# Electronic Supplementary Material (ESI) for Inorganic Chemistry Frontiers.
# This journal is © the Partner Organisations 2021

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
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data_pr555
_database_code_depnum_ccdc_archive 'CCDC 2111041'
loop_
_audit_author_name
_audit_author_address
'Taisiya Sukhikh'
;NIIC SB RAS
Russia
;
_audit_update_record             
;
2021-09-21 deposited with the CCDC.	2021-11-15 downloaded from the CCDC.
;
_audit_creation_date             2021-05-21
_audit_creation_method           
;
Olex2 1.2
(compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506)
;
_shelx_SHELXL_version_number     2017/1
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C12 K6 Mo2 N12 Re2 Se4, 10(O H2)'
_chemical_formula_sum            'C12 H20 K6 Mo2 N12 O10 Re2 Se4'
_chemical_formula_weight         1607.08
_chemical_absolute_configuration ad
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
K K 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mo Mo -1.6832 0.6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Re Re -1.0185 7.2310 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Se Se -0.0929 2.2259 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      trigonal
_space_group_IT_number           143
_space_group_name_H-M_alt        'P 3'
_space_group_name_Hall           'P 3'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'

_cell_length_a                   33.127(3)
_cell_length_b                   33.127(3)
_cell_length_c                   9.3387(7)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_volume                     8875.5(17)
_cell_formula_units_Z            9
_cell_measurement_reflns_used    4574
_cell_measurement_temperature    150(2)
_cell_measurement_theta_max      26.91
_cell_measurement_theta_min      2.50
_shelx_estimated_absorpt_T_max   0.606
_shelx_estimated_absorpt_T_min   0.167
_exptl_absorpt_coefficient_mu    11.151
_exptl_absorpt_correction_T_max  0.7456
_exptl_absorpt_correction_T_min  0.5657
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
'SADABS-2012/1 (Bruker,2012) was used for absorption correction. wR2(int) was 0.0722 before and 0.0608 after correction. The Ratio of minimum to maximum transmission is 0.7587. The λ/2 correction factor is 0.0015.'
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            black
_exptl_crystal_colour_primary    black
_exptl_crystal_density_diffrn    2.674
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       prism
_exptl_crystal_F_000             6484
_exptl_crystal_size_max          0.25
_exptl_crystal_size_mid          0.08
_exptl_crystal_size_min          0.05
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0641
_diffrn_reflns_av_unetI/netI     0.0939
_diffrn_reflns_Laue_measured_fraction_full 0.997
_diffrn_reflns_Laue_measured_fraction_max 0.997
_diffrn_reflns_limit_h_max       32
_diffrn_reflns_limit_h_min       -38
_diffrn_reflns_limit_k_max       25
_diffrn_reflns_limit_k_min       -35
_diffrn_reflns_limit_l_max       8
_diffrn_reflns_limit_l_min       -10
_diffrn_reflns_number            34885
_diffrn_reflns_point_group_measured_fraction_full 0.997
_diffrn_reflns_point_group_measured_fraction_max 0.997
_diffrn_reflns_theta_full        24.406
_diffrn_reflns_theta_max         24.406
_diffrn_reflns_theta_min         1.420
_diffrn_ambient_temperature      150(2)
_diffrn_detector                 CCD
_diffrn_detector_area_resol_mean 8.33
_diffrn_detector_type            'Bruker APEXII CCD area detector'
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device       'κ-geometry diffractometer'
_diffrn_measurement_device_type  'Bruker APEX diffractometer'
_diffrn_measurement_method       'ω and φ scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   'sealed tube'
_diffrn_special_details          ?
_diffrn_standards_interval_count .
_diffrn_standards_interval_time  .
_diffrn_standards_number         .
_reflns_Friedel_coverage         1.000
_reflns_Friedel_fraction_full    0.997
_reflns_Friedel_fraction_max     0.997
_reflns_number_gt                12387
_reflns_number_total             15373
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'Bruker SAINT'
_computing_data_collection       'Bruker APEX2'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    'ShelXS (Sheldrick, 2008)'
_refine_diff_density_max         2.345
_refine_diff_density_min         -1.144
_refine_diff_density_rms         0.283
_refine_ls_abs_structure_details 
;
 Refined as an inversion twin.
;
_refine_ls_abs_structure_Flack   0.55(2)
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.022
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1162
_refine_ls_number_reflns         15373
_refine_ls_number_restraints     546
_refine_ls_R_factor_all          0.0732
_refine_ls_R_factor_gt           0.0518
_refine_ls_restrained_S_all      1.005
_refine_ls_shift/su_max          0.006
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0301P)²+108.0093P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0957
_refine_ls_wR_factor_ref         0.1051
_refine_special_details          
;
 Refined as a 2-component inversion twin.
;
_olex2_refinement_description    
;
1. Twinned data refinement
 Scales: 0.45(2)
 0.55(2)
2. Shared sites
{Mo1, Re1}
{Mo2, Re2}
{Mo3, Re3}
{Mo4, Re4}
{Mo5, Re5}
{Mo6, Re6}
{Mo7, Re7}
{Mo8, Re8}
{Mo9, Re9}
{Mo10, Re10}
{Mo11, Re11}
{Mo12, Re12}
{Mo13, Re13}
{Mo14, Re14}
3. Uiso/Uaniso restraints and constraints
Uanis(C11) \\sim Ueq, Uanis(C12) \\sim Ueq, Uanis(C13) \\sim Ueq, Uanis(C21)
\\sim Ueq, Uanis(C22) \\sim Ueq, Uanis(C23) \\sim Ueq, Uanis(C31) \\sim Ueq,
Uanis(C32) \\sim Ueq, Uanis(C33) \\sim Ueq, Uanis(C41) \\sim Ueq, Uanis(C42)
\\sim Ueq, Uanis(C43) \\sim Ueq, Uanis(C51) \\sim Ueq, Uanis(C52) \\sim Ueq,
Uanis(C53) \\sim Ueq, Uanis(C61) \\sim Ueq, Uanis(C62) \\sim Ueq, Uanis(C63)
\\sim Ueq, Uanis(C71) \\sim Ueq, Uanis(C72) \\sim Ueq, Uanis(C73) \\sim Ueq,
Uanis(C81) \\sim Ueq, Uanis(C82) \\sim Ueq, Uanis(C83) \\sim Ueq, Uanis(C91)
\\sim Ueq, Uanis(C92) \\sim Ueq, Uanis(C93) \\sim Ueq, Uanis(C101) \\sim Ueq,
Uanis(C111) \\sim Ueq, Uanis(C112) \\sim Ueq, Uanis(C113) \\sim Ueq,
Uanis(C121) \\sim Ueq, Uanis(C131) \\sim Ueq, Uanis(C141) \\sim Ueq,
Uanis(C142) \\sim Ueq, Uanis(C143) \\sim Ueq: with sigma of 0.001 and sigma for
terminal atoms of 0.002
Uanis(N11) \\sim Ueq, Uanis(N12) \\sim Ueq, Uanis(N13) \\sim Ueq, Uanis(N21)
\\sim Ueq, Uanis(N22) \\sim Ueq, Uanis(N23) \\sim Ueq, Uanis(N31) \\sim Ueq,
Uanis(N32) \\sim Ueq, Uanis(N33) \\sim Ueq, Uanis(N41) \\sim Ueq, Uanis(N42)
\\sim Ueq, Uanis(N43) \\sim Ueq, Uanis(N51) \\sim Ueq, Uanis(N52) \\sim Ueq,
Uanis(N53) \\sim Ueq, Uanis(N61) \\sim Ueq, Uanis(N62) \\sim Ueq, Uanis(N63)
\\sim Ueq, Uanis(N71) \\sim Ueq, Uanis(N72) \\sim Ueq, Uanis(N73) \\sim Ueq,
Uanis(N81) \\sim Ueq, Uanis(N82) \\sim Ueq, Uanis(N83) \\sim Ueq, Uanis(N91)
\\sim Ueq, Uanis(N92) \\sim Ueq, Uanis(N93) \\sim Ueq, Uanis(N101) \\sim Ueq,
Uanis(N111) \\sim Ueq, Uanis(N112) \\sim Ueq, Uanis(N113) \\sim Ueq,
Uanis(N121) \\sim Ueq, Uanis(N131) \\sim Ueq, Uanis(N141) \\sim Ueq,
Uanis(N142) \\sim Ueq, Uanis(N143) \\sim Ueq: with sigma of 0.001 and sigma for
terminal atoms of 0.002
Uanis(Mo1) = Uanis(Re1)
Uanis(Mo2) = Uanis(Re2)
Uanis(Mo3) = Uanis(Re3)
Uanis(Mo4) = Uanis(Re4)
Uanis(Mo7) = Uanis(Re7)
Uanis(Mo8) = Uanis(Re8)
Uanis(Mo6) = Uanis(Re6)
Uanis(Mo5) = Uanis(Re5)
Uanis(Mo11) = Uanis(Re11)
Uanis(Mo12) = Uanis(Re12)
Uanis(Mo10) = Uanis(Re10)
Uanis(Mo9) = Uanis(Re9)
Uanis(Mo13) = Uanis(Re13)
Uanis(Mo14) = Uanis(Re14)
4. Rigid body (RIGU) restrains
 C11, C12, C13, C21, C22, C23, C31, C32, C33, C41, C42, C43, C51, C52, C53,
 C61, C62, C63, C71, C72, C73, C81, C82, C83, C91, C92, C93, C101, C111, C112,
 C113, C121, C131, C141, C142, C143, N11, N12, N13, N21, N22, N23, N31, N32,
 N33, N41, N42, N43, N51, N52, N53, N61, N62, N63, N71, N72, N73, N81, N82, N83,
  N91, N92, N93, N101, N111, N112, N113, N121, N131, N141, N142, N143
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
5. Others
 1*[Sof(Re1)+Sof(Mo1)]+1*[Sof(Re2)+Sof(Mo2)]+1*[Sof(Re3)+Sof(Mo3)]+1*[Sof(Re4)+
 Sof(Mo4)]=2 with esd of 0.0001
 1*[Sof(Re5)+Sof(Mo5)]+1*[Sof(Re6)+Sof(Mo6)]+1*[Sof(Re7)+Sof(Mo7)]+1*[Sof(Re8)+
 Sof(Mo8)]=2 with esd of 0.0001
 1*[Sof(Re9)+Sof(Mo9)]+1*[Sof(Re10)+Sof(Mo10)]=1 with esd of 0.0001
 1*[Sof(Re11)+Sof(Mo11)]+1*[Sof(Re12)+Sof(Mo12)]=1 with esd of 0.0001
 1*[Sof(Re13)+Sof(Mo13)]+1*[Sof(Re14)+Sof(Mo14)]=1 with esd of 0.0001
 Sof(Re1)=1-FVAR(1)
 Sof(Mo1)=FVAR(1)
 Sof(Re2)=1-FVAR(2)
 Sof(Mo2)=FVAR(2)
 Sof(Re3)=1-FVAR(3)
 Sof(Mo3)=FVAR(3)
 Sof(Re4)=1-FVAR(4)
 Sof(Mo4)=FVAR(4)
 Sof(Re5)=1-FVAR(5)
 Sof(Mo5)=FVAR(5)
 Sof(Re6)=1-FVAR(6)
 Sof(Mo6)=FVAR(6)
 Sof(Re7)=1-FVAR(7)
 Sof(Mo7)=FVAR(7)
 Sof(Re8)=1-FVAR(8)
 Sof(Mo8)=FVAR(8)
 Sof(Re9)=1-FVAR(9)
 Sof(Mo9)=FVAR(9)
 Sof(Re10)=0.33333*(1-FVAR(11))
 Sof(Mo10)=0.33333*FVAR(11)
 Sof(Re11)=1-FVAR(11)
 Sof(Mo11)=FVAR(11)
 Sof(Re12)=0.3334*(1-FVAR(13))
 Sof(Mo12)=0.3334*FVAR(13)
 Sof(Re13)=0.3334*(1-FVAR(14))
 Sof(Mo13)=0.3334*FVAR(14)
 Sof(Re14)=1-FVAR(14)
 Sof(Mo14)=FVAR(14)
;
_atom_sites_solution_hydrogens   .
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Re1 Re 0.28590(6) 0.27696(5) 0.49918(16) 0.0116(4) Uani 0.484(4) 1 d . . . A 2
Re2 Re 0.31824(5) 0.33413(5) 0.25071(15) 0.0104(4) Uani 0.523(4) 1 d . . . A 2
Re3 Re 0.37339(5) 0.36185(5) 0.50250(16) 0.0097(4) Uani 0.518(4) 1 d . . . A 2
Re4 Re 0.28886(6) 0.36461(6) 0.49533(16) 0.0117(4) Uani 0.475(4) 1 d . . . A 2
Re5 Re 0.66252(5) 0.65047(6) 0.29424(17) 0.0105(4) Uani 0.503(4) 1 d . . . B 2
Re6 Re 0.69074(5) 0.70702(5) 0.04383(16) 0.0111(4) Uani 0.496(4) 1 d . . . B 2
Re7 Re 0.60573(5) 0.61997(5) 0.04432(16) 0.0112(4) Uani 0.511(4) 1 d . . . B 2
Re8 Re 0.69246(6) 0.62146(5) 0.04796(17) 0.0124(4) Uani 0.490(4) 1 d . . . B 2
Re9 Re 0.95449(5) 0.94687(5) 0.09825(15) 0.0095(4) Uani 0.537(3) 1 d . . . C 2
Re10 Re 1.000000 1.000000 0.3475(3) 0.0106(7) Uani 0.463(3) 3 d S T P C 2
Re11 Re 0.61442(5) 0.32716(5) 0.41617(15) 0.0066(4) Uani 0.490(3) 1 d . . . D 2
Re12 Re 0.666667 0.333333 0.1655(3) 0.0111(7) Uani 0.510(3) 3 d S T P D 2
Re13 Re 0.333333 0.666667 0.3399(3) 0.0136(7) Uani 0.470(3) 3 d S T P E 2
Re14 Re 0.38465(5) 0.67051(5) 0.08890(15) 0.0125(4) Uani 0.530(3) 1 d . . . E 2
Mo1 Mo 0.28590(6) 0.27696(5) 0.49918(16) 0.0116(4) Uani 0.516(4) 1 d . . . A 1
Mo2 Mo 0.31824(5) 0.33413(5) 0.25071(15) 0.0104(4) Uani 0.477(4) 1 d . . . A 1
Mo3 Mo 0.37339(5) 0.36185(5) 0.50250(16) 0.0097(4) Uani 0.482(4) 1 d . . . A 1
Mo4 Mo 0.28886(6) 0.36461(6) 0.49533(16) 0.0117(4) Uani 0.525(4) 1 d . . . A 1
Mo5 Mo 0.66252(5) 0.65047(6) 0.29424(17) 0.0105(4) Uani 0.497(4) 1 d . . . B 1
Mo6 Mo 0.69074(5) 0.70702(5) 0.04383(16) 0.0111(4) Uani 0.504(4) 1 d . . . B 1
Mo7 Mo 0.60573(5) 0.61997(5) 0.04432(16) 0.0112(4) Uani 0.489(4) 1 d . . . B 1
Mo8 Mo 0.69246(6) 0.62146(5) 0.04796(17) 0.0124(4) Uani 0.510(4) 1 d . . . B 1
Mo9 Mo 0.95449(5) 0.94687(5) 0.09825(15) 0.0095(4) Uani 0.463(3) 1 d . . . C 1
Mo10 Mo 1.000000 1.000000 0.3475(3) 0.0106(7) Uani 0.537(3) 3 d S T P C 1
Mo11 Mo 0.61442(5) 0.32716(5) 0.41617(15) 0.0066(4) Uani 0.510(3) 1 d . . . D 1
Mo12 Mo 0.666667 0.333333 0.1655(3) 0.0111(7) Uani 0.490(3) 3 d S T P D 1
Mo13 Mo 0.333333 0.666667 0.3399(3) 0.0136(7) Uani 0.530(3) 3 d S T P E 1
Mo14 Mo 0.38465(5) 0.67051(5) 0.08890(15) 0.0125(4) Uani 0.470(3) 1 d . . . E 1
Se1 Se 0.23707(10) 0.29648(10) 0.3447(3) 0.0141(7) Uani 1 1 d . . . . .
Se2 Se 0.35521(10) 0.29176(10) 0.3581(3) 0.0122(7) Uani 1 1 d . . . . .
Se3 Se 0.31480(10) 0.33442(9) 0.6977(3) 0.0101(6) Uani 1 1 d . . . . .
Se4 Se 0.35909(10) 0.41459(10) 0.3489(3) 0.0120(7) Uani 1 1 d . . . . .
Se5 Se 0.62367(10) 0.56949(9) 0.1981(3) 0.0114(6) Uani 1 1 d . . . . .
Se6 Se 0.66373(10) 0.64898(10) -0.1530(3) 0.0115(7) Uani 1 1 d . . . . .
Se7 Se 0.62119(10) 0.68906(10) 0.1919(3) 0.0109(6) Uani 1 1 d . . . . .
Se8 Se 0.74304(10) 0.69108(10) 0.1954(3) 0.0143(7) Uani 1 1 d . . . . .
Se9 Se 1.000000 1.000000 -0.0999(5) 0.0061(10) Uani 1 3 d S T P . .
Se10 Se 1.01038(9) 0.93612(9) 0.2471(3) 0.0086(6) Uani 1 1 d . . . . .
Se11 Se 0.60170(10) 0.26010(9) 0.2663(3) 0.0083(6) Uani 1 1 d . . . . .
Se12 Se 0.666667 0.333333 0.6156(5) 0.0049(10) Uani 1 3 d S T P . .
Se13 Se 0.333333 0.666667 -0.1101(5) 0.0104(11) Uani 1 3 d S T P . .
Se14 Se 0.39998(10) 0.73846(10) 0.2390(3) 0.0126(6) Uani 1 1 d . . . . .
K1 K 0.0965(2) 0.1145(3) 0.6563(7) 0.0266(17) Uani 1 1 d . . . . .
K2 K 0.2181(3) 0.1653(3) 0.9184(10) 0.055(3) Uani 1 1 d . . . . .
K3 K 0.2005(2) 0.2806(2) 0.9426(7) 0.0245(17) Uani 1 1 d . . . . .
K4 K 0.3744(3) 0.2653(3) 0.9347(8) 0.041(2) Uani 1 1 d . . . . .
K5 K 0.5065(2) 0.3114(3) 0.7826(7) 0.0263(17) Uani 1 1 d . . . . .
K6 K 0.4886(2) 0.4275(2) 0.8694(7) 0.0207(16) Uani 1 1 d . . . . .
K7 K 0.3805(2) 0.4534(2) 0.9443(7) 0.0230(17) Uani 1 1 d . . . . .
K8 K 0.2513(4) 0.4370(4) 0.9324(14) 0.091(4) Uani 1 1 d . . . . .
K9 K 0.3391(3) 0.5602(3) 0.6423(7) 0.0302(18) Uani 1 1 d . . . . .
K10 K 0.4934(2) 0.5516(2) 0.6772(6) 0.0171(15) Uani 1 1 d . . . . .
K11 K 0.6041(2) 0.5316(2) 0.6015(7) 0.0187(15) Uani 1 1 d . . . . .
K12 K 0.6542(2) 0.4355(2) 0.8682(7) 0.0204(16) Uani 1 1 d . . . . .
K13 K 0.7468(3) 0.5587(3) 0.5341(12) 0.063(3) Uani 1 1 d . . . . .
K14 K 0.7822(3) 0.7077(3) 0.6083(9) 0.036(2) Uani 1 1 d . . . . .
K15 K 0.8663(2) 0.8404(2) 0.7270(7) 0.0285(18) Uani 1 1 d . . . . .
K16 K 0.7277(2) 0.8223(2) 0.6631(7) 0.0231(16) Uani 1 1 d . . . . .
K17 K 0.6054(2) 0.7103(3) 0.5958(7) 0.0255(17) Uani 1 1 d . . . . .
K18 K 0.4876(3) 0.6833(3) 0.7321(8) 0.039(2) Uani 1 1 d . . . . .
O1 O 0.1600(7) 0.1019(7) 0.494(2) 0.027(5) Uiso 1 1 d . . . . .
O3 O 0.1031(9) 0.1982(9) 0.557(3) 0.055(7) Uiso 1 1 d . . . . .
O5 O 0.4284(10) 0.2212(10) 0.830(3) 0.066(8) Uiso 1 1 d . . . . .
O6 O 0.4589(8) 0.2781(8) 0.504(2) 0.045(6) Uiso 1 1 d . . . . .
O8 O 0.5365(7) 0.4367(7) 0.625(2) 0.022(5) Uiso 1 1 d . . . . .
O10 O 0.5773(8) 0.4431(8) 0.968(2) 0.032(6) Uiso 1 1 d . . . . .
O11 O 0.6486(7) 0.4949(7) 0.452(2) 0.027(5) Uiso 1 1 d . . . . .
O13 O 0.8205(9) 0.6547(9) 0.489(3) 0.053(7) Uiso 1 1 d . . . . .
O14 O 0.8781(9) 0.7612(9) 0.681(3) 0.050(7) Uiso 1 1 d . . . . .
O16 O 0.8088(8) 0.7964(8) 0.479(2) 0.039(6) Uiso 1 1 d . . . . .
O18 O 0.7635(6) 0.8677(6) 0.9213(19) 0.014(4) Uiso 1 1 d . . . . .
O19 O 0.5700(9) 0.7677(9) 0.673(2) 0.049(7) Uiso 1 1 d . . . . .
O21 O 0.5186(8) 0.6553(8) 0.477(2) 0.038(6) Uiso 1 1 d . . . . .
O23 O 0.4117(9) 0.5423(9) 0.560(3) 0.057(7) Uiso 1 1 d . . . . .
O25 O 0.2629(8) 0.5012(8) 0.463(2) 0.036(6) Uiso 1 1 d . . . . .
O27 O 0.4473(7) 0.5468(7) 0.9245(19) 0.022(5) Uiso 1 1 d . . . . .
O29 O 0.5216(6) 0.5120(6) 0.4503(18) 0.016(5) Uiso 1 1 d . . . . .
O30 O 0.6566(8) 0.7901(8) 0.432(2) 0.037(6) Uiso 1 1 d . . . . .
N11 N 0.2294(9) 0.1786(9) 0.324(3) 0.028(6) Uani 1 1 d . U . . .
N12 N 0.1925(9) 0.2179(9) 0.694(2) 0.023(5) Uani 1 1 d . U . . .
N13 N 0.3157(8) 0.2146(8) 0.700(2) 0.018(5) Uani 1 1 d . U . . .
N21 N 0.2803(10) 0.2523(9) 0.007(3) 0.032(6) Uani 1 1 d . U . . .
N22 N 0.4041(9) 0.3680(9) 0.026(3) 0.027(6) Uani 1 1 d . U . . .
N23 N 0.2842(9) 0.3794(9) -0.005(3) 0.029(6) Uani 1 1 d . U . . .
N31 N 0.4750(8) 0.4115(8) 0.341(2) 0.011(5) Uani 1 1 d . U . . .
N32 N 0.4317(8) 0.4537(8) 0.699(2) 0.012(5) Uani 1 1 d . U . . .
N33 N 0.4322(8) 0.3298(8) 0.706(2) 0.016(5) Uani 1 1 d . U . . .
N41 N 0.2416(10) 0.4143(9) 0.309(3) 0.032(6) Uani 1 1 d . U . . .
N42 N 0.1963(9) 0.3315(9) 0.692(3) 0.030(6) Uani 1 1 d . U . . .
N43 N 0.3224(8) 0.4574(9) 0.691(2) 0.021(5) Uani 1 1 d . U . . .
N51 N 0.7072(8) 0.7366(8) 0.529(2) 0.011(5) Uani 1 1 d . U . . .
N52 N 0.5793(8) 0.6129(8) 0.533(2) 0.014(5) Uani 1 1 d . U . . .
N53 N 0.7041(8) 0.6117(8) 0.545(2) 0.016(5) Uani 1 1 d . U . . .
N61 N 0.6511(8) 0.7598(9) -0.157(2) 0.019(5) Uani 1 1 d . U . . .
N62 N 0.7828(9) 0.7703(9) -0.161(3) 0.028(6) Uani 1 1 d . U . . .
N63 N 0.7357(8) 0.8075(9) 0.208(2) 0.020(5) Uani 1 1 d . U . . .
N71 N 0.5494(8) 0.5250(8) -0.146(2) 0.012(5) Uani 1 1 d . U . . .
N72 N 0.5048(8) 0.5678(8) 0.206(2) 0.014(5) Uani 1 1 d . U . . .
N73 N 0.5465(8) 0.6501(8) -0.171(2) 0.015(5) Uani 1 1 d . U . . .
N81 N 0.6613(8) 0.5278(8) -0.152(2) 0.013(5) Uani 1 1 d . U . . .
N82 N 0.7404(9) 0.5702(9) 0.220(3) 0.026(5) Uani 1 1 d . U . . .
N83 N 0.7876(9) 0.6593(9) -0.146(3) 0.030(6) Uani 1 1 d . U . . .
N91 N 0.8651(8) 0.9183(8) -0.102(2) 0.014(5) Uani 1 1 d . U . . .
N92 N 0.8770(9) 0.8546(9) 0.269(3) 0.022(5) Uani 1 1 d . U . . .
N93 N 0.9534(7) 0.8664(7) -0.115(2) 0.008(4) Uani 1 1 d . U . . .
N101 N 0.9298(8) 0.9225(8) 0.585(2) 0.019(5) Uani 1 1 d . U . . .
N111 N 0.5222(8) 0.3170(8) 0.252(2) 0.015(5) Uani 1 1 d . U . . .
N112 N 0.5895(8) 0.3928(8) 0.624(2) 0.009(5) Uani 1 1 d . U . . .
N113 N 0.5347(8) 0.2493(8) 0.626(2) 0.015(5) Uani 1 1 d . U . . .
N121 N 0.5893(8) 0.3285(8) -0.071(2) 0.018(5) Uani 1 1 d . U . . .
N131 N 0.2622(9) 0.5929(9) 0.573(3) 0.022(5) Uani 1 1 d . U . . .
N141 N 0.4045(8) 0.6009(8) -0.118(2) 0.014(5) Uani 1 1 d . U . . .
N142 N 0.4752(9) 0.6768(8) 0.251(2) 0.023(5) Uani 1 1 d . U . . .
N143 N 0.4680(8) 0.7481(8) -0.115(2) 0.021(5) Uani 1 1 d . U . . .
C11 C 0.2509(11) 0.2132(11) 0.384(3) 0.025(6) Uani 1 1 d . U . . .
C12 C 0.2246(10) 0.2385(10) 0.622(3) 0.013(5) Uani 1 1 d . U . . .
C13 C 0.3060(9) 0.2374(9) 0.631(3) 0.009(5) Uani 1 1 d . U . . .
C21 C 0.2928(11) 0.2803(11) 0.102(3) 0.021(6) Uani 1 1 d . U . . .
C22 C 0.3743(10) 0.3574(10) 0.110(3) 0.019(6) Uani 1 1 d . U . . .
C23 C 0.2940(10) 0.3622(10) 0.092(3) 0.019(6) Uani 1 1 d . U . . .
C31 C 0.4384(9) 0.3934(9) 0.392(3) 0.007(5) Uani 1 1 d . U . . .
C32 C 0.4113(9) 0.4228(9) 0.625(3) 0.008(5) Uani 1 1 d . U . . .
C33 C 0.4102(10) 0.3379(10) 0.639(3) 0.012(5) Uani 1 1 d . U . . .
C41 C 0.2585(10) 0.3972(10) 0.376(3) 0.018(6) Uani 1 1 d . U . . .
C42 C 0.2307(10) 0.3432(10) 0.619(3) 0.021(6) Uani 1 1 d . U . . .
C43 C 0.3120(10) 0.4265(10) 0.627(3) 0.016(5) Uani 1 1 d . U . . .
C51 C 0.6930(9) 0.7086(9) 0.446(3) 0.006(5) Uani 1 1 d . U . . .
C52 C 0.6085(9) 0.6248(9) 0.451(3) 0.007(5) Uani 1 1 d . U . . .
C53 C 0.6888(9) 0.6237(10) 0.452(3) 0.012(5) Uani 1 1 d . U . . .
C61 C 0.6654(10) 0.7418(10) -0.092(3) 0.016(6) Uani 1 1 d . U . . .
C62 C 0.7464(11) 0.7450(11) -0.088(3) 0.024(6) Uani 1 1 d . U . . .
C63 C 0.7202(11) 0.7704(11) 0.154(3) 0.022(6) Uani 1 1 d . U . . .
C71 C 0.5719(9) 0.5584(9) -0.081(3) 0.009(5) Uani 1 1 d . U . . .
C72 C 0.5410(10) 0.5866(10) 0.154(3) 0.012(5) Uani 1 1 d . U . . .
C73 C 0.5670(9) 0.6394(9) -0.093(3) 0.010(5) Uani 1 1 d . U . . .
C81 C 0.6712(9) 0.5619(9) -0.081(3) 0.005(5) Uani 1 1 d . U . . .
C82 C 0.7238(11) 0.5894(11) 0.161(3) 0.024(6) Uani 1 1 d . U . . .
C83 C 0.7532(11) 0.6452(11) -0.076(3) 0.022(6) Uani 1 1 d . U . . .
C91 C 0.8954(9) 0.9296(9) -0.033(3) 0.007(5) Uani 1 1 d . U . . .
C92 C 0.9032(10) 0.8865(10) 0.213(3) 0.013(5) Uani 1 1 d . U . . .
C93 C 0.9544(10) 0.8951(10) -0.038(3) 0.015(5) Uani 1 1 d . U . . .
C101 C 0.9556(10) 0.9503(10) 0.504(3) 0.016(6) Uani 1 1 d . U . . .
C111 C 0.5543(10) 0.3208(10) 0.304(3) 0.013(6) Uani 1 1 d . U . . .
C112 C 0.5987(9) 0.3707(9) 0.550(3) 0.005(5) Uani 1 1 d . U . . .
C113 C 0.5615(10) 0.2751(10) 0.553(3) 0.011(5) Uani 1 1 d . U . . .
C121 C 0.6151(10) 0.3298(10) 0.018(3) 0.015(6) Uani 1 1 d . U . . .
C131 C 0.2858(10) 0.6172(10) 0.492(3) 0.019(6) Uani 1 1 d . U . . .
C141 C 0.3960(9) 0.6240(9) -0.046(3) 0.010(5) Uani 1 1 d . U . . .
C142 C 0.4431(10) 0.6762(10) 0.194(3) 0.016(6) Uani 1 1 d . U . . .
C143 C 0.4385(10) 0.7211(10) -0.048(3) 0.016(5) Uani 1 1 d . U . . .
O2 O 0.1700(7) 0.1973(7) 0.104(2) 0.029(5) Uiso 1 1 d . . . . .
O4 O 0.3375(18) 0.1879(18) 0.151(5) 0.171(19) Uiso 1 1 d . . . . .
O7 O 0.4688(9) 0.3301(8) 0.037(3) 0.045(7) Uiso 1 1 d . . . . .
O9 O 0.5660(9) 0.4271(9) 0.262(3) 0.044(7) Uiso 1 1 d . . . . .
O12 O 0.7342(7) 0.4966(7) 0.034(2) 0.021(5) Uiso 1 1 d . . . . .
O15 O 0.8601(13) 0.7729(13) 0.061(4) 0.112(12) Uiso 1 1 d . . . . .
O17 O 0.8089(8) 0.8999(8) 0.260(2) 0.037(6) Uiso 1 1 d . . . . .
O20 O 0.5503(9) 0.7296(9) 0.023(3) 0.059(8) Uiso 1 1 d . . . . .
O22 O 0.4168(10) 0.5599(10) 0.275(3) 0.074(9) Uiso 1 1 d . . . . .
O24 O 0.3380(10) 0.4955(10) 0.091(3) 0.066(8) Uiso 1 1 d . . . . .
O26 O 0.1789(9) 0.3451(8) 0.070(3) 0.048(7) Uiso 1 1 d . . . . .
O28 O 0.4615(7) 0.4675(7) 0.092(2) 0.025(5) Uiso 1 1 d . . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Re1 Re2 2.844(2) . ?
Re1 Re3 2.857(2) . ?
Re1 Re4 2.856(2) . ?
Re1 Se1 2.482(3) . ?
Re1 Se2 2.474(3) . ?
Re1 Se3 2.481(3) . ?
Re1 C11 2.13(3) . ?
Re1 C12 2.11(3) . ?
Re1 C13 2.13(3) . ?
Re2 Re3 2.834(2) . ?
Re2 Re4 2.858(2) . ?
Re2 Se1 2.491(3) . ?
Re2 Se2 2.489(3) . ?
Re2 Se4 2.484(3) . ?
Re2 C21 2.08(3) . ?
Re2 C22 2.08(3) . ?
Re2 C23 2.11(3) . ?
Re3 Re4 2.848(2) . ?
Re3 Se2 2.485(3) . ?
Re3 Se3 2.481(3) . ?
Re3 Se4 2.482(3) . ?
Re3 C31 2.13(3) . ?
Re3 C32 2.10(3) . ?
Re3 C33 2.17(3) . ?
Re4 Se1 2.479(3) . ?
Re4 Se3 2.484(3) . ?
Re4 Se4 2.484(3) . ?
Re4 C41 2.12(3) . ?
Re4 C42 2.05(3) . ?
Re4 C43 2.18(3) . ?
Re5 Re6 2.846(2) . ?
Re5 Re7 2.847(2) . ?
Re5 Re8 2.855(2) . ?
Re5 Se5 2.491(3) . ?
Re5 Se7 2.485(3) . ?
Re5 Se8 2.488(3) . ?
Re5 C51 2.19(3) . ?
Re5 C52 2.13(3) . ?
Re5 C53 2.12(3) . ?
Re6 Re7 2.851(2) . ?
Re6 Re8 2.864(2) . ?
Re6 Se6 2.481(3) . ?
Re6 Se7 2.491(3) . ?
Re6 Se8 2.490(3) . ?
Re6 C61 2.14(3) . ?
Re6 C62 2.04(3) . ?
Re6 C63 2.09(3) . ?
Re7 Re8 2.849(2) . ?
Re7 Se5 2.491(3) . ?
Re7 Se6 2.483(3) . ?
Re7 Se7 2.496(3) . ?
Re7 C71 2.12(3) . ?
Re7 C72 2.12(3) . ?
Re7 C73 2.13(3) . ?
Re8 Se5 2.490(3) . ?
Re8 Se6 2.475(3) . ?
Re8 Se8 2.481(3) . ?
Re8 C81 2.11(3) . ?
Re8 C82 2.10(3) . ?
Re8 C83 2.10(3) . ?
Re9 Re9 2.855(3) 3_675 ?
Re9 Re9 2.855(3) 2_765 ?
Re9 Re10 2.853(3) . ?
Re9 Se9 2.478(4) . ?
Re9 Se10 2.489(3) 3_675 ?
Re9 Se10 2.479(3) . ?
Re9 C91 2.13(3) . ?
Re9 C92 2.15(3) . ?
Re9 C93 2.13(3) . ?
Re10 Se10 2.491(3) 3_675 ?
Re10 Se10 2.491(3) . ?
Re10 Se10 2.491(3) 2_765 ?
Re10 C101 2.14(3) . ?
Re10 C101 2.14(3) 3_675 ?
Re10 C101 2.14(3) 2_765 ?
Re11 Re11 2.837(3) 3_665 ?
Re11 Re11 2.837(3) 2_655 ?
Re11 Re12 2.857(3) . ?
Re11 Se11 2.490(3) 3_665 ?
Re11 Se11 2.477(3) . ?
Re11 Se12 2.480(4) . ?
Re11 C111 2.17(3) . ?
Re11 C112 2.16(3) . ?
Re11 C113 2.16(3) . ?
Re12 Se11 2.487(3) 3_665 ?
Re12 Se11 2.487(3) 2_655 ?
Re12 Se11 2.487(3) . ?
Re12 C121 2.15(3) . ?
Re12 C121 2.15(3) 3_665 ?
Re12 C121 2.15(3) 2_655 ?
Re13 Re14 2.861(3) 3_565 ?
Re13 Re14 2.861(3) 2_665 ?
Re13 Re14 2.861(3) . ?
Re13 Se14 2.484(3) . ?
Re13 Se14 2.484(3) 3_565 ?
Re13 Se14 2.484(3) 2_665 ?
Re13 C131 2.14(3) 2_665 ?
Re13 C131 2.14(3) 3_565 ?
Re13 C131 2.14(3) . ?
Re14 Re14 2.840(3) 2_665 ?
Re14 Re14 2.840(3) 3_565 ?
Re14 Se13 2.478(4) . ?
Re14 Se14 2.487(3) 3_565 ?
Re14 Se14 2.479(3) . ?
Re14 C141 2.17(3) . ?
Re14 C142 2.09(3) . ?
Re14 C143 2.15(3) . ?
Mo1 Mo2 2.844(2) . ?
Mo1 Mo3 2.857(2) . ?
Mo1 Mo4 2.856(2) . ?
Mo1 Se1 2.482(3) . ?
Mo1 Se2 2.474(3) . ?
Mo1 Se3 2.481(3) . ?
Mo1 C11 2.13(3) . ?
Mo1 C12 2.11(3) . ?
Mo1 C13 2.13(3) . ?
Mo2 Mo3 2.834(2) . ?
Mo2 Mo4 2.858(2) . ?
Mo2 Se1 2.491(3) . ?
Mo2 Se2 2.489(3) . ?
Mo2 Se4 2.484(3) . ?
Mo2 C21 2.08(3) . ?
Mo2 C22 2.08(3) . ?
Mo2 C23 2.11(3) . ?
Mo3 Mo4 2.848(2) . ?
Mo3 Se2 2.485(3) . ?
Mo3 Se3 2.481(3) . ?
Mo3 Se4 2.482(3) . ?
Mo3 C31 2.13(3) . ?
Mo3 C32 2.10(3) . ?
Mo3 C33 2.17(3) . ?
Mo4 Se1 2.479(3) . ?
Mo4 Se3 2.484(3) . ?
Mo4 Se4 2.484(3) . ?
Mo4 C41 2.12(3) . ?
Mo4 C42 2.05(3) . ?
Mo4 C43 2.18(3) . ?
Mo5 Mo6 2.846(2) . ?
Mo5 Mo7 2.847(2) . ?
Mo5 Mo8 2.855(2) . ?
Mo5 Se5 2.491(3) . ?
Mo5 Se7 2.485(3) . ?
Mo5 Se8 2.488(3) . ?
Mo5 C51 2.19(3) . ?
Mo5 C52 2.13(3) . ?
Mo5 C53 2.12(3) . ?
Mo6 Mo7 2.851(2) . ?
Mo6 Mo8 2.864(2) . ?
Mo6 Se6 2.481(3) . ?
Mo6 Se7 2.491(3) . ?
Mo6 Se8 2.490(3) . ?
Mo6 C61 2.14(3) . ?
Mo6 C62 2.04(3) . ?
Mo6 C63 2.09(3) . ?
Mo7 Mo8 2.849(2) . ?
Mo7 Se5 2.491(3) . ?
Mo7 Se6 2.483(3) . ?
Mo7 Se7 2.496(3) . ?
Mo7 C71 2.12(3) . ?
Mo7 C72 2.12(3) . ?
Mo7 C73 2.13(3) . ?
Mo8 Se5 2.490(3) . ?
Mo8 Se6 2.475(3) . ?
Mo8 Se8 2.481(3) . ?
Mo8 C81 2.11(3) . ?
Mo8 C82 2.10(3) . ?
Mo8 C83 2.10(3) . ?
Mo9 Mo10 2.853(3) . ?
Mo9 Se9 2.478(4) . ?
Mo9 Se10 2.489(3) 3_675 ?
Mo9 Se10 2.479(3) . ?
Mo9 C91 2.13(3) . ?
Mo9 C92 2.15(3) . ?
Mo9 C93 2.13(3) . ?
Mo10 Se10 2.491(3) . ?
Mo10 Se10 2.491(3) 2_765 ?
Mo10 Se10 2.491(3) 3_675 ?
Mo10 C101 2.14(3) 3_675 ?
Mo10 C101 2.14(3) 2_765 ?
Mo10 C101 2.14(3) . ?
Mo11 Mo12 2.857(3) . ?
Mo11 Se11 2.477(3) . ?
Mo11 Se11 2.490(3) 3_665 ?
Mo11 Se12 2.480(4) . ?
Mo11 C111 2.17(3) . ?
Mo11 C112 2.16(3) . ?
Mo11 C113 2.16(3) . ?
Mo12 Se11 2.487(3) 3_665 ?
Mo12 Se11 2.487(3) . ?
Mo12 Se11 2.487(3) 2_655 ?
Mo12 C121 2.15(3) 3_665 ?
Mo12 C121 2.15(3) 2_655 ?
Mo12 C121 2.15(3) . ?
Mo13 Mo14 2.861(3) . ?
Mo13 Se14 2.484(3) 3_565 ?
Mo13 Se14 2.484(3) . ?
Mo13 Se14 2.484(3) 2_665 ?
Mo13 C131 2.14(3) 3_565 ?
Mo13 C131 2.14(3) . ?
Mo13 C131 2.14(3) 2_665 ?
Mo14 Se13 2.478(4) . ?
Mo14 Se14 2.479(3) . ?
Mo14 Se14 2.487(3) 3_565 ?
Mo14 C141 2.17(3) . ?
Mo14 C142 2.09(3) . ?
Mo14 C143 2.15(3) . ?
Se1 K3 3.900(7) 1_554 ?
Se4 K7 3.940(7) 1_554 ?
Se5 K11 3.921(7) . ?
Se7 K17 3.919(7) . ?
K1 K2 4.276(11) . ?
K1 O1 2.79(2) . ?
K1 O3 2.83(3) . ?
K1 N12 3.33(3) . ?
K1 N91 2.93(2) 3_566 ?
K1 N93 2.83(2) 2_656 ?
K1 N101 3.35(3) 2_655 ?
K1 N101 3.06(3) 3_565 ?
K1 C91 3.48(3) 3_566 ?
K1 C93 3.48(3) 2_656 ?
K1 C101 3.45(3) 2_655 ?
K1 C101 3.31(3) 3_565 ?
K2 K3 4.150(11) . ?
K2 K4 4.543(11) . ?
K2 K15 4.396(11) 2_655 ?
K2 O14 3.00(3) 2_655 ?
K2 N12 3.10(3) . ?
K2 N13 3.47(2) . ?
K2 N21 2.70(3) 1_556 ?
K2 N93 2.72(2) 2_656 ?
K2 O2 2.90(2) 1_556 ?
K2 O15 3.05(4) 2_656 ?
K3 O18 2.776(19) 3_565 ?
K3 N12 3.03(2) . ?
K3 N21 3.27(3) 1_556 ?
K3 N23 3.09(3) 1_556 ?
K3 N42 2.93(3) . ?
K3 C21 3.41(3) 1_556 ?
K3 C23 3.24(3) 1_556 ?
K3 C42 3.51(3) . ?
K3 O2 2.85(2) 1_556 ?
K3 O26 2.83(3) 1_556 ?
K4 K5 4.100(10) . ?
K4 O5 2.98(3) . ?
K4 N13 2.86(2) . ?
K4 N21 3.00(3) 1_556 ?
K4 N22 3.15(3) 1_556 ?
K4 N33 2.95(2) . ?
K4 C13 3.46(3) . ?
K4 C21 3.36(3) 1_556 ?
K4 C22 3.46(3) 1_556 ?
K4 C33 3.46(3) . ?
K4 O4 3.00(5) 1_556 ?
K4 O7 2.93(3) 1_556 ?
K5 K13 4.233(11) 2_655 ?
K5 O5 2.84(3) . ?
K5 O6 2.96(2) . ?
K5 N33 2.90(3) . ?
K5 N112 3.10(2) . ?
K5 N113 3.03(2) . ?
K5 N121 2.86(3) 1_556 ?
K5 C112 3.45(3) . ?
K5 C113 3.40(3) . ?
K5 O7 2.89(3) 1_556 ?
K5 O12 3.35(2) 2_656 ?
K6 K7 4.140(10) . ?
K6 O8 2.71(2) . ?
K6 O10 2.87(2) . ?
K6 N22 2.89(3) 1_556 ?
K6 N32 2.91(2) . ?
K6 N33 3.20(2) . ?
K6 N71 2.83(2) 1_556 ?
K6 C32 3.38(3) . ?
K6 C33 3.53(3) . ?
K6 O7 3.35(3) 1_556 ?
K6 O28 2.84(2) 1_556 ?
K7 K8 4.038(13) . ?
K7 O27 2.77(2) . ?
K7 N22 3.38(3) 1_556 ?
K7 N23 2.93(3) 1_556 ?
K7 N32 2.84(2) . ?
K7 N43 3.10(2) . ?
K7 C22 3.45(3) 1_556 ?
K7 C23 3.25(3) 1_556 ?
K7 C32 3.47(3) . ?
K7 O24 2.78(3) 1_556 ?
K7 O28 2.84(2) 1_556 ?
K8 K9 4.538(13) . ?
K8 K18 4.210(12) 3_565 ?
K8 O19 2.95(3) 3_565 ?
K8 N23 2.69(3) 1_556 ?
K8 N43 3.08(3) . ?
K8 N143 2.83(3) 3_566 ?
K8 O20 2.75(3) 3_566 ?
K8 O24 2.94(3) 1_556 ?
K8 O26 3.06(3) 1_556 ?
K9 K18 4.272(11) 3_565 ?
K9 O23 2.86(3) . ?
K9 O25 2.84(2) . ?
K9 N43 3.20(3) . ?
K9 N131 3.23(3) 2_665 ?
K9 N131 3.29(3) . ?
K9 N141 2.93(2) 1_556 ?
K9 N143 2.83(2) 3_566 ?
K9 C131 3.46(3) . ?
K9 C131 3.43(3) 2_665 ?
K9 C141 3.53(3) 1_556 ?
K9 C143 3.46(3) 3_566 ?
K10 K11 4.098(9) . ?
K10 O23 2.79(3) . ?
K10 O27 2.730(19) . ?
K10 O29 2.882(19) . ?
K10 N32 2.85(2) . ?
K10 N52 2.87(2) . ?
K10 N71 2.92(2) 1_556 ?
K10 N73 3.17(2) 1_556 ?
K10 C71 3.37(3) 1_556 ?
K10 C73 3.45(3) 1_556 ?
K11 O8 2.81(2) . ?
K11 O11 2.72(2) . ?
K11 O29 2.847(19) . ?
K11 N52 3.25(2) . ?
K11 N53 3.08(2) . ?
K11 N71 2.91(2) 1_556 ?
K11 N81 3.03(2) 1_556 ?
K11 C52 3.33(3) . ?
K11 C53 3.25(3) . ?
K11 C71 3.42(3) 1_556 ?
K11 C81 3.54(3) 1_556 ?
K12 O10 2.84(2) . ?
K12 N81 2.95(2) 1_556 ?
K12 N112 2.96(2) . ?
K12 N113 2.85(2) 3_665 ?
K12 N121 3.35(3) 3_666 ?
K12 N121 3.14(2) 1_556 ?
K12 C113 3.51(3) 3_665 ?
K12 C121 3.37(3) 1_556 ?
K12 C121 3.49(3) 3_666 ?
K12 O12 2.86(2) 1_556 ?
K13 K14 4.520(11) . ?
K13 O5 3.08(3) 3_665 ?
K13 O6 2.75(3) 3_665 ?
K13 O11 2.96(2) . ?
K13 O13 2.91(3) . ?
K13 N53 2.75(2) . ?
K13 N82 2.98(3) . ?
K13 N113 2.85(2) 3_665 ?
K14 K15 4.010(10) . ?
K14 O13 2.86(3) . ?
K14 O14 2.84(3) . ?
K14 O16 2.88(2) . ?
K14 N51 3.17(2) . ?
K14 N53 2.99(3) . ?
K14 N62 2.98(3) 1_556 ?
K14 N83 2.86(3) 1_556 ?
K14 C51 3.34(3) . ?
K14 C53 3.29(3) . ?
K14 C62 3.53(3) 1_556 ?
K14 C83 3.45(3) 1_556 ?
K15 K16 4.362(10) . ?
K15 O1 3.32(2) 3_665 ?
K15 O14 2.87(3) . ?
K15 O16 2.89(2) . ?
K15 N62 2.78(3) 1_556 ?
K15 N91 3.05(2) 1_556 ?
K15 N93 2.96(2) 1_556 ?
K15 N101 2.80(3) . ?
K15 C91 3.44(3) 1_556 ?
K15 C93 3.37(3) 1_556 ?
K16 K17 3.943(10) . ?
K16 O3 2.79(3) 2_665 ?
K16 O18 2.774(19) . ?
K16 O30 2.97(2) . ?
K16 N42 2.94(3) 2_665 ?
K16 N51 2.86(2) . ?
K16 N61 2.88(2) 1_556 ?
K16 C61 3.33(3) 1_556 ?
K17 K18 3.766(10) . ?
K17 O19 2.78(3) . ?
K17 O21 2.75(2) . ?
K17 O30 2.78(2) . ?
K17 N51 3.10(2) . ?
K17 N52 2.95(2) . ?
K17 N61 2.80(2) 1_556 ?
K17 N73 2.94(2) 1_556 ?
K17 C51 3.25(3) . ?
K17 C52 3.19(3) . ?
K17 C61 3.39(3) 1_556 ?
K18 O19 2.82(3) . ?
K18 O21 2.93(2) . ?
K18 N73 2.83(2) 1_556 ?
K18 N131 2.88(3) 2_665 ?
K18 N141 3.08(2) 1_556 ?
K18 N143 2.91(2) 1_556 ?
K18 C141 3.37(3) 1_556 ?
K18 C143 3.23(3) 1_556 ?
K18 O20 3.30(3) 1_556 ?
N11 C11 1.15(4) . ?
N12 C12 1.15(3) . ?
N13 C13 1.15(3) . ?
N21 C21 1.19(4) . ?
N22 C22 1.17(4) . ?
N23 C23 1.20(4) . ?
N31 C31 1.15(3) . ?
N32 C32 1.14(3) . ?
N33 C33 1.09(3) . ?
N41 C41 1.16(4) . ?
N42 C42 1.21(4) . ?
N43 C43 1.08(3) . ?
N51 C51 1.12(3) . ?
N52 C52 1.14(3) . ?
N53 C53 1.17(3) . ?
N61 C61 1.11(3) . ?
N62 C62 1.27(4) . ?
N63 C63 1.18(4) . ?
N71 C71 1.15(3) . ?
N72 C72 1.14(3) . ?
N73 C73 1.16(3) . ?
N81 C81 1.21(3) . ?
N82 C82 1.16(4) . ?
N83 C83 1.19(4) . ?
N91 C91 1.09(3) . ?
N92 C92 1.11(3) . ?
N93 C93 1.18(3) . ?
N101 C101 1.16(3) . ?
N111 C111 1.12(3) . ?
N112 C112 1.15(3) . ?
N113 C113 1.10(3) . ?
N121 C121 1.18(3) . ?
N131 C131 1.09(3) . ?
N141 C141 1.15(3) . ?
N142 C142 1.18(3) . ?
N143 C143 1.13(3) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Re2 Re1 Re3 59.62(5) . . ?
Re2 Re1 Re4 60.18(5) . . ?
Re4 Re1 Re3 59.81(6) . . ?
Se1 Re1 Re2 55.26(8) . . ?
Se1 Re1 Re3 102.86(9) . . ?
Se1 Re1 Re4 54.79(8) . . ?
Se2 Re1 Re2 55.28(8) . . ?
Se2 Re1 Re3 55.00(8) . . ?
Se2 Re1 Re4 103.60(9) . . ?
Se2 Re1 Se1 107.47(11) . . ?
Se2 Re1 Se3 106.38(11) . . ?
Se3 Re1 Re2 103.09(9) . . ?
Se3 Re1 Re3 54.85(8) . . ?
Se3 Re1 Re4 54.94(8) . . ?
Se3 Re1 Se1 106.63(11) . . ?
C11 Re1 Re2 94.9(8) . . ?
C11 Re1 Re3 139.9(8) . . ?
C11 Re1 Re4 136.8(8) . . ?
C11 Re1 Se1 82.0(8) . . ?
C11 Re1 Se2 85.3(8) . . ?
C11 Re1 Se3 161.9(8) . . ?
C11 Re1 C13 82.2(11) . . ?
C12 Re1 Re2 140.5(7) . . ?
C12 Re1 Re3 141.6(7) . . ?
C12 Re1 Re4 98.9(8) . . ?
C12 Re1 Se1 85.3(7) . . ?
C12 Re1 Se2 157.5(8) . . ?
C12 Re1 Se3 86.7(7) . . ?
C12 Re1 C11 78.1(11) . . ?
C12 Re1 C13 79.5(10) . . ?
C13 Re1 Re2 138.6(7) . . ?
C13 Re1 Re3 97.1(7) . . ?
C13 Re1 Re4 140.4(7) . . ?
C13 Re1 Se1 160.0(7) . . ?
C13 Re1 Se2 83.4(7) . . ?
C13 Re1 Se3 85.5(7) . . ?
Re1 Re2 Re4 60.11(5) . . ?
Re3 Re2 Re1 60.40(5) . . ?
Re3 Re2 Re4 60.04(5) . . ?
Se1 Re2 Re1 54.97(8) . . ?
Se1 Re2 Re3 103.26(9) . . ?
Se1 Re2 Re4 54.69(8) . . ?
Se2 Re2 Re1 54.79(8) . . ?
Se2 Re2 Re3 55.19(8) . . ?
Se2 Re2 Re4 103.15(9) . . ?
Se2 Re2 Se1 106.73(11) . . ?
Se4 Re2 Re1 103.59(9) . . ?
Se4 Re2 Re3 55.17(8) . . ?
Se4 Re2 Re4 54.89(8) . . ?
Se4 Re2 Se1 106.24(11) . . ?
Se4 Re2 Se2 107.37(11) . . ?
C21 Re2 Re1 96.8(8) . . ?
C21 Re2 Re3 138.8(8) . . ?
C21 Re2 Re4 140.8(9) . . ?
C21 Re2 Se1 86.2(9) . . ?
C21 Re2 Se2 83.6(8) . . ?
C21 Re2 Se4 159.6(8) . . ?
C21 Re2 C22 78.4(12) . . ?
C21 Re2 C23 80.2(12) . . ?
C22 Re2 Re1 136.9(8) . . ?
C22 Re2 Re3 95.3(8) . . ?
C22 Re2 Re4 140.5(8) . . ?
C22 Re2 Se1 161.4(8) . . ?
C22 Re2 Se2 82.1(8) . . ?
C22 Re2 Se4 85.9(8) . . ?
C22 Re2 C23 82.0(11) . . ?
C23 Re2 Re1 140.0(8) . . ?
C23 Re2 Re3 139.9(8) . . ?
C23 Re2 Re4 97.6(8) . . ?
C23 Re2 Se1 85.1(8) . . ?
C23 Re2 Se2 159.2(8) . . ?
C23 Re2 Se4 84.8(8) . . ?
Re2 Re3 Re1 59.97(5) . . ?
Re2 Re3 Re4 60.40(5) . . ?
Re4 Re3 Re1 60.09(6) . . ?
Se2 Re3 Re1 54.66(8) . . ?
Se2 Re3 Re2 55.34(8) . . ?
Se2 Re3 Re4 103.56(9) . . ?
Se3 Re3 Re1 54.86(8) . . ?
Se3 Re3 Re2 103.39(9) . . ?
Se3 Re3 Re4 55.06(8) . . ?
Se3 Re3 Se2 106.07(11) . . ?
Se3 Re3 Se4 107.03(11) . . ?
Se4 Re3 Re1 103.29(9) . . ?
Se4 Re3 Re2 55.23(8) . . ?
Se4 Re3 Re4 55.04(8) . . ?
Se4 Re3 Se2 107.57(11) . . ?
C31 Re3 Re1 139.2(7) . . ?
C31 Re3 Re2 95.0(7) . . ?
C31 Re3 Re4 137.8(7) . . ?
C31 Re3 Se2 84.8(7) . . ?
C31 Re3 Se3 161.6(7) . . ?
C31 Re3 Se4 82.9(7) . . ?
C31 Re3 C33 81.3(10) . . ?
C32 Re3 Re1 140.9(7) . . ?
C32 Re3 Re2 137.8(7) . . ?
C32 Re3 Re4 96.2(7) . . ?
C32 Re3 Se2 160.2(7) . . ?
C32 Re3 Se3 86.3(7) . . ?
C32 Re3 Se4 82.6(7) . . ?
C32 Re3 C31 79.6(10) . . ?
C32 Re3 C33 81.8(10) . . ?
C33 Re3 Re1 97.2(7) . . ?
C33 Re3 Re2 139.3(7) . . ?
C33 Re3 Re4 140.1(7) . . ?
C33 Re3 Se2 83.9(7) . . ?
C33 Re3 Se3 85.1(7) . . ?
C33 Re3 Se4 159.5(7) . . ?
Re1 Re4 Re2 59.70(5) . . ?
Re3 Re4 Re1 60.10(5) . . ?
Re3 Re4 Re2 59.56(5) . . ?
Se1 Re4 Re1 54.90(8) . . ?
Se1 Re4 Re2 55.09(8) . . ?
Se1 Re4 Re3 103.19(9) . . ?
Se1 Re4 Se3 106.64(11) . . ?
Se1 Re4 Se4 106.61(11) . . ?
Se3 Re4 Re1 54.83(8) . . ?
Se3 Re4 Re2 102.62(9) . . ?
Se3 Re4 Re3 54.94(8) . . ?
Se3 Re4 Se4 106.85(11) . . ?
Se4 Re4 Re1 103.25(9) . . ?
Se4 Re4 Re2 54.88(8) . . ?
Se4 Re4 Re3 54.98(8) . . ?
C41 Re4 Re1 137.7(8) . . ?
C41 Re4 Re2 95.4(8) . . ?
C41 Re4 Re3 138.9(8) . . ?
C41 Re4 Se1 83.0(8) . . ?
C41 Re4 Se3 162.0(8) . . ?
C41 Re4 Se4 84.1(8) . . ?
C41 Re4 C43 81.4(11) . . ?
C42 Re4 Re1 95.3(9) . . ?
C42 Re4 Re2 139.2(8) . . ?
C42 Re4 Re3 138.2(8) . . ?
C42 Re4 Se1 84.4(8) . . ?
C42 Re4 Se3 83.4(8) . . ?
C42 Re4 Se4 161.5(9) . . ?
C42 Re4 C41 82.5(11) . . ?
C42 Re4 C43 80.4(11) . . ?
C43 Re4 Re1 140.1(7) . . ?
C43 Re4 Re2 139.8(7) . . ?
C43 Re4 Re3 97.4(8) . . ?
C43 Re4 Se1 159.4(8) . . ?
C43 Re4 Se3 85.3(7) . . ?
C43 Re4 Se4 85.0(7) . . ?
Re6 Re5 Re7 60.09(6) . . ?
Re6 Re5 Re8 60.30(6) . . ?
Re7 Re5 Re8 59.95(6) . . ?
Se5 Re5 Re6 103.61(9) . . ?
Se5 Re5 Re7 55.14(8) . . ?
Se5 Re5 Re8 55.00(8) . . ?
Se7 Re5 Re6 55.20(8) . . ?
Se7 Re5 Re7 55.31(8) . . ?
Se7 Re5 Re8 103.70(9) . . ?
Se7 Re5 Se5 107.12(11) . . ?
Se7 Re5 Se8 107.25(11) . . ?
Se8 Re5 Re6 55.15(8) . . ?
Se8 Re5 Re7 103.13(9) . . ?
Se8 Re5 Re8 54.83(8) . . ?
Se8 Re5 Se5 106.59(11) . . ?
C51 Re5 Re6 95.5(7) . . ?
C51 Re5 Re7 140.7(7) . . ?
C51 Re5 Re8 137.1(7) . . ?
C51 Re5 Se5 160.7(7) . . ?
C51 Re5 Se7 85.7(7) . . ?
C51 Re5 Se8 82.3(7) . . ?
C52 Re5 Re6 139.4(7) . . ?
C52 Re5 Re7 98.4(7) . . ?
C52 Re5 Re8 141.4(7) . . ?
C52 Re5 Se5 86.5(7) . . ?
C52 Re5 Se7 84.2(7) . . ?
C52 Re5 Se8 158.5(7) . . ?
C52 Re5 C51 80.4(10) . . ?
C53 Re5 Re6 141.1(7) . . ?
C53 Re5 Re7 139.3(8) . . ?
C53 Re5 Re8 97.8(7) . . ?
C53 Re5 Se5 84.2(8) . . ?
C53 Re5 Se7 158.5(7) . . ?
C53 Re5 Se8 86.0(7) . . ?
C53 Re5 C51 79.3(10) . . ?
C53 Re5 C52 78.2(10) . . ?
Re5 Re6 Re7 59.97(5) . . ?
Re5 Re6 Re8 60.00(6) . . ?
Re7 Re6 Re8 59.81(5) . . ?
Se6 Re6 Re5 103.07(9) . . ?
Se6 Re6 Re7 54.98(8) . . ?
Se6 Re6 Re8 54.61(8) . . ?
Se6 Re6 Se7 107.10(11) . . ?
Se6 Re6 Se8 106.04(11) . . ?
Se7 Re6 Re5 55.01(8) . . ?
Se7 Re6 Re7 55.21(8) . . ?
Se7 Re6 Re8 103.29(9) . . ?
Se8 Re6 Re5 55.09(8) . . ?
Se8 Re6 Re7 102.99(9) . . ?
Se8 Re6 Re8 54.69(8) . . ?
Se8 Re6 Se7 107.01(11) . . ?
C61 Re6 Re5 138.6(7) . . ?
C61 Re6 Re7 95.2(8) . . ?
C61 Re6 Re8 138.3(8) . . ?
C61 Re6 Se6 83.9(8) . . ?
C61 Re6 Se7 83.8(7) . . ?
C61 Re6 Se8 161.8(8) . . ?
C62 Re6 Re5 142.9(9) . . ?
C62 Re6 Re7 139.0(9) . . ?
C62 Re6 Re8 99.1(9) . . ?
C62 Re6 Se6 84.1(9) . . ?
C62 Re6 Se7 157.5(9) . . ?
C62 Re6 Se8 87.8(9) . . ?
C62 Re6 C61 77.9(12) . . ?
C62 Re6 C63 81.6(12) . . ?
C63 Re6 Re5 95.2(8) . . ?
C63 Re6 Re7 138.0(8) . . ?
C63 Re6 Re8 139.2(8) . . ?
C63 Re6 Se6 161.8(8) . . ?
C63 Re6 Se7 82.9(8) . . ?
C63 Re6 Se8 84.7(8) . . ?
C63 Re6 C61 82.1(11) . . ?
Re5 Re7 Re6 59.94(5) . . ?
Re5 Re7 Re8 60.15(5) . . ?
Re8 Re7 Re6 60.32(6) . . ?
Se5 Re7 Re5 55.15(8) . . ?
Se5 Re7 Re6 103.50(9) . . ?
Se5 Re7 Re8 55.09(8) . . ?
Se5 Re7 Se7 106.80(11) . . ?
Se6 Re7 Re5 102.99(9) . . ?
Se6 Re7 Re6 54.92(8) . . ?
Se6 Re7 Re8 54.80(8) . . ?
Se6 Re7 Se5 106.82(11) . . ?
Se6 Re7 Se7 106.89(11) . . ?
Se7 Re7 Re5 54.95(8) . . ?
Se7 Re7 Re6 55.05(8) . . ?
Se7 Re7 Re8 103.58(9) . . ?
C71 Re7 Re5 136.9(7) . . ?
C71 Re7 Re6 138.8(7) . . ?
C71 Re7 Re8 93.8(7) . . ?
C71 Re7 Se5 82.0(7) . . ?
C71 Re7 Se6 84.2(7) . . ?
C71 Re7 Se7 162.5(7) . . ?
C71 Re7 C72 81.6(10) . . ?
C71 Re7 C73 81.4(10) . . ?
C72 Re7 Re5 96.0(7) . . ?
C72 Re7 Re6 139.3(7) . . ?
C72 Re7 Re8 138.7(7) . . ?
C72 Re7 Se5 83.7(7) . . ?
C72 Re7 Se6 161.0(7) . . ?
C72 Re7 Se7 84.4(8) . . ?
C72 Re7 C73 81.0(10) . . ?
C73 Re7 Re5 141.0(7) . . ?
C73 Re7 Re6 97.6(7) . . ?
C73 Re7 Re8 139.2(7) . . ?
C73 Re7 Se5 158.8(7) . . ?
C73 Re7 Se6 84.4(7) . . ?
C73 Re7 Se7 86.2(7) . . ?
Re5 Re8 Re6 59.70(5) . . ?
Re7 Re8 Re5 59.90(5) . . ?
Re7 Re8 Re6 59.87(5) . . ?
Se5 Re8 Re5 55.06(8) . . ?
Se5 Re8 Re6 103.17(9) . . ?
Se5 Re8 Re7 55.13(8) . . ?
Se6 Re8 Re5 102.98(9) . . ?
Se6 Re8 Re6 54.80(8) . . ?
Se6 Re8 Re7 55.05(8) . . ?
Se6 Re8 Se5 107.10(11) . . ?
Se6 Re8 Se8 106.47(11) . . ?
Se8 Re8 Re5 55.04(8) . . ?
Se8 Re8 Re6 54.96(8) . . ?
Se8 Re8 Re7 103.25(9) . . ?
Se8 Re8 Se5 106.84(11) . . ?
C81 Re8 Re5 139.9(7) . . ?
C81 Re8 Re6 139.0(7) . . ?
C81 Re8 Re7 96.6(7) . . ?
C81 Re8 Se5 85.0(7) . . ?
C81 Re8 Se6 84.3(7) . . ?
C81 Re8 Se8 160.2(7) . . ?
C82 Re8 Re5 96.1(8) . . ?
C82 Re8 Re6 139.9(8) . . ?
C82 Re8 Re7 138.1(8) . . ?
C82 Re8 Se5 83.1(8) . . ?
C82 Re8 Se6 160.9(8) . . ?
C82 Re8 Se8 85.1(9) . . ?
C82 Re8 C81 80.5(11) . . ?
C82 Re8 C83 81.1(12) . . ?
C83 Re8 Re5 138.3(8) . . ?
C83 Re8 Re6 96.4(8) . . ?
C83 Re8 Re7 140.1(8) . . ?
C83 Re8 Se5 160.4(8) . . ?
C83 Re8 Se6 85.2(8) . . ?
C83 Re8 Se8 83.3(8) . . ?
C83 Re8 C81 81.0(10) . . ?
Re9 Re9 Re9 60.000(1) 3_675 2_765 ?
Re10 Re9 Re9 59.97(4) . 2_765 ?
Se9 Re9 Re9 54.83(6) . 3_675 ?
Se9 Re9 Re9 54.82(6) . 2_765 ?
Se9 Re9 Re10 103.00(9) . . ?
Se9 Re9 Se10 106.73(9) . . ?
Se9 Re9 Se10 106.44(9) . 3_675 ?
Se10 Re9 Re9 103.40(8) . 3_675 ?
Se10 Re9 Re9 55.08(8) . 2_765 ?
Se10 Re9 Re9 54.77(8) 3_675 3_675 ?
Se10 Re9 Re9 103.16(8) 3_675 2_765 ?
Se10 Re9 Re10 55.08(7) 3_675 . ?
Se10 Re9 Re10 55.16(7) . . ?
Se10 Re9 Se10 107.11(14) . 3_675 ?
C91 Re9 Re9 97.2(7) . 3_675 ?
C91 Re9 Re9 139.7(7) . 2_765 ?
C91 Re9 Re10 140.0(7) . . ?
C91 Re9 Se9 84.9(7) . . ?
C91 Re9 Se10 85.0(7) . 3_675 ?
C91 Re9 Se10 159.4(7) . . ?
C91 Re9 C92 81.0(10) . . ?
C91 Re9 C93 79.0(10) . . ?
C92 Re9 Re9 139.0(7) . 3_675 ?
C92 Re9 Re9 138.5(7) . 2_765 ?
C92 Re9 Re10 95.6(7) . . ?
C92 Re9 Se9 161.4(7) . . ?
C92 Re9 Se10 84.4(7) . 3_675 ?
C92 Re9 Se10 83.6(7) . . ?
C93 Re9 Re9 138.0(8) . 3_675 ?
C93 Re9 Re9 96.2(8) . 2_765 ?
C93 Re9 Re10 140.3(8) . . ?
C93 Re9 Se9 83.2(8) . . ?
C93 Re9 Se10 160.6(8) . 3_675 ?
C93 Re9 Se10 85.4(8) . . ?
C93 Re9 C92 82.3(10) . . ?
Re9 Re10 Re9 60.06(7) 3_675 2_765 ?
Re9 Re10 Re9 60.06(7) . 2_765 ?
Re9 Re10 Re9 60.06(7) 3_675 . ?
Se10 Re10 Re9 55.02(8) 3_675 . ?
Se10 Re10 Re9 55.02(8) 2_765 3_675 ?
Se10 Re10 Re9 103.18(11) 2_765 . ?
Se10 Re10 Re9 55.02(8) . 2_765 ?
Se10 Re10 Re9 54.79(8) . . ?
Se10 Re10 Re9 54.79(8) 2_765 2_765 ?
Se10 Re10 Re9 54.79(8) 3_675 3_675 ?
Se10 Re10 Re9 103.18(11) 3_675 2_765 ?
Se10 Re10 Re9 103.18(11) . 3_675 ?
Se10 Re10 Se10 106.70(9) . 2_765 ?
Se10 Re10 Se10 106.70(9) 3_675 2_765 ?
Se10 Re10 Se10 106.70(9) . 3_675 ?
C101 Re10 Re9 141.4(8) 3_675 . ?
C101 Re10 Re9 139.0(8) 3_675 2_765 ?
C101 Re10 Re9 97.8(8) 2_765 2_765 ?
C101 Re10 Re9 141.4(8) 2_765 3_675 ?
C101 Re10 Re9 139.0(8) 2_765 . ?
C101 Re10 Re9 97.8(8) . . ?
C101 Re10 Re9 141.4(8) . 2_765 ?
C101 Re10 Re9 139.0(8) . 3_675 ?
C101 Re10 Re9 97.8(8) 3_675 3_675 ?
C101 Re10 Se10 84.2(8) 2_765 . ?
C101 Re10 Se10 84.2(8) . 3_675 ?
C101 Re10 Se10 159.0(8) 2_765 3_675 ?
C101 Re10 Se10 86.4(8) 3_675 3_675 ?
C101 Re10 Se10 86.4(8) . . ?
C101 Re10 Se10 86.4(8) 2_765 2_765 ?
C101 Re10 Se10 84.2(8) 3_675 2_765 ?
C101 Re10 Se10 159.0(8) 3_675 . ?
C101 Re10 Se10 159.0(8) . 2_765 ?
C101 Re10 C101 78.5(12) 2_765 3_675 ?
C101 Re10 C101 78.5(12) . 2_765 ?
C101 Re10 C101 78.5(12) . 3_675 ?
Re11 Re11 Re12 60.23(3) 3_665 . ?
Re11 Re11 Re12 60.23(3) 2_655 . ?
Se11 Re11 Re11 55.38(8) . 2_655 ?
Se11 Re11 Re11 103.20(8) 3_665 2_655 ?
Se11 Re11 Re11 54.94(8) 3_665 3_665 ?
Se11 Re11 Re11 103.55(8) . 3_665 ?
Se11 Re11 Re12 55.01(7) . . ?
Se11 Re11 Re12 54.90(7) 3_665 . ?
Se11 Re11 Se11 106.74(14) . 3_665 ?
Se11 Re11 Se12 107.27(9) . . ?
Se12 Re11 Re11 55.11(6) . 2_655 ?
Se12 Re11 Re11 55.11(6) . 3_665 ?
Se12 Re11 Re12 103.68(9) . . ?
Se12 Re11 Se11 106.85(9) . 3_665 ?
C111 Re11 Re11 138.8(7) . 3_665 ?
C111 Re11 Re11 139.7(8) . 2_655 ?
C111 Re11 Re12 96.0(7) . . ?
C111 Re11 Se11 84.4(8) . . ?
C111 Re11 Se11 83.9(8) . 3_665 ?
C111 Re11 Se12 160.3(7) . . ?
C112 Re11 Re11 139.4(7) . 2_655 ?
C112 Re11 Re11 97.0(7) . 3_665 ?
C112 Re11 Re12 140.0(7) . . ?
C112 Re11 Se11 85.1(7) . 3_665 ?
C112 Re11 Se11 159.4(7) . . ?
C112 Re11 Se12 84.4(7) . . ?
C112 Re11 C111 80.1(10) . . ?
C112 Re11 C113 79.7(10) . . ?
C113 Re11 Re11 95.6(7) . 2_655 ?
C113 Re11 Re11 137.8(7) . 3_665 ?
C113 Re11 Re12 139.8(7) . . ?
C113 Re11 Se11 161.2(7) . 3_665 ?
C113 Re11 Se11 84.9(7) . . ?
C113 Re11 Se12 82.8(7) . . ?
C113 Re11 C111 82.6(10) . . ?
Re11 Re12 Re11 59.53(7) 3_665 . ?
Re11 Re12 Re11 59.53(7) 2_655 . ?
Se11 Re12 Re11 54.69(8) 3_665 3_665 ?
Se11 Re12 Re11 55.02(8) 3_665 . ?
Se11 Re12 Re11 102.72(11) 2_655 . ?
Se11 Re12 Re11 102.71(11) 3_665 2_655 ?
Se11 Re12 Re11 55.02(8) 2_655 3_665 ?
Se11 Re12 Re11 102.72(11) . 3_665 ?
Se11 Re12 Re11 54.69(8) 2_655 2_655 ?
Se11 Re12 Re11 54.69(8) . . ?
Se11 Re12 Re11 55.01(8) . 2_655 ?
Se11 Re12 Se11 106.54(9) 2_655 3_665 ?
Se11 Re12 Se11 106.54(9) 2_655 . ?
Se11 Re12 Se11 106.54(9) . 3_665 ?
C121 Re12 Re11 136.6(8) 2_655 . ?
C121 Re12 Re11 136.6(8) . 3_665 ?
C121 Re12 Re11 94.9(8) . . ?
C121 Re12 Re11 139.7(8) . 2_655 ?
C121 Re12 Re11 94.9(8) 2_655 2_655 ?
C121 Re12 Re11 139.7(8) 2_655 3_665 ?
C121 Re12 Re11 94.9(8) 3_665 3_665 ?
C121 Re12 Re11 136.7(8) 3_665 2_655 ?
C121 Re12 Re11 139.7(8) 3_665 . ?
C121 Re12 Se11 162.3(8) 3_665 . ?
C121 Re12 Se11 162.3(8) 2_655 3_665 ?
C121 Re12 Se11 162.3(8) . 2_655 ?
C121 Re12 Se11 85.1(8) . . ?
C121 Re12 Se11 82.1(8) 3_665 2_655 ?
C121 Re12 Se11 82.1(8) . 3_665 ?
C121 Re12 Se11 82.1(8) 2_655 . ?
C121 Re12 Se11 85.1(8) 2_655 2_655 ?
C121 Re12 Se11 85.1(8) 3_665 3_665 ?
C121 Re12 C121 83.3(11) 3_665 . ?
C121 Re12 C121 83.3(11) 2_655 . ?
C121 Re12 C121 83.3(11) 2_655 3_665 ?
Re14 Re13 Re14 59.52(7) 3_565 . ?
Re14 Re13 Re14 59.52(7) 2_665 . ?
Se14 Re13 Re14 54.72(8) 2_665 2_665 ?
Se14 Re13 Re14 102.66(11) . 3_565 ?
Se14 Re13 Re14 54.72(8) . . ?
Se14 Re13 Re14 54.91(8) 2_665 3_565 ?
Se14 Re13 Re14 102.66(11) 2_665 . ?
Se14 Re13 Re14 54.72(8) 3_565 3_565 ?
Se14 Re13 Re14 54.91(8) 3_565 . ?
Se14 Re13 Re14 54.91(8) . 2_665 ?
Se14 Re13 Re14 102.66(11) 3_565 2_665 ?
Se14 Re13 Se14 106.48(9) 2_665 3_565 ?
Se14 Re13 Se14 106.48(9) 2_665 . ?
Se14 Re13 Se14 106.49(9) . 3_565 ?
C131 Re13 Re14 140.3(8) 2_665 2_665 ?
C131 Re13 Re14 138.2(8) 2_665 3_565 ?
C131 Re13 Re14 140.3(8) . . ?
C131 Re13 Re14 96.5(8) 2_665 . ?
C131 Re13 Re14 138.2(8) 3_565 . ?
C131 Re13 Re14 138.2(8) . 2_665 ?
C131 Re13 Re14 140.3(8) 3_565 3_565 ?
C131 Re13 Re14 96.5(8) 3_565 2_665 ?
C131 Re13 Re14 96.5(8) . 3_565 ?
C131 Re13 Se14 83.5(8) 2_665 3_565 ?
C131 Re13 Se14 160.8(8) . . ?
C131 Re13 Se14 85.5(8) . 3_565 ?
C131 Re13 Se14 83.5(8) 3_565 . ?
C131 Re13 Se14 83.5(8) . 2_665 ?
C131 Re13 Se14 85.5(8) 2_665 . ?
C131 Re13 Se14 160.8(8) 2_665 2_665 ?
C131 Re13 Se14 85.5(8) 3_565 2_665 ?
C131 Re13 Se14 160.8(8) 3_565 3_565 ?
C131 Re13 C131 80.9(11) 3_565 2_665 ?
C131 Re13 C131 80.9(11) . 2_665 ?
C131 Re13 C131 80.9(11) 3_565 . ?
Re14 Re14 Re13 60.24(4) 3_565 . ?
Re14 Re14 Re13 60.24(4) 2_665 . ?
Se13 Re14 Re13 103.60(9) . . ?
Se13 Re14 Re14 55.04(6) . 3_565 ?
Se13 Re14 Re14 55.04(6) . 2_665 ?
Se13 Re14 Se14 107.12(9) . . ?
Se13 Re14 Se14 106.88(9) . 3_565 ?
Se14 Re14 Re13 54.87(7) . . ?
Se14 Re14 Re13 54.81(7) 3_565 . ?
Se14 Re14 Re14 103.37(8) . 3_565 ?
Se14 Re14 Re14 103.16(8) 3_565 2_665 ?
Se14 Re14 Re14 55.24(8) . 2_665 ?
Se14 Re14 Re14 54.98(8) 3_565 3_565 ?
Se14 Re14 Se14 106.54(14) . 3_565 ?
C141 Re14 Re13 139.2(7) . . ?
C141 Re14 Re14 95.5(7) . 3_565 ?
C141 Re14 Re14 138.4(7) . 2_665 ?
C141 Re14 Se13 83.4(7) . . ?
C141 Re14 Se14 84.5(7) . 3_565 ?
C141 Re14 Se14 161.1(7) . . ?
C142 Re14 Re13 96.9(7) . . ?
C142 Re14 Re14 140.7(8) . 3_565 ?
C142 Re14 Re14 139.0(8) . 2_665 ?
C142 Re14 Se13 159.4(7) . . ?
C142 Re14 Se14 83.8(8) . . ?
C142 Re14 Se14 85.8(8) . 3_565 ?
C142 Re14 C141 81.7(10) . . ?
C142 Re14 C143 80.8(11) . . ?
C143 Re14 Re13 139.9(7) . . ?
C143 Re14 Re14 95.6(8) . 2_665 ?
C143 Re14 Re14 137.7(7) . 3_565 ?
C143 Re14 Se13 82.8(7) . . ?
C143 Re14 Se14 161.2(8) . 3_565 ?
C143 Re14 Se14 85.2(7) . . ?
C143 Re14 C141 80.5(10) . . ?
Mo2 Mo1 Mo3 59.62(5) . . ?
Mo2 Mo1 Mo4 60.18(5) . . ?
Mo4 Mo1 Mo3 59.81(6) . . ?
Se1 Mo1 Mo2 55.26(8) . . ?
Se1 Mo1 Mo3 102.86(9) . . ?
Se1 Mo1 Mo4 54.79(8) . . ?
Se2 Mo1 Mo2 55.28(8) . . ?
Se2 Mo1 Mo3 55.00(8) . . ?
Se2 Mo1 Mo4 103.60(9) . . ?
Se2 Mo1 Se1 107.47(11) . . ?
Se2 Mo1 Se3 106.38(11) . . ?
Se3 Mo1 Mo2 103.09(9) . . ?
Se3 Mo1 Mo3 54.85(8) . . ?
Se3 Mo1 Mo4 54.94(8) . . ?
Se3 Mo1 Se1 106.63(11) . . ?
C11 Mo1 Mo2 94.9(8) . . ?
C11 Mo1 Mo3 139.9(8) . . ?
C11 Mo1 Mo4 136.8(8) . . ?
C11 Mo1 Se1 82.0(8) . . ?
C11 Mo1 Se2 85.3(8) . . ?
C11 Mo1 Se3 161.9(8) . . ?
C11 Mo1 C13 82.2(11) . . ?
C12 Mo1 Mo2 140.5(7) . . ?
C12 Mo1 Mo3 141.6(7) . . ?
C12 Mo1 Mo4 98.9(8) . . ?
C12 Mo1 Se1 85.3(7) . . ?
C12 Mo1 Se2 157.5(8) . . ?
C12 Mo1 Se3 86.7(7) . . ?
C12 Mo1 C11 78.1(11) . . ?
C12 Mo1 C13 79.5(10) . . ?
C13 Mo1 Mo2 138.6(7) . . ?
C13 Mo1 Mo3 97.1(7) . . ?
C13 Mo1 Mo4 140.4(7) . . ?
C13 Mo1 Se1 160.0(7) . . ?
C13 Mo1 Se2 83.4(7) . . ?
C13 Mo1 Se3 85.5(7) . . ?
Mo1 Mo2 Mo4 60.11(5) . . ?
Mo3 Mo2 Mo1 60.40(5) . . ?
Mo3 Mo2 Mo4 60.04(5) . . ?
Se1 Mo2 Mo1 54.97(8) . . ?
Se1 Mo2 Mo3 103.26(9) . . ?
Se1 Mo2 Mo4 54.69(8) . . ?
Se2 Mo2 Mo1 54.79(8) . . ?
Se2 Mo2 Mo3 55.19(8) . . ?
Se2 Mo2 Mo4 103.15(9) . . ?
Se2 Mo2 Se1 106.73(11) . . ?
Se4 Mo2 Mo1 103.59(9) . . ?
Se4 Mo2 Mo3 55.17(8) . . ?
Se4 Mo2 Mo4 54.89(8) . . ?
Se4 Mo2 Se1 106.24(11) . . ?
Se4 Mo2 Se2 107.37(11) . . ?
C21 Mo2 Mo1 96.8(8) . . ?
C21 Mo2 Mo3 138.8(8) . . ?
C21 Mo2 Mo4 140.8(9) . . ?
C21 Mo2 Se1 86.2(9) . . ?
C21 Mo2 Se2 83.6(8) . . ?
C21 Mo2 Se4 159.6(8) . . ?
C21 Mo2 C22 78.4(12) . . ?
C21 Mo2 C23 80.2(12) . . ?
C22 Mo2 Mo1 136.9(8) . . ?
C22 Mo2 Mo3 95.3(8) . . ?
C22 Mo2 Mo4 140.5(8) . . ?
C22 Mo2 Se1 161.4(8) . . ?
C22 Mo2 Se2 82.1(8) . . ?
C22 Mo2 Se4 85.9(8) . . ?
C22 Mo2 C23 82.0(11) . . ?
C23 Mo2 Mo1 140.0(8) . . ?
C23 Mo2 Mo3 139.9(8) . . ?
C23 Mo2 Mo4 97.6(8) . . ?
C23 Mo2 Se1 85.1(8) . . ?
C23 Mo2 Se2 159.2(8) . . ?
C23 Mo2 Se4 84.8(8) . . ?
Mo2 Mo3 Mo1 59.97(5) . . ?
Mo2 Mo3 Mo4 60.40(5) . . ?
Mo4 Mo3 Mo1 60.09(6) . . ?
Se2 Mo3 Mo1 54.66(8) . . ?
Se2 Mo3 Mo2 55.34(8) . . ?
Se2 Mo3 Mo4 103.56(9) . . ?
Se3 Mo3 Mo1 54.86(8) . . ?
Se3 Mo3 Mo2 103.39(9) . . ?
Se3 Mo3 Mo4 55.06(8) . . ?
Se3 Mo3 Se2 106.07(11) . . ?
Se3 Mo3 Se4 107.03(11) . . ?
Se4 Mo3 Mo1 103.29(9) . . ?
Se4 Mo3 Mo2 55.23(8) . . ?
Se4 Mo3 Mo4 55.04(8) . . ?
Se4 Mo3 Se2 107.57(11) . . ?
C31 Mo3 Mo1 139.2(7) . . ?
C31 Mo3 Mo2 95.0(7) . . ?
C31 Mo3 Mo4 137.8(7) . . ?
C31 Mo3 Se2 84.8(7) . . ?
C31 Mo3 Se3 161.6(7) . . ?
C31 Mo3 Se4 82.9(7) . . ?
C31 Mo3 C33 81.3(10) . . ?
C32 Mo3 Mo1 140.9(7) . . ?
C32 Mo3 Mo2 137.8(7) . . ?
C32 Mo3 Mo4 96.2(7) . . ?
C32 Mo3 Se2 160.2(7) . . ?
C32 Mo3 Se3 86.3(7) . . ?
C32 Mo3 Se4 82.6(7) . . ?
C32 Mo3 C31 79.6(10) . . ?
C32 Mo3 C33 81.8(10) . . ?
C33 Mo3 Mo1 97.2(7) . . ?
C33 Mo3 Mo2 139.3(7) . . ?
C33 Mo3 Mo4 140.1(7) . . ?
C33 Mo3 Se2 83.9(7) . . ?
C33 Mo3 Se3 85.1(7) . . ?
C33 Mo3 Se4 159.5(7) . . ?
Mo1 Mo4 Mo2 59.70(5) . . ?
Mo3 Mo4 Mo1 60.10(5) . . ?
Mo3 Mo4 Mo2 59.56(5) . . ?
Se1 Mo4 Mo1 54.90(8) . . ?
Se1 Mo4 Mo2 55.09(8) . . ?
Se1 Mo4 Mo3 103.19(9) . . ?
Se1 Mo4 Se3 106.64(11) . . ?
Se1 Mo4 Se4 106.61(11) . . ?
Se3 Mo4 Mo1 54.83(8) . . ?
Se3 Mo4 Mo2 102.62(9) . . ?
Se3 Mo4 Mo3 54.94(8) . . ?
Se3 Mo4 Se4 106.85(11) . . ?
Se4 Mo4 Mo1 103.25(9) . . ?
Se4 Mo4 Mo2 54.88(8) . . ?
Se4 Mo4 Mo3 54.98(8) . . ?
C41 Mo4 Mo1 137.7(8) . . ?
C41 Mo4 Mo2 95.4(8) . . ?
C41 Mo4 Mo3 138.9(8) . . ?
C41 Mo4 Se1 83.0(8) . . ?
C41 Mo4 Se3 162.0(8) . . ?
C41 Mo4 Se4 84.1(8) . . ?
C41 Mo4 C43 81.4(11) . . ?
C42 Mo4 Mo1 95.3(9) . . ?
C42 Mo4 Mo2 139.2(8) . . ?
C42 Mo4 Mo3 138.2(8) . . ?
C42 Mo4 Se1 84.4(8) . . ?
C42 Mo4 Se3 83.4(8) . . ?
C42 Mo4 Se4 161.5(9) . . ?
C42 Mo4 C41 82.5(11) . . ?
C42 Mo4 C43 80.4(11) . . ?
C43 Mo4 Mo1 140.1(7) . . ?
C43 Mo4 Mo2 139.8(7) . . ?
C43 Mo4 Mo3 97.4(8) . . ?
C43 Mo4 Se1 159.4(8) . . ?
C43 Mo4 Se3 85.3(7) . . ?
C43 Mo4 Se4 85.0(7) . . ?
Mo6 Mo5 Mo7 60.09(6) . . ?
Mo6 Mo5 Mo8 60.30(6) . . ?
Mo7 Mo5 Mo8 59.95(6) . . ?
Se5 Mo5 Mo6 103.61(9) . . ?
Se5 Mo5 Mo7 55.14(8) . . ?
Se5 Mo5 Mo8 55.00(8) . . ?
Se7 Mo5 Mo6 55.20(8) . . ?
Se7 Mo5 Mo7 55.31(8) . . ?
Se7 Mo5 Mo8 103.70(9) . . ?
Se7 Mo5 Se5 107.12(11) . . ?
Se7 Mo5 Se8 107.25(11) . . ?
Se8 Mo5 Mo6 55.15(8) . . ?
Se8 Mo5 Mo7 103.13(9) . . ?
Se8 Mo5 Mo8 54.83(8) . . ?
Se8 Mo5 Se5 106.59(11) . . ?
C51 Mo5 Mo6 95.5(7) . . ?
C51 Mo5 Mo7 140.7(7) . . ?
C51 Mo5 Mo8 137.1(7) . . ?
C51 Mo5 Se5 160.7(7) . . ?
C51 Mo5 Se7 85.7(7) . . ?
C51 Mo5 Se8 82.3(7) . . ?
C52 Mo5 Mo6 139.4(7) . . ?
C52 Mo5 Mo7 98.4(7) . . ?
C52 Mo5 Mo8 141.4(7) . . ?
C52 Mo5 Se5 86.5(7) . . ?
C52 Mo5 Se7 84.2(7) . . ?
C52 Mo5 Se8 158.5(7) . . ?
C52 Mo5 C51 80.4(10) . . ?
C53 Mo5 Mo6 141.1(7) . . ?
C53 Mo5 Mo7 139.3(8) . . ?
C53 Mo5 Mo8 97.8(7) . . ?
C53 Mo5 Se5 84.2(8) . . ?
C53 Mo5 Se7 158.5(7) . . ?
C53 Mo5 Se8 86.0(7) . . ?
C53 Mo5 C51 79.3(10) . . ?
C53 Mo5 C52 78.2(10) . . ?
Mo5 Mo6 Mo7 59.97(5) . . ?
Mo5 Mo6 Mo8 60.00(6) . . ?
Mo7 Mo6 Mo8 59.81(5) . . ?
Se6 Mo6 Mo5 103.07(9) . . ?
Se6 Mo6 Mo7 54.98(8) . . ?
Se6 Mo6 Mo8 54.61(8) . . ?
Se6 Mo6 Se7 107.10(11) . . ?
Se6 Mo6 Se8 106.04(11) . . ?
Se7 Mo6 Mo5 55.01(8) . . ?
Se7 Mo6 Mo7 55.21(8) . . ?
Se7 Mo6 Mo8 103.29(9) . . ?
Se8 Mo6 Mo5 55.09(8) . . ?
Se8 Mo6 Mo7 102.99(9) . . ?
Se8 Mo6 Mo8 54.69(8) . . ?
Se8 Mo6 Se7 107.01(11) . . ?
C61 Mo6 Mo5 138.6(7) . . ?
C61 Mo6 Mo7 95.2(8) . . ?
C61 Mo6 Mo8 138.3(8) . . ?
C61 Mo6 Se6 83.9(8) . . ?
C61 Mo6 Se7 83.8(7) . . ?
C61 Mo6 Se8 161.8(8) . . ?
C62 Mo6 Mo5 142.9(9) . . ?
C62 Mo6 Mo7 139.0(9) . . ?
C62 Mo6 Mo8 99.1(9) . . ?
C62 Mo6 Se6 84.1(9) . . ?
C62 Mo6 Se7 157.5(9) . . ?
C62 Mo6 Se8 87.8(9) . . ?
C62 Mo6 C61 77.9(12) . . ?
C62 Mo6 C63 81.6(12) . . ?
C63 Mo6 Mo5 95.2(8) . . ?
C63 Mo6 Mo7 138.0(8) . . ?
C63 Mo6 Mo8 139.2(8) . . ?
C63 Mo6 Se6 161.8(8) . . ?
C63 Mo6 Se7 82.9(8) . . ?
C63 Mo6 Se8 84.7(8) . . ?
C63 Mo6 C61 82.1(11) . . ?
Mo5 Mo7 Mo6 59.94(5) . . ?
Mo5 Mo7 Mo8 60.15(5) . . ?
Mo8 Mo7 Mo6 60.32(6) . . ?
Se5 Mo7 Mo5 55.15(8) . . ?
Se5 Mo7 Mo6 103.50(9) . . ?
Se5 Mo7 Mo8 55.09(8) . . ?
Se5 Mo7 Se7 106.80(11) . . ?
Se6 Mo7 Mo5 102.99(9) . . ?
Se6 Mo7 Mo6 54.92(8) . . ?
Se6 Mo7 Mo8 54.80(8) . . ?
Se6 Mo7 Se5 106.82(11) . . ?
Se6 Mo7 Se7 106.89(11) . . ?
Se7 Mo7 Mo5 54.95(8) . . ?
Se7 Mo7 Mo6 55.05(8) . . ?
Se7 Mo7 Mo8 103.58(9) . . ?
C71 Mo7 Mo5 136.9(7) . . ?
C71 Mo7 Mo6 138.8(7) . . ?
C71 Mo7 Mo8 93.8(7) . . ?
C71 Mo7 Se5 82.0(7) . . ?
C71 Mo7 Se6 84.2(7) . . ?
C71 Mo7 Se7 162.5(7) . . ?
C71 Mo7 C72 81.6(10) . . ?
C71 Mo7 C73 81.4(10) . . ?
C72 Mo7 Mo5 96.0(7) . . ?
C72 Mo7 Mo6 139.3(7) . . ?
C72 Mo7 Mo8 138.7(7) . . ?
C72 Mo7 Se5 83.7(7) . . ?
C72 Mo7 Se6 161.0(7) . . ?
C72 Mo7 Se7 84.4(8) . . ?
C72 Mo7 C73 81.0(10) . . ?
C73 Mo7 Mo5 141.0(7) . . ?
C73 Mo7 Mo6 97.6(7) . . ?
C73 Mo7 Mo8 139.2(7) . . ?
C73 Mo7 Se5 158.8(7) . . ?
C73 Mo7 Se6 84.4(7) . . ?
C73 Mo7 Se7 86.2(7) . . ?
Mo5 Mo8 Mo6 59.70(5) . . ?
Mo7 Mo8 Mo5 59.90(5) . . ?
Mo7 Mo8 Mo6 59.87(5) . . ?
Se5 Mo8 Mo5 55.06(8) . . ?
Se5 Mo8 Mo6 103.17(9) . . ?
Se5 Mo8 Mo7 55.13(8) . . ?
Se6 Mo8 Mo5 102.98(9) . . ?
Se6 Mo8 Mo6 54.80(8) . . ?
Se6 Mo8 Mo7 55.05(8) . . ?
Se6 Mo8 Se5 107.10(11) . . ?
Se6 Mo8 Se8 106.47(11) . . ?
Se8 Mo8 Mo5 55.04(8) . . ?
Se8 Mo8 Mo6 54.96(8) . . ?
Se8 Mo8 Mo7 103.25(9) . . ?
Se8 Mo8 Se5 106.84(11) . . ?
C81 Mo8 Mo5 139.9(7) . . ?
C81 Mo8 Mo6 139.0(7) . . ?
C81 Mo8 Mo7 96.6(7) . . ?
C81 Mo8 Se5 85.0(7) . . ?
C81 Mo8 Se6 84.3(7) . . ?
C81 Mo8 Se8 160.2(7) . . ?
C82 Mo8 Mo5 96.1(8) . . ?
C82 Mo8 Mo6 139.9(8) . . ?
C82 Mo8 Mo7 138.1(8) . . ?
C82 Mo8 Se5 83.1(8) . . ?
C82 Mo8 Se6 160.9(8) . . ?
C82 Mo8 Se8 85.1(9) . . ?
C82 Mo8 C81 80.5(11) . . ?
C82 Mo8 C83 81.1(12) . . ?
C83 Mo8 Mo5 138.3(8) . . ?
C83 Mo8 Mo6 96.4(8) . . ?
C83 Mo8 Mo7 140.1(8) . . ?
C83 Mo8 Se5 160.4(8) . . ?
C83 Mo8 Se6 85.2(8) . . ?
C83 Mo8 Se8 83.3(8) . . ?
C83 Mo8 C81 81.0(10) . . ?
Se9 Mo9 Mo10 103.00(9) . . ?
Se9 Mo9 Se10 106.73(9) . . ?
Se9 Mo9 Se10 106.44(9) . 3_675 ?
Se10 Mo9 Mo10 55.16(7) . . ?
Se10 Mo9 Mo10 55.08(7) 3_675 . ?
Se10 Mo9 Se10 107.11(14) . 3_675 ?
C91 Mo9 Mo10 140.0(7) . . ?
C91 Mo9 Se9 84.9(7) . . ?
C91 Mo9 Se10 159.4(7) . . ?
C91 Mo9 Se10 85.0(7) . 3_675 ?
C91 Mo9 C92 81.0(10) . . ?
C91 Mo9 C93 79.0(10) . . ?
C92 Mo9 Mo10 95.6(7) . . ?
C92 Mo9 Se9 161.4(7) . . ?
C92 Mo9 Se10 84.4(7) . 3_675 ?
C92 Mo9 Se10 83.6(7) . . ?
C93 Mo9 Mo10 140.3(8) . . ?
C93 Mo9 Se9 83.2(8) . . ?
C93 Mo9 Se10 160.6(8) . 3_675 ?
C93 Mo9 Se10 85.4(8) . . ?
C93 Mo9 C92 82.3(10) . . ?
Se10 Mo10 Mo9 54.79(8) . . ?
Se10 Mo10 Mo9 103.18(11) 2_765 . ?
Se10 Mo10 Mo9 55.02(8) 3_675 . ?
Se10 Mo10 Se10 106.70(9) 3_675 2_765 ?
Se10 Mo10 Se10 106.70(9) . 3_675 ?
Se10 Mo10 Se10 106.70(9) . 2_765 ?
C101 Mo10 Mo9 141.4(8) 3_675 . ?
C101 Mo10 Mo9 97.8(8) . . ?
C101 Mo10 Mo9 139.0(8) 2_765 . ?
C101 Mo10 Se10 86.4(8) 2_765 2_765 ?
C101 Mo10 Se10 84.2(8) . 3_675 ?
C101 Mo10 Se10 159.0(8) . 2_765 ?
C101 Mo10 Se10 159.0(8) 3_675 . ?
C101 Mo10 Se10 86.4(8) . . ?
C101 Mo10 Se10 159.0(8) 2_765 3_675 ?
C101 Mo10 Se10 84.2(8) 2_765 . ?
C101 Mo10 Se10 84.2(8) 3_675 2_765 ?
C101 Mo10 Se10 86.4(8) 3_675 3_675 ?
C101 Mo10 C101 78.5(12) . 2_765 ?
C101 Mo10 C101 78.5(12) 2_765 3_675 ?
C101 Mo10 C101 78.5(12) . 3_675 ?
Se11 Mo11 Mo12 54.90(7) 3_665 . ?
Se11 Mo11 Mo12 55.01(7) . . ?
Se11 Mo11 Se11 106.74(14) . 3_665 ?
Se11 Mo11 Se12 107.27(9) . . ?
Se12 Mo11 Mo12 103.68(9) . . ?
Se12 Mo11 Se11 106.85(9) . 3_665 ?
C111 Mo11 Mo12 96.0(7) . . ?
C111 Mo11 Se11 84.4(8) . . ?
C111 Mo11 Se11 83.9(8) . 3_665 ?
C111 Mo11 Se12 160.3(7) . . ?
C112 Mo11 Mo12 140.0(7) . . ?
C112 Mo11 Se11 159.4(7) . . ?
C112 Mo11 Se11 85.1(7) . 3_665 ?
C112 Mo11 Se12 84.4(7) . . ?
C112 Mo11 C111 80.1(10) . . ?
C112 Mo11 C113 79.7(10) . . ?
C113 Mo11 Mo12 139.8(7) . . ?
C113 Mo11 Se11 84.9(7) . . ?
C113 Mo11 Se11 161.2(7) . 3_665 ?
C113 Mo11 Se12 82.8(7) . . ?
C113 Mo11 C111 82.6(10) . . ?
Se11 Mo12 Mo11 54.69(8) . . ?
Se11 Mo12 Mo11 102.72(11) 2_655 . ?
Se11 Mo12 Mo11 55.02(8) 3_665 . ?
Se11 Mo12 Se11 106.54(9) . 3_665 ?
Se11 Mo12 Se11 106.54(9) 2_655 3_665 ?
Se11 Mo12 Se11 106.54(9) 2_655 . ?
C121 Mo12 Mo11 139.7(8) 3_665 . ?
C121 Mo12 Mo11 136.6(8) 2_655 . ?
C121 Mo12 Mo11 94.9(8) . . ?
C121 Mo12 Se11 82.1(8) . 3_665 ?
C121 Mo12 Se11 82.1(8) 2_655 . ?
C121 Mo12 Se11 85.1(8) . . ?
C121 Mo12 Se11 162.3(8) 2_655 3_665 ?
C121 Mo12 Se11 85.1(8) 3_665 3_665 ?
C121 Mo12 Se11 162.3(8) 3_665 . ?
C121 Mo12 Se11 85.1(8) 2_655 2_655 ?
C121 Mo12 Se11 82.1(8) 3_665 2_655 ?
C121 Mo12 Se11 162.3(8) . 2_655 ?
C121 Mo12 C121 83.3(11) 2_655 . ?
C121 Mo12 C121 83.3(11) 2_655 3_665 ?
C121 Mo12 C121 83.3(11) 3_665 . ?
Se14 Mo13 Mo14 102.66(11) 2_665 . ?
Se14 Mo13 Mo14 54.72(8) . . ?
Se14 Mo13 Mo14 54.91(8) 3_565 . ?
Se14 Mo13 Se14 106.48(9) 2_665 3_565 ?
Se14 Mo13 Se14 106.49(9) . 3_565 ?
Se14 Mo13 Se14 106.48(9) 2_665 . ?
C131 Mo13 Mo14 140.3(8) . . ?
C131 Mo13 Mo14 138.2(8) 3_565 . ?
C131 Mo13 Mo14 96.5(8) 2_665 . ?
C131 Mo13 Se14 83.5(8) . 2_665 ?
C131 Mo13 Se14 83.5(8) 3_565 . ?
C131 Mo13 Se14 85.5(8) . 3_565 ?
C131 Mo13 Se14 85.5(8) 3_565 2_665 ?
C131 Mo13 Se14 160.8(8) 3_565 3_565 ?
C131 Mo13 Se14 160.8(8) 2_665 2_665 ?
C131 Mo13 Se14 83.5(8) 2_665 3_565 ?
C131 Mo13 Se14 85.5(8) 2_665 . ?
C131 Mo13 Se14 160.8(8) . . ?
C131 Mo13 C131 80.9(11) . 2_665 ?
C131 Mo13 C131 80.9(11) 3_565 . ?
C131 Mo13 C131 80.9(11) 3_565 2_665 ?
Se13 Mo14 Mo13 103.60(9) . . ?
Se13 Mo14 Se14 106.88(9) . 3_565 ?
Se13 Mo14 Se14 107.12(9) . . ?
Se14 Mo14 Mo13 54.81(7) 3_565 . ?
Se14 Mo14 Mo13 54.87(7) . . ?
Se14 Mo14 Se14 106.54(14) . 3_565 ?
C141 Mo14 Mo13 139.2(7) . . ?
C141 Mo14 Se13 83.4(7) . . ?
C141 Mo14 Se14 84.5(7) . 3_565 ?
C141 Mo14 Se14 161.1(7) . . ?
C142 Mo14 Mo13 96.9(7) . . ?
C142 Mo14 Se13 159.4(7) . . ?
C142 Mo14 Se14 85.8(8) . 3_565 ?
C142 Mo14 Se14 83.8(8) . . ?
C142 Mo14 C141 81.7(10) . . ?
C142 Mo14 C143 80.8(11) . . ?
C143 Mo14 Mo13 139.9(7) . . ?
C143 Mo14 Se13 82.8(7) . . ?
C143 Mo14 Se14 85.2(7) . . ?
C143 Mo14 Se14 161.2(8) . 3_565 ?
C143 Mo14 C141 80.5(10) . . ?
Re1 Se1 Re2 69.78(9) . . ?
Re4 Se1 Re1 70.31(9) . . ?
Re4 Se1 Re2 70.22(9) . . ?
Mo1 Se1 Mo2 69.78(9) . . ?
Mo1 Se1 K3 136.34(15) . 1_554 ?
Mo2 Se1 K3 85.00(13) . 1_554 ?
Mo4 Se1 Mo1 70.31(9) . . ?
Mo4 Se1 Mo2 70.22(9) . . ?
Mo4 Se1 K3 134.10(15) . 1_554 ?
Re1 Se2 Re2 69.93(9) . . ?
Re1 Se2 Re3 70.35(9) . . ?
Re3 Se2 Re2 69.48(9) . . ?
Mo1 Se2 Mo2 69.93(9) . . ?
Mo1 Se2 Mo3 70.35(9) . . ?
Mo3 Se2 Mo2 69.48(9) . . ?
Re1 Se3 Re4 70.23(9) . . ?
Re3 Se3 Re1 70.30(9) . . ?
Re3 Se3 Re4 70.00(9) . . ?
Mo1 Se3 Mo4 70.23(9) . . ?
Mo3 Se3 Mo1 70.30(9) . . ?
Mo3 Se3 Mo4 70.00(9) . . ?
Re2 Se4 Re4 70.24(9) . . ?
Re3 Se4 Re2 69.60(9) . . ?
Re3 Se4 Re4 69.98(9) . . ?
Mo2 Se4 Mo4 70.24(9) . . ?
Mo2 Se4 K7 84.76(13) . 1_554 ?
Mo3 Se4 Mo2 69.60(9) . . ?
Mo3 Se4 Mo4 69.98(9) . . ?
Mo3 Se4 K7 135.84(15) . 1_554 ?
Mo4 Se4 K7 134.51(15) . 1_554 ?
Re5 Se5 K11 84.94(13) . . ?
Re7 Se5 Re5 69.71(9) . . ?
Re7 Se5 K11 135.36(14) . . ?
Re8 Se5 Re5 69.94(9) . . ?
Re8 Se5 Re7 69.78(9) . . ?
Re8 Se5 K11 135.25(14) . . ?
Mo5 Se5 K11 84.94(13) . . ?
Mo7 Se5 Mo5 69.71(9) . . ?
Mo7 Se5 K11 135.36(14) . . ?
Mo8 Se5 Mo5 69.94(9) . . ?
Mo8 Se5 Mo7 69.78(9) . . ?
Mo8 Se5 K11 135.25(14) . . ?
Re6 Se6 Re7 70.10(9) . . ?
Re8 Se6 Re6 70.59(9) . . ?
Re8 Se6 Re7 70.14(9) . . ?
Mo6 Se6 Mo7 70.10(9) . . ?
Mo8 Se6 Mo6 70.59(9) . . ?
Mo8 Se6 Mo7 70.14(9) . . ?
Re5 Se7 Re6 69.79(9) . . ?
Re5 Se7 Re7 69.74(9) . . ?
Re5 Se7 K17 83.05(13) . . ?
Re6 Se7 Re7 69.74(9) . . ?
Re6 Se7 K17 132.97(15) . . ?
Re7 Se7 K17 135.33(15) . . ?
Mo5 Se7 Mo6 69.79(9) . . ?
Mo5 Se7 Mo7 69.74(9) . . ?
Mo5 Se7 K17 83.05(13) . . ?
Mo6 Se7 Mo7 69.74(9) . . ?
Mo6 Se7 K17 132.97(15) . . ?
Mo7 Se7 K17 135.33(15) . . ?
Re5 Se8 Re6 69.76(9) . . ?
Re8 Se8 Re5 70.13(9) . . ?
Re8 Se8 Re6 70.35(9) . . ?
Mo5 Se8 Mo6 69.76(9) . . ?
Mo8 Se8 Mo5 70.13(9) . . ?
Mo8 Se8 Mo6 70.35(9) . . ?
Re9 Se9 Re9 70.35(12) . 2_765 ?
Mo9 Se9 Re9 70.35(12) . 3_675 ?
Mo9 Se9 Re9 70.35(12) . 2_765 ?
Re9 Se10 Re9 70.16(10) . 2_765 ?
Re9 Se10 Re10 69.90(9) 2_765 . ?
Re9 Se10 Re10 70.05(9) . . ?
Mo9 Se10 Re9 70.16(10) . 2_765 ?
Mo9 Se10 Mo10 70.05(9) . . ?
Re11 Se11 Re11 69.67(10) . 2_655 ?
Re11 Se11 Re12 70.29(9) . . ?
Re12 Se11 Re11 70.08(9) . 2_655 ?
Mo11 Se11 Re11 69.67(10) . 2_655 ?
Mo11 Se11 Mo12 70.29(9) . . ?
Mo12 Se11 Re11 70.08(9) . 2_655 ?
Re11 Se12 Re11 69.78(12) 3_665 . ?
Re11 Se12 Re11 69.78(12) 2_655 . ?
Re14 Se13 Re14 69.92(12) 3_565 . ?
Re14 Se13 Re14 69.92(12) 2_665 . ?
Re13 Se14 Re14 70.28(9) . 2_665 ?
Re14 Se14 Re13 70.41(9) . . ?
Re14 Se14 Re14 69.78(10) . 2_665 ?
Mo13 Se14 Re14 70.28(9) . 2_665 ?
Mo14 Se14 Re14 69.78(10) . 2_665 ?
Mo14 Se14 Mo13 70.41(9) . . ?
O1 K1 K2 74.7(5) . . ?
O1 K1 O3 105.9(7) . . ?
O1 K1 N12 78.9(6) . . ?
O1 K1 N91 161.2(7) . 3_566 ?
O1 K1 N93 83.1(6) . 2_656 ?
O1 K1 N101 124.1(7) . 3_565 ?
O1 K1 N101 59.3(6) . 2_655 ?
O1 K1 C91 153.5(6) . 3_566 ?
O1 K1 C93 95.9(6) . 2_656 ?
O1 K1 C101 66.2(7) . 2_655 ?
O1 K1 C101 104.0(7) . 3_565 ?
O3 K1 K2 101.9(6) . . ?
O3 K1 N12 57.3(7) . . ?
O3 K1 N91 80.4(7) . 3_566 ?
O3 K1 N93 136.9(7) . 2_656 ?
O3 K1 N101 85.2(7) . 3_565 ?
O3 K1 N101 148.9(7) . 2_655 ?
O3 K1 C91 96.8(7) . 3_566 ?
O3 K1 C93 143.0(7) . 2_656 ?
O3 K1 C101 95.7(8) . 3_565 ?
O3 K1 C101 131.9(7) . 2_655 ?
N12 K1 K2 46.1(4) . . ?
N12 K1 N101 133.5(6) . 2_655 ?
N12 K1 C91 103.0(6) . 3_566 ?
N12 K1 C93 99.6(6) . 2_656 ?
N12 K1 C101 145.1(7) . 2_655 ?
N91 K1 K2 86.7(5) 3_566 . ?
N91 K1 N12 90.4(6) 3_566 . ?
N91 K1 N101 73.5(6) 3_566 3_565 ?
N91 K1 N101 122.9(6) 3_566 2_655 ?
N91 K1 C91 17.0(6) 3_566 3_566 ?
N91 K1 C93 70.4(7) 3_566 2_656 ?
N91 K1 C101 92.7(7) 3_566 3_565 ?
N91 K1 C101 123.0(7) 3_566 2_655 ?
N93 K1 K2 38.7(5) 2_656 . ?
N93 K1 N12 84.6(6) 2_656 . ?
N93 K1 N91 80.5(6) 2_656 3_566 ?
N93 K1 N101 125.0(7) 2_656 3_565 ?
N93 K1 N101 71.9(6) 2_656 2_655 ?
N93 K1 C91 71.0(6) 2_656 3_566 ?
N93 K1 C93 18.1(6) 2_656 2_656 ?
N93 K1 C101 123.5(7) 2_656 3_565 ?
N93 K1 C101 90.7(7) 2_656 2_655 ?
N101 K1 K2 157.6(5) 3_565 . ?
N101 K1 K2 99.9(5) 2_655 . ?
N101 K1 N12 141.5(7) 3_565 . ?
N101 K1 N101 83.0(9) 3_565 2_655 ?
N101 K1 C91 70.4(6) 3_565 3_566 ?
N101 K1 C91 106.1(6) 2_655 3_566 ?
N101 K1 C93 107.0(7) 3_565 2_656 ?
N101 K1 C93 68.1(6) 2_655 2_656 ?
N101 K1 C101 20.6(6) 3_565 3_565 ?
N101 K1 C101 66.4(7) 3_565 2_655 ?
N101 K1 C101 19.7(6) 2_655 2_655 ?
C91 K1 K2 87.6(5) 3_566 . ?
C93 K1 K2 55.2(5) 2_656 . ?
C93 K1 C91 57.7(6) 2_656 3_566 ?
C101 K1 K2 119.2(5) 2_655 . ?
C101 K1 K2 162.0(5) 3_565 . ?
C101 K1 N12 151.9(7) 3_565 . ?
C101 K1 N101 65.5(7) 3_565 2_655 ?
C101 K1 C91 108.0(7) 2_655 3_566 ?
C101 K1 C91 86.7(7) 3_565 3_566 ?
C101 K1 C93 107.8(7) 3_565 2_656 ?
C101 K1 C93 84.2(7) 2_655 2_656 ?
C101 K1 C101 47.3(10) 3_565 2_655 ?
K1 K2 K4 144.3(3) . . ?
K1 K2 K15 61.32(16) . 2_655 ?
K3 K2 K1 81.6(2) . . ?
K3 K2 K4 87.7(2) . . ?
K3 K2 K15 142.9(3) . 2_655 ?
K15 K2 K4 121.5(2) 2_655 . ?
O14 K2 K1 77.9(5) 2_655 . ?
O14 K2 K3 134.9(6) 2_655 . ?
O14 K2 K4 86.2(5) 2_655 . ?
O14 K2 K15 40.4(5) 2_655 2_655 ?
O14 K2 N12 90.1(7) 2_655 . ?
O14 K2 N13 53.8(6) 2_655 . ?
O14 K2 O15 74.0(8) 2_655 2_656 ?
N12 K2 K1 50.6(5) . . ?
N12 K2 K3 46.8(5) . . ?
N12 K2 K4 98.3(5) . . ?
N12 K2 K15 102.4(5) . 2_655 ?
N12 K2 N13 77.9(6) . . ?
N13 K2 K1 108.8(4) . . ?
N13 K2 K3 97.2(4) . . ?
N13 K2 K4 38.9(4) . . ?
N13 K2 K15 94.2(4) . 2_655 ?
N21 K2 K1 131.4(7) 1_556 . ?
N21 K2 K3 52.0(6) 1_556 . ?
N21 K2 K4 39.6(6) 1_556 . ?
N21 K2 K15 161.1(7) 1_556 2_655 ?
N21 K2 O14 122.7(8) 1_556 2_655 ?
N21 K2 N12 83.3(8) 1_556 . ?
N21 K2 N13 69.2(7) 1_556 . ?
N21 K2 N93 157.6(8) 1_556 2_656 ?
N21 K2 O2 72.0(7) 1_556 1_556 ?
N21 K2 O15 115.2(10) 1_556 2_656 ?
N93 K2 K1 40.6(5) 2_656 . ?
N93 K2 K3 109.4(5) 2_656 . ?
N93 K2 K4 162.4(5) 2_656 . ?
N93 K2 K15 41.3(5) 2_656 2_655 ?
N93 K2 O14 78.9(7) 2_656 2_655 ?
N93 K2 N12 91.0(7) 2_656 . ?
N93 K2 N13 130.8(6) 2_656 . ?
N93 K2 O2 85.7(6) 2_656 1_556 ?
N93 K2 O15 74.5(9) 2_656 2_656 ?
O2 K2 K1 84.5(5) 1_556 . ?
O2 K2 K3 43.4(4) 1_556 . ?
O2 K2 K4 110.4(5) 1_556 . ?
O2 K2 K15 126.5(5) 1_556 2_655 ?
O2 K2 O14 162.1(7) 1_556 2_655 ?
O2 K2 N12 81.0(6) 1_556 . ?
O2 K2 N13 137.4(6) 1_556 . ?
O2 K2 O15 110.8(9) 1_556 2_656 ?
O15 K2 K1 112.8(7) 2_656 . ?
O15 K2 K3 151.0(7) 2_656 . ?
O15 K2 K4 92.6(8) 2_656 . ?
O15 K2 K15 57.7(7) 2_656 2_655 ?
O15 K2 N12 160.1(9) 2_656 . ?
O15 K2 N13 101.1(8) 2_656 . ?
Se1 K3 K2 89.95(19) 1_556 . ?
O18 K3 Se1 109.7(4) 3_565 1_556 ?
O18 K3 K2 99.5(4) 3_565 . ?
O18 K3 N12 84.3(6) 3_565 . ?
O18 K3 N21 138.0(7) 3_565 1_556 ?
O18 K3 N23 139.1(7) 3_565 1_556 ?
O18 K3 N42 82.7(7) 3_565 . ?
O18 K3 C21 145.9(7) 3_565 1_556 ?
O18 K3 C23 147.0(7) 3_565 1_556 ?
O18 K3 C42 99.4(6) 3_565 . ?
O18 K3 O2 76.7(6) 3_565 1_556 ?
O18 K3 O26 76.7(7) 3_565 1_556 ?
N12 K3 Se1 137.9(5) . 1_556 ?
N12 K3 K2 48.1(5) . . ?
N12 K3 N21 75.6(7) . 1_556 ?
N12 K3 N23 124.8(7) . 1_556 ?
N12 K3 C21 95.8(7) . 1_556 ?
N12 K3 C23 128.4(7) . 1_556 ?
N12 K3 C42 69.5(7) . . ?
N21 K3 Se1 67.7(5) 1_556 1_556 ?
N21 K3 K2 40.6(5) 1_556 . ?
N21 K3 C21 20.5(6) 1_556 1_556 ?
N21 K3 C42 107.2(7) 1_556 . ?
N23 K3 Se1 69.5(5) 1_556 1_556 ?
N23 K3 K2 121.2(5) 1_556 . ?
N23 K3 N21 81.3(7) 1_556 1_556 ?
N23 K3 C21 66.6(7) 1_556 1_556 ?
N23 K3 C23 21.7(7) 1_556 1_556 ?
N23 K3 C42 70.9(7) 1_556 . ?
N42 K3 Se1 142.5(6) . 1_556 ?
N42 K3 K2 123.8(6) . . ?
N42 K3 N12 76.8(7) . . ?
N42 K3 N21 126.2(7) . 1_556 ?
N42 K3 N23 78.1(7) . 1_556 ?
N42 K3 C21 130.7(8) . 1_556 ?
N42 K3 C23 99.6(8) . 1_556 ?
N42 K3 C42 19.1(7) . . ?
C21 K3 Se1 50.3(5) 1_556 1_556 ?
C21 K3 K2 58.7(6) 1_556 . ?
C21 K3 C42 112.7(7) 1_556 . ?
C23 K3 Se1 50.8(5) 1_556 1_556 ?
C23 K3 K2 106.0(6) 1_556 . ?
C23 K3 N21 65.6(7) 1_556 1_556 ?
C23 K3 C21 47.8(8) 1_556 1_556 ?
C23 K3 C42 90.4(7) 1_556 . ?
C42 K3 Se1 140.4(5) . 1_556 ?
C42 K3 K2 111.5(5) . . ?
O2 K3 Se1 63.6(4) 1_556 1_556 ?
O2 K3 K2 44.2(4) 1_556 . ?
O2 K3 N12 82.8(6) 1_556 . ?
O2 K3 N21 64.6(6) 1_556 1_556 ?
O2 K3 N23 129.5(7) 1_556 1_556 ?
O2 K3 N42 152.2(7) 1_556 . ?
O2 K3 C21 69.5(7) 1_556 1_556 ?
O2 K3 C23 107.9(7) 1_556 1_556 ?
O2 K3 C42 152.3(7) 1_556 . ?
O26 K3 Se1 70.9(5) 1_556 1_556 ?
O26 K3 K2 157.3(5) 1_556 . ?
O26 K3 N12 150.3(7) 1_556 . ?
O26 K3 N21 133.2(7) 1_556 1_556 ?
O26 K3 N23 64.3(7) 1_556 1_556 ?
O26 K3 N42 78.4(7) 1_556 . ?
O26 K3 C21 112.7(7) 1_556 1_556 ?
O26 K3 C23 71.7(7) 1_556 1_556 ?
O26 K3 C42 91.2(7) 1_556 . ?
O26 K3 O2 114.0(7) 1_556 1_556 ?
O5 K4 K5 43.9(6) . . ?
O5 K4 N21 146.8(8) . 1_556 ?
O5 K4 N22 132.7(8) . 1_556 ?
O5 K4 C13 94.2(7) . . ?
O5 K4 C21 161.2(8) . 1_556 ?
O5 K4 C22 148.3(8) . 1_556 ?
O5 K4 C33 89.8(7) . . ?
O5 K4 O4 83.7(11) . 1_556 ?
N13 K4 K5 103.8(5) . . ?
N13 K4 O5 81.8(8) . . ?
N13 K4 N21 74.7(7) . 1_556 ?
N13 K4 N22 126.7(7) . 1_556 ?
N13 K4 N33 82.7(7) . . ?
N13 K4 C13 18.0(6) . . ?
N13 K4 C21 94.7(7) . 1_556 ?
N13 K4 C22 125.6(7) . 1_556 ?
N13 K4 C33 72.0(7) . . ?
N13 K4 O4 98.5(11) . 1_556 ?
N13 K4 O7 147.7(7) . 1_556 ?
N21 K4 K5 165.8(6) 1_556 . ?
N21 K4 N22 80.5(8) 1_556 1_556 ?
N21 K4 C13 69.7(7) 1_556 . ?
N21 K4 C21 20.6(7) 1_556 1_556 ?
N21 K4 C22 64.0(7) 1_556 1_556 ?
N21 K4 C33 104.5(7) 1_556 . ?
N22 K4 K5 89.6(5) 1_556 . ?
N22 K4 C13 108.7(7) 1_556 . ?
N22 K4 C21 63.6(7) 1_556 1_556 ?
N22 K4 C22 19.6(6) 1_556 1_556 ?
N22 K4 C33 69.7(7) 1_556 . ?
N33 K4 K5 45.1(5) . . ?
N33 K4 O5 77.6(8) . . ?
N33 K4 N21 121.2(8) . 1_556 ?
N33 K4 N22 71.1(7) . 1_556 ?
N33 K4 C13 72.6(6) . . ?
N33 K4 C21 120.5(7) . 1_556 ?
N33 K4 C22 89.5(7) . 1_556 ?
N33 K4 C33 17.4(6) . . ?
N33 K4 O4 160.9(11) . 1_556 ?
C13 K4 K5 104.5(5) . . ?
C13 K4 C22 109.6(7) . 1_556 ?
C13 K4 C33 58.8(6) . . ?
C21 K4 K5 153.1(6) 1_556 . ?
C21 K4 C13 87.3(7) 1_556 . ?
C21 K4 C22 45.3(7) 1_556 1_556 ?
C21 K4 C33 106.8(7) 1_556 . ?
C22 K4 K5 107.8(5) 1_556 . ?
C33 K4 K5 62.2(5) . . ?
C33 K4 C22 85.2(7) . 1_556 ?
O4 K4 K5 117.0(10) 1_556 . ?
O4 K4 N21 77.1(11) 1_556 1_556 ?
O4 K4 N22 120.9(11) 1_556 1_556 ?
O4 K4 C13 113.1(11) 1_556 . ?
O4 K4 C21 78.5(11) 1_556 1_556 ?
O4 K4 C22 104.8(11) 1_556 1_556 ?
O4 K4 C33 169.3(11) 1_556 . ?
O7 K4 K5 44.8(5) 1_556 . ?
O7 K4 O5 77.5(8) 1_556 . ?
O7 K4 N21 133.0(8) 1_556 1_556 ?
O7 K4 N22 58.5(7) 1_556 1_556 ?
O7 K4 N33 68.8(7) 1_556 . ?
O7 K4 C13 141.4(7) 1_556 . ?
O7 K4 C21 112.5(8) 1_556 1_556 ?
O7 K4 C22 70.8(7) 1_556 1_556 ?
O7 K4 C33 83.3(7) 1_556 . ?
O7 K4 O4 103.6(11) 1_556 1_556 ?
K4 K5 K13 84.0(2) . 2_655 ?
O5 K5 K4 46.7(6) . . ?
O5 K5 K13 46.6(6) . 2_655 ?
O5 K5 O6 73.1(7) . . ?
O5 K5 N33 80.7(8) . . ?
O5 K5 N112 158.9(7) . . ?
O5 K5 N113 77.8(8) . . ?
O5 K5 N121 114.4(8) . 1_556 ?
O5 K5 C112 140.9(8) . . ?
O5 K5 C113 95.3(8) . . ?
O5 K5 O7 80.5(8) . 1_556 ?
O5 K5 O12 56.3(7) . 2_656 ?
O6 K5 K4 84.0(5) . . ?
O6 K5 K13 40.3(5) . 2_655 ?
O6 K5 N112 88.8(6) . . ?
O6 K5 N113 66.9(6) . . ?
O6 K5 C112 79.2(6) . . ?
O6 K5 C113 66.0(7) . . ?
O6 K5 O12 121.8(6) . 2_656 ?
N33 K5 K4 46.0(5) . . ?
N33 K5 K13 89.4(5) . 2_655 ?
N33 K5 O6 60.8(7) . . ?
N33 K5 N112 100.1(6) . . ?
N33 K5 N113 127.1(7) . . ?
N33 K5 C112 109.1(6) . . ?
N33 K5 C113 125.4(7) . . ?
N33 K5 O12 127.3(6) . 2_656 ?
N112 K5 K4 143.8(5) . . ?
N112 K5 K13 112.3(5) . 2_655 ?
N112 K5 C112 19.3(5) . . ?
N112 K5 C113 66.8(6) . . ?
N112 K5 O12 131.2(6) . 2_656 ?
N113 K5 K4 123.2(5) . . ?
N113 K5 K13 42.3(5) . 2_655 ?
N113 K5 N112 85.3(6) . . ?
N113 K5 C112 66.2(6) . . ?
N113 K5 C113 18.6(6) . . ?
N113 K5 O12 75.6(6) . 2_656 ?
N121 K5 K4 130.5(5) 1_556 . ?
N121 K5 K13 115.4(5) 1_556 2_655 ?
N121 K5 O6 140.7(7) 1_556 . ?
N121 K5 N33 155.1(7) 1_556 . ?
N121 K5 N112 73.1(6) 1_556 . ?
N121 K5 N113 76.9(7) 1_556 . ?
N121 K5 C112 72.4(6) 1_556 . ?
N121 K5 C113 74.8(7) 1_556 . ?
N121 K5 O7 92.3(7) 1_556 1_556 ?
N121 K5 O12 59.1(6) 1_556 2_656 ?
C112 K5 K4 155.0(5) . . ?
C112 K5 K13 94.8(5) . 2_655 ?
C113 K5 K4 138.4(5) . . ?
C113 K5 K13 54.4(5) . 2_655 ?
C113 K5 C112 47.6(6) . . ?
O7 K5 K4 45.6(5) 1_556 . ?
O7 K5 K13 126.2(5) 1_556 2_655 ?
O7 K5 O6 126.7(7) 1_556 . ?
O7 K5 N33 70.0(7) 1_556 . ?
O7 K5 N112 119.9(7) 1_556 . ?
O7 K5 N113 148.8(7) 1_556 . ?
O7 K5 C112 138.6(7) 1_556 . ?
O7 K5 C113 163.5(7) 1_556 . ?
O7 K5 O12 73.8(6) 1_556 2_656 ?
O12 K5 K4 81.3(4) 2_656 . ?
O12 K5 K13 82.2(4) 2_656 2_655 ?
O12 K5 C112 123.4(6) 2_656 . ?
O12 K5 C113 90.5(6) 2_656 . ?
K7 K6 K5 138.3(2) . . ?
O8 K6 K5 66.6(5) . . ?
O8 K6 K7 129.6(5) . . ?
O8 K6 O10 76.2(6) . . ?
O8 K6 N22 144.8(7) . 1_556 ?
O8 K6 N32 86.4(6) . . ?
O8 K6 N33 74.0(6) . . ?
O8 K6 N71 77.6(6) . 1_556 ?
O8 K6 C32 79.8(6) . . ?
O8 K6 C33 74.0(6) . . ?
O8 K6 O7 109.0(6) . 1_556 ?
O8 K6 O28 150.3(6) . 1_556 ?
O10 K6 K5 68.3(5) . . ?
O10 K6 K7 145.4(5) . . ?
O10 K6 N22 121.1(7) . 1_556 ?
O10 K6 N32 151.6(7) . . ?
O10 K6 N33 111.3(7) . . ?
O10 K6 C32 155.5(7) . . ?
O10 K6 C33 127.1(7) . . ?
O10 K6 O7 73.3(6) . 1_556 ?
N22 K6 K5 90.3(5) 1_556 . ?
N22 K6 K7 54.0(5) 1_556 . ?
N22 K6 N32 85.9(7) 1_556 . ?
N22 K6 N33 71.1(7) 1_556 . ?
N22 K6 C32 81.8(7) 1_556 . ?
N22 K6 C33 71.4(7) 1_556 . ?
N22 K6 O7 56.5(7) 1_556 1_556 ?
N32 K6 K5 124.7(5) . . ?
N32 K6 K7 43.4(4) . . ?
N32 K6 N33 84.4(6) . . ?
N32 K6 C32 19.1(6) . . ?
N32 K6 C33 66.7(6) . . ?
N32 K6 O7 134.4(6) . 1_556 ?
N33 K6 K5 43.1(5) . . ?
N33 K6 K7 99.3(5) . . ?
N33 K6 C32 65.5(6) . . ?
N33 K6 C33 17.8(6) . . ?
N33 K6 O7 61.0(6) . 1_556 ?
N71 K6 K5 133.0(5) 1_556 . ?
N71 K6 K7 88.1(5) 1_556 . ?
N71 K6 O10 74.4(6) 1_556 . ?
N71 K6 N22 134.3(7) 1_556 1_556 ?
N71 K6 N32 80.1(6) 1_556 . ?
N71 K6 N33 148.4(6) 1_556 . ?
N71 K6 C32 96.2(6) 1_556 . ?
N71 K6 C33 137.1(7) 1_556 . ?
N71 K6 O7 144.1(6) 1_556 1_556 ?
N71 K6 O28 73.5(6) 1_556 1_556 ?
C32 K6 K5 106.0(5) . . ?
C32 K6 K7 53.8(5) . . ?
C32 K6 C33 47.7(7) . . ?
C33 K6 K5 60.0(5) . . ?
C33 K6 K7 85.9(5) . . ?
O7 K6 K5 42.7(4) 1_556 . ?
O7 K6 K7 110.4(5) 1_556 . ?
O7 K6 C32 119.6(6) 1_556 . ?
O7 K6 C33 76.6(6) 1_556 . ?
O28 K6 K5 141.3(5) 1_556 . ?
O28 K6 K7 43.3(4) 1_556 . ?
O28 K6 O10 102.4(6) 1_556 . ?
O28 K6 N22 61.5(7) 1_556 1_556 ?
O28 K6 N32 81.8(6) 1_556 . ?
O28 K6 N33 131.3(6) 1_556 . ?
O28 K6 C32 96.2(6) 1_556 . ?
O28 K6 C33 124.5(6) 1_556 . ?
O28 K6 O7 98.7(6) 1_556 1_556 ?
Se4 K7 K8 88.7(2) 1_556 . ?
O27 K7 Se4 110.0(4) . 1_556 ?
O27 K7 K8 110.5(5) . . ?
O27 K7 N22 124.1(6) . 1_556 ?
O27 K7 N23 150.8(7) . 1_556 ?
O27 K7 N32 78.5(6) . . ?
O27 K7 N43 93.8(6) . . ?
O27 K7 C22 134.9(7) . 1_556 ?
O27 K7 C23 155.1(7) . 1_556 ?
O27 K7 C32 94.7(6) . . ?
O27 K7 O24 78.1(7) . 1_556 ?
O27 K7 O28 71.8(6) . 1_556 ?
N22 K7 Se4 65.7(5) 1_556 1_556 ?
N22 K7 K8 124.6(5) 1_556 . ?
N22 K7 C22 19.7(6) 1_556 1_556 ?
N22 K7 C32 74.0(6) 1_556 . ?
N23 K7 Se4 68.2(5) 1_556 1_556 ?
N23 K7 K8 41.8(5) 1_556 . ?
N23 K7 N22 82.7(7) 1_556 1_556 ?
N23 K7 N43 73.8(7) 1_556 . ?
N23 K7 C22 67.6(7) 1_556 1_556 ?
N23 K7 C23 21.6(7) 1_556 1_556 ?
N23 K7 C32 104.6(7) 1_556 . ?
N32 K7 Se4 141.4(5) . 1_556 ?
N32 K7 K8 124.7(5) . . ?
N32 K7 N22 78.3(7) . 1_556 ?
N32 K7 N23 122.1(7) . 1_556 ?
N32 K7 N43 76.5(6) . . ?
N32 K7 C22 97.1(7) . 1_556 ?
N32 K7 C23 126.3(7) . 1_556 ?
N32 K7 C32 17.5(6) . . ?
N43 K7 Se4 137.2(5) . 1_556 ?
N43 K7 K8 49.1(5) . . ?
N43 K7 N22 128.2(7) . 1_556 ?
N43 K7 C22 129.2(7) . 1_556 ?
N43 K7 C23 95.0(7) . 1_556 ?
N43 K7 C32 68.6(6) . . ?
C22 K7 Se4 49.5(5) 1_556 1_556 ?
C22 K7 K8 108.6(5) 1_556 . ?
C22 K7 C32 90.4(7) 1_556 . ?
C23 K7 Se4 50.1(5) 1_556 1_556 ?
C23 K7 K8 60.3(6) 1_556 . ?
C23 K7 N22 65.9(7) 1_556 1_556 ?
C23 K7 C22 48.3(7) 1_556 1_556 ?
C23 K7 C32 110.3(7) 1_556 . ?
C32 K7 Se4 139.6(5) . 1_556 ?
C32 K7 K8 112.6(5) . . ?
O24 K7 Se4 68.8(6) 1_556 1_556 ?
O24 K7 K8 46.7(6) 1_556 . ?
O24 K7 N22 134.0(8) 1_556 1_556 ?
O24 K7 N23 74.2(8) 1_556 1_556 ?
O24 K7 N32 147.5(8) 1_556 . ?
O24 K7 N43 82.8(8) 1_556 . ?
O24 K7 C22 115.4(8) 1_556 1_556 ?
O24 K7 C23 79.9(8) 1_556 1_556 ?
O24 K7 C32 150.0(8) 1_556 . ?
O24 K7 O28 110.5(7) 1_556 1_556 ?
O28 K7 Se4 65.7(4) 1_556 1_556 ?
O28 K7 K8 152.4(5) 1_556 . ?
O28 K7 N22 55.4(6) 1_556 1_556 ?
O28 K7 N23 127.0(7) 1_556 1_556 ?
O28 K7 N32 83.0(6) 1_556 . ?
O28 K7 N43 157.1(7) 1_556 . ?
O28 K7 C22 63.2(7) 1_556 1_556 ?
O28 K7 C23 105.4(7) 1_556 1_556 ?
O28 K7 C32 94.2(6) 1_556 . ?
K7 K8 K3 85.2(2) . . ?
K7 K8 K9 74.7(2) . . ?
K7 K8 K18 132.9(3) . 3_565 ?
K9 K8 K3 137.5(3) . . ?
K18 K8 K3 131.2(3) 3_565 . ?
K18 K8 K9 58.32(19) 3_565 . ?
O19 K8 K3 93.5(6) 3_565 . ?
O19 K8 K7 126.1(6) 3_565 . ?
O19 K8 K9 70.7(5) 3_565 . ?
O19 K8 K18 41.9(5) 3_565 3_565 ?
O19 K8 N43 77.2(7) 3_565 . ?
O19 K8 O26 97.2(8) 3_565 1_556 ?
N23 K8 K3 40.9(6) 1_556 . ?
N23 K8 K7 46.5(6) 1_556 . ?
N23 K8 K9 117.6(7) 1_556 . ?
N23 K8 K18 165.7(7) 1_556 3_565 ?
N23 K8 O19 124.4(9) 1_556 3_565 ?
N23 K8 N43 77.3(8) 1_556 . ?
N23 K8 N143 142.3(9) 1_556 3_566 ?
N23 K8 O20 136.8(9) 1_556 3_566 ?
N23 K8 O24 75.4(8) 1_556 1_556 ?
N23 K8 O26 66.2(8) 1_556 1_556 ?
N43 K8 K3 94.1(5) . . ?
N43 K8 K7 49.3(5) . . ?
N43 K8 K9 44.7(5) . . ?
N43 K8 K18 93.3(5) . 3_565 ?
N143 K8 K3 172.1(7) 3_566 . ?
N143 K8 K7 96.2(6) 3_566 . ?
N143 K8 K9 36.7(5) 3_566 . ?
N143 K8 K18 43.6(5) 3_566 3_565 ?
N143 K8 O19 79.3(7) 3_566 3_565 ?
N143 K8 N43 81.1(7) 3_566 . ?
N143 K8 O24 70.7(8) 3_566 1_556 ?
N143 K8 O26 146.4(8) 3_566 1_556 ?
O20 K8 K3 108.1(6) 3_566 . ?
O20 K8 K7 155.8(7) 3_566 . ?
O20 K8 K9 105.1(6) 3_566 . ?
O20 K8 K18 51.5(6) 3_566 3_565 ?
O20 K8 O19 74.4(8) 3_566 3_565 ?
O20 K8 N43 144.7(8) 3_566 . ?
O20 K8 N143 73.4(8) 3_566 3_566 ?
O20 K8 O24 112.4(9) 3_566 1_556 ?
O20 K8 O26 73.5(8) 3_566 1_556 ?
O24 K8 K3 114.9(6) 1_556 . ?
O24 K8 K7 43.6(6) 1_556 . ?
O24 K8 K9 74.4(6) 1_556 . ?
O24 K8 K18 113.9(6) 1_556 3_565 ?
O24 K8 O19 145.0(8) 1_556 3_565 ?
O24 K8 N43 80.5(7) 1_556 . ?
O24 K8 O26 117.8(8) 1_556 1_556 ?
O26 K8 K3 37.2(5) 1_556 . ?
O26 K8 K7 111.9(5) 1_556 . ?
O26 K8 K9 167.5(6) 1_556 . ?
O26 K8 K18 114.8(6) 1_556 3_565 ?
O26 K8 N43 131.1(8) 1_556 . ?
O23 K9 K18 150.6(6) . 3_565 ?
O23 K9 N43 62.1(7) . . ?
O23 K9 N131 152.2(7) . . ?
O23 K9 N131 89.4(7) . 2_665 ?
O23 K9 N141 78.3(7) . 1_556 ?
O23 K9 C131 98.5(7) . 2_665 ?
O23 K9 C131 135.7(7) . . ?
O23 K9 C141 95.4(7) . 1_556 ?
O23 K9 C143 138.3(7) . 3_566 ?
O25 K9 K18 54.6(5) . 3_565 ?
O25 K9 O23 104.4(7) . . ?
O25 K9 N43 74.3(6) . . ?
O25 K9 N131 62.7(6) . . ?
O25 K9 N131 122.3(7) . 2_665 ?
O25 K9 N141 164.8(7) . 1_556 ?
O25 K9 C131 67.4(7) . . ?
O25 K9 C131 104.1(7) . 2_665 ?
O25 K9 C141 157.2(7) . 1_556 ?
O25 K9 C143 101.6(7) . 3_566 ?
N43 K9 K18 90.5(5) . 3_565 ?
N43 K9 N131 150.9(7) . 2_665 ?
N43 K9 N131 128.9(7) . . ?
N43 K9 C131 140.7(7) . . ?
N43 K9 C131 158.5(7) . 2_665 ?
N43 K9 C141 106.1(6) . 1_556 ?
N43 K9 C143 95.1(6) . 3_566 ?
N131 K9 K18 118.6(5) 2_665 3_565 ?
N131 K9 K18 42.3(5) . 3_565 ?
N131 K9 N131 79.3(9) 2_665 . ?
N131 K9 C131 18.4(6) . . ?
N131 K9 C131 64.4(7) 2_665 . ?
N131 K9 C131 64.3(7) . 2_665 ?
N131 K9 C131 18.6(6) 2_665 2_665 ?
N131 K9 C141 103.6(6) . 1_556 ?
N131 K9 C141 68.4(6) 2_665 1_556 ?
N131 K9 C143 69.4(6) . 3_566 ?
N131 K9 C143 103.5(7) 2_665 3_566 ?
N141 K9 K18 116.7(5) 1_556 3_565 ?
N141 K9 N43 94.4(6) 1_556 . ?
N141 K9 N131 121.0(6) 1_556 . ?
N141 K9 N131 72.4(6) 1_556 2_665 ?
N141 K9 C131 121.3(7) 1_556 . ?
N141 K9 C131 90.2(7) 1_556 2_665 ?
N141 K9 C141 17.5(6) 1_556 1_556 ?
N141 K9 C143 68.7(7) 1_556 3_566 ?
N143 K9 K18 42.6(5) 3_566 3_565 ?
N143 K9 O23 131.5(8) 3_566 . ?
N143 K9 O25 90.9(7) 3_566 . ?
N143 K9 N43 79.1(7) 3_566 . ?
N143 K9 N131 75.3(7) 3_566 . ?
N143 K9 N131 120.8(7) 3_566 2_665 ?
N143 K9 N141 76.7(7) 3_566 1_556 ?
N143 K9 C131 92.8(7) 3_566 . ?
N143 K9 C131 122.3(7) 3_566 2_665 ?
N143 K9 C141 67.2(6) 3_566 1_556 ?
N143 K9 C143 17.2(6) 3_566 3_566 ?
C131 K9 K18 60.4(5) . 3_565 ?
C131 K9 K18 106.1(5) 2_665 3_565 ?
C131 K9 C131 47.7(10) 2_665 . ?
C131 K9 C141 83.8(7) 2_665 1_556 ?
C131 K9 C141 105.9(7) . 1_556 ?
C131 K9 C143 106.1(7) 2_665 3_566 ?
C141 K9 K18 102.8(5) 1_556 3_565 ?
C143 K9 K18 48.0(5) 3_566 3_565 ?
C143 K9 C131 84.5(7) 3_566 . ?
C143 K9 C141 55.6(6) 3_566 1_556 ?
K7 K10 K6 56.59(15) . . ?
K11 K10 K6 62.53(15) . . ?
K11 K10 K7 119.1(2) . . ?
O23 K10 K6 118.4(6) . . ?
O23 K10 K7 73.6(5) . . ?
O23 K10 K11 144.2(6) . . ?
O23 K10 O29 100.2(7) . . ?
O23 K10 N32 78.4(7) . . ?
O23 K10 N52 117.2(7) . . ?
O23 K10 N71 156.1(7) . 1_556 ?
O23 K10 N73 107.3(7) . 1_556 ?
O23 K10 C71 160.9(7) . 1_556 ?
O23 K10 C73 125.0(7) . 1_556 ?
O27 K10 K6 81.0(4) . . ?
O27 K10 K7 38.6(4) . . ?
O27 K10 K11 131.1(5) . . ?
O27 K10 O23 80.9(7) . . ?
O27 K10 O29 153.5(6) . . ?
O27 K10 N32 79.1(6) . . ?
O27 K10 N52 139.9(7) . . ?
O27 K10 N71 85.8(6) . 1_556 ?
O27 K10 N73 71.7(6) . 1_556 ?
O27 K10 C71 80.0(6) . 1_556 ?
O27 K10 C73 70.2(6) . 1_556 ?
O29 K10 K6 75.2(4) . . ?
O29 K10 K7 116.0(4) . . ?
O29 K10 K11 44.0(4) . . ?
O29 K10 N71 83.1(6) . 1_556 ?
O29 K10 N73 131.3(6) . 1_556 ?
O29 K10 C71 96.3(6) . 1_556 ?
O29 K10 C73 126.0(6) . 1_556 ?
N32 K10 K6 40.5(5) . . ?
N32 K10 K7 40.7(5) . . ?
N32 K10 K11 91.1(5) . . ?
N32 K10 O29 75.3(6) . . ?
N32 K10 N52 137.1(7) . . ?
N32 K10 N71 79.6(6) . 1_556 ?
N32 K10 N73 148.6(6) . 1_556 ?
N32 K10 C71 96.8(6) . 1_556 ?
N32 K10 C73 135.8(6) . 1_556 ?
N52 K10 K6 114.3(5) . . ?
N52 K10 K7 169.2(5) . . ?
N52 K10 K11 52.0(5) . . ?
N52 K10 O29 63.0(6) . . ?
N52 K10 N71 85.6(6) . 1_556 ?
N52 K10 N73 68.8(6) . 1_556 ?
N52 K10 C71 79.0(6) . 1_556 ?
N52 K10 C73 70.3(6) . 1_556 ?
N71 K10 K6 39.1(5) 1_556 . ?
N71 K10 K7 83.6(5) 1_556 . ?
N71 K10 K11 45.3(4) 1_556 . ?
N71 K10 N73 87.1(6) 1_556 1_556 ?
N71 K10 C71 19.6(6) 1_556 1_556 ?
N71 K10 C73 67.5(6) 1_556 1_556 ?
N73 K10 K6 121.4(4) 1_556 . ?
N73 K10 K7 110.0(4) 1_556 . ?
N73 K10 K11 99.4(4) 1_556 . ?
N73 K10 C71 67.5(6) 1_556 1_556 ?
N73 K10 C73 19.6(6) 1_556 1_556 ?
C71 K10 K6 57.1(5) 1_556 . ?
C71 K10 K7 90.7(5) 1_556 . ?
C71 K10 K11 53.4(5) 1_556 . ?
C71 K10 C73 48.0(7) 1_556 1_556 ?
C73 K10 K6 102.4(5) 1_556 . ?
C73 K10 K7 104.9(5) 1_556 . ?
C73 K10 K11 86.1(5) 1_556 . ?
O8 K11 Se5 110.1(4) . . ?
O8 K11 O29 69.3(6) . . ?
O8 K11 N52 123.6(6) . . ?
O8 K11 N53 152.5(6) . . ?
O8 K11 N71 74.7(6) . 1_556 ?
O8 K11 N81 93.4(6) . 1_556 ?
O8 K11 C52 135.3(6) . . ?
O8 K11 C53 156.0(7) . . ?
O8 K11 C71 92.6(6) . 1_556 ?
O8 K11 C81 106.8(6) . 1_556 ?
O11 K11 Se5 67.0(4) . . ?
O11 K11 O8 81.1(6) . . ?
O11 K11 O29 108.5(6) . . ?
O11 K11 N52 133.5(6) . . ?
O11 K11 N53 72.9(6) . . ?
O11 K11 N71 146.9(7) . 1_556 ?
O11 K11 N81 83.1(6) . 1_556 ?
O11 K11 C52 114.5(7) . . ?
O11 K11 C53 78.0(7) . . ?
O11 K11 C71 150.6(7) . 1_556 ?
O11 K11 C81 98.8(6) . 1_556 ?
O29 K11 Se5 65.4(4) . . ?
O29 K11 N52 58.7(6) . . ?
O29 K11 N53 127.4(6) . . ?
O29 K11 N71 83.9(6) . 1_556 ?
O29 K11 N81 156.6(6) . 1_556 ?
O29 K11 C52 66.1(6) . . ?
O29 K11 C53 106.4(6) . . ?
O29 K11 C71 95.8(6) . 1_556 ?
O29 K11 C81 151.2(6) . 1_556 ?
N52 K11 Se5 67.5(4) . . ?
N52 K11 C52 20.0(5) . . ?
N52 K11 C53 66.2(7) . . ?
N52 K11 C71 73.4(6) . 1_556 ?
N52 K11 C81 108.2(6) . 1_556 ?
N53 K11 Se5 68.0(4) . . ?
N53 K11 N52 82.0(6) . . ?
N53 K11 C52 66.4(6) . . ?
N53 K11 C53 21.0(6) . . ?
N53 K11 C71 105.4(7) . 1_556 ?
N53 K11 C81 69.3(6) . 1_556 ?
N71 K11 Se5 143.0(5) 1_556 . ?
N71 K11 N52 79.3(6) 1_556 . ?
N71 K11 N53 124.3(7) 1_556 . ?
N71 K11 N81 76.1(6) 1_556 1_556 ?
N71 K11 C52 98.6(7) 1_556 . ?
N71 K11 C53 129.1(7) 1_556 . ?
N71 K11 C71 18.9(6) 1_556 1_556 ?
N71 K11 C81 67.8(6) 1_556 1_556 ?
N81 K11 Se5 137.5(5) 1_556 . ?
N81 K11 N52 127.4(6) 1_556 . ?
N81 K11 N53 75.0(6) 1_556 . ?
N81 K11 C52 128.6(7) 1_556 . ?
N81 K11 C53 95.8(7) 1_556 . ?
N81 K11 C71 68.5(6) 1_556 1_556 ?
N81 K11 C81 19.2(6) 1_556 1_556 ?
C52 K11 Se5 51.2(5) . . ?
C52 K11 C71 90.1(6) . 1_556 ?
C52 K11 C81 111.2(6) . 1_556 ?
C53 K11 Se5 50.2(5) . . ?
C53 K11 C52 48.1(7) . . ?
C53 K11 C71 111.4(7) . 1_556 ?
C53 K11 C81 88.2(6) . 1_556 ?
C71 K11 Se5 140.8(5) 1_556 . ?
C71 K11 C81 55.4(6) 1_556 1_556 ?
C81 K11 Se5 137.3(5) 1_556 . ?
K5 K12 K5 144.7(2) 3_665 . ?
O10 K12 K5 152.5(5) . 3_665 ?
O10 K12 K5 62.4(5) . . ?
O10 K12 N81 62.6(6) . 1_556 ?
O10 K12 N112 80.1(6) . . ?
O10 K12 N113 137.4(7) . 3_665 ?
O10 K12 N121 84.4(7) . 1_556 ?
O10 K12 N121 150.1(6) . 3_666 ?
O10 K12 C113 141.9(7) . 3_665 ?
O10 K12 C121 93.5(7) . 1_556 ?
O10 K12 C121 131.9(7) . 3_666 ?
O10 K12 O12 108.5(6) . 1_556 ?
N81 K12 K5 92.9(5) 1_556 3_665 ?
N81 K12 K5 114.3(5) 1_556 . ?
N81 K12 N112 96.4(6) 1_556 . ?
N81 K12 N121 146.6(7) 1_556 1_556 ?
N81 K12 N121 128.5(6) 1_556 3_666 ?
N81 K12 C113 99.5(6) 1_556 3_665 ?
N81 K12 C121 153.3(7) 1_556 1_556 ?
N81 K12 C121 139.2(7) 1_556 3_666 ?
N112 K12 K5 117.2(5) . 3_665 ?
N112 K12 K5 41.5(4) . . ?
N112 K12 N121 120.5(6) . 3_666 ?
N112 K12 N121 71.1(6) . 1_556 ?
N112 K12 C113 68.2(6) . 3_665 ?
N112 K12 C121 122.1(7) . 3_666 ?
N112 K12 C121 90.7(7) . 1_556 ?
N113 K12 K5 114.7(5) 3_665 . ?
N113 K12 K5 42.5(5) 3_665 3_665 ?
N113 K12 N81 85.0(7) 3_665 1_556 ?
N113 K12 N112 76.6(6) 3_665 . ?
N113 K12 N121 119.9(7) 3_665 1_556 ?
N113 K12 N121 71.8(6) 3_665 3_666 ?
N113 K12 C113 16.1(6) 3_665 3_665 ?
N113 K12 C121 121.8(7) 3_665 1_556 ?
N113 K12 C121 90.6(7) 3_665 3_666 ?
N113 K12 O12 86.7(6) 3_665 1_556 ?
N121 K12 K5 120.5(5) 1_556 3_665 ?
N121 K12 K5 40.1(4) 3_666 3_665 ?
N121 K12 K5 37.4(5) 1_556 . ?
N121 K12 K5 117.1(5) 3_666 . ?
N121 K12 N121 82.9(9) 1_556 3_666 ?
N121 K12 C113 103.8(7) 1_556 3_665 ?
N121 K12 C113 67.7(6) 3_666 3_665 ?
N121 K12 C121 20.5(6) 1_556 1_556 ?
N121 K12 C121 66.9(7) 3_666 1_556 ?
N121 K12 C121 67.5(7) 1_556 3_666 ?
N121 K12 C121 19.7(6) 3_666 3_666 ?
C113 K12 K5 102.1(5) 3_665 . ?
C113 K12 K5 49.0(5) 3_665 3_665 ?
C121 K12 K5 59.1(5) 3_666 3_665 ?
C121 K12 K5 104.4(5) 3_666 . ?
C121 K12 K5 106.7(5) 1_556 3_665 ?
C121 K12 K5 57.5(5) 1_556 . ?
C121 K12 C113 84.2(7) 3_666 3_665 ?
C121 K12 C113 107.1(7) 1_556 3_665 ?
C121 K12 C121 49.3(10) 1_556 3_666 ?
O12 K12 K5 156.7(4) 1_556 . ?
O12 K12 K5 49.1(4) 1_556 3_665 ?
O12 K12 N81 74.7(6) 1_556 1_556 ?
O12 K12 N112 161.8(6) 1_556 . ?
O12 K12 N121 59.1(6) 1_556 3_666 ?
O12 K12 N121 124.7(6) 1_556 1_556 ?
O12 K12 C113 97.2(6) 1_556 3_665 ?
O12 K12 C121 104.4(7) 1_556 1_556 ?
O12 K12 C121 64.5(6) 1_556 3_666 ?
K5 K13 K11 122.4(3) 3_665 . ?
K5 K13 K12 58.24(17) 3_665 . ?
K5 K13 K14 122.5(3) 3_665 . ?
K11 K13 K12 64.56(18) . . ?
K11 K13 K14 82.3(2) . . ?
K14 K13 K12 122.2(3) . . ?
O5 K13 K5 42.2(6) 3_665 3_665 ?
O5 K13 K11 107.9(6) 3_665 . ?
O5 K13 K12 66.4(6) 3_665 . ?
O5 K13 K14 82.6(6) 3_665 . ?
O6 K13 K5 44.1(5) 3_665 3_665 ?
O6 K13 K11 159.1(6) 3_665 . ?
O6 K13 K12 98.1(6) 3_665 . ?
O6 K13 K14 118.0(6) 3_665 . ?
O6 K13 O5 72.5(8) 3_665 3_665 ?
O6 K13 O11 125.8(7) 3_665 . ?
O6 K13 O13 82.7(8) 3_665 . ?
O6 K13 N53 156.8(8) 3_665 . ?
O6 K13 N82 92.9(8) 3_665 . ?
O6 K13 N113 72.2(7) 3_665 3_665 ?
O11 K13 K5 113.3(5) . 3_665 ?
O11 K13 K11 37.4(4) . . ?
O11 K13 K12 63.7(4) . . ?
O11 K13 K14 114.3(5) . . ?
O11 K13 O5 128.5(8) . 3_665 ?
O11 K13 N82 73.3(7) . . ?
O13 K13 K5 106.8(6) . 3_665 ?
O13 K13 K11 118.2(6) . . ?
O13 K13 K12 148.0(6) . . ?
O13 K13 K14 38.0(5) . . ?
O13 K13 O5 83.7(8) . 3_665 ?
O13 K13 O11 139.8(7) . . ?
O13 K13 N82 78.0(7) . . ?
N53 K13 K5 144.6(6) . 3_665 ?
N53 K13 K11 44.0(5) . . ?
N53 K13 K12 101.7(6) . . ?
N53 K13 K14 39.9(5) . . ?
N53 K13 O5 104.8(8) . 3_665 ?
N53 K13 O11 74.5(7) . . ?
N53 K13 O13 74.1(7) . . ?
N53 K13 N82 82.0(7) . . ?
N53 K13 N113 130.4(8) . 3_665 ?
N82 K13 K5 133.2(6) . 3_665 ?
N82 K13 K11 91.7(5) . . ?
N82 K13 K12 133.6(6) . . ?
N82 K13 K14 90.4(5) . . ?
N82 K13 O5 158.0(8) . 3_665 ?
N113 K13 K5 45.7(5) 3_665 3_665 ?
N113 K13 K11 87.5(5) 3_665 . ?
N113 K13 K12 32.3(5) 3_665 . ?
N113 K13 K14 152.9(6) 3_665 . ?
N113 K13 O5 76.8(8) 3_665 3_665 ?
N113 K13 O11 67.8(7) 3_665 . ?
N113 K13 O13 151.8(8) 3_665 . ?
N113 K13 N82 115.0(7) 3_665 . ?
O13 K14 K15 120.2(6) . . ?
O13 K14 O16 117.5(7) . . ?
O13 K14 N51 138.7(7) . . ?
O13 K14 N53 71.5(7) . . ?
O13 K14 N62 149.1(8) . 1_556 ?
O13 K14 C51 119.7(7) . . ?
O13 K14 C53 80.0(7) . . ?
O13 K14 C62 149.2(8) . 1_556 ?
O13 K14 C83 92.3(7) . 1_556 ?
O14 K14 K15 45.7(5) . . ?
O14 K14 O13 77.0(8) . . ?
O14 K14 O16 77.7(7) . . ?
O14 K14 N51 132.0(7) . . ?
O14 K14 N53 144.6(7) . . ?
O14 K14 N62 77.1(7) . 1_556 ?
O14 K14 N83 78.0(8) . 1_556 ?
O14 K14 C51 145.4(7) . . ?
O14 K14 C53 156.8(8) . . ?
O14 K14 C62 93.1(7) . 1_556 ?
O14 K14 C83 93.3(7) . 1_556 ?
O16 K14 K15 46.0(5) . . ?
O16 K14 N51 58.5(6) . . ?
O16 K14 N53 131.6(7) . . ?
O16 K14 N62 72.5(7) . 1_556 ?
O16 K14 C51 67.7(7) . . ?
O16 K14 C53 110.9(7) . . ?
O16 K14 C62 87.9(7) . 1_556 ?
O16 K14 C83 145.3(7) . 1_556 ?
N51 K14 K15 87.3(5) . . ?
N51 K14 C51 19.5(6) . . ?
N51 K14 C53 66.7(7) . . ?
N51 K14 C62 68.4(7) . 1_556 ?
N51 K14 C83 110.9(7) . 1_556 ?
N53 K14 K15 168.3(5) . . ?
N53 K14 N51 83.3(6) . . ?
N53 K14 C51 67.7(6) . . ?
N53 K14 C53 20.7(6) . . ?
N53 K14 C62 105.6(7) . 1_556 ?
N53 K14 C83 72.4(7) . 1_556 ?
N62 K14 K15 43.8(5) 1_556 . ?
N62 K14 N51 72.1(7) 1_556 . ?
N62 K14 N53 125.8(7) 1_556 . ?
N62 K14 C51 91.2(7) 1_556 . ?
N62 K14 C53 125.8(8) 1_556 . ?
N62 K14 C62 20.4(7) 1_556 1_556 ?
N62 K14 C83 72.8(7) 1_556 1_556 ?
N83 K14 K15 100.9(6) 1_556 . ?
N83 K14 O13 78.2(7) 1_556 . ?
N83 K14 O16 146.8(8) 1_556 . ?
N83 K14 N51 129.7(7) 1_556 . ?
N83 K14 N53 80.0(7) 1_556 . ?
N83 K14 N62 80.2(8) 1_556 1_556 ?
N83 K14 C51 132.5(8) 1_556 . ?
N83 K14 C53 100.2(8) 1_556 . ?
N83 K14 C62 71.1(8) 1_556 1_556 ?
N83 K14 C83 18.9(7) 1_556 1_556 ?
C51 K14 K15 104.4(5) . . ?
C51 K14 C62 84.8(7) . 1_556 ?
C51 K14 C83 114.4(7) . 1_556 ?
C53 K14 K15 153.4(6) . . ?
C53 K14 C51 49.0(7) . . ?
C53 K14 C62 108.3(7) . 1_556 ?
C53 K14 C83 90.5(7) . 1_556 ?
C62 K14 K15 64.2(5) 1_556 . ?
C83 K14 K15 104.7(5) 1_556 . ?
C83 K14 C62 58.8(7) 1_556 1_556 ?
K14 K15 K2 82.6(2) . 3_665 ?
K14 K15 K16 72.82(18) . . ?
K16 K15 K2 145.7(2) . 3_665 ?
O1 K15 K2 68.7(4) 3_665 3_665 ?
O1 K15 K14 85.8(4) 3_665 . ?
O1 K15 K16 130.8(4) 3_665 . ?
O1 K15 C91 122.8(6) 3_665 1_556 ?
O1 K15 C93 88.6(6) 3_665 1_556 ?
O14 K15 K2 42.7(5) . 3_665 ?
O14 K15 K14 45.1(5) . . ?
O14 K15 K16 118.0(5) . . ?
O14 K15 O1 56.7(6) . 3_665 ?
O14 K15 O16 77.1(7) . . ?
O14 K15 N91 156.3(7) . 1_556 ?
O14 K15 N93 77.3(7) . 1_556 ?
O14 K15 C91 140.7(7) . 1_556 ?
O14 K15 C93 96.3(7) . 1_556 ?
O16 K15 K2 119.8(5) . 3_665 ?
O16 K15 K14 45.8(5) . . ?
O16 K15 K16 55.7(5) . . ?
O16 K15 O1 77.4(6) . 3_665 ?
O16 K15 N91 124.2(7) . 1_556 ?
O16 K15 N93 148.0(7) . 1_556 ?
O16 K15 C91 141.9(7) . 1_556 ?
O16 K15 C93 166.0(7) . 1_556 ?
N62 K15 K2 92.8(6) 1_556 3_665 ?
N62 K15 K14 48.0(6) 1_556 . ?
N62 K15 K16 52.9(6) 1_556 . ?
N62 K15 O1 132.8(7) 1_556 3_665 ?
N62 K15 O14 79.9(8) 1_556 . ?
N62 K15 O16 75.4(7) 1_556 . ?
N62 K15 N91 94.7(7) 1_556 1_556 ?
N62 K15 N93 118.4(7) 1_556 1_556 ?
N62 K15 N101 160.0(8) 1_556 . ?
N62 K15 C91 102.1(7) 1_556 1_556 ?
N62 K15 C93 116.0(7) 1_556 1_556 ?
N91 K15 K2 115.4(5) 1_556 3_665 ?
N91 K15 K14 140.9(5) 1_556 . ?
N91 K15 K16 74.3(5) 1_556 . ?
N91 K15 O1 132.4(6) 1_556 3_665 ?
N91 K15 C91 18.1(5) 1_556 1_556 ?
N91 K15 C93 65.1(7) 1_556 1_556 ?
N93 K15 K2 37.4(4) 1_556 3_665 ?
N93 K15 K14 119.9(5) 1_556 . ?
N93 K15 K16 156.1(5) 1_556 . ?
N93 K15 O1 72.5(6) 1_556 3_665 ?
N93 K15 N91 85.2(6) 1_556 1_556 ?
N93 K15 C91 67.2(6) 1_556 1_556 ?
N93 K15 C93 20.2(6) 1_556 1_556 ?
N101 K15 K2 107.1(5) . 3_665 ?
N101 K15 K14 134.9(5) . . ?
N101 K15 K16 107.2(5) . . ?
N101 K15 O1 59.6(6) . 3_665 ?
N101 K15 O14 115.9(7) . . ?
N101 K15 O16 95.5(7) . . ?
N101 K15 N91 75.4(7) . 1_556 ?
N101 K15 N93 78.7(7) . 1_556 ?
N101 K15 C91 73.9(7) . 1_556 ?
N101 K15 C93 76.0(7) . 1_556 ?
C91 K15 K2 98.2(5) 1_556 3_665 ?
C91 K15 K14 149.9(5) 1_556 . ?
C91 K15 K16 91.8(5) 1_556 . ?
C93 K15 K2 54.3(5) 1_556 3_665 ?
C93 K15 K14 135.3(5) 1_556 . ?
C93 K15 K16 137.1(5) 1_556 . ?
C93 K15 C91 47.0(7) 1_556 1_556 ?
K3 K16 K14 145.7(2) 2_665 . ?
K3 K16 K15 105.92(19) 2_665 . ?
K15 K16 K14 50.32(15) . . ?
K17 K16 K3 112.6(2) . 2_665 ?
K17 K16 K14 81.91(17) . . ?
K17 K16 K15 131.8(2) . . ?
O3 K16 K3 80.4(6) 2_665 2_665 ?
O3 K16 K14 103.6(6) 2_665 . ?
O3 K16 K15 64.2(6) 2_665 . ?
O3 K16 K17 148.5(6) 2_665 . ?
O3 K16 O30 104.2(7) 2_665 . ?
O3 K16 N42 91.9(8) 2_665 2_665 ?
O3 K16 N51 118.3(7) 2_665 . ?
O3 K16 N61 160.0(8) 2_665 1_556 ?
O3 K16 C61 156.7(8) 2_665 1_556 ?
O18 K16 K3 39.7(4) . 2_665 ?
O18 K16 K14 106.4(4) . . ?
O18 K16 K15 70.8(4) . . ?
O18 K16 K17 127.5(4) . . ?
O18 K16 O3 81.4(7) . 2_665 ?
O18 K16 O30 150.8(6) . . ?
O18 K16 N42 82.4(7) . 2_665 ?
O18 K16 N51 138.2(6) . . ?
O18 K16 N61 82.4(6) . 1_556 ?
O18 K16 C61 76.2(6) . 1_556 ?
O30 K16 K3 112.0(5) . 2_665 ?
O30 K16 K14 100.2(5) . . ?
O30 K16 K15 137.7(5) . . ?
O30 K16 K17 44.7(5) . . ?
O30 K16 C61 98.5(7) . 1_556 ?
N42 K16 K3 43.2(5) 2_665 2_665 ?
N42 K16 K14 163.0(6) 2_665 . ?
N42 K16 K15 146.0(6) 2_665 . ?
N42 K16 K17 81.2(6) 2_665 . ?
N42 K16 O30 68.9(7) 2_665 . ?
N42 K16 C61 91.4(7) 2_665 1_556 ?
N51 K16 K3 161.3(5) . 2_665 ?
N51 K16 K14 36.3(5) . . ?
N51 K16 K15 84.7(5) . . ?
N51 K16 K17 51.2(5) . . ?
N51 K16 O30 64.7(7) . . ?
N51 K16 N42 129.1(7) . 2_665 ?
N51 K16 N61 81.7(7) . 1_556 ?
N51 K16 C61 76.3(7) . 1_556 ?
N61 K16 K3 79.7(5) 1_556 2_665 ?
N61 K16 K14 92.1(5) 1_556 . ?
N61 K16 K15 120.5(5) 1_556 . ?
N61 K16 K17 45.1(5) 1_556 . ?
N61 K16 O30 84.7(7) 1_556 . ?
N61 K16 N42 74.4(7) 1_556 2_665 ?
N61 K16 C61 18.9(6) 1_556 1_556 ?
C61 K16 K3 86.4(5) 1_556 2_665 ?
C61 K16 K14 77.1(5) 1_556 . ?
C61 K16 K15 101.8(5) 1_556 . ?
C61 K16 K17 54.8(5) 1_556 . ?
K18 K17 Se7 119.9(2) . . ?
O19 K17 Se7 120.7(5) . . ?
O19 K17 K18 48.2(5) . . ?
O19 K17 N51 129.2(7) . . ?
O19 K17 N52 143.6(7) . . ?
O19 K17 N61 71.0(7) . 1_556 ?
O19 K17 N73 84.7(7) . 1_556 ?
O19 K17 C51 143.9(7) . . ?
O19 K17 C52 158.3(7) . . ?
O19 K17 C61 87.1(7) . 1_556 ?
O21 K17 Se7 71.5(5) . . ?
O21 K17 K18 50.4(5) . . ?
O21 K17 O19 84.2(7) . . ?
O21 K17 O30 110.2(7) . . ?
O21 K17 N51 137.3(7) . . ?
O21 K17 N52 63.8(7) . . ?
O21 K17 N61 143.1(7) . 1_556 ?
O21 K17 N73 74.4(7) . 1_556 ?
O21 K17 C51 117.5(7) . . ?
O21 K17 C52 74.2(7) . . ?
O21 K17 C61 144.0(7) . 1_556 ?
O30 K17 Se7 64.5(5) . . ?
O30 K17 K18 118.6(5) . . ?
O30 K17 O19 75.9(7) . . ?
O30 K17 N51 63.9(7) . . ?
O30 K17 N52 129.7(7) . . ?
O30 K17 N61 90.1(7) . 1_556 ?
O30 K17 N73 159.2(7) . 1_556 ?
O30 K17 C51 69.7(7) . . ?
O30 K17 C52 109.7(7) . . ?
O30 K17 C61 101.3(7) . 1_556 ?
N51 K17 Se7 68.4(4) . . ?
N51 K17 K18 171.7(5) . . ?
N51 K17 C51 20.1(6) . . ?
N51 K17 C52 69.5(7) . . ?
N51 K17 C61 72.5(6) . 1_556 ?
N52 K17 Se7 66.8(5) . . ?
N52 K17 K18 96.0(5) . . ?
N52 K17 N51 87.2(6) . . ?
N52 K17 C51 70.9(6) . . ?
N52 K17 C52 21.0(6) . . ?
N52 K17 C61 108.3(7) . 1_556 ?
N61 K17 Se7 144.9(5) 1_556 . ?
N61 K17 K18 93.0(5) 1_556 . ?
N61 K17 N51 79.0(7) 1_556 . ?
N61 K17 N52 125.6(7) 1_556 . ?
N61 K17 N73 76.5(7) 1_556 1_556 ?
N61 K17 C51 98.1(7) 1_556 . ?
N61 K17 C52 128.7(7) 1_556 . ?
N61 K17 C61 17.6(7) 1_556 1_556 ?
N73 K17 Se7 134.0(5) 1_556 . ?
N73 K17 K18 47.9(5) 1_556 . ?
N73 K17 N51 127.0(6) 1_556 . ?
N73 K17 N52 70.9(6) 1_556 . ?
N73 K17 C51 127.2(7) 1_556 . ?
N73 K17 C52 91.1(7) 1_556 . ?
N73 K17 C61 70.0(7) 1_556 1_556 ?
C51 K17 Se7 51.8(5) . . ?
C51 K17 K18 166.2(5) . . ?
C51 K17 C61 89.2(7) . 1_556 ?
C52 K17 Se7 50.6(5) . . ?
C52 K17 K18 115.0(5) . . ?
C52 K17 C51 51.4(7) . . ?
C52 K17 C61 111.5(7) . 1_556 ?
C61 K17 Se7 140.7(5) 1_556 . ?
C61 K17 K18 99.2(5) 1_556 . ?
K8 K18 K9 64.7(2) 2_665 2_665 ?
K17 K18 K8 84.0(3) . 2_665 ?
K17 K18 K9 118.9(2) . 2_665 ?
O19 K18 K8 44.3(5) . 2_665 ?
O19 K18 K9 76.2(5) . 2_665 ?
O19 K18 K17 47.3(5) . . ?
O19 K18 O21 80.4(7) . . ?
O19 K18 N73 86.2(7) . 1_556 ?
O19 K18 N131 114.6(7) . 2_665 ?
O19 K18 N141 164.2(7) . 1_556 ?
O19 K18 N143 80.1(7) . 1_556 ?
O19 K18 C141 147.3(7) . 1_556 ?
O19 K18 C143 99.6(7) . 1_556 ?
O19 K18 O20 68.1(7) . 1_556 ?
O21 K18 K8 124.6(5) . 2_665 ?
O21 K18 K9 113.2(5) . 2_665 ?
O21 K18 K17 46.6(5) . . ?
O21 K18 N141 113.0(7) . 1_556 ?
O21 K18 C141 132.2(7) . 1_556 ?
O21 K18 C143 164.7(7) . 1_556 ?
O21 K18 O20 125.4(7) . 1_556 ?
N73 K18 K8 95.1(5) 1_556 2_665 ?
N73 K18 K9 159.3(6) 1_556 2_665 ?
N73 K18 K17 50.6(5) 1_556 . ?
N73 K18 O21 73.6(6) 1_556 . ?
N73 K18 N131 150.1(7) 1_556 2_665 ?
N73 K18 N141 89.7(7) 1_556 1_556 ?
N73 K18 N143 125.5(7) 1_556 1_556 ?
N73 K18 C141 99.8(7) 1_556 1_556 ?
N73 K18 C143 121.7(7) 1_556 1_556 ?
N73 K18 O20 61.2(7) 1_556 1_556 ?
N131 K18 K8 114.8(6) 2_665 2_665 ?
N131 K18 K9 50.3(5) 2_665 2_665 ?
N131 K18 K17 129.0(5) 2_665 . ?
N131 K18 O21 88.4(7) 2_665 . ?
N131 K18 N141 75.4(7) 2_665 1_556 ?
N131 K18 N143 81.0(7) 2_665 1_556 ?
N131 K18 C141 74.6(7) 2_665 1_556 ?
N131 K18 C143 77.7(7) 2_665 1_556 ?
N131 K18 O20 144.9(7) 2_665 1_556 ?
N141 K18 K8 121.2(5) 1_556 2_665 ?
N141 K18 K9 104.4(5) 1_556 2_665 ?
N141 K18 K17 136.5(5) 1_556 . ?
N141 K18 C141 19.9(6) 1_556 1_556 ?
N141 K18 C143 69.8(7) 1_556 1_556 ?
N141 K18 O20 96.5(6) 1_556 1_556 ?
N143 K18 K8 42.1(5) 1_556 2_665 ?
N143 K18 K9 41.2(5) 1_556 2_665 ?
N143 K18 K17 125.3(6) 1_556 . ?
N143 K18 O21 151.4(7) 1_556 . ?
N143 K18 N141 90.0(7) 1_556 1_556 ?
N143 K18 C141 70.2(7) 1_556 1_556 ?
N143 K18 C143 20.3(6) 1_556 1_556 ?
N143 K18 O20 64.7(7) 1_556 1_556 ?
C141 K18 K8 103.0(5) 1_556 2_665 ?
C141 K18 K9 89.7(5) 1_556 2_665 ?
C141 K18 K17 150.3(5) 1_556 . ?
C143 K18 K8 58.2(6) 1_556 2_665 ?
C143 K18 K9 52.6(5) 1_556 2_665 ?
C143 K18 K17 141.8(6) 1_556 . ?
C143 K18 C141 50.0(7) 1_556 1_556 ?
C143 K18 O20 67.6(7) 1_556 1_556 ?
O20 K18 K8 40.8(5) 1_556 2_665 ?
O20 K18 K9 101.4(5) 1_556 2_665 ?
O20 K18 K17 80.2(5) 1_556 . ?
O20 K18 C141 86.6(7) 1_556 1_556 ?
K1 O1 K15 92.3(6) . 2_655 ?
K16 O3 K1 138.9(10) 3_565 . ?
K4 O5 K13 133.9(10) . 2_655 ?
K5 O5 K4 89.4(9) . . ?
K5 O5 K13 91.1(8) . 2_655 ?
K13 O6 K5 95.6(7) 2_655 . ?
K6 O8 K11 106.5(7) . . ?
K12 O10 K6 139.7(8) . . ?
K11 O11 K13 101.3(7) . . ?
K14 O13 K13 103.1(8) . . ?
K14 O14 K2 143.6(10) . 3_665 ?
K14 O14 K15 89.1(7) . . ?
K15 O14 K2 96.8(7) . 3_665 ?
K14 O16 K15 88.2(7) . . ?
K16 O18 K3 100.6(6) . 2_665 ?
K17 O19 K8 137.8(9) . 2_665 ?
K17 O19 K18 84.5(7) . . ?
K18 O19 K8 93.8(7) . 2_665 ?
K17 O21 K18 83.0(6) . . ?
K10 O23 K9 137.9(10) . . ?
K10 O27 K7 103.4(6) . . ?
K11 O29 K10 91.3(5) . . ?
K17 O30 K16 86.6(6) . . ?
K2 N12 K1 83.3(6) . . ?
K3 N12 K1 119.8(8) . . ?
K3 N12 K2 85.1(6) . . ?
C12 N12 K1 132(2) . . ?
C12 N12 K2 107(2) . . ?
C12 N12 K3 108(2) . . ?
K4 N13 K2 91.4(6) . . ?
C13 N13 K2 97.9(19) . . ?
C13 N13 K4 112.0(19) . . ?
K2 N21 K3 87.4(8) 1_554 1_554 ?
K2 N21 K4 105.5(9) 1_554 1_554 ?
K4 N21 K3 147.8(10) 1_554 1_554 ?
C21 N21 K2 147(2) . 1_554 ?
C21 N21 K3 86(2) . 1_554 ?
C21 N21 K4 97(2) . 1_554 ?
K4 N22 K7 139.9(9) 1_554 1_554 ?
K6 N22 K4 105.8(8) 1_554 1_554 ?
K6 N22 K7 82.3(7) 1_554 1_554 ?
C22 N22 K4 96(2) . 1_554 ?
C22 N22 K6 158(2) . 1_554 ?
C22 N22 K7 84(2) . 1_554 ?
K7 N23 K3 152.1(10) 1_554 1_554 ?
K8 N23 K3 104.4(9) 1_554 1_554 ?
K8 N23 K7 91.6(8) 1_554 1_554 ?
C23 N23 K3 86(2) . 1_554 ?
C23 N23 K7 95(2) . 1_554 ?
C23 N23 K8 143(2) . 1_554 ?
K7 N32 K6 92.0(6) . . ?
K7 N32 K10 98.6(7) . . ?
K10 N32 K6 100.1(7) . . ?
C32 N32 K6 104.3(19) . . ?
C32 N32 K7 113.9(19) . . ?
C32 N32 K10 138(2) . . ?
K4 N33 K6 103.1(7) . . ?
K5 N33 K4 88.9(7) . . ?
K5 N33 K6 88.1(6) . . ?
C33 N33 K4 109(2) . . ?
C33 N33 K5 159(2) . . ?
C33 N33 K6 99(2) . . ?
K3 N42 K16 93.3(8) . 3_565 ?
C42 N42 K3 109(2) . . ?
C42 N42 K16 138(2) . 3_565 ?
K7 N43 K9 112.0(8) . . ?
K8 N43 K7 81.6(6) . . ?
K8 N43 K9 92.5(7) . . ?
C43 N43 K7 107(2) . . ?
C43 N43 K8 110(2) . . ?
C43 N43 K9 137(2) . . ?
K16 N51 K14 111.4(7) . . ?
K16 N51 K17 82.9(6) . . ?
K17 N51 K14 140.9(8) . . ?
C51 N51 K14 88.9(19) . . ?
C51 N51 K16 157(2) . . ?
C51 N51 K17 87.6(18) . . ?
K10 N52 K11 83.9(6) . . ?
K10 N52 K17 109.1(8) . . ?
K17 N52 K11 144.1(8) . . ?
C52 N52 K10 158(2) . . ?
C52 N52 K11 84.2(18) . . ?
C52 N52 K17 91.2(19) . . ?
K13 N53 K11 97.6(7) . . ?
K13 N53 K14 103.8(8) . . ?
K14 N53 K11 150.2(9) . . ?
C53 N53 K11 87.6(19) . . ?
C53 N53 K13 130(2) . . ?
C53 N53 K14 94(2) . . ?
K17 N61 K16 88.0(7) 1_554 1_554 ?
C61 N61 K16 104(2) . 1_554 ?
C61 N61 K17 113(2) . 1_554 ?
K15 N62 K14 88.2(7) 1_554 1_554 ?
C62 N62 K14 105(2) . 1_554 ?
C62 N62 K15 167(2) . 1_554 ?
K6 N71 K10 100.2(7) 1_554 1_554 ?
K6 N71 K11 100.9(7) 1_554 1_554 ?
K11 N71 K10 89.2(6) 1_554 1_554 ?
C71 N71 K6 144.8(19) . 1_554 ?
C71 N71 K10 102.4(18) . 1_554 ?
C71 N71 K11 106.2(18) . 1_554 ?
K17 N73 K10 101.8(7) 1_554 1_554 ?
K18 N73 K10 97.0(7) 1_554 1_554 ?
K18 N73 K17 81.5(6) 1_554 1_554 ?
C73 N73 K10 94.2(19) . 1_554 ?
C73 N73 K17 112.1(19) . 1_554 ?
C73 N73 K18 160(2) . 1_554 ?
K12 N81 K11 111.4(7) 1_554 1_554 ?
C81 N81 K11 105.1(17) . 1_554 ?
C81 N81 K12 141.2(18) . 1_554 ?
C82 N82 K13 128(2) . . ?
C83 N83 K14 110(2) . 1_554 ?
K1 N91 K15 96.3(6) 2_664 1_554 ?
C91 N91 K1 111.4(19) . 2_664 ?
C91 N91 K15 101.5(19) . 1_554 ?
K1 N93 K15 99.6(6) 3_664 1_554 ?
K2 N93 K1 100.7(7) 3_664 3_664 ?
K2 N93 K15 101.4(7) 3_664 1_554 ?
C93 N93 K1 113.6(19) . 3_664 ?
C93 N93 K2 135.6(19) . 3_664 ?
C93 N93 K15 99.8(18) . 1_554 ?
K1 N101 K1 145.3(8) 2_665 3_665 ?
K15 N101 K1 91.4(7) . 3_665 ?
K15 N101 K1 98.8(7) . 2_665 ?
C101 N101 K1 92(2) . 2_665 ?
C101 N101 K1 84.9(19) . 3_665 ?
C101 N101 K15 166(2) . . ?
K12 N112 K5 99.3(6) . . ?
C112 N112 K5 97.8(18) . . ?
C112 N112 K12 114.1(18) . . ?
K12 N113 K5 97.9(7) 2_655 . ?
K13 N113 K5 92.0(7) 2_655 . ?
K13 N113 K12 115.5(8) 2_655 2_655 ?
C113 N113 K5 100(2) . . ?
C113 N113 K12 118(2) . 2_655 ?
C113 N113 K13 122(2) . 2_655 ?
K5 N121 K12 90.8(7) 1_554 2_654 ?
K5 N121 K12 100.6(7) 1_554 1_554 ?
K12 N121 K12 148.4(8) 1_554 2_654 ?
C121 N121 K5 162(2) . 1_554 ?
C121 N121 K12 90.6(19) . 1_554 ?
C121 N121 K12 86.5(19) . 2_654 ?
K9 N131 K9 148.8(8) 3_565 . ?
K18 N131 K9 98.4(7) 3_565 3_565 ?
K18 N131 K9 87.3(7) 3_565 . ?
C131 N131 K9 91(2) . 3_565 ?
C131 N131 K9 90(2) . . ?
C131 N131 K18 166(2) . 3_565 ?
K9 N141 K18 100.8(6) 1_554 1_554 ?
C141 N141 K9 112.3(18) . 1_554 ?
C141 N141 K18 94.8(18) . 1_554 ?
K8 N143 K9 106.6(8) 2_664 2_664 ?
K8 N143 K18 94.4(8) 2_664 1_554 ?
K9 N143 K18 96.2(7) 2_664 1_554 ?
C143 N143 K8 136(2) . 2_664 ?
C143 N143 K9 115(2) . 2_664 ?
C143 N143 K18 96(2) . 1_554 ?
N11 C11 Re1 176(3) . . ?
N11 C11 Mo1 176(3) . . ?
N12 C12 Re1 177(2) . . ?
N12 C12 Mo1 177(2) . . ?
Re1 C13 K4 132.3(10) . . ?
Mo1 C13 K4 132.3(10) . . ?
N13 C13 Re1 178(2) . . ?
N13 C13 Mo1 178(2) . . ?
N13 C13 K4 50.0(16) . . ?
Mo2 C21 K3 105.6(11) . 1_554 ?
Mo2 C21 K4 115.2(12) . 1_554 ?
K4 C21 K3 126.0(9) 1_554 1_554 ?
N21 C21 Re2 174(3) . . ?
N21 C21 Mo2 174(3) . . ?
N21 C21 K3 74(2) . 1_554 ?
N21 C21 K4 62(2) . 1_554 ?
Mo2 C22 K4 111.5(11) . 1_554 ?
Mo2 C22 K7 104.7(11) . 1_554 ?
K7 C22 K4 125.0(9) 1_554 1_554 ?
N22 C22 Re2 176(3) . . ?
N22 C22 Mo2 176(3) . . ?
N22 C22 K4 64.9(19) . 1_554 ?
N22 C22 K7 77(2) . 1_554 ?
Mo2 C23 K3 110.6(11) . 1_554 ?
Mo2 C23 K7 110.8(11) . 1_554 ?
K3 C23 K7 128.4(10) 1_554 1_554 ?
N23 C23 Re2 174(3) . . ?
N23 C23 Mo2 174(3) . . ?
N23 C23 K3 72.3(19) . 1_554 ?
N23 C23 K7 63.9(19) . 1_554 ?
N31 C31 Re3 175(2) . . ?
N31 C31 Mo3 175(2) . . ?
Re3 C32 K6 119.1(10) . . ?
Re3 C32 K7 128.7(11) . . ?
Mo3 C32 K6 119.1(10) . . ?
Mo3 C32 K7 128.7(11) . . ?
K6 C32 K7 74.4(5) . . ?
N32 C32 Re3 175(2) . . ?
N32 C32 Mo3 175(2) . . ?
N32 C32 K6 56.6(16) . . ?
N32 C32 K7 48.6(16) . . ?
Re3 C33 K4 131.5(11) . . ?
Re3 C33 K6 111.2(10) . . ?
Mo3 C33 K4 131.5(11) . . ?
Mo3 C33 K6 111.2(10) . . ?
K4 C33 K6 87.1(6) . . ?
N33 C33 Re3 173(3) . . ?
N33 C33 Mo3 173(3) . . ?
N33 C33 K4 53.9(18) . . ?
N33 C33 K6 63.7(19) . . ?
N41 C41 Re4 179(3) . . ?
N41 C41 Mo4 179(3) . . ?
Re4 C42 K3 129.2(12) . . ?
Mo4 C42 K3 129.2(12) . . ?
N42 C42 Re4 178(3) . . ?
N42 C42 Mo4 178(3) . . ?
N42 C42 K3 52.1(17) . . ?
N43 C43 Re4 178(3) . . ?
N43 C43 Mo4 178(3) . . ?
Re5 C51 K14 107.9(9) . . ?
Re5 C51 K17 105.7(9) . . ?
Mo5 C51 K14 107.9(9) . . ?
Mo5 C51 K17 105.7(9) . . ?
K17 C51 K14 127.3(8) . . ?
N51 C51 Re5 176(2) . . ?
N51 C51 Mo5 176(2) . . ?
N51 C51 K14 71.6(17) . . ?
N51 C51 K17 72.3(18) . . ?
Re5 C52 K11 107.3(10) . . ?
Re5 C52 K17 109.3(10) . . ?
Mo5 C52 K11 107.3(10) . . ?
Mo5 C52 K17 109.3(10) . . ?
K17 C52 K11 129.6(8) . . ?
N52 C52 Re5 177(2) . . ?
N52 C52 Mo5 177(2) . . ?
N52 C52 K11 75.9(18) . . ?
N52 C52 K17 67.8(18) . . ?
Re5 C53 K11 110.4(10) . . ?
Re5 C53 K14 111.3(11) . . ?
Mo5 C53 K11 110.4(10) . . ?
Mo5 C53 K14 111.3(11) . . ?
K11 C53 K14 127.5(9) . . ?
N53 C53 Re5 175(2) . . ?
N53 C53 Mo5 175(2) . . ?
N53 C53 K11 71.4(18) . . ?
N53 C53 K14 64.9(18) . . ?
Re6 C61 K16 125.6(11) . 1_554 ?
Mo6 C61 K16 125.6(11) . 1_554 ?
Mo6 C61 K17 132.0(12) . 1_554 ?
K16 C61 K17 71.8(6) 1_554 1_554 ?
N61 C61 Re6 177(3) . . ?
N61 C61 Mo6 177(3) . . ?
N61 C61 K16 56.9(18) . 1_554 ?
N61 C61 K17 49.4(18) . 1_554 ?
Mo6 C62 K14 128.8(13) . 1_554 ?
N62 C62 Re6 176(3) . . ?
N62 C62 Mo6 176(3) . . ?
N62 C62 K14 54.7(17) . 1_554 ?
N63 C63 Re6 175(3) . . ?
N63 C63 Mo6 175(3) . . ?
Mo7 C71 K10 117.0(10) . 1_554 ?
Mo7 C71 K11 130.1(10) . 1_554 ?
K10 C71 K11 74.3(5) 1_554 1_554 ?
N71 C71 Re7 173(2) . . ?
N71 C71 Mo7 173(2) . . ?
N71 C71 K10 58.1(16) . 1_554 ?
N71 C71 K11 54.9(15) . 1_554 ?
N72 C72 Re7 176(2) . . ?
N72 C72 Mo7 176(2) . . ?
Mo7 C73 K10 113.4(10) . 1_554 ?
N73 C73 Re7 178(2) . . ?
N73 C73 Mo7 178(2) . . ?
N73 C73 K10 66.2(17) . 1_554 ?
Mo8 C81 K11 127.8(10) . 1_554 ?
N81 C81 Re8 176(2) . . ?
N81 C81 Mo8 176(2) . . ?
N81 C81 K11 55.7(14) . 1_554 ?
N82 C82 Re8 177(3) . . ?
N82 C82 Mo8 177(3) . . ?
Mo8 C83 K14 128.5(12) . 1_554 ?
N83 C83 Re8 179(3) . . ?
N83 C83 Mo8 179(3) . . ?
N83 C83 K14 51.0(18) . 1_554 ?
Mo9 C91 K1 130.5(10) . 2_664 ?
Mo9 C91 K15 115.5(10) . 1_554 ?
K15 C91 K1 80.2(6) 1_554 2_664 ?
N91 C91 Re9 176(2) . . ?
N91 C91 Mo9 176(2) . . ?
N91 C91 K1 51.6(16) . 2_664 ?
N91 C91 K15 60.4(17) . 1_554 ?
N92 C92 Re9 178(3) . . ?
N92 C92 Mo9 178(3) . . ?
Re9 C93 K1 131.9(11) . 3_664 ?
Mo9 C93 K1 131.9(11) . 3_664 ?
Mo9 C93 K15 118.2(11) . 1_554 ?
K15 C93 K1 80.5(6) 1_554 3_664 ?
N93 C93 Re9 178(2) . . ?
N93 C93 Mo9 178(2) . . ?
N93 C93 K1 48.3(15) . 3_664 ?
N93 C93 K15 60.0(16) . 1_554 ?
Re10 C101 K1 111.7(11) . 2_665 ?
Mo10 C101 K1 106.9(10) . 3_665 ?
Mo10 C101 K1 111.7(11) . 2_665 ?
K1 C101 K1 129.8(9) 2_665 3_665 ?
N101 C101 Re10 177(2) . . ?
N101 C101 Mo10 177(2) . . ?
N101 C101 K1 75.4(19) . 3_665 ?
N101 C101 K1 67.5(18) . 2_665 ?
N111 C111 Re11 176(2) . . ?
N111 C111 Mo11 176(2) . . ?
Re11 C112 K5 115.1(10) . . ?
Mo11 C112 K5 115.1(10) . . ?
N112 C112 Re11 178(2) . . ?
N112 C112 Mo11 178(2) . . ?
N112 C112 K5 62.9(16) . . ?
Re11 C113 K5 117.1(10) . . ?
Mo11 C113 K5 117.1(10) . . ?
Mo11 C113 K12 134.0(11) . 2_655 ?
K5 C113 K12 79.8(6) . 2_655 ?
N113 C113 Re11 178(2) . . ?
N113 C113 Mo11 178(2) . . ?
N113 C113 K5 61.3(18) . . ?
N113 C113 K12 45.7(17) . 2_655 ?
Mo12 C121 K12 105.3(10) . 2_654 ?
Mo12 C121 K12 109.1(11) . 1_554 ?
K12 C121 K12 131.6(9) 1_554 2_654 ?
N121 C121 Re12 175(2) . . ?
N121 C121 Mo12 175(2) . . ?
N121 C121 K12 73.8(18) . 2_654 ?
N121 C121 K12 68.9(18) . 1_554 ?
Re13 C131 K9 107.8(11) . . ?
Mo13 C131 K9 107.8(11) . . ?
Mo13 C131 K9 108.9(11) . 3_565 ?
K9 C131 K9 131.4(9) 3_565 . ?
N131 C131 Re13 178(3) . . ?
N131 C131 Mo13 178(3) . . ?
N131 C131 K9 70(2) . 3_565 ?
N131 C131 K9 72(2) . . ?
Re14 C141 K18 111.6(10) . 1_554 ?
Mo14 C141 K9 132.4(10) . 1_554 ?
Mo14 C141 K18 111.6(10) . 1_554 ?
K18 C141 K9 84.2(6) 1_554 1_554 ?
N141 C141 Re14 176(2) . . ?
N141 C141 Mo14 176(2) . . ?
N141 C141 K9 50.2(15) . 1_554 ?
N141 C141 K18 65.4(16) . 1_554 ?
N142 C142 Re14 176(2) . . ?
N142 C142 Mo14 176(2) . . ?
Re14 C143 K18 117.3(11) . 1_554 ?
Mo14 C143 K9 134.7(11) . 2_664 ?
Mo14 C143 K18 117.3(11) . 1_554 ?
K18 C143 K9 79.3(6) 1_554 2_664 ?
N143 C143 Re14 177(2) . . ?
N143 C143 Mo14 177(2) . . ?
N143 C143 K9 48.1(17) . 2_664 ?
N143 C143 K18 63.5(18) . 1_554 ?
K3 O2 K2 92.4(6) 1_554 1_554 ?
K4 O7 K6 100.1(7) 1_554 1_554 ?
K5 O7 K4 89.5(7) 1_554 1_554 ?
K5 O7 K6 85.6(6) 1_554 1_554 ?
K12 O12 K5 90.9(5) 1_554 3_664 ?
K8 O20 K18 87.8(8) 2_664 1_554 ?
K7 O24 K8 89.7(8) 1_554 1_554 ?
K3 O26 K8 101.9(8) 1_554 1_554 ?
K7 O28 K6 93.5(6) 1_554 1_554 ?

# end Validation Reply Form
_olex2_submission_special_instructions 'No special instructions were received'
loop_
_twin_individual_id
_twin_individual_mass_fraction_refined
1 0.45(2)
2 0.55(2)

_vrf_PLAT043_pr555               
;
PROBLEM: Calculated and Reported Mol. Weight Differ by ..     170.61 Check
RESPONSE: Hydrogen atoms of H2O molecules were not localized,
but included in the formula of the compound.
;
# start Validation Reply Form
_vrf_PLAT306_pr555               
;
PROBLEM: Isolated Oxygen Atom (H-atoms Missing ?) .......         O1-O30
RESPONSE: These oxygen atoms belong to H2O molecules.
Hydrogen atoms were not localized, but included in the formula of the compound.
;
_exptl_crystal_preparation       'Magnetic properties'
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_pr939
_database_code_depnum_ccdc_archive 'CCDC 2111042'
loop_
_audit_author_name
_audit_author_address
'Taisiya Sukhikh'
;NIIC SB RAS
Russia
;
_audit_update_record             
;
2021-09-21 deposited with the CCDC.	2021-11-15 downloaded from the CCDC.
;
_audit_creation_date             2021-05-29
_audit_creation_method           
;
Olex2 1.2
(compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506)
;
_shelx_SHELXL_version_number     2017/1
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C13 H16.48 Cs6 N12 O6.24 Re Se4 W3'
_chemical_formula_sum            'C13 H16.48 Cs6 N12 O6.24 Re Se4 W3'
_chemical_formula_weight         2291.66
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cs Cs -0.3680 2.1192 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Re Re -1.0185 7.2310 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Se Se -0.0929 2.2259 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
W W -0.8490 6.8722 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_H-M_alt        'P 1 21/n 1'
_space_group_name_Hall           '-P 2yn'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'

_cell_length_a                   18.6439(3)
_cell_length_b                   10.4129(2)
_cell_length_c                   22.0131(4)
_cell_angle_alpha                90
_cell_angle_beta                 108.4950(10)
_cell_angle_gamma                90
_cell_volume                     4052.83(13)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    9239
_cell_measurement_temperature    150(2)
_cell_measurement_theta_max      33.12
_cell_measurement_theta_min      2.32
_shelx_estimated_absorpt_T_max   0.292
_shelx_estimated_absorpt_T_min   0.064
_exptl_absorpt_coefficient_mu    20.407
_exptl_absorpt_correction_T_max  0.7465
_exptl_absorpt_correction_T_min  0.1888
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
'SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1840 before and 0.0724 after correction. The Ratio of minimum to maximum transmission is 0.2529. The λ/2 correction factor is Not present.'
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            brown
_exptl_crystal_colour_primary    brown
_exptl_crystal_density_diffrn    3.733
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       needle
_exptl_crystal_F_000             3911
_exptl_crystal_size_max          0.3
_exptl_crystal_size_mid          0.08
_exptl_crystal_size_min          0.08
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0568
_diffrn_reflns_av_unetI/netI     0.0397
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 1.000
_diffrn_reflns_limit_h_max       25
_diffrn_reflns_limit_h_min       -21
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_l_max       29
_diffrn_reflns_limit_l_min       -29
_diffrn_reflns_number            64300
_diffrn_reflns_point_group_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 1.000
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         28.696
_diffrn_reflns_theta_min         1.729
_diffrn_ambient_temperature      150(2)
_diffrn_detector                 PIXEL
_diffrn_detector_area_resol_mean 7.41
_diffrn_detector_type            'Bruker PHOTON III area detector'
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device       'three-circle diffractometer'
_diffrn_measurement_device_type  'Bruker D8 Venture diffractometer'
_diffrn_measurement_method       'ω and φ scans'
_diffrn_radiation_monochromator  'Incoatec HELIOS multilayer mirrors'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   'Incoatec IuS3.0 microfocus X-ray tube'
_diffrn_special_details          ?
_diffrn_standards_interval_count .
_diffrn_standards_interval_time  .
_diffrn_standards_number         .
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                10088
_reflns_number_total             10457
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'Bruker SAINT'
_computing_data_collection       'Bruker APEX3'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    'ShelXT (Sheldrick, 2015)'
_refine_diff_density_max         1.945
_refine_diff_density_min         -2.831
_refine_diff_density_rms         0.280
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.148
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     456
_refine_ls_number_reflns         10457
_refine_ls_number_restraints     26
_refine_ls_R_factor_all          0.0326
_refine_ls_R_factor_gt           0.0314
_refine_ls_restrained_S_all      1.150
_refine_ls_shift/su_max          0.008
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0099P)²+51.2679P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0752
_refine_ls_wR_factor_ref         0.0758
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.5 times of:
  All C(H,H,H) groups
2. Shared sites
{Re2, W2}
{Re4, W4}
{Re3, W3}
{Re1, W1}
3. Uiso/Uaniso restraints and constraints
Uanis(Cs2) \\sim Ueq, Uanis(Cs6) \\sim Ueq, Uanis(Cs9) \\sim Ueq, Uanis(Cs10)
\\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(Re2) = Uanis(W2)
Uanis(Re4) = Uanis(W4)
Uanis(Re3) = Uanis(W3)
Uanis(Re1) = Uanis(W1)
4. Others
 1*[Sof(Cs2)+Sof(O2)]+1*[Sof(Cs9)]+1*[Sof(Cs8)]=1 with esd of 0.001
 1*[Sof(Cs6)+Sof(O5)+Sof(O6)]+1*[Sof(Cs10)]+1*[Sof(Cs7)+Sof(O8)]=1 with esd of
 0.001
 Sof(O2)=1-FVAR(1)
 Sof(Cs2)=FVAR(1)
 Sof(O8)=1-FVAR(4)
 Sof(Cs7)=FVAR(4)
 Sof(O6)=1-FVAR(6)
 Sof(Cs6)=Sof(O5)=FVAR(6)
 Fixed Sof: Re1(0.25) Re2(0.25) Re3(0.25) Re4(0.25) W1(0.75) W2(0.75) W3(0.75)
 W4(0.75)
5.a Riding coordinates:
 C1(H1A,H1B,H1C)
;
_atom_sites_solution_hydrogens   difmap
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Re1 Re 0.46898(2) 0.96670(2) 0.67572(2) 0.01115(6) Uani 0.25 1 d . . P A 1
Re2 Re 0.38552(2) 0.73304(2) 0.66533(2) 0.01126(6) Uani 0.25 1 d . . P A 1
Re3 Re 0.48795(2) 0.81122(2) 0.78738(2) 0.01418(6) Uani 0.25 1 d . . P A 1
Re4 Re 0.54705(2) 0.72771(2) 0.68848(2) 0.01110(6) Uani 0.25 1 d . . P A 1
W1 W 0.46898(2) 0.96670(2) 0.67572(2) 0.01115(6) Uani 0.75 1 d . . P A 2
W2 W 0.38552(2) 0.73304(2) 0.66533(2) 0.01126(6) Uani 0.75 1 d . . P A 2
W3 W 0.48795(2) 0.81122(2) 0.78738(2) 0.01418(6) Uani 0.75 1 d . . P A 2
W4 W 0.54705(2) 0.72771(2) 0.68848(2) 0.01110(6) Uani 0.75 1 d . . P A 2
Cs1 Cs 0.28048(2) 0.92999(4) 0.43660(2) 0.02064(9) Uani 1 1 d . . . . .
Cs3 Cs 0.56609(2) 0.69386(4) 0.48551(2) 0.01939(8) Uani 1 1 d . . . . .
Cs4 Cs 0.29894(3) 0.29279(5) 0.69211(3) 0.02835(10) Uani 1 1 d . . . . .
Cs5 Cs 0.66753(3) 0.28284(4) 0.73588(2) 0.02611(10) Uani 1 1 d . . . . .
Cs6 Cs 0.5255(2) 0.3652(4) 0.8867(2) 0.0230(6) Uani 0.51(2) 1 d . U P A 1
Cs9 Cs 0.6798(2) 0.9567(4) 0.98438(19) 0.0474(15) Uani 0.167(3) 1 d . U P A 1
Cs8 Cs 0.6416(6) 0.9107(10) 1.0053(6) 0.114(4) Uiso 0.162(4) 1 d . U P A 2
Cs10 Cs 0.5158(6) 0.3898(12) 0.8865(4) 0.0468(16) Uani 0.40(2) 1 d . U P A 2
Cs2 Cs 0.37018(5) 1.05480(11) 0.95495(6) 0.0518(4) Uani 0.666(3) 1 d . U P A 3
Cs7 Cs 0.4915(6) 0.3072(9) 0.9673(5) 0.063(3) Uiso 0.093(3) 1 d . U P A 3
Se1 Se 0.59293(3) 0.91757(6) 0.75875(3) 0.01552(12) Uani 1 1 d . . . . .
Se2 Se 0.36969(4) 0.92575(6) 0.72730(3) 0.01525(12) Uani 1 1 d . . . . .
Se3 Se 0.45025(3) 0.80554(6) 0.58823(3) 0.01246(11) Uani 1 1 d . . . . .
Se4 Se 0.47667(4) 0.58892(6) 0.74231(3) 0.01661(12) Uani 1 1 d . . . . .
O1 O 0.2974(4) 0.8154(8) 0.9930(4) 0.058(2) Uani 1 1 d . . . . .
O3 O 0.3465(4) 0.4047(6) 0.8312(3) 0.0356(13) Uani 1 1 d . . . . .
O4 O 0.6407(5) 0.4283(8) 1.0200(3) 0.057(2) Uani 1 1 d . . . . .
O9 O 0.3066(4) 0.6558(7) 0.4013(4) 0.0440(16) Uani 1 1 d . . . . .
O2 O 0.5746(11) 1.114(2) 1.0249(8) 0.041(5) Uani 0.334(3) 1 d . . P A 1
O5 O 0.6789(7) 0.2632(16) 0.8809(7) 0.034(3) Uani 0.51(2) 1 d . . P A 1
O8 O 0.4641(6) 0.2948(13) 0.9942(5) 0.078(3) Uani 0.907(3) 1 d . . P A 1
O6 O 0.6489(19) 0.210(3) 0.8713(12) 0.086(8) Uani 0.49(2) 1 d . . P A 2
N11 N 0.5685(3) 1.1244(6) 0.6002(3) 0.0221(12) Uani 1 1 d . . . . .
N12 N 0.4872(4) 1.2487(6) 0.7471(3) 0.0288(14) Uani 1 1 d . . . . .
N13 N 0.3335(3) 1.1254(6) 0.5688(3) 0.0204(11) Uani 1 1 d . . . . .
N21 N 0.2260(3) 0.8366(6) 0.5630(3) 0.0226(12) Uani 1 1 d . . . . .
N22 N 0.3364(4) 0.4736(6) 0.5763(3) 0.0263(13) Uani 1 1 d . . . . .
N23 N 0.2573(5) 0.5984(7) 0.7184(5) 0.045(2) Uani 1 1 d . . . . .
N31 N 0.5132(4) 1.0380(7) 0.8967(4) 0.0376(17) Uani 1 1 d . . . . .
N32 N 0.6170(4) 0.6741(8) 0.9077(3) 0.0375(17) Uani 1 1 d . . . . .
N34 N 0.3859(5) 0.7019(9) 0.8733(4) 0.0403(18) Uani 1 1 d . . . . .
N41 N 0.6754(3) 0.8125(6) 0.6217(3) 0.0223(12) Uani 1 1 d . . . . .
N42 N 0.5594(3) 0.4767(6) 0.6009(3) 0.0221(12) Uani 1 1 d . . . . .
N43 N 0.7009(4) 0.5823(6) 0.7813(3) 0.0246(13) Uani 1 1 d . . . . .
C1 C 0.2627(6) 0.5491(11) 0.4035(6) 0.053(3) Uani 1 1 d . . . . .
H1A H 0.264760 0.534799 0.447977 0.079 Uiso 1 1 d R . . . .
H1B H 0.210040 0.560609 0.376657 0.079 Uiso 1 1 d R . . . .
H1C H 0.284350 0.474759 0.388197 0.079 Uiso 1 1 d R . . . .
C11 C 0.5353(3) 1.0661(6) 0.6272(3) 0.0156(12) Uani 1 1 d . . . . .
C12 C 0.4807(4) 1.1489(6) 0.7239(3) 0.0188(13) Uani 1 1 d . . . . .
C13 C 0.3802(4) 1.0682(6) 0.6063(3) 0.0157(12) Uani 1 1 d . . . . .
C21 C 0.2835(4) 0.8015(6) 0.5971(3) 0.0144(11) Uani 1 1 d . . . . .
C22 C 0.3566(4) 0.5655(6) 0.6063(3) 0.0173(12) Uani 1 1 d . . . . .
C23 C 0.3036(4) 0.6473(7) 0.7022(4) 0.0234(15) Uani 1 1 d . . . . .
C31 C 0.4204(5) 0.7383(8) 0.8413(4) 0.0257(15) Uani 1 1 d . . . . .
C32 C 0.5050(4) 0.9624(8) 0.8570(4) 0.0249(15) Uani 1 1 d . . . . .
C33 C 0.5738(4) 0.7234(8) 0.8648(4) 0.0245(15) Uani 1 1 d . . . . .
C41 C 0.6293(4) 0.7879(6) 0.6449(3) 0.0151(12) Uani 1 1 d . . . . .
C42 C 0.5507(3) 0.5613(6) 0.6317(3) 0.0146(11) Uani 1 1 d . . . . .
C43 C 0.6470(4) 0.6355(6) 0.7511(3) 0.0159(12) Uani 1 1 d . . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Re1 Re2 2.8579(3) . ?
Re1 Re3 2.8698(3) . ?
Re1 Re4 2.8515(3) . ?
Re1 Se1 2.5025(7) . ?
Re1 Se2 2.4961(7) . ?
Re1 Se3 2.4942(7) . ?
Re1 C11 2.140(7) . ?
Re1 C12 2.151(7) . ?
Re1 C13 2.142(6) . ?
Re2 Re3 2.8761(3) . ?
Re2 Re4 2.8911(3) . ?
Re2 Se2 2.4960(7) . ?
Re2 Se3 2.4913(7) . ?
Re2 Se4 2.4868(7) . ?
Re2 C21 2.138(6) . ?
Re2 C22 2.140(7) . ?
Re2 C23 2.139(7) . ?
Re3 Re4 2.8691(3) . ?
Re3 Se1 2.4974(7) . ?
Re3 Se2 2.4864(7) . ?
Re3 Se4 2.5008(7) . ?
Re3 C31 2.125(8) . ?
Re3 C32 2.149(8) . ?
Re3 C33 2.138(7) . ?
Re4 Se1 2.4886(7) . ?
Re4 Se3 2.5013(6) . ?
Re4 Se4 2.4903(7) . ?
Re4 C41 2.144(7) . ?
Re4 C42 2.150(6) . ?
Re4 C43 2.160(6) . ?
W1 W2 2.8579(3) . ?
W1 W3 2.8698(3) . ?
W1 W4 2.8515(3) . ?
W1 Se1 2.5025(7) . ?
W1 Se2 2.4961(7) . ?
W1 Se3 2.4942(7) . ?
W1 C11 2.140(7) . ?
W1 C12 2.151(7) . ?
W1 C13 2.142(6) . ?
W2 W3 2.8761(3) . ?
W2 W4 2.8911(3) . ?
W2 Se2 2.4960(7) . ?
W2 Se3 2.4913(7) . ?
W2 Se4 2.4868(7) . ?
W2 C21 2.138(6) . ?
W2 C22 2.140(7) . ?
W2 C23 2.139(7) . ?
W3 W4 2.8691(3) . ?
W3 Se1 2.4974(7) . ?
W3 Se2 2.4864(7) . ?
W3 Se4 2.5008(7) . ?
W3 C31 2.125(8) . ?
W3 C32 2.149(8) . ?
W3 C33 2.138(7) . ?
W4 Se1 2.4886(7) . ?
W4 Se3 2.5013(6) . ?
W4 Se4 2.4903(7) . ?
W4 C41 2.144(7) . ?
W4 C42 2.150(6) . ?
W4 C43 2.160(6) . ?
Cs1 Cs9 4.701(4) 4_575 ?
Cs1 Se3 4.0170(7) . ?
Cs1 O9 3.039(7) . ?
Cs1 O5 3.718(16) 4_575 ?
Cs1 N11 3.218(6) 3_676 ?
Cs1 N13 3.429(6) . ?
Cs1 N21 3.393(6) . ?
Cs1 N32 3.106(7) 4_575 ?
Cs1 N41 3.191(6) 3_676 ?
Cs1 N43 3.269(6) 4_575 ?
Cs1 C13 3.882(7) . ?
Cs1 C21 3.762(6) . ?
Cs3 Se3 3.7720(7) . ?
Cs3 N11 3.230(6) 3_676 ?
Cs3 N13 3.146(6) 3_676 ?
Cs3 N22 3.125(7) 3_666 ?
Cs3 N41 3.284(6) . ?
Cs3 N42 3.433(6) . ?
Cs3 N42 3.070(6) 3_666 ?
Cs3 C11 3.606(7) 3_676 ?
Cs3 C13 3.537(7) 3_676 ?
Cs3 C41 3.469(6) . ?
Cs3 C42 3.597(6) . ?
Cs3 C42 3.859(6) 3_666 ?
Cs4 O3 3.129(6) . ?
Cs4 N12 3.362(7) 1_545 ?
Cs4 N13 3.455(6) 1_545 ?
Cs4 N22 3.414(7) . ?
Cs4 N23 3.224(8) 2_546 ?
Cs4 N23 3.369(7) . ?
Cs4 N34 3.420(8) 2_546 ?
Cs4 C12 3.565(6) 1_545 ?
Cs4 C13 3.626(6) 1_545 ?
Cs4 C22 3.752(7) . ?
Cs4 C23 3.697(7) . ?
Cs4 C23 3.766(7) 2_546 ?
Cs5 O9 3.269(7) 3_666 ?
Cs5 O5 3.139(15) . ?
Cs5 O6 3.20(3) . ?
Cs5 N11 3.399(7) 1_545 ?
Cs5 N12 3.466(7) 1_545 ?
Cs5 N41 3.561(6) 2_646 ?
Cs5 N42 3.628(6) . ?
Cs5 N43 3.274(6) . ?
Cs5 N43 3.333(7) 2_646 ?
Cs5 C11 3.626(6) 1_545 ?
Cs5 C12 3.683(7) 1_545 ?
Cs5 C43 3.709(6) 2_646 ?
Cs6 Se4 3.811(5) . ?
Cs6 O3 3.195(8) . ?
Cs6 O4 3.107(9) . ?
Cs6 O5 3.092(15) . ?
Cs6 O8 3.025(12) . ?
Cs6 N12 3.169(8) 1_545 ?
Cs6 N31 3.426(9) 1_545 ?
Cs6 N32 3.601(10) . ?
Cs6 C33 3.902(9) . ?
Cs9 O1 2.435(10) 3_677 ?
Cs9 O9 3.612(8) 4_676 ?
Cs9 O2 2.90(2) . ?
Cs9 N21 3.482(8) 4_676 ?
Cs9 N22 3.067(8) 4_676 ?
Cs9 N31 3.207(9) . ?
Cs9 N32 3.409(10) . ?
Cs9 C1 2.704(13) 4_676 ?
Cs9 C21 3.752(8) 4_676 ?
Cs9 C22 3.537(8) 4_676 ?
Cs9 C32 3.563(8) . ?
Cs9 C33 3.666(9) . ?
Cs8 Cs10 5.341(14) 3_667 ?
Cs8 O1 3.066(14) 3_677 ?
Cs8 N21 3.075(12) 4_676 ?
Cs8 N22 3.672(13) 4_676 ?
Cs8 N31 3.094(13) . ?
Cs8 N32 3.204(14) . ?
Cs8 C1 3.674(19) 4_676 ?
Cs8 C21 3.545(12) 4_676 ?
Cs8 C32 3.487(13) . ?
Cs8 C33 3.533(14) . ?
Cs10 Se4 3.665(9) . ?
Cs10 O3 3.005(12) . ?
Cs10 O4 3.144(11) . ?
Cs10 O6 3.21(3) . ?
Cs10 N12 3.289(12) 1_545 ?
Cs10 N31 3.671(14) 1_545 ?
Cs10 N32 3.462(13) . ?
Cs10 C33 3.713(13) . ?
Cs2 Cs2 4.7517(19) 3_677 ?
Cs2 Cs7 3.421(10) 1_565 ?
Cs2 Cs7 4.581(10) 3_667 ?
Cs2 O1 3.078(9) . ?
Cs2 N21 3.397(7) 2_556 ?
Cs2 N22 3.788(7) 2_556 ?
Cs2 N23 3.829(10) 2_556 ?
Cs2 N31 3.310(8) . ?
Cs2 N31 3.438(8) 3_677 ?
Cs2 C21 3.746(6) 2_556 ?
Cs2 C32 3.916(8) . ?
Cs7 Cs7 4.245(19) 3_667 ?
Cs7 O3 3.490(12) . ?
Cs7 O4 3.765(14) 3_667 ?
Cs7 O4 2.937(12) . ?
Cs7 N31 3.291(12) 1_545 ?
Cs7 N34 3.530(13) 3_667 ?
O9 C1 1.389(13) . ?
N11 C11 1.156(9) . ?
N12 C12 1.147(9) . ?
N13 C13 1.157(9) . ?
N21 C21 1.155(9) . ?
N22 C22 1.155(9) . ?
N23 C23 1.152(10) . ?
N31 C32 1.150(10) . ?
N32 C33 1.149(10) . ?
N34 C31 1.160(11) . ?
N41 C41 1.160(9) . ?
N42 C42 1.154(9) . ?
N43 C43 1.155(9) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Re2 Re1 Re3 60.282(9) . . ?
Re4 Re1 Re2 60.844(8) . . ?
Re4 Re1 Re3 60.194(8) . . ?
Se1 Re1 Re2 103.742(17) . . ?
Se1 Re1 Re3 54.888(17) . . ?
Se1 Re1 Re4 54.929(16) . . ?
Se2 Re1 Re2 55.074(16) . . ?
Se2 Re1 Re3 54.674(16) . . ?
Se2 Re1 Re4 103.600(17) . . ?
Se2 Re1 Se1 106.21(2) . . ?
Se3 Re1 Re2 54.975(16) . . ?
Se3 Re1 Re3 103.341(17) . . ?
Se3 Re1 Re4 55.310(15) . . ?
Se3 Re1 Se1 107.28(2) . . ?
Se3 Re1 Se2 107.09(2) . . ?
C11 Re1 Re2 139.29(17) . . ?
C11 Re1 Re3 140.04(17) . . ?
C11 Re1 Re4 96.51(17) . . ?
C11 Re1 Se1 85.25(17) . . ?
C11 Re1 Se2 159.89(17) . . ?
C11 Re1 Se3 84.35(17) . . ?
C11 Re1 C12 80.5(3) . . ?
C11 Re1 C13 81.0(2) . . ?
C12 Re1 Re2 139.28(19) . . ?
C12 Re1 Re3 96.29(19) . . ?
C12 Re1 Re4 138.81(18) . . ?
C12 Re1 Se1 83.94(18) . . ?
C12 Re1 Se2 84.27(19) . . ?
C12 Re1 Se3 160.37(19) . . ?
C13 Re1 Re2 94.87(17) . . ?
C13 Re1 Re3 138.32(18) . . ?
C13 Re1 Re4 139.07(17) . . ?
C13 Re1 Se1 161.38(17) . . ?
C13 Re1 Se2 83.81(18) . . ?
C13 Re1 Se3 83.89(17) . . ?
C13 Re1 C12 81.5(2) . . ?
Re1 Re2 Re3 60.064(8) . . ?
Re1 Re2 Re4 59.470(8) . . ?
Re3 Re2 Re4 59.668(8) . . ?
Se2 Re2 Re1 55.078(16) . . ?
Se2 Re2 Re3 54.588(16) . . ?
Se2 Re2 Re4 102.490(17) . . ?
Se3 Re2 Re1 55.072(16) . . ?
Se3 Re2 Re3 103.240(17) . . ?
Se3 Re2 Re4 54.777(15) . . ?
Se3 Re2 Se2 107.19(2) . . ?
Se4 Re2 Re1 102.840(18) . . ?
Se4 Re2 Re3 55.013(17) . . ?
Se4 Re2 Re4 54.543(17) . . ?
Se4 Re2 Se2 106.65(2) . . ?
Se4 Re2 Se3 105.85(2) . . ?
C21 Re2 Re1 96.49(17) . . ?
C21 Re2 Re3 137.82(17) . . ?
C21 Re2 Re4 140.84(17) . . ?
C21 Re2 Se2 83.26(17) . . ?
C21 Re2 Se3 86.33(17) . . ?
C21 Re2 Se4 160.62(17) . . ?
C21 Re2 C22 81.3(2) . . ?
C21 Re2 C23 79.8(3) . . ?
C22 Re2 Re1 140.22(18) . . ?
C22 Re2 Re3 139.72(18) . . ?
C22 Re2 Re4 97.99(17) . . ?
C22 Re2 Se2 159.50(17) . . ?
C22 Re2 Se3 85.20(18) . . ?
C22 Re2 Se4 84.73(18) . . ?
C23 Re2 Re1 139.56(19) . . ?
C23 Re2 Re3 96.1(2) . . ?
C23 Re2 Re4 139.0(2) . . ?
C23 Re2 Se2 84.59(19) . . ?
C23 Re2 Se3 160.7(2) . . ?
C23 Re2 Se4 84.6(2) . . ?
C23 Re2 C22 79.5(3) . . ?
Re1 Re3 Re2 59.654(8) . . ?
Re4 Re3 Re1 59.588(8) . . ?
Re4 Re3 Re2 60.426(8) . . ?
Se1 Re3 Re1 55.056(16) . . ?
Se1 Re3 Re2 103.361(17) . . ?
Se1 Re3 Re4 54.728(16) . . ?
Se1 Re3 Se4 106.52(2) . . ?
Se2 Re3 Re1 54.990(16) . . ?
Se2 Re3 Re2 54.898(16) . . ?
Se2 Re3 Re4 103.353(17) . . ?
Se2 Re3 Se1 106.66(2) . . ?
Se2 Re3 Se4 106.51(2) . . ?
Se4 Re3 Re1 102.151(18) . . ?
Se4 Re3 Re2 54.559(16) . . ?
Se4 Re3 Re4 54.739(17) . . ?
C31 Re3 Re1 138.2(2) . . ?
C31 Re3 Re2 94.9(2) . . ?
C31 Re3 Re4 138.9(2) . . ?
C31 Re3 Se1 161.8(2) . . ?
C31 Re3 Se2 83.5(2) . . ?
C31 Re3 Se4 84.3(2) . . ?
C31 Re3 C32 81.0(3) . . ?
C31 Re3 C33 80.1(3) . . ?
C32 Re3 Re1 98.5(2) . . ?
C32 Re3 Re2 141.0(2) . . ?
C32 Re3 Re4 139.2(2) . . ?
C32 Re3 Se1 84.5(2) . . ?
C32 Re3 Se2 86.2(2) . . ?
C32 Re3 Se4 159.4(2) . . ?
C33 Re3 Re1 141.4(2) . . ?
C33 Re3 Re2 136.9(2) . . ?
C33 Re3 Re4 96.0(2) . . ?
C33 Re3 Se1 86.7(2) . . ?
C33 Re3 Se2 160.4(2) . . ?
C33 Re3 Se4 82.4(2) . . ?
C33 Re3 C32 80.9(3) . . ?
Re1 Re4 Re2 59.687(8) . . ?
Re1 Re4 Re3 60.218(8) . . ?
Re3 Re4 Re2 59.906(8) . . ?
Se1 Re4 Re1 55.387(16) . . ?
Se1 Re4 Re2 103.162(17) . . ?
Se1 Re4 Re3 55.013(17) . . ?
Se1 Re4 Se3 107.49(2) . . ?
Se1 Re4 Se4 107.12(2) . . ?
Se3 Re4 Re1 55.076(15) . . ?
Se3 Re4 Re2 54.453(15) . . ?
Se3 Re4 Re3 103.177(17) . . ?
Se4 Re4 Re1 102.931(17) . . ?
Se4 Re4 Re2 54.432(16) . . ?
Se4 Re4 Re3 55.083(17) . . ?
Se4 Re4 Se3 105.44(2) . . ?
C41 Re4 Re1 96.66(16) . . ?
C41 Re4 Re2 140.20(17) . . ?
C41 Re4 Re3 138.79(17) . . ?
C41 Re4 Se1 83.82(17) . . ?
C41 Re4 Se3 85.91(17) . . ?
C41 Re4 Se4 160.40(17) . . ?
C41 Re4 C42 79.4(2) . . ?
C41 Re4 C43 79.7(2) . . ?
C42 Re4 Re1 139.07(17) . . ?
C42 Re4 Re2 97.83(16) . . ?
C42 Re4 Re3 140.86(17) . . ?
C42 Re4 Se1 158.99(16) . . ?
C42 Re4 Se3 84.01(17) . . ?
C42 Re4 Se4 85.82(17) . . ?
C42 Re4 C43 80.4(2) . . ?
C43 Re4 Re1 139.53(17) . . ?
C43 Re4 Re2 139.52(17) . . ?
C43 Re4 Re3 96.41(17) . . ?
C43 Re4 Se1 84.22(17) . . ?
C43 Re4 Se3 160.41(17) . . ?
C43 Re4 Se4 85.22(17) . . ?
W2 W1 W3 60.282(9) . . ?
W4 W1 W2 60.844(8) . . ?
W4 W1 W3 60.194(8) . . ?
Se1 W1 W2 103.742(17) . . ?
Se1 W1 W3 54.888(17) . . ?
Se1 W1 W4 54.929(16) . . ?
Se2 W1 W2 55.074(16) . . ?
Se2 W1 W3 54.674(16) . . ?
Se2 W1 W4 103.600(17) . . ?
Se2 W1 Se1 106.21(2) . . ?
Se3 W1 W2 54.975(16) . . ?
Se3 W1 W3 103.341(17) . . ?
Se3 W1 W4 55.310(15) . . ?
Se3 W1 Se1 107.28(2) . . ?
Se3 W1 Se2 107.09(2) . . ?
C11 W1 W2 139.29(17) . . ?
C11 W1 W3 140.04(17) . . ?
C11 W1 W4 96.51(17) . . ?
C11 W1 Se1 85.25(17) . . ?
C11 W1 Se2 159.89(17) . . ?
C11 W1 Se3 84.35(17) . . ?
C11 W1 C12 80.5(3) . . ?
C11 W1 C13 81.0(2) . . ?
C12 W1 W2 139.28(19) . . ?
C12 W1 W3 96.29(19) . . ?
C12 W1 W4 138.81(18) . . ?
C12 W1 Se1 83.94(18) . . ?
C12 W1 Se2 84.27(19) . . ?
C12 W1 Se3 160.37(19) . . ?
C13 W1 W2 94.87(17) . . ?
C13 W1 W3 138.32(18) . . ?
C13 W1 W4 139.07(17) . . ?
C13 W1 Se1 161.38(17) . . ?
C13 W1 Se2 83.81(18) . . ?
C13 W1 Se3 83.89(17) . . ?
C13 W1 C12 81.5(2) . . ?
W1 W2 W3 60.064(8) . . ?
W1 W2 W4 59.470(8) . . ?
W3 W2 W4 59.668(8) . . ?
Se2 W2 W1 55.078(16) . . ?
Se2 W2 W3 54.588(16) . . ?
Se2 W2 W4 102.490(17) . . ?
Se3 W2 W1 55.072(16) . . ?
Se3 W2 W3 103.240(17) . . ?
Se3 W2 W4 54.777(15) . . ?
Se3 W2 Se2 107.19(2) . . ?
Se4 W2 W1 102.840(18) . . ?
Se4 W2 W3 55.013(17) . . ?
Se4 W2 W4 54.543(17) . . ?
Se4 W2 Se2 106.65(2) . . ?
Se4 W2 Se3 105.85(2) . . ?
C21 W2 W1 96.49(17) . . ?
C21 W2 W3 137.82(17) . . ?
C21 W2 W4 140.84(17) . . ?
C21 W2 Se2 83.26(17) . . ?
C21 W2 Se3 86.33(17) . . ?
C21 W2 Se4 160.62(17) . . ?
C21 W2 C22 81.3(2) . . ?
C21 W2 C23 79.8(3) . . ?
C22 W2 W1 140.22(18) . . ?
C22 W2 W3 139.72(18) . . ?
C22 W2 W4 97.99(17) . . ?
C22 W2 Se2 159.50(17) . . ?
C22 W2 Se3 85.20(18) . . ?
C22 W2 Se4 84.73(18) . . ?
C23 W2 W1 139.56(19) . . ?
C23 W2 W3 96.1(2) . . ?
C23 W2 W4 139.0(2) . . ?
C23 W2 Se2 84.59(19) . . ?
C23 W2 Se3 160.7(2) . . ?
C23 W2 Se4 84.6(2) . . ?
C23 W2 C22 79.5(3) . . ?
W1 W3 W2 59.654(8) . . ?
W4 W3 W1 59.588(8) . . ?
W4 W3 W2 60.426(8) . . ?
Se1 W3 W1 55.056(16) . . ?
Se1 W3 W2 103.361(17) . . ?
Se1 W3 W4 54.728(16) . . ?
Se1 W3 Se4 106.52(2) . . ?
Se2 W3 W1 54.990(16) . . ?
Se2 W3 W2 54.898(16) . . ?
Se2 W3 W4 103.353(17) . . ?
Se2 W3 Se1 106.66(2) . . ?
Se2 W3 Se4 106.51(2) . . ?
Se4 W3 W1 102.151(18) . . ?
Se4 W3 W2 54.559(16) . . ?
Se4 W3 W4 54.739(17) . . ?
C31 W3 W1 138.2(2) . . ?
C31 W3 W2 94.9(2) . . ?
C31 W3 W4 138.9(2) . . ?
C31 W3 Se1 161.8(2) . . ?
C31 W3 Se2 83.5(2) . . ?
C31 W3 Se4 84.3(2) . . ?
C31 W3 C32 81.0(3) . . ?
C31 W3 C33 80.1(3) . . ?
C32 W3 W1 98.5(2) . . ?
C32 W3 W2 141.0(2) . . ?
C32 W3 W4 139.2(2) . . ?
C32 W3 Se1 84.5(2) . . ?
C32 W3 Se2 86.2(2) . . ?
C32 W3 Se4 159.4(2) . . ?
C33 W3 W1 141.4(2) . . ?
C33 W3 W2 136.9(2) . . ?
C33 W3 W4 96.0(2) . . ?
C33 W3 Se1 86.7(2) . . ?
C33 W3 Se2 160.4(2) . . ?
C33 W3 Se4 82.4(2) . . ?
C33 W3 C32 80.9(3) . . ?
W1 W4 W2 59.687(8) . . ?
W1 W4 W3 60.218(8) . . ?
W3 W4 W2 59.906(8) . . ?
Se1 W4 W1 55.387(16) . . ?
Se1 W4 W2 103.162(17) . . ?
Se1 W4 W3 55.013(17) . . ?
Se1 W4 Se3 107.49(2) . . ?
Se1 W4 Se4 107.12(2) . . ?
Se3 W4 W1 55.076(15) . . ?
Se3 W4 W2 54.453(15) . . ?
Se3 W4 W3 103.177(17) . . ?
Se4 W4 W1 102.931(17) . . ?
Se4 W4 W2 54.432(16) . . ?
Se4 W4 W3 55.083(17) . . ?
Se4 W4 Se3 105.44(2) . . ?
C41 W4 W1 96.66(16) . . ?
C41 W4 W2 140.20(17) . . ?
C41 W4 W3 138.79(17) . . ?
C41 W4 Se1 83.82(17) . . ?
C41 W4 Se3 85.91(17) . . ?
C41 W4 Se4 160.40(17) . . ?
C41 W4 C42 79.4(2) . . ?
C41 W4 C43 79.7(2) . . ?
C42 W4 W1 139.07(17) . . ?
C42 W4 W2 97.83(16) . . ?
C42 W4 W3 140.86(17) . . ?
C42 W4 Se1 158.99(16) . . ?
C42 W4 Se3 84.01(17) . . ?
C42 W4 Se4 85.82(17) . . ?
C42 W4 C43 80.4(2) . . ?
C43 W4 W1 139.53(17) . . ?
C43 W4 W2 139.52(17) . . ?
C43 W4 W3 96.41(17) . . ?
C43 W4 Se1 84.22(17) . . ?
C43 W4 Se3 160.41(17) . . ?
C43 W4 Se4 85.22(17) . . ?
Se3 Cs1 Cs9 78.64(4) . 4_575 ?
O9 Cs1 Cs9 50.21(14) . 4_575 ?
O9 Cs1 Se3 76.19(14) . . ?
O9 Cs1 O5 146.0(3) . 4_575 ?
O9 Cs1 N11 63.01(17) . 3_676 ?
O9 Cs1 N13 138.41(17) . . ?
O9 Cs1 N21 93.11(17) . . ?
O9 Cs1 N32 81.1(2) . 4_575 ?
O9 Cs1 N41 127.18(18) . 3_676 ?
O9 Cs1 N43 75.66(18) . 4_575 ?
O9 Cs1 C13 121.83(17) . . ?
O9 Cs1 C21 87.13(17) . . ?
O5 Cs1 Cs9 127.7(2) 4_575 4_575 ?
O5 Cs1 Se3 137.4(2) 4_575 . ?
O5 Cs1 C13 92.1(2) 4_575 . ?
O5 Cs1 C21 118.0(3) 4_575 . ?
N11 Cs1 Cs9 110.43(12) 3_676 4_575 ?
N11 Cs1 Se3 68.33(11) 3_676 . ?
N11 Cs1 O5 117.6(3) 3_676 4_575 ?
N11 Cs1 N13 106.17(15) 3_676 . ?
N11 Cs1 N21 132.03(15) 3_676 . ?
N11 Cs1 N43 82.70(16) 3_676 4_575 ?
N11 Cs1 C13 96.75(15) 3_676 . ?
N11 Cs1 C21 114.86(15) 3_676 . ?
N13 Cs1 Cs9 110.27(11) . 4_575 ?
N13 Cs1 Se3 63.08(10) . . ?
N13 Cs1 O5 75.5(2) . 4_575 ?
N13 Cs1 C13 16.77(13) . . ?
N13 Cs1 C21 59.98(14) . . ?
N21 Cs1 Cs9 47.65(12) . 4_575 ?
N21 Cs1 Se3 65.66(10) . . ?
N21 Cs1 O5 105.2(3) . 4_575 ?
N21 Cs1 N13 63.56(15) . . ?
N21 Cs1 C13 59.57(14) . . ?
N21 Cs1 C21 17.62(14) . . ?
N32 Cs1 Cs9 46.44(17) 4_575 4_575 ?
N32 Cs1 Se3 121.41(15) 4_575 . ?
N32 Cs1 O5 82.4(3) 4_575 4_575 ?
N32 Cs1 N11 140.14(19) 4_575 3_676 ?
N32 Cs1 N13 112.39(17) 4_575 . ?
N32 Cs1 N21 62.50(17) 4_575 . ?
N32 Cs1 N41 124.9(2) 4_575 3_676 ?
N32 Cs1 N43 71.44(18) 4_575 4_575 ?
N32 Cs1 C13 117.75(17) 4_575 . ?
N32 Cs1 C21 77.83(17) 4_575 . ?
N41 Cs1 Cs9 169.11(12) 3_676 4_575 ?
N41 Cs1 Se3 111.68(11) 3_676 . ?
N41 Cs1 O5 46.7(2) 3_676 4_575 ?
N41 Cs1 N11 71.88(15) 3_676 3_676 ?
N41 Cs1 N13 78.50(15) 3_676 . ?
N41 Cs1 N21 138.83(16) 3_676 . ?
N41 Cs1 N43 72.67(16) 3_676 4_575 ?
N41 Cs1 C13 88.25(15) 3_676 . ?
N41 Cs1 C21 138.37(15) 3_676 . ?
N43 Cs1 Cs9 96.85(12) 4_575 4_575 ?
N43 Cs1 Se3 146.40(12) 4_575 . ?
N43 Cs1 O5 71.0(2) 4_575 4_575 ?
N43 Cs1 N13 145.46(15) 4_575 . ?
N43 Cs1 N21 133.77(16) 4_575 . ?
N43 Cs1 C13 160.16(15) 4_575 . ?
N43 Cs1 C21 146.59(15) 4_575 . ?
C13 Cs1 Cs9 101.86(11) . 4_575 ?
C13 Cs1 Se3 46.33(9) . . ?
C21 Cs1 Cs9 51.18(11) . 4_575 ?
C21 Cs1 Se3 48.07(10) . . ?
C21 Cs1 C13 50.82(14) . . ?
Se3 Cs3 C42 107.72(9) . 3_666 ?
N11 Cs3 Se3 71.54(11) 3_676 . ?
N11 Cs3 N41 117.07(16) 3_676 . ?
N11 Cs3 N42 127.91(15) 3_676 . ?
N11 Cs3 C11 18.43(15) 3_676 3_676 ?
N11 Cs3 C13 64.15(15) 3_676 3_676 ?
N11 Cs3 C41 112.17(15) 3_676 . ?
N11 Cs3 C42 118.69(15) 3_676 . ?
N11 Cs3 C42 81.00(15) 3_676 3_666 ?
N13 Cs3 Se3 124.49(11) 3_676 . ?
N13 Cs3 N11 82.71(15) 3_676 3_676 ?
N13 Cs3 N41 81.37(15) 3_676 . ?
N13 Cs3 N42 147.25(15) 3_676 . ?
N13 Cs3 C11 64.48(14) 3_676 3_676 ?
N13 Cs3 C13 18.78(15) 3_676 3_676 ?
N13 Cs3 C41 99.40(15) 3_676 . ?
N13 Cs3 C42 115.80(15) 3_676 3_666 ?
N13 Cs3 C42 142.73(15) 3_676 . ?
N22 Cs3 Se3 162.91(13) 3_666 . ?
N22 Cs3 N11 121.57(17) 3_666 3_676 ?
N22 Cs3 N13 70.73(16) 3_666 3_676 ?
N22 Cs3 N41 109.22(16) 3_666 . ?
N22 Cs3 N42 96.75(16) 3_666 . ?
N22 Cs3 C11 109.72(16) 3_666 3_676 ?
N22 Cs3 C13 80.38(16) 3_666 3_676 ?
N22 Cs3 C41 122.70(16) 3_666 . ?
N22 Cs3 C42 66.87(15) 3_666 3_666 ?
N22 Cs3 C42 113.47(16) 3_666 . ?
N41 Cs3 Se3 69.17(11) . . ?
N41 Cs3 N42 74.34(15) . . ?
N41 Cs3 C11 113.92(15) . 3_676 ?
N41 Cs3 C13 92.96(15) . 3_676 ?
N41 Cs3 C41 19.53(15) . . ?
N41 Cs3 C42 157.56(14) . 3_666 ?
N41 Cs3 C42 61.98(15) . . ?
N42 Cs3 Se3 94.66(12) 3_666 . ?
N42 Cs3 Se3 66.25(10) . . ?
N42 Cs3 N11 71.26(16) 3_666 3_676 ?
N42 Cs3 N13 122.62(17) 3_666 3_676 ?
N42 Cs3 N22 80.87(16) 3_666 3_666 ?
N42 Cs3 N41 155.99(16) 3_666 . ?
N42 Cs3 N42 83.00(17) 3_666 . ?
N42 Cs3 C11 146.26(14) . 3_676 ?
N42 Cs3 C11 81.04(15) 3_666 3_676 ?
N42 Cs3 C13 165.38(15) . 3_676 ?
N42 Cs3 C13 110.46(16) 3_666 3_676 ?
N42 Cs3 C41 137.54(17) 3_666 . ?
N42 Cs3 C41 61.18(14) . . ?
N42 Cs3 C42 94.08(16) 3_666 . ?
N42 Cs3 C42 18.71(14) . . ?
N42 Cs3 C42 14.05(15) 3_666 3_666 ?
N42 Cs3 C42 84.04(14) . 3_666 ?
C11 Cs3 Se3 85.63(10) 3_676 . ?
C11 Cs3 C42 87.45(14) 3_676 3_666 ?
C13 Cs3 Se3 116.50(10) 3_676 . ?
C13 Cs3 C11 45.81(14) 3_676 3_676 ?
C13 Cs3 C42 153.85(15) 3_676 . ?
C13 Cs3 C42 107.59(14) 3_676 3_666 ?
C41 Cs3 Se3 51.83(11) . . ?
C41 Cs3 C11 115.85(15) . 3_676 ?
C41 Cs3 C13 108.25(15) . 3_676 ?
C41 Cs3 C42 144.02(14) . 3_666 ?
C41 Cs3 C42 45.66(15) . . ?
C42 Cs3 Se3 50.09(10) . . ?
C42 Cs3 C11 135.12(14) . 3_676 ?
C42 Cs3 C42 98.40(13) . 3_666 ?
O3 Cs4 N12 76.07(17) . 1_545 ?
O3 Cs4 N13 153.01(15) . 1_545 ?
O3 Cs4 N22 117.58(16) . . ?
O3 Cs4 N23 59.3(2) . . ?
O3 Cs4 N23 71.5(2) . 2_546 ?
O3 Cs4 N34 116.74(17) . 2_546 ?
O3 Cs4 C12 90.44(16) . 1_545 ?
O3 Cs4 C13 135.59(15) . 1_545 ?
O3 Cs4 C22 99.96(16) . . ?
O3 Cs4 C23 64.86(17) . . ?
O3 Cs4 C23 65.65(16) . 2_546 ?
N12 Cs4 N13 77.31(15) 1_545 1_545 ?
N12 Cs4 N22 84.63(17) 1_545 . ?
N12 Cs4 N23 109.79(19) 1_545 . ?
N12 Cs4 N34 155.69(18) 1_545 2_546 ?
N12 Cs4 C12 18.76(16) 1_545 1_545 ?
N12 Cs4 C13 62.51(15) 1_545 1_545 ?
N12 Cs4 C22 81.46(16) 1_545 . ?
N12 Cs4 C23 113.54(18) 1_545 2_546 ?
N12 Cs4 C23 96.48(17) 1_545 . ?
N13 Cs4 C12 62.60(15) 1_545 1_545 ?
N13 Cs4 C13 18.60(14) 1_545 1_545 ?
N13 Cs4 C22 80.30(14) 1_545 . ?
N13 Cs4 C23 122.69(15) 1_545 2_546 ?
N13 Cs4 C23 122.99(15) 1_545 . ?
N22 Cs4 N13 63.79(14) . 1_545 ?
N22 Cs4 N34 104.82(18) . 2_546 ?
N22 Cs4 C12 88.37(16) . 1_545 ?
N22 Cs4 C13 75.43(15) . 1_545 ?
N22 Cs4 C22 17.76(15) . . ?
N22 Cs4 C23 59.20(15) . . ?
N22 Cs4 C23 161.28(17) . 2_546 ?
N23 Cs4 N12 101.5(2) 2_546 1_545 ?
N23 Cs4 N13 136.24(18) . 1_545 ?
N23 Cs4 N13 109.96(17) 2_546 1_545 ?
N23 Cs4 N22 73.75(17) . . ?
N23 Cs4 N22 170.3(2) 2_546 . ?
N23 Cs4 N23 110.54(8) 2_546 . ?
N23 Cs4 N34 94.4(2) . 2_546 ?
N23 Cs4 N34 66.7(2) 2_546 2_546 ?
N23 Cs4 C12 95.12(19) 2_546 1_545 ?
N23 Cs4 C12 128.30(19) . 1_545 ?
N23 Cs4 C13 100.60(17) 2_546 1_545 ?
N23 Cs4 C13 148.85(17) . 1_545 ?
N23 Cs4 C22 59.33(16) . . ?
N23 Cs4 C22 169.68(17) 2_546 . ?
N23 Cs4 C23 17.99(16) . . ?
N23 Cs4 C23 94.83(16) . 2_546 ?
N23 Cs4 C23 126.59(17) 2_546 . ?
N23 Cs4 C23 16.76(17) 2_546 2_546 ?
N34 Cs4 N13 86.77(16) 2_546 1_545 ?
N34 Cs4 C12 137.25(18) 2_546 1_545 ?
N34 Cs4 C13 97.69(16) 2_546 1_545 ?
N34 Cs4 C22 114.12(18) 2_546 . ?
N34 Cs4 C23 60.50(19) 2_546 2_546 ?
N34 Cs4 C23 107.63(19) 2_546 . ?
C12 Cs4 C13 45.84(15) 1_545 1_545 ?
C12 Cs4 C22 90.62(15) 1_545 . ?
C12 Cs4 C23 113.89(16) 1_545 . ?
C12 Cs4 C23 110.28(17) 1_545 2_546 ?
C13 Cs4 C22 89.55(15) 1_545 . ?
C13 Cs4 C23 116.11(15) 1_545 2_546 ?
C13 Cs4 C23 132.04(15) 1_545 . ?
C22 Cs4 C23 153.92(15) . 2_546 ?
C23 Cs4 C22 43.09(15) . . ?
C23 Cs4 C23 111.79(11) . 2_546 ?
O9 Cs5 N11 58.76(17) 3_666 1_545 ?
O9 Cs5 N12 121.09(17) 3_666 1_545 ?
O9 Cs5 N41 118.39(16) 3_666 2_646 ?
O9 Cs5 N42 48.80(15) 3_666 . ?
O9 Cs5 N43 71.81(16) 3_666 2_646 ?
O9 Cs5 N43 91.53(18) 3_666 . ?
O9 Cs5 C11 77.34(17) 3_666 1_545 ?
O9 Cs5 C12 114.92(17) 3_666 1_545 ?
O9 Cs5 C43 75.23(15) 3_666 2_646 ?
O5 Cs5 O9 166.0(3) . 3_666 ?
O5 Cs5 N11 134.8(3) . 1_545 ?
O5 Cs5 N12 71.0(3) . 1_545 ?
O5 Cs5 N41 48.6(2) . 2_646 ?
O5 Cs5 N42 135.2(3) . . ?
O5 Cs5 N43 105.1(3) . 2_646 ?
O5 Cs5 N43 78.8(3) . . ?
O5 Cs5 C11 116.3(3) . 1_545 ?
O5 Cs5 C12 78.8(3) . 1_545 ?
O5 Cs5 C43 97.7(3) . 2_646 ?
O6 Cs5 N42 134.3(5) . . ?
O6 Cs5 N43 90.4(6) . . ?
O6 Cs5 C43 101.8(5) . 2_646 ?
N11 Cs5 N12 75.15(15) 1_545 1_545 ?
N11 Cs5 N41 151.85(14) 1_545 2_646 ?
N11 Cs5 N42 62.91(14) 1_545 . ?
N11 Cs5 C11 18.58(15) 1_545 1_545 ?
N11 Cs5 C12 61.02(15) 1_545 1_545 ?
N11 Cs5 C43 95.77(14) 1_545 2_646 ?
N12 Cs5 N41 119.44(16) 1_545 2_646 ?
N12 Cs5 N42 79.39(16) 1_545 . ?
N12 Cs5 C11 60.76(15) 1_545 1_545 ?
N12 Cs5 C12 18.13(15) 1_545 1_545 ?
N12 Cs5 C43 148.57(15) 1_545 2_646 ?
N41 Cs5 N42 139.56(14) 2_646 . ?
N41 Cs5 C11 146.29(14) 2_646 1_545 ?
N41 Cs5 C12 126.21(15) 2_646 1_545 ?
N41 Cs5 C43 58.79(14) 2_646 2_646 ?
N42 Cs5 C12 83.39(15) . 1_545 ?
N42 Cs5 C43 123.74(14) . 2_646 ?
N43 Cs5 N11 136.75(15) . 1_545 ?
N43 Cs5 N11 79.08(15) 2_646 1_545 ?
N43 Cs5 N12 135.17(16) 2_646 1_545 ?
N43 Cs5 N12 99.82(16) . 1_545 ?
N43 Cs5 N41 67.97(15) . 2_646 ?
N43 Cs5 N41 74.03(15) 2_646 2_646 ?
N43 Cs5 N42 119.55(15) 2_646 . ?
N43 Cs5 N42 73.90(14) . . ?
N43 Cs5 N43 123.78(9) . 2_646 ?
N43 Cs5 C11 84.60(15) 2_646 1_545 ?
N43 Cs5 C11 144.88(15) . 1_545 ?
N43 Cs5 C12 117.91(15) 2_646 1_545 ?
N43 Cs5 C12 117.79(16) . 1_545 ?
N43 Cs5 C43 106.75(15) . 2_646 ?
N43 Cs5 C43 17.86(15) 2_646 2_646 ?
C11 Cs5 N42 73.81(14) 1_545 . ?
C11 Cs5 C12 44.58(15) 1_545 1_545 ?
C11 Cs5 C43 102.43(14) 1_545 2_646 ?
C12 Cs5 C43 133.32(15) 1_545 2_646 ?
Cs1 Cs6 Cs4 137.18(10) 4_676 . ?
Cs5 Cs6 Cs1 63.02(5) . 4_676 ?
Cs5 Cs6 Cs4 83.43(7) . . ?
Se4 Cs6 Cs1 83.18(8) . 4_676 ?
Se4 Cs6 Cs4 57.80(7) . . ?
Se4 Cs6 Cs5 65.29(6) . . ?
Se4 Cs6 C33 46.85(13) . . ?
O3 Cs6 Cs1 146.42(18) . 4_676 ?
O3 Cs6 Cs4 36.89(13) . . ?
O3 Cs6 Cs5 118.86(17) . . ?
O3 Cs6 Se4 69.99(15) . . ?
O3 Cs6 N31 94.0(2) . 1_545 ?
O3 Cs6 N32 109.2(2) . . ?
O3 Cs6 C33 94.79(19) . . ?
O4 Cs6 Cs1 51.60(16) . 4_676 ?
O4 Cs6 Cs4 168.1(2) . . ?
O4 Cs6 Cs5 108.32(19) . . ?
O4 Cs6 Se4 124.7(2) . . ?
O4 Cs6 O3 131.3(2) . . ?
O4 Cs6 N12 150.7(3) . 1_545 ?
O4 Cs6 N31 101.0(2) . 1_545 ?
O4 Cs6 N32 62.1(2) . . ?
O4 Cs6 C33 78.3(2) . . ?
O5 Cs6 Cs1 47.8(3) . 4_676 ?
O5 Cs6 Cs4 116.8(3) . . ?
O5 Cs6 Cs5 37.9(3) . . ?
O5 Cs6 Se4 98.9(3) . . ?
O5 Cs6 O3 153.6(4) . . ?
O5 Cs6 O4 75.0(3) . . ?
O5 Cs6 N12 75.8(3) . 1_545 ?
O5 Cs6 N31 75.1(3) . 1_545 ?
O5 Cs6 N32 84.6(3) . . ?
O5 Cs6 C33 94.0(3) . . ?
O8 Cs6 Cs1 120.0(3) . 4_676 ?
O8 Cs6 Cs4 101.9(2) . . ?
O8 Cs6 Cs5 154.2(3) . . ?
O8 Cs6 Se4 138.6(3) . . ?
O8 Cs6 O3 73.9(2) . . ?
O8 Cs6 O4 68.5(3) . . ?
O8 Cs6 O5 122.2(4) . . ?
O8 Cs6 N12 129.8(3) . 1_545 ?
O8 Cs6 N31 70.1(3) . 1_545 ?
O8 Cs6 N32 113.4(3) . . ?
O8 Cs6 C33 119.2(3) . . ?
N12 Cs6 Cs1 106.36(16) 1_545 4_676 ?
N12 Cs6 Cs4 41.07(14) 1_545 . ?
N12 Cs6 Cs5 44.30(14) 1_545 . ?
N12 Cs6 Se4 60.27(15) 1_545 . ?
N12 Cs6 O3 78.0(2) 1_545 . ?
N12 Cs6 N31 71.5(2) 1_545 1_545 ?
N12 Cs6 N32 114.7(2) 1_545 . ?
N12 Cs6 C33 103.6(2) 1_545 . ?
N31 Cs6 Cs1 119.19(17) 1_545 4_676 ?
N31 Cs6 Cs4 81.39(16) 1_545 . ?
N31 Cs6 Cs5 86.05(16) 1_545 . ?
N31 Cs6 Se4 131.14(19) 1_545 . ?
N31 Cs6 N32 156.7(2) 1_545 . ?
N31 Cs6 C33 168.8(2) 1_545 . ?
N32 Cs6 Cs1 38.09(12) . 4_676 ?
N32 Cs6 Cs4 118.61(16) . . ?
N32 Cs6 Cs5 84.72(14) . . ?
N32 Cs6 Se4 62.55(14) . . ?
N32 Cs6 C33 17.02(16) . . ?
C33 Cs6 Cs1 51.64(12) . 4_676 ?
C33 Cs6 Cs4 101.67(15) . . ?
C33 Cs6 Cs5 83.60(13) . . ?
O1 Cs9 O9 108.6(3) 3_677 4_676 ?
O1 Cs9 O2 58.6(5) 3_677 . ?
O1 Cs9 N21 138.9(3) 3_677 4_676 ?
O1 Cs9 N22 64.3(2) 3_677 4_676 ?
O1 Cs9 N31 86.5(3) 3_677 . ?
O1 Cs9 N32 162.3(3) 3_677 . ?
O1 Cs9 C1 93.3(4) 3_677 4_676 ?
O1 Cs9 C21 122.9(2) 3_677 4_676 ?
O1 Cs9 C22 81.3(2) 3_677 4_676 ?
O1 Cs9 C32 101.6(3) 3_677 . ?
O1 Cs9 C33 144.3(3) 3_677 . ?
O9 Cs9 C21 79.63(17) 4_676 4_676 ?
O9 Cs9 C33 73.27(18) 4_676 . ?
O2 Cs9 O9 162.3(5) . 4_676 ?
O2 Cs9 N21 115.2(5) . 4_676 ?
O2 Cs9 N22 105.0(4) . 4_676 ?
O2 Cs9 N31 54.3(4) . . ?
O2 Cs9 N32 118.6(5) . . ?
O2 Cs9 C21 117.2(4) . 4_676 ?
O2 Cs9 C22 111.2(4) . 4_676 ?
O2 Cs9 C32 72.2(4) . . ?
O2 Cs9 C33 109.3(4) . . ?
N21 Cs9 O9 82.45(18) 4_676 4_676 ?
N21 Cs9 C21 17.87(14) 4_676 4_676 ?
N21 Cs9 C22 62.69(16) 4_676 4_676 ?
N21 Cs9 C32 115.3(2) 4_676 . ?
N21 Cs9 C33 76.57(18) 4_676 . ?
N22 Cs9 O9 76.79(19) 4_676 4_676 ?
N22 Cs9 N21 81.12(18) 4_676 4_676 ?
N22 Cs9 N31 150.7(2) 4_676 . ?
N22 Cs9 N32 129.6(2) 4_676 . ?
N22 Cs9 C21 63.26(17) 4_676 4_676 ?
N22 Cs9 C22 18.44(16) 4_676 4_676 ?
N22 Cs9 C32 163.2(2) 4_676 . ?
N22 Cs9 C33 144.5(2) 4_676 . ?
N31 Cs9 O9 116.5(2) . 4_676 ?
N31 Cs9 N21 124.8(2) . 4_676 ?
N31 Cs9 N32 79.3(2) . . ?
N31 Cs9 C21 141.7(2) . 4_676 ?
N31 Cs9 C22 164.9(2) . 4_676 ?
N31 Cs9 C32 18.63(18) . . ?
N31 Cs9 C33 62.89(19) . . ?
N32 Cs9 O9 69.33(18) . 4_676 ?
N32 Cs9 N21 58.74(17) . 4_676 ?
N32 Cs9 C21 74.53(18) . 4_676 ?
N32 Cs9 C22 114.2(2) . 4_676 ?
N32 Cs9 C32 62.61(18) . . ?
N32 Cs9 C33 18.24(17) . . ?
C1 Cs9 O9 19.4(3) 4_676 4_676 ?
C1 Cs9 O2 142.9(5) 4_676 . ?
C1 Cs9 N21 101.8(3) 4_676 4_676 ?
C1 Cs9 N22 79.4(3) 4_676 4_676 ?
C1 Cs9 N31 104.9(3) 4_676 . ?
C1 Cs9 N32 80.4(3) 4_676 . ?
C1 Cs9 C21 97.9(3) 4_676 4_676 ?
C1 Cs9 C22 84.7(3) 4_676 4_676 ?
C1 Cs9 C32 93.0(3) 4_676 . ?
C1 Cs9 C33 78.6(3) 4_676 . ?
C22 Cs9 O9 76.14(18) 4_676 4_676 ?
C22 Cs9 C21 44.82(15) 4_676 4_676 ?
C22 Cs9 C32 176.5(2) 4_676 . ?
C22 Cs9 C33 131.5(2) 4_676 . ?
C32 Cs9 O9 100.9(2) . 4_676 ?
C32 Cs9 C21 133.1(2) . 4_676 ?
C32 Cs9 C33 45.22(18) . . ?
C33 Cs9 C21 92.72(18) . 4_676 ?
Cs1 Cs8 Cs4 116.7(2) 4_676 4_676 ?
Cs1 Cs8 Cs10 97.6(2) 4_676 3_667 ?
Cs4 Cs8 Cs10 104.2(2) 4_676 3_667 ?
O1 Cs8 Cs1 116.5(4) 3_677 4_676 ?
O1 Cs8 Cs4 47.8(2) 3_677 4_676 ?
O1 Cs8 Cs10 142.5(4) 3_677 3_667 ?
O1 Cs8 N21 129.4(4) 3_677 4_676 ?
O1 Cs8 N22 51.4(2) 3_677 4_676 ?
O1 Cs8 N31 78.7(3) 3_677 . ?
O1 Cs8 N32 134.2(5) 3_677 . ?
O1 Cs8 C1 66.7(3) 3_677 4_676 ?
O1 Cs8 C21 111.5(4) 3_677 4_676 ?
O1 Cs8 C32 91.5(3) 3_677 . ?
O1 Cs8 C33 123.6(4) 3_677 . ?
N21 Cs8 Cs1 43.2(2) 4_676 4_676 ?
N21 Cs8 Cs4 94.8(3) 4_676 4_676 ?
N21 Cs8 Cs10 66.8(3) 4_676 3_667 ?
N21 Cs8 N22 78.0(3) 4_676 4_676 ?
N21 Cs8 N31 147.9(4) 4_676 . ?
N21 Cs8 N32 65.1(3) 4_676 . ?
N21 Cs8 C1 90.9(4) 4_676 4_676 ?
N21 Cs8 C21 18.38(16) 4_676 4_676 ?
N21 Cs8 C32 130.0(4) 4_676 . ?
N21 Cs8 C33 83.9(3) 4_676 . ?
N22 Cs8 Cs1 79.7(2) 4_676 4_676 ?
N22 Cs8 Cs4 40.51(15) 4_676 4_676 ?
N22 Cs8 Cs10 127.7(3) 4_676 3_667 ?
N22 Cs8 C1 60.4(3) 4_676 4_676 ?
N31 Cs8 Cs1 115.3(3) . 4_676 ?
N31 Cs8 Cs4 117.2(3) . 4_676 ?
N31 Cs8 Cs10 101.3(3) . 3_667 ?
N31 Cs8 N22 127.4(4) . 4_676 ?
N31 Cs8 N32 84.3(3) . . ?
N31 Cs8 C1 87.4(4) . 4_676 ?
N31 Cs8 C21 164.2(4) . 4_676 ?
N31 Cs8 C32 18.9(2) . . ?
N31 Cs8 C33 65.6(3) . . ?
N32 Cs8 Cs1 38.27(18) . 4_676 ?
N32 Cs8 Cs4 154.9(3) . 4_676 ?
N32 Cs8 Cs10 82.3(3) . 3_667 ?
N32 Cs8 N22 116.8(4) . 4_676 ?
N32 Cs8 C1 70.4(3) . 4_676 ?
N32 Cs8 C21 80.0(3) . 4_676 ?
N32 Cs8 C32 65.4(3) . . ?
N32 Cs8 C33 18.84(19) . . ?
C1 Cs8 Cs1 53.7(2) 4_676 4_676 ?
C1 Cs8 Cs4 96.5(3) 4_676 4_676 ?
C1 Cs8 Cs10 150.4(4) 4_676 3_667 ?
C21 Cs8 Cs1 49.76(17) 4_676 4_676 ?
C21 Cs8 Cs4 77.8(2) 4_676 4_676 ?
C21 Cs8 Cs10 78.3(3) 4_676 3_667 ?
C21 Cs8 N22 60.2(2) 4_676 4_676 ?
C21 Cs8 C1 85.8(3) 4_676 4_676 ?
C32 Cs8 Cs1 97.1(3) . 4_676 ?
C32 Cs8 Cs4 134.8(3) . 4_676 ?
C32 Cs8 Cs10 99.6(3) . 3_667 ?
C32 Cs8 N22 132.7(4) . 4_676 ?
C32 Cs8 C1 79.6(3) . 4_676 ?
C32 Cs8 C21 145.2(4) . 4_676 ?
C32 Cs8 C33 46.7(2) . . ?
C33 Cs8 Cs1 53.7(2) . 4_676 ?
C33 Cs8 Cs4 165.7(4) . 4_676 ?
C33 Cs8 Cs10 88.4(3) . 3_667 ?
C33 Cs8 N22 125.8(4) . 4_676 ?
C33 Cs8 C1 69.4(3) . 4_676 ?
C33 Cs8 C21 98.7(3) . 4_676 ?
Cs1 Cs10 Cs5 61.38(11) 4_676 . ?
Cs1 Cs10 Cs8 139.1(2) 4_676 3_667 ?
Cs4 Cs10 Cs1 137.18(17) . 4_676 ?
Cs4 Cs10 Cs5 82.18(13) . . ?
Cs4 Cs10 Cs8 81.54(16) . 3_667 ?
Cs5 Cs10 Cs8 131.1(3) . 3_667 ?
Se4 Cs10 Cs1 83.77(14) . 4_676 ?
Se4 Cs10 Cs4 59.03(11) . . ?
Se4 Cs10 Cs5 63.98(13) . . ?
Se4 Cs10 Cs8 137.0(2) . 3_667 ?
Se4 Cs10 N31 127.9(3) . 1_545 ?
Se4 Cs10 C33 49.13(17) . . ?
O3 Cs10 Cs1 153.5(4) . 4_676 ?
O3 Cs10 Cs4 36.74(15) . . ?
O3 Cs10 Cs5 118.3(2) . . ?
O3 Cs10 Cs8 63.6(2) . 3_667 ?
O3 Cs10 Se4 74.0(2) . . ?
O3 Cs10 O4 138.0(4) . . ?
O3 Cs10 O6 137.4(8) . . ?
O3 Cs10 N12 78.8(2) . 1_545 ?
O3 Cs10 N31 92.5(3) . 1_545 ?
O3 Cs10 N32 117.9(4) . . ?
O3 Cs10 C33 102.2(4) . . ?
O4 Cs10 Cs1 50.76(18) . 4_676 ?
O4 Cs10 Cs4 171.9(3) . . ?
O4 Cs10 Cs5 103.7(3) . . ?
O4 Cs10 Cs8 90.4(2) . 3_667 ?
O4 Cs10 Se4 128.5(3) . . ?
O4 Cs10 O6 78.7(5) . . ?
O4 Cs10 N12 141.5(5) . 1_545 ?
O4 Cs10 N31 95.2(3) . 1_545 ?
O4 Cs10 N32 63.5(2) . . ?
O4 Cs10 C33 80.9(3) . . ?
O6 Cs10 Cs4 103.7(7) . . ?
O6 Cs10 Cs5 37.0(4) . . ?
O6 Cs10 Se4 100.8(5) . . ?
O6 Cs10 N32 96.1(6) . . ?
O6 Cs10 C33 105.4(6) . . ?
N12 Cs10 Cs1 103.1(3) 1_545 4_676 ?
N12 Cs10 Cs4 42.21(15) 1_545 . ?
N12 Cs10 Cs5 42.08(18) 1_545 . ?
N12 Cs10 Cs8 101.8(3) 1_545 3_667 ?
N12 Cs10 Se4 61.07(18) 1_545 . ?
N12 Cs10 N31 67.1(3) 1_545 1_545 ?
N12 Cs10 N32 115.4(3) 1_545 . ?
N12 Cs10 C33 105.4(3) 1_545 . ?
N31 Cs10 Cs1 112.8(3) 1_545 4_676 ?
N31 Cs10 Cs4 80.04(19) 1_545 . ?
N31 Cs10 Cs5 81.0(3) 1_545 . ?
N31 Cs10 Cs8 50.8(2) 1_545 3_667 ?
N31 Cs10 C33 162.0(4) 1_545 . ?
N32 Cs10 Cs1 37.06(15) . 4_676 ?
N32 Cs10 Cs4 123.3(3) . . ?
N32 Cs10 Cs5 83.3(2) . . ?
N32 Cs10 Cs8 142.5(3) . 3_667 ?
N32 Cs10 Se4 65.4(2) . . ?
N32 Cs10 N31 149.6(4) . 1_545 ?
N32 Cs10 C33 18.00(17) . . ?
C33 Cs10 Cs1 51.54(15) . 4_676 ?
C33 Cs10 Cs4 105.7(2) . . ?
C33 Cs10 Cs5 82.94(18) . . ?
C33 Cs10 Cs8 146.0(4) . 3_667 ?
Cs4 Cs2 Cs2 121.91(4) 2_556 3_677 ?
Cs7 Cs2 C32 73.1(2) 1_565 . ?
O1 Cs2 Cs4 56.71(16) . 2_556 ?
O1 Cs2 Cs2 99.82(15) . 3_677 ?
O1 Cs2 Cs7 159.7(2) . 1_565 ?
O1 Cs2 Cs7 58.4(2) . 3_667 ?
O1 Cs2 N21 117.98(19) . 2_556 ?
O1 Cs2 N22 50.06(18) . 2_556 ?
O1 Cs2 N23 100.32(19) . 2_556 ?
O1 Cs2 N31 122.8(2) . . ?
O1 Cs2 N31 73.4(2) . 3_677 ?
O1 Cs2 C21 106.15(18) . 2_556 ?
O1 Cs2 C32 111.5(2) . . ?
N21 Cs2 Cs4 102.15(10) 2_556 2_556 ?
N21 Cs2 Cs2 133.37(11) 2_556 3_677 ?
N21 Cs2 Cs7 165.54(17) 2_556 3_667 ?
N21 Cs2 Cs7 69.9(2) 2_556 1_565 ?
N21 Cs2 N22 72.70(14) 2_556 2_556 ?
N21 Cs2 N23 69.12(15) 2_556 2_556 ?
N21 Cs2 N31 120.34(17) 2_556 3_677 ?
N21 Cs2 C21 17.75(14) 2_556 2_556 ?
N21 Cs2 C32 123.75(16) 2_556 . ?
N22 Cs2 Cs4 46.59(11) 2_556 2_556 ?
N22 Cs2 Cs2 149.88(10) 2_556 3_677 ?
N22 Cs2 Cs7 107.68(17) 2_556 3_667 ?
N22 Cs2 N23 64.61(15) 2_556 2_556 ?
N22 Cs2 C32 129.67(16) 2_556 . ?
N23 Cs2 Cs4 45.77(11) 2_556 2_556 ?
N23 Cs2 Cs2 132.26(12) 2_556 3_677 ?
N23 Cs2 Cs7 124.60(17) 2_556 3_667 ?
N23 Cs2 C32 77.53(15) 2_556 . ?
N31 Cs2 Cs4 98.73(13) . 2_556 ?
N31 Cs2 Cs4 125.75(13) 3_677 2_556 ?
N31 Cs2 Cs2 46.35(14) . 3_677 ?
N31 Cs2 Cs2 44.14(14) 3_677 3_677 ?
N31 Cs2 Cs7 45.76(18) 3_677 3_667 ?
N31 Cs2 Cs7 58.5(2) . 1_565 ?
N31 Cs2 Cs7 71.0(2) . 3_667 ?
N31 Cs2 N21 117.45(18) . 2_556 ?
N31 Cs2 N22 144.65(17) . 2_556 ?
N31 Cs2 N22 114.22(18) 3_677 2_556 ?
N31 Cs2 N23 170.21(17) 3_677 2_556 ?
N31 Cs2 N23 86.66(17) . 2_556 ?
N31 Cs2 N31 90.5(2) . 3_677 ?
N31 Cs2 C21 123.32(17) . 2_556 ?
N31 Cs2 C21 132.48(16) 3_677 2_556 ?
N31 Cs2 C32 15.61(17) . . ?
N31 Cs2 C32 97.53(18) 3_677 . ?
C21 Cs2 Cs4 84.54(10) 2_556 2_556 ?
C21 Cs2 Cs2 150.61(11) 2_556 3_677 ?
C21 Cs2 Cs7 164.50(17) 2_556 3_667 ?
C21 Cs2 N22 57.49(14) 2_556 2_556 ?
C21 Cs2 N23 56.02(15) 2_556 2_556 ?
C21 Cs2 C32 124.19(15) 2_556 . ?
C32 Cs2 Cs4 83.32(12) . 2_556 ?
C32 Cs2 Cs2 54.83(11) . 3_677 ?
C32 Cs2 Cs7 67.68(18) . 3_667 ?
Cs2 Cs7 O3 81.0(2) 1_545 . ?
O3 Cs7 Cs2 138.7(3) . 3_667 ?
O3 Cs7 Cs7 88.3(3) . 3_667 ?
O3 Cs7 O4 60.2(2) . 3_667 ?
O3 Cs7 N34 160.4(4) . 3_667 ?
O4 Cs7 Cs2 151.7(4) . 1_545 ?
O4 Cs7 Cs2 81.7(3) . 3_667 ?
O4 Cs7 Cs2 151.4(3) 3_667 3_667 ?
O4 Cs7 Cs7 60.0(3) . 3_667 ?
O4 Cs7 Cs7 42.5(2) 3_667 3_667 ?
O4 Cs7 O3 126.4(4) . . ?
O4 Cs7 O4 102.5(3) . 3_667 ?
O4 Cs7 N31 108.1(4) . 1_545 ?
O4 Cs7 N34 52.0(2) . 3_667 ?
N31 Cs7 Cs2 59.0(2) 1_545 1_545 ?
N31 Cs7 Cs2 48.46(19) 1_545 3_667 ?
N31 Cs7 Cs7 163.5(5) 1_545 3_667 ?
N31 Cs7 O3 91.2(3) 1_545 . ?
N31 Cs7 O4 147.1(4) 1_545 3_667 ?
N31 Cs7 N34 108.0(3) 1_545 3_667 ?
N34 Cs7 Cs2 59.7(2) 3_667 3_667 ?
N34 Cs7 Cs7 74.5(3) 3_667 3_667 ?
N34 Cs7 O4 100.3(3) 3_667 3_667 ?
Re1 Se1 Cs5 89.504(19) . 1_565 ?
Re3 Se1 Re1 70.056(18) . . ?
Re3 Se1 Cs5 139.41(2) . 1_565 ?
Re4 Se1 Re1 69.684(18) . . ?
Re4 Se1 Re3 70.259(18) . . ?
Re4 Se1 Cs5 135.86(2) . 1_565 ?
W3 Se1 W1 70.056(18) . . ?
W4 Se1 W1 69.684(18) . . ?
W4 Se1 W3 70.259(18) . . ?
Re1 Se2 Cs4 170.93(2) . 2_556 ?
Re1 Se2 Cs4 89.730(19) . 1_565 ?
Re2 Se2 Re1 69.848(18) . . ?
Re2 Se2 Cs4 138.10(2) . 1_565 ?
Re2 Se2 Cs4 101.26(2) . 2_556 ?
Re3 Se2 Re1 70.336(18) . . ?
Re3 Se2 Re2 70.514(18) . . ?
Re3 Se2 Cs4 137.46(2) . 1_565 ?
Re3 Se2 Cs4 105.49(2) . 2_556 ?
W2 Se2 W1 69.848(18) . . ?
W3 Se2 W1 70.336(18) . . ?
W3 Se2 W2 70.514(18) . . ?
Cs4 Se2 Cs4 98.444(14) 1_565 2_556 ?
Re1 Se3 Re4 69.615(18) . . ?
Re1 Se3 Cs1 107.75(2) . . ?
Re1 Se3 Cs3 134.73(2) . . ?
Re2 Se3 Re1 69.953(18) . . ?
Re2 Se3 Re4 70.770(18) . . ?
Re2 Se3 Cs1 103.860(19) . . ?
Re2 Se3 Cs3 143.92(2) . . ?
Re4 Se3 Cs1 174.50(2) . . ?
Re4 Se3 Cs3 92.232(19) . . ?
W1 Se3 W4 69.615(18) . . ?
W1 Se3 Cs1 107.75(2) . . ?
W1 Se3 Cs3 134.73(2) . . ?
W2 Se3 W1 69.953(18) . . ?
W2 Se3 W4 70.770(18) . . ?
W2 Se3 Cs1 103.860(19) . . ?
W2 Se3 Cs3 143.92(2) . . ?
W4 Se3 Cs1 174.50(2) . . ?
W4 Se3 Cs3 92.232(19) . . ?
Cs3 Se3 Cs1 92.946(16) . . ?
Re2 Se4 Re3 70.429(19) . . ?
Re2 Se4 Re4 71.024(19) . . ?
Re2 Se4 Cs6 150.22(6) . . ?
Re3 Se4 Cs6 105.49(7) . . ?
Re4 Se4 Re3 70.178(19) . . ?
Re4 Se4 Cs6 136.83(7) . . ?
W2 Se4 W3 70.429(19) . . ?
W2 Se4 W4 71.024(19) . . ?
W2 Se4 Cs10 146.79(19) . . ?
W3 Se4 Cs10 102.22(19) . . ?
W4 Se4 W3 70.178(19) . . ?
W4 Se4 Cs10 138.60(14) . . ?
Cs9 O1 Cs8 18.3(3) 3_677 3_677 ?
Cs4 O3 Cs6 105.32(19) . . ?
Cs4 O3 Cs7 129.3(3) . . ?
Cs10 O3 Cs4 108.2(3) . . ?
Cs6 O4 Cs7 87.3(3) . 3_667 ?
Cs1 O9 Cs5 97.75(19) . 3_666 ?
Cs1 O9 Cs9 89.52(18) . 4_575 ?
Cs5 O9 Cs9 147.5(2) 3_666 4_575 ?
C1 O9 Cs1 126.8(7) . . ?
C1 O9 Cs5 116.7(7) . 3_666 ?
C1 O9 Cs9 40.2(6) . 4_575 ?
Cs5 O5 Cs1 98.2(4) . 4_676 ?
Cs6 O5 Cs1 94.2(4) . 4_676 ?
Cs6 O5 Cs5 104.8(4) . . ?
Cs5 O6 Cs10 106.0(7) . . ?
Cs1 N11 Cs3 122.38(19) 3_676 3_676 ?
Cs1 N11 Cs5 91.82(15) 3_676 1_565 ?
Cs3 N11 Cs5 109.51(17) 3_676 1_565 ?
C11 N11 Cs1 133.6(5) . 3_676 ?
C11 N11 Cs3 99.5(5) . 3_676 ?
C11 N11 Cs5 91.9(5) . 1_565 ?
Cs4 N12 Cs5 152.3(2) 1_565 1_565 ?
Cs6 N12 Cs4 100.7(2) 1_565 1_565 ?
Cs6 N12 Cs5 96.02(19) 1_565 1_565 ?
Cs6 N12 Cs10 5.1(2) 1_565 1_565 ?
C12 N12 Cs4 90.7(5) . 1_565 ?
C12 N12 Cs5 91.7(5) . 1_565 ?
C12 N12 Cs6 137.6(6) . 1_565 ?
C12 N12 Cs10 141.5(6) . 1_565 ?
Cs1 N13 Cs4 152.98(19) . 1_565 ?
Cs3 N13 Cs1 94.52(16) 3_676 . ?
Cs3 N13 Cs4 106.17(17) 3_676 1_565 ?
C13 N13 Cs1 104.4(5) . . ?
C13 N13 Cs3 100.1(5) . 3_676 ?
C13 N13 Cs4 89.1(5) . 1_565 ?
Cs1 N21 Cs9 86.27(16) . 4_575 ?
Cs1 N21 Cs2 115.87(18) . 2_546 ?
Cs8 N21 Cs1 98.5(3) 4_575 . ?
C21 N21 Cs1 99.6(5) . . ?
C21 N21 Cs9 94.4(5) . 4_575 ?
C21 N21 Cs8 104.5(5) . 4_575 ?
C21 N21 Cs2 98.5(5) . 2_546 ?
Cs3 N22 Cs4 107.61(19) 3_666 . ?
Cs3 N22 Cs8 129.1(3) 3_666 4_575 ?
Cs3 N22 Cs2 138.1(2) 3_666 2_546 ?
Cs4 N22 Cs8 95.2(3) . 4_575 ?
Cs4 N22 Cs2 79.72(14) . 2_546 ?
Cs9 N22 Cs3 114.1(2) 4_575 3_666 ?
Cs9 N22 Cs4 104.2(2) 4_575 . ?
Cs9 N22 Cs8 15.2(2) 4_575 4_575 ?
Cs9 N22 Cs2 29.11(11) 4_575 2_546 ?
C22 N22 Cs3 125.6(5) . 3_666 ?
C22 N22 Cs4 97.9(5) . . ?
C22 N22 Cs9 104.5(5) . 4_575 ?
C22 N22 Cs8 94.0(5) . 4_575 ?
C22 N22 Cs2 92.7(5) . 2_546 ?
Cs4 N23 Cs4 146.7(3) 2_556 . ?
Cs4 N23 Cs2 117.7(2) 2_556 2_546 ?
Cs4 N23 Cs2 79.69(19) . 2_546 ?
C23 N23 Cs4 97.4(5) . . ?
C23 N23 Cs4 109.4(6) . 2_556 ?
C23 N23 Cs2 91.9(7) . 2_546 ?
Cs6 N31 Cs10 3.1(2) 1_565 1_565 ?
Cs6 N31 Cs2 107.8(2) 1_565 3_677 ?
Cs9 N31 Cs6 103.3(2) . 1_565 ?
Cs9 N31 Cs10 105.7(3) . 1_565 ?
Cs9 N31 Cs2 32.24(11) . 3_677 ?
Cs9 N31 Cs7 100.4(3) . 1_565 ?
Cs7 N31 Cs2 62.4(2) 1_565 . ?
C32 N31 Cs6 128.9(7) . 1_565 ?
C32 N31 Cs9 98.4(6) . . ?
C32 N31 Cs8 100.2(6) . . ?
C32 N31 Cs10 129.6(7) . 1_565 ?
C32 N31 Cs2 113.7(6) . . ?
C32 N31 Cs2 114.9(6) . 3_677 ?
C32 N31 Cs7 159.3(7) . 1_565 ?
Cs1 N32 Cs6 96.2(2) 4_676 . ?
Cs1 N32 Cs9 92.2(2) 4_676 . ?
Cs1 N32 Cs8 102.0(3) 4_676 . ?
Cs1 N32 Cs10 100.7(3) 4_676 . ?
Cs9 N32 Cs6 155.3(3) . . ?
Cs8 N32 Cs10 134.8(4) . . ?
C33 N32 Cs1 135.3(6) . 4_676 ?
C33 N32 Cs6 96.5(6) . . ?
C33 N32 Cs9 93.6(6) . . ?
C33 N32 Cs8 97.0(7) . . ?
C33 N32 Cs10 93.5(6) . . ?
Cs4 N34 Cs7 132.4(3) 2_556 3_667 ?
C31 N34 Cs4 109.5(6) . 2_556 ?
C31 N34 Cs7 107.7(7) . 3_667 ?
Cs1 N41 Cs3 96.53(17) 3_676 . ?
Cs1 N41 Cs5 100.47(16) 3_676 2_656 ?
Cs3 N41 Cs5 150.5(2) . 2_656 ?
C41 N41 Cs1 133.2(5) . 3_676 ?
C41 N41 Cs3 89.3(5) . . ?
C41 N41 Cs5 96.3(5) . 2_656 ?
Cs3 N42 Cs3 97.00(17) 3_666 . ?
Cs3 N42 Cs5 107.58(17) 3_666 . ?
Cs3 N42 Cs5 146.22(19) . . ?
C42 N42 Cs3 125.8(5) . 3_666 ?
C42 N42 Cs3 88.7(5) . . ?
C42 N42 Cs5 95.1(5) . . ?
Cs1 N43 Cs5 92.12(16) 4_676 2_656 ?
Cs1 N43 Cs5 105.15(17) 4_676 . ?
Cs5 N43 Cs5 129.6(2) . 2_656 ?
C43 N43 Cs1 130.1(5) . 4_676 ?
C43 N43 Cs5 103.6(5) . . ?
C43 N43 Cs5 99.8(5) . 2_656 ?
Cs9 C1 Cs8 8.4(2) 4_575 4_575 ?
O9 C1 Cs9 120.4(8) . 4_575 ?
O9 C1 Cs8 114.3(7) . 4_575 ?
Re1 C11 Cs3 114.7(2) . 3_676 ?
Re1 C11 Cs5 110.6(2) . 1_565 ?
Cs3 C11 Cs5 96.94(15) 3_676 1_565 ?
N11 C11 Re1 176.6(6) . . ?
N11 C11 W1 176.6(6) . . ?
N11 C11 Cs3 62.0(4) . 3_676 ?
N11 C11 Cs5 69.5(4) . 1_565 ?
Re1 C12 Cs4 109.4(2) . 1_565 ?
Re1 C12 Cs5 108.4(2) . 1_565 ?
Cs4 C12 Cs5 132.31(19) 1_565 1_565 ?
N12 C12 Re1 176.8(7) . . ?
N12 C12 W1 176.8(7) . . ?
N12 C12 Cs4 70.5(5) . 1_565 ?
N12 C12 Cs5 70.2(5) . 1_565 ?
Re1 C13 Cs1 122.0(2) . . ?
Re1 C13 Cs3 117.3(2) . 3_676 ?
Re1 C13 Cs4 107.6(2) . 1_565 ?
W1 C13 Cs1 122.0(2) . . ?
Cs3 C13 Cs1 81.14(13) 3_676 . ?
Cs3 C13 Cs4 94.96(15) 3_676 1_565 ?
Cs4 C13 Cs1 126.07(17) 1_565 . ?
N13 C13 Re1 178.3(6) . . ?
N13 C13 W1 178.3(6) . . ?
N13 C13 Cs1 58.8(4) . . ?
N13 C13 Cs3 61.1(4) . 3_676 ?
N13 C13 Cs4 72.3(4) . 1_565 ?
Re2 C21 Cs1 121.5(2) . . ?
Re2 C21 Cs9 112.5(2) . 4_575 ?
Re2 C21 Cs8 122.0(3) . 4_575 ?
Re2 C21 Cs2 114.2(2) . 2_546 ?
W2 C21 Cs1 121.5(2) . . ?
Cs9 C21 Cs1 77.44(14) 4_575 . ?
Cs8 C21 Cs1 84.2(2) 4_575 . ?
Cs2 C21 Cs1 100.04(15) 2_546 . ?
N21 C21 Re2 175.7(6) . . ?
N21 C21 W2 175.7(6) . . ?
N21 C21 Cs1 62.8(4) . . ?
N21 C21 Cs9 67.7(4) . 4_575 ?
N21 C21 Cs8 57.1(5) . 4_575 ?
N21 C21 Cs2 63.7(4) . 2_546 ?
Re2 C22 Cs3 144.4(2) . 3_666 ?
Re2 C22 Cs4 111.6(2) . . ?
Re2 C22 Cs9 120.6(3) . 4_575 ?
W2 C22 Cs4 111.6(2) . . ?
Cs4 C22 Cs3 87.07(14) . 3_666 ?
Cs9 C22 Cs3 88.31(17) 4_575 3_666 ?
Cs9 C22 Cs4 89.18(16) 4_575 . ?
N22 C22 Re2 174.7(6) . . ?
N22 C22 W2 174.7(6) . . ?
N22 C22 Cs3 40.5(4) . 3_666 ?
N22 C22 Cs4 64.3(5) . . ?
N22 C22 Cs9 57.1(4) . 4_575 ?
Re2 C23 Cs4 113.6(2) . . ?
Re2 C23 Cs4 129.1(3) . 2_556 ?
W2 C23 Cs4 113.6(2) . . ?
Cs4 C23 Cs4 115.59(18) . 2_556 ?
N23 C23 Re2 175.8(8) . . ?
N23 C23 W2 175.8(8) . . ?
N23 C23 Cs4 53.8(5) . 2_556 ?
N23 C23 Cs4 64.6(5) . . ?
N34 C31 Re3 176.5(8) . . ?
N34 C31 W3 176.5(8) . . ?
Re3 C32 Cs9 116.1(3) . . ?
W3 C32 Cs8 116.9(3) . . ?
N31 C32 Re3 175.9(8) . . ?
N31 C32 W3 175.9(8) . . ?
N31 C32 Cs9 62.9(5) . . ?
N31 C32 Cs8 60.8(5) . . ?
N31 C32 Cs2 50.7(5) . . ?
Re3 C33 Cs6 111.3(3) . . ?
Re3 C33 Cs9 112.7(3) . . ?
W3 C33 Cs8 115.5(3) . . ?
W3 C33 Cs10 109.1(3) . . ?
Cs9 C33 Cs6 129.6(2) . . ?
Cs8 C33 Cs10 116.2(3) . . ?
N32 C33 Re3 176.4(7) . . ?
N32 C33 W3 176.4(7) . . ?
N32 C33 Cs6 66.5(6) . . ?
N32 C33 Cs9 68.2(6) . . ?
N32 C33 Cs8 64.1(6) . . ?
N32 C33 Cs10 68.5(6) . . ?
Re4 C41 Cs3 108.0(2) . . ?
Re4 C41 Cs5 112.2(2) . 2_656 ?
W4 C41 Cs3 108.0(2) . . ?
Cs3 C41 Cs5 128.93(18) . 2_656 ?
N41 C41 Re4 175.7(6) . . ?
N41 C41 W4 175.7(6) . . ?
N41 C41 Cs3 71.2(4) . . ?
N41 C41 Cs5 66.3(4) . 2_656 ?
Re4 C42 Cs3 103.7(2) . . ?
Re4 C42 Cs3 145.9(2) . 3_666 ?
Re4 C42 Cs5 111.8(2) . . ?
W4 C42 Cs3 103.7(2) . . ?
W4 C42 Cs5 111.8(2) . . ?
Cs3 C42 Cs3 81.60(13) . 3_666 ?
Cs3 C42 Cs5 88.44(13) 3_666 . ?
Cs3 C42 Cs5 128.50(17) . . ?
N42 C42 Re4 173.2(6) . . ?
N42 C42 W4 173.2(6) . . ?
N42 C42 Cs3 40.2(4) . 3_666 ?
N42 C42 Cs3 72.6(4) . . ?
N42 C42 Cs5 67.8(4) . . ?
Re4 C43 Cs5 117.4(2) . 2_656 ?
Re4 C43 Cs5 118.3(2) . . ?
W4 C43 Cs5 118.3(2) . . ?
Cs5 C43 Cs5 107.18(16) 2_656 . ?
N43 C43 Re4 175.8(6) . . ?
N43 C43 W4 175.8(6) . . ?
N43 C43 Cs5 58.8(4) . . ?
N43 C43 Cs5 62.3(4) . 2_656 ?

_olex2_submission_special_instructions 'No special instructions were received'
_vrf_PLAT430_pr939               
;
PROBLEM: Short Inter D...A Contact O1 ..O5 . 2.79 Ang. and related alerts
RESPONSE: These oxygen atoms belong to H2O molecules.
Hydrogen atoms were not localized, but included in the formula of the compound.
;
_vrf_PLAT972_pr939               
;
PROBLEM: Check Calcd Resid. Dens. 0.50A From Cs2 -3.13 eA-3 and related alerts
RESPONSE: Cs cations are disordered over three positions; actual disorder is more complicated.
;
_exptl_crystal_preparation       'Magnetic properties'
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_pr908
_database_code_depnum_ccdc_archive 'CCDC 2111044'
loop_
_audit_author_name
_audit_author_address
'Taisiya Sukhikh'
;NIIC SB RAS
Russia
;
_audit_update_record             
;
2021-09-21 deposited with the CCDC.	2021-11-15 downloaded from the CCDC.
;
_audit_creation_date             2021-06-28
_audit_creation_method           
;
Olex2 1.2
(compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506)
;
_shelx_SHELXL_version_number     2017/1
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C14 H24 K7 Mo3 N12 O10 Re1 Se4'
_chemical_formula_sum            'C14 H24 K7 Mo3 N12 O10 Re1 Se4'
_chemical_formula_weight         1584.77
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
K K 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mo Mo -1.6832 0.6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Re Re -1.0185 7.2310 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Se Se -0.0929 2.2259 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      orthorhombic
_space_group_IT_number           62
_space_group_name_H-M_alt        'P n m a'
_space_group_name_Hall           '-P 2ac 2n'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, -y, z+1/2'
'-x, y+1/2, -z'
'x+1/2, -y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, y, -z-1/2'
'x, -y-1/2, z'
'-x-1/2, y-1/2, z-1/2'

_cell_length_a                   11.8651(2)
_cell_length_b                   21.2079(4)
_cell_length_c                   15.7889(3)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_volume                     3973.02(13)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    9862
_cell_measurement_temperature    150(2)
_cell_measurement_theta_max      30.38
_cell_measurement_theta_min      2.88
_shelx_estimated_absorpt_T_max   0.677
_shelx_estimated_absorpt_T_min   0.486
_exptl_absorpt_coefficient_mu    8.446
_exptl_absorpt_correction_T_max  0.4935
_exptl_absorpt_correction_T_min  0.3481
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
'SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.0990 before and 0.0650 after correction. The Ratio of minimum to maximum transmission is 0.7054. The λ/2 correction factor is Not present.'
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            black
_exptl_crystal_colour_primary    black
_exptl_crystal_density_diffrn    2.619
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       prism
_exptl_crystal_F_000             2897
_exptl_crystal_size_max          0.1
_exptl_crystal_size_mid          0.08
_exptl_crystal_size_min          0.05
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0549
_diffrn_reflns_av_unetI/netI     0.0291
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.999
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -16
_diffrn_reflns_limit_k_max       30
_diffrn_reflns_limit_k_min       -30
_diffrn_reflns_limit_l_max       22
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            54820
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.999
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         30.512
_diffrn_reflns_theta_min         2.352
_diffrn_ambient_temperature      150(2)
_diffrn_detector                 PIXEL
_diffrn_detector_area_resol_mean 7.41
_diffrn_detector_type            'Bruker PHOTON III area detector'
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device       'three-circle diffractometer'
_diffrn_measurement_device_type  'Bruker D8 Venture diffractometer'
_diffrn_measurement_method       'ω and φ scans'
_diffrn_radiation_monochromator  'Incoatec HELIOS multilayer mirrors'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   'Incoatec IuS3.0 microfocus X-ray tube'
_diffrn_special_details          ?
_diffrn_standards_interval_count .
_diffrn_standards_interval_time  .
_diffrn_standards_number         .
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                5543
_reflns_number_total             6215
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'Bruker SAINT'
_computing_data_collection       'Bruker APEX3'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    'ShelXT (Sheldrick, 2015)'
_refine_diff_density_max         1.524
_refine_diff_density_min         -1.333
_refine_diff_density_rms         0.206
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.181
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     254
_refine_ls_number_reflns         6215
_refine_ls_number_restraints     3
_refine_ls_R_factor_all          0.0478
_refine_ls_R_factor_gt           0.0420
_refine_ls_restrained_S_all      1.181
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0062P)²+48.9908P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0863
_refine_ls_wR_factor_ref         0.0883
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.5 times of:
  All C(H,H,H) groups
2. Shared sites
{Mo1, Re1}
{Mo2, Re2}
{Mo3, Re3}
3. Uiso/Uaniso restraints and constraints
Uanis(Mo1) = Uanis(Re1)
Uanis(Mo2) = Uanis(Re2)
Uanis(Mo3) = Uanis(Re3)
4. Rigid body (RIGU) restrains
 O4, C4
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
5. Others
 Sof(Re1)=0.5*(1-FVAR(2))
 Sof(Mo1)=0.5*FVAR(2)
 Sof(Re2)=0.5*(1-FVAR(3))
 Sof(Mo2)=0.5*FVAR(3)
 Sof(Re3)=1-FVAR(3)
 Sof(Mo3)=FVAR(3)
 Fixed Sof: K5(0.5)
6.a Idealised Me refined as rotating group:
 C4(H4A,H4B,H4C)
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Re1 Re -0.27166(4) 0.250000 0.88943(3) 0.01423(17) Uani 0.173(4) 2 d S T P A 2
Re2 Re -0.31278(4) 0.250000 1.06874(3) 0.01476(16) Uani 0.252(4) 2 d S T P A 2
Re3 Re -0.12106(3) 0.18230(2) 1.00107(2) 0.01456(11) Uani 0.293(3) 1 d . . . A
2
Mo1 Mo -0.27166(4) 0.250000 0.88943(3) 0.01423(17) Uani 0.827(4) 2 d S T P A 1
Mo2 Mo -0.31278(4) 0.250000 1.06874(3) 0.01476(16) Uani 0.748(4) 2 d S T P A 1
Mo3 Mo -0.12106(3) 0.18230(2) 1.00107(2) 0.01456(11) Uani 0.707(3) 1 d . . . A
1
Se1 Se -0.32211(5) 0.15539(3) 0.97533(3) 0.01729(13) Uani 1 1 d . . . . .
Se2 Se -0.06213(6) 0.250000 0.87946(5) 0.01625(16) Uani 1 2 d S T P . .
Se3 Se -0.11807(6) 0.250000 1.13017(4) 0.01494(15) Uani 1 2 d S T P . .
K1 K -0.53706(13) 0.11210(8) 0.79717(10) 0.0351(3) Uani 1 1 d . . . . .
K2 K -0.75626(16) 0.250000 0.90142(12) 0.0281(4) Uani 1 2 d S T P . .
K3 K -0.76797(16) 0.250000 1.16509(11) 0.0227(3) Uani 1 2 d S T P . .
K4 K 0.14721(14) 0.05808(7) 1.15274(11) 0.0372(4) Uani 1 1 d . . . . .
O1 O -0.6257(7) -0.0099(3) 0.8460(5) 0.078(2) Uani 1 1 d . . . . .
O2 O -0.6171(5) 0.1233(3) 0.9634(4) 0.0518(15) Uani 1 1 d . . . . .
O3 O 0.3555(4) 0.1359(2) 1.1879(3) 0.0356(11) Uani 1 1 d . . . . .
O4 O 0.1837(8) 0.0330(4) 0.9753(7) 0.094(3) Uani 1 1 d . U . . .
O5 O 0.3437(5) -0.0205(3) 1.2136(4) 0.0545(16) Uani 1 1 d . . . . .
N11 N -0.2745(5) 0.1484(3) 0.7303(3) 0.0270(11) Uani 1 1 d . . . . .
N12 N -0.5405(6) 0.250000 0.8366(5) 0.0245(15) Uani 1 2 d S T P A .
N21 N -0.3820(5) 0.3520(3) 1.2178(3) 0.0338(13) Uani 1 1 d . . . . .
N22 N -0.5894(6) 0.250000 1.0486(5) 0.0310(17) Uani 1 2 d S T P A .
N31 N -0.1165(5) 0.0686(2) 1.1435(3) 0.0278(11) Uani 1 1 d . . . . .
N32 N 0.1525(4) 0.1653(3) 1.0314(3) 0.0260(11) Uani 1 1 d . . . . .
N33 N -0.0628(5) 0.0652(3) 0.8700(3) 0.0287(11) Uani 1 1 d . . . . .
C4 C 0.1806(6) 0.0569(4) 0.9022(8) 0.066(3) Uani 1 1 d . U . . .
H4A H 0.256092 0.055811 0.877078 0.098 Uiso 1 1 calc GR . . . .
H4B H 0.154804 0.100737 0.906031 0.098 Uiso 1 1 calc GR . . . .
H4C H 0.128390 0.032819 0.866577 0.098 Uiso 1 1 calc GR . . . .
C11 C -0.2695(4) 0.1829(3) 0.7856(3) 0.0190(10) Uani 1 1 d . . . . .
C12 C -0.4469(6) 0.250000 0.8568(5) 0.0158(13) Uani 1 2 d S T P . .
C21 C -0.3542(5) 0.3169(3) 1.1660(3) 0.0204(11) Uani 1 1 d . . . . .
C22 C -0.4932(6) 0.250000 1.0561(5) 0.0194(15) Uani 1 2 d S T P . .
C31 C -0.1225(5) 0.1083(3) 1.0930(4) 0.0198(10) Uani 1 1 d . . . . .
C32 C 0.0555(5) 0.1735(3) 1.0220(3) 0.0187(10) Uani 1 1 d . . . . .
C33 C -0.0856(5) 0.1063(3) 0.9160(4) 0.0213(11) Uani 1 1 d . . . . .
K5 K 0.4307(6) 0.0132(3) 1.0458(4) 0.107(2) Uani 0.5 1 d . . . B -1


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Re1 Re2 2.8729(7) . ?
Re1 Re3 2.8916(6) 7_565 ?
Re1 Re3 2.8916(6) . ?
Re1 Se1 2.4948(6) 7_565 ?
Re1 Se1 2.4948(6) . ?
Re1 Se2 2.4911(9) . ?
Re1 C11 2.171(6) . ?
Re1 C11 2.171(6) 7_565 ?
Re1 C12 2.142(7) . ?
Re2 Re3 2.8944(5) 7_565 ?
Re2 Re3 2.8944(5) . ?
Re2 Se1 2.4927(6) . ?
Re2 Se1 2.4928(6) 7_565 ?
Re2 Se3 2.5056(9) . ?
Re2 C21 2.147(6) 7_565 ?
Re2 C21 2.147(6) . ?
Re2 C22 2.150(8) . ?
Re3 Re3 2.8716(7) 7_565 ?
Re3 Se1 2.4862(6) . ?
Re3 Se2 2.4974(7) . ?
Re3 Se3 2.4934(7) . ?
Re3 C31 2.137(6) . ?
Re3 C32 2.129(6) . ?
Re3 C33 2.140(6) . ?
Mo1 Mo2 2.8729(7) . ?
Mo1 Mo3 2.8916(6) . ?
Mo1 Se1 2.4948(6) 7_565 ?
Mo1 Se1 2.4948(6) . ?
Mo1 Se2 2.4911(9) . ?
Mo1 C11 2.171(6) . ?
Mo1 C11 2.171(6) 7_565 ?
Mo1 C12 2.142(7) . ?
Mo2 Mo3 2.8944(5) . ?
Mo2 Se1 2.4927(6) . ?
Mo2 Se1 2.4928(6) 7_565 ?
Mo2 Se3 2.5056(9) . ?
Mo2 C21 2.147(6) 7_565 ?
Mo2 C21 2.147(6) . ?
Mo2 C22 2.150(8) . ?
Mo3 Se1 2.4862(6) . ?
Mo3 Se2 2.4974(7) . ?
Mo3 Se3 2.4934(7) . ?
Mo3 C31 2.137(6) . ?
Mo3 C32 2.129(6) . ?
Mo3 C33 2.140(6) . ?
Se1 K1 3.9064(16) . ?
Se2 K2 3.646(2) 1_655 ?
Se3 K3 3.6896(19) 6_658 ?
K1 O1 2.897(7) . ?
K1 O2 2.802(6) . ?
K1 O5 3.011(6) 5_557 ?
K1 N11 2.952(6) 6_557 ?
K1 N11 3.379(6) . ?
K1 N12 2.990(2) . ?
K1 N33 2.837(6) 6_557 ?
K1 C11 3.517(5) . ?
K1 C11 3.402(6) 6_557 ?
K1 C12 3.254(4) . ?
K1 C33 3.417(6) 6_557 ?
K2 O2 3.302(7) 7_565 ?
K2 O2 3.302(7) . ?
K2 N11 3.003(6) 6_557 ?
K2 N11 3.003(6) 4_456 ?
K2 N12 2.758(7) . ?
K2 N22 3.053(8) . ?
K2 N32 2.934(6) 1_455 ?
K2 N32 2.934(6) 7_465 ?
K2 C11 3.282(6) 4_456 ?
K2 C11 3.282(6) 6_557 ?
K2 C32 3.352(6) 1_455 ?
K2 C32 3.352(6) 7_465 ?
K3 O3 2.852(5) 1_455 ?
K3 O3 2.852(5) 7_465 ?
K3 N21 3.151(6) 4_457 ?
K3 N21 3.151(6) 6_558 ?
K3 N22 2.806(8) . ?
K3 N32 2.928(5) 7_465 ?
K3 N32 2.928(5) 1_455 ?
K3 C21 3.190(6) 4_457 ?
K3 C21 3.190(6) 6_558 ?
K3 C32 3.482(6) 7_465 ?
K3 C32 3.482(6) 1_455 ?
K4 O1 3.228(8) 2_455 ?
K4 O3 3.022(5) . ?
K4 O4 2.884(10) . ?
K4 O5 3.023(6) . ?
K4 N21 2.816(6) 4_557 ?
K4 N31 3.140(6) . ?
K4 N32 2.975(6) . ?
K4 N33 2.823(6) 5_557 ?
K4 C31 3.502(6) . ?
K4 C32 3.383(6) . ?
K4 K5 3.882(8) . ?
O4 C4 1.262(14) . ?
O4 K5 3.163(12) . ?
O5 K5 2.932(9) . ?
N11 C11 1.142(7) . ?
N12 C12 1.155(10) . ?
N21 C21 1.155(8) . ?
N22 C22 1.148(10) . ?
N31 C31 1.162(8) . ?
N32 C32 1.173(7) . ?
N33 C33 1.166(8) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Re2 Re1 Re3 60.277(14) . . ?
Re3 Re1 Re3 59.542(16) 7_565 . ?
Se1 Re1 Re2 54.796(16) . . ?
Se1 Re1 Re2 54.797(16) 7_565 . ?
Se1 Re1 Re3 102.49(2) 7_565 . ?
Se1 Re1 Re3 54.374(16) 7_565 7_565 ?
Se1 Re1 Re3 102.49(2) . 7_565 ?
Se1 Re1 Re3 54.374(16) . . ?
Se1 Re1 Se1 107.08(3) . 7_565 ?
Se2 Re1 Re2 103.40(3) . . ?
Se2 Re1 Re3 54.677(18) . . ?
Se2 Re1 Re3 54.677(18) . 7_565 ?
Se2 Re1 Se1 105.89(2) . 7_565 ?
Se2 Re1 Se1 105.89(2) . . ?
C11 Re1 Re2 138.26(14) . . ?
C11 Re1 Re2 138.26(14) 7_565 . ?
C11 Re1 Re3 97.34(15) . . ?
C11 Re1 Re3 141.13(14) 7_565 . ?
C11 Re1 Re3 141.13(14) . 7_565 ?
C11 Re1 Re3 97.33(15) 7_565 7_565 ?
C11 Re1 Se1 160.14(15) 7_565 . ?
C11 Re1 Se1 160.13(15) . 7_565 ?
C11 Re1 Se1 83.46(14) 7_565 7_565 ?
C11 Re1 Se1 83.46(15) . . ?
C11 Re1 Se2 86.60(14) . . ?
C11 Re1 Se2 86.60(14) 7_565 . ?
C11 Re1 C11 81.9(3) 7_565 . ?
C12 Re1 Re2 94.12(19) . . ?
C12 Re1 Re3 138.26(13) . 7_565 ?
C12 Re1 Re3 138.27(13) . . ?
C12 Re1 Se1 84.12(12) . . ?
C12 Re1 Se1 84.12(12) . 7_565 ?
C12 Re1 Se2 162.48(19) . . ?
C12 Re1 C11 80.2(2) . . ?
C12 Re1 C11 80.2(2) . 7_565 ?
Re1 Re2 Re3 60.182(14) . . ?
Se1 Re2 Re1 54.862(15) . . ?
Se1 Re2 Re1 54.862(15) 7_565 . ?
Se1 Re2 Re3 102.46(2) 7_565 . ?
Se1 Re2 Re3 54.350(16) 7_565 7_565 ?
Se1 Re2 Re3 54.351(16) . . ?
Se1 Re2 Re3 102.46(2) . 7_565 ?
Se1 Re2 Se1 107.21(3) . 7_565 ?
Se1 Re2 Se3 105.66(2) 7_565 . ?
Se1 Re2 Se3 105.66(2) . . ?
Se3 Re2 Re1 102.99(3) . . ?
Se3 Re2 Re3 54.425(17) . 7_565 ?
Se3 Re2 Re3 54.423(17) . . ?
C21 Re2 Re1 138.03(16) . . ?
C21 Re2 Re1 138.03(16) 7_565 . ?
C21 Re2 Re3 140.50(15) . . ?
C21 Re2 Re3 96.68(15) . 7_565 ?
C21 Re2 Re3 96.68(15) 7_565 . ?
C21 Re2 Re3 140.50(15) 7_565 7_565 ?
C21 Re2 Se1 160.83(15) . . ?
C21 Re2 Se1 160.83(15) 7_565 7_565 ?
C21 Re2 Se1 83.18(16) 7_565 . ?
C21 Re2 Se1 83.18(16) . 7_565 ?
C21 Re2 Se3 86.24(15) . . ?
C21 Re2 Se3 86.24(15) 7_565 . ?
C21 Re2 C21 82.7(3) . 7_565 ?
C21 Re2 C22 80.7(2) . . ?
C21 Re2 C22 80.7(2) 7_565 . ?
C22 Re2 Re1 94.4(2) . . ?
C22 Re2 Re3 138.44(14) . . ?
C22 Re2 Re3 138.44(14) . 7_565 ?
C22 Re2 Se1 84.31(12) . 7_565 ?
C22 Re2 Se1 84.31(12) . . ?
C22 Re2 Se3 162.6(2) . . ?
Re1 Re3 Re2 59.541(15) . . ?
Re3 Re3 Re1 60.229(8) 7_565 . ?
Re3 Re3 Re2 60.261(8) 7_565 . ?
Se1 Re3 Re1 54.651(16) . . ?
Se1 Re3 Re2 54.562(16) . . ?
Se1 Re3 Re3 103.271(15) . 7_565 ?
Se1 Re3 Se2 105.96(2) . . ?
Se1 Re3 Se3 106.23(2) . . ?
Se2 Re3 Re1 54.47(2) . . ?
Se2 Re3 Re2 102.632(18) . . ?
Se2 Re3 Re3 54.908(12) . 7_565 ?
Se3 Re3 Re1 102.782(19) . . ?
Se3 Re3 Re2 54.82(2) . . ?
Se3 Re3 Re3 54.843(12) . 7_565 ?
Se3 Re3 Se2 107.065(19) . . ?
C31 Re3 Re1 140.67(15) . . ?
C31 Re3 Re2 96.15(15) . . ?
C31 Re3 Re3 137.22(14) . 7_565 ?
C31 Re3 Se1 86.26(15) . . ?
C31 Re3 Se2 161.14(15) . . ?
C31 Re3 Se3 82.39(14) . . ?
C31 Re3 C33 82.8(2) . . ?
C32 Re3 Re1 138.23(15) . . ?
C32 Re3 Re2 139.42(14) . . ?
C32 Re3 Re3 95.00(15) . 7_565 ?
C32 Re3 Se1 161.71(15) . . ?
C32 Re3 Se2 83.89(15) . . ?
C32 Re3 Se3 84.81(14) . . ?
C32 Re3 C31 80.7(2) . . ?
C32 Re3 C33 80.7(2) . . ?
C33 Re3 Re1 96.48(16) . . ?
C33 Re3 Re2 139.44(16) . . ?
C33 Re3 Re3 138.88(16) . 7_565 ?
C33 Re3 Se1 85.00(16) . . ?
C33 Re3 Se2 84.00(16) . . ?
C33 Re3 Se3 160.74(16) . . ?
Mo2 Mo1 Mo3 60.277(14) . . ?
Se1 Mo1 Mo2 54.797(16) 7_565 . ?
Se1 Mo1 Mo2 54.796(16) . . ?
Se1 Mo1 Mo3 54.374(16) . . ?
Se1 Mo1 Mo3 102.49(2) 7_565 . ?
Se1 Mo1 Se1 107.08(3) . 7_565 ?
Se2 Mo1 Mo2 103.40(3) . . ?
Se2 Mo1 Mo3 54.677(18) . . ?
Se2 Mo1 Se1 105.89(2) . . ?
Se2 Mo1 Se1 105.89(2) . 7_565 ?
C11 Mo1 Mo2 138.26(14) . . ?
C11 Mo1 Mo2 138.26(14) 7_565 . ?
C11 Mo1 Mo3 97.34(15) . . ?
C11 Mo1 Mo3 141.13(14) 7_565 . ?
C11 Mo1 Se1 160.14(15) 7_565 . ?
C11 Mo1 Se1 83.46(15) . . ?
C11 Mo1 Se1 160.13(15) . 7_565 ?
C11 Mo1 Se1 83.46(14) 7_565 7_565 ?
C11 Mo1 Se2 86.60(14) 7_565 . ?
C11 Mo1 Se2 86.60(14) . . ?
C11 Mo1 C11 81.9(3) 7_565 . ?
C12 Mo1 Mo2 94.12(19) . . ?
C12 Mo1 Mo3 138.27(13) . . ?
C12 Mo1 Se1 84.12(12) . 7_565 ?
C12 Mo1 Se1 84.12(12) . . ?
C12 Mo1 Se2 162.48(19) . . ?
C12 Mo1 C11 80.2(2) . 7_565 ?
C12 Mo1 C11 80.2(2) . . ?
Mo1 Mo2 Mo3 60.182(14) . . ?
Se1 Mo2 Mo1 54.862(15) . . ?
Se1 Mo2 Mo1 54.862(15) 7_565 . ?
Se1 Mo2 Mo3 102.46(2) 7_565 . ?
Se1 Mo2 Mo3 54.351(16) . . ?
Se1 Mo2 Se1 107.21(3) . 7_565 ?
Se1 Mo2 Se3 105.66(2) . . ?
Se1 Mo2 Se3 105.66(2) 7_565 . ?
Se3 Mo2 Mo1 102.99(3) . . ?
Se3 Mo2 Mo3 54.423(17) . . ?
C21 Mo2 Mo1 138.03(16) . . ?
C21 Mo2 Mo1 138.03(16) 7_565 . ?
C21 Mo2 Mo3 96.68(15) 7_565 . ?
C21 Mo2 Mo3 140.50(15) . . ?
C21 Mo2 Se1 83.18(16) . 7_565 ?
C21 Mo2 Se1 160.83(15) 7_565 7_565 ?
C21 Mo2 Se1 83.18(16) 7_565 . ?
C21 Mo2 Se1 160.83(15) . . ?
C21 Mo2 Se3 86.24(15) 7_565 . ?
C21 Mo2 Se3 86.24(15) . . ?
C21 Mo2 C21 82.7(3) . 7_565 ?
C21 Mo2 C22 80.7(2) 7_565 . ?
C21 Mo2 C22 80.7(2) . . ?
C22 Mo2 Mo1 94.4(2) . . ?
C22 Mo2 Mo3 138.44(14) . . ?
C22 Mo2 Se1 84.31(12) . . ?
C22 Mo2 Se1 84.31(12) . 7_565 ?
C22 Mo2 Se3 162.6(2) . . ?
Mo1 Mo3 Mo2 59.541(15) . . ?
Se1 Mo3 Mo1 54.651(16) . . ?
Se1 Mo3 Mo2 54.562(16) . . ?
Se1 Mo3 Se2 105.96(2) . . ?
Se1 Mo3 Se3 106.23(2) . . ?
Se2 Mo3 Mo1 54.47(2) . . ?
Se2 Mo3 Mo2 102.632(18) . . ?
Se3 Mo3 Mo1 102.782(19) . . ?
Se3 Mo3 Mo2 54.82(2) . . ?
Se3 Mo3 Se2 107.065(19) . . ?
C31 Mo3 Mo1 140.67(15) . . ?
C31 Mo3 Mo2 96.15(15) . . ?
C31 Mo3 Se1 86.26(15) . . ?
C31 Mo3 Se2 161.14(15) . . ?
C31 Mo3 Se3 82.39(14) . . ?
C31 Mo3 C33 82.8(2) . . ?
C32 Mo3 Mo1 138.23(15) . . ?
C32 Mo3 Mo2 139.42(14) . . ?
C32 Mo3 Se1 161.71(15) . . ?
C32 Mo3 Se2 83.89(15) . . ?
C32 Mo3 Se3 84.81(14) . . ?
C32 Mo3 C31 80.7(2) . . ?
C32 Mo3 C33 80.7(2) . . ?
C33 Mo3 Mo1 96.48(16) . . ?
C33 Mo3 Mo2 139.44(16) . . ?
C33 Mo3 Se1 85.00(16) . . ?
C33 Mo3 Se2 84.00(16) . . ?
C33 Mo3 Se3 160.74(16) . . ?
Re1 Se1 K1 87.38(3) . . ?
Re2 Se1 Re1 70.34(2) . . ?
Re2 Se1 K1 130.11(3) . . ?
Re3 Se1 Re1 70.98(2) . . ?
Re3 Se1 Re2 71.087(19) . . ?
Re3 Se1 K1 142.95(3) . . ?
Mo1 Se1 K1 87.38(3) . . ?
Mo2 Se1 Mo1 70.34(2) . . ?
Mo2 Se1 K1 130.11(3) . . ?
Mo3 Se1 Mo1 70.98(2) . . ?
Mo3 Se1 Mo2 71.087(19) . . ?
Mo3 Se1 K1 142.95(3) . . ?
Re1 Se2 Re3 70.85(2) . . ?
Mo1 Se2 Re3 70.85(2) . 7_565 ?
Mo1 Se2 Mo3 70.85(2) . . ?
Mo1 Se2 K2 170.92(4) . 1_655 ?
Mo3 Se2 Re3 70.19(2) . 7_565 ?
Mo3 Se2 K2 101.87(3) . 1_655 ?
Re3 Se3 Re2 70.76(2) 7_565 . ?
Re3 Se3 Re2 70.76(2) . . ?
Mo2 Se3 K3 83.95(4) . 6_658 ?
Mo3 Se3 Re3 70.32(2) . 7_565 ?
Mo3 Se3 Mo2 70.76(2) . . ?
Mo3 Se3 K3 135.18(3) . 6_658 ?
O1 K1 Se1 104.78(19) . . ?
O1 K1 O5 73.5(2) . 5_557 ?
O1 K1 N11 85.7(2) . 6_557 ?
O1 K1 N11 128.40(19) . . ?
O1 K1 N12 144.4(2) . . ?
O1 K1 C11 136.3(2) . . ?
O1 K1 C11 101.7(2) . 6_557 ?
O1 K1 C12 147.7(2) . . ?
O1 K1 C33 99.7(2) . 6_557 ?
O2 K1 Se1 61.74(13) . . ?
O2 K1 O1 72.8(2) . . ?
O2 K1 O5 111.5(2) . 5_557 ?
O2 K1 N11 125.88(16) . . ?
O2 K1 N11 78.00(17) . 6_557 ?
O2 K1 N12 73.58(19) . . ?
O2 K1 N33 149.88(18) . 6_557 ?
O2 K1 C11 92.74(17) . 6_557 ?
O2 K1 C11 108.56(16) . . ?
O2 K1 C12 76.33(18) . . ?
O2 K1 C33 150.33(17) . 6_557 ?
O5 K1 Se1 72.22(13) 5_557 . ?
O5 K1 N11 55.00(15) 5_557 . ?
O5 K1 C11 151.76(16) 5_557 6_557 ?
O5 K1 C11 65.46(15) 5_557 . ?
O5 K1 C12 110.21(17) 5_557 . ?
O5 K1 C33 92.84(17) 5_557 6_557 ?
N11 K1 Se1 131.88(12) 6_557 . ?
N11 K1 Se1 64.50(9) . . ?
N11 K1 O5 152.49(17) 6_557 5_557 ?
N11 K1 N11 140.78(15) 6_557 . ?
N11 K1 N12 76.28(18) 6_557 . ?
N11 K1 C11 121.81(14) . 6_557 ?
N11 K1 C11 137.94(15) 6_557 . ?
N11 K1 C11 19.06(13) 6_557 6_557 ?
N11 K1 C11 18.92(12) . . ?
N11 K1 C12 97.01(17) 6_557 . ?
N11 K1 C33 72.77(14) 6_557 6_557 ?
N11 K1 C33 81.72(14) . 6_557 ?
N12 K1 Se1 68.23(14) . . ?
N12 K1 O5 130.76(19) . 5_557 ?
N12 K1 N11 81.65(17) . . ?
N12 K1 C11 68.73(17) . 6_557 ?
N12 K1 C11 66.75(17) . . ?
N12 K1 C12 20.78(18) . . ?
N12 K1 C33 103.77(18) . 6_557 ?
N33 K1 Se1 145.34(13) 6_557 . ?
N33 K1 O1 84.0(2) 6_557 . ?
N33 K1 O5 78.66(17) 6_557 5_557 ?
N33 K1 N11 81.49(16) 6_557 6_557 ?
N33 K1 N11 83.59(15) 6_557 . ?
N33 K1 N12 122.35(18) 6_557 . ?
N33 K1 C11 101.46(15) 6_557 . ?
N33 K1 C11 73.14(15) 6_557 6_557 ?
N33 K1 C12 128.31(18) 6_557 . ?
N33 K1 C33 18.70(14) 6_557 6_557 ?
C11 K1 Se1 134.61(10) 6_557 . ?
C11 K1 Se1 49.28(9) . . ?
C11 K1 C11 121.56(16) 6_557 . ?
C11 K1 C33 60.05(14) 6_557 6_557 ?
C12 K1 Se1 50.62(12) . . ?
C12 K1 N11 65.33(15) . . ?
C12 K1 C11 88.91(15) . 6_557 ?
C12 K1 C11 48.26(16) . . ?
C12 K1 C33 111.91(16) . 6_557 ?
C33 K1 Se1 145.88(11) 6_557 . ?
C33 K1 C11 96.69(14) 6_557 . ?
O2 K2 O2 108.9(2) 7_565 . ?
O2 K2 C32 123.95(15) 7_565 1_455 ?
O2 K2 C32 76.78(14) 7_565 7_465 ?
O2 K2 C32 76.78(14) . 1_455 ?
O2 K2 C32 123.94(15) . 7_465 ?
N11 K2 O2 69.96(14) 4_456 7_565 ?
N11 K2 O2 69.96(14) 6_557 . ?
N11 K2 O2 145.62(16) 4_456 . ?
N11 K2 O2 145.62(16) 6_557 7_565 ?
N11 K2 N11 91.7(2) 6_557 4_456 ?
N11 K2 N22 125.02(13) 6_557 . ?
N11 K2 N22 125.02(13) 4_456 . ?
N11 K2 C11 71.61(15) 6_557 4_456 ?
N11 K2 C11 71.61(15) 4_456 6_557 ?
N11 K2 C11 20.31(14) 4_456 4_456 ?
N11 K2 C11 20.31(14) 6_557 6_557 ?
N11 K2 C32 89.89(14) 4_456 7_465 ?
N11 K2 C32 133.82(15) 6_557 7_465 ?
N11 K2 C32 133.82(15) 4_456 1_455 ?
N11 K2 C32 89.89(14) 6_557 1_455 ?
N12 K2 O2 69.25(13) . . ?
N12 K2 O2 69.25(13) . 7_565 ?
N12 K2 N11 79.03(15) . 6_557 ?
N12 K2 N11 79.03(15) . 4_456 ?
N12 K2 N22 71.4(2) . . ?
N12 K2 N32 127.03(15) . 1_455 ?
N12 K2 N32 127.03(15) . 7_465 ?
N12 K2 C11 73.17(17) . 4_456 ?
N12 K2 C11 73.17(17) . 6_557 ?
N12 K2 C32 146.03(13) . 1_455 ?
N12 K2 C32 146.03(13) . 7_465 ?
N22 K2 O2 56.63(11) . 7_565 ?
N22 K2 O2 56.63(11) . . ?
N22 K2 C11 135.73(15) . 6_557 ?
N22 K2 C11 135.73(16) . 4_456 ?
N22 K2 C32 90.00(16) . 7_465 ?
N22 K2 C32 90.00(16) . 1_455 ?
N32 K2 O2 58.61(15) 1_455 . ?
N32 K2 O2 118.37(16) 1_455 7_565 ?
N32 K2 O2 118.37(16) 7_465 . ?
N32 K2 O2 58.61(15) 7_465 7_565 ?
N32 K2 N11 153.79(16) 1_455 4_456 ?
N32 K2 N11 153.79(16) 7_465 6_557 ?
N32 K2 N11 91.06(15) 1_455 6_557 ?
N32 K2 N11 91.06(14) 7_465 4_456 ?
N32 K2 N22 72.96(15) 7_465 . ?
N32 K2 N22 72.96(15) 1_455 . ?
N32 K2 N32 75.5(2) 7_465 1_455 ?
N32 K2 C11 151.29(15) 1_455 4_456 ?
N32 K2 C11 110.27(15) 1_455 6_557 ?
N32 K2 C11 110.27(15) 7_465 4_456 ?
N32 K2 C11 151.29(15) 7_465 6_557 ?
N32 K2 C32 20.13(14) 1_455 1_455 ?
N32 K2 C32 69.70(14) 1_455 7_465 ?
N32 K2 C32 69.70(14) 7_465 1_455 ?
N32 K2 C32 20.13(14) 7_465 7_465 ?
C11 K2 O2 86.45(14) 6_557 . ?
C11 K2 O2 130.05(15) 6_557 7_565 ?
C11 K2 O2 86.45(14) 4_456 7_565 ?
C11 K2 O2 130.05(15) 4_456 . ?
C11 K2 C11 51.4(2) 6_557 4_456 ?
C11 K2 C32 133.52(15) 4_456 1_455 ?
C11 K2 C32 105.62(14) 4_456 7_465 ?
C11 K2 C32 133.52(14) 6_557 7_465 ?
C11 K2 C32 105.62(14) 6_557 1_455 ?
C32 K2 C32 57.85(19) 1_455 7_465 ?
O3 K3 Se3 69.02(11) 1_455 6_558 ?
O3 K3 Se3 69.02(11) 7_465 6_558 ?
O3 K3 O3 116.2(2) 7_465 1_455 ?
O3 K3 N21 64.14(15) 7_465 6_558 ?
O3 K3 N21 136.83(15) 1_455 6_558 ?
O3 K3 N21 64.14(15) 1_455 4_457 ?
O3 K3 N21 136.83(15) 7_465 4_457 ?
O3 K3 N32 140.99(16) 1_455 7_465 ?
O3 K3 N32 74.68(15) 1_455 1_455 ?
O3 K3 N32 140.99(16) 7_465 1_455 ?
O3 K3 N32 74.68(15) 7_465 7_465 ?
O3 K3 C21 115.90(15) 7_465 4_457 ?
O3 K3 C21 115.90(15) 1_455 6_558 ?
O3 K3 C21 71.46(15) 1_455 4_457 ?
O3 K3 C21 71.46(15) 7_465 6_558 ?
O3 K3 C32 141.81(15) 1_455 7_465 ?
O3 K3 C32 141.81(15) 7_465 1_455 ?
O3 K3 C32 89.74(14) 7_465 7_465 ?
O3 K3 C32 89.74(14) 1_455 1_455 ?
N21 K3 Se3 72.12(11) 6_558 6_558 ?
N21 K3 Se3 72.12(11) 4_457 6_558 ?
N21 K3 N21 86.7(2) 6_558 4_457 ?
N21 K3 C21 20.98(14) 4_457 4_457 ?
N21 K3 C21 20.98(14) 6_558 6_558 ?
N21 K3 C21 71.15(15) 6_558 4_457 ?
N21 K3 C21 71.15(15) 4_457 6_558 ?
N21 K3 C32 78.63(14) 6_558 7_465 ?
N21 K3 C32 116.25(15) 4_457 7_465 ?
N21 K3 C32 116.25(15) 6_558 1_455 ?
N21 K3 C32 78.63(14) 4_457 1_455 ?
N22 K3 Se3 102.14(17) . 6_558 ?
N22 K3 O3 72.23(13) . 1_455 ?
N22 K3 O3 72.23(13) . 7_465 ?
N22 K3 N21 135.14(12) . 6_558 ?
N22 K3 N21 135.14(12) . 4_457 ?
N22 K3 N32 76.75(17) . 7_465 ?
N22 K3 N32 76.75(17) . 1_455 ?
N22 K3 C21 142.24(16) . 6_558 ?
N22 K3 C21 142.24(16) . 4_457 ?
N22 K3 C32 91.64(17) . 7_465 ?
N22 K3 C32 91.64(17) . 1_455 ?
N32 K3 Se3 141.91(11) 1_455 6_558 ?
N32 K3 Se3 141.91(11) 7_465 6_558 ?
N32 K3 N21 134.90(17) 1_455 6_558 ?
N32 K3 N21 82.15(15) 1_455 4_457 ?
N32 K3 N21 82.15(14) 7_465 6_558 ?
N32 K3 N21 134.90(17) 7_465 4_457 ?
N32 K3 N32 75.7(2) 1_455 7_465 ?
N32 K3 C21 140.56(16) 7_465 4_457 ?
N32 K3 C21 103.11(15) 1_455 4_457 ?
N32 K3 C21 103.11(15) 7_465 6_558 ?
N32 K3 C21 140.56(16) 1_455 6_558 ?
N32 K3 C32 67.90(14) 1_455 7_465 ?
N32 K3 C32 67.90(14) 7_465 1_455 ?
N32 K3 C32 18.64(14) 1_455 1_455 ?
N32 K3 C32 18.64(14) 7_465 7_465 ?
C21 K3 Se3 54.69(10) 4_457 6_558 ?
C21 K3 Se3 54.69(10) 6_558 6_558 ?
C21 K3 C21 52.8(2) 6_558 4_457 ?
C21 K3 C32 123.84(15) 6_558 1_455 ?
C21 K3 C32 98.21(14) 6_558 7_465 ?
C21 K3 C32 123.84(15) 4_457 7_465 ?
C21 K3 C32 98.21(14) 4_457 1_455 ?
C32 K3 Se3 149.17(9) 1_455 6_558 ?
C32 K3 Se3 149.17(9) 7_465 6_558 ?
C32 K3 C32 55.51(18) 1_455 7_465 ?
O1 K4 K3 106.38(13) 2_455 1_655 ?
O1 K4 C31 106.17(18) 2_455 . ?
O1 K4 C32 141.32(18) 2_455 . ?
O1 K4 K5 113.72(18) 2_455 . ?
O3 K4 K3 42.79(10) . 1_655 ?
O3 K4 O1 93.68(16) . 2_455 ?
O3 K4 O5 67.19(15) . . ?
O3 K4 N31 141.66(15) . . ?
O3 K4 C31 129.07(14) . . ?
O3 K4 C32 88.84(14) . . ?
O3 K4 K5 60.34(16) . . ?
O4 K4 K3 100.84(17) . 1_655 ?
O4 K4 O1 150.6(2) . 2_455 ?
O4 K4 O3 99.0(2) . . ?
O4 K4 O5 95.2(2) . . ?
O4 K4 N31 96.8(2) . . ?
O4 K4 N32 60.8(2) . . ?
O4 K4 C31 86.1(2) . . ?
O4 K4 C32 65.7(2) . . ?
O4 K4 K5 53.3(2) . . ?
O5 K4 K3 109.58(13) . 1_655 ?
O5 K4 O1 65.5(2) . 2_455 ?
O5 K4 N31 145.32(17) . . ?
O5 K4 C31 163.35(16) . . ?
O5 K4 C32 147.28(17) . . ?
O5 K4 K5 48.31(15) . . ?
N21 K4 K3 48.65(13) 4_557 1_655 ?
N21 K4 O1 61.22(19) 4_557 2_455 ?
N21 K4 O3 66.30(16) 4_557 . ?
N21 K4 O4 148.0(2) 4_557 . ?
N21 K4 O5 103.74(18) 4_557 . ?
N21 K4 N31 82.12(16) 4_557 . ?
N21 K4 N32 87.28(17) 4_557 . ?
N21 K4 N33 132.49(18) 4_557 5_557 ?
N21 K4 C31 82.93(16) 4_557 . ?
N21 K4 C32 85.03(16) 4_557 . ?
N21 K4 K5 126.02(18) 4_557 . ?
N31 K4 K3 99.92(11) . 1_655 ?
N31 K4 O1 89.28(18) . 2_455 ?
N31 K4 C31 19.17(13) . . ?
N31 K4 C32 66.41(14) . . ?
N31 K4 K5 149.38(16) . . ?
N32 K4 K3 44.22(11) . 1_655 ?
N32 K4 O1 148.49(18) . 2_455 ?
N32 K4 O3 71.55(14) . . ?
N32 K4 O5 127.61(17) . . ?
N32 K4 N31 86.38(14) . . ?
N32 K4 C31 67.24(14) . . ?
N32 K4 C32 19.97(14) . . ?
N32 K4 K5 83.62(14) . . ?
N33 K4 K3 171.57(13) 5_557 1_655 ?
N33 K4 O1 78.39(17) 5_557 2_455 ?
N33 K4 O3 144.99(16) 5_557 . ?
N33 K4 O4 76.0(2) 5_557 . ?
N33 K4 O5 78.65(17) 5_557 . ?
N33 K4 N31 72.92(15) 5_557 . ?
N33 K4 N32 129.34(16) 5_557 . ?
N33 K4 C31 85.61(15) 5_557 . ?
N33 K4 C32 118.61(16) 5_557 . ?
N33 K4 K5 91.45(17) 5_557 . ?
C31 K4 K3 86.36(10) . 1_655 ?
C31 K4 K5 138.52(14) . . ?
C32 K4 K3 53.38(10) . 1_655 ?
C32 K4 C31 47.28(14) . . ?
C32 K4 K5 100.98(13) . . ?
K5 K4 K3 92.87(12) . 1_655 ?
K1 O1 K4 93.4(2) . 2_454 ?
K1 O2 K2 87.76(17) . . ?
K3 O3 K4 91.17(14) 1_655 . ?
K4 O4 K5 79.7(3) . . ?
C4 O4 K4 144.1(7) . . ?
C4 O4 K5 113.7(6) . . ?
K1 O5 K4 157.7(3) 5_557 . ?
K5 O5 K1 80.7(2) . 5_557 ?
K5 O5 K4 81.4(2) . . ?
K1 N11 K1 150.1(2) 6_657 . ?
K1 N11 K2 90.95(15) 6_657 6_657 ?
K2 N11 K1 116.50(18) 6_657 . ?
C11 N11 K1 103.3(4) . 6_657 ?
C11 N11 K1 87.4(4) . . ?
C11 N11 K2 93.8(4) . 6_657 ?
K1 N12 K1 155.9(3) . 7_565 ?
K2 N12 K1 95.15(14) . . ?
K2 N12 K1 95.15(14) . 7_565 ?
C12 N12 K1 92.56(17) . 7_565 ?
C12 N12 K1 92.56(17) . . ?
C12 N12 K2 142.1(6) . . ?
K4 N21 K3 89.20(16) 4_457 6_658 ?
C21 N21 K3 81.4(4) . 6_658 ?
C21 N21 K4 156.4(5) . 4_457 ?
K3 N22 K2 90.5(2) . . ?
C22 N22 K2 136.3(7) . . ?
C22 N22 K3 133.1(7) . . ?
C31 N31 K4 98.3(4) . . ?
K2 N32 K4 157.9(2) 1_655 . ?
K3 N32 K2 90.57(15) 1_655 1_655 ?
K3 N32 K4 90.65(14) 1_655 . ?
C32 N32 K2 100.5(4) . 1_655 ?
C32 N32 K3 108.5(4) . 1_655 ?
C32 N32 K4 100.1(4) . . ?
K4 N33 K1 104.16(18) 5_557 6_657 ?
C33 N33 K1 110.0(4) . 6_657 ?
C33 N33 K4 133.5(5) . 5_557 ?
Re1 C11 K1 103.31(18) . . ?
Mo1 C11 K1 126.1(2) . 6_657 ?
Mo1 C11 K1 103.31(18) . . ?
Mo1 C11 K2 113.3(2) . 6_657 ?
K1 C11 K1 124.28(18) 6_657 . ?
K2 C11 K1 78.86(12) 6_657 6_657 ?
K2 C11 K1 105.97(15) 6_657 . ?
N11 C11 Re1 176.3(5) . . ?
N11 C11 Mo1 176.3(5) . . ?
N11 C11 K1 73.7(4) . . ?
N11 C11 K1 57.6(4) . 6_657 ?
N11 C11 K2 65.9(4) . 6_657 ?
Re1 C12 K1 112.88(13) . . ?
Mo1 C12 K1 112.88(13) . 7_565 ?
Mo1 C12 K1 112.88(13) . . ?
K1 C12 K1 128.0(2) . 7_565 ?
N12 C12 Re1 177.8(7) . . ?
N12 C12 Mo1 177.8(7) . . ?
N12 C12 K1 66.66(16) . 7_565 ?
N12 C12 K1 66.66(16) . . ?
Mo2 C21 K3 103.3(2) . 6_658 ?
N21 C21 Re2 176.7(5) . . ?
N21 C21 Mo2 176.7(5) . . ?
N21 C21 K3 77.6(4) . 6_658 ?
N22 C22 Re2 179.4(7) . . ?
N22 C22 Mo2 179.4(7) . . ?
Re3 C31 K4 113.5(2) . . ?
Mo3 C31 K4 113.5(2) . . ?
N31 C31 Re3 176.0(5) . . ?
N31 C31 Mo3 176.0(5) . . ?
N31 C31 K4 62.5(4) . . ?
Re3 C32 K4 118.3(2) . . ?
Mo3 C32 K2 121.7(2) . 1_655 ?
Mo3 C32 K3 130.7(2) . 1_655 ?
Mo3 C32 K4 118.3(2) . . ?
K2 C32 K3 75.08(12) 1_655 1_655 ?
K2 C32 K4 118.84(17) 1_655 . ?
K4 C32 K3 75.37(11) . 1_655 ?
N32 C32 Re3 176.1(5) . . ?
N32 C32 Mo3 176.1(5) . . ?
N32 C32 K2 59.4(4) . 1_655 ?
N32 C32 K3 52.9(4) . 1_655 ?
N32 C32 K4 60.0(4) . . ?
Mo3 C33 K1 128.6(2) . 6_657 ?
N33 C33 Re3 177.9(5) . . ?
N33 C33 Mo3 177.9(5) . . ?
N33 C33 K1 51.3(4) . 6_657 ?
O4 K5 K4 47.0(2) . . ?
O5 K5 K4 50.33(17) . . ?
O5 K5 O4 91.4(3) . . ?

_olex2_submission_special_instructions 'No special instructions were received'
_exptl_crystal_preparation       'Magnetic properties'
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_pr913
_database_code_depnum_ccdc_archive 'CCDC 2111043'
loop_
_audit_author_name
_audit_author_address
'Taisiya Sukhikh'
;NIIC SB RAS
Russia
;
_audit_update_record             
;
2021-09-21 deposited with the CCDC.	2021-11-15 downloaded from the CCDC.
;
_audit_creation_date             2021-05-29
_audit_creation_method           
;
Olex2 1.2
(compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506)
;
_shelx_SHELXL_version_number     2017/1
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C12 K6 N12 Re2 Se4 W2, 10(O H2)'
_chemical_formula_sum            'C12 H20 K6 N12 O10 Re2 Se4 W2'
_chemical_formula_weight         1782.9
_chemical_absolute_configuration ad
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
K K 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Re Re -1.0185 7.2310 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Se Se -0.0929 2.2259 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
W W -0.8490 6.8722 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      trigonal
_space_group_IT_number           143
_space_group_name_H-M_alt        'P 3'
_space_group_name_Hall           'P 3'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'

_cell_length_a                   33.1303(10)
_cell_length_b                   33.1303(10)
_cell_length_c                   9.3359(5)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_volume                     8874.4(7)
_cell_formula_units_Z            9
_cell_measurement_reflns_used    9267
_cell_measurement_temperature    150(2)
_cell_measurement_theta_max      25.62
_cell_measurement_theta_min      2.29
_shelx_estimated_absorpt_T_max   0.561
_shelx_estimated_absorpt_T_min   0.193
_exptl_absorpt_coefficient_mu    16.313
_exptl_absorpt_correction_T_max  0.7453
_exptl_absorpt_correction_T_min  0.4137
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
'SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1472 before and 0.0715 after correction. The Ratio of minimum to maximum transmission is 0.5551. The λ/2 correction factor is Not present.'
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            brown
_exptl_crystal_colour_primary    brown
_exptl_crystal_density_diffrn    3.002
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       needle
_exptl_crystal_F_000             7057
_exptl_crystal_size_max          0.15
_exptl_crystal_size_mid          0.04
_exptl_crystal_size_min          0.04
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0705
_diffrn_reflns_av_unetI/netI     0.0410
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.999
_diffrn_reflns_limit_h_max       40
_diffrn_reflns_limit_h_min       -38
_diffrn_reflns_limit_k_max       40
_diffrn_reflns_limit_k_min       -40
_diffrn_reflns_limit_l_max       11
_diffrn_reflns_limit_l_min       -11
_diffrn_reflns_number            159689
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.999
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         25.690
_diffrn_reflns_theta_min         1.229
_diffrn_ambient_temperature      150(2)
_diffrn_detector                 PIXEL
_diffrn_detector_area_resol_mean 7.41
_diffrn_detector_type            'Bruker PHOTON III area detector'
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device       'three-circle diffractometer'
_diffrn_measurement_device_type  'Bruker D8 Venture diffractometer'
_diffrn_measurement_method       'ω and φ scans'
_diffrn_radiation_monochromator  'Incoatec HELIOS multilayer mirrors'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   'Incoatec IuS3.0 microfocus X-ray tube'
_diffrn_special_details          ?
_diffrn_standards_interval_count .
_diffrn_standards_interval_time  .
_diffrn_standards_number         .
_reflns_Friedel_coverage         1.000
_reflns_Friedel_fraction_full    0.999
_reflns_Friedel_fraction_max     0.999
_reflns_number_gt                21355
_reflns_number_total             22473
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'Bruker SAINT'
_computing_data_collection       'Bruker APEX3'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    'ShelXT (Sheldrick, 2015)'
_refine_diff_density_max         2.600
_refine_diff_density_min         -1.727
_refine_diff_density_rms         0.230
_refine_ls_abs_structure_details 
;
 Refined as an inversion twin.
;
_refine_ls_abs_structure_Flack   0.397(10)
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.106
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1289
_refine_ls_number_reflns         22473
_refine_ls_number_restraints     154
_refine_ls_R_factor_all          0.0359
_refine_ls_R_factor_gt           0.0329
_refine_ls_restrained_S_all      1.103
_refine_ls_shift/su_max          0.004
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0105P)²+103.1436P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0649
_refine_ls_wR_factor_ref         0.0661
_refine_special_details          
;
 Refined as a 2-component inversion twin.
;
_olex2_refinement_description    
;
1. Twinned data refinement
 Scales: 0.603(10)
 0.397(10)
2. Shared sites
{W14, Re14}
{W12, Re12}
{W11, Re11}
{W10, Re10}
{W4, Re4}
{W7, Re7}
{W13, Re13}
{W3, Re3}
{W2, Re2}
{W8, Re8}
{W5, Re5}
{W1, Re1}
{W9, Re9}
{W6, Re6}
3. Uiso/Uaniso restraints and constraints
Uanis(C43) \\sim Ueq, Uanis(C22) \\sim Ueq, Uanis(C31) \\sim Ueq, Uanis(C32)
\\sim Ueq, Uanis(C33) \\sim Ueq, Uanis(C42) \\sim Ueq, Uanis(C71) \\sim Ueq,
Uanis(C72) \\sim Ueq, Uanis(C82) \\sim Ueq, Uanis(C62) \\sim Ueq, Uanis(C63)
\\sim Ueq, Uanis(C53) \\sim Ueq, Uanis(C51) \\sim Ueq, Uanis(C91) \\sim Ueq,
Uanis(C133) \\sim Ueq, Uanis(C112) \\sim Ueq, Uanis(C111) \\sim Ueq, Uanis(C83)
\\sim Ueq, Uanis(C41) \\sim Ueq, Uanis(C13) \\sim Ueq: with sigma of 0.001 and
sigma for terminal atoms of 0.001
Uanis(W14) = Uanis(Re14)
Uanis(W12) = Uanis(Re12)
Uanis(W11) = Uanis(Re11)
Uanis(W10) = Uanis(Re10)
Uanis(W4) = Uanis(Re4)
Uanis(W7) = Uanis(Re7)
Uanis(W13) = Uanis(Re13)
Uanis(W3) = Uanis(Re3)
Uanis(W2) = Uanis(Re2)
Uanis(W8) = Uanis(Re8)
Uanis(W5) = Uanis(Re5)
Uanis(W1) = Uanis(Re1)
Uanis(W9) = Uanis(Re9)
Uanis(W6) = Uanis(Re6)
4. Rigid body (RIGU) restrains
 N23, C23
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 N82, C82
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 N21, C21
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 N41, C41
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 N92, C92
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 N13, C13
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 N113, C113
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 N121, C121
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 N131, C131
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 N81, C81
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 N83, C83
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
5. Others
 Sof(Re1)=Sof(Re2)=Sof(Re4)=Sof(Re5)=Sof(Re6)=Sof(Re7)=Sof(Re8)=Sof(Re9)=
 Sof(Re11)=Sof(Re13)=1-FVAR(1)
 Sof(Re10)=Sof(Re12)=Sof(Re14)=0.33333*(1-FVAR(2))
 Sof(W10)=Sof(W12)=0.33333*FVAR(2)
 Sof(W1)=Sof(W2)=Sof(W3)=Sof(W4)=Sof(W5)=Sof(W6)=Sof(W7)=Sof(W8)=Sof(W9)=
 Sof(W11)=Sof(W13)=FVAR(1)
 Fixed Sof: Re3(0.5) W14(0.16667)
;
_atom_sites_solution_hydrogens   .
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Re1 Re 0.74284(2) 1.04451(2) 0.32037(7) 0.01235(14) Uani 0.495(3) 1 d . . . A 2
Re2 Re 0.65548(2) 0.96022(2) 0.32797(7) 0.01027(13) Uani 0.495(3) 1 d . . . A 2
Re3 Re 0.65843(2) 1.04791(2) 0.32443(7) 0.0121(2) Uani 0.5 1 d . . . A 2
Re4 Re 0.68291(2) 1.01526(2) 0.07601(7) 0.01098(14) Uani 0.495(3) 1 d . . . A 2
Re5 Re 1.04699(2) 1.31886(2) -0.13040(7) 0.01095(14) Uani 0.495(3) 1 d . . . A
2
Re6 Re 1.04551(2) 1.40399(2) -0.12749(7) 0.01221(14) Uani 0.495(3) 1 d . . . A
2
Re7 Re 1.01644(2) 1.34538(2) 0.11906(7) 0.01077(14) Uani 0.495(3) 1 d . . . A 2
Re8 Re 0.96009(2) 1.31685(2) -0.13114(7) 0.01177(14) Uani 0.495(3) 1 d . . . A
2
Re9 Re 0.99629(2) 1.04757(2) -0.08630(7) 0.01269(14) Uani 0.495(3) 1 d . . . A
2
Re10 Re 1.000000 1.000000 0.16386(12) 0.0127(2) Uani 0.495(3) 3 d S T P A 2
Re11 Re 0.37939(2) 0.71902(2) 0.23846(7) 0.00821(13) Uani 0.495(3) 1 d . . . A
2
Re12 Re 0.333333 0.666667 -0.01215(12) 0.0078(2) Uani 0.495(3) 3 d S T P A 2
Re13 Re 0.62122(2) 1.28037(2) -0.07370(7) 0.00944(13) Uani 0.495(3) 1 d . . . A
2
Re14 Re 0.666667 1.333333 0.17599(12) 0.0099(3) Uani 0.495(3) 3 d S T P A 2
W1 W 0.74284(2) 1.04451(2) 0.32037(7) 0.01235(14) Uani 0.505(3) 1 d . . . A 1
W2 W 0.65548(2) 0.96022(2) 0.32797(7) 0.01027(13) Uani 0.505(3) 1 d . . . A 1
W3 W 0.65843(2) 1.04791(2) 0.32443(7) 0.0121(2) Uani 0.505(3) 1 d . . . A 1
W4 W 0.68291(2) 1.01526(2) 0.07601(7) 0.01098(14) Uani 0.505(3) 1 d . . . A 1
W5 W 1.04699(2) 1.31886(2) -0.13040(7) 0.01095(14) Uani 0.505(3) 1 d . . . A 1
W6 W 1.04551(2) 1.40399(2) -0.12749(7) 0.01221(14) Uani 0.505(3) 1 d . . . A 1
W7 W 1.01644(2) 1.34538(2) 0.11906(7) 0.01077(14) Uani 0.505(3) 1 d . . . A 1
W8 W 0.96009(2) 1.31685(2) -0.13114(7) 0.01177(14) Uani 0.505(3) 1 d . . . A 1
W9 W 0.99629(2) 1.04757(2) -0.08630(7) 0.01269(14) Uani 0.505(3) 1 d . . . A 1
W10 W 1.000000 1.000000 0.16386(12) 0.0127(2) Uani 0.505(3) 3 d S T P A 1
W11 W 0.37939(2) 0.71902(2) 0.23846(7) 0.00821(13) Uani 0.505(3) 1 d . . . A 1
W12 W 0.333333 0.666667 -0.01215(12) 0.0078(2) Uani 0.505(3) 3 d S T P A 1
W13 W 0.62122(2) 1.28037(2) -0.07370(7) 0.00944(13) Uani 0.505(3) 1 d . . . A 1
W14 W 0.666667 1.333333 0.17599(12) 0.0099(3) Uani 0.5 3 d S T P A 1
Se1 Se 0.68693(6) 1.01888(6) 0.52463(18) 0.0124(3) Uani 1 1 d . . . . .
Se2 Se 0.60362(6) 0.97857(6) 0.18267(18) 0.0128(3) Uani 1 1 d . . . . .
Se3 Se 0.72673(6) 1.09654(6) 0.16918(18) 0.0148(4) Uani 1 1 d . . . . .
Se4 Se 0.72241(6) 0.97413(6) 0.17394(18) 0.0132(3) Uani 1 1 d . . . . .
Se5 Se 1.09749(6) 1.38728(6) 0.02283(18) 0.0139(3) Uani 1 1 d . . . . .
Se6 Se 0.97592(6) 1.38528(6) 0.02003(18) 0.0151(4) Uani 1 1 d . . . . .
Se7 Se 1.01803(6) 1.34758(6) -0.32989(18) 0.0130(4) Uani 1 1 d . . . . .
Se8 Se 0.97806(6) 1.26541(6) 0.01638(18) 0.0135(4) Uani 1 1 d . . . . .
Se9 Se 1.06690(6) 1.07198(6) 0.06395(18) 0.0149(4) Uani 1 1 d . . . . .
Se10 Se 1.000000 1.000000 -0.2860(3) 0.0137(6) Uani 1 3 d S T P . .
Se11 Se 0.59233(6) 1.32298(6) 0.07552(18) 0.0119(3) Uani 1 1 d . . . . .
Se12 Se 0.666667 1.333333 -0.2736(3) 0.0103(6) Uani 1 3 d S T P . .
Se13 Se 0.333333 0.666667 0.4383(3) 0.0080(5) Uani 1 3 d S T P . .
Se14 Se 0.32481(6) 0.73162(6) 0.08834(17) 0.0103(3) Uani 1 1 d . . . . .
K1 K 0.74749(16) 1.13280(15) -0.2312(5) 0.0285(10) Uani 1 1 d . . . . .
K2 K 0.6154(2) 1.1156(2) 0.7392(8) 0.0644(19) Uani 1 1 d . . . . .
K3 K 0.55750(19) 0.95959(17) -0.2376(5) 0.0378(12) Uani 1 1 d . . . . .
K4 K 0.72486(14) 0.84014(14) 0.5015(4) 0.0230(9) Uani 1 1 d . . . . .
K5 K 0.88723(18) 0.99375(16) 0.4666(5) 0.0331(11) Uani 1 1 d . . . . .
K6 K 0.60540(15) 0.84459(15) 0.6931(5) 0.0237(9) Uani 1 1 d . . . . .
K7 K 0.73924(16) 0.95256(15) -0.2295(5) 0.0254(9) Uani 1 1 d . . . . .
K8 K 0.8524(2) 1.0816(2) 0.7579(10) 0.082(3) Uani 1 1 d . . . . .
K9 K 0.98339(18) 1.13764(17) 0.5558(5) 0.0356(11) Uani 1 1 d . . . . .
K10 K 0.95642(16) 1.22884(16) 0.4193(5) 0.0287(10) Uani 1 1 d . . . . .
K11 K 0.59396(14) 0.72945(14) 0.4260(4) 0.0199(8) Uani 1 1 d . . . . .
K12 K 0.84490(15) 1.23922(16) 0.4885(5) 0.0283(10) Uani 1 1 d . . . . .
K13 K 0.68460(16) 1.23730(17) 0.4855(5) 0.0320(11) Uani 1 1 d . . . . .
K14 K 0.44940(19) 1.04152(16) 0.4299(6) 0.0387(12) Uani 1 1 d . . . . .
K15 K 0.53288(15) 1.17377(15) 0.5550(5) 0.0309(10) Uani 1 1 d . . . . .
K16 K 0.41395(19) 0.89223(18) 0.3559(7) 0.0503(15) Uani 1 1 d . . . . .
K17 K 0.47119(15) 0.82730(15) 0.6046(5) 0.0251(9) Uani 1 1 d . . . . .
K18 K 0.44826(15) 0.67940(15) 0.6908(4) 0.0214(9) Uani 1 1 d . . . . .
O1 O 0.8337(7) 1.1546(6) -0.106(2) 0.058(5) Uani 1 1 d . . . . .
O2 O 0.6950(5) 1.1639(5) -0.0727(17) 0.037(4) Uani 1 1 d . . . . .
O3 O 0.7998(5) 1.2289(5) 0.7432(14) 0.023(3) Uani 1 1 d . . . . .
O4 O 0.7607(5) 1.2296(6) 0.3851(18) 0.043(4) Uani 1 1 d . . . . .
O5 O 0.6075(5) 1.1719(5) 0.3195(16) 0.033(3) Uani 1 1 d . . . . .
O7 O 0.5466(6) 1.0953(6) 0.511(2) 0.055(5) Uani 1 1 d . . . . .
O8 O 0.5261(12) 1.1038(12) 0.897(4) 0.143(12) Uiso 1 1 d . . . . .
O9 O 0.4863(6) 0.9864(6) 0.316(2) 0.061(6) Uani 1 1 d . . . . .
O10 O 0.4861(5) 0.8734(5) 0.3277(16) 0.038(4) Uani 1 1 d . . . . .
O11 O 0.5131(5) 0.6864(6) 0.2731(18) 0.040(4) Uani 1 1 d . . . . .
O12 O 0.4756(5) 1.1305(6) 0.3084(16) 0.038(4) Uani 1 1 d . . . . .
O13 O 0.8740(6) 1.2001(5) 0.2600(18) 0.047(4) Uani 1 1 d . . . . .
O14 O 0.9374(7) 1.1544(6) 0.842(2) 0.061(5) Uani 1 1 d . . . . .
O15 O 0.8972(6) 1.1352(6) 0.497(2) 0.056(5) Uani 1 1 d . . . . .
O16 O 1.0115(6) 1.1965(6) 0.2996(17) 0.041(4) Uani 1 1 d . . . . .
O17 O 0.9060(5) 1.0706(5) 0.2932(17) 0.039(4) Uani 1 1 d . . . . .
O18 O 0.8240(7) 0.9965(7) -0.086(3) 0.082(8) Uani 1 1 d . . . . .
O20 O 0.7673(4) 0.8873(5) 0.7481(14) 0.025(3) Uani 1 1 d . . . . .
O21 O 0.7970(6) 0.9221(6) 0.3867(18) 0.051(5) Uani 1 1 d . . . . .
O22 O 0.6731(5) 0.8719(5) -0.0815(14) 0.026(3) Uani 1 1 d . . . . .
O23 O 0.6567(5) 0.8116(5) 0.2779(15) 0.031(3) Uani 1 1 d . . . . .
O24 O 0.5281(6) 0.8650(6) -0.1402(18) 0.049(5) Uani 1 1 d . . . . .
O26 O 0.5327(6) 0.7566(6) 0.7906(19) 0.045(4) Uani 1 1 d . . . . .
O27 O 0.5656(5) 0.7967(4) 0.4450(15) 0.024(3) Uani 1 1 d . . . . .
O28 O 0.5116(10) 0.9802(10) -0.014(3) 0.115(9) Uiso 1 1 d . . . . .
O29 O 0.4606(6) 0.9056(6) 0.651(2) 0.053(5) Uani 1 1 d . . . . .
O30 O 0.3998(5) 0.8302(5) 0.8532(15) 0.029(3) Uani 1 1 d . . . . .
N11 N 0.8028(7) 1.1377(7) 0.5163(18) 0.036(5) Uani 1 1 d . . . . .
N12 N 0.8405(6) 1.0928(8) 0.136(2) 0.047(6) Uani 1 1 d . . . . .
N13 N 0.8018(5) 1.0096(6) 0.5175(17) 0.026(4) Uani 1 1 d . U . . .
N21 N 0.5643(6) 0.9025(6) 0.5369(17) 0.022(3) Uani 1 1 d . U . . .
N22 N 0.6899(5) 0.9017(5) 0.5268(16) 0.018(3) Uani 1 1 d . . . . .
N23 N 0.6044(6) 0.8595(6) 0.1651(18) 0.022(4) Uani 1 1 d . U . . .
N31 N 0.5659(6) 1.0177(6) 0.5244(18) 0.026(4) Uani 1 1 d . . . . .
N32 N 0.6150(6) 1.1042(6) 0.149(2) 0.032(4) Uani 1 1 d . . . . .
N33 N 0.6918(7) 1.1414(6) 0.5243(19) 0.035(4) Uani 1 1 d . . . . .
N41 N 0.6306(6) 0.9291(6) -0.1509(18) 0.030(4) Uani 1 1 d . U . . .
N42 N 0.6418(6) 1.0546(6) -0.1678(19) 0.026(4) Uani 1 1 d . . . . .
N43 N 0.7614(5) 1.0493(6) -0.1777(17) 0.020(3) Uani 1 1 d . . . . .
N51 N 1.0175(5) 1.2291(5) -0.3439(15) 0.016(3) Uani 1 1 d . . . . .
N52 N 1.0991(6) 1.2696(6) 0.0338(17) 0.024(4) Uani 1 1 d . . . . .
N53 N 1.1415(5) 1.3576(6) -0.3284(16) 0.021(4) Uani 1 1 d . . . . .
N61 N 1.0961(6) 1.5040(6) 0.0440(18) 0.035(5) Uani 1 1 d . . . . .
N62 N 1.0086(6) 1.4611(6) -0.3232(19) 0.028(4) Uani 1 1 d . . . . .
N63 N 1.1388(6) 1.4656(5) -0.3287(17) 0.022(4) Uani 1 1 d . . . . .
N71 N 1.0551(5) 1.3002(5) 0.3556(17) 0.021(3) Uani 1 1 d . . . . .
N72 N 0.9305(6) 1.3038(6) 0.3499(17) 0.025(4) Uani 1 1 d . . . . .
N73 N 1.0544(6) 1.4249(5) 0.3696(17) 0.023(4) Uani 1 1 d . . . . .
N81 N 0.8592(6) 1.2619(6) 0.0343(19) 0.028(4) Uani 1 1 d . U . . .
N82 N 0.8981(6) 1.3461(7) -0.3370(19) 0.033(4) Uani 1 1 d . U . . .
N83 N 0.9059(6) 1.2237(5) -0.3329(16) 0.022(3) Uani 1 1 d . U . . .
N91 N 0.9894(6) 1.1311(6) 0.0762(18) 0.030(4) Uani 1 1 d . . . . .
N92 N 1.0643(6) 1.1355(6) -0.2900(16) 0.028(4) Uani 1 1 d . U . . .
N93 N 0.9197(7) 1.0532(7) -0.294(2) 0.037(5) Uani 1 1 d . . . . .
N101 N 0.9977(6) 1.0724(6) 0.3981(17) 0.028(4) Uani 1 1 d . . . . .
N111 N 0.4678(5) 0.7435(6) 0.4478(16) 0.019(3) Uani 1 1 d . . . . .
N112 N 0.4616(5) 0.8102(6) 0.0724(17) 0.021(3) Uani 1 1 d . . . . .
N113 N 0.3808(6) 0.7991(6) 0.4494(18) 0.023(4) Uani 1 1 d . U . . .
N121 N 0.4046(5) 0.7430(5) -0.2470(15) 0.015(3) Uani 1 1 d . U . . .
N131 N 0.6202(5) 1.2007(5) -0.2861(15) 0.016(3) Uani 1 1 d . U . . .
N132 N 0.5435(6) 1.1889(6) 0.0983(17) 0.025(4) Uani 1 1 d . . . . .
N133 N 0.5296(5) 1.2516(5) -0.2756(16) 0.020(3) Uani 1 1 d . . . . .
N141 N 0.7440(6) 1.3407(6) 0.4115(18) 0.026(4) Uani 1 1 d . . . . .
C11 C 0.7800(7) 1.1035(7) 0.449(2) 0.025(5) Uani 1 1 d . . . . .
C12 C 0.8069(7) 1.0757(8) 0.201(2) 0.027(5) Uani 1 1 d . . . . .
C13 C 0.7808(6) 1.0215(6) 0.4495(18) 0.014(3) Uani 1 1 d . U . . .
C21 C 0.5963(7) 0.9240(6) 0.466(2) 0.019(4) Uani 1 1 d . U . . .
C22 C 0.6784(6) 0.9229(6) 0.4583(17) 0.011(3) Uani 1 1 d . U . . .
C23 C 0.6222(6) 0.8947(6) 0.2177(18) 0.011(3) Uani 1 1 d . U . . .
C31 C 0.5979(6) 1.0264(6) 0.4557(19) 0.017(4) Uani 1 1 d . U . . .
C32 C 0.6291(7) 1.0833(7) 0.209(2) 0.020(4) Uani 1 1 d . U . . .
C33 C 0.6824(6) 1.1089(6) 0.4544(19) 0.018(4) Uani 1 1 d . U . . .
C41 C 0.6502(6) 0.9592(6) -0.0688(18) 0.015(3) Uani 1 1 d . U . . .
C42 C 0.6548(6) 1.0414(6) -0.0778(19) 0.014(4) Uani 1 1 d . U . . .
C43 C 0.7359(6) 1.0388(6) -0.0841(19) 0.016(4) Uani 1 1 d . U . . .
C51 C 1.0263(6) 1.2596(6) -0.2671(19) 0.016(4) Uani 1 1 d . U . . .
C52 C 1.0806(7) 1.2881(7) -0.0205(19) 0.022(4) Uani 1 1 d . . . . .
C53 C 1.1082(6) 1.3451(6) -0.2573(17) 0.010(3) Uani 1 1 d . U . . .
C61 C 1.0766(7) 1.4665(7) -0.010(2) 0.023(4) Uani 1 1 d . . . . .
C62 C 1.0208(7) 1.4408(7) -0.257(2) 0.022(4) Uani 1 1 d . U . . .
C63 C 1.1065(6) 1.4433(6) -0.2579(19) 0.016(4) Uani 1 1 d . U . . .
C71 C 1.0422(6) 1.3162(6) 0.2692(17) 0.008(3) Uani 1 1 d . U . . .
C72 C 0.9597(6) 1.3177(6) 0.2691(18) 0.011(3) Uani 1 1 d . U . . .
C73 C 1.0423(6) 1.3981(6) 0.2740(17) 0.013(4) Uani 1 1 d . . . . .
C81 C 0.8958(7) 1.2827(7) -0.0242(19) 0.019(4) Uani 1 1 d . U . . .
C82 C 0.9206(6) 1.3372(6) -0.2643(19) 0.016(4) Uani 1 1 d . U . . .
C83 C 0.9251(6) 1.2557(6) -0.2633(18) 0.013(3) Uani 1 1 d . U . . .
C91 C 0.9916(7) 1.1016(7) 0.023(2) 0.024(4) Uani 1 1 d . U . . .
C92 C 1.0418(6) 1.1046(6) -0.2171(17) 0.016(3) Uani 1 1 d . U . . .
C93 C 0.9463(6) 1.0511(6) -0.2214(18) 0.016(4) Uani 1 1 d . . . . .
C101 C 0.9985(6) 1.0472(7) 0.317(2) 0.023(4) Uani 1 1 d . . . . .
C111 C 0.4364(6) 0.7337(6) 0.3736(17) 0.008(3) Uani 1 1 d . U . . .
C112 C 0.4317(6) 0.7784(6) 0.1288(18) 0.011(3) Uani 1 1 d . U . . .
C113 C 0.3799(6) 0.7713(6) 0.3721(18) 0.012(3) Uani 1 1 d . U . . .
C121 C 0.3795(7) 0.7165(8) -0.162(2) 0.030(5) Uani 1 1 d . U . . .
C131 C 0.6212(6) 1.2297(6) -0.2081(18) 0.013(3) Uani 1 1 d . U . . .
C132 C 0.5711(6) 1.2219(6) 0.0402(19) 0.018(4) Uani 1 1 d . . . . .
C133 C 0.5622(6) 1.2636(6) -0.2021(18) 0.014(4) Uani 1 1 d . U . . .
C141 C 0.7174(6) 1.3389(6) 0.3303(19) 0.012(4) Uani 1 1 d . . . . .
O6 O 0.7672(5) 1.2426(5) 0.0903(15) 0.030(3) Uani 1 1 d . . . . .
O19 O 0.8090(7) 0.9174(6) 0.099(2) 0.069(6) Uani 1 1 d . . . . .
O25 O 0.5280(6) 0.7676(6) 0.085(2) 0.057(5) Uani 1 1 d . . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Re1 Re2 2.8456(9) . ?
Re1 Re3 2.8549(9) . ?
Re1 Re4 2.8570(9) . ?
Re1 Se1 2.4931(18) . ?
Re1 Se3 2.4837(18) . ?
Re1 Se4 2.4871(18) . ?
Re1 C11 2.09(2) . ?
Re1 C12 2.15(2) . ?
Re1 C13 2.140(18) . ?
Re2 Re3 2.8578(9) . ?
Re2 Re4 2.8331(9) . ?
Re2 Se1 2.4915(18) . ?
Re2 Se2 2.4912(18) . ?
Re2 Se4 2.4850(18) . ?
Re2 C21 2.14(2) . ?
Re2 C22 2.128(17) . ?
Re2 C23 2.144(18) . ?
Re3 Re4 2.8433(9) . ?
Re3 Se1 2.4937(18) . ?
Re3 Se2 2.4809(18) . ?
Re3 Se3 2.4841(19) . ?
Re3 C31 2.146(18) . ?
Re3 C32 2.148(19) . ?
Re3 C33 2.140(19) . ?
Re4 Se2 2.4853(18) . ?
Re4 Se3 2.4913(18) . ?
Re4 Se4 2.4876(18) . ?
Re4 C41 2.107(17) . ?
Re4 C42 2.117(18) . ?
Re4 C43 2.134(18) . ?
Re5 Re6 2.8451(9) . ?
Re5 Re7 2.8477(10) . ?
Re5 Re8 2.8463(9) . ?
Re5 Se5 2.4883(18) . ?
Re5 Se7 2.4915(18) . ?
Re5 Se8 2.4868(18) . ?
Re5 C51 2.146(18) . ?
Re5 C52 2.11(2) . ?
Re5 C53 2.122(16) . ?
Re6 Re7 2.8506(10) . ?
Re6 Re8 2.8590(9) . ?
Re6 Se5 2.4889(18) . ?
Re6 Se6 2.4834(19) . ?
Re6 Se7 2.4880(18) . ?
Re6 C61 2.10(2) . ?
Re6 C62 2.15(2) . ?
Re6 C63 2.152(18) . ?
Re7 Re8 2.8409(10) . ?
Re7 Se5 2.4934(18) . ?
Re7 Se6 2.4856(18) . ?
Re7 Se8 2.4871(18) . ?
Re7 C71 2.109(16) . ?
Re7 C72 2.147(17) . ?
Re7 C73 2.094(18) . ?
Re8 Se6 2.4933(19) . ?
Re8 Se7 2.4920(19) . ?
Re8 Se8 2.4840(18) . ?
Re8 C81 2.10(2) . ?
Re8 C82 2.142(18) . ?
Re8 C83 2.150(17) . ?
Re9 Re9 2.8420(12) 2_765 ?
Re9 Re9 2.8420(12) 3_675 ?
Re9 Re10 2.8542(11) . ?
Re9 Se9 2.4860(18) 2_765 ?
Re9 Se9 2.4903(18) . ?
Re9 Se10 2.484(2) . ?
Re9 C91 2.14(2) . ?
Re9 C92 2.119(19) . ?
Re9 C93 2.132(19) . ?
Re10 Se9 2.4866(17) . ?
Re10 Se9 2.4865(17) 2_765 ?
Re10 Se9 2.4865(17) 3_675 ?
Re10 C101 2.14(2) . ?
Re10 C101 2.14(2) 3_675 ?
Re10 C101 2.14(2) 2_765 ?
Re11 Re11 2.8407(11) 3_565 ?
Re11 Re11 2.8407(11) 2_665 ?
Re11 Re12 2.8572(11) . ?
Re11 Se13 2.484(2) . ?
Re11 Se14 2.4826(17) . ?
Re11 Se14 2.4932(17) 3_565 ?
Re11 C111 2.116(16) . ?
Re11 C112 2.125(17) . ?
Re11 C113 2.127(17) . ?
Re12 Se14 2.4895(17) 3_565 ?
Re12 Se14 2.4895(16) . ?
Re12 Se14 2.4895(16) 2_665 ?
Re12 C121 2.12(2) 2_665 ?
Re12 C121 2.12(2) 3_565 ?
Re12 C121 2.12(2) . ?
Re13 Re13 2.8483(11) 2_775 ?
Re13 Re13 2.8482(11) 3_575 ?
Re13 Re14 2.8527(11) . ?
Re13 Se11 2.4831(18) 2_775 ?
Re13 Se11 2.4901(17) . ?
Re13 Se12 2.487(2) . ?
Re13 C131 2.095(17) . ?
Re13 C132 2.104(19) . ?
Re13 C133 2.118(17) . ?
Re14 Se11 2.4935(17) 2_775 ?
Re14 Se11 2.4935(17) 3_575 ?
Re14 Se11 2.4935(17) . ?
Re14 C141 2.152(17) . ?
Re14 C141 2.152(17) 3_575 ?
Re14 C141 2.152(17) 2_775 ?
W1 W2 2.8456(9) . ?
W1 W3 2.8549(9) . ?
W1 W4 2.8570(9) . ?
W1 Se1 2.4931(18) . ?
W1 Se3 2.4837(18) . ?
W1 Se4 2.4871(18) . ?
W1 C11 2.09(2) . ?
W1 C12 2.15(2) . ?
W1 C13 2.140(18) . ?
W2 W3 2.8578(9) . ?
W2 W4 2.8331(9) . ?
W2 Se1 2.4915(18) . ?
W2 Se2 2.4912(18) . ?
W2 Se4 2.4850(18) . ?
W2 C21 2.14(2) . ?
W2 C22 2.128(17) . ?
W2 C23 2.144(18) . ?
W3 W4 2.8433(9) . ?
W3 Se1 2.4937(18) . ?
W3 Se2 2.4809(18) . ?
W3 Se3 2.4841(19) . ?
W3 C31 2.146(18) . ?
W3 C32 2.148(19) . ?
W3 C33 2.140(19) . ?
W4 Se2 2.4853(18) . ?
W4 Se3 2.4913(18) . ?
W4 Se4 2.4876(18) . ?
W4 C41 2.107(17) . ?
W4 C42 2.117(18) . ?
W4 C43 2.134(18) . ?
W5 W6 2.8451(9) . ?
W5 W7 2.8477(10) . ?
W5 W8 2.8463(9) . ?
W5 Se5 2.4883(18) . ?
W5 Se7 2.4915(18) . ?
W5 Se8 2.4868(18) . ?
W5 C51 2.146(18) . ?
W5 C52 2.11(2) . ?
W5 C53 2.122(16) . ?
W6 W7 2.8506(10) . ?
W6 W8 2.8590(9) . ?
W6 Se5 2.4889(18) . ?
W6 Se6 2.4834(19) . ?
W6 Se7 2.4880(18) . ?
W6 C61 2.10(2) . ?
W6 C62 2.15(2) . ?
W6 C63 2.152(18) . ?
W7 W8 2.8409(10) . ?
W7 Se5 2.4934(18) . ?
W7 Se6 2.4856(18) . ?
W7 Se8 2.4871(18) . ?
W7 C71 2.109(16) . ?
W7 C72 2.147(17) . ?
W7 C73 2.094(18) . ?
W8 Se6 2.4933(19) . ?
W8 Se7 2.4920(19) . ?
W8 Se8 2.4840(18) . ?
W8 C81 2.10(2) . ?
W8 C82 2.142(18) . ?
W8 C83 2.150(17) . ?
W9 W10 2.8542(11) . ?
W9 Se9 2.4903(18) . ?
W9 Se9 2.4860(18) 2_765 ?
W9 Se10 2.484(2) . ?
W9 C91 2.14(2) . ?
W9 C92 2.119(19) . ?
W9 C93 2.132(19) . ?
W10 Se9 2.4865(17) 3_675 ?
W10 Se9 2.4866(17) . ?
W10 Se9 2.4865(17) 2_765 ?
W10 C101 2.14(2) 2_765 ?
W10 C101 2.14(2) . ?
W10 C101 2.14(2) 3_675 ?
W11 W12 2.8572(11) . ?
W11 Se13 2.484(2) . ?
W11 Se14 2.4932(17) 3_565 ?
W11 Se14 2.4826(17) . ?
W11 C111 2.116(16) . ?
W11 C112 2.125(17) . ?
W11 C113 2.127(17) . ?
W12 Se14 2.4895(16) 2_665 ?
W12 Se14 2.4895(17) 3_565 ?
W12 Se14 2.4895(16) . ?
W12 C121 2.12(2) . ?
W12 C121 2.12(2) 3_565 ?
W12 C121 2.12(2) 2_665 ?
W13 W14 2.8527(11) . ?
W13 Se11 2.4901(17) . ?
W13 Se11 2.4831(18) 2_775 ?
W13 Se12 2.487(2) . ?
W13 C131 2.095(17) . ?
W13 C132 2.104(19) . ?
W13 C133 2.118(17) . ?
W14 Se11 2.4935(17) . ?
W14 Se11 2.4935(17) 3_575 ?
W14 Se11 2.4935(17) 2_775 ?
W14 C141 2.152(17) . ?
W14 C141 2.152(17) 2_775 ?
W14 C141 2.152(17) 3_575 ?
Se3 K1 3.881(5) . ?
Se4 K7 3.926(5) . ?
Se5 K11 3.918(4) 3_675 ?
Se8 K10 3.906(5) . ?
Se14 K18 3.935(4) 2_664 ?
K1 O1 2.82(2) . ?
K1 O2 2.841(16) . ?
K1 O3 2.772(14) 1_554 ?
K1 N11 2.940(19) 1_554 ?
K1 N33 3.037(19) 1_554 ?
K1 N42 3.201(18) . ?
K1 N43 3.063(16) . ?
K1 C11 3.47(2) 1_554 ?
K1 C33 3.491(19) 1_554 ?
K1 C42 3.369(18) . ?
K1 C43 3.245(18) . ?
K2 K3 4.532(7) 1_556 ?
K2 K13 4.228(8) . ?
K2 K15 4.406(7) . ?
K2 O2 2.893(17) 1_556 ?
K2 O7 2.941(19) . ?
K2 O8 3.15(4) . ?
K2 N31 3.453(18) . ?
K2 N33 3.00(2) . ?
K2 N42 2.716(17) 1_556 ?
K2 N131 2.754(16) 1_556 ?
K3 K17 4.126(6) 1_554 ?
K3 O24 2.922(18) . ?
K3 O28 2.86(3) . ?
K3 O29 2.97(2) 1_554 ?
K3 N21 2.914(17) 1_554 ?
K3 N31 2.861(18) 1_554 ?
K3 N41 3.160(19) . ?
K3 N42 3.057(18) . ?
K3 C21 3.497(19) 1_554 ?
K3 C31 3.454(19) 1_554 ?
K3 C41 3.458(19) . ?
K3 C42 3.351(18) . ?
K4 K6 4.412(6) . ?
K4 K7 4.316(6) 1_556 ?
K4 K11 4.105(6) . ?
K4 O20 2.741(14) . ?
K4 O21 2.784(17) . ?
K4 O23 2.866(16) . ?
K4 N22 2.814(16) . ?
K4 N51 3.157(16) 2_766 ?
K4 N53 2.892(16) 2_766 ?
K4 N71 2.859(16) 2_765 ?
K4 C51 3.478(18) 2_766 ?
K4 C53 3.324(17) 2_766 ?
K5 K8 4.533(8) . ?
K5 K9 4.287(7) . ?
K5 O17 2.812(16) . ?
K5 O21 2.833(18) . ?
K5 N13 3.163(17) . ?
K5 N92 2.955(17) 2_766 ?
K5 N93 2.815(19) 1_556 ?
K5 N101 3.325(19) . ?
K5 N101 3.221(18) 2_765 ?
K5 C93 3.493(19) 1_556 ?
K5 C101 3.420(19) 2_765 ?
K5 C101 3.484(19) . ?
K6 K7 4.137(6) 1_556 ?
K6 K17 4.270(6) . ?
K6 O22 2.872(15) 1_556 ?
K6 O24 3.343(18) 1_556 ?
K6 O26 2.847(17) . ?
K6 O27 2.745(14) . ?
K6 N21 3.205(17) . ?
K6 N22 2.921(16) . ?
K6 N41 2.883(17) 1_556 ?
K6 N53 2.838(16) 2_766 ?
K6 C21 3.509(19) . ?
K6 C22 3.333(17) . ?
K7 K8 4.039(8) 1_554 ?
K7 O18 2.779(19) . ?
K7 O20 2.756(14) 1_554 ?
K7 O22 2.829(14) . ?
K7 N13 3.086(17) 1_554 ?
K7 N22 2.816(16) 1_554 ?
K7 N41 3.36(2) . ?
K7 N43 2.949(16) . ?
K7 C22 3.397(17) 1_554 ?
K7 C41 3.413(18) . ?
K7 C43 3.216(18) . ?
K8 K9 4.217(8) . ?
K8 O1 3.06(2) 1_556 ?
K8 O14 2.751(19) . ?
K8 O15 2.94(2) . ?
K8 O18 2.88(2) 1_556 ?
K8 N13 3.089(18) . ?
K8 N43 2.715(17) 1_556 ?
K8 N93 2.86(2) 1_556 ?
K9 K10 3.775(7) . ?
K9 O14 3.26(2) . ?
K9 O15 2.87(2) . ?
K9 O16 2.929(18) . ?
K9 N51 2.814(15) 1_556 ?
K9 N92 3.076(18) 1_556 ?
K9 N93 2.89(2) 1_556 ?
K9 N101 2.843(18) . ?
K9 C92 3.398(17) 1_556 ?
K9 C93 3.246(17) 1_556 ?
K10 O13 2.824(19) . ?
K10 O15 2.813(18) . ?
K10 O16 2.773(17) . ?
K10 N51 2.993(15) 1_556 ?
K10 N71 2.984(16) . ?
K10 N72 3.075(18) . ?
K10 N83 2.810(16) 1_556 ?
K10 C71 3.193(17) . ?
K10 C72 3.212(17) . ?
K10 C83 3.403(17) 1_556 ?
K11 O11 2.725(15) . ?
K11 O23 2.826(15) . ?
K11 O27 2.824(14) . ?
K11 N53 2.863(16) 2_766 ?
K11 N63 2.989(16) 2_766 ?
K11 N71 3.237(16) 2_765 ?
K11 N73 3.091(17) 2_765 ?
K11 C53 3.437(16) 2_766 ?
K11 C63 3.512(18) 2_766 ?
K11 C71 3.369(17) 2_765 ?
K11 C73 3.287(17) 2_765 ?
K12 K14 4.966(7) 2_775 ?
K12 K15 4.359(7) 2_775 ?
K12 O3 2.737(14) . ?
K12 O4 2.816(16) . ?
K12 O13 2.901(19) . ?
K12 N11 2.94(2) . ?
K12 N72 2.869(18) . ?
K12 N83 2.858(18) 1_556 ?
K12 C83 3.357(17) 1_556 ?
K13 O4 2.818(15) . ?
K13 O5 2.844(16) . ?
K13 N33 3.322(19) . ?
K13 N131 2.825(15) 1_556 ?
K13 N133 2.901(16) 2_776 ?
K13 N141 3.339(17) 3_575 ?
K13 N141 3.055(18) . ?
K13 C131 3.483(18) 1_556 ?
K13 C133 3.478(18) 2_776 ?
K13 C141 3.445(18) 3_575 ?
K13 C141 3.308(18) . ?
K14 K15 4.012(6) . ?
K14 O7 2.894(19) . ?
K14 O9 2.86(2) . ?
K14 O12 2.857(17) . ?
K14 N62 2.872(18) 3_576 ?
K14 N72 3.179(17) 3_575 ?
K14 N73 2.991(17) 3_575 ?
K14 N82 2.972(19) 3_576 ?
K14 C62 3.42(2) 3_576 ?
K14 C72 3.364(17) 3_575 ?
K14 C73 3.291(17) 3_575 ?
K14 C82 3.504(18) 3_576 ?
K15 O5 3.332(16) . ?
K15 O7 2.883(16) . ?
K15 O12 2.870(16) . ?
K15 N82 2.811(17) 3_576 ?
K15 N131 2.964(16) 1_556 ?
K15 N133 3.072(16) 1_556 ?
K15 N141 2.816(18) 3_575 ?
K15 C131 3.385(17) 1_556 ?
K15 C133 3.472(18) 1_556 ?
K16 K17 4.207(7) . ?
K16 K18 4.838(7) 2_665 ?
K16 O9 2.852(18) . ?
K16 O10 2.769(16) . ?
K16 O11 3.024(18) 2_665 ?
K16 O29 3.08(2) . ?
K16 N61 2.957(18) 3_575 ?
K16 N73 2.787(17) 3_575 ?
K16 N113 2.845(18) . ?
K17 O10 2.916(16) . ?
K17 O24 2.904(19) 1_556 ?
K17 O29 2.820(17) . ?
K17 O30 3.349(16) . ?
K17 N21 2.905(17) . ?
K17 N111 3.092(17) . ?
K17 N113 3.023(17) . ?
K17 N121 2.903(15) 1_556 ?
K17 C111 3.468(16) . ?
K17 C113 3.419(17) . ?
K18 O26 2.842(17) . ?
K18 O30 2.824(15) 3_565 ?
K18 N63 2.968(16) 2_766 ?
K18 N111 2.950(16) . ?
K18 N113 2.841(17) 3_565 ?
K18 N121 3.347(16) 3_566 ?
K18 N121 3.148(15) 1_556 ?
K18 C121 3.38(2) 1_556 ?
K18 C121 3.48(2) 3_566 ?
N11 C11 1.18(3) . ?
N12 C12 1.14(3) . ?
N13 C13 1.15(2) . ?
N21 C21 1.15(2) . ?
N22 C22 1.15(2) . ?
N23 C23 1.12(2) . ?
N31 C31 1.14(2) . ?
N32 C32 1.16(2) . ?
N33 C33 1.16(2) . ?
N41 C41 1.16(2) . ?
N42 C42 1.13(2) . ?
N43 C43 1.14(2) . ?
N51 C51 1.15(2) . ?
N52 C52 1.18(2) . ?
N53 C53 1.17(2) . ?
N61 C61 1.19(3) . ?
N62 C62 1.13(2) . ?
N63 C63 1.16(2) . ?
N71 C71 1.16(2) . ?
N72 C72 1.13(2) . ?
N73 C73 1.18(2) . ?
N81 C81 1.19(3) . ?
N82 C82 1.15(2) . ?
N83 C83 1.13(2) . ?
N91 C91 1.13(2) . ?
N92 C92 1.14(2) . ?
N93 C93 1.14(2) . ?
N101 C101 1.14(3) . ?
N111 C111 1.15(2) . ?
N112 C112 1.15(2) . ?
N113 C113 1.16(2) . ?
N121 C121 1.17(2) . ?
N131 C131 1.19(2) . ?
N132 C132 1.15(2) . ?
N133 C133 1.17(2) . ?
N141 C141 1.14(2) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Re2 Re1 Re3 60.18(2) . . ?
Re2 Re1 Re4 59.58(2) . . ?
Re3 Re1 Re4 59.71(2) . . ?
Se1 Re1 Re2 55.16(4) . . ?
Se1 Re1 Re3 55.09(4) . . ?
Se1 Re1 Re4 102.90(5) . . ?
Se3 Re1 Re2 103.25(5) . . ?
Se3 Re1 Re3 54.93(4) . . ?
Se3 Re1 Re4 55.08(4) . . ?
Se3 Re1 Se1 106.87(6) . . ?
Se3 Re1 Se4 106.62(6) . . ?
Se4 Re1 Re2 55.05(4) . . ?
Se4 Re1 Re3 103.38(5) . . ?
Se4 Re1 Re4 54.96(4) . . ?
Se4 Re1 Se1 107.07(6) . . ?
C11 Re1 Re2 137.5(5) . . ?
C11 Re1 Re3 95.0(6) . . ?
C11 Re1 Re4 139.6(6) . . ?
C11 Re1 Se1 82.4(5) . . ?
C11 Re1 Se3 84.8(6) . . ?
C11 Re1 Se4 161.6(6) . . ?
C11 Re1 C12 82.5(8) . . ?
C11 Re1 C13 80.4(7) . . ?
C12 Re1 Re2 139.5(6) . . ?
C12 Re1 Re3 137.7(6) . . ?
C12 Re1 Re4 95.9(5) . . ?
C12 Re1 Se1 161.2(5) . . ?
C12 Re1 Se3 82.9(6) . . ?
C12 Re1 Se4 84.7(6) . . ?
C13 Re1 Re2 97.3(5) . . ?
C13 Re1 Re3 140.3(5) . . ?
C13 Re1 Re4 139.6(5) . . ?
C13 Re1 Se1 85.2(5) . . ?
C13 Re1 Se3 159.5(5) . . ?
C13 Re1 Se4 84.7(5) . . ?
C13 Re1 C12 81.2(7) . . ?
Re1 Re2 Re3 60.07(2) . . ?
Re4 Re2 Re1 60.41(2) . . ?
Re4 Re2 Re3 59.95(2) . . ?
Se1 Re2 Re1 55.21(4) . . ?
Se1 Re2 Re3 55.06(4) . . ?
Se1 Re2 Re4 103.62(5) . . ?
Se2 Re2 Re1 103.54(5) . . ?
Se2 Re2 Re3 54.75(4) . . ?
Se2 Re2 Re4 55.20(4) . . ?
Se2 Re2 Se1 106.34(6) . . ?
Se4 Re2 Re1 55.12(4) . . ?
Se4 Re2 Re3 103.36(5) . . ?
Se4 Re2 Re4 55.31(4) . . ?
Se4 Re2 Se1 107.18(6) . . ?
Se4 Re2 Se2 107.46(6) . . ?
C21 Re2 Re1 139.6(5) . . ?
C21 Re2 Re3 97.6(5) . . ?
C21 Re2 Re4 140.2(5) . . ?
C21 Re2 Se1 84.4(5) . . ?
C21 Re2 Se2 85.1(5) . . ?
C21 Re2 Se4 159.0(5) . . ?
C21 Re2 C23 81.9(6) . . ?
C22 Re2 Re1 95.8(4) . . ?
C22 Re2 Re3 139.2(4) . . ?
C22 Re2 Re4 139.1(4) . . ?
C22 Re2 Se1 84.3(4) . . ?
C22 Re2 Se2 160.6(5) . . ?
C22 Re2 Se4 83.9(4) . . ?
C22 Re2 C21 79.9(7) . . ?
C22 Re2 C23 80.7(6) . . ?
C23 Re2 Re1 137.5(4) . . ?
C23 Re2 Re3 139.7(4) . . ?
C23 Re2 Re4 95.2(4) . . ?
C23 Re2 Se1 161.2(4) . . ?
C23 Re2 Se2 85.3(4) . . ?
C23 Re2 Se4 82.5(4) . . ?
Re1 Re3 Re2 59.75(2) . . ?
Re4 Re3 Re1 60.18(2) . . ?
Re4 Re3 Re2 59.60(2) . . ?
Se1 Re3 Re1 55.07(4) . . ?
Se1 Re3 Re2 54.99(4) . . ?
Se1 Re3 Re4 103.27(5) . . ?
Se2 Re3 Re1 103.55(5) . . ?
Se2 Re3 Re2 55.09(4) . . ?
Se2 Re3 Re4 55.14(4) . . ?
Se2 Re3 Se1 106.59(6) . . ?
Se2 Re3 Se3 107.27(6) . . ?
Se3 Re3 Re1 54.92(4) . . ?
Se3 Re3 Re2 102.89(5) . . ?
Se3 Re3 Re4 55.27(4) . . ?
Se3 Re3 Se1 106.84(6) . . ?
C31 Re3 Re1 140.0(5) . . ?
C31 Re3 Re2 96.0(5) . . ?
C31 Re3 Re4 137.4(5) . . ?
C31 Re3 Se1 85.1(5) . . ?
C31 Re3 Se2 82.4(5) . . ?
C31 Re3 Se3 161.1(5) . . ?
C31 Re3 C32 82.3(7) . . ?
C32 Re3 Re1 137.2(5) . . ?
C32 Re3 Re2 140.0(5) . . ?
C32 Re3 Re4 95.2(5) . . ?
C32 Re3 Se1 161.4(5) . . ?
C32 Re3 Se2 85.2(5) . . ?
C32 Re3 Se3 82.4(5) . . ?
C33 Re3 Re1 97.8(5) . . ?
C33 Re3 Re2 139.5(5) . . ?
C33 Re3 Re4 141.3(5) . . ?
C33 Re3 Se1 84.6(5) . . ?
C33 Re3 Se2 158.6(5) . . ?
C33 Re3 Se3 86.0(5) . . ?
C33 Re3 C31 80.4(7) . . ?
C33 Re3 C32 79.9(7) . . ?
Re2 Re4 Re1 60.01(2) . . ?
Re2 Re4 Re3 60.46(2) . . ?
Re3 Re4 Re1 60.11(2) . . ?
Se2 Re4 Re1 103.37(5) . . ?
Se2 Re4 Re2 55.40(4) . . ?
Se2 Re4 Re3 55.00(4) . . ?
Se2 Re4 Se3 106.91(6) . . ?
Se2 Re4 Se4 107.56(6) . . ?
Se3 Re4 Re1 54.83(4) . . ?
Se3 Re4 Re2 103.40(5) . . ?
Se3 Re4 Re3 55.03(4) . . ?
Se4 Re4 Re1 54.94(4) . . ?
Se4 Re4 Re2 55.22(4) . . ?
Se4 Re4 Re3 103.70(5) . . ?
Se4 Re4 Se3 106.37(6) . . ?
C41 Re4 Re1 140.8(5) . . ?
C41 Re4 Re2 96.1(5) . . ?
C41 Re4 Re3 137.7(5) . . ?
C41 Re4 Se2 82.8(5) . . ?
C41 Re4 Se3 160.4(5) . . ?
C41 Re4 Se4 86.1(5) . . ?
C41 Re4 C42 77.8(7) . . ?
C41 Re4 C43 80.8(7) . . ?
C42 Re4 Re1 140.9(5) . . ?
C42 Re4 Re2 139.6(5) . . ?
C42 Re4 Re3 97.5(5) . . ?
C42 Re4 Se2 84.2(5) . . ?
C42 Re4 Se3 86.1(5) . . ?
C42 Re4 Se4 158.8(5) . . ?
C42 Re4 C43 79.9(7) . . ?
C43 Re4 Re1 97.5(5) . . ?
C43 Re4 Re2 139.2(5) . . ?
C43 Re4 Re3 140.4(5) . . ?
C43 Re4 Se2 159.1(5) . . ?
C43 Re4 Se3 85.5(5) . . ?
C43 Re4 Se4 84.0(5) . . ?
Re6 Re5 Re7 60.10(2) . . ?
Re6 Re5 Re8 60.31(2) . . ?
Re8 Re5 Re7 59.86(2) . . ?
Se5 Re5 Re6 55.15(4) . . ?
Se5 Re5 Re7 55.22(4) . . ?
Se5 Re5 Re8 103.55(5) . . ?
Se5 Re5 Se7 107.08(6) . . ?
Se7 Re5 Re6 55.10(4) . . ?
Se7 Re5 Re7 103.26(5) . . ?
Se7 Re5 Re8 55.18(4) . . ?
Se8 Re5 Re6 103.64(5) . . ?
Se8 Re5 Re7 55.08(4) . . ?
Se8 Re5 Re8 55.02(4) . . ?
Se8 Re5 Se5 106.96(6) . . ?
Se8 Re5 Se7 106.98(6) . . ?
C51 Re5 Re6 139.1(5) . . ?
C51 Re5 Re7 140.2(5) . . ?
C51 Re5 Re8 96.9(5) . . ?
C51 Re5 Se5 159.5(5) . . ?
C51 Re5 Se7 84.1(5) . . ?
C51 Re5 Se8 85.2(5) . . ?
C52 Re5 Re6 138.4(5) . . ?
C52 Re5 Re7 96.1(5) . . ?
C52 Re5 Re8 139.5(5) . . ?
C52 Re5 Se5 83.3(5) . . ?
C52 Re5 Se7 160.7(5) . . ?
C52 Re5 Se8 84.6(5) . . ?
C52 Re5 C51 81.5(7) . . ?
C52 Re5 C53 81.0(7) . . ?
C53 Re5 Re6 94.9(4) . . ?
C53 Re5 Re7 138.1(4) . . ?
C53 Re5 Re8 139.1(4) . . ?
C53 Re5 Se5 83.0(4) . . ?
C53 Re5 Se7 84.1(4) . . ?
C53 Re5 Se8 161.5(4) . . ?
C53 Re5 C51 81.1(6) . . ?
Re5 Re6 Re7 60.00(2) . . ?
Re5 Re6 Re8 59.87(2) . . ?
Re7 Re6 Re8 59.68(2) . . ?
Se5 Re6 Re5 55.13(4) . . ?
Se5 Re6 Re7 55.18(4) . . ?
Se5 Re6 Re8 103.17(5) . . ?
Se6 Re6 Re5 103.40(5) . . ?
Se6 Re6 Re7 55.03(4) . . ?
Se6 Re6 Re8 55.10(5) . . ?
Se6 Re6 Se5 106.92(6) . . ?
Se6 Re6 Se7 106.76(6) . . ?
Se7 Re6 Re5 55.21(4) . . ?
Se7 Re6 Re7 103.27(5) . . ?
Se7 Re6 Re8 55.03(4) . . ?
Se7 Re6 Se5 107.18(6) . . ?
C61 Re6 Re5 137.7(5) . . ?
C61 Re6 Re7 94.8(5) . . ?
C61 Re6 Re8 138.7(5) . . ?
C61 Re6 Se5 82.7(5) . . ?
C61 Re6 Se6 83.9(5) . . ?
C61 Re6 Se7 161.9(5) . . ?
C61 Re6 C62 82.7(7) . . ?
C61 Re6 C63 81.3(7) . . ?
C62 Re6 Re5 139.2(5) . . ?
C62 Re6 Re7 138.3(5) . . ?
C62 Re6 Re8 95.8(5) . . ?
C62 Re6 Se5 161.0(5) . . ?
C62 Re6 Se6 83.4(5) . . ?
C62 Re6 Se7 84.1(5) . . ?
C63 Re6 Re5 96.8(5) . . ?
C63 Re6 Re7 139.8(5) . . ?
C63 Re6 Re8 139.5(5) . . ?
C63 Re6 Se5 84.8(5) . . ?
C63 Re6 Se6 159.8(5) . . ?
C63 Re6 Se7 84.5(5) . . ?
C63 Re6 C62 81.2(7) . . ?
Re5 Re7 Re6 59.91(2) . . ?
Re8 Re7 Re5 60.05(2) . . ?
Re8 Re7 Re6 60.31(2) . . ?
Se5 Re7 Re5 55.05(4) . . ?
Se5 Re7 Re6 55.03(4) . . ?
Se5 Re7 Re8 103.57(5) . . ?
Se6 Re7 Re5 103.27(5) . . ?
Se6 Re7 Re6 54.96(5) . . ?
Se6 Re7 Re8 55.34(5) . . ?
Se6 Re7 Se5 106.71(6) . . ?
Se6 Re7 Se8 107.38(6) . . ?
Se8 Re7 Re5 55.07(4) . . ?
Se8 Re7 Re6 103.47(5) . . ?
Se8 Re7 Re8 55.10(4) . . ?
Se8 Re7 Se5 106.79(6) . . ?
C71 Re7 Re5 96.6(4) . . ?
C71 Re7 Re6 140.6(4) . . ?
C71 Re7 Re8 138.0(4) . . ?
C71 Re7 Se5 85.7(4) . . ?
C71 Re7 Se6 160.1(4) . . ?
C71 Re7 Se8 82.9(4) . . ?
C71 Re7 C72 80.7(6) . . ?
C72 Re7 Re5 140.5(4) . . ?
C72 Re7 Re6 138.0(4) . . ?
C72 Re7 Re8 96.0(4) . . ?
C72 Re7 Se5 160.3(5) . . ?
C72 Re7 Se6 83.1(4) . . ?
C72 Re7 Se8 85.6(4) . . ?
C73 Re7 Re5 139.7(5) . . ?
C73 Re7 Re6 97.5(5) . . ?
C73 Re7 Re8 140.6(5) . . ?
C73 Re7 Se5 84.7(5) . . ?
C73 Re7 Se6 85.3(5) . . ?
C73 Re7 Se8 159.0(5) . . ?
C73 Re7 C71 80.4(6) . . ?
C73 Re7 C72 79.2(6) . . ?
Re5 Re8 Re6 59.82(2) . . ?
Re7 Re8 Re5 60.10(2) . . ?
Re7 Re8 Re6 60.01(2) . . ?
Se6 Re8 Re5 103.11(5) . . ?
Se6 Re8 Re6 54.77(5) . . ?
Se6 Re8 Re7 55.08(4) . . ?
Se7 Re8 Re5 55.16(4) . . ?
Se7 Re8 Re6 54.90(4) . . ?
Se7 Re8 Re7 103.44(5) . . ?
Se7 Re8 Se6 106.33(6) . . ?
Se8 Re8 Re5 55.12(4) . . ?
Se8 Re8 Re6 103.31(5) . . ?
Se8 Re8 Re7 55.20(4) . . ?
Se8 Re8 Se6 107.23(6) . . ?
Se8 Re8 Se7 107.05(6) . . ?
C81 Re8 Re5 138.9(5) . . ?
C81 Re8 Re6 139.8(5) . . ?
C81 Re8 Re7 96.3(5) . . ?
C81 Re8 Se6 85.2(5) . . ?
C81 Re8 Se7 160.3(5) . . ?
C81 Re8 Se8 83.9(5) . . ?
C81 Re8 C82 80.2(7) . . ?
C81 Re8 C83 80.9(7) . . ?
C82 Re8 Re5 139.8(5) . . ?
C82 Re8 Re6 98.1(5) . . ?
C82 Re8 Re7 140.8(5) . . ?
C82 Re8 Se6 85.8(5) . . ?
C82 Re8 Se7 84.6(5) . . ?
C82 Re8 Se8 158.5(5) . . ?
C82 Re8 C83 80.6(7) . . ?
C83 Re8 Re5 95.0(4) . . ?
C83 Re8 Re6 138.9(5) . . ?
C83 Re8 Re7 137.8(4) . . ?
C83 Re8 Se6 161.9(5) . . ?
C83 Re8 Se7 84.3(5) . . ?
C83 Re8 Se8 82.7(4) . . ?
Re9 Re9 Re10 60.142(15) 3_675 . ?
Re9 Re9 Re10 60.142(15) 2_765 . ?
Se9 Re9 Re9 103.31(4) . 2_765 ?
Se9 Re9 Re9 103.42(4) 2_765 3_675 ?
Se9 Re9 Re9 55.24(5) 2_765 2_765 ?
Se9 Re9 Re9 55.10(5) . 3_675 ?
Se9 Re9 Re10 54.98(4) 2_765 . ?
Se9 Re9 Re10 54.95(4) . . ?
Se9 Re9 Se9 106.70(8) 2_765 . ?
Se10 Re9 Re9 55.10(4) . 3_675 ?
Se10 Re9 Re9 55.10(4) . 2_765 ?
Se10 Re9 Re10 103.56(5) . . ?
Se10 Re9 Se9 107.14(5) . 2_765 ?
Se10 Re9 Se9 107.00(5) . . ?
C91 Re9 Re9 139.7(5) . 3_675 ?
C91 Re9 Re9 139.2(5) . 2_765 ?
C91 Re9 Re10 96.4(5) . . ?
C91 Re9 Se9 84.0(5) . 2_765 ?
C91 Re9 Se9 84.7(5) . . ?
C91 Re9 Se10 160.0(5) . . ?
C92 Re9 Re9 96.0(5) . 3_675 ?
C92 Re9 Re9 138.9(4) . 2_765 ?
C92 Re9 Re10 139.2(5) . . ?
C92 Re9 Se9 160.6(5) . 2_765 ?
C92 Re9 Se9 84.3(5) . . ?
C92 Re9 Se10 84.0(4) . . ?
C92 Re9 C91 81.1(7) . . ?
C92 Re9 C93 80.5(6) . . ?
C93 Re9 Re9 95.7(5) . 2_765 ?
C93 Re9 Re9 138.0(5) . 3_675 ?
C93 Re9 Re10 139.8(5) . . ?
C93 Re9 Se9 160.9(5) . . ?
C93 Re9 Se9 85.0(5) . 2_765 ?
C93 Re9 Se10 82.9(5) . . ?
C93 Re9 C91 81.6(7) . . ?
Re9 Re10 Re9 59.72(3) 2_765 . ?
Se9 Re10 Re9 54.96(4) 3_675 2_765 ?
Se9 Re10 Re9 55.06(4) 3_675 3_675 ?
Se9 Re10 Re9 103.06(5) 2_765 3_675 ?
Se9 Re10 Re9 54.96(4) 2_765 . ?
Se9 Re10 Re9 103.06(5) 3_675 . ?
Se9 Re10 Re9 55.06(4) 2_765 2_765 ?
Se9 Re10 Re9 55.07(4) . . ?
Se9 Re10 Re9 54.96(4) . 3_675 ?
Se9 Re10 Re9 103.06(5) . 2_765 ?
Se9 Re10 Se9 106.79(5) 2_765 . ?
Se9 Re10 Se9 106.79(5) 3_675 . ?
Se9 Re10 Se9 106.79(5) 2_765 3_675 ?
C101 Re10 Re9 97.0(5) 3_675 3_675 ?
C101 Re10 Re9 97.0(5) . . ?
C101 Re10 Re9 138.4(5) . 3_675 ?
C101 Re10 Re9 97.0(5) 2_765 2_765 ?
C101 Re10 Re9 138.4(5) 2_765 . ?
C101 Re10 Re9 140.8(5) 3_675 . ?
C101 Re10 Re9 140.8(5) 2_765 3_675 ?
C101 Re10 Re9 138.4(5) 3_675 2_765 ?
C101 Re10 Re9 140.8(5) . 2_765 ?
C101 Re10 Se9 85.9(5) . 2_765 ?
C101 Re10 Se9 159.9(5) . 3_675 ?
C101 Re10 Se9 83.4(5) 2_765 2_765 ?
C101 Re10 Se9 85.9(5) 3_675 . ?
C101 Re10 Se9 83.4(5) . . ?
C101 Re10 Se9 159.9(5) 3_675 2_765 ?
C101 Re10 Se9 85.9(5) 2_765 3_675 ?
C101 Re10 Se9 83.4(5) 3_675 3_675 ?
C101 Re10 Se9 159.9(5) 2_765 . ?
C101 Re10 C101 80.0(7) 3_675 . ?
C101 Re10 C101 80.0(7) 2_765 . ?
C101 Re10 C101 80.0(7) 3_675 2_765 ?
Re11 Re11 Re11 60.0 3_565 2_665 ?
Re11 Re11 Re12 60.190(14) 3_565 . ?
Re11 Re11 Re12 60.189(14) 2_665 . ?
Se13 Re11 Re11 55.12(3) . 3_565 ?
Se13 Re11 Re11 55.12(4) . 2_665 ?
Se13 Re11 Re12 103.64(5) . . ?
Se13 Re11 Se14 106.91(5) . 3_565 ?
Se14 Re11 Re11 55.36(4) . 2_665 ?
Se14 Re11 Re11 55.01(4) 3_565 3_565 ?
Se14 Re11 Re11 103.54(4) . 3_565 ?
Se14 Re11 Re11 103.26(4) 3_565 2_665 ?
Se14 Re11 Re12 55.04(4) . . ?
Se14 Re11 Re12 54.95(4) 3_565 . ?
Se14 Re11 Se13 107.25(5) . . ?
Se14 Re11 Se14 106.78(8) . 3_565 ?
C111 Re11 Re11 138.1(4) . 2_665 ?
C111 Re11 Re11 96.4(4) . 3_565 ?
C111 Re11 Re12 140.5(4) . . ?
C111 Re11 Se13 83.0(4) . . ?
C111 Re11 Se14 85.7(4) . 3_565 ?
C111 Re11 Se14 160.0(4) . . ?
C111 Re11 C112 81.6(6) . . ?
C111 Re11 C113 79.7(6) . . ?
C112 Re11 Re11 139.3(5) . 3_565 ?
C112 Re11 Re11 139.4(5) . 2_665 ?
C112 Re11 Re12 96.2(5) . . ?
C112 Re11 Se13 160.1(5) . . ?
C112 Re11 Se14 84.4(5) . 3_565 ?
C112 Re11 Se14 84.2(5) . . ?
C112 Re11 C113 81.9(6) . . ?
C113 Re11 Re11 138.1(5) . 3_565 ?
C113 Re11 Re11 95.5(5) . 2_665 ?
C113 Re11 Re12 139.4(4) . . ?
C113 Re11 Se13 83.1(5) . . ?
C113 Re11 Se14 84.5(4) . . ?
C113 Re11 Se14 161.2(5) . 3_565 ?
Re11 Re12 Re11 59.62(3) 2_665 . ?
Se14 Re12 Re11 55.07(4) 3_565 . ?
Se14 Re12 Re11 54.81(4) . . ?
Se14 Re12 Re11 55.07(4) . 2_665 ?
Se14 Re12 Re11 55.07(4) 2_665 3_565 ?
Se14 Re12 Re11 102.89(5) . 3_565 ?
Se14 Re12 Re11 102.89(5) 2_665 . ?
Se14 Re12 Re11 54.81(4) 3_565 3_565 ?
Se14 Re12 Re11 54.81(4) 2_665 2_665 ?
Se14 Re12 Re11 102.89(5) 3_565 2_665 ?
Se14 Re12 Se14 106.68(5) 2_665 3_565 ?
Se14 Re12 Se14 106.67(5) . 2_665 ?
Se14 Re12 Se14 106.68(5) . 3_565 ?
C121 Re12 Re11 96.2(6) 3_565 3_565 ?
C121 Re12 Re11 140.5(6) . 2_665 ?
C121 Re12 Re11 137.6(6) 2_665 . ?
C121 Re12 Re11 96.2(6) 2_665 2_665 ?
C121 Re12 Re11 137.6(6) . 3_565 ?
C121 Re12 Re11 140.5(6) 2_665 3_565 ?
C121 Re12 Re11 96.2(6) . . ?
C121 Re12 Re11 140.5(6) 3_565 . ?
C121 Re12 Re11 137.6(6) 3_565 2_665 ?
C121 Re12 Se14 160.8(6) 3_565 . ?
C121 Re12 Se14 160.8(6) 2_665 3_565 ?
C121 Re12 Se14 85.7(6) . . ?
C121 Re12 Se14 82.9(6) 2_665 . ?
C121 Re12 Se14 85.7(6) 3_565 3_565 ?
C121 Re12 Se14 82.9(6) 3_565 2_665 ?
C121 Re12 Se14 82.9(6) . 3_565 ?
C121 Re12 Se14 85.7(6) 2_665 2_665 ?
C121 Re12 Se14 160.8(6) . 2_665 ?
C121 Re12 C121 81.3(10) 2_665 . ?
C121 Re12 C121 81.3(9) 2_665 3_565 ?
C121 Re12 C121 81.3(10) . 3_565 ?
Re13 Re13 Re13 59.998(2) 3_575 2_775 ?
Re13 Re13 Re14 60.051(15) 3_575 . ?
Re13 Re13 Re14 60.051(15) 2_775 . ?
Se11 Re13 Re13 103.32(4) . 2_775 ?
Se11 Re13 Re13 54.95(4) . 3_575 ?
Se11 Re13 Re13 103.50(4) 2_775 3_575 ?
Se11 Re13 Re13 55.18(4) 2_775 2_775 ?
Se11 Re13 Re14 55.19(4) 2_775 . ?
Se11 Re13 Re14 55.14(4) . . ?
Se11 Re13 Se11 107.15(8) 2_775 . ?
Se11 Re13 Se12 106.98(5) 2_775 . ?
Se12 Re13 Re13 55.07(4) . 3_575 ?
Se12 Re13 Re13 55.07(4) . 2_775 ?
Se12 Re13 Re14 103.41(5) . . ?
Se12 Re13 Se11 106.76(5) . . ?
C131 Re13 Re13 96.1(5) . 2_775 ?
C131 Re13 Re13 137.8(5) . 3_575 ?
C131 Re13 Re14 140.4(5) . . ?
C131 Re13 Se11 160.5(5) . . ?
C131 Re13 Se11 85.4(5) . 2_775 ?
C131 Re13 Se12 82.7(5) . . ?
C131 Re13 C132 83.2(7) . . ?
C131 Re13 C133 79.6(7) . . ?
C132 Re13 Re13 138.3(5) . 2_775 ?
C132 Re13 Re13 138.4(5) . 3_575 ?
C132 Re13 Re14 94.8(5) . . ?
C132 Re13 Se11 83.3(5) . 2_775 ?
C132 Re13 Se11 83.6(5) . . ?
C132 Re13 Se12 161.8(5) . . ?
C132 Re13 C133 81.0(7) . . ?
C133 Re13 Re13 97.0(5) . 3_575 ?
C133 Re13 Re13 140.1(5) . 2_775 ?
C133 Re13 Re14 139.3(5) . . ?
C133 Re13 Se11 159.5(5) . 2_775 ?
C133 Re13 Se11 84.2(5) . . ?
C133 Re13 Se12 85.1(5) . . ?
Re13 Re14 Re13 59.90(3) 2_775 . ?
Se11 Re14 Re13 54.85(4) 3_575 2_775 ?
Se11 Re14 Re13 54.85(4) 2_775 . ?
Se11 Re14 Re13 103.11(5) 3_575 . ?
Se11 Re14 Re13 55.03(4) 3_575 3_575 ?
Se11 Re14 Re13 55.03(4) 2_775 2_775 ?
Se11 Re14 Re13 103.10(5) . 2_775 ?
Se11 Re14 Re13 103.10(5) 2_775 3_575 ?
Se11 Re14 Re13 55.02(4) . . ?
Se11 Re14 Re13 54.86(4) . 3_575 ?
Se11 Re14 Se11 106.72(5) 2_775 . ?
Se11 Re14 Se11 106.73(5) 3_575 . ?
Se11 Re14 Se11 106.72(5) 2_775 3_575 ?
C141 Re14 Re13 96.9(4) 3_575 . ?
C141 Re14 Re13 140.6(4) . 3_575 ?
C141 Re14 Re13 140.6(4) 2_775 . ?
C141 Re14 Re13 138.5(5) 3_575 3_575 ?
C141 Re14 Re13 138.5(5) . . ?
C141 Re14 Re13 138.5(5) 2_775 2_775 ?
C141 Re14 Re13 140.6(4) 3_575 2_775 ?
C141 Re14 Re13 96.9(4) 2_775 3_575 ?
C141 Re14 Re13 96.9(4) . 2_775 ?
C141 Re14 Se11 85.7(4) 3_575 2_775 ?
C141 Re14 Se11 160.0(4) . . ?
C141 Re14 Se11 85.7(4) 2_775 . ?
C141 Re14 Se11 160.0(4) 2_775 2_775 ?
C141 Re14 Se11 83.7(5) 2_775 3_575 ?
C141 Re14 Se11 85.7(4) . 3_575 ?
C141 Re14 Se11 83.7(5) 3_575 . ?
C141 Re14 Se11 160.0(4) 3_575 3_575 ?
C141 Re14 Se11 83.7(5) . 2_775 ?
C141 Re14 C141 80.1(7) 3_575 2_775 ?
C141 Re14 C141 80.1(7) . 3_575 ?
C141 Re14 C141 80.1(7) . 2_775 ?
W2 W1 W3 60.18(2) . . ?
W2 W1 W4 59.58(2) . . ?
W3 W1 W4 59.71(2) . . ?
Se1 W1 W2 55.16(4) . . ?
Se1 W1 W3 55.09(4) . . ?
Se1 W1 W4 102.90(5) . . ?
Se3 W1 W2 103.25(5) . . ?
Se3 W1 W3 54.93(4) . . ?
Se3 W1 W4 55.08(4) . . ?
Se3 W1 Se1 106.87(6) . . ?
Se3 W1 Se4 106.62(6) . . ?
Se4 W1 W2 55.05(4) . . ?
Se4 W1 W3 103.38(5) . . ?
Se4 W1 W4 54.96(4) . . ?
Se4 W1 Se1 107.07(6) . . ?
C11 W1 W2 137.5(5) . . ?
C11 W1 W3 95.0(6) . . ?
C11 W1 W4 139.6(6) . . ?
C11 W1 Se1 82.4(5) . . ?
C11 W1 Se3 84.8(6) . . ?
C11 W1 Se4 161.6(6) . . ?
C11 W1 C12 82.5(8) . . ?
C11 W1 C13 80.4(7) . . ?
C12 W1 W2 139.5(6) . . ?
C12 W1 W3 137.7(6) . . ?
C12 W1 W4 95.9(5) . . ?
C12 W1 Se1 161.2(5) . . ?
C12 W1 Se3 82.9(6) . . ?
C12 W1 Se4 84.7(6) . . ?
C13 W1 W2 97.3(5) . . ?
C13 W1 W3 140.3(5) . . ?
C13 W1 W4 139.6(5) . . ?
C13 W1 Se1 85.2(5) . . ?
C13 W1 Se3 159.5(5) . . ?
C13 W1 Se4 84.7(5) . . ?
C13 W1 C12 81.2(7) . . ?
W1 W2 W3 60.07(2) . . ?
W4 W2 W1 60.41(2) . . ?
W4 W2 W3 59.95(2) . . ?
Se1 W2 W1 55.21(4) . . ?
Se1 W2 W3 55.06(4) . . ?
Se1 W2 W4 103.62(5) . . ?
Se2 W2 W1 103.54(5) . . ?
Se2 W2 W3 54.75(4) . . ?
Se2 W2 W4 55.20(4) . . ?
Se2 W2 Se1 106.34(6) . . ?
Se4 W2 W1 55.12(4) . . ?
Se4 W2 W3 103.36(5) . . ?
Se4 W2 W4 55.31(4) . . ?
Se4 W2 Se1 107.18(6) . . ?
Se4 W2 Se2 107.46(6) . . ?
C21 W2 W1 139.6(5) . . ?
C21 W2 W3 97.6(5) . . ?
C21 W2 W4 140.2(5) . . ?
C21 W2 Se1 84.4(5) . . ?
C21 W2 Se2 85.1(5) . . ?
C21 W2 Se4 159.0(5) . . ?
C21 W2 C23 81.9(6) . . ?
C22 W2 W1 95.8(4) . . ?
C22 W2 W3 139.2(4) . . ?
C22 W2 W4 139.1(4) . . ?
C22 W2 Se1 84.3(4) . . ?
C22 W2 Se2 160.6(5) . . ?
C22 W2 Se4 83.9(4) . . ?
C22 W2 C21 79.9(7) . . ?
C22 W2 C23 80.7(6) . . ?
C23 W2 W1 137.5(4) . . ?
C23 W2 W3 139.7(4) . . ?
C23 W2 W4 95.2(4) . . ?
C23 W2 Se1 161.2(4) . . ?
C23 W2 Se2 85.3(4) . . ?
C23 W2 Se4 82.5(4) . . ?
W1 W3 W2 59.75(2) . . ?
W4 W3 W1 60.18(2) . . ?
W4 W3 W2 59.60(2) . . ?
Se1 W3 W1 55.07(4) . . ?
Se1 W3 W2 54.99(4) . . ?
Se1 W3 W4 103.27(5) . . ?
Se2 W3 W1 103.55(5) . . ?
Se2 W3 W2 55.09(4) . . ?
Se2 W3 W4 55.14(4) . . ?
Se2 W3 Se1 106.59(6) . . ?
Se2 W3 Se3 107.27(6) . . ?
Se3 W3 W1 54.92(4) . . ?
Se3 W3 W2 102.89(5) . . ?
Se3 W3 W4 55.27(4) . . ?
Se3 W3 Se1 106.84(6) . . ?
C31 W3 W1 140.0(5) . . ?
C31 W3 W2 96.0(5) . . ?
C31 W3 W4 137.4(5) . . ?
C31 W3 Se1 85.1(5) . . ?
C31 W3 Se2 82.4(5) . . ?
C31 W3 Se3 161.1(5) . . ?
C31 W3 C32 82.3(7) . . ?
C32 W3 W1 137.2(5) . . ?
C32 W3 W2 140.0(5) . . ?
C32 W3 W4 95.2(5) . . ?
C32 W3 Se1 161.4(5) . . ?
C32 W3 Se2 85.2(5) . . ?
C32 W3 Se3 82.4(5) . . ?
C33 W3 W1 97.8(5) . . ?
C33 W3 W2 139.5(5) . . ?
C33 W3 W4 141.3(5) . . ?
C33 W3 Se1 84.6(5) . . ?
C33 W3 Se2 158.6(5) . . ?
C33 W3 Se3 86.0(5) . . ?
C33 W3 C31 80.4(7) . . ?
C33 W3 C32 79.9(7) . . ?
W2 W4 W1 60.01(2) . . ?
W2 W4 W3 60.46(2) . . ?
W3 W4 W1 60.11(2) . . ?
Se2 W4 W1 103.37(5) . . ?
Se2 W4 W2 55.40(4) . . ?
Se2 W4 W3 55.00(4) . . ?
Se2 W4 Se3 106.91(6) . . ?
Se2 W4 Se4 107.56(6) . . ?
Se3 W4 W1 54.83(4) . . ?
Se3 W4 W2 103.40(5) . . ?
Se3 W4 W3 55.03(4) . . ?
Se4 W4 W1 54.94(4) . . ?
Se4 W4 W2 55.22(4) . . ?
Se4 W4 W3 103.70(5) . . ?
Se4 W4 Se3 106.37(6) . . ?
C41 W4 W1 140.8(5) . . ?
C41 W4 W2 96.1(5) . . ?
C41 W4 W3 137.7(5) . . ?
C41 W4 Se2 82.8(5) . . ?
C41 W4 Se3 160.4(5) . . ?
C41 W4 Se4 86.1(5) . . ?
C41 W4 C42 77.8(7) . . ?
C41 W4 C43 80.8(7) . . ?
C42 W4 W1 140.9(5) . . ?
C42 W4 W2 139.6(5) . . ?
C42 W4 W3 97.5(5) . . ?
C42 W4 Se2 84.2(5) . . ?
C42 W4 Se3 86.1(5) . . ?
C42 W4 Se4 158.8(5) . . ?
C42 W4 C43 79.9(7) . . ?
C43 W4 W1 97.5(5) . . ?
C43 W4 W2 139.2(5) . . ?
C43 W4 W3 140.4(5) . . ?
C43 W4 Se2 159.1(5) . . ?
C43 W4 Se3 85.5(5) . . ?
C43 W4 Se4 84.0(5) . . ?
W6 W5 W7 60.10(2) . . ?
W6 W5 W8 60.31(2) . . ?
W8 W5 W7 59.86(2) . . ?
Se5 W5 W6 55.15(4) . . ?
Se5 W5 W7 55.22(4) . . ?
Se5 W5 W8 103.55(5) . . ?
Se5 W5 Se7 107.08(6) . . ?
Se7 W5 W6 55.10(4) . . ?
Se7 W5 W7 103.26(5) . . ?
Se7 W5 W8 55.18(4) . . ?
Se8 W5 W6 103.64(5) . . ?
Se8 W5 W7 55.08(4) . . ?
Se8 W5 W8 55.02(4) . . ?
Se8 W5 Se5 106.96(6) . . ?
Se8 W5 Se7 106.98(6) . . ?
C51 W5 W6 139.1(5) . . ?
C51 W5 W7 140.2(5) . . ?
C51 W5 W8 96.9(5) . . ?
C51 W5 Se5 159.5(5) . . ?
C51 W5 Se7 84.1(5) . . ?
C51 W5 Se8 85.2(5) . . ?
C52 W5 W6 138.4(5) . . ?
C52 W5 W7 96.1(5) . . ?
C52 W5 W8 139.5(5) . . ?
C52 W5 Se5 83.3(5) . . ?
C52 W5 Se7 160.7(5) . . ?
C52 W5 Se8 84.6(5) . . ?
C52 W5 C51 81.5(7) . . ?
C52 W5 C53 81.0(7) . . ?
C53 W5 W6 94.9(4) . . ?
C53 W5 W7 138.1(4) . . ?
C53 W5 W8 139.1(4) . . ?
C53 W5 Se5 83.0(4) . . ?
C53 W5 Se7 84.1(4) . . ?
C53 W5 Se8 161.5(4) . . ?
C53 W5 C51 81.1(6) . . ?
W5 W6 W7 60.00(2) . . ?
W5 W6 W8 59.87(2) . . ?
W7 W6 W8 59.68(2) . . ?
Se5 W6 W5 55.13(4) . . ?
Se5 W6 W7 55.18(4) . . ?
Se5 W6 W8 103.17(5) . . ?
Se6 W6 W5 103.40(5) . . ?
Se6 W6 W7 55.03(4) . . ?
Se6 W6 W8 55.10(5) . . ?
Se6 W6 Se5 106.92(6) . . ?
Se6 W6 Se7 106.76(6) . . ?
Se7 W6 W5 55.21(4) . . ?
Se7 W6 W7 103.27(5) . . ?
Se7 W6 W8 55.03(4) . . ?
Se7 W6 Se5 107.18(6) . . ?
C61 W6 W5 137.7(5) . . ?
C61 W6 W7 94.8(5) . . ?
C61 W6 W8 138.7(5) . . ?
C61 W6 Se5 82.7(5) . . ?
C61 W6 Se6 83.9(5) . . ?
C61 W6 Se7 161.9(5) . . ?
C61 W6 C62 82.7(7) . . ?
C61 W6 C63 81.3(7) . . ?
C62 W6 W5 139.2(5) . . ?
C62 W6 W7 138.3(5) . . ?
C62 W6 W8 95.8(5) . . ?
C62 W6 Se5 161.0(5) . . ?
C62 W6 Se6 83.4(5) . . ?
C62 W6 Se7 84.1(5) . . ?
C63 W6 W5 96.8(5) . . ?
C63 W6 W7 139.8(5) . . ?
C63 W6 W8 139.5(5) . . ?
C63 W6 Se5 84.8(5) . . ?
C63 W6 Se6 159.8(5) . . ?
C63 W6 Se7 84.5(5) . . ?
C63 W6 C62 81.2(7) . . ?
W5 W7 W6 59.91(2) . . ?
W8 W7 W5 60.05(2) . . ?
W8 W7 W6 60.31(2) . . ?
Se5 W7 W5 55.05(4) . . ?
Se5 W7 W6 55.03(4) . . ?
Se5 W7 W8 103.57(5) . . ?
Se6 W7 W5 103.27(5) . . ?
Se6 W7 W6 54.96(5) . . ?
Se6 W7 W8 55.34(5) . . ?
Se6 W7 Se5 106.71(6) . . ?
Se6 W7 Se8 107.38(6) . . ?
Se8 W7 W5 55.07(4) . . ?
Se8 W7 W6 103.47(5) . . ?
Se8 W7 W8 55.10(4) . . ?
Se8 W7 Se5 106.79(6) . . ?
C71 W7 W5 96.6(4) . . ?
C71 W7 W6 140.6(4) . . ?
C71 W7 W8 138.0(4) . . ?
C71 W7 Se5 85.7(4) . . ?
C71 W7 Se6 160.1(4) . . ?
C71 W7 Se8 82.9(4) . . ?
C71 W7 C72 80.7(6) . . ?
C72 W7 W5 140.5(4) . . ?
C72 W7 W6 138.0(4) . . ?
C72 W7 W8 96.0(4) . . ?
C72 W7 Se5 160.3(5) . . ?
C72 W7 Se6 83.1(4) . . ?
C72 W7 Se8 85.6(4) . . ?
C73 W7 W5 139.7(5) . . ?
C73 W7 W6 97.5(5) . . ?
C73 W7 W8 140.6(5) . . ?
C73 W7 Se5 84.7(5) . . ?
C73 W7 Se6 85.3(5) . . ?
C73 W7 Se8 159.0(5) . . ?
C73 W7 C71 80.4(6) . . ?
C73 W7 C72 79.2(6) . . ?
W5 W8 W6 59.82(2) . . ?
W7 W8 W5 60.10(2) . . ?
W7 W8 W6 60.01(2) . . ?
Se6 W8 W5 103.11(5) . . ?
Se6 W8 W6 54.77(5) . . ?
Se6 W8 W7 55.08(4) . . ?
Se7 W8 W5 55.16(4) . . ?
Se7 W8 W6 54.90(4) . . ?
Se7 W8 W7 103.44(5) . . ?
Se7 W8 Se6 106.33(6) . . ?
Se8 W8 W5 55.12(4) . . ?
Se8 W8 W6 103.31(5) . . ?
Se8 W8 W7 55.20(4) . . ?
Se8 W8 Se6 107.23(6) . . ?
Se8 W8 Se7 107.05(6) . . ?
C81 W8 W5 138.9(5) . . ?
C81 W8 W6 139.8(5) . . ?
C81 W8 W7 96.3(5) . . ?
C81 W8 Se6 85.2(5) . . ?
C81 W8 Se7 160.3(5) . . ?
C81 W8 Se8 83.9(5) . . ?
C81 W8 C82 80.2(7) . . ?
C81 W8 C83 80.9(7) . . ?
C82 W8 W5 139.8(5) . . ?
C82 W8 W6 98.1(5) . . ?
C82 W8 W7 140.8(5) . . ?
C82 W8 Se6 85.8(5) . . ?
C82 W8 Se7 84.6(5) . . ?
C82 W8 Se8 158.5(5) . . ?
C82 W8 C83 80.6(7) . . ?
C83 W8 W5 95.0(4) . . ?
C83 W8 W6 138.9(5) . . ?
C83 W8 W7 137.8(4) . . ?
C83 W8 Se6 161.9(5) . . ?
C83 W8 Se7 84.3(5) . . ?
C83 W8 Se8 82.7(4) . . ?
Se9 W9 W10 54.95(4) . . ?
Se9 W9 W10 54.98(4) 2_765 . ?
Se9 W9 Se9 106.70(8) 2_765 . ?
Se10 W9 W10 103.56(5) . . ?
Se10 W9 Se9 107.14(5) . 2_765 ?
Se10 W9 Se9 107.00(5) . . ?
C91 W9 W10 96.4(5) . . ?
C91 W9 Se9 84.7(5) . . ?
C91 W9 Se9 84.0(5) . 2_765 ?
C91 W9 Se10 160.0(5) . . ?
C92 W9 W10 139.2(5) . . ?
C92 W9 Se9 84.3(5) . . ?
C92 W9 Se9 160.6(5) . 2_765 ?
C92 W9 Se10 84.0(4) . . ?
C92 W9 C91 81.1(7) . . ?
C92 W9 C93 80.5(6) . . ?
C93 W9 W10 139.8(5) . . ?
C93 W9 Se9 160.9(5) . . ?
C93 W9 Se9 85.0(5) . 2_765 ?
C93 W9 Se10 82.9(5) . . ?
C93 W9 C91 81.6(7) . . ?
Se9 W10 W9 55.07(4) . . ?
Se9 W10 W9 54.96(4) 2_765 . ?
Se9 W10 W9 103.06(5) 3_675 . ?
Se9 W10 Se9 106.79(5) 2_765 . ?
Se9 W10 Se9 106.79(5) 2_765 3_675 ?
Se9 W10 Se9 106.79(5) 3_675 . ?
C101 W10 W9 140.8(5) 3_675 . ?
C101 W10 W9 97.0(5) . . ?
C101 W10 W9 138.4(5) 2_765 . ?
C101 W10 Se9 159.9(5) 2_765 . ?
C101 W10 Se9 83.4(5) 3_675 3_675 ?
C101 W10 Se9 159.9(5) . 3_675 ?
C101 W10 Se9 85.9(5) . 2_765 ?
C101 W10 Se9 159.9(5) 3_675 2_765 ?
C101 W10 Se9 85.9(5) 2_765 3_675 ?
C101 W10 Se9 83.4(5) 2_765 2_765 ?
C101 W10 Se9 83.4(5) . . ?
C101 W10 Se9 85.9(5) 3_675 . ?
C101 W10 C101 80.0(7) 2_765 . ?
C101 W10 C101 80.0(7) 3_675 . ?
C101 W10 C101 80.0(7) 3_675 2_765 ?
Se13 W11 W12 103.64(5) . . ?
Se13 W11 Se14 106.91(5) . 3_565 ?
Se14 W11 W12 55.04(4) . . ?
Se14 W11 W12 54.95(4) 3_565 . ?
Se14 W11 Se13 107.25(5) . . ?
Se14 W11 Se14 106.78(8) . 3_565 ?
C111 W11 W12 140.5(4) . . ?
C111 W11 Se13 83.0(4) . . ?
C111 W11 Se14 85.7(4) . 3_565 ?
C111 W11 Se14 160.0(4) . . ?
C111 W11 C112 81.6(6) . . ?
C111 W11 C113 79.7(6) . . ?
C112 W11 W12 96.2(5) . . ?
C112 W11 Se13 160.1(5) . . ?
C112 W11 Se14 84.2(5) . . ?
C112 W11 Se14 84.4(5) . 3_565 ?
C112 W11 C113 81.9(6) . . ?
C113 W11 W12 139.4(4) . . ?
C113 W11 Se13 83.1(5) . . ?
C113 W11 Se14 84.5(4) . . ?
C113 W11 Se14 161.2(5) . 3_565 ?
Se14 W12 W11 55.07(4) 3_565 . ?
Se14 W12 W11 102.89(5) 2_665 . ?
Se14 W12 W11 54.81(4) . . ?
Se14 W12 Se14 106.68(5) 2_665 3_565 ?
Se14 W12 Se14 106.68(5) . 3_565 ?
Se14 W12 Se14 106.67(5) . 2_665 ?
C121 W12 W11 140.5(6) 3_565 . ?
C121 W12 W11 96.2(6) . . ?
C121 W12 W11 137.6(6) 2_665 . ?
C121 W12 Se14 85.7(6) 2_665 2_665 ?
C121 W12 Se14 160.8(6) 2_665 3_565 ?
C121 W12 Se14 85.7(6) 3_565 3_565 ?
C121 W12 Se14 160.8(6) . 2_665 ?
C121 W12 Se14 160.8(6) 3_565 . ?
C121 W12 Se14 85.7(6) . . ?
C121 W12 Se14 82.9(6) 3_565 2_665 ?
C121 W12 Se14 82.9(6) 2_665 . ?
C121 W12 Se14 82.9(6) . 3_565 ?
C121 W12 C121 81.3(10) . 3_565 ?
C121 W12 C121 81.3(10) 2_665 . ?
C121 W12 C121 81.3(9) 2_665 3_565 ?
Se11 W13 W14 55.14(4) . . ?
Se11 W13 W14 55.19(4) 2_775 . ?
Se11 W13 Se11 107.15(8) 2_775 . ?
Se11 W13 Se12 106.98(5) 2_775 . ?
Se12 W13 W14 103.41(5) . . ?
Se12 W13 Se11 106.76(5) . . ?
C131 W13 W14 140.4(5) . . ?
C131 W13 Se11 160.5(5) . . ?
C131 W13 Se11 85.4(5) . 2_775 ?
C131 W13 Se12 82.7(5) . . ?
C131 W13 C132 83.2(7) . . ?
C131 W13 C133 79.6(7) . . ?
C132 W13 W14 94.8(5) . . ?
C132 W13 Se11 83.3(5) . 2_775 ?
C132 W13 Se11 83.6(5) . . ?
C132 W13 Se12 161.8(5) . . ?
C132 W13 C133 81.0(7) . . ?
C133 W13 W14 139.3(5) . . ?
C133 W13 Se11 159.5(5) . 2_775 ?
C133 W13 Se11 84.2(5) . . ?
C133 W13 Se12 85.1(5) . . ?
Se11 W14 W13 54.85(4) 2_775 . ?
Se11 W14 W13 103.11(5) 3_575 . ?
Se11 W14 W13 55.02(4) . . ?
Se11 W14 Se11 106.73(5) 3_575 . ?
Se11 W14 Se11 106.72(5) 2_775 3_575 ?
Se11 W14 Se11 106.72(5) 2_775 . ?
C141 W14 W13 140.6(4) 2_775 . ?
C141 W14 W13 96.9(4) 3_575 . ?
C141 W14 W13 138.5(5) . . ?
C141 W14 Se11 83.7(5) 3_575 . ?
C141 W14 Se11 160.0(4) 3_575 3_575 ?
C141 W14 Se11 160.0(4) 2_775 2_775 ?
C141 W14 Se11 160.0(4) . . ?
C141 W14 Se11 85.7(4) . 3_575 ?
C141 W14 Se11 85.7(4) 3_575 2_775 ?
C141 W14 Se11 83.7(5) 2_775 3_575 ?
C141 W14 Se11 83.7(5) . 2_775 ?
C141 W14 Se11 85.7(4) 2_775 . ?
C141 W14 C141 80.1(7) . 3_575 ?
C141 W14 C141 80.1(7) 3_575 2_775 ?
C141 W14 C141 80.1(7) . 2_775 ?
Re1 Se1 Re3 69.85(5) . . ?
Re2 Se1 Re1 69.62(5) . . ?
Re2 Se1 Re3 69.96(5) . . ?
W1 Se1 W3 69.85(5) . . ?
W2 Se1 W1 69.62(5) . . ?
W2 Se1 W3 69.96(5) . . ?
Re3 Se2 Re2 70.17(5) . . ?
Re3 Se2 Re4 69.86(5) . . ?
Re4 Se2 Re2 69.40(5) . . ?
W3 Se2 W2 70.17(5) . . ?
W3 Se2 W4 69.86(5) . . ?
W4 Se2 W2 69.40(5) . . ?
Re1 Se3 Re3 70.15(5) . . ?
Re1 Se3 Re4 70.10(5) . . ?
Re1 Se3 K1 134.10(9) . . ?
Re3 Se3 Re4 69.71(5) . . ?
Re3 Se3 K1 136.53(9) . . ?
Re4 Se3 K1 85.16(8) . . ?
W1 Se3 W3 70.15(5) . . ?
W1 Se3 W4 70.10(5) . . ?
W1 Se3 K1 134.10(9) . . ?
W3 Se3 W4 69.71(5) . . ?
W3 Se3 K1 136.53(9) . . ?
W4 Se3 K1 85.16(8) . . ?
Re1 Se4 Re4 70.10(5) . . ?
Re1 Se4 K7 134.53(9) . . ?
Re2 Se4 Re1 69.83(5) . . ?
Re2 Se4 Re4 69.47(5) . . ?
Re2 Se4 K7 135.76(9) . . ?
Re4 Se4 K7 84.75(8) . . ?
W1 Se4 W4 70.10(5) . . ?
W1 Se4 K7 134.53(9) . . ?
W2 Se4 W1 69.83(5) . . ?
W2 Se4 W4 69.47(5) . . ?
W2 Se4 K7 135.76(9) . . ?
W4 Se4 K7 84.75(8) . . ?
Re5 Se5 Re6 69.73(5) . . ?
Re5 Se5 Re7 69.73(5) . . ?
Re6 Se5 Re7 69.80(5) . . ?
W5 Se5 W6 69.73(5) . . ?
W5 Se5 W7 69.73(5) . . ?
W5 Se5 K11 135.48(9) . 3_675 ?
W6 Se5 W7 69.80(5) . . ?
W6 Se5 K11 135.20(9) . 3_675 ?
W7 Se5 K11 85.03(8) . 3_675 ?
Re6 Se6 Re7 70.01(5) . . ?
Re6 Se6 Re8 70.13(5) . . ?
Re7 Se6 Re8 69.58(5) . . ?
W6 Se6 W7 70.01(5) . . ?
W6 Se6 W8 70.13(5) . . ?
W7 Se6 W8 69.58(5) . . ?
Re5 Se7 Re8 69.66(5) . . ?
Re6 Se7 Re5 69.69(5) . . ?
Re6 Se7 Re8 70.07(5) . . ?
W5 Se7 W8 69.66(5) . . ?
W6 Se7 W5 69.69(5) . . ?
W6 Se7 W8 70.07(5) . . ?
Re5 Se8 Re7 69.85(5) . . ?
Re5 Se8 K10 135.42(9) . . ?
Re7 Se8 K10 82.88(8) . . ?
Re8 Se8 Re5 69.86(5) . . ?
Re8 Se8 Re7 69.71(5) . . ?
Re8 Se8 K10 132.60(9) . . ?
W5 Se8 W7 69.85(5) . . ?
W5 Se8 K10 135.42(9) . . ?
W7 Se8 K10 82.88(8) . . ?
W8 Se8 W5 69.86(5) . . ?
W8 Se8 W7 69.71(5) . . ?
W8 Se8 K10 132.60(9) . . ?
Re9 Se9 Re9 69.65(5) 3_675 . ?
Re9 Se9 Re10 70.06(5) 3_675 . ?
Re10 Se9 Re9 69.99(5) . . ?
W10 Se9 W9 69.99(5) . . ?
Re9 Se10 Re9 69.80(7) 3_675 . ?
Re9 Se10 Re9 69.80(7) 2_765 . ?
Re9 Se10 Re9 69.80(7) 3_675 2_765 ?
Re13 Se11 Re13 69.88(5) 3_575 . ?
Re13 Se11 Re14 69.84(5) . . ?
Re13 Se11 Re14 69.95(5) 3_575 . ?
W13 Se11 W14 69.84(5) . . ?
Re13 Se12 Re13 69.86(7) 2_775 . ?
W13 Se12 Re13 69.86(7) . 3_575 ?
Re11 Se13 Re11 69.76(7) 2_665 . ?
W11 Se13 Re11 69.76(7) . 3_565 ?
Re11 Se14 Re11 69.63(5) . 2_665 ?
Re11 Se14 Re12 70.15(5) . . ?
Re12 Se14 Re11 69.98(5) . 2_665 ?
W11 Se14 Re11 69.63(5) . 2_665 ?
W11 Se14 W12 70.15(5) . . ?
W11 Se14 K18 136.72(9) . 2_664 ?
W12 Se14 Re11 69.98(5) . 2_665 ?
W12 Se14 K18 87.29(8) . 2_664 ?
O1 K1 Se3 71.4(4) . . ?
O1 K1 O2 114.5(5) . . ?
O1 K1 N11 78.2(6) . 1_554 ?
O1 K1 N33 150.6(6) . 1_554 ?
O1 K1 N42 133.4(5) . . ?
O1 K1 N43 64.8(4) . . ?
O1 K1 C11 90.7(5) . 1_554 ?
O1 K1 C33 146.8(5) . 1_554 ?
O1 K1 C42 113.8(5) . . ?
O1 K1 C43 72.0(5) . . ?
O2 K1 Se3 64.2(3) . . ?
O2 K1 N11 151.1(5) . 1_554 ?
O2 K1 N33 81.2(5) . 1_554 ?
O2 K1 N42 65.0(4) . . ?
O2 K1 N43 129.7(5) . . ?
O2 K1 C11 151.8(5) . 1_554 ?
O2 K1 C33 95.7(5) . 1_554 ?
O2 K1 C42 69.9(4) . . ?
O2 K1 C43 109.1(5) . . ?
O3 K1 Se3 110.5(3) 1_554 . ?
O3 K1 O1 76.7(4) 1_554 . ?
O3 K1 O2 76.9(4) 1_554 . ?
O3 K1 N11 81.5(5) 1_554 1_554 ?
O3 K1 N33 83.6(5) 1_554 1_554 ?
O3 K1 N42 138.5(4) 1_554 . ?
O3 K1 N43 139.6(4) 1_554 . ?
O3 K1 C11 98.3(5) 1_554 1_554 ?
O3 K1 C33 98.6(4) 1_554 1_554 ?
O3 K1 C42 146.6(4) 1_554 . ?
O3 K1 C43 147.6(5) 1_554 . ?
N11 K1 Se3 143.0(4) 1_554 . ?
N11 K1 N33 77.5(5) 1_554 1_554 ?
N11 K1 N42 126.3(5) 1_554 . ?
N11 K1 N43 79.0(5) 1_554 . ?
N11 K1 C11 19.0(5) 1_554 1_554 ?
N11 K1 C33 68.6(5) 1_554 1_554 ?
N11 K1 C42 130.8(5) 1_554 . ?
N11 K1 C43 99.4(5) 1_554 . ?
N33 K1 Se3 137.0(4) 1_554 . ?
N33 K1 N42 75.2(5) 1_554 . ?
N33 K1 N43 125.5(5) 1_554 . ?
N33 K1 C11 70.7(5) 1_554 1_554 ?
N33 K1 C33 18.9(4) 1_554 1_554 ?
N33 K1 C42 94.6(5) 1_554 . ?
N33 K1 C43 128.5(5) 1_554 . ?
N42 K1 Se3 67.6(3) . . ?
N42 K1 C11 107.4(5) . 1_554 ?
N42 K1 C33 70.8(4) . 1_554 ?
N42 K1 C42 19.6(4) . . ?
N42 K1 C43 65.7(4) . . ?
N43 K1 Se3 69.3(3) . . ?
N43 K1 N42 80.6(4) . . ?
N43 K1 C11 71.3(5) . 1_554 ?
N43 K1 C33 106.7(4) . 1_554 ?
N43 K1 C42 66.4(4) . . ?
N43 K1 C43 20.6(4) . . ?
C11 K1 Se3 140.6(4) 1_554 . ?
C11 K1 C33 57.1(4) 1_554 1_554 ?
C33 K1 Se3 138.2(3) 1_554 . ?
C42 K1 Se3 51.1(3) . . ?
C42 K1 C11 112.6(5) . 1_554 ?
C42 K1 C33 88.4(4) . 1_554 ?
C43 K1 Se3 51.5(3) . . ?
C43 K1 C11 90.0(5) . 1_554 ?
C43 K1 C33 112.0(5) . 1_554 ?
C43 K1 C42 48.7(5) . . ?
K1 K2 K3 88.23(14) 1_556 1_556 ?
K1 K2 K13 82.78(16) 1_556 . ?
K1 K2 K15 144.33(19) 1_556 . ?
K13 K2 K3 146.4(2) . 1_556 ?
K13 K2 K15 61.55(11) . . ?
K15 K2 K3 121.06(17) . 1_556 ?
O2 K2 K1 43.4(3) 1_556 1_556 ?
O2 K2 K3 110.5(3) 1_556 1_556 ?
O2 K2 K13 84.5(3) 1_556 . ?
O2 K2 K15 126.0(4) 1_556 . ?
O2 K2 O7 162.5(5) 1_556 . ?
O2 K2 O8 108.9(7) 1_556 . ?
O2 K2 N31 138.2(5) 1_556 . ?
O2 K2 N33 81.0(5) 1_556 . ?
O7 K2 K1 136.6(4) . 1_556 ?
O7 K2 K3 86.3(4) . 1_556 ?
O7 K2 K13 78.6(4) . . ?
O7 K2 K15 40.3(3) . . ?
O7 K2 O8 74.8(8) . . ?
O7 K2 N31 54.2(4) . . ?
O7 K2 N33 91.6(6) . . ?
O8 K2 K1 148.2(7) . 1_556 ?
O8 K2 K3 90.0(7) . 1_556 ?
O8 K2 K13 114.1(7) . . ?
O8 K2 K15 59.2(6) . . ?
O8 K2 N31 100.4(7) . . ?
N31 K2 K1 98.1(3) . 1_556 ?
N31 K2 K3 39.1(3) . 1_556 ?
N31 K2 K13 110.3(3) . . ?
N31 K2 K15 94.4(3) . . ?
N33 K2 K1 47.2(4) . 1_556 ?
N33 K2 K3 99.9(4) . 1_556 ?
N33 K2 K13 51.4(4) . . ?
N33 K2 K15 103.5(4) . . ?
N33 K2 O8 162.7(8) . . ?
N33 K2 N31 79.4(5) . . ?
N42 K2 K1 50.8(4) 1_556 1_556 ?
N42 K2 K3 41.0(4) 1_556 1_556 ?
N42 K2 K13 131.8(4) 1_556 . ?
N42 K2 K15 162.1(4) 1_556 . ?
N42 K2 O2 71.0(5) 1_556 1_556 ?
N42 K2 O7 124.2(5) 1_556 . ?
N42 K2 O8 112.9(8) 1_556 . ?
N42 K2 N31 70.4(5) 1_556 . ?
N42 K2 N33 83.5(6) 1_556 . ?
N42 K2 N131 156.2(5) 1_556 1_556 ?
N131 K2 K1 110.5(4) 1_556 1_556 ?
N131 K2 K3 161.2(4) 1_556 1_556 ?
N131 K2 K13 41.4(3) 1_556 . ?
N131 K2 K15 41.4(3) 1_556 . ?
N131 K2 O2 85.2(5) 1_556 1_556 ?
N131 K2 O7 79.3(5) 1_556 . ?
N131 K2 O8 74.8(7) 1_556 . ?
N131 K2 N31 132.0(5) 1_556 . ?
N131 K2 N33 92.4(5) 1_556 . ?
O24 K3 K17 44.7(4) . 1_554 ?
O24 K3 O29 77.4(5) . 1_554 ?
O24 K3 N41 58.4(5) . . ?
O24 K3 N42 132.9(5) . . ?
O24 K3 C21 82.3(5) . 1_554 ?
O24 K3 C31 139.4(5) . 1_554 ?
O24 K3 C41 71.0(5) . . ?
O24 K3 C42 113.5(5) . . ?
O28 K3 K17 110.2(6) . 1_554 ?
O28 K3 O24 95.6(7) . . ?
O28 K3 O29 81.7(7) . 1_554 ?
O28 K3 N21 154.9(7) . 1_554 ?
O28 K3 N31 106.9(7) . 1_554 ?
O28 K3 N41 118.3(7) . . ?
O28 K3 N42 85.4(7) . . ?
O28 K3 C21 171.0(7) . 1_554 ?
O28 K3 C31 122.3(7) . 1_554 ?
O28 K3 C41 104.4(7) . . ?
O28 K3 C42 83.9(7) . . ?
O29 K3 K17 43.1(3) 1_554 1_554 ?
O29 K3 N41 131.8(5) 1_554 . ?
O29 K3 N42 148.2(5) 1_554 . ?
O29 K3 C21 89.4(5) 1_554 1_554 ?
O29 K3 C31 93.0(5) 1_554 1_554 ?
O29 K3 C41 148.3(5) 1_554 . ?
O29 K3 C42 162.7(5) 1_554 . ?
N21 K3 K17 44.8(3) 1_554 1_554 ?
N21 K3 O24 67.8(5) 1_554 . ?
N21 K3 O29 76.6(5) 1_554 1_554 ?
N21 K3 N41 69.9(4) 1_554 . ?
N21 K3 N42 119.7(5) 1_554 . ?
N21 K3 C21 17.8(4) 1_554 1_554 ?
N21 K3 C31 71.7(5) 1_554 1_554 ?
N21 K3 C41 88.3(4) 1_554 . ?
N21 K3 C42 119.4(5) 1_554 . ?
N31 K3 K17 102.7(4) 1_554 1_554 ?
N31 K3 O24 146.2(5) 1_554 . ?
N31 K3 O29 81.2(5) 1_554 1_554 ?
N31 K3 N21 82.1(5) 1_554 1_554 ?
N31 K3 N41 125.6(5) 1_554 . ?
N31 K3 N42 75.0(5) 1_554 . ?
N31 K3 C21 71.5(5) 1_554 1_554 ?
N31 K3 C31 17.9(4) 1_554 1_554 ?
N31 K3 C41 124.7(5) 1_554 . ?
N31 K3 C42 94.1(5) 1_554 . ?
N41 K3 K17 89.2(3) . 1_554 ?
N41 K3 C21 68.0(5) . 1_554 ?
N41 K3 C31 107.7(5) . 1_554 ?
N41 K3 C41 19.6(4) . . ?
N41 K3 C42 64.1(4) . . ?
N42 K3 K17 164.0(4) . 1_554 ?
N42 K3 N41 79.8(5) . . ?
N42 K3 C21 102.4(5) . 1_554 ?
N42 K3 C31 69.8(5) . 1_554 ?
N42 K3 C41 63.3(4) . . ?
N42 K3 C42 19.6(4) . . ?
C21 K3 K17 62.3(3) 1_554 1_554 ?
C31 K3 K17 103.0(3) 1_554 1_554 ?
C31 K3 C21 58.0(4) 1_554 1_554 ?
C31 K3 C41 108.7(4) 1_554 . ?
C41 K3 K17 107.7(3) . 1_554 ?
C41 K3 C21 83.3(4) . 1_554 ?
C42 K3 K17 153.3(4) . 1_554 ?
C42 K3 C21 104.9(4) . 1_554 ?
C42 K3 C31 86.7(4) . 1_554 ?
C42 K3 C41 45.8(4) . . ?
K7 K4 K6 56.58(9) 1_556 . ?
K11 K4 K6 62.28(9) . . ?
K11 K4 K7 118.84(13) . 1_556 ?
O20 K4 K6 81.6(3) . . ?
O20 K4 K7 38.4(3) . 1_556 ?
O20 K4 K11 131.7(3) . . ?
O20 K4 O21 79.7(5) . . ?
O20 K4 O23 153.4(4) . . ?
O20 K4 N22 78.2(4) . . ?
O20 K4 N51 71.1(4) . 2_766 ?
O20 K4 N53 87.5(4) . 2_766 ?
O20 K4 N71 140.9(5) . 2_765 ?
O20 K4 C51 70.4(4) . 2_766 ?
O20 K4 C53 80.3(4) . 2_766 ?
O21 K4 K6 118.1(4) . . ?
O21 K4 K7 73.2(4) . 1_556 ?
O21 K4 K11 144.5(4) . . ?
O21 K4 O23 101.1(5) . . ?
O21 K4 N22 77.8(5) . . ?
O21 K4 N51 107.1(5) . 2_766 ?
O21 K4 N53 156.1(5) . 2_766 ?
O21 K4 N71 117.6(5) . 2_765 ?
O21 K4 C51 124.5(5) . 2_766 ?
O21 K4 C53 160.0(5) . 2_766 ?
O23 K4 K6 74.6(3) . . ?
O23 K4 K7 115.9(3) . 1_556 ?
O23 K4 K11 43.5(3) . . ?
O23 K4 N51 132.0(4) . 2_766 ?
O23 K4 N53 81.6(4) . 2_766 ?
O23 K4 C51 126.1(4) . 2_766 ?
O23 K4 C53 96.2(4) . 2_766 ?
N22 K4 K6 40.6(3) . . ?
N22 K4 K7 40.0(3) . 1_556 ?
N22 K4 K11 91.6(3) . . ?
N22 K4 O23 76.0(4) . . ?
N22 K4 N51 147.3(4) . 2_766 ?
N22 K4 N53 79.8(4) . 2_766 ?
N22 K4 N71 137.2(5) . 2_765 ?
N22 K4 C51 135.5(4) . 2_766 ?
N22 K4 C53 96.8(4) . 2_766 ?
N51 K4 K6 121.2(3) 2_766 . ?
N51 K4 K7 109.2(3) 2_766 1_556 ?
N51 K4 K11 100.0(3) 2_766 . ?
N51 K4 C51 19.2(4) 2_766 2_766 ?
N51 K4 C53 67.3(4) 2_766 2_766 ?
N53 K4 K6 39.2(3) 2_766 . ?
N53 K4 K7 84.1(3) 2_766 1_556 ?
N53 K4 K11 44.2(3) 2_766 . ?
N53 K4 N51 87.5(4) 2_766 2_766 ?
N53 K4 C51 68.3(4) 2_766 2_766 ?
N53 K4 C53 20.2(4) 2_766 2_766 ?
N71 K4 K6 113.8(3) 2_765 . ?
N71 K4 K7 169.0(4) 2_765 1_556 ?
N71 K4 K11 51.7(3) 2_765 . ?
N71 K4 O23 62.3(4) 2_765 . ?
N71 K4 N51 70.2(4) 2_765 2_766 ?
N71 K4 N53 84.9(5) 2_765 2_766 ?
N71 K4 C51 71.1(4) 2_765 2_766 ?
N71 K4 C53 79.5(4) 2_765 2_766 ?
C51 K4 K6 102.7(3) 2_766 . ?
C51 K4 K7 104.6(3) 2_766 1_556 ?
C51 K4 K11 86.6(3) 2_766 . ?
C53 K4 K6 57.2(3) 2_766 . ?
C53 K4 K7 90.2(3) 2_766 1_556 ?
C53 K4 K11 53.9(3) 2_766 . ?
C53 K4 C51 48.1(4) 2_766 2_766 ?
K9 K5 K8 57.03(12) . . ?
O17 K5 K8 77.1(3) . . ?
O17 K5 K9 53.1(4) . . ?
O17 K5 O21 105.7(5) . . ?
O17 K5 N13 75.4(4) . . ?
O17 K5 N92 164.1(5) . 2_766 ?
O17 K5 N93 89.5(5) . 1_556 ?
O17 K5 N101 61.4(4) . . ?
O17 K5 N101 122.8(4) . 2_765 ?
O17 K5 C93 100.2(4) . 1_556 ?
O17 K5 C101 67.1(4) . . ?
O17 K5 C101 103.8(5) . 2_765 ?
O21 K5 K8 101.2(4) . . ?
O21 K5 K9 150.3(4) . . ?
O21 K5 N13 61.4(5) . . ?
O21 K5 N92 79.3(5) . 2_766 ?
O21 K5 N101 89.6(5) . 2_765 ?
O21 K5 N101 153.2(5) . . ?
O21 K5 C93 138.1(5) . 1_556 ?
O21 K5 C101 136.5(5) . . ?
O21 K5 C101 99.8(5) . 2_765 ?
N13 K5 K8 42.9(3) . . ?
N13 K5 K9 90.9(3) . . ?
N13 K5 N101 150.2(5) . 2_765 ?
N13 K5 N101 128.6(4) . . ?
N13 K5 C93 95.1(4) . 1_556 ?
N13 K5 C101 159.2(5) . 2_765 ?
N13 K5 C101 141.6(5) . . ?
N92 K5 K8 87.2(4) 2_766 . ?
N92 K5 K9 115.9(4) 2_766 . ?
N92 K5 N13 94.7(5) 2_766 . ?
N92 K5 N101 119.9(5) 2_766 . ?
N92 K5 N101 71.6(5) 2_766 2_765 ?
N92 K5 C93 67.9(4) 2_766 1_556 ?
N92 K5 C101 119.8(5) 2_766 . ?
N92 K5 C101 89.9(5) 2_766 2_765 ?
N93 K5 K8 37.4(4) 1_556 . ?
N93 K5 K9 41.9(4) 1_556 . ?
N93 K5 O21 132.0(6) 1_556 . ?
N93 K5 N13 80.0(5) 1_556 . ?
N93 K5 N92 76.5(5) 1_556 2_766 ?
N93 K5 N101 73.6(5) 1_556 . ?
N93 K5 N101 120.1(5) 1_556 2_765 ?
N93 K5 C93 16.7(4) 1_556 1_556 ?
N93 K5 C101 91.4(6) 1_556 . ?
N93 K5 C101 120.8(5) 1_556 2_765 ?
N101 K5 K8 98.4(3) . . ?
N101 K5 K8 154.1(3) 2_765 . ?
N101 K5 K9 118.8(3) 2_765 . ?
N101 K5 K9 41.5(3) . . ?
N101 K5 N101 80.4(6) 2_765 . ?
N101 K5 C93 103.4(4) 2_765 1_556 ?
N101 K5 C93 68.7(4) . 1_556 ?
N101 K5 C101 64.7(5) 2_765 . ?
N101 K5 C101 64.4(5) . 2_765 ?
N101 K5 C101 19.4(4) 2_765 2_765 ?
N101 K5 C101 19.0(4) . . ?
C93 K5 K8 53.4(3) 1_556 . ?
C93 K5 K9 48.0(3) 1_556 . ?
C101 K5 K8 157.9(4) 2_765 . ?
C101 K5 K8 117.3(4) . . ?
C101 K5 K9 60.3(4) . . ?
C101 K5 K9 105.3(4) 2_765 . ?
C101 K5 C93 105.4(4) 2_765 1_556 ?
C101 K5 C93 84.0(4) . 1_556 ?
C101 K5 C101 46.9(7) 2_765 . ?
K7 K6 K17 138.05(13) 1_556 . ?
O22 K6 K7 43.1(3) 1_556 1_556 ?
O22 K6 K17 141.4(3) 1_556 . ?
O22 K6 O24 98.8(4) 1_556 1_556 ?
O22 K6 N21 130.1(4) 1_556 . ?
O22 K6 N22 80.8(4) 1_556 . ?
O22 K6 N41 61.5(4) 1_556 1_556 ?
O22 K6 C21 123.6(4) 1_556 . ?
O22 K6 C22 95.1(4) 1_556 . ?
O24 K6 K7 110.0(3) 1_556 1_556 ?
O24 K6 K17 42.7(3) 1_556 . ?
O24 K6 C21 76.6(4) 1_556 . ?
O26 K6 K7 145.3(4) . 1_556 ?
O26 K6 K17 68.5(4) . . ?
O26 K6 O22 102.5(5) . 1_556 ?
O26 K6 O24 73.5(5) . 1_556 ?
O26 K6 N21 111.3(5) . . ?
O26 K6 N22 151.6(5) . . ?
O26 K6 N41 121.2(5) . 1_556 ?
O26 K6 C21 127.9(5) . . ?
O26 K6 C22 157.0(5) . . ?
O27 K6 K7 130.2(3) . 1_556 ?
O27 K6 K17 65.9(3) . . ?
O27 K6 O22 151.0(4) . 1_556 ?
O27 K6 O24 108.3(4) . 1_556 ?
O27 K6 O26 76.2(5) . . ?
O27 K6 N21 74.7(4) . . ?
O27 K6 N22 87.4(4) . . ?
O27 K6 N41 144.1(5) . 1_556 ?
O27 K6 N53 77.5(4) . 2_766 ?
O27 K6 C21 74.1(4) . . ?
O27 K6 C22 81.2(4) . . ?
N21 K6 K7 98.9(3) . 1_556 ?
N21 K6 K17 42.9(3) . . ?
N21 K6 O24 59.5(4) . 1_556 ?
N21 K6 C21 19.0(4) . . ?
N21 K6 C22 66.1(4) . . ?
N22 K6 K7 42.8(3) . 1_556 ?
N22 K6 K17 125.5(3) . . ?
N22 K6 O24 134.4(4) . 1_556 ?
N22 K6 N21 85.8(4) . . ?
N22 K6 C21 66.8(5) . . ?
N22 K6 C22 19.7(4) . . ?
N41 K6 K7 53.7(4) 1_556 1_556 ?
N41 K6 K17 90.3(4) 1_556 . ?
N41 K6 O24 56.5(5) 1_556 1_556 ?
N41 K6 N21 69.6(5) 1_556 . ?
N41 K6 N22 85.5(5) 1_556 . ?
N41 K6 C21 70.7(5) 1_556 . ?
N41 K6 C22 80.3(5) 1_556 . ?
N53 K6 K7 88.2(4) 2_766 1_556 ?
N53 K6 K17 132.9(4) 2_766 . ?
N53 K6 O22 74.2(4) 2_766 1_556 ?
N53 K6 O24 145.4(5) 2_766 1_556 ?
N53 K6 O26 75.0(5) 2_766 . ?
N53 K6 N21 148.8(4) 2_766 . ?
N53 K6 N22 78.9(5) 2_766 . ?
N53 K6 N41 134.9(5) 2_766 1_556 ?
N53 K6 C21 135.9(5) 2_766 . ?
N53 K6 C22 95.9(4) 2_766 . ?
C21 K6 K7 85.1(3) . 1_556 ?
C21 K6 K17 60.6(3) . . ?
C22 K6 K7 52.8(3) . 1_556 ?
C22 K6 K17 106.2(3) . . ?
C22 K6 O24 118.7(4) . 1_556 ?
C22 K6 C21 47.1(4) . . ?
Se4 K7 K8 88.64(15) . 1_554 ?
O18 K7 Se4 68.8(6) . . ?
O18 K7 K8 45.5(4) . 1_554 ?
O18 K7 O22 111.1(5) . . ?
O18 K7 N13 81.7(6) . 1_554 ?
O18 K7 N22 146.7(7) . 1_554 ?
O18 K7 N41 134.5(7) . . ?
O18 K7 N43 73.4(6) . . ?
O18 K7 C22 149.8(6) . 1_554 ?
O18 K7 C41 115.7(7) . . ?
O18 K7 C43 78.8(6) . . ?
O20 K7 Se4 110.5(3) 1_554 . ?
O20 K7 K8 109.3(3) 1_554 1_554 ?
O20 K7 O18 78.4(6) 1_554 . ?
O20 K7 O22 72.6(4) 1_554 . ?
O20 K7 N13 92.1(4) 1_554 1_554 ?
O20 K7 N22 78.0(4) 1_554 1_554 ?
O20 K7 N41 125.2(4) 1_554 . ?
O20 K7 N43 150.2(4) 1_554 . ?
O20 K7 C22 95.3(4) 1_554 1_554 ?
O20 K7 C41 136.5(4) 1_554 . ?
O20 K7 C43 154.8(5) 1_554 . ?
O22 K7 Se4 65.8(3) . . ?
O22 K7 K8 152.2(3) . 1_554 ?
O22 K7 N13 156.7(5) . 1_554 ?
O22 K7 N41 56.0(4) . . ?
O22 K7 N43 127.0(4) . . ?
O22 K7 C22 94.5(4) . 1_554 ?
O22 K7 C41 63.9(4) . . ?
O22 K7 C43 106.2(4) . . ?
N13 K7 Se4 137.4(3) 1_554 . ?
N13 K7 K8 49.2(3) 1_554 1_554 ?
N13 K7 N41 128.5(4) 1_554 . ?
N13 K7 C22 68.9(4) 1_554 1_554 ?
N13 K7 C41 129.4(5) 1_554 . ?
N13 K7 C43 95.2(5) 1_554 . ?
N22 K7 Se4 142.3(3) 1_554 . ?
N22 K7 K8 124.3(4) 1_554 1_554 ?
N22 K7 O22 83.4(4) 1_554 . ?
N22 K7 N13 76.1(4) 1_554 1_554 ?
N22 K7 N41 78.7(4) 1_554 . ?
N22 K7 N43 122.5(5) 1_554 . ?
N22 K7 C22 18.4(4) 1_554 1_554 ?
N22 K7 C41 97.6(4) 1_554 . ?
N22 K7 C43 127.2(5) 1_554 . ?
N41 K7 Se4 66.4(3) . . ?
N41 K7 K8 124.8(3) . 1_554 ?
N41 K7 C22 73.1(4) . 1_554 ?
N41 K7 C41 19.8(4) . . ?
N43 K7 Se4 68.0(3) . . ?
N43 K7 K8 42.2(3) . 1_554 ?
N43 K7 N13 74.6(5) . 1_554 ?
N43 K7 N41 82.6(4) . . ?
N43 K7 C22 104.2(4) . 1_554 ?
N43 K7 C41 67.1(4) . . ?
N43 K7 C43 20.8(4) . . ?
C22 K7 Se4 139.3(3) 1_554 . ?
C22 K7 K8 112.6(3) 1_554 1_554 ?
C22 K7 C41 89.4(4) 1_554 . ?
C41 K7 Se4 50.2(3) . . ?
C41 K7 K8 108.6(3) . 1_554 ?
C43 K7 Se4 50.4(3) . . ?
C43 K7 K8 59.9(3) . 1_554 ?
C43 K7 N41 66.7(4) . . ?
C43 K7 C22 109.9(4) . 1_554 ?
C43 K7 C41 48.9(4) . . ?
K5 K8 K1 137.5(2) . 1_556 ?
K7 K8 K1 85.21(14) 1_556 1_556 ?
K7 K8 K5 74.79(14) 1_556 . ?
K7 K8 K9 133.3(2) 1_556 . ?
K9 K8 K1 130.8(2) . 1_556 ?
K9 K8 K5 58.54(12) . . ?
O1 K8 K1 37.2(4) 1_556 1_556 ?
O1 K8 K5 167.0(5) 1_556 . ?
O1 K8 K7 112.2(4) 1_556 1_556 ?
O1 K8 K9 114.1(4) 1_556 . ?
O1 K8 N13 131.8(6) 1_556 . ?
O14 K8 K1 107.6(5) . 1_556 ?
O14 K8 K5 104.9(5) . . ?
O14 K8 K7 157.0(5) . 1_556 ?
O14 K8 K9 50.6(5) . . ?
O14 K8 O1 73.2(6) . 1_556 ?
O14 K8 O15 73.9(6) . . ?
O14 K8 O18 113.7(6) . 1_556 ?
O14 K8 N13 143.9(6) . . ?
O14 K8 N93 73.3(6) . 1_556 ?
O15 K8 K1 92.4(4) . 1_556 ?
O15 K8 K5 71.2(4) . . ?
O15 K8 K7 125.7(4) . 1_556 ?
O15 K8 K9 42.8(4) . . ?
O15 K8 O1 96.2(6) . 1_556 ?
O15 K8 N13 77.3(5) . . ?
O18 K8 K1 114.5(5) 1_556 1_556 ?
O18 K8 K5 74.9(6) 1_556 . ?
O18 K8 K7 43.5(4) 1_556 1_556 ?
O18 K8 K9 114.7(6) 1_556 . ?
O18 K8 O1 117.8(7) 1_556 1_556 ?
O18 K8 O15 146.0(7) 1_556 . ?
O18 K8 N13 80.1(6) 1_556 . ?
N13 K8 K1 94.7(4) . 1_556 ?
N13 K8 K5 44.2(3) . . ?
N13 K8 K7 49.1(3) . 1_556 ?
N13 K8 K9 93.3(4) . . ?
N43 K8 K1 40.5(4) 1_556 1_556 ?
N43 K8 K5 118.0(4) 1_556 . ?
N43 K8 K7 46.9(4) 1_556 1_556 ?
N43 K8 K9 165.5(5) 1_556 . ?
N43 K8 O1 66.1(5) 1_556 1_556 ?
N43 K8 O14 136.8(6) 1_556 . ?
N43 K8 O15 123.1(6) 1_556 . ?
N43 K8 O18 75.4(6) 1_556 1_556 ?
N43 K8 N13 77.8(5) 1_556 . ?
N43 K8 N93 143.4(6) 1_556 1_556 ?
N93 K8 K1 171.4(5) 1_556 1_556 ?
N93 K8 K5 36.7(4) 1_556 . ?
N93 K8 K7 96.9(4) 1_556 1_556 ?
N93 K8 K9 43.1(4) 1_556 . ?
N93 K8 O1 146.1(6) 1_556 1_556 ?
N93 K8 O15 79.5(6) 1_556 . ?
N93 K8 O18 72.0(7) 1_556 1_556 ?
N93 K8 N13 80.5(5) 1_556 . ?
K8 K9 K5 64.42(14) . . ?
K10 K9 K5 118.86(16) . . ?
K10 K9 K8 84.28(17) . . ?
O14 K9 K5 101.4(3) . . ?
O14 K9 K8 40.7(3) . . ?
O14 K9 K10 79.8(3) . . ?
O14 K9 C92 86.1(4) . 1_556 ?
O15 K9 K5 75.8(4) . . ?
O15 K9 K8 44.2(4) . . ?
O15 K9 K10 47.7(4) . . ?
O15 K9 O14 67.6(5) . . ?
O15 K9 O16 81.0(5) . . ?
O15 K9 N92 163.0(5) . 1_556 ?
O15 K9 N93 80.3(5) . 1_556 ?
O15 K9 C92 146.0(5) . 1_556 ?
O15 K9 C93 99.5(5) . 1_556 ?
O16 K9 K5 113.2(3) . . ?
O16 K9 K8 125.0(4) . . ?
O16 K9 K10 46.8(3) . . ?
O16 K9 O14 125.3(5) . . ?
O16 K9 N92 114.0(5) . 1_556 ?
O16 K9 C92 132.9(5) . 1_556 ?
O16 K9 C93 164.9(5) . 1_556 ?
N51 K9 K5 159.6(4) 1_556 . ?
N51 K9 K8 95.5(3) 1_556 . ?
N51 K9 K10 51.6(3) 1_556 . ?
N51 K9 O14 60.9(4) 1_556 . ?
N51 K9 O15 87.3(5) 1_556 . ?
N51 K9 O16 74.4(4) 1_556 . ?
N51 K9 N92 89.1(4) 1_556 1_556 ?
N51 K9 N93 126.0(5) 1_556 1_556 ?
N51 K9 N101 149.5(5) 1_556 . ?
N51 K9 C92 98.8(4) 1_556 1_556 ?
N51 K9 C93 120.6(5) 1_556 1_556 ?
N92 K9 K5 103.7(3) 1_556 . ?
N92 K9 K8 119.8(4) 1_556 . ?
N92 K9 K10 137.3(3) 1_556 . ?
N92 K9 O14 96.2(5) 1_556 . ?
N92 K9 C92 19.5(4) 1_556 1_556 ?
N92 K9 C93 68.2(5) 1_556 1_556 ?
N93 K9 K5 40.6(4) 1_556 . ?
N93 K9 K8 42.6(4) 1_556 . ?
N93 K9 K10 126.1(4) 1_556 . ?
N93 K9 O14 65.7(5) 1_556 . ?
N93 K9 O16 151.3(5) 1_556 . ?
N93 K9 N92 88.4(5) 1_556 1_556 ?
N93 K9 C92 69.0(5) 1_556 1_556 ?
N93 K9 C93 20.3(5) 1_556 1_556 ?
N101 K9 K5 50.8(4) . . ?
N101 K9 K8 115.0(4) . . ?
N101 K9 K10 129.0(4) . . ?
N101 K9 O14 145.5(5) . . ?
N101 K9 O15 114.9(5) . . ?
N101 K9 O16 88.0(5) . . ?
N101 K9 N92 75.3(5) . 1_556 ?
N101 K9 N93 80.4(5) . 1_556 ?
N101 K9 C92 75.0(4) . 1_556 ?
N101 K9 C93 78.1(5) . 1_556 ?
C92 K9 K5 89.4(3) 1_556 . ?
C92 K9 K8 101.8(4) 1_556 . ?
C92 K9 K10 150.3(3) 1_556 . ?
C93 K9 K5 53.1(3) 1_556 . ?
C93 K9 K8 58.1(3) 1_556 . ?
C93 K9 K10 141.9(3) 1_556 . ?
C93 K9 O14 67.8(4) 1_556 . ?
C93 K9 C92 48.8(5) 1_556 1_556 ?
K9 K10 Se8 119.55(14) . . ?
O13 K10 Se8 66.1(4) . . ?
O13 K10 K9 118.9(4) . . ?
O13 K10 N51 158.1(5) . 1_556 ?
O13 K10 N71 130.9(5) . . ?
O13 K10 N72 63.2(5) . . ?
O13 K10 C71 110.3(5) . . ?
O13 K10 C72 70.3(4) . . ?
O13 K10 C83 100.2(5) . 1_556 ?
O15 K10 Se8 120.6(4) . . ?
O15 K10 K9 49.0(4) . . ?
O15 K10 O13 74.9(5) . . ?
O15 K10 N51 84.9(5) . 1_556 ?
O15 K10 N71 144.0(5) . . ?
O15 K10 N72 128.5(5) . . ?
O15 K10 C71 158.0(5) . . ?
O15 K10 C72 143.9(5) . . ?
O15 K10 C83 85.9(5) . 1_556 ?
O16 K10 Se8 71.2(4) . . ?
O16 K10 K9 50.3(4) . . ?
O16 K10 O13 111.7(5) . . ?
O16 K10 O15 84.8(6) . . ?
O16 K10 N51 74.0(4) . 1_556 ?
O16 K10 N71 63.5(5) . . ?
O16 K10 N72 137.0(5) . . ?
O16 K10 N83 142.7(5) . 1_556 ?
O16 K10 C71 73.4(5) . . ?
O16 K10 C72 116.8(5) . . ?
O16 K10 C83 143.0(5) . 1_556 ?
N51 K10 Se8 133.7(3) 1_556 . ?
N51 K10 K9 47.4(3) 1_556 . ?
N51 K10 N72 127.9(4) 1_556 . ?
N51 K10 C71 91.6(4) 1_556 . ?
N51 K10 C72 127.3(4) 1_556 . ?
N51 K10 C83 69.5(4) 1_556 1_556 ?
N71 K10 Se8 66.7(3) . . ?
N71 K10 K9 95.6(3) . . ?
N71 K10 N51 70.9(4) . 1_556 ?
N71 K10 N72 87.5(5) . . ?
N71 K10 C71 21.3(4) . . ?
N71 K10 C72 70.5(4) . . ?
N71 K10 C83 108.8(5) . 1_556 ?
N72 K10 Se8 68.2(3) . . ?
N72 K10 K9 172.2(4) . . ?
N72 K10 C71 69.9(4) . . ?
N72 K10 C72 20.5(4) . . ?
N72 K10 C83 74.2(4) . 1_556 ?
N83 K10 Se8 145.4(4) 1_556 . ?
N83 K10 K9 92.6(4) 1_556 . ?
N83 K10 O13 88.1(5) 1_556 . ?
N83 K10 O15 69.9(5) 1_556 . ?
N83 K10 N51 76.9(5) 1_556 1_556 ?
N83 K10 N71 126.5(5) 1_556 . ?
N83 K10 N72 79.9(5) 1_556 . ?
N83 K10 C71 130.4(5) 1_556 . ?
N83 K10 C72 99.3(5) 1_556 . ?
N83 K10 C83 17.9(4) 1_556 1_556 ?
C71 K10 Se8 49.8(3) . . ?
C71 K10 K9 114.5(3) . . ?
C71 K10 C72 51.0(4) . . ?
C71 K10 C83 113.2(4) . 1_556 ?
C72 K10 Se8 51.6(3) . . ?
C72 K10 K9 165.3(3) . . ?
C72 K10 C83 90.9(4) . 1_556 ?
C83 K10 Se8 142.2(3) 1_556 . ?
C83 K10 K9 98.1(3) 1_556 . ?
O11 K11 Se5 66.8(4) . 2_765 ?
O11 K11 O23 107.8(5) . . ?
O11 K11 O27 79.5(4) . . ?
O11 K11 N53 147.6(5) . 2_766 ?
O11 K11 N63 84.6(5) . 2_766 ?
O11 K11 N71 133.1(5) . 2_765 ?
O11 K11 N73 74.4(5) . 2_765 ?
O11 K11 C53 152.2(5) . 2_766 ?
O11 K11 C63 99.6(5) . 2_766 ?
O11 K11 C71 114.1(5) . 2_765 ?
O11 K11 C73 78.7(5) . 2_765 ?
O23 K11 Se5 65.6(3) . 2_765 ?
O23 K11 N53 82.8(4) . 2_766 ?
O23 K11 N63 156.0(5) . 2_766 ?
O23 K11 N71 58.0(4) . 2_765 ?
O23 K11 N73 127.3(4) . 2_765 ?
O23 K11 C53 94.5(4) . 2_766 ?
O23 K11 C63 150.7(4) . 2_766 ?
O23 K11 C71 65.4(4) . 2_765 ?
O23 K11 C73 106.3(4) . 2_765 ?
O27 K11 Se5 109.3(3) . 2_765 ?
O27 K11 O23 69.2(4) . . ?
O27 K11 N53 75.9(4) . 2_766 ?
O27 K11 N63 93.8(4) . 2_766 ?
O27 K11 N71 123.5(4) . 2_765 ?
O27 K11 N73 152.5(4) . 2_765 ?
O27 K11 C53 93.7(4) . 2_766 ?
O27 K11 C63 106.8(4) . 2_766 ?
O27 K11 C71 134.6(4) . 2_765 ?
O27 K11 C73 155.0(4) . 2_765 ?
N53 K11 Se5 142.0(3) 2_766 2_765 ?
N53 K11 N63 76.5(5) 2_766 2_766 ?
N53 K11 N71 78.8(4) 2_766 2_765 ?
N53 K11 N73 124.1(5) 2_766 2_765 ?
N53 K11 C53 18.7(4) 2_766 2_766 ?
N53 K11 C63 68.4(4) 2_766 2_766 ?
N53 K11 C71 98.2(4) 2_766 2_765 ?
N53 K11 C73 128.8(4) 2_766 2_765 ?
N63 K11 Se5 138.0(3) 2_766 2_765 ?
N63 K11 N71 127.5(4) 2_766 2_765 ?
N63 K11 N73 75.3(4) 2_766 2_765 ?
N63 K11 C53 68.9(4) 2_766 2_766 ?
N63 K11 C63 18.3(4) 2_766 2_766 ?
N63 K11 C71 129.1(4) 2_766 2_765 ?
N63 K11 C73 96.1(5) 2_766 2_765 ?
N71 K11 Se5 66.9(3) 2_765 2_765 ?
N71 K11 C53 72.9(4) 2_765 2_766 ?
N71 K11 C63 109.2(4) 2_765 2_766 ?
N71 K11 C71 20.1(4) 2_765 2_765 ?
N71 K11 C73 66.1(4) 2_765 2_765 ?
N73 K11 Se5 68.0(3) 2_765 2_765 ?
N73 K11 N71 81.8(4) 2_765 2_765 ?
N73 K11 C53 105.3(4) 2_765 2_766 ?
N73 K11 C63 69.8(4) 2_765 2_766 ?
N73 K11 C71 66.3(4) 2_765 2_765 ?
N73 K11 C73 21.0(4) 2_765 2_765 ?
C53 K11 Se5 139.8(3) 2_766 2_765 ?
C53 K11 C63 56.3(4) 2_766 2_766 ?
C63 K11 Se5 137.7(3) 2_766 2_765 ?
C71 K11 Se5 50.4(3) 2_765 2_765 ?
C71 K11 C53 90.0(4) 2_765 2_766 ?
C71 K11 C63 112.6(4) 2_765 2_766 ?
C73 K11 Se5 50.1(3) 2_765 2_765 ?
C73 K11 C53 111.3(4) 2_765 2_766 ?
C73 K11 C63 88.8(4) 2_765 2_766 ?
C73 K11 C71 48.1(4) 2_765 2_765 ?
K1 K12 K14 146.04(14) 1_556 2_775 ?
K1 K12 K15 105.75(13) 1_556 2_775 ?
K10 K12 K1 112.52(14) . 1_556 ?
K10 K12 K14 82.17(11) . 2_775 ?
K10 K12 K15 132.13(14) . 2_775 ?
K15 K12 K14 50.45(10) 2_775 2_775 ?
O3 K12 K1 39.3(3) . 1_556 ?
O3 K12 K10 127.6(3) . . ?
O3 K12 K14 107.2(3) . 2_775 ?
O3 K12 K15 70.9(3) . 2_775 ?
O3 K12 O4 80.5(4) . . ?
O3 K12 O13 150.0(4) . . ?
O3 K12 N11 82.2(5) . . ?
O3 K12 N72 139.4(5) . . ?
O3 K12 N83 82.0(4) . 1_556 ?
O3 K12 C83 76.0(4) . 1_556 ?
O4 K12 K1 79.6(4) . 1_556 ?
O4 K12 K10 148.8(4) . . ?
O4 K12 K14 103.9(4) . 2_775 ?
O4 K12 K15 64.4(4) . 2_775 ?
O4 K12 O13 103.2(5) . . ?
O4 K12 N11 91.4(5) . . ?
O4 K12 N72 119.0(5) . . ?
O4 K12 N83 158.3(5) . 1_556 ?
O4 K12 C83 156.0(5) . 1_556 ?
O13 K12 K1 111.3(3) . 1_556 ?
O13 K12 K10 45.8(4) . . ?
O13 K12 K14 100.8(3) . 2_775 ?
O13 K12 K15 137.9(3) . 2_775 ?
O13 K12 N11 68.1(5) . . ?
O13 K12 C83 99.7(5) . 1_556 ?
N11 K12 K1 43.3(4) . 1_556 ?
N11 K12 K10 81.0(4) . . ?
N11 K12 K14 163.1(4) . 2_775 ?
N11 K12 K15 145.9(4) . 2_775 ?
N11 K12 C83 90.5(5) . 1_556 ?
N72 K12 K1 161.3(4) . 1_556 ?
N72 K12 K10 50.9(4) . . ?
N72 K12 K14 36.9(3) . 2_775 ?
N72 K12 K15 85.5(4) . 2_775 ?
N72 K12 O13 64.9(5) . . ?
N72 K12 N11 128.3(5) . . ?
N72 K12 C83 77.5(5) . 1_556 ?
N83 K12 K1 78.8(3) 1_556 1_556 ?
N83 K12 K10 45.6(3) 1_556 . ?
N83 K12 K14 93.5(3) 1_556 2_775 ?
N83 K12 K15 121.1(3) 1_556 2_775 ?
N83 K12 O13 85.7(5) 1_556 . ?
N83 K12 N11 73.5(5) 1_556 . ?
N83 K12 N72 82.7(5) 1_556 . ?
N83 K12 C83 18.8(4) 1_556 1_556 ?
C83 K12 K1 85.5(3) 1_556 1_556 ?
C83 K12 K10 55.0(3) 1_556 . ?
C83 K12 K14 78.5(3) 1_556 2_775 ?
C83 K12 K15 102.4(3) 1_556 2_775 ?
O4 K13 K2 100.5(4) . . ?
O4 K13 O5 104.7(5) . . ?
O4 K13 N33 56.9(5) . . ?
O4 K13 N131 136.9(5) . 1_556 ?
O4 K13 N133 79.7(5) . 2_776 ?
O4 K13 N141 85.6(5) . . ?
O4 K13 N141 148.3(5) . 3_575 ?
O4 K13 C131 143.2(5) . 1_556 ?
O4 K13 C133 97.4(5) . 2_776 ?
O4 K13 C141 131.7(5) . 3_575 ?
O4 K13 C141 95.3(5) . . ?
O5 K13 K2 74.1(3) . . ?
O5 K13 N33 78.3(4) . . ?
O5 K13 N133 160.3(5) . 2_776 ?
O5 K13 N141 59.6(4) . 3_575 ?
O5 K13 N141 124.1(5) . . ?
O5 K13 C131 96.5(4) . 1_556 ?
O5 K13 C133 153.5(5) . 2_776 ?
O5 K13 C141 104.5(4) . . ?
O5 K13 C141 66.0(4) . 3_575 ?
N33 K13 K2 44.8(4) . . ?
N33 K13 N141 133.4(5) . 3_575 ?
N33 K13 C131 99.8(4) . 1_556 ?
N33 K13 C133 102.5(4) . 2_776 ?
N33 K13 C141 144.3(4) . 3_575 ?
N131 K13 K2 40.1(3) 1_556 . ?
N131 K13 O5 83.5(5) 1_556 . ?
N131 K13 N33 84.7(5) 1_556 . ?
N131 K13 N133 80.6(4) 1_556 2_776 ?
N131 K13 N141 72.2(5) 1_556 3_575 ?
N131 K13 N141 125.2(5) 1_556 . ?
N131 K13 C131 18.2(4) 1_556 1_556 ?
N131 K13 C133 70.3(4) 1_556 2_776 ?
N131 K13 C141 90.6(4) 1_556 3_575 ?
N131 K13 C141 124.1(5) 1_556 . ?
N133 K13 K2 86.2(3) 2_776 . ?
N133 K13 N33 88.7(5) 2_776 . ?
N133 K13 N141 75.0(5) 2_776 . ?
N133 K13 N141 125.0(5) 2_776 3_575 ?
N133 K13 C131 71.1(4) 2_776 1_556 ?
N133 K13 C133 18.4(4) 2_776 2_776 ?
N133 K13 C141 94.1(5) 2_776 . ?
N133 K13 C141 125.5(4) 2_776 3_575 ?
N141 K13 K2 159.0(4) . . ?
N141 K13 K2 100.7(3) 3_575 . ?
N141 K13 N33 141.5(5) . . ?
N141 K13 N141 83.0(6) . 3_575 ?
N141 K13 C131 107.1(4) . 1_556 ?
N141 K13 C131 68.4(4) 3_575 1_556 ?
N141 K13 C133 71.5(4) . 2_776 ?
N141 K13 C133 106.7(4) 3_575 2_776 ?
N141 K13 C141 20.1(4) . . ?
N141 K13 C141 19.3(4) 3_575 3_575 ?
N141 K13 C141 66.9(5) . 3_575 ?
C131 K13 K2 56.7(3) 1_556 . ?
C133 K13 K2 87.7(3) 2_776 . ?
C133 K13 C131 57.1(4) 2_776 1_556 ?
C141 K13 K2 163.9(3) . . ?
C141 K13 K2 119.5(3) 3_575 . ?
C141 K13 N33 151.2(5) . . ?
C141 K13 N141 66.1(4) . 3_575 ?
C141 K13 C131 108.2(4) . 1_556 ?
C141 K13 C131 84.3(4) 3_575 1_556 ?
C141 K13 C133 109.2(4) 3_575 2_776 ?
C141 K13 C133 87.6(4) . 2_776 ?
C141 K13 C141 48.3(6) . 3_575 ?
O7 K14 K15 45.9(3) . . ?
O7 K14 N72 133.0(5) . 3_575 ?
O7 K14 N73 144.7(5) . 3_575 ?
O7 K14 N82 77.3(5) . 3_576 ?
O7 K14 C62 92.3(6) . 3_576 ?
O7 K14 C72 147.4(5) . 3_575 ?
O7 K14 C73 157.5(5) . 3_575 ?
O7 K14 C82 90.8(5) . 3_576 ?
O9 K14 K15 121.6(4) . . ?
O9 K14 O7 78.0(5) . . ?
O9 K14 N62 77.2(5) . 3_576 ?
O9 K14 N72 138.8(5) . 3_575 ?
O9 K14 N73 71.2(5) . 3_575 ?
O9 K14 N82 148.9(6) . 3_576 ?
O9 K14 C62 90.8(5) . 3_576 ?
O9 K14 C72 119.8(5) . 3_575 ?
O9 K14 C73 79.6(5) . 3_575 ?
O9 K14 C82 147.0(5) . 3_576 ?
O12 K14 K15 45.7(3) . . ?
O12 K14 O7 78.4(5) . . ?
O12 K14 O9 120.3(6) . . ?
O12 K14 N62 146.5(5) . 3_576 ?
O12 K14 N72 58.9(5) . 3_575 ?
O12 K14 N73 132.4(5) . 3_575 ?
O12 K14 N82 72.3(5) . 3_576 ?
O12 K14 C62 143.9(5) . 3_576 ?
O12 K14 C72 69.1(4) . 3_575 ?
O12 K14 C73 111.5(5) . 3_575 ?
O12 K14 C82 86.7(4) . 3_576 ?
N62 K14 K15 101.1(4) 3_576 . ?
N62 K14 O7 78.1(6) 3_576 . ?
N62 K14 N72 128.3(5) 3_576 3_575 ?
N62 K14 N73 78.6(5) 3_576 3_575 ?
N62 K14 N82 79.5(5) 3_576 3_576 ?
N62 K14 C62 18.0(5) 3_576 3_576 ?
N62 K14 C72 130.1(5) 3_576 3_575 ?
N62 K14 C73 99.1(5) 3_576 3_575 ?
N62 K14 C82 70.1(5) 3_576 3_576 ?
N72 K14 K15 88.0(3) 3_575 . ?
N72 K14 C62 110.3(5) 3_575 3_576 ?
N72 K14 C72 19.6(4) 3_575 3_575 ?
N72 K14 C73 65.9(5) 3_575 3_575 ?
N72 K14 C82 69.7(4) 3_575 3_576 ?
N73 K14 K15 167.0(4) 3_575 . ?
N73 K14 N72 82.3(5) 3_575 3_575 ?
N73 K14 C62 71.7(5) 3_575 3_576 ?
N73 K14 C72 66.4(4) 3_575 3_575 ?
N73 K14 C73 20.9(4) 3_575 3_575 ?
N73 K14 C82 105.7(5) 3_575 3_576 ?
N82 K14 K15 44.4(3) 3_576 . ?
N82 K14 N72 72.2(5) 3_576 3_575 ?
N82 K14 N73 123.6(5) 3_576 3_575 ?
N82 K14 C62 71.7(5) 3_576 3_576 ?
N82 K14 C72 91.0(5) 3_576 3_575 ?
N82 K14 C73 124.5(5) 3_576 3_575 ?
N82 K14 C82 18.2(4) 3_576 3_576 ?
C62 K14 K15 104.1(4) 3_576 . ?
C62 K14 C82 58.4(4) 3_576 3_576 ?
C72 K14 K15 105.6(3) 3_575 . ?
C72 K14 C62 113.0(5) 3_575 3_576 ?
C72 K14 C82 85.9(4) 3_575 3_576 ?
C73 K14 K15 153.4(4) 3_575 . ?
C73 K14 C62 90.2(5) 3_575 3_576 ?
C73 K14 C72 47.9(4) 3_575 3_575 ?
C73 K14 C82 109.4(4) 3_575 3_576 ?
C82 K14 K15 62.6(3) 3_576 . ?
K12 K15 K2 146.45(15) 3_575 . ?
K14 K15 K2 82.87(14) . . ?
K14 K15 K12 72.64(12) . 3_575 ?
O5 K15 K2 67.7(3) . . ?
O5 K15 K12 129.9(3) . 3_575 ?
O5 K15 K14 84.3(3) . . ?
O5 K15 C131 89.7(4) . 1_556 ?
O5 K15 C133 123.7(4) . 1_556 ?
O7 K15 K2 41.3(4) . . ?
O7 K15 K12 118.8(4) . 3_575 ?
O7 K15 K14 46.1(4) . . ?
O7 K15 O5 55.7(5) . . ?
O7 K15 N131 76.9(5) . 1_556 ?
O7 K15 N133 156.5(5) . 1_556 ?
O7 K15 C131 95.9(5) . 1_556 ?
O7 K15 C133 139.7(5) . 1_556 ?
O12 K15 K2 119.6(4) . . ?
O12 K15 K12 55.2(3) . 3_575 ?
O12 K15 K14 45.4(3) . . ?
O12 K15 O5 76.9(4) . . ?
O12 K15 O7 78.4(5) . . ?
O12 K15 N131 148.6(5) . 1_556 ?
O12 K15 N133 122.7(5) . 1_556 ?
O12 K15 C131 166.4(5) . 1_556 ?
O12 K15 C133 141.6(5) . 1_556 ?
N82 K15 K2 93.8(4) 3_576 . ?
N82 K15 K12 52.7(4) 3_576 3_575 ?
N82 K15 K14 47.8(4) 3_576 . ?
N82 K15 O5 131.2(5) 3_576 . ?
N82 K15 O7 80.1(6) 3_576 . ?
N82 K15 O12 74.5(5) 3_576 . ?
N82 K15 N131 119.2(5) 3_576 1_556 ?
N82 K15 N133 94.9(5) 3_576 1_556 ?
N82 K15 N141 160.0(6) 3_576 3_575 ?
N82 K15 C131 117.0(5) 3_576 1_556 ?
N82 K15 C133 103.0(5) 3_576 1_556 ?
N131 K15 K2 37.9(3) 1_556 . ?
N131 K15 K12 156.1(3) 1_556 3_575 ?
N131 K15 K14 120.7(3) 1_556 . ?
N131 K15 O5 73.4(4) 1_556 . ?
N131 K15 N133 85.9(4) 1_556 1_556 ?
N131 K15 C131 20.3(4) 1_556 1_556 ?
N131 K15 C133 66.6(4) 1_556 1_556 ?
N133 K15 K2 117.1(3) 1_556 . ?
N133 K15 K12 73.5(3) 1_556 3_575 ?
N133 K15 K14 140.5(3) 1_556 . ?
N133 K15 O5 133.9(4) 1_556 . ?
N133 K15 C131 65.7(4) 1_556 1_556 ?
N133 K15 C133 19.4(4) 1_556 1_556 ?
N141 K15 K2 106.2(4) 3_575 . ?
N141 K15 K12 107.3(4) 3_575 3_575 ?
N141 K15 K14 133.8(4) 3_575 . ?
N141 K15 O5 59.9(4) 3_575 . ?
N141 K15 O7 115.2(6) 3_575 . ?
N141 K15 O12 95.2(5) 3_575 . ?
N141 K15 N131 78.4(4) 3_575 1_556 ?
N141 K15 N133 76.0(5) 3_575 1_556 ?
N141 K15 C131 75.9(5) 3_575 1_556 ?
N141 K15 C133 74.2(5) 3_575 1_556 ?
C131 K15 K2 55.2(3) 1_556 . ?
C131 K15 K12 137.0(3) 1_556 3_575 ?
C131 K15 K14 136.3(3) 1_556 . ?
C131 K15 C133 46.3(4) 1_556 1_556 ?
C133 K15 K2 98.7(3) 1_556 . ?
C133 K15 K12 92.2(3) 1_556 3_575 ?
C133 K15 K14 150.6(3) 1_556 . ?
K11 K16 K14 82.48(13) 2_665 . ?
K11 K16 K18 63.99(11) 2_665 2_665 ?
K14 K16 K18 122.09(17) . 2_665 ?
K17 K16 K11 121.69(16) . 2_665 ?
K17 K16 K14 122.50(17) . . ?
K17 K16 K18 58.15(10) . 2_665 ?
O9 K16 K11 118.4(4) . 2_665 ?
O9 K16 K14 37.6(4) . . ?
O9 K16 K17 106.5(4) . . ?
O9 K16 K18 147.2(5) . 2_665 ?
O9 K16 O11 140.6(5) . 2_665 ?
O9 K16 O29 82.7(5) . . ?
O9 K16 N61 78.7(6) . 3_575 ?
O10 K16 K11 158.2(4) . 2_665 ?
O10 K16 K14 118.6(4) . . ?
O10 K16 K17 43.6(3) . . ?
O10 K16 K18 97.5(4) . 2_665 ?
O10 K16 O9 83.4(5) . . ?
O10 K16 O11 125.3(5) . 2_665 ?
O10 K16 O29 71.9(5) . . ?
O10 K16 N61 93.4(5) . 3_575 ?
O10 K16 N73 157.8(5) . 3_575 ?
O10 K16 N113 72.1(5) . . ?
O11 K16 K11 37.4(3) 2_665 2_665 ?
O11 K16 K14 114.5(3) 2_665 . ?
O11 K16 K17 112.9(3) 2_665 . ?
O11 K16 K18 63.2(3) 2_665 2_665 ?
O11 K16 O29 128.6(5) 2_665 . ?
O29 K16 K11 107.9(4) . 2_665 ?
O29 K16 K14 82.5(3) . . ?
O29 K16 K17 42.1(3) . . ?
O29 K16 K18 66.8(4) . 2_665 ?
N61 K16 K11 92.1(4) 3_575 2_665 ?
N61 K16 K14 90.3(4) 3_575 . ?
N61 K16 K17 133.4(4) 3_575 . ?
N61 K16 K18 133.6(4) 3_575 2_665 ?
N61 K16 O11 73.8(5) 3_575 2_665 ?
N61 K16 O29 157.5(6) 3_575 . ?
N73 K16 K11 44.0(4) 3_575 2_665 ?
N73 K16 K14 40.0(4) 3_575 . ?
N73 K16 K17 143.8(4) 3_575 . ?
N73 K16 K18 101.0(4) 3_575 2_665 ?
N73 K16 O9 74.4(5) 3_575 . ?
N73 K16 O11 74.7(5) 3_575 2_665 ?
N73 K16 O29 104.4(5) 3_575 . ?
N73 K16 N61 82.7(5) 3_575 3_575 ?
N73 K16 N113 129.2(5) 3_575 . ?
N113 K16 K11 86.4(4) . 2_665 ?
N113 K16 K14 152.4(4) . . ?
N113 K16 K17 45.9(3) . . ?
N113 K16 K18 31.7(3) . 2_665 ?
N113 K16 O9 152.0(5) . . ?
N113 K16 O11 67.1(5) . 2_665 ?
N113 K16 O29 77.0(5) . . ?
N113 K16 N61 115.4(5) . 3_575 ?
K3 K17 K16 84.50(14) 1_556 . ?
O10 K17 K3 85.1(3) . 1_556 ?
O10 K17 K16 40.9(3) . . ?
O10 K17 O30 122.4(4) . . ?
O10 K17 N111 88.4(4) . . ?
O10 K17 N113 67.6(4) . . ?
O10 K17 C111 79.1(4) . . ?
O10 K17 C113 66.1(4) . . ?
O24 K17 K3 45.1(4) 1_556 1_556 ?
O24 K17 K16 126.5(4) 1_556 . ?
O24 K17 O10 126.7(5) 1_556 . ?
O24 K17 O30 74.6(4) 1_556 . ?
O24 K17 N21 68.1(4) 1_556 . ?
O24 K17 N111 119.9(5) 1_556 . ?
O24 K17 N113 148.8(5) 1_556 . ?
O24 K17 C111 138.5(5) 1_556 . ?
O24 K17 C113 164.1(5) 1_556 . ?
O29 K17 K3 46.1(4) . 1_556 ?
O29 K17 K16 47.1(4) . . ?
O29 K17 O10 73.8(5) . . ?
O29 K17 O24 80.2(6) . 1_556 ?
O29 K17 O30 56.8(5) . . ?
O29 K17 N21 79.2(5) . . ?
O29 K17 N111 159.1(5) . . ?
O29 K17 N113 78.4(5) . . ?
O29 K17 N121 115.3(5) . 1_556 ?
O29 K17 C111 141.3(5) . . ?
O29 K17 C113 96.6(5) . . ?
O30 K17 K3 81.2(3) . 1_556 ?
O30 K17 K16 82.1(3) . . ?
O30 K17 C111 122.2(4) . . ?
O30 K17 C113 90.6(4) . . ?
N21 K17 K3 44.9(3) . 1_556 ?
N21 K17 K16 89.9(3) . . ?
N21 K17 O10 61.9(4) . . ?
N21 K17 O30 126.1(4) . . ?
N21 K17 N111 102.3(4) . . ?
N21 K17 N113 128.6(5) . . ?
N21 K17 C111 111.5(4) . . ?
N21 K17 C113 126.8(4) . . ?
N111 K17 K3 144.9(3) . 1_556 ?
N111 K17 K16 112.0(3) . . ?
N111 K17 O30 130.2(4) . . ?
N111 K17 C111 19.2(4) . . ?
N111 K17 C113 65.6(4) . . ?
N113 K17 K3 123.5(3) . 1_556 ?
N113 K17 K16 42.5(3) . . ?
N113 K17 O30 74.7(4) . . ?
N113 K17 N111 84.9(4) . . ?
N113 K17 C111 65.9(4) . . ?
N113 K17 C113 19.5(4) . . ?
N121 K17 K3 129.9(3) 1_556 1_556 ?
N121 K17 K16 115.8(3) 1_556 . ?
N121 K17 O10 140.8(4) 1_556 . ?
N121 K17 O24 92.3(4) 1_556 1_556 ?
N121 K17 O30 59.3(4) 1_556 . ?
N121 K17 N21 154.1(5) 1_556 . ?
N121 K17 N111 72.1(4) 1_556 . ?
N121 K17 N113 76.9(5) 1_556 . ?
N121 K17 C111 71.5(4) 1_556 . ?
N121 K17 C113 74.9(4) 1_556 . ?
C111 K17 K3 156.4(3) . 1_556 ?
C111 K17 K16 94.6(3) . . ?
C113 K17 K3 139.4(3) . 1_556 ?
C113 K17 K16 54.9(3) . . ?
C113 K17 C111 46.5(4) . . ?
Se14 K18 K17 95.72(11) 3_566 3_565 ?
Se14 K18 K17 94.07(10) 3_566 . ?
K17 K18 K17 144.57(14) 3_565 . ?
O26 K18 Se14 83.8(4) . 3_566 ?
O26 K18 K17 152.5(4) . 3_565 ?
O26 K18 K17 62.5(4) . . ?
O26 K18 N63 62.3(5) . 2_766 ?
O26 K18 N111 80.8(5) . . ?
O26 K18 N121 84.9(5) . 1_556 ?
O26 K18 N121 149.7(5) . 3_566 ?
O26 K18 C121 94.5(5) . 1_556 ?
O26 K18 C121 131.7(5) . 3_566 ?
O30 K18 Se14 63.5(3) 3_565 3_566 ?
O30 K18 K17 157.2(3) 3_565 . ?
O30 K18 K17 49.1(3) 3_565 3_565 ?
O30 K18 O26 108.4(5) 3_565 . ?
O30 K18 N63 74.4(4) 3_565 2_766 ?
O30 K18 N111 161.8(5) 3_565 . ?
O30 K18 N113 86.3(5) 3_565 3_565 ?
O30 K18 N121 59.9(4) 3_565 3_566 ?
O30 K18 N121 124.7(4) 3_565 1_556 ?
O30 K18 C121 66.1(5) 3_565 3_566 ?
O30 K18 C121 104.7(5) 3_565 1_556 ?
N63 K18 Se14 112.7(3) 2_766 3_566 ?
N63 K18 K17 114.0(3) 2_766 . ?
N63 K18 K17 93.2(3) 2_766 3_565 ?
N63 K18 N121 146.8(4) 2_766 1_556 ?
N63 K18 N121 129.6(4) 2_766 3_566 ?
N63 K18 C121 140.5(5) 2_766 3_566 ?
N63 K18 C121 153.8(5) 2_766 1_556 ?
N111 K18 Se14 134.3(3) . 3_566 ?
N111 K18 K17 116.8(3) . 3_565 ?
N111 K18 K17 41.0(3) . . ?
N111 K18 N63 97.4(4) . 2_766 ?
N111 K18 N121 119.2(4) . 3_566 ?
N111 K18 N121 70.7(4) . 1_556 ?
N111 K18 C121 89.9(5) . 1_556 ?
N111 K18 C121 119.9(5) . 3_566 ?
N113 K18 Se14 136.9(4) 3_565 3_566 ?
N113 K18 K17 42.5(3) 3_565 3_565 ?
N113 K18 K17 114.8(3) 3_565 . ?
N113 K18 O26 137.2(5) 3_565 . ?
N113 K18 N63 85.0(5) 3_565 2_766 ?
N113 K18 N111 76.7(5) 3_565 . ?
N113 K18 N121 120.0(4) 3_565 1_556 ?
N113 K18 N121 72.6(4) 3_565 3_566 ?
N113 K18 C121 121.1(5) 3_565 1_556 ?
N113 K18 C121 91.2(5) 3_565 3_566 ?
N121 K18 Se14 65.9(3) 3_566 3_566 ?
N121 K18 Se14 65.2(3) 1_556 3_566 ?
N121 K18 K17 116.4(3) 3_566 . ?
N121 K18 K17 40.9(3) 3_566 3_565 ?
N121 K18 K17 38.0(3) 1_556 . ?
N121 K18 K17 119.9(3) 1_556 3_565 ?
N121 K18 N121 81.5(5) 1_556 3_566 ?
N121 K18 C121 19.6(4) 3_566 3_566 ?
N121 K18 C121 20.3(4) 1_556 1_556 ?
N121 K18 C121 65.8(4) 1_556 3_566 ?
N121 K18 C121 65.2(5) 3_566 1_556 ?
C121 K18 Se14 49.7(4) 3_566 3_566 ?
C121 K18 Se14 48.8(4) 1_556 3_566 ?
C121 K18 K17 105.9(4) 1_556 3_565 ?
C121 K18 K17 103.2(4) 3_566 . ?
C121 K18 K17 60.0(3) 3_566 3_565 ?
C121 K18 K17 58.0(4) 1_556 . ?
C121 K18 C121 47.4(7) 1_556 3_566 ?
K1 O1 K8 101.8(6) . 1_554 ?
K1 O2 K2 92.1(5) . 1_554 ?
K12 O3 K1 101.9(5) . 1_556 ?
K12 O4 K13 139.1(7) . . ?
K13 O5 K15 91.1(4) . . ?
K14 O7 K2 145.9(8) . . ?
K15 O7 K2 98.3(5) . . ?
K15 O7 K14 87.9(5) . . ?
K16 O9 K14 104.9(7) . . ?
K16 O10 K17 95.4(5) . . ?
K11 O11 K16 100.2(5) . 3_565 ?
K14 O12 K15 88.9(4) . . ?
K10 O13 K12 86.7(5) . . ?
K8 O14 K9 88.6(6) . . ?
K9 O15 K8 93.0(6) . . ?
K10 O15 K8 137.9(7) . . ?
K10 O15 K9 83.3(5) . . ?
K10 O16 K9 82.9(5) . . ?
K7 O18 K8 91.0(5) . 1_554 ?
K4 O20 K7 103.5(4) . 1_556 ?
K4 O21 K5 138.4(7) . . ?
K7 O22 K6 93.0(4) . 1_554 ?
K11 O23 K4 92.3(4) . . ?
K3 O24 K6 101.2(4) . 1_554 ?
K17 O24 K3 90.2(5) 1_554 . ?
K17 O24 K6 85.9(5) 1_554 1_554 ?
K18 O26 K6 139.9(7) . . ?
K6 O27 K11 104.8(5) . . ?
K3 O29 K16 135.3(7) 1_556 . ?
K17 O29 K3 90.8(5) . 1_556 ?
K17 O29 K16 90.8(5) . . ?
K18 O30 K17 91.3(4) 2_665 . ?
K12 N11 K1 93.4(6) . 1_556 ?
C11 N11 K1 106.9(15) . 1_556 ?
C11 N11 K12 139.7(15) . . ?
K7 N13 K5 113.3(5) 1_556 . ?
K7 N13 K8 81.7(4) 1_556 . ?
K8 N13 K5 92.9(4) . . ?
C13 N13 K5 136.0(14) . . ?
C13 N13 K7 107.4(13) . 1_556 ?
C13 N13 K8 109.0(14) . . ?
K3 N21 K6 104.7(5) 1_556 . ?
K17 N21 K3 90.3(5) . 1_556 ?
K17 N21 K6 88.5(5) . . ?
C21 N21 K3 111.3(13) . 1_556 ?
C21 N21 K6 95.6(13) . . ?
C21 N21 K17 156.0(14) . . ?
K4 N22 K6 100.6(5) . . ?
K4 N22 K7 100.1(5) . 1_556 ?
K7 N22 K6 92.3(5) 1_556 . ?
C22 N22 K4 141.2(13) . . ?
C22 N22 K6 100.9(12) . . ?
C22 N22 K7 110.9(12) . 1_556 ?
K3 N31 K2 91.2(5) 1_556 . ?
C31 N31 K2 98.3(13) . . ?
C31 N31 K3 111.8(14) . 1_556 ?
K1 N33 K13 120.6(6) 1_556 . ?
K2 N33 K1 86.3(5) . 1_556 ?
K2 N33 K13 83.8(5) . . ?
C33 N33 K1 103.2(14) . 1_556 ?
C33 N33 K2 108.4(15) . . ?
C33 N33 K13 135.4(14) . . ?
K3 N41 K7 140.6(6) . . ?
K6 N41 K3 106.6(5) 1_554 . ?
K6 N41 K7 82.6(5) 1_554 . ?
C41 N41 K3 94.8(13) . . ?
C41 N41 K6 158.5(15) . 1_554 ?
C41 N41 K7 82.6(13) . . ?
K2 N42 K1 88.1(5) 1_554 . ?
K2 N42 K3 103.3(5) 1_554 . ?
K3 N42 K1 149.4(6) . . ?
C42 N42 K1 88.7(13) . . ?
C42 N42 K2 148.8(15) . 1_554 ?
C42 N42 K3 95.1(13) . . ?
K7 N43 K1 152.4(6) . . ?
K8 N43 K1 104.3(5) 1_554 . ?
K8 N43 K7 90.9(5) 1_554 . ?
C43 N43 K1 88.7(13) . . ?
C43 N43 K7 92.9(13) . . ?
C43 N43 K8 142.8(14) . 1_554 ?
K9 N51 K4 97.5(4) 1_554 3_674 ?
K9 N51 K10 81.0(4) 1_554 1_554 ?
K10 N51 K4 101.1(4) 1_554 3_674 ?
C51 N51 K4 96.4(12) . 3_674 ?
C51 N51 K9 160.4(14) . 1_554 ?
C51 N51 K10 109.8(12) . 1_554 ?
K6 N53 K4 100.7(5) 3_674 3_674 ?
K6 N53 K11 101.4(5) 3_674 3_674 ?
K11 N53 K4 91.0(4) 3_674 3_674 ?
C53 N53 K4 101.1(12) . 3_674 ?
C53 N53 K6 141.5(13) . 3_674 ?
C53 N53 K11 109.5(12) . 3_674 ?
C61 N61 K16 125.2(15) . 2_775 ?
C62 N62 K14 110.0(14) . 2_774 ?
K18 N63 K11 111.2(5) 3_674 3_674 ?
C63 N63 K11 107.4(13) . 3_674 ?
C63 N63 K18 139.4(14) . 3_674 ?
K4 N71 K10 108.8(5) 3_675 . ?
K4 N71 K11 84.4(4) 3_675 3_675 ?
K10 N71 K11 143.1(6) . 3_675 ?
C71 N71 K4 159.3(14) . 3_675 ?
C71 N71 K10 89.5(12) . . ?
C71 N71 K11 86.4(11) . 3_675 ?
K10 N72 K14 141.2(6) . 2_775 ?
K12 N72 K10 82.7(4) . . ?
K12 N72 K14 110.3(5) . 2_775 ?
C72 N72 K10 86.6(13) . . ?
C72 N72 K12 158.8(14) . . ?
C72 N72 K14 89.5(12) . 2_775 ?
K14 N73 K11 151.5(6) 2_775 3_675 ?
K16 N73 K11 97.2(5) 2_775 3_675 ?
K16 N73 K14 103.2(5) 2_775 2_775 ?
C73 N73 K11 88.9(12) . 3_675 ?
C73 N73 K14 94.1(12) . 2_775 ?
C73 N73 K16 127.7(13) . 2_775 ?
K15 N82 K14 87.8(5) 2_774 2_774 ?
C82 N82 K14 108.1(14) . 2_774 ?
C82 N82 K15 163.3(15) . 2_774 ?
K10 N83 K12 87.8(4) 1_554 1_554 ?
C83 N83 K10 112.3(13) . 1_554 ?
C83 N83 K12 106.5(13) . 1_554 ?
K5 N92 K9 100.1(5) 3_674 1_554 ?
C92 N92 K5 114.4(13) . 3_674 ?
C92 N92 K9 96.4(14) . 1_554 ?
K5 N93 K8 106.0(6) 1_554 1_554 ?
K5 N93 K9 97.4(6) 1_554 1_554 ?
K8 N93 K9 94.3(6) 1_554 1_554 ?
C93 N93 K5 117.8(14) . 1_554 ?
C93 N93 K8 132.3(15) . 1_554 ?
C93 N93 K9 97.8(15) . 1_554 ?
K5 N101 K5 148.4(6) 3_675 . ?
K9 N101 K5 87.7(5) . . ?
K9 N101 K5 99.2(5) . 3_675 ?
C101 N101 K5 90.2(13) . 3_675 ?
C101 N101 K5 88.4(13) . . ?
C101 N101 K9 167.7(15) . . ?
K18 N111 K17 100.3(5) . . ?
C111 N111 K17 99.2(12) . . ?
C111 N111 K18 114.6(12) . . ?
K16 N113 K17 91.5(5) . . ?
K18 N113 K16 116.6(6) 2_665 . ?
K18 N113 K17 98.1(5) 2_665 . ?
C113 N113 K16 121.0(14) . . ?
C113 N113 K17 99.9(12) . . ?
C113 N113 K18 118.5(13) . 2_665 ?
K17 N121 K18 90.0(4) 1_554 2_664 ?
K17 N121 K18 100.0(4) 1_554 1_554 ?
K18 N121 K18 149.1(5) 1_554 2_664 ?
C121 N121 K17 163.9(15) . 1_554 ?
C121 N121 K18 86.5(13) . 2_664 ?
C121 N121 K18 90.9(14) . 1_554 ?
K2 N131 K13 98.5(5) 1_554 1_554 ?
K2 N131 K15 100.7(5) 1_554 1_554 ?
K13 N131 K15 99.5(5) 1_554 1_554 ?
C131 N131 K2 137.4(12) . 1_554 ?
C131 N131 K13 113.9(12) . 1_554 ?
C131 N131 K15 100.2(12) . 1_554 ?
K13 N133 K15 96.2(5) 3_574 1_554 ?
C133 N133 K13 110.0(13) . 3_574 ?
C133 N133 K15 100.0(12) . 1_554 ?
K13 N141 K13 144.5(6) . 2_775 ?
K15 N141 K13 98.4(5) 2_775 . ?
K15 N141 K13 91.4(5) 2_775 2_775 ?
C141 N141 K13 85.6(12) . 2_775 ?
C141 N141 K13 92.5(13) . . ?
C141 N141 K15 164.9(15) . 2_775 ?
W1 C11 K1 129.5(8) . 1_556 ?
N11 C11 Re1 176.4(19) . . ?
N11 C11 W1 176.4(19) . . ?
N11 C11 K1 54.2(12) . 1_556 ?
N12 C12 Re1 178(2) . . ?
N12 C12 W1 178(2) . . ?
N13 C13 Re1 179.0(17) . . ?
N13 C13 W1 179.0(17) . . ?
Re2 C21 K6 112.7(7) . . ?
W2 C21 K3 132.4(7) . 1_556 ?
W2 C21 K6 112.7(7) . . ?
K3 C21 K6 87.6(4) 1_556 . ?
N21 C21 Re2 176.5(16) . . ?
N21 C21 W2 176.5(16) . . ?
N21 C21 K3 50.9(11) . 1_556 ?
N21 C21 K6 65.4(12) . . ?
Re2 C22 K6 119.8(6) . . ?
W2 C22 K6 119.8(6) . . ?
W2 C22 K7 130.9(7) . 1_556 ?
K6 C22 K7 75.9(4) . 1_556 ?
N22 C22 Re2 178.2(16) . . ?
N22 C22 W2 178.2(16) . . ?
N22 C22 K6 59.4(11) . . ?
N22 C22 K7 50.8(10) . 1_556 ?
N23 C23 Re2 177.2(16) . . ?
N23 C23 W2 177.2(16) . . ?
W3 C31 K3 133.2(7) . 1_556 ?
N31 C31 Re3 175.6(16) . . ?
N31 C31 W3 175.6(16) . . ?
N31 C31 K3 50.3(12) . 1_556 ?
N32 C32 Re3 177.0(18) . . ?
N32 C32 W3 177.0(18) . . ?
W3 C33 K1 125.9(7) . 1_556 ?
N33 C33 Re3 174.5(17) . . ?
N33 C33 W3 174.5(17) . . ?
N33 C33 K1 57.9(12) . 1_556 ?
Re4 C41 K3 110.8(6) . . ?
Re4 C41 K7 105.0(6) . . ?
W4 C41 K3 110.8(6) . . ?
W4 C41 K7 105.0(6) . . ?
K7 C41 K3 126.7(5) . . ?
N41 C41 Re4 176.4(16) . . ?
N41 C41 W4 176.4(16) . . ?
N41 C41 K3 65.6(12) . . ?
N41 C41 K7 77.6(13) . . ?
Re4 C42 K1 105.5(6) . . ?
Re4 C42 K3 114.4(7) . . ?
W4 C42 K1 105.5(6) . . ?
W4 C42 K3 114.4(7) . . ?
K3 C42 K1 127.9(5) . . ?
N42 C42 Re4 174.5(17) . . ?
N42 C42 W4 174.5(17) . . ?
N42 C42 K1 71.8(12) . . ?
N42 C42 K3 65.3(12) . . ?
Re4 C43 K1 109.2(7) . . ?
Re4 C43 K7 111.0(7) . . ?
W4 C43 K1 109.2(7) . . ?
W4 C43 K7 111.0(7) . . ?
K7 C43 K1 129.3(6) . . ?
N43 C43 Re4 174.4(17) . . ?
N43 C43 W4 174.4(17) . . ?
N43 C43 K1 70.7(12) . . ?
N43 C43 K7 66.4(12) . . ?
Re5 C51 K4 112.0(6) . 3_674 ?
W5 C51 K4 112.0(6) . 3_674 ?
N51 C51 Re5 176.4(16) . . ?
N51 C51 W5 176.4(16) . . ?
N51 C51 K4 64.4(11) . 3_674 ?
N52 C52 Re5 176.2(16) . . ?
N52 C52 W5 176.2(16) . . ?
Re5 C53 K4 118.6(6) . 3_674 ?
Re5 C53 K11 129.7(6) . 3_674 ?
W5 C53 K4 118.6(6) . 3_674 ?
W5 C53 K11 129.7(6) . 3_674 ?
K4 C53 K11 74.8(3) 3_674 3_674 ?
N53 C53 Re5 177.0(15) . . ?
N53 C53 W5 177.0(15) . . ?
N53 C53 K4 58.6(10) . 3_674 ?
N53 C53 K11 51.7(10) . 3_674 ?
N61 C61 Re6 173.7(17) . . ?
N61 C61 W6 173.7(17) . . ?
W6 C62 K14 129.8(8) . 2_774 ?
N62 C62 Re6 178.1(19) . . ?
N62 C62 W6 178.1(19) . . ?
N62 C62 K14 52.0(12) . 2_774 ?
Re6 C63 K11 127.0(7) . 3_674 ?
W6 C63 K11 127.0(7) . 3_674 ?
N63 C63 Re6 177.5(16) . . ?
N63 C63 W6 177.5(16) . . ?
N63 C63 K11 54.3(11) . 3_674 ?
Re7 C71 K10 109.1(6) . . ?
W7 C71 K10 109.1(6) . . ?
W7 C71 K11 106.7(6) . 3_675 ?
K10 C71 K11 128.2(5) . 3_675 ?
N71 C71 Re7 177.3(15) . . ?
N71 C71 W7 177.3(15) . . ?
N71 C71 K10 69.2(11) . . ?
N71 C71 K11 73.5(11) . 3_675 ?
Re7 C72 K10 107.4(6) . . ?
W7 C72 K10 107.4(6) . . ?
W7 C72 K14 107.9(6) . 2_775 ?
K10 C72 K14 127.5(5) . 2_775 ?
N72 C72 Re7 178.5(18) . . ?
N72 C72 W7 178.5(18) . . ?
N72 C72 K10 72.9(12) . . ?
N72 C72 K14 70.9(11) . 2_775 ?
W7 C73 K11 109.9(6) . 3_675 ?
W7 C73 K14 112.0(7) . 2_775 ?
K11 C73 K14 127.3(5) 3_675 2_775 ?
N73 C73 Re7 174.1(16) . . ?
N73 C73 W7 174.1(16) . . ?
N73 C73 K11 70.1(11) . 3_675 ?
N73 C73 K14 65.0(11) . 2_775 ?
N81 C81 Re8 177.5(16) . . ?
N81 C81 W8 177.5(16) . . ?
W8 C82 K14 127.7(7) . 2_774 ?
N82 C82 Re8 177.0(17) . . ?
N82 C82 W8 177.0(17) . . ?
N82 C82 K14 53.7(12) . 2_774 ?
Re8 C83 K12 124.1(7) . 1_554 ?
W8 C83 K10 130.9(7) . 1_554 ?
W8 C83 K12 124.1(7) . 1_554 ?
K12 C83 K10 71.1(3) 1_554 1_554 ?
N83 C83 Re8 178.6(16) . . ?
N83 C83 W8 178.6(16) . . ?
N83 C83 K10 49.8(11) . 1_554 ?
N83 C83 K12 54.7(11) . 1_554 ?
N91 C91 Re9 177.2(17) . . ?
N91 C91 W9 177.2(17) . . ?
W9 C92 K9 112.4(7) . 1_554 ?
N92 C92 Re9 176.5(16) . . ?
N92 C92 W9 176.5(16) . . ?
N92 C92 K9 64.1(12) . 1_554 ?
Re9 C93 K5 134.6(7) . 1_554 ?
W9 C93 K5 134.6(7) . 1_554 ?
W9 C93 K9 117.8(7) . 1_554 ?
K9 C93 K5 78.9(4) 1_554 1_554 ?
N93 C93 Re9 180(2) . . ?
N93 C93 W9 180(2) . . ?
N93 C93 K5 45.4(12) . 1_554 ?
N93 C93 K9 61.9(13) . 1_554 ?
Re10 C101 K5 107.6(7) . . ?
W10 C101 K5 109.8(7) . 3_675 ?
W10 C101 K5 107.6(7) . . ?
K5 C101 K5 131.7(6) 3_675 . ?
N101 C101 Re10 179.5(17) . . ?
N101 C101 W10 179.5(17) . . ?
N101 C101 K5 70.4(13) . 3_675 ?
N101 C101 K5 72.5(13) . . ?
Re11 C111 K17 115.8(6) . . ?
W11 C111 K17 115.8(6) . . ?
N111 C111 Re11 177.2(15) . . ?
N111 C111 W11 177.2(15) . . ?
N111 C111 K17 61.6(11) . . ?
N112 C112 Re11 176.8(16) . . ?
N112 C112 W11 176.8(16) . . ?
Re11 C113 K17 117.4(6) . . ?
W11 C113 K17 117.4(6) . . ?
N113 C113 Re11 177.3(16) . . ?
N113 C113 W11 177.3(16) . . ?
N113 C113 K17 60.6(11) . . ?
W12 C121 K18 106.4(7) . 2_664 ?
W12 C121 K18 109.9(8) . 1_554 ?
K18 C121 K18 132.0(7) 1_554 2_664 ?
N121 C121 Re12 178(2) . . ?
N121 C121 W12 178(2) . . ?
N121 C121 K18 73.9(13) . 2_664 ?
N121 C121 K18 68.8(12) . 1_554 ?
W13 C131 K13 132.5(7) . 1_554 ?
W13 C131 K15 118.9(7) . 1_554 ?
K15 C131 K13 80.1(4) 1_554 1_554 ?
N131 C131 Re13 178.5(15) . . ?
N131 C131 W13 178.5(15) . . ?
N131 C131 K13 47.8(10) . 1_554 ?
N131 C131 K15 59.5(10) . 1_554 ?
N132 C132 Re13 177.5(16) . . ?
N132 C132 W13 177.5(16) . . ?
Re13 C133 K13 130.1(7) . 3_574 ?
W13 C133 K13 130.1(7) . 3_574 ?
W13 C133 K15 114.9(6) . 1_554 ?
K15 C133 K13 79.6(4) 1_554 3_574 ?
N133 C133 Re13 175.4(15) . . ?
N133 C133 W13 175.4(15) . . ?
N133 C133 K13 51.6(10) . 3_574 ?
N133 C133 K15 60.6(11) . 1_554 ?
Re14 C141 K13 111.2(6) . . ?
Re14 C141 K13 106.5(6) . 2_775 ?
W14 C141 K13 111.2(6) . . ?
W14 C141 K13 106.5(6) . 2_775 ?
K13 C141 K13 128.8(6) . 2_775 ?
N141 C141 Re14 178.3(16) . . ?
N141 C141 W14 178.3(16) . . ?
N141 C141 K13 75.1(12) . 2_775 ?
N141 C141 K13 67.3(12) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
K1 N42 C42 K3 -149.5(7) . . . . ?
K1 N43 C43 K7 152.5(6) . . . . ?
K2 N31 C31 K3 94.7(10) . . . 1_556 ?
K2 N33 C33 K1 -90.5(10) . . . 1_556 ?
K2 N42 C42 K1 -84(3) 1_554 . . . ?
K2 N42 C42 K3 126(3) 1_554 . . . ?
K2 N131 C131 K13 136(2) 1_554 . . 1_554 ?
K2 N131 C131 K15 -118.4(18) 1_554 . . 1_554 ?
K3 N21 C21 K6 108.2(9) 1_556 . . . ?
K3 N41 C41 K7 -140.5(6) . . . . ?
K3 N42 C42 K1 149.5(7) . . . . ?
K4 N22 C22 K6 123(2) . . . . ?
K4 N22 C22 K7 -141(2) . . . 1_556 ?
K4 N53 C53 K11 -95.1(8) 3_674 . . 3_674 ?
K4 N71 C71 K10 153(4) 3_675 . . . ?
K4 N71 C71 K11 -64(4) 3_675 . . 3_675 ?
K5 N92 C92 K9 -104.1(10) 3_674 . . 1_554 ?
K5 N93 C93 K9 102.7(13) 1_554 . . 1_554 ?
K5 N101 C101 K5 -148.4(5) . . . 3_675 ?
K5 N101 C101 K5 148.4(5) 3_675 . . . ?
K6 N21 C21 K3 -108.2(9) . . . 1_556 ?
K6 N22 C22 K7 96.7(9) . . . 1_556 ?
K6 N41 C41 K3 -173(5) 1_554 . . . ?
K6 N41 C41 K7 47(4) 1_554 . . . ?
K6 N53 C53 K4 -123(2) 3_674 . . 3_674 ?
K6 N53 C53 K11 142(2) 3_674 . . 3_674 ?
K7 N22 C22 K6 -96.7(9) 1_556 . . . ?
K7 N41 C41 K3 140.5(6) . . . . ?
K7 N43 C43 K1 -152.5(6) . . . . ?
K8 N43 C43 K1 112(2) 1_554 . . . ?
K8 N43 C43 K7 -95(2) 1_554 . . . ?
K8 N93 C93 K5 154(3) 1_554 . . 1_554 ?
K8 N93 C93 K9 -103.1(18) 1_554 . . 1_554 ?
K9 N51 C51 K4 135(4) 1_554 . . 3_674 ?
K9 N93 C93 K5 -102.7(13) 1_554 . . 1_554 ?
K9 N101 C101 K5 140(8) . . . 3_675 ?
K9 N101 C101 K5 -71(7) . . . . ?
K10 N51 C51 K4 -104.3(8) 1_554 . . 3_674 ?
K10 N71 C71 K11 143.3(5) . . . 3_675 ?
K10 N72 C72 K14 -141.3(5) . . . 2_775 ?
K10 N83 C83 K12 94.5(10) 1_554 . . 1_554 ?
K11 N53 C53 K4 95.1(8) 3_674 . . 3_674 ?
K11 N71 C71 K10 -143.3(5) 3_675 . . . ?
K11 N73 C73 K14 151.6(6) 3_675 . . 2_775 ?
K12 N11 C11 K1 -117(3) . . . 1_556 ?
K12 N72 C72 K10 -60(4) . . . . ?
K12 N72 C72 K14 159(4) . . . 2_775 ?
K12 N83 C83 K10 -94.5(10) 1_554 . . 1_554 ?
K13 N33 C33 K1 169(2) . . . 1_556 ?
K13 N131 C131 K15 105.3(10) 1_554 . . 1_554 ?
K13 N133 C133 K15 -100.4(9) 3_574 . . 1_554 ?
K13 N141 C141 K13 144.5(6) . . . 2_775 ?
K13 N141 C141 K13 -144.5(6) 2_775 . . . ?
K14 N72 C72 K10 141.3(5) 2_775 . . . ?
K14 N73 C73 K11 -151.6(6) 2_775 . . 3_675 ?
K15 N82 C82 K14 -162(6) 2_774 . . 2_774 ?
K15 N131 C131 K13 -105.3(10) 1_554 . . 1_554 ?
K15 N133 C133 K13 100.4(9) 1_554 . . 3_574 ?
K15 N141 C141 K13 -79(5) 2_775 . . 2_775 ?
K15 N141 C141 K13 136(6) 2_775 . . . ?
K16 N73 C73 K11 98.3(13) 2_775 . . 3_675 ?
K16 N73 C73 K14 -110.1(14) 2_775 . . 2_775 ?
K16 N113 C113 K17 97.9(12) . . . . ?
K17 N21 C21 K3 153(4) . . . 1_556 ?
K17 N21 C21 K6 -99(3) . . . . ?
K17 N121 C121 K18 -133(5) 1_554 . . 1_554 ?
K17 N121 C121 K18 78(5) 1_554 . . 2_664 ?
K18 N63 C63 K11 -162(2) 3_674 . . 3_674 ?
K18 N111 C111 K17 105.8(10) . . . . ?
K18 N113 C113 K17 -104.9(12) 2_665 . . . ?
K18 N121 C121 K18 -149.2(5) 1_554 . . 2_664 ?
K18 N121 C121 K18 149.2(5) 2_664 . . 1_554 ?

_olex2_submission_special_instructions 'No special instructions were received'
loop_
_twin_individual_id
_twin_individual_mass_fraction_refined
1 0.603(10)
2 0.397(10)

_vrf_PLAT306_pr913               
;
PROBLEM: Isolated Oxygen Atom (H-atoms Missing ?) .......         O1-O30
RESPONSE: These oxygen atoms belong to H2O molecules.
Hydrogen atoms were not localized, but included in the formula of the compound.
;
_exptl_crystal_preparation       'Magnetic properties'
