# Electronic Supplementary Material (ESI) for Inorganic Chemistry Frontiers.
# This journal is © the Partner Organisations 2021

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_aaa
_database_code_depnum_ccdc_archive 'CCDC 2079727'
loop_
_audit_author_name
_audit_author_address
'Yueying Zhu'
;Jilin University
China
;
_audit_update_record             
;
2021-04-23 deposited with the CCDC.	2021-09-22 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2016/6
_shelx_SHELXL_version_number     2016/6
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         'C44 H64 Cu2 N8 O22'
_chemical_formula_sum            'C44 H64 Cu2 N8 O22'
_chemical_formula_weight         1184.11

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      monoclinic
_space_group_IT_number           15
_space_group_name_H-M_alt        'C 2/c'
_space_group_name_Hall           '-C 2yc'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'

_cell_length_a                   33.183(7)
_cell_length_b                   19.468(4)
_cell_length_c                   16.287(3)
_cell_angle_alpha                90
_cell_angle_beta                 102.34(3)
_cell_angle_gamma                90
_cell_volume                     10279(4)
_cell_formula_units_Z            8
_cell_measurement_temperature    293(2)
_cell_measurement_reflns_used    40505
_cell_measurement_theta_min      2.292
_cell_measurement_theta_max      25.379

_exptl_crystal_description       block
_exptl_crystal_colour            green
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    1.530
_exptl_crystal_F_000             4944
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          0.23
_exptl_crystal_size_mid          0.21
_exptl_crystal_size_min          0.20
_exptl_absorpt_coefficient_mu    0.917
_shelx_estimated_absorpt_T_min   ?
_shelx_estimated_absorpt_T_max   ?
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_correction_T_min  0.7357
_exptl_absorpt_correction_T_max  0.7518
_exptl_absorpt_process_details   SADABS
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      293(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_source                   'fine-focus sealed tube'
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_detector_area_resol_mean 100cm
_diffrn_reflns_number            40505
_diffrn_reflns_av_unetI/netI     0.0285
_diffrn_reflns_av_R_equivalents  0.0321
_diffrn_reflns_limit_h_min       -39
_diffrn_reflns_limit_h_max       39
_diffrn_reflns_limit_k_min       -23
_diffrn_reflns_limit_k_max       20
_diffrn_reflns_limit_l_min       -19
_diffrn_reflns_limit_l_max       19
_diffrn_reflns_theta_min         2.292
_diffrn_reflns_theta_max         25.379
_diffrn_reflns_theta_full        25.242
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measured_fraction_theta_full 0.998
_diffrn_reflns_Laue_measured_fraction_max 0.997
_diffrn_reflns_Laue_measured_fraction_full 0.998
_diffrn_reflns_point_group_measured_fraction_max 0.997
_diffrn_reflns_point_group_measured_fraction_full 0.998
_reflns_number_total             9423
_reflns_number_gt                8080
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       ?
_computing_cell_refinement       ?
_computing_data_reduction        ?
_computing_structure_solution    ?
_computing_structure_refinement  'SHELXL-2016/6 (Sheldrick, 2016)'
_computing_molecular_graphics    ?
_computing_publication_material  ?
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0547P)²+19.6495P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   mixed
_refine_ls_hydrogen_treatment    mixed
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_number_reflns         9423
_refine_ls_number_parameters     388
_refine_ls_number_restraints     15
_refine_ls_R_factor_all          0.0407
_refine_ls_R_factor_gt           0.0353
_refine_ls_wR_factor_ref         0.1124
_refine_ls_wR_factor_gt          0.1100
_refine_ls_goodness_of_fit_ref   1.086
_refine_ls_restrained_S_all      1.091
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Cu1 Cu 0.27582(2) 0.23018(2) 0.45000(2) 0.01763(9) Uani 1 1 d . . . . .
Cu2 Cu 0.50876(2) 0.95825(2) 0.33242(2) 0.01751(9) Uani 1 1 d . . . . .
O1 O 0.29070(7) 0.32852(10) 0.46289(14) 0.0413(5) Uani 1 1 d . . . . .
O2 O 0.24873(6) 0.36126(10) 0.54549(13) 0.0373(5) Uani 1 1 d . . . . .
O3 O 0.46956(5) 0.88409(10) 0.32824(11) 0.0291(4) Uani 1 1 d . . . . .
O4 O 0.44700(5) 0.89400(10) 0.18911(11) 0.0295(4) Uani 1 1 d . . . . .
O5 O 0.27228(6) 0.75248(11) 0.14108(12) 0.0340(5) Uani 1 1 d . . . . .
O6 O 0.31394(6) 0.78712(11) 0.05796(11) 0.0350(5) Uani 1 1 d . . . . .
O7 O 0.45592(6) 0.96476(10) 0.67599(12) 0.0315(4) Uani 1 1 d . . . . .
O8 O 0.46088(6) 0.97593(10) 0.81440(12) 0.0317(4) Uani 1 1 d . . . . .
O9 O 0.31336(6) 0.78459(11) 0.86081(13) 0.0386(5) Uani 1 1 d . . . . .
O10 O 0.33925(18) 0.8822(3) 0.9119(4) 0.0662(11) Uani 0.5 1 d . U P A 1
O10' O 0.36117(18) 0.8449(3) 0.9399(4) 0.0662(11) Uani 0.5 1 d . U P A 2
O11 O 0.52641(8) 0.95348(15) 0.46637(14) 0.0564(7) Uani 1 1 d D . . . .
H11A H 0.5295(11) 0.9054(11) 0.491(2) 0.068 Uiso 1 1 d D U . . .
H11B H 0.5529(8) 0.9790(16) 0.487(2) 0.068 Uiso 1 1 d D U . . .
C1 C 0.34396(9) 0.64697(14) 0.51653(17) 0.0307(6) Uani 1 1 d . . . . .
C2 C 0.34909(9) 0.67466(14) 0.44060(17) 0.0313(6) Uani 1 1 d . . . . .
H2 H 0.342759 0.648089 0.392096 0.038 Uiso 1 1 calc R U . . .
C3 C 0.36356(8) 0.74153(14) 0.43593(16) 0.0266(6) Uani 1 1 d . . . . .
C4 C 0.37284(8) 0.78065(14) 0.50820(17) 0.0280(6) Uani 1 1 d . . . . .
H4 H 0.382785 0.825076 0.505533 0.034 Uiso 1 1 calc R U . . .
C5 C 0.36759(8) 0.75480(14) 0.58543(16) 0.0270(6) Uani 1 1 d . . . . .
C6 C 0.35300(9) 0.68761(14) 0.58799(17) 0.0312(6) Uani 1 1 d . . . . .
H6 H 0.349272 0.669785 0.638827 0.037 Uiso 1 1 calc R U . . .
C7 C 0.32816(9) 0.57555(15) 0.51760(18) 0.0334(6) Uani 1 1 d . . . . .
C8 C 0.33843(12) 0.52579(17) 0.4654(2) 0.0520(9) Uani 1 1 d . . . . .
H8 H 0.356524 0.536838 0.430954 0.062 Uiso 1 1 calc R U . . .
C9 C 0.32262(12) 0.46010(16) 0.4627(2) 0.0504(9) Uani 1 1 d . . . . .
H9 H 0.330639 0.427441 0.427686 0.061 Uiso 1 1 calc R U . . .
C10 C 0.29501(9) 0.44249(14) 0.51160(18) 0.0338(6) Uani 1 1 d . . . . .
C11 C 0.28495(11) 0.49143(16) 0.5647(2) 0.0453(8) Uani 1 1 d . . . . .
H11 H 0.266750 0.480408 0.598913 0.054 Uiso 1 1 calc R U . . .
C12 C 0.30151(11) 0.55680(15) 0.5680(2) 0.0432(8) Uani 1 1 d . . . . .
H12 H 0.294522 0.588790 0.605014 0.052 Uiso 1 1 calc R U . . .
C13 C 0.27658(9) 0.37222(14) 0.50634(17) 0.0291(6) Uani 1 1 d . . . . .
C14 C 0.36765(8) 0.76934(13) 0.35291(16) 0.0257(6) Uani 1 1 d . . . . .
C15 C 0.40300(8) 0.80580(14) 0.34464(16) 0.0268(6) Uani 1 1 d . . . . .
H15 H 0.423877 0.813562 0.391776 0.032 Uiso 1 1 calc R U . . .
C16 C 0.40721(8) 0.83050(13) 0.26681(16) 0.0243(5) Uani 1 1 d . . . . .
C17 C 0.37597(8) 0.81914(14) 0.19602(16) 0.0254(5) Uani 1 1 d . . . . .
H17 H 0.378835 0.834980 0.143699 0.030 Uiso 1 1 calc R U . . .
C18 C 0.34057(8) 0.78410(13) 0.20392(16) 0.0242(5) Uani 1 1 d . . . . .
C19 C 0.33675(8) 0.75958(14) 0.28216(17) 0.0271(6) Uani 1 1 d . . . . .
H19 H 0.312928 0.736158 0.286933 0.032 Uiso 1 1 calc R U . . .
C20 C 0.44414(7) 0.87220(13) 0.26022(16) 0.0229(5) Uani 1 1 d . . . . .
C21 C 0.30626(8) 0.77358(13) 0.12842(16) 0.0224(5) Uani 1 1 d . . . . .
C22 C 0.37677(8) 0.79905(14) 0.66210(16) 0.0267(6) Uani 1 1 d . . . . .
C23 C 0.40600(8) 0.85091(14) 0.66936(16) 0.0275(6) Uani 1 1 d . . . . .
H23 H 0.419741 0.857859 0.625911 0.033 Uiso 1 1 calc R U . . .
C24 C 0.41520(8) 0.89261(14) 0.73993(16) 0.0264(6) Uani 1 1 d . . . . .
C25 C 0.39452(9) 0.88344(16) 0.80436(18) 0.0373(7) Uani 1 1 d . . . . .
H25 H 0.400768 0.911007 0.852030 0.045 Uiso 1 1 calc R U . . .
C26 C 0.36427(10) 0.83276(17) 0.79773(18) 0.0390(7) Uani 1 1 d . . . . .
C27 C 0.35614(9) 0.79091(15) 0.72725(17) 0.0327(6) Uani 1 1 d . . . . .
H27 H 0.336386 0.756516 0.723499 0.039 Uiso 1 1 calc R U . . .
C28 C 0.44638(8) 0.94854(13) 0.74454(17) 0.0249(6) Uani 1 1 d . . . . .
C29 C 0.34029(12) 0.8262(2) 0.8663(2) 0.0626(12) Uani 1 1 d . . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Cu1 O6 1.9634(19) 6_566 ?
Cu1 O2 1.9655(19) 7_556 ?
Cu1 O1 1.977(2) . ?
Cu1 O5 1.981(2) 4_545 ?
Cu1 O9 2.1256(19) 6_565 ?
Cu1 Cu1 2.7161(8) 7_556 ?
Cu2 O7 1.9254(18) 5_676 ?
Cu2 O3 1.9348(17) . ?
Cu2 O8 2.0134(18) 6_575 ?
Cu2 O4 2.0155(17) 2_655 ?
Cu2 O11 2.137(2) . ?
Cu2 Cu2 2.6227(8) 2_655 ?
O1 C13 1.259(3) . ?
O2 C13 1.248(3) . ?
O3 C20 1.262(3) . ?
O4 C20 1.256(3) . ?
O5 C21 1.258(3) . ?
O6 C21 1.256(3) . ?
O7 C28 1.264(3) . ?
O8 C28 1.256(3) . ?
O9 C29 1.195(4) . ?
O10 C29 1.324(7) . ?
O10' C29 1.303(6) . ?
O11 H11A 1.012(18) . ?
O11 H11B 1.005(18) . ?
C1 C6 1.386(4) . ?
C1 C2 1.393(4) . ?
C1 C7 1.487(4) . ?
C2 C3 1.395(4) . ?
C2 H2 0.9300 . ?
C3 C4 1.380(4) . ?
C3 C14 1.489(3) . ?
C4 C5 1.400(4) . ?
C4 H4 0.9300 . ?
C5 C6 1.399(4) . ?
C5 C22 1.494(4) . ?
C6 H6 0.9300 . ?
C7 C12 1.378(4) . ?
C7 C8 1.379(4) . ?
C8 C9 1.379(4) . ?
C8 H8 0.9300 . ?
C9 C10 1.379(4) . ?
C9 H9 0.9300 . ?
C10 C11 1.375(4) . ?
C10 C13 1.494(4) . ?
C11 C12 1.383(4) . ?
C11 H11 0.9300 . ?
C12 H12 0.9300 . ?
C14 C19 1.382(4) . ?
C14 C15 1.402(4) . ?
C15 C16 1.390(4) . ?
C15 H15 0.9300 . ?
C16 C17 1.394(4) . ?
C16 C20 1.493(3) . ?
C17 C18 1.388(3) . ?
C17 H17 0.9300 . ?
C18 C19 1.392(4) . ?
C18 C21 1.501(4) . ?
C19 H19 0.9300 . ?
C22 C23 1.387(4) . ?
C22 C27 1.389(4) . ?
C23 C24 1.387(4) . ?
C23 H23 0.9300 . ?
C24 C25 1.383(4) . ?
C24 C28 1.493(3) . ?
C25 C26 1.395(4) . ?
C25 H25 0.9300 . ?
C26 C27 1.386(4) . ?
C26 C29 1.509(4) . ?
C27 H27 0.9300 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O6 Cu1 O2 90.23(9) 6_566 7_556 ?
O6 Cu1 O1 88.42(10) 6_566 . ?
O2 Cu1 O1 165.72(8) 7_556 . ?
O6 Cu1 O5 165.94(8) 6_566 4_545 ?
O2 Cu1 O5 87.28(9) 7_556 4_545 ?
O1 Cu1 O5 90.59(10) . 4_545 ?
O6 Cu1 O9 103.26(8) 6_566 6_565 ?
O2 Cu1 O9 102.19(9) 7_556 6_565 ?
O1 Cu1 O9 91.95(9) . 6_565 ?
O5 Cu1 O9 90.80(8) 4_545 6_565 ?
O6 Cu1 Cu1 83.11(6) 6_566 7_556 ?
O2 Cu1 Cu1 85.15(6) 7_556 7_556 ?
O1 Cu1 Cu1 80.58(6) . 7_556 ?
O5 Cu1 Cu1 82.89(6) 4_545 7_556 ?
O9 Cu1 Cu1 170.13(6) 6_565 7_556 ?
O7 Cu2 O3 173.33(8) 5_676 . ?
O7 Cu2 O8 88.14(9) 5_676 6_575 ?
O3 Cu2 O8 88.06(9) . 6_575 ?
O7 Cu2 O4 89.65(8) 5_676 2_655 ?
O3 Cu2 O4 92.29(8) . 2_655 ?
O8 Cu2 O4 162.01(7) 6_575 2_655 ?
O7 Cu2 O11 93.92(10) 5_676 . ?
O3 Cu2 O11 92.23(10) . . ?
O8 Cu2 O11 102.24(10) 6_575 . ?
O4 Cu2 O11 95.72(9) 2_655 . ?
O7 Cu2 Cu2 86.12(6) 5_676 2_655 ?
O3 Cu2 Cu2 87.91(6) . 2_655 ?
O8 Cu2 Cu2 81.68(6) 6_575 2_655 ?
O4 Cu2 Cu2 80.35(6) 2_655 2_655 ?
O11 Cu2 Cu2 176.08(8) . 2_655 ?
C13 O1 Cu1 126.83(18) . . ?
C13 O2 Cu1 122.13(18) . 7_556 ?
C20 O3 Cu2 119.08(16) . . ?
C20 O4 Cu2 124.85(16) . 2_655 ?
C21 O5 Cu1 123.77(17) . 4 ?
C21 O6 Cu1 124.39(16) . 6_565 ?
C28 O7 Cu2 121.91(17) . 5_676 ?
C28 O8 Cu2 122.69(16) . 6_576 ?
C29 O9 Cu1 125.4(2) . 6_566 ?
Cu2 O11 H11A 115(2) . . ?
Cu2 O11 H11B 111(2) . . ?
H11A O11 H11B 108(2) . . ?
C6 C1 C2 118.6(2) . . ?
C6 C1 C7 122.5(2) . . ?
C2 C1 C7 118.9(2) . . ?
C1 C2 C3 121.2(2) . . ?
C1 C2 H2 119.4 . . ?
C3 C2 H2 119.4 . . ?
C4 C3 C2 119.0(2) . . ?
C4 C3 C14 121.8(2) . . ?
C2 C3 C14 119.2(2) . . ?
C3 C4 C5 121.3(2) . . ?
C3 C4 H4 119.3 . . ?
C5 C4 H4 119.3 . . ?
C6 C5 C4 118.3(2) . . ?
C6 C5 C22 121.6(2) . . ?
C4 C5 C22 120.1(2) . . ?
C1 C6 C5 121.5(2) . . ?
C1 C6 H6 119.2 . . ?
C5 C6 H6 119.2 . . ?
C12 C7 C8 117.1(3) . . ?
C12 C7 C1 121.8(3) . . ?
C8 C7 C1 121.0(3) . . ?
C7 C8 C9 121.9(3) . . ?
C7 C8 H8 119.1 . . ?
C9 C8 H8 119.1 . . ?
C8 C9 C10 120.5(3) . . ?
C8 C9 H9 119.8 . . ?
C10 C9 H9 119.8 . . ?
C11 C10 C9 118.1(3) . . ?
C11 C10 C13 121.3(3) . . ?
C9 C10 C13 120.6(3) . . ?
C10 C11 C12 120.9(3) . . ?
C10 C11 H11 119.5 . . ?
C12 C11 H11 119.5 . . ?
C7 C12 C11 121.4(3) . . ?
C7 C12 H12 119.3 . . ?
C11 C12 H12 119.3 . . ?
O2 C13 O1 125.2(2) . . ?
O2 C13 C10 117.8(3) . . ?
O1 C13 C10 117.0(2) . . ?
C19 C14 C15 118.5(2) . . ?
C19 C14 C3 120.8(2) . . ?
C15 C14 C3 120.8(2) . . ?
C16 C15 C14 120.8(2) . . ?
C16 C15 H15 119.6 . . ?
C14 C15 H15 119.6 . . ?
C15 C16 C17 119.8(2) . . ?
C15 C16 C20 119.8(2) . . ?
C17 C16 C20 120.2(2) . . ?
C18 C17 C16 119.7(2) . . ?
C18 C17 H17 120.1 . . ?
C16 C17 H17 120.1 . . ?
C17 C18 C19 119.9(2) . . ?
C17 C18 C21 120.0(2) . . ?
C19 C18 C21 120.1(2) . . ?
C14 C19 C18 121.3(2) . . ?
C14 C19 H19 119.3 . . ?
C18 C19 H19 119.3 . . ?
O4 C20 O3 125.4(2) . . ?
O4 C20 C16 118.4(2) . . ?
O3 C20 C16 116.2(2) . . ?
O6 C21 O5 125.6(2) . . ?
O6 C21 C18 117.0(2) . . ?
O5 C21 C18 117.4(2) . . ?
C23 C22 C27 117.9(2) . . ?
C23 C22 C5 120.3(2) . . ?
C27 C22 C5 121.8(2) . . ?
C24 C23 C22 121.5(2) . . ?
C24 C23 H23 119.2 . . ?
C22 C23 H23 119.2 . . ?
C25 C24 C23 119.8(2) . . ?
C25 C24 C28 120.5(2) . . ?
C23 C24 C28 119.7(2) . . ?
C24 C25 C26 119.9(3) . . ?
C24 C25 H25 120.1 . . ?
C26 C25 H25 120.1 . . ?
C27 C26 C25 119.3(2) . . ?
C27 C26 C29 121.5(3) . . ?
C25 C26 C29 119.2(3) . . ?
C26 C27 C22 121.7(2) . . ?
C26 C27 H27 119.2 . . ?
C22 C27 H27 119.2 . . ?
O8 C28 O7 125.1(2) . . ?
O8 C28 C24 118.9(2) . . ?
O7 C28 C24 116.1(2) . . ?
O9 C29 O10' 120.1(4) . . ?
O9 C29 O10 119.4(4) . . ?
O9 C29 C26 120.5(3) . . ?
O10' C29 C26 113.4(4) . . ?
O10 C29 C26 115.2(4) . . ?

_refine_diff_density_max         1.228
_refine_diff_density_min         -0.562
_refine_diff_density_rms         0.069

