dy7A O25 Dy4 114.2(9) . . ?
Dy7A O25 Dy6 116.6(8) . . ?
Dy7A O25 Dy7 34.8(4) . . ?
Dy3 O26 Dy7A 98.0(7) . . ?
Dy4 O26 Dy3 103.2(6) . . ?
Dy4 O26 Dy7A 97.1(6) . . ?
Dy7 O26 Dy3 123.9(8) . . ?
Dy7 O26 Dy4 114.6(6) . . ?
Dy7 O26 Dy7A 40.0(3) . . ?
Dy7A O27 Dy7 37.4(3) . . ?
Dy7A O27 Dy12 118.4(8) . . ?
Dy7A O27 Dy13 111.0(6) . . ?
Dy12 O27 Dy7 92.6(7) . . ?
Dy13 O27 Dy7 90.7(6) . . ?
Dy13 O27 Dy12 98.5(6) . . ?
Dy12 O28 Dy13 95.4(5) . . ?
Dy12 O28 Dy16 98.9(5) . . ?
Dy16 O28 Dy13 94.9(4) . . ?
Dy13 O29 Dy12 94.2(4) . . ?
Dy16 O29 Dy12 97.5(5) . . ?
Dy16 O29 Dy13 96.1(4) . . ?
Dy6 O30 Dy7A 101.1(8) . . ?
Dy7 O30 Dy6 129.0(9) . . ?
Dy7 O30 Dy7A 39.6(3) . . ?
Dy7 O30 Dy13 113.9(7) . . ?
Dy13 O30 Dy6 99.3(7) . . ?
Dy13 O30 Dy7A 97.7(6) . . ?
Dy13 O31 Dy15 103.4(6) . . ?
Dy13 O31 Dy16 98.2(5) . . ?
Dy15 O31 Dy16 112.2(5) . . ?
Dy13 O32 Dy14 96.0(4) . . ?
Dy13 O32 Dy15 102.3(6) . . ?
Dy15 O32 Dy14 111.2(6) . . ?
Dy6 O33 Dy13 95.0(4) . . ?
Dy14 O33 Dy6 96.9(5) . . ?
Dy14 O33 Dy13 95.5(5) . . ?
Dy6 O34 Dy13 95.6(5) . . ?
Dy14 O34 Dy6 97.8(4) . . ?
Dy14 O34 Dy13 96.2(4) . . ?
N19 O47 Dy9 100(2) . . ?
N19 O49 Dy9 94.0(19) . . ?
N20 O50 Dy10 99(2) . . ?
N20 O51 Dy10 109(2) . . ?
N26 O53 Dy10 101.9(9) . . ?
N26 O54 Dy10 108.3(9) . . ?
N24 O57 Dy2 93.9(11) . . ?
N24 O58 Dy2 77.4(10) . . ?
N27 O60 Dy1 95.3(13) . . ?
N27 O61 Dy1 96.2(13) . . ?
N22 O62 Dy5 94.0(19) . . ?
N22 O63 Dy5 105(2) . . ?
N25 O65 Dy11 87.6(8) . . ?
N25 O66 Dy11 96.5(9) . . ?
N21 O68 Dy16 90.7(16) . . ?
N21 O70 Dy16 90.6(15) . . ?
N23 O71 Dy15 123(2) . . ?
N29 O75 Dy15 100.8(15) . . ?
N29 O76 Dy15 107.5(17) . . ?
N28 O77 Dy14 86.1(17) . . ?
N28 O79 Dy14 90.4(16) . . ?
Dy5 O80 Dy4 91.9(5) . . ?
Dy5 O80 Dy6 97.9(5) . . ?
Dy6 O80 Dy4 92.5(4) . . ?
Dy4 O81 Dy5 97.4(4) . . ?
Dy4 O81 Dy6 98.1(5) . . ?
Dy5 O81 Dy6 95.3(4) . . ?
N2 N1 Dy9 116.1(12) . . ?
C7 N1 Dy9 132.2(18) . . ?
C7 N1 N2 111.2(19) . . ?
C8 N2 N1 110.1(16) . . ?
C9 N3 Dy10 120.9(14) . . ?
C9 N3 C17 118(2) . . ?
C17 N3 Dy10 121.3(16) . . ?
C16 N4 Dy10 119.8(14) . . ?
C20 N4 Dy10 119.5(14) . . ?
C20 N4 C16 120.7(19) . . ?
C21 N5 N6 109.2(17) . . ?
N5 N6 Dy11 117.8(12) . . ?
C22 N6 Dy11 132.5(15) . . ?
C22 N6 N5 109.2(17) . . ?
N8 N7 Dy16 119.8(10) . . ?
C35 N7 Dy16 130.6(14) . . ?
C35 N7 N8 109.4(16) . . ?
C36 N8 N7 105.2(14) . . ?
C37 N9 Dy15 121.9(12) . . ?
C37 N9 C45 117.0(16) . . ?
C45 N9 Dy15 121.0(12) . . ?
C44 N10 Dy15 121.0(14) . . ?
C48 N10 Dy15 121.4(12) . . ?
C48 N10 C44 116.9(17) . . ?
C49 N11 N12 107.3(15) . . ?
N11 N12 Dy14 118.5(12) . . ?
C50 N12 Dy14 129.0(15) . . ?
C50 N12 N11 112.3(16) . . ?
N14 N13 Dy5 116.7(11) . . ?
C63 N13 Dy5 130.9(14) . . ?
C63 N13 N14 112.4(18) . . ?
C64 N14 N13 110.8(16) . . ?
C65 N15 Dy1 121.1(14) . . ?
C65 N15 C69 117(2) . . ?
C69 N15 Dy1 122.1(16) . . ?
C73 N16 Dy1 121.7(15) . . ?
C73 N16 C76 117.3(18) . . ?
C76 N16 Dy1 120.9(15) . . ?
C77 N17 N18 110(2) . . ?
N17 N18 Dy2 118.2(14) . . ?
C78 N18 Dy2 129(2) . . ?
C78 N18 N17 111(2) . . ?
O47 N19 Dy9 54.4(18) . . ?
O47 N19 O48 137(4) . . ?
O47 N19 O49 112(3) . . ?
O48 N19 Dy9 168(3) . . ?
O48 N19 O49 111(3) . . ?
O49 N19 Dy9 57.4(16) . . ?
O51 N20 O50 103(3) . . ?
O51 N20 O52 127(3) . . ?
O52 N20 O50 127(3) . . ?
O68 N21 Dy16 60.3(14) . . ?
O68 N21 O70 117(2) . . ?
O69 N21 Dy16 174(2) . . ?
O69 N21 O68 118(3) . . ?
O69 N21 O70 120(3) . . ?
O70 N21 Dy16 59.5(13) . . ?
O62 N22 O64 112(3) . . ?
O63 N22 O62 113(3) . . ?
O63 N22 O64 135(3) . . ?
O71 N23 O72 120(3) . . ?
O71 N23 O73 129(3) . . ?
O72 N23 O73 111(3) . . ?
O56 N24 Dy2 162.2(14) . . ?
O57 N24 Dy2 57.5(10) . . ?
O57 N24 O56 128.6(10) . . ?
O57 N24 O58 129.6(10) . . ?
O58 N24 Dy2 74.5(10) . . ?
O58 N24 O56 101.8(10) . . ?
O65 N25 Dy11 68.2(8) . . ?
O65 N25 O66 126.3(7) . . ?
O65 N25 O67 119.9(7) . . ?
O66 N25 Dy11 58.4(8) . . ?
O66 N25 O67 113.8(7) . . ?
O67 N25 Dy11 170.2(11) . . ?
O53 N26 O55 124(2) . . ?
O54 N26 O53 101.7(10) . . ?
O54 N26 O55 134(2) . . ?
O59 N27 Dy1 171.8(18) . . ?
O60 N27 Dy1 58.8(11) . . ?
O60 N27 O59 116(2) . . ?
O60 N27 O61 116.6(19) . . ?
O61 N27 Dy1 57.8(11) . . ?
O61 N27 O59 127(2) . . ?
O77 N28 Dy14 65.6(15) . . ?
O78 N28 Dy14 176(3) . . ?
O78 N28 O77 115(3) . . ?
O78 N28 O79 118(3) . . ?
O79 N28 Dy14 61.3(14) . . ?
O79 N28 O77 126(3) . . ?
O75 N29 O74 125(2) . . ?
O76 N29 O74 129(2) . . ?
O76 N29 O75 104(2) . . ?
C6 C1 O1 123.0(16) . . ?
C6 C1 C2 120.0 . . ?
C2 C1 O1 116.2(16) . . ?
C1 C6 C7 120.3(18) . . ?
C4 C6 C1 120.0 . . ?
C4 C6 C7 118.1(17) . . ?
C6 C4 C5 120.0 . . ?
C3 C5 C4 120.0 . . ?
C2 C3 C5 120.0 . . ?
C3 C2 C1 120.0 . . ?
N1 C7 C6 128(2) . . ?
O2 C8 N2 129(2) . . ?
O2 C8 C9 114.2(18) . . ?
N2 C8 C9 117.1(18) . . ?
N3 C9 C8 112.9(18) . . ?
N3 C9 C10 121(2) . . ?
C10 C9 C8 126(2) . . ?
C11 C10 C9 122(2) . . ?
C10 C11 C12 118(2) . . ?
C11 C12 C13 125(2) . . ?
C11 C12 C17 120(3) . . ?
C17 C12 C13 115(2) . . ?
C14 C13 C12 126(2) . . ?
C13 C14 C15 116(3) . . ?
C14 C15 C18 122(2) . . ?
C16 C15 C14 120(2) . . ?
C16 C15 C18 118(2) . . ?
C15 C16 N4 121(2) . . ?
C17 C16 N4 115(2) . . ?
C17 C16 C15 124(2) . . ?
N3 C17 C12 121(3) . . ?
N3 C17 C16 120(2) . . ?
C16 C17 C12 119(3) . . ?
C19 C18 C15 119(2) . . ?
C18 C19 C20 123(2) . . ?
N4 C20 C19 118(2) . . ?
N4 C20 C21 115(2) . . ?
C21 C20 C19 126(2) . . ?
O3 C21 C20 114.8(18) . . ?
N5 C21 O3 124.1(17) . . ?
N5 C21 C20 119(2) . . ?
N6 C22 C23 123(2) . . ?
C24 C23 C22 117.2(18) . . ?
C24 C23 C28 120.8(17) . . ?
C28 C23 C22 122.0(19) . . ?
C25 C24 C23 121.6(19) . . ?
C24 C25 C26 120(2) . . ?
C25 C26 C27 120(2) . . ?
C26 C27 C28 120(2) . . ?
O4 C28 C23 124.8(17) . . ?
O4 C28 C27 119.3(18) . . ?
C27 C28 C23 115.8(17) . . ?
O5 C29 C30 118.5(18) . . ?
O5 C29 C34 123.6(18) . . ?
C34 C29 C30 117.8(19) . . ?
C31 C30 C29 120(3) . . ?
C32 C31 C30 120(3) . . ?
C31 C32 C33 121(3) . . ?
C34 C33 C32 123(2) . . ?
C29 C34 C35 125.2(19) . . ?
C33 C34 C29 118(2) . . ?
C33 C34 C35 116(2) . . ?
N7 C35 C34 124(2) . . ?
O6 C36 N8 127.7(17) . . ?
O6 C36 C37 114.4(17) . . ?
N8 C36 C37 117.8(17) . . ?
N9 C37 C36 111.0(17) . . ?
N9 C37 C38 122.8(18) . . ?
C38 C37 C36 126(2) . . ?
C39 C38 C37 119(2) . . ?
C38 C39 C40 119.6(19) . . ?
C41 C40 C39 123(2) . . ?
C45 C40 C39 116.4(19) . . ?
C45 C40 C41 121(2) . . ?
C42 C41 C40 122(2) . . ?
C41 C42 C43 120.4(19) . . ?
C44 C43 C42 117(2) . . ?
C46 C43 C42 125.2(18) . . ?
C46 C43 C44 118.2(19) . . ?
N10 C44 C43 122(2) . . ?
N10 C44 C45 116.3(16) . . ?
C43 C44 C45 120.7(18) . . ?
N9 C45 C40 124.3(19) . . ?
N9 C45 C44 116.1(15) . . ?
C40 C45 C44 119.6(17) . . ?
C43 C46 C47 122.5(19) . . ?
C46 C47 C48 115(2) . . ?
N10 C48 C47 124.1(19) . . ?
N10 C48 C49 109.7(15) . . ?
C47 C48 C49 125.9(19) . . ?
O7 C49 N11 127.2(18) . . ?
O7 C49 C48 116.2(18) . . ?
N11 C49 C48 116.6(17) . . ?
N12 C50 C51 125.1(19) . . ?
C52 C51 C50 114(2) . . ?
C52 C51 C56 119.5(19) . . ?
C56 C51 C50 125.7(17) . . ?
C53 C52 C51 120(2) . . ?
C54 C53 C52 122(2) . . ?
C55 C54 C53 116(2) . . ?
C54 C55 C56 126(2) . . ?
O8 C56 C51 120.8(18) . . ?
O8 C56 C55 123.5(18) . . ?
C55 C56 C51 115.6(17) . . ?
C57 C58 C59 120.0 . . ?
O12 C57 C58 117.4(9) . . ?
O12 C57 C61 122.2(9) . . ?
C58 C57 C61 120.0 . . ?
C57 C61 C62 120.0 . . ?
C57 C61 C63 125.1(10) . . ?
C62 C61 C63 114.9(10) . . ?
C60 C62 C61 120.0 . . ?
C62 C60 C59 120.0 . . ?
C60 C59 C58 120.0 . . ?
N13 C63 C61 124.1(18) . . ?
O9 C64 C65 115.8(18) . . ?
N14 C64 O9 125.5(19) . . ?
N14 C64 C65 118.7(18) . . ?
N15 C65 C64 111.2(19) . . ?
N15 C65 C66 121(2) . . ?
C66 C65 C64 127(2) . . ?
C65 C66 C67 121(3) . . ?
C68 C67 C66 120(2) . . ?
C67 C68 C69 118(2) . . ?
C67 C68 C70 126(3) . . ?
C69 C68 C70 117(3) . . ?
N15 C69 C68 122(3) . . ?
N15 C69 C73 113(2) . . ?
C68 C69 C73 124(2) . . ?
C71 C70 C68 119(3) . . ?
C70 C71 C72 124(2) . . ?
C71 C72 C73 118(3) . . ?
C74 C72 C71 125(2) . . ?
C74 C72 C73 117(3) . . ?
N16 C73 C69 118.2(18) . . ?
N16 C73 C72 123(2) . . ?
C72 C73 C69 118(3) . . ?
C72 C74 C75 123(2) . . ?
C74 C75 C76 116(2) . . ?
N16 C76 C75 123(2) . . ?
N16 C76 C77 109.3(19) . . ?
C75 C76 C77 128(2) . . ?
O10 C77 N17 123(3) . . ?
O10 C77 C76 120(2) . . ?
N17 C77 C76 116(2) . . ?
N18 C78 C79 124(3) . . ?
C84 C79 C78 130(2) . . ?
C84 C79 C81 120.0 . . ?
C81 C79 C78 109(2) . . ?
O11 C84 C79 118(2) . . ?
O11 C84 C83 122(2) . . ?
C83 C84 C79 120.0 . . ?
C84 C83 C82 120.0 . . ?
C83 C82 C80 120.0 . . ?
C81 C80 C82 120.0 . . ?
C80 C81 C79 120.0 . . ?

_olex2_submission_special_instructions 'No special instructions were received'
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_l-lj-331-100k
_database_code_depnum_ccdc_archive 'CCDC 2058346'
loop_
_audit_author_name
_audit_author_address
'Hai-Ling Wang'
;Guangxi Normal University
China
;
_audit_update_record             
;
2021-01-24 deposited with the CCDC.	2021-02-19 downloaded from the CCDC.
;
_audit_creation_date             2020-02-05
_audit_creation_method           
;
Olex2 1.2
(compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C126 H112 Dy10 N30 O44, C H4 O, 8(H2 O)'
_chemical_formula_sum            'C127 H132 Dy10 N30 O53'
_chemical_formula_weight         4551.63
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0030 0.0020 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1890 4.4100 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0060 0.0030 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0110 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   14.9384(7)
_cell_length_b                   16.6305(6)
_cell_length_c                   17.5360(7)
_cell_angle_alpha                79.223(3)
_cell_angle_beta                 88.320(4)
_cell_angle_gamma                73.352(4)
_cell_volume                     4098.9(3)
_cell_formula_units_Z            1
_cell_measurement_reflns_used    11526
_cell_measurement_temperature    100.00(10)
_cell_measurement_theta_max      31.0900
_cell_measurement_theta_min      1.7270
_shelx_estimated_absorpt_T_max   ?
_shelx_estimated_absorpt_T_min   ?
_exptl_absorpt_coefficient_mu    4.583
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.34686
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
CrysAlisPro 1.171.40.14a (Rigaku Oxford Diffraction, 2018)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.844
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             2188
_exptl_crystal_size_max          0.05
_exptl_crystal_size_mid          0.04
_exptl_crystal_size_min          0.03
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0561
_diffrn_reflns_av_unetI/netI     0.0553
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.999
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -19
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            44675
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.999
_diffrn_reflns_theta_full        24.999
_diffrn_reflns_theta_max         24.999
_diffrn_reflns_theta_min         1.874
_diffrn_ambient_environment      N~2~
_diffrn_ambient_temperature      100.00(10)
_diffrn_detector                 'CCD plate'
_diffrn_detector_area_resol_mean ?
_diffrn_detector_type            HyPix
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_details      
;
List of Runs (angles in degrees, time in seconds):

  # Type    Start    End  Width  tₑₓₚ   ω     θ     κ     φ   Frames
#--------------------------------------------------------------------------
  1  ω     -6.00  37.00   0.50    2.99    --    6.28  37.00 -30.00   86
  2  ω      0.00  80.00   0.50    2.99    --    6.28  37.00  90.00  160
  3  ω     38.00  70.00   0.50    2.99    --    6.28  57.00 120.00   64
  4  ω    -41.00  -6.00   0.50    2.99    --   -3.78 -57.00 -90.00   70
  5  ω     -9.00  78.00   0.50    2.99    --    6.28  57.00-180.00  174
  6  ω    -10.00  32.00   0.50    2.99    --    6.28 -99.00  30.00   84
  7  ω    -50.00  19.00   0.50    2.99    --    6.28 -57.00 -30.00  138
;
_diffrn_measurement_device       'four-circle diffractometer'
_diffrn_measurement_device_type  'ROD, Synergy Custom DW system, HyPix'
_diffrn_measurement_method       'ω scans'
_diffrn_orient_matrix_type       
'CrysAlisPro convention (1999,Acta A55,543-557)'
_diffrn_orient_matrix_UB_11      0.0363628000
_diffrn_orient_matrix_UB_12      0.0106767000
_diffrn_orient_matrix_UB_13      0.0172516000
_diffrn_orient_matrix_UB_21      0.0093304000
_diffrn_orient_matrix_UB_22      0.0219573000
_diffrn_orient_matrix_UB_23      -0.0367070000
_diffrn_orient_matrix_UB_31      -0.0323792000
_diffrn_orient_matrix_UB_32      0.0381707000
_diffrn_orient_matrix_UB_33      0.0071724000
_diffrn_radiation_monochromator  mirror
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   'Rotating-anode X-ray tube'
_diffrn_source_type              'Rigaku (Mo) X-ray Source'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                9831
_reflns_number_total             14423
_reflns_odcompleteness_completeness 99.83
_reflns_odcompleteness_iscentric 1
_reflns_odcompleteness_theta     26.32
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'CrysAlisPro 1.171.40.14a (Rigaku OD, 2018)'
_computing_data_collection       'CrysAlisPro 1.171.40.14a (Rigaku OD, 2018)'
_computing_data_reduction        'CrysAlisPro 1.171.40.14a (Rigaku OD, 2018)'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    'ShelXS-1997 (Sheldrick, 2008)'
_refine_diff_density_max         3.482
_refine_diff_density_min         -1.106
_refine_diff_density_rms         0.245
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.040
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1051
_refine_ls_number_reflns         14423
_refine_ls_number_restraints     99
_refine_ls_R_factor_all          0.1039
_refine_ls_R_factor_gt           0.0678
_refine_ls_restrained_S_all      1.040
_refine_ls_shift/su_max          0.003
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.1051P)²+64.6133P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1775
_refine_ls_wR_factor_ref         0.2110
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups
 At 1.5 times of:
  All C(H,H,H) groups, All O(H) groups, All O(H,H) groups, All O(H,H,H) groups
2. Restrained distances
 O23-C64
 1.48 with sigma of 0.02
 C58-C57
 1.48 with sigma of 0.01
 N15-C57
 1.2 with sigma of 0.01
3. Uiso/Uaniso restraints and constraints
C64 \\sim O23: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(O23) \\sim Ueq, Uanis(C64) \\sim Ueq: with sigma of 0.01 and sigma for
terminal atoms of 0.02
Uanis(O28) \\sim Ueq, Uanis(O30) \\sim Ueq, Uanis(O23) \\sim Ueq, Uanis(O31)
\\sim Ueq, Uanis(O24) \\sim Ueq, Uanis(O25) \\sim Ueq, Uanis(O26) \\sim Ueq,
Uanis(O32) \\sim Ueq, Uanis(O29) \\sim Ueq: with sigma of 0.01 and sigma for
terminal atoms of 0.02
Uanis(C57) \\sim Ueq, Uanis(N15) \\sim Ueq, Uanis(C58) \\sim Ueq: with sigma of
0.01 and sigma for terminal atoms of 0.02
4. Rigid body (RIGU) restrains
 O23, C64
 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01
 N15, C57, C58
 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01
5. Others
 Fixed Sof: O23(0.5) H23(0.5) C64(0.5) H64a(0.5) H64b(0.5) H64c(0.5) O25(0.5)
 H25a(0.5) H25b(0.5) O26(0.25) H26a(0.25) H26b(0.25) O27(0.5) H27a(0.5)
 H27b(0.5) O28(0.5) H28a(0.5) H28b(0.5) O29(0.25) H29a(0.25) H29b(0.25)
 O30(0.25) H30a(0.25) H30b(0.25) O31(0.25) H31a(0.25) H31b(0.25) O32(0.5)
 H32a(0.5) H32b(0.5)
6.a Riding coordinates:
 O14(H14), O19(H19a,H19b), O20(H20a,H20b), O5(H5a,H5b,H5c), C58(H58a,H58b,
 H58c), O23(H23), C64(H64a,H64b,H64c), O24(H24a,H24b), O25(H25a,H25b), O26(H26a,
 H26b), O27(H27a,H27b), O28(H28a,H28b), O29(H29a,H29b), O30(H30a,H30b),
 O31(H31a,H31b), O32(H32a,H32b)
6.b Rotating group:
 O18(H18a,H18b)
6.c Aromatic/amide H refined with riding coordinates:
 C3(H3), C52(H52), C4(H4), C24(H24), C49(H49), C41(H41), C16(H16), C50(H50),
 C25(H25), C28(H28), C61(H61), C53(H53), C40(H40), C9(H9), C39(H39), C27(H27),
 C20(H20), C59(H59), C56(H56), C60(H60), C30(H30), C55(H55), C31(H31), C22(H22),
  C21(H21), C32(H32), C34(H34), C33(H33)
6.d Idealised Me refined as rotating group:
 C42(H42a,H42b,H42c), C63(H63a,H63b,H63c), C23(H23a,H23b,H23c), C36(H36a,H36b,
 H36c), C37(H37a,H37b,H37c)
;
_atom_sites_solution_hydrogens   mixed
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Dy1 Dy 0.27459(4) 0.65291(4) 0.70616(3) 0.03863(18) Uani 1 1 d . . . . .
Dy4 Dy 0.89195(5) 0.23331(4) 0.15088(4) 0.0465(2) Uani 1 1 d . . . . .
Dy5 Dy 0.74204(5) 0.11829(4) 0.29660(4) 0.0480(2) Uani 1 1 d . . . . .
Dy3 Dy 0.84945(5) 0.47639(5) 0.15873(4) 0.0487(2) Uani 1 1 d . . . . .
Dy2 Dy 0.59629(5) 0.53849(6) 0.53112(4) 0.0593(3) Uani 1 1 d . . . . .
O6 O 0.7048(6) 0.4634(6) 0.1903(5) 0.046(2) Uani 1 1 d . . . . .
O3 O 0.2225(6) 0.7889(6) 0.6337(5) 0.048(2) Uani 1 1 d . . . . .
O1 O 0.2573(6) 0.7505(6) 0.7905(5) 0.044(2) Uani 1 1 d . . . . .
O2 O 0.1285(7) 0.6642(6) 0.7639(5) 0.044(2) Uani 1 1 d . . . . .
O22 O 0.4301(6) 0.6275(6) 0.7429(5) 0.041(2) Uani 1 1 d . . . . .
O21 O 0.8156(6) 0.3700(6) 0.3899(5) 0.049(2) Uani 1 1 d . . . . .
O8 O 0.8853(7) 0.1079(6) 0.2363(6) 0.050(2) Uani 1 1 d . . . . .
O7 O 0.8902(8) 0.3723(7) 0.0827(6) 0.062(3) Uani 1 1 d . . . . .
O4 O 0.5282(7) 0.4317(7) 0.5521(5) 0.056(3) Uani 1 1 d . . . . .
O14 O 0.5823(7) 0.1996(7) 0.2816(7) 0.060(3) Uani 1 1 d . . . . .
H14 H 0.567746 0.250545 0.255858 0.089 Uiso 1 1 d R . . . .
O19 O 1.0074(8) 0.4688(8) 0.1540(6) 0.070(3) Uani 1 1 d . . . . .
H19A H 1.033823 0.462144 0.202155 0.105 Uiso 1 1 d R . . . .
H19B H 1.030432 0.413914 0.144425 0.105 Uiso 1 1 d R . . . .
O20 O 0.8794(8) 0.4925(8) 0.2847(7) 0.072(3) Uani 1 1 d . . . . .
H20A H 0.867270 0.549491 0.289950 0.107 Uiso 1 1 d R . . . .
H20B H 0.942520 0.471551 0.299860 0.107 Uiso 1 1 d R . . . .
O13 O 0.7823(8) 0.6129(7) 0.1367(6) 0.061(3) Uani 1 1 d . . . . .
O12 O 0.7045(9) 0.0629(7) 0.4126(6) 0.067(3) Uani 1 1 d . . . . .
O9 O 0.7163(10) 0.0785(10) 0.1736(8) 0.086(4) Uani 1 1 d . . . . .
O10 O 0.6530(10) 0.0188(9) 0.2734(10) 0.087(4) Uani 1 1 d . . . . .
O18 O 1.0423(9) 0.2110(10) 0.2080(9) 0.107(6) Uani 1 1 d . . . . .
H18A H 1.064435 0.259084 0.194949 0.161 Uiso 1 1 d GR . . . .
H18B H 1.089194 0.169899 0.188182 0.161 Uiso 1 1 d GR . . . .
O5 O 0.7094(10) 0.6039(9) 0.5586(7) 0.089(4) Uani 1 1 d . . . . .
H5A H 0.696229 0.622650 0.608529 0.134 Uiso 1 1 d R . . . .
H5B H 0.707059 0.653340 0.517509 0.134 Uiso 1 1 d R . . . .
H5C H 0.771639 0.562860 0.561129 0.134 Uiso 1 1 d R . . . .
O15 O 0.8118(9) 0.1809(12) 0.0609(7) 0.094(5) Uani 1 1 d . . . . .
O17 O 0.7219(10) 0.2253(11) -0.0350(8) 0.113(6) Uani 1 1 d . . . . .
O16 O 0.7713(12) 0.3043(11) 0.0370(9) 0.108(5) Uani 1 1 d . . . . .
O11 O 0.6287(13) -0.0002(13) 0.1563(13) 0.137(8) Uani 1 1 d . . . . .
N10 N 0.9075(8) 0.4669(8) -0.0249(6) 0.047(3) Uani 1 1 d . . . . .
N13 N 0.7464(8) 0.4202(8) 0.5729(6) 0.047(3) Uani 1 1 d . . . . .
N1 N 0.3872(8) 0.6728(7) 0.6001(6) 0.042(3) Uani 1 1 d . . . . .
N4 N 0.6657(8) 0.4847(7) 0.3443(6) 0.045(3) Uani 1 1 d . . . . .
N9 N 0.9832(8) 0.2429(9) 0.0250(8) 0.053(3) Uani 1 1 d . . . . .
N11 N 0.8617(8) 0.5272(9) 0.0197(7) 0.054(3) Uani 1 1 d . . . . .
N3 N 0.6920(8) 0.4774(8) 0.4227(6) 0.046(3) Uani 1 1 d . . . . .
N14 N 0.6329(8) 0.4971(8) 0.6750(6) 0.048(3) Uani 1 1 d . . . . .
N6 N 0.8613(9) -0.0187(8) 0.3332(8) 0.058(3) Uani 1 1 d . . . . .
N2 N 0.4790(7) 0.6218(8) 0.6174(6) 0.047(3) Uani 1 1 d . . . . .
N7 N 0.9339(9) -0.0385(8) 0.2824(8) 0.059(3) Uani 1 1 d . . . . .
N12 N 0.7575(15) 0.2356(9) 0.0209(9) 0.088(6) Uani 1 1 d . . . . .
N5 N 0.6656(11) 0.0310(12) 0.2004(12) 0.080(5) Uani 1 1 d . . . . .
N8 N 0.9975(8) 0.0939(8) 0.1214(8) 0.055(3) Uani 1 1 d . . . . .
N15 N 0.5901(12) 0.6825(11) 0.4509(10) 0.081(4) Uani 1 1 d D U . . .
C6 C 0.6263(9) 0.5293(8) 0.1748(8) 0.038(3) Uani 1 1 d . . . . .
C3 C 0.3722(10) 0.7226(10) 0.5340(8) 0.046(3) Uani 1 1 d . . . . .
H3 H 0.423646 0.722289 0.500769 0.055 Uiso 1 1 calc R . . . .
C15 C 0.9196(10) 0.3921(10) 0.0130(8) 0.048(4) Uani 1 1 d . . . . .
C13 C 1.0374(10) 0.1718(10) 0.0021(10) 0.054(4) Uani 1 1 d . . . . .
C5 C 0.5836(10) 0.5755(9) 0.2315(8) 0.045(3) Uani 1 1 d . . . . .
C43 C 0.7685(9) 0.4127(9) 0.4395(7) 0.044(3) Uani 1 1 d . . . . .
C52 C 0.8215(12) 0.3465(12) 0.8068(9) 0.072(5) Uani 1 1 d . . . . .
H52 H 0.836905 0.327365 0.860554 0.087 Uiso 1 1 calc R . . . .
C14 C 0.9747(9) 0.3170(9) -0.0205(8) 0.041(3) Uani 1 1 d . . . . .
C62 C 0.1209(11) 0.8609(10) 0.5221(9) 0.055(4) Uani 1 1 d . . . . .
C4 C 0.6164(10) 0.5579(9) 0.3104(8) 0.048(4) Uani 1 1 d . . . . .
H4 H 0.600649 0.603130 0.338943 0.058 Uiso 1 1 calc R . . . .
C48 C 0.4892(9) 0.5991(8) 0.6936(7) 0.039(3) Uani 1 1 d . . . . .
C51 C 0.7362(11) 0.4133(12) 0.7825(8) 0.062(5) Uani 1 1 d . . . . .
C58 C 0.630(2) 0.8263(16) 0.3754(18) 0.142(10) Uani 1 1 d D U . . .
H58A H 0.587379 0.858714 0.331914 0.213 Uiso 1 1 d R . . . .
H58B H 0.693499 0.806333 0.356004 0.213 Uiso 1 1 d R . . . .
H58C H 0.630579 0.863124 0.412944 0.213 Uiso 1 1 d R . . . .
C46 C 0.7130(10) 0.4353(11) 0.7037(8) 0.055(4) Uani 1 1 d . . . . .
C24 C 1.0156(11) 0.3253(12) -0.0930(10) 0.063(4) Uani 1 1 d . . . . .
H24 H 1.007228 0.379717 -0.125341 0.075 Uiso 1 1 calc R . . . .
C1 C 0.2098(10) 0.8086(9) 0.5557(9) 0.051(4) Uani 1 1 d . . . . .
C45 C 0.7726(10) 0.3950(10) 0.6487(8) 0.052(4) Uani 1 1 d . . . . .
C44 C 0.8029(9) 0.3875(10) 0.5201(8) 0.048(4) Uani 1 1 d . . . . .
C42 C 0.6271(11) 0.4974(11) 0.0385(8) 0.056(4) Uani 1 1 d . . . . .
H42A H 0.685171 0.510274 0.020710 0.085 Uiso 1 1 calc GR . . . .
H42B H 0.583066 0.511447 -0.005628 0.085 Uiso 1 1 calc GR . . . .
H42C H 0.640683 0.436548 0.061094 0.085 Uiso 1 1 calc GR . . . .
C2 C 0.2820(10) 0.7790(9) 0.5066(8) 0.047(3) Uani 1 1 d . . . . .
C38 C 0.5839(11) 0.5507(10) 0.1000(8) 0.052(4) Uani 1 1 d . . . . .
C49 C 0.5990(10) 0.5179(11) 0.8043(8) 0.055(4) Uani 1 1 d . . . . .
H49 H 0.558796 0.549861 0.837832 0.066 Uiso 1 1 calc R . . . .
C12 C 1.0461(12) 0.0919(11) 0.0550(9) 0.062(4) Uani 1 1 d . . . . .
C41 C 0.5044(12) 0.6481(10) 0.2095(10) 0.062(4) Uani 1 1 d . . . . .
H41 H 0.478051 0.682800 0.246433 0.074 Uiso 1 1 calc R . . . .
C16 C 0.8341(10) 0.6044(11) -0.0231(9) 0.056(4) Uani 1 1 d . . . . .
H16 H 0.847251 0.609851 -0.076833 0.067 Uiso 1 1 calc R . . . .
C29 C 1.1042(11) 0.0152(12) 0.0360(11) 0.066(5) Uani 1 1 d . . . . .
C47 C 0.5774(10) 0.5355(10) 0.7259(8) 0.050(4) Uani 1 1 d . . . . .
C50 C 0.6767(12) 0.4559(12) 0.8342(8) 0.067(5) Uani 1 1 d . . . . .
H50 H 0.690288 0.441981 0.888469 0.080 Uiso 1 1 calc R . . . .
C57 C 0.604(3) 0.7482(16) 0.4148(19) 0.146(10) Uani 1 1 d D U . . .
C10 C 0.9392(11) 0.0289(11) 0.2349(10) 0.058(4) Uani 1 1 d . . . . .
C25 C 1.0693(11) 0.2507(13) -0.1163(10) 0.062(5) Uani 1 1 d . . . . .
H25 H 1.097561 0.254355 -0.165580 0.074 Uiso 1 1 calc R . . . .
C63 C 0.0431(12) 0.8873(12) 0.5755(10) 0.070(5) Uani 1 1 d . . . . .
H63A H 0.032765 0.836427 0.608405 0.105 Uiso 1 1 calc GR . . . .
H63B H -0.013995 0.919791 0.544980 0.105 Uiso 1 1 calc GR . . . .
H63C H 0.059400 0.923077 0.608167 0.105 Uiso 1 1 calc GR . . . .
C28 C 1.1485(13) 0.0173(13) -0.0372(11) 0.071(5) Uani 1 1 d . . . . .
H28 H 1.184974 -0.034424 -0.051409 0.085 Uiso 1 1 calc R . . . .
C61 C 0.1120(13) 0.8831(11) 0.4431(10) 0.068(5) Uani 1 1 d . . . . .
H61 H 0.053096 0.917663 0.421014 0.082 Uiso 1 1 calc R . . . .
C7 C 0.7214(13) -0.0091(11) 0.4608(11) 0.064(4) Uani 1 1 d . . . . .
C53 C 0.8797(12) 0.3110(13) 0.7542(9) 0.076(6) Uani 1 1 d . . . . .
H53 H 0.936657 0.268980 0.771776 0.092 Uiso 1 1 calc R . . . .
C40 C 0.4661(13) 0.6683(11) 0.1370(9) 0.070(5) Uani 1 1 d . . . . .
H40 H 0.411758 0.715285 0.123762 0.084 Uiso 1 1 calc R . . . .
C9 C 0.8611(13) -0.0806(12) 0.3934(12) 0.075(5) Uani 1 1 d . . . . .
H9 H 0.910430 -0.131845 0.395169 0.089 Uiso 1 1 calc R . . . .
C39 C 0.5073(12) 0.6196(10) 0.0821(10) 0.064(5) Uani 1 1 d . . . . .
H39 H 0.481278 0.634648 0.030804 0.077 Uiso 1 1 calc R . . . .
C54 C 0.8586(10) 0.3343(11) 0.6748(9) 0.061(5) Uani 1 1 d . . . . .
C26 C 1.0818(10) 0.1724(13) -0.0694(10) 0.061(5) Uani 1 1 d . . . . .
C27 C 1.1392(11) 0.0907(13) -0.0853(11) 0.068(5) Uani 1 1 d . . . . .
H27 H 1.171649 0.090193 -0.132750 0.081 Uiso 1 1 calc R . . . .
C20 C 0.6888(12) 0.8345(11) 0.0501(12) 0.069(5) Uani 1 1 d . . . . .
H20 H 0.655895 0.886970 0.064991 0.083 Uiso 1 1 calc R . . . .
C59 C 0.2699(13) 0.8065(11) 0.4239(9) 0.067(5) Uani 1 1 d . . . . .
H59 H 0.320084 0.789618 0.390332 0.080 Uiso 1 1 calc R . . . .
C11 C 1.0027(12) 0.0220(11) 0.1702(10) 0.061(4) Uani 1 1 d . . . . .
C56 C 0.8888(11) 0.3278(12) 0.5400(9) 0.064(5) Uani 1 1 d . . . . .
H56 H 0.927223 0.304614 0.500657 0.077 Uiso 1 1 calc R . . . .
C23 C 0.6842(15) 0.7636(11) 0.1870(13) 0.088(7) Uani 1 1 d . . . . .
H23A H 0.663680 0.822670 0.195555 0.131 Uiso 1 1 calc GR . . . .
H23B H 0.739370 0.731591 0.220046 0.131 Uiso 1 1 calc GR . . . .
H23C H 0.633752 0.736920 0.200032 0.131 Uiso 1 1 calc GR . . . .
C60 C 0.1830(14) 0.8584(11) 0.3941(9) 0.070(5) Uani 1 1 d . . . . .
H60 H 0.173036 0.876690 0.339575 0.085 Uiso 1 1 calc R . . . .
C18 C 0.7582(11) 0.6816(10) 0.0846(10) 0.055(4) Uani 1 1 d . . . . .
C19 C 0.7082(12) 0.7632(11) 0.1035(11) 0.065(5) Uani 1 1 d . . . . .
C17 C 0.7846(13) 0.6828(11) 0.0053(9) 0.064(4) Uani 1 1 d . . . . .
C30 C 1.1118(12) -0.0598(12) 0.0905(11) 0.073(5) Uani 1 1 d . . . . .
H30 H 1.151376 -0.112278 0.079985 0.087 Uiso 1 1 calc R . . . .
C8 C 0.7992(14) -0.0809(14) 0.4540(11) 0.076(5) Uani 1 1 d . . . . .
C55 C 0.9187(11) 0.3019(12) 0.6165(9) 0.069(5) Uani 1 1 d . . . . .
H55 H 0.978707 0.262997 0.630141 0.083 Uiso 1 1 calc R . . . .
C31 C 1.0642(12) -0.0601(12) 0.1586(11) 0.069(5) Uani 1 1 d . . . . .
H31 H 1.070885 -0.110944 0.195973 0.083 Uiso 1 1 calc R . . . .
C22 C 0.7627(14) 0.7583(12) -0.0490(11) 0.076(5) Uani 1 1 d . . . . .
H22 H 0.780477 0.757025 -0.101364 0.092 Uiso 1 1 calc R . . . .
C35 C 0.6596(16) -0.0169(13) 0.5249(10) 0.076(5) Uani 1 1 d . . . . .
C21 C 0.7154(16) 0.8352(12) -0.0283(13) 0.086(6) Uani 1 1 d . . . . .
H21 H 0.701229 0.886984 -0.065325 0.103 Uiso 1 1 calc R . . . .
C36 C 0.5803(15) 0.0551(13) 0.5321(11) 0.080(6) Uani 1 1 d . . . . .
H36A H 0.600141 0.107337 0.523566 0.120 Uiso 1 1 calc GR . . . .
H36B H 0.555248 0.046193 0.584273 0.120 Uiso 1 1 calc GR . . . .
H36C H 0.531909 0.060640 0.493382 0.120 Uiso 1 1 calc GR . . . .
C32 C 0.8126(19) -0.1555(16) 0.5103(16) 0.115(9) Uani 1 1 d . . . . .
H32 H 0.865344 -0.202658 0.506629 0.138 Uiso 1 1 calc R . . . .
C37 C 0.5006(17) 0.1818(16) 0.3243(16) 0.111(8) Uani 1 1 d . . . . .
H37A H 0.444854 0.204250 0.290076 0.167 Uiso 1 1 calc GR . . . .
H37B H 0.490494 0.209473 0.369779 0.167 Uiso 1 1 calc GR . . . .
H37C H 0.512533 0.120008 0.341225 0.167 Uiso 1 1 calc GR . . . .
C34 C 0.678(2) -0.0934(19) 0.5748(14) 0.113(9) Uani 1 1 d . . . . .
H34 H 0.636537 -0.099478 0.616075 0.136 Uiso 1 1 calc R . . . .
C33 C 0.754(2) -0.163(2) 0.5690(17) 0.133(11) Uani 1 1 d . . . . .
H33 H 0.764971 -0.215028 0.605736 0.159 Uiso 1 1 calc R . . . .
O23 O 0.8549(19) 0.573(2) 0.7310(17) 0.097(8) Uani 0.5 1 d D U P . .
H23 H 0.862056 0.534002 0.706615 0.146 Uiso 0.5 1 d R . P . .
C64 C 0.768(2) 0.636(2) 0.740(2) 0.076(8) Uani 0.5 1 d D U P . .
H64A H 0.736777 0.613338 0.786023 0.114 Uiso 0.5 1 d R . P . .
H64B H 0.727437 0.648079 0.694283 0.114 Uiso 0.5 1 d R . P . .
H64C H 0.780707 0.688328 0.748193 0.114 Uiso 0.5 1 d R . P . .
O24 O 1.0370(16) 0.3132(17) 0.3388(14) 0.188(10) Uani 1 1 d . U . . .
H24A H 1.074167 0.258390 0.335084 0.281 Uiso 1 1 d R . . . .
H24B H 1.066877 0.325400 0.374804 0.281 Uiso 1 1 d R . . . .
O25 O 0.899(3) 0.635(2) 0.322(2) 0.123(12) Uani 0.5 1 d . U P A -2
H25A H 0.922761 0.585090 0.350036 0.185 Uiso 0.5 1 d R . P A -2
H25B H 0.890321 0.658320 0.356776 0.185 Uiso 0.5 1 d R . P A -2
O26 O 0.420(4) 0.847(4) 0.269(4) 0.098(17) Uani 0.25 1 d . U P B -1
H26A H 0.362443 0.857672 0.242908 0.147 Uiso 0.25 1 d R . P B -1
H26B H 0.439353 0.895002 0.247238 0.147 Uiso 0.25 1 d R . P B -1
O27 O 0.430(3) 0.7286(18) -0.1104(14) 0.111(12) Uani 0.5 1 d . . P . .
H27A H 0.395220 0.746335 -0.072636 0.166 Uiso 0.5 1 d R . P . .
H27B H 0.480210 0.743825 -0.106116 0.166 Uiso 0.5 1 d R . P . .
O28 O 0.848(4) -0.366(3) 0.390(3) 0.178(19) Uani 0.5 1 d . U P C -4
H28A H 0.856903 -0.416580 0.418937 0.267 Uiso 0.5 1 d R . P C -4
H28B H 0.870933 -0.338260 0.418447 0.267 Uiso 0.5 1 d R . P C -4
O29 O 0.592(6) 1.106(6) -0.024(5) 0.16(3) Uani 0.25 1 d . U P . .
H29A H 0.571185 1.077384 -0.052638 0.245 Uiso 0.25 1 d R . P . .
H29B H 0.545765 1.151544 -0.023118 0.245 Uiso 0.25 1 d R . P . .
O30 O 1.155(5) 0.232(5) 0.687(4) 0.13(2) Uani 0.25 1 d . U P . .
H30A H 1.173900 0.214375 0.643412 0.189 Uiso 0.25 1 d R . P . .
H30B H 1.113030 0.207845 0.706562 0.189 Uiso 0.25 1 d R . P . .
O31 O 0.557(5) 0.743(5) 0.891(4) 0.13(2) Uani 0.25 1 d . U P D -3
H31A H 0.503924 0.779686 0.874653 0.195 Uiso 0.25 1 d R . P D -3
H31B H 0.592554 0.773416 0.899573 0.195 Uiso 0.25 1 d R . P D -3
O32 O 0.193(3) 1.061(3) 0.242(3) 0.146(14) Uani 0.5 1 d . U P . .
H32A H 0.181455 1.105897 0.205146 0.219 Uiso 0.5 1 d R . P . .
H32B H 0.174355 1.075927 0.285806 0.219 Uiso 0.5 1 d R . P . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Dy1 Dy4 3.8427(8) 2_666 ?
Dy1 Dy5 3.7328(10) 2_666 ?
Dy1 Dy3 3.7137(10) 2_666 ?
Dy1 O6 2.348(10) 2_666 ?
Dy1 O3 2.304(10) . ?
Dy1 O1 2.350(8) . ?
Dy1 O2 2.352(9) . ?
Dy1 O22 2.327(9) . ?
Dy1 O21 2.337(10) 2_666 ?
Dy1 N1 2.510(11) . ?
Dy1 N4 2.521(11) 2_666 ?
Dy4 Dy5 3.9363(11) . ?
Dy4 Dy3 3.9367(10) . ?
Dy4 O1 2.393(9) 2_666 ?
Dy4 O2 2.421(8) 2_666 ?
Dy4 O8 2.355(10) . ?
Dy4 O7 2.389(11) . ?
Dy4 O18 2.388(13) . ?
Dy4 O15 2.431(14) . ?
Dy4 O16 2.596(16) . ?
Dy4 N9 2.563(12) . ?
Dy4 N8 2.536(11) . ?
Dy5 O3 2.318(10) 2_666 ?
Dy5 O1 2.420(10) 2_666 ?
Dy5 O8 2.334(10) . ?
Dy5 O14 2.377(10) . ?
Dy5 O12 2.197(11) . ?
Dy5 O9 2.442(12) . ?
Dy5 O10 2.493(15) . ?
Dy5 N6 2.443(12) . ?
Dy5 N5 2.869(16) . ?
Dy3 O6 2.274(10) . ?
Dy3 O2 2.411(10) 2_666 ?
Dy3 O7 2.315(9) . ?
Dy3 O19 2.326(11) . ?
Dy3 O20 2.345(11) . ?
Dy3 O13 2.168(11) . ?
Dy3 N11 2.446(12) . ?
Dy2 Dy2 3.7313(17) 2_666 ?
Dy2 O4 2.279(9) 2_666 ?
Dy2 O4 2.257(13) . ?
Dy2 O5 2.359(15) . ?
Dy2 N13 2.542(11) . ?
Dy2 N3 2.534(9) . ?
Dy2 N14 2.521(11) . ?
Dy2 N2 2.552(9) . ?
Dy2 N15 2.519(18) . ?
O6 C6 1.350(15) . ?
O3 C1 1.351(18) . ?
O22 C48 1.271(14) . ?
O21 C43 1.290(15) . ?
O8 C10 1.335(17) . ?
O7 C15 1.303(17) . ?
O14 H14 0.8527 . ?
O14 C37 1.49(2) . ?
O19 H19A 0.9169 . ?
O19 H19B 0.9233 . ?
O20 H20A 0.9341 . ?
O20 H20B 0.9350 . ?
O13 C18 1.289(19) . ?
O12 C7 1.29(2) . ?
O9 N5 1.26(2) . ?
O10 N5 1.28(2) . ?
O18 H18A 0.9378 . ?
O18 H18B 0.9376 . ?
O5 H5A 0.9802 . ?
O5 H5B 0.9799 . ?
O5 H5C 0.9799 . ?
O15 N12 1.161(19) . ?
O17 N12 1.191(19) . ?
O16 N12 1.30(2) . ?
O11 N5 1.23(2) . ?
N10 N11 1.398(15) . ?
N10 C15 1.262(19) . ?
N13 C45 1.351(17) . ?
N13 C44 1.320(16) . ?
N1 N2 1.398(15) . ?
N1 C3 1.277(18) . ?
N4 N3 1.415(15) . ?
N4 C4 1.272(18) . ?
N9 C13 1.351(17) . ?
N9 C14 1.313(19) . ?
N11 C16 1.32(2) . ?
N3 C43 1.321(17) . ?
N14 C46 1.371(18) . ?
N14 C47 1.326(17) . ?
N6 N7 1.389(18) . ?
N6 C9 1.33(2) . ?
N2 C48 1.321(16) . ?
N7 C10 1.29(2) . ?
N8 C12 1.355(19) . ?
N8 C11 1.32(2) . ?
N15 C57 1.225(10) . ?
C6 C5 1.397(18) . ?
C6 C38 1.411(19) . ?
C3 H3 0.9500 . ?
C3 C2 1.44(2) . ?
C15 C14 1.496(18) . ?
C13 C12 1.45(2) . ?
C13 C26 1.40(2) . ?
C5 C4 1.43(2) . ?
C5 C41 1.43(2) . ?
C43 C44 1.462(19) . ?
C52 H52 0.9500 . ?
C52 C51 1.44(2) . ?
C52 C53 1.35(2) . ?
C14 C24 1.39(2) . ?
C62 C1 1.44(2) . ?
C62 C63 1.49(2) . ?
C62 C61 1.37(2) . ?
C4 H4 0.9500 . ?
C48 C47 1.482(19) . ?
C51 C46 1.39(2) . ?
C51 C50 1.39(2) . ?
C58 H58A 0.9798 . ?
C58 H58B 0.9799 . ?
C58 H58C 0.9802 . ?
C58 C57 1.503(10) . ?
C46 C45 1.422(18) . ?
C24 H24 0.9500 . ?
C24 C25 1.40(2) . ?
C1 C2 1.39(2) . ?
C45 C54 1.41(2) . ?
C44 C56 1.39(2) . ?
C42 H42A 0.9800 . ?
C42 H42B 0.9800 . ?
C42 H42C 0.9800 . ?
C42 C38 1.535(19) . ?
C2 C59 1.44(2) . ?
C38 C39 1.36(2) . ?
C49 H49 0.9500 . ?
C49 C47 1.379(19) . ?
C49 C50 1.35(2) . ?
C12 C29 1.41(2) . ?
C41 H41 0.9500 . ?
C41 C40 1.35(2) . ?
C16 H16 0.9500 . ?
C16 C17 1.47(2) . ?
C29 C28 1.43(2) . ?
C29 C30 1.40(3) . ?
C50 H50 0.9500 . ?
C10 C11 1.46(2) . ?
C25 H25 0.9500 . ?
C25 C26 1.37(3) . ?
C63 H63A 0.9800 . ?
C63 H63B 0.9800 . ?
C63 H63C 0.9800 . ?
C28 H28 0.9500 . ?
C28 C27 1.32(3) . ?
C61 H61 0.9500 . ?
C61 C60 1.36(3) . ?
C7 C8 1.43(3) . ?
C7 C35 1.44(3) . ?
C53 H53 0.9500 . ?
C53 C54 1.39(2) . ?
C40 H40 0.9500 . ?
C40 C39 1.39(2) . ?
C9 H9 0.9500 . ?
C9 C8 1.39(3) . ?
C39 H39 0.9500 . ?
C54 C55 1.42(2) . ?
C26 C27 1.46(2) . ?
C27 H27 0.9500 . ?
C20 H20 0.9500 . ?
C20 C19 1.33(3) . ?
C20 C21 1.42(3) . ?
C59 H59 0.9500 . ?
C59 C60 1.39(2) . ?
C11 C31 1.46(2) . ?
C56 H56 0.9500 . ?
C56 C55 1.38(2) . ?
C23 H23A 0.9800 . ?
C23 H23B 0.9800 . ?
C23 H23C 0.9800 . ?
C23 C19 1.50(3) . ?
C60 H60 0.9500 . ?
C18 C19 1.44(2) . ?
C18 C17 1.43(2) . ?
C17 C22 1.39(3) . ?
C30 H30 0.9500 . ?
C30 C31 1.37(2) . ?
C8 C32 1.40(3) . ?
C55 H55 0.9500 . ?
C31 H31 0.9500 . ?
C22 H22 0.9500 . ?
C22 C21 1.38(3) . ?
C35 C36 1.44(3) . ?
C35 C34 1.36(3) . ?
C21 H21 0.9500 . ?
C36 H36A 0.9800 . ?
C36 H36B 0.9800 . ?
C36 H36C 0.9800 . ?
C32 H32 0.9500 . ?
C32 C33 1.34(4) . ?
C37 H37A 0.9800 . ?
C37 H37B 0.9800 . ?
C37 H37C 0.9800 . ?
C34 H34 0.9500 . ?
C34 C33 1.39(4) . ?
C33 H33 0.9500 . ?
O23 H23 0.8258 . ?
O23 C64 1.440(19) . ?
C64 H64A 0.9798 . ?
C64 H64B 0.9800 . ?
C64 H64C 0.9798 . ?
O24 H24A 0.9344 . ?
O24 H24B 0.8699 . ?
O25 H25A 0.8702 . ?
O25 H25B 0.7724 . ?
O26 H26A 0.9382 . ?
O26 H26B 0.9453 . ?
O27 H27A 0.8703 . ?
O27 H27B 0.8697 . ?
O28 H28A 0.8699 . ?
O28 H28B 0.8699 . ?
O29 H29A 0.8698 . ?
O29 H29B 0.8701 . ?
O30 H30A 0.8697 . ?
O30 H30B 0.8703 . ?
O31 H31A 0.8702 . ?
O31 H31B 0.8699 . ?
O32 H32A 0.8700 . ?
O32 H32B 0.8701 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Dy5 Dy1 Dy4 62.592(18) 2_666 2_666 ?
Dy3 Dy1 Dy4 62.768(18) 2_666 2_666 ?
Dy3 Dy1 Dy5 125.31(2) 2_666 2_666 ?
O6 Dy1 Dy4 81.72(19) 2_666 2_666 ?
O6 Dy1 Dy5 131.1(2) 2_666 2_666 ?
O6 Dy1 Dy3 35.9(2) 2_666 2_666 ?
O6 Dy1 O1 92.4(3) 2_666 . ?
O6 Dy1 O2 72.9(3) 2_666 . ?
O6 Dy1 N1 127.0(3) 2_666 . ?
O6 Dy1 N4 70.4(3) 2_666 2_666 ?
O3 Dy1 Dy4 79.3(2) . 2_666 ?
O3 Dy1 Dy5 36.3(2) . 2_666 ?
O3 Dy1 Dy3 131.1(2) . 2_666 ?
O3 Dy1 O6 161.0(3) . 2_666 ?
O3 Dy1 O1 71.9(3) . . ?
O3 Dy1 O2 91.9(3) . . ?
O3 Dy1 O22 108.6(4) . . ?
O3 Dy1 O21 79.2(4) . 2_666 ?
O3 Dy1 N1 70.5(3) . . ?
O3 Dy1 N4 127.1(3) . 2_666 ?
O1 Dy1 Dy4 36.3(2) . 2_666 ?
O1 Dy1 Dy5 39.2(2) . 2_666 ?
O1 Dy1 Dy3 91.2(2) . 2_666 ?
O1 Dy1 O2 73.2(3) . . ?
O1 Dy1 N1 112.7(4) . . ?
O1 Dy1 N4 158.8(3) . 2_666 ?
O2 Dy1 Dy4 37.0(2) . 2_666 ?
O2 Dy1 Dy5 93.1(2) . 2_666 ?
O2 Dy1 Dy3 39.3(2) . 2_666 ?
O2 Dy1 N1 157.2(3) . . ?
O2 Dy1 N4 111.5(4) . 2_666 ?
O22 Dy1 Dy4 111.32(18) . 2_666 ?
O22 Dy1 Dy5 84.7(2) . 2_666 ?
O22 Dy1 Dy3 113.2(2) . 2_666 ?
O22 Dy1 O6 78.1(3) . 2_666 ?
O22 Dy1 O1 80.0(3) . . ?
O22 Dy1 O2 139.1(3) . . ?
O22 Dy1 O21 140.5(3) . 2_666 ?
O22 Dy1 N1 62.7(3) . . ?
O22 Dy1 N4 84.3(3) . 2_666 ?
O21 Dy1 Dy4 108.2(2) 2_666 2_666 ?
O21 Dy1 Dy5 114.8(2) 2_666 2_666 ?
O21 Dy1 Dy3 84.3(3) 2_666 2_666 ?
O21 Dy1 O6 107.3(4) 2_666 2_666 ?
O21 Dy1 O1 137.1(3) 2_666 . ?
O21 Dy1 O2 76.7(3) 2_666 . ?
O21 Dy1 N1 85.6(3) 2_666 . ?
O21 Dy1 N4 62.5(3) 2_666 2_666 ?
N1 Dy1 Dy4 143.8(3) . 2_666 ?
N1 Dy1 Dy5 81.2(3) . 2_666 ?
N1 Dy1 Dy3 153.4(3) . 2_666 ?
N1 Dy1 N4 71.4(4) . 2_666 ?
N4 Dy1 Dy4 144.7(3) 2_666 2_666 ?
N4 Dy1 Dy5 152.6(3) 2_666 2_666 ?
N4 Dy1 Dy3 82.1(3) 2_666 2_666 ?
Dy1 Dy4 Dy5 57.336(17) 2_666 . ?
Dy1 Dy4 Dy3 57.014(16) 2_666 . ?
Dy5 Dy4 Dy3 114.311(19) . . ?
O1 Dy4 Dy1 35.5(2) 2_666 2_666 ?
O1 Dy4 Dy5 35.4(2) 2_666 . ?
O1 Dy4 Dy3 85.3(2) 2_666 . ?
O1 Dy4 O2 71.3(3) 2_666 2_666 ?
O1 Dy4 O15 79.1(4) 2_666 . ?
O1 Dy4 O16 75.2(4) 2_666 . ?
O1 Dy4 N9 147.2(4) 2_666 . ?
O1 Dy4 N8 124.7(4) 2_666 . ?
O2 Dy4 Dy1 35.8(2) 2_666 2_666 ?
O2 Dy4 Dy5 87.2(2) 2_666 . ?
O2 Dy4 Dy3 35.3(2) 2_666 . ?
O2 Dy4 O15 144.2(4) 2_666 . ?
O2 Dy4 O16 106.4(4) 2_666 . ?
O2 Dy4 N9 122.9(4) 2_666 . ?
O2 Dy4 N8 144.1(4) 2_666 . ?
O8 Dy4 Dy1 84.1(2) . 2_666 ?
O8 Dy4 Dy5 32.8(2) . . ?
O8 Dy4 Dy3 137.6(2) . . ?
O8 Dy4 O1 68.1(3) . 2_666 ?
O8 Dy4 O2 102.9(3) . 2_666 ?
O8 Dy4 O7 170.2(3) . . ?
O8 Dy4 O18 86.7(5) . . ?
O8 Dy4 O15 83.6(5) . . ?
O8 Dy4 O16 121.5(5) . . ?
O8 Dy4 N9 126.9(4) . . ?
O8 Dy4 N8 63.7(4) . . ?
O7 Dy4 Dy1 86.7(2) . 2_666 ?
O7 Dy4 Dy5 140.7(2) . . ?
O7 Dy4 Dy3 32.6(2) . . ?
O7 Dy4 O1 105.9(3) . 2_666 ?
O7 Dy4 O2 67.4(3) . 2_666 ?
O7 Dy4 O15 103.2(5) . . ?
O7 Dy4 O16 62.1(5) . . ?
O7 Dy4 N9 62.4(4) . . ?
O7 Dy4 N8 125.0(4) . . ?
O18 Dy4 Dy1 102.7(3) . 2_666 ?
O18 Dy4 Dy5 109.8(5) . . ?
O18 Dy4 Dy3 86.2(4) . . ?
O18 Dy4 O1 130.2(4) . 2_666 ?
O18 Dy4 O2 73.8(3) . 2_666 ?
O18 Dy4 O7 91.9(5) . . ?
O18 Dy4 O15 142.0(4) . . ?
O18 Dy4 O16 149.8(6) . . ?
O18 Dy4 N9 82.2(5) . . ?
O18 Dy4 N8 72.3(4) . . ?
O15 Dy4 Dy1 112.6(3) . 2_666 ?
O15 Dy4 Dy5 79.8(4) . . ?
O15 Dy4 Dy3 124.4(4) . . ?
O15 Dy4 O16 45.1(6) . . ?
O15 Dy4 N9 74.7(4) . . ?
O15 Dy4 N8 70.5(5) . . ?
O16 Dy4 Dy1 91.4(3) . 2_666 ?
O16 Dy4 Dy5 100.3(4) . . ?
O16 Dy4 Dy3 79.3(4) . . ?
N9 Dy4 Dy1 149.0(3) . 2_666 ?
N9 Dy4 Dy5 150.0(3) . . ?
N9 Dy4 Dy3 93.4(3) . . ?
N9 Dy4 O16 72.5(5) . . ?
N8 Dy4 Dy1 147.4(3) . 2_666 ?
N8 Dy4 Dy5 93.3(3) . . ?
N8 Dy4 Dy3 149.8(3) . . ?
N8 Dy4 O16 108.9(5) . . ?
N8 Dy4 N9 63.4(4) . . ?
Dy1 Dy5 Dy4 60.072(17) 2_666 . ?
O3 Dy5 Dy1 36.0(2) 2_666 2_666 ?
O3 Dy5 Dy4 77.1(2) 2_666 . ?
O3 Dy5 O1 70.5(3) 2_666 2_666 ?
O3 Dy5 O8 87.8(3) 2_666 . ?
O3 Dy5 O14 92.1(3) 2_666 . ?
O3 Dy5 O9 151.1(5) 2_666 . ?
O3 Dy5 O10 152.9(4) 2_666 . ?
O3 Dy5 N6 106.5(4) 2_666 . ?
O3 Dy5 N5 168.6(4) 2_666 . ?
O1 Dy5 Dy1 37.85(18) 2_666 2_666 ?
O1 Dy5 Dy4 34.9(2) 2_666 . ?
O1 Dy5 O9 80.9(5) 2_666 . ?
O1 Dy5 O10 125.1(4) 2_666 . ?
O1 Dy5 N6 132.5(4) 2_666 . ?
O1 Dy5 N5 102.8(5) 2_666 . ?
O8 Dy5 Dy1 87.0(2) . 2_666 ?
O8 Dy5 Dy4 33.1(2) . . ?
O8 Dy5 O1 68.0(3) . 2_666 ?
O8 Dy5 O14 141.1(4) . . ?
O8 Dy5 O9 77.2(4) . . ?
O8 Dy5 O10 117.9(4) . . ?
O8 Dy5 N6 64.5(4) . . ?
O8 Dy5 N5 98.3(4) . . ?
O14 Dy5 Dy1 71.2(3) . 2_666 ?
O14 Dy5 Dy4 109.4(3) . . ?
O14 Dy5 O1 75.4(3) . 2_666 ?
O14 Dy5 O9 84.7(4) . . ?
O14 Dy5 O10 73.5(4) . . ?
O14 Dy5 N6 150.1(4) . . ?
O14 Dy5 N5 77.1(4) . . ?
O12 Dy5 Dy1 108.2(3) . 2_666 ?
O12 Dy5 Dy4 153.9(3) . . ?
O12 Dy5 O3 81.3(4) . 2_666 ?
O12 Dy5 O1 145.0(3) . 2_666 ?
O12 Dy5 O8 132.5(4) . . ?
O12 Dy5 O14 85.7(4) . . ?
O12 Dy5 O9 126.9(5) . . ?
O12 Dy5 O10 74.9(5) . . ?
O12 Dy5 N6 74.7(5) . . ?
O12 Dy5 N5 101.2(6) . . ?
O9 Dy5 Dy1 117.4(4) . 2_666 ?
O9 Dy5 Dy4 76.9(4) . . ?
O9 Dy5 O10 52.3(5) . . ?
O9 Dy5 N6 89.3(5) . . ?
O9 Dy5 N5 26.0(5) . . ?
O10 Dy5 Dy1 144.2(3) . 2_666 ?
O10 Dy5 Dy4 129.0(4) . . ?
O10 Dy5 N5 26.3(5) . . ?
N6 Dy5 Dy1 136.1(3) . 2_666 ?
N6 Dy5 Dy4 97.6(3) . . ?
N6 Dy5 O10 79.7(5) . . ?
N6 Dy5 N5 84.8(5) . . ?
N5 Dy5 Dy1 134.2(4) . 2_666 ?
N5 Dy5 Dy4 102.9(5) . . ?
Dy1 Dy3 Dy4 60.220(17) 2_666 . ?
O6 Dy3 Dy1 37.2(2) . 2_666 ?
O6 Dy3 Dy4 80.4(2) . . ?
O6 Dy3 O2 73.1(3) . 2_666 ?
O6 Dy3 O7 97.4(4) . . ?
O6 Dy3 O19 166.7(4) . . ?
O6 Dy3 O20 92.0(4) . . ?
O6 Dy3 N11 112.4(4) . . ?
O2 Dy3 Dy1 38.2(2) 2_666 2_666 ?
O2 Dy3 Dy4 35.52(19) 2_666 . ?
O2 Dy3 N11 132.7(4) 2_666 . ?
O7 Dy3 Dy1 90.9(3) . 2_666 ?
O7 Dy3 Dy4 33.8(3) . . ?
O7 Dy3 O2 68.7(3) . 2_666 ?
O7 Dy3 O19 84.2(4) . . ?
O7 Dy3 O20 138.6(4) . . ?
O7 Dy3 N11 64.0(4) . . ?
O19 Dy3 Dy1 129.9(3) . 2_666 ?
O19 Dy3 Dy4 94.2(3) . . ?
O19 Dy3 O2 95.4(4) . 2_666 ?
O19 Dy3 O20 78.4(4) . . ?
O19 Dy3 N11 80.2(4) . . ?
O20 Dy3 Dy1 73.0(3) . 2_666 ?
O20 Dy3 Dy4 110.4(3) . . ?
O20 Dy3 O2 75.8(4) . 2_666 ?
O20 Dy3 N11 145.9(4) . . ?
O13 Dy3 Dy1 115.1(3) . 2_666 ?
O13 Dy3 Dy4 158.8(3) . . ?
O13 Dy3 O6 85.6(4) . . ?
O13 Dy3 O2 151.1(3) . 2_666 ?
O13 Dy3 O7 134.9(4) . . ?
O13 Dy3 O19 102.6(4) . . ?
O13 Dy3 O20 85.8(4) . . ?
O13 Dy3 N11 73.3(4) . . ?
N11 Dy3 Dy1 140.4(3) . 2_666 ?
N11 Dy3 Dy4 97.5(3) . . ?
O4 Dy2 Dy2 34.5(3) 2_666 2_666 ?
O4 Dy2 Dy2 34.8(2) . 2_666 ?
O4 Dy2 O4 69.3(4) . 2_666 ?
O4 Dy2 O5 138.0(5) 2_666 . ?
O4 Dy2 O5 152.7(4) . . ?
O4 Dy2 N13 139.1(4) 2_666 . ?
O4 Dy2 N13 84.6(4) . . ?
O4 Dy2 N3 91.4(4) . . ?
O4 Dy2 N3 85.0(3) 2_666 . ?
O4 Dy2 N14 139.0(4) 2_666 . ?
O4 Dy2 N14 84.3(4) . . ?
O4 Dy2 N2 85.0(3) 2_666 . ?
O4 Dy2 N2 91.1(4) . . ?
O4 Dy2 N15 145.0(5) . . ?
O4 Dy2 N15 75.7(5) 2_666 . ?
O5 Dy2 Dy2 172.4(3) . 2_666 ?
O5 Dy2 N13 72.6(5) . . ?
O5 Dy2 N3 92.0(4) . . ?
O5 Dy2 N14 72.3(4) . . ?
O5 Dy2 N2 91.1(5) . . ?
O5 Dy2 N15 62.3(5) . . ?
N13 Dy2 Dy2 113.9(3) . 2_666 ?
N13 Dy2 N2 127.8(3) . . ?
N3 Dy2 Dy2 87.8(3) . 2_666 ?
N3 Dy2 N13 64.0(4) . . ?
N3 Dy2 N2 168.1(4) . . ?
N14 Dy2 Dy2 113.6(3) . 2_666 ?
N14 Dy2 N13 63.8(3) . . ?
N14 Dy2 N3 127.8(4) . . ?
N14 Dy2 N2 64.0(4) . . ?
N2 Dy2 Dy2 87.6(3) . 2_666 ?
N15 Dy2 Dy2 110.1(4) . 2_666 ?
N15 Dy2 N13 124.3(5) . . ?
N15 Dy2 N3 85.7(4) . . ?
N15 Dy2 N14 124.3(5) . . ?
N15 Dy2 N2 85.6(4) . . ?
Dy3 O6 Dy1 106.9(4) . 2_666 ?
C6 O6 Dy1 125.0(8) . 2_666 ?
C6 O6 Dy3 122.9(8) . . ?
Dy1 O3 Dy5 107.7(4) . 2_666 ?
C1 O3 Dy1 125.6(8) . . ?
C1 O3 Dy5 121.7(9) . 2_666 ?
Dy1 O1 Dy4 108.2(4) . 2_666 ?
Dy1 O1 Dy5 103.0(3) . 2_666 ?
Dy4 O1 Dy5 109.7(3) 2_666 2_666 ?
Dy1 O2 Dy4 107.2(4) . 2_666 ?
Dy1 O2 Dy3 102.5(3) . 2_666 ?
Dy3 O2 Dy4 109.1(3) 2_666 2_666 ?
C48 O22 Dy1 114.8(8) . . ?
C43 O21 Dy1 114.9(8) . 2_666 ?
Dy5 O8 Dy4 114.2(4) . . ?
C10 O8 Dy4 126.2(10) . . ?
C10 O8 Dy5 116.0(10) . . ?
Dy3 O7 Dy4 113.6(4) . . ?
C15 O7 Dy4 127.2(9) . . ?
C15 O7 Dy3 118.6(9) . . ?
Dy2 O4 Dy2 110.7(4) . 2_666 ?
Dy5 O14 H14 119.4 . . ?
C37 O14 Dy5 128.7(12) . . ?
C37 O14 H14 110.7 . . ?
Dy3 O19 H19A 112.8 . . ?
Dy3 O19 H19B 98.5 . . ?
H19A O19 H19B 100.5 . . ?
Dy3 O20 H20A 113.4 . . ?
Dy3 O20 H20B 113.6 . . ?
H20A O20 H20B 100.5 . . ?
C18 O13 Dy3 145.5(9) . . ?
C7 O12 Dy5 140.9(11) . . ?
N5 O9 Dy5 96.2(11) . . ?
N5 O10 Dy5 93.5(12) . . ?
Dy4 O18 H18A 112.5 . . ?
Dy4 O18 H18B 112.6 . . ?
H18A O18 H18B 101.2 . . ?
Dy2 O5 H5A 109.4 . . ?
Dy2 O5 H5B 109.4 . . ?
Dy2 O5 H5C 109.6 . . ?
H5A O5 H5B 109.5 . . ?
H5A O5 H5C 109.5 . . ?
H5B O5 H5C 109.5 . . ?
N12 O15 Dy4 112.5(14) . . ?
N12 O16 Dy4 98.5(11) . . ?
C15 N10 N11 110.7(11) . . ?
C45 N13 Dy2 120.4(8) . . ?
C44 N13 Dy2 120.1(9) . . ?
C44 N13 C45 119.3(12) . . ?
N2 N1 Dy1 114.2(7) . . ?
C3 N1 Dy1 129.2(9) . . ?
C3 N1 N2 116.6(11) . . ?
N3 N4 Dy1 113.4(8) . 2_666 ?
C4 N4 Dy1 130.2(9) . 2_666 ?
C4 N4 N3 116.4(11) . . ?
C13 N9 Dy4 121.0(11) . . ?
C14 N9 Dy4 120.5(8) . . ?
C14 N9 C13 118.4(13) . . ?
N10 N11 Dy3 117.5(10) . . ?
C16 N11 Dy3 131.3(10) . . ?
C16 N11 N10 111.2(12) . . ?
N4 N3 Dy2 129.4(8) . . ?
C43 N3 Dy2 119.9(8) . . ?
C43 N3 N4 108.4(10) . . ?
C46 N14 Dy2 121.1(8) . . ?
C47 N14 Dy2 121.8(9) . . ?
C47 N14 C46 117.1(11) . . ?
N7 N6 Dy5 117.2(10) . . ?
C9 N6 Dy5 127.5(11) . . ?
C9 N6 N7 115.1(13) . . ?
N1 N2 Dy2 129.5(7) . . ?
C48 N2 Dy2 119.5(8) . . ?
C48 N2 N1 108.0(9) . . ?
C10 N7 N6 110.8(12) . . ?
O15 N12 O17 123.0(15) . . ?
O15 N12 O16 103.5(18) . . ?
O17 N12 O16 130.0(18) . . ?
O9 N5 Dy5 57.8(9) . . ?
O9 N5 O10 117.9(16) . . ?
O10 N5 Dy5 60.2(9) . . ?
O11 N5 Dy5 175.0(17) . . ?
O11 N5 O9 120(2) . . ?
O11 N5 O10 122(2) . . ?
C12 N8 Dy4 121.0(11) . . ?
C11 N8 Dy4 119.5(9) . . ?
C11 N8 C12 119.4(13) . . ?
C57 N15 Dy2 168(2) . . ?
O6 C6 C5 121.9(12) . . ?
O6 C6 C38 119.3(11) . . ?
C5 C6 C38 118.7(12) . . ?
N1 C3 H3 118.0 . . ?
N1 C3 C2 123.9(13) . . ?
C2 C3 H3 118.0 . . ?
O7 C15 C14 114.3(13) . . ?
N10 C15 O7 125.5(12) . . ?
N10 C15 C14 120.2(12) . . ?
N9 C13 C12 116.3(14) . . ?
N9 C13 C26 123.5(16) . . ?
C26 C13 C12 120.1(14) . . ?
C6 C5 C4 124.5(13) . . ?
C6 C5 C41 118.7(13) . . ?
C41 C5 C4 116.7(12) . . ?
O21 C43 N3 124.9(12) . . ?
O21 C43 C44 117.2(12) . . ?
N3 C43 C44 117.9(11) . . ?
C51 C52 H52 119.5 . . ?
C53 C52 H52 119.5 . . ?
C53 C52 C51 120.9(14) . . ?
N9 C14 C15 114.2(11) . . ?
N9 C14 C24 123.0(13) . . ?
C24 C14 C15 122.8(14) . . ?
C1 C62 C63 118.0(14) . . ?
C61 C62 C1 118.3(15) . . ?
C61 C62 C63 123.6(15) . . ?
N4 C4 C5 123.2(12) . . ?
N4 C4 H4 118.4 . . ?
C5 C4 H4 118.4 . . ?
O22 C48 N2 125.9(11) . . ?
O22 C48 C47 116.2(11) . . ?
N2 C48 C47 117.9(10) . . ?
C46 C51 C52 117.7(13) . . ?
C46 C51 C50 119.1(14) . . ?
C50 C51 C52 123.2(14) . . ?
H58A C58 H58B 109.5 . . ?
H58A C58 H58C 109.5 . . ?
H58B C58 H58C 109.5 . . ?
C57 C58 H58A 111.9 . . ?
C57 C58 H58B 106.7 . . ?
C57 C58 H58C 109.8 . . ?
N14 C46 C51 122.1(12) . . ?
N14 C46 C45 116.8(12) . . ?
C51 C46 C45 121.1(13) . . ?
C14 C24 H24 121.2 . . ?
C14 C24 C25 117.5(17) . . ?
C25 C24 H24 121.2 . . ?
O3 C1 C62 120.0(13) . . ?
O3 C1 C2 121.1(13) . . ?
C2 C1 C62 118.9(14) . . ?
N13 C45 C46 118.0(12) . . ?
N13 C45 C54 122.9(12) . . ?
C54 C45 C46 119.0(13) . . ?
N13 C44 C43 117.0(12) . . ?
N13 C44 C56 122.1(13) . . ?
C56 C44 C43 120.8(12) . . ?
H42A C42 H42B 109.5 . . ?
H42A C42 H42C 109.5 . . ?
H42B C42 H42C 109.5 . . ?
C38 C42 H42A 109.5 . . ?
C38 C42 H42B 109.5 . . ?
C38 C42 H42C 109.5 . . ?
C1 C2 C3 123.6(13) . . ?
C1 C2 C59 120.4(14) . . ?
C59 C2 C3 116.0(13) . . ?
C6 C38 C42 119.3(13) . . ?
C39 C38 C6 120.3(13) . . ?
C39 C38 C42 120.4(14) . . ?
C47 C49 H49 119.5 . . ?
C50 C49 H49 119.5 . . ?
C50 C49 C47 121.1(13) . . ?
N8 C12 C13 118.0(13) . . ?
N8 C12 C29 122.6(17) . . ?
C29 C12 C13 119.4(15) . . ?
C5 C41 H41 119.4 . . ?
C40 C41 C5 121.2(14) . . ?
C40 C41 H41 119.4 . . ?
N11 C16 H16 117.2 . . ?
N11 C16 C17 125.5(14) . . ?
C17 C16 H16 117.2 . . ?
C12 C29 C28 119.4(18) . . ?
C30 C29 C12 116.8(15) . . ?
C30 C29 C28 123.8(15) . . ?
N14 C47 C48 115.9(12) . . ?
N14 C47 C49 122.8(13) . . ?
C49 C47 C48 121.2(12) . . ?
C51 C50 H50 121.2 . . ?
C49 C50 C51 117.7(13) . . ?
C49 C50 H50 121.2 . . ?
N15 C57 C58 174(4) . . ?
O8 C10 C11 114.6(16) . . ?
N7 C10 O8 124.8(14) . . ?
N7 C10 C11 120.4(14) . . ?
C24 C25 H25 119.4 . . ?
C26 C25 C24 121.2(15) . . ?
C26 C25 H25 119.4 . . ?
C62 C63 H63A 109.5 . . ?
C62 C63 H63B 109.5 . . ?
C62 C63 H63C 109.5 . . ?
H63A C63 H63B 109.5 . . ?
H63A C63 H63C 109.5 . . ?
H63B C63 H63C 109.5 . . ?
C29 C28 H28 119.8 . . ?
C27 C28 C29 120.4(15) . . ?
C27 C28 H28 119.8 . . ?
C62 C61 H61 118.1 . . ?
C60 C61 C62 123.7(16) . . ?
C60 C61 H61 118.1 . . ?
O12 C7 C8 122.9(17) . . ?
O12 C7 C35 118.6(17) . . ?
C8 C7 C35 118.5(17) . . ?
C52 C53 H53 119.1 . . ?
C52 C53 C54 121.8(15) . . ?
C54 C53 H53 119.1 . . ?
C41 C40 H40 120.4 . . ?
C41 C40 C39 119.2(15) . . ?
C39 C40 H40 120.4 . . ?
N6 C9 H9 115.4 . . ?
N6 C9 C8 129.2(17) . . ?
C8 C9 H9 115.4 . . ?
C38 C39 C40 121.6(15) . . ?
C38 C39 H39 119.2 . . ?
C40 C39 H39 119.2 . . ?
C45 C54 C55 116.3(13) . . ?
C53 C54 C45 119.2(13) . . ?
C53 C54 C55 124.5(14) . . ?
C13 C26 C27 117.2(18) . . ?
C25 C26 C13 116.3(14) . . ?
C25 C26 C27 126.4(15) . . ?
C28 C27 C26 123.3(16) . . ?
C28 C27 H27 118.4 . . ?
C26 C27 H27 118.4 . . ?
C19 C20 H20 118.8 . . ?
C19 C20 C21 122.5(17) . . ?
C21 C20 H20 118.8 . . ?
C2 C59 H59 120.8 . . ?
C60 C59 C2 118.4(16) . . ?
C60 C59 H59 120.8 . . ?
N8 C11 C10 115.6(13) . . ?
N8 C11 C31 122.7(16) . . ?
C10 C11 C31 121.6(17) . . ?
C44 C56 H56 119.9 . . ?
C55 C56 C44 120.2(13) . . ?
C55 C56 H56 119.9 . . ?
H23A C23 H23B 109.5 . . ?
H23A C23 H23C 109.5 . . ?
H23B C23 H23C 109.5 . . ?
C19 C23 H23A 109.5 . . ?
C19 C23 H23B 109.5 . . ?
C19 C23 H23C 109.5 . . ?
C61 C60 C59 120.0(15) . . ?
C61 C60 H60 120.0 . . ?
C59 C60 H60 120.0 . . ?
O13 C18 C19 122.0(15) . . ?
O13 C18 C17 122.2(13) . . ?
C17 C18 C19 115.7(16) . . ?
C20 C19 C23 122.1(15) . . ?
C20 C19 C18 121.5(17) . . ?
C18 C19 C23 116.3(16) . . ?
C18 C17 C16 121.9(15) . . ?
C22 C17 C16 116.7(15) . . ?
C22 C17 C18 121.4(16) . . ?
C29 C30 H30 118.9 . . ?
C31 C30 C29 122.3(15) . . ?
C31 C30 H30 118.9 . . ?
C9 C8 C7 122.9(18) . . ?
C9 C8 C32 119(2) . . ?
C32 C8 C7 119(2) . . ?
C54 C55 H55 120.4 . . ?
C56 C55 C54 119.1(13) . . ?
C56 C55 H55 120.4 . . ?
C11 C31 H31 121.9 . . ?
C30 C31 C11 116.1(18) . . ?
C30 C31 H31 121.9 . . ?
C17 C22 H22 119.5 . . ?
C21 C22 C17 121.1(19) . . ?
C21 C22 H22 119.5 . . ?
C7 C35 C36 119.0(17) . . ?
C34 C35 C7 118(2) . . ?
C34 C35 C36 123.2(19) . . ?
C20 C21 H21 121.0 . . ?
C22 C21 C20 118.0(19) . . ?
C22 C21 H21 121.0 . . ?
C35 C36 H36A 109.5 . . ?
C35 C36 H36B 109.5 . . ?
C35 C36 H36C 109.5 . . ?
H36A C36 H36B 109.5 . . ?
H36A C36 H36C 109.5 . . ?
H36B C36 H36C 109.5 . . ?
C8 C32 H32 118.5 . . ?
C33 C32 C8 123(3) . . ?
C33 C32 H32 118.5 . . ?
O14 C37 H37A 109.5 . . ?
O14 C37 H37B 109.5 . . ?
O14 C37 H37C 109.5 . . ?
H37A C37 H37B 109.5 . . ?
H37A C37 H37C 109.5 . . ?
H37B C37 H37C 109.5 . . ?
C35 C34 H34 118.0 . . ?
C35 C34 C33 124(2) . . ?
C33 C34 H34 118.0 . . ?
C32 C33 C34 118(2) . . ?
C32 C33 H33 120.9 . . ?
C34 C33 H33 120.9 . . ?
C64 O23 H23 126.1 . . ?
O23 C64 H64A 109.1 . . ?
O23 C64 H64B 110.1 . . ?
O23 C64 H64C 109.2 . . ?
H64A C64 H64B 109.5 . . ?
H64A C64 H64C 109.5 . . ?
H64B C64 H64C 109.5 . . ?
H24A O24 H24B 101.5 . . ?
H25A O25 H25B 93.9 . . ?
H26A O26 H26B 102.0 . . ?
H27A O27 H27B 104.5 . . ?
H28A O28 H28B 104.5 . . ?
H29A O29 H29B 104.5 . . ?
H30A O30 H30B 109.4 . . ?
H31A O31 H31B 104.5 . . ?
H32A O32 H32B 109.5 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Dy1 O6 C6 C5 51.6(17) 2_666 . . . ?
Dy1 O6 C6 C38 -126.3(12) 2_666 . . . ?
Dy1 O3 C1 C62 125.1(13) . . . . ?
Dy1 O3 C1 C2 -54.9(19) . . . . ?
Dy1 O22 C48 N2 37.0(18) . . . . ?
Dy1 O22 C48 C47 -143.6(10) . . . . ?
Dy1 O21 C43 N3 -37.2(19) 2_666 . . . ?
Dy1 O21 C43 C44 143.0(11) 2_666 . . . ?
Dy1 N1 N2 Dy2 137.9(7) . . . . ?
Dy1 N1 N2 C48 -21.8(14) . . . . ?
Dy1 N1 C3 C2 -1(2) . . . . ?
Dy1 N4 N3 Dy2 -138.0(7) 2_666 . . . ?
Dy1 N4 N3 C43 24.4(14) 2_666 . . . ?
Dy1 N4 C4 C5 0(2) 2_666 . . . ?
Dy4 O8 C10 N7 -180.0(12) . . . . ?
Dy4 O8 C10 C11 -4.5(19) . . . . ?
Dy4 O7 C15 N10 170.9(12) . . . . ?
Dy4 O7 C15 C14 -11.3(19) . . . . ?
Dy4 O15 N12 O17 167.5(19) . . . . ?
Dy4 O15 N12 O16 6.8(19) . . . . ?
Dy4 O16 N12 O15 -6.0(17) . . . . ?
Dy4 O16 N12 O17 -165(2) . . . . ?
Dy4 N9 C13 C12 -4.5(19) . . . . ?
Dy4 N9 C13 C26 173.9(12) . . . . ?
Dy4 N9 C14 C15 7.9(17) . . . . ?
Dy4 N9 C14 C24 -173.8(12) . . . . ?
Dy4 N8 C12 C13 1(2) . . . . ?
Dy4 N8 C12 C29 -178.8(13) . . . . ?
Dy4 N8 C11 C10 5.2(19) . . . . ?
Dy4 N8 C11 C31 -177.9(12) . . . . ?
Dy5 O3 C1 C62 -82.8(16) 2_666 . . . ?
Dy5 O3 C1 C2 97.2(15) 2_666 . . . ?
Dy5 O8 C10 N7 -23(2) . . . . ?
Dy5 O8 C10 C11 152.7(11) . . . . ?
Dy5 O12 C7 C8 16(3) . . . . ?
Dy5 O12 C7 C35 -164.5(14) . . . . ?
Dy5 O9 N5 O10 -3.7(16) . . . . ?
Dy5 O9 N5 O11 174.7(15) . . . . ?
Dy5 O10 N5 O9 3.6(16) . . . . ?
Dy5 O10 N5 O11 -174.7(16) . . . . ?
Dy5 N6 N7 C10 17.6(17) . . . . ?
Dy5 N6 C9 C8 -6(3) . . . . ?
Dy3 O6 C6 C5 -99.6(13) . . . . ?
Dy3 O6 C6 C38 82.5(14) . . . . ?
Dy3 O7 C15 N10 -18(2) . . . . ?
Dy3 O7 C15 C14 159.6(9) . . . . ?
Dy3 O13 C18 C19 178.5(13) . . . . ?
Dy3 O13 C18 C17 -6(3) . . . . ?
Dy3 N11 C16 C17 -1(2) . . . . ?
Dy2 N13 C45 C46 1(2) . . . . ?
Dy2 N13 C45 C54 -175.1(13) . . . . ?
Dy2 N13 C44 C43 -9.0(19) . . . . ?
Dy2 N13 C44 C56 174.8(13) . . . . ?
Dy2 N3 C43 O21 170.8(12) . . . . ?
Dy2 N3 C43 C44 -9.3(19) . . . . ?
Dy2 N14 C46 C51 177.9(14) . . . . ?
Dy2 N14 C46 C45 -1(2) . . . . ?
Dy2 N14 C47 C48 4.7(19) . . . . ?
Dy2 N14 C47 C49 -175.6(13) . . . . ?
Dy2 N2 C48 O22 -170.4(11) . . . . ?
Dy2 N2 C48 C47 10.2(18) . . . . ?
O6 C6 C5 C4 -1(2) . . . . ?
O6 C6 C5 C41 175.7(14) . . . . ?
O6 C6 C38 C42 1(2) . . . . ?
O6 C6 C38 C39 -176.7(15) . . . . ?
O3 C1 C2 C3 3(2) . . . . ?
O3 C1 C2 C59 -174.7(15) . . . . ?
O22 C48 C47 N14 170.8(14) . . . . ?
O22 C48 C47 C49 -9(2) . . . . ?
O21 C43 C44 N13 -168.0(14) . . . . ?
O21 C43 C44 C56 8(2) . . . . ?
O8 C10 C11 N8 -1(2) . . . . ?
O8 C10 C11 C31 -177.9(15) . . . . ?
O7 C15 C14 N9 1.2(19) . . . . ?
O7 C15 C14 C24 -177.1(15) . . . . ?
O13 C18 C19 C20 175.7(17) . . . . ?
O13 C18 C19 C23 -1(3) . . . . ?
O13 C18 C17 C16 5(3) . . . . ?
O13 C18 C17 C22 -176.2(17) . . . . ?
O12 C7 C8 C9 -3(3) . . . . ?
O12 C7 C8 C32 179(2) . . . . ?
O12 C7 C35 C36 1(3) . . . . ?
O12 C7 C35 C34 180(2) . . . . ?
N10 N11 C16 C17 -179.4(15) . . . . ?
N10 C15 C14 N9 179.1(14) . . . . ?
N10 C15 C14 C24 1(2) . . . . ?
N13 C45 C54 C53 -179.2(18) . . . . ?
N13 C45 C54 C55 2(3) . . . . ?
N13 C44 C56 C55 -1(3) . . . . ?
N1 N2 C48 O22 -8(2) . . . . ?
N1 N2 C48 C47 172.3(13) . . . . ?
N1 C3 C2 C1 23(2) . . . . ?
N1 C3 C2 C59 -158.4(15) . . . . ?
N4 N3 C43 O21 6(2) . . . . ?
N4 N3 C43 C44 -173.7(13) . . . . ?
N9 C13 C12 N8 2(2) . . . . ?
N9 C13 C12 C29 -177.8(15) . . . . ?
N9 C13 C26 C25 1(2) . . . . ?
N9 C13 C26 C27 179.0(15) . . . . ?
N9 C14 C24 C25 -1(2) . . . . ?
N11 N10 C15 O7 3(2) . . . . ?
N11 N10 C15 C14 -174.6(12) . . . . ?
N11 C16 C17 C18 -2(3) . . . . ?
N11 C16 C17 C22 179.1(17) . . . . ?
N3 N4 C4 C5 -179.4(13) . . . . ?
N3 C43 C44 N13 12(2) . . . . ?
N3 C43 C44 C56 -171.7(16) . . . . ?
N14 C46 C45 N13 0(2) . . . . ?
N14 C46 C45 C54 176.5(16) . . . . ?
N6 N7 C10 O8 3(2) . . . . ?
N6 N7 C10 C11 -172.3(14) . . . . ?
N6 C9 C8 C7 0(3) . . . . ?
N6 C9 C8 C32 178(2) . . . . ?
N2 N1 C3 C2 179.7(13) . . . . ?
N2 C48 C47 N14 -10(2) . . . . ?
N2 C48 C47 C49 170.4(15) . . . . ?
N7 N6 C9 C8 179.7(19) . . . . ?
N7 C10 C11 N8 174.8(15) . . . . ?
N7 C10 C11 C31 -2(3) . . . . ?
N8 C12 C29 C28 176.1(17) . . . . ?
N8 C12 C29 C30 -2(3) . . . . ?
N8 C11 C31 C30 -5(3) . . . . ?
C6 C5 C4 N4 -25(2) . . . . ?
C6 C5 C41 C40 5(3) . . . . ?
C6 C38 C39 C40 -3(3) . . . . ?
C3 N1 N2 Dy2 -42.4(17) . . . . ?
C3 N1 N2 C48 158.0(13) . . . . ?
C3 C2 C59 C60 177.5(16) . . . . ?
C15 N10 N11 Dy3 12.6(15) . . . . ?
C15 N10 N11 C16 -168.9(13) . . . . ?
C15 C14 C24 C25 176.9(14) . . . . ?
C13 N9 C14 C15 -175.4(13) . . . . ?
C13 N9 C14 C24 3(2) . . . . ?
C13 C12 C29 C28 -4(3) . . . . ?
C13 C12 C29 C30 178.3(16) . . . . ?
C13 C26 C27 C28 2(3) . . . . ?
C5 C6 C38 C42 -176.8(14) . . . . ?
C5 C6 C38 C39 5(2) . . . . ?
C5 C41 C40 C39 -3(3) . . . . ?
C43 C44 C56 C55 -177.3(17) . . . . ?
C52 C51 C46 N14 179.1(17) . . . . ?
C52 C51 C46 C45 -2(3) . . . . ?
C52 C51 C50 C49 179.5(19) . . . . ?
C52 C53 C54 C45 -2(3) . . . . ?
C52 C53 C54 C55 177(2) . . . . ?
C14 N9 C13 C12 178.8(14) . . . . ?
C14 N9 C13 C26 -3(2) . . . . ?
C14 C24 C25 C26 -1(2) . . . . ?
C62 C1 C2 C3 -176.5(14) . . . . ?
C62 C1 C2 C59 5(2) . . . . ?
C62 C61 C60 C59 1(3) . . . . ?
C4 N4 N3 Dy2 41.7(18) . . . . ?
C4 N4 N3 C43 -155.8(14) . . . . ?
C4 C5 C41 C40 -177.7(17) . . . . ?
C51 C52 C53 C54 -3(3) . . . . ?
C51 C46 C45 N13 -179.2(17) . . . . ?
C51 C46 C45 C54 -3(3) . . . . ?
C46 N14 C47 C48 -177.3(14) . . . . ?
C46 N14 C47 C49 2(2) . . . . ?
C46 C51 C50 C49 -1(3) . . . . ?
C46 C45 C54 C53 5(3) . . . . ?
C46 C45 C54 C55 -174.5(17) . . . . ?
C24 C25 C26 C13 1(2) . . . . ?
C24 C25 C26 C27 -177.1(16) . . . . ?
C1 C62 C61 C60 0(3) . . . . ?
C1 C2 C59 C60 -4(3) . . . . ?
C45 N13 C44 C43 176.1(14) . . . . ?
C45 N13 C44 C56 0(2) . . . . ?
C45 C54 C55 C56 -3(3) . . . . ?
C44 N13 C45 C46 176.1(16) . . . . ?
C44 N13 C45 C54 0(3) . . . . ?
C44 C56 C55 C54 3(3) . . . . ?
C42 C38 C39 C40 179.2(17) . . . . ?
C2 C59 C60 C61 1(3) . . . . ?
C38 C6 C5 C4 176.8(15) . . . . ?
C38 C6 C5 C41 -6(2) . . . . ?
C12 N8 C11 C10 -172.4(15) . . . . ?
C12 N8 C11 C31 5(3) . . . . ?
C12 C13 C26 C25 179.4(15) . . . . ?
C12 C13 C26 C27 -3(2) . . . . ?
C12 C29 C28 C27 3(3) . . . . ?
C12 C29 C30 C31 1(3) . . . . ?
C41 C5 C4 N4 158.3(15) . . . . ?
C41 C40 C39 C38 2(3) . . . . ?
C16 C17 C22 C21 179.3(18) . . . . ?
C29 C28 C27 C26 -2(3) . . . . ?
C29 C30 C31 C11 2(3) . . . . ?
C47 N14 C46 C51 0(3) . . . . ?
C47 N14 C46 C45 -179.4(15) . . . . ?
C47 C49 C50 C51 3(3) . . . . ?
C50 C51 C46 N14 -1(3) . . . . ?
C50 C51 C46 C45 178.5(18) . . . . ?
C50 C49 C47 N14 -4(3) . . . . ?
C50 C49 C47 C48 175.7(17) . . . . ?
C10 C11 C31 C30 172.0(17) . . . . ?
C25 C26 C27 C28 179.8(18) . . . . ?
C63 C62 C1 O3 -4(2) . . . . ?
C63 C62 C1 C2 176.2(16) . . . . ?
C63 C62 C61 C60 -179.5(18) . . . . ?
C28 C29 C30 C31 -176.4(18) . . . . ?
C61 C62 C1 O3 176.8(15) . . . . ?
C61 C62 C1 C2 -3(2) . . . . ?
C7 C8 C32 C33 2(4) . . . . ?
C7 C35 C34 C33 2(4) . . . . ?
C53 C52 C51 C46 4(3) . . . . ?
C53 C52 C51 C50 -176(2) . . . . ?
C53 C54 C55 C56 178(2) . . . . ?
C9 N6 N7 C10 -167.8(15) . . . . ?
C9 C8 C32 C33 -177(3) . . . . ?
C26 C13 C12 N8 -176.3(15) . . . . ?
C26 C13 C12 C29 4(2) . . . . ?
C11 N8 C12 C13 178.8(15) . . . . ?
C11 N8 C12 C29 -1(3) . . . . ?
C18 C17 C22 C21 1(3) . . . . ?
C19 C20 C21 C22 0(3) . . . . ?
C19 C18 C17 C16 -178.6(16) . . . . ?
C19 C18 C17 C22 0(3) . . . . ?
C17 C18 C19 C20 0(3) . . . . ?
C17 C18 C19 C23 -177.1(17) . . . . ?
C17 C22 C21 C20 -1(3) . . . . ?
C30 C29 C28 C27 -179.0(19) . . . . ?
C8 C7 C35 C36 -179.7(19) . . . . ?
C8 C7 C35 C34 -1(3) . . . . ?
C8 C32 C33 C34 -1(5) . . . . ?
C35 C7 C8 C9 178.2(19) . . . . ?
C35 C7 C8 C32 -1(3) . . . . ?
C35 C34 C33 C32 -1(5) . . . . ?
C21 C20 C19 C23 176.8(19) . . . . ?
C21 C20 C19 C18 0(3) . . . . ?
C36 C35 C34 C33 -180(3) . . . . ?

_olex2_submission_special_instructions 'No special instructions were received'
_oxdiff_exptl_absorpt_empirical_details 
;
Empirical correction (ABSPACK) includes:
- Absorption correction using spherical harmonics
- Frame scaling
;
_oxdiff_exptl_absorpt_empirical_full_max 2.518
_oxdiff_exptl_absorpt_empirical_full_min 0.460
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_l-lt-17-100k
_database_code_depnum_ccdc_archive 'CCDC 2058348'
loop_
_audit_author_name
_audit_author_address
'Hai-Ling Wang'
;Guangxi Normal University
China
;
_audit_update_record             
;
2021-01-24 deposited with the CCDC.	2021-02-19 downloaded from the CCDC.
;
_audit_creation_date             2021-01-20
_audit_creation_method           
;
Olex2 1.2-beta
(compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         
'2(C75 H78 Dy5 N14 O20), 4(C2 H3 N), 11(C H4 O)'
_chemical_formula_sum            'C169 H212 Dy10 N32 O51'
_chemical_formula_weight         5132.71
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0030 0.0020 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1890 4.4100 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0060 0.0030 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0110 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           15
_space_group_name_H-M_alt        'I 1 2/a 1'
_space_group_name_Hall           '-I 2ya'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y, -z'
'x+1/2, y+1/2, z+1/2'
'-x+1, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y, z'
'-x+1/2, -y+1/2, -z+1/2'
'x, -y+1/2, z+1/2'

_cell_length_a                   20.1938(3)
_cell_length_b                   23.6957(3)
_cell_length_c                   20.2544(3)
_cell_angle_alpha                90
_cell_angle_beta                 101.8860(10)
_cell_angle_gamma                90
_cell_volume                     9484.1(2)
_cell_formula_units_Z            2
_cell_measurement_reflns_used    40915
_cell_measurement_temperature    100.00(10)
_cell_measurement_theta_max      30.4910
_cell_measurement_theta_min      1.7710
_shelx_estimated_absorpt_T_max   ?
_shelx_estimated_absorpt_T_min   ?
_exptl_absorpt_coefficient_mu    3.972
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.72145
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
CrysAlisPro 1.171.40.14a (Rigaku Oxford Diffraction, 2018)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.797
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             5035
_exptl_crystal_size_max          0.05
_exptl_crystal_size_mid          0.03
_exptl_crystal_size_min          0.02
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0864
_diffrn_reflns_av_unetI/netI     0.0838
_diffrn_reflns_Laue_measured_fraction_full 0.996
_diffrn_reflns_Laue_measured_fraction_max 0.814
_diffrn_reflns_limit_h_max       25
_diffrn_reflns_limit_h_min       -28
_diffrn_reflns_limit_k_max       29
_diffrn_reflns_limit_k_min       -33
_diffrn_reflns_limit_l_max       27
_diffrn_reflns_limit_l_min       -27
_diffrn_reflns_number            50416
_diffrn_reflns_point_group_measured_fraction_full 0.996
_diffrn_reflns_point_group_measured_fraction_max 0.814
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         30.227
_diffrn_reflns_theta_min         2.055
_diffrn_ambient_environment      N~2~
_diffrn_ambient_temperature      100.00(10)
_diffrn_detector                 'CCD plate'
_diffrn_detector_area_resol_mean ?
_diffrn_detector_type            HyPix
_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.814
_diffrn_measurement_details      
;
List of Runs (angles in degrees, time in seconds):

  # Type    Start    End  Width  tₑₓₚ   ω     θ     κ     φ   Frames
#--------------------------------------------------------------------------
  1  ω    -13.00  13.00   0.50    2.00    --   -1.74  87.00 -52.00   52
  2  ω    -44.00 -11.00   0.50    2.00    --   -1.74 -87.00-169.00   66
  3  ω    -10.00  25.00   0.50    2.00    --   -1.74 -99.00   0.00   70
  4  ω    -14.00  29.00   0.50    2.00    --   -1.74 -99.00  60.00   86
  5  ω      3.00  30.00   0.50    2.00    --   -1.74  68.00-158.00   54
  6  ω    -13.00  32.00   0.50    2.00    --   -1.74 -99.00 120.00   90
  7  ω     -3.00  53.00   0.50    2.00    --    4.16  37.00  60.00  112
  8  ω    -13.00  38.00   0.50    2.00    --    4.16 -99.00 -60.00  102
;
_diffrn_measurement_device       'four-circle diffractometer'
_diffrn_measurement_device_type  'ROD, Synergy Custom DW system, HyPix'
_diffrn_measurement_method       'ω scans'
_diffrn_orient_matrix_type       
'CrysAlisPro convention (1999,Acta A55,543-557)'
_diffrn_orient_matrix_UB_11      0.0326888000
_diffrn_orient_matrix_UB_12      0.0097011000
_diffrn_orient_matrix_UB_13      -0.0022830000
_diffrn_orient_matrix_UB_21      -0.0144147000
_diffrn_orient_matrix_UB_22      0.0251003000
_diffrn_orient_matrix_UB_23      -0.0158715000
_diffrn_orient_matrix_UB_31      0.0034393000
_diffrn_orient_matrix_UB_32      0.0131366000
_diffrn_orient_matrix_UB_33      0.0319821000
_diffrn_radiation_monochromator  mirror
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   'Rotating-anode X-ray tube'
_diffrn_source_type              'Rigaku (Mo) X-ray Source'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                9861
_reflns_number_total             11499
_reflns_odcompleteness_completeness 99.93
_reflns_odcompleteness_iscentric 1
_reflns_odcompleteness_theta     25.30
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'CrysAlisPro 1.171.40.14a (Rigaku OD, 2018)'
_computing_data_collection       'CrysAlisPro 1.171.40.14a (Rigaku OD, 2018)'
_computing_data_reduction        'CrysAlisPro 1.171.40.14a (Rigaku OD, 2018)'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    'ShelXT (Sheldrick, 2015)'
_refine_diff_density_max         4.141
_refine_diff_density_min         -3.681
_refine_diff_density_rms         0.413
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.180
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     636
_refine_ls_number_reflns         11499
_refine_ls_number_restraints     177
_refine_ls_R_factor_all          0.1354
_refine_ls_R_factor_gt           0.1272
_refine_ls_restrained_S_all      1.172
_refine_ls_shift/su_max          0.003
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0121P)²+2619.4104P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.3020
_refine_ls_wR_factor_ref         0.3049
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups, {H37A,H37B,H37C} of C37, All N(H) groups
 At 1.5 times of:
  All O(H) groups, {H43D,H43E,H43F} of C43A, {H28A,H28B,H28C} of C28, {H27A,
  H27B,H27C} of C27, {H26A,H26B,H26C} of C26, {H40A,H40B,H40C} of C40, {H41A,
  H41B,H41C} of C41, {H39A,H39B,H39C} of C39, {H43A,H43B,H43C} of C43, {H38A,
  H38B,H38C} of C38, {H12A,H12B,H12C} of C12, {H11A,H11B,H11C} of C11, {H10A,
  H10B,H10C} of C10
2. Restrained distances
 N8-C42
 1.15 with sigma of 0.01
 C43-C42
 1.48 with sigma of 0.01
 N8-C43
 2.4 with sigma of 0.02
 N8A-C42A
 1.15 with sigma of 0.01
 C43A-C42A
 1.48 with sigma of 0.02
 C43A-N8A
 2.4 with sigma of 0.02
3. Uiso/Uaniso restraints and constraints
O13 \\sim C40: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02
C42 \\sim N8 \\sim C43: within 2A with sigma of 0.01 and sigma for terminal
atoms of 0.02
N8 \\sim C42 \\sim C43 \\sim N8A \\sim C42A \\sim C43A: within 2A with sigma of
0.01 and sigma for terminal atoms of 0.02
Uanis(C40) \\sim Ueq, Uanis(O13) \\sim Ueq: with sigma of 0.01 and sigma for
terminal atoms of 0.02
Uanis(O9) \\sim Ueq, Uanis(C37) \\sim Ueq: with sigma of 0.01 and sigma for
terminal atoms of 0.02
Uanis(C24) \\sim Ueq, Uanis(C18) \\sim Ueq: with sigma of 0.01 and sigma for
terminal atoms of 0.02
Uanis(C16) \\sim Ueq, Uanis(C31) \\sim Ueq, Uanis(C13) \\sim Ueq: with sigma of
0.01 and sigma for terminal atoms of 0.02
Uanis(C16) \\sim Ueq: with sigma of 0.005 and sigma for terminal atoms of 0.01
Uanis(C13) \\sim Ueq: with sigma of 0.005 and sigma for terminal atoms of 0.01
Uanis(C42) \\sim Ueq, Uanis(C43) \\sim Ueq, Uanis(N8) \\sim Ueq: with sigma of
0.01 and sigma for terminal atoms of 0.02
Uanis(N8) \\sim Ueq, Uanis(C42) \\sim Ueq, Uanis(C43) \\sim Ueq, Uanis(N8A)
\\sim Ueq, Uanis(C42A) \\sim Ueq, Uanis(C43A) \\sim Ueq: with sigma of 0.01 and
sigma for terminal atoms of 0.02
4. Rigid body (RIGU) restrains
 O13, C40
 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01
 C43, C42, N8
 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01
 N8, C42, C43, N8A, C42A, C43A
 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01
5. Others
 Sof(N8A)=Sof(C42A)=Sof(C43A)=Sof(H43D)=Sof(H43E)=Sof(H43F)=1-FVAR(1)
 Sof(N8)=Sof(C42)=Sof(C43)=Sof(H43A)=Sof(H43B)=Sof(H43C)=FVAR(1)
 Fixed Sof: H7(0.5) H37A(0.5) H37B(0.5) H37C(0.5) O13(0.75) H13(0.75)
 C40(0.75) H40A(0.75) H40B(0.75) H40C(0.75)
6.a Riding coordinates:
 O11(H11), O10(H10), C37(H37A,H37B,H37C), O12(H12), O13(H13), O14(H14),
 C43A(H43D,H43E,H43F)
6.b Aromatic/amide H refined with riding coordinates:
 N7(H7), C23(H23), C22(H22), C21(H21), C20(H20), C29(H29), C30(H30), C32(H32),
 C33(H33), C35(H35), C36(H36), C2(H2), C8(H8), C7(H7A), C6(H6)
6.c Idealised Me refined as rotating group:
 C26(H26A,H26B,H26C), C27(H27A,H27B,H27C), C28(H28A,H28B,H28C), C10(H10A,H10B,
 H10C), C11(H11A,H11B,H11C), C12(H12A,H12B,H12C), C38(H38A,H38B,H38C), C43(H43A,
 H43B,H43C), C39(H39A,H39B,H39C), C40(H40A,H40B,H40C), C41(H41A,H41B,H41C)
;
_atom_sites_solution_hydrogens   mixed
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Dy3 Dy 0.750000 0.76382(5) 0.500000 0.0160(3) Uani 1 2 d S T P . .
Dy1 Dy 0.65909(4) 0.62178(4) 0.42585(4) 0.0155(2) Uani 1 1 d . . . . .
Dy2 Dy 0.70198(5) 0.52170(4) 0.56702(4) 0.0165(2) Uani 1 1 d . . . . .
O8 O 0.8345(8) 0.8209(6) 0.5212(7) 0.024(3) Uani 1 1 d . . . . .
O4 O 0.7049(8) 0.7086(6) 0.4046(7) 0.021(3) Uani 1 1 d . . . . .
O2 O 0.6123(7) 0.5503(6) 0.4799(7) 0.020(3) Uani 1 1 d . . . . .
O3 O 0.7050(7) 0.4611(6) 0.6489(7) 0.024(3) Uani 1 1 d . . . . .
O1 O 0.750000 0.5857(8) 0.500000 0.014(4) Uani 1 2 d S T P . .
O11 O 0.7061(7) 0.5613(7) 0.3656(7) 0.027(4) Uani 1 1 d . . . . .
H11 H 0.700239 0.545189 0.329062 0.040 Uiso 1 1 d R . . . .
O5 O 0.8407(7) 0.6909(6) 0.4796(7) 0.020(3) Uani 1 1 d . . . . .
O7 O 0.9317(8) 0.7381(7) 0.4678(9) 0.030(4) Uani 1 1 d . . . . .
O6 O 0.9374(8) 0.6770(7) 0.5508(8) 0.028(3) Uani 1 1 d . . . . .
O9 O 0.750000 0.4693(9) 0.500000 0.025(4) Uani 1 2 d S TU P . .
O10 O 0.6449(8) 0.5928(6) 0.6202(7) 0.026(3) Uani 1 1 d . . . . .
H10 H 0.604546 0.595287 0.617798 0.038 Uiso 1 1 d R . . . .
N6 N 0.7686(9) 0.8005(7) 0.3905(9) 0.021(3) Uani 1 1 d . . . . .
N7 N 0.7239(9) 0.7800(8) 0.3330(8) 0.021(3) Uani 1 1 d . . . . .
H7 H 0.717523 0.796311 0.293125 0.025 Uiso 0.5 1 calc R . . . .
N4 N 0.6111(8) 0.6646(7) 0.3136(8) 0.019(3) Uani 1 1 d . . . . .
N3 N 0.5558(8) 0.5746(8) 0.3583(8) 0.019(3) Uani 1 1 d . . . . .
N1 N 0.5602(8) 0.4635(8) 0.4731(8) 0.019(3) Uani 1 1 d . . . . .
N2 N 0.6051(9) 0.4540(7) 0.5364(8) 0.020(3) Uani 1 1 d . . . . .
N5 N 0.9051(8) 0.7035(7) 0.4991(9) 0.017(3) Uani 1 1 d . . . . .
C26 C 1.0001(15) 0.9128(15) 0.6535(17) 0.056(9) Uani 1 1 d . . . . .
H26A H 0.993751 0.952767 0.641638 0.083 Uiso 1 1 calc GR . . . .
H26B H 1.041347 0.898905 0.640649 0.083 Uiso 1 1 calc GR . . . .
H26C H 1.004080 0.908227 0.702292 0.083 Uiso 1 1 calc GR . . . .
C27 C 0.9555(12) 0.8172(11) 0.6342(13) 0.035(5) Uani 1 1 d . . . . .
H27A H 0.958539 0.811436 0.682633 0.053 Uiso 1 1 calc GR . . . .
H27B H 0.998595 0.806791 0.622403 0.053 Uiso 1 1 calc GR . . . .
H27C H 0.919238 0.793505 0.608740 0.053 Uiso 1 1 calc GR . . . .
C28 C 0.8753(13) 0.8964(11) 0.6444(13) 0.036(6) Uani 1 1 d . . . . .
H28A H 0.837004 0.872746 0.623031 0.054 Uiso 1 1 calc GR . . . .
H28B H 0.864453 0.936115 0.634100 0.054 Uiso 1 1 calc GR . . . .
H28C H 0.884236 0.890709 0.693375 0.054 Uiso 1 1 calc GR . . . .
C25 C 0.9400(12) 0.8794(11) 0.6166(12) 0.031(5) Uani 1 1 d . . . . .
C24 C 0.9220(12) 0.8867(10) 0.5397(11) 0.028(5) Uani 1 1 d . U . . .
C23 C 0.9623(15) 0.9274(11) 0.5090(13) 0.042(7) Uani 1 1 d . . . . .
H23 H 0.998012 0.947034 0.537746 0.050 Uiso 1 1 calc R . . . .
C22 C 0.9511(17) 0.9378(11) 0.4442(16) 0.049(8) Uani 1 1 d . . . . .
H22 H 0.979289 0.963544 0.426966 0.058 Uiso 1 1 calc R . . . .
C21 C 0.8961(15) 0.9102(11) 0.3986(14) 0.038(6) Uani 1 1 d . . . . .
H21 H 0.886378 0.918913 0.351847 0.045 Uiso 1 1 calc R . . . .
C19 C 0.8568(12) 0.8698(8) 0.4257(11) 0.024(4) Uani 1 1 d . . . . .
C18 C 0.8682(12) 0.8547(10) 0.4940(12) 0.029(5) Uani 1 1 d . U . . .
C20 C 0.8062(12) 0.8413(9) 0.3783(11) 0.026(5) Uani 1 1 d . . . . .
H20 H 0.799495 0.853721 0.332842 0.031 Uiso 1 1 calc R . . . .
C17 C 0.6932(10) 0.7341(7) 0.3452(10) 0.017(4) Uani 1 1 d . . . . .
C16 C 0.6431(9) 0.7130(8) 0.2925(9) 0.016(3) Uani 1 1 d . U . . .
C29 C 0.6188(12) 0.7336(9) 0.2279(11) 0.027(5) Uani 1 1 d . . . . .
H29 H 0.640819 0.764831 0.212372 0.032 Uiso 1 1 calc R . . . .
C30 C 0.5625(12) 0.7094(10) 0.1848(12) 0.028(5) Uani 1 1 d . . . . .
H30 H 0.547767 0.723502 0.140279 0.033 Uiso 1 1 calc R . . . .
C31 C 0.5279(9) 0.6643(8) 0.2078(9) 0.015(3) Uani 1 1 d . U . . .
C15 C 0.5569(10) 0.6418(9) 0.2717(10) 0.022(4) Uani 1 1 d . . . . .
C32 C 0.4700(12) 0.6371(11) 0.1678(11) 0.033(5) Uani 1 1 d . . . . .
H32 H 0.451198 0.651314 0.124070 0.039 Uiso 1 1 calc R . . . .
C33 C 0.4413(12) 0.5910(11) 0.1912(11) 0.031(5) Uani 1 1 d . . . . .
H33 H 0.401827 0.574695 0.164377 0.037 Uiso 1 1 calc R . . . .
C34 C 0.4700(12) 0.5668(11) 0.2562(11) 0.029(5) Uani 1 1 d . . . . .
C14 C 0.5273(10) 0.5939(8) 0.2961(10) 0.019(4) Uani 1 1 d . . . . .
C35 C 0.4449(12) 0.5187(10) 0.2816(10) 0.027(5) Uani 1 1 d . . . . .
H35 H 0.407779 0.498797 0.255373 0.032 Uiso 1 1 calc R . . . .
C36 C 0.4748(10) 0.5002(9) 0.3455(10) 0.020(4) Uani 1 1 d . . . . .
H36 H 0.456671 0.468640 0.364717 0.024 Uiso 1 1 calc R . . . .
C13 C 0.5318(9) 0.5282(7) 0.3816(8) 0.011(3) Uani 1 1 d . U . . .
C1 C 0.5698(10) 0.5114(9) 0.4498(9) 0.019(4) Uani 1 1 d . . . . .
C2 C 0.5916(10) 0.4070(9) 0.5633(11) 0.022(4) Uani 1 1 d . . . . .
H2 H 0.554755 0.385383 0.539569 0.026 Uiso 1 1 calc R . . . .
C3 C 0.6286(11) 0.3849(11) 0.6271(12) 0.029(5) Uani 1 1 d . . . . .
C8 C 0.6031(12) 0.3333(9) 0.6473(11) 0.026(5) Uani 1 1 d . . . . .
H8 H 0.565449 0.315031 0.619725 0.031 Uiso 1 1 calc R . . . .
C7 C 0.6355(15) 0.3102(10) 0.7092(12) 0.037(6) Uani 1 1 d . . . . .
H7A H 0.620109 0.275240 0.723458 0.045 Uiso 1 1 calc R . . . .
C6 C 0.6889(13) 0.3372(13) 0.7494(14) 0.041(6) Uani 1 1 d . . . . .
H6 H 0.709577 0.320179 0.790972 0.049 Uiso 1 1 calc R . . . .
C5 C 0.7143(12) 0.3890(11) 0.7319(12) 0.031(5) Uani 1 1 d . . . . .
C4 C 0.6825(10) 0.4117(9) 0.6684(10) 0.022(4) Uani 1 1 d . . . . .
C9 C 0.7738(13) 0.4187(13) 0.7779(12) 0.039(6) Uani 1 1 d . . . . .
C10 C 0.8306(14) 0.4240(15) 0.7394(15) 0.053(9) Uani 1 1 d . . . . .
H10A H 0.848640 0.386392 0.733020 0.079 Uiso 1 1 calc GR . . . .
H10B H 0.866759 0.447621 0.765009 0.079 Uiso 1 1 calc GR . . . .
H10C H 0.813140 0.441223 0.695260 0.079 Uiso 1 1 calc GR . . . .
C11 C 0.7533(15) 0.4749(13) 0.8005(13) 0.046(7) Uani 1 1 d . . . . .
H11A H 0.790743 0.490959 0.833768 0.069 Uiso 1 1 calc GR . . . .
H11B H 0.713682 0.470357 0.821005 0.069 Uiso 1 1 calc GR . . . .
H11C H 0.742006 0.500293 0.761609 0.069 Uiso 1 1 calc GR . . . .
C12 C 0.8010(16) 0.3841(16) 0.8426(13) 0.055(9) Uani 1 1 d . . . . .
H12A H 0.817829 0.347637 0.830332 0.082 Uiso 1 1 calc GR . . . .
H12B H 0.764506 0.378006 0.867070 0.082 Uiso 1 1 calc GR . . . .
H12C H 0.837978 0.404902 0.871459 0.082 Uiso 1 1 calc GR . . . .
C37 C 0.750000 0.4075(15) 0.500000 0.040(8) Uani 1 2 d S TU P . .
H37A H 0.775690 0.394075 0.542270 0.048 Uiso 0.5 1 d R . . . .
H37B H 0.769990 0.394075 0.463900 0.048 Uiso 0.5 1 d R . . . .
H37C H 0.704320 0.394075 0.493830 0.048 Uiso 0.5 1 d R . . . .
C38 C 0.6807(19) 0.6271(12) 0.6769(13) 0.051(8) Uani 1 1 d . . . . .
H38A H 0.710152 0.602801 0.709489 0.077 Uiso 1 1 calc GR . . . .
H38B H 0.647729 0.645786 0.698876 0.077 Uiso 1 1 calc GR . . . .
H38C H 0.708175 0.655701 0.660001 0.077 Uiso 1 1 calc GR . . . .
N8 N 0.676(2) 1.0164(14) 0.5434(16) 0.051(7) Uani 0.68(4) 1 d D U . A -1
C42 C 0.655(2) 1.0368(17) 0.4914(17) 0.050(6) Uani 0.68(4) 1 d D U . A -1
C43 C 0.681(3) 1.087(2) 0.462(2) 0.046(7) Uani 0.68(4) 1 d D U . A -1
H43A H 0.654859 1.093721 0.416274 0.069 Uiso 0.68(4) 1 calc GR . . A -1
H43B H 0.728919 1.080795 0.459647 0.069 Uiso 0.68(4) 1 calc GR . . A -1
H43C H 0.678211 1.120211 0.490087 0.069 Uiso 0.68(4) 1 calc GR . . A -1
O12 O 0.5186(9) 0.6264(8) 0.5833(9) 0.035(4) Uani 1 1 d . . . . .
H12 H 0.517799 0.646733 0.544638 0.052 Uiso 1 1 d R . . . .
C39 C 0.4798(19) 0.6534(16) 0.6241(19) 0.064(9) Uani 1 1 d . . . . .
H39A H 0.509190 0.677425 0.657162 0.095 Uiso 1 1 calc GR . . . .
H39B H 0.458126 0.625014 0.647768 0.095 Uiso 1 1 calc GR . . . .
H39C H 0.444969 0.676693 0.595845 0.095 Uiso 1 1 calc GR . . . .
O13 O 0.8013(19) 0.2788(14) 0.5532(17) 0.068(8) Uani 0.75 1 d . U . . .
H13 H 0.837179 0.261881 0.553919 0.101 Uiso 0.75 1 d R . . . .
C40 C 0.785(3) 0.2830(18) 0.613(2) 0.056(8) Uani 0.75 1 d . U . . .
H40A H 0.763500 0.319638 0.616786 0.085 Uiso 0.75 1 calc GR . . . .
H40B H 0.825818 0.279664 0.648539 0.085 Uiso 0.75 1 calc GR . . . .
H40C H 0.753267 0.252710 0.618207 0.085 Uiso 0.75 1 calc GR . . . .
O14 O 0.3661(14) 0.8102(11) 0.5270(14) 0.070(7) Uani 1 1 d . . . . .
H14 H 0.346097 0.840293 0.518819 0.105 Uiso 1 1 d R . . . .
C41 C 0.4099(18) 0.803(2) 0.4862(18) 0.082(15) Uani 1 1 d . . . . .
H41A H 0.386962 0.784290 0.444597 0.123 Uiso 1 1 calc GR . . . .
H41B H 0.447833 0.779694 0.508933 0.123 Uiso 1 1 calc GR . . . .
H41C H 0.426799 0.839876 0.475213 0.123 Uiso 1 1 calc GR . . . .
N8A N 0.691(4) 1.084(4) 0.476(5) 0.046(8) Uani 0.32(4) 1 d D U . A -2
C42A C 0.646(4) 1.054(3) 0.463(5) 0.051(7) Uani 0.32(4) 1 d D U . A -2
C43A C 0.579(4) 1.061(5) 0.418(5) 0.061(12) Uani 0.32(4) 1 d D U . A -2
H43D H 0.583112 1.059598 0.370385 0.091 Uiso 0.32(4) 1 d R . . A -2
H43E H 0.560162 1.097928 0.426755 0.091 Uiso 0.32(4) 1 d R . . A -2
H43F H 0.548402 1.031128 0.426405 0.091 Uiso 0.32(4) 1 d R . . A -2


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Dy3 Dy1 3.9772(14) . ?
Dy3 Dy1 3.9772(14) 2_656 ?
Dy3 O8 2.150(15) . ?
Dy3 O8 2.150(15) 2_656 ?
Dy3 O4 2.357(14) . ?
Dy3 O4 2.357(14) 2_656 ?
Dy3 O5 2.611(14) 2_656 ?
Dy3 O5 2.611(14) . ?
Dy3 N6 2.482(17) . ?
Dy3 N6 2.481(17) 2_656 ?
Dy1 Dy2 3.6536(12) 2_656 ?
Dy1 Dy2 3.6783(13) . ?
Dy1 O4 2.331(14) . ?
Dy1 O2 2.320(14) . ?
Dy1 O1 2.285(7) . ?
Dy1 O11 2.219(14) . ?
Dy1 O5 2.519(13) 2_656 ?
Dy1 O6 2.473(16) 2_656 ?
Dy1 N4 2.496(17) . ?
Dy1 N3 2.510(17) . ?
Dy1 N5 2.924(16) 2_656 ?
Dy2 Dy2 3.6470(18) 2_656 ?
Dy2 O2 2.354(14) . ?
Dy2 O3 2.186(15) . ?
Dy2 O1 2.372(12) . ?
Dy2 O11 2.268(14) 2_656 ?
Dy2 O9 2.206(12) . ?
Dy2 O10 2.416(15) . ?
Dy2 N2 2.507(17) . ?
O8 C18 1.25(3) . ?
O4 C17 1.32(2) . ?
O2 C1 1.32(2) . ?
O3 C4 1.34(3) . ?
O11 H11 0.8189 . ?
O5 N5 1.31(2) . ?
O7 N5 1.23(2) . ?
O6 N5 1.28(2) . ?
O9 C37 1.46(4) . ?
O10 H10 0.8078 . ?
O10 C38 1.47(3) . ?
N6 N7 1.41(2) . ?
N6 C20 1.28(3) . ?
N7 H7 0.8800 . ?
N7 C17 1.30(3) . ?
N4 C16 1.42(3) . ?
N4 C15 1.35(3) . ?
N3 C14 1.35(2) . ?
N3 C13 1.33(2) . ?
N1 N2 1.43(2) . ?
N1 C1 1.26(3) . ?
N2 C2 1.29(3) . ?
C26 H26A 0.9800 . ?
C26 H26B 0.9800 . ?
C26 H26C 0.9800 . ?
C26 C25 1.51(3) . ?
C27 H27A 0.9800 . ?
C27 H27B 0.9800 . ?
C27 H27C 0.9800 . ?
C27 C25 1.54(4) . ?
C28 H28A 0.9800 . ?
C28 H28B 0.9800 . ?
C28 H28C 0.9800 . ?
C28 C25 1.58(3) . ?
C25 C24 1.53(3) . ?
C24 C23 1.48(3) . ?
C24 C18 1.48(3) . ?
C23 H23 0.9500 . ?
C23 C22 1.31(4) . ?
C22 H22 0.9500 . ?
C22 C21 1.44(4) . ?
C21 H21 0.9500 . ?
C21 C19 1.43(3) . ?
C19 C18 1.40(3) . ?
C19 C20 1.42(3) . ?
C20 H20 0.9500 . ?
C17 C16 1.40(3) . ?
C16 C29 1.39(3) . ?
C29 H29 0.9500 . ?
C29 C30 1.40(3) . ?
C30 H30 0.9500 . ?
C30 C31 1.41(3) . ?
C31 C15 1.41(3) . ?
C31 C32 1.43(3) . ?
C15 C14 1.42(3) . ?
C32 H32 0.9500 . ?
C32 C33 1.37(3) . ?
C33 H33 0.9500 . ?
C33 C34 1.44(3) . ?
C34 C14 1.42(3) . ?
C34 C35 1.39(3) . ?
C35 H35 0.9500 . ?
C35 C36 1.38(3) . ?
C36 H36 0.9500 . ?
C36 C13 1.40(3) . ?
C13 C1 1.49(2) . ?
C2 H2 0.9500 . ?
C2 C3 1.45(3) . ?
C3 C8 1.42(3) . ?
C3 C4 1.38(3) . ?
C8 H8 0.9500 . ?
C8 C7 1.40(3) . ?
C7 H7A 0.9500 . ?
C7 C6 1.37(4) . ?
C6 H6 0.9500 . ?
C6 C5 1.40(4) . ?
C5 C4 1.42(3) . ?
C5 C9 1.53(3) . ?
C9 C10 1.52(4) . ?
C9 C11 1.49(4) . ?
C9 C12 1.55(3) . ?
C10 H10A 0.9800 . ?
C10 H10B 0.9800 . ?
C10 H10C 0.9800 . ?
C11 H11A 0.9800 . ?
C11 H11B 0.9800 . ?
C11 H11C 0.9800 . ?
C12 H12A 0.9800 . ?
C12 H12B 0.9800 . ?
C12 H12C 0.9800 . ?
C37 H37A 0.9595 . ?
C37 H37B 0.9595 . ?
C37 H37C 0.9594 . ?
C38 H38A 0.9800 . ?
C38 H38B 0.9800 . ?
C38 H38C 0.9800 . ?
N8 C42 1.159(10) . ?
C42 C43 1.485(10) . ?
C43 H43A 0.9800 . ?
C43 H43B 0.9800 . ?
C43 H43C 0.9800 . ?
O12 H12 0.9173 . ?
O12 C39 1.41(3) . ?
C39 H39A 0.9800 . ?
C39 H39B 0.9800 . ?
C39 H39C 0.9800 . ?
O13 H13 0.8260 . ?
O13 C40 1.33(5) . ?
C40 H40A 0.9800 . ?
C40 H40B 0.9800 . ?
C40 H40C 0.9800 . ?
O14 H14 0.8200 . ?
O14 C41 1.34(4) . ?
C41 H41A 0.9800 . ?
C41 H41B 0.9800 . ?
C41 H41C 0.9800 . ?
N8A C42A 1.150(10) . ?
C42A C43A 1.48(2) . ?
C43A H43D 0.9800 . ?
C43A H43E 0.9800 . ?
C43A H43F 0.9801 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Dy1 Dy3 Dy1 64.39(3) . 2_656 ?
O8 Dy3 Dy1 99.9(4) 2_656 . ?
O8 Dy3 Dy1 153.3(4) . . ?
O8 Dy3 Dy1 153.3(4) 2_656 2_656 ?
O8 Dy3 Dy1 99.9(4) . 2_656 ?
O8 Dy3 O8 102.0(9) . 2_656 ?
O8 Dy3 O4 132.1(5) . . ?
O8 Dy3 O4 91.7(5) 2_656 . ?
O8 Dy3 O4 91.7(5) . 2_656 ?
O8 Dy3 O4 132.1(5) 2_656 2_656 ?
O8 Dy3 O5 159.7(5) . 2_656 ?
O8 Dy3 O5 83.9(5) . . ?
O8 Dy3 O5 159.7(5) 2_656 . ?
O8 Dy3 O5 83.9(5) 2_656 2_656 ?
O8 Dy3 N6 72.4(6) 2_656 2_656 ?
O8 Dy3 N6 82.0(6) . 2_656 ?
O8 Dy3 N6 72.4(6) . . ?
O8 Dy3 N6 82.0(6) 2_656 . ?
O4 Dy3 Dy1 84.8(3) . 2_656 ?
O4 Dy3 Dy1 31.8(3) . . ?
O4 Dy3 Dy1 31.8(3) 2_656 2_656 ?
O4 Dy3 Dy1 84.8(4) 2_656 . ?
O4 Dy3 O4 112.5(7) . 2_656 ?
O4 Dy3 O5 70.6(5) . . ?
O4 Dy3 O5 70.6(5) 2_656 2_656 ?
O4 Dy3 O5 66.2(5) 2_656 . ?
O4 Dy3 O5 66.2(5) . 2_656 ?
O4 Dy3 N6 145.4(5) 2_656 . ?
O4 Dy3 N6 64.3(5) . . ?
O4 Dy3 N6 64.3(5) 2_656 2_656 ?
O4 Dy3 N6 145.4(5) . 2_656 ?
O5 Dy3 Dy1 70.4(3) 2_656 2_656 ?
O5 Dy3 Dy1 38.3(3) . 2_656 ?
O5 Dy3 Dy1 70.4(3) . . ?
O5 Dy3 Dy1 38.3(3) 2_656 . ?
O5 Dy3 O5 97.2(6) 2_656 . ?
N6 Dy3 Dy1 95.9(4) . . ?
N6 Dy3 Dy1 119.4(4) . 2_656 ?
N6 Dy3 Dy1 119.4(4) 2_656 . ?
N6 Dy3 Dy1 95.9(4) 2_656 2_656 ?
N6 Dy3 O5 81.4(5) . . ?
N6 Dy3 O5 81.4(5) 2_656 2_656 ?
N6 Dy3 O5 127.8(5) 2_656 . ?
N6 Dy3 O5 127.8(5) . 2_656 ?
N6 Dy3 N6 139.0(8) 2_656 . ?
Dy2 Dy1 Dy3 104.09(3) 2_656 . ?
Dy2 Dy1 Dy3 103.63(3) . . ?
Dy2 Dy1 Dy2 59.66(3) 2_656 . ?
O4 Dy1 Dy3 32.2(3) . . ?
O4 Dy1 Dy2 104.4(4) . 2_656 ?
O4 Dy1 Dy2 132.4(3) . . ?
O4 Dy1 O5 68.2(5) . 2_656 ?
O4 Dy1 O6 85.8(5) . 2_656 ?
O4 Dy1 N4 64.4(5) . . ?
O4 Dy1 N3 127.5(5) . . ?
O4 Dy1 N5 75.4(5) . 2_656 ?
O2 Dy1 Dy3 129.8(3) . . ?
O2 Dy1 Dy2 83.8(4) . 2_656 ?
O2 Dy1 Dy2 38.4(3) . . ?
O2 Dy1 O4 161.2(5) . . ?
O2 Dy1 O5 93.1(5) . 2_656 ?
O2 Dy1 O6 83.2(5) . 2_656 ?
O2 Dy1 N4 127.4(5) . . ?
O2 Dy1 N3 63.8(5) . . ?
O2 Dy1 N5 88.3(5) . 2_656 ?
O1 Dy1 Dy3 79.8(4) . . ?
O1 Dy1 Dy2 39.2(3) . 2_656 ?
O1 Dy1 Dy2 38.7(3) . . ?
O1 Dy1 O4 99.0(5) . . ?
O1 Dy1 O2 76.5(4) . . ?
O1 Dy1 O5 82.4(5) . 2_656 ?
O1 Dy1 O6 129.1(4) . 2_656 ?
O1 Dy1 N4 149.2(4) . . ?
O1 Dy1 N3 131.0(6) . . ?
O1 Dy1 N5 106.8(4) . 2_656 ?
O11 Dy1 Dy3 122.5(4) . . ?
O11 Dy1 Dy2 35.9(4) . 2_656 ?
O11 Dy1 Dy2 87.3(4) . . ?
O11 Dy1 O4 103.7(6) . . ?
O11 Dy1 O2 92.9(6) . . ?
O11 Dy1 O1 75.1(4) . . ?
O11 Dy1 O5 154.7(5) . 2_656 ?
O11 Dy1 O6 153.0(5) . 2_656 ?
O11 Dy1 N4 83.7(5) . . ?
O11 Dy1 N3 79.3(6) . . ?
O11 Dy1 N5 178.0(5) . 2_656 ?
O5 Dy1 Dy3 40.0(3) 2_656 . ?
O5 Dy1 Dy2 82.3(3) 2_656 . ?
O5 Dy1 Dy2 120.7(3) 2_656 2_656 ?
O5 Dy1 N5 26.6(4) 2_656 2_656 ?
O6 Dy1 Dy3 78.5(4) 2_656 . ?
O6 Dy1 Dy2 164.8(4) 2_656 2_656 ?
O6 Dy1 Dy2 105.1(4) 2_656 . ?
O6 Dy1 O5 52.3(5) 2_656 2_656 ?
O6 Dy1 N4 77.7(5) 2_656 . ?
O6 Dy1 N3 75.0(5) 2_656 . ?
O6 Dy1 N5 25.7(5) 2_656 2_656 ?
N4 Dy1 Dy3 93.6(4) . . ?
N4 Dy1 Dy2 162.8(4) . . ?
N4 Dy1 Dy2 116.8(4) . 2_656 ?
N4 Dy1 O5 111.6(5) . 2_656 ?
N4 Dy1 N3 64.0(5) . . ?
N4 Dy1 N5 94.3(5) . 2_656 ?
N3 Dy1 Dy3 148.2(4) . . ?
N3 Dy1 Dy2 106.1(4) . 2_656 ?
N3 Dy1 Dy2 99.9(4) . . ?
N3 Dy1 O5 125.1(5) . 2_656 ?
N3 Dy1 N5 99.8(5) . 2_656 ?
N5 Dy1 Dy3 57.5(3) 2_656 . ?
N5 Dy1 Dy2 94.7(3) 2_656 . ?
N5 Dy1 Dy2 145.9(3) 2_656 2_656 ?
Dy1 Dy2 Dy1 70.62(3) 2_656 . ?
Dy2 Dy2 Dy1 60.51(2) 2_656 2_656 ?
Dy2 Dy2 Dy1 59.83(2) 2_656 . ?
O2 Dy2 Dy1 108.0(3) . 2_656 ?
O2 Dy2 Dy1 37.8(3) . . ?
O2 Dy2 Dy2 83.5(3) . 2_656 ?
O2 Dy2 O1 74.3(3) . . ?
O2 Dy2 O10 76.7(5) . . ?
O2 Dy2 N2 63.8(5) . . ?
O3 Dy2 Dy1 119.7(4) . 2_656 ?
O3 Dy2 Dy1 168.2(4) . . ?
O3 Dy2 Dy2 129.0(4) . 2_656 ?
O3 Dy2 O2 130.9(5) . . ?
O3 Dy2 O1 154.7(4) . . ?
O3 Dy2 O11 85.6(5) . 2_656 ?
O3 Dy2 O9 98.6(6) . . ?
O3 Dy2 O10 93.5(5) . . ?
O3 Dy2 N2 70.5(6) . . ?
O1 Dy2 Dy1 37.00(10) . . ?
O1 Dy2 Dy1 37.48(10) . 2_656 ?
O1 Dy2 Dy2 39.7(3) . 2_656 ?
O1 Dy2 O10 95.6(5) . . ?
O1 Dy2 N2 131.1(4) . . ?
O11 Dy2 Dy1 35.0(3) 2_656 2_656 ?
O11 Dy2 Dy1 103.5(4) 2_656 . ?
O11 Dy2 Dy2 87.3(4) 2_656 2_656 ?
O11 Dy2 O2 137.7(5) 2_656 . ?
O11 Dy2 O1 72.5(4) 2_656 . ?
O11 Dy2 O10 81.4(6) 2_656 . ?
O11 Dy2 N2 156.0(5) 2_656 . ?
O9 Dy2 Dy1 87.0(4) . . ?
O9 Dy2 Dy1 87.6(4) . 2_656 ?
O9 Dy2 Dy2 34.2(5) . 2_656 ?
O9 Dy2 O2 93.9(4) . . ?
O9 Dy2 O1 74.0(6) . . ?
O9 Dy2 O11 101.2(5) . 2_656 ?
O9 Dy2 O10 167.7(5) . . ?
O9 Dy2 N2 84.7(5) . . ?
O10 Dy2 Dy1 80.8(4) . . ?
O10 Dy2 Dy1 87.9(4) . 2_656 ?
O10 Dy2 Dy2 135.0(4) . 2_656 ?
O10 Dy2 N2 97.8(6) . . ?
N2 Dy2 Dy1 168.2(4) . 2_656 ?
N2 Dy2 Dy1 100.0(4) . . ?
N2 Dy2 Dy2 108.9(4) . 2_656 ?
C18 O8 Dy3 142.8(15) . . ?
Dy1 O4 Dy3 116.1(6) . . ?
C17 O4 Dy3 117.2(12) . . ?
C17 O4 Dy1 124.6(12) . . ?
Dy1 O2 Dy2 103.8(5) . . ?
C1 O2 Dy1 125.6(12) . . ?
C1 O2 Dy2 118.1(12) . . ?
C4 O3 Dy2 146.8(13) . . ?
Dy1 O1 Dy1 136.1(8) . 2_656 ?
Dy1 O1 Dy2 104.34(16) . . ?
Dy1 O1 Dy2 103.35(16) 2_656 . ?
Dy1 O1 Dy2 104.34(16) 2_656 2_656 ?
Dy1 O1 Dy2 103.35(16) . 2_656 ?
Dy2 O1 Dy2 100.5(7) 2_656 . ?
Dy1 O11 Dy2 109.0(6) . 2_656 ?
Dy1 O11 H11 143.0 . . ?
Dy2 O11 H11 107.4 2_656 . ?
Dy1 O5 Dy3 101.6(5) 2_656 . ?
N5 O5 Dy3 119.1(11) . . ?
N5 O5 Dy1 94.2(10) . 2_656 ?
N5 O6 Dy1 97.3(11) . 2_656 ?
Dy2 O9 Dy2 111.5(10) 2_656 . ?
C37 O9 Dy2 124.2(5) . 2_656 ?
C37 O9 Dy2 124.2(5) . . ?
Dy2 O10 H10 126.3 . . ?
C38 O10 Dy2 122.0(18) . . ?
C38 O10 H10 109.5 . . ?
N7 N6 Dy3 115.5(12) . . ?
C20 N6 Dy3 129.8(15) . . ?
C20 N6 N7 113.9(18) . . ?
N6 N7 H7 123.8 . . ?
C17 N7 N6 112.4(17) . . ?
C17 N7 H7 123.8 . . ?
C16 N4 Dy1 119.0(12) . . ?
C15 N4 Dy1 121.4(13) . . ?
C15 N4 C16 119.5(17) . . ?
C14 N3 Dy1 120.2(13) . . ?
C13 N3 Dy1 119.9(12) . . ?
C13 N3 C14 119.7(17) . . ?
C1 N1 N2 111.1(16) . . ?
N1 N2 Dy2 116.2(11) . . ?
C2 N2 Dy2 131.8(14) . . ?
C2 N2 N1 111.4(17) . . ?
O5 N5 Dy1 59.2(8) . 2_656 ?
O7 N5 Dy1 179.5(14) . 2_656 ?
O7 N5 O5 120.6(16) . . ?
O7 N5 O6 123.2(17) . . ?
O6 N5 Dy1 57.0(9) . 2_656 ?
O6 N5 O5 116.2(15) . . ?
H26A C26 H26B 109.5 . . ?
H26A C26 H26C 109.5 . . ?
H26B C26 H26C 109.5 . . ?
C25 C26 H26A 109.5 . . ?
C25 C26 H26B 109.5 . . ?
C25 C26 H26C 109.5 . . ?
H27A C27 H27B 109.5 . . ?
H27A C27 H27C 109.5 . . ?
H27B C27 H27C 109.5 . . ?
C25 C27 H27A 109.5 . . ?
C25 C27 H27B 109.5 . . ?
C25 C27 H27C 109.5 . . ?
H28A C28 H28B 109.5 . . ?
H28A C28 H28C 109.5 . . ?
H28B C28 H28C 109.5 . . ?
C25 C28 H28A 109.5 . . ?
C25 C28 H28B 109.5 . . ?
C25 C28 H28C 109.5 . . ?
C26 C25 C27 106(2) . . ?
C26 C25 C28 109(2) . . ?
C26 C25 C24 116(2) . . ?
C27 C25 C28 108(2) . . ?
C24 C25 C27 109.8(19) . . ?
C24 C25 C28 107(2) . . ?
C23 C24 C25 118(2) . . ?
C23 C24 C18 118(2) . . ?
C18 C24 C25 124(2) . . ?
C24 C23 H23 118.4 . . ?
C22 C23 C24 123(2) . . ?
C22 C23 H23 118.4 . . ?
C23 C22 H22 119.7 . . ?
C23 C22 C21 121(2) . . ?
C21 C22 H22 119.7 . . ?
C22 C21 H21 120.9 . . ?
C19 C21 C22 118(2) . . ?
C19 C21 H21 120.9 . . ?
C18 C19 C21 124(2) . . ?
C18 C19 C20 119.7(19) . . ?
C20 C19 C21 116(2) . . ?
O8 C18 C24 117(2) . . ?
O8 C18 C19 127(2) . . ?
C19 C18 C24 116(2) . . ?
N6 C20 C19 127(2) . . ?
N6 C20 H20 116.6 . . ?
C19 C20 H20 116.6 . . ?
O4 C17 C16 119.5(17) . . ?
N7 C17 O4 123.5(18) . . ?
N7 C17 C16 116.9(18) . . ?
C17 C16 N4 111.2(16) . . ?
C29 C16 N4 118.1(18) . . ?
C29 C16 C17 131(2) . . ?
C16 C29 H29 119.1 . . ?
C16 C29 C30 122(2) . . ?
C30 C29 H29 119.1 . . ?
C29 C30 H30 120.1 . . ?
C29 C30 C31 120(2) . . ?
C31 C30 H30 120.1 . . ?
C30 C31 C15 116.7(19) . . ?
C30 C31 C32 123.9(18) . . ?
C15 C31 C32 119.1(18) . . ?
N4 C15 C31 124(2) . . ?
N4 C15 C14 116.5(18) . . ?
C31 C15 C14 119.7(19) . . ?
C31 C32 H32 119.4 . . ?
C33 C32 C31 121(2) . . ?
C33 C32 H32 119.4 . . ?
C32 C33 H33 119.5 . . ?
C32 C33 C34 121(2) . . ?
C34 C33 H33 119.5 . . ?
C14 C34 C33 118(2) . . ?
C35 C34 C33 124(2) . . ?
C35 C34 C14 118(2) . . ?
N3 C14 C15 117.8(18) . . ?
N3 C14 C34 121.2(19) . . ?
C34 C14 C15 121.0(19) . . ?
C34 C35 H35 120.5 . . ?
C36 C35 C34 119(2) . . ?
C36 C35 H35 120.5 . . ?
C35 C36 H36 120.3 . . ?
C35 C36 C13 119(2) . . ?
C13 C36 H36 120.3 . . ?
N3 C13 C36 121.9(16) . . ?
N3 C13 C1 113.4(16) . . ?
C36 C13 C1 124.7(17) . . ?
O2 C1 C13 113.7(17) . . ?
N1 C1 O2 126.3(18) . . ?
N1 C1 C13 120.0(18) . . ?
N2 C2 H2 117.5 . . ?
N2 C2 C3 125(2) . . ?
C3 C2 H2 117.5 . . ?
C8 C3 C2 115(2) . . ?
C4 C3 C2 125(2) . . ?
C4 C3 C8 121(2) . . ?
C3 C8 H8 121.1 . . ?
C7 C8 C3 118(2) . . ?
C7 C8 H8 121.1 . . ?
C8 C7 H7A 119.5 . . ?
C6 C7 C8 121(2) . . ?
C6 C7 H7A 119.5 . . ?
C7 C6 H6 118.6 . . ?
C7 C6 C5 123(2) . . ?
C5 C6 H6 118.6 . . ?
C6 C5 C4 116(2) . . ?
C6 C5 C9 122(2) . . ?
C4 C5 C9 122(2) . . ?
O3 C4 C3 119.6(19) . . ?
O3 C4 C5 118.6(19) . . ?
C3 C4 C5 122(2) . . ?
C5 C9 C12 112(2) . . ?
C10 C9 C5 108(2) . . ?
C10 C9 C12 108(2) . . ?
C11 C9 C5 111(2) . . ?
C11 C9 C10 112(2) . . ?
C11 C9 C12 107(2) . . ?
C9 C10 H10A 109.5 . . ?
C9 C10 H10B 109.5 . . ?
C9 C10 H10C 109.5 . . ?
H10A C10 H10B 109.5 . . ?
H10A C10 H10C 109.5 . . ?
H10B C10 H10C 109.5 . . ?
C9 C11 H11A 109.5 . . ?
C9 C11 H11B 109.5 . . ?
C9 C11 H11C 109.5 . . ?
H11A C11 H11B 109.5 . . ?
H11A C11 H11C 109.5 . . ?
H11B C11 H11C 109.5 . . ?
C9 C12 H12A 109.5 . . ?
C9 C12 H12B 109.5 . . ?
C9 C12 H12C 109.5 . . ?
H12A C12 H12B 109.5 . . ?
H12A C12 H12C 109.5 . . ?
H12B C12 H12C 109.5 . . ?
O9 C37 H37A 109.4 . . ?
O9 C37 H37B 109.4 . . ?
O9 C37 H37C 109.4 . . ?
H37A C37 H37B 109.6 . . ?
H37A C37 H37C 109.6 . . ?
H37B C37 H37C 109.6 . . ?
O10 C38 H38A 109.5 . . ?
O10 C38 H38B 109.5 . . ?
O10 C38 H38C 109.5 . . ?
H38A C38 H38B 109.5 . . ?
H38A C38 H38C 109.5 . . ?
H38B C38 H38C 109.5 . . ?
N8 C42 C43 127(2) . . ?
C42 C43 H43A 109.5 . . ?
C42 C43 H43B 109.5 . . ?
C42 C43 H43C 109.5 . . ?
H43A C43 H43B 109.5 . . ?
H43A C43 H43C 109.5 . . ?
H43B C43 H43C 109.5 . . ?
C39 O12 H12 110.3 . . ?
O12 C39 H39A 109.5 . . ?
O12 C39 H39B 109.5 . . ?
O12 C39 H39C 109.5 . . ?
H39A C39 H39B 109.5 . . ?
H39A C39 H39C 109.5 . . ?
H39B C39 H39C 109.5 . . ?
C40 O13 H13 113.7 . . ?
O13 C40 H40A 109.5 . . ?
O13 C40 H40B 109.5 . . ?
O13 C40 H40C 109.5 . . ?
H40A C40 H40B 109.5 . . ?
H40A C40 H40C 109.5 . . ?
H40B C40 H40C 109.5 . . ?
C41 O14 H14 110.1 . . ?
O14 C41 H41A 109.5 . . ?
O14 C41 H41B 109.5 . . ?
O14 C41 H41C 109.5 . . ?
H41A C41 H41B 109.5 . . ?
H41A C41 H41C 109.5 . . ?
H41B C41 H41C 109.5 . . ?
N8A C42A C43A 131(3) . . ?
C42A C43A H43D 110.7 . . ?
C42A C43A H43E 108.7 . . ?
C42A C43A H43F 109.1 . . ?
H43D C43A H43E 109.5 . . ?
H43D C43A H43F 109.5 . . ?
H43E C43A H43F 109.5 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Dy3 O8 C18 C24 175.7(16) . . . . ?
Dy3 O8 C18 C19 2(4) . . . . ?
Dy3 O4 C17 N7 23(2) . . . . ?
Dy3 O4 C17 C16 -153.6(13) . . . . ?
Dy3 O5 N5 Dy1 105.8(10) . . . 2_656 ?
Dy3 O5 N5 O7 -74(2) . . . . ?
Dy3 O5 N5 O6 107.5(15) . . . . ?
Dy3 N6 N7 C17 -18(2) . . . . ?
Dy3 N6 C20 C19 12(3) . . . . ?
Dy1 O4 C17 N7 -173.6(14) . . . . ?
Dy1 O4 C17 C16 9(2) . . . . ?
Dy1 O2 C1 N1 156.1(16) . . . . ?
Dy1 O2 C1 C13 -23(2) . . . . ?
Dy1 O5 N5 O7 -179.4(16) 2_656 . . . ?
Dy1 O5 N5 O6 1.7(17) 2_656 . . . ?
Dy1 O6 N5 O5 -1.8(17) 2_656 . . . ?
Dy1 O6 N5 O7 179.4(16) 2_656 . . . ?
Dy1 N4 C16 C17 -9(2) . . . . ?
Dy1 N4 C16 C29 175.2(14) . . . . ?
Dy1 N4 C15 C31 180.0(15) . . . . ?
Dy1 N4 C15 C14 2(3) . . . . ?
Dy1 N3 C14 C15 -1(2) . . . . ?
Dy1 N3 C14 C34 178.1(15) . . . . ?
Dy1 N3 C13 C36 -179.4(14) . . . . ?
Dy1 N3 C13 C1 3(2) . . . . ?
Dy2 O2 C1 N1 20(3) . . . . ?
Dy2 O2 C1 C13 -158.8(12) . . . . ?
Dy2 O3 C4 C3 -12(4) . . . . ?
Dy2 O3 C4 C5 169.6(18) . . . . ?
Dy2 N2 C2 C3 8(3) . . . . ?
O4 C17 C16 N4 0(2) . . . . ?
O4 C17 C16 C29 176(2) . . . . ?
N6 N7 C17 O4 -3(3) . . . . ?
N6 N7 C17 C16 174.5(16) . . . . ?
N7 N6 C20 C19 -179(2) . . . . ?
N7 C17 C16 N4 -177.0(16) . . . . ?
N7 C17 C16 C29 -1(3) . . . . ?
N4 C16 C29 C30 3(3) . . . . ?
N4 C15 C14 N3 -1(3) . . . . ?
N4 C15 C14 C34 179.8(19) . . . . ?
N3 C13 C1 O2 11(2) . . . . ?
N3 C13 C1 N1 -167.9(18) . . . . ?
N1 N2 C2 C3 179.1(19) . . . . ?
N2 N1 C1 O2 -4(3) . . . . ?
N2 N1 C1 C13 175.4(16) . . . . ?
N2 C2 C3 C8 178(2) . . . . ?
N2 C2 C3 C4 1(4) . . . . ?
C26 C25 C24 C23 -3(3) . . . . ?
C26 C25 C24 C18 175(2) . . . . ?
C27 C25 C24 C23 -124(2) . . . . ?
C27 C25 C24 C18 54(3) . . . . ?
C28 C25 C24 C23 119(2) . . . . ?
C28 C25 C24 C18 -62(3) . . . . ?
C25 C24 C23 C22 -179(3) . . . . ?
C25 C24 C18 O8 2(3) . . . . ?
C25 C24 C18 C19 176(2) . . . . ?
C24 C23 C22 C21 2(5) . . . . ?
C23 C24 C18 O8 -179(2) . . . . ?
C23 C24 C18 C19 -5(3) . . . . ?
C23 C22 C21 C19 -3(4) . . . . ?
C22 C21 C19 C18 0(4) . . . . ?
C22 C21 C19 C20 -176(2) . . . . ?
C21 C19 C18 O8 178(2) . . . . ?
C21 C19 C18 C24 4(3) . . . . ?
C21 C19 C20 N6 174(2) . . . . ?
C18 C24 C23 C22 3(4) . . . . ?
C18 C19 C20 N6 -2(4) . . . . ?
C20 N6 N7 C17 171.3(18) . . . . ?
C20 C19 C18 O8 -7(4) . . . . ?
C20 C19 C18 C24 -180(2) . . . . ?
C17 C16 C29 C30 -173(2) . . . . ?
C16 N4 C15 C31 -2(3) . . . . ?
C16 N4 C15 C14 -179.6(17) . . . . ?
C16 C29 C30 C31 2(3) . . . . ?
C29 C30 C31 C15 -7(3) . . . . ?
C29 C30 C31 C32 180(2) . . . . ?
C30 C31 C15 N4 7(3) . . . . ?
C30 C31 C15 C14 -175.8(19) . . . . ?
C30 C31 C32 C33 176(2) . . . . ?
C31 C15 C14 N3 -178.4(18) . . . . ?
C31 C15 C14 C34 2(3) . . . . ?
C31 C32 C33 C34 -3(4) . . . . ?
C15 N4 C16 C17 173.4(18) . . . . ?
C15 N4 C16 C29 -3(3) . . . . ?
C15 C31 C32 C33 2(3) . . . . ?
C32 C31 C15 N4 -179(2) . . . . ?
C32 C31 C15 C14 -2(3) . . . . ?
C32 C33 C34 C14 3(3) . . . . ?
C32 C33 C34 C35 -177(2) . . . . ?
C33 C34 C14 N3 178(2) . . . . ?
C33 C34 C14 C15 -2(3) . . . . ?
C33 C34 C35 C36 -178(2) . . . . ?
C34 C35 C36 C13 -4(3) . . . . ?
C14 N3 C13 C36 -4(3) . . . . ?
C14 N3 C13 C1 178.2(17) . . . . ?
C14 C34 C35 C36 2(3) . . . . ?
C35 C34 C14 N3 -2(3) . . . . ?
C35 C34 C14 C15 177(2) . . . . ?
C35 C36 C13 N3 5(3) . . . . ?
C35 C36 C13 C1 -178.0(19) . . . . ?
C36 C13 C1 O2 -166.3(18) . . . . ?
C36 C13 C1 N1 14(3) . . . . ?
C13 N3 C14 C15 -176.6(18) . . . . ?
C13 N3 C14 C34 3(3) . . . . ?
C1 N1 N2 Dy2 -13(2) . . . . ?
C1 N1 N2 C2 174.5(18) . . . . ?
C2 C3 C8 C7 -179(2) . . . . ?
C2 C3 C4 O3 -2(3) . . . . ?
C2 C3 C4 C5 177(2) . . . . ?
C3 C8 C7 C6 1(4) . . . . ?
C8 C3 C4 O3 -179(2) . . . . ?
C8 C3 C4 C5 0(3) . . . . ?
C8 C7 C6 C5 0(4) . . . . ?
C7 C6 C5 C4 -2(4) . . . . ?
C7 C6 C5 C9 180(3) . . . . ?
C6 C5 C4 O3 -180(2) . . . . ?
C6 C5 C4 C3 1(3) . . . . ?
C6 C5 C9 C10 119(3) . . . . ?
C6 C5 C9 C11 -118(3) . . . . ?
C6 C5 C9 C12 1(4) . . . . ?
C4 C3 C8 C7 -1(3) . . . . ?
C4 C5 C9 C10 -60(3) . . . . ?
C4 C5 C9 C11 63(3) . . . . ?
C4 C5 C9 C12 -178(2) . . . . ?
C9 C5 C4 O3 -1(3) . . . . ?
C9 C5 C4 C3 -180(2) . . . . ?

_olex2_submission_special_instructions 'No special instructions were received'
_oxdiff_exptl_absorpt_empirical_details 
;
Empirical correction (ABSPACK) includes:
- Absorption correction using spherical harmonics
- Frame scaling
;
_oxdiff_exptl_absorpt_empirical_full_max 2.105
_oxdiff_exptl_absorpt_empirical_full_min 0.548
