# Electronic Supplementary Material (ESI) for Dalton Transactions.
# This journal is © The Royal Society of Chemistry 2023

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_1_a
_database_code_depnum_ccdc_archive 'CCDC 2207960'
loop_
_audit_author_name
_audit_author_address
'Bin Liu'
;Northwest University
China
;
_audit_update_record             
;
2022-09-18 deposited with the CCDC.	2022-12-26 downloaded from the CCDC.
;
# start Validation Reply Form
_vrf_PLAT420_1_a                 
;
PROBLEM:  D-H Bond Without Acceptor O9 --H9B . Please Check
RESPONSE: Crystals diffracted weakly at high angle. Multiple attempts were made
 to produce and collect better diffracting crystals without success.
;
_vrf_PLAT971_1_a                 
;
PROBLEM: Check Calcd Resid. Dens. 1.66Ang From O11 2.52 eA-3 
RESPONSE: Crystals diffracted weakly at high angle. Multiple attempts were made
 to produce and collect better diffracting crystals without success.
;
_vrf_PLAT975_1_a                 
;
PROBLEM:  Check Calcd Resid. Dens. 1.03Ang From O10 . 1.62 eA-3
RESPONSE: Crystals diffracted weakly at high angle. Multiple attempts were made
 to produce and collect better diffracting crystals without success.
;
# end Validation Reply Form
_audit_creation_method           SHELXL-2018/3
_shelx_SHELXL_version_number     2018/3
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         'C4 H18 Na4 O21 Ru2, H2 O'
_chemical_formula_sum            'C4 H20 Na4 O22 Ru2'
_chemical_formula_weight         714.30

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0137 0.0067 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Na Na 0.1104 0.0938 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0389 0.0241 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ru Ru -0.0760 2.5955 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      monoclinic
_space_group_IT_number           15
_space_group_name_H-M_alt        'C 2/c'
_space_group_name_Hall           '-C 2yc'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'

_cell_length_a                   23.0029(12)
_cell_length_b                   9.0127(4)
_cell_length_c                   9.9585(5)
_cell_angle_alpha                90
_cell_angle_beta                 107.461(2)
_cell_angle_gamma                90
_cell_volume                     1969.45(17)
_cell_formula_units_Z            4
_cell_measurement_temperature    150(2)
_cell_measurement_reflns_used    8380
_cell_measurement_theta_min      3.50
_cell_measurement_theta_max      53.16

_exptl_crystal_description       plate
_exptl_crystal_colour            brown
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    2.409
_exptl_crystal_F_000             1408
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          0.220
_exptl_crystal_size_mid          0.150
_exptl_crystal_size_min          0.120
_exptl_absorpt_coefficient_mu    9.660
_shelx_estimated_absorpt_T_min   0.225
_shelx_estimated_absorpt_T_max   0.390
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_correction_T_min  0.242
_exptl_absorpt_correction_T_max  0.359
_exptl_absorpt_process_details   sadabs
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      150(2)
_diffrn_radiation_wavelength     1.34139
_diffrn_radiation_type           GaK\a
_diffrn_source                   ?
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            10766
_diffrn_reflns_av_unetI/netI     0.0375
_diffrn_reflns_av_R_equivalents  0.0549
_diffrn_reflns_limit_h_min       -27
_diffrn_reflns_limit_h_max       27
_diffrn_reflns_limit_k_min       -9
_diffrn_reflns_limit_k_max       10
_diffrn_reflns_limit_l_min       -11
_diffrn_reflns_limit_l_max       9
_diffrn_reflns_theta_min         4.614
_diffrn_reflns_theta_max         53.204
_diffrn_reflns_theta_full        53.205
_diffrn_measured_fraction_theta_max 0.990
_diffrn_measured_fraction_theta_full 0.990
_diffrn_reflns_Laue_measured_fraction_max 0.990
_diffrn_reflns_Laue_measured_fraction_full 0.990
_diffrn_reflns_point_group_measured_fraction_max 0.990
_diffrn_reflns_point_group_measured_fraction_full 0.990
_reflns_number_total             1739
_reflns_number_gt                1641
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       'Bruker APEX2'
_computing_cell_refinement       'Bruker SAINT'
_computing_data_reduction        'Bruker SAINT'
_computing_structure_solution    'SHELXT 2014/5 (Sheldrick, 2014)'
_computing_structure_refinement  'SHELXL-2018/3 (Sheldrick, 2018)'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0876P)²+50.6458P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   difmap
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_number_reflns         1739
_refine_ls_number_parameters     146
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0555
_refine_ls_R_factor_gt           0.0530
_refine_ls_wR_factor_ref         0.1442
_refine_ls_wR_factor_gt          0.1422
_refine_ls_goodness_of_fit_ref   1.042
_refine_ls_restrained_S_all      1.042
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ru1 Ru 0.23482(2) 0.80049(5) 0.39131(5) 0.0102(2) Uani 1 1 d . . . . .
Na1 Na 0.30466(13) 0.1287(3) 0.4249(3) 0.0169(6) Uani 1 1 d . . . . .
Na2 Na 0.4426(2) 0.2655(6) 0.8106(5) 0.0557(11) Uani 1 1 d . . . . .
C1 C 0.3674(3) 0.8247(8) 0.5240(8) 0.0173(15) Uani 1 1 d . . . . .
C2 C 0.2763(3) 0.4908(8) 0.3902(7) 0.0117(13) Uani 1 1 d . . . . .
O1 O 0.3544(2) 0.7619(6) 0.6297(5) 0.0167(10) Uani 1 1 d . . . . .
O2 O 0.3243(2) 0.8630(5) 0.4131(5) 0.0144(10) Uani 1 1 d . . . . .
O3 O 0.4225(3) 0.8502(7) 0.5301(7) 0.0335(14) Uani 1 1 d . . . . .
O4 O 0.2537(2) 0.6010(6) 0.3095(5) 0.0142(10) Uani 1 1 d . . . . .
O5 O 0.2817(2) 0.4976(5) 0.5244(5) 0.0139(10) Uani 1 1 d . . . . .
O6 O 0.2937(2) 0.3748(5) 0.3428(5) 0.0142(10) Uani 1 1 d . . . . .
O7 O 0.4047(2) 0.1327(6) 0.4042(6) 0.0247(12) Uani 1 1 d . . . . .
H7B H 0.417856 0.221435 0.412337 0.037 Uiso 1 1 d R U . . .
H7C H 0.427926 0.079595 0.468897 0.037 Uiso 1 1 d R U . . .
O8 O 0.3410(2) 0.2306(7) 0.6532(6) 0.0235(12) Uani 1 1 d . . . . .
H8A H 0.322905 0.180899 0.701320 0.028 Uiso 1 1 d R U . . .
H8B H 0.325225 0.316759 0.645140 0.028 Uiso 1 1 d R U . . .
O9 O 0.4491(6) 0.3414(10) 0.5874(9) 0.081(3) Uani 1 1 d . . . . .
H9A H 0.432055 0.425505 0.566402 0.121 Uiso 1 1 d R U . . .
H9B H 0.486475 0.348205 0.591572 0.121 Uiso 1 1 d R U . . .
O10 O 0.500000 0.0489(17) 0.750000 0.068(4) Uani 1 2 d S T P . .
H10A H 0.536970 0.051947 0.800940 0.102 Uiso 0.5 1 d R U P . .
H10B H 0.483880 -0.031783 0.765050 0.102 Uiso 0.5 1 d R U P . .
O11 O 0.4142(4) 0.5065(10) 0.8488(10) 0.064(2) Uani 1 1 d . . . . .
H11A H 0.382462 0.503499 0.875687 0.097 Uiso 1 1 d R U . . .
H11C H 0.406662 0.555589 0.772617 0.097 Uiso 1 1 d R U . . .
O12 O 0.500000 0.6648(14) 0.750000 0.056(3) Uani 1 2 d S T P . .
H12A H 0.494640 0.757422 0.757440 0.085 Uiso 0.5 1 d R U P . .
H12C H 0.495290 0.643322 0.664280 0.085 Uiso 0.5 1 d R U P . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ru1 O4 2.074(5) . ?
Ru1 O1 2.076(5) 7_566 ?
Ru1 O2 2.081(5) . ?
Ru1 O5 2.087(5) 7_566 ?
Ru1 Ru1 2.2572(9) 7_566 ?
Ru1 O6 2.323(4) 4 ?
Ru1 Na1 3.335(3) 1_565 ?
Ru1 Na1 3.380(3) 4 ?
Na1 O4 2.331(5) 4_545 ?
Na1 O6 2.351(5) . ?
Na1 O8 2.360(6) . ?
Na1 O7 2.372(6) . ?
Na1 O2 2.447(6) 1_545 ?
Na1 O5 2.470(6) 7_556 ?
Na1 C1 3.116(8) 1_545 ?
Na1 Na1 3.949(6) 7_556 ?
Na2 O11 2.333(11) . ?
Na2 O9 2.373(10) . ?
Na2 O8 2.413(7) . ?
Na2 O9 2.487(13) 2_656 ?
Na2 O10 2.528(13) . ?
Na2 O3 2.586(8) 6_566 ?
Na2 Na2 3.215(9) 2_656 ?
Na2 H9B 1.792(12) 2_656 ?
Na2 H10A 2.339(14) 2_656 ?
C1 O3 1.272(10) . ?
C1 O2 1.290(9) . ?
C1 O1 1.305(9) . ?
C2 O6 1.261(8) . ?
C2 O4 1.285(8) . ?
C2 O5 1.305(8) . ?
O7 H7B 0.8501 . ?
O7 H7C 0.8500 . ?
O8 H8A 0.8499 . ?
O8 H8B 0.8500 . ?
O9 H9A 0.8501 . ?
O9 H9B 0.8501 . ?
O10 H10A 0.8499 . ?
O10 H10B 0.8500 . ?
O10 H10A 0.8500 2_656 ?
O10 H10B 0.8501 2_656 ?
O11 H11A 0.8501 . ?
O11 H11C 0.8500 . ?
O12 H12A 0.8500 . ?
O12 H12C 0.8500 . ?
O12 H12A 0.8500 2_656 ?
O12 H12C 0.8501 2_656 ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O4 Ru1 O1 92.5(2) . 7_566 ?
O4 Ru1 O2 87.60(19) . . ?
O1 Ru1 O2 179.79(18) 7_566 . ?
O4 Ru1 O5 178.44(19) . 7_566 ?
O1 Ru1 O5 89.0(2) 7_566 7_566 ?
O2 Ru1 O5 90.89(19) . 7_566 ?
O4 Ru1 Ru1 89.22(12) . 7_566 ?
O1 Ru1 Ru1 89.96(13) 7_566 7_566 ?
O2 Ru1 Ru1 89.84(13) . 7_566 ?
O5 Ru1 Ru1 90.40(13) 7_566 7_566 ?
O4 Ru1 O6 83.40(17) . 4 ?
O1 Ru1 O6 90.23(18) 7_566 4 ?
O2 Ru1 O6 89.98(17) . 4 ?
O5 Ru1 O6 96.98(17) 7_566 4 ?
Ru1 Ru1 O6 172.62(12) 7_566 4 ?
O4 Ru1 Na1 131.07(14) . 1_565 ?
O1 Ru1 Na1 133.01(15) 7_566 1_565 ?
O2 Ru1 Na1 46.99(14) . 1_565 ?
O5 Ru1 Na1 47.64(14) 7_566 1_565 ?
Ru1 Ru1 Na1 105.09(5) 7_566 1_565 ?
O6 Ru1 Na1 80.07(13) 4 1_565 ?
O4 Ru1 Na1 42.78(13) . 4 ?
O1 Ru1 Na1 78.52(15) 7_566 4 ?
O2 Ru1 Na1 101.67(14) . 4 ?
O5 Ru1 Na1 138.08(13) 7_566 4 ?
Ru1 Ru1 Na1 128.93(6) 7_566 4 ?
O6 Ru1 Na1 44.02(13) 4 4 ?
Na1 Ru1 Na1 119.11(5) 1_565 4 ?
O4 Na1 O6 77.50(18) 4_545 . ?
O4 Na1 O8 159.6(2) 4_545 . ?
O6 Na1 O8 86.5(2) . . ?
O4 Na1 O7 101.4(2) 4_545 . ?
O6 Na1 O7 87.8(2) . . ?
O8 Na1 O7 90.3(2) . . ?
O4 Na1 O2 84.61(19) 4_545 1_545 ?
O6 Na1 O2 155.34(19) . 1_545 ?
O8 Na1 O2 114.2(2) . 1_545 ?
O7 Na1 O2 79.20(19) . 1_545 ?
O4 Na1 O5 84.15(18) 4_545 7_556 ?
O6 Na1 O5 119.8(2) . 7_556 ?
O8 Na1 O5 93.23(19) . 7_556 ?
O7 Na1 O5 152.3(2) . 7_556 ?
O2 Na1 O5 74.33(17) 1_545 7_556 ?
O4 Na1 C1 107.2(2) 4_545 1_545 ?
O6 Na1 C1 158.6(2) . 1_545 ?
O8 Na1 C1 92.3(2) . 1_545 ?
O7 Na1 C1 70.8(2) . 1_545 ?
O2 Na1 C1 23.03(18) 1_545 1_545 ?
O5 Na1 C1 81.61(19) 7_556 1_545 ?
O4 Na1 Ru1 71.86(14) 4_545 1_545 ?
O6 Na1 Ru1 143.50(16) . 1_545 ?
O8 Na1 Ru1 117.55(17) . 1_545 ?
O7 Na1 Ru1 117.09(17) . 1_545 ?
O2 Na1 Ru1 38.47(12) 1_545 1_545 ?
O5 Na1 Ru1 38.63(11) 7_556 1_545 ?
C1 Na1 Ru1 54.19(15) 1_545 1_545 ?
O4 Na1 Ru1 37.17(13) 4_545 4_545 ?
O6 Na1 Ru1 43.36(12) . 4_545 ?
O8 Na1 Ru1 129.64(17) . 4_545 ?
O7 Na1 Ru1 84.75(15) . 4_545 ?
O2 Na1 Ru1 113.92(14) 1_545 4_545 ?
O5 Na1 Ru1 113.20(14) 7_556 4_545 ?
C1 Na1 Ru1 131.86(17) 1_545 4_545 ?
Ru1 Na1 Ru1 109.03(7) 1_545 4_545 ?
O4 Na1 Na1 101.39(17) 4_545 7_556 ?
O6 Na1 Na1 66.16(14) . 7_556 ?
O8 Na1 Na1 60.09(15) . 7_556 ?
O7 Na1 Na1 140.30(19) . 7_556 ?
O2 Na1 Na1 135.05(17) 1_545 7_556 ?
O5 Na1 Na1 62.29(13) 7_556 7_556 ?
C1 Na1 Na1 130.82(18) 1_545 7_556 ?
Ru1 Na1 Na1 100.76(10) 1_545 7_556 ?
Ru1 Na1 Na1 94.34(9) 4_545 7_556 ?
O11 Na2 O9 89.1(3) . . ?
O11 Na2 O8 87.9(3) . . ?
O9 Na2 O8 75.5(4) . . ?
O11 Na2 O9 88.4(4) . 2_656 ?
O9 Na2 O9 88.1(4) . 2_656 ?
O8 Na2 O9 163.2(3) . 2_656 ?
O11 Na2 O10 161.8(4) . . ?
O9 Na2 O10 79.3(3) . . ?
O8 Na2 O10 102.6(3) . . ?
O9 Na2 O10 77.3(3) 2_656 . ?
O11 Na2 O3 96.2(3) . 6_566 ?
O9 Na2 O3 170.3(4) . 6_566 ?
O8 Na2 O3 96.4(2) . 6_566 ?
O9 Na2 O3 100.2(3) 2_656 6_566 ?
O10 Na2 O3 97.4(3) . 6_566 ?
O11 Na2 Na2 111.3(2) . 2_656 ?
O9 Na2 Na2 50.1(3) . 2_656 ?
O8 Na2 Na2 120.1(3) . 2_656 ?
O9 Na2 Na2 47.1(2) 2_656 2_656 ?
O10 Na2 Na2 50.5(3) . 2_656 ?
O3 Na2 Na2 133.9(2) 6_566 2_656 ?
O11 Na2 H9B 77.1(5) . 2_656 ?
O9 Na2 H9B 95.0(5) . 2_656 ?
O8 Na2 H9B 162.5(5) . 2_656 ?
O9 Na2 H9B 13.33(14) 2_656 2_656 ?
O10 Na2 H9B 89.8(4) . 2_656 ?
O3 Na2 H9B 94.2(3) 6_566 2_656 ?
Na2 Na2 H9B 59.2(3) 2_656 2_656 ?
O11 Na2 H10A 161.8(4) . 2_656 ?
O9 Na2 H10A 73.4(3) . 2_656 ?
O8 Na2 H10A 83.0(2) . 2_656 ?
O9 Na2 H10A 95.8(3) 2_656 2_656 ?
O10 Na2 H10A 19.62(11) . 2_656 ?
O3 Na2 H10A 100.5(3) 6_566 2_656 ?
Na2 Na2 H10A 61.1(2) 2_656 2_656 ?
H9B Na2 H10A 108.7 2_656 2_656 ?
O3 C1 O2 119.4(7) . . ?
O3 C1 O1 120.4(7) . . ?
O2 C1 O1 120.2(6) . . ?
O3 C1 Na1 102.5(5) . 1_565 ?
O2 C1 Na1 47.9(3) . 1_565 ?
O1 C1 Na1 116.1(5) . 1_565 ?
O6 C2 O4 121.3(6) . . ?
O6 C2 O5 118.6(6) . . ?
O4 C2 O5 120.0(6) . . ?
C1 O1 Ru1 119.6(4) . 7_566 ?
C1 O2 Ru1 119.9(4) . . ?
C1 O2 Na1 109.1(4) . 1_565 ?
Ru1 O2 Na1 94.54(19) . 1_565 ?
C1 O3 Na2 108.4(5) . 6_565 ?
C2 O4 Ru1 121.1(4) . . ?
C2 O4 Na1 135.4(4) . 4 ?
Ru1 O4 Na1 100.1(2) . 4 ?
C2 O5 Ru1 118.7(4) . 7_566 ?
C2 O5 Na1 110.6(4) . 7_556 ?
Ru1 O5 Na1 93.73(19) 7_566 7_556 ?
C2 O6 Ru1 126.1(4) . 4_545 ?
C2 O6 Na1 131.6(4) . . ?
Ru1 O6 Na1 92.62(18) 4_545 . ?
Na1 O7 H7B 109.4 . . ?
Na1 O7 H7C 109.3 . . ?
H7B O7 H7C 109.5 . . ?
Na1 O8 Na2 132.1(3) . . ?
Na1 O8 H8A 104.2 . . ?
Na2 O8 H8A 104.2 . . ?
Na1 O8 H8B 104.3 . . ?
Na2 O8 H8B 104.2 . . ?
H8A O8 H8B 105.6 . . ?
Na2 O9 Na2 82.8(4) . 2_656 ?
Na2 O9 H9A 109.5 . . ?
Na2 O9 H9A 132.7 2_656 . ?
Na2 O9 H9B 108.8 . . ?
Na2 O9 H9B 29.1 2_656 . ?
H9A O9 H9B 109.5 . . ?
Na2 O10 Na2 79.0(5) 2_656 . ?
Na2 O10 H10A 67.5 2_656 . ?
Na2 O10 H10A 109.5 . . ?
Na2 O10 H10B 171.6 2_656 . ?
Na2 O10 H10B 109.4 . . ?
H10A O10 H10B 109.5 . . ?
Na2 O10 H10A 109.48(15) 2_656 2_656 ?
Na2 O10 H10A 67.49(15) . 2_656 ?
H10A O10 H10A 176.3 . 2_656 ?
H10B O10 H10A 73.8 . 2_656 ?
Na2 O10 H10B 109.4(3) 2_656 2_656 ?
Na2 O10 H10B 171.6(2) . 2_656 ?
H10A O10 H10B 73.8 . 2_656 ?
H10B O10 H10B 62.3 . 2_656 ?
H10A O10 H10B 109.5 2_656 2_656 ?
Na2 O11 H11A 109.3 . . ?
Na2 O11 H11C 109.3 . . ?
H11A O11 H11C 109.5 . . ?
H12A O12 H12C 109.5 . . ?
H12A O12 H12A 21.9 . 2_656 ?
H12C O12 H12A 96.6 . 2_656 ?
H12A O12 H12C 96.6 . 2_656 ?
H12C O12 H12C 153.6 . 2_656 ?
H12A O12 H12C 109.5 2_656 2_656 ?

_refine_diff_density_max         2.486
_refine_diff_density_min         -1.404
_refine_diff_density_rms         0.240



