# Electronic Supplementary Material (ESI) for ChemComm.
# This journal is © The Royal Society of Chemistry 2022

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
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data_ag36
_database_code_depnum_ccdc_archive 'CCDC 2150327'
loop_
_audit_author_name
_audit_author_address
'wuyage '
;Henan Polytechnic University
China
;
_audit_update_record             
;
2022-05-28 deposited with the CCDC.	2022-05-31 downloaded from the CCDC.
;
_audit_creation_date             2022-05-26
_audit_creation_method           
;
Olex2 1.2
(compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506)
;
_shelx_SHELXL_version_number     2016/6
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C194 H184 Ag36 F30 N4 O24 P2 S18'
_chemical_formula_sum            'C224 H258 Ag36 F30 N14 O36 P2 S18'
_chemical_formula_weight         8814.77
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           15
_space_group_name_H-M_alt        'C 1 2/c 1'
_space_group_name_Hall           '-C 2yc'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'

_cell_length_a                   40.552(10)
_cell_length_b                   30.945(7)
_cell_length_c                   22.193(5)
_cell_angle_alpha                90
_cell_angle_beta                 99.116(12)
_cell_angle_gamma                90
_cell_volume                     27497(11)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    9411
_cell_measurement_temperature    200(2)
_cell_measurement_theta_max      26.76
_cell_measurement_theta_min      2.28
_shelx_estimated_absorpt_T_max   0.772
_shelx_estimated_absorpt_T_min   0.718
_exptl_absorpt_coefficient_mu    2.727
_exptl_absorpt_correction_T_max  0.772
_exptl_absorpt_correction_T_min  0.718
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(SADABS; Sheldrick, 2003)'
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            black
_exptl_crystal_colour_primary    black
_exptl_crystal_density_diffrn    2.129
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             17072
_exptl_crystal_size_max          0.13
_exptl_crystal_size_mid          0.12
_exptl_crystal_size_min          0.1
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.1231
_diffrn_reflns_av_unetI/netI     0.0332
_diffrn_reflns_Laue_measured_fraction_full 0.998
_diffrn_reflns_Laue_measured_fraction_max 0.998
_diffrn_reflns_limit_h_max       48
_diffrn_reflns_limit_h_min       -48
_diffrn_reflns_limit_k_max       36
_diffrn_reflns_limit_k_min       -36
_diffrn_reflns_limit_l_max       26
_diffrn_reflns_limit_l_min       -26
_diffrn_reflns_number            650255
_diffrn_reflns_point_group_measured_fraction_full 0.998
_diffrn_reflns_point_group_measured_fraction_max 0.998
_diffrn_reflns_theta_full        25.000
_diffrn_reflns_theta_max         25.000
_diffrn_reflns_theta_min         1.961
_diffrn_ambient_temperature      200.0
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                16477
_reflns_number_total             24206
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT v8.37A (Bruker, 2015)'
_computing_data_collection       'SAINT v8.37A (Bruker, 2015)'
_computing_data_reduction        SAINT
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    'olex2.solve (Bourhis et al., 2015)'
_refine_diff_density_max         2.182
_refine_diff_density_min         -1.894
_refine_diff_density_rms         0.227
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.134
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1414
_refine_ls_number_reflns         24206
_refine_ls_number_restraints     1100
_refine_ls_R_factor_all          0.1400
_refine_ls_R_factor_gt           0.0959
_refine_ls_restrained_S_all      1.140
_refine_ls_shift/su_max          0.004
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0520P)²+2145.8477P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2080
_refine_ls_wR_factor_ref         0.2606
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups, All C(H,H) groups
 At 1.5 times of:
  All C(H,H,H) groups
2. Restrained distances
 C6-C5
 1.51 with sigma of 0.01
 C1AA-C0AA
 1.51 with sigma of 0.01
 C4-C3
 1.51 with sigma of 0.01
 C77-O12
 1.2 with sigma of 0.02
 N2-C79 = N2-C78
 1.45 with sigma of 0.02
 C33-C32
 1.51 with sigma of 0.01
 O11-C74
 1.2 with sigma of 0.02
 N1-C75 = N1-C76
 1.45 with sigma of 0.01
 C10-C9
 1.51 with sigma of 0.01
 C2-C1
 1.51 with sigma of 0.01
 F18-C1AA
 1.45 with sigma of 0.02
 C1AA-F16
 1.45 with sigma of 0.02
 F16-C1AA = F18-C1AA
 1.45 with sigma of 0.01
 F17-C1AA
 1.45 with sigma of 0.01
 S7-C54 = S7-C53
 1.85 with sigma of 0.01
 C55-C54 = C61-C53
 1.51 with sigma of 0.01
 C71-C70 = C71-C72 = C72-C73 = C70-C69 = C69-C68 = C73-C68
 1.39 with sigma of 0.01
 C1AA-O1AA
 2.2 with sigma of 0.04
 F10-C8 \\sim F11-C8 \\sim F12-C8
 with sigma of 0.02
 F11-F12 \\sim F11-F10 \\sim F12-F10
 with sigma of 0.02
 C7-F10 \\sim C7-F11 \\sim C7-F12
 with sigma of 0.02
 F2-C2 \\sim F3-C2 \\sim F1-C2
 with sigma of 0.01
 C1-F1 \\sim C1-F2 \\sim C1-F3
 with sigma of 0.02
 F2A-C2 \\sim F3A-C2 \\sim F3-C2 \\sim F1A-C2
 with sigma of 0.02
 F16-F17 \\sim F16-F18 \\sim F17-F18
 with sigma of 0.02
 O1AA-C0AA \\sim O0AA-C0AA
 with sigma of 0.01
3. Restrained planarity
 F1, F1A, F2, F2A, F3, F3A
 with sigma of 0.1
4. Rigid bond restraints
 F4, F5, F6, O3, O4, C3, C4
 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01
 F7, F8, F9, O5, O6, C5, C6
 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01
 O12, N2, C77, C78, C79
 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01
 F10, F11, F12, C8
 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01
 S4, C32, C33, C34, C35, C36, C37, C38
 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01
 F13, F14, F15, O9, O10, C9, C10
 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01
 S7, C54, C55, C56, C57, C58, C59, C60
 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01
 S7, C53, C54, C55, C56, C57, C58, C59, C60, C61, C62, C63, C64, C65, C66, C70,
  C71
 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01
5. Uiso/Uaniso restraints and constraints
Ag15 \\sim F16 \\sim F18 \\sim O1AA \\sim C0AA \\sim C1AA: within 3A with sigma
of 0.01 and sigma for terminal atoms of 0.01
Ag15 \\sim F16 \\sim F17 \\sim F18 \\sim O0AA \\sim O1AA \\sim C1AA: within 3A
with sigma of 0.01 and sigma for terminal atoms of 0.01
Ag23 \\sim O11 \\sim N1 \\sim C74 \\sim C75 \\sim C76: within 3A with sigma of
0.01 and sigma for terminal atoms of 0.01
Ag15: within 3A with sigma of 0.01 and sigma for terminal atoms of 0.01
Ag19 \\sim Ag20: within 3A with sigma of 0.01 and sigma for terminal atoms of
0.01
Uanis(Ag1) \\sim Ueq, Uanis(Ag2) \\sim Ueq: with sigma of 0.01 and sigma for
terminal atoms of 0.02
Uanis(O3) \\sim Ueq, Uanis(C3) \\sim Ueq, Uanis(O4) \\sim Ueq, Uanis(F6) \\sim
Ueq, Uanis(F5) \\sim Ueq, Uanis(C4) \\sim Ueq, Uanis(F4) \\sim Ueq: with sigma
of 0.01 and sigma for terminal atoms of 0.02
Uanis(O6) \\sim Ueq, Uanis(C5) \\sim Ueq, Uanis(C6) \\sim Ueq, Uanis(F7) \\sim
Ueq, Uanis(F8) \\sim Ueq, Uanis(F9) \\sim Ueq, Uanis(O5) \\sim Ueq: with sigma
of 0.01 and sigma for terminal atoms of 0.02
Uanis(Ag5) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(C78) \\sim Ueq, Uanis(N2) \\sim Ueq, Uanis(C79) \\sim Ueq, Uanis(C77)
\\sim Ueq, Uanis(O12) \\sim Ueq: with sigma of 0.01 and sigma for terminal
atoms of 0.02
Uanis(C22) \\sim Ueq, Uanis(C21) \\sim Ueq, Uanis(C20) \\sim Ueq, Uanis(C19)
\\sim Ueq, Uanis(C24) \\sim Ueq, Uanis(C23) \\sim Ueq, Uanis(C18) \\sim Ueq,
Uanis(C52) \\sim Ueq, Uanis(C47) \\sim Ueq, Uanis(C46) \\sim Ueq, Uanis(C51)
\\sim Ueq, Uanis(C49) \\sim Ueq, Uanis(C48) \\sim Ueq, Uanis(C50) \\sim Ueq,
Uanis(C101) \\sim Ueq, Uanis(C100) \\sim Ueq, Uanis(C99) \\sim Ueq, Uanis(C98)
\\sim Ueq, Uanis(C104) \\sim Ueq, Uanis(C103) \\sim Ueq, Uanis(C102) \\sim Ueq:
with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(F10) \\sim Ueq, Uanis(F11) \\sim Ueq, Uanis(F12) \\sim Ueq: with sigma of
0.01 and sigma for terminal atoms of 0.02
Uanis(C34) \\sim Ueq, Uanis(C35) \\sim Ueq, Uanis(C37) \\sim Ueq, Uanis(C36)
\\sim Ueq, Uanis(C38) \\sim Ueq, Uanis(C33) \\sim Ueq, Uanis(C32) \\sim Ueq:
with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(P2) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(O9) \\sim Ueq, Uanis(O10) \\sim Ueq, Uanis(C9) \\sim Ueq, Uanis(C10)
\\sim Ueq, Uanis(F13) \\sim Ueq, Uanis(F14) \\sim Ueq, Uanis(F15) \\sim Ueq:
with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(C68) \\sim Ueq, Uanis(C39) \\sim Ueq, Uanis(C67) \\sim Ueq, Uanis(C40)
\\sim Ueq, Uanis(C41) \\sim Ueq, Uanis(C42) \\sim Ueq, Uanis(C43) \\sim Ueq,
Uanis(C44) \\sim Ueq, Uanis(C45) \\sim Ueq, Uanis(C69) \\sim Ueq, Uanis(C73)
\\sim Ueq, Uanis(C70) \\sim Ueq, Uanis(C72) \\sim Ueq, Uanis(C71) \\sim Ueq:
with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(F1A) \\sim Ueq, Uanis(F2) \\sim Ueq, Uanis(F2A) \\sim Ueq, Uanis(F3)
\\sim Ueq, Uanis(F3A) \\sim Ueq, Uanis(F1) \\sim Ueq: with sigma of 0.01 and
sigma for terminal atoms of 0.02
Uanis(C66) \\sim Ueq, Uanis(C65) \\sim Ueq, Uanis(C64) \\sim Ueq, Uanis(C63)
\\sim Ueq, Uanis(C62) \\sim Ueq, Uanis(C61) \\sim Ueq, Uanis(C53) \\sim Ueq:
with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(C60) \\sim Ueq, Uanis(C59) \\sim Ueq, Uanis(C58) \\sim Ueq, Uanis(C57)
\\sim Ueq, Uanis(C56) \\sim Ueq, Uanis(C55) \\sim Ueq, Uanis(C54) \\sim Ueq:
with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(C28) \\sim Ueq, Uanis(C27) \\sim Ueq, Uanis(C31) \\sim Ueq, Uanis(C30)
\\sim Ueq, Uanis(C29) \\sim Ueq: with sigma of 0.01 and sigma for terminal
atoms of 0.02
Uanis(C13) \\sim Ueq, Uanis(C14) \\sim Ueq, Uanis(C15) \\sim Ueq, Uanis(C16)
\\sim Ueq, Uanis(C11) \\sim Ueq, Uanis(C94) \\sim Ueq, Uanis(C93) \\sim Ueq,
Uanis(C95) \\sim Ueq, Uanis(C96) \\sim Ueq: with sigma of 0.01 and sigma for
terminal atoms of 0.02
Uanis(Ag7) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(O0AA) = Uanis(C0AA)
6. Same fragment restrains
{F1, F2, F3, O1, O2, C1, C2} sigma for 1-2: 0.02, 1-3: 0.04
as
{F4, F5, F6, O3, O4, C3, C4}
{F1, F2, F3, O1, O2, C1, C2} sigma for 1-2: 0.02, 1-3: 0.04
as
{F7, F8, F9, O5, O6, C5, C6}
{F1, F2, F3, O1, O2, C1, C2} sigma for 1-2: 0.02, 1-3: 0.04
as
{F13, F14, F15, O9, O10, C9, C10}
7. Others
 Sof(F1A)=Sof(F2A)=Sof(F3A)=1-FVAR(1)
 Sof(F1)=Sof(F2)=Sof(F3)=FVAR(1)
 Sof(C53)=Sof(H53A)=Sof(H53B)=Sof(C61)=Sof(C62)=Sof(H62)=Sof(C63)=Sof(H63)=
 Sof(C64)=Sof(H64)=Sof(C65)=Sof(H65)=Sof(C66)=Sof(H66)=1-FVAR(2)
 Sof(C54)=Sof(H54A)=Sof(H54B)=Sof(C55)=Sof(C56)=Sof(H56)=Sof(C57)=Sof(H57)=
 Sof(C58)=Sof(H58)=Sof(C59)=Sof(H59)=Sof(C60)=Sof(H60)=FVAR(2)
 Sof(Ag2)=1-FVAR(3)
 Sof(Ag1)=FVAR(3)
 Fixed Sof: F10(0.5) F11(0.5) F12(0.5) F16(0.5) F17(0.5) F18(0.5) O0AA(0.5)
 O1AA(0.5) C0AA(0.5) C1AA(0.5)
8.a Secondary CH2 refined with riding coordinates:
 C11(H11A,H11B), C18(H18A,H18B), C25(H25A,H25B), C32(H32A,H32B), C39(H39A,
 H39B), C46(H46A,H46B), C53(H53A,H53B), C54(H54A,H54B), C67(H67A,H67B),
 C98(H98A,H98B)
8.b Aromatic/amide H refined with riding coordinates:
 C15(H15), C14(H14), C13(H13), C17(H17), C16(H16), C23(H23), C24(H24),
 C20(H20), C21(H21), C22(H22), C27(H27), C28(H28), C29(H29), C30(H30), C31(H31),
  C34(H34), C35(H35), C37(H37), C36(H36), C38(H38), C41(H41), C42(H42),
 C43(H43), C44(H44), C45(H45), C48(H48), C49(H49), C50(H50), C51(H51), C52(H52),
  C56(H56), C57(H57), C58(H58), C59(H59), C60(H60), C62(H62), C63(H63),
 C64(H64), C65(H65), C66(H66), C69(H69), C70(H70), C71(H71), C72(H72), C73(H73),
  C74(H74), C77(H77), C81(H81), C82(H82), C83(H83), C84(H84), C85(H85),
 C90(H90), C89(H89), C88(H88), C87(H87), C91(H91), C94(H94), C93(H93), C97(H97),
  C96(H96), C95(H95), C104(H104), C103(H103), C102(H102), C101(H101), C100(H100)
8.c Fitted hexagon refined as free rotating group:
 C15(C14,C13,C12,C17,C16), C23(C24,C19,C20,C21,C22), C33(C34,C35,C37,C36,C38),
 C40(C41,C42,C43,C44,C45), C55(C56,C57,C58,C59,C60), C61(C62,C63,C64,C65,C66),
 C80(C81,C82,C83,C84,C85), C90(C89,C88,C87,C86,C91), C94(C93,C92,C97,C96,C95),
 C104(C103,C102,C101,C100,C99)
8.d Idealised Me refined as rotating group:
 C75(H75A,H75B,H75C), C76(H76A,H76B,H76C), C78(H78A,H78B,H78C), C79(H79A,H79B,
 H79C)
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.3706(3) 0.7454(4) 0.3834(6) 0.162(3) Uani 0.61(2) 1 d . U . A 2
Ag2 Ag 0.3809(2) 0.7541(2) 0.4129(5) 0.076(3) Uani 0.39(2) 1 d . U . A 1
Ag5 Ag 0.44477(7) 0.75283(7) 0.47204(12) 0.1154(8) Uani 1 1 d . U . . .
Ag7 Ag 0.37978(6) 0.82420(8) 0.29902(10) 0.1009(7) Uani 1 1 d . U . . .
Ag8 Ag 0.49935(5) 0.81221(5) 0.46335(7) 0.0667(4) Uani 1 1 d . . . . .
Ag9 Ag 0.46765(3) 0.79876(4) 0.33067(5) 0.0448(3) Uani 1 1 d . . . . .
Ag10 Ag 0.46724(3) 0.82743(4) 0.20499(5) 0.0444(3) Uani 1 1 d . . . . .
Ag11 Ag 0.47917(4) 0.89263(4) 0.30666(6) 0.0514(3) Uani 1 1 d . . . . .
Ag12 Ag 0.500000 0.75122(5) 0.250000 0.0364(3) Uani 1 2 d S T P . .
Ag13 Ag 0.46820(4) 0.70432(4) 0.33278(5) 0.0492(3) Uani 1 1 d . . . . .
Ag14 Ag 0.52204(5) 0.66405(5) 0.42291(6) 0.0642(4) Uani 1 1 d . . . . .
Ag15 Ag 0.500000 0.58867(7) 0.250000 0.0802(8) Uani 1 2 d S TU P C .
Ag16 Ag 0.53161(4) 0.67323(4) 0.29156(6) 0.0511(3) Uani 1 1 d . . . . .
Ag17 Ag 0.56998(3) 0.74985(4) 0.27009(6) 0.0500(3) Uani 1 1 d . . . . .
Ag18 Ag 0.60823(4) 0.82540(6) 0.32877(8) 0.0736(5) Uani 1 1 d . . . . .
Ag19 Ag 0.56051(6) 0.61547(7) 0.20055(9) 0.0969(7) Uani 1 1 d . U . . .
Ag20 Ag 0.61631(8) 0.67324(9) 0.19689(12) 0.1291(9) Uani 1 1 d . U . . .
Ag21 Ag 0.52959(3) 0.75323(4) 0.37347(5) 0.0466(3) Uani 1 1 d . . . . .
Ag22 Ag 0.59137(5) 0.69696(5) 0.38398(7) 0.0680(4) Uani 1 1 d . . . . .
Ag23 Ag 0.56608(4) 0.83418(5) 0.42830(7) 0.0643(4) Uani 1 1 d . U . . .
S1 S 0.42163(13) 0.81559(16) 0.3901(2) 0.0591(12) Uani 1 1 d . . . . .
S2 S 0.42568(14) 0.69212(16) 0.4034(2) 0.0620(13) Uani 1 1 d . . . . .
S3 S 0.51407(13) 0.87574(13) 0.4043(2) 0.0534(11) Uani 1 1 d . . . . .
S4 S 0.57424(13) 0.88247(15) 0.2611(2) 0.0572(11) Uani 1 1 d . U . . .
S5 S 0.60260(14) 0.77312(17) 0.4127(2) 0.0644(13) Uani 1 1 d . . . . .
S6 S 0.49650(17) 0.60560(16) 0.3564(2) 0.0701(15) Uani 1 1 d . . . . .
S7 S 0.59083(15) 0.64004(17) 0.3063(2) 0.0685(14) Uani 1 1 d D U . . .
S8 S 0.62744(14) 0.74484(19) 0.2407(2) 0.0684(13) Uani 1 1 d . . . . .
S9 S 0.51455(14) 0.73132(14) 0.47838(19) 0.0593(13) Uani 1 1 d . . . . .
P2 P 0.32484(19) 0.7505(3) 0.4407(4) 0.103(2) Uani 1 1 d . U . . .
F1 F 0.4346(7) 0.8535(9) 0.6437(9) 0.122(10) Uani 0.72(4) 1 d D U . B 1
F2 F 0.4565(10) 0.7970(6) 0.6836(8) 0.133(11) Uani 0.72(4) 1 d D U . B 1
F3 F 0.4867(6) 0.8487(11) 0.6730(9) 0.124(10) Uani 0.72(4) 1 d D U . B 1
O1 O 0.4433(4) 0.7857(5) 0.5615(7) 0.094(5) Uani 1 1 d D . . . .
O2 O 0.4881(4) 0.8260(5) 0.5616(6) 0.082(5) Uani 1 1 d D . . . .
C1 C 0.4644(5) 0.8111(6) 0.5807(7) 0.077(7) Uani 1 1 d D . . . .
C2 C 0.4605(4) 0.8276(5) 0.6435(7) 0.094(8) Uani 1 1 d D . . . .
F1A F 0.4390(13) 0.8052(15) 0.6708(16) 0.084(18) Uani 0.28(4) 1 d D U . B 2
F2A F 0.4867(14) 0.817(3) 0.685(2) 0.13(3) Uani 0.28(4) 1 d D U . B 2
F3A F 0.4587(18) 0.8697(8) 0.651(2) 0.10(2) Uani 0.28(4) 1 d D U . B 2
F4 F 0.5986(7) 0.5939(10) 0.5869(11) 0.238(10) Uani 1 1 d D U . . .
F5 F 0.6198(7) 0.5664(7) 0.5200(12) 0.217(9) Uani 1 1 d D U . . .
F6 F 0.6443(6) 0.6168(8) 0.5622(12) 0.222(9) Uani 1 1 d D U . . .
O3 O 0.5656(4) 0.6232(6) 0.4789(7) 0.098(4) Uani 1 1 d D U . . .
O4 O 0.6089(5) 0.6646(6) 0.4802(9) 0.122(6) Uani 1 1 d D U . . .
C3 C 0.5930(6) 0.6349(8) 0.4943(12) 0.119(7) Uani 1 1 d D U . . .
C4 C 0.6133(6) 0.6058(8) 0.5413(11) 0.159(8) Uani 1 1 d D U . . .
F7 F 0.6348(6) 0.5021(7) 0.1528(14) 0.216(9) Uani 1 1 d D U . C 1
F8 F 0.6497(7) 0.5430(9) 0.0894(11) 0.222(9) Uani 1 1 d D U . C 1
F9 F 0.6784(6) 0.5411(9) 0.1723(13) 0.220(9) Uani 1 1 d D U . C 1
O5 O 0.5985(5) 0.5667(7) 0.1766(10) 0.129(6) Uani 1 1 d D U . C 1
O6 O 0.6399(5) 0.6113(7) 0.1732(10) 0.132(6) Uani 1 1 d D U . C 1
C5 C 0.6253(6) 0.5777(8) 0.1688(15) 0.133(7) Uani 1 1 d D U . C 1
C6 C 0.6461(6) 0.5416(8) 0.1482(12) 0.170(8) Uani 1 1 d D U . C 1
F10 F 0.4818(7) 1.0494(7) 0.2858(14) 0.102(8) Uani 0.5 1 d D U . D -1
F11 F 0.5317(5) 1.0452(6) 0.2745(14) 0.097(7) Uani 0.5 1 d D U . D -1
F12 F 0.4950(8) 1.0496(6) 0.1973(9) 0.097(7) Uani 0.5 1 d D U . D -1
F13 F 0.7344(5) 0.8573(8) 0.3150(12) 0.206(8) Uani 1 1 d D U . E 1
F14 F 0.7144(5) 0.9043(8) 0.3637(10) 0.194(8) Uani 1 1 d D U . E 1
F15 F 0.7151(7) 0.9148(9) 0.2728(12) 0.226(9) Uani 1 1 d D U . E 1
O9 O 0.6608(5) 0.8546(7) 0.3380(9) 0.122(6) Uani 1 1 d D U . E 1
O10 O 0.6676(5) 0.8572(7) 0.2425(9) 0.125(6) Uani 1 1 d D U . E 1
C9 C 0.6748(6) 0.8617(10) 0.2960(11) 0.124(7) Uani 1 1 d D U . E 1
C10 C 0.7086(5) 0.8833(8) 0.3106(11) 0.151(7) Uani 1 1 d D U . E 1
F16 F 0.5341(7) 0.4273(9) 0.2964(12) 0.124(4) Uani 0.5 1 d D U . C -1
F17 F 0.4996(7) 0.4352(10) 0.2138(12) 0.124(4) Uani 0.5 1 d D U . C -1
F18 F 0.5518(7) 0.4477(10) 0.2157(13) 0.124(4) Uani 0.5 1 d D U . C -1
O0AA O 0.4763(12) 0.5131(12) 0.241(2) 0.111(3) Uani 0.5 1 d D U . C -1
O1AA O 0.5435(11) 0.5248(10) 0.2546(18) 0.110(4) Uani 0.5 1 d D U . C -1
O7 O 0.4943(4) 0.9648(4) 0.2979(6) 0.068(4) Uani 1 1 d . . . . .
O11 O 0.6144(5) 0.8868(7) 0.4473(10) 0.118(4) Uani 1 1 d D U . . .
O12 O 0.5678(5) 0.8506(6) 0.5425(9) 0.101(5) Uani 1 1 d D U . . .
N1 N 0.6451(7) 0.9361(9) 0.4934(12) 0.134(5) Uani 1 1 d D U . . .
N2 N 0.5826(6) 0.8586(8) 0.6438(11) 0.116(6) Uani 1 1 d D U . . .
C0AA C 0.5113(8) 0.5051(10) 0.247(4) 0.111(3) Uani 0.5 1 d D U . C -1
C1AA C 0.5257(7) 0.4600(9) 0.2500(12) 0.118(4) Uani 0.5 1 d D U . C -1
C7 C 0.500000 0.9813(8) 0.250000 0.070(9) Uani 1 2 d DS T P D .
C8 C 0.500000 1.0313(8) 0.250000 0.069(6) Uani 1 2 d DS TU P . .
C11 C 0.4228(6) 0.8675(7) 0.4303(11) 0.080(6) Uani 1 1 d . U . . .
H11A H 0.435759 0.863952 0.471712 0.096 Uiso 1 1 calc R . . . .
H11B H 0.434508 0.888941 0.408311 0.096 Uiso 1 1 calc R . . . .
C15 C 0.3257(3) 0.9154(6) 0.4482(10) 0.129(11) Uani 1 1 d . U . . .
H15 H 0.304177 0.925940 0.452369 0.155 Uiso 1 1 calc R . . . .
C14 C 0.3431(5) 0.8891(6) 0.4931(8) 0.111(9) Uani 1 1 d G U . . .
H14 H 0.333433 0.881589 0.527974 0.133 Uiso 1 1 calc R . . . .
C13 C 0.3746(4) 0.8736(5) 0.4869(7) 0.097(8) Uani 1 1 d G U . . .
H13 H 0.386435 0.855622 0.517582 0.116 Uiso 1 1 calc R . . . .
C12 C 0.3887(3) 0.8845(5) 0.4358(7) 0.071(6) Uani 1 1 d G . . . .
C17 C 0.3713(4) 0.9109(5) 0.3909(6) 0.078(6) Uani 1 1 d G . . . .
H17 H 0.380925 0.918357 0.355980 0.094 Uiso 1 1 calc R . . . .
C16 C 0.3398(4) 0.9263(6) 0.3971(8) 0.113(9) Uani 1 1 d G U . . .
H16 H 0.327923 0.944324 0.366371 0.136 Uiso 1 1 calc R . . . .
C18 C 0.4282(6) 0.6438(8) 0.4539(11) 0.083(7) Uani 1 1 d . U . . .
H18A H 0.413225 0.621002 0.433661 0.100 Uiso 1 1 calc R . . . .
H18B H 0.451273 0.632439 0.460077 0.100 Uiso 1 1 calc R . . . .
C23 C 0.4364(6) 0.6804(7) 0.6163(8) 0.150(14) Uani 1 1 d . U . . .
H23 H 0.453512 0.691545 0.646621 0.180 Uiso 1 1 calc R . . . .
C24 C 0.4434(4) 0.6704(6) 0.5587(10) 0.115(10) Uani 1 1 d G U . . .
H24 H 0.465308 0.674653 0.549489 0.138 Uiso 1 1 calc R . . . .
C19 C 0.4185(5) 0.6541(5) 0.5144(7) 0.070(5) Uani 1 1 d G U . . .
C20 C 0.3865(4) 0.6478(6) 0.5278(9) 0.121(10) Uani 1 1 d G U . . .
H20 H 0.369377 0.636640 0.497495 0.145 Uiso 1 1 calc R . . . .
C21 C 0.3794(5) 0.6578(7) 0.5855(11) 0.136(12) Uani 1 1 d G U . . .
H21 H 0.357580 0.653532 0.594627 0.164 Uiso 1 1 calc R . . . .
C22 C 0.4044(7) 0.6741(7) 0.6298(8) 0.140(12) Uani 1 1 d G U . . .
H22 H 0.399647 0.680984 0.669191 0.168 Uiso 1 1 calc R . . . .
C25 C 0.5220(5) 0.9270(6) 0.4489(9) 0.066(5) Uani 1 1 d . . . . .
H25A H 0.539330 0.921764 0.484756 0.079 Uiso 1 1 calc R . . . .
H25B H 0.530639 0.949065 0.423070 0.079 Uiso 1 1 calc R . . . .
C26 C 0.4916(5) 0.9442(6) 0.4699(7) 0.058(5) Uani 1 1 d . . . . .
C27 C 0.4834(5) 0.9320(7) 0.5256(9) 0.069(5) Uani 1 1 d . U . . .
H27 H 0.497809 0.913039 0.551142 0.082 Uiso 1 1 calc R . . . .
C28 C 0.4551(6) 0.9469(8) 0.5446(11) 0.087(7) Uani 1 1 d . U . . .
H28 H 0.449882 0.937593 0.582727 0.104 Uiso 1 1 calc R . . . .
C29 C 0.4344(6) 0.9745(7) 0.5101(10) 0.073(6) Uani 1 1 d . U . . .
H29 H 0.415424 0.986063 0.524497 0.087 Uiso 1 1 calc R . . . .
C30 C 0.4416(6) 0.9856(7) 0.4537(10) 0.073(6) Uani 1 1 d . U . . .
H30 H 0.426557 1.003607 0.427632 0.088 Uiso 1 1 calc R . . . .
C31 C 0.4706(5) 0.9708(6) 0.4344(9) 0.063(5) Uani 1 1 d . U . . .
H31 H 0.475698 0.979508 0.395835 0.076 Uiso 1 1 calc R . . . .
C32 C 0.5814(6) 0.9313(7) 0.3066(11) 0.091(5) Uani 1 1 d D U . . .
H32A H 0.560030 0.946415 0.307630 0.109 Uiso 1 1 calc R . . . .
H32B H 0.591438 0.923921 0.348964 0.109 Uiso 1 1 calc R . . . .
C33 C 0.6050(6) 0.9603(7) 0.2781(11) 0.127(7) Uani 1 1 d D U . . .
C34 C 0.6394(7) 0.9577(7) 0.2961(10) 0.150(8) Uani 1 1 d G U . . .
H34 H 0.648362 0.938980 0.328447 0.180 Uiso 1 1 calc R . . . .
C35 C 0.6605(5) 0.9827(9) 0.2668(13) 0.162(9) Uani 1 1 d G U . . .
H35 H 0.684036 0.980926 0.279158 0.194 Uiso 1 1 calc R . . . .
C37 C 0.6474(7) 1.0101(8) 0.2195(12) 0.171(9) Uani 1 1 d G U . . .
H37 H 0.661851 1.027154 0.199519 0.205 Uiso 1 1 calc R . . . .
C36 C 0.6130(7) 1.0127(8) 0.2015(10) 0.166(9) Uani 1 1 d G U . . .
H36 H 0.603993 1.031435 0.169167 0.199 Uiso 1 1 calc R . . . .
C38 C 0.5918(5) 0.9878(9) 0.2308(12) 0.157(9) Uani 1 1 d G U . . .
H38 H 0.568319 0.989489 0.218455 0.189 Uiso 1 1 calc R . . . .
C39 C 0.6356(6) 0.7760(8) 0.4813(10) 0.078(6) Uani 1 1 d . U . . .
H39A H 0.637482 0.806099 0.496699 0.094 Uiso 1 1 calc R . . . .
H39B H 0.629319 0.757374 0.513867 0.094 Uiso 1 1 calc R . . . .
C40 C 0.6684(5) 0.7618(8) 0.4663(10) 0.100(8) Uani 1 1 d . U . . .
C41 C 0.6779(6) 0.7186(7) 0.4711(11) 0.166(15) Uani 1 1 d G U . . .
H41 H 0.663740 0.697870 0.485502 0.199 Uiso 1 1 calc R . . . .
C42 C 0.7082(7) 0.7058(7) 0.4548(11) 0.139(12) Uani 1 1 d G U . . .
H42 H 0.714649 0.676249 0.458144 0.167 Uiso 1 1 calc R . . . .
C43 C 0.7289(5) 0.7361(10) 0.4338(12) 0.172(16) Uani 1 1 d G U . . .
H43 H 0.749566 0.727316 0.422661 0.206 Uiso 1 1 calc R . . . .
C44 C 0.7194(6) 0.7793(9) 0.4289(12) 0.196(19) Uani 1 1 d G U . . .
H44 H 0.733574 0.800005 0.414535 0.235 Uiso 1 1 calc R . . . .
C45 C 0.6892(6) 0.7921(6) 0.4452(10) 0.125(11) Uani 1 1 d G U . . .
H45 H 0.682665 0.821627 0.441893 0.150 Uiso 1 1 calc R . . . .
C46 C 0.5049(6) 0.5523(7) 0.3977(10) 0.077(6) Uani 1 1 d . U . . .
H46A H 0.498487 0.528223 0.368810 0.093 Uiso 1 1 calc R . . . .
H46B H 0.529008 0.549689 0.413524 0.093 Uiso 1 1 calc R . . . .
C47 C 0.4858(6) 0.5493(7) 0.4486(11) 0.076(6) Uani 1 1 d . U . . .
C48 C 0.4545(8) 0.5313(10) 0.4407(15) 0.111(9) Uani 1 1 d . U . . .
H48 H 0.445181 0.520986 0.401322 0.133 Uiso 1 1 calc R . . . .
C49 C 0.4360(9) 0.5276(11) 0.4879(17) 0.128(11) Uani 1 1 d . U . . .
H49 H 0.414320 0.515206 0.482329 0.154 Uiso 1 1 calc R . . . .
C50 C 0.4507(8) 0.5423(9) 0.5405(14) 0.104(9) Uani 1 1 d . U . . .
H50 H 0.438355 0.539550 0.573281 0.125 Uiso 1 1 calc R . . . .
C51 C 0.4795(8) 0.5600(10) 0.5540(15) 0.111(9) Uani 1 1 d . U . . .
H51 H 0.487334 0.569850 0.594253 0.133 Uiso 1 1 calc R . . . .
C52 C 0.4997(7) 0.5646(8) 0.5059(11) 0.086(7) Uani 1 1 d . U . . .
H52 H 0.521282 0.577317 0.513214 0.103 Uiso 1 1 calc R . . . .
C53 C 0.5901(11) 0.5859(19) 0.341(5) 0.078(9) Uani 0.343(19) 1 d D U . F 2
H53A H 0.573598 0.586487 0.369740 0.093 Uiso 0.343(19) 1 calc R . . F 2
H53B H 0.581881 0.565015 0.308619 0.093 Uiso 0.343(19) 1 calc R . . F 2
C54 C 0.5949(6) 0.5874(13) 0.346(3) 0.092(7) Uani 0.657(19) 1 d D U . F 1
H54A H 0.588677 0.590093 0.387389 0.111 Uiso 0.657(19) 1 calc R . . F 1
H54B H 0.580303 0.565511 0.322896 0.111 Uiso 0.657(19) 1 calc R . . F 1
C55 C 0.6312(6) 0.5745(10) 0.3507(15) 0.103(8) Uani 0.657(19) 1 d D U . F 1
C56 C 0.6540(8) 0.5939(9) 0.3959(13) 0.120(9) Uani 0.657(19) 1 d G U . F 1
H56 H 0.646600 0.614420 0.422722 0.144 Uiso 0.657(19) 1 calc R . . F 1
C57 C 0.6877(7) 0.5833(11) 0.4019(14) 0.126(10) Uani 0.657(19) 1 d G U . F 1
H57 H 0.703289 0.596604 0.432865 0.151 Uiso 0.657(19) 1 calc R . . F 1
C58 C 0.6985(6) 0.5534(11) 0.3627(17) 0.136(10) Uani 0.657(19) 1 d G U . F 1
H58 H 0.721515 0.546127 0.366850 0.163 Uiso 0.657(19) 1 calc R . . F 1
C59 C 0.6757(8) 0.5340(10) 0.3175(14) 0.127(10) Uani 0.657(19) 1 d G U . F 1
H59 H 0.683052 0.513466 0.290693 0.152 Uiso 0.657(19) 1 calc R . . F 1
C60 C 0.6420(8) 0.5445(10) 0.3115(13) 0.121(9) Uani 0.657(19) 1 d G U . F 1
H60 H 0.626362 0.531282 0.280550 0.146 Uiso 0.657(19) 1 calc R . . F 1
C61 C 0.6225(9) 0.5684(15) 0.376(2) 0.080(9) Uani 0.343(19) 1 d D U . F 2
C62 C 0.6242(10) 0.5469(16) 0.431(2) 0.086(10) Uani 0.343(19) 1 d G U . F 2
H62 H 0.605230 0.545993 0.451506 0.104 Uiso 0.343(19) 1 calc R . . F 2
C63 C 0.6537(12) 0.5266(15) 0.4572(18) 0.094(11) Uani 0.343(19) 1 d G U . F 2
H63 H 0.654810 0.511866 0.495040 0.112 Uiso 0.343(19) 1 calc R . . F 2
C64 C 0.6814(9) 0.5279(16) 0.428(2) 0.097(11) Uani 0.343(19) 1 d G U . F 2
H64 H 0.701561 0.514011 0.445379 0.117 Uiso 0.343(19) 1 calc R . . F 2
C65 C 0.6798(10) 0.5494(17) 0.372(2) 0.093(11) Uani 0.343(19) 1 d G U . F 2
H65 H 0.698734 0.550285 0.352184 0.112 Uiso 0.343(19) 1 calc R . . F 2
C66 C 0.6503(12) 0.5697(15) 0.3465(17) 0.087(10) Uani 0.343(19) 1 d G U . F 2
H66 H 0.649155 0.584413 0.308649 0.105 Uiso 0.343(19) 1 calc R . . F 2
C67 C 0.6635(6) 0.7380(8) 0.3004(12) 0.089(7) Uani 1 1 d . U . . .
H67A H 0.671790 0.766889 0.314717 0.107 Uiso 1 1 calc R . . . .
H67B H 0.656231 0.722882 0.335370 0.107 Uiso 1 1 calc R . . . .
C68 C 0.6906(5) 0.7140(7) 0.2814(10) 0.076(6) Uani 1 1 d D U . . .
C69 C 0.6918(7) 0.6693(7) 0.2853(12) 0.100(8) Uani 1 1 d D U . . .
H69 H 0.674365 0.654356 0.300466 0.120 Uiso 1 1 calc R . . . .
C70 C 0.7179(7) 0.6458(11) 0.2674(16) 0.143(11) Uani 1 1 d D U . . .
H70 H 0.717721 0.615083 0.268332 0.172 Uiso 1 1 calc R . . . .
C71 C 0.7440(9) 0.6680(10) 0.2484(17) 0.137(11) Uani 1 1 d D U . . .
H71 H 0.762371 0.651994 0.238305 0.164 Uiso 1 1 calc R . . . .
C72 C 0.7444(8) 0.7125(10) 0.2434(16) 0.137(12) Uani 1 1 d D U . . .
H72 H 0.761939 0.727384 0.228535 0.164 Uiso 1 1 calc R . . . .
C73 C 0.7176(6) 0.7342(9) 0.2616(13) 0.103(8) Uani 1 1 d D U . . .
H73 H 0.717743 0.764916 0.260349 0.123 Uiso 1 1 calc R . . . .
C74 C 0.6197(10) 0.9122(10) 0.4863(15) 0.135(5) Uani 1 1 d D U . . .
H74 H 0.604127 0.915039 0.513906 0.162 Uiso 1 1 calc R . . . .
C75 C 0.6766(7) 0.9145(11) 0.4917(16) 0.139(5) Uani 1 1 d D U . . .
H75A H 0.694793 0.935761 0.498307 0.208 Uiso 1 1 calc GR . . . .
H75B H 0.676180 0.900724 0.451863 0.208 Uiso 1 1 calc GR . . . .
H75C H 0.680279 0.892563 0.523872 0.208 Uiso 1 1 calc GR . . . .
C76 C 0.6480(9) 0.9628(11) 0.5473(14) 0.140(5) Uani 1 1 d D U . . .
H76A H 0.669474 0.957292 0.573164 0.211 Uiso 1 1 calc GR . . . .
H76B H 0.629787 0.955915 0.569983 0.211 Uiso 1 1 calc GR . . . .
H76C H 0.646596 0.993313 0.535341 0.211 Uiso 1 1 calc GR . . . .
C77 C 0.5859(8) 0.8424(12) 0.5887(13) 0.129(8) Uani 1 1 d D U . . .
H77 H 0.603848 0.823071 0.586545 0.155 Uiso 1 1 calc R . . . .
C78 C 0.5564(9) 0.8873(13) 0.6516(19) 0.174(13) Uani 1 1 d D U . . .
H78A H 0.565557 0.916312 0.660481 0.262 Uiso 1 1 calc GR . . . .
H78B H 0.545592 0.877335 0.685504 0.262 Uiso 1 1 calc GR . . . .
H78C H 0.540033 0.888025 0.614057 0.262 Uiso 1 1 calc GR . . . .
C79 C 0.5991(11) 0.8411(14) 0.7011(15) 0.180(13) Uani 1 1 d D U . . .
H79A H 0.591560 0.811408 0.705711 0.270 Uiso 1 1 calc GR . . . .
H79B H 0.593696 0.858841 0.734805 0.270 Uiso 1 1 calc GR . . . .
H79C H 0.623349 0.841286 0.701692 0.270 Uiso 1 1 calc GR . . . .
C80 C 0.2912(4) 0.7816(6) 0.3982(8) 0.092(8) Uani 1 1 d . . . G 1
C81 C 0.2991(4) 0.8209(7) 0.3735(9) 0.106(9) Uani 1 1 d G . . G 1
H81 H 0.321767 0.829960 0.377823 0.127 Uiso 1 1 calc R . . G 1
C82 C 0.2740(7) 0.8467(5) 0.3425(9) 0.110(9) Uani 1 1 d G . . G 1
H82 H 0.279445 0.873529 0.325615 0.132 Uiso 1 1 calc R . . G 1
C83 C 0.2409(6) 0.8334(8) 0.3361(8) 0.123(11) Uani 1 1 d G . . G 1
H83 H 0.223718 0.851091 0.314932 0.148 Uiso 1 1 calc R . . G 1
C84 C 0.2329(4) 0.7942(8) 0.3608(10) 0.119(11) Uani 1 1 d G . . G 1
H84 H 0.210311 0.785085 0.356457 0.143 Uiso 1 1 calc R . . G 1
C85 C 0.2581(5) 0.7683(6) 0.3918(9) 0.120(11) Uani 1 1 d G . . G 1
H85 H 0.252633 0.741515 0.408666 0.144 Uiso 1 1 calc R . . G 1
C90 C 0.2789(6) 0.6436(7) 0.5006(10) 0.131(12) Uani 1 1 d . . . H 1
H90 H 0.269562 0.634655 0.535275 0.157 Uiso 1 1 calc R . . H 1
C89 C 0.2784(6) 0.6159(6) 0.4512(13) 0.145(14) Uani 1 1 d G . . H 1
H89 H 0.268730 0.587929 0.452146 0.174 Uiso 1 1 calc R . . H 1
C88 C 0.2919(6) 0.6290(7) 0.4005(11) 0.144(14) Uani 1 1 d G . . H 1
H88 H 0.291610 0.610007 0.366759 0.173 Uiso 1 1 calc R . . H 1
C87 C 0.3060(5) 0.6698(8) 0.3992(8) 0.117(10) Uani 1 1 d G . . H 1
H87 H 0.315321 0.678811 0.364500 0.140 Uiso 1 1 calc R . . H 1
C86 C 0.3065(5) 0.6976(6) 0.4485(10) 0.110(10) Uani 1 1 d G . . H 1
C91 C 0.2929(6) 0.6845(7) 0.4993(9) 0.131(12) Uani 1 1 d G . . H 1
H91 H 0.293273 0.703461 0.533015 0.157 Uiso 1 1 calc R . . H 1
C94 C 0.3643(4) 0.7828(7) 0.6144(9) 0.136(12) Uani 1 1 d . U . I 1
H94 H 0.384832 0.778633 0.641005 0.163 Uiso 1 1 calc R . . I 1
C93 C 0.3601(4) 0.7667(6) 0.5553(10) 0.116(10) Uani 1 1 d G U . I 1
H93 H 0.377820 0.751431 0.541410 0.139 Uiso 1 1 calc R . . I 1
C92 C 0.3301(5) 0.7729(6) 0.5164(7) 0.096(8) Uani 1 1 d G . . I 1
C97 C 0.3042(4) 0.7952(7) 0.5367(8) 0.107(9) Uani 1 1 d G . . I 1
H97 H 0.283652 0.799386 0.510182 0.128 Uiso 1 1 calc R . . I 1
C96 C 0.3084(5) 0.8113(6) 0.5959(10) 0.120(10) Uani 1 1 d G U . I 1
H96 H 0.290663 0.826589 0.609777 0.143 Uiso 1 1 calc R . . I 1
C95 C 0.3384(6) 0.8052(7) 0.6348(7) 0.121(10) Uani 1 1 d G U . I 1
H95 H 0.341253 0.816212 0.675189 0.145 Uiso 1 1 calc R . . I 1
C98 C 0.5497(6) 0.7367(7) 0.5406(9) 0.076(6) Uani 1 1 d . U . . .
H98A H 0.569691 0.722915 0.528486 0.091 Uiso 1 1 calc R . . . .
H98B H 0.554766 0.767768 0.547935 0.091 Uiso 1 1 calc R . . . .
C104 C 0.5400(6) 0.7427(5) 0.6478(10) 0.133(12) Uani 1 1 d . U . . .
H104 H 0.541346 0.773263 0.644458 0.160 Uiso 1 1 calc R . . . .
C103 C 0.5354(6) 0.7240(8) 0.7027(8) 0.159(15) Uani 1 1 d G U . . .
H103 H 0.533487 0.741719 0.736956 0.191 Uiso 1 1 calc R . . . .
C102 C 0.5335(6) 0.6793(9) 0.7076(9) 0.145(13) Uani 1 1 d G U . . .
H102 H 0.530286 0.666497 0.745141 0.175 Uiso 1 1 calc R . . . .
C101 C 0.5362(6) 0.6534(6) 0.6575(12) 0.160(15) Uani 1 1 d G U . . .
H101 H 0.534945 0.622819 0.660829 0.191 Uiso 1 1 calc R . . . .
C100 C 0.5409(5) 0.6721(6) 0.6026(9) 0.121(10) Uani 1 1 d G U . . .
H100 H 0.542803 0.654363 0.568330 0.145 Uiso 1 1 calc R . . . .
C99 C 0.5428(5) 0.7168(6) 0.5977(7) 0.075(6) Uani 1 1 d G U . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 Ag5 3.330(15) . ?
Ag1 Ag7 3.133(8) . ?
Ag1 Ag20 2.956(14) 2_655 ?
Ag1 S2 2.754(10) . ?
Ag1 S8 2.768(13) 2_655 ?
Ag1 P2 2.416(8) . ?
Ag2 Ag5 2.712(11) . ?
Ag2 Ag7 3.326(9) . ?
Ag2 S1 2.621(7) . ?
Ag2 S2 2.673(9) . ?
Ag2 P2 2.451(9) . ?
Ag5 Ag8 2.907(3) . ?
Ag5 S1 2.724(6) . ?
Ag5 S2 2.465(6) . ?
Ag5 S9 2.888(6) . ?
Ag5 O1 2.239(14) . ?
Ag7 Ag18 2.953(3) 2_655 ?
Ag7 S1 2.439(6) . ?
Ag7 S8 2.610(6) 2_655 ?
Ag7 O10 2.241(19) 2_655 ?
Ag8 Ag9 3.049(2) . ?
Ag8 Ag21 3.0964(19) . ?
Ag8 Ag23 3.009(2) . ?
Ag8 S3 2.487(5) . ?
Ag8 S9 2.587(5) . ?
Ag8 O2 2.337(12) . ?
Ag9 Ag10 3.0078(19) 2_655 ?
Ag9 Ag10 2.9245(18) . ?
Ag9 Ag11 3.0032(19) . ?
Ag9 Ag12 2.7990(15) . ?
Ag9 Ag13 2.9227(19) . ?
Ag9 Ag17 2.9219(19) 2_655 ?
Ag9 Ag21 2.905(2) . ?
Ag9 S1 2.504(5) . ?
Ag10 Ag10 3.061(3) 2_655 ?
Ag10 Ag11 3.0083(18) . ?
Ag10 Ag11 3.0064(19) 2_655 ?
Ag10 Ag12 2.8112(18) . ?
Ag10 Ag17 2.9346(18) 2_655 ?
Ag10 Ag18 3.034(2) 2_655 ?
Ag10 Ag21 2.8967(17) 2_655 ?
Ag10 Ag23 3.058(2) 2_655 ?
Ag10 S4 2.588(5) 2_655 ?
Ag11 Ag11 3.244(3) 2_655 ?
Ag11 S3 2.450(5) . ?
Ag11 S4 2.454(6) 2_655 ?
Ag11 O7 2.331(12) . ?
Ag12 Ag13 2.8098(15) 2_655 ?
Ag12 Ag13 2.8099(15) . ?
Ag12 Ag16 2.8186(19) . ?
Ag12 Ag16 2.8186(19) 2_655 ?
Ag12 Ag17 2.8021(15) 2_655 ?
Ag12 Ag17 2.8022(15) . ?
Ag12 Ag21 2.8124(14) 2_655 ?
Ag12 Ag21 2.8125(14) . ?
Ag13 Ag14 2.989(2) . ?
Ag13 Ag16 3.020(2) . ?
Ag13 Ag16 2.9237(18) 2_655 ?
Ag13 Ag17 2.9109(19) 2_655 ?
Ag13 Ag19 3.031(2) 2_655 ?
Ag13 Ag21 2.931(2) . ?
Ag13 S2 2.535(5) . ?
Ag14 Ag16 3.0143(19) . ?
Ag14 Ag21 3.003(2) . ?
Ag14 Ag22 3.234(3) . ?
Ag14 S6 2.457(6) . ?
Ag14 S9 2.462(5) . ?
Ag14 O3 2.359(17) . ?
Ag15 Ag16 2.995(2) 2_655 ?
Ag15 Ag16 2.995(2) . ?
Ag15 Ag19 2.961(3) 2_655 ?
Ag15 Ag19 2.961(3) . ?
Ag15 S6 2.445(5) . ?
Ag15 S6 2.445(5) 2_655 ?
Ag15 O0AA 2.52(4) . ?
Ag15 C0AA 2.63(3) . ?
Ag16 Ag16 2.912(3) 2_655 ?
Ag16 Ag17 2.916(2) . ?
Ag16 Ag19 3.065(2) . ?
Ag16 Ag21 3.0801(18) . ?
Ag16 Ag22 3.007(2) . ?
Ag16 S7 2.584(6) . ?
Ag17 Ag18 2.988(2) . ?
Ag17 Ag21 3.0247(18) . ?
Ag17 Ag22 3.021(2) . ?
Ag17 S8 2.522(5) . ?
Ag18 Ag23 3.012(2) . ?
Ag18 S4 2.572(5) . ?
Ag18 S5 2.504(5) . ?
Ag18 O9 2.293(19) . ?
Ag19 Ag20 2.895(4) . ?
Ag19 S6 2.472(7) 2_655 ?
Ag19 S7 2.585(6) . ?
Ag19 O5 2.28(2) . ?
Ag20 S2 2.644(6) 2_655 ?
Ag20 S7 2.968(6) . ?
Ag20 S8 2.433(6) . ?
Ag20 O6 2.24(2) . ?
Ag21 Ag22 3.030(2) . ?
Ag21 Ag23 3.062(2) . ?
Ag21 S9 2.589(4) . ?
Ag22 S5 2.465(6) . ?
Ag22 S7 2.463(5) . ?
Ag22 O4 2.36(2) . ?
Ag23 S3 2.456(5) . ?
Ag23 S5 2.459(5) . ?
Ag23 O11 2.53(2) . ?
Ag23 O12 2.576(19) . ?
S1 C11 1.83(2) . ?
S2 C18 1.86(2) . ?
S3 C25 1.870(17) . ?
S4 C32 1.81(2) . ?
S5 C39 1.86(2) . ?
S6 C46 1.89(2) . ?
S7 C53 1.851(10) . ?
S7 C54 1.850(10) . ?
S8 C67 1.82(2) . ?
S9 C98 1.83(2) . ?
P2 C80 1.810(19) . ?
P2 C86 1.817(17) . ?
P2 C92 1.798(17) . ?
F1 C2 1.324(11) . ?
F2 C2 1.326(11) . ?
F3 C2 1.326(11) . ?
O1 C1 1.189(18) . ?
O2 C1 1.201(17) . ?
C1 C2 1.515(8) . ?
C2 F1A 1.333(18) . ?
C2 F2A 1.334(19) . ?
C2 F3A 1.319(19) . ?
F4 C4 1.305(18) . ?
F5 C4 1.349(19) . ?
F6 C4 1.316(17) . ?
O3 C3 1.168(19) . ?
O4 C3 1.194(19) . ?
C3 C4 1.516(8) . ?
F7 C6 1.315(18) . ?
F8 C6 1.335(19) . ?
F9 C6 1.332(18) . ?
O5 C5 1.177(19) . ?
O6 C5 1.19(2) . ?
C5 C6 1.515(9) . ?
F10 C8 1.294(19) . ?
F11 C8 1.382(18) . ?
F12 C8 1.287(19) . ?
F13 C10 1.312(18) . ?
F14 C10 1.335(18) . ?
F15 C10 1.340(17) . ?
O9 C9 1.187(19) . ?
O10 C9 1.184(19) . ?
C9 C10 1.514(8) . ?
F16 C1AA 1.445(9) . ?
F17 C1AA 1.445(10) . ?
F18 C1AA 1.449(9) . ?
O0AA C0AA 1.43(3) . ?
O1AA C0AA 1.43(3) . ?
O7 C7 1.235(15) . ?
O11 C74 1.164(18) . ?
O12 C77 1.188(18) . ?
N1 C74 1.26(4) . ?
N1 C75 1.448(10) . ?
N1 C76 1.444(10) . ?
N2 C77 1.35(4) . ?
N2 C78 1.415(18) . ?
N2 C79 1.445(18) . ?
C0AA C1AA 1.511(10) . ?
C7 C8 1.55(3) . ?
C11 H11A 0.9900 . ?
C11 H11B 0.9900 . ?
C11 C12 1.50(2) . ?
C15 H15 0.9500 . ?
C15 C14 1.3900 . ?
C15 C16 1.3900 . ?
C14 H14 0.9500 . ?
C14 C13 1.3900 . ?
C13 H13 0.9500 . ?
C13 C12 1.3900 . ?
C12 C17 1.3900 . ?
C17 H17 0.9500 . ?
C17 C16 1.3900 . ?
C16 H16 0.9500 . ?
C18 H18A 0.9900 . ?
C18 H18B 0.9900 . ?
C18 C19 1.49(3) . ?
C23 H23 0.9500 . ?
C23 C24 1.3900 . ?
C23 C22 1.3900 . ?
C24 H24 0.9500 . ?
C24 C19 1.3900 . ?
C19 C20 1.3900 . ?
C20 H20 0.9500 . ?
C20 C21 1.3900 . ?
C21 H21 0.9500 . ?
C21 C22 1.3900 . ?
C22 H22 0.9500 . ?
C25 H25A 0.9900 . ?
C25 H25B 0.9900 . ?
C25 C26 1.48(3) . ?
C26 C27 1.38(3) . ?
C26 C31 1.34(3) . ?
C27 H27 0.9500 . ?
C27 C28 1.36(3) . ?
C28 H28 0.9500 . ?
C28 C29 1.35(3) . ?
C29 H29 0.9500 . ?
C29 C30 1.37(3) . ?
C30 H30 0.9500 . ?
C30 C31 1.40(3) . ?
C31 H31 0.9500 . ?
C32 H32A 0.9900 . ?
C32 H32B 0.9900 . ?
C32 C33 1.519(10) . ?
C33 C34 1.3900 . ?
C33 C38 1.3900 . ?
C34 H34 0.9500 . ?
C34 C35 1.3900 . ?
C35 H35 0.9500 . ?
C35 C37 1.3900 . ?
C37 H37 0.9500 . ?
C37 C36 1.3900 . ?
C36 H36 0.9500 . ?
C36 C38 1.3900 . ?
C38 H38 0.9500 . ?
C39 H39A 0.9900 . ?
C39 H39B 0.9900 . ?
C39 C40 1.49(3) . ?
C40 C41 1.3900 . ?
C40 C45 1.3900 . ?
C41 H41 0.9500 . ?
C41 C42 1.3900 . ?
C42 H42 0.9500 . ?
C42 C43 1.3900 . ?
C43 H43 0.9500 . ?
C43 C44 1.3900 . ?
C44 H44 0.9500 . ?
C44 C45 1.3900 . ?
C45 H45 0.9500 . ?
C46 H46A 0.9900 . ?
C46 H46B 0.9900 . ?
C46 C47 1.47(3) . ?
C47 C48 1.37(4) . ?
C47 C52 1.39(3) . ?
C48 H48 0.9500 . ?
C48 C49 1.39(4) . ?
C49 H49 0.9500 . ?
C49 C50 1.31(4) . ?
C50 H50 0.9500 . ?
C50 C51 1.28(4) . ?
C51 H51 0.9500 . ?
C51 C52 1.45(4) . ?
C52 H52 0.9500 . ?
C53 H53A 0.9900 . ?
C53 H53B 0.9900 . ?
C53 C61 1.512(10) . ?
C54 H54A 0.9900 . ?
C54 H54B 0.9900 . ?
C54 C55 1.510(10) . ?
C55 C56 1.3900 . ?
C55 C60 1.3900 . ?
C56 H56 0.9500 . ?
C56 C57 1.3900 . ?
C57 H57 0.9500 . ?
C57 C58 1.3900 . ?
C58 H58 0.9500 . ?
C58 C59 1.3900 . ?
C59 H59 0.9500 . ?
C59 C60 1.3900 . ?
C60 H60 0.9500 . ?
C61 C62 1.3900 . ?
C61 C66 1.3900 . ?
C62 H62 0.9500 . ?
C62 C63 1.3900 . ?
C63 H63 0.9500 . ?
C63 C64 1.3900 . ?
C64 H64 0.9500 . ?
C64 C65 1.3900 . ?
C65 H65 0.9500 . ?
C65 C66 1.3900 . ?
C66 H66 0.9500 . ?
C67 H67A 0.9900 . ?
C67 H67B 0.9900 . ?
C67 C68 1.44(3) . ?
C68 C69 1.387(10) . ?
C68 C73 1.391(10) . ?
C69 H69 0.9500 . ?
C69 C70 1.392(10) . ?
C70 H70 0.9500 . ?
C70 C71 1.384(10) . ?
C71 H71 0.9500 . ?
C71 C72 1.383(10) . ?
C72 H72 0.9500 . ?
C72 C73 1.390(10) . ?
C73 H73 0.9500 . ?
C74 H74 0.9500 . ?
C75 H75A 0.9800 . ?
C75 H75B 0.9800 . ?
C75 H75C 0.9800 . ?
C76 H76A 0.9800 . ?
C76 H76B 0.9800 . ?
C76 H76C 0.9800 . ?
C77 H77 0.9500 . ?
C78 H78A 0.9800 . ?
C78 H78B 0.9800 . ?
C78 H78C 0.9800 . ?
C79 H79A 0.9800 . ?
C79 H79B 0.9800 . ?
C79 H79C 0.9800 . ?
C80 C81 1.3900 . ?
C80 C85 1.3900 . ?
C81 H81 0.9500 . ?
C81 C82 1.3900 . ?
C82 H82 0.9500 . ?
C82 C83 1.3900 . ?
C83 H83 0.9500 . ?
C83 C84 1.3900 . ?
C84 H84 0.9500 . ?
C84 C85 1.3900 . ?
C85 H85 0.9500 . ?
C90 H90 0.9500 . ?
C90 C89 1.3900 . ?
C90 C91 1.3900 . ?
C89 H89 0.9500 . ?
C89 C88 1.3900 . ?
C88 H88 0.9500 . ?
C88 C87 1.3900 . ?
C87 H87 0.9500 . ?
C87 C86 1.3900 . ?
C86 C91 1.3900 . ?
C91 H91 0.9500 . ?
C94 H94 0.9500 . ?
C94 C93 1.3900 . ?
C94 C95 1.3900 . ?
C93 H93 0.9500 . ?
C93 C92 1.3900 . ?
C92 C97 1.3900 . ?
C97 H97 0.9500 . ?
C97 C96 1.3900 . ?
C96 H96 0.9500 . ?
C96 C95 1.3900 . ?
C95 H95 0.9500 . ?
C98 H98A 0.9900 . ?
C98 H98B 0.9900 . ?
C98 C99 1.47(3) . ?
C104 H104 0.9500 . ?
C104 C103 1.3900 . ?
C104 C99 1.3900 . ?
C103 H103 0.9500 . ?
C103 C102 1.3900 . ?
C102 H102 0.9500 . ?
C102 C101 1.3900 . ?
C101 H101 0.9500 . ?
C101 C100 1.3900 . ?
C100 H100 0.9500 . ?
C100 C99 1.3900 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Ag7 Ag1 Ag5 96.8(3) . . ?
Ag20 Ag1 Ag5 100.2(2) 2_655 . ?
Ag20 Ag1 Ag7 100.2(3) 2_655 . ?
S2 Ag1 Ag5 46.6(2) . . ?
S2 Ag1 Ag7 113.1(2) . . ?
S2 Ag1 Ag20 55.0(2) . 2_655 ?
S2 Ag1 S8 90.4(3) . 2_655 ?
S8 Ag1 Ag5 115.0(2) 2_655 . ?
S8 Ag1 Ag7 52.05(19) 2_655 . ?
S8 Ag1 Ag20 50.2(3) 2_655 2_655 ?
P2 Ag1 Ag5 112.4(6) . . ?
P2 Ag1 Ag7 115.9(4) . . ?
P2 Ag1 Ag20 126.4(6) . 2_655 ?
P2 Ag1 S2 128.7(4) . . ?
P2 Ag1 S8 132.0(6) . 2_655 ?
Ag5 Ag2 Ag7 105.93(18) . . ?
S1 Ag2 Ag5 61.4(2) . . ?
S1 Ag2 Ag7 46.59(17) . . ?
S1 Ag2 S2 92.8(2) . . ?
S2 Ag2 Ag5 54.5(2) . . ?
S2 Ag2 Ag7 109.6(3) . . ?
P2 Ag2 Ag5 136.9(5) . . ?
P2 Ag2 Ag7 108.6(4) . . ?
P2 Ag2 S1 136.1(4) . . ?
P2 Ag2 S2 131.0(3) . . ?
Ag2 Ag5 Ag8 129.60(17) . . ?
Ag2 Ag5 S1 57.64(18) . . ?
Ag2 Ag5 S9 151.7(2) . . ?
Ag8 Ag5 Ag1 129.08(16) . . ?
S1 Ag5 Ag1 58.1(2) . . ?
S1 Ag5 Ag8 71.96(13) . . ?
S1 Ag5 S9 115.34(15) . . ?
S2 Ag5 Ag1 54.3(3) . . ?
S2 Ag5 Ag2 62.0(2) . . ?
S2 Ag5 Ag8 127.50(14) . . ?
S2 Ag5 S1 95.13(18) . . ?
S2 Ag5 S9 93.66(18) . . ?
S9 Ag5 Ag1 143.0(2) . . ?
S9 Ag5 Ag8 53.02(11) . . ?
O1 Ag5 Ag1 114.0(5) . . ?
O1 Ag5 Ag2 105.4(5) . . ?
O1 Ag5 Ag8 84.2(4) . . ?
O1 Ag5 S1 102.3(5) . . ?
O1 Ag5 S2 147.6(4) . . ?
O1 Ag5 S9 103.0(5) . . ?
Ag18 Ag7 Ag1 129.6(3) 2_655 . ?
Ag18 Ag7 Ag2 138.93(17) 2_655 . ?
S1 Ag7 Ag1 63.4(3) . . ?
S1 Ag7 Ag2 51.3(2) . . ?
S1 Ag7 Ag18 126.75(14) . 2_655 ?
S1 Ag7 S8 101.71(19) . 2_655 ?
S8 Ag7 Ag1 56.7(3) 2_655 . ?
S8 Ag7 Ag2 68.3(2) 2_655 . ?
S8 Ag7 Ag18 73.41(13) 2_655 2_655 ?
O10 Ag7 Ag2 121.2(5) 2_655 . ?
O10 Ag7 Ag18 82.0(5) 2_655 2_655 ?
O10 Ag7 S1 146.0(5) 2_655 . ?
O10 Ag7 S8 104.3(6) 2_655 2_655 ?
Ag5 Ag8 Ag9 76.63(7) . . ?
Ag5 Ag8 Ag21 93.07(7) . . ?
Ag5 Ag8 Ag23 152.29(8) . . ?
Ag9 Ag8 Ag21 56.42(4) . . ?
Ag23 Ag8 Ag9 92.30(5) . . ?
Ag23 Ag8 Ag21 60.17(5) . . ?
S3 Ag8 Ag5 141.59(15) . . ?
S3 Ag8 Ag9 72.48(12) . . ?
S3 Ag8 Ag21 88.52(11) . . ?
S3 Ag8 Ag23 52.02(12) . . ?
S3 Ag8 S9 139.53(16) . . ?
S9 Ag8 Ag5 63.13(14) . . ?
S9 Ag8 Ag9 92.74(11) . . ?
S9 Ag8 Ag21 53.28(10) . . ?
S9 Ag8 Ag23 92.65(13) . . ?
O2 Ag8 Ag5 77.9(4) . . ?
O2 Ag8 Ag9 144.2(4) . . ?
O2 Ag8 Ag21 149.8(4) . . ?
O2 Ag8 Ag23 121.1(4) . . ?
O2 Ag8 S3 116.5(4) . . ?
O2 Ag8 S9 97.7(4) . . ?
Ag10 Ag9 Ag8 87.73(6) 2_655 . ?
Ag10 Ag9 Ag8 144.83(6) . . ?
Ag10 Ag9 Ag10 62.10(5) . 2_655 ?
Ag10 Ag9 Ag11 60.98(4) . . ?
Ag11 Ag9 Ag8 89.18(5) . . ?
Ag11 Ag9 Ag10 60.02(4) . 2_655 ?
Ag12 Ag9 Ag8 121.39(6) . . ?
Ag12 Ag9 Ag10 57.78(4) . 2_655 ?
Ag12 Ag9 Ag10 58.79(4) . . ?
Ag12 Ag9 Ag11 107.03(5) . . ?
Ag12 Ag9 Ag13 58.78(4) . . ?
Ag12 Ag9 Ag17 58.61(4) . 2_655 ?
Ag12 Ag9 Ag21 59.05(4) . . ?
Ag13 Ag9 Ag8 96.90(5) . . ?
Ag13 Ag9 Ag10 108.51(5) . . ?
Ag13 Ag9 Ag10 107.12(5) . 2_655 ?
Ag13 Ag9 Ag11 165.68(6) . . ?
Ag17 Ag9 Ag8 154.02(6) 2_655 . ?
Ag17 Ag9 Ag10 60.26(4) 2_655 . ?
Ag17 Ag9 Ag10 108.98(5) 2_655 2_655 ?
Ag17 Ag9 Ag11 116.25(6) 2_655 . ?
Ag17 Ag9 Ag13 59.74(5) 2_655 . ?
Ag21 Ag9 Ag8 62.61(5) . . ?
Ag21 Ag9 Ag10 58.64(4) . 2_655 ?
Ag21 Ag9 Ag10 109.44(5) . . ?
Ag21 Ag9 Ag11 112.11(6) . . ?
Ag21 Ag9 Ag13 60.39(5) . . ?
Ag21 Ag9 Ag17 108.58(5) . 2_655 ?
S1 Ag9 Ag8 72.46(13) . . ?
S1 Ag9 Ag10 123.15(13) . . ?
S1 Ag9 Ag10 146.68(13) . 2_655 ?
S1 Ag9 Ag11 92.41(12) . . ?
S1 Ag9 Ag12 155.50(13) . . ?
S1 Ag9 Ag13 101.77(12) . . ?
S1 Ag9 Ag17 99.69(13) . 2_655 ?
S1 Ag9 Ag21 127.34(13) . . ?
Ag9 Ag10 Ag9 106.79(5) . 2_655 ?
Ag9 Ag10 Ag10 60.28(5) . 2_655 ?
Ag9 Ag10 Ag10 57.61(5) 2_655 2_655 ?
Ag9 Ag10 Ag11 110.59(6) 2_655 . ?
Ag9 Ag10 Ag11 60.80(4) . . ?
Ag9 Ag10 Ag11 113.00(6) . 2_655 ?
Ag9 Ag10 Ag17 59.83(4) . 2_655 ?
Ag9 Ag10 Ag18 94.72(6) . 2_655 ?
Ag9 Ag10 Ag18 145.30(6) 2_655 2_655 ?
Ag9 Ag10 Ag23 151.41(6) . 2_655 ?
Ag9 Ag10 Ag23 92.14(5) 2_655 2_655 ?
Ag11 Ag10 Ag9 59.92(4) 2_655 2_655 ?
Ag11 Ag10 Ag10 59.44(4) 2_655 2_655 ?
Ag11 Ag10 Ag10 59.38(4) . 2_655 ?
Ag11 Ag10 Ag11 65.28(5) 2_655 . ?
Ag11 Ag10 Ag18 135.01(6) 2_655 2_655 ?
Ag11 Ag10 Ag18 103.60(6) . 2_655 ?
Ag11 Ag10 Ag23 132.34(6) . 2_655 ?
Ag11 Ag10 Ag23 94.91(5) 2_655 2_655 ?
Ag12 Ag10 Ag9 58.38(3) . . ?
Ag12 Ag10 Ag9 57.38(3) . 2_655 ?
Ag12 Ag10 Ag10 57.02(3) . 2_655 ?
Ag12 Ag10 Ag11 106.63(5) . 2_655 ?
Ag12 Ag10 Ag11 106.58(5) . . ?
Ag12 Ag10 Ag17 58.33(4) . 2_655 ?
Ag12 Ag10 Ag18 118.15(6) . 2_655 ?
Ag12 Ag10 Ag21 59.02(4) . 2_655 ?
Ag12 Ag10 Ag23 120.83(5) . 2_655 ?
Ag17 Ag10 Ag9 107.90(5) 2_655 2_655 ?
Ag17 Ag10 Ag10 107.22(5) 2_655 2_655 ?
Ag17 Ag10 Ag11 115.70(5) 2_655 . ?
Ag17 Ag10 Ag11 164.93(6) 2_655 2_655 ?
Ag17 Ag10 Ag18 60.06(5) 2_655 2_655 ?
Ag17 Ag10 Ag23 94.40(5) 2_655 2_655 ?
Ag18 Ag10 Ag10 153.96(7) 2_655 2_655 ?
Ag18 Ag10 Ag23 59.25(5) 2_655 2_655 ?
Ag21 Ag10 Ag9 58.91(4) 2_655 2_655 ?
Ag21 Ag10 Ag9 109.80(5) 2_655 . ?
Ag21 Ag10 Ag10 106.00(5) 2_655 2_655 ?
Ag21 Ag10 Ag11 164.85(6) 2_655 . ?
Ag21 Ag10 Ag11 112.25(5) 2_655 2_655 ?
Ag21 Ag10 Ag17 62.49(4) 2_655 2_655 ?
Ag21 Ag10 Ag18 88.53(6) 2_655 2_655 ?
Ag21 Ag10 Ag23 61.82(5) 2_655 2_655 ?
Ag23 Ag10 Ag10 146.74(7) 2_655 2_655 ?
S4 Ag10 Ag9 155.33(12) 2_655 2_655 ?
S4 Ag10 Ag9 80.10(11) 2_655 . ?
S4 Ag10 Ag10 110.32(12) 2_655 2_655 ?
S4 Ag10 Ag11 51.34(12) 2_655 . ?
S4 Ag10 Ag11 95.47(12) 2_655 2_655 ?
S4 Ag10 Ag12 137.82(11) 2_655 . ?
S4 Ag10 Ag17 96.09(12) 2_655 2_655 ?
S4 Ag10 Ag18 53.75(12) 2_655 2_655 ?
S4 Ag10 Ag21 142.11(13) 2_655 2_655 ?
S4 Ag10 Ag23 91.62(12) 2_655 2_655 ?
Ag9 Ag11 Ag10 58.22(4) . . ?
Ag9 Ag11 Ag10 60.07(4) . 2_655 ?
Ag9 Ag11 Ag11 104.62(3) . 2_655 ?
Ag10 Ag11 Ag10 61.18(5) 2_655 . ?
Ag10 Ag11 Ag11 57.39(4) 2_655 2_655 ?
Ag10 Ag11 Ag11 57.33(4) . 2_655 ?
S3 Ag11 Ag9 73.80(11) . . ?
S3 Ag11 Ag10 121.48(11) . . ?
S3 Ag11 Ag10 66.97(11) . 2_655 ?
S3 Ag11 Ag11 112.77(13) . 2_655 ?
S3 Ag11 S4 147.68(17) . 2_655 ?
S4 Ag11 Ag9 80.66(12) 2_655 . ?
S4 Ag11 Ag10 55.45(11) 2_655 . ?
S4 Ag11 Ag10 116.18(12) 2_655 2_655 ?
S4 Ag11 Ag11 92.43(12) 2_655 2_655 ?
O7 Ag11 Ag9 172.4(4) . . ?
O7 Ag11 Ag10 115.6(4) . 2_655 ?
O7 Ag11 Ag10 126.4(3) . . ?
O7 Ag11 Ag11 76.1(3) . 2_655 ?
O7 Ag11 S3 98.9(4) . . ?
O7 Ag11 S4 106.9(4) . 2_655 ?
Ag9 Ag12 Ag9 116.59(7) . 2_655 ?
Ag9 Ag12 Ag10 62.84(4) 2_655 2_655 ?
Ag9 Ag12 Ag10 64.84(5) 2_655 . ?
Ag9 Ag12 Ag10 62.84(4) . . ?
Ag9 Ag12 Ag10 64.84(5) . 2_655 ?
Ag9 Ag12 Ag13 62.81(4) . . ?
Ag9 Ag12 Ag13 178.95(5) . 2_655 ?
Ag9 Ag12 Ag13 62.81(4) 2_655 2_655 ?
Ag9 Ag12 Ag13 178.95(5) 2_655 . ?
Ag9 Ag12 Ag16 118.40(4) 2_655 2_655 ?
Ag9 Ag12 Ag16 115.11(4) 2_655 . ?
Ag9 Ag12 Ag16 118.40(4) . . ?
Ag9 Ag12 Ag16 115.11(4) . 2_655 ?
Ag9 Ag12 Ag17 118.15(5) . . ?
Ag9 Ag12 Ag17 118.15(5) 2_655 2_655 ?
Ag9 Ag12 Ag17 62.89(4) 2_655 . ?
Ag9 Ag12 Ag17 62.89(4) . 2_655 ?
Ag9 Ag12 Ag21 116.15(5) 2_655 . ?
Ag9 Ag12 Ag21 116.15(5) . 2_655 ?
Ag9 Ag12 Ag21 62.35(4) 2_655 2_655 ?
Ag9 Ag12 Ag21 62.36(4) . . ?
Ag10 Ag12 Ag10 65.97(6) . 2_655 ?
Ag10 Ag12 Ag16 177.97(5) . . ?
Ag10 Ag12 Ag16 115.92(4) 2_655 . ?
Ag10 Ag12 Ag16 177.98(5) 2_655 2_655 ?
Ag10 Ag12 Ag16 115.92(4) . 2_655 ?
Ag10 Ag12 Ag21 62.01(4) 2_655 . ?
Ag10 Ag12 Ag21 62.01(4) . 2_655 ?
Ag10 Ag12 Ag21 115.61(6) . . ?
Ag10 Ag12 Ag21 115.62(6) 2_655 2_655 ?
Ag13 Ag12 Ag10 116.16(4) 2_655 . ?
Ag13 Ag12 Ag10 115.19(4) 2_655 2_655 ?
Ag13 Ag12 Ag10 115.19(4) . . ?
Ag13 Ag12 Ag10 116.16(4) . 2_655 ?
Ag13 Ag12 Ag13 117.80(8) 2_655 . ?
Ag13 Ag12 Ag16 64.90(5) . . ?
Ag13 Ag12 Ag16 62.59(5) 2_655 . ?
Ag13 Ag12 Ag16 62.59(5) . 2_655 ?
Ag13 Ag12 Ag16 64.90(5) 2_655 2_655 ?
Ag13 Ag12 Ag21 118.64(5) . 2_655 ?
Ag13 Ag12 Ag21 62.84(4) . . ?
Ag13 Ag12 Ag21 118.64(5) 2_655 . ?
Ag13 Ag12 Ag21 62.84(4) 2_655 2_655 ?
Ag16 Ag12 Ag16 62.20(7) 2_655 . ?
Ag17 Ag12 Ag10 118.62(6) 2_655 2_655 ?
Ag17 Ag12 Ag10 118.61(6) . . ?
Ag17 Ag12 Ag10 63.04(4) 2_655 . ?
Ag17 Ag12 Ag10 63.04(4) . 2_655 ?
Ag17 Ag12 Ag13 62.49(4) 2_655 . ?
Ag17 Ag12 Ag13 116.50(5) 2_655 2_655 ?
Ag17 Ag12 Ag13 116.50(5) . . ?
Ag17 Ag12 Ag13 62.49(4) . 2_655 ?
Ag17 Ag12 Ag16 62.50(4) 2_655 2_655 ?
Ag17 Ag12 Ag16 62.50(4) . . ?
Ag17 Ag12 Ag16 115.83(6) 2_655 . ?
Ag17 Ag12 Ag16 115.83(6) . 2_655 ?
Ag17 Ag12 Ag17 178.26(8) 2_655 . ?
Ag17 Ag12 Ag21 65.19(4) 2_655 2_655 ?
Ag17 Ag12 Ag21 114.85(4) . 2_655 ?
Ag17 Ag12 Ag21 65.19(4) . . ?
Ag17 Ag12 Ag21 114.85(4) 2_655 . ?
Ag21 Ag12 Ag16 66.32(4) 2_655 2_655 ?
Ag21 Ag12 Ag16 116.07(5) 2_655 . ?
Ag21 Ag12 Ag16 116.07(6) . 2_655 ?
Ag21 Ag12 Ag16 66.32(4) . . ?
Ag21 Ag12 Ag21 177.47(8) 2_655 . ?
Ag9 Ag13 Ag14 115.50(6) . . ?
Ag9 Ag13 Ag16 108.57(5) . . ?
Ag9 Ag13 Ag16 108.36(5) . 2_655 ?
Ag9 Ag13 Ag19 154.33(8) . 2_655 ?
Ag9 Ag13 Ag21 59.51(5) . . ?
Ag12 Ag13 Ag9 58.41(4) . . ?
Ag12 Ag13 Ag14 106.89(6) . . ?
Ag12 Ag13 Ag16 58.85(4) . 2_655 ?
Ag12 Ag13 Ag16 57.69(4) . . ?
Ag12 Ag13 Ag17 58.62(4) . 2_655 ?
Ag12 Ag13 Ag19 120.48(6) . 2_655 ?
Ag12 Ag13 Ag21 58.62(4) . . ?
Ag14 Ag13 Ag16 60.21(5) . . ?
Ag14 Ag13 Ag19 89.81(6) . 2_655 ?
Ag16 Ag13 Ag14 112.55(6) 2_655 . ?
Ag16 Ag13 Ag16 58.64(6) 2_655 . ?
Ag16 Ag13 Ag19 61.94(5) 2_655 2_655 ?
Ag16 Ag13 Ag19 87.12(6) . 2_655 ?
Ag16 Ag13 Ag21 109.37(5) 2_655 . ?
Ag17 Ag13 Ag9 60.12(4) 2_655 . ?
Ag17 Ag13 Ag14 165.41(6) 2_655 . ?
Ag17 Ag13 Ag16 59.97(5) 2_655 2_655 ?
Ag17 Ag13 Ag16 106.81(5) 2_655 . ?
Ag17 Ag13 Ag19 96.41(6) 2_655 2_655 ?
Ag17 Ag13 Ag21 108.17(5) 2_655 . ?
Ag21 Ag13 Ag14 60.95(5) . . ?
Ag21 Ag13 Ag16 62.32(5) . . ?
Ag21 Ag13 Ag19 144.90(7) . 2_655 ?
S2 Ag13 Ag9 98.89(12) . . ?
S2 Ag13 Ag12 155.31(13) . . ?
S2 Ag13 Ag14 91.18(13) . . ?
S2 Ag13 Ag16 129.65(14) . 2_655 ?
S2 Ag13 Ag16 146.61(13) . . ?
S2 Ag13 Ag17 103.15(14) . 2_655 ?
S2 Ag13 Ag19 75.12(13) . 2_655 ?
S2 Ag13 Ag21 120.94(13) . . ?
Ag13 Ag14 Ag16 60.40(5) . . ?
Ag13 Ag14 Ag21 58.56(5) . . ?
Ag13 Ag14 Ag22 105.29(6) . . ?
Ag16 Ag14 Ag22 57.41(5) . . ?
Ag21 Ag14 Ag16 61.57(4) . . ?
Ag21 Ag14 Ag22 57.98(5) . . ?
S6 Ag14 Ag13 73.22(13) . . ?
S6 Ag14 Ag16 66.13(12) . . ?
S6 Ag14 Ag21 120.98(12) . . ?
S6 Ag14 Ag22 111.90(15) . . ?
S6 Ag14 S9 148.1(2) . . ?
S9 Ag14 Ag13 81.21(13) . . ?
S9 Ag14 Ag16 116.67(11) . . ?
S9 Ag14 Ag21 55.49(11) . . ?
S9 Ag14 Ag22 92.79(14) . . ?
O3 Ag14 Ag13 169.2(4) . . ?
O3 Ag14 Ag16 111.1(4) . . ?
O3 Ag14 Ag21 125.0(4) . . ?
O3 Ag14 Ag22 72.5(4) . . ?
O3 Ag14 S6 97.5(4) . . ?
O3 Ag14 S9 109.3(4) . . ?
Ag16 Ag15 Ag16 58.18(7) . 2_655 ?
Ag19 Ag15 Ag16 61.96(5) 2_655 2_655 ?
Ag19 Ag15 Ag16 88.88(7) . 2_655 ?
Ag19 Ag15 Ag16 61.96(5) . . ?
Ag19 Ag15 Ag16 88.88(7) 2_655 . ?
Ag19 Ag15 Ag19 147.46(11) 2_655 . ?
S6 Ag15 Ag16 91.30(13) . 2_655 ?
S6 Ag15 Ag16 66.59(14) . . ?
S6 Ag15 Ag16 91.30(13) 2_655 . ?
S6 Ag15 Ag16 66.59(14) 2_655 2_655 ?
S6 Ag15 Ag19 118.44(16) . . ?
S6 Ag15 Ag19 53.39(16) 2_655 . ?
S6 Ag15 Ag19 118.45(16) 2_655 2_655 ?
S6 Ag15 Ag19 53.39(16) . 2_655 ?
S6 Ag15 S6 155.3(2) 2_655 . ?
S6 Ag15 O0AA 101.2(12) . . ?
S6 Ag15 O0AA 101.7(11) 2_655 . ?
S6 Ag15 C0AA 98.8(19) 2_655 . ?
S6 Ag15 C0AA 105.6(19) . . ?
O0AA Ag15 Ag16 130.3(10) . 2_655 ?
O0AA Ag15 Ag16 166.6(10) . . ?
O0AA Ag15 Ag19 124.0(12) . . ?
O0AA Ag15 Ag19 87.7(12) . 2_655 ?
O0AA Ag15 C0AA 32.1(8) . . ?
C0AA Ag15 Ag16 143.0(9) . . ?
C0AA Ag15 Ag16 157.0(15) . 2_655 ?
C0AA Ag15 Ag19 96.3(11) . . ?
C0AA Ag15 Ag19 116.2(12) . 2_655 ?
Ag12 Ag16 Ag13 58.56(3) . 2_655 ?
Ag12 Ag16 Ag13 57.41(4) . . ?
Ag12 Ag16 Ag14 106.00(5) . . ?
Ag12 Ag16 Ag15 119.81(6) . . ?
Ag12 Ag16 Ag16 58.90(3) . 2_655 ?
Ag12 Ag16 Ag17 58.47(4) . . ?
Ag12 Ag16 Ag19 119.02(6) . . ?
Ag12 Ag16 Ag21 56.74(4) . . ?
Ag12 Ag16 Ag22 106.84(5) . . ?
Ag13 Ag16 Ag13 108.10(5) 2_655 . ?
Ag13 Ag16 Ag14 164.52(6) 2_655 . ?
Ag13 Ag16 Ag15 93.54(5) 2_655 . ?
Ag13 Ag16 Ag19 144.89(7) . . ?
Ag13 Ag16 Ag19 60.76(5) 2_655 . ?
Ag13 Ag16 Ag21 107.27(5) 2_655 . ?
Ag13 Ag16 Ag21 57.42(4) . . ?
Ag13 Ag16 Ag22 116.17(6) 2_655 . ?
Ag14 Ag16 Ag13 59.39(5) . . ?
Ag14 Ag16 Ag19 134.70(7) . . ?
Ag14 Ag16 Ag21 59.04(4) . . ?
Ag15 Ag16 Ag13 91.61(5) . . ?
Ag15 Ag16 Ag14 95.80(5) . . ?
Ag15 Ag16 Ag19 58.48(5) . . ?
Ag15 Ag16 Ag21 146.51(6) . . ?
Ag15 Ag16 Ag22 133.07(6) . . ?
Ag16 Ag16 Ag13 59.03(5) 2_655 . ?
Ag16 Ag16 Ag13 62.33(5) 2_655 2_655 ?
Ag16 Ag16 Ag14 112.17(8) 2_655 . ?
Ag16 Ag16 Ag15 60.91(3) 2_655 . ?
Ag16 Ag16 Ag17 109.60(5) 2_655 . ?
Ag16 Ag16 Ag19 88.43(6) 2_655 . ?
Ag16 Ag16 Ag21 105.71(5) 2_655 . ?
Ag16 Ag16 Ag22 164.94(4) 2_655 . ?
Ag17 Ag16 Ag13 107.00(5) . . ?
Ag17 Ag16 Ag13 59.80(4) . 2_655 ?
Ag17 Ag16 Ag14 112.86(6) . . ?
Ag17 Ag16 Ag15 150.88(5) . . ?
Ag17 Ag16 Ag19 95.56(7) . . ?
Ag17 Ag16 Ag21 60.52(4) . . ?
Ag17 Ag16 Ag22 61.30(5) . . ?
Ag19 Ag16 Ag21 154.99(8) . . ?
Ag22 Ag16 Ag13 110.39(6) . . ?
Ag22 Ag16 Ag14 64.96(6) . . ?
Ag22 Ag16 Ag19 103.94(7) . . ?
Ag22 Ag16 Ag21 59.68(5) . . ?
S7 Ag16 Ag12 138.32(14) . . ?
S7 Ag16 Ag13 155.10(13) . . ?
S7 Ag16 Ag13 96.24(13) . 2_655 ?
S7 Ag16 Ag14 95.73(13) . . ?
S7 Ag16 Ag15 92.04(13) . . ?
S7 Ag16 Ag16 141.93(13) . 2_655 ?
S7 Ag16 Ag17 80.48(14) . . ?
S7 Ag16 Ag19 53.63(13) . . ?
S7 Ag16 Ag21 110.86(13) . . ?
S7 Ag16 Ag22 51.59(13) . . ?
Ag9 Ag17 Ag10 59.92(4) 2_655 2_655 ?
Ag9 Ag17 Ag18 95.76(6) 2_655 . ?
Ag9 Ag17 Ag21 106.42(5) 2_655 . ?
Ag9 Ag17 Ag22 165.21(7) 2_655 . ?
Ag10 Ag17 Ag18 61.62(5) 2_655 . ?
Ag10 Ag17 Ag21 58.14(4) 2_655 . ?
Ag10 Ag17 Ag22 111.93(5) 2_655 . ?
Ag12 Ag17 Ag9 58.50(4) . 2_655 ?
Ag12 Ag17 Ag10 58.63(5) . 2_655 ?
Ag12 Ag17 Ag13 58.88(4) . 2_655 ?
Ag12 Ag17 Ag16 59.02(5) . . ?
Ag12 Ag17 Ag18 120.01(6) . . ?
Ag12 Ag17 Ag21 57.57(4) . . ?
Ag12 Ag17 Ag22 106.90(6) . . ?
Ag13 Ag17 Ag9 60.14(5) 2_655 2_655 ?
Ag13 Ag17 Ag10 108.56(6) 2_655 2_655 ?
Ag13 Ag17 Ag16 60.23(5) 2_655 . ?
Ag13 Ag17 Ag18 153.56(6) 2_655 . ?
Ag13 Ag17 Ag21 109.09(6) 2_655 . ?
Ag13 Ag17 Ag22 116.14(6) 2_655 . ?
Ag16 Ag17 Ag9 108.59(6) . 2_655 ?
Ag16 Ag17 Ag10 109.31(6) . 2_655 ?
Ag16 Ag17 Ag18 144.93(6) . . ?
Ag16 Ag17 Ag21 62.43(4) . . ?
Ag16 Ag17 Ag22 60.83(5) . . ?
Ag18 Ag17 Ag21 87.04(5) . . ?
Ag18 Ag17 Ag22 89.93(6) . . ?
Ag22 Ag17 Ag21 60.15(5) . . ?
S8 Ag17 Ag9 103.04(13) . 2_655 ?
S8 Ag17 Ag10 128.53(15) . 2_655 ?
S8 Ag17 Ag12 156.00(14) . . ?
S8 Ag17 Ag13 99.54(14) . 2_655 ?
S8 Ag17 Ag16 122.07(14) . . ?
S8 Ag17 Ag18 73.97(14) . . ?
S8 Ag17 Ag21 146.30(14) . . ?
S8 Ag17 Ag22 91.64(14) . . ?
Ag7 Ag18 Ag10 94.38(7) 2_655 2_655 ?
Ag7 Ag18 Ag17 74.02(7) 2_655 . ?
Ag7 Ag18 Ag23 154.77(9) 2_655 . ?
Ag17 Ag18 Ag10 58.32(5) . 2_655 ?
Ag17 Ag18 Ag23 94.27(6) . . ?
Ag23 Ag18 Ag10 60.77(5) . 2_655 ?
S4 Ag18 Ag7 66.58(12) . 2_655 ?
S4 Ag18 Ag10 54.23(11) . 2_655 ?
S4 Ag18 Ag17 95.14(13) . . ?
S4 Ag18 Ag23 93.00(12) . . ?
S5 Ag18 Ag7 138.98(14) . 2_655 ?
S5 Ag18 Ag10 89.42(14) . 2_655 ?
S5 Ag18 Ag17 73.53(13) . . ?
S5 Ag18 Ag23 51.96(12) . . ?
S5 Ag18 S4 140.72(18) . . ?
O9 Ag18 Ag7 78.4(5) . 2_655 ?
O9 Ag18 Ag10 154.2(6) . 2_655 ?
O9 Ag18 Ag17 139.3(5) . . ?
O9 Ag18 Ag23 121.7(5) . . ?
O9 Ag18 S4 100.7(6) . . ?
O9 Ag18 S5 112.4(5) . . ?
Ag13 Ag19 Ag16 57.31(5) 2_655 . ?
Ag15 Ag19 Ag13 92.05(7) . 2_655 ?
Ag15 Ag19 Ag16 59.56(6) . . ?
Ag20 Ag19 Ag13 72.83(8) . 2_655 ?
Ag20 Ag19 Ag15 151.73(9) . . ?
Ag20 Ag19 Ag16 92.32(8) . . ?
S6 Ag19 Ag13 72.27(13) 2_655 2_655 ?
S6 Ag19 Ag15 52.56(12) 2_655 . ?
S6 Ag19 Ag16 89.14(13) 2_655 . ?
S6 Ag19 Ag20 137.21(15) 2_655 . ?
S6 Ag19 S7 140.58(19) 2_655 . ?
S7 Ag19 Ag13 93.65(13) . 2_655 ?
S7 Ag19 Ag15 92.81(14) . . ?
S7 Ag19 Ag16 53.62(13) . . ?
S7 Ag19 Ag20 65.31(15) . . ?
O5 Ag19 Ag13 142.3(6) . 2_655 ?
O5 Ag19 Ag15 122.1(5) . . ?
O5 Ag19 Ag16 152.0(6) . . ?
O5 Ag19 Ag20 80.9(5) . . ?
O5 Ag19 S6 114.3(6) . 2_655 ?
O5 Ag19 S7 99.5(6) . . ?
Ag1 Ag20 S7 150.84(19) 2_655 . ?
Ag19 Ag20 Ag1 134.3(3) . 2_655 ?
Ag19 Ag20 S7 52.29(13) . . ?
S2 Ag20 Ag1 58.6(3) 2_655 2_655 ?
S2 Ag20 Ag19 76.00(14) 2_655 . ?
S2 Ag20 S7 120.23(19) 2_655 . ?
S8 Ag20 Ag1 60.9(2) . 2_655 ?
S8 Ag20 Ag19 130.36(17) . . ?
S8 Ag20 S2 100.89(19) . 2_655 ?
S8 Ag20 S7 93.16(18) . . ?
O6 Ag20 Ag1 112.4(6) . 2_655 ?
O6 Ag20 Ag19 81.0(5) . . ?
O6 Ag20 S2 103.5(6) . 2_655 ?
O6 Ag20 S7 96.5(6) . . ?
O6 Ag20 S8 144.4(6) . . ?
Ag9 Ag21 Ag8 60.97(5) . . ?
Ag9 Ag21 Ag13 60.11(5) . . ?
Ag9 Ag21 Ag14 115.61(6) . . ?
Ag9 Ag21 Ag16 107.42(6) . . ?
Ag9 Ag21 Ag17 108.23(5) . . ?
Ag9 Ag21 Ag22 164.91(6) . . ?
Ag9 Ag21 Ag23 94.11(5) . . ?
Ag10 Ag21 Ag8 88.84(5) 2_655 . ?
Ag10 Ag21 Ag9 62.45(4) 2_655 . ?
Ag10 Ag21 Ag13 109.91(6) 2_655 . ?
Ag10 Ag21 Ag14 164.74(6) 2_655 . ?
Ag10 Ag21 Ag16 105.93(5) 2_655 . ?
Ag10 Ag21 Ag17 59.37(4) 2_655 . ?
Ag10 Ag21 Ag22 112.76(6) 2_655 . ?
Ag10 Ag21 Ag23 61.69(5) 2_655 . ?
Ag12 Ag21 Ag8 119.30(6) . . ?
Ag12 Ag21 Ag9 58.59(4) . . ?
Ag12 Ag21 Ag10 58.98(5) . 2_655 ?
Ag12 Ag21 Ag13 58.54(4) . . ?
Ag12 Ag21 Ag14 106.45(6) . . ?
Ag12 Ag21 Ag16 56.94(4) . . ?
Ag12 Ag21 Ag17 57.24(4) . . ?
Ag12 Ag21 Ag22 106.39(5) . . ?
Ag12 Ag21 Ag23 120.66(6) . . ?
Ag13 Ag21 Ag8 95.69(6) . . ?
Ag13 Ag21 Ag14 60.48(5) . . ?
Ag13 Ag21 Ag16 60.26(5) . . ?
Ag13 Ag21 Ag17 106.50(5) . . ?
Ag13 Ag21 Ag22 112.24(6) . . ?
Ag13 Ag21 Ag23 151.45(6) . . ?
Ag14 Ag21 Ag8 103.46(5) . . ?
Ag14 Ag21 Ag16 59.39(4) . . ?
Ag14 Ag21 Ag17 110.12(5) . . ?
Ag14 Ag21 Ag22 64.82(5) . . ?
Ag14 Ag21 Ag23 132.64(6) . . ?
Ag16 Ag21 Ag8 154.72(6) . . ?
Ag17 Ag21 Ag8 145.72(6) . . ?
Ag17 Ag21 Ag16 57.06(4) . . ?
Ag17 Ag21 Ag22 59.86(5) . . ?
Ag17 Ag21 Ag23 92.52(5) . . ?
Ag22 Ag21 Ag8 134.12(6) . . ?
Ag22 Ag21 Ag16 58.96(5) . . ?
Ag22 Ag21 Ag23 95.62(6) . . ?
Ag23 Ag21 Ag8 58.50(5) . . ?
Ag23 Ag21 Ag16 146.68(6) . . ?
S9 Ag21 Ag8 53.22(11) . . ?
S9 Ag21 Ag9 96.11(13) . . ?
S9 Ag21 Ag10 141.94(11) . 2_655 ?
S9 Ag21 Ag12 138.20(14) . . ?
S9 Ag21 Ag13 80.34(13) . . ?
S9 Ag21 Ag14 51.59(10) . . ?
S9 Ag21 Ag16 110.63(11) . . ?
S9 Ag21 Ag17 154.98(13) . . ?
S9 Ag21 Ag22 95.16(13) . . ?
S9 Ag21 Ag23 91.42(12) . . ?
Ag16 Ag22 Ag14 57.63(5) . . ?
Ag16 Ag22 Ag17 57.86(5) . . ?
Ag16 Ag22 Ag21 61.36(5) . . ?
Ag17 Ag22 Ag14 104.34(6) . . ?
Ag17 Ag22 Ag21 59.99(4) . . ?
Ag21 Ag22 Ag14 57.19(5) . . ?
S5 Ag22 Ag14 111.41(14) . . ?
S5 Ag22 Ag16 120.38(14) . . ?
S5 Ag22 Ag17 73.45(12) . . ?
S5 Ag22 Ag21 65.61(14) . . ?
S7 Ag22 Ag14 92.88(15) . . ?
S7 Ag22 Ag16 55.31(14) . . ?
S7 Ag22 Ag17 80.33(13) . . ?
S7 Ag22 Ag21 116.21(15) . . ?
S7 Ag22 S5 147.73(19) . . ?
O4 Ag22 Ag14 77.0(5) . . ?
O4 Ag22 Ag16 127.4(5) . . ?
O4 Ag22 Ag17 172.3(5) . . ?
O4 Ag22 Ag21 116.1(5) . . ?
O4 Ag22 S5 98.9(5) . . ?
O4 Ag22 S7 107.3(5) . . ?
Ag8 Ag23 Ag10 87.54(6) . 2_655 ?
Ag8 Ag23 Ag18 143.83(7) . . ?
Ag8 Ag23 Ag21 61.32(5) . . ?
Ag10 Ag23 Ag21 56.50(4) 2_655 . ?
Ag18 Ag23 Ag10 59.97(5) . 2_655 ?
Ag18 Ag23 Ag21 85.96(6) . . ?
S3 Ag23 Ag8 52.97(11) . . ?
S3 Ag23 Ag10 66.02(11) . 2_655 ?
S3 Ag23 Ag18 117.14(12) . . ?
S3 Ag23 Ag21 89.88(12) . . ?
S3 Ag23 S5 152.60(17) . . ?
S3 Ag23 O11 108.3(5) . . ?
S3 Ag23 O12 89.9(4) . . ?
S5 Ag23 Ag8 116.70(15) . . ?
S5 Ag23 Ag10 89.71(12) . 2_655 ?
S5 Ag23 Ag18 53.33(13) . . ?
S5 Ag23 Ag21 65.13(14) . . ?
S5 Ag23 O11 92.9(5) . . ?
S5 Ag23 O12 111.5(4) . . ?
O11 Ag23 Ag8 143.7(5) . . ?
O11 Ag23 Ag10 114.6(5) . 2_655 ?
O11 Ag23 Ag18 70.5(5) . . ?
O11 Ag23 Ag21 154.8(5) . . ?
O11 Ag23 O12 79.0(6) . . ?
O12 Ag23 Ag8 71.1(4) . . ?
O12 Ag23 Ag10 154.8(4) . 2_655 ?
O12 Ag23 Ag18 144.0(4) . . ?
O12 Ag23 Ag21 119.3(4) . . ?
Ag2 S1 Ag5 60.9(3) . . ?
Ag7 S1 Ag2 82.1(3) . . ?
Ag7 S1 Ag5 138.8(2) . . ?
Ag7 S1 Ag9 93.75(17) . . ?
Ag9 S1 Ag2 119.7(2) . . ?
Ag9 S1 Ag5 89.81(17) . . ?
C11 S1 Ag2 120.6(8) . . ?
C11 S1 Ag5 108.6(8) . . ?
C11 S1 Ag7 105.6(8) . . ?
C11 S1 Ag9 118.4(8) . . ?
Ag5 S2 Ag1 79.1(4) . . ?
Ag5 S2 Ag2 63.6(3) . . ?
Ag5 S2 Ag13 95.20(18) . . ?
Ag5 S2 Ag20 141.8(2) . 2_655 ?
Ag13 S2 Ag1 115.1(2) . . ?
Ag13 S2 Ag2 118.6(2) . . ?
Ag13 S2 Ag20 85.59(15) . 2_655 ?
Ag20 S2 Ag1 66.4(4) 2_655 . ?
Ag20 S2 Ag2 82.6(3) 2_655 . ?
C18 S2 Ag1 122.9(8) . . ?
C18 S2 Ag2 120.1(8) . . ?
C18 S2 Ag5 105.0(8) . . ?
C18 S2 Ag13 121.0(8) . . ?
C18 S2 Ag20 107.2(8) . 2_655 ?
Ag11 S3 Ag8 118.8(2) . . ?
Ag11 S3 Ag23 131.25(18) . . ?
Ag23 S3 Ag8 75.01(14) . . ?
C25 S3 Ag8 115.3(7) . . ?
C25 S3 Ag11 108.2(7) . . ?
C25 S3 Ag23 105.1(7) . . ?
Ag11 S4 Ag10 73.22(14) 2_655 2_655 ?
Ag11 S4 Ag18 141.7(2) 2_655 . ?
Ag18 S4 Ag10 72.02(13) . 2_655 ?
C32 S4 Ag10 116.2(6) . 2_655 ?
C32 S4 Ag11 106.4(9) . 2_655 ?
C32 S4 Ag18 102.9(9) . . ?
Ag22 S5 Ag18 117.4(2) . . ?
Ag23 S5 Ag18 74.71(15) . . ?
Ag23 S5 Ag22 132.9(3) . . ?
C39 S5 Ag18 116.0(8) . . ?
C39 S5 Ag22 109.7(8) . . ?
C39 S5 Ag23 102.6(8) . . ?
Ag14 S6 Ag19 119.2(2) . 2_655 ?
Ag15 S6 Ag14 130.9(2) . . ?
Ag15 S6 Ag19 74.05(16) . 2_655 ?
C46 S6 Ag14 109.0(8) . . ?
C46 S6 Ag15 104.3(7) . . ?
C46 S6 Ag19 115.9(8) . 2_655 ?
Ag16 S7 Ag19 72.75(16) . . ?
Ag16 S7 Ag20 101.31(18) . . ?
Ag19 S7 Ag20 62.40(14) . . ?
Ag22 S7 Ag16 73.10(15) . . ?
Ag22 S7 Ag19 142.8(2) . . ?
Ag22 S7 Ag20 111.1(2) . . ?
C53 S7 Ag16 109.7(19) . . ?
C53 S7 Ag19 95(3) . . ?
C53 S7 Ag20 133(4) . . ?
C53 S7 Ag22 111(4) . . ?
C54 S7 Ag16 115.0(8) . . ?
C54 S7 Ag19 100(2) . . ?
C54 S7 Ag20 133(2) . . ?
C54 S7 Ag22 108(3) . . ?
Ag7 S8 Ag1 71.2(3) 2_655 2_655 ?
Ag17 S8 Ag1 115.5(3) . 2_655 ?
Ag17 S8 Ag7 88.33(17) . 2_655 ?
Ag20 S8 Ag1 68.9(3) . 2_655 ?
Ag20 S8 Ag7 135.9(2) . 2_655 ?
Ag20 S8 Ag17 92.2(2) . . ?
C67 S8 Ag1 125.3(9) . 2_655 ?
C67 S8 Ag7 112.9(9) . 2_655 ?
C67 S8 Ag17 119.1(9) . . ?
C67 S8 Ag20 105.1(8) . . ?
Ag8 S9 Ag5 63.85(13) . . ?
Ag8 S9 Ag21 73.49(12) . . ?
Ag14 S9 Ag5 111.6(2) . . ?
Ag14 S9 Ag8 143.09(19) . . ?
Ag14 S9 Ag21 72.92(12) . . ?
Ag21 S9 Ag5 105.33(18) . . ?
C98 S9 Ag5 131.0(8) . . ?
C98 S9 Ag8 98.6(7) . . ?
C98 S9 Ag14 108.2(8) . . ?
C98 S9 Ag21 112.9(8) . . ?
C80 P2 Ag2 119.8(7) . . ?
C80 P2 C86 104.1(10) . . ?
C86 P2 Ag2 118.4(7) . . ?
C92 P2 Ag2 103.9(8) . . ?
C92 P2 C80 104.5(10) . . ?
C92 P2 C86 104.3(10) . . ?
C1 O1 Ag5 120.0(12) . . ?
C1 O2 Ag8 123.0(12) . . ?
O1 C1 O2 134.2(16) . . ?
O1 C1 C2 112.2(13) . . ?
O2 C1 C2 113.6(14) . . ?
F1 C2 F2 104.3(17) . . ?
F1 C2 F3 105.9(18) . . ?
F1 C2 C1 113.9(11) . . ?
F2 C2 C1 114.9(11) . . ?
F3 C2 F2 101.1(17) . . ?
F3 C2 C1 115.3(11) . . ?
F1A C2 C1 114.5(14) . . ?
F1A C2 F2A 94(4) . . ?
F2A C2 C1 112(3) . . ?
F3A C2 C1 118(2) . . ?
F3A C2 F1A 114(3) . . ?
F3A C2 F2A 102(4) . . ?
C3 O3 Ag14 125.9(15) . . ?
C3 O4 Ag22 117.8(16) . . ?
O3 C3 O4 134(2) . . ?
O3 C3 C4 113.9(19) . . ?
O4 C3 C4 112.5(19) . . ?
F4 C4 F5 99(2) . . ?
F4 C4 F6 109(2) . . ?
F4 C4 C3 116(2) . . ?
F5 C4 C3 114(2) . . ?
F6 C4 F5 97(2) . . ?
F6 C4 C3 118.3(19) . . ?
C5 O5 Ag19 121.1(16) . . ?
C5 O6 Ag20 122.6(16) . . ?
O5 C5 O6 134(2) . . ?
O5 C5 C6 114(2) . . ?
O6 C5 C6 112.0(19) . . ?
F7 C6 F8 102(2) . . ?
F7 C6 F9 107(2) . . ?
F7 C6 C5 116.3(19) . . ?
F8 C6 C5 115(2) . . ?
F9 C6 F8 98(2) . . ?
F9 C6 C5 117(2) . . ?
C9 O9 Ag18 123.8(16) . . ?
C9 O10 Ag7 121.6(16) . 2_655 ?
O9 C9 C10 116.3(19) . . ?
O10 C9 O9 134(2) . . ?
O10 C9 C10 109.7(19) . . ?
F13 C10 F14 102(2) . . ?
F13 C10 F15 105(2) . . ?
F13 C10 C9 115(2) . . ?
F14 C10 F15 100(2) . . ?
F14 C10 C9 115.5(18) . . ?
F15 C10 C9 117(2) . . ?
C0AA O0AA Ag15 78(2) . . ?
C7 O7 Ag11 123.8(12) . . ?
C74 O11 Ag23 127(3) . . ?
C77 O12 Ag23 136(2) . . ?
C74 N1 C75 116(3) . . ?
C74 N1 C76 113(3) . . ?
C76 N1 C75 109(3) . . ?
C77 N2 C78 122(3) . . ?
C77 N2 C79 124(3) . . ?
C78 N2 C79 112(3) . . ?
O0AA C0AA Ag15 70(2) . . ?
O0AA C0AA O1AA 145(3) . . ?
O0AA C0AA C1AA 122(3) . . ?
O1AA C0AA Ag15 74.7(19) . . ?
O1AA C0AA C1AA 92.8(18) . . ?
C1AA C0AA Ag15 167(2) . . ?
F16 C1AA F17 95.4(19) . . ?
F16 C1AA F18 94.7(19) . . ?
F16 C1AA C0AA 136(4) . . ?
F17 C1AA F18 96(2) . . ?
F17 C1AA C0AA 103(3) . . ?
F18 C1AA C0AA 122(3) . . ?
O7 C7 O7 131(2) . 2_655 ?
O7 C7 C8 114.5(11) . . ?
O7 C7 C8 114.5(11) 2_655 . ?
F10 C8 F11 101.9(15) . . ?
F10 C8 C7 115.7(15) . . ?
F11 C8 C7 108.2(14) . . ?
F12 C8 F10 110.2(18) . . ?
F12 C8 F11 102.8(15) . . ?
F12 C8 C7 116.1(15) . . ?
S1 C11 H11A 108.9 . . ?
S1 C11 H11B 108.9 . . ?
H11A C11 H11B 107.7 . . ?
C12 C11 S1 113.2(15) . . ?
C12 C11 H11A 108.9 . . ?
C12 C11 H11B 108.9 . . ?
C14 C15 H15 120.0 . . ?
C14 C15 C16 120.0 . . ?
C16 C15 H15 120.0 . . ?
C15 C14 H14 120.0 . . ?
C15 C14 C13 120.0 . . ?
C13 C14 H14 120.0 . . ?
C14 C13 H13 120.0 . . ?
C12 C13 C14 120.0 . . ?
C12 C13 H13 120.0 . . ?
C13 C12 C11 118.9(15) . . ?
C17 C12 C11 121.1(15) . . ?
C17 C12 C13 120.0 . . ?
C12 C17 H17 120.0 . . ?
C12 C17 C16 120.0 . . ?
C16 C17 H17 120.0 . . ?
C15 C16 H16 120.0 . . ?
C17 C16 C15 120.0 . . ?
C17 C16 H16 120.0 . . ?
S2 C18 H18A 109.2 . . ?
S2 C18 H18B 109.2 . . ?
H18A C18 H18B 107.9 . . ?
C19 C18 S2 112.0(16) . . ?
C19 C18 H18A 109.2 . . ?
C19 C18 H18B 109.2 . . ?
C24 C23 H23 120.0 . . ?
C24 C23 C22 120.0 . . ?
C22 C23 H23 120.0 . . ?
C23 C24 H24 120.0 . . ?
C23 C24 C19 120.0 . . ?
C19 C24 H24 120.0 . . ?
C24 C19 C18 116.5(17) . . ?
C20 C19 C18 123.5(17) . . ?
C20 C19 C24 120.0 . . ?
C19 C20 H20 120.0 . . ?
C19 C20 C21 120.0 . . ?
C21 C20 H20 120.0 . . ?
C20 C21 H21 120.0 . . ?
C20 C21 C22 120.0 . . ?
C22 C21 H21 120.0 . . ?
C23 C22 H22 120.0 . . ?
C21 C22 C23 120.0 . . ?
C21 C22 H22 120.0 . . ?
S3 C25 H25A 109.0 . . ?
S3 C25 H25B 109.0 . . ?
H25A C25 H25B 107.8 . . ?
C26 C25 S3 112.9(14) . . ?
C26 C25 H25A 109.0 . . ?
C26 C25 H25B 109.0 . . ?
C27 C26 C25 120.9(19) . . ?
C31 C26 C25 120.8(18) . . ?
C31 C26 C27 118(2) . . ?
C26 C27 H27 119.4 . . ?
C28 C27 C26 121(2) . . ?
C28 C27 H27 119.4 . . ?
C27 C28 H28 119.4 . . ?
C29 C28 C27 121(2) . . ?
C29 C28 H28 119.4 . . ?
C28 C29 H29 120.8 . . ?
C28 C29 C30 118(2) . . ?
C30 C29 H29 120.8 . . ?
C29 C30 H30 119.7 . . ?
C29 C30 C31 121(2) . . ?
C31 C30 H30 119.7 . . ?
C26 C31 C30 120(2) . . ?
C26 C31 H31 119.8 . . ?
C30 C31 H31 119.8 . . ?
S4 C32 H32A 110.0 . . ?
S4 C32 H32B 110.0 . . ?
H32A C32 H32B 108.4 . . ?
C33 C32 S4 108.5(15) . . ?
C33 C32 H32A 110.0 . . ?
C33 C32 H32B 110.0 . . ?
C34 C33 C32 121(2) . . ?
C34 C33 C38 120.0 . . ?
C38 C33 C32 119(2) . . ?
C33 C34 H34 120.0 . . ?
C33 C34 C35 120.0 . . ?
C35 C34 H34 120.0 . . ?
C34 C35 H35 120.0 . . ?
C34 C35 C37 120.0 . . ?
C37 C35 H35 120.0 . . ?
C35 C37 H37 120.0 . . ?
C35 C37 C36 120.0 . . ?
C36 C37 H37 120.0 . . ?
C37 C36 H36 120.0 . . ?
C38 C36 C37 120.0 . . ?
C38 C36 H36 120.0 . . ?
C33 C38 H38 120.0 . . ?
C36 C38 C33 120.0 . . ?
C36 C38 H38 120.0 . . ?
S5 C39 H39A 109.5 . . ?
S5 C39 H39B 109.5 . . ?
H39A C39 H39B 108.1 . . ?
C40 C39 S5 110.8(15) . . ?
C40 C39 H39A 109.5 . . ?
C40 C39 H39B 109.5 . . ?
C41 C40 C39 121(2) . . ?
C41 C40 C45 120.0 . . ?
C45 C40 C39 119(2) . . ?
C40 C41 H41 120.0 . . ?
C42 C41 C40 120.0 . . ?
C42 C41 H41 120.0 . . ?
C41 C42 H42 120.0 . . ?
C43 C42 C41 120.0 . . ?
C43 C42 H42 120.0 . . ?
C42 C43 H43 120.0 . . ?
C44 C43 C42 120.0 . . ?
C44 C43 H43 120.0 . . ?
C43 C44 H44 120.0 . . ?
C43 C44 C45 120.0 . . ?
C45 C44 H44 120.0 . . ?
C40 C45 H45 120.0 . . ?
C44 C45 C40 120.0 . . ?
C44 C45 H45 120.0 . . ?
S6 C46 H46A 109.5 . . ?
S6 C46 H46B 109.5 . . ?
H46A C46 H46B 108.1 . . ?
C47 C46 S6 110.6(16) . . ?
C47 C46 H46A 109.5 . . ?
C47 C46 H46B 109.5 . . ?
C48 C47 C46 121(2) . . ?
C48 C47 C52 119(2) . . ?
C52 C47 C46 120(2) . . ?
C47 C48 H48 118.8 . . ?
C47 C48 C49 122(3) . . ?
C49 C48 H48 118.8 . . ?
C48 C49 H49 122.5 . . ?
C50 C49 C48 115(3) . . ?
C50 C49 H49 122.5 . . ?
C49 C50 H50 115.6 . . ?
C51 C50 C49 129(3) . . ?
C51 C50 H50 115.6 . . ?
C50 C51 H51 121.0 . . ?
C50 C51 C52 118(3) . . ?
C52 C51 H51 121.0 . . ?
C47 C52 C51 116(3) . . ?
C47 C52 H52 121.8 . . ?
C51 C52 H52 121.8 . . ?
S7 C53 H53A 107.8 . . ?
S7 C53 H53B 107.8 . . ?
H53A C53 H53B 107.2 . . ?
C61 C53 S7 118(3) . . ?
C61 C53 H53A 107.8 . . ?
C61 C53 H53B 107.8 . . ?
S7 C54 H54A 110.5 . . ?
S7 C54 H54B 110.5 . . ?
H54A C54 H54B 108.7 . . ?
C55 C54 S7 106.0(17) . . ?
C55 C54 H54A 110.5 . . ?
C55 C54 H54B 110.5 . . ?
C56 C55 C54 118(4) . . ?
C56 C55 C60 120.0 . . ?
C60 C55 C54 122(4) . . ?
C55 C56 H56 120.0 . . ?
C55 C56 C57 120.0 . . ?
C57 C56 H56 120.0 . . ?
C56 C57 H57 120.0 . . ?
C58 C57 C56 120.0 . . ?
C58 C57 H57 120.0 . . ?
C57 C58 H58 120.0 . . ?
C57 C58 C59 120.0 . . ?
C59 C58 H58 120.0 . . ?
C58 C59 H59 120.0 . . ?
C60 C59 C58 120.0 . . ?
C60 C59 H59 120.0 . . ?
C55 C60 H60 120.0 . . ?
C59 C60 C55 120.0 . . ?
C59 C60 H60 120.0 . . ?
C62 C61 C53 122(5) . . ?
C62 C61 C66 120.0 . . ?
C66 C61 C53 117(5) . . ?
C61 C62 H62 120.0 . . ?
C61 C62 C63 120.0 . . ?
C63 C62 H62 120.0 . . ?
C62 C63 H63 120.0 . . ?
C64 C63 C62 120.0 . . ?
C64 C63 H63 120.0 . . ?
C63 C64 H64 120.0 . . ?
C63 C64 C65 120.0 . . ?
C65 C64 H64 120.0 . . ?
C64 C65 H65 120.0 . . ?
C66 C65 C64 120.0 . . ?
C66 C65 H65 120.0 . . ?
C61 C66 H66 120.0 . . ?
C65 C66 C61 120.0 . . ?
C65 C66 H66 120.0 . . ?
S8 C67 H67A 108.7 . . ?
S8 C67 H67B 108.7 . . ?
H67A C67 H67B 107.6 . . ?
C68 C67 S8 114.0(18) . . ?
C68 C67 H67A 108.7 . . ?
C68 C67 H67B 108.7 . . ?
C69 C68 C67 121(2) . . ?
C69 C68 C73 117(2) . . ?
C73 C68 C67 122(2) . . ?
C68 C69 H69 119.2 . . ?
C68 C69 C70 122(3) . . ?
C70 C69 H69 119.2 . . ?
C69 C70 H70 120.6 . . ?
C71 C70 C69 119(3) . . ?
C71 C70 H70 120.6 . . ?
C70 C71 H71 118.7 . . ?
C72 C71 C70 123(3) . . ?
C72 C71 H71 118.7 . . ?
C71 C72 H72 122.0 . . ?
C71 C72 C73 116(3) . . ?
C73 C72 H72 122.0 . . ?
C68 C73 H73 117.8 . . ?
C72 C73 C68 124(3) . . ?
C72 C73 H73 117.8 . . ?
O11 C74 N1 123(4) . . ?
O11 C74 H74 118.7 . . ?
N1 C74 H74 118.7 . . ?
N1 C75 H75A 109.5 . . ?
N1 C75 H75B 109.5 . . ?
N1 C75 H75C 109.5 . . ?
H75A C75 H75B 109.5 . . ?
H75A C75 H75C 109.5 . . ?
H75B C75 H75C 109.5 . . ?
N1 C76 H76A 109.5 . . ?
N1 C76 H76B 109.5 . . ?
N1 C76 H76C 109.5 . . ?
H76A C76 H76B 109.5 . . ?
H76A C76 H76C 109.5 . . ?
H76B C76 H76C 109.5 . . ?
O12 C77 N2 125(3) . . ?
O12 C77 H77 117.7 . . ?
N2 C77 H77 117.7 . . ?
N2 C78 H78A 109.5 . . ?
N2 C78 H78B 109.5 . . ?
N2 C78 H78C 109.5 . . ?
H78A C78 H78B 109.5 . . ?
H78A C78 H78C 109.5 . . ?
H78B C78 H78C 109.5 . . ?
N2 C79 H79A 109.5 . . ?
N2 C79 H79B 109.5 . . ?
N2 C79 H79C 109.5 . . ?
H79A C79 H79B 109.5 . . ?
H79A C79 H79C 109.5 . . ?
H79B C79 H79C 109.5 . . ?
C81 C80 P2 117.9(13) . . ?
C81 C80 C85 120.0 . . ?
C85 C80 P2 122.1(13) . . ?
C80 C81 H81 120.0 . . ?
C82 C81 C80 120.0 . . ?
C82 C81 H81 120.0 . . ?
C81 C82 H82 120.0 . . ?
C81 C82 C83 120.0 . . ?
C83 C82 H82 120.0 . . ?
C82 C83 H83 120.0 . . ?
C84 C83 C82 120.0 . . ?
C84 C83 H83 120.0 . . ?
C83 C84 H84 120.0 . . ?
C83 C84 C85 120.0 . . ?
C85 C84 H84 120.0 . . ?
C80 C85 H85 120.0 . . ?
C84 C85 C80 120.0 . . ?
C84 C85 H85 120.0 . . ?
C89 C90 H90 120.0 . . ?
C89 C90 C91 120.0 . . ?
C91 C90 H90 120.0 . . ?
C90 C89 H89 120.0 . . ?
C88 C89 C90 120.0 . . ?
C88 C89 H89 120.0 . . ?
C89 C88 H88 120.0 . . ?
C87 C88 C89 120.0 . . ?
C87 C88 H88 120.0 . . ?
C88 C87 H87 120.0 . . ?
C88 C87 C86 120.0 . . ?
C86 C87 H87 120.0 . . ?
C87 C86 P2 115.9(13) . . ?
C91 C86 P2 124.1(13) . . ?
C91 C86 C87 120.0 . . ?
C90 C91 H91 120.0 . . ?
C86 C91 C90 120.0 . . ?
C86 C91 H91 120.0 . . ?
C93 C94 H94 120.0 . . ?
C93 C94 C95 120.0 . . ?
C95 C94 H94 120.0 . . ?
C94 C93 H93 120.0 . . ?
C94 C93 C92 120.0 . . ?
C92 C93 H93 120.0 . . ?
C93 C92 P2 119.3(13) . . ?
C97 C92 P2 120.7(13) . . ?
C97 C92 C93 120.0 . . ?
C92 C97 H97 120.0 . . ?
C92 C97 C96 120.0 . . ?
C96 C97 H97 120.0 . . ?
C97 C96 H96 120.0 . . ?
C95 C96 C97 120.0 . . ?
C95 C96 H96 120.0 . . ?
C94 C95 H95 120.0 . . ?
C96 C95 C94 120.0 . . ?
C96 C95 H95 120.0 . . ?
S9 C98 H98A 109.2 . . ?
S9 C98 H98B 109.2 . . ?
H98A C98 H98B 107.9 . . ?
C99 C98 S9 112.2(16) . . ?
C99 C98 H98A 109.2 . . ?
C99 C98 H98B 109.2 . . ?
C103 C104 H104 120.0 . . ?
C103 C104 C99 120.0 . . ?
C99 C104 H104 120.0 . . ?
C104 C103 H103 120.0 . . ?
C104 C103 C102 120.0 . . ?
C102 C103 H103 120.0 . . ?
C103 C102 H102 120.0 . . ?
C101 C102 C103 120.0 . . ?
C101 C102 H102 120.0 . . ?
C102 C101 H101 120.0 . . ?
C102 C101 C100 120.0 . . ?
C100 C101 H101 120.0 . . ?
C101 C100 H100 120.0 . . ?
C99 C100 C101 120.0 . . ?
C99 C100 H100 120.0 . . ?
C104 C99 C98 119.7(17) . . ?
C100 C99 C98 120.2(17) . . ?
C100 C99 C104 120.0 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Ag1 S2 C18 C19 -49(2) . . . . ?
Ag1 S8 C67 C68 -27(2) 2_655 . . . ?
Ag2 S1 C11 C12 -43.1(19) . . . . ?
Ag2 S2 C18 C19 -31(2) . . . . ?
Ag2 P2 C80 C81 -31.5(13) . . . . ?
Ag2 P2 C80 C85 151.1(9) . . . . ?
Ag2 P2 C86 C87 -52.8(15) . . . . ?
Ag2 P2 C86 C91 128.5(11) . . . . ?
Ag2 P2 C92 C93 -32.7(11) . . . . ?
Ag2 P2 C92 C97 148.9(9) . . . . ?
Ag5 S1 C11 C12 -109.8(15) . . . . ?
Ag5 S2 C18 C19 37.3(18) . . . . ?
Ag5 S9 C98 C99 52.2(19) . . . . ?
Ag5 O1 C1 O2 3(4) . . . . ?
Ag5 O1 C1 C2 -176.1(10) . . . . ?
Ag7 S1 C11 C12 46.8(17) . . . . ?
Ag7 S8 C67 C68 -109.2(17) 2_655 . . . ?
Ag7 O10 C9 O9 -6(6) 2_655 . . . ?
Ag7 O10 C9 C10 177.6(15) 2_655 . . . ?
Ag8 S3 C25 C26 -66.6(16) . . . . ?
Ag8 S9 C98 C99 114.9(15) . . . . ?
Ag8 O2 C1 O1 6(4) . . . . ?
Ag8 O2 C1 C2 -175.0(10) . . . . ?
Ag9 S1 C11 C12 150.0(13) . . . . ?
Ag10 S4 C32 C33 -177.3(15) 2_655 . . . ?
Ag11 S3 C25 C26 69.2(15) . . . . ?
Ag11 S4 C32 C33 -98.3(18) 2_655 . . . ?
Ag11 O7 C7 O7 -16.0(7) . . . 2_655 ?
Ag11 O7 C7 C8 164.0(7) . . . . ?
Ag13 S2 C18 C19 142.9(14) . . . . ?
Ag14 S6 C46 C47 69.8(18) . . . . ?
Ag14 S9 C98 C99 -90.8(16) . . . . ?
Ag14 O3 C3 O4 -15(6) . . . . ?
Ag14 O3 C3 C4 166.9(15) . . . . ?
Ag15 S6 C46 C47 -146.9(16) . . . . ?
Ag15 O0AA C0AA O1AA 0(9) . . . . ?
Ag15 O0AA C0AA C1AA 178(7) . . . . ?
Ag15 C0AA C1AA F16 87(24) . . . . ?
Ag15 C0AA C1AA F17 -160(24) . . . . ?
Ag15 C0AA C1AA F18 -55(26) . . . . ?
Ag16 S7 C53 C61 -157(7) . . . . ?
Ag16 S7 C54 C55 -179(3) . . . . ?
Ag17 S8 C67 C68 149.4(15) . . . . ?
Ag18 S4 C32 C33 106.6(17) . . . . ?
Ag18 S5 C39 C40 -67.6(19) . . . . ?
Ag18 O9 C9 O10 1(6) . . . . ?
Ag18 O9 C9 C10 176.8(16) . . . . ?
Ag19 S6 C46 C47 -67.9(19) 2_655 . . . ?
Ag19 S7 C53 C61 130(8) . . . . ?
Ag19 S7 C54 C55 106(4) . . . . ?
Ag19 O5 C5 O6 4(6) . . . . ?
Ag19 O5 C5 C6 -175.2(16) . . . . ?
Ag20 S2 C18 C19 -121.8(15) 2_655 . . . ?
Ag20 S7 C53 C61 75(9) . . . . ?
Ag20 S7 C54 C55 44(6) . . . . ?
Ag20 S8 C67 C68 48(2) . . . . ?
Ag20 O6 C5 O5 -4(6) . . . . ?
Ag20 O6 C5 C6 176.1(16) . . . . ?
Ag21 S9 C98 C99 -169.5(13) . . . . ?
Ag22 S5 C39 C40 68.3(18) . . . . ?
Ag22 S7 C53 C61 -78(9) . . . . ?
Ag22 S7 C54 C55 -100(4) . . . . ?
Ag22 O4 C3 O3 -22(5) . . . . ?
Ag22 O4 C3 C4 156.0(16) . . . . ?
Ag23 S3 C25 C26 -146.9(13) . . . . ?
Ag23 S5 C39 C40 -146.6(16) . . . . ?
Ag23 O11 C74 N1 177(3) . . . . ?
Ag23 O12 C77 N2 174(2) . . . . ?
S1 C11 C12 C13 90.8(16) . . . . ?
S1 C11 C12 C17 -89.2(17) . . . . ?
S2 C18 C19 C24 -85.2(18) . . . . ?
S2 C18 C19 C20 95.3(17) . . . . ?
S3 C25 C26 C27 90(2) . . . . ?
S3 C25 C26 C31 -88(2) . . . . ?
S4 C32 C33 C34 -91.1(19) . . . . ?
S4 C32 C33 C38 85.0(19) . . . . ?
S5 C39 C40 C41 -89.2(18) . . . . ?
S5 C39 C40 C45 88.6(18) . . . . ?
S6 C46 C47 C48 91(3) . . . . ?
S6 C46 C47 C52 -89(2) . . . . ?
S7 C53 C61 C62 138(6) . . . . ?
S7 C53 C61 C66 -50(10) . . . . ?
S7 C54 C55 C56 79(4) . . . . ?
S7 C54 C55 C60 -101(4) . . . . ?
S8 C67 C68 C69 -88(3) . . . . ?
S8 C67 C68 C73 96(3) . . . . ?
S9 C98 C99 C104 -113.2(15) . . . . ?
S9 C98 C99 C100 70.3(19) . . . . ?
P2 C80 C81 C82 -177.5(13) . . . . ?
P2 C80 C85 C84 177.4(14) . . . . ?
P2 C86 C91 C90 178.7(17) . . . . ?
P2 C92 C97 C96 178.4(14) . . . . ?
O1 C1 C2 F1 -71(2) . . . . ?
O1 C1 C2 F2 49(3) . . . . ?
O1 C1 C2 F3 166(2) . . . . ?
O1 C1 C2 F1A 12(4) . . . . ?
O1 C1 C2 F2A 117(5) . . . . ?
O1 C1 C2 F3A -125(4) . . . . ?
O2 C1 C2 F1 110(2) . . . . ?
O2 C1 C2 F2 -130(3) . . . . ?
O2 C1 C2 F3 -13(3) . . . . ?
O2 C1 C2 F1A -167(4) . . . . ?
O2 C1 C2 F2A -62(5) . . . . ?
O2 C1 C2 F3A 56(4) . . . . ?
O3 C3 C4 F4 -46(4) . . . . ?
O3 C3 C4 F5 68(3) . . . . ?
O3 C3 C4 F6 -179(3) . . . . ?
O4 C3 C4 F4 135(3) . . . . ?
O4 C3 C4 F5 -111(3) . . . . ?
O4 C3 C4 F6 2(4) . . . . ?
O5 C5 C6 F7 -12(4) . . . . ?
O5 C5 C6 F8 106(3) . . . . ?
O5 C5 C6 F9 -140(3) . . . . ?
O6 C5 C6 F7 168(3) . . . . ?
O6 C5 C6 F8 -74(4) . . . . ?
O6 C5 C6 F9 40(4) . . . . ?
O9 C9 C10 F13 98(3) . . . . ?
O9 C9 C10 F14 -21(4) . . . . ?
O9 C9 C10 F15 -138(3) . . . . ?
O10 C9 C10 F13 -85(3) . . . . ?
O10 C9 C10 F14 156(3) . . . . ?
O10 C9 C10 F15 39(4) . . . . ?
O0AA C0AA C1AA F16 -82(6) . . . . ?
O0AA C0AA C1AA F17 30(6) . . . . ?
O0AA C0AA C1AA F18 135(4) . . . . ?
O1AA C0AA C1AA F16 96(5) . . . . ?
O1AA C0AA C1AA F17 -151(4) . . . . ?
O1AA C0AA C1AA F18 -46(6) . . . . ?
O7 C7 C8 F10 -26.9(19) . . . . ?
O7 C7 C8 F10 153.1(19) 2_655 . . . ?
O7 C7 C8 F11 -93.4(16) 2_655 . . . ?
O7 C7 C8 F11 86.6(16) . . . . ?
O7 C7 C8 F12 -158.4(19) . . . . ?
O7 C7 C8 F12 21.6(19) 2_655 . . . ?
C11 C12 C17 C16 -179.9(16) . . . . ?
C15 C14 C13 C12 0.0 . . . . ?
C14 C15 C16 C17 0.0 . . . . ?
C14 C13 C12 C11 179.9(16) . . . . ?
C14 C13 C12 C17 0.0 . . . . ?
C13 C12 C17 C16 0.0 . . . . ?
C12 C17 C16 C15 0.0 . . . . ?
C16 C15 C14 C13 0.0 . . . . ?
C18 C19 C20 C21 179.5(18) . . . . ?
C23 C24 C19 C18 -179.5(17) . . . . ?
C23 C24 C19 C20 0.0 . . . . ?
C24 C23 C22 C21 0.0 . . . . ?
C24 C19 C20 C21 0.0 . . . . ?
C19 C20 C21 C22 0.0 . . . . ?
C20 C21 C22 C23 0.0 . . . . ?
C22 C23 C24 C19 0.0 . . . . ?
C25 C26 C27 C28 -178.4(19) . . . . ?
C25 C26 C31 C30 177.9(18) . . . . ?
C26 C27 C28 C29 -1(4) . . . . ?
C27 C26 C31 C30 0(3) . . . . ?
C27 C28 C29 C30 4(4) . . . . ?
C28 C29 C30 C31 -4(3) . . . . ?
C29 C30 C31 C26 2(3) . . . . ?
C31 C26 C27 C28 -1(3) . . . . ?
C32 C33 C34 C35 176(2) . . . . ?
C32 C33 C38 C36 -176(2) . . . . ?
C33 C34 C35 C37 0.0 . . . . ?
C34 C33 C38 C36 0.0 . . . . ?
C34 C35 C37 C36 0.0 . . . . ?
C35 C37 C36 C38 0.0 . . . . ?
C37 C36 C38 C33 0.0 . . . . ?
C38 C33 C34 C35 0.0 . . . . ?
C39 C40 C41 C42 178(2) . . . . ?
C39 C40 C45 C44 -178(2) . . . . ?
C40 C41 C42 C43 0.0 . . . . ?
C41 C40 C45 C44 0.0 . . . . ?
C41 C42 C43 C44 0.0 . . . . ?
C42 C43 C44 C45 0.0 . . . . ?
C43 C44 C45 C40 0.0 . . . . ?
C45 C40 C41 C42 0.0 . . . . ?
C46 C47 C48 C49 179(3) . . . . ?
C46 C47 C52 C51 -179(2) . . . . ?
C47 C48 C49 C50 0(5) . . . . ?
C48 C47 C52 C51 0(4) . . . . ?
C48 C49 C50 C51 1(6) . . . . ?
C49 C50 C51 C52 -1(5) . . . . ?
C50 C51 C52 C47 0(4) . . . . ?
C52 C47 C48 C49 0(4) . . . . ?
C53 C61 C62 C63 172(6) . . . . ?
C53 C61 C66 C65 -172(5) . . . . ?
C54 C55 C56 C57 -180(3) . . . . ?
C54 C55 C60 C59 180(3) . . . . ?
C55 C56 C57 C58 0.0 . . . . ?
C56 C55 C60 C59 0.0 . . . . ?
C56 C57 C58 C59 0.0 . . . . ?
C57 C58 C59 C60 0.0 . . . . ?
C58 C59 C60 C55 0.0 . . . . ?
C60 C55 C56 C57 0.0 . . . . ?
C61 C62 C63 C64 0.0 . . . . ?
C62 C61 C66 C65 0.0 . . . . ?
C62 C63 C64 C65 0.0 . . . . ?
C63 C64 C65 C66 0.0 . . . . ?
C64 C65 C66 C61 0.0 . . . . ?
C66 C61 C62 C63 0.0 . . . . ?
C67 C68 C69 C70 -180(3) . . . . ?
C67 C68 C73 C72 179(3) . . . . ?
C68 C69 C70 C71 3(5) . . . . ?
C69 C68 C73 C72 3(4) . . . . ?
C69 C70 C71 C72 -3(6) . . . . ?
C70 C71 C72 C73 3(6) . . . . ?
C71 C72 C73 C68 -3(5) . . . . ?
C73 C68 C69 C70 -3(4) . . . . ?
C75 N1 C74 O11 -48(5) . . . . ?
C76 N1 C74 O11 -175(3) . . . . ?
C78 N2 C77 O12 1(6) . . . . ?
C79 N2 C77 O12 164(4) . . . . ?
C80 P2 C86 C87 83.1(13) . . . . ?
C80 P2 C86 C91 -95.6(14) . . . . ?
C80 P2 C92 C93 -159.1(11) . . . . ?
C80 P2 C92 C97 22.5(13) . . . . ?
C80 C81 C82 C83 0.0 . . . . ?
C81 C80 C85 C84 0.0 . . . . ?
C81 C82 C83 C84 0.0 . . . . ?
C82 C83 C84 C85 0.0 . . . . ?
C83 C84 C85 C80 0.0 . . . . ?
C85 C80 C81 C82 0.0 . . . . ?
C90 C89 C88 C87 0.0 . . . . ?
C89 C90 C91 C86 0.0 . . . . ?
C89 C88 C87 C86 0.0 . . . . ?
C88 C87 C86 P2 -178.8(16) . . . . ?
C88 C87 C86 C91 0.0 . . . . ?
C87 C86 C91 C90 0.0 . . . . ?
C86 P2 C80 C81 -166.6(10) . . . . ?
C86 P2 C80 C85 16.0(13) . . . . ?
C86 P2 C92 C93 91.9(12) . . . . ?
C86 P2 C92 C97 -86.5(13) . . . . ?
C91 C90 C89 C88 0.0 . . . . ?
C94 C93 C92 P2 -178.4(13) . . . . ?
C94 C93 C92 C97 0.0 . . . . ?
C93 C94 C95 C96 0.0 . . . . ?
C93 C92 C97 C96 0.0 . . . . ?
C92 P2 C80 C81 84.3(11) . . . . ?
C92 P2 C80 C85 -93.1(12) . . . . ?
C92 P2 C86 C87 -167.6(12) . . . . ?
C92 P2 C86 C91 13.7(16) . . . . ?
C92 C97 C96 C95 0.0 . . . . ?
C97 C96 C95 C94 0.0 . . . . ?
C95 C94 C93 C92 0.0 . . . . ?
C104 C103 C102 C101 0.0 . . . . ?
C103 C104 C99 C98 -176.4(19) . . . . ?
C103 C104 C99 C100 0.0 . . . . ?
C103 C102 C101 C100 0.0 . . . . ?
C102 C101 C100 C99 0.0 . . . . ?
C101 C100 C99 C98 176.4(19) . . . . ?
C101 C100 C99 C104 0.0 . . . . ?
C99 C104 C103 C102 0.0 . . . . ?

_smtbx_masks_special_details     ?
loop_
_smtbx_masks_void_nr
_smtbx_masks_void_average_x
_smtbx_masks_void_average_y
_smtbx_masks_void_average_z
_smtbx_masks_void_volume
_smtbx_masks_void_count_electrons
_smtbx_masks_void_content
1 0.250 -0.594 -0.390 3225.1 785.6 ?
2 0.750 -0.966 -0.038 3225.1 785.6 ?

_olex2_submission_special_instructions 'No special instructions were received'
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_pd@ag35
_database_code_depnum_ccdc_archive 'CCDC 2150328'
loop_
_audit_author_name
_audit_author_address
'wuyage '
;Henan Polytechnic University
China
;
_audit_update_record             
;
2022-05-28 deposited with the CCDC.	2022-05-31 downloaded from the CCDC.
;
_audit_creation_date             2022-05-27
_audit_creation_method           
;
Olex2 1.2
(compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506)
;
_shelx_SHELXL_version_number     2016/6
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         
'C194 H184 Ag34.99 F30 N4 O24 P2 Pd S18, 2(H2 O), 8(C3 H7 N O), 2(C3 N O)'
_chemical_formula_sum            'C224 H258 Ag35 F30 N14 O36 P2 Pd S18'
_chemical_formula_weight         8813.30
_chemical_melting_point          ?
_chemical_oxdiff_formula         'C H O N S Cu'
_chemical_oxdiff_usercomment     ' '
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag 0.1306 4.2820 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0727 0.0534 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pd Pd 0.1215 3.9337 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           15
_space_group_name_H-M_alt        'C 1 2/c 1'
_space_group_name_Hall           '-C 2yc'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'

_cell_length_a                   41.1371(3)
_cell_length_b                   30.7832(2)
_cell_length_c                   21.93730(10)
_cell_angle_alpha                90
_cell_angle_beta                 98.3850(10)
_cell_angle_gamma                90
_cell_volume                     27482.9(3)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    39869
_cell_measurement_temperature    199.99(10)
_cell_measurement_theta_max      73.8190
_cell_measurement_theta_min      3.0330
_shelx_estimated_absorpt_T_max   0.096
_shelx_estimated_absorpt_T_min   0.058
_exptl_absorpt_coefficient_mu    22.094
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.09786
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
CrysAlisPro 1.171.39.27b (Rigaku Oxford Diffraction, 2015)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            black
_exptl_crystal_colour_primary    black
_exptl_crystal_density_diffrn    2.130
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             17068
_exptl_crystal_size_max          0.3
_exptl_crystal_size_mid          0.2
_exptl_crystal_size_min          0.2
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0636
_diffrn_reflns_av_unetI/netI     0.0545
_diffrn_reflns_Laue_measured_fraction_full 0.997
_diffrn_reflns_Laue_measured_fraction_max 0.967
_diffrn_reflns_limit_h_max       51
_diffrn_reflns_limit_h_min       -46
_diffrn_reflns_limit_k_max       23
_diffrn_reflns_limit_k_min       -37
_diffrn_reflns_limit_l_max       26
_diffrn_reflns_limit_l_min       -22
_diffrn_reflns_number            75567
_diffrn_reflns_point_group_measured_fraction_full 0.997
_diffrn_reflns_point_group_measured_fraction_max 0.967
_diffrn_reflns_theta_full        67.684
_diffrn_reflns_theta_max         74.145
_diffrn_reflns_theta_min         2.171
_diffrn_ambient_environment      N~2~
_diffrn_ambient_temperature      199.99(10)
_diffrn_detector                 'CCD plate'
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.967
_diffrn_measurement_details      
;
List of Runs (angles in degrees, time in seconds):

  # Type    Start    End  Width  tₑₓₚ   ω     θ     κ     φ   Frames
#--------------------------------------------------------------------------
  1  ω    -28.00  23.00   0.50    1.34    --    0.00 -57.00  90.00  102
  2  ω    -18.00  27.00   0.50    1.34    --    0.00  38.00 -30.00   90
  3  ω     48.00  75.00   0.50    1.34    --    0.00  36.00 132.00   54
  4  ω     47.00  89.00   0.50    1.34    --    0.00  38.00 -30.00   84
  5  ω    -66.00 -37.00   0.50    1.34    --    0.00 -57.00  90.00   58
  6  ω    129.00 177.00   0.50    5.35    --   95.20  77.00-150.00   96
  7  ω      8.00 114.00   0.50    5.35    --   95.20 -30.00-180.00  212
  8  ω     85.00 185.00   0.50    5.35    --   95.20  30.00 150.00  200
  9  ω      7.00  90.00   0.50    5.35    --   95.20 -15.00   0.00  166
 10  ω     70.00 114.00   0.50    5.35    --   95.20 -45.00-150.00   88
 11  ω     31.00  94.00   0.50    5.35    --   95.20 -45.00-180.00  126
 12  ω      8.00  34.00   0.50    5.35    --   95.20 -61.00  30.00   52
 13  ω     11.00 118.00   0.50    5.35    --   95.20 -61.00-180.00  214
;
_diffrn_measurement_device       'four-circle diffractometer'
_diffrn_measurement_device_type  'XtaLAB AFC12 (RINC): Kappa single'
_diffrn_measurement_method       'ω scans'
_diffrn_orient_matrix_type       
'CrysAlisPro convention (1999,Acta A55,543-557)'
_diffrn_orient_matrix_UB_11      0.0302556000
_diffrn_orient_matrix_UB_12      0.0136185000
_diffrn_orient_matrix_UB_13      0.0458853000
_diffrn_orient_matrix_UB_21      -0.0227134000
_diffrn_orient_matrix_UB_22      0.0187437000
_diffrn_orient_matrix_UB_23      0.0433499000
_diffrn_orient_matrix_UB_31      -0.0003480000
_diffrn_orient_matrix_UB_32      -0.0443987000
_diffrn_orient_matrix_UB_33      0.0324481000
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54184
_diffrn_source                   'fine-focus sealed X-ray tube'
_diffrn_source_type              'Enhance (Cu) X-ray Source'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                21320
_reflns_number_total             27045
_reflns_odcompleteness_completeness 99.66
_reflns_odcompleteness_iscentric 1
_reflns_odcompleteness_theta     66.97
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'CrysAlisPro 1.171.39.27b (Rigaku OD, 2015)'
_computing_data_collection       'CrysAlisPro 1.171.39.27b (Rigaku OD, 2015)'
_computing_data_reduction        'CrysAlisPro 1.171.39.27b (Rigaku OD, 2015)'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    'olex2.solve (Bourhis et al., 2015)'
_refine_diff_density_max         2.530
_refine_diff_density_min         -3.272
_refine_diff_density_rms         0.550
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.060
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1687
_refine_ls_number_reflns         27045
_refine_ls_number_restraints     446
_refine_ls_R_factor_all          0.0906
_refine_ls_R_factor_gt           0.0722
_refine_ls_restrained_S_all      1.069
_refine_ls_shift/su_max          0.006
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.1101P)²+615.2066P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1877
_refine_ls_wR_factor_ref         0.2066
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups, All C(H,H) groups
 At 1.5 times of:
  All C(H,H,H) groups, All O(H,H) groups
2. Restrained distances
 C66-C65
 1.51 with sigma of 0.02
 N7-C119 = N7-C117 = N7-C114
 1.5 with sigma of 0.02
 C116-N7
 1.5 with sigma of 0.02
 C72-C71
 1.5 with sigma of 0.02
 O6-C71
 1.2 with sigma of 0.02
 F10-C72 = F11-C72
 1.35 with sigma of 0.01
 O16-C110
 1.2 with sigma of 0.02
 O18-C118 = O17-C113
 1.2 with sigma of 0.02
 F2-F1 \\sim F2-F3 \\sim F1-F3
 with sigma of 0.02
 F3-C66 \\sim F1-C66 \\sim F2-C66
 with sigma of 0.02
 F8A-C70 \\sim F8-C70 \\sim F9-C70 \\sim F9A-C70 \\sim F7-C70 \\sim F7A-C70
 with sigma of 0.02
3. Restrained planarity
 F1, F1_$1, F2, F2_$1, F3, F3_$1
 with sigma of 0.1
4. Rigid bond restraints
 O13, N3, C101, C102, C103
 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01
 C37, C38, C39, C40, C41, C42
 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01
 F7, C70, F8A, F8, F7A, F9, F9A
 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01
5. Uiso/Uaniso restraints and constraints
F15 \\sim F16 \\sim F17: within 2A with sigma of 0.02 and sigma for terminal
atoms of 0.04
C36 \\sim C37 \\sim C38 \\sim C39 \\sim C40 \\sim C41 \\sim C42: within 2A with
sigma of 0.02 and sigma for terminal atoms of 0.04
Uanis(C56) \\sim Ueq, Uanis(C51) \\sim Ueq, Uanis(C52) \\sim Ueq, Uanis(C53)
\\sim Ueq, Uanis(C54) \\sim Ueq, Uanis(C55) \\sim Ueq: with sigma of 0.01 and
sigma for terminal atoms of 0.02
Uanis(C53) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(F8) \\sim Ueq, Uanis(F7) \\sim Ueq, Uanis(F9) \\sim Ueq, Uanis(F15) \\sim
Ueq, Uanis(F16) \\sim Ueq, Uanis(F8) \\sim Ueq, Uanis(F7) \\sim Ueq, Uanis(F9)
\\sim Ueq, Uanis(F13) \\sim Ueq: with sigma of 0.01 and sigma for terminal
atoms of 0.02
Uanis(C62) \\sim Ueq, Uanis(C61) \\sim Ueq: with sigma of 0.01 and sigma for
terminal atoms of 0.02
Uanis(C61) \\sim Ueq, Uanis(C62) \\sim Ueq: with sigma of 0.01 and sigma for
terminal atoms of 0.02
Uanis(C100) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(F2) \\sim Ueq, Uanis(F3) \\sim Ueq, Uanis(C66) \\sim Ueq, Uanis(F1) \\sim
Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(C72) \\sim Ueq, Uanis(C71) \\sim Ueq, Uanis(O6) \\sim Ueq, Uanis(F10)
\\sim Ueq, Uanis(F11) \\sim Ueq: with sigma of 0.01 and sigma for terminal
atoms of 0.02
Uanis(F5) \\sim Ueq, Uanis(F13) \\sim Ueq, Uanis(F15) \\sim Ueq, Uanis(F9)
\\sim Ueq, Uanis(C63) \\sim Ueq, Uanis(C109) \\sim Ueq: with sigma of 0.01 and
sigma for terminal atoms of 0.02
Uanis(C102) \\sim Ueq, Uanis(O13) \\sim Ueq, Uanis(C101) \\sim Ueq, Uanis(N3)
\\sim Ueq, Uanis(C103) \\sim Ueq, Uanis(C111) \\sim Ueq, Uanis(N6) \\sim Ueq,
Uanis(C110) \\sim Ueq, Uanis(C112) \\sim Ueq, Uanis(O16) \\sim Ueq: with sigma
of 0.01 and sigma for terminal atoms of 0.02
Uanis(O14) \\sim Ueq, Uanis(N4) \\sim Ueq, Uanis(C105) \\sim Ueq, Uanis(C104)
\\sim Ueq, Uanis(C106) \\sim Ueq: with sigma of 0.01 and sigma for terminal
atoms of 0.02
Uanis(C38) \\sim Ueq, Uanis(C40) \\sim Ueq, Uanis(C41) \\sim Ueq, Uanis(C42)
\\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(F9) \\sim Ueq, Uanis(F13) \\sim Ueq, Uanis(F15) \\sim Ueq: with sigma of
0.01 and sigma for terminal atoms of 0.02
Uanis(F8A) \\sim Ueq, Uanis(F9A) \\sim Ueq, Uanis(F7A) \\sim Ueq, Uanis(F9)
\\sim Ueq, Uanis(C70) \\sim Ueq, Uanis(F7) \\sim Ueq, Uanis(F8) \\sim Ueq: with
sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(F8A) \\sim Ueq, Uanis(C70) \\sim Ueq, Uanis(F9) \\sim Ueq, Uanis(F9A)
\\sim Ueq, Uanis(F7A) \\sim Ueq, Uanis(F7) \\sim Ueq, Uanis(F8) \\sim Ueq: with
sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(Ag0A) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(Ag17) \\sim Ueq, Uanis(Ag1) \\sim Ueq: with sigma of 0.01 and sigma for
terminal atoms of 0.02
Uanis(Ag20) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
6. Others
 Sof(F7A)=Sof(F8A)=Sof(F9A)=1-FVAR(1)
 Sof(F7)=Sof(F8)=Sof(F9)=FVAR(1)
 Sof(Ag1)=1-FVAR(2)
 Sof(Ag17)=FVAR(2)
 Sof(O18)=Sof(C114)=Sof(C118)=Sof(C119)=1-FVAR(3)
 Sof(O17)=Sof(C113)=Sof(C116)=Sof(C117)=FVAR(3)
 Fixed Sof: F1(0.5) F2(0.5) F3(0.5) F10(0.5) C72(0.5)
7.a Riding coordinates:
 O1W(H1Wa,H1Wb)
7.b Secondary CH2 refined with riding coordinates:
 C1(H1a,H1b), C8(H8a,H8b), C15(H15a,H15b), C22(H22a,H22b), C29(H29a,H29b),
 C36(H36a,H36b), C43(H43a,H43b), C50(H50a,H50b), C57(H57a,H57b)
7.c Aromatic/amide H refined with riding coordinates:
 C3(H3), C4(H4), C5(H5), C6(H6), C7(H7), C10(H10), C11(H11), C12(H12),
 C13(H13), C14(H14), C17(H17), C18(H18), C19(H19), C20(H20), C21(H21), C23(H23),
  C25(H25), C26(H26), C27(H27), C28(H28), C31(H31), C32(H32), C33(H33),
 C34(H34), C35(H35), C38(H38), C39(H39), C40(H40), C41(H41), C42(H42), C45(H45),
  C46(H46), C47(H47), C48(H48), C49(H49), C56(H56), C55(H55), C54(H54),
 C53(H53), C52(H52), C60(H60), C61(H61), C62(H62), C63(H63), C64(H64), C78(H78),
  C79(H79), C80(H80), C81(H81), C82(H82), C84(H84), C85(H85), C86(H86),
 C87(H87), C88(H88), C90(H90), C91(H91), C92(H92), C93(H93), C94(H94), C95(H95),
  C98(H98), C101(H101), C104(H104), C107(H107), C110(H110)
7.d Fitted hexagon refined as free rotating group:
 C56(C55,C54,C53,C52,C51)
7.e Idealised Me refined as rotating group:
 C96(H96a,H96b,H96c), C97(H97a,H97b,H97c), C99(H99a,H99b,H99c), C100(H10a,H10b,
 H10c), C102(H10d,H10e,H10f), C103(H10g,H10h,H10i), C105(H10j,H10k,H10l),
 C106(H10m,H10n,H10o), C108(H10p,H10q,H10r), C109(H10s,H10t,H10u), C111(H11a,
 H11b,H11c), C112(H11d,H11e,H11f)
;
_atom_sites_solution_hydrogens   mixed
_atom_sites_solution_primary     iterative
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag2 Ag 0.43103(2) 0.75086(2) 0.22764(3) 0.02775(15) Uani 1 1 d . . . . .
Ag3 Ag 0.46821(2) 0.67318(2) 0.20337(3) 0.02651(14) Uani 1 1 d . . . . .
Ag4 Ag 0.52726(2) 0.74784(2) 0.37482(3) 0.02724(14) Uani 1 1 d . . . . .
Ag5 Ag 0.46733(2) 0.79647(2) 0.33240(3) 0.02808(15) Uani 1 1 d . . . . .
Ag6 Ag 0.53342(2) 0.70194(2) 0.17019(3) 0.02791(15) Uani 1 1 d . . . . .
Ag7 Ag 0.53066(2) 0.82749(2) 0.29247(3) 0.02770(14) Uani 1 1 d . . . . .
Ag8 Ag 0.47909(2) 0.60804(2) 0.30738(3) 0.03419(16) Uani 1 1 d . . . . .
Ag9 Ag 0.51928(2) 0.83659(2) 0.42556(3) 0.03565(17) Uani 1 1 d . . . . .
Ag10 Ag 0.58814(2) 0.80524(2) 0.38663(3) 0.03630(17) Uani 1 1 d . . . . .
Ag11 Ag 0.56301(2) 0.66800(2) 0.43232(3) 0.03720(17) Uani 1 1 d . . . . .
Ag12 Ag 0.60553(2) 0.67434(3) 0.33293(4) 0.04199(18) Uani 1 1 d . . . . .
Ag13 Ag 0.500000 0.91204(3) 0.250000 0.0430(3) Uani 1 2 d S T P . .
Ag14 Ag 0.49432(2) 0.68870(3) 0.46299(4) 0.04493(19) Uani 1 1 d . . . . .
Ag15 Ag 0.44011(2) 0.88558(3) 0.29918(4) 0.0515(2) Uani 1 1 d . . . . .
Ag16 Ag 0.38226(3) 0.67770(4) 0.29669(5) 0.0627(3) Uani 1 1 d . . . . .
Ag17 Ag 0.4358(3) 0.7465(3) 0.4686(3) 0.051(2) Uani 0.51(5) 1 d . U . A 1
Ag19 Ag 0.36796(10) 0.7673(2) 0.37873(15) 0.0551(16) Uani 0.462(16) 1 d . . . A
1
Ag20 Ag 0.37395(14) 0.7496(3) 0.3919(4) 0.1070(18) Uani 0.535(16) 1 d . U . A 2
Pd1 Pd 0.500000 0.74955(2) 0.250000 0.01961(17) Uani 1 2 d S T P . .
S1 S 0.57872(6) 0.68514(8) 0.10790(11) 0.0362(5) Uani 1 1 d . . . . .
S2 S 0.59960(6) 0.72848(7) 0.41548(11) 0.0335(5) Uani 1 1 d . . . . .
S3 S 0.58890(6) 0.86264(7) 0.30884(11) 0.0345(5) Uani 1 1 d . . . . .
S4 S 0.51272(6) 0.62528(7) 0.40662(11) 0.0332(5) Uani 1 1 d . . . . .
S5 S 0.42685(6) 0.61874(7) 0.23856(11) 0.0324(5) Uani 1 1 d . . . . .
S6 S 0.51081(6) 0.76890(8) 0.48050(11) 0.0362(5) Uani 1 1 d . . . . .
S7 S 0.49585(6) 0.89568(7) 0.35787(11) 0.0351(5) Uani 1 1 d . . . . .
S8 S 0.42361(6) 0.81083(8) 0.40009(11) 0.0343(5) Uani 1 1 d . . . . .
S9 S 0.37402(6) 0.75735(8) 0.25787(11) 0.0344(5) Uani 1 1 d . . . . .
P1 P 0.32188(8) 0.75643(12) 0.43301(16) 0.0554(8) Uani 1 1 d . . . . .
F1 F 0.5307(4) 0.4527(4) 0.2652(13) 0.105(7) Uani 0.5 1 d D U . B -1
F2 F 0.4863(5) 0.4521(4) 0.2947(8) 0.066(4) Uani 0.5 1 d D U . B .
F3 F 0.4889(8) 0.4508(6) 0.2003(8) 0.125(9) Uani 0.5 1 d D U . B -1
F4 F 0.7300(2) 0.6485(4) 0.3233(7) 0.112(4) Uani 1 1 d . . . . .
F5 F 0.7093(2) 0.5953(4) 0.3679(5) 0.105(4) Uani 1 1 d . U . . .
F6 F 0.7156(2) 0.5909(3) 0.2755(5) 0.094(3) Uani 1 1 d . . . . .
F7 F 0.6043(6) 0.8585(6) 0.6117(7) 0.093(6) Uani 0.65(3) 1 d D U . C 1
F8 F 0.6366(3) 0.8894(8) 0.5607(8) 0.100(6) Uani 0.65(3) 1 d D U . C 1
F9 F 0.5941(7) 0.9239(7) 0.5760(13) 0.120(8) Uani 0.65(3) 1 d D U . C 1
F10 F 0.4693(6) 1.0583(8) 0.3010(12) 0.119(8) Uani 0.5 1 d D U . . .
F11 F 0.4773(4) 1.0710(4) 0.2145(7) 0.139(5) Uani 1 1 d D U . . .
F12 F 0.3686(3) 1.0049(4) 0.3390(9) 0.148(6) Uani 1 1 d . . . . .
F13 F 0.3271(3) 0.9723(5) 0.2953(8) 0.163(6) Uani 1 1 d . U . . .
F14 F 0.3437(4) 0.9654(5) 0.3900(8) 0.146(6) Uani 1 1 d . . . . .
F15 F 0.4769(4) 0.6506(6) 0.6734(6) 0.141(5) Uani 1 1 d . U . . .
F16 F 0.4439(4) 0.7017(5) 0.6829(5) 0.128(4) Uani 1 1 d . U . . .
F17 F 0.4292(4) 0.6461(5) 0.6413(6) 0.147(5) Uani 1 1 d . U . . .
O1 O 0.4941(2) 0.5351(2) 0.2982(4) 0.050(2) Uani 1 1 d . . . . .
O2 O 0.6656(2) 0.6454(3) 0.2424(4) 0.055(2) Uani 1 1 d . . . . .
O3 O 0.65791(19) 0.6467(3) 0.3425(4) 0.052(2) Uani 1 1 d . . . . .
O4 O 0.6006(2) 0.8334(3) 0.4867(4) 0.069(3) Uani 1 1 d . . . . .
O5 O 0.5596(2) 0.8790(3) 0.4839(4) 0.0517(19) Uani 1 1 d . . . . .
O6 O 0.5279(3) 0.9846(4) 0.2565(7) 0.109(4) Uani 1 1 d D U . . .
O7 O 0.3589(3) 0.8942(3) 0.3217(5) 0.071(3) Uani 1 1 d . . . . .
O8 O 0.4020(2) 0.9364(3) 0.3156(5) 0.064(3) Uani 1 1 d . . . . .
O9 O 0.4817(2) 0.6739(3) 0.5603(4) 0.058(2) Uani 1 1 d . . . . .
O10 O 0.4391(2) 0.7192(3) 0.5623(4) 0.066(3) Uani 1 1 d . . . . .
O11 O 0.6104(3) 0.6148(4) 0.4457(5) 0.077(3) Uani 1 1 d . . . . .
O12 O 0.5668(2) 0.6509(4) 0.5440(4) 0.066(3) Uani 1 1 d . . . . .
N1 N 0.6462(3) 0.5735(4) 0.5061(5) 0.063(3) Uani 1 1 d . . . . .
N2 N 0.5816(3) 0.6438(4) 0.6472(4) 0.053(2) Uani 1 1 d . . . . .
C1 C 0.5796(3) 0.6320(5) 0.0700(7) 0.062(4) Uani 1 1 d . . . . .
H1A H 0.567497 0.611203 0.091201 0.074 Uiso 1 1 calc R . . . .
H1B H 0.568586 0.634412 0.027907 0.074 Uiso 1 1 calc R . . . .
C2 C 0.6135(3) 0.6158(3) 0.0696(5) 0.040(2) Uani 1 1 d . . . . .
C3 C 0.6317(4) 0.6277(4) 0.0234(6) 0.055(3) Uani 1 1 d . . . . .
H3 H 0.622684 0.646661 -0.007502 0.066 Uiso 1 1 calc R . . . .
C4 C 0.6628(4) 0.6118(5) 0.0232(8) 0.067(4) Uani 1 1 d . . . . .
H4 H 0.674303 0.619062 -0.008815 0.080 Uiso 1 1 calc R . . . .
C5 C 0.6766(3) 0.5860(5) 0.0683(8) 0.065(4) Uani 1 1 d . . . . .
H5 H 0.697918 0.576032 0.067690 0.078 Uiso 1 1 calc R . . . .
C6 C 0.6604(3) 0.5737(4) 0.1153(7) 0.061(3) Uani 1 1 d . . . . .
H6 H 0.670246 0.555522 0.146536 0.073 Uiso 1 1 calc R . . . .
C7 C 0.6286(3) 0.5893(4) 0.1152(6) 0.049(3) Uani 1 1 d . . . . .
H7 H 0.617176 0.581310 0.147075 0.059 Uiso 1 1 calc R . . . .
C8 C 0.6323(3) 0.7274(5) 0.4833(6) 0.055(3) Uani 1 1 d . . . . .
H8A H 0.625242 0.744273 0.516259 0.066 Uiso 1 1 calc R . . . .
H8B H 0.635551 0.697647 0.497598 0.066 Uiso 1 1 calc R . . . .
C9 C 0.6643(3) 0.7451(4) 0.4691(6) 0.051(3) Uani 1 1 d . . . . .
C10 C 0.6875(3) 0.7178(6) 0.4501(6) 0.066(4) Uani 1 1 d . . . . .
H10 H 0.683864 0.687958 0.447494 0.079 Uiso 1 1 calc R . . . .
C11 C 0.7172(4) 0.7361(9) 0.4344(9) 0.095(6) Uani 1 1 d . . . . .
H11 H 0.733082 0.718387 0.421067 0.114 Uiso 1 1 calc R . . . .
C12 C 0.7219(4) 0.7797(9) 0.4392(8) 0.091(6) Uani 1 1 d . . . . .
H12 H 0.741212 0.791587 0.429040 0.110 Uiso 1 1 calc R . . . .
C13 C 0.7000(4) 0.8055(7) 0.4577(8) 0.084(5) Uani 1 1 d . . . . .
H13 H 0.704142 0.835213 0.460873 0.101 Uiso 1 1 calc R . . . .
C14 C 0.6702(4) 0.7890(6) 0.4729(7) 0.071(4) Uani 1 1 d . . . . .
H14 H 0.654637 0.807725 0.485375 0.085 Uiso 1 1 calc R . . . .
C15 C 0.5875(3) 0.9162(4) 0.3448(6) 0.051(3) Uani 1 1 d . . . . .
H15A H 0.578222 0.936699 0.313508 0.061 Uiso 1 1 calc R . . . .
H15B H 0.572626 0.914573 0.375295 0.061 Uiso 1 1 calc R . . . .
C16 C 0.6197(3) 0.9336(4) 0.3755(6) 0.051(3) Uani 1 1 d . . . . .
C17 C 0.6209(4) 0.9547(5) 0.4324(7) 0.068(4) Uani 1 1 d . . . . .
H17 H 0.602063 0.956408 0.451115 0.082 Uiso 1 1 calc R . . . .
C18 C 0.6496(5) 0.9729(7) 0.4608(9) 0.101(6) Uani 1 1 d . . . . .
H18 H 0.650517 0.985542 0.499505 0.121 Uiso 1 1 calc R . . . .
C19 C 0.6779(5) 0.9722(7) 0.4303(9) 0.096(6) Uani 1 1 d . . . . .
H19 H 0.697166 0.986100 0.447590 0.115 Uiso 1 1 calc R . . . .
C20 C 0.6764(4) 0.9511(6) 0.3756(9) 0.084(5) Uani 1 1 d . . . . .
H20 H 0.695264 0.948521 0.356934 0.100 Uiso 1 1 calc R . . . .
C21 C 0.6466(4) 0.9329(5) 0.3468(7) 0.068(4) Uani 1 1 d . . . . .
H21 H 0.645481 0.920412 0.307969 0.082 Uiso 1 1 calc R . . . .
C22 C 0.5210(3) 0.5745(4) 0.4527(6) 0.046(3) Uani 1 1 d . . . . .
H22A H 0.530293 0.552836 0.428188 0.055 Uiso 1 1 calc R . . . .
H22B H 0.536941 0.580514 0.488826 0.055 Uiso 1 1 calc R . . . .
C23 C 0.4819(4) 0.5698(4) 0.5295(5) 0.053(3) Uani 1 1 d . . . . .
H23 H 0.495384 0.589066 0.554373 0.063 Uiso 1 1 calc R . . . .
C24 C 0.4900(3) 0.5571(3) 0.4724(5) 0.039(2) Uani 1 1 d . . . . .
C25 C 0.4690(3) 0.5296(4) 0.4362(6) 0.049(3) Uani 1 1 d . . . . .
H25 H 0.473894 0.521053 0.397903 0.059 Uiso 1 1 calc R . . . .
C26 C 0.4407(3) 0.5145(4) 0.4561(6) 0.057(3) Uani 1 1 d . . . . .
H26 H 0.426930 0.495801 0.431104 0.068 Uiso 1 1 calc R . . . .
C27 C 0.4328(4) 0.5266(4) 0.5117(7) 0.061(3) Uani 1 1 d . . . . .
H27 H 0.413418 0.516798 0.524296 0.073 Uiso 1 1 calc R . . . .
C28 C 0.4536(4) 0.5534(5) 0.5488(7) 0.067(4) Uani 1 1 d . . . . .
H28 H 0.448777 0.560790 0.587602 0.080 Uiso 1 1 calc R . . . .
C29 C 0.4191(3) 0.5684(3) 0.1929(5) 0.043(2) Uani 1 1 d . . . . .
H29A H 0.408968 0.575552 0.151376 0.052 Uiso 1 1 calc R . . . .
H29B H 0.439745 0.553826 0.190356 0.052 Uiso 1 1 calc R . . . .
C30 C 0.3974(3) 0.5392(4) 0.2212(5) 0.046(3) Uani 1 1 d . . . . .
C31 C 0.4091(4) 0.5110(4) 0.2692(6) 0.060(3) Uani 1 1 d . . . . .
H31 H 0.431462 0.510449 0.283722 0.072 Uiso 1 1 calc R . . . .
C32 C 0.3884(4) 0.4839(4) 0.2958(7) 0.068(4) Uani 1 1 d . . . . .
H32 H 0.396801 0.464842 0.327042 0.082 Uiso 1 1 calc R . . . .
C33 C 0.3555(4) 0.4853(5) 0.2758(7) 0.072(4) Uani 1 1 d . . . . .
H33 H 0.341341 0.467427 0.293812 0.086 Uiso 1 1 calc R . . . .
C34 C 0.3432(4) 0.5130(5) 0.2291(7) 0.064(4) Uani 1 1 d . . . . .
H34 H 0.320718 0.514036 0.215516 0.077 Uiso 1 1 calc R . . . .
C35 C 0.3641(3) 0.5393(4) 0.2026(7) 0.059(3) Uani 1 1 d . . . . .
H35 H 0.355386 0.557809 0.170877 0.070 Uiso 1 1 calc R . . . .
C36 C 0.5455(3) 0.7620(4) 0.5424(5) 0.051(3) Uani 1 1 d . U . . .
H36A H 0.549610 0.731180 0.548619 0.061 Uiso 1 1 calc R . . . .
H36B H 0.564891 0.774735 0.529308 0.061 Uiso 1 1 calc R . . . .
C37 C 0.5406(4) 0.7817(5) 0.6020(7) 0.065(3) Uani 1 1 d . U . . .
C38 C 0.5468(6) 0.7596(8) 0.6541(10) 0.112(5) Uani 1 1 d . U . . .
H38 H 0.548730 0.729546 0.654904 0.134 Uiso 1 1 calc R . . . .
C39 C 0.5503(8) 0.7859(9) 0.7108(11) 0.140(6) Uani 1 1 d . U . . .
H39 H 0.563082 0.775672 0.746390 0.168 Uiso 1 1 calc R . . . .
C40 C 0.5358(7) 0.8230(9) 0.7114(12) 0.124(5) Uani 1 1 d . U . . .
H40 H 0.530243 0.833770 0.748141 0.148 Uiso 1 1 calc R . . . .
C41 C 0.5286(5) 0.8459(8) 0.6596(9) 0.099(4) Uani 1 1 d . U . . .
H41 H 0.522529 0.874963 0.660263 0.119 Uiso 1 1 calc R . . . .
C42 C 0.5307(5) 0.8253(6) 0.6069(9) 0.085(4) Uani 1 1 d . U . . .
H42 H 0.525156 0.840873 0.570480 0.102 Uiso 1 1 calc R . . . .
C43 C 0.5032(3) 0.9478(4) 0.3997(5) 0.046(3) Uani 1 1 d . . . . .
H43A H 0.526117 0.949625 0.417637 0.055 Uiso 1 1 calc R . . . .
H43B H 0.498605 0.971640 0.370732 0.055 Uiso 1 1 calc R . . . .
C44 C 0.4823(3) 0.9526(3) 0.4494(5) 0.039(2) Uani 1 1 d . . . . .
C45 C 0.4933(4) 0.9388(4) 0.5077(6) 0.054(3) Uani 1 1 d . . . . .
H45 H 0.514278 0.927067 0.517536 0.064 Uiso 1 1 calc R . . . .
C46 C 0.4727(5) 0.9424(5) 0.5523(7) 0.076(5) Uani 1 1 d . . . . .
H46 H 0.479557 0.931954 0.591897 0.092 Uiso 1 1 calc R . . . .
C47 C 0.4425(5) 0.9613(6) 0.5382(10) 0.086(6) Uani 1 1 d . . . . .
H47 H 0.429349 0.964534 0.569015 0.103 Uiso 1 1 calc R . . . .
C48 C 0.4310(4) 0.9755(6) 0.4800(9) 0.081(5) Uani 1 1 d . . . . .
H48 H 0.410029 0.987121 0.470552 0.097 Uiso 1 1 calc R . . . .
C49 C 0.4511(4) 0.9720(4) 0.4366(8) 0.067(4) Uani 1 1 d . . . . .
H49 H 0.444066 0.982812 0.397286 0.081 Uiso 1 1 calc R . . . .
C50 C 0.4253(4) 0.8586(3) 0.4509(6) 0.054(3) Uani 1 1 d . . . . .
H50A H 0.447774 0.868888 0.458820 0.065 Uiso 1 1 calc R . . . .
H50B H 0.412022 0.881512 0.429520 0.065 Uiso 1 1 calc R . . . .
C56 C 0.3818(2) 0.8605(4) 0.5188(5) 0.087(5) Uani 1 1 d . U . . .
H56 H 0.367265 0.872386 0.486583 0.104 Uiso 1 1 calc R . . . .
C55 C 0.3715(3) 0.8530(5) 0.5755(7) 0.115(7) Uani 1 1 d G U . . .
H55 H 0.350182 0.859795 0.581248 0.138 Uiso 1 1 calc R . . . .
C54 C 0.3932(4) 0.8353(5) 0.6235(5) 0.132(9) Uani 1 1 d G U . . .
H54 H 0.386395 0.830218 0.661497 0.158 Uiso 1 1 calc R . . . .
C53 C 0.4252(4) 0.8251(5) 0.6149(5) 0.120(8) Uani 1 1 d G U . . .
H53 H 0.439690 0.813231 0.647080 0.144 Uiso 1 1 calc R . . . .
C52 C 0.4354(2) 0.8326(4) 0.5582(5) 0.077(4) Uani 1 1 d G U . . .
H52 H 0.456773 0.825822 0.552415 0.092 Uiso 1 1 calc R . . . .
C51 C 0.4137(2) 0.8504(3) 0.5101(4) 0.051(3) Uani 1 1 d G U . . .
C57 C 0.3380(3) 0.7599(4) 0.1965(6) 0.054(3) Uani 1 1 d . . . . .
H57A H 0.344705 0.772145 0.159527 0.065 Uiso 1 1 calc R . . . .
H57B H 0.330028 0.730657 0.186817 0.065 Uiso 1 1 calc R . . . .
C59 C 0.3106(3) 0.7868(4) 0.2150(5) 0.046(3) Uani 1 1 d . . . . .
C60 C 0.3107(4) 0.8314(5) 0.2080(8) 0.069(4) Uani 1 1 d . . . . .
H60 H 0.328322 0.844791 0.193430 0.083 Uiso 1 1 calc R . . . .
C61 C 0.2851(5) 0.8563(7) 0.2225(10) 0.100(6) Uani 1 1 d . U . . .
H61 H 0.285449 0.886369 0.217981 0.120 Uiso 1 1 calc R . . . .
C62 C 0.2592(5) 0.8367(7) 0.2433(9) 0.095(6) Uani 1 1 d . U . . .
H62 H 0.242014 0.853317 0.254120 0.114 Uiso 1 1 calc R . . . .
C63 C 0.2584(4) 0.7938(7) 0.2483(8) 0.084(5) Uani 1 1 d . U . . .
H63 H 0.240085 0.780742 0.260641 0.101 Uiso 1 1 calc R . . . .
C64 C 0.2839(3) 0.7679(6) 0.2357(7) 0.067(4) Uani 1 1 d . . . . .
H64 H 0.283133 0.738001 0.241132 0.081 Uiso 1 1 calc R . . . .
C65 C 0.500000 0.5177(4) 0.250000 0.046(4) Uani 1 2 d DS T P B .
C66 C 0.500000 0.4681(5) 0.250000 0.060(5) Uani 1 2 d DS TU P . .
C67 C 0.6729(3) 0.6391(4) 0.2986(6) 0.044(2) Uani 1 1 d . . . . .
C68 C 0.7073(3) 0.6185(5) 0.3179(8) 0.068(4) Uani 1 1 d . . . . .
C69 C 0.5861(3) 0.8648(4) 0.5065(6) 0.050(3) Uani 1 1 d . . . . .
C70 C 0.6049(3) 0.8856(4) 0.5644(6) 0.074(3) Uani 1 1 d D U . . .
C71 C 0.500000 1.0010(8) 0.250000 0.088(7) Uani 1 2 d DS TU P . .
C72 C 0.4912(7) 1.0476(8) 0.2632(9) 0.084(10) Uani 0.5 1 d D U . . .
C73 C 0.3741(3) 0.9288(4) 0.3231(6) 0.054(3) Uani 1 1 d . . . . .
C74 C 0.3531(4) 0.9690(6) 0.3359(10) 0.087(5) Uani 1 1 d . . . . .
C75 C 0.4586(3) 0.6912(4) 0.5827(6) 0.050(3) Uani 1 1 d . . . . .
C76 C 0.4545(5) 0.6733(6) 0.6475(7) 0.073(4) Uani 1 1 d . . . . .
C77 C 0.2883(3) 0.7245(4) 0.3915(6) 0.051(3) Uani 1 1 d . . . . .
C78 C 0.2963(4) 0.6857(4) 0.3667(6) 0.056(3) Uani 1 1 d . . . . .
H78 H 0.318154 0.677040 0.369417 0.067 Uiso 1 1 calc R . . . .
C79 C 0.2714(4) 0.6599(5) 0.3376(7) 0.067(4) Uani 1 1 d . . . . .
H79 H 0.276669 0.633653 0.320558 0.080 Uiso 1 1 calc R . . . .
C80 C 0.2383(4) 0.6723(5) 0.3330(7) 0.070(4) Uani 1 1 d . . . . .
H80 H 0.221857 0.654308 0.313563 0.084 Uiso 1 1 calc R . . . .
C81 C 0.2307(4) 0.7107(5) 0.3573(7) 0.067(4) Uani 1 1 d . . . . .
H81 H 0.208994 0.719819 0.354299 0.080 Uiso 1 1 calc R . . . .
C82 C 0.2562(4) 0.7366(6) 0.3869(7) 0.068(4) Uani 1 1 d . . . . .
H82 H 0.251079 0.762859 0.403986 0.082 Uiso 1 1 calc R . . . .
C83 C 0.3281(3) 0.7332(4) 0.5095(6) 0.053(3) Uani 1 1 d . . . . .
C84 C 0.3567(3) 0.7406(5) 0.5461(7) 0.062(3) Uani 1 1 d . . . . .
H84 H 0.372828 0.757132 0.531474 0.075 Uiso 1 1 calc R . . . .
C85 C 0.3627(4) 0.7235(6) 0.6068(9) 0.081(5) Uani 1 1 d . . . . .
H85 H 0.382484 0.728929 0.631969 0.097 Uiso 1 1 calc R . . . .
C86 C 0.3389(5) 0.6987(5) 0.6278(7) 0.072(4) Uani 1 1 d . . . . .
H86 H 0.342580 0.687489 0.667619 0.087 Uiso 1 1 calc R . . . .
C87 C 0.3098(4) 0.6904(5) 0.5911(8) 0.067(4) Uani 1 1 d . . . . .
H87 H 0.293911 0.673305 0.605604 0.080 Uiso 1 1 calc R . . . .
C88 C 0.3039(3) 0.7078(4) 0.5306(6) 0.057(3) Uani 1 1 d . . . . .
H88 H 0.284141 0.702464 0.505291 0.068 Uiso 1 1 calc R . . . .
C89 C 0.3045(4) 0.8088(4) 0.4433(7) 0.060(3) Uani 1 1 d . . . . .
C90 C 0.3041(4) 0.8402(5) 0.3954(7) 0.072(4) Uani 1 1 d . . . . .
H90 H 0.313684 0.833938 0.360537 0.087 Uiso 1 1 calc R . . . .
C91 C 0.2896(5) 0.8796(6) 0.4012(10) 0.096(6) Uani 1 1 d . . . . .
H91 H 0.288718 0.899801 0.369469 0.116 Uiso 1 1 calc R . . . .
C92 C 0.2761(6) 0.8899(6) 0.4531(11) 0.097(6) Uani 1 1 d . . . . .
H92 H 0.267297 0.917415 0.457157 0.117 Uiso 1 1 calc R . . . .
C93 C 0.2758(5) 0.8604(5) 0.4979(9) 0.083(5) Uani 1 1 d . . . . .
H93 H 0.265913 0.867094 0.532302 0.100 Uiso 1 1 calc R . . . .
C94 C 0.2900(4) 0.8202(5) 0.4934(8) 0.075(5) Uani 1 1 d . . . . .
H94 H 0.289659 0.800320 0.525170 0.090 Uiso 1 1 calc R . . . .
C95 C 0.6161(4) 0.5876(6) 0.4808(8) 0.079(4) Uani 1 1 d . . . . .
H95 H 0.598235 0.573553 0.493345 0.095 Uiso 1 1 calc R . . . .
C96 C 0.6482(4) 0.5386(7) 0.5519(9) 0.090(5) Uani 1 1 d . . . . .
H96A H 0.659512 0.514172 0.537743 0.135 Uiso 1 1 calc GR . . . .
H96B H 0.626447 0.530036 0.557827 0.135 Uiso 1 1 calc GR . . . .
H96C H 0.659991 0.548772 0.590301 0.135 Uiso 1 1 calc GR . . . .
C97 C 0.6749(5) 0.5917(8) 0.4935(12) 0.122(9) Uani 1 1 d . . . . .
H97A H 0.689819 0.595103 0.531179 0.184 Uiso 1 1 calc GR . . . .
H97B H 0.670375 0.619588 0.474626 0.184 Uiso 1 1 calc GR . . . .
H97C H 0.684620 0.573117 0.466024 0.184 Uiso 1 1 calc GR . . . .
C98 C 0.5868(4) 0.6527(5) 0.5903(7) 0.061(3) Uani 1 1 d . . . . .
H98 H 0.607976 0.661276 0.585422 0.073 Uiso 1 1 calc R . . . .
C99 C 0.6068(5) 0.6468(7) 0.7001(7) 0.087(5) Uani 1 1 d . . . . .
H99A H 0.627781 0.650878 0.686621 0.131 Uiso 1 1 calc GR . . . .
H99B H 0.607161 0.620589 0.723841 0.131 Uiso 1 1 calc GR . . . .
H99C H 0.602308 0.671074 0.725155 0.131 Uiso 1 1 calc GR . . . .
C100 C 0.5508(6) 0.6322(9) 0.6574(10) 0.122(8) Uani 1 1 d . U . . .
H10A H 0.535224 0.639126 0.621667 0.182 Uiso 1 1 calc GR . . . .
H10B H 0.545234 0.647774 0.692336 0.182 Uiso 1 1 calc GR . . . .
H10C H 0.550222 0.601550 0.665169 0.182 Uiso 1 1 calc GR . . . .
O1W O 0.6858(4) 0.6076(4) 0.6681(7) 0.106(4) Uani 1 1 d . . . . .
H1WA H 0.685713 0.611949 0.706339 0.160 Uiso 1 1 d R . . . .
H1WB H 0.680643 0.631989 0.651329 0.160 Uiso 1 1 d R . . . .
O13 O 0.6681(4) 0.6939(5) 0.6269(7) 0.117(5) Uani 1 1 d . U . . .
N3 N 0.6771(5) 0.7639(7) 0.6562(10) 0.115(5) Uani 1 1 d . U . . .
C101 C 0.6847(5) 0.7277(8) 0.6312(10) 0.098(5) Uani 1 1 d . U . . .
H101 H 0.704376 0.726993 0.615096 0.117 Uiso 1 1 calc R . . . .
C102 C 0.6954(8) 0.8036(10) 0.6567(16) 0.167(10) Uani 1 1 d . U . . .
H10D H 0.712333 0.803904 0.691749 0.251 Uiso 1 1 calc GR . . . .
H10E H 0.680908 0.827805 0.659007 0.251 Uiso 1 1 calc GR . . . .
H10F H 0.705141 0.805629 0.619619 0.251 Uiso 1 1 calc GR . . . .
C103 C 0.6455(9) 0.7688(13) 0.6803(18) 0.192(12) Uani 1 1 d . U . . .
H10G H 0.628437 0.775567 0.647032 0.288 Uiso 1 1 calc GR . . . .
H10H H 0.647323 0.791821 0.710152 0.288 Uiso 1 1 calc GR . . . .
H10I H 0.640322 0.742134 0.699472 0.288 Uiso 1 1 calc GR . . . .
O14 O 0.7451(5) 1.0063(7) 0.6314(11) 0.158(7) Uani 1 1 d . U . . .
N4 N 0.7207(4) 0.9419(6) 0.5968(9) 0.098(5) Uani 1 1 d . U . . .
C104 C 0.7386(6) 0.9768(8) 0.5895(12) 0.106(6) Uani 1 1 d . U . . .
H104 H 0.746893 0.980197 0.552572 0.127 Uiso 1 1 calc R . . . .
C105 C 0.7045(5) 0.9339(7) 0.6545(11) 0.108(7) Uani 1 1 d . U . . .
H10J H 0.712122 0.955223 0.685237 0.162 Uiso 1 1 calc GR . . . .
H10K H 0.710278 0.905389 0.670415 0.162 Uiso 1 1 calc GR . . . .
H10L H 0.681104 0.935971 0.644110 0.162 Uiso 1 1 calc GR . . . .
C106 C 0.7182(7) 0.9070(9) 0.5499(13) 0.138(9) Uani 1 1 d . U . . .
H10M H 0.730739 0.882273 0.566524 0.207 Uiso 1 1 calc GR . . . .
H10N H 0.726659 0.917258 0.514033 0.207 Uiso 1 1 calc GR . . . .
H10O H 0.695606 0.898749 0.538911 0.207 Uiso 1 1 calc GR . . . .
O15 O 0.3189(5) 0.6089(5) 0.7044(7) 0.116(5) Uani 1 1 d . . . . .
N5 N 0.3311(4) 0.5664(5) 0.6286(6) 0.083(4) Uani 1 1 d . . . . .
C107 C 0.3111(6) 0.5832(7) 0.6647(9) 0.089(5) Uani 1 1 d . . . . .
H107 H 0.289274 0.574045 0.658370 0.107 Uiso 1 1 calc R . . . .
C108 C 0.3655(5) 0.5760(7) 0.6375(9) 0.097(6) Uani 1 1 d . . . . .
H10P H 0.369616 0.601025 0.663656 0.146 Uiso 1 1 calc GR . . . .
H10Q H 0.372416 0.581875 0.598409 0.146 Uiso 1 1 calc GR . . . .
H10R H 0.377469 0.551612 0.656496 0.146 Uiso 1 1 calc GR . . . .
C109 C 0.3193(6) 0.5320(7) 0.5826(10) 0.114(7) Uani 1 1 d . U . . .
H10S H 0.295927 0.528826 0.580174 0.170 Uiso 1 1 calc GR . . . .
H10T H 0.329804 0.504927 0.595105 0.170 Uiso 1 1 calc GR . . . .
H10U H 0.324565 0.540089 0.542900 0.170 Uiso 1 1 calc GR . . . .
O16 O 0.2643(5) 0.4906(8) 0.4448(10) 0.157(7) Uani 1 1 d D U . . .
N6 N 0.2545(5) 0.4961(7) 0.3413(10) 0.119(6) Uani 1 1 d . U . . .
C110 C 0.2662(6) 0.4757(9) 0.3935(12) 0.122(8) Uani 1 1 d D U . . .
H110 H 0.276322 0.448861 0.390932 0.146 Uiso 1 1 calc R . . . .
C111 C 0.2389(7) 0.5395(10) 0.3450(16) 0.152(10) Uani 1 1 d . U . . .
H11A H 0.236657 0.545747 0.387043 0.228 Uiso 1 1 calc GR . . . .
H11B H 0.217536 0.539470 0.320407 0.228 Uiso 1 1 calc GR . . . .
H11C H 0.252332 0.561317 0.329818 0.228 Uiso 1 1 calc GR . . . .
C112 C 0.2568(7) 0.4755(10) 0.2761(14) 0.147(10) Uani 1 1 d . U . . .
H11D H 0.276374 0.458153 0.278562 0.220 Uiso 1 1 calc GR . . . .
H11E H 0.257592 0.498224 0.246391 0.220 Uiso 1 1 calc GR . . . .
H11F H 0.237928 0.457521 0.263679 0.220 Uiso 1 1 calc GR . . . .
O17 O 0.3317(10) 0.8834(13) 0.7297(19) 0.131(13) Uiso 0.53(4) 1 d D . . D 1
O18 O 0.3219(18) 0.905(3) 0.697(4) 0.22(3) Uiso 0.47(4) 1 d D . . D 2
N7 N 0.3750(5) 0.9251(7) 0.7146(9) 0.113(6) Uiso 1 1 d D . . . .
C113 C 0.3609(11) 0.8852(19) 0.749(2) 0.134(19) Uiso 0.53(4) 1 d D . . D 1
C114 C 0.3935(15) 0.900(2) 0.767(2) 0.15(2) Uiso 0.47(4) 1 d D . . D 2
C116 C 0.4090(10) 0.942(2) 0.740(3) 0.18(3) Uiso 0.53(4) 1 d D . . D 1
C117 C 0.3632(19) 0.948(2) 0.655(2) 0.19(3) Uiso 0.53(4) 1 d D . . D 1
C118 C 0.3414(19) 0.929(2) 0.680(4) 0.16(3) Uiso 0.47(4) 1 d D . . D 2
F7A F 0.6226(14) 0.8603(15) 0.605(2) 0.129(13) Uani 0.35(3) 1 d D U . C 2
F8A F 0.6235(12) 0.9175(13) 0.5482(19) 0.120(12) Uani 0.35(3) 1 d D U . C 2
F9A F 0.5838(7) 0.9100(10) 0.5901(15) 0.074(8) Uani 0.35(3) 1 d D U . C 2
Ag1 Ag 0.4443(5) 0.7517(4) 0.4723(6) 0.080(2) Uani 0.49(5) 1 d . U . A 2
Ag0A Ag 0.38247(3) 0.83223(4) 0.29662(6) 0.0792(3) Uani 1 1 d . U . . .
C119 C 0.3999(15) 0.955(2) 0.693(4) 0.16(3) Uiso 0.47(4) 1 d D . . D 2


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag2 Ag3 2.9287(9) . ?
Ag2 Ag4 3.0215(9) 2_655 ?
Ag2 Ag5 2.9124(9) . ?
Ag2 Ag6 2.9110(9) 2_655 ?
Ag2 Ag7 2.9063(9) 2_655 ?
Ag2 Ag10 3.0217(9) 2_655 ?
Ag2 Ag12 2.9991(10) 2_655 ?
Ag2 Pd1 2.8081(6) . ?
Ag2 S9 2.537(2) . ?
Ag3 Ag3 3.0768(12) 2_655 ?
Ag3 Ag4 2.8899(9) 2_655 ?
Ag3 Ag6 3.0131(9) . ?
Ag3 Ag6 2.9217(9) 2_655 ?
Ag3 Ag8 3.0217(9) . ?
Ag3 Ag8 2.9878(9) 2_655 ?
Ag3 Ag11 3.0692(9) 2_655 ?
Ag3 Ag12 3.0221(10) 2_655 ?
Ag3 Pd1 2.8094(9) . ?
Ag3 S5 2.585(2) . ?
Ag4 Ag5 2.9181(9) . ?
Ag4 Ag6 2.9125(9) 2_655 ?
Ag4 Ag7 3.0609(9) . ?
Ag4 Ag9 2.9862(9) . ?
Ag4 Ag10 3.0449(9) . ?
Ag4 Ag11 3.0419(9) . ?
Ag4 Ag14 3.1074(10) . ?
Ag4 Pd1 2.8040(6) . ?
Ag4 S6 2.590(3) . ?
Ag5 Ag6 2.9107(9) 2_655 ?
Ag5 Ag7 3.0218(9) . ?
Ag5 Ag7 2.9135(9) 2_655 ?
Ag5 Ag9 2.9992(9) . ?
Ag5 Ag15 3.0118(11) . ?
Ag5 Pd1 2.8052(7) . ?
Ag5 S8 2.532(2) . ?
Ag6 Ag8 2.9892(9) 2_655 ?
Ag6 Ag14 3.0054(10) 2_655 ?
Ag6 Pd1 2.7938(7) . ?
Ag6 S1 2.520(2) . ?
Ag7 Ag7 2.9088(12) 2_655 ?
Ag7 Ag9 3.0366(9) . ?
Ag7 Ag10 2.9838(9) . ?
Ag7 Ag13 2.9816(11) . ?
Ag7 Ag15 3.0644(10) 2_655 ?
Ag7 Pd1 2.8057(9) . ?
Ag7 S3 2.606(2) . ?
Ag8 Ag8 3.2499(14) 2_655 ?
Ag8 S4 2.461(2) . ?
Ag8 S5 2.462(2) . ?
Ag8 O1 2.346(7) . ?
Ag9 Ag10 3.2233(11) . ?
Ag9 S6 2.457(3) . ?
Ag9 S7 2.454(2) . ?
Ag9 O5 2.340(8) . ?
Ag10 S2 2.474(2) . ?
Ag10 S3 2.460(2) . ?
Ag10 O4 2.346(9) . ?
Ag11 Ag12 2.9940(11) . ?
Ag11 Ag14 3.0656(11) . ?
Ag11 S2 2.456(2) . ?
Ag11 S4 2.447(2) . ?
Ag11 O11 2.528(9) . ?
Ag11 O12 2.488(9) . ?
Ag12 Ag16 2.9606(13) 2_655 ?
Ag12 S2 2.499(2) . ?
Ag12 S5 2.560(2) 2_655 ?
Ag12 O3 2.298(7) . ?
Ag13 Ag15 2.9448(10) 2_655 ?
Ag13 Ag15 2.9447(10) . ?
Ag13 S7 2.450(2) 2_655 ?
Ag13 S7 2.450(2) . ?
Ag13 O6 2.505(14) 2_655 ?
Ag13 O6 2.505(14) . ?
Ag14 Ag17 3.009(9) . ?
Ag14 S4 2.487(2) . ?
Ag14 S6 2.574(3) . ?
Ag14 O9 2.316(8) . ?
Ag14 Ag1 2.855(11) . ?
Ag15 S3 2.591(3) 2_655 ?
Ag15 S7 2.480(3) . ?
Ag15 O8 2.282(8) . ?
Ag15 Ag0A 2.8782(16) . ?
Ag16 Ag20 3.096(5) . ?
Ag16 S1 2.456(3) 2_655 ?
Ag16 S9 2.602(3) . ?
Ag16 O2 2.260(8) 2_655 ?
Ag17 Ag19 3.239(12) . ?
Ag17 S1 2.539(9) 2_655 ?
Ag17 S8 2.493(8) . ?
Ag17 O10 2.208(11) . ?
Ag19 S8 2.634(4) . ?
Ag19 S9 2.717(4) . ?
Ag19 P1 2.405(4) . ?
Ag19 Ag0A 2.811(6) . ?
Ag20 S1 2.779(9) 2_655 ?
Ag20 S8 2.767(5) . ?
Ag20 S9 2.951(9) . ?
Ag20 P1 2.451(5) . ?
Ag20 Ag1 3.16(2) . ?
Ag20 Ag0A 3.345(10) . ?
S1 C1 1.836(12) . ?
S1 Ag1 2.776(18) 2_655 ?
S2 C8 1.855(12) . ?
S3 C15 1.832(11) . ?
S3 Ag0A 2.900(3) 2_655 ?
S4 C22 1.864(10) . ?
S5 C29 1.849(10) . ?
S6 C36 1.832(11) . ?
S6 Ag1 2.77(2) . ?
S7 C43 1.852(11) . ?
S8 C50 1.839(11) . ?
S8 Ag1 2.481(10) . ?
S8 Ag0A 2.707(3) . ?
S9 C57 1.854(12) . ?
S9 Ag0A 2.464(3) . ?
P1 C77 1.826(14) . ?
P1 C83 1.808(14) . ?
P1 C89 1.790(16) . ?
F1 C66 1.343(15) . ?
F2 F3 1.01(3) 2_655 ?
F2 C66 1.298(13) . ?
F3 C66 1.239(15) . ?
F4 C68 1.307(19) . ?
F5 C68 1.300(18) . ?
F6 C68 1.339(19) . ?
F7 C70 1.334(14) . ?
F8 C70 1.322(14) . ?
F9 C70 1.299(14) . ?
F10 C72 1.350(10) . ?
F11 C72 1.50(4) 2_655 ?
F11 C72 1.344(10) . ?
F12 C74 1.27(2) . ?
F13 C74 1.29(2) . ?
F14 C74 1.30(2) . ?
F15 C76 1.23(2) . ?
F16 C76 1.289(19) . ?
F17 C76 1.33(2) . ?
O1 C65 1.240(9) . ?
O2 C67 1.240(14) . ?
O3 C67 1.239(14) . ?
O4 C69 1.246(15) . ?
O5 C69 1.213(14) . ?
O6 C71 1.244(14) . ?
O7 C73 1.234(16) . ?
O7 Ag0A 2.243(10) . ?
O8 C73 1.204(15) . ?
O9 C75 1.249(14) . ?
O10 C75 1.217(16) . ?
O10 Ag1 2.252(12) . ?
O11 C95 1.139(19) . ?
O12 C98 1.211(16) . ?
N1 C95 1.351(19) . ?
N1 C96 1.466(19) . ?
N1 C97 1.37(2) . ?
N2 C98 1.328(17) . ?
N2 C99 1.443(18) . ?
N2 C100 1.37(2) . ?
C1 H1A 0.9700 . ?
C1 H1B 0.9700 . ?
C1 C2 1.486(16) . ?
C2 C3 1.394(17) . ?
C2 C7 1.366(17) . ?
C3 H3 0.9300 . ?
C3 C4 1.369(19) . ?
C4 H4 0.9300 . ?
C4 C5 1.33(2) . ?
C5 H5 0.9300 . ?
C5 C6 1.36(2) . ?
C6 H6 0.9300 . ?
C6 C7 1.394(18) . ?
C7 H7 0.9300 . ?
C8 H8A 0.9700 . ?
C8 H8B 0.9700 . ?
C8 C9 1.496(18) . ?
C9 C10 1.38(2) . ?
C9 C14 1.38(2) . ?
C10 H10 0.9300 . ?
C10 C11 1.44(3) . ?
C11 H11 0.9300 . ?
C11 C12 1.36(3) . ?
C12 H12 0.9300 . ?
C12 C13 1.31(3) . ?
C13 H13 0.9300 . ?
C13 C14 1.41(2) . ?
C14 H14 0.9300 . ?
C15 H15A 0.9700 . ?
C15 H15B 0.9700 . ?
C15 C16 1.494(16) . ?
C16 C17 1.402(19) . ?
C16 C21 1.35(2) . ?
C17 H17 0.9300 . ?
C17 C18 1.37(2) . ?
C18 H18 0.9300 . ?
C18 C19 1.43(3) . ?
C19 H19 0.9300 . ?
C19 C20 1.36(2) . ?
C20 H20 0.9300 . ?
C20 C21 1.411(19) . ?
C21 H21 0.9300 . ?
C22 H22A 0.9700 . ?
C22 H22B 0.9700 . ?
C22 C24 1.505(15) . ?
C23 H23 0.9300 . ?
C23 C24 1.398(16) . ?
C23 C28 1.39(2) . ?
C24 C25 1.376(16) . ?
C25 H25 0.9300 . ?
C25 C26 1.380(18) . ?
C26 H26 0.9300 . ?
C26 C27 1.36(2) . ?
C27 H27 0.9300 . ?
C27 C28 1.37(2) . ?
C28 H28 0.9300 . ?
C29 H29A 0.9700 . ?
C29 H29B 0.9700 . ?
C29 C30 1.465(16) . ?
C30 C31 1.394(18) . ?
C30 C35 1.372(18) . ?
C31 H31 0.9300 . ?
C31 C32 1.382(19) . ?
C32 H32 0.9300 . ?
C32 C33 1.36(2) . ?
C33 H33 0.9300 . ?
C33 C34 1.37(2) . ?
C34 H34 0.9300 . ?
C34 C35 1.369(18) . ?
C35 H35 0.9300 . ?
C36 H36A 0.9700 . ?
C36 H36B 0.9700 . ?
C36 C37 1.479(19) . ?
C37 C38 1.32(2) . ?
C37 C42 1.41(2) . ?
C38 H38 0.9300 . ?
C38 C39 1.47(3) . ?
C39 H39 0.9300 . ?
C39 C40 1.29(3) . ?
C40 H40 0.9300 . ?
C40 C41 1.33(3) . ?
C41 H41 0.9300 . ?
C41 C42 1.33(3) . ?
C42 H42 0.9300 . ?
C43 H43A 0.9700 . ?
C43 H43B 0.9700 . ?
C43 C44 1.491(16) . ?
C44 C45 1.362(16) . ?
C44 C49 1.407(18) . ?
C45 H45 0.9300 . ?
C45 C46 1.39(2) . ?
C46 H46 0.9300 . ?
C46 C47 1.37(3) . ?
C47 H47 0.9300 . ?
C47 C48 1.37(3) . ?
C48 H48 0.9300 . ?
C48 C49 1.35(2) . ?
C49 H49 0.9300 . ?
C50 H50A 0.9700 . ?
C50 H50B 0.9700 . ?
C50 C51 1.470(14) . ?
C56 H56 0.9300 . ?
C56 C55 1.3900 . ?
C56 C51 1.3900 . ?
C55 H55 0.9300 . ?
C55 C54 1.3900 . ?
C54 H54 0.9300 . ?
C54 C53 1.3900 . ?
C53 H53 0.9300 . ?
C53 C52 1.3900 . ?
C52 H52 0.9300 . ?
C52 C51 1.3900 . ?
C57 H57A 0.9700 . ?
C57 H57B 0.9700 . ?
C57 C59 1.500(17) . ?
C59 C60 1.383(19) . ?
C59 C64 1.376(18) . ?
C60 H60 0.9300 . ?
C60 C61 1.38(2) . ?
C61 H61 0.9300 . ?
C61 C62 1.36(3) . ?
C62 H62 0.9300 . ?
C62 C63 1.33(3) . ?
C63 H63 0.9300 . ?
C63 C64 1.38(2) . ?
C64 H64 0.9300 . ?
C65 C66 1.528(15) . ?
C67 C68 1.554(17) . ?
C69 C70 1.527(17) . ?
C70 F7A 1.317(17) . ?
C70 F8A 1.327(17) . ?
C70 F9A 1.335(16) . ?
C71 C72 1.518(18) 2_655 ?
C71 C72 1.518(18) . ?
C72 C72 0.99(5) 2_655 ?
C73 C74 1.557(19) . ?
C75 C76 1.557(18) . ?
C77 C78 1.374(18) . ?
C77 C82 1.36(2) . ?
C78 H78 0.9300 . ?
C78 C79 1.38(2) . ?
C79 H79 0.9300 . ?
C79 C80 1.40(2) . ?
C80 H80 0.9300 . ?
C80 C81 1.35(2) . ?
C81 H81 0.9300 . ?
C81 C82 1.40(2) . ?
C82 H82 0.9300 . ?
C83 C84 1.344(19) . ?
C83 C88 1.396(18) . ?
C84 H84 0.9300 . ?
C84 C85 1.42(2) . ?
C85 H85 0.9300 . ?
C85 C86 1.37(2) . ?
C86 H86 0.9300 . ?
C86 C87 1.37(2) . ?
C87 H87 0.9300 . ?
C87 C88 1.42(2) . ?
C88 H88 0.9300 . ?
C89 C90 1.43(2) . ?
C89 C94 1.37(2) . ?
C90 H90 0.9300 . ?
C90 C91 1.37(3) . ?
C91 H91 0.9300 . ?
C91 C92 1.37(3) . ?
C92 H92 0.9300 . ?
C92 C93 1.34(3) . ?
C93 H93 0.9300 . ?
C93 C94 1.38(2) . ?
C94 H94 0.9300 . ?
C95 H95 0.9300 . ?
C96 H96A 0.9600 . ?
C96 H96B 0.9600 . ?
C96 H96C 0.9600 . ?
C97 H97A 0.9600 . ?
C97 H97B 0.9600 . ?
C97 H97C 0.9600 . ?
C98 H98 0.9300 . ?
C99 H99A 0.9600 . ?
C99 H99B 0.9600 . ?
C99 H99C 0.9600 . ?
C100 H10A 0.9600 . ?
C100 H10B 0.9600 . ?
C100 H10C 0.9600 . ?
O1W H1WA 0.8505 . ?
O1W H1WB 0.8491 . ?
O13 C101 1.24(2) . ?
N3 C101 1.30(3) . ?
N3 C102 1.43(3) . ?
N3 C103 1.48(3) . ?
C101 H101 0.9300 . ?
C102 H10D 0.9600 . ?
C102 H10E 0.9600 . ?
C102 H10F 0.9600 . ?
C103 H10G 0.9600 . ?
C103 H10H 0.9600 . ?
C103 H10I 0.9600 . ?
O14 C104 1.29(3) . ?
N4 C104 1.33(3) . ?
N4 C105 1.53(3) . ?
N4 C106 1.48(3) . ?
C104 H104 0.9300 . ?
C105 H10J 0.9600 . ?
C105 H10K 0.9600 . ?
C105 H10L 0.9600 . ?
C106 H10M 0.9600 . ?
C106 H10N 0.9600 . ?
C106 H10O 0.9600 . ?
O15 C107 1.19(2) . ?
N5 C107 1.33(2) . ?
N5 C108 1.43(2) . ?
N5 C109 1.50(2) . ?
C107 H107 0.9300 . ?
C108 H10P 0.9600 . ?
C108 H10Q 0.9600 . ?
C108 H10R 0.9600 . ?
C109 H10S 0.9600 . ?
C109 H10T 0.9600 . ?
C109 H10U 0.9600 . ?
O16 C110 1.229(17) . ?
N6 C110 1.33(3) . ?
N6 C111 1.49(3) . ?
N6 C112 1.58(3) . ?
C110 H110 0.9300 . ?
C111 H11A 0.9600 . ?
C111 H11B 0.9600 . ?
C111 H11C 0.9600 . ?
C112 H11D 0.9600 . ?
C112 H11E 0.9600 . ?
C112 H11F 0.9600 . ?
O17 C113 1.21(2) . ?
O18 C118 1.20(2) . ?
N7 C113 1.59(6) . ?
N7 C114 1.50(2) . ?
N7 C116 1.52(2) . ?
N7 C117 1.51(2) . ?
N7 C118 1.48(8) . ?
N7 C119 1.51(2) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Ag3 Ag2 Ag4 58.09(2) . 2_655 ?
Ag3 Ag2 Ag10 112.42(3) . 2_655 ?
Ag3 Ag2 Ag12 61.29(2) . 2_655 ?
Ag4 Ag2 Ag10 60.51(2) 2_655 2_655 ?
Ag5 Ag2 Ag3 108.41(3) . . ?
Ag5 Ag2 Ag4 108.69(3) . 2_655 ?
Ag5 Ag2 Ag10 115.42(3) . 2_655 ?
Ag5 Ag2 Ag12 153.46(3) . 2_655 ?
Ag6 Ag2 Ag3 60.04(2) 2_655 . ?
Ag6 Ag2 Ag4 106.31(3) 2_655 2_655 ?
Ag6 Ag2 Ag5 59.98(2) 2_655 . ?
Ag6 Ag2 Ag10 165.08(3) 2_655 2_655 ?
Ag6 Ag2 Ag12 95.63(3) 2_655 2_655 ?
Ag7 Ag2 Ag3 109.02(3) 2_655 . ?
Ag7 Ag2 Ag4 62.14(2) 2_655 2_655 ?
Ag7 Ag2 Ag5 60.09(2) 2_655 . ?
Ag7 Ag2 Ag6 108.30(3) 2_655 2_655 ?
Ag7 Ag2 Ag10 60.41(2) 2_655 2_655 ?
Ag7 Ag2 Ag12 144.92(3) 2_655 2_655 ?
Ag12 Ag2 Ag4 87.06(3) 2_655 2_655 ?
Ag12 Ag2 Ag10 90.81(3) 2_655 2_655 ?
Pd1 Ag2 Ag3 58.60(2) . . ?
Pd1 Ag2 Ag4 57.359(17) . 2_655 ?
Pd1 Ag2 Ag5 58.696(19) . . ?
Pd1 Ag2 Ag6 58.45(2) . 2_655 ?
Pd1 Ag2 Ag7 58.78(2) . 2_655 ?
Pd1 Ag2 Ag10 106.71(3) . 2_655 ?
Pd1 Ag2 Ag12 119.66(3) . 2_655 ?
S9 Ag2 Ag3 129.73(6) . . ?
S9 Ag2 Ag4 147.56(6) . 2_655 ?
S9 Ag2 Ag5 98.22(6) . . ?
S9 Ag2 Ag6 102.67(6) . 2_655 ?
S9 Ag2 Ag7 121.22(6) . 2_655 ?
S9 Ag2 Ag10 91.94(6) . 2_655 ?
S9 Ag2 Ag12 75.80(6) . 2_655 ?
S9 Ag2 Pd1 154.77(6) . . ?
Ag2 Ag3 Ag3 107.15(2) . 2_655 ?
Ag2 Ag3 Ag6 108.12(3) . . ?
Ag2 Ag3 Ag8 115.36(3) . . ?
Ag2 Ag3 Ag8 165.13(3) . 2_655 ?
Ag2 Ag3 Ag11 93.61(2) . 2_655 ?
Ag2 Ag3 Ag12 60.50(2) . 2_655 ?
Ag4 Ag3 Ag2 62.56(2) 2_655 . ?
Ag4 Ag3 Ag3 105.81(2) 2_655 2_655 ?
Ag4 Ag3 Ag6 109.57(3) 2_655 2_655 ?
Ag4 Ag3 Ag6 59.09(2) 2_655 . ?
Ag4 Ag3 Ag8 112.12(3) 2_655 2_655 ?
Ag4 Ag3 Ag8 163.88(3) 2_655 . ?
Ag4 Ag3 Ag11 61.30(2) 2_655 2_655 ?
Ag4 Ag3 Ag12 89.05(3) 2_655 2_655 ?
Ag6 Ag3 Ag2 59.68(2) 2_655 . ?
Ag6 Ag3 Ag3 57.33(2) . 2_655 ?
Ag6 Ag3 Ag3 60.24(2) 2_655 2_655 ?
Ag6 Ag3 Ag6 106.54(3) 2_655 . ?
Ag6 Ag3 Ag8 60.37(2) 2_655 . ?
Ag6 Ag3 Ag8 109.77(3) . . ?
Ag6 Ag3 Ag8 113.31(3) 2_655 2_655 ?
Ag6 Ag3 Ag11 92.43(3) . 2_655 ?
Ag6 Ag3 Ag11 150.72(3) 2_655 2_655 ?
Ag6 Ag3 Ag12 94.91(3) 2_655 2_655 ?
Ag6 Ag3 Ag12 145.87(3) . 2_655 ?
Ag8 Ag3 Ag3 59.75(2) 2_655 2_655 ?
Ag8 Ag3 Ag3 58.66(2) . 2_655 ?
Ag8 Ag3 Ag6 59.75(2) 2_655 . ?
Ag8 Ag3 Ag8 65.47(3) 2_655 . ?
Ag8 Ag3 Ag11 133.85(3) . 2_655 ?
Ag8 Ag3 Ag11 95.42(3) 2_655 2_655 ?
Ag8 Ag3 Ag12 134.36(3) 2_655 2_655 ?
Ag8 Ag3 Ag12 103.84(3) . 2_655 ?
Ag11 Ag3 Ag3 147.12(4) 2_655 2_655 ?
Ag12 Ag3 Ag3 153.97(4) 2_655 2_655 ?
Ag12 Ag3 Ag11 58.87(2) 2_655 2_655 ?
Pd1 Ag3 Ag2 58.556(18) . . ?
Pd1 Ag3 Ag3 56.799(15) . 2_655 ?
Pd1 Ag3 Ag4 58.921(18) . 2_655 ?
Pd1 Ag3 Ag6 58.310(17) . 2_655 ?
Pd1 Ag3 Ag6 57.220(16) . . ?
Pd1 Ag3 Ag8 106.60(2) . 2_655 ?
Pd1 Ag3 Ag8 105.70(2) . . ?
Pd1 Ag3 Ag11 120.22(3) . 2_655 ?
Pd1 Ag3 Ag12 118.83(3) . 2_655 ?
S5 Ag3 Ag2 95.23(6) . . ?
S5 Ag3 Ag3 109.52(6) . 2_655 ?
S5 Ag3 Ag4 142.66(6) . 2_655 ?
S5 Ag3 Ag6 155.58(6) . . ?
S5 Ag3 Ag6 78.80(6) . 2_655 ?
S5 Ag3 Ag8 51.37(6) . . ?
S5 Ag3 Ag8 96.04(6) . 2_655 ?
S5 Ag3 Ag11 93.18(6) . 2_655 ?
S5 Ag3 Ag12 53.65(6) . 2_655 ?
S5 Ag3 Pd1 136.50(6) . . ?
Ag2 Ag4 Ag7 57.08(2) 2_655 . ?
Ag2 Ag4 Ag10 59.75(2) 2_655 . ?
Ag2 Ag4 Ag11 92.33(3) 2_655 . ?
Ag2 Ag4 Ag14 145.85(3) 2_655 . ?
Ag3 Ag4 Ag2 59.35(2) 2_655 2_655 ?
Ag3 Ag4 Ag5 110.08(3) 2_655 . ?
Ag3 Ag4 Ag6 62.57(2) 2_655 2_655 ?
Ag3 Ag4 Ag7 105.92(3) 2_655 . ?
Ag3 Ag4 Ag9 165.67(3) 2_655 . ?
Ag3 Ag4 Ag10 112.86(3) 2_655 . ?
Ag3 Ag4 Ag11 62.25(2) 2_655 . ?
Ag3 Ag4 Ag14 88.58(2) 2_655 . ?
Ag5 Ag4 Ag2 106.98(3) . 2_655 ?
Ag5 Ag4 Ag7 60.66(2) . . ?
Ag5 Ag4 Ag9 61.04(2) . . ?
Ag5 Ag4 Ag10 112.06(3) . . ?
Ag5 Ag4 Ag11 151.84(3) . . ?
Ag5 Ag4 Ag14 94.26(3) . . ?
Ag6 Ag4 Ag2 108.32(3) 2_655 2_655 ?
Ag6 Ag4 Ag5 59.89(2) 2_655 . ?
Ag6 Ag4 Ag7 107.41(3) 2_655 . ?
Ag6 Ag4 Ag9 115.78(3) 2_655 . ?
Ag6 Ag4 Ag10 164.56(3) 2_655 . ?
Ag6 Ag4 Ag11 95.00(2) 2_655 . ?
Ag6 Ag4 Ag14 59.79(2) 2_655 . ?
Ag7 Ag4 Ag14 153.93(3) . . ?
Ag9 Ag4 Ag2 110.75(3) . 2_655 ?
Ag9 Ag4 Ag7 60.27(2) . . ?
Ag9 Ag4 Ag10 64.60(2) . . ?
Ag9 Ag4 Ag11 131.10(3) . . ?
Ag9 Ag4 Ag14 102.85(3) . . ?
Ag10 Ag4 Ag7 58.51(2) . . ?
Ag10 Ag4 Ag14 135.64(3) . . ?
Ag11 Ag4 Ag7 146.20(3) . . ?
Ag11 Ag4 Ag10 95.26(3) . . ?
Ag11 Ag4 Ag14 59.79(2) . . ?
Pd1 Ag4 Ag2 57.491(17) . 2_655 ?
Pd1 Ag4 Ag3 59.11(2) . 2_655 ?
Pd1 Ag4 Ag5 58.672(19) . . ?
Pd1 Ag4 Ag6 58.475(19) . 2_655 ?
Pd1 Ag4 Ag7 56.96(2) . . ?
Pd1 Ag4 Ag9 107.27(3) . . ?
Pd1 Ag4 Ag10 106.20(3) . . ?
Pd1 Ag4 Ag11 121.36(3) . . ?
Pd1 Ag4 Ag14 118.05(3) . . ?
S6 Ag4 Ag2 155.34(6) . 2_655 ?
S6 Ag4 Ag3 141.09(6) . 2_655 ?
S6 Ag4 Ag5 80.69(6) . . ?
S6 Ag4 Ag6 95.86(6) . 2_655 ?
S6 Ag4 Ag7 111.60(6) . . ?
S6 Ag4 Ag9 51.70(6) . . ?
S6 Ag4 Ag10 95.60(6) . . ?
S6 Ag4 Ag11 90.26(6) . . ?
S6 Ag4 Ag14 52.77(6) . . ?
S6 Ag4 Pd1 138.58(6) . . ?
Ag2 Ag5 Ag4 108.44(3) . . ?
Ag2 Ag5 Ag7 106.74(3) . . ?
Ag2 Ag5 Ag7 59.85(2) . 2_655 ?
Ag2 Ag5 Ag9 165.61(3) . . ?
Ag2 Ag5 Ag15 96.80(3) . . ?
Ag4 Ag5 Ag7 62.01(2) . . ?
Ag4 Ag5 Ag9 60.60(2) . . ?
Ag4 Ag5 Ag15 144.23(3) . . ?
Ag6 Ag5 Ag2 59.99(2) 2_655 . ?
Ag6 Ag5 Ag4 59.96(2) 2_655 . ?
Ag6 Ag5 Ag7 108.12(3) 2_655 2_655 ?
Ag6 Ag5 Ag7 108.50(3) 2_655 . ?
Ag6 Ag5 Ag9 115.44(3) 2_655 . ?
Ag6 Ag5 Ag15 154.60(3) 2_655 . ?
Ag7 Ag5 Ag4 109.23(3) 2_655 . ?
Ag7 Ag5 Ag7 58.66(2) 2_655 . ?
Ag7 Ag5 Ag9 112.99(3) 2_655 . ?
Ag7 Ag5 Ag15 62.26(2) 2_655 . ?
Ag9 Ag5 Ag7 60.57(2) . . ?
Ag9 Ag5 Ag15 89.58(3) . . ?
Ag15 Ag5 Ag7 87.01(3) . . ?
Pd1 Ag5 Ag2 58.795(18) . . ?
Pd1 Ag5 Ag4 58.632(18) . . ?
Pd1 Ag5 Ag6 58.48(2) . 2_655 ?
Pd1 Ag5 Ag7 58.73(2) . 2_655 ?
Pd1 Ag5 Ag7 57.42(2) . . ?
Pd1 Ag5 Ag9 106.88(3) . . ?
Pd1 Ag5 Ag15 120.61(3) . . ?
S8 Ag5 Ag2 102.75(6) . . ?
S8 Ag5 Ag4 122.80(6) . . ?
S8 Ag5 Ag6 100.34(6) . 2_655 ?
S8 Ag5 Ag7 127.89(6) . 2_655 ?
S8 Ag5 Ag7 146.18(6) . . ?
S8 Ag5 Ag9 91.43(6) . . ?
S8 Ag5 Ag15 73.28(6) . . ?
S8 Ag5 Pd1 156.30(6) . . ?
Ag2 Ag6 Ag3 60.28(2) 2_655 2_655 ?
Ag2 Ag6 Ag3 109.33(3) 2_655 . ?
Ag2 Ag6 Ag4 108.63(3) 2_655 2_655 ?
Ag2 Ag6 Ag8 116.92(3) 2_655 2_655 ?
Ag2 Ag6 Ag14 153.58(3) 2_655 2_655 ?
Ag3 Ag6 Ag3 62.43(2) 2_655 . ?
Ag3 Ag6 Ag8 61.48(2) 2_655 2_655 ?
Ag3 Ag6 Ag14 145.47(3) 2_655 2_655 ?
Ag4 Ag6 Ag3 58.35(2) 2_655 . ?
Ag4 Ag6 Ag3 109.37(3) 2_655 2_655 ?
Ag4 Ag6 Ag8 111.43(3) 2_655 2_655 ?
Ag4 Ag6 Ag14 63.32(2) 2_655 2_655 ?
Ag5 Ag6 Ag2 60.03(2) 2_655 2_655 ?
Ag5 Ag6 Ag3 106.93(3) 2_655 . ?
Ag5 Ag6 Ag3 108.65(3) 2_655 2_655 ?
Ag5 Ag6 Ag4 60.14(2) 2_655 2_655 ?
Ag5 Ag6 Ag8 165.56(3) 2_655 2_655 ?
Ag5 Ag6 Ag14 96.61(3) 2_655 2_655 ?
Ag8 Ag6 Ag3 59.70(2) 2_655 . ?
Ag8 Ag6 Ag14 88.79(3) 2_655 2_655 ?
Ag14 Ag6 Ag3 88.27(3) 2_655 . ?
Pd1 Ag6 Ag2 58.933(18) . 2_655 ?
Pd1 Ag6 Ag3 57.72(2) . . ?
Pd1 Ag6 Ag3 58.83(2) . 2_655 ?
Pd1 Ag6 Ag4 58.816(18) . 2_655 ?
Pd1 Ag6 Ag5 58.87(2) . 2_655 ?
Pd1 Ag6 Ag8 106.97(3) . 2_655 ?
Pd1 Ag6 Ag14 121.91(3) . 2_655 ?
S1 Ag6 Ag2 101.28(6) . 2_655 ?
S1 Ag6 Ag3 145.64(6) . . ?
S1 Ag6 Ag3 125.02(6) . 2_655 ?
S1 Ag6 Ag4 125.50(6) . 2_655 ?
S1 Ag6 Ag5 101.60(6) . 2_655 ?
S1 Ag6 Ag8 92.84(6) . 2_655 ?
S1 Ag6 Ag14 69.57(6) . 2_655 ?
S1 Ag6 Pd1 156.62(6) . . ?
Ag2 Ag7 Ag4 60.78(2) 2_655 . ?
Ag2 Ag7 Ag5 60.06(2) 2_655 2_655 ?
Ag2 Ag7 Ag5 107.28(3) 2_655 . ?
Ag2 Ag7 Ag7 109.97(2) 2_655 2_655 ?
Ag2 Ag7 Ag9 112.57(3) 2_655 . ?
Ag2 Ag7 Ag10 61.72(2) 2_655 . ?
Ag2 Ag7 Ag13 151.07(3) 2_655 . ?
Ag2 Ag7 Ag15 95.78(3) 2_655 2_655 ?
Ag4 Ag7 Ag15 155.61(3) . 2_655 ?
Ag5 Ag7 Ag4 107.60(2) 2_655 . ?
Ag5 Ag7 Ag4 57.33(2) . . ?
Ag5 Ag7 Ag5 108.24(3) 2_655 . ?
Ag5 Ag7 Ag9 59.35(2) . . ?
Ag5 Ag7 Ag9 164.53(3) 2_655 . ?
Ag5 Ag7 Ag10 116.57(3) 2_655 . ?
Ag5 Ag7 Ag13 93.50(2) 2_655 . ?
Ag5 Ag7 Ag15 144.29(3) . 2_655 ?
Ag5 Ag7 Ag15 60.45(2) 2_655 2_655 ?
Ag7 Ag7 Ag4 105.55(2) 2_655 . ?
Ag7 Ag7 Ag5 58.81(2) 2_655 . ?
Ag7 Ag7 Ag5 62.53(2) 2_655 2_655 ?
Ag7 Ag7 Ag9 112.03(4) 2_655 . ?
Ag7 Ag7 Ag10 165.69(2) 2_655 . ?
Ag7 Ag7 Ag13 60.802(15) 2_655 . ?
Ag7 Ag7 Ag15 88.07(3) 2_655 2_655 ?
Ag9 Ag7 Ag4 58.65(2) . . ?
Ag9 Ag7 Ag15 135.01(3) . 2_655 ?
Ag10 Ag7 Ag4 60.48(2) . . ?
Ag10 Ag7 Ag5 110.88(3) . . ?
Ag10 Ag7 Ag9 64.74(2) . . ?
Ag10 Ag7 Ag15 103.94(3) . 2_655 ?
Ag13 Ag7 Ag4 146.10(3) . . ?
Ag13 Ag7 Ag5 91.33(2) . . ?
Ag13 Ag7 Ag9 95.88(2) . . ?
Ag13 Ag7 Ag10 132.31(3) . . ?
Ag13 Ag7 Ag15 58.28(2) . 2_655 ?
Pd1 Ag7 Ag2 58.864(18) . 2_655 ?
Pd1 Ag7 Ag4 56.905(17) . . ?
Pd1 Ag7 Ag5 57.406(17) . . ?
Pd1 Ag7 Ag5 58.708(17) . 2_655 ?
Pd1 Ag7 Ag7 58.776(15) . 2_655 ?
Pd1 Ag7 Ag9 105.86(2) . . ?
Pd1 Ag7 Ag10 107.82(3) . . ?
Pd1 Ag7 Ag13 119.58(2) . . ?
Pd1 Ag7 Ag15 118.79(3) . 2_655 ?
S3 Ag7 Ag2 81.37(6) . 2_655 ?
S3 Ag7 Ag4 111.81(6) . . ?
S3 Ag7 Ag5 154.89(6) . . ?
S3 Ag7 Ag5 96.55(6) . 2_655 ?
S3 Ag7 Ag7 141.47(6) . 2_655 ?
S3 Ag7 Ag9 95.55(6) . . ?
S3 Ag7 Ag10 51.68(6) . . ?
S3 Ag7 Ag13 91.09(6) . . ?
S3 Ag7 Ag15 53.64(6) . 2_655 ?
S3 Ag7 Pd1 139.52(6) . . ?
Ag3 Ag8 Ag3 61.59(3) 2_655 . ?
Ag3 Ag8 Ag6 60.54(2) 2_655 2_655 ?
Ag3 Ag8 Ag8 56.76(2) . 2_655 ?
Ag3 Ag8 Ag8 57.77(2) 2_655 2_655 ?
Ag6 Ag8 Ag3 58.16(2) 2_655 . ?
Ag6 Ag8 Ag8 104.522(18) 2_655 2_655 ?
S4 Ag8 Ag3 66.69(6) . 2_655 ?
S4 Ag8 Ag3 121.81(6) . . ?
S4 Ag8 Ag6 74.57(6) . 2_655 ?
S4 Ag8 Ag8 113.11(7) . 2_655 ?
S4 Ag8 S5 147.30(8) . . ?
S5 Ag8 Ag3 116.13(6) . 2_655 ?
S5 Ag8 Ag3 55.12(5) . . ?
S5 Ag8 Ag6 79.38(6) . 2_655 ?
S5 Ag8 Ag8 92.20(6) . 2_655 ?
O1 Ag8 Ag3 115.6(2) . 2_655 ?
O1 Ag8 Ag3 125.63(19) . . ?
O1 Ag8 Ag6 173.6(2) . 2_655 ?
O1 Ag8 Ag8 75.98(18) . 2_655 ?
O1 Ag8 S4 99.3(2) . . ?
O1 Ag8 S5 107.0(2) . . ?
Ag4 Ag9 Ag5 58.36(2) . . ?
Ag4 Ag9 Ag7 61.08(2) . . ?
Ag4 Ag9 Ag10 58.58(2) . . ?
Ag5 Ag9 Ag7 60.08(2) . . ?
Ag5 Ag9 Ag10 105.22(3) . . ?
Ag7 Ag9 Ag10 56.84(2) . . ?
S6 Ag9 Ag4 55.81(6) . . ?
S6 Ag9 Ag5 81.21(6) . . ?
S6 Ag9 Ag7 116.49(6) . . ?
S6 Ag9 Ag10 93.95(7) . . ?
S7 Ag9 Ag4 120.48(6) . . ?
S7 Ag9 Ag5 73.44(6) . . ?
S7 Ag9 Ag7 65.71(6) . . ?
S7 Ag9 Ag10 110.14(7) . . ?
S7 Ag9 S6 148.63(9) . . ?
O5 Ag9 Ag4 127.4(2) . . ?
O5 Ag9 Ag5 168.6(2) . . ?
O5 Ag9 Ag7 112.4(2) . . ?
O5 Ag9 Ag10 74.5(2) . . ?
O5 Ag9 S6 110.2(2) . . ?
O5 Ag9 S7 95.8(2) . . ?
Ag2 Ag10 Ag4 59.74(2) 2_655 . ?
Ag2 Ag10 Ag9 104.63(3) 2_655 . ?
Ag4 Ag10 Ag9 56.82(2) . . ?
Ag7 Ag10 Ag2 57.88(2) . 2_655 ?
Ag7 Ag10 Ag4 61.01(2) . . ?
Ag7 Ag10 Ag9 58.42(2) . . ?
S2 Ag10 Ag2 72.55(6) . 2_655 ?
S2 Ag10 Ag4 65.87(6) . . ?
S2 Ag10 Ag7 119.91(6) . . ?
S2 Ag10 Ag9 111.12(6) . . ?
S3 Ag10 Ag2 81.41(6) . 2_655 ?
S3 Ag10 Ag4 116.84(6) . . ?
S3 Ag10 Ag7 56.21(6) . . ?
S3 Ag10 Ag9 93.98(6) . . ?
S3 Ag10 S2 147.40(9) . . ?
O4 Ag10 Ag2 167.4(3) . 2_655 ?
O4 Ag10 Ag4 111.0(3) . . ?
O4 Ag10 Ag7 127.3(2) . . ?
O4 Ag10 Ag9 73.8(2) . . ?
O4 Ag10 S2 96.1(3) . . ?
O4 Ag10 S3 111.1(3) . . ?
Ag4 Ag11 Ag3 56.44(2) . 2_655 ?
Ag4 Ag11 Ag14 61.16(2) . . ?
Ag12 Ag11 Ag3 59.78(2) . 2_655 ?
Ag12 Ag11 Ag4 86.78(3) . . ?
Ag12 Ag11 Ag14 143.26(3) . . ?
Ag14 Ag11 Ag3 86.18(3) . 2_655 ?
S2 Ag11 Ag3 89.63(6) . 2_655 ?
S2 Ag11 Ag4 66.10(6) . . ?
S2 Ag11 Ag12 53.49(6) . . ?
S2 Ag11 Ag14 118.70(6) . . ?
S2 Ag11 O11 91.7(3) . . ?
S2 Ag11 O12 110.9(2) . . ?
S4 Ag11 Ag3 65.44(6) . 2_655 ?
S4 Ag11 Ag4 89.85(6) . . ?
S4 Ag11 Ag12 115.55(6) . . ?
S4 Ag11 Ag14 52.18(6) . . ?
S4 Ag11 S2 152.75(8) . . ?
S4 Ag11 O11 106.9(3) . . ?
S4 Ag11 O12 92.5(2) . . ?
O11 Ag11 Ag3 110.7(3) . 2_655 ?
O11 Ag11 Ag4 152.7(2) . . ?
O11 Ag11 Ag12 66.7(2) . . ?
O11 Ag11 Ag14 145.9(3) . . ?
O12 Ag11 Ag3 157.4(2) . 2_655 ?
O12 Ag11 Ag4 122.5(2) . . ?
O12 Ag11 Ag12 140.4(2) . . ?
O12 Ag11 Ag14 75.9(2) . . ?
O12 Ag11 O11 79.1(3) . . ?
Ag2 Ag12 Ag3 58.21(2) 2_655 2_655 ?
Ag11 Ag12 Ag2 93.74(3) . 2_655 ?
Ag11 Ag12 Ag3 61.35(2) . 2_655 ?
Ag16 Ag12 Ag2 72.02(3) 2_655 2_655 ?
Ag16 Ag12 Ag3 92.96(3) 2_655 2_655 ?
Ag16 Ag12 Ag11 154.24(4) 2_655 . ?
S2 Ag12 Ag2 72.63(6) . 2_655 ?
S2 Ag12 Ag3 89.91(6) . 2_655 ?
S2 Ag12 Ag11 52.16(6) . . ?
S2 Ag12 Ag16 136.12(7) . 2_655 ?
S2 Ag12 S5 142.43(8) . 2_655 ?
S5 Ag12 Ag2 94.07(6) 2_655 2_655 ?
S5 Ag12 Ag3 54.41(5) 2_655 2_655 ?
S5 Ag12 Ag11 95.48(6) 2_655 . ?
S5 Ag12 Ag16 65.22(6) 2_655 2_655 ?
O3 Ag12 Ag2 137.3(2) . 2_655 ?
O3 Ag12 Ag3 155.7(2) . 2_655 ?
O3 Ag12 Ag11 123.3(2) . . ?
O3 Ag12 Ag16 79.2(2) . 2_655 ?
O3 Ag12 S2 111.8(2) . . ?
O3 Ag12 S5 101.8(2) . 2_655 ?
Ag7 Ag13 Ag7 58.39(3) 2_655 . ?
Ag15 Ag13 Ag7 62.27(3) . 2_655 ?
Ag15 Ag13 Ag7 62.27(2) 2_655 . ?
Ag15 Ag13 Ag7 88.99(3) . . ?
Ag15 Ag13 Ag7 88.99(3) 2_655 2_655 ?
Ag15 Ag13 Ag15 147.88(5) . 2_655 ?
S7 Ag13 Ag7 66.71(6) 2_655 2_655 ?
S7 Ag13 Ag7 92.09(6) . 2_655 ?
S7 Ag13 Ag7 92.09(6) 2_655 . ?
S7 Ag13 Ag7 66.70(6) . . ?
S7 Ag13 Ag15 118.48(6) . 2_655 ?
S7 Ag13 Ag15 53.79(6) . . ?
S7 Ag13 Ag15 118.48(6) 2_655 . ?
S7 Ag13 Ag15 53.80(6) 2_655 2_655 ?
S7 Ag13 S7 156.26(11) . 2_655 ?
S7 Ag13 O6 102.9(4) 2_655 2_655 ?
S7 Ag13 O6 98.2(4) 2_655 . ?
S7 Ag13 O6 102.9(4) . . ?
S7 Ag13 O6 98.2(4) . 2_655 ?
O6 Ag13 Ag7 126.2(3) 2_655 2_655 ?
O6 Ag13 Ag7 126.2(3) . . ?
O6 Ag13 Ag7 164.9(3) . 2_655 ?
O6 Ag13 Ag7 164.9(3) 2_655 . ?
O6 Ag13 Ag15 82.3(3) . 2_655 ?
O6 Ag13 Ag15 82.3(3) 2_655 . ?
O6 Ag13 Ag15 128.8(3) 2_655 2_655 ?
O6 Ag13 Ag15 128.8(3) . . ?
O6 Ag13 O6 54.0(6) 2_655 . ?
Ag6 Ag14 Ag4 56.88(2) 2_655 . ?
Ag6 Ag14 Ag11 92.65(3) 2_655 . ?
Ag6 Ag14 Ag17 76.53(11) 2_655 . ?
Ag11 Ag14 Ag4 59.04(2) . . ?
Ag17 Ag14 Ag4 95.9(2) . . ?
Ag17 Ag14 Ag11 154.2(2) . . ?
S4 Ag14 Ag4 87.62(6) . . ?
S4 Ag14 Ag6 73.92(6) . 2_655 ?
S4 Ag14 Ag11 51.00(6) . . ?
S4 Ag14 Ag17 141.9(2) . . ?
S4 Ag14 S6 137.24(9) . . ?
S4 Ag14 Ag1 147.5(4) . . ?
S6 Ag14 Ag4 53.25(6) . . ?
S6 Ag14 Ag6 93.99(6) . 2_655 ?
S6 Ag14 Ag11 90.04(6) . . ?
S6 Ag14 Ag17 67.8(3) . . ?
S6 Ag14 Ag1 61.0(4) . . ?
O9 Ag14 Ag4 150.0(2) . . ?
O9 Ag14 Ag6 145.0(3) . 2_655 ?
O9 Ag14 Ag11 120.0(2) . . ?
O9 Ag14 Ag17 77.9(3) . . ?
O9 Ag14 S4 115.4(2) . . ?
O9 Ag14 S6 98.1(2) . . ?
O9 Ag14 Ag1 78.8(3) . . ?
Ag1 Ag14 Ag4 91.8(3) . . ?
Ag1 Ag14 Ag11 148.6(4) . . ?
Ag5 Ag15 Ag7 57.30(2) . 2_655 ?
Ag13 Ag15 Ag5 92.25(3) . . ?
Ag13 Ag15 Ag7 59.45(3) . 2_655 ?
S3 Ag15 Ag5 94.51(6) 2_655 . ?
S3 Ag15 Ag7 54.09(6) 2_655 2_655 ?
S3 Ag15 Ag13 92.22(6) 2_655 . ?
S3 Ag15 Ag0A 63.79(6) 2_655 . ?
S7 Ag15 Ag5 72.88(6) . . ?
S7 Ag15 Ag7 89.55(6) . 2_655 ?
S7 Ag15 Ag13 52.84(6) . . ?
S7 Ag15 S3 140.96(9) . 2_655 ?
S7 Ag15 Ag0A 141.10(7) . . ?
O8 Ag15 Ag5 145.7(3) . . ?
O8 Ag15 Ag7 148.0(3) . 2_655 ?
O8 Ag15 Ag13 120.0(3) . . ?
O8 Ag15 S3 95.5(3) . 2_655 ?
O8 Ag15 S7 115.9(2) . . ?
O8 Ag15 Ag0A 79.1(2) . . ?
Ag0A Ag15 Ag5 76.18(4) . . ?
Ag0A Ag15 Ag7 93.17(4) . 2_655 ?
Ag0A Ag15 Ag13 151.83(4) . . ?
Ag12 Ag16 Ag20 136.40(19) 2_655 . ?
S1 Ag16 Ag12 129.83(7) 2_655 2_655 ?
S1 Ag16 Ag20 58.73(19) 2_655 . ?
S1 Ag16 S9 103.23(9) 2_655 . ?
S9 Ag16 Ag12 75.57(6) . 2_655 ?
S9 Ag16 Ag20 61.7(2) . . ?
O2 Ag16 Ag12 83.1(2) 2_655 2_655 ?
O2 Ag16 Ag20 113.2(2) 2_655 . ?
O2 Ag16 S1 142.1(2) 2_655 2_655 ?
O2 Ag16 S9 103.0(3) 2_655 . ?
Ag14 Ag17 Ag19 135.7(2) . . ?
S1 Ag17 Ag14 69.28(15) 2_655 . ?
S1 Ag17 Ag19 69.3(3) 2_655 . ?
S8 Ag17 Ag14 122.5(4) . . ?
S8 Ag17 Ag19 52.8(2) . . ?
S8 Ag17 S1 100.7(2) . 2_655 ?
O10 Ag17 Ag14 82.7(3) . . ?
O10 Ag17 Ag19 124.9(6) . . ?
O10 Ag17 S1 108.0(5) . 2_655 ?
O10 Ag17 S8 147.5(4) . . ?
S8 Ag19 Ag17 48.9(2) . . ?
S8 Ag19 S9 91.72(11) . . ?
S8 Ag19 Ag0A 59.52(11) . . ?
S9 Ag19 Ag17 112.2(2) . . ?
S9 Ag19 Ag0A 52.90(10) . . ?
P1 Ag19 Ag17 110.1(3) . . ?
P1 Ag19 S8 135.27(18) . . ?
P1 Ag19 S9 131.19(16) . . ?
P1 Ag19 Ag0A 132.3(3) . . ?
Ag0A Ag19 Ag17 106.6(2) . . ?
Ag16 Ag20 Ag1 102.1(3) . . ?
Ag16 Ag20 Ag0A 95.2(2) . . ?
S1 Ag20 Ag16 49.05(11) 2_655 . ?
S1 Ag20 S9 87.53(12) 2_655 . ?
S1 Ag20 Ag1 55.2(2) 2_655 . ?
S1 Ag20 Ag0A 113.98(14) 2_655 . ?
S8 Ag20 Ag16 112.18(12) . . ?
S8 Ag20 S1 88.61(17) . 2_655 ?
S8 Ag20 S9 84.3(2) . . ?
S8 Ag20 Ag1 48.9(2) . . ?
S8 Ag20 Ag0A 51.54(16) . . ?
S9 Ag20 Ag16 50.90(10) . . ?
S9 Ag20 Ag1 114.8(2) . . ?
S9 Ag20 Ag0A 45.55(15) . . ?
P1 Ag20 Ag16 119.89(19) . . ?
P1 Ag20 S1 135.3(4) . 2_655 ?
P1 Ag20 S8 126.4(2) . . ?
P1 Ag20 S9 119.2(4) . . ?
P1 Ag20 Ag1 124.8(3) . . ?
P1 Ag20 Ag0A 109.9(4) . . ?
Ag1 Ag20 Ag0A 99.3(3) . . ?
Ag2 Pd1 Ag2 178.35(4) 2_655 . ?
Ag2 Pd1 Ag3 118.71(3) . 2_655 ?
Ag2 Pd1 Ag3 62.846(19) . . ?
Ag2 Pd1 Ag3 118.71(3) 2_655 . ?
Ag2 Pd1 Ag3 62.846(19) 2_655 2_655 ?
Ag3 Pd1 Ag3 66.40(3) . 2_655 ?
Ag4 Pd1 Ag2 114.885(19) . . ?
Ag4 Pd1 Ag2 65.148(19) . 2_655 ?
Ag4 Pd1 Ag2 114.886(19) 2_655 2_655 ?
Ag4 Pd1 Ag2 65.149(19) 2_655 . ?
Ag4 Pd1 Ag3 61.972(19) 2_655 . ?
Ag4 Pd1 Ag3 116.01(3) 2_655 2_655 ?
Ag4 Pd1 Ag3 116.01(3) . . ?
Ag4 Pd1 Ag3 61.972(19) . 2_655 ?
Ag4 Pd1 Ag4 177.85(4) 2_655 . ?
Ag4 Pd1 Ag5 62.695(19) . . ?
Ag4 Pd1 Ag5 62.696(19) 2_655 2_655 ?
Ag4 Pd1 Ag5 118.56(2) 2_655 . ?
Ag4 Pd1 Ag5 118.56(2) . 2_655 ?
Ag4 Pd1 Ag7 115.89(3) 2_655 . ?
Ag4 Pd1 Ag7 66.14(2) 2_655 2_655 ?
Ag4 Pd1 Ag7 115.89(3) . 2_655 ?
Ag4 Pd1 Ag7 66.14(2) . . ?
Ag5 Pd1 Ag2 62.509(19) 2_655 2_655 ?
Ag5 Pd1 Ag2 116.54(2) . 2_655 ?
Ag5 Pd1 Ag2 116.54(2) 2_655 . ?
Ag5 Pd1 Ag2 62.509(19) . . ?
Ag5 Pd1 Ag3 115.10(2) 2_655 2_655 ?
Ag5 Pd1 Ag3 115.95(2) 2_655 . ?
Ag5 Pd1 Ag3 115.10(2) . . ?
Ag5 Pd1 Ag3 115.95(2) . 2_655 ?
Ag5 Pd1 Ag5 118.01(4) 2_655 . ?
Ag5 Pd1 Ag7 65.17(2) 2_655 2_655 ?
Ag5 Pd1 Ag7 62.56(2) 2_655 . ?
Ag5 Pd1 Ag7 65.17(2) . . ?
Ag5 Pd1 Ag7 62.56(2) . 2_655 ?
Ag6 Pd1 Ag2 118.36(2) 2_655 2_655 ?
Ag6 Pd1 Ag2 62.615(19) . 2_655 ?
Ag6 Pd1 Ag2 62.616(19) 2_655 . ?
Ag6 Pd1 Ag2 118.36(2) . . ?
Ag6 Pd1 Ag3 62.85(2) . 2_655 ?
Ag6 Pd1 Ag3 62.86(2) 2_655 . ?
Ag6 Pd1 Ag3 65.06(2) 2_655 2_655 ?
Ag6 Pd1 Ag3 65.06(2) . . ?
Ag6 Pd1 Ag4 116.03(2) 2_655 2_655 ?
Ag6 Pd1 Ag4 62.709(19) . 2_655 ?
Ag6 Pd1 Ag4 62.705(19) 2_655 . ?
Ag6 Pd1 Ag4 116.03(2) . . ?
Ag6 Pd1 Ag5 62.645(19) 2_655 . ?
Ag6 Pd1 Ag5 62.647(19) . 2_655 ?
Ag6 Pd1 Ag5 178.70(2) . . ?
Ag6 Pd1 Ag5 178.71(2) 2_655 2_655 ?
Ag6 Pd1 Ag6 116.72(4) 2_655 . ?
Ag6 Pd1 Ag7 118.62(2) . 2_655 ?
Ag6 Pd1 Ag7 114.72(2) . . ?
Ag6 Pd1 Ag7 114.73(2) 2_655 2_655 ?
Ag6 Pd1 Ag7 118.62(2) 2_655 . ?
Ag7 Pd1 Ag2 62.35(2) . 2_655 ?
Ag7 Pd1 Ag2 116.07(3) . . ?
Ag7 Pd1 Ag2 116.07(3) 2_655 2_655 ?
Ag7 Pd1 Ag2 62.36(2) 2_655 . ?
Ag7 Pd1 Ag3 115.582(18) . 2_655 ?
Ag7 Pd1 Ag3 115.586(18) 2_655 . ?
Ag7 Pd1 Ag3 177.80(2) 2_655 2_655 ?
Ag7 Pd1 Ag3 177.80(2) . . ?
Ag7 Pd1 Ag7 62.45(3) 2_655 . ?
Ag6 S1 Ag17 94.8(3) . 2_655 ?
Ag6 S1 Ag20 115.23(18) . 2_655 ?
Ag6 S1 Ag1 88.9(3) . 2_655 ?
Ag16 S1 Ag6 90.00(9) 2_655 . ?
Ag16 S1 Ag17 134.0(2) 2_655 2_655 ?
Ag16 S1 Ag20 72.22(16) 2_655 2_655 ?
Ag16 S1 Ag1 136.8(3) 2_655 2_655 ?
Ag17 S1 Ag20 64.4(3) 2_655 2_655 ?
Ag17 S1 Ag1 6.5(3) 2_655 2_655 ?
C1 S1 Ag6 119.5(5) . . ?
C1 S1 Ag16 104.5(5) . 2_655 ?
C1 S1 Ag17 112.4(5) . 2_655 ?
C1 S1 Ag20 125.2(5) . 2_655 ?
C1 S1 Ag1 113.4(5) . 2_655 ?
Ag10 S2 Ag12 119.13(10) . . ?
Ag11 S2 Ag10 131.65(10) . . ?
Ag11 S2 Ag12 74.35(7) . . ?
C8 S2 Ag10 108.2(4) . . ?
C8 S2 Ag11 104.7(4) . . ?
C8 S2 Ag12 115.6(4) . . ?
Ag7 S3 Ag0A 103.18(8) . 2_655 ?
Ag10 S3 Ag7 72.11(7) . . ?
Ag10 S3 Ag15 141.20(10) . 2_655 ?
Ag10 S3 Ag0A 111.67(9) . 2_655 ?
Ag15 S3 Ag7 72.26(7) 2_655 . ?
Ag15 S3 Ag0A 62.93(6) 2_655 2_655 ?
C15 S3 Ag7 110.3(4) . . ?
C15 S3 Ag10 110.0(4) . . ?
C15 S3 Ag15 96.3(4) . 2_655 ?
C15 S3 Ag0A 132.6(4) . 2_655 ?
Ag8 S4 Ag14 115.88(9) . . ?
Ag11 S4 Ag8 131.84(10) . . ?
Ag11 S4 Ag14 76.82(7) . . ?
C22 S4 Ag8 109.5(4) . . ?
C22 S4 Ag11 104.1(4) . . ?
C22 S4 Ag14 115.7(4) . . ?
Ag8 S5 Ag3 73.52(7) . . ?
Ag8 S5 Ag12 142.65(10) . 2_655 ?
Ag12 S5 Ag3 71.94(6) 2_655 . ?
C29 S5 Ag3 116.8(4) . . ?
C29 S5 Ag8 106.7(4) . . ?
C29 S5 Ag12 101.3(4) . 2_655 ?
Ag4 S6 Ag1 106.2(3) . . ?
Ag9 S6 Ag4 72.49(7) . . ?
Ag9 S6 Ag14 142.48(10) . . ?
Ag9 S6 Ag1 109.9(2) . . ?
Ag14 S6 Ag4 73.98(7) . . ?
Ag14 S6 Ag1 64.5(2) . . ?
C36 S6 Ag4 111.0(4) . . ?
C36 S6 Ag9 108.1(5) . . ?
C36 S6 Ag14 99.2(4) . . ?
C36 S6 Ag1 132.9(5) . . ?
Ag9 S7 Ag15 118.23(10) . . ?
Ag13 S7 Ag9 131.33(10) . . ?
Ag13 S7 Ag15 73.36(7) . . ?
C43 S7 Ag9 108.8(4) . . ?
C43 S7 Ag13 105.7(4) . . ?
C43 S7 Ag15 115.9(4) . . ?
Ag5 S8 Ag19 118.69(13) . . ?
Ag5 S8 Ag20 115.08(12) . . ?
Ag5 S8 Ag0A 87.79(8) . . ?
Ag17 S8 Ag5 96.7(2) . . ?
Ag17 S8 Ag19 78.3(4) . . ?
Ag17 S8 Ag0A 138.2(3) . . ?
Ag19 S8 Ag0A 63.49(14) . . ?
C50 S8 Ag5 121.8(5) . . ?
C50 S8 Ag17 106.5(4) . . ?
C50 S8 Ag19 117.9(5) . . ?
C50 S8 Ag20 123.1(5) . . ?
C50 S8 Ag1 102.7(5) . . ?
C50 S8 Ag0A 106.1(4) . . ?
Ag1 S8 Ag5 92.3(3) . . ?
Ag1 S8 Ag20 73.9(6) . . ?
Ag1 S8 Ag0A 145.9(5) . . ?
Ag0A S8 Ag20 75.3(2) . . ?
Ag2 S9 Ag16 85.98(8) . . ?
Ag2 S9 Ag19 118.95(13) . . ?
Ag2 S9 Ag20 112.92(15) . . ?
Ag16 S9 Ag19 79.25(18) . . ?
Ag16 S9 Ag20 67.42(17) . . ?
C57 S9 Ag2 119.0(5) . . ?
C57 S9 Ag16 109.3(4) . . ?
C57 S9 Ag19 121.8(5) . . ?
C57 S9 Ag20 127.6(5) . . ?
C57 S9 Ag0A 105.6(4) . . ?
Ag0A S9 Ag2 94.27(9) . . ?
Ag0A S9 Ag16 139.79(11) . . ?
Ag0A S9 Ag19 65.52(16) . . ?
Ag0A S9 Ag20 75.69(16) . . ?
C77 P1 Ag19 115.0(4) . . ?
C77 P1 Ag20 114.1(4) . . ?
C83 P1 Ag19 120.0(5) . . ?
C83 P1 Ag20 107.1(5) . . ?
C83 P1 C77 104.1(6) . . ?
C89 P1 Ag19 107.1(5) . . ?
C89 P1 Ag20 120.7(5) . . ?
C89 P1 C77 105.1(6) . . ?
C89 P1 C83 104.1(6) . . ?
F3 F2 F1 117.4(16) 2_655 2_655 ?
F3 F2 C66 63.5(10) 2_655 . ?
C66 F2 F1 59.7(7) . 2_655 ?
C72 F11 C72 40.3(18) . 2_655 ?
C65 O1 Ag8 124.9(7) . . ?
C67 O2 Ag16 121.1(7) . 2_655 ?
C67 O3 Ag12 124.4(7) . . ?
C69 O4 Ag10 124.3(8) . . ?
C69 O5 Ag9 123.0(8) . . ?
C71 O6 Ag13 87.0(13) . . ?
C73 O7 Ag0A 120.4(9) . . ?
C73 O8 Ag15 125.3(8) . . ?
C75 O9 Ag14 124.3(8) . . ?
C75 O10 Ag17 123.9(8) . . ?
C75 O10 Ag1 119.5(9) . . ?
C95 O11 Ag11 129.5(12) . . ?
C98 O12 Ag11 138.9(10) . . ?
C95 N1 C96 118.3(14) . . ?
C95 N1 C97 123.4(15) . . ?
C97 N1 C96 118.2(13) . . ?
C98 N2 C99 123.2(13) . . ?
C98 N2 C100 119.3(14) . . ?
C100 N2 C99 117.5(14) . . ?
S1 C1 H1A 109.1 . . ?
S1 C1 H1B 109.1 . . ?
H1A C1 H1B 107.8 . . ?
C2 C1 S1 112.5(8) . . ?
C2 C1 H1A 109.1 . . ?
C2 C1 H1B 109.1 . . ?
C3 C2 C1 121.4(12) . . ?
C7 C2 C1 121.5(12) . . ?
C7 C2 C3 117.1(11) . . ?
C2 C3 H3 119.7 . . ?
C4 C3 C2 120.5(13) . . ?
C4 C3 H3 119.7 . . ?
C3 C4 H4 119.7 . . ?
C5 C4 C3 120.6(13) . . ?
C5 C4 H4 119.7 . . ?
C4 C5 H5 119.1 . . ?
C4 C5 C6 121.7(13) . . ?
C6 C5 H5 119.1 . . ?
C5 C6 H6 121.1 . . ?
C5 C6 C7 117.8(13) . . ?
C7 C6 H6 121.1 . . ?
C2 C7 C6 122.1(12) . . ?
C2 C7 H7 118.9 . . ?
C6 C7 H7 118.9 . . ?
S2 C8 H8A 109.1 . . ?
S2 C8 H8B 109.1 . . ?
H8A C8 H8B 107.8 . . ?
C9 C8 S2 112.6(9) . . ?
C9 C8 H8A 109.1 . . ?
C9 C8 H8B 109.1 . . ?
C10 C9 C8 120.5(13) . . ?
C14 C9 C8 119.9(13) . . ?
C14 C9 C10 119.5(13) . . ?
C9 C10 H10 120.5 . . ?
C9 C10 C11 119.0(17) . . ?
C11 C10 H10 120.5 . . ?
C10 C11 H11 120.4 . . ?
C12 C11 C10 119.2(17) . . ?
C12 C11 H11 120.4 . . ?
C11 C12 H12 119.1 . . ?
C13 C12 C11 121.8(18) . . ?
C13 C12 H12 119.1 . . ?
C12 C13 H13 119.5 . . ?
C12 C13 C14 121.1(19) . . ?
C14 C13 H13 119.5 . . ?
C9 C14 C13 119.5(16) . . ?
C9 C14 H14 120.3 . . ?
C13 C14 H14 120.3 . . ?
S3 C15 H15A 108.3 . . ?
S3 C15 H15B 108.3 . . ?
H15A C15 H15B 107.4 . . ?
C16 C15 S3 115.8(9) . . ?
C16 C15 H15A 108.3 . . ?
C16 C15 H15B 108.3 . . ?
C17 C16 C15 118.8(12) . . ?
C21 C16 C15 121.2(12) . . ?
C21 C16 C17 119.7(12) . . ?
C16 C17 H17 119.6 . . ?
C18 C17 C16 120.8(15) . . ?
C18 C17 H17 119.6 . . ?
C17 C18 H18 120.4 . . ?
C17 C18 C19 119.3(16) . . ?
C19 C18 H18 120.4 . . ?
C18 C19 H19 120.5 . . ?
C20 C19 C18 119.1(15) . . ?
C20 C19 H19 120.5 . . ?
C19 C20 H20 119.7 . . ?
C19 C20 C21 120.6(16) . . ?
C21 C20 H20 119.7 . . ?
C16 C21 C20 120.3(14) . . ?
C16 C21 H21 119.9 . . ?
C20 C21 H21 119.9 . . ?
S4 C22 H22A 109.4 . . ?
S4 C22 H22B 109.4 . . ?
H22A C22 H22B 108.0 . . ?
C24 C22 S4 111.1(7) . . ?
C24 C22 H22A 109.4 . . ?
C24 C22 H22B 109.4 . . ?
C24 C23 H23 120.4 . . ?
C28 C23 H23 120.4 . . ?
C28 C23 C24 119.3(12) . . ?
C23 C24 C22 118.6(11) . . ?
C25 C24 C22 122.7(11) . . ?
C25 C24 C23 118.7(11) . . ?
C24 C25 H25 119.7 . . ?
C24 C25 C26 120.7(12) . . ?
C26 C25 H25 119.7 . . ?
C25 C26 H26 119.4 . . ?
C27 C26 C25 121.1(13) . . ?
C27 C26 H26 119.4 . . ?
C26 C27 H27 120.5 . . ?
C26 C27 C28 119.0(13) . . ?
C28 C27 H27 120.5 . . ?
C23 C28 H28 119.4 . . ?
C27 C28 C23 121.2(13) . . ?
C27 C28 H28 119.4 . . ?
S5 C29 H29A 109.5 . . ?
S5 C29 H29B 109.5 . . ?
H29A C29 H29B 108.1 . . ?
C30 C29 S5 110.7(8) . . ?
C30 C29 H29A 109.5 . . ?
C30 C29 H29B 109.5 . . ?
C31 C30 C29 122.5(12) . . ?
C35 C30 C29 121.0(12) . . ?
C35 C30 C31 116.4(12) . . ?
C30 C31 H31 119.0 . . ?
C32 C31 C30 122.0(15) . . ?
C32 C31 H31 119.0 . . ?
C31 C32 H32 120.3 . . ?
C33 C32 C31 119.3(15) . . ?
C33 C32 H32 120.3 . . ?
C32 C33 H33 119.9 . . ?
C32 C33 C34 120.1(14) . . ?
C34 C33 H33 119.9 . . ?
C33 C34 H34 120.1 . . ?
C35 C34 C33 119.9(15) . . ?
C35 C34 H34 120.1 . . ?
C30 C35 H35 118.9 . . ?
C34 C35 C30 122.3(15) . . ?
C34 C35 H35 118.9 . . ?
S6 C36 H36A 108.6 . . ?
S6 C36 H36B 108.6 . . ?
H36A C36 H36B 107.6 . . ?
C37 C36 S6 114.6(10) . . ?
C37 C36 H36A 108.6 . . ?
C37 C36 H36B 108.6 . . ?
C38 C37 C36 121.4(16) . . ?
C38 C37 C42 116.3(17) . . ?
C42 C37 C36 122.3(14) . . ?
C37 C38 H38 122.2 . . ?
C37 C38 C39 116(2) . . ?
C39 C38 H38 122.2 . . ?
C38 C39 H39 119.8 . . ?
C40 C39 C38 120(2) . . ?
C40 C39 H39 119.8 . . ?
C39 C40 H40 119.9 . . ?
C39 C40 C41 120(2) . . ?
C41 C40 H40 119.9 . . ?
C40 C41 H41 121.5 . . ?
C42 C41 C40 117(2) . . ?
C42 C41 H41 121.5 . . ?
C37 C42 H42 117.5 . . ?
C41 C42 C37 125.0(19) . . ?
C41 C42 H42 117.5 . . ?
S7 C43 H43A 109.2 . . ?
S7 C43 H43B 109.2 . . ?
H43A C43 H43B 107.9 . . ?
C44 C43 S7 112.2(7) . . ?
C44 C43 H43A 109.2 . . ?
C44 C43 H43B 109.2 . . ?
C45 C44 C43 120.5(11) . . ?
C45 C44 C49 119.3(12) . . ?
C49 C44 C43 120.1(12) . . ?
C44 C45 H45 120.6 . . ?
C44 C45 C46 118.9(14) . . ?
C46 C45 H45 120.6 . . ?
C45 C46 H46 119.9 . . ?
C47 C46 C45 120.2(15) . . ?
C47 C46 H46 119.9 . . ?
C46 C47 H47 119.1 . . ?
C46 C47 C48 121.7(14) . . ?
C48 C47 H47 119.1 . . ?
C47 C48 H48 121.0 . . ?
C49 C48 C47 118.0(16) . . ?
C49 C48 H48 121.0 . . ?
C44 C49 H49 119.2 . . ?
C48 C49 C44 121.7(16) . . ?
C48 C49 H49 119.2 . . ?
S8 C50 H50A 108.7 . . ?
S8 C50 H50B 108.7 . . ?
H50A C50 H50B 107.6 . . ?
C51 C50 S8 114.2(8) . . ?
C51 C50 H50A 108.7 . . ?
C51 C50 H50B 108.7 . . ?
C55 C56 H56 120.0 . . ?
C55 C56 C51 120.0 . . ?
C51 C56 H56 120.0 . . ?
C56 C55 H55 120.0 . . ?
C54 C55 C56 120.0 . . ?
C54 C55 H55 120.0 . . ?
C55 C54 H54 120.0 . . ?
C55 C54 C53 120.0 . . ?
C53 C54 H54 120.0 . . ?
C54 C53 H53 120.0 . . ?
C52 C53 C54 120.0 . . ?
C52 C53 H53 120.0 . . ?
C53 C52 H52 120.0 . . ?
C53 C52 C51 120.0 . . ?
C51 C52 H52 120.0 . . ?
C56 C51 C50 121.1(9) . . ?
C52 C51 C50 118.9(9) . . ?
C52 C51 C56 120.0 . . ?
S9 C57 H57A 109.2 . . ?
S9 C57 H57B 109.2 . . ?
H57A C57 H57B 107.9 . . ?
C59 C57 S9 112.2(9) . . ?
C59 C57 H57A 109.2 . . ?
C59 C57 H57B 109.2 . . ?
C60 C59 C57 120.3(12) . . ?
C64 C59 C57 121.5(12) . . ?
C64 C59 C60 118.1(13) . . ?
C59 C60 H60 119.5 . . ?
C61 C60 C59 120.9(17) . . ?
C61 C60 H60 119.5 . . ?
C60 C61 H61 120.2 . . ?
C62 C61 C60 120(2) . . ?
C62 C61 H61 120.2 . . ?
C61 C62 H62 120.0 . . ?
C63 C62 C61 119.9(19) . . ?
C63 C62 H62 120.1 . . ?
C62 C63 H63 118.9 . . ?
C62 C63 C64 122.2(17) . . ?
C64 C63 H63 118.9 . . ?
C59 C64 H64 120.3 . . ?
C63 C64 C59 119.4(16) . . ?
C63 C64 H64 120.3 . . ?
O1 C65 O1 128.9(13) 2_655 . ?
O1 C65 C66 115.5(6) . . ?
O1 C65 C66 115.5(6) 2_655 . ?
F1 C66 F1 138.8(17) 2_655 . ?
F1 C66 C65 110.6(8) 2_655 . ?
F1 C66 C65 110.6(8) . . ?
F2 C66 F1 100.1(11) 2_655 2_655 ?
F2 C66 F1 63.8(10) . 2_655 ?
F2 C66 F1 63.8(10) 2_655 . ?
F2 C66 F1 100.1(11) . . ?
F2 C66 F2 135.4(17) 2_655 . ?
F2 C66 C65 112.3(8) 2_655 . ?
F2 C66 C65 112.3(8) . . ?
F3 C66 F1 106.3(12) 2_655 2_655 ?
F3 C66 F1 54.4(11) . 2_655 ?
F3 C66 F1 106.3(12) . . ?
F3 C66 F1 54.4(11) 2_655 . ?
F3 C66 F2 110.9(13) 2_655 2_655 ?
F3 C66 F2 110.9(13) . . ?
F3 C66 F2 46.9(12) 2_655 . ?
F3 C66 F2 46.9(12) . 2_655 ?
F3 C66 F3 129(2) . 2_655 ?
F3 C66 C65 115.4(11) 2_655 . ?
F3 C66 C65 115.4(11) . . ?
O2 C67 C68 114.5(11) . . ?
O3 C67 O2 131.8(11) . . ?
O3 C67 C68 113.7(11) . . ?
F4 C68 F6 105.2(12) . . ?
F4 C68 C67 110.2(12) . . ?
F5 C68 F4 110.9(15) . . ?
F5 C68 F6 104.3(13) . . ?
F5 C68 C67 113.5(11) . . ?
F6 C68 C67 112.4(13) . . ?
O4 C69 C70 114.0(10) . . ?
O5 C69 O4 125.7(11) . . ?
O5 C69 C70 120.3(11) . . ?
F7 C70 C69 108.7(12) . . ?
F8 C70 F7 103.5(15) . . ?
F8 C70 C69 111.7(12) . . ?
F9 C70 F7 111.7(19) . . ?
F9 C70 F8 107.5(18) . . ?
F9 C70 C69 113.3(14) . . ?
F7A C70 C69 118(3) . . ?
F7A C70 F8A 110(3) . . ?
F7A C70 F9A 112(3) . . ?
F8A C70 C69 109(2) . . ?
F8A C70 F9A 98(2) . . ?
F9A C70 C69 107.8(17) . . ?
O6 C71 O6 132(2) 2_655 . ?
O6 C71 C72 127.3(15) 2_655 2_655 ?
O6 C71 C72 99.4(17) 2_655 . ?
O6 C71 C72 127.3(15) . . ?
O6 C71 C72 99.4(17) . 2_655 ?
C72 C71 C72 38.2(19) 2_655 . ?
F10 C72 F11 108(2) . 2_655 ?
F10 C72 C71 123(2) . . ?
F11 C72 F10 96.6(19) . . ?
F11 C72 F11 105(2) . 2_655 ?
F11 C72 C71 116.1(18) . . ?
F11 C72 C71 107.1(14) 2_655 . ?
C72 C72 F10 165(2) 2_655 . ?
C72 C72 F11 61(2) 2_655 2_655 ?
C72 C72 F11 79(2) 2_655 . ?
C72 C72 C71 70.9(9) 2_655 . ?
O7 C73 C74 113.5(13) . . ?
O8 C73 O7 130.7(12) . . ?
O8 C73 C74 115.8(13) . . ?
F12 C74 F13 109.0(19) . . ?
F12 C74 F14 103.7(18) . . ?
F12 C74 C73 114.2(15) . . ?
F13 C74 F14 108.1(18) . . ?
F13 C74 C73 111.4(15) . . ?
F14 C74 C73 110.0(16) . . ?
O9 C75 C76 113.3(12) . . ?
O10 C75 O9 131.1(12) . . ?
O10 C75 C76 115.6(11) . . ?
F15 C76 F16 113.8(16) . . ?
F15 C76 F17 102.2(16) . . ?
F15 C76 C75 116.9(14) . . ?
F16 C76 F17 99.2(16) . . ?
F16 C76 C75 113.7(13) . . ?
F17 C76 C75 108.5(14) . . ?
C78 C77 P1 117.2(10) . . ?
C82 C77 P1 123.2(11) . . ?
C82 C77 C78 119.6(13) . . ?
C77 C78 H78 120.7 . . ?
C77 C78 C79 118.6(13) . . ?
C79 C78 H78 120.7 . . ?
C78 C79 H79 119.1 . . ?
C78 C79 C80 121.7(14) . . ?
C80 C79 H79 119.1 . . ?
C79 C80 H80 120.4 . . ?
C81 C80 C79 119.2(14) . . ?
C81 C80 H80 120.4 . . ?
C80 C81 H81 120.7 . . ?
C80 C81 C82 118.6(15) . . ?
C82 C81 H81 120.7 . . ?
C77 C82 C81 122.3(15) . . ?
C77 C82 H82 118.8 . . ?
C81 C82 H82 118.8 . . ?
C84 C83 P1 118.8(11) . . ?
C84 C83 C88 120.1(14) . . ?
C88 C83 P1 121.2(11) . . ?
C83 C84 H84 119.5 . . ?
C83 C84 C85 121.0(15) . . ?
C85 C84 H84 119.5 . . ?
C84 C85 H85 120.4 . . ?
C86 C85 C84 119.1(16) . . ?
C86 C85 H85 120.4 . . ?
C85 C86 H86 119.6 . . ?
C87 C86 C85 120.8(16) . . ?
C87 C86 H86 119.6 . . ?
C86 C87 H87 120.1 . . ?
C86 C87 C88 119.7(15) . . ?
C88 C87 H87 120.1 . . ?
C83 C88 C87 119.3(14) . . ?
C83 C88 H88 120.4 . . ?
C87 C88 H88 120.4 . . ?
C90 C89 P1 118.6(12) . . ?
C94 C89 P1 124.2(11) . . ?
C94 C89 C90 117.1(15) . . ?
C89 C90 H90 120.3 . . ?
C91 C90 C89 119.4(16) . . ?
C91 C90 H90 120.3 . . ?
C90 C91 H91 119.4 . . ?
C90 C91 C92 121.1(17) . . ?
C92 C91 H91 119.4 . . ?
C91 C92 H92 120.0 . . ?
C93 C92 C91 120.0(18) . . ?
C93 C92 H92 120.0 . . ?
C92 C93 H93 119.8 . . ?
C92 C93 C94 120.4(18) . . ?
C94 C93 H93 119.8 . . ?
C89 C94 C93 121.9(16) . . ?
C89 C94 H94 119.1 . . ?
C93 C94 H94 119.1 . . ?
O11 C95 N1 127.0(18) . . ?
O11 C95 H95 116.5 . . ?
N1 C95 H95 116.5 . . ?
N1 C96 H96A 109.5 . . ?
N1 C96 H96B 109.5 . . ?
N1 C96 H96C 109.5 . . ?
H96A C96 H96B 109.5 . . ?
H96A C96 H96C 109.5 . . ?
H96B C96 H96C 109.5 . . ?
N1 C97 H97A 109.5 . . ?
N1 C97 H97B 109.5 . . ?
N1 C97 H97C 109.5 . . ?
H97A C97 H97B 109.5 . . ?
H97A C97 H97C 109.5 . . ?
H97B C97 H97C 109.5 . . ?
O12 C98 N2 126.6(14) . . ?
O12 C98 H98 116.7 . . ?
N2 C98 H98 116.7 . . ?
N2 C99 H99A 109.5 . . ?
N2 C99 H99B 109.5 . . ?
N2 C99 H99C 109.5 . . ?
H99A C99 H99B 109.5 . . ?
H99A C99 H99C 109.5 . . ?
H99B C99 H99C 109.5 . . ?
N2 C100 H10A 109.5 . . ?
N2 C100 H10B 109.5 . . ?
N2 C100 H10C 109.5 . . ?
H10A C100 H10B 109.5 . . ?
H10A C100 H10C 109.5 . . ?
H10B C100 H10C 109.5 . . ?
H1WA O1W H1WB 104.5 . . ?
C101 N3 C102 125(2) . . ?
C101 N3 C103 121(2) . . ?
C102 N3 C103 113(3) . . ?
O13 C101 N3 126(2) . . ?
O13 C101 H101 117.0 . . ?
N3 C101 H101 117.0 . . ?
N3 C102 H10D 109.5 . . ?
N3 C102 H10E 109.5 . . ?
N3 C102 H10F 109.5 . . ?
H10D C102 H10E 109.5 . . ?
H10D C102 H10F 109.5 . . ?
H10E C102 H10F 109.5 . . ?
N3 C103 H10G 109.5 . . ?
N3 C103 H10H 109.5 . . ?
N3 C103 H10I 109.5 . . ?
H10G C103 H10H 109.5 . . ?
H10G C103 H10I 109.5 . . ?
H10H C103 H10I 109.5 . . ?
C104 N4 C105 123(2) . . ?
C104 N4 C106 119(2) . . ?
C106 N4 C105 117.5(19) . . ?
O14 C104 N4 123(3) . . ?
O14 C104 H104 118.5 . . ?
N4 C104 H104 118.5 . . ?
N4 C105 H10J 109.5 . . ?
N4 C105 H10K 109.5 . . ?
N4 C105 H10L 109.5 . . ?
H10J C105 H10K 109.5 . . ?
H10J C105 H10L 109.5 . . ?
H10K C105 H10L 109.5 . . ?
N4 C106 H10M 109.5 . . ?
N4 C106 H10N 109.5 . . ?
N4 C106 H10O 109.5 . . ?
H10M C106 H10N 109.5 . . ?
H10M C106 H10O 109.5 . . ?
H10N C106 H10O 109.5 . . ?
C107 N5 C108 121.8(17) . . ?
C107 N5 C109 120.5(19) . . ?
C108 N5 C109 117.2(19) . . ?
O15 C107 N5 125(2) . . ?
O15 C107 H107 117.6 . . ?
N5 C107 H107 117.6 . . ?
N5 C108 H10P 109.5 . . ?
N5 C108 H10Q 109.5 . . ?
N5 C108 H10R 109.5 . . ?
H10P C108 H10Q 109.5 . . ?
H10P C108 H10R 109.5 . . ?
H10Q C108 H10R 109.5 . . ?
N5 C109 H10S 109.5 . . ?
N5 C109 H10T 109.5 . . ?
N5 C109 H10U 109.5 . . ?
H10S C109 H10T 109.5 . . ?
H10S C109 H10U 109.5 . . ?
H10T C109 H10U 109.5 . . ?
C110 N6 C111 119(2) . . ?
C110 N6 C112 122(2) . . ?
C111 N6 C112 120(2) . . ?
O16 C110 N6 123(3) . . ?
O16 C110 H110 118.4 . . ?
N6 C110 H110 118.4 . . ?
N6 C111 H11A 109.5 . . ?
N6 C111 H11B 109.5 . . ?
N6 C111 H11C 109.5 . . ?
H11A C111 H11B 109.5 . . ?
H11A C111 H11C 109.5 . . ?
H11B C111 H11C 109.5 . . ?
N6 C112 H11D 109.5 . . ?
N6 C112 H11E 109.5 . . ?
N6 C112 H11F 109.5 . . ?
H11D C112 H11E 109.5 . . ?
H11D C112 H11F 109.5 . . ?
H11E C112 H11F 109.5 . . ?
C114 N7 C119 106(4) . . ?
C116 N7 C113 119(4) . . ?
C117 N7 C113 133(4) . . ?
C117 N7 C116 108(4) . . ?
C118 N7 C114 140(4) . . ?
C118 N7 C119 114(4) . . ?
O17 C113 N7 107(4) . . ?
O18 C118 N7 114(8) . . ?
Ag14 Ag1 Ag20 123.8(6) . . ?
S1 Ag1 Ag14 68.7(2) 2_655 . ?
S1 Ag1 Ag20 55.3(4) 2_655 . ?
S6 Ag1 Ag14 54.5(3) . . ?
S6 Ag1 Ag20 148.9(4) . . ?
S6 Ag1 S1 115.2(3) . 2_655 ?
S8 Ag1 Ag14 129.5(4) . . ?
S8 Ag1 Ag20 57.2(4) . . ?
S8 Ag1 S1 94.8(6) . 2_655 ?
S8 Ag1 S6 98.3(5) . . ?
O10 Ag1 Ag14 85.6(4) . . ?
O10 Ag1 Ag20 106.4(8) . . ?
O10 Ag1 S1 99.2(6) . 2_655 ?
O10 Ag1 S6 104.4(8) . . ?
O10 Ag1 S8 144.9(6) . . ?
Ag15 Ag0A Ag20 125.68(13) . . ?
Ag15 Ag0A S3 53.28(6) . 2_655 ?
Ag19 Ag0A Ag15 130.11(9) . . ?
Ag19 Ag0A S3 152.80(14) . 2_655 ?
S3 Ag0A Ag20 146.74(10) 2_655 . ?
S8 Ag0A Ag15 73.15(6) . . ?
S8 Ag0A Ag19 56.99(9) . . ?
S8 Ag0A Ag20 53.16(13) . . ?
S8 Ag0A S3 118.07(8) . 2_655 ?
S9 Ag0A Ag15 127.95(8) . . ?
S9 Ag0A Ag19 61.58(12) . . ?
S9 Ag0A Ag20 58.76(10) . . ?
S9 Ag0A S3 94.59(8) . 2_655 ?
S9 Ag0A S8 95.81(9) . . ?
O7 Ag0A Ag15 83.9(3) . . ?
O7 Ag0A Ag19 107.9(3) . . ?
O7 Ag0A Ag20 113.9(3) . . ?
O7 Ag0A S3 99.3(3) . 2_655 ?
O7 Ag0A S8 103.9(3) . . ?
O7 Ag0A S9 146.7(3) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Ag2 S9 C57 C59 -148.4(8) . . . . ?
Ag3 S5 C29 C30 175.2(7) . . . . ?
Ag4 S6 C36 C37 167.9(9) . . . . ?
Ag5 S8 C50 C51 -143.3(8) . . . . ?
Ag6 S1 C1 C2 -144.5(9) . . . . ?
Ag7 S3 C15 C16 160.7(9) . . . . ?
Ag8 S4 C22 C24 -67.8(9) . . . . ?
Ag8 S5 C29 C30 95.6(8) . . . . ?
Ag8 O1 C65 O1 16.2(4) . . . 2_655 ?
Ag8 O1 C65 C66 -163.8(4) . . . . ?
Ag9 S6 C36 C37 90.3(11) . . . . ?
Ag9 S7 C43 C44 -71.8(9) . . . . ?
Ag9 O5 C69 O4 26.9(19) . . . . ?
Ag9 O5 C69 C70 -153.2(9) . . . . ?
Ag10 S2 C8 C9 -64.3(10) . . . . ?
Ag10 S3 C15 C16 83.1(10) . . . . ?
Ag10 O4 C69 O5 18(2) . . . . ?
Ag10 O4 C69 C70 -162.2(9) . . . . ?
Ag11 S2 C8 C9 151.6(9) . . . . ?
Ag11 S4 C22 C24 147.3(8) . . . . ?
Ag11 O11 C95 N1 -146.9(14) . . . . ?
Ag11 O12 C98 N2 174.9(10) . . . . ?
Ag12 S2 C8 C9 72.2(10) . . . . ?
Ag12 S5 C29 C30 -109.5(8) 2_655 . . . ?
Ag12 O3 C67 O2 4(2) . . . . ?
Ag12 O3 C67 C68 -177.3(9) . . . . ?
Ag13 S7 C43 C44 143.1(8) . . . . ?
Ag13 O6 C71 O6 -0.001(1) . . . 2_655 ?
Ag13 O6 C71 C72 164.0(11) . . . . ?
Ag13 O6 C71 C72 -167.1(8) . . . 2_655 ?
Ag14 S4 C22 C24 65.4(9) . . . . ?
Ag14 S6 C36 C37 -115.8(10) . . . . ?
Ag14 O9 C75 O10 -3(2) . . . . ?
Ag14 O9 C75 C76 176.7(10) . . . . ?
Ag15 S3 C15 C16 -125.9(10) 2_655 . . . ?
Ag15 S7 C43 C44 64.3(9) . . . . ?
Ag15 O8 C73 O7 -3(2) . . . . ?
Ag15 O8 C73 C74 177.8(11) . . . . ?
Ag16 S1 C1 C2 -46.1(12) 2_655 . . . ?
Ag16 S9 C57 C59 115.3(9) . . . . ?
Ag16 O2 C67 O3 1.6(19) 2_655 . . . ?
Ag16 O2 C67 C68 -177.4(9) 2_655 . . . ?
Ag17 S1 C1 C2 105.8(10) 2_655 . . . ?
Ag17 S8 C50 C51 -34.2(11) . . . . ?
Ag17 O10 C75 O9 6(2) . . . . ?
Ag17 O10 C75 C76 -174.3(11) . . . . ?
Ag19 S8 C50 C51 51.0(11) . . . . ?
Ag19 S9 C57 C59 26.2(12) . . . . ?
Ag19 P1 C77 C78 49.8(11) . . . . ?
Ag19 P1 C77 C82 -133.3(11) . . . . ?
Ag19 P1 C83 C84 30.7(12) . . . . ?
Ag19 P1 C83 C88 -149.0(9) . . . . ?
Ag19 P1 C89 C90 36.4(13) . . . . ?
Ag19 P1 C89 C94 -147.0(13) . . . . ?
Ag20 S1 C1 C2 32.1(13) 2_655 . . . ?
Ag20 S8 C50 C51 36.4(12) . . . . ?
Ag20 S9 C57 C59 39.4(12) . . . . ?
Ag20 P1 C77 C78 32.9(12) . . . . ?
Ag20 P1 C77 C82 -150.2(11) . . . . ?
Ag20 P1 C83 C84 39.8(12) . . . . ?
Ag20 P1 C83 C88 -139.8(9) . . . . ?
Ag20 P1 C89 C90 44.3(14) . . . . ?
Ag20 P1 C89 C94 -139.0(13) . . . . ?
S1 C1 C2 C3 -85.9(13) . . . . ?
S1 C1 C2 C7 92.8(13) . . . . ?
S2 C8 C9 C10 -91.9(13) . . . . ?
S2 C8 C9 C14 85.7(14) . . . . ?
S3 C15 C16 C17 -138.6(11) . . . . ?
S3 C15 C16 C21 47.4(16) . . . . ?
S4 C22 C24 C23 -92.1(11) . . . . ?
S4 C22 C24 C25 87.0(12) . . . . ?
S5 C29 C30 C31 -83.4(13) . . . . ?
S5 C29 C30 C35 94.6(12) . . . . ?
S6 C36 C37 C38 131.5(18) . . . . ?
S6 C36 C37 C42 -51.5(19) . . . . ?
S7 C43 C44 C45 90.7(11) . . . . ?
S7 C43 C44 C49 -90.1(11) . . . . ?
S8 C50 C51 C56 -97.3(10) . . . . ?
S8 C50 C51 C52 83.6(11) . . . . ?
S9 C57 C59 C60 84.0(14) . . . . ?
S9 C57 C59 C64 -100.0(13) . . . . ?
P1 C77 C78 C79 177.0(10) . . . . ?
P1 C77 C82 C81 -177.1(12) . . . . ?
P1 C83 C84 C85 179.3(12) . . . . ?
P1 C83 C88 C87 -179.8(10) . . . . ?
P1 C89 C90 C91 176.9(14) . . . . ?
P1 C89 C94 C93 -177.3(15) . . . . ?
F1 F2 C66 F1 -139.9(15) 2_655 . . . ?
F1 F2 C66 F2 -77.2(7) 2_655 . . 2_655 ?
F1 F2 C66 F3 -152.6(17) 2_655 . . 2_655 ?
F1 F2 C66 F3 -28.0(13) 2_655 . . . ?
F1 F2 C66 C65 102.8(7) 2_655 . . . ?
F3 F2 C66 F1 12.7(16) 2_655 . . . ?
F3 F2 C66 F1 152.6(17) 2_655 . . 2_655 ?
F3 F2 C66 F2 75.4(13) 2_655 . . 2_655 ?
F3 F2 C66 F3 125(2) 2_655 . . . ?
F3 F2 C66 C65 -104.6(13) 2_655 . . . ?
O1 C65 C66 F1 -95.5(13) . . . . ?
O1 C65 C66 F1 -95.5(13) 2_655 . . 2_655 ?
O1 C65 C66 F1 84.5(13) . . . 2_655 ?
O1 C65 C66 F1 84.5(13) 2_655 . . . ?
O1 C65 C66 F2 15.3(11) . . . . ?
O1 C65 C66 F2 15.3(11) 2_655 . . 2_655 ?
O1 C65 C66 F2 -164.7(11) 2_655 . . . ?
O1 C65 C66 F2 -164.7(11) . . . 2_655 ?
O1 C65 C66 F3 143.9(17) . . . . ?
O1 C65 C66 F3 -36.1(17) . . . 2_655 ?
O1 C65 C66 F3 -36.1(17) 2_655 . . . ?
O1 C65 C66 F3 143.9(17) 2_655 . . 2_655 ?
O2 C67 C68 F4 83.3(16) . . . . ?
O2 C67 C68 F5 -151.7(14) . . . . ?
O2 C67 C68 F6 -33.6(17) . . . . ?
O3 C67 C68 F4 -95.9(15) . . . . ?
O3 C67 C68 F5 29.2(19) . . . . ?
O3 C67 C68 F6 147.2(12) . . . . ?
O4 C69 C70 F7 -71.2(19) . . . . ?
O4 C69 C70 F8 42.4(19) . . . . ?
O4 C69 C70 F9 164(2) . . . . ?
O4 C69 C70 F7A -35(4) . . . . ?
O4 C69 C70 F8A 92(3) . . . . ?
O4 C69 C70 F9A -163(2) . . . . ?
O5 C69 C70 F7 108.9(17) . . . . ?
O5 C69 C70 F8 -137.6(17) . . . . ?
O5 C69 C70 F9 -16(3) . . . . ?
O5 C69 C70 F7A 145(3) . . . . ?
O5 C69 C70 F8A -88(3) . . . . ?
O5 C69 C70 F9A 17(2) . . . . ?
O6 C71 C72 F10 43(3) 2_655 . . . ?
O6 C71 C72 F10 -125(2) . . . . ?
O6 C71 C72 F11 168.3(14) 2_655 . . 2_655 ?
O6 C71 C72 F11 117(2) . . . . ?
O6 C71 C72 F11 -75(2) 2_655 . . . ?
O6 C71 C72 F11 0(2) . . . 2_655 ?
O6 C71 C72 C72 -141(3) 2_655 . . 2_655 ?
O6 C71 C72 C72 51(3) . . . 2_655 ?
O7 C73 C74 F12 178.4(18) . . . . ?
O7 C73 C74 F13 -58(2) . . . . ?
O7 C73 C74 F14 62(2) . . . . ?
O8 C73 C74 F12 -2(3) . . . . ?
O8 C73 C74 F13 121.6(19) . . . . ?
O8 C73 C74 F14 -118.6(18) . . . . ?
O9 C75 C76 F15 12(2) . . . . ?
O9 C75 C76 F16 147.8(16) . . . . ?
O9 C75 C76 F17 -102.9(16) . . . . ?
O10 C75 C76 F15 -168.2(18) . . . . ?
O10 C75 C76 F16 -32(2) . . . . ?
O10 C75 C76 F17 77.0(18) . . . . ?
C1 C2 C3 C4 -178.8(12) . . . . ?
C1 C2 C7 C6 179.9(11) . . . . ?
C2 C3 C4 C5 -3(2) . . . . ?
C3 C2 C7 C6 -1.4(17) . . . . ?
C3 C4 C5 C6 1(2) . . . . ?
C4 C5 C6 C7 0(2) . . . . ?
C5 C6 C7 C2 0.3(19) . . . . ?
C7 C2 C3 C4 2.5(17) . . . . ?
C8 C9 C10 C11 177.3(13) . . . . ?
C8 C9 C14 C13 -178.1(13) . . . . ?
C9 C10 C11 C12 1(2) . . . . ?
C10 C9 C14 C13 0(2) . . . . ?
C10 C11 C12 C13 0(3) . . . . ?
C11 C12 C13 C14 -1(3) . . . . ?
C12 C13 C14 C9 1(3) . . . . ?
C14 C9 C10 C11 0(2) . . . . ?
C15 C16 C17 C18 -177.1(17) . . . . ?
C15 C16 C21 C20 177.6(14) . . . . ?
C16 C17 C18 C19 3(3) . . . . ?
C17 C16 C21 C20 4(2) . . . . ?
C17 C18 C19 C20 -4(3) . . . . ?
C18 C19 C20 C21 5(3) . . . . ?
C19 C20 C21 C16 -5(3) . . . . ?
C21 C16 C17 C18 -3(2) . . . . ?
C22 C24 C25 C26 -179.7(10) . . . . ?
C23 C24 C25 C26 -0.6(17) . . . . ?
C24 C23 C28 C27 -3(2) . . . . ?
C24 C25 C26 C27 0.4(19) . . . . ?
C25 C26 C27 C28 -1(2) . . . . ?
C26 C27 C28 C23 3(2) . . . . ?
C28 C23 C24 C22 -179.0(11) . . . . ?
C28 C23 C24 C25 1.9(17) . . . . ?
C29 C30 C31 C32 179.5(12) . . . . ?
C29 C30 C35 C34 -178.5(12) . . . . ?
C30 C31 C32 C33 -2(2) . . . . ?
C31 C30 C35 C34 -0.4(19) . . . . ?
C31 C32 C33 C34 1(2) . . . . ?
C32 C33 C34 C35 0(2) . . . . ?
C33 C34 C35 C30 0(2) . . . . ?
C35 C30 C31 C32 1.4(19) . . . . ?
C36 C37 C38 C39 163(2) . . . . ?
C36 C37 C42 C41 -173.9(18) . . . . ?
C37 C38 C39 C40 27(4) . . . . ?
C38 C37 C42 C41 3(3) . . . . ?
C38 C39 C40 C41 -26(5) . . . . ?
C39 C40 C41 C42 14(4) . . . . ?
C40 C41 C42 C37 -2(3) . . . . ?
C42 C37 C38 C39 -14(3) . . . . ?
C43 C44 C45 C46 -177.8(11) . . . . ?
C43 C44 C49 C48 177.6(12) . . . . ?
C44 C45 C46 C47 -3(2) . . . . ?
C45 C44 C49 C48 -3.3(18) . . . . ?
C45 C46 C47 C48 3(2) . . . . ?
C46 C47 C48 C49 -3(2) . . . . ?
C47 C48 C49 C44 3(2) . . . . ?
C49 C44 C45 C46 3.0(17) . . . . ?
C56 C55 C54 C53 0.0 . . . . ?
C55 C56 C51 C50 -179.1(10) . . . . ?
C55 C56 C51 C52 0.0 . . . . ?
C55 C54 C53 C52 0.0 . . . . ?
C54 C53 C52 C51 0.0 . . . . ?
C53 C52 C51 C50 179.2(10) . . . . ?
C53 C52 C51 C56 0.0 . . . . ?
C51 C56 C55 C54 0.0 . . . . ?
C57 C59 C60 C61 177.3(15) . . . . ?
C57 C59 C64 C63 -175.7(14) . . . . ?
C59 C60 C61 C62 -1(3) . . . . ?
C60 C59 C64 C63 0(2) . . . . ?
C60 C61 C62 C63 -2(3) . . . . ?
C61 C62 C63 C64 3(3) . . . . ?
C62 C63 C64 C59 -3(3) . . . . ?
C64 C59 C60 C61 1(2) . . . . ?
C72 F11 C72 F10 166(3) 2_655 . . . ?
C72 F11 C72 F11 55.8(15) 2_655 . . 2_655 ?
C72 F11 C72 C71 -61.9(15) 2_655 . . . ?
C72 C71 C72 F10 -176(5) 2_655 . . . ?
C72 C71 C72 F11 66(2) 2_655 . . . ?
C72 C71 C72 F11 -50(2) 2_655 . . 2_655 ?
C77 P1 C83 C84 161.1(11) . . . . ?
C77 P1 C83 C88 -18.6(12) . . . . ?
C77 P1 C89 C90 -86.4(12) . . . . ?
C77 P1 C89 C94 90.3(15) . . . . ?
C77 C78 C79 C80 0(2) . . . . ?
C78 C77 C82 C81 0(2) . . . . ?
C78 C79 C80 C81 1(2) . . . . ?
C79 C80 C81 C82 -1(2) . . . . ?
C80 C81 C82 C77 1(2) . . . . ?
C82 C77 C78 C79 0(2) . . . . ?
C83 P1 C77 C78 -83.6(11) . . . . ?
C83 P1 C77 C82 93.4(13) . . . . ?
C83 P1 C89 C90 164.4(12) . . . . ?
C83 P1 C89 C94 -18.9(16) . . . . ?
C83 C84 C85 C86 1(2) . . . . ?
C84 C83 C88 C87 0.5(19) . . . . ?
C84 C85 C86 C87 0(2) . . . . ?
C85 C86 C87 C88 -1(2) . . . . ?
C86 C87 C88 C83 0.3(19) . . . . ?
C88 C83 C84 C85 -1(2) . . . . ?
C89 P1 C77 C78 167.3(10) . . . . ?
C89 P1 C77 C82 -15.8(13) . . . . ?
C89 P1 C83 C84 -89.1(12) . . . . ?
C89 P1 C83 C88 91.3(11) . . . . ?
C89 C90 C91 C92 2(3) . . . . ?
C90 C89 C94 C93 -1(3) . . . . ?
C90 C91 C92 C93 -3(3) . . . . ?
C91 C92 C93 C94 3(3) . . . . ?
C92 C93 C94 C89 -1(3) . . . . ?
C94 C89 C90 C91 0(2) . . . . ?
C96 N1 C95 O11 178.3(19) . . . . ?
C97 N1 C95 O11 2(3) . . . . ?
C99 N2 C98 O12 180.0(16) . . . . ?
C100 N2 C98 O12 -2(3) . . . . ?
C102 N3 C101 O13 -175(3) . . . . ?
C103 N3 C101 O13 -3(4) . . . . ?
C105 N4 C104 O14 3(3) . . . . ?
C106 N4 C104 O14 -172(2) . . . . ?
C108 N5 C107 O15 5(3) . . . . ?
C109 N5 C107 O15 175.9(18) . . . . ?
C111 N6 C110 O16 1(4) . . . . ?
C112 N6 C110 O16 -179(2) . . . . ?
C114 N7 C118 O18 -2(12) . . . . ?
C116 N7 C113 O17 165(5) . . . . ?
C117 N7 C113 O17 -23(7) . . . . ?
Ag1 S1 C1 C2 112.7(10) 2_655 . . . ?
Ag1 S6 C36 C37 -52.3(13) . . . . ?
Ag1 S8 C50 C51 -42.5(11) . . . . ?
Ag1 O10 C75 O9 -5(2) . . . . ?
Ag1 O10 C75 C76 175.4(12) . . . . ?
Ag0A S3 C15 C16 -67.3(12) 2_655 . . . ?
Ag0A S8 C50 C51 119.1(9) . . . . ?
Ag0A S9 C57 C59 -44.3(11) . . . . ?
Ag0A O7 C73 O8 -4(2) . . . . ?
Ag0A O7 C73 C74 175.1(11) . . . . ?
C119 N7 C118 O18 179(7) . . . . ?

_olex2_submission_special_instructions 'No special instructions were received'
_oxdiff_exptl_absorpt_empirical_details 
;
Empirical correction (ABSPACK) includes:
- Absorption correction using spherical harmonics
- Frame scaling
;
_oxdiff_exptl_absorpt_empirical_full_max 5.777
_oxdiff_exptl_absorpt_empirical_full_min 0.410
