# Electronic Supplementary Material (ESI) for Dalton Transactions.
# This journal is © The Royal Society of Chemistry 2022

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_33333
_database_code_depnum_ccdc_archive 'CCDC 2206328'
loop_
_audit_author_name
_audit_author_address
'Jianlong Huang'
;ShiHeZi University
China
;
_audit_update_record             
;
2022-09-09 deposited with the CCDC.	2022-09-28 downloaded from the CCDC.
;
_audit_creation_date             2022-03-28
_audit_creation_method           
;
Olex2 1.3
(compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6408)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'B8 Na3 O15 Y'
_chemical_formula_sum            'B8 Na3 O15 Y'
_chemical_formula_weight         484.36
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Y Y -2.7962 3.5667 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   6.4122(2)
_cell_length_b                   7.3634(3)
_cell_length_c                   13.1781(5)
_cell_angle_alpha                89.126(2)
_cell_angle_beta                 78.657(2)
_cell_angle_gamma                66.8170(10)
_cell_volume                     559.46(4)
_cell_formula_units_Z            2
_cell_measurement_reflns_used    7662
_cell_measurement_temperature    273.15
_cell_measurement_theta_max      27.51
_cell_measurement_theta_min      3.02
_shelx_estimated_absorpt_T_max   ?
_shelx_estimated_absorpt_T_min   ?
_exptl_absorpt_coefficient_mu    5.430
_exptl_absorpt_correction_T_max  0.7456
_exptl_absorpt_correction_T_min  0.6266
_exptl_absorpt_correction_type   none
_exptl_absorpt_process_details   
;
SADABS-2016/2 (Bruker,2016/2) was used for absorption correction.
wR2(int) was 0.1540 before and 0.0551 after correction.
The Ratio of minimum to maximum transmission is 0.8404.
The λ/2 correction factor is Not present.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            'clear light colourless'
_exptl_crystal_colour_lustre     clear
_exptl_crystal_colour_modifier   light
_exptl_crystal_colour_primary    colourless
_exptl_crystal_density_diffrn    2.875
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             464
_exptl_crystal_size_max          0.1
_exptl_crystal_size_mid          0.1
_exptl_crystal_size_min          0.1
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0547
_diffrn_reflns_av_unetI/netI     0.0286
_diffrn_reflns_Laue_measured_fraction_full 0.986
_diffrn_reflns_Laue_measured_fraction_max 0.986
_diffrn_reflns_limit_h_max       8
_diffrn_reflns_limit_h_min       -7
_diffrn_reflns_limit_k_max       9
_diffrn_reflns_limit_k_min       -9
_diffrn_reflns_limit_l_max       17
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_number            17964
_diffrn_reflns_point_group_measured_fraction_full 0.986
_diffrn_reflns_point_group_measured_fraction_max 0.986
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         27.517
_diffrn_reflns_theta_min         1.580
_diffrn_ambient_temperature      273.15
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.986
_diffrn_measured_fraction_theta_max 0.986
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_diffrn_source_current           1.4
_diffrn_source_power             0.07
_diffrn_source_voltage           50.0
_diffrn_standards_number         0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                2438
_reflns_number_total             2545
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT V8.40B (?, 2016)'
_computing_data_collection       ?
_computing_data_reduction        'SAINT V8.40B (?, 2016)'
_computing_molecular_graphics    'Olex2 1.3 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.3 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2018/3 (Sheldrick, 2015)'
_computing_structure_solution    'SHELXT 2018/2 (Sheldrick, 2018)'
_refine_diff_density_max         0.379
_refine_diff_density_min         -0.322
_refine_diff_density_rms         0.087
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.147
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     244
_refine_ls_number_reflns         2545
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0216
_refine_ls_R_factor_gt           0.0202
_refine_ls_restrained_S_all      1.147
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0250P)²+0.6362P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0607
_refine_ls_wR_factor_ref         0.0612
_refine_special_details          ?
_olex2_refinement_description    
;
;
_atom_sites_solution_hydrogens   .
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Na1 Na 1.03800(19) 0.26961(15) 0.88836(8) 0.0187(2) Uani 1 1 d . . . . .
Na2 Na 0.76721(19) 0.23926(16) 0.47700(8) 0.0200(2) Uani 1 1 d . . . . .
Na3 Na 0.62444(19) 1.09515(16) 0.76472(9) 0.0205(2) Uani 1 1 d . . . . .
Y1 Y -0.10077(4) 1.25120(3) 1.17082(2) 0.00799(8) Uani 1 1 d . . . . .
B1 B 0.6524(5) 0.6129(4) 1.0149(2) 0.0111(5) Uani 1 1 d . . . . .
B2 B 0.3282(5) 0.9207(4) 0.9934(2) 0.0103(5) Uani 1 1 d . . . . .
B3 B 0.5943(4) 0.6991(4) 0.8353(2) 0.0098(5) Uani 1 1 d . . . . .
B4 B 0.9010(4) 0.6411(4) 0.6677(2) 0.0089(5) Uani 1 1 d . . . . .
B5 B 0.6314(5) 0.4805(4) 0.6842(2) 0.0091(5) Uani 1 1 d . . . . .
B6 B 0.7815(5) 0.7851(4) 0.4969(2) 0.0106(5) Uani 1 1 d . . . . .
B7 B 0.6803(4) 0.6295(4) 0.3608(2) 0.0086(5) Uani 1 1 d . . . . .
B8 B 0.8433(5) 0.8872(4) 0.3216(2) 0.0105(5) Uani 1 1 d . . . . .
O1 O 0.7874(3) 0.5031(3) 1.07581(14) 0.0148(4) Uani 1 1 d . . . . .
O2 O 0.6959(3) 0.5628(2) 0.90983(13) 0.0129(3) Uani 1 1 d . . . . .
O3 O 0.4596(3) 0.7889(3) 1.05629(13) 0.0133(3) Uani 1 1 d . . . . .
O4 O 0.1511(3) 1.0855(3) 1.03349(13) 0.0146(4) Uani 1 1 d . . . . .
O5 O 0.3865(3) 0.8715(2) 0.88683(12) 0.0108(3) Uani 1 1 d . . . . .
O6 O 0.7728(3) 0.7513(2) 0.77013(13) 0.0106(3) Uani 1 1 d . . . . .
O7 O 0.4944(3) 0.6110(3) 0.76632(13) 0.0121(3) Uani 1 1 d . . . . .
O8 O 0.8468(3) 0.4725(2) 0.64692(13) 0.0105(3) Uani 1 1 d . . . . .
O9 O 0.5569(3) 0.3538(2) 0.64289(13) 0.0099(3) Uani 1 1 d . . . . .
O10 O 0.8507(3) 0.7847(2) 0.58772(13) 0.0121(3) Uani 1 1 d . . . . .
O11 O 0.8303(3) 0.9170(2) 0.42826(13) 0.0123(3) Uani 1 1 d . . . . .
O12 O 0.6709(3) 0.6755(2) 0.47104(12) 0.0109(3) Uani 1 1 d . . . . .
O13 O 0.9547(3) 0.9699(3) 0.25229(13) 0.0132(3) Uani 1 1 d . . . . .
O14 O 0.7328(3) 0.7738(2) 0.29298(12) 0.0100(3) Uani 1 1 d . . . . .
O15 O 0.8502(3) 0.4258(2) 0.32796(12) 0.0093(3) Uani 1 1 d . . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Na1 Na3 3.5065(16) 1_645 ?
Na1 B1 2.949(3) 2_767 ?
Na1 B1 2.978(3) . ?
Na1 B2 3.019(3) 1_645 ?
Na1 B8 2.854(3) 2_766 ?
Na1 O1 2.834(2) . ?
Na1 O1 2.446(2) 2_767 ?
Na1 O2 2.3661(19) . ?
Na1 O4 2.391(2) 1_645 ?
Na1 O5 2.9006(19) 1_645 ?
Na1 O13 2.559(2) 2_766 ?
Na1 O14 2.4990(19) 2_766 ?
Na2 B4 2.962(3) 2_766 ?
Na2 B5 3.060(3) . ?
Na2 B6 2.916(3) 2_766 ?
Na2 B7 3.034(3) 2_666 ?
Na2 B7 3.139(3) . ?
Na2 B8 3.150(3) 1_545 ?
Na2 O9 2.3045(19) . ?
Na2 O10 2.367(2) 2_766 ?
Na2 O11 2.903(2) 2_766 ?
Na2 O11 2.3224(19) 1_545 ?
Na2 O12 2.573(2) 2_666 ?
Na2 O15 2.4719(19) . ?
Na3 Y1 3.3728(11) 2_677 ?
Na3 B3 3.114(3) . ?
Na3 B5 3.028(3) 1_565 ?
Na3 B7 2.952(3) 2_676 ?
Na3 O3 2.405(2) 2_677 ?
Na3 O5 2.926(2) . ?
Na3 O6 2.3338(19) . ?
Na3 O9 2.434(2) 1_565 ?
Na3 O10 2.998(2) . ?
Na3 O13 2.512(2) 2_776 ?
Na3 O14 2.383(2) 2_676 ?
Y1 B3 3.056(3) 2_577 ?
Y1 B4 2.953(3) 2_677 ?
Y1 O1 2.1812(17) 1_465 ?
Y1 O4 2.1768(17) . ?
Y1 O5 2.5730(17) 2_577 ?
Y1 O6 2.3750(17) 2_677 ?
Y1 O7 2.2965(17) 2_577 ?
Y1 O13 2.2520(17) 1_456 ?
Y1 O15 2.3553(16) 1_466 ?
B1 O1 1.323(3) . ?
B1 O2 1.383(3) . ?
B1 O3 1.414(3) . ?
B2 O3 1.395(3) . ?
B2 O4 1.319(3) . ?
B2 O5 1.394(3) . ?
B3 O2 1.451(3) . ?
B3 O5 1.479(3) . ?
B3 O6 1.465(3) . ?
B3 O7 1.493(3) . ?
B4 O6 1.492(3) . ?
B4 O8 1.458(3) . ?
B4 O10 1.472(3) . ?
B4 O15 1.486(3) 2_766 ?
B5 O7 1.364(3) . ?
B5 O8 1.350(3) . ?
B5 O9 1.365(3) . ?
B6 O10 1.355(3) . ?
B6 O11 1.401(3) . ?
B6 O12 1.351(3) . ?
B7 O9 1.487(3) 2_666 ?
B7 O12 1.481(3) . ?
B7 O14 1.475(3) . ?
B7 O15 1.473(3) . ?
B8 O11 1.407(3) . ?
B8 O13 1.336(3) . ?
B8 O14 1.387(3) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
B1 Na1 Na3 142.99(6) . 1_645 ?
B1 Na1 Na3 62.26(6) 2_767 1_645 ?
B1 Na1 B1 85.83(8) 2_767 . ?
B1 Na1 B2 120.11(8) . 1_645 ?
B1 Na1 B2 71.42(8) 2_767 1_645 ?
B2 Na1 Na3 69.19(6) 1_645 1_645 ?
B8 Na1 Na3 62.95(6) 2_766 1_645 ?
B8 Na1 B1 135.60(8) 2_766 . ?
B8 Na1 B1 123.20(9) 2_766 2_767 ?
B8 Na1 B2 101.94(8) 2_766 1_645 ?
B8 Na1 O5 74.93(7) 2_766 1_645 ?
O1 Na1 Na3 68.52(5) 2_767 1_645 ?
O1 Na1 Na3 132.14(5) . 1_645 ?
O1 Na1 B1 69.91(7) . 2_767 ?
O1 Na1 B1 74.61(7) 2_767 . ?
O1 Na1 B1 26.34(7) 2_767 2_767 ?
O1 Na1 B1 26.16(6) . . ?
O1 Na1 B2 94.68(7) . 1_645 ?
O1 Na1 B2 97.59(7) 2_767 1_645 ?
O1 Na1 B8 115.56(8) 2_767 2_766 ?
O1 Na1 B8 161.46(8) . 2_766 ?
O1 Na1 O1 69.63(7) 2_767 . ?
O1 Na1 O5 121.81(6) . 1_645 ?
O1 Na1 O5 106.81(7) 2_767 1_645 ?
O1 Na1 O13 142.77(7) 2_767 2_766 ?
O1 Na1 O14 86.66(7) 2_767 2_766 ?
O2 Na1 Na3 139.68(6) . 1_645 ?
O2 Na1 B1 103.10(8) . 2_767 ?
O2 Na1 B1 27.02(7) . . ?
O2 Na1 B2 145.61(8) . 1_645 ?
O2 Na1 B8 108.66(8) . 2_766 ?
O2 Na1 O1 83.28(7) . 2_767 ?
O2 Na1 O1 53.19(6) . . ?
O2 Na1 O4 121.05(7) . 1_645 ?
O2 Na1 O5 166.93(7) . 1_645 ?
O2 Na1 O13 110.67(7) . 2_766 ?
O2 Na1 O14 110.10(7) . 2_766 ?
O4 Na1 Na3 88.93(6) 1_645 1_645 ?
O4 Na1 B1 66.42(7) 1_645 2_767 ?
O4 Na1 B1 95.19(7) 1_645 . ?
O4 Na1 B2 24.92(7) 1_645 1_645 ?
O4 Na1 B8 125.84(8) 1_645 2_766 ?
O4 Na1 O1 69.95(6) 1_645 . ?
O4 Na1 O1 91.44(7) 1_645 2_767 ?
O4 Na1 O5 51.89(5) 1_645 1_645 ?
O4 Na1 O13 108.18(7) 1_645 2_766 ?
O4 Na1 O14 128.21(7) 1_645 2_766 ?
O5 Na1 Na3 53.34(4) 1_645 1_645 ?
O5 Na1 B1 84.37(7) 1_645 2_767 ?
O5 Na1 B1 146.76(7) 1_645 . ?
O5 Na1 B2 27.15(6) 1_645 1_645 ?
O13 Na1 Na3 80.24(5) 2_766 1_645 ?
O13 Na1 B1 132.01(8) 2_766 . ?
O13 Na1 B1 141.78(8) 2_766 2_767 ?
O13 Na1 B2 89.38(7) 2_766 1_645 ?
O13 Na1 B8 27.89(7) 2_766 2_766 ?
O13 Na1 O1 146.45(7) 2_766 . ?
O13 Na1 O5 66.37(6) 2_766 1_645 ?
O14 Na1 Na3 42.79(5) 2_766 1_645 ?
O14 Na1 B1 95.91(7) 2_766 2_767 ?
O14 Na1 B1 133.35(8) 2_766 . ?
O14 Na1 B2 104.26(7) 2_766 1_645 ?
O14 Na1 B8 29.06(6) 2_766 2_766 ?
O14 Na1 O1 151.48(7) 2_766 . ?
O14 Na1 O5 79.33(6) 2_766 1_645 ?
O14 Na1 O13 56.26(6) 2_766 2_766 ?
B4 Na2 B5 108.36(8) 2_766 . ?
B4 Na2 B7 147.12(8) 2_766 2_666 ?
B4 Na2 B7 50.25(7) 2_766 . ?
B4 Na2 B8 92.05(7) 2_766 1_545 ?
B5 Na2 B7 89.55(7) . . ?
B5 Na2 B8 158.06(8) . 1_545 ?
B6 Na2 B4 52.44(8) 2_766 2_766 ?
B6 Na2 B5 79.13(8) 2_766 . ?
B6 Na2 B7 127.75(8) 2_766 2_666 ?
B6 Na2 B7 91.45(8) 2_766 . ?
B6 Na2 B8 108.76(8) 2_766 1_545 ?
B7 Na2 B5 50.51(7) 2_666 . ?
B7 Na2 B7 100.00(7) 2_666 . ?
B7 Na2 B8 110.22(7) . 1_545 ?
B7 Na2 B8 114.23(8) 2_666 1_545 ?
O9 Na2 B4 132.74(8) . 2_766 ?
O9 Na2 B5 24.72(6) . . ?
O9 Na2 B6 99.38(8) . 2_766 ?
O9 Na2 B7 28.38(6) . 2_666 ?
O9 Na2 B7 103.10(7) . . ?
O9 Na2 B8 135.11(8) . 1_545 ?
O9 Na2 O10 125.24(7) . 2_766 ?
O9 Na2 O11 85.70(6) . 2_766 ?
O9 Na2 O11 115.45(7) . 1_545 ?
O9 Na2 O12 57.46(6) . 2_666 ?
O9 Na2 O15 129.65(7) . . ?
O10 Na2 B4 29.46(6) 2_766 2_766 ?
O10 Na2 B5 102.52(7) 2_766 . ?
O10 Na2 B6 27.28(7) 2_766 2_766 ?
O10 Na2 B7 77.84(7) 2_766 . ?
O10 Na2 B7 153.02(8) 2_766 2_666 ?
O10 Na2 B8 91.25(7) 2_766 1_545 ?
O10 Na2 O11 50.71(6) 2_766 2_766 ?
O10 Na2 O12 169.29(8) 2_766 2_666 ?
O10 Na2 O15 59.44(6) 2_766 . ?
O11 Na2 B4 108.76(7) 1_545 2_766 ?
O11 Na2 B4 79.06(7) 2_766 2_766 ?
O11 Na2 B5 73.82(6) 2_766 . ?
O11 Na2 B5 134.86(8) 1_545 . ?
O11 Na2 B6 27.85(6) 2_766 2_766 ?
O11 Na2 B6 104.57(8) 1_545 2_766 ?
O11 Na2 B7 134.46(8) 1_545 . ?
O11 Na2 B7 118.28(7) 2_766 . ?
O11 Na2 B7 111.35(7) 2_766 2_666 ?
O11 Na2 B7 102.69(7) 1_545 2_666 ?
O11 Na2 B8 24.28(6) 1_545 1_545 ?
O11 Na2 B8 103.28(7) 2_766 1_545 ?
O11 Na2 O10 97.34(7) 1_545 2_766 ?
O11 Na2 O11 88.99(6) 1_545 2_766 ?
O11 Na2 O12 89.66(7) 1_545 2_666 ?
O11 Na2 O15 112.83(7) 1_545 . ?
O12 Na2 B4 140.11(8) 2_666 2_766 ?
O12 Na2 B5 77.75(7) 2_666 . ?
O12 Na2 B6 156.67(8) 2_666 2_766 ?
O12 Na2 B7 91.47(7) 2_666 . ?
O12 Na2 B7 29.17(6) 2_666 2_666 ?
O12 Na2 B8 91.86(7) 2_666 1_545 ?
O12 Na2 O11 137.96(6) 2_666 2_766 ?
O15 Na2 B4 30.06(6) . 2_766 ?
O15 Na2 B5 112.20(7) . . ?
O15 Na2 B6 81.42(7) . 2_766 ?
O15 Na2 B7 125.91(7) . 2_666 ?
O15 Na2 B7 27.28(6) . . ?
O15 Na2 B8 89.46(7) . 1_545 ?
O15 Na2 O11 108.79(6) . 2_766 ?
O15 Na2 O12 110.35(7) . 2_666 ?
Y1 Na3 Na1 130.96(4) 2_677 1_465 ?
B3 Na3 Na1 79.92(6) . 1_465 ?
B3 Na3 Y1 62.95(5) . 2_677 ?
B5 Na3 Na1 98.57(6) 1_565 1_465 ?
B5 Na3 Y1 120.52(6) 1_565 2_677 ?
B5 Na3 B3 175.61(8) 1_565 . ?
B7 Na3 Na1 67.97(6) 2_676 1_465 ?
B7 Na3 Y1 160.29(6) 2_676 2_677 ?
B7 Na3 B3 124.26(8) 2_676 . ?
B7 Na3 B5 51.52(7) 2_676 1_565 ?
B7 Na3 O10 91.84(7) 2_676 . ?
O3 Na3 Na1 64.88(5) 2_677 1_465 ?
O3 Na3 Y1 82.96(5) 2_677 2_677 ?
O3 Na3 B3 89.39(7) 2_677 . ?
O3 Na3 B5 93.70(7) 2_677 1_565 ?
O3 Na3 B7 113.98(7) 2_677 2_676 ?
O3 Na3 O5 72.37(6) 2_677 . ?
O3 Na3 O9 114.86(7) 2_677 1_565 ?
O3 Na3 O10 153.54(7) 2_677 . ?
O3 Na3 O13 91.21(7) 2_677 2_776 ?
O5 Na3 Na1 52.67(4) . 1_465 ?
O5 Na3 Y1 83.68(4) . 2_677 ?
O5 Na3 B3 28.13(6) . . ?
O5 Na3 B5 151.06(7) . 1_565 ?
O5 Na3 B7 110.33(7) . 2_676 ?
O5 Na3 O10 93.98(5) . . ?
O6 Na3 Na1 106.28(6) . 1_465 ?
O6 Na3 Y1 44.74(4) . 2_677 ?
O6 Na3 B3 26.58(6) . . ?
O6 Na3 B5 154.04(8) . 1_565 ?
O6 Na3 B7 132.73(8) . 2_676 ?
O6 Na3 O3 103.45(7) . 2_677 ?
O6 Na3 O5 54.63(6) . . ?
O6 Na3 O9 141.52(8) . 1_565 ?
O6 Na3 O10 51.35(6) . . ?
O6 Na3 O13 81.17(7) . 2_776 ?
O6 Na3 O14 113.03(7) . 2_676 ?
O9 Na3 Na1 93.45(5) 1_565 1_465 ?
O9 Na3 Y1 134.65(6) 1_565 2_677 ?
O9 Na3 B3 149.51(8) 1_565 . ?
O9 Na3 B5 26.17(6) 1_565 1_565 ?
O9 Na3 B7 30.14(6) 1_565 2_676 ?
O9 Na3 O5 140.44(7) 1_565 . ?
O9 Na3 O10 90.24(6) 1_565 . ?
O9 Na3 O13 94.17(7) 1_565 2_776 ?
O10 Na3 Na1 124.72(5) . 1_465 ?
O10 Na3 Y1 72.88(4) . 2_677 ?
O10 Na3 B3 70.28(6) . . ?
O10 Na3 B5 107.64(7) . 1_565 ?
O13 Na3 Na1 155.90(6) 2_776 1_465 ?
O13 Na3 Y1 41.89(4) 2_776 2_677 ?
O13 Na3 B3 103.98(7) 2_776 . ?
O13 Na3 B5 79.10(7) 2_776 1_565 ?
O13 Na3 B7 123.92(8) 2_776 2_676 ?
O13 Na3 O5 125.19(6) 2_776 . ?
O13 Na3 O10 78.09(6) 2_776 . ?
O14 Na3 Na1 45.42(5) 2_676 1_465 ?
O14 Na3 Y1 157.77(6) 2_676 2_677 ?
O14 Na3 B3 96.68(7) 2_676 . ?
O14 Na3 B5 79.44(7) 2_676 1_565 ?
O14 Na3 B7 29.73(6) 2_676 2_676 ?
O14 Na3 O3 106.92(7) 2_676 2_677 ?
O14 Na3 O5 80.64(6) 2_676 . ?
O14 Na3 O9 59.87(6) 2_676 1_565 ?
O14 Na3 O10 92.54(6) 2_676 . ?
O14 Na3 O13 152.65(8) 2_676 2_776 ?
Na1 Y1 Na1 71.54(3) 1_465 2_677 ?
Na3 Y1 Na1 106.25(3) 2_677 1_465 ?
Na3 Y1 Na1 112.83(3) 2_677 2_677 ?
B3 Y1 Na1 109.25(5) 2_577 2_677 ?
B3 Y1 Na1 91.16(5) 2_577 1_465 ?
B3 Y1 Na3 137.65(5) 2_577 2_677 ?
B4 Y1 Na1 129.81(5) 2_677 1_465 ?
B4 Y1 Na1 70.87(5) 2_677 2_677 ?
B4 Y1 Na3 61.29(5) 2_677 2_677 ?
B4 Y1 B3 132.28(7) 2_677 2_577 ?
O1 Y1 Na1 50.53(5) 1_465 1_465 ?
O1 Y1 Na1 38.10(5) 1_465 2_677 ?
O1 Y1 Na3 142.46(5) 1_465 2_677 ?
O1 Y1 B3 77.74(7) 1_465 2_577 ?
O1 Y1 B4 107.81(7) 1_465 2_677 ?
O1 Y1 O5 89.38(6) 1_465 2_577 ?
O1 Y1 O6 107.76(6) 1_465 2_677 ?
O1 Y1 O7 78.08(7) 1_465 2_577 ?
O1 Y1 O13 165.99(7) 1_465 1_456 ?
O1 Y1 O15 98.45(6) 1_465 1_466 ?
O4 Y1 Na1 94.68(5) . 2_677 ?
O4 Y1 Na1 38.65(5) . 1_465 ?
O4 Y1 Na3 68.79(5) . 2_677 ?
O4 Y1 B3 112.70(7) . 2_577 ?
O4 Y1 B4 114.85(7) . 2_677 ?
O4 Y1 O1 87.62(7) . 1_465 ?
O4 Y1 O5 87.19(6) . 2_577 ?
O4 Y1 O6 84.75(6) . 2_677 ?
O4 Y1 O7 140.16(6) . 2_577 ?
O4 Y1 O13 90.90(7) . 1_456 ?
O4 Y1 O15 144.24(6) . 1_466 ?
O5 Y1 Na1 78.26(4) 2_577 1_465 ?
O5 Y1 Na1 127.06(4) 2_577 2_677 ?
O5 Y1 Na3 116.92(4) 2_577 2_677 ?
O5 Y1 B3 28.86(6) 2_577 2_577 ?
O5 Y1 B4 151.92(6) 2_577 2_677 ?
O6 Y1 Na1 105.47(4) 2_677 1_465 ?
O6 Y1 Na1 71.22(4) 2_677 2_677 ?
O6 Y1 Na3 43.76(4) 2_677 2_677 ?
O6 Y1 B3 162.18(6) 2_677 2_577 ?
O6 Y1 B4 30.10(6) 2_677 2_677 ?
O6 Y1 O5 160.68(6) 2_677 2_577 ?
O7 Y1 Na1 96.26(5) 2_577 2_677 ?
O7 Y1 Na1 111.12(5) 2_577 1_465 ?
O7 Y1 Na3 138.29(5) 2_577 2_677 ?
O7 Y1 B3 28.08(6) 2_577 2_577 ?
O7 Y1 B4 104.93(6) 2_577 2_677 ?
O7 Y1 O5 56.06(5) 2_577 2_577 ?
O7 Y1 O6 134.98(6) 2_577 2_677 ?
O7 Y1 O15 75.22(6) 2_577 1_466 ?
O13 Y1 Na1 124.02(5) 1_456 1_465 ?
O13 Y1 Na1 155.83(5) 1_456 2_677 ?
O13 Y1 Na3 48.13(5) 1_456 2_677 ?
O13 Y1 B3 90.03(7) 1_456 2_577 ?
O13 Y1 B4 85.44(7) 1_456 2_677 ?
O13 Y1 O5 76.63(6) 1_456 2_577 ?
O13 Y1 O6 85.95(6) 1_456 2_677 ?
O13 Y1 O7 94.38(6) 1_456 2_577 ?
O13 Y1 O15 90.88(6) 1_456 1_466 ?
O15 Y1 Na1 142.55(4) 1_466 1_465 ?
O15 Y1 Na1 71.08(4) 1_466 2_677 ?
O15 Y1 Na3 86.33(4) 1_466 2_677 ?
O15 Y1 B3 103.01(6) 1_466 2_577 ?
O15 Y1 B4 29.90(6) 1_466 2_677 ?
O15 Y1 O5 127.83(5) 1_466 2_577 ?
O15 Y1 O6 59.77(6) 1_466 2_677 ?
Na1 B1 Na1 94.17(8) 2_767 . ?
O1 B1 Na1 55.12(12) . 2_767 ?
O1 B1 Na1 70.83(14) . . ?
O1 B1 O2 121.8(2) . . ?
O1 B1 O3 120.1(2) . . ?
O2 B1 Na1 122.99(16) . 2_767 ?
O2 B1 Na1 51.00(11) . . ?
O2 B1 O3 118.1(2) . . ?
O3 B1 Na1 91.52(14) . 2_767 ?
O3 B1 Na1 168.95(18) . . ?
O3 B2 Na1 168.34(17) . 1_465 ?
O4 B2 Na1 49.79(12) . 1_465 ?
O4 B2 O3 121.1(2) . . ?
O4 B2 O5 120.8(2) . . ?
O5 B2 Na1 71.68(13) . 1_465 ?
O5 B2 O3 118.1(2) . . ?
Y1 B3 Na3 105.28(8) 2_577 . ?
O2 B3 Na3 132.77(16) . . ?
O2 B3 Y1 113.64(15) . 2_577 ?
O2 B3 O5 111.44(19) . . ?
O2 B3 O6 109.4(2) . . ?
O2 B3 O7 111.89(19) . . ?
O5 B3 Na3 68.86(12) . . ?
O5 B3 Y1 57.11(11) . 2_577 ?
O5 B3 O7 101.46(18) . . ?
O6 B3 Na3 45.48(10) . . ?
O6 B3 Y1 135.94(16) . 2_577 ?
O6 B3 O5 114.1(2) . . ?
O6 B3 O7 108.25(19) . . ?
O7 B3 Na3 114.18(15) . . ?
O7 B3 Y1 46.38(10) . 2_577 ?
Y1 B4 Na2 84.15(7) 2_677 2_766 ?
O6 B4 Na2 122.04(14) . 2_766 ?
O6 B4 Y1 52.97(10) . 2_677 ?
O8 B4 Na2 124.14(15) . 2_766 ?
O8 B4 Y1 134.30(16) . 2_677 ?
O8 B4 O6 113.82(19) . . ?
O8 B4 O10 111.74(19) . . ?
O8 B4 O15 110.53(18) . 2_766 ?
O10 B4 Na2 52.27(11) . 2_766 ?
O10 B4 Y1 113.93(14) . 2_677 ?
O10 B4 O6 107.25(18) . . ?
O10 B4 O15 108.49(19) . 2_766 ?
O15 B4 Na2 56.42(11) 2_766 2_766 ?
O15 B4 Y1 52.18(10) 2_766 2_677 ?
O15 B4 O6 104.63(18) 2_766 . ?
Na3 B5 Na2 80.95(7) 1_545 . ?
O7 B5 Na2 158.99(17) . . ?
O7 B5 Na3 101.16(15) . 1_545 ?
O7 B5 O9 120.9(2) . . ?
O8 B5 Na2 78.08(13) . . ?
O8 B5 Na3 113.72(15) . 1_545 ?
O8 B5 O7 118.9(2) . . ?
O8 B5 O9 120.2(2) . . ?
O9 B5 Na2 44.91(11) . . ?
O9 B5 Na3 51.84(11) . 1_545 ?
O10 B6 Na2 53.16(12) . 2_766 ?
O10 B6 O11 113.7(2) . . ?
O11 B6 Na2 75.54(13) . 2_766 ?
O12 B6 Na2 142.82(17) . 2_766 ?
O12 B6 O10 125.8(2) . . ?
O12 B6 O11 120.4(2) . . ?
Na2 B7 Na2 80.00(7) 2_666 . ?
Na3 B7 Na2 143.43(9) 2_676 . ?
Na3 B7 Na2 82.62(7) 2_676 2_666 ?
O9 B7 Na2 89.83(13) 2_666 . ?
O9 B7 Na2 47.43(10) 2_666 2_666 ?
O9 B7 Na3 55.26(11) 2_666 2_676 ?
O12 B7 Na2 57.91(11) . 2_666 ?
O12 B7 Na2 71.88(11) . . ?
O12 B7 Na3 123.45(15) . 2_676 ?
O12 B7 O9 105.13(18) . 2_666 ?
O14 B7 Na2 120.26(15) . 2_666 ?
O14 B7 Na2 158.72(16) . . ?
O14 B7 Na3 53.25(11) . 2_676 ?
O14 B7 O9 108.50(19) . 2_666 ?
O14 B7 O12 111.87(18) . . ?
O15 B7 Na2 50.26(10) . . ?
O15 B7 Na2 127.89(15) . 2_666 ?
O15 B7 Na3 126.59(15) . 2_676 ?
O15 B7 O9 110.00(18) . 2_666 ?
O15 B7 O12 109.85(19) . . ?
O15 B7 O14 111.29(19) . . ?
Na1 B8 Na2 147.77(10) 2_766 1_565 ?
O11 B8 Na1 165.10(17) . 2_766 ?
O11 B8 Na2 42.75(10) . 1_565 ?
O13 B8 Na1 63.67(13) . 2_766 ?
O13 B8 Na2 85.52(14) . 1_565 ?
O13 B8 O11 120.2(2) . . ?
O13 B8 O14 122.4(2) . . ?
O14 B8 Na1 61.10(12) . 2_766 ?
O14 B8 Na2 142.05(17) . 1_565 ?
O14 B8 O11 117.4(2) . . ?
Na1 O1 Na1 110.37(7) 2_767 . ?
Y1 O1 Na1 108.51(8) 1_645 2_767 ?
Y1 O1 Na1 93.02(6) 1_645 . ?
B1 O1 Na1 98.54(15) . 2_767 ?
B1 O1 Na1 83.01(14) . . ?
B1 O1 Y1 152.25(17) . 1_645 ?
B1 O2 Na1 101.98(15) . . ?
B1 O2 B3 123.94(19) . . ?
B3 O2 Na1 131.12(14) . . ?
B1 O3 Na3 121.79(15) . 2_677 ?
B2 O3 Na3 115.45(14) . 2_677 ?
B2 O3 B1 122.1(2) . . ?
Y1 O4 Na1 106.69(8) . 1_465 ?
B2 O4 Na1 105.29(15) . 1_465 ?
B2 O4 Y1 147.67(17) . . ?
Na1 O5 Na3 74.00(5) 1_465 . ?
Y1 O5 Na1 86.91(5) 2_577 1_465 ?
Y1 O5 Na3 126.10(6) 2_577 . ?
B2 O5 Na1 81.17(13) . 1_465 ?
B2 O5 Na3 114.48(14) . . ?
B2 O5 Y1 111.44(14) . 2_577 ?
B2 O5 B3 123.84(19) . . ?
B3 O5 Na1 151.92(14) . 1_465 ?
B3 O5 Na3 83.01(13) . . ?
B3 O5 Y1 94.03(13) . 2_577 ?
Na3 O6 Y1 91.49(6) . 2_677 ?
B3 O6 Na3 107.94(14) . . ?
B3 O6 Y1 122.47(14) . 2_677 ?
B3 O6 B4 120.40(18) . . ?
B4 O6 Na3 114.20(13) . . ?
B4 O6 Y1 96.92(13) . 2_677 ?
B3 O7 Y1 105.54(13) . 2_577 ?
B5 O7 Y1 132.90(15) . 2_577 ?
B5 O7 B3 121.54(19) . . ?
B5 O8 B4 119.53(19) . . ?
Na2 O9 Na3 113.00(8) . 1_545 ?
B5 O9 Na2 110.36(15) . . ?
B5 O9 Na3 101.99(14) . 1_545 ?
B5 O9 B7 131.36(19) . 2_666 ?
B7 O9 Na2 104.19(13) 2_666 . ?
B7 O9 Na3 94.60(13) 2_666 1_545 ?
Na2 O10 Na3 109.01(7) 2_766 . ?
B4 O10 Na2 98.27(14) . 2_766 ?
B4 O10 Na3 85.91(12) . . ?
B6 O10 Na2 99.57(15) . 2_766 ?
B6 O10 Na3 127.00(15) . . ?
B6 O10 B4 133.41(19) . . ?
Na2 O11 Na2 91.01(6) 1_565 2_766 ?
B6 O11 Na2 124.09(15) . 1_565 ?
B6 O11 Na2 76.61(13) . 2_766 ?
B6 O11 B8 119.48(19) . . ?
B8 O11 Na2 112.97(14) . 1_565 ?
B8 O11 Na2 122.93(15) . 2_766 ?
B6 O12 Na2 126.14(15) . 2_666 ?
B6 O12 B7 120.63(19) . . ?
B7 O12 Na2 92.92(13) . 2_666 ?
Na3 O13 Na1 103.15(7) 2_776 2_766 ?
Y1 O13 Na1 103.08(7) 1_654 2_766 ?
Y1 O13 Na3 89.98(6) 1_654 2_776 ?
B8 O13 Na1 88.44(14) . 2_766 ?
B8 O13 Na3 123.27(16) . 2_776 ?
B8 O13 Y1 141.65(16) . 1_654 ?
Na3 O14 Na1 91.79(7) 2_676 2_766 ?
B7 O14 Na1 130.88(14) . 2_766 ?
B7 O14 Na3 97.02(13) . 2_676 ?
B8 O14 Na1 89.84(14) . 2_766 ?
B8 O14 Na3 124.44(15) . 2_676 ?
B8 O14 B7 122.23(19) . . ?
Y1 O15 Na2 110.36(7) 1_644 . ?
B4 O15 Na2 93.53(13) 2_766 . ?
B4 O15 Y1 97.92(12) 2_766 1_644 ?
B7 O15 Na2 102.45(13) . . ?
B7 O15 Y1 125.52(14) . 1_644 ?
B7 O15 B4 122.53(17) . 2_766 ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Na1 B1 O1 Na1 109.65(7) . . . 2_767 ?
Na1 B1 O1 Na1 -109.65(7) 2_767 . . . ?
Na1 B1 O1 Y1 167.2(4) 2_767 . . 1_645 ?
Na1 B1 O1 Y1 -83.2(3) . . . 1_645 ?
Na1 B1 O2 Na1 65.55(17) 2_767 . . . ?
Na1 B1 O2 B3 -162.4(3) . . . . ?
Na1 B1 O2 B3 -96.8(2) 2_767 . . . ?
Na1 B1 O3 Na3 -47.22(15) 2_767 . . 2_677 ?
Na1 B1 O3 Na3 -168.3(8) . . . 2_677 ?
Na1 B1 O3 B2 1.8(10) . . . . ?
Na1 B1 O3 B2 122.8(2) 2_767 . . . ?
Na1 B2 O3 Na3 27.5(9) 1_465 . . 2_677 ?
Na1 B2 O3 B1 -143.1(8) 1_465 . . . ?
Na1 B2 O4 Y1 171.3(4) 1_465 . . . ?
Na1 B2 O5 Na3 67.83(9) 1_465 . . . ?
Na1 B2 O5 Y1 -83.13(9) 1_465 . . 2_577 ?
Na1 B2 O5 B3 166.1(2) 1_465 . . . ?
Na1 B8 O11 Na2 141.4(6) 2_766 . . 1_565 ?
Na1 B8 O11 Na2 34.1(8) 2_766 . . 2_766 ?
Na1 B8 O11 B6 -58.8(8) 2_766 . . . ?
Na1 B8 O13 Na3 -104.74(14) 2_766 . . 2_776 ?
Na1 B8 O13 Y1 109.3(2) 2_766 . . 1_654 ?
Na1 B8 O14 Na3 -92.05(13) 2_766 . . 2_676 ?
Na1 B8 O14 B7 140.5(2) 2_766 . . . ?
Na2 B4 O6 Na3 43.30(19) 2_766 . . . ?
Na2 B4 O6 Y1 -51.48(16) 2_766 . . 2_677 ?
Na2 B4 O6 B3 174.23(16) 2_766 . . . ?
Na2 B4 O8 B5 -147.17(18) 2_766 . . . ?
Na2 B4 O10 Na3 -108.64(7) 2_766 . . . ?
Na2 B4 O10 B6 111.6(3) 2_766 . . . ?
Na2 B5 O7 Y1 18.6(6) . . . 2_577 ?
Na2 B5 O7 B3 -159.6(4) . . . . ?
Na2 B5 O8 B4 145.30(18) . . . . ?
Na2 B5 O9 Na3 120.32(13) . . . 1_545 ?
Na2 B5 O9 B7 -132.5(3) . . . 2_666 ?
Na2 B6 O10 Na3 122.72(17) 2_766 . . . ?
Na2 B6 O10 B4 -111.1(3) 2_766 . . . ?
Na2 B6 O11 Na2 -82.00(13) 2_766 . . 1_565 ?
Na2 B6 O11 B8 120.48(19) 2_766 . . . ?
Na2 B6 O12 Na2 156.75(18) 2_766 . . 2_666 ?
Na2 B6 O12 B7 -82.9(3) 2_766 . . . ?
Na2 B7 O12 Na2 -89.41(6) . . . 2_666 ?
Na2 B7 O12 B6 134.8(2) . . . . ?
Na2 B7 O12 B6 -135.8(2) 2_666 . . . ?
Na2 B7 O14 Na1 -150.10(10) 2_666 . . 2_766 ?
Na2 B7 O14 Na1 49.1(5) . . . 2_766 ?
Na2 B7 O14 Na3 147.6(4) . . . 2_676 ?
Na2 B7 O14 Na3 -51.58(15) 2_666 . . 2_676 ?
Na2 B7 O14 B8 -73.7(5) . . . . ?
Na2 B7 O14 B8 87.1(2) 2_666 . . . ?
Na2 B7 O15 Na2 -21.11(19) 2_666 . . . ?
Na2 B7 O15 Y1 105.43(17) 2_666 . . 1_644 ?
Na2 B7 O15 Y1 126.54(16) . . . 1_644 ?
Na2 B7 O15 B4 -102.45(19) . . . 2_766 ?
Na2 B7 O15 B4 -123.56(19) 2_666 . . 2_766 ?
Na2 B8 O11 Na2 -107.30(16) 1_565 . . 2_766 ?
Na2 B8 O11 B6 159.9(3) 1_565 . . . ?
Na2 B8 O13 Na1 -170.25(7) 1_565 . . 2_766 ?
Na2 B8 O13 Na3 85.02(13) 1_565 . . 2_776 ?
Na2 B8 O13 Y1 -61.0(2) 1_565 . . 1_654 ?
Na2 B8 O14 Na1 149.7(2) 1_565 . . 2_766 ?
Na2 B8 O14 Na3 57.6(3) 1_565 . . 2_676 ?
Na2 B8 O14 B7 -69.8(3) 1_565 . . . ?
Na3 B3 O2 Na1 -95.0(2) . . . . ?
Na3 B3 O2 B1 61.8(3) . . . . ?
Na3 B3 O5 Na1 34.9(3) . . . 1_465 ?
Na3 B3 O5 Y1 125.91(6) . . . 2_577 ?
Na3 B3 O5 B2 -114.9(2) . . . . ?
Na3 B3 O6 Y1 103.80(14) . . . 2_677 ?
Na3 B3 O6 B4 -133.6(2) . . . . ?
Na3 B3 O7 Y1 -88.35(12) . . . 2_577 ?
Na3 B3 O7 B5 90.3(2) . . . . ?
Na3 B5 O7 Y1 -75.20(19) 1_545 . . 2_577 ?
Na3 B5 O7 B3 106.56(19) 1_545 . . . ?
Na3 B5 O8 B4 -140.27(17) 1_545 . . . ?
Na3 B5 O9 Na2 -120.32(13) 1_545 . . . ?
Na3 B5 O9 B7 107.2(2) 1_545 . . 2_666 ?
Na3 B7 O12 Na2 53.41(15) 2_676 . . 2_666 ?
Na3 B7 O12 B6 -82.4(2) 2_676 . . . ?
Na3 B7 O14 Na1 -98.52(16) 2_676 . . 2_766 ?
Na3 B7 O14 B8 138.7(2) 2_676 . . . ?
Na3 B7 O15 Na2 -133.13(13) 2_676 . . . ?
Na3 B7 O15 Y1 -6.6(2) 2_676 . . 1_644 ?
Na3 B7 O15 B4 124.42(19) 2_676 . . 2_766 ?
Y1 B3 O2 Na1 122.14(14) 2_577 . . . ?
Y1 B3 O2 B1 -81.0(2) 2_577 . . . ?
Y1 B3 O5 Na1 -91.0(3) 2_577 . . 1_465 ?
Y1 B3 O5 Na3 -125.91(6) 2_577 . . . ?
Y1 B3 O5 B2 119.2(2) 2_577 . . . ?
Y1 B3 O6 Na3 61.0(2) 2_577 . . . ?
Y1 B3 O6 Y1 164.82(12) 2_577 . . 2_677 ?
Y1 B3 O6 B4 -72.6(3) 2_577 . . . ?
Y1 B3 O7 B5 178.7(2) 2_577 . . . ?
Y1 B4 O6 Na3 94.78(10) 2_677 . . . ?
Y1 B4 O6 B3 -134.3(2) 2_677 . . . ?
Y1 B4 O8 B5 93.5(3) 2_677 . . . ?
Y1 B4 O10 Na2 61.03(13) 2_677 . . 2_766 ?
Y1 B4 O10 Na3 -47.60(11) 2_677 . . . ?
Y1 B4 O10 B6 172.7(2) 2_677 . . . ?
O1 B1 O2 Na1 -0.9(3) . . . . ?
O1 B1 O2 B3 -163.3(2) . . . . ?
O1 B1 O3 Na3 2.6(3) . . . 2_677 ?
O1 B1 O3 B2 172.6(2) . . . . ?
O2 B1 O1 Na1 0.7(2) . . . . ?
O2 B1 O1 Na1 110.4(2) . . . 2_767 ?
O2 B1 O1 Y1 -82.4(4) . . . 1_645 ?
O2 B1 O3 Na3 -176.37(15) . . . 2_677 ?
O2 B1 O3 B2 -6.3(3) . . . . ?
O2 B3 O5 Na1 164.0(2) . . . 1_465 ?
O2 B3 O5 Na3 129.08(18) . . . . ?
O2 B3 O5 Y1 -105.02(17) . . . 2_577 ?
O2 B3 O5 B2 14.2(3) . . . . ?
O2 B3 O6 Na3 -131.53(15) . . . . ?
O2 B3 O6 Y1 -27.7(2) . . . 2_677 ?
O2 B3 O6 B4 94.9(2) . . . . ?
O2 B3 O7 Y1 102.36(18) . . . 2_577 ?
O2 B3 O7 B5 -79.0(3) . . . . ?
O3 B1 O1 Na1 -68.5(2) . . . 2_767 ?
O3 B1 O1 Na1 -178.1(2) . . . . ?
O3 B1 O1 Y1 98.7(4) . . . 1_645 ?
O3 B1 O2 Na1 178.01(18) . . . . ?
O3 B1 O2 B3 15.6(3) . . . . ?
O3 B2 O4 Na1 171.08(19) . . . 1_465 ?
O3 B2 O4 Y1 -17.6(5) . . . . ?
O3 B2 O5 Na1 -173.1(2) . . . 1_465 ?
O3 B2 O5 Na3 -105.2(2) . . . . ?
O3 B2 O5 Y1 103.8(2) . . . 2_577 ?
O3 B2 O5 B3 -6.9(3) . . . . ?
O4 B2 O3 Na3 -8.4(3) . . . 2_677 ?
O4 B2 O3 B1 -179.0(2) . . . . ?
O4 B2 O5 Na1 8.2(2) . . . 1_465 ?
O4 B2 O5 Na3 76.0(3) . . . . ?
O4 B2 O5 Y1 -74.9(2) . . . 2_577 ?
O4 B2 O5 B3 174.3(2) . . . . ?
O5 B2 O3 Na3 172.88(16) . . . 2_677 ?
O5 B2 O3 B1 2.3(3) . . . . ?
O5 B2 O4 Na1 -10.2(3) . . . 1_465 ?
O5 B2 O4 Y1 161.1(2) . . . . ?
O5 B3 O2 Na1 -175.56(13) . . . . ?
O5 B3 O2 B1 -18.7(3) . . . . ?
O5 B3 O6 Na3 -5.9(2) . . . . ?
O5 B3 O6 Y1 97.9(2) . . . 2_677 ?
O5 B3 O6 B4 -139.5(2) . . . . ?
O5 B3 O7 Y1 -16.55(18) . . . 2_577 ?
O5 B3 O7 B5 162.11(19) . . . . ?
O6 B3 O2 Na1 -48.4(3) . . . . ?
O6 B3 O2 B1 108.5(2) . . . . ?
O6 B3 O5 Na1 39.4(4) . . . 1_465 ?
O6 B3 O5 Na3 4.48(17) . . . . ?
O6 B3 O5 Y1 130.39(17) . . . 2_577 ?
O6 B3 O5 B2 -110.4(2) . . . . ?
O6 B3 O7 Y1 -136.96(15) . . . 2_577 ?
O6 B3 O7 B5 41.7(3) . . . . ?
O6 B4 O8 B5 32.8(3) . . . . ?
O6 B4 O10 Na2 117.52(15) . . . 2_766 ?
O6 B4 O10 Na3 8.89(15) . . . . ?
O6 B4 O10 B6 -130.8(2) . . . . ?
O7 B3 O2 Na1 71.6(3) . . . . ?
O7 B3 O2 B1 -131.5(2) . . . . ?
O7 B3 O5 Na1 -76.8(3) . . . 1_465 ?
O7 B3 O5 Na3 -111.69(15) . . . . ?
O7 B3 O5 Y1 14.21(16) . . . 2_577 ?
O7 B3 O5 B2 133.4(2) . . . . ?
O7 B3 O6 Na3 106.29(16) . . . . ?
O7 B3 O6 Y1 -149.92(13) . . . 2_677 ?
O7 B3 O6 B4 -27.3(3) . . . . ?
O7 B5 O8 B4 -21.4(3) . . . . ?
O7 B5 O9 Na2 160.21(18) . . . . ?
O7 B5 O9 Na3 -79.5(2) . . . 1_545 ?
O7 B5 O9 B7 27.8(4) . . . 2_666 ?
O8 B4 O6 Na3 -136.67(16) . . . . ?
O8 B4 O6 Y1 128.55(17) . . . 2_677 ?
O8 B4 O6 B3 -5.7(3) . . . . ?
O8 B4 O10 Na2 -117.09(17) . . . 2_766 ?
O8 B4 O10 Na3 134.28(17) . . . . ?
O8 B4 O10 B6 -5.5(4) . . . . ?
O8 B5 O7 Y1 159.57(16) . . . 2_577 ?
O8 B5 O7 B3 -18.7(3) . . . . ?
O8 B5 O9 Na2 -22.6(3) . . . . ?
O8 B5 O9 Na3 97.7(2) . . . 1_545 ?
O8 B5 O9 B7 -155.1(2) . . . 2_666 ?
O9 B5 O7 Y1 -23.2(3) . . . 2_577 ?
O9 B5 O7 B3 158.6(2) . . . . ?
O9 B5 O8 B4 161.4(2) . . . . ?
O9 B7 O12 Na2 -4.66(16) 2_666 . . 2_666 ?
O9 B7 O12 B6 -140.4(2) 2_666 . . . ?
O9 B7 O14 Na1 -99.2(2) 2_666 . . 2_766 ?
O9 B7 O14 Na3 -0.68(18) 2_666 . . 2_676 ?
O9 B7 O14 B8 138.0(2) 2_666 . . . ?
O9 B7 O15 Na2 -72.15(18) 2_666 . . . ?
O9 B7 O15 Y1 54.4(2) 2_666 . . 1_644 ?
O9 B7 O15 B4 -174.59(18) 2_666 . . 2_766 ?
O10 B4 O6 Na3 -12.5(2) . . . . ?
O10 B4 O6 Y1 -107.32(16) . . . 2_677 ?
O10 B4 O6 B3 118.4(2) . . . . ?
O10 B4 O8 B5 -88.9(2) . . . . ?
O10 B6 O11 Na2 37.83(18) . . . 2_766 ?
O10 B6 O11 Na2 -44.2(3) . . . 1_565 ?
O10 B6 O11 B8 158.3(2) . . . . ?
O10 B6 O12 Na2 82.5(3) . . . 2_666 ?
O10 B6 O12 B7 -157.1(2) . . . . ?
O11 B6 O10 Na2 -47.9(2) . . . 2_766 ?
O11 B6 O10 Na3 74.8(2) . . . . ?
O11 B6 O10 B4 -159.0(2) . . . . ?
O11 B6 O12 Na2 -96.1(2) . . . 2_666 ?
O11 B6 O12 B7 24.3(3) . . . . ?
O11 B8 O13 Na1 163.7(2) . . . 2_766 ?
O11 B8 O13 Na3 58.9(3) . . . 2_776 ?
O11 B8 O13 Y1 -87.1(3) . . . 1_654 ?
O11 B8 O14 Na1 -163.18(19) . . . 2_766 ?
O11 B8 O14 Na3 104.8(2) . . . 2_676 ?
O11 B8 O14 B7 -22.6(3) . . . . ?
O12 B6 O10 Na2 133.4(2) . . . 2_766 ?
O12 B6 O10 Na3 -103.9(2) . . . . ?
O12 B6 O10 B4 22.3(4) . . . . ?
O12 B6 O11 Na2 134.61(19) . . . 1_565 ?
O12 B6 O11 Na2 -143.4(2) . . . 2_766 ?
O12 B6 O11 B8 -22.9(3) . . . . ?
O12 B7 O14 Na1 145.28(15) . . . 2_766 ?
O12 B7 O14 Na3 -116.20(17) . . . 2_676 ?
O12 B7 O14 B8 22.5(3) . . . . ?
O12 B7 O15 Na2 43.11(19) . . . . ?
O12 B7 O15 Y1 169.65(12) . . . 1_644 ?
O12 B7 O15 B4 -59.3(3) . . . 2_766 ?
O13 B8 O11 Na2 40.3(3) . . . 1_565 ?
O13 B8 O11 Na2 -67.0(3) . . . 2_766 ?
O13 B8 O11 B6 -159.9(2) . . . . ?
O13 B8 O14 Na1 18.2(2) . . . 2_766 ?
O13 B8 O14 Na3 -73.9(3) . . . 2_676 ?
O13 B8 O14 B7 158.7(2) . . . . ?
O14 B7 O12 Na2 112.90(17) . . . 2_666 ?
O14 B7 O12 B6 -22.9(3) . . . . ?
O14 B7 O15 Na2 167.57(15) . . . . ?
O14 B7 O15 Y1 -65.9(2) . . . 1_644 ?
O14 B7 O15 B4 65.1(3) . . . 2_766 ?
O14 B8 O11 Na2 114.3(2) . . . 2_766 ?
O14 B8 O11 Na2 -138.41(18) . . . 1_565 ?
O14 B8 O11 B6 21.5(3) . . . . ?
O14 B8 O13 Na1 -17.8(2) . . . 2_766 ?
O14 B8 O13 Na3 -122.5(2) . . . 2_776 ?
O14 B8 O13 Y1 91.5(3) . . . 1_654 ?
O15 B4 O6 Na3 102.57(16) 2_766 . . . ?
O15 B4 O6 Y1 7.79(16) 2_766 . . 2_677 ?
O15 B4 O6 B3 -126.5(2) 2_766 . . . ?
O15 B4 O8 B5 150.2(2) 2_766 . . . ?
O15 B4 O10 Na2 5.02(18) 2_766 . . 2_766 ?
O15 B4 O10 Na3 -103.62(15) 2_766 . . . ?
O15 B4 O10 B6 116.7(3) 2_766 . . . ?
O15 B7 O12 Na2 -122.98(16) . . . 2_666 ?
O15 B7 O12 B6 101.3(2) . . . . ?
O15 B7 O14 Na1 22.0(3) . . . 2_766 ?
O15 B7 O14 Na3 120.49(16) . . . 2_676 ?
O15 B7 O14 B8 -100.8(2) . . . . ?

_olex2_submission_special_instructions 'No special instructions were received'
