# Electronic Supplementary Material (ESI) for Chemical Science.
# This journal is © The Royal Society of Chemistry 2022

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
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data_20180421a_0m
_database_code_depnum_ccdc_archive 'CCDC 2115749'
loop_
_audit_author_name
_audit_author_address
'Xi Xi Kang'
;Anhui University
China
;
_audit_update_record             
;
2021-10-14 deposited with the CCDC.	2022-01-03 downloaded from the CCDC.
;
_audit_creation_date             2019-07-17
_audit_creation_method           
;
Olex2 1.2
(compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506)
;
_shelx_SHELXL_version_number     2016/4
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         '1(C218 H282 Ag29 N7 O9 P4 S15), 2.5(F6 Sb1)'
_chemical_formula_sum            'C218 H279 Ag29 F15 N7 O9 P4 S15 Sb2.50'
_chemical_formula_weight         7463.92
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      trigonal
_space_group_IT_number           165
_space_group_name_H-M_alt        'P -3 c 1'
_space_group_name_Hall           '-P 3 2"c'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'
'y, x, -z+1/2'
'x-y, -y, -z+1/2'
'-x, -x+y, -z+1/2'
'-x, -y, -z'
'y, -x+y, -z'
'x-y, x, -z'
'-y, -x, z-1/2'
'-x+y, y, z-1/2'
'x, x-y, z-1/2'

_cell_length_a                   22.224(4)
_cell_length_b                   22.224(4)
_cell_length_c                   68.128(12)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_volume                     29141(12)
_cell_formula_units_Z            3.99996
_cell_measurement_reflns_used    9754
_cell_measurement_temperature    170
_cell_measurement_theta_max      22.642
_cell_measurement_theta_min      2.188
_shelx_estimated_absorpt_T_max   ?
_shelx_estimated_absorpt_T_min   ?
_exptl_absorpt_coefficient_mu    2.307
_exptl_absorpt_correction_T_max  0.7456
_exptl_absorpt_correction_T_min  0.5929
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
'SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.0921 before and 0.0644 after correction. The Ratio of minimum to maximum transmission is 0.7952. The λ/2 correction factor is Not present.'
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            'dark red'
_exptl_crystal_colour_modifier   dark
_exptl_crystal_colour_primary    red
_exptl_crystal_density_diffrn    1.701
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             14534
_exptl_crystal_size_max          0.1
_exptl_crystal_size_mid          0.1
_exptl_crystal_size_min          0.05
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0851
_diffrn_reflns_av_unetI/netI     0.0667
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 0.950
_diffrn_reflns_limit_h_max       28
_diffrn_reflns_limit_h_min       -28
_diffrn_reflns_limit_k_max       28
_diffrn_reflns_limit_k_min       -28
_diffrn_reflns_limit_l_max       84
_diffrn_reflns_limit_l_min       -78
_diffrn_reflns_number            197542
_diffrn_reflns_point_group_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 0.950
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         27.489
_diffrn_reflns_theta_min         0.598
_diffrn_ambient_temperature      170
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 0.950
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_diffrn_standards_number         0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                15489
_reflns_number_total             21198
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT V8.38A (?, 2016)'
_computing_data_collection       ?
_computing_data_reduction        'SAINT V8.38A (?, 2016)'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    'ShelXT (Sheldrick, 2015)'
_refine_diff_density_max         2.612
_refine_diff_density_min         -2.571
_refine_diff_density_rms         0.366
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.094
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     865
_refine_ls_number_reflns         21198
_refine_ls_number_restraints     1848
_refine_ls_R_factor_all          0.1651
_refine_ls_R_factor_gt           0.1337
_refine_ls_restrained_S_all      1.051
_refine_ls_shift/su_max          0.008
_refine_ls_shift/su_mean         0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0702P)²+2571.6443P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.3092
_refine_ls_wR_factor_ref         0.3296
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups, All C(H,H) groups, All N(H) groups
2. Shared sites
{C01J, N01J}
3. Restrained distances
 N012-O021
 1.25 with sigma of 0.01
 Sb00-F56 = Sb00-F15 = Sb00-F27 = Sb00-F8 = Sb00-F14 = Sb00-F34
 1.85 with sigma of 0.01
 F14-F27
 2.62 with sigma of 0.01
 F14-F34
 2.62 with sigma of 0.01
 F34-F15
 2.62 with sigma of 0.01
 F15-F56
 2.62 with sigma of 0.01
 F56-F14
 2.62 with sigma of 0.01
 F14-F8
 2.62 with sigma of 0.01
 F8-F15
 2.62 with sigma of 0.01
 F8-F27
 2.62 with sigma of 0.01
 F27-F56
 2.62 with sigma of 0.01
 F56-F34
 2.62 with sigma of 0.01
 F8-F34
 2.62 with sigma of 0.01
 C13-C10
 1.45 with sigma of 0.01
 C23-C10
 1.45 with sigma of 0.01
 C01V-C01O
 1.45 with sigma of 0.01
 C23-C01O
 1.45 with sigma of 0.01
 C12-C01V
 1.45 with sigma of 0.01
 C13-C12
 1.45 with sigma of 0.01
4. Uiso/Uaniso restraints and constraints
C00L \\sim C00N \\sim C00O \\sim C00P \\sim C00Q \\sim C00S \\sim C01U \\sim
C026 \\sim C02H \\sim C7 \\sim C01J \\sim C00T \\sim C00U \\sim C02M \\sim C02W
\\sim C02C \\sim C02B \\sim C01R \\sim C00W \\sim C00X \\sim C00Y \\sim C010
\\sim C029 \\sim C02U \\sim C02I \\sim C01P \\sim C01F \\sim C011 \\sim C01G
\\sim C024 \\sim C02R \\sim C01Y \\sim C013 \\sim C014 \\sim C015 \\sim C016
\\sim C017 \\sim C018 \\sim C019 \\sim C01A \\sim C01B \\sim C01D \\sim C01H
\\sim C01I \\sim C01K \\sim C01L \\sim C01M \\sim C01N \\sim C01O \\sim C01S
\\sim C01T \\sim C01V \\sim C01W \\sim C01X \\sim C01Z \\sim C022 \\sim C023
\\sim C025 \\sim C027 \\sim C028 \\sim C02A \\sim C02F \\sim C02G \\sim C02J
\\sim C02K \\sim C02O \\sim C02P \\sim C02Y \\sim C5 \\sim C10 \\sim C12 \\sim
C13 \\sim C23: within 3.8A with sigma of 0.01 and sigma for terminal atoms of
0.02
F34 \\sim Sb00 \\sim F8 \\sim F14 \\sim F15 \\sim F27 \\sim F56: within 2A with
sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(O00R) \\sim Ueq: with sigma of 0.001 and sigma for terminal atoms of 0.002
Uanis(N012) \\sim Ueq, Uanis(O021) \\sim Ueq: with sigma of 0.001 and sigma for
terminal atoms of 0.002
Uanis(O00Z) \\sim Ueq: with sigma of 0.001 and sigma for terminal atoms of 0.002
Uanis(C01J) = Uanis(N01J)
Uanis(N012) = Uanis(O021) = Uanis(O00R) = Uanis(O00Z)
5. Others
 Fixed Sof: Sb00(0.5) H7A(0.66667) H7B(0.33333) C01J(0.66667) H01J(0.66667)
 N01J(0.33333) H5AA(0.33333) F8(0.5) F14(0.5) F15(0.5) F27(0.5) F34(0.5)
 F56(0.5)
6.a Ternary CH refined with riding coordinates:
 C014(H014), C015(H015), C016(H016), C019(H019), C01A(H01E), C01B(H01H),
 C01I(H01L), C01V(H1AA), C025(H025), C028(H028), C02G(H02P), C02K(H02T),
 C02P(H02Y), C13(H13), C23(H23)
6.b Secondary CH2 refined with riding coordinates:
 C00O(H00A,H00B), C00Q(H00C,H00D), C00T(H00E,H00F), C00W(H00G,H00H), C00X(H00I,
 H00J), C00Y(H00K,H00L), C013(H01A,H01B), C017(H01C,H01D), C01H(H01I,H01K),
 C01K(H01M,H01N), C01L(H01O,H01Q), C01M(H01S,H01T), C01N(H01V,H01W), C01O(H01X,
 H01Z), C01S(H01,H), C01T(H0AA,HA), C01W(H2AA,HB), C01X(H3AA,HC), C01Z(H4AA,HD),
  C022(H02A,H02D), C023(H02E,H02F), C027(H02G,H02J), C02A(H02K,H02L), C02F(H02N,
 H02O), C02J(H02Q,H02S), C02O(H02V,H02X), C02Y(H02Z,HE), C5(H5A,H5B), C10(H10A,
 H10B), C12(H12A,H12B)
6.c Aromatic/amide H refined with riding coordinates:
 C01U(H01U), C026(H026), C02H(H02H), C7(H7A), C7(H7B), C01J(H01J), C02M(H02M),
 C02W(H02W), C02C(H02C), C02B(H02B), C01R(H01R), C029(H029), C02U(H02U),
 C02I(H02I), C01P(H01P), C01F(H01F), C01G(H01G), C024(H024), C02R(H02R),
 C01Y(H01Y), N01J(H5AA)
6.d Fitted hexagon refined as free rotating group:
 C00S(C01U,C026,C02H,C7,C01J), C00U(C02M,C02W,C02C,C02B,C01R), C010(C029,C02U,
 C02I,C01P,C01F), C011(N00M,C01G,C024,C02R,C01Y)
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag01 Ag 0.666667 0.333333 0.62666(3) 0.0220(4) Uani 1 3 d S T P . .
Ag02 Ag 0.52501(7) 0.24377(7) 0.63438(2) 0.0311(3) Uani 1 1 d . . . . .
Ag03 Ag 0.61472(7) 0.36457(7) 0.65947(2) 0.0304(3) Uani 1 1 d . . . . .
Ag04 Ag 0.71885(8) 0.29210(7) 0.59528(2) 0.0310(3) Uani 1 1 d . . . . .
Ag05 Ag 0.58560(7) 0.39415(8) 0.61830(2) 0.0314(3) Uani 1 1 d . . . . .
Ag06 Ag 0.56414(8) 0.16407(8) 0.57444(2) 0.0374(4) Uani 1 1 d . . . . .
Ag07 Ag 0.48024(9) 0.09854(8) 0.65204(2) 0.0414(4) Uani 1 1 d . . . . .
Ag08 Ag 0.47256(9) 0.04159(9) 0.61186(2) 0.0437(4) Uani 1 1 d . . . . .
Ag09 Ag 0.666667 0.333333 0.54005(4) 0.0450(7) Uani 1 3 d S T P . .
Ag0A Ag 0.45788(8) 0.28800(8) 0.66658(3) 0.0434(4) Uani 1 1 d . . . . .
Ag0B Ag 0.58172(10) 0.01587(9) 0.66295(3) 0.0466(4) Uani 1 1 d . . . . .
Sb0C Sb 0.333333 -0.333333 0.58630(6) 0.1059(16) Uani 1 3 d S T P . .
S00D S 0.5470(3) 0.4099(3) 0.67512(7) 0.0327(10) Uani 1 1 d . . . . .
S00E S 0.6785(3) 0.2424(3) 0.56230(7) 0.0359(11) Uani 1 1 d . . . . .
S00F S 0.4233(3) 0.1687(3) 0.65594(8) 0.0377(11) Uani 1 1 d . . . . .
S00G S 0.4467(3) 0.0838(3) 0.58301(8) 0.0392(11) Uani 1 1 d . . . . .
S00H S 0.4797(3) -0.0101(3) 0.64177(8) 0.0407(12) Uani 1 1 d . . . . .
P00I P 0.666667 0.333333 0.50467(13) 0.039(2) Uani 1 3 d S T P C .
Sb00 Sb 0.2523(4) -0.0234(3) 0.72220(11) 0.134(3) Uani 0.5 1 d D U . . .
P00K P 0.6455(4) -0.0217(3) 0.68301(10) 0.0523(16) Uani 1 1 d . . . . .
C00L C 0.3974(14) -0.0893(13) 0.6485(5) 0.066(3) Uani 1 1 d . U . . .
C00N C 0.3441(16) 0.1320(18) 0.6401(6) 0.087(4) Uani 1 1 d . U . . .
C00O C 0.2956(16) 0.1572(18) 0.6466(6) 0.089(4) Uani 1 1 d . U . . .
H00A H 0.318003 0.208025 0.644626 0.107 Uiso 1 1 calc R . . . .
H00B H 0.284882 0.147220 0.660715 0.107 Uiso 1 1 calc R . . . .
C00P C 0.5703(13) 0.4304(13) 0.7013(3) 0.046(3) Uani 1 1 d . U . . .
C00Q C 0.5575(13) 0.4891(12) 0.7074(3) 0.044(3) Uani 1 1 d . U . . .
H00C H 0.507979 0.474552 0.705212 0.053 Uiso 1 1 calc R . . . .
H00D H 0.585955 0.530401 0.699102 0.053 Uiso 1 1 calc R . . . .
O00R O 0.4509(14) 0.3491(14) 0.6334(4) 0.101(4) Uani 1 1 d . U . . .
C00S C 0.6754(9) 0.4125(7) 0.4935(2) 0.058(4) Uani 1 1 d . U . . .
C01U C 0.7081(9) 0.4391(9) 0.4756(2) 0.063(4) Uani 1 1 d G U . C .
H01U H 0.726310 0.415385 0.468341 0.076 Uiso 1 1 calc R . . . .
C026 C 0.7140(9) 0.5004(9) 0.46843(19) 0.063(4) Uani 1 1 d G U . C .
H026 H 0.736387 0.518541 0.456210 0.075 Uiso 1 1 calc R . . . .
C02H C 0.6873(10) 0.5350(7) 0.4791(2) 0.065(4) Uani 1 1 d G U . C .
H02H H 0.691435 0.576905 0.474183 0.078 Uiso 1 1 calc R . . . .
C7 C 0.6547(9) 0.5084(9) 0.4970(2) 0.066(4) Uani 1 1 d G U . C .
H7A H 0.636407 0.532114 0.504287 0.080 Uiso 0.6667 1 calc R . . A 1
H7B H 0.636407 0.532114 0.504287 0.080 Uiso 0.3333 1 calc R . . B 2
C01J C 0.6487(9) 0.4471(9) 0.50420(19) 0.062(4) Uani 0.6667 1 d G U . C 1
H01J H 0.626329 0.428957 0.516419 0.074 Uiso 0.6667 1 calc R . . C 1
C00T C 0.3780(15) -0.0826(13) 0.6688(5) 0.070(3) Uani 1 1 d . U . . .
H00E H 0.370074 -0.042573 0.669652 0.084 Uiso 1 1 calc R . . . .
H00F H 0.415868 -0.074465 0.677924 0.084 Uiso 1 1 calc R . . . .
C00U C 0.5941(12) -0.0979(9) 0.6980(3) 0.087(4) Uani 1 1 d . U . . .
C02M C 0.5242(13) -0.1199(11) 0.7010(3) 0.090(4) Uani 1 1 d G U . . .
H02M H 0.504350 -0.094646 0.695447 0.108 Uiso 1 1 calc R . . . .
C02W C 0.4834(10) -0.1789(11) 0.7122(3) 0.091(4) Uani 1 1 d G U . . .
H02W H 0.435649 -0.193958 0.714261 0.110 Uiso 1 1 calc R . . . .
C02C C 0.5125(12) -0.2158(9) 0.7204(3) 0.089(4) Uani 1 1 d G U . . .
H02C H 0.484568 -0.256161 0.728028 0.107 Uiso 1 1 calc R . . . .
C02B C 0.5823(13) -0.1938(10) 0.7174(3) 0.089(4) Uani 1 1 d G U . . .
H02B H 0.602188 -0.219053 0.722981 0.107 Uiso 1 1 calc R . . . .
C01R C 0.6231(10) -0.1348(11) 0.7062(3) 0.087(4) Uani 1 1 d G U . . .
H01R H 0.670891 -0.119741 0.704167 0.104 Uiso 1 1 calc R . . . .
C00W C 0.4109(14) -0.1497(13) 0.6468(5) 0.069(3) Uani 1 1 d . U . . .
H00G H 0.450554 -0.141709 0.655255 0.082 Uiso 1 1 calc R . . . .
H00H H 0.422009 -0.154995 0.633078 0.082 Uiso 1 1 calc R . . . .
C00X C 0.2520(14) -0.1610(13) 0.6607(5) 0.069(3) Uani 1 1 d . U . . .
H00I H 0.208234 -0.202792 0.664714 0.083 Uiso 1 1 calc R . . . .
H00J H 0.245118 -0.120369 0.661273 0.083 Uiso 1 1 calc R . . . .
C00Y C 0.5292(13) 0.3650(13) 0.7138(3) 0.047(3) Uani 1 1 d . U . . .
H00K H 0.540926 0.329181 0.709973 0.056 Uiso 1 1 calc R . . . .
H00L H 0.478701 0.345849 0.711831 0.056 Uiso 1 1 calc R . . . .
O00Z O 0.4862(14) 0.3832(14) 0.6077(4) 0.101(4) Uani 1 1 d . U . . .
C010 C 0.7031(12) -0.0411(11) 0.6693(3) 0.085(4) Uani 1 1 d . U . . .
C029 C 0.7646(13) -0.0307(11) 0.6776(2) 0.092(4) Uani 1 1 d G U . . .
H029 H 0.777329 -0.011524 0.690450 0.111 Uiso 1 1 calc R . . . .
C02U C 0.8074(11) -0.0484(12) 0.6673(3) 0.096(5) Uani 1 1 d G U . . .
H02U H 0.849459 -0.041319 0.673045 0.115 Uiso 1 1 calc R . . . .
C02I C 0.7888(12) -0.0765(11) 0.6486(3) 0.094(4) Uani 1 1 d G U . . .
H02I H 0.818070 -0.088639 0.641507 0.113 Uiso 1 1 calc R . . . .
C01P C 0.7273(13) -0.0870(11) 0.6402(2) 0.095(5) Uani 1 1 d G U . . .
H01P H 0.714551 -0.106166 0.627373 0.114 Uiso 1 1 calc R . . . .
C01F C 0.6844(11) -0.0693(11) 0.6505(3) 0.091(4) Uani 1 1 d G U . . .
H01F H 0.642420 -0.076372 0.644778 0.110 Uiso 1 1 calc R . . . .
C011 C 0.7018(9) 0.0417(7) 0.7004(2) 0.081(4) Uani 1 1 d . U . . .
N00M N 0.7448(9) 0.1064(8) 0.69198(17) 0.050(5) Uani 1 1 d G . . . .
C01G C 0.7945(9) 0.1603(7) 0.7034(2) 0.080(4) Uani 1 1 d G U . . .
H01G H 0.823854 0.204444 0.697611 0.096 Uiso 1 1 calc R . . . .
C024 C 0.8011(10) 0.1496(8) 0.7232(2) 0.078(4) Uani 1 1 d G U . . .
H024 H 0.835063 0.186392 0.730930 0.094 Uiso 1 1 calc R . . . .
C02R C 0.7581(12) 0.0849(10) 0.73157(18) 0.081(4) Uani 1 1 d G U . . .
H02R H 0.762671 0.077595 0.745092 0.097 Uiso 1 1 calc R . . . .
C01Y C 0.7085(11) 0.0310(8) 0.7202(2) 0.083(4) Uani 1 1 d G U . . .
H01Y H 0.679068 -0.013152 0.725935 0.100 Uiso 1 1 calc R . . . .
N012 N 0.4312(15) 0.3619(17) 0.6189(5) 0.101(4) Uani 1 1 d D U . . .
C013 C 0.3401(14) -0.1037(13) 0.6343(5) 0.069(3) Uani 1 1 d . U . . .
H01A H 0.353323 -0.111122 0.620993 0.083 Uiso 1 1 calc R . . . .
H01B H 0.333009 -0.063177 0.633704 0.083 Uiso 1 1 calc R . . . .
C014 C 0.5758(12) 0.5085(13) 0.7290(3) 0.045(3) Uani 1 1 d . U . . .
H014 H 0.566274 0.546250 0.732985 0.054 Uiso 1 1 calc R . . . .
C015 C 0.8107(16) 0.1883(17) 0.5334(4) 0.068(3) Uani 1 1 d . U . . .
H015 H 0.858466 0.218368 0.527975 0.081 Uiso 1 1 calc R . . . .
C016 C 0.6688(13) 0.4746(12) 0.7265(3) 0.046(3) Uani 1 1 d . U . . .
H016 H 0.719158 0.491154 0.728736 0.056 Uiso 1 1 calc R . . . .
C017 C 0.6517(13) 0.5304(13) 0.7322(3) 0.049(3) Uani 1 1 d . U . . .
H01C H 0.663189 0.541957 0.746279 0.059 Uiso 1 1 calc R . . . .
H01D H 0.681022 0.572848 0.724498 0.059 Uiso 1 1 calc R . . . .
C018 C 0.7116(15) 0.1901(16) 0.5510(4) 0.064(3) Uani 1 1 d . U . . .
C019 C 0.5481(13) 0.3849(13) 0.7358(3) 0.049(3) Uani 1 1 d . U . . .
H019 H 0.520132 0.342869 0.744150 0.058 Uiso 1 1 calc R . . . .
C01A C 0.2709(15) -0.1698(13) 0.6408(5) 0.069(3) Uani 1 1 d . U . . .
H01E H 0.232777 -0.177322 0.631527 0.083 Uiso 1 1 calc R . . . .
C01B C 0.3417(15) -0.2175(14) 0.6538(5) 0.070(3) Uani 1 1 d . U . . .
H01H H 0.349912 -0.257810 0.653168 0.084 Uiso 1 1 calc R . . . .
C01D C 0.4218(18) 0.0116(14) 0.5654(4) 0.076(4) Uani 1 1 d . U . . .
C01H C 0.7120(15) 0.1390(16) 0.5669(4) 0.064(3) Uani 1 1 d . U . . .
H01I H 0.664475 0.108251 0.571902 0.077 Uiso 1 1 calc R . . . .
H01K H 0.742420 0.165365 0.577996 0.077 Uiso 1 1 calc R . . . .
C01I C 0.3110(15) -0.1502(14) 0.6743(5) 0.073(3) Uani 1 1 d . U . . .
H01L H 0.297977 -0.145284 0.688044 0.088 Uiso 1 1 calc R . . . .
C01K C 0.5318(13) 0.4411(13) 0.7418(3) 0.050(3) Uani 1 1 d . U . . .
H01M H 0.542820 0.452339 0.755827 0.061 Uiso 1 1 calc R . . . .
H01N H 0.481682 0.424009 0.739860 0.061 Uiso 1 1 calc R . . . .
C01L C 0.8101(15) 0.1387(16) 0.5488(4) 0.069(3) Uani 1 1 d . U . . .
H01O H 0.828748 0.110475 0.543044 0.082 Uiso 1 1 calc R . . . .
H01Q H 0.840646 0.165730 0.559856 0.082 Uiso 1 1 calc R . . . .
C01M C 0.4131(19) 0.0376(14) 0.5455(4) 0.079(4) Uani 1 1 d . U . . .
H01S H 0.457572 0.078179 0.541281 0.095 Uiso 1 1 calc R . . . .
H01T H 0.377679 0.052147 0.546334 0.095 Uiso 1 1 calc R . . . .
C01N C 0.7610(14) 0.1428(16) 0.5176(4) 0.065(3) Uani 1 1 d . U . . .
H01V H 0.777957 0.112789 0.512065 0.078 Uiso 1 1 calc R . . . .
H01W H 0.760793 0.172756 0.506840 0.078 Uiso 1 1 calc R . . . .
C01O C 0.2506(16) 0.1457(18) 0.6144(4) 0.094(4) Uani 1 1 d D U . . .
H01X H 0.210069 0.129975 0.605585 0.113 Uiso 1 1 calc R . . . .
H01Z H 0.275300 0.197066 0.614822 0.113 Uiso 1 1 calc R . . . .
C01S C 0.3498(18) -0.0498(14) 0.5706(5) 0.081(4) Uani 1 1 d . U . . .
H01 H 0.313804 -0.036348 0.568842 0.097 Uiso 1 1 calc R . . . .
H H 0.348905 -0.063751 0.584422 0.097 Uiso 1 1 calc R . . . .
C01T C 0.6508(12) 0.4594(13) 0.7045(3) 0.047(3) Uani 1 1 d . U . . .
H0AA H 0.663233 0.424781 0.699845 0.056 Uiso 1 1 calc R . . . .
HA H 0.677833 0.502509 0.696769 0.056 Uiso 1 1 calc R . . . .
C01V C 0.2259(16) 0.1188(14) 0.6341(5) 0.092(4) Uani 1 1 d D U . . .
H1AA H 0.192021 0.132875 0.638705 0.110 Uiso 1 1 calc R . . . .
C01W C 0.6233(12) 0.4099(13) 0.7389(3) 0.049(3) Uani 1 1 d . U . . .
H2AA H 0.633222 0.372525 0.735309 0.058 Uiso 1 1 calc R . . . .
HB H 0.634929 0.421046 0.752939 0.058 Uiso 1 1 calc R . . . .
C01X C 0.2857(15) -0.2295(13) 0.6387(5) 0.071(3) Uani 1 1 d . U . . .
H3AA H 0.302225 -0.230446 0.625282 0.085 Uiso 1 1 calc R . . . .
HC H 0.242993 -0.274456 0.641233 0.085 Uiso 1 1 calc R . . . .
C01Z C 0.6642(15) 0.1479(16) 0.5345(4) 0.066(3) Uani 1 1 d . U . . .
H4AA H 0.665549 0.179877 0.524136 0.080 Uiso 1 1 calc R . . . .
HD H 0.616020 0.121509 0.539471 0.080 Uiso 1 1 calc R . . . .
O021 O 0.3763(13) 0.3583(14) 0.6120(4) 0.101(4) Uani 1 1 d D U . . .
C022 C 0.7850(15) 0.2308(17) 0.5434(4) 0.069(3) Uani 1 1 d . U . . .
H02A H 0.787915 0.266366 0.534082 0.083 Uiso 1 1 calc R . . . .
H02D H 0.816287 0.255589 0.554555 0.083 Uiso 1 1 calc R . . . .
C023 C 0.3884(18) -0.1278(15) 0.5549(5) 0.082(4) Uani 1 1 d . U . . .
H02E H 0.374227 -0.165176 0.545046 0.098 Uiso 1 1 calc R . . . .
H02F H 0.394717 -0.145404 0.567622 0.098 Uiso 1 1 calc R . . . .
C025 C 0.3353(19) -0.1104(15) 0.5568(5) 0.081(4) Uani 1 1 d . U . . .
H025 H 0.292292 -0.152628 0.561458 0.097 Uiso 1 1 calc R . . . .
C027 C 0.3267(15) -0.2091(13) 0.6739(5) 0.073(3) Uani 1 1 d . U . . .
H02G H 0.367105 -0.197990 0.682395 0.088 Uiso 1 1 calc R . . . .
H02J H 0.286211 -0.252485 0.678755 0.088 Uiso 1 1 calc R . . . .
C028 C 0.3898(18) -0.0224(14) 0.5303(5) 0.080(4) Uani 1 1 d . U . . .
H028 H 0.382306 -0.006597 0.517299 0.096 Uiso 1 1 calc R . . . .
C02A C 0.4776(18) -0.0079(15) 0.5644(5) 0.081(4) Uani 1 1 d . U . . .
H02K H 0.483187 -0.024621 0.577359 0.098 Uiso 1 1 calc R . . . .
H02L H 0.522474 0.033075 0.560669 0.098 Uiso 1 1 calc R . . . .
C02F C 0.6900(16) 0.0517(17) 0.5402(4) 0.070(3) Uani 1 1 d . U . . .
H02N H 0.704562 0.020709 0.534002 0.085 Uiso 1 1 calc R . . . .
H02O H 0.643781 0.022076 0.546233 0.085 Uiso 1 1 calc R . . . .
C02G C 0.7413(15) 0.0935(16) 0.5561(4) 0.065(3) Uani 1 1 d . U . . .
H02P H 0.743039 0.060911 0.565852 0.078 Uiso 1 1 calc R . . . .
C02J C 0.4500(18) -0.0401(15) 0.5285(4) 0.081(4) Uani 1 1 d . U . . .
H02Q H 0.438563 -0.076336 0.518431 0.097 Uiso 1 1 calc R . . . .
H02S H 0.494259 0.001847 0.524854 0.097 Uiso 1 1 calc R . . . .
C02K C 0.4556(19) -0.0662(14) 0.5488(4) 0.081(4) Uani 1 1 d . U . . .
H02T H 0.491849 -0.080229 0.548256 0.097 Uiso 1 1 calc R . . . .
C02O C 0.3053(17) 0.0528(17) 0.6428(6) 0.091(4) Uani 1 1 d . U . . .
H02V H 0.287307 0.040337 0.656357 0.110 Uiso 1 1 calc R . . . .
H02X H 0.336646 0.034110 0.640183 0.110 Uiso 1 1 calc R . . . .
C02P C 0.6844(15) 0.0956(16) 0.5251(4) 0.068(3) Uani 1 1 d . U . . .
H02Y H 0.652071 0.067529 0.514305 0.081 Uiso 1 1 calc R . . . .
F02Q F 0.372(3) -0.255(3) 0.6010(6) 0.32(3) Uani 1 1 d . . . . .
F02S F 0.4151(16) -0.288(2) 0.5719(7) 0.25(2) Uani 1 1 d . . . . .
C02Y C 0.3677(17) 0.1513(19) 0.6194(6) 0.093(4) Uani 1 1 d . U . . .
H02Z H 0.394452 0.129089 0.615084 0.112 Uiso 1 1 calc R . . . .
HE H 0.397405 0.202334 0.618138 0.112 Uiso 1 1 calc R . . . .
C5 C 0.3203(18) -0.0913(14) 0.5368(4) 0.081(4) Uani 1 1 d . U . . .
H5A H 0.280884 -0.082588 0.537488 0.098 Uiso 1 1 calc R . . . .
H5B H 0.308774 -0.129266 0.527254 0.098 Uiso 1 1 calc R . . . .
C10 C 0.2674(16) 0.0482(14) 0.6075(5) 0.093(4) Uani 1 1 d D U . . .
H10A H 0.229059 0.025373 0.597941 0.112 Uiso 1 1 calc R . . . .
H10B H 0.303605 0.036531 0.603966 0.112 Uiso 1 1 calc R . . . .
C12 C 0.1964(15) 0.0443(14) 0.6360(5) 0.093(4) Uani 1 1 d D U . . .
H12A H 0.150297 0.020316 0.629515 0.112 Uiso 1 1 calc R . . . .
H12B H 0.189692 0.031452 0.650039 0.112 Uiso 1 1 calc R . . . .
C13 C 0.2413(15) 0.0216(18) 0.6271(4) 0.092(4) Uani 1 1 d D U . . .
H13 H 0.217436 -0.030334 0.627031 0.111 Uiso 1 1 calc R . . . .
C23 C 0.2968(15) 0.1232(14) 0.6065(6) 0.095(4) Uani 1 1 d D U . . .
H23 H 0.308787 0.139230 0.592553 0.114 Uiso 1 1 calc R . . . .
N01J N 0.6487(9) 0.4471(9) 0.50420(19) 0.062(4) Uani 0.3333 1 d . . . C 2
H5AA H 0.627976 0.430297 0.515518 0.074 Uiso 0.3333 1 calc R . . C 2
F8 F 0.3107(12) -0.0604(14) 0.7243(5) 0.145(12) Uani 0.5 1 d D U . . .
F14 F 0.3007(14) 0.0389(11) 0.7420(3) 0.137(8) Uani 0.5 1 d D U . . .
F15 F 0.2048(16) -0.0847(13) 0.7020(3) 0.162(14) Uani 0.5 1 d D U . . .
F27 F 0.3105(14) 0.0387(13) 0.7036(3) 0.142(12) Uani 0.5 1 d D U . . .
F34 F 0.1929(13) -0.0869(12) 0.7404(3) 0.163(13) Uani 0.5 1 d D U . . .
F56 F 0.1937(12) 0.0134(14) 0.7200(5) 0.155(13) Uani 0.5 1 d D U . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag01 Ag02 2.8076(15) 2_655 ?
Ag01 Ag02 2.8076(15) 3_665 ?
Ag01 Ag02 2.8076(15) . ?
Ag01 Ag03 2.759(2) 2_655 ?
Ag01 Ag03 2.759(2) . ?
Ag01 Ag03 2.759(2) 3_665 ?
Ag01 Ag04 2.796(2) 3_665 ?
Ag01 Ag04 2.796(2) 2_655 ?
Ag01 Ag04 2.796(2) . ?
Ag01 Ag05 2.7986(15) 2_655 ?
Ag01 Ag05 2.7986(15) . ?
Ag01 Ag05 2.7986(15) 3_665 ?
Ag02 Ag03 2.935(2) 2_655 ?
Ag02 Ag03 2.958(2) . ?
Ag02 Ag04 2.836(2) 3_665 ?
Ag02 Ag05 3.111(2) . ?
Ag02 Ag05 2.805(2) 2_655 ?
Ag02 Ag07 3.106(2) . ?
Ag02 Ag0A 3.077(2) . ?
Ag02 S00F 2.505(5) . ?
Ag03 Ag02 2.936(2) 3_665 ?
Ag03 Ag03 2.801(2) 2_655 ?
Ag03 Ag03 2.801(2) 3_665 ?
Ag03 Ag05 3.024(2) . ?
Ag03 Ag0A 3.058(2) . ?
Ag03 S00D 2.434(5) . ?
Ag04 Ag02 2.836(2) 2_655 ?
Ag04 Ag04 3.121(3) 3_665 ?
Ag04 Ag04 3.121(3) 2_655 ?
Ag04 Ag05 2.899(2) 3_665 ?
Ag04 Ag05 2.855(2) 2_655 ?
Ag04 Ag06 2.881(2) 2_655 ?
Ag04 S00E 2.467(5) . ?
Ag05 Ag02 2.805(2) 3_665 ?
Ag05 Ag04 2.855(2) 3_665 ?
Ag05 Ag04 2.899(2) 2_655 ?
Ag05 Ag06 3.097(2) 3_665 ?
Ag05 Ag08 3.193(2) 3_665 ?
Ag05 O00Z 2.22(3) . ?
Ag06 Ag04 2.881(2) 3_665 ?
Ag06 Ag05 3.097(2) 2_655 ?
Ag06 S00E 2.398(5) . ?
Ag06 S00G 2.383(6) . ?
Ag07 Ag08 2.985(2) . ?
Ag07 S00D 2.660(5) 2_655 ?
Ag07 S00F 2.464(6) . ?
Ag07 S00H 2.508(6) . ?
Ag08 Ag05 3.193(2) 2_655 ?
Ag08 S00G 2.370(6) . ?
Ag08 S00H 2.383(6) . ?
Ag09 S00E 2.642(5) 2_655 ?
Ag09 S00E 2.642(5) 3_665 ?
Ag09 S00E 2.642(5) . ?
Ag09 P00I 2.411(9) . ?
Ag0A Ag0B 3.201(3) 3_665 ?
Ag0A S00D 2.497(5) . ?
Ag0A S00F 2.472(6) . ?
Ag0B Ag0A 3.201(3) 2_655 ?
Ag0B S00D 2.736(5) 2_655 ?
Ag0B S00H 2.499(6) . ?
Ag0B P00K 2.399(7) . ?
Sb0C F02Q 1.81(4) . ?
Sb0C F02Q 1.81(4) 2_545 ?
Sb0C F02Q 1.81(4) 3_655 ?
Sb0C F02S 1.86(3) 3_655 ?
Sb0C F02S 1.86(3) . ?
Sb0C F02S 1.86(3) 2_545 ?
S00D Ag07 2.660(5) 3_665 ?
S00D Ag0B 2.736(5) 3_665 ?
S00D C00P 1.85(2) . ?
S00E C018 1.83(3) . ?
S00F C00N 1.87(3) . ?
S00G C01D 1.85(3) . ?
S00H C00L 1.85(3) . ?
P00I C00S 1.835(12) . ?
P00I C00S 1.835(12) 3_665 ?
P00I C00S 1.835(12) 2_655 ?
Sb00 F8 1.856(9) . ?
Sb00 F14 1.845(9) . ?
Sb00 F14 2.49(3) 5_556 ?
Sb00 F15 1.849(9) . ?
Sb00 F27 1.844(9) . ?
Sb00 F34 1.846(9) . ?
Sb00 F56 1.857(9) . ?
P00K C00U 1.812(16) . ?
P00K C010 1.805(18) . ?
P00K C011 1.787(15) . ?
C00L C00T 1.47(4) . ?
C00L C00W 1.52(4) . ?
C00L C013 1.50(4) . ?
C00N C00O 1.51(5) . ?
C00N C02O 1.54(5) . ?
C00N C02Y 1.49(5) . ?
C00O C01V 1.59(4) . ?
C00P C00Q 1.53(3) . ?
C00P C00Y 1.53(3) . ?
C00P C01T 1.58(3) . ?
C00Q C014 1.53(3) . ?
O00R N012 1.17(3) . ?
C00S C01U 1.3900 . ?
C00S C01J 1.3900 . ?
C00S N01J 1.3900 . ?
C01U C026 1.3900 . ?
C026 C02H 1.3900 . ?
C02H C7 1.3900 . ?
C7 C01J 1.3900 . ?
C7 N01J 1.3900 . ?
C00T C01I 1.54(3) . ?
C00U C02M 1.3900 . ?
C00U C01R 1.3900 . ?
C02M C02W 1.3900 . ?
C02W C02C 1.3900 . ?
C02C C02B 1.3900 . ?
C02B C01R 1.3900 . ?
C00W C01B 1.60(3) . ?
C00X C01A 1.46(4) . ?
C00X C01I 1.52(4) . ?
C00Y C019 1.56(3) . ?
O00Z N012 1.31(4) . ?
C010 C029 1.3900 . ?
C010 C01F 1.3900 . ?
C029 C02U 1.3900 . ?
C02U C02I 1.3900 . ?
C02I C01P 1.3900 . ?
C01P C01F 1.3900 . ?
C011 N00M 1.3900 . ?
C011 C01Y 1.3900 . ?
N00M Ag0A 2.559(13) 2_655 ?
N00M C01G 1.3900 . ?
C01G C024 1.3900 . ?
C024 C02R 1.3900 . ?
C02R C01Y 1.3900 . ?
N012 O021 1.273(10) . ?
C013 C01A 1.57(3) . ?
C014 C017 1.52(3) . ?
C014 C01K 1.58(3) . ?
C015 C01L 1.52(4) . ?
C015 C01N 1.51(4) . ?
C015 C022 1.49(3) . ?
C016 C017 1.52(3) . ?
C016 C01T 1.54(3) . ?
C016 C01W 1.53(3) . ?
C018 C01H 1.57(4) . ?
C018 C01Z 1.51(4) . ?
C018 C022 1.51(4) . ?
C019 C01K 1.52(3) . ?
C019 C01W 1.49(3) . ?
C01A C01X 1.53(4) . ?
C01B C01X 1.53(4) . ?
C01B C027 1.45(4) . ?
C01D C01M 1.53(4) . ?
C01D C01S 1.54(4) . ?
C01D C02A 1.50(5) . ?
C01H C02G 1.63(3) . ?
C01I C027 1.52(4) . ?
C01L C02G 1.43(4) . ?
C01M C028 1.56(4) . ?
C01N C02P 1.57(4) . ?
C01O C01V 1.458(10) . ?
C01O C23 1.452(10) . ?
C01S C025 1.54(4) . ?
C01V C12 1.449(10) . ?
C01Z C02P 1.58(3) . ?
C023 C025 1.42(5) . ?
C023 C02K 1.49(4) . ?
C025 C5 1.51(4) . ?
C028 C02J 1.58(5) . ?
C028 C5 1.60(4) . ?
C02A C02K 1.55(4) . ?
C02F C02G 1.51(4) . ?
C02F C02P 1.47(4) . ?
C02J C02K 1.53(4) . ?
C02O C13 1.63(4) . ?
C02Y C23 1.63(4) . ?
C10 C13 1.454(10) . ?
C10 C23 1.458(10) . ?
C12 C13 1.458(10) . ?
F14 Sb00 2.49(3) 5_556 ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Ag02 Ag01 Ag02 116.58(3) 2_655 3_665 ?
Ag02 Ag01 Ag02 116.58(3) 2_655 . ?
Ag02 Ag01 Ag02 116.58(3) . 3_665 ?
Ag03 Ag01 Ag02 63.64(5) 2_655 . ?
Ag03 Ag01 Ag02 64.21(5) 3_665 3_665 ?
Ag03 Ag01 Ag02 63.65(5) 3_665 2_655 ?
Ag03 Ag01 Ag02 64.21(5) 2_655 2_655 ?
Ag03 Ag01 Ag02 115.11(8) . 2_655 ?
Ag03 Ag01 Ag02 64.20(5) . . ?
Ag03 Ag01 Ag02 115.10(8) 3_665 . ?
Ag03 Ag01 Ag02 115.10(8) 2_655 3_665 ?
Ag03 Ag01 Ag02 63.65(5) . 3_665 ?
Ag03 Ag01 Ag03 61.02(7) 2_655 3_665 ?
Ag03 Ag01 Ag03 61.02(7) 2_655 . ?
Ag03 Ag01 Ag03 61.02(6) 3_665 . ?
Ag03 Ag01 Ag04 113.98(4) 3_665 2_655 ?
Ag03 Ag01 Ag04 175.01(6) . . ?
Ag03 Ag01 Ag04 113.99(4) 2_655 . ?
Ag03 Ag01 Ag04 117.11(4) . 2_655 ?
Ag03 Ag01 Ag04 175.00(6) 3_665 3_665 ?
Ag03 Ag01 Ag04 117.11(4) 3_665 . ?
Ag03 Ag01 Ag04 113.98(4) . 3_665 ?
Ag03 Ag01 Ag04 175.00(6) 2_655 2_655 ?
Ag03 Ag01 Ag04 117.11(4) 2_655 3_665 ?
Ag03 Ag01 Ag05 114.92(6) 3_665 . ?
Ag03 Ag01 Ag05 118.78(6) 3_665 2_655 ?
Ag03 Ag01 Ag05 65.92(5) 3_665 3_665 ?
Ag03 Ag01 Ag05 65.92(5) . . ?
Ag03 Ag01 Ag05 118.78(6) 2_655 . ?
Ag03 Ag01 Ag05 114.92(6) . 2_655 ?
Ag03 Ag01 Ag05 118.78(6) . 3_665 ?
Ag03 Ag01 Ag05 65.92(5) 2_655 2_655 ?
Ag03 Ag01 Ag05 114.92(6) 2_655 3_665 ?
Ag04 Ag01 Ag02 114.37(6) . . ?
Ag04 Ag01 Ag02 114.36(6) 3_665 3_665 ?
Ag04 Ag01 Ag02 114.36(6) 2_655 2_655 ?
Ag04 Ag01 Ag02 60.81(5) . 2_655 ?
Ag04 Ag01 Ag02 60.80(5) 2_655 3_665 ?
Ag04 Ag01 Ag02 120.30(6) 3_665 2_655 ?
Ag04 Ag01 Ag02 120.30(6) . 3_665 ?
Ag04 Ag01 Ag02 60.81(5) 3_665 . ?
Ag04 Ag01 Ag02 120.30(6) 2_655 . ?
Ag04 Ag01 Ag04 67.85(7) 2_655 . ?
Ag04 Ag01 Ag04 67.85(7) 3_665 2_655 ?
Ag04 Ag01 Ag04 67.85(7) 3_665 . ?
Ag04 Ag01 Ag05 118.38(8) 2_655 2_655 ?
Ag04 Ag01 Ag05 62.41(5) 2_655 . ?
Ag04 Ag01 Ag05 61.37(5) 3_665 . ?
Ag04 Ag01 Ag05 61.37(5) . 2_655 ?
Ag04 Ag01 Ag05 62.41(5) 3_665 2_655 ?
Ag04 Ag01 Ag05 62.41(5) . 3_665 ?
Ag04 Ag01 Ag05 118.37(8) . . ?
Ag04 Ag01 Ag05 61.37(5) 2_655 3_665 ?
Ag04 Ag01 Ag05 118.38(8) 3_665 3_665 ?
Ag05 Ag01 Ag02 60.05(4) 3_665 2_655 ?
Ag05 Ag01 Ag02 60.05(4) . 3_665 ?
Ag05 Ag01 Ag02 175.99(5) 3_665 . ?
Ag05 Ag01 Ag02 67.42(4) 3_665 3_665 ?
Ag05 Ag01 Ag02 175.99(5) 2_655 3_665 ?
Ag05 Ag01 Ag02 67.42(4) . . ?
Ag05 Ag01 Ag02 67.42(4) 2_655 2_655 ?
Ag05 Ag01 Ag02 175.99(5) . 2_655 ?
Ag05 Ag01 Ag02 60.05(4) 2_655 . ?
Ag05 Ag01 Ag05 115.96(3) 2_655 . ?
Ag05 Ag01 Ag05 115.97(3) 3_665 . ?
Ag05 Ag01 Ag05 115.97(3) 2_655 3_665 ?
Ag01 Ag02 Ag03 57.37(5) . 2_655 ?
Ag01 Ag02 Ag03 57.10(5) . . ?
Ag01 Ag02 Ag04 59.39(6) . 3_665 ?
Ag01 Ag02 Ag05 56.15(4) . . ?
Ag01 Ag02 Ag07 118.19(6) . . ?
Ag01 Ag02 Ag0A 117.25(6) . . ?
Ag03 Ag02 Ag03 56.76(6) 2_655 . ?
Ag03 Ag02 Ag05 104.52(6) 2_655 . ?
Ag03 Ag02 Ag05 59.70(5) . . ?
Ag03 Ag02 Ag07 116.08(6) . . ?
Ag03 Ag02 Ag07 69.53(5) 2_655 . ?
Ag03 Ag02 Ag0A 95.54(6) 2_655 . ?
Ag03 Ag02 Ag0A 60.83(5) . . ?
Ag04 Ag02 Ag03 107.00(6) 3_665 . ?
Ag04 Ag02 Ag03 110.39(6) 3_665 2_655 ?
Ag04 Ag02 Ag05 57.15(5) 3_665 . ?
Ag04 Ag02 Ag07 123.10(6) 3_665 . ?
Ag04 Ag02 Ag0A 138.47(7) 3_665 . ?
Ag05 Ag02 Ag01 59.82(4) 2_655 . ?
Ag05 Ag02 Ag03 63.52(5) 2_655 2_655 ?
Ag05 Ag02 Ag03 108.73(6) 2_655 . ?
Ag05 Ag02 Ag04 61.84(5) 2_655 3_665 ?
Ag05 Ag02 Ag05 106.55(7) 2_655 . ?
Ag05 Ag02 Ag07 70.08(5) 2_655 . ?
Ag05 Ag02 Ag0A 157.52(7) 2_655 . ?
Ag07 Ag02 Ag05 173.94(7) . . ?
Ag0A Ag02 Ag05 85.78(5) . . ?
Ag0A Ag02 Ag07 95.81(6) . . ?
S00F Ag02 Ag01 154.17(14) . . ?
S00F Ag02 Ag03 103.88(14) . . ?
S00F Ag02 Ag03 98.32(14) . 2_655 ?
S00F Ag02 Ag04 145.96(14) . 3_665 ?
S00F Ag02 Ag05 133.12(14) . . ?
S00F Ag02 Ag05 120.28(14) . 2_655 ?
S00F Ag02 Ag07 50.73(13) . . ?
S00F Ag02 Ag0A 51.32(13) . . ?
Ag01 Ag03 Ag02 58.70(4) . . ?
Ag01 Ag03 Ag02 58.98(4) . 3_665 ?
Ag01 Ag03 Ag03 59.49(3) . 2_655 ?
Ag01 Ag03 Ag03 59.49(3) . 3_665 ?
Ag01 Ag03 Ag05 57.67(5) . . ?
Ag01 Ag03 Ag0A 119.49(6) . . ?
Ag02 Ag03 Ag02 108.29(7) 3_665 . ?
Ag02 Ag03 Ag05 62.67(5) . . ?
Ag02 Ag03 Ag05 56.14(5) 3_665 . ?
Ag02 Ag03 Ag0A 139.44(7) 3_665 . ?
Ag02 Ag03 Ag0A 61.51(5) . . ?
Ag03 Ag03 Ag02 109.25(5) 3_665 . ?
Ag03 Ag03 Ag02 61.21(6) 2_655 . ?
Ag03 Ag03 Ag02 62.04(6) 3_665 3_665 ?
Ag03 Ag03 Ag02 109.91(5) 2_655 3_665 ?
Ag03 Ag03 Ag03 59.999(1) 2_655 3_665 ?
Ag03 Ag03 Ag05 107.02(4) 3_665 . ?
Ag03 Ag03 Ag05 110.33(4) 2_655 . ?
Ag03 Ag03 Ag0A 98.84(8) 2_655 . ?
Ag03 Ag03 Ag0A 157.15(7) 3_665 . ?
Ag05 Ag03 Ag0A 87.68(6) . . ?
S00D Ag03 Ag01 151.84(13) . . ?
S00D Ag03 Ag02 110.67(13) . . ?
S00D Ag03 Ag02 107.50(13) . 3_665 ?
S00D Ag03 Ag03 139.93(13) . 3_665 ?
S00D Ag03 Ag03 142.30(14) . 2_655 ?
S00D Ag03 Ag05 94.17(12) . . ?
S00D Ag03 Ag0A 52.60(13) . . ?
Ag01 Ag04 Ag02 59.79(5) . 2_655 ?
Ag01 Ag04 Ag04 56.07(3) . 3_665 ?
Ag01 Ag04 Ag04 56.07(3) . 2_655 ?
Ag01 Ag04 Ag05 58.83(4) . 3_665 ?
Ag01 Ag04 Ag05 59.35(4) . 2_655 ?
Ag01 Ag04 Ag06 116.98(6) . 2_655 ?
Ag02 Ag04 Ag04 104.37(5) 2_655 2_655 ?
Ag02 Ag04 Ag04 109.25(4) 2_655 3_665 ?
Ag02 Ag04 Ag05 58.55(5) 2_655 3_665 ?
Ag02 Ag04 Ag05 66.28(5) 2_655 2_655 ?
Ag02 Ag04 Ag06 110.65(6) 2_655 2_655 ?
Ag04 Ag04 Ag04 60.000(1) 2_655 3_665 ?
Ag05 Ag04 Ag04 57.82(6) 2_655 3_665 ?
Ag05 Ag04 Ag04 106.94(5) 2_655 2_655 ?
Ag05 Ag04 Ag04 56.48(5) 3_665 2_655 ?
Ag05 Ag04 Ag04 105.85(5) 3_665 3_665 ?
Ag05 Ag04 Ag05 111.13(7) 2_655 3_665 ?
Ag05 Ag04 Ag06 175.93(7) 2_655 2_655 ?
Ag06 Ag04 Ag04 70.88(6) 2_655 2_655 ?
Ag06 Ag04 Ag04 122.30(5) 2_655 3_665 ?
Ag06 Ag04 Ag05 64.81(5) 2_655 3_665 ?
S00E Ag04 Ag01 136.54(14) . . ?
S00E Ag04 Ag02 150.91(13) . 2_655 ?
S00E Ag04 Ag04 80.47(13) . 3_665 ?
S00E Ag04 Ag04 104.14(12) . 2_655 ?
S00E Ag04 Ag05 99.74(13) . 2_655 ?
S00E Ag04 Ag05 146.98(13) . 3_665 ?
S00E Ag04 Ag06 84.20(13) . 2_655 ?
Ag01 Ag05 Ag02 60.14(4) . 3_665 ?
Ag01 Ag05 Ag02 56.43(4) . . ?
Ag01 Ag05 Ag03 56.41(6) . . ?
Ag01 Ag05 Ag04 58.75(5) . 2_655 ?
Ag01 Ag05 Ag04 59.27(5) . 3_665 ?
Ag01 Ag05 Ag06 110.26(7) . 3_665 ?
Ag01 Ag05 Ag08 151.25(6) . 3_665 ?
Ag02 Ag05 Ag02 107.57(7) 3_665 . ?
Ag02 Ag05 Ag03 60.34(5) 3_665 . ?
Ag02 Ag05 Ag04 112.61(6) 3_665 3_665 ?
Ag02 Ag05 Ag04 59.60(5) 3_665 2_655 ?
Ag02 Ag05 Ag06 105.50(6) 3_665 3_665 ?
Ag02 Ag05 Ag08 91.92(6) 3_665 3_665 ?
Ag02 Ag05 Ag08 148.89(7) . 3_665 ?
Ag03 Ag05 Ag02 57.64(5) . . ?
Ag03 Ag05 Ag06 163.48(7) . 3_665 ?
Ag03 Ag05 Ag08 117.75(6) . 3_665 ?
Ag04 Ag05 Ag02 107.88(6) 2_655 . ?
Ag04 Ag05 Ag02 56.56(5) 3_665 . ?
Ag04 Ag05 Ag03 104.78(6) 3_665 . ?
Ag04 Ag05 Ag03 106.28(6) 2_655 . ?
Ag04 Ag05 Ag04 65.70(7) 3_665 2_655 ?
Ag04 Ag05 Ag06 57.32(5) 2_655 3_665 ?
Ag04 Ag05 Ag06 71.56(5) 3_665 3_665 ?
Ag04 Ag05 Ag08 137.36(6) 3_665 3_665 ?
Ag04 Ag05 Ag08 102.85(6) 2_655 3_665 ?
Ag06 Ag05 Ag02 125.85(6) 3_665 . ?
Ag06 Ag05 Ag08 68.41(5) 3_665 3_665 ?
O00Z Ag05 Ag01 149.2(7) . . ?
O00Z Ag05 Ag02 150.6(7) . 3_665 ?
O00Z Ag05 Ag02 97.1(7) . . ?
O00Z Ag05 Ag03 126.0(7) . . ?
O00Z Ag05 Ag04 94.1(7) . 3_665 ?
O00Z Ag05 Ag04 127.5(7) . 2_655 ?
O00Z Ag05 Ag06 70.5(7) . 3_665 ?
O00Z Ag05 Ag08 59.1(7) . 3_665 ?
Ag04 Ag06 Ag05 57.87(5) 3_665 2_655 ?
S00E Ag06 Ag04 86.80(13) . 3_665 ?
S00E Ag06 Ag05 94.93(13) . 2_655 ?
S00G Ag06 Ag04 96.39(13) . 3_665 ?
S00G Ag06 Ag05 91.10(14) . 2_655 ?
S00G Ag06 S00E 173.98(19) . . ?
Ag08 Ag07 Ag02 90.34(6) . . ?
S00D Ag07 Ag02 97.36(12) 2_655 . ?
S00D Ag07 Ag08 121.84(12) 2_655 . ?
S00F Ag07 Ag02 51.92(12) . . ?
S00F Ag07 Ag08 115.36(14) . . ?
S00F Ag07 S00D 114.26(18) . 2_655 ?
S00F Ag07 S00H 151.92(19) . . ?
S00H Ag07 Ag02 137.48(14) . . ?
S00H Ag07 Ag08 50.51(13) . . ?
S00H Ag07 S00D 92.14(17) . 2_655 ?
Ag07 Ag08 Ag05 66.74(5) . 2_655 ?
S00G Ag08 Ag05 89.04(14) . 2_655 ?
S00G Ag08 Ag07 124.51(14) . . ?
S00G Ag08 S00H 171.1(2) . . ?
S00H Ag08 Ag05 97.72(14) . 2_655 ?
S00H Ag08 Ag07 54.31(14) . . ?
S00E Ag09 S00E 90.39(16) 3_665 . ?
S00E Ag09 S00E 90.39(16) 2_655 . ?
S00E Ag09 S00E 90.39(16) 2_655 3_665 ?
P00I Ag09 S00E 124.99(12) . 2_655 ?
P00I Ag09 S00E 124.99(12) . 3_665 ?
P00I Ag09 S00E 124.99(12) . . ?
Ag02 Ag0A Ag0B 124.00(7) . 3_665 ?
Ag03 Ag0A Ag02 57.66(5) . . ?
Ag03 Ag0A Ag0B 98.15(6) . 3_665 ?
S00D Ag0A Ag02 105.31(12) . . ?
S00D Ag0A Ag03 50.77(11) . . ?
S00D Ag0A Ag0B 55.75(12) . 3_665 ?
S00D Ag0A N00M 104(2) . 3_665 ?
S00F Ag0A Ag02 52.30(12) . . ?
S00F Ag0A Ag03 101.94(13) . . ?
S00F Ag0A Ag0B 147.59(15) . 3_665 ?
S00F Ag0A S00D 152.17(18) . . ?
S00F Ag0A N00M 97(3) . 3_665 ?
N00M Ag0A Ag0B 79(3) 3_665 3_665 ?
S00D Ag0B Ag0A 48.96(11) 2_655 2_655 ?
S00H Ag0B Ag0A 121.49(13) . 2_655 ?
S00H Ag0B S00D 90.55(17) . 2_655 ?
P00K Ag0B Ag0A 87.28(18) . 2_655 ?
P00K Ag0B S00D 114.2(2) . 2_655 ?
P00K Ag0B S00H 150.9(2) . . ?
F02Q Sb0C F02Q 92(2) 2_545 3_655 ?
F02Q Sb0C F02Q 92(2) . 2_545 ?
F02Q Sb0C F02Q 92(2) . 3_655 ?
F02Q Sb0C F02S 85(2) 2_545 2_545 ?
F02Q Sb0C F02S 88(2) . 2_545 ?
F02Q Sb0C F02S 88(2) 2_545 3_655 ?
F02Q Sb0C F02S 177(3) . 3_655 ?
F02Q Sb0C F02S 177(3) 3_655 2_545 ?
F02Q Sb0C F02S 177(3) 2_545 . ?
F02Q Sb0C F02S 85(2) 3_655 3_655 ?
F02Q Sb0C F02S 85(2) . . ?
F02Q Sb0C F02S 88(2) 3_655 . ?
F02S Sb0C F02S 95(2) 3_655 . ?
F02S Sb0C F02S 95(2) 2_545 3_655 ?
F02S Sb0C F02S 95(2) 2_545 . ?
Ag03 S00D Ag07 85.04(15) . 3_665 ?
Ag03 S00D Ag0A 76.63(15) . . ?
Ag03 S00D Ag0B 132.3(2) . 3_665 ?
Ag07 S00D Ag0B 84.45(15) 3_665 3_665 ?
Ag0A S00D Ag07 130.0(2) . 3_665 ?
Ag0A S00D Ag0B 75.29(14) . 3_665 ?
C00P S00D Ag03 111.7(7) . . ?
C00P S00D Ag07 112.3(9) . 3_665 ?
C00P S00D Ag0A 117.7(9) . . ?
C00P S00D Ag0B 115.4(7) . 3_665 ?
Ag04 S00E Ag09 109.44(19) . . ?
Ag06 S00E Ag04 91.53(17) . . ?
Ag06 S00E Ag09 106.2(2) . . ?
C018 S00E Ag04 119.8(9) . . ?
C018 S00E Ag06 107.6(10) . . ?
C018 S00E Ag09 118.1(10) . . ?
Ag07 S00F Ag02 77.35(15) . . ?
Ag07 S00F Ag0A 136.7(2) . . ?
Ag0A S00F Ag02 76.38(16) . . ?
C00N S00F Ag02 106.9(13) . . ?
C00N S00F Ag07 109.3(11) . . ?
C00N S00F Ag0A 110.9(11) . . ?
Ag08 S00G Ag06 96.2(2) . . ?
C01D S00G Ag06 103.3(11) . . ?
C01D S00G Ag08 102.7(10) . . ?
Ag08 S00H Ag07 75.18(16) . . ?
Ag08 S00H Ag0B 130.8(2) . . ?
Ag0B S00H Ag07 92.84(19) . . ?
C00L S00H Ag07 111.9(9) . . ?
C00L S00H Ag08 113.5(10) . . ?
C00L S00H Ag0B 115.2(10) . . ?
C00S P00I Ag09 114.4(6) 2_655 . ?
C00S P00I Ag09 114.4(6) . . ?
C00S P00I Ag09 114.4(6) 3_665 . ?
C00S P00I C00S 104.1(7) 2_655 . ?
C00S P00I C00S 104.1(7) 3_665 2_655 ?
C00S P00I C00S 104.1(7) 3_665 . ?
F8 Sb00 F14 74.8(8) . 5_556 ?
F8 Sb00 F56 179.7(7) . . ?
F14 Sb00 F8 90.2(5) . . ?
F14 Sb00 F14 47.9(13) . 5_556 ?
F14 Sb00 F15 179.0(9) . . ?
F14 Sb00 F34 90.5(6) . . ?
F14 Sb00 F56 90.2(5) . . ?
F15 Sb00 F8 89.9(5) . . ?
F15 Sb00 F14 133.1(13) . 5_556 ?
F15 Sb00 F56 89.8(5) . . ?
F27 Sb00 F8 90.0(5) . . ?
F27 Sb00 F14 90.8(6) . . ?
F27 Sb00 F14 134.6(13) . 5_556 ?
F27 Sb00 F15 88.2(10) . . ?
F27 Sb00 F34 178.7(9) . . ?
F27 Sb00 F56 90.0(5) . . ?
F34 Sb00 F8 90.1(5) . . ?
F34 Sb00 F14 46.6(12) . 5_556 ?
F34 Sb00 F15 90.5(6) . . ?
F34 Sb00 F56 90.0(5) . . ?
F56 Sb00 F14 105.5(8) . 5_556 ?
C00U P00K Ag0B 116.2(9) . . ?
C010 P00K Ag0B 113.6(8) . . ?
C010 P00K C00U 105.2(10) . . ?
C011 P00K Ag0B 113.9(7) . . ?
C011 P00K C00U 103.2(9) . . ?
C011 P00K C010 103.4(11) . . ?
C00T C00L S00H 110(2) . . ?
C00T C00L C00W 111(3) . . ?
C00T C00L C013 111(2) . . ?
C00W C00L S00H 106.5(19) . . ?
C013 C00L S00H 111.7(19) . . ?
C013 C00L C00W 106(2) . . ?
C00O C00N S00F 111(3) . . ?
C00O C00N C02O 107(3) . . ?
C02O C00N S00F 107(2) . . ?
C02Y C00N S00F 108(2) . . ?
C02Y C00N C00O 113(3) . . ?
C02Y C00N C02O 111(3) . . ?
C00N C00O C01V 109(3) . . ?
C00Q C00P S00D 108.8(15) . . ?
C00Q C00P C00Y 112.5(19) . . ?
C00Q C00P C01T 105.8(19) . . ?
C00Y C00P S00D 110.0(16) . . ?
C00Y C00P C01T 109.2(18) . . ?
C01T C00P S00D 110.5(15) . . ?
C00P C00Q C014 111.3(18) . . ?
C01U C00S P00I 123.6(9) . . ?
C01U C00S C01J 120.0 . . ?
C026 C01U C00S 120.0 . . ?
C01U C026 C02H 120.0 . . ?
C026 C02H C7 120.0 . . ?
C00L C00T C01I 109(2) . . ?
C02M C00U P00K 118.9(14) . . ?
C02M C00U C01R 120.0 . . ?
C01R C00U P00K 121.1(14) . . ?
C02W C02M C00U 120.0 . . ?
C02M C02W C02C 120.0 . . ?
C02B C02C C02W 120.0 . . ?
C02C C02B C01R 120.0 . . ?
C02B C01R C00U 120.0 . . ?
C00L C00W C01B 107(2) . . ?
C01A C00X C01I 108(3) . . ?
C00P C00Y C019 108(2) . . ?
N012 O00Z Ag05 123(2) . . ?
C029 C010 P00K 120.2(14) . . ?
C01F C010 P00K 119.8(14) . . ?
C01F C010 C029 120.0 . . ?
C02U C029 C010 120.0 . . ?
C02I C02U C029 120.0 . . ?
C02U C02I C01P 120.0 . . ?
C02I C01P C01F 120.0 . . ?
C01P C01F C010 120.0 . . ?
N00M C011 P00K 113.0(10) . . ?
N00M C011 C01Y 120.0 . . ?
C01Y C011 P00K 126.9(10) . . ?
C011 N00M Ag0A 127.6(9) . 2_655 ?
C011 N00M C01G 120.0 . . ?
C01G N00M Ag0A 103.0(8) . 2_655 ?
C024 C01G N00M 120.0 . . ?
C01G C024 C02R 120.0 . . ?
C01Y C02R C024 120.0 . . ?
C02R C01Y C011 120.0 . . ?
O00R N012 O00Z 101(3) . . ?
O00R N012 O021 139(4) . . ?
O021 N012 O00Z 120(3) . . ?
C00L C013 C01A 110(2) . . ?
C00Q C014 C01K 108.2(19) . . ?
C017 C014 C00Q 109.0(18) . . ?
C017 C014 C01K 106.6(19) . . ?
C01N C015 C01L 106(3) . . ?
C022 C015 C01L 106(2) . . ?
C022 C015 C01N 112(2) . . ?
C017 C016 C01T 106.7(18) . . ?
C017 C016 C01W 107.8(19) . . ?
C01W C016 C01T 111(2) . . ?
C014 C017 C016 113(2) . . ?
C01H C018 S00E 108.7(17) . . ?
C01Z C018 S00E 109.4(18) . . ?
C01Z C018 C01H 109(3) . . ?
C01Z C018 C022 109(2) . . ?
C022 C018 S00E 115(2) . . ?
C022 C018 C01H 106(2) . . ?
C01K C019 C00Y 110.4(19) . . ?
C01W C019 C00Y 109.5(19) . . ?
C01W C019 C01K 110(2) . . ?
C00X C01A C013 110(2) . . ?
C00X C01A C01X 114(3) . . ?
C01X C01A C013 105(2) . . ?
C01X C01B C00W 106(2) . . ?
C027 C01B C00W 110(2) . . ?
C027 C01B C01X 116(3) . . ?
C01M C01D S00G 106.6(19) . . ?
C01M C01D C01S 105(3) . . ?
C01S C01D S00G 110(2) . . ?
C02A C01D S00G 110(2) . . ?
C02A C01D C01M 110(3) . . ?
C02A C01D C01S 113(3) . . ?
C018 C01H C02G 107(2) . . ?
C00X C01I C00T 110(3) . . ?
C027 C01I C00T 108(2) . . ?
C027 C01I C00X 114(3) . . ?
C019 C01K C014 110.2(19) . . ?
C02G C01L C015 111(3) . . ?
C01D C01M C028 108(2) . . ?
C015 C01N C02P 113(2) . . ?
C23 C01O C01V 113(3) . . ?
C01D C01S C025 108(3) . . ?
C016 C01T C00P 109.7(18) . . ?
C01O C01V C00O 102(3) . . ?
C12 C01V C00O 109(3) . . ?
C12 C01V C01O 114(3) . . ?
C019 C01W C016 111(2) . . ?
C01A C01X C01B 107(3) . . ?
C018 C01Z C02P 113(2) . . ?
C015 C022 C018 115(3) . . ?
C025 C023 C02K 111(3) . . ?
C023 C025 C01S 117(3) . . ?
C023 C025 C5 109(3) . . ?
C5 C025 C01S 106(3) . . ?
C01B C027 C01I 107(3) . . ?
C01M C028 C02J 108(3) . . ?
C01M C028 C5 113(3) . . ?
C02J C028 C5 108(3) . . ?
C01D C02A C02K 108(3) . . ?
C02P C02F C02G 112(3) . . ?
C01L C02G C01H 110(2) . . ?
C01L C02G C02F 113(2) . . ?
C02F C02G C01H 107(2) . . ?
C02K C02J C028 105(3) . . ?
C023 C02K C02A 109(3) . . ?
C023 C02K C02J 112(3) . . ?
C02J C02K C02A 111(3) . . ?
C00N C02O C13 106(3) . . ?
C01N C02P C01Z 105(2) . . ?
C02F C02P C01N 105(2) . . ?
C02F C02P C01Z 111(2) . . ?
C00N C02Y C23 106(3) . . ?
C025 C5 C028 106(3) . . ?
C13 C10 C23 112(3) . . ?
C01V C12 C13 111(3) . . ?
C10 C13 C02O 110(3) . . ?
C10 C13 C12 116(3) . . ?
C12 C13 C02O 100(3) . . ?
C01O C23 C02Y 112(3) . . ?
C01O C23 C10 113(3) . . ?
C10 C23 C02Y 102(3) . . ?
Sb00 F14 Sb00 127.3(13) . 5_556 ?

_smtbx_masks_special_details     ?
loop_
_smtbx_masks_void_nr
_smtbx_masks_void_average_x
_smtbx_masks_void_average_y
_smtbx_masks_void_average_z
_smtbx_masks_void_volume
_smtbx_masks_void_count_electrons
_smtbx_masks_void_content
1 -0.462 -0.603 -0.445 7501.7 3702.6 ?
2 0.122 0.509 0.717 20.3 0.0 ?
3 0.122 0.613 0.217 20.3 0.0 ?
4 0.333 0.667 0.712 45.9 0.0 ?
5 0.333 0.667 0.212 45.9 0.0 ?
6 0.333 0.667 0.297 13.2 0.0 ?
7 0.333 0.667 0.797 13.2 0.0 ?
8 0.387 0.509 0.217 20.3 0.0 ?
9 0.387 0.878 0.717 20.3 0.0 ?
10 0.491 0.613 0.717 20.3 0.0 ?
11 0.491 0.878 0.217 20.3 0.0 ?
12 0.509 0.122 0.783 20.3 0.0 ?
13 0.509 0.387 0.283 20.3 0.0 ?
14 0.613 0.122 0.283 20.3 0.0 ?
15 0.613 0.491 0.783 20.3 0.0 ?
16 0.667 0.333 0.788 45.9 0.0 ?
17 0.667 0.333 0.288 45.9 0.0 ?
18 0.667 0.333 0.203 13.2 0.0 ?
19 0.667 0.333 0.703 13.2 0.0 ?
20 0.878 0.387 0.783 20.3 0.0 ?
21 0.878 0.491 0.283 20.3 0.0 ?

_olex2_submission_special_instructions 'No special instructions were received'
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_1_sq
_database_code_depnum_ccdc_archive 'CCDC 2117814'
loop_
_audit_author_name
_audit_author_address
'Xi Xi Kang'
;Anhui University
China
;
_audit_update_record             
;
2021-10-26 deposited with the CCDC.	2022-01-03 downloaded from the CCDC.
;
_audit_creation_date             2021-10-25
_audit_creation_method           
;
Olex2 1.2
(compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         '0.5(C496.5 H651 Ag56 N6 P8 Pt2 S36)'
_chemical_formula_sum            'C248.25 H325.50 Ag28 N3 P4 Pt S18'
_chemical_formula_weight         7268.08
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag 0.1306 4.2820 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -4.5932 6.9264 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      trigonal
_space_group_IT_number           167
_space_group_name_H-M_alt        'R -3 c'
_space_group_name_Hall           '-R 3 2"c'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'
'y, x, -z+1/2'
'x-y, -y, -z+1/2'
'-x, -x+y, -z+1/2'
'x+2/3, y+1/3, z+1/3'
'-y+2/3, x-y+1/3, z+1/3'
'-x+y+2/3, -x+1/3, z+1/3'
'y+2/3, x+1/3, -z+5/6'
'x-y+2/3, -y+1/3, -z+5/6'
'-x+2/3, -x+y+1/3, -z+5/6'
'x+1/3, y+2/3, z+2/3'
'-y+1/3, x-y+2/3, z+2/3'
'-x+y+1/3, -x+2/3, z+2/3'
'y+1/3, x+2/3, -z+7/6'
'x-y+1/3, -y+2/3, -z+7/6'
'-x+1/3, -x+y+2/3, -z+7/6'
'-x, -y, -z'
'y, -x+y, -z'
'x-y, x, -z'
'-y, -x, z-1/2'
'-x+y, y, z-1/2'
'x, x-y, z-1/2'
'-x+2/3, -y+1/3, -z+1/3'
'y+2/3, -x+y+1/3, -z+1/3'
'x-y+2/3, x+1/3, -z+1/3'
'-y+2/3, -x+1/3, z-1/6'
'-x+y+2/3, y+1/3, z-1/6'
'x+2/3, x-y+1/3, z-1/6'
'-x+1/3, -y+2/3, -z+2/3'
'y+1/3, -x+y+2/3, -z+2/3'
'x-y+1/3, x+2/3, -z+2/3'
'-y+1/3, -x+2/3, z+1/6'
'-x+y+1/3, y+2/3, z+1/6'
'x+1/3, x-y+2/3, z+1/6'

_cell_length_a                   29.410(8)
_cell_length_b                   29.410(8)
_cell_length_c                   141.76(4)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_volume                     106187(63)
_cell_formula_units_Z            11.99988
_cell_measurement_reflns_used    15971
_cell_measurement_temperature    120(2)
_cell_measurement_theta_max      67.91
_cell_measurement_theta_min      5.74
_shelx_estimated_absorpt_T_max   ?
_shelx_estimated_absorpt_T_min   ?
_exptl_absorpt_coefficient_mu    14.251
_exptl_absorpt_correction_T_max  ?
_exptl_absorpt_correction_T_min  ?
_exptl_absorpt_correction_type   ?
_exptl_absorpt_process_details   ?
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    1.364
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             42936
_exptl_crystal_size_max          ?
_exptl_crystal_size_mid          ?
_exptl_crystal_size_min          ?
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0646
_diffrn_reflns_av_unetI/netI     0.0829
_diffrn_reflns_Laue_measured_fraction_full 0.983
_diffrn_reflns_Laue_measured_fraction_max 0.983
_diffrn_reflns_limit_h_max       33
_diffrn_reflns_limit_h_min       -28
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -33
_diffrn_reflns_limit_l_max       162
_diffrn_reflns_limit_l_min       -151
_diffrn_reflns_number            64119
_diffrn_reflns_point_group_measured_fraction_full 0.983
_diffrn_reflns_point_group_measured_fraction_max 0.983
_diffrn_reflns_theta_full        62.496
_diffrn_reflns_theta_max         62.496
_diffrn_reflns_theta_min         5.737
_diffrn_ambient_temperature      120(2)
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.983
_diffrn_measured_fraction_theta_max 0.983
_diffrn_measurement_device_type  STOE
_diffrn_measurement_method       ?
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54186
_diffrn_source                   ?
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                10056
_reflns_number_total             18509
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       ?
_computing_data_collection       ?
_computing_data_reduction        ?
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    'SHELXT 2018/2 (Sheldrick, 2018)'
_refine_diff_density_max         2.207
_refine_diff_density_min         -3.396
_refine_diff_density_rms         0.170
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.922
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1105
_refine_ls_number_reflns         18509
_refine_ls_number_restraints     2161
_refine_ls_R_factor_all          0.1103
_refine_ls_R_factor_gt           0.0764
_refine_ls_restrained_S_all      0.893
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.1557P)²] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2112
_refine_ls_wR_factor_ref         0.2450
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups, All C(H,H) groups, All N(H) groups
2. Restrained distances
 C21-C0 = C19-C0 = C19-C02J = C02P-C02J = C02J-C02G = C55-C02P = C55-C21 =
 C02L-C0 = C02L-C02E = C02K-C02E = C55-C02K = C02G-C02E
 1.54 with sigma of 0.01
 C0-C02E
 2.54 with sigma of 0.01
 C0-C55
 2.54 with sigma of 0.01
 C0-C02J
 2.54 with sigma of 0.01
 C02L-C02K
 2.54 with sigma of 0.01
 C02L-C21
 2.54 with sigma of 0.01
 C02L-C19
 2.54 with sigma of 0.01
 C02E-C55
 2.54 with sigma of 0.01
 C02E-C02J
 2.54 with sigma of 0.01
 C02K-C02P
 2.54 with sigma of 0.01
 C02K-C21
 2.54 with sigma of 0.01
 C02K-C02G
 2.54 with sigma of 0.01
 C55-C02J
 2.54 with sigma of 0.01
 C02P-C19
 2.54 with sigma of 0.01
 C02P-C21
 2.54 with sigma of 0.01
 C02P-C02G
 2.54 with sigma of 0.01
 C19-C21
 2.54 with sigma of 0.01
 C19-C02G
 2.54 with sigma of 0.01
 C0-C02K
 2.93 with sigma of 0.01
 C0-C02P
 2.93 with sigma of 0.01
 C0-C02G
 2.93 with sigma of 0.01
 C02L-C55
 2.93 with sigma of 0.01
 C02L-C02J
 2.93 with sigma of 0.01
 C02E-C21
 2.93 with sigma of 0.01
 C02E-C19
 2.93 with sigma of 0.01
 C02E-C02P
 2.93 with sigma of 0.01
 C02K-C02J
 2.93 with sigma of 0.01
 C55-C02G
 2.93 with sigma of 0.01
 C55-C19
 2.93 with sigma of 0.01
 C02J-C21
 2.93 with sigma of 0.01
 C011-C00S = C023-C011 = C024-C023 = C023-C021 = C028-C01H = C028-C024 = C01H-
 C00S = C025-C00S = C021-C01L = C025-C01L = C01V-C01L = C028-C01V
 1.54 with sigma of 0.01
 C00S-C023
 2.54 with sigma of 0.01
 C00S-C01L
 2.54 with sigma of 0.01
 C00S-C028
 2.54 with sigma of 0.01
 C011-C024
 2.54 with sigma of 0.01
 C011-C021
 2.54 with sigma of 0.01
 C011-C01H
 2.54 with sigma of 0.01
 C011-C025
 2.54 with sigma of 0.01
 C023-C01L
 2.54 with sigma of 0.01
 C023-C028
 2.54 with sigma of 0.01
 C024-C01V
 2.54 with sigma of 0.01
 C024-C021
 2.54 with sigma of 0.01
 C028-C01L
 2.54 with sigma of 0.01
 C01V-C021
 2.54 with sigma of 0.01
 C01V-C025
 2.54 with sigma of 0.01
 C025-C01H
 2.54 with sigma of 0.01
 C00S-C024
 2.93 with sigma of 0.01
 C00S-C01V
 2.93 with sigma of 0.01
 C00S-C021
 2.93 with sigma of 0.01
 C011-C028
 2.93 with sigma of 0.01
 C011-C01L
 2.93 with sigma of 0.01
 C023-C025
 2.93 with sigma of 0.01
 C023-C01H
 2.93 with sigma of 0.01
 C023-C01V
 2.93 with sigma of 0.01
 C024-C01L
 2.93 with sigma of 0.01
 C028-C011
 2.93 with sigma of 0.01
 C028-C025
 2.93 with sigma of 0.01
 C028-C021
 2.93 with sigma of 0.01
 C01L-C01H
 2.93 with sigma of 0.01
 C76-C1BA = C76-C2BA = C76-C0BA = C3BA-C0BA = C4BA-C3BA = C3BA-C11 = C80-C11 =
 C80-C2BA = C80-C6BA = C7BA-C1BA = C7BA-C6BA = C7BA-C4BA
 1.54 with sigma of 0.01
 C76-C7BA
 2.54 with sigma of 0.01
 C76-C80
 2.54 with sigma of 0.01
 C76-C3BA
 2.54 with sigma of 0.01
 C0BA-C4BA
 2.54 with sigma of 0.01
 C0BA-C2BA
 2.54 with sigma of 0.01
 C0BA-C11
 2.54 with sigma of 0.01
 C3BA-C7BA
 2.54 with sigma of 0.01
 C3BA-C80
 2.54 with sigma of 0.01
 C4BA-C6BA
 2.54 with sigma of 0.01
 C4BA-C11
 2.54 with sigma of 0.01
 C4BA-C1BA
 2.54 with sigma of 0.01
 C7BA-C80
 2.54 with sigma of 0.01
 C6BA-C11
 2.54 with sigma of 0.01
 C6BA-C2BA
 2.54 with sigma of 0.01
 C2BA-C1BA
 2.54 with sigma of 0.01
 C76-C4BA
 2.93 with sigma of 0.01
 C76-C6BA
 2.93 with sigma of 0.01
 C76-C11
 2.93 with sigma of 0.01
 C0BA-C7BA
 2.93 with sigma of 0.01
 C0BA-C80
 2.93 with sigma of 0.01
 C3BA-C6BA
 2.93 with sigma of 0.01
 C3BA-C2BA
 2.93 with sigma of 0.01
 C3BA-C1BA
 2.93 with sigma of 0.01
 C4BA-C80
 2.93 with sigma of 0.01
 C7BA-C11
 2.93 with sigma of 0.01
 C7BA-C2BA
 2.93 with sigma of 0.01
 C80-C1BA
 2.93 with sigma of 0.01
 C2BA-C7BA
 2.93 with sigma of 0.01
3. Uiso/Uaniso restraints and constraints
C00M \\sim C00N \\sim C00O \\sim C00R \\sim C00S \\sim C00T \\sim C00U \\sim
C00V \\sim C00W \\sim C00Y \\sim C00Z \\sim C010 \\sim C011 \\sim C012 \\sim
C013 \\sim C014 \\sim C015 \\sim C018 \\sim C019 \\sim C0 \\sim C01B \\sim C01C
\\sim C01G \\sim C01H \\sim C01L \\sim C01M \\sim C01N \\sim C01O \\sim C01P
\\sim C43 \\sim C132 \\sim C01Y \\sim C01E \\sim C01Q \\sim C01R \\sim C01S
\\sim C01T \\sim C01U \\sim C01V \\sim C01X \\sim C021 \\sim C022 \\sim C023
\\sim C024 \\sim C025 \\sim C028 \\sim C02E \\sim C02G \\sim C02J \\sim C02K
\\sim C02L \\sim C02P \\sim C19 \\sim C21 \\sim C55 \\sim C16 \\sim C4 \\sim
C42 \\sim C116 \\sim C71 \\sim C13 \\sim C20 \\sim C8 \\sim C29 \\sim C46 \\sim
C0AA \\sim C49 \\sim C2 \\sim C1 \\sim C17 \\sim C5 \\sim C79 \\sim C18 \\sim
C12 \\sim C26 \\sim C102 \\sim N107 \\sim C90 \\sim C129 \\sim C82 \\sim C87
\\sim C38 \\sim C25 \\sim C40 \\sim C30: within 2A with sigma of 0.01 and sigma
for terminal atoms of 0.02
C02B \\sim N \\sim C10 \\sim C141 \\sim N6 \\sim C113 \\sim C3: within 2A with
sigma of 0.01 and sigma for terminal atoms of 0.02
C13 \\sim P1 \\sim C16 \\sim C0AA: within 3.8A with sigma of 0.01 and sigma for
terminal atoms of 0.02
P00H \\sim C01P \\sim C02B \\sim C43 \\sim C132 \\sim C01Y \\sim C01E: within
3.8A with sigma of 0.01 and sigma for terminal atoms of 0.02
C2BA \\sim C0BA \\sim C1BA \\sim C6BA \\sim C11 \\sim C3BA \\sim C4BA \\sim
C7BA \\sim C80 \\sim C76 \\sim S0AA: within 3.8A with sigma of 0.01 and sigma
for terminal atoms of 0.02
C1AA \\sim C3AA \\sim C2AA \\sim C4AA \\sim C6 \\sim C5AA \\sim C6AA \\sim C8AA
\\sim C7AA \\sim C9AA \\sim S1: within 3.8A with sigma of 0.01 and sigma for
terminal atoms of 0.02
Uanis(C00M) \\sim Ueq, Uanis(C00N) \\sim Ueq, Uanis(C00O) \\sim Ueq,
Uanis(C00R) \\sim Ueq, Uanis(C00S) \\sim Ueq, Uanis(C00T) \\sim Ueq,
Uanis(C00U) \\sim Ueq, Uanis(C00V) \\sim Ueq, Uanis(C00W) \\sim Ueq,
Uanis(C00Y) \\sim Ueq, Uanis(C00Z) \\sim Ueq, Uanis(C010) \\sim Ueq,
Uanis(C011) \\sim Ueq, Uanis(C012) \\sim Ueq, Uanis(C013) \\sim Ueq,
Uanis(C014) \\sim Ueq, Uanis(C015) \\sim Ueq, Uanis(C018) \\sim Ueq,
Uanis(C019) \\sim Ueq, Uanis(C0) \\sim Ueq, Uanis(C01B) \\sim Ueq, Uanis(C01C)
\\sim Ueq, Uanis(C01G) \\sim Ueq, Uanis(C01H) \\sim Ueq, Uanis(C01L) \\sim Ueq,
Uanis(C01M) \\sim Ueq, Uanis(C01N) \\sim Ueq, Uanis(C01O) \\sim Ueq,
Uanis(C01P) \\sim Ueq, Uanis(C43) \\sim Ueq, Uanis(C132) \\sim Ueq, Uanis(C01Y)
\\sim Ueq, Uanis(C01E) \\sim Ueq, Uanis(C01Q) \\sim Ueq, Uanis(C01R) \\sim Ueq,
Uanis(C01S) \\sim Ueq, Uanis(C01T) \\sim Ueq, Uanis(C01U) \\sim Ueq,
Uanis(C01V) \\sim Ueq, Uanis(C01X) \\sim Ueq, Uanis(C021) \\sim Ueq,
Uanis(C022) \\sim Ueq, Uanis(C023) \\sim Ueq, Uanis(C024) \\sim Ueq,
Uanis(C025) \\sim Ueq, Uanis(C028) \\sim Ueq, Uanis(C02E) \\sim Ueq,
Uanis(C02G) \\sim Ueq, Uanis(C02J) \\sim Ueq, Uanis(C02K) \\sim Ueq,
Uanis(C02L) \\sim Ueq, Uanis(C02P) \\sim Ueq, Uanis(C19) \\sim Ueq, Uanis(C21)
\\sim Ueq, Uanis(C55) \\sim Ueq, Uanis(C16) \\sim Ueq, Uanis(C4) \\sim Ueq,
Uanis(C42) \\sim Ueq, Uanis(C116) \\sim Ueq, Uanis(C71) \\sim Ueq, Uanis(C13)
\\sim Ueq, Uanis(C20) \\sim Ueq, Uanis(C8) \\sim Ueq, Uanis(C29) \\sim Ueq,
Uanis(C46) \\sim Ueq, Uanis(C0AA) \\sim Ueq, Uanis(C49) \\sim Ueq, Uanis(C2)
\\sim Ueq, Uanis(C1) \\sim Ueq, Uanis(C17) \\sim Ueq, Uanis(C5) \\sim Ueq,
Uanis(C79) \\sim Ueq, Uanis(C18) \\sim Ueq, Uanis(C12) \\sim Ueq, Uanis(C26)
\\sim Ueq, Uanis(C102) \\sim Ueq, Uanis(N107) \\sim Ueq, Uanis(C90) \\sim Ueq,
Uanis(C129) \\sim Ueq, Uanis(C82) \\sim Ueq, Uanis(C87) \\sim Ueq, Uanis(C38)
\\sim Ueq, Uanis(C25) \\sim Ueq, Uanis(C40) \\sim Ueq, Uanis(C30) \\sim Ueq:
with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(C02B) \\sim Ueq, Uanis(N) \\sim Ueq, Uanis(C10) \\sim Ueq, Uanis(C141)
\\sim Ueq, Uanis(N6) \\sim Ueq, Uanis(C113) \\sim Ueq, Uanis(C3) \\sim Ueq:
with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(P1) \\sim Ueq, Uanis(C16) \\sim Ueq, Uanis(C13) \\sim Ueq, Uanis(C0AA)
\\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(P00H) \\sim Ueq, Uanis(C01P) \\sim Ueq, Uanis(C02B) \\sim Ueq, Uanis(C43)
\\sim Ueq, Uanis(C132) \\sim Ueq, Uanis(C01Y) \\sim Ueq, Uanis(C01E) \\sim Ueq:
with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(C2BA) \\sim Ueq, Uanis(C0BA) \\sim Ueq, Uanis(C1BA) \\sim Ueq,
Uanis(C6BA) \\sim Ueq, Uanis(C11) \\sim Ueq, Uanis(C3BA) \\sim Ueq, Uanis(C4BA)
\\sim Ueq, Uanis(C7BA) \\sim Ueq, Uanis(C80) \\sim Ueq, Uanis(C76) \\sim Ueq,
Uanis(S0AA) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(C1AA) \\sim Ueq, Uanis(C3AA) \\sim Ueq, Uanis(C2AA) \\sim Ueq,
Uanis(C4AA) \\sim Ueq, Uanis(C6) \\sim Ueq, Uanis(C5AA) \\sim Ueq, Uanis(C6AA)
\\sim Ueq, Uanis(C8AA) \\sim Ueq, Uanis(C7AA) \\sim Ueq, Uanis(C9AA) \\sim Ueq,
Uanis(S1) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
4. Others
 Fixed Sof: Ag(0.4) P0(0.5) C0(0.6) C02E(0.6) H02J(0.6) C02G(0.6) H02K(0.6)
 H02L(0.6) C02J(0.6) H02M(0.6) C02K(0.6) H02N(0.6) H02O(0.6) C02L(0.6)
 H02P(0.6) H02Q(0.6) C02P(0.6) H02R(0.6) H02S(0.6) C19(0.6) H19A(0.6) H19B(0.6)
 C21(0.6) H21A(0.6) H21B(0.6) C55(0.6) H55(0.6) C16(0.5) C4(0.5) H4(0.5)
 C42(0.5) H42(0.5) C116(0.5) H116(0.5) C71(0.5) H71(0.5) N(0.5) H(0.5) C13(0.5)
 C20(0.5) H20(0.5) C8(0.5) H8(0.5) C29(0.5) H29(0.5) C46(0.5) H46(0.5) C10(0.5)
 H10(0.5) C0AA(0.5) C49(0.5) H49(0.5) C2(0.5) H2(0.5) C1(0.5) H1(0.5) C17(0.5)
 H17(0.5) C141(0.5) H141(0.5) C5(0.5) N6(0.5) HA(0.5) C79(0.5) H79(0.5)
 C18(0.5) C12(0.25) C26(0.5) C102(0.5) N107(0.5) H107(0.5) C90(0.5) H90(0.5)
 C129(0.5) H129(0.5) C82(0.5) H82(0.5) C113(0.5) H113(0.5) C87(0.5) C3(0.5)
 H3(0.5) C38(0.5) H38(0.5) C25(0.5) H25(0.5) C40(0.5) H40(0.5) C30(0.5)
 H30(0.5) P1(0.5) S1A(0.6) S0AA(0.4) C2BA(0.4) H2BA(0.4) H2BB(0.4) C0BA(0.4)
 H0BA(0.4) H0BB(0.4) C1BA(0.4) H1BA(0.4) H1BB(0.4) C6BA(0.4) H6BA(0.4)
 H6BB(0.4) C11(0.4) H11A(0.4) H11B(0.4) C3BA(0.4) H3BA(0.4) C4BA(0.4) H4BA(0.4)
 H4BB(0.4) C7BA(0.4) H7BA(0.4) C80(0.4) H80(0.4) C76(0.4) Ag1(0.6)
5.a Ternary CH refined with riding coordinates:
 C00O(H00O), C014(H014), C015(H015), C01B(H01M), C01C(H01N), C01L(H01S),
 C01Q(H0AA), C01R(H1AA), C01S(H2AA), C01X(H6AA), C023(H023), C028(H028),
 C02E(H02J), C02J(H02M), C55(H55), C3BA(H3BA), C7BA(H7BA), C80(H80), C6(H6),
 C6AA(H6AB), C7AA(H7AA)
5.b Secondary CH2 refined with riding coordinates:
 C00N(H00A,H00B), C00T(H00C,H00D), C00V(H00E,H00F), C00W(H00G,H00H), C00Y(H00I,
 H00J), C00Z(H00K,H00L), C010(H01A,H01B), C011(H01C,H01D), C012(H01E,H01F),
 C013(H01G,H01H), C018(H01I,H01J), C019(H01K,H01L), C01G(H01O,H01P), C01H(H01Q,
 H01R), C01M(H01T,H01U), C01N(H01V,H01W), C01O(H01X,H01Y), C01T(H3AA,HB),
 C01U(H4AA,HC), C01V(H5AA,HD), C021(H02A,H02C), C022(H02D,H02E), C024(H02F,
 H02G), C025(H02H,H02I), C02G(H02K,H02L), C02K(H02N,H02O), C02L(H02P,H02Q),
 C02P(H02R,H02S), C19(H19A,H19B), C21(H21A,H21B), C2BA(H2BA,H2BB), C0BA(H0BA,
 H0BB), C1BA(H1BA,H1BB), C6BA(H6BA,H6BB), C11(H11A,H11B), C4BA(H4BA,H4BB),
 C1AA(H1AB,H1AC), C3AA(H3AB,H3AC), C4AA(H4AB,H4AC), C5AA(H5AB,H5AC), C8AA(H8AA,
 H8AB), C9AA(H9AA,H9AB)
5.c Aromatic/amide H refined with riding coordinates:
 C02B(H02B), C43(H43), C132(H132), C01Y(H01Z), C01E(H01), C4(H4), C42(H42),
 C116(H116), C71(H71), N(H), C20(H20), C8(H8), C29(H29), C46(H46), C10(H10),
 C49(H49), C2(H2), C1(H1), C17(H17), C141(H141), N6(HA), C79(H79), N107(H107),
 C90(H90), C129(H129), C82(H82), C113(H113), C3(H3), C38(H38), C25(H25),
 C40(H40), C30(H30)
5.d Fitted hexagon refined as free rotating group:
 C01P(C02B,C43,C132,C01Y,C01E), C16(C4,C42,C116,C71,N), C13(C20,C8,C29,C46,
 C10), C0AA(C49,C2,C1,C17,C141), C5(N6,C79,C18,C12,C26), C102(N107,C90,C129,C82,
 C113), C87(C3,C38,C25,C40,C30)
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt01 Pt 0.666667 0.333333 0.46576(2) 0.0580(2) Uani 1 3 d S T P A .
Ag02 Ag 0.61377(4) 0.27576(4) 0.48190(2) 0.0649(3) Uani 1 1 d . . . . .
Ag03 Ag 0.59827(4) 0.37259(4) 0.46650(2) 0.0668(3) Uani 1 1 d . . . . .
Ag04 Ag 0.71702(4) 0.39119(4) 0.44955(2) 0.0681(3) Uani 1 1 d . . . . .
Ag05 Ag 0.55742(4) 0.26267(4) 0.46562(2) 0.0699(3) Uani 1 1 d . . . . .
Ag06 Ag 0.55833(4) 0.31995(4) 0.49365(2) 0.0686(3) Uani 1 1 d . . . . .
Ag07 Ag 0.666667 0.333333 0.51044(2) 0.0712(5) Uani 1 3 d S T P . .
Ag08 Ag 0.49226(5) 0.30705(5) 0.47621(2) 0.0740(3) Uani 1 1 d . . . . .
Ag09 Ag 0.59095(5) 0.41580(5) 0.44746(2) 0.0836(3) Uani 1 1 d . . . . .
Ag0A Ag 0.45075(5) 0.30124(6) 0.45146(2) 0.0927(4) Uani 1 1 d . . . . .
Ag Ag 0.7165(4) 0.4909(3) 0.44476(3) 0.0774(14) Uani 0.4 1 d . . . A 2
S00C S 0.59424(13) 0.26636(13) 0.49906(2) 0.0622(8) Uani 1 1 d . . . . .
S00D S 0.50530(15) 0.35846(15) 0.49042(2) 0.0674(8) Uani 1 1 d . . . . .
S00E S 0.78489(16) 0.46840(17) 0.44052(2) 0.0781(10) Uani 1 1 d . . . . .
S00G S 0.46397(14) 0.23937(15) 0.46370(2) 0.0693(8) Uani 1 1 d . . . . .
P00H P 0.666667 0.333333 0.52740(4) 0.0798(16) Uani 1 3 d S TU P . .
P0 P 0.3670(4) 0.2874(6) 0.44622(9) 0.065(2) Uani 0.5 1 d . . . B 2
C00M C 0.5393(6) 0.2047(6) 0.50335(9) 0.066(3) Uani 1 1 d . U . . .
C00N C 0.5041(6) 0.2157(6) 0.50953(10) 0.072(3) Uani 1 1 d . U . . .
H00A H 0.489005 0.232999 0.505922 0.086 Uiso 1 1 calc R . . . .
H00B H 0.523874 0.238316 0.514752 0.086 Uiso 1 1 calc R . . . .
C00O C 0.5168(6) 0.1220(6) 0.51248(9) 0.069(3) Uani 1 1 d . U . . .
H00O H 0.531500 0.103611 0.515992 0.083 Uiso 1 1 calc R . . . .
C00R C 0.4497(6) 0.3282(6) 0.49811(10) 0.075(3) Uani 1 1 d . U . . .
C00S C 0.7844(4) 0.4691(4) 0.42758(5) 0.084(3) Uani 1 1 d D U . . .
C00T C 0.4787(6) 0.1327(6) 0.51896(10) 0.073(3) Uani 1 1 d . U . . .
H00C H 0.449011 0.099714 0.521022 0.088 Uiso 1 1 calc R . . . .
H00D H 0.497316 0.152828 0.524487 0.088 Uiso 1 1 calc R . . . .
C00U C 0.4101(7) 0.1764(7) 0.46712(11) 0.082(3) Uani 1 1 d . U . . .
C00V C 0.5599(6) 0.1750(6) 0.50895(10) 0.074(3) Uani 1 1 d . U . . .
H00E H 0.579591 0.196183 0.514314 0.088 Uiso 1 1 calc R . . . .
H00F H 0.583854 0.169694 0.505023 0.088 Uiso 1 1 calc R . . . .
C00W C 0.5061(6) 0.1697(6) 0.49478(9) 0.071(3) Uani 1 1 d . U . . .
H00G H 0.492242 0.188076 0.491146 0.085 Uiso 1 1 calc R . . . .
H00H H 0.528065 0.162469 0.490669 0.085 Uiso 1 1 calc R . . . .
C00Y C 0.3782(7) 0.1825(7) 0.47517(12) 0.085(3) Uani 1 1 d . U . . .
H00I H 0.367425 0.207456 0.473300 0.102 Uiso 1 1 calc R . . . .
H00J H 0.400152 0.196239 0.480734 0.102 Uiso 1 1 calc R . . . .
C00Z C 0.4243(7) 0.1349(7) 0.47054(12) 0.088(3) Uani 1 1 d . U . . .
H00K H 0.445099 0.130729 0.465677 0.105 Uiso 1 1 calc R . . . .
H00L H 0.446202 0.148560 0.476104 0.105 Uiso 1 1 calc R . . . .
C010 C 0.3484(7) 0.0913(7) 0.48055(12) 0.091(4) Uani 1 1 d . U . . .
H01A H 0.371275 0.106399 0.485964 0.109 Uiso 1 1 calc R . . . .
H01B H 0.318804 0.058006 0.482522 0.109 Uiso 1 1 calc R . . . .
C011 C 0.7336(4) 0.4210(4) 0.42395(7) 0.093(4) Uani 1 1 d D U . . .
H01C H 0.703264 0.422358 0.426254 0.111 Uiso 1 1 calc R . . . .
H01D H 0.731530 0.388967 0.426267 0.111 Uiso 1 1 calc R . . . .
C012 C 0.4164(6) 0.3562(7) 0.49644(11) 0.081(3) Uani 1 1 d . U . . .
H01E H 0.437985 0.393539 0.497629 0.097 Uiso 1 1 calc R . . . .
H01F H 0.404528 0.351417 0.489940 0.097 Uiso 1 1 calc R . . . .
C013 C 0.4847(6) 0.0902(6) 0.50431(10) 0.078(3) Uani 1 1 d . U . . .
H01G H 0.456294 0.056957 0.506592 0.093 Uiso 1 1 calc R . . . .
H01H H 0.506438 0.082719 0.500170 0.093 Uiso 1 1 calc R . . . .
C014 C 0.4614(6) 0.1188(6) 0.49862(11) 0.078(3) Uani 1 1 d . U . . .
H014 H 0.440811 0.096550 0.493342 0.094 Uiso 1 1 calc R . . . .
C015 C 0.4179(7) 0.3129(7) 0.51521(12) 0.092(3) Uani 1 1 d . U . . .
H015 H 0.430351 0.318681 0.521754 0.110 Uiso 1 1 calc R . . . .
C018 C 0.4646(7) 0.3341(7) 0.50855(10) 0.083(3) Uani 1 1 d . U . . .
H01I H 0.483856 0.315851 0.509756 0.100 Uiso 1 1 calc R . . . .
H01J H 0.487851 0.370979 0.509911 0.100 Uiso 1 1 calc R . . . .
C019 C 0.4254(6) 0.1280(6) 0.50510(10) 0.082(3) Uani 1 1 d . U . . .
H01K H 0.397272 0.094896 0.507501 0.098 Uiso 1 1 calc R . . . .
H01L H 0.410056 0.145857 0.501755 0.098 Uiso 1 1 calc R . . . .
C0 C 0.6416(7) 0.5320(6) 0.43508(9) 0.090(5) Uani 0.6 1 d D U . A 1
C01B C 0.3223(8) 0.0980(7) 0.46134(12) 0.098(4) Uani 1 1 d . U . . .
H01M H 0.299290 0.083638 0.455836 0.117 Uiso 1 1 calc R . . . .
C01C C 0.3682(7) 0.3320(8) 0.50322(12) 0.095(3) Uani 1 1 d . U . . .
H01N H 0.347938 0.349602 0.502061 0.113 Uiso 1 1 calc R . . . .
C01G C 0.3835(8) 0.2530(8) 0.51332(11) 0.099(4) Uani 1 1 d . U . . .
H01O H 0.353764 0.237736 0.517599 0.118 Uiso 1 1 calc R . . . .
H01P H 0.403949 0.235842 0.514360 0.118 Uiso 1 1 calc R . . . .
C01H C 0.7869(5) 0.5197(4) 0.42395(7) 0.095(4) Uani 1 1 d D U . . .
H01Q H 0.757036 0.521730 0.426301 0.114 Uiso 1 1 calc R . . . .
H01R H 0.818663 0.550062 0.426247 0.114 Uiso 1 1 calc R . . . .
C01L C 0.8326(4) 0.4672(5) 0.41307(7) 0.105(4) Uani 1 1 d D U . . .
H01S H 0.863311 0.465954 0.410717 0.126 Uiso 1 1 calc R . . . .
C01M C 0.4124(7) 0.2702(7) 0.49606(11) 0.085(3) Uani 1 1 d . U . . .
H01T H 0.431409 0.251342 0.496641 0.103 Uiso 1 1 calc R . . . .
H01U H 0.400069 0.266544 0.489606 0.103 Uiso 1 1 calc R . . . .
C01N C 0.3408(8) 0.0601(7) 0.46466(12) 0.096(4) Uani 1 1 d . U . . .
H01V H 0.310404 0.027014 0.466439 0.115 Uiso 1 1 calc R . . . .
H01W H 0.357993 0.053362 0.459454 0.115 Uiso 1 1 calc R . . . .
C01O C 0.3731(7) 0.1536(7) 0.45882(11) 0.092(4) Uani 1 1 d . U . . .
H01X H 0.391644 0.148941 0.453578 0.110 Uiso 1 1 calc R . . . .
H01Y H 0.361881 0.177993 0.456858 0.110 Uiso 1 1 calc R . . . .
C01P C 0.7304(4) 0.3746(5) 0.53247(9) 0.112(3) Uani 1 1 d . U . . .
C02B C 0.7487(5) 0.3577(4) 0.53996(9) 0.122(3) Uani 1 1 d G U . . .
H02B H 0.727485 0.324542 0.542546 0.146 Uiso 1 1 calc R . . . .
C43 C 0.7987(6) 0.3902(6) 0.54357(8) 0.126(4) Uani 1 1 d G U . . .
H43 H 0.810896 0.378849 0.548581 0.151 Uiso 1 1 calc R . . . .
C132 C 0.8304(4) 0.4397(6) 0.53970(10) 0.125(4) Uani 1 1 d G U . . .
H132 H 0.863805 0.461455 0.542118 0.150 Uiso 1 1 calc R . . . .
C01Y C 0.8121(5) 0.4566(4) 0.53221(10) 0.124(4) Uani 1 1 d G U . . .
H01Z H 0.833304 0.489756 0.529622 0.149 Uiso 1 1 calc R . . . .
C01E C 0.7621(6) 0.4241(6) 0.52860(8) 0.113(3) Uani 1 1 d G U . . .
H01 H 0.749894 0.435449 0.523587 0.136 Uiso 1 1 calc R . . . .
C01Q C 0.3781(7) 0.0809(7) 0.47291(12) 0.095(3) Uani 1 1 d . U . . .
H0AA H 0.389525 0.056314 0.474963 0.114 Uiso 1 1 calc R . . . .
C01R C 0.4606(6) 0.1623(6) 0.51320(11) 0.078(3) Uani 1 1 d . U . . .
H1AA H 0.438217 0.169631 0.517310 0.094 Uiso 1 1 calc R . . . .
C01S C 0.3278(7) 0.1280(7) 0.47765(13) 0.095(3) Uani 1 1 d . U . . .
H2AA H 0.307516 0.131888 0.482757 0.114 Uiso 1 1 calc R . . . .
C01T C 0.3340(8) 0.2754(8) 0.50122(13) 0.099(4) Uani 1 1 d . U . . .
H3AA H 0.321972 0.270922 0.494728 0.119 Uiso 1 1 calc R . . . .
HB H 0.303386 0.261264 0.505286 0.119 Uiso 1 1 calc R . . . .
C01U C 0.2948(7) 0.1048(8) 0.46907(12) 0.094(4) Uani 1 1 d . U . . .
H4AA H 0.265018 0.070904 0.470706 0.113 Uiso 1 1 calc R . . . .
HC H 0.281305 0.127293 0.467056 0.113 Uiso 1 1 calc R . . . .
C01V C 0.8351(4) 0.5182(4) 0.40962(8) 0.113(4) Uani 1 1 d D U . . .
H5AA H 0.866711 0.548451 0.411976 0.135 Uiso 1 1 calc R . . . .
HD H 0.836028 0.519447 0.402783 0.135 Uiso 1 1 calc R . . . .
C01X C 0.3638(8) 0.2448(8) 0.50284(12) 0.095(3) Uani 1 1 d . U . . .
H6AA H 0.341129 0.207433 0.501433 0.114 Uiso 1 1 calc R . . . .
C021 C 0.7824(5) 0.4190(4) 0.40954(8) 0.111(4) Uani 1 1 d D U . . .
H02A H 0.781057 0.387328 0.411838 0.133 Uiso 1 1 calc R . . . .
H02C H 0.782478 0.418218 0.402695 0.133 Uiso 1 1 calc R . . . .
C022 C 0.3859(8) 0.3413(8) 0.51343(12) 0.103(4) Uani 1 1 d . U . . .
H02D H 0.355708 0.327294 0.517585 0.124 Uiso 1 1 calc R . . . .
H02E H 0.407623 0.378574 0.514634 0.124 Uiso 1 1 calc R . . . .
C023 C 0.7339(4) 0.4212(4) 0.41305(7) 0.103(4) Uani 1 1 d D U . . .
H023 H 0.701904 0.390676 0.410684 0.123 Uiso 1 1 calc R . . . .
C024 C 0.7362(4) 0.4723(5) 0.40960(8) 0.110(4) Uani 1 1 d D U . . .
H02F H 0.735412 0.472748 0.402759 0.132 Uiso 1 1 calc R . . . .
H02G H 0.705944 0.473735 0.411939 0.132 Uiso 1 1 calc R . . . .
C025 C 0.8323(4) 0.4660(5) 0.42390(8) 0.102(4) Uani 1 1 d D U . . .
H02H H 0.864467 0.495472 0.426306 0.122 Uiso 1 1 calc R . . . .
H02I H 0.830461 0.433873 0.426087 0.122 Uiso 1 1 calc R . . . .
C028 C 0.7867(5) 0.5199(4) 0.41318(7) 0.111(4) Uani 1 1 d D U . . .
H028 H 0.788162 0.552111 0.410937 0.133 Uiso 1 1 calc R . . . .
C02E C 0.6831(6) 0.6135(5) 0.42507(12) 0.110(5) Uani 0.6 1 d D U . A 1
H02J H 0.712329 0.649747 0.424618 0.132 Uiso 0.6 1 calc R . . A 1
C02G C 0.6309(8) 0.6136(6) 0.42504(13) 0.113(5) Uani 0.6 1 d D U . A 1
H02K H 0.628152 0.630168 0.419317 0.135 Uiso 0.6 1 calc R . . A 1
H02L H 0.629672 0.633513 0.430387 0.135 Uiso 0.6 1 calc R . . A 1
C02J C 0.5848(6) 0.5567(7) 0.42558(12) 0.104(5) Uani 0.6 1 d D U . A 1
H02M H 0.551594 0.556878 0.425453 0.124 Uiso 0.6 1 calc R . . A 1
C02K C 0.6851(6) 0.5816(7) 0.41660(10) 0.105(5) Uani 0.6 1 d D U . A 1
H02N H 0.682239 0.597159 0.410750 0.126 Uiso 0.6 1 calc R . . A 1
H02O H 0.718259 0.581995 0.416562 0.126 Uiso 0.6 1 calc R . . A 1
C02L C 0.6874(6) 0.5892(7) 0.43436(10) 0.096(5) Uani 0.6 1 d D U . A 1
H02P H 0.686162 0.609473 0.439643 0.116 Uiso 0.6 1 calc R . . A 1
H02Q H 0.720634 0.589691 0.434585 0.116 Uiso 0.6 1 calc R . . A 1
C02P C 0.5867(6) 0.5244(7) 0.41720(11) 0.106(5) Uani 0.6 1 d D U . A 1
H02R H 0.583421 0.539368 0.411325 0.127 Uiso 0.6 1 calc R . . A 1
H02S H 0.557724 0.488585 0.417629 0.127 Uiso 0.6 1 calc R . . A 1
C19 C 0.5889(6) 0.5315(7) 0.43493(10) 0.099(5) Uani 0.6 1 d D U . A 1
H19A H 0.586944 0.551134 0.440270 0.119 Uiso 0.6 1 calc R . . A 1
H19B H 0.559947 0.495694 0.435388 0.119 Uiso 0.6 1 calc R . . A 1
C21 C 0.6437(7) 0.4998(6) 0.42668(12) 0.099(5) Uani 0.6 1 d D U . A 1
H21A H 0.676446 0.499346 0.426788 0.118 Uiso 0.6 1 calc R . . A 1
H21B H 0.614996 0.463833 0.427122 0.118 Uiso 0.6 1 calc R . . A 1
C55 C 0.6393(7) 0.5247(6) 0.41739(9) 0.103(5) Uani 0.6 1 d D U . A 1
H55 H 0.640587 0.504195 0.412045 0.124 Uiso 0.6 1 calc R . . A 1
C16 C 0.3606(16) 0.3260(16) 0.4393(2) 0.169(5) Uani 0.5 1 d . U . B 1
C4 C 0.4079(13) 0.3697(18) 0.4367(3) 0.179(6) Uani 0.5 1 d G U . B 1
H4 H 0.436929 0.381959 0.440632 0.215 Uiso 0.5 1 calc R . . B 1
C42 C 0.4117(15) 0.3949(14) 0.4282(3) 0.187(7) Uani 0.5 1 d G U . B 1
H42 H 0.443291 0.424116 0.426449 0.224 Uiso 0.5 1 calc R . . B 1
C116 C 0.368(2) 0.3765(16) 0.4223(2) 0.206(9) Uani 0.5 1 d G U . B 1
H116 H 0.370755 0.393445 0.416618 0.247 Uiso 0.5 1 calc R . . B 1
C71 C 0.3209(15) 0.3329(16) 0.4249(2) 0.211(10) Uani 0.5 1 d G U . B 1
H71 H 0.291857 0.320615 0.420970 0.254 Uiso 0.5 1 calc R . . B 1
N N 0.3171(12) 0.3077(11) 0.4334(2) 0.122(11) Uani 0.5 1 d G U . B 1
H H 0.287875 0.280656 0.435021 0.147 Uiso 0.5 1 calc R . . B 1
C13 C 0.3387(16) 0.3019(18) 0.4558(2) 0.165(6) Uani 0.5 1 d . U . B 1
C20 C 0.3337(16) 0.3464(18) 0.4556(3) 0.179(6) Uani 0.5 1 d G U . B 1
H20 H 0.337106 0.363837 0.449928 0.214 Uiso 0.5 1 calc R . . B 1
C8 C 0.3235(17) 0.3649(15) 0.4639(4) 0.193(8) Uani 0.5 1 d G U . B 1
H8 H 0.320094 0.394706 0.463776 0.232 Uiso 0.5 1 calc R . . B 1
C29 C 0.3184(17) 0.339(2) 0.4723(3) 0.196(8) Uani 0.5 1 d G U . B 1
H29 H 0.311543 0.351273 0.477899 0.235 Uiso 0.5 1 calc R . . B 1
C46 C 0.3234(16) 0.2944(18) 0.4725(2) 0.190(8) Uani 0.5 1 d G U . B 1
H46 H 0.320005 0.276972 0.478175 0.228 Uiso 0.5 1 calc R . . B 1
C10 C 0.3336(16) 0.2759(14) 0.4642(3) 0.129(9) Uani 0.5 1 d G U . B 1
H10 H 0.337017 0.246102 0.464328 0.155 Uiso 0.5 1 calc R . . B 1
C0AA C 0.3195(16) 0.2188(12) 0.4448(3) 0.163(5) Uani 0.5 1 d . U . B 1
C49 C 0.2703(18) 0.1915(19) 0.4490(2) 0.171(6) Uani 0.5 1 d G U . B 1
H49 H 0.259581 0.208536 0.453234 0.205 Uiso 0.5 1 calc R . . B 1
C2 C 0.2370(13) 0.1388(18) 0.4469(3) 0.185(7) Uani 0.5 1 d G U . B 1
H2 H 0.204118 0.120563 0.449721 0.222 Uiso 0.5 1 calc R . . B 1
C1 C 0.2530(16) 0.1134(12) 0.4406(3) 0.184(8) Uani 0.5 1 d G U . B 1
H1 H 0.230786 0.078100 0.439191 0.221 Uiso 0.5 1 calc R . . B 1
C17 C 0.3022(17) 0.1406(15) 0.4364(2) 0.170(8) Uani 0.5 1 d G U . B 1
H17 H 0.312917 0.123609 0.432174 0.204 Uiso 0.5 1 calc R . . B 1
C141 C 0.3355(12) 0.1933(14) 0.4385(2) 0.096(8) Uani 0.5 1 d G U . B 1
H141 H 0.368381 0.211582 0.435687 0.115 Uiso 0.5 1 calc R . . B 1
C5 C 0.3473(14) 0.2462(13) 0.4346(2) 0.148(7) Uani 0.5 1 d . U . B 2
N6 C 0.3437(13) 0.1975(14) 0.4357(2) 0.098(8) Uani 0.5 1 d G U . B 2
HA H 0.351093 0.188074 0.441569 0.118 Uiso 0.5 1 calc R . . B 2
C79 C 0.3292(15) 0.1630(11) 0.4282(3) 0.159(8) Uani 0.5 1 d G U . B 2
H79 H 0.326747 0.130448 0.428928 0.190 Uiso 0.5 1 calc R . . B 2
C18 C 0.3182(16) 0.1771(16) 0.4195(2) 0.153(8) Uani 0.5 1 d G U . B 2
C12 C 0.3218(18) 0.2258(18) 0.4183(2) 0.144(8) Uani 0.25 1 d G U . B 2
C26 C 0.3364(17) 0.2603(13) 0.4259(3) 0.142(8) Uani 0.5 1 d G U . B 2
C102 C 0.3160(15) 0.2589(15) 0.4534(3) 0.168(6) Uani 0.5 1 d . U . B 2
N107 N 0.2651(18) 0.2278(16) 0.4501(2) 0.171(6) Uani 0.5 1 d G U . B 2
H107 H 0.259699 0.221245 0.444160 0.205 Uiso 0.5 1 calc R . . B 2
C90 C 0.2231(13) 0.2074(15) 0.4563(3) 0.178(7) Uani 0.5 1 d G U . B 2
H90 H 0.189017 0.186563 0.454095 0.214 Uiso 0.5 1 calc R . . B 2
C129 C 0.2319(16) 0.2180(17) 0.4659(3) 0.184(8) Uani 0.5 1 d G U . B 2
H129 H 0.203698 0.204276 0.470102 0.221 Uiso 0.5 1 calc R . . B 2
C82 C 0.283(2) 0.2490(17) 0.4693(2) 0.187(8) Uani 0.5 1 d G U . B 2
H82 H 0.288618 0.256137 0.475692 0.224 Uiso 0.5 1 calc R . . B 2
C113 C 0.3248(14) 0.2695(15) 0.4630(3) 0.130(9) Uani 0.5 1 d G U . B 2
H113 H 0.358857 0.290286 0.465274 0.156 Uiso 0.5 1 calc R . . B 2
C87 C 0.3708(13) 0.3374(11) 0.4388(2) 0.174(6) Uani 0.5 1 d . U . B 2
C3 C 0.4171(12) 0.3693(12) 0.43391(17) 0.077(8) Uani 0.5 1 d G U . B 2
H3 H 0.433257 0.354436 0.430476 0.093 Uiso 0.5 1 calc R . . B 2
C38 C 0.4392(12) 0.4236(11) 0.4342(2) 0.184(7) Uani 0.5 1 d G U . B 2
H38 H 0.470108 0.444971 0.430923 0.221 Uiso 0.5 1 calc R . . B 2
C25 C 0.4150(19) 0.4459(12) 0.4393(3) 0.191(8) Uani 0.5 1 d G U . B 2
H25 H 0.429749 0.482175 0.439498 0.229 Uiso 0.5 1 calc R . . B 2
C40 C 0.3687(18) 0.414(2) 0.4442(2) 0.188(8) Uani 0.5 1 d G U . B 2
H40 H 0.352538 0.428845 0.447626 0.225 Uiso 0.5 1 calc R . . B 2
C30 C 0.3466(12) 0.3597(19) 0.4439(2) 0.179(6) Uani 0.5 1 d G U . B 2
H30 H 0.315685 0.338310 0.447179 0.215 Uiso 0.5 1 calc R . . B 2
P1 P 0.3685(12) 0.2851(14) 0.4457(2) 0.156(6) Uani 0.5 1 d . U . B 1
S1A S 0.6463(3) 0.5073(2) 0.44670(4) 0.0708(15) Uani 0.6 1 d . . . A 1
S0AA S 0.6548(4) 0.4753(4) 0.43676(7) 0.081(2) Uani 0.4 1 d . U . A 2
C2BA C 0.5846(8) 0.5041(6) 0.43043(16) 0.085(3) Uani 0.4 1 d D U . A 2
H2BA H 0.579810 0.483930 0.424724 0.103 Uiso 0.4 1 calc R . . A 2
H2BB H 0.560873 0.480483 0.435200 0.103 Uiso 0.4 1 calc R . . A 2
C0BA C 0.6488(9) 0.5589(9) 0.44305(12) 0.085(3) Uani 0.4 1 d D U . A 2
H0BA H 0.684783 0.574451 0.445231 0.102 Uiso 0.4 1 calc R . . A 2
H0BB H 0.625971 0.535208 0.447901 0.102 Uiso 0.4 1 calc R . . A 2
C1BA C 0.6794(8) 0.5665(9) 0.42639(16) 0.085(3) Uani 0.4 1 d D U . A 2
H1BA H 0.715417 0.581841 0.428564 0.101 Uiso 0.4 1 calc R . . A 2
H1BB H 0.676064 0.547533 0.420586 0.101 Uiso 0.4 1 calc R . . A 2
C6BA C 0.6098(9) 0.5854(9) 0.42091(12) 0.086(4) Uani 0.4 1 d D U . A 2
H6BA H 0.606124 0.566181 0.415129 0.103 Uiso 0.4 1 calc R . . A 2
H6BB H 0.601460 0.612701 0.419546 0.103 Uiso 0.4 1 calc R . . A 2
C11 C 0.5777(8) 0.5772(10) 0.43771(15) 0.085(4) Uani 0.4 1 d D U . A 2
H11A H 0.554197 0.552895 0.442416 0.102 Uiso 0.4 1 calc R . . A 2
H11B H 0.568434 0.604141 0.436714 0.102 Uiso 0.4 1 calc R . . A 2
C3BA C 0.6350(8) 0.6026(8) 0.44124(11) 0.085(4) Uani 0.4 1 d D U . A 2
H3BA H 0.638664 0.621660 0.447116 0.102 Uiso 0.4 1 calc R . . A 2
C4BA C 0.6727(8) 0.6409(6) 0.43373(16) 0.085(4) Uani 0.4 1 d D U . A 2
H4BA H 0.708631 0.656786 0.435949 0.102 Uiso 0.4 1 calc R . . A 2
H4BB H 0.664610 0.668573 0.432580 0.102 Uiso 0.4 1 calc R . . A 2
C7BA C 0.6663(8) 0.6101(8) 0.42451(13) 0.087(4) Uani 0.4 1 d D U . A 2
H7BA H 0.690327 0.634143 0.419723 0.105 Uiso 0.4 1 calc R . . A 2
C80 C 0.5718(6) 0.5478(8) 0.42844(15) 0.087(4) Uani 0.4 1 d D U . A 2
H80 H 0.535629 0.532371 0.426167 0.105 Uiso 0.4 1 calc R . . A 2
C76 C 0.6420(9) 0.5283(7) 0.43389(15) 0.084(4) Uani 0.4 1 d D U . A 2
Ag1 Ag 0.7203(3) 0.4941(3) 0.44786(2) 0.0888(11) Uani 0.6 1 d . . . A 1
S1 S 0.52213(14) 0.37974(15) 0.46097(2) 0.0685(8) Uani 1 1 d . U . . .
C1AA C 0.4629(6) 0.4139(6) 0.47103(10) 0.074(2) Uani 1 1 d . U . . .
H1AB H 0.432883 0.391104 0.467134 0.089 Uiso 1 1 calc R . . . .
H1AC H 0.463555 0.393495 0.476356 0.089 Uiso 1 1 calc R . . . .
C3AA C 0.5599(6) 0.4691(6) 0.47143(10) 0.073(2) Uani 1 1 d . U . . .
H3AB H 0.591957 0.481852 0.467800 0.088 Uiso 1 1 calc R . . . .
H3AC H 0.561664 0.449217 0.476730 0.088 Uiso 1 1 calc R . . . .
C2AA C 0.5133(6) 0.4335(6) 0.46528(10) 0.075(2) Uani 1 1 d . U . . .
C4AA C 0.5104(6) 0.4645(6) 0.45666(10) 0.075(2) Uani 1 1 d . U . . .
H4AB H 0.542181 0.477720 0.452926 0.090 Uiso 1 1 calc R . . . .
H4AC H 0.480756 0.441649 0.452712 0.090 Uiso 1 1 calc R . . . .
C6 C 0.5043(6) 0.5110(6) 0.46027(10) 0.077(2) Uani 1 1 d . U . . .
H6 H 0.502347 0.530931 0.454897 0.092 Uiso 1 1 calc R . . . .
C5AA C 0.5044(6) 0.4938(6) 0.48084(10) 0.077(2) Uani 1 1 d . U . . .
H5AB H 0.500231 0.522301 0.483277 0.092 Uiso 1 1 calc R . . . .
H5AC H 0.505887 0.473750 0.486142 0.092 Uiso 1 1 calc R . . . .
C6AA C 0.5558(6) 0.5163(6) 0.47513(10) 0.074(2) Uani 1 1 d . U . . .
H6AB H 0.586084 0.538975 0.479106 0.089 Uiso 1 1 calc R . . . .
C8AA C 0.4546(6) 0.4897(6) 0.46604(10) 0.076(2) Uani 1 1 d . U . . .
H8AA H 0.424516 0.467184 0.462134 0.092 Uiso 1 1 calc R . . . .
H8AB H 0.450299 0.518418 0.468309 0.092 Uiso 1 1 calc R . . . .
C7AA C 0.4573(6) 0.4581(6) 0.47447(10) 0.075(2) Uani 1 1 d . U . . .
H7AA H 0.424831 0.444366 0.478151 0.090 Uiso 1 1 calc R . . . .
C9AA C 0.5522(6) 0.5476(6) 0.46658(10) 0.078(2) Uani 1 1 d . U . . .
H9AA H 0.584247 0.561765 0.462895 0.094 Uiso 1 1 calc R . . . .
H9AB H 0.548545 0.576739 0.468835 0.094 Uiso 1 1 calc R . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt01 Ag02 2.8096(13) 2_655 ?
Pt01 Ag02 2.8096(13) 3_665 ?
Pt01 Ag02 2.8093(13) . ?
Pt01 Ag03 2.7773(13) 3_665 ?
Pt01 Ag03 2.7773(13) 2_655 ?
Pt01 Ag03 2.7773(13) . ?
Pt01 Ag04 2.8016(13) 3_665 ?
Pt01 Ag04 2.8013(13) . ?
Pt01 Ag04 2.8016(13) 2_655 ?
Pt01 Ag05 2.8222(13) 2_655 ?
Pt01 Ag05 2.8224(13) 3_665 ?
Pt01 Ag05 2.8223(13) . ?
Ag02 Ag02 2.8212(19) 3_665 ?
Ag02 Ag02 2.821(2) 2_655 ?
Ag02 Ag03 2.7732(14) 2_655 ?
Ag02 Ag05 2.7538(14) . ?
Ag02 Ag06 3.1503(16) 2_655 ?
Ag02 Ag06 3.0395(16) . ?
Ag02 S00C 2.483(3) . ?
Ag03 Ag04 2.8616(15) 2_655 ?
Ag03 Ag05 2.8330(17) . ?
Ag03 Ag05 2.7705(18) 3_665 ?
Ag03 Ag08 3.0530(17) . ?
Ag03 Ag09 3.0365(16) . ?
Ag03 S1 2.478(4) . ?
Ag04 Ag04 2.776(2) 2_655 ?
Ag04 Ag04 2.776(2) 3_665 ?
Ag04 Ag05 2.8495(15) 3_665 ?
Ag04 Ag09 2.9589(19) 3_665 ?
Ag04 Ag 3.016(8) . ?
Ag04 S00E 2.499(4) . ?
Ag04 Ag1 2.988(7) . ?
Ag05 Ag08 3.1827(17) . ?
Ag05 Ag 3.225(5) 2_655 ?
Ag05 S00G 2.493(4) . ?
Ag05 Ag1 2.856(4) 2_655 ?
Ag06 Ag08 3.0486(16) . ?
Ag06 S00C 2.419(4) . ?
Ag06 S00D 2.386(4) . ?
Ag07 S00C 2.612(3) 2_655 ?
Ag07 S00C 2.613(3) 3_665 ?
Ag07 S00C 2.613(3) . ?
Ag07 P00H 2.404(6) . ?
Ag08 S00D 2.431(3) . ?
Ag08 S00G 2.479(4) . ?
Ag08 S1 2.851(4) . ?
Ag09 Ag 3.241(10) . ?
Ag09 S00E 2.729(5) 2_655 ?
Ag09 S1A 2.350(7) . ?
Ag09 S0AA 2.367(10) . ?
Ag09 Ag1 3.318(7) . ?
Ag09 S1 2.597(4) . ?
Ag0A S00E 2.682(4) 2_655 ?
Ag0A S00G 2.680(4) . ?
Ag0A P0 2.404(10) . ?
Ag0A P1 2.37(3) . ?
Ag0A Ag1 3.369(7) 2_655 ?
Ag0A S1 2.591(4) . ?
Ag S00E 2.484(10) . ?
Ag S0AA 1.990(14) . ?
S00C C00M 1.827(15) . ?
S00D C00R 1.789(16) . ?
S00E C00S 1.834(8) . ?
S00E Ag1 2.589(8) . ?
S00G C00U 1.800(18) . ?
S00G Ag1 2.682(6) 2_655 ?
P00H C01P 1.797(10) . ?
P00H C01P 1.797(10) 3_665 ?
P00H C01P 1.797(10) 2_655 ?
P0 C5 1.95(3) . ?
P0 C102 1.66(4) . ?
P0 C87 1.77(3) . ?
C00M C00N 1.511(18) . ?
C00M C00V 1.513(19) . ?
C00M C00W 1.576(18) . ?
C00N C01R 1.54(2) . ?
C00O C00T 1.597(19) . ?
C00O C00V 1.519(19) . ?
C00O C013 1.49(2) . ?
C00R C012 1.58(2) . ?
C00R C018 1.53(2) . ?
C00R C01M 1.52(2) . ?
C00S C011 1.543(8) . ?
C00S C01H 1.542(8) . ?
C00S C025 1.547(8) . ?
C00T C01R 1.47(2) . ?
C00U C00Y 1.54(2) . ?
C00U C00Z 1.55(2) . ?
C00U C01O 1.51(2) . ?
C00W C014 1.52(2) . ?
C00Y C01S 1.59(2) . ?
C00Z C01Q 1.52(2) . ?
C010 C01Q 1.52(2) . ?
C010 C01S 1.53(2) . ?
C011 C023 1.547(8) . ?
C012 C01C 1.56(2) . ?
C013 C014 1.55(2) . ?
C014 C019 1.52(2) . ?
C015 C018 1.52(2) . ?
C015 C01G 1.55(2) . ?
C015 C022 1.56(3) . ?
C019 C01R 1.54(2) . ?
C0 C02L 1.544(8) . ?
C0 C19 1.545(8) . ?
C0 C21 1.543(8) . ?
C0 S1A 1.833(12) . ?
C01B C01N 1.54(2) . ?
C01B C01O 1.61(2) . ?
C01B C01U 1.43(2) . ?
C01C C01T 1.48(3) . ?
C01C C022 1.52(2) . ?
C01G C01X 1.57(2) . ?
C01H C028 1.526(8) . ?
C01L C01V 1.544(8) . ?
C01L C021 1.532(8) . ?
C01L C025 1.536(8) . ?
C01M C01X 1.57(2) . ?
C01N C01Q 1.51(2) . ?
C01P C02B 1.3900 . ?
C01P C01E 1.3900 . ?
C02B C43 1.3900 . ?
C43 C132 1.3900 . ?
C132 C01Y 1.3900 . ?
C01Y C01E 1.3900 . ?
C01S C01U 1.49(2) . ?
C01T C01X 1.56(3) . ?
C01V C028 1.533(8) . ?
C021 C023 1.542(8) . ?
C023 C024 1.549(8) . ?
C024 C028 1.530(8) . ?
C02E C02G 1.537(8) . ?
C02E C02K 1.543(8) . ?
C02E C02L 1.535(8) . ?
C02G C02J 1.541(8) . ?
C02J C02P 1.540(8) . ?
C02J C19 1.553(8) . ?
C02K C55 1.541(8) . ?
C02P C55 1.543(8) . ?
C21 C55 1.543(8) . ?
C16 C4 1.3900(15) . ?
C16 N 1.3900 . ?
C16 P1 1.61(4) . ?
C4 C42 1.3900 . ?
C42 C116 1.3900 . ?
C116 C71 1.3900(12) . ?
C71 N 1.3900 . ?
C13 C20 1.3900 . ?
C13 C10 1.3900 . ?
C13 P1 1.87(5) . ?
C20 C8 1.3900 . ?
C8 C29 1.3900 . ?
C29 C46 1.3900 . ?
C46 C10 1.3900 . ?
C0AA C49 1.3900 . ?
C0AA C141 1.3900 . ?
C0AA P1 1.76(4) . ?
C49 C2 1.3900 . ?
C2 C1 1.3900 . ?
C1 C17 1.3900(11) . ?
C17 C141 1.3900(11) . ?
C5 N6 1.3900 . ?
C5 C26 1.3900 . ?
N6 C79 1.3900 . ?
C79 C18 1.3900 . ?
C18 C18 1.11(7) 12 ?
C18 C12 1.66(5) 12 ?
C18 C12 1.3900 . ?
C12 C12 0.76(9) 12 ?
C12 C26 1.3900 . ?
C12 C26 1.76(8) 12 ?
C102 N107 1.3900 . ?
C102 C113 1.3900 . ?
N107 C90 1.3900 . ?
C90 C129 1.3900 . ?
C129 C82 1.3900(12) . ?
C82 C113 1.3900 . ?
C87 C3 1.3900 . ?
C87 C30 1.3900 . ?
C3 C38 1.3900 . ?
C38 C25 1.3900 . ?
C25 C40 1.3900(11) . ?
C40 C30 1.3900 . ?
S1A Ag1 2.398(9) . ?
S0AA C76 1.825(18) . ?
C2BA C80 1.537(8) . ?
C2BA C76 1.547(8) . ?
C0BA C3BA 1.550(8) . ?
C0BA C76 1.535(8) . ?
C1BA C7BA 1.537(9) . ?
C1BA C76 1.539(9) . ?
C6BA C7BA 1.530(8) . ?
C6BA C80 1.541(8) . ?
C11 C3BA 1.544(8) . ?
C11 C80 1.532(8) . ?
C3BA C4BA 1.544(8) . ?
C4BA C7BA 1.546(8) . ?
S1 C2AA 1.830(16) . ?
C1AA C2AA 1.53(2) . ?
C1AA C7AA 1.47(2) . ?
C3AA C2AA 1.52(2) . ?
C3AA C6AA 1.54(2) . ?
C2AA C4AA 1.553(19) . ?
C4AA C6 1.55(2) . ?
C6 C8AA 1.51(2) . ?
C6 C9AA 1.56(2) . ?
C5AA C6AA 1.54(2) . ?
C5AA C7AA 1.54(2) . ?
C6AA C9AA 1.56(2) . ?
C8AA C7AA 1.54(2) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Ag02 Pt01 Ag02 60.28(4) . 2_655 ?
Ag02 Pt01 Ag02 60.28(4) 2_655 3_665 ?
Ag02 Pt01 Ag02 60.28(4) . 3_665 ?
Ag02 Pt01 Ag05 118.54(4) 3_665 2_655 ?
Ag02 Pt01 Ag05 58.55(3) . . ?
Ag02 Pt01 Ag05 58.55(3) 2_655 2_655 ?
Ag02 Pt01 Ag05 58.55(3) 3_665 3_665 ?
Ag02 Pt01 Ag05 93.46(3) 3_665 . ?
Ag02 Pt01 Ag05 118.55(4) 2_655 . ?
Ag02 Pt01 Ag05 118.55(4) . 3_665 ?
Ag02 Pt01 Ag05 93.46(3) . 2_655 ?
Ag02 Pt01 Ag05 93.45(3) 2_655 3_665 ?
Ag03 Pt01 Ag02 119.53(4) . 2_655 ?
Ag03 Pt01 Ag02 85.51(3) . . ?
Ag03 Pt01 Ag02 59.52(3) 3_665 2_655 ?
Ag03 Pt01 Ag02 59.52(3) 2_655 . ?
Ag03 Pt01 Ag02 85.52(3) 2_655 2_655 ?
Ag03 Pt01 Ag02 119.53(4) 2_655 3_665 ?
Ag03 Pt01 Ag02 119.53(4) 3_665 . ?
Ag03 Pt01 Ag02 59.52(3) . 3_665 ?
Ag03 Pt01 Ag02 85.52(3) 3_665 3_665 ?
Ag03 Pt01 Ag03 119.858(4) 2_655 3_665 ?
Ag03 Pt01 Ag03 119.859(4) 2_655 . ?
Ag03 Pt01 Ag03 119.857(4) 3_665 . ?
Ag03 Pt01 Ag04 92.94(3) 2_655 2_655 ?
Ag03 Pt01 Ag04 121.05(4) 2_655 . ?
Ag03 Pt01 Ag04 92.94(3) . . ?
Ag03 Pt01 Ag04 121.04(4) 3_665 2_655 ?
Ag03 Pt01 Ag04 61.71(3) 3_665 . ?
Ag03 Pt01 Ag04 61.72(3) 2_655 3_665 ?
Ag03 Pt01 Ag04 61.72(3) . 2_655 ?
Ag03 Pt01 Ag04 92.94(3) 3_665 3_665 ?
Ag03 Pt01 Ag04 121.04(4) . 3_665 ?
Ag03 Pt01 Ag05 59.30(3) 2_655 . ?
Ag03 Pt01 Ag05 59.30(3) . 3_665 ?
Ag03 Pt01 Ag05 60.78(3) 2_655 2_655 ?
Ag03 Pt01 Ag05 178.06(4) . 2_655 ?
Ag03 Pt01 Ag05 60.78(3) . . ?
Ag03 Pt01 Ag05 178.07(4) 2_655 3_665 ?
Ag03 Pt01 Ag05 60.78(3) 3_665 3_665 ?
Ag03 Pt01 Ag05 178.07(4) 3_665 . ?
Ag03 Pt01 Ag05 59.30(3) 3_665 2_655 ?
Ag04 Pt01 Ag02 178.38(3) 2_655 2_655 ?
Ag04 Pt01 Ag02 119.29(4) . 3_665 ?
Ag04 Pt01 Ag02 121.06(3) . 2_655 ?
Ag04 Pt01 Ag02 178.38(3) . . ?
Ag04 Pt01 Ag02 121.06(3) 2_655 3_665 ?
Ag04 Pt01 Ag02 121.06(3) 3_665 . ?
Ag04 Pt01 Ag02 119.30(3) 3_665 2_655 ?
Ag04 Pt01 Ag02 119.29(4) 2_655 . ?
Ag04 Pt01 Ag02 178.38(4) 3_665 3_665 ?
Ag04 Pt01 Ag04 59.40(4) . 3_665 ?
Ag04 Pt01 Ag04 59.40(4) . 2_655 ?
Ag04 Pt01 Ag04 59.39(4) 3_665 2_655 ?
Ag04 Pt01 Ag05 88.10(3) 2_655 3_665 ?
Ag04 Pt01 Ag05 60.89(3) 3_665 2_655 ?
Ag04 Pt01 Ag05 120.21(4) 3_665 3_665 ?
Ag04 Pt01 Ag05 88.10(3) 3_665 . ?
Ag04 Pt01 Ag05 60.89(3) 2_655 . ?
Ag04 Pt01 Ag05 88.10(3) . 2_655 ?
Ag04 Pt01 Ag05 120.21(4) . . ?
Ag04 Pt01 Ag05 120.21(4) 2_655 2_655 ?
Ag04 Pt01 Ag05 60.89(3) . 3_665 ?
Ag05 Pt01 Ag05 119.997(2) 2_655 3_665 ?
Ag05 Pt01 Ag05 119.996(1) 2_655 . ?
Ag05 Pt01 Ag05 119.993(1) . 3_665 ?
Pt01 Ag02 Ag02 59.867(19) . 3_665 ?
Pt01 Ag02 Ag02 59.867(19) . 2_655 ?
Pt01 Ag02 Ag06 116.26(4) . . ?
Pt01 Ag02 Ag06 112.84(4) . 2_655 ?
Ag02 Ag02 Ag02 60.001(1) 3_665 2_655 ?
Ag02 Ag02 Ag06 114.35(4) 2_655 . ?
Ag02 Ag02 Ag06 111.06(4) 3_665 2_655 ?
Ag02 Ag02 Ag06 64.89(4) 3_665 . ?
Ag02 Ag02 Ag06 60.90(4) 2_655 2_655 ?
Ag03 Ag02 Pt01 59.67(3) 2_655 . ?
Ag03 Ag02 Ag02 85.37(5) 2_655 2_655 ?
Ag03 Ag02 Ag02 119.27(3) 2_655 3_665 ?
Ag03 Ag02 Ag06 87.24(4) 2_655 2_655 ?
Ag03 Ag02 Ag06 155.43(5) 2_655 . ?
Ag05 Ag02 Pt01 60.96(3) . . ?
Ag05 Ag02 Ag02 120.54(3) . 2_655 ?
Ag05 Ag02 Ag02 94.70(4) . 3_665 ?
Ag05 Ag02 Ag03 60.17(4) . 2_655 ?
Ag05 Ag02 Ag06 145.94(5) . 2_655 ?
Ag05 Ag02 Ag06 96.02(5) . . ?
Ag06 Ag02 Ag06 114.67(5) . 2_655 ?
S00C Ag02 Pt01 153.24(9) . . ?
S00C Ag02 Ag02 94.77(9) . 3_665 ?
S00C Ag02 Ag02 101.50(8) . 2_655 ?
S00C Ag02 Ag03 143.06(9) . 2_655 ?
S00C Ag02 Ag05 135.72(10) . . ?
S00C Ag02 Ag06 50.74(9) . . ?
S00C Ag02 Ag06 65.95(9) . 2_655 ?
Pt01 Ag03 Ag04 59.56(3) . 2_655 ?
Pt01 Ag03 Ag05 60.40(3) . . ?
Pt01 Ag03 Ag08 118.55(4) . . ?
Pt01 Ag03 Ag09 110.97(4) . . ?
Ag02 Ag03 Pt01 60.82(3) 3_665 . ?
Ag02 Ag03 Ag04 120.21(5) 3_665 2_655 ?
Ag02 Ag03 Ag05 94.01(4) 3_665 . ?
Ag02 Ag03 Ag08 97.99(4) 3_665 . ?
Ag02 Ag03 Ag09 145.46(6) 3_665 . ?
Ag04 Ag03 Ag08 113.39(5) 2_655 . ?
Ag04 Ag03 Ag09 60.13(4) 2_655 . ?
Ag05 Ag03 Pt01 61.16(3) 3_665 . ?
Ag05 Ag03 Ag02 59.57(4) 3_665 3_665 ?
Ag05 Ag03 Ag04 60.05(4) . 2_655 ?
Ag05 Ag03 Ag04 87.93(4) 3_665 2_655 ?
Ag05 Ag03 Ag05 121.47(5) 3_665 . ?
Ag05 Ag03 Ag08 65.34(4) . . ?
Ag05 Ag03 Ag08 155.66(4) 3_665 . ?
Ag05 Ag03 Ag09 111.11(5) . . ?
Ag05 Ag03 Ag09 86.62(4) 3_665 . ?
Ag09 Ag03 Ag08 113.66(5) . . ?
S1 Ag03 Pt01 153.67(9) . . ?
S1 Ag03 Ag02 144.13(9) . 3_665 ?
S1 Ag03 Ag04 95.45(9) . 2_655 ?
S1 Ag03 Ag05 101.38(10) . . ?
S1 Ag03 Ag05 131.41(11) . 3_665 ?
S1 Ag03 Ag08 61.01(9) . . ?
S1 Ag03 Ag09 55.08(9) . . ?
Pt01 Ag04 Ag03 58.73(3) . 3_665 ?
Pt01 Ag04 Ag05 59.92(3) . 3_665 ?
Pt01 Ag04 Ag09 112.58(4) . 3_665 ?
Pt01 Ag04 Ag 121.14(13) . . ?
Pt01 Ag04 Ag1 114.84(9) . . ?
Ag03 Ag04 Ag09 62.86(4) 3_665 3_665 ?
Ag03 Ag04 Ag 111.88(14) 3_665 . ?
Ag03 Ag04 Ag1 103.80(10) 3_665 . ?
Ag04 Ag04 Pt01 60.31(2) 2_655 . ?
Ag04 Ag04 Pt01 60.31(2) 3_665 . ?
Ag04 Ag04 Ag03 118.97(3) 2_655 3_665 ?
Ag04 Ag04 Ag03 91.69(4) 3_665 3_665 ?
Ag04 Ag04 Ag04 60.0 2_655 3_665 ?
Ag04 Ag04 Ag05 120.15(3) 3_665 3_665 ?
Ag04 Ag04 Ag05 88.06(5) 2_655 3_665 ?
Ag04 Ag04 Ag09 92.03(6) 3_665 3_665 ?
Ag04 Ag04 Ag09 151.50(6) 2_655 3_665 ?
Ag04 Ag04 Ag 96.4(2) 2_655 . ?
Ag04 Ag04 Ag 153.40(19) 3_665 . ?
Ag04 Ag04 Ag1 98.41(14) 2_655 . ?
Ag04 Ag04 Ag1 157.97(14) 3_665 . ?
Ag05 Ag04 Ag03 59.48(4) 3_665 3_665 ?
Ag05 Ag04 Ag09 112.92(5) 3_665 3_665 ?
Ag05 Ag04 Ag 66.65(9) 3_665 . ?
Ag05 Ag04 Ag1 58.52(7) 3_665 . ?
Ag09 Ag04 Ag 109.31(19) 3_665 . ?
Ag09 Ag04 Ag1 108.87(14) 3_665 . ?
S00E Ag04 Pt01 155.71(10) . . ?
S00E Ag04 Ag03 99.91(10) . 3_665 ?
S00E Ag04 Ag04 137.73(11) . 3_665 ?
S00E Ag04 Ag04 138.36(10) . 2_655 ?
S00E Ag04 Ag05 100.45(10) . 3_665 ?
S00E Ag04 Ag09 59.29(11) . 3_665 ?
S00E Ag04 Ag 52.5(2) . . ?
S00E Ag04 Ag1 55.43(15) . . ?
Pt01 Ag05 Ag03 58.82(3) . . ?
Pt01 Ag05 Ag04 59.20(3) . 2_655 ?
Pt01 Ag05 Ag08 113.08(4) . . ?
Pt01 Ag05 Ag 113.68(16) . 2_655 ?
Pt01 Ag05 Ag1 118.49(13) . 2_655 ?
Ag02 Ag05 Pt01 60.49(3) . . ?
Ag02 Ag05 Ag03 85.50(4) . . ?
Ag02 Ag05 Ag03 60.26(4) . 2_655 ?
Ag02 Ag05 Ag04 119.54(5) . 2_655 ?
Ag02 Ag05 Ag08 89.49(4) . . ?
Ag02 Ag05 Ag 161.49(18) . 2_655 ?
Ag02 Ag05 Ag1 163.78(14) . 2_655 ?
Ag03 Ag05 Pt01 59.54(3) 2_655 . ?
Ag03 Ag05 Ag03 118.15(5) 2_655 . ?
Ag03 Ag05 Ag04 60.47(4) . 2_655 ?
Ag03 Ag05 Ag04 92.05(4) 2_655 2_655 ?
Ag03 Ag05 Ag08 60.67(4) . . ?
Ag03 Ag05 Ag08 149.07(4) 2_655 . ?
Ag03 Ag05 Ag 106.82(17) . 2_655 ?
Ag03 Ag05 Ag 101.34(18) 2_655 2_655 ?
Ag03 Ag05 Ag1 108.06(13) . 2_655 ?
Ag03 Ag05 Ag1 104.50(14) 2_655 2_655 ?
Ag04 Ag05 Ag08 109.98(5) 2_655 . ?
Ag04 Ag05 Ag 59.15(15) 2_655 2_655 ?
Ag04 Ag05 Ag1 63.17(13) 2_655 2_655 ?
Ag08 Ag05 Ag 108.49(18) . 2_655 ?
S00G Ag05 Pt01 153.63(10) . . ?
S00G Ag05 Ag02 129.33(9) . . ?
S00G Ag05 Ag03 95.66(10) . . ?
S00G Ag05 Ag03 146.15(10) . 2_655 ?
S00G Ag05 Ag04 104.14(9) . 2_655 ?
S00G Ag05 Ag08 50.00(9) . . ?
S00G Ag05 Ag 64.42(18) . 2_655 ?
S00G Ag05 Ag1 59.73(15) . 2_655 ?
Ag1 Ag05 Ag08 104.77(14) 2_655 . ?
Ag1 Ag05 Ag 4.9(3) 2_655 2_655 ?
Ag02 Ag06 Ag02 54.20(4) . 3_665 ?
Ag02 Ag06 Ag08 86.99(4) . . ?
Ag08 Ag06 Ag02 90.45(4) . 3_665 ?
S00C Ag06 Ag02 52.63(7) . . ?
S00C Ag06 Ag02 88.18(9) . 3_665 ?
S00C Ag06 Ag08 129.42(9) . . ?
S00D Ag06 Ag02 135.70(8) . . ?
S00D Ag06 Ag02 105.36(10) . 3_665 ?
S00D Ag06 Ag08 51.40(8) . . ?
S00D Ag06 S00C 166.44(13) . . ?
S00C Ag07 S00C 85.85(10) 2_655 3_665 ?
S00C Ag07 S00C 85.85(10) 2_655 . ?
S00C Ag07 S00C 85.85(10) . 3_665 ?
P00H Ag07 S00C 128.15(7) . . ?
P00H Ag07 S00C 128.15(7) . 3_665 ?
P00H Ag07 S00C 128.15(7) . 2_655 ?
Ag03 Ag08 Ag05 53.99(3) . . ?
Ag06 Ag08 Ag03 84.31(4) . . ?
Ag06 Ag08 Ag05 87.50(4) . . ?
S00D Ag08 Ag03 100.79(10) . . ?
S00D Ag08 Ag05 134.88(10) . . ?
S00D Ag08 Ag06 50.08(9) . . ?
S00D Ag08 S00G 167.82(13) . . ?
S00D Ag08 S1 105.53(12) . . ?
S00G Ag08 Ag03 90.64(9) . . ?
S00G Ag08 Ag05 50.38(9) . . ?
S00G Ag08 Ag06 128.11(10) . . ?
S00G Ag08 S1 85.07(11) . . ?
S1 Ag08 Ag03 49.49(8) . . ?
S1 Ag08 Ag05 85.83(8) . . ?
S1 Ag08 Ag06 125.64(9) . . ?
Ag03 Ag09 Ag 95.45(10) . . ?
Ag03 Ag09 Ag1 88.76(7) . . ?
Ag04 Ag09 Ag03 57.00(3) 2_655 . ?
Ag04 Ag09 Ag 88.26(15) 2_655 . ?
Ag04 Ag09 Ag1 87.95(12) 2_655 . ?
S00E Ag09 Ag03 90.79(8) 2_655 . ?
S00E Ag09 Ag04 51.94(9) 2_655 2_655 ?
S00E Ag09 Ag 125.99(17) 2_655 . ?
S00E Ag09 Ag1 130.28(14) 2_655 . ?
S1A Ag09 Ag03 111.48(15) . . ?
S1A Ag09 Ag04 134.20(17) . 2_655 ?
S1A Ag09 S00E 156.25(16) . 2_655 ?
S1A Ag09 Ag1 46.3(2) . . ?
S1A Ag09 S1 116.99(17) . . ?
S0AA Ag09 Ag03 133.1(3) . . ?
S0AA Ag09 Ag04 107.2(3) . 2_655 ?
S0AA Ag09 Ag 37.6(3) . . ?
S0AA Ag09 S00E 114.0(3) . 2_655 ?
S0AA Ag09 S1 160.5(3) . . ?
S1 Ag09 Ag03 51.47(8) . . ?
S1 Ag09 Ag04 90.66(9) . 2_655 ?
S1 Ag09 Ag 139.03(12) . . ?
S1 Ag09 S00E 83.00(12) . 2_655 ?
S1 Ag09 Ag1 131.24(10) . . ?
S00E Ag0A Ag1 49.06(14) 2_655 2_655 ?
S00G Ag0A S00E 94.04(12) . 2_655 ?
S00G Ag0A Ag1 51.10(10) . 2_655 ?
P0 Ag0A S00E 126.7(3) . 2_655 ?
P0 Ag0A S00G 124.7(3) . . ?
P0 Ag0A Ag1 129.1(4) . 2_655 ?
P0 Ag0A S1 128.1(4) . . ?
P1 Ag0A S00E 124.4(8) . 2_655 ?
P1 Ag0A S00G 124.7(8) . . ?
P1 Ag0A Ag1 126.5(9) . 2_655 ?
P1 Ag0A S1 130.6(9) . . ?
S1 Ag0A S00E 84.05(13) . 2_655 ?
S1 Ag0A S00G 86.55(12) . . ?
S1 Ag0A Ag1 102.79(13) . 2_655 ?
Ag04 Ag Ag05 54.20(11) . 3_665 ?
Ag04 Ag Ag09 82.5(2) . . ?
Ag05 Ag Ag09 76.15(17) 3_665 . ?
S00E Ag Ag04 52.99(19) . . ?
S00E Ag Ag05 91.3(2) . 3_665 ?
S00E Ag Ag09 130.2(3) . . ?
S0AA Ag Ag04 110.6(5) . . ?
S0AA Ag Ag09 46.6(3) . . ?
S0AA Ag S00E 124.6(4) . . ?
Ag02 S00C Ag07 117.72(13) . . ?
Ag06 S00C Ag02 76.63(9) . . ?
Ag06 S00C Ag07 99.31(12) . . ?
C00M S00C Ag02 118.5(4) . . ?
C00M S00C Ag06 107.2(5) . . ?
C00M S00C Ag07 121.7(4) . . ?
Ag06 S00D Ag08 78.53(11) . . ?
C00R S00D Ag06 107.4(5) . . ?
C00R S00D Ag08 112.0(5) . . ?
Ag04 S00E Ag09 68.77(11) . 3_665 ?
Ag04 S00E Ag0A 113.76(13) . 3_665 ?
Ag04 S00E Ag1 71.91(17) . . ?
Ag0A S00E Ag09 90.55(12) 3_665 3_665 ?
Ag S00E Ag04 74.5(2) . . ?
Ag S00E Ag09 138.39(19) . 3_665 ?
C00S S00E Ag04 121.0(4) . . ?
C00S S00E Ag09 112.1(4) . 3_665 ?
C00S S00E Ag0A 125.1(4) . 3_665 ?
C00S S00E Ag 103.1(4) . . ?
C00S S00E Ag1 112.8(4) . . ?
Ag1 S00E Ag09 130.93(16) . 3_665 ?
Ag1 S00E Ag0A 79.43(19) . 3_665 ?
Ag05 S00G Ag0A 113.49(14) . . ?
Ag05 S00G Ag1 66.88(16) . 2_655 ?
Ag08 S00G Ag05 79.62(11) . . ?
Ag08 S00G Ag0A 91.29(13) . . ?
Ag08 S00G Ag1 136.1(2) . 2_655 ?
Ag0A S00G Ag1 77.85(16) . 2_655 ?
C00U S00G Ag05 122.4(6) . . ?
C00U S00G Ag08 113.7(5) . . ?
C00U S00G Ag0A 121.4(5) . . ?
C00U S00G Ag1 108.0(6) . 2_655 ?
C01P P00H Ag07 113.6(5) 2_655 . ?
C01P P00H Ag07 113.6(5) 3_665 . ?
C01P P00H Ag07 113.6(5) . . ?
C01P P00H C01P 105.1(5) 3_665 2_655 ?
C01P P00H C01P 105.1(5) . 2_655 ?
C01P P00H C01P 105.1(5) 3_665 . ?
C5 P0 Ag0A 109.0(13) . . ?
C102 P0 Ag0A 119.1(16) . . ?
C102 P0 C5 107(2) . . ?
C102 P0 C87 117(2) . . ?
C87 P0 Ag0A 114.2(12) . . ?
C87 P0 C5 83.7(17) . . ?
C00N C00M S00C 109.9(10) . . ?
C00N C00M C00V 109.5(12) . . ?
C00N C00M C00W 108.6(12) . . ?
C00V C00M S00C 109.7(10) . . ?
C00V C00M C00W 109.0(12) . . ?
C00W C00M S00C 110.1(9) . . ?
C00M C00N C01R 106.6(13) . . ?
C00V C00O C00T 107.2(12) . . ?
C013 C00O C00T 106.4(13) . . ?
C013 C00O C00V 109.2(12) . . ?
C012 C00R S00D 107.4(10) . . ?
C018 C00R S00D 113.3(11) . . ?
C018 C00R C012 107.6(13) . . ?
C01M C00R S00D 114.1(10) . . ?
C01M C00R C012 105.5(13) . . ?
C01M C00R C018 108.5(13) . . ?
C011 C00S S00E 109.5(6) . . ?
C011 C00S C025 109.1(6) . . ?
C01H C00S S00E 110.3(6) . . ?
C01H C00S C011 109.3(6) . . ?
C01H C00S C025 109.7(6) . . ?
C025 C00S S00E 108.9(6) . . ?
C01R C00T C00O 107.1(11) . . ?
C00Y C00U S00G 110.7(12) . . ?
C00Y C00U C00Z 106.1(13) . . ?
C00Z C00U S00G 116.7(12) . . ?
C01O C00U S00G 108.4(11) . . ?
C01O C00U C00Y 106.5(15) . . ?
C01O C00U C00Z 108.0(15) . . ?
C00M C00V C00O 113.3(13) . . ?
C014 C00W C00M 108.4(11) . . ?
C00U C00Y C01S 111.2(14) . . ?
C01Q C00Z C00U 116.1(16) . . ?
C01Q C010 C01S 114.9(15) . . ?
C00S C011 C023 109.2(4) . . ?
C01C C012 C00R 109.1(13) . . ?
C00O C013 C014 112.0(13) . . ?
C00W C014 C013 108.9(13) . . ?
C00W C014 C019 112.2(14) . . ?
C019 C014 C013 108.5(12) . . ?
C018 C015 C01G 107.4(14) . . ?
C018 C015 C022 110.1(15) . . ?
C01G C015 C022 110.7(16) . . ?
C015 C018 C00R 114.0(14) . . ?
C014 C019 C01R 105.4(13) . . ?
C02L C0 C19 109.5(6) . . ?
C02L C0 S1A 107.1(10) . . ?
C19 C0 S1A 106.5(9) . . ?
C21 C0 C02L 109.7(6) . . ?
C21 C0 C19 109.3(6) . . ?
C21 C0 S1A 114.6(10) . . ?
C01N C01B C01O 108.6(16) . . ?
C01U C01B C01N 107.2(15) . . ?
C01U C01B C01O 109.3(17) . . ?
C01T C01C C012 110.3(15) . . ?
C01T C01C C022 111.4(16) . . ?
C022 C01C C012 110.8(16) . . ?
C015 C01G C01X 108.5(15) . . ?
C028 C01H C00S 109.9(4) . . ?
C021 C01L C01V 110.5(6) . . ?
C021 C01L C025 108.3(6) . . ?
C025 C01L C01V 109.6(6) . . ?
C00R C01M C01X 113.1(13) . . ?
C01Q C01N C01B 113.2(16) . . ?
C00U C01O C01B 112.0(13) . . ?
C02B C01P P00H 121.5(9) . . ?
C02B C01P C01E 120.0 . . ?
C01E C01P P00H 118.5(8) . . ?
C01P C02B C43 120.0 . . ?
C132 C43 C02B 120.0 . . ?
C43 C132 C01Y 120.0 . . ?
C132 C01Y C01E 120.0 . . ?
C01Y C01E C01P 120.0 . . ?
C010 C01Q C00Z 104.4(16) . . ?
C01N C01Q C00Z 109.9(15) . . ?
C01N C01Q C010 104.9(16) . . ?
C00T C01R C00N 115.4(14) . . ?
C00T C01R C019 110.5(14) . . ?
C019 C01R C00N 111.1(12) . . ?
C010 C01S C00Y 105.8(15) . . ?
C01U C01S C00Y 110.3(15) . . ?
C01U C01S C010 106.9(16) . . ?
C01C C01T C01X 111.0(16) . . ?
C01B C01U C01S 113.8(16) . . ?
C028 C01V C01L 109.5(4) . . ?
C01M C01X C01G 109.2(15) . . ?
C01T C01X C01G 108.9(15) . . ?
C01T C01X C01M 106.0(15) . . ?
C01L C021 C023 109.9(4) . . ?
C01C C022 C015 107.7(16) . . ?
C011 C023 C024 108.5(5) . . ?
C021 C023 C011 109.0(6) . . ?
C021 C023 C024 110.3(5) . . ?
C028 C024 C023 109.5(4) . . ?
C01L C025 C00S 109.3(4) . . ?
C01H C028 C01V 108.8(6) . . ?
C01H C028 C024 109.5(6) . . ?
C024 C028 C01V 110.7(6) . . ?
C02G C02E C02K 109.9(6) . . ?
C02L C02E C02G 108.6(7) . . ?
C02L C02E C02K 110.3(6) . . ?
C02E C02G C02J 109.6(4) . . ?
C02G C02J C19 109.0(6) . . ?
C02P C02J C02G 110.4(6) . . ?
C02P C02J C19 109.2(6) . . ?
C55 C02K C02E 109.1(4) . . ?
C02E C02L C0 109.6(4) . . ?
C02J C02P C55 109.2(4) . . ?
C0 C19 C02J 108.9(4) . . ?
C55 C21 C0 109.2(4) . . ?
C02K C55 C02P 109.5(6) . . ?
C02K C55 C21 110.1(6) . . ?
C02P C55 C21 109.5(6) . . ?
C4 C16 N 120.0 . . ?
C4 C16 P1 113(3) . . ?
N C16 P1 120(3) . . ?
C16 C4 C42 120.0 . . ?
C116 C42 C4 120.00(8) . . ?
C42 C116 C71 120.0 . . ?
C116 C71 N 120.0 . . ?
C71 N C16 120.00(10) . . ?
C20 C13 C10 120.0 . . ?
C20 C13 P1 121(3) . . ?
C10 C13 P1 117(3) . . ?
C8 C20 C13 120.0 . . ?
C20 C8 C29 120.0 . . ?
C8 C29 C46 120.0 . . ?
C29 C46 C10 120.0 . . ?
C46 C10 C13 120.0 . . ?
C49 C0AA C141 120.00(7) . . ?
C49 C0AA P1 131(3) . . ?
C141 C0AA P1 109(3) . . ?
C2 C49 C0AA 120.0 . . ?
C1 C2 C49 120.00(5) . . ?
C2 C1 C17 120.00(6) . . ?
C141 C17 C1 120.0 . . ?
C17 C141 C0AA 120.00(6) . . ?
N6 C5 P0 113(2) . . ?
C26 C5 P0 127(2) . . ?
C26 C5 N6 120.0 . . ?
C79 N6 C5 120.0 . . ?
N6 C79 C18 120.0 . . ?
C18 C18 C79 120(5) 12 . ?
C18 C18 C12 82.6(2) 12 . ?
C12 C18 C79 120.0 . . ?
C18 C12 C26 120.0 . . ?
C12 C12 C18 97.1(4) 12 . ?
C12 C12 C26 106(6) 12 . ?
C5 C26 C12 120.00(6) . . ?
N107 C102 P0 122(3) . . ?
N107 C102 C113 120.00(6) . . ?
C113 C102 P0 118(3) . . ?
C102 N107 C90 120.0 . . ?
C129 C90 N107 120.00(10) . . ?
C90 C129 C82 120.00(7) . . ?
C113 C82 C129 120.0 . . ?
C82 C113 C102 120.00(8) . . ?
C3 C87 P0 119(2) . . ?
C3 C87 C30 120.00(6) . . ?
C30 C87 P0 104(2) . . ?
C38 C3 C87 120.0 . . ?
C25 C38 C3 120.00(6) . . ?
C38 C25 C40 120.00(9) . . ?
C30 C40 C25 120.0 . . ?
C40 C30 C87 120.00(6) . . ?
C16 P1 Ag0A 124(2) . . ?
C16 P1 C13 88(3) . . ?
C16 P1 C0AA 117(3) . . ?
C13 P1 Ag0A 104.4(18) . . ?
C0AA P1 Ag0A 116(2) . . ?
C0AA P1 C13 97(3) . . ?
Ag09 S1A Ag1 88.7(3) . . ?
C0 S1A Ag09 110.4(6) . . ?
C0 S1A Ag1 112.4(6) . . ?
Ag S0AA Ag09 95.7(4) . . ?
C76 S0AA Ag09 110.4(9) . . ?
C76 S0AA Ag 119.0(9) . . ?
C80 C2BA C76 109.8(4) . . ?
C76 C0BA C3BA 109.5(4) . . ?
C7BA C1BA C76 109.9(5) . . ?
C7BA C6BA C80 109.6(4) . . ?
C80 C11 C3BA 109.9(4) . . ?
C11 C3BA C0BA 109.1(6) . . ?
C4BA C3BA C0BA 109.2(6) . . ?
C4BA C3BA C11 109.9(6) . . ?
C3BA C4BA C7BA 108.9(4) . . ?
C1BA C7BA C4BA 109.6(6) . . ?
C6BA C7BA C1BA 109.1(7) . . ?
C6BA C7BA C4BA 110.2(6) . . ?
C2BA C80 C6BA 109.5(6) . . ?
C11 C80 C2BA 108.0(7) . . ?
C11 C80 C6BA 110.7(6) . . ?
C2BA C76 S0AA 108.7(13) . . ?
C0BA C76 S0AA 106.8(12) . . ?
C0BA C76 C2BA 109.4(6) . . ?
C0BA C76 C1BA 108.8(7) . . ?
C1BA C76 S0AA 113.5(13) . . ?
C1BA C76 C2BA 109.6(6) . . ?
Ag04 Ag1 Ag09 81.60(17) . . ?
Ag04 Ag1 Ag0A 85.91(16) . 3_665 ?
Ag05 Ag1 Ag04 58.31(11) 3_665 . ?
Ag05 Ag1 Ag09 80.09(15) 3_665 . ?
Ag05 Ag1 Ag0A 87.66(13) 3_665 3_665 ?
Ag09 Ag1 Ag0A 165.82(19) . 3_665 ?
S00E Ag1 Ag04 52.66(15) . . ?
S00E Ag1 Ag05 98.1(2) . 3_665 ?
S00E Ag1 Ag09 123.0(2) . . ?
S00E Ag1 Ag0A 51.51(15) . 3_665 ?
S00E Ag1 S00G 96.2(2) . 3_665 ?
S00G Ag1 Ag04 96.02(17) 3_665 . ?
S00G Ag1 Ag05 53.39(10) 3_665 3_665 ?
S00G Ag1 Ag09 123.60(17) 3_665 . ?
S00G Ag1 Ag0A 51.05(14) 3_665 3_665 ?
S1A Ag1 Ag04 126.7(3) . . ?
S1A Ag1 Ag05 103.6(2) . 3_665 ?
S1A Ag1 Ag09 45.08(19) . . ?
S1A Ag1 Ag0A 146.8(3) . 3_665 ?
S1A Ag1 S00E 151.3(2) . . ?
S1A Ag1 S00G 111.8(3) . 3_665 ?
Ag03 S1 Ag08 69.50(9) . . ?
Ag03 S1 Ag09 73.45(11) . . ?
Ag03 S1 Ag0A 116.93(15) . . ?
Ag09 S1 Ag08 138.60(15) . . ?
Ag0A S1 Ag08 85.28(12) . . ?
Ag0A S1 Ag09 95.65(12) . . ?
C2AA S1 Ag03 119.5(5) . . ?
C2AA S1 Ag08 105.7(5) . . ?
C2AA S1 Ag09 108.2(5) . . ?
C2AA S1 Ag0A 122.8(5) . . ?
C7AA C1AA C2AA 111.0(13) . . ?
C2AA C3AA C6AA 111.5(13) . . ?
C1AA C2AA S1 112.4(11) . . ?
C1AA C2AA C4AA 108.3(13) . . ?
C3AA C2AA S1 108.6(11) . . ?
C3AA C2AA C1AA 109.0(12) . . ?
C3AA C2AA C4AA 110.0(13) . . ?
C4AA C2AA S1 108.5(10) . . ?
C6 C4AA C2AA 108.8(12) . . ?
C4AA C6 C9AA 109.5(13) . . ?
C8AA C6 C4AA 109.1(13) . . ?
C8AA C6 C9AA 109.3(12) . . ?
C6AA C5AA C7AA 109.9(12) . . ?
C3AA C6AA C9AA 109.0(12) . . ?
C5AA C6AA C3AA 107.0(13) . . ?
C5AA C6AA C9AA 108.8(12) . . ?
C6 C8AA C7AA 109.9(13) . . ?
C1AA C7AA C5AA 109.6(13) . . ?
C1AA C7AA C8AA 109.7(12) . . ?
C8AA C7AA C5AA 110.1(13) . . ?
C6AA C9AA C6 110.1(13) . . ?

_olex2_submission_special_instructions 'No special instructions were received'
