# Electronic Supplementary Material (ESI) for Inorganic Chemistry Frontiers.
# This journal is © the Partner Organisations 2022

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_3
_database_code_depnum_ccdc_archive 'CCDC 2128946'
loop_
_audit_author_name
_audit_author_address
'Jia Lin'
;Shanghai University of Electric Power
China
;
_audit_update_record             
;
2022-02-24 deposited with the CCDC.	2022-06-13 downloaded from the CCDC.
;
_audit_creation_date             2020-10-20
_audit_creation_method           
;
Olex2 1.2
(compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506)
;
_shelx_SHELXL_version_number     2017/1
_chemical_name_common            ?
_chemical_name_systematic        Rb8CuIn3Cl18
_chemical_formula_moiety         '0.33(Cl216 Cu12 In36 Rb96)'
_chemical_formula_sum            'Cl72 Cu4 In12 Rb32'
_chemical_formula_weight         6919.44
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
In In -0.7276 1.3100 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Rb Rb -0.9393 2.9676 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      trigonal
_space_group_IT_number           167
_space_group_name_H-M_alt        'R -3 c'
_space_group_name_Hall           '-R 3 2"c'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'
'y, x, -z+1/2'
'x-y, -y, -z+1/2'
'-x, -x+y, -z+1/2'
'x+2/3, y+1/3, z+1/3'
'-y+2/3, x-y+1/3, z+1/3'
'-x+y+2/3, -x+1/3, z+1/3'
'y+2/3, x+1/3, -z+5/6'
'x-y+2/3, -y+1/3, -z+5/6'
'-x+2/3, -x+y+1/3, -z+5/6'
'x+1/3, y+2/3, z+2/3'
'-y+1/3, x-y+2/3, z+2/3'
'-x+y+1/3, -x+2/3, z+2/3'
'y+1/3, x+2/3, -z+7/6'
'x-y+1/3, -y+2/3, -z+7/6'
'-x+1/3, -x+y+2/3, -z+7/6'
'-x, -y, -z'
'y, -x+y, -z'
'x-y, x, -z'
'-y, -x, z-1/2'
'-x+y, y, z-1/2'
'x, x-y, z-1/2'
'-x+2/3, -y+1/3, -z+1/3'
'y+2/3, -x+y+1/3, -z+1/3'
'x-y+2/3, x+1/3, -z+1/3'
'-y+2/3, -x+1/3, z-1/6'
'-x+y+2/3, y+1/3, z-1/6'
'x+2/3, x-y+1/3, z-1/6'
'-x+1/3, -y+2/3, -z+2/3'
'y+1/3, -x+y+2/3, -z+2/3'
'x-y+1/3, x+2/3, -z+2/3'
'-y+1/3, -x+2/3, z+1/6'
'-x+y+1/3, y+2/3, z+1/6'
'x+1/3, x-y+2/3, z+1/6'

_cell_length_a                   12.6551(19)
_cell_length_b                   12.6551(19)
_cell_length_c                   75.154(12)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_volume                     10423(4)
_cell_formula_units_Z            3
_cell_measurement_reflns_used    2468
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      27.00
_cell_measurement_theta_min      3.22
_shelx_estimated_absorpt_T_max   0.298
_shelx_estimated_absorpt_T_min   0.256
_exptl_absorpt_coefficient_mu    15.090
_exptl_absorpt_correction_T_max  0.0943
_exptl_absorpt_correction_T_min  0.0496
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
'SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1229 before and 0.0662 after correction. The Ratio of minimum to maximum transmission is 0.5260. The λ/2 correction factor is Not present.'
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            'metallic light yellow'
_exptl_crystal_colour_lustre     metallic
_exptl_crystal_colour_modifier   light
_exptl_crystal_colour_primary    yellow
_exptl_crystal_density_diffrn    3.307
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             9336
_exptl_crystal_size_max          0.124
_exptl_crystal_size_mid          0.119
_exptl_crystal_size_min          0.106
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0827
_diffrn_reflns_av_unetI/netI     0.0604
_diffrn_reflns_Laue_measured_fraction_full 0.997
_diffrn_reflns_Laue_measured_fraction_max 0.997
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -10
_diffrn_reflns_limit_k_max       11
_diffrn_reflns_limit_k_min       -11
_diffrn_reflns_limit_l_max       89
_diffrn_reflns_limit_l_min       -89
_diffrn_reflns_number            10702
_diffrn_reflns_point_group_measured_fraction_full 0.997
_diffrn_reflns_point_group_measured_fraction_max 0.997
_diffrn_reflns_theta_full        25.022
_diffrn_reflns_theta_max         25.022
_diffrn_reflns_theta_min         2.151
_diffrn_ambient_temperature      100.04
_diffrn_detector_area_resol_mean 7.9
_diffrn_detector_type            'CMOS area detector'
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device       'three-circle diffractometer'
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_diffrn_standards_number         0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                1419
_reflns_number_total             2048
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT V8.38A (?, 2016)'
_computing_data_collection       ?
_computing_data_reduction        'SAINT V8.38A (?, 2016)'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    'ShelXT (Sheldrick, 2015)'
_refine_diff_density_max         2.287
_refine_diff_density_min         -1.692
_refine_diff_density_rms         0.284
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.035
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     92
_refine_ls_number_reflns         2048
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0836
_refine_ls_R_factor_gt           0.0482
_refine_ls_restrained_S_all      1.035
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0459P)²+295.9114P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1017
_refine_ls_wR_factor_ref         0.1166
_refine_special_details          ?
_olex2_refinement_description    
;
;
_atom_sites_solution_hydrogens   .
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
In1 In 1.000000 1.000000 0.33564(2) 0.0100(3) Uani 1 3 d S T P . .
In2 In 0.666667 0.333333 0.333333 0.0091(4) Uani 1 6 d S T P . .
In3 In 0.32559(8) 0.32559(8) 0.250000 0.0100(3) Uani 1 2 d S T P . .
Rb1 Rb 1.000000 1.000000 0.38907(2) 0.0155(4) Uani 1 3 d S T P . .
Rb2 Rb 0.66108(10) 0.66490(10) 0.34962(2) 0.0176(3) Uani 1 1 d . . . . .
Rb3 Rb 0.70088(10) 0.70014(11) 0.28217(2) 0.0169(3) Uani 1 1 d . . . . .
Rb4 Rb 0.666667 0.333333 0.27883(2) 0.0165(4) Uani 1 3 d S T P . .
Cu1 Cu 0.000000 0.000000 0.22946(3) 0.0276(7) Uani 1 3 d S T P . .
Cl1 Cl 0.8285(3) 0.9806(3) 0.35516(3) 0.0207(7) Uani 1 1 d . . . . .
Cl2 Cl 0.8447(3) 0.8314(3) 0.31713(3) 0.0199(7) Uani 1 1 d . . . . .
Cl3 Cl 0.6746(3) 0.4991(2) 0.31386(3) 0.0161(6) Uani 1 1 d . . . . .
Cl4 Cl 0.4493(3) 0.4482(3) 0.27526(3) 0.0213(7) Uani 1 1 d . . . . .
Cl5 Cl 0.4323(2) 0.2026(3) 0.25014(3) 0.0177(6) Uani 1 1 d . . . . .
Cl6 Cl 0.1779(3) 0.1772(2) 0.22605(3) 0.0195(7) Uani 1 1 d . . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
In1 Rb1 4.015(2) . ?
In1 Rb2 4.3876(13) 32 ?
In1 Rb2 4.3874(13) 31_665 ?
In1 Rb2 4.3925(13) . ?
In1 Rb2 4.3924(13) 2_765 ?
In1 Rb2 4.3875(13) 33_655 ?
In1 Cl1 2.528(3) . ?
In1 Cl1 2.528(3) 2_765 ?
In1 Cl1 2.528(3) 3_675 ?
In1 Cl2 2.481(3) . ?
In1 Cl2 2.481(3) 3_675 ?
In1 Cl2 2.481(3) 2_765 ?
In2 Rb2 4.4053(13) 32 ?
In2 Rb2 4.4054(12) 31_655 ?
In2 Rb2 4.4052(12) 3_665 ?
In2 Rb2 4.4052(12) 33_545 ?
In2 Rb4 4.0956(18) 31_655 ?
In2 Rb4 4.0959(18) . ?
In2 Cl3 2.518(3) 33_545 ?
In2 Cl3 2.518(3) 32 ?
In2 Cl3 2.518(3) 2_655 ?
In2 Cl3 2.518(3) 31_655 ?
In2 Cl3 2.518(3) 3_665 ?
In2 Cl3 2.518(3) . ?
In3 Cl4 2.456(3) 4 ?
In3 Cl4 2.456(3) . ?
In3 Cl5 2.519(3) . ?
In3 Cl5 2.519(3) 4 ?
In3 Cl6 2.598(3) 4 ?
In3 Cl6 2.598(3) . ?
Rb1 Rb3 4.4679(13) 31_665 ?
Rb1 Rb4 4.241(2) 34_665 ?
Rb1 Cl1 3.276(3) . ?
Rb1 Cl1 3.276(3) 3_675 ?
Rb1 Cl1 3.276(3) 2_765 ?
Rb1 Cl4 3.726(3) 32 ?
Rb1 Cl4 3.726(3) 31_665 ?
Rb1 Cl4 3.726(3) 33_655 ?
Rb1 Cl5 3.312(3) 34_665 ?
Rb1 Cl5 3.313(3) 35_655 ?
Rb1 Cl5 3.312(3) 36 ?
Rb2 Cl1 3.566(3) 31_665 ?
Rb2 Cl1 3.487(3) . ?
Rb2 Cl1 3.949(3) 2_765 ?
Rb2 Cl2 3.302(3) . ?
Rb2 Cl2 3.756(3) 31_665 ?
Rb2 Cl2 3.447(3) 33_545 ?
Rb2 Cl3 3.789(3) 32 ?
Rb2 Cl3 3.557(3) 33_545 ?
Rb2 Cl3 3.467(3) . ?
Rb2 Cl4 3.488(3) 32 ?
Rb2 Cl6 3.761(3) 36 ?
Rb3 Rb4 4.4484(13) . ?
Rb3 Cu1 3.8895(14) 4_665 ?
Rb3 Cl1 3.256(3) 31_665 ?
Rb3 Cl2 3.155(3) . ?
Rb3 Cl3 3.378(3) . ?
Rb3 Cl4 3.228(3) . ?
Rb3 Cl5 3.320(3) 6_665 ?
Rb3 Cl5 3.294(3) 3_665 ?
Rb3 Cl6 3.356(3) 6_665 ?
Rb3 Cl6 3.361(3) 5_665 ?
Rb4 Cl3 3.336(3) 3_665 ?
Rb4 Cl3 3.336(3) 2_655 ?
Rb4 Cl3 3.336(3) . ?
Rb4 Cl4 3.708(3) . ?
Rb4 Cl4 3.708(3) 3_665 ?
Rb4 Cl4 3.708(3) 2_655 ?
Rb4 Cl5 3.358(3) 3_665 ?
Rb4 Cl5 3.358(3) 2_655 ?
Rb4 Cl5 3.358(3) . ?
Cu1 Cl6 2.261(3) 2 ?
Cu1 Cl6 2.261(3) 3 ?
Cu1 Cl6 2.261(3) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Rb1 In1 Rb2 108.575(19) . 31_665 ?
Rb1 In1 Rb2 76.162(19) . . ?
Rb1 In1 Rb2 108.575(19) . 33_655 ?
Rb1 In1 Rb2 108.575(19) . 32 ?
Rb1 In1 Rb2 76.165(19) . 2_765 ?
Rb2 In1 Rb2 67.16(2) 31_665 . ?
Rb2 In1 Rb2 110.351(18) 33_655 32 ?
Rb2 In1 Rb2 67.67(3) 33_655 2_765 ?
Rb2 In1 Rb2 175.25(3) 31_665 2_765 ?
Rb2 In1 Rb2 67.16(2) 32 2_765 ?
Rb2 In1 Rb2 114.470(15) 2_765 . ?
Rb2 In1 Rb2 110.354(19) 31_665 33_655 ?
Rb2 In1 Rb2 110.352(19) 31_665 32 ?
Rb2 In1 Rb2 175.25(3) 33_655 . ?
Rb2 In1 Rb2 67.67(3) 32 . ?
Cl1 In1 Rb1 54.52(6) 2_765 . ?
Cl1 In1 Rb1 54.52(6) 3_675 . ?
Cl1 In1 Rb1 54.52(6) . . ?
Cl1 In1 Rb2 54.37(6) 3_675 33_655 ?
Cl1 In1 Rb2 130.31(7) . 2_765 ?
Cl1 In1 Rb2 54.37(6) . 31_665 ?
Cl1 In1 Rb2 119.78(7) . 32 ?
Cl1 In1 Rb2 62.98(7) 3_675 2_765 ?
Cl1 In1 Rb2 130.31(7) 3_675 . ?
Cl1 In1 Rb2 52.49(7) . . ?
Cl1 In1 Rb2 129.83(7) 3_675 32 ?
Cl1 In1 Rb2 62.97(7) 2_765 . ?
Cl1 In1 Rb2 129.84(7) . 33_655 ?
Cl1 In1 Rb2 119.77(7) 2_765 33_655 ?
Cl1 In1 Rb2 129.83(7) 2_765 31_665 ?
Cl1 In1 Rb2 119.78(7) 3_675 31_665 ?
Cl1 In1 Rb2 54.37(6) 2_765 32 ?
Cl1 In1 Rb2 52.49(7) 2_765 2_765 ?
Cl1 In1 Cl1 89.70(9) . 3_675 ?
Cl1 In1 Cl1 89.70(9) . 2_765 ?
Cl1 In1 Cl1 89.70(9) 3_675 2_765 ?
Cl2 In1 Rb1 124.11(6) . . ?
Cl2 In1 Rb1 124.11(6) 2_765 . ?
Cl2 In1 Rb1 124.11(6) 3_675 . ?
Cl2 In1 Rb2 51.60(7) 3_675 31_665 ?
Cl2 In1 Rb2 127.16(7) 2_765 31_665 ?
Cl2 In1 Rb2 126.21(7) 2_765 . ?
Cl2 In1 Rb2 51.60(7) . 32 ?
Cl2 In1 Rb2 126.21(7) 3_675 2_765 ?
Cl2 In1 Rb2 48.14(6) 2_765 2_765 ?
Cl2 In1 Rb2 58.75(7) 3_675 33_655 ?
Cl2 In1 Rb2 127.16(7) . 33_655 ?
Cl2 In1 Rb2 51.60(7) 2_765 33_655 ?
Cl2 In1 Rb2 127.16(7) 3_675 32 ?
Cl2 In1 Rb2 118.61(7) 3_675 . ?
Cl2 In1 Rb2 48.15(6) . . ?
Cl2 In1 Rb2 58.75(7) 2_765 32 ?
Cl2 In1 Rb2 118.61(7) . 2_765 ?
Cl2 In1 Rb2 58.75(7) . 31_665 ?
Cl2 In1 Cl1 177.94(10) 3_675 2_765 ?
Cl2 In1 Cl1 90.43(10) 2_765 3_675 ?
Cl2 In1 Cl1 90.43(9) 3_675 . ?
Cl2 In1 Cl1 88.25(9) . . ?
Cl2 In1 Cl1 177.95(9) 2_765 . ?
Cl2 In1 Cl1 177.95(10) . 3_675 ?
Cl2 In1 Cl1 88.25(9) 3_675 3_675 ?
Cl2 In1 Cl1 88.25(9) 2_765 2_765 ?
Cl2 In1 Cl1 90.43(10) . 2_765 ?
Cl2 In1 Cl2 91.63(9) 3_675 2_765 ?
Cl2 In1 Cl2 91.62(9) 3_675 . ?
Cl2 In1 Cl2 91.62(9) 2_765 . ?
Rb2 In2 Rb2 112.595(11) 33_545 32 ?
Rb2 In2 Rb2 112.593(12) 33_545 31_655 ?
Rb2 In2 Rb2 112.591(11) 32 31_655 ?
Rb2 In2 Rb2 180.00(3) 33_545 3_665 ?
Rb2 In2 Rb2 67.404(11) 3_665 32 ?
Rb2 In2 Rb2 67.405(11) 3_665 31_655 ?
Rb4 In2 Rb2 73.868(13) . 31_655 ?
Rb4 In2 Rb2 73.867(13) . 32 ?
Rb4 In2 Rb2 106.133(13) 31_655 33_545 ?
Rb4 In2 Rb2 106.132(13) 31_655 31_655 ?
Rb4 In2 Rb2 73.869(13) 31_655 3_665 ?
Rb4 In2 Rb2 106.133(13) 31_655 32 ?
Rb4 In2 Rb2 106.131(13) . 3_665 ?
Rb4 In2 Rb2 73.867(13) . 33_545 ?
Rb4 In2 Rb4 180.0 . 31_655 ?
Cl3 In2 Rb2 120.88(6) 32 31_655 ?
Cl3 In2 Rb2 51.76(6) 31_655 31_655 ?
Cl3 In2 Rb2 51.76(6) 32 32 ?
Cl3 In2 Rb2 128.23(6) 2_655 32 ?
Cl3 In2 Rb2 120.88(7) . 3_665 ?
Cl3 In2 Rb2 126.17(7) 31_655 32 ?
Cl3 In2 Rb2 128.23(6) 3_665 33_545 ?
Cl3 In2 Rb2 59.12(7) 31_655 3_665 ?
Cl3 In2 Rb2 126.17(7) 33_545 31_655 ?
Cl3 In2 Rb2 120.88(7) 33_545 32 ?
Cl3 In2 Rb2 128.24(6) . 31_655 ?
Cl3 In2 Rb2 120.88(7) 31_655 33_545 ?
Cl3 In2 Rb2 59.12(6) 2_655 31_655 ?
Cl3 In2 Rb2 53.83(7) 3_665 31_655 ?
Cl3 In2 Rb2 51.76(6) 33_545 33_545 ?
Cl3 In2 Rb2 53.83(7) . 32 ?
Cl3 In2 Rb2 128.24(6) 33_545 3_665 ?
Cl3 In2 Rb2 126.17(6) 32 33_545 ?
Cl3 In2 Rb2 51.77(6) 3_665 3_665 ?
Cl3 In2 Rb2 126.17(6) 2_655 3_665 ?
Cl3 In2 Rb2 53.83(6) 2_655 33_545 ?
Cl3 In2 Rb2 59.12(7) 3_665 32 ?
Cl3 In2 Rb2 59.12(7) . 33_545 ?
Cl3 In2 Rb2 53.83(6) 32 3_665 ?
Cl3 In2 Rb4 54.46(6) . . ?
Cl3 In2 Rb4 54.46(6) 31_655 31_655 ?
Cl3 In2 Rb4 125.54(6) 3_665 31_655 ?
Cl3 In2 Rb4 125.54(6) 2_655 31_655 ?
Cl3 In2 Rb4 125.54(6) 33_545 . ?
Cl3 In2 Rb4 125.54(6) . 31_655 ?
Cl3 In2 Rb4 125.54(6) 31_655 . ?
Cl3 In2 Rb4 54.46(6) 3_665 . ?
Cl3 In2 Rb4 125.54(6) 32 . ?
Cl3 In2 Rb4 54.46(6) 33_545 31_655 ?
Cl3 In2 Rb4 54.46(6) 2_655 . ?
Cl3 In2 Rb4 54.46(6) 32 31_655 ?
Cl3 In2 Cl3 180.00(9) . 31_655 ?
Cl3 In2 Cl3 89.61(8) . 2_655 ?
Cl3 In2 Cl3 89.61(8) . 3_665 ?
Cl3 In2 Cl3 90.39(8) 2_655 31_655 ?
Cl3 In2 Cl3 89.61(8) 3_665 2_655 ?
Cl3 In2 Cl3 89.61(8) 31_655 32 ?
Cl3 In2 Cl3 90.39(8) . 32 ?
Cl3 In2 Cl3 180.0 3_665 33_545 ?
Cl3 In2 Cl3 180.0 2_655 32 ?
Cl3 In2 Cl3 90.39(8) 3_665 32 ?
Cl3 In2 Cl3 90.39(8) . 33_545 ?
Cl3 In2 Cl3 89.61(8) 31_655 33_545 ?
Cl3 In2 Cl3 90.39(8) 3_665 31_655 ?
Cl3 In2 Cl3 90.39(8) 2_655 33_545 ?
Cl3 In2 Cl3 89.61(8) 32 33_545 ?
Cl4 In3 Cl4 101.25(14) . 4 ?
Cl4 In3 Cl5 91.95(9) 4 . ?
Cl4 In3 Cl5 91.95(9) . 4 ?
Cl4 In3 Cl5 91.02(9) 4 4 ?
Cl4 In3 Cl5 91.02(9) . . ?
Cl4 In3 Cl6 85.54(9) . 4 ?
Cl4 In3 Cl6 85.53(9) 4 . ?
Cl4 In3 Cl6 173.21(10) 4 4 ?
Cl4 In3 Cl6 173.21(10) . . ?
Cl5 In3 Cl5 175.32(14) 4 . ?
Cl5 In3 Cl6 88.31(9) 4 4 ?
Cl5 In3 Cl6 88.31(9) . 4 ?
Cl5 In3 Cl6 88.32(9) 4 . ?
Cl5 In3 Cl6 88.31(9) . . ?
Cl6 In3 Cl6 87.69(13) 4 . ?
In1 Rb1 Rb3 85.59(2) . 31_665 ?
In1 Rb1 Rb4 180.0 . 34_665 ?
Rb4 Rb1 Rb3 94.41(2) 34_665 31_665 ?
Cl1 Rb1 In1 38.94(5) 3_675 . ?
Cl1 Rb1 In1 38.94(5) . . ?
Cl1 Rb1 In1 38.94(5) 2_765 . ?
Cl1 Rb1 Rb3 104.01(6) 3_675 31_665 ?
Cl1 Rb1 Rb3 46.66(5) . 31_665 ?
Cl1 Rb1 Rb3 105.35(6) 2_765 31_665 ?
Cl1 Rb1 Rb4 141.06(5) 3_675 34_665 ?
Cl1 Rb1 Rb4 141.06(5) . 34_665 ?
Cl1 Rb1 Rb4 141.06(5) 2_765 34_665 ?
Cl1 Rb1 Cl1 65.95(8) 2_765 3_675 ?
Cl1 Rb1 Cl1 65.95(8) 3_675 . ?
Cl1 Rb1 Cl1 65.95(8) 2_765 . ?
Cl1 Rb1 Cl4 66.43(7) 2_765 32 ?
Cl1 Rb1 Cl4 82.18(7) 3_675 31_665 ?
Cl1 Rb1 Cl4 130.21(7) 3_675 32 ?
Cl1 Rb1 Cl4 66.43(7) 3_675 33_655 ?
Cl1 Rb1 Cl4 66.43(6) . 31_665 ?
Cl1 Rb1 Cl4 130.21(7) 2_765 31_665 ?
Cl1 Rb1 Cl4 82.19(7) . 32 ?
Cl1 Rb1 Cl4 130.21(7) . 33_655 ?
Cl1 Rb1 Cl4 82.18(7) 2_765 33_655 ?
Cl1 Rb1 Cl5 124.89(7) 2_765 36 ?
Cl1 Rb1 Cl5 91.79(7) 2_765 35_655 ?
Cl1 Rb1 Cl5 91.79(7) 3_675 34_665 ?
Cl1 Rb1 Cl5 124.89(7) . 34_665 ?
Cl1 Rb1 Cl5 149.90(7) . 35_655 ?
Cl1 Rb1 Cl5 124.89(7) 3_675 35_655 ?
Cl1 Rb1 Cl5 91.80(7) . 36 ?
Cl1 Rb1 Cl5 149.90(7) 3_675 36 ?
Cl1 Rb1 Cl5 149.90(7) 2_765 34_665 ?
Cl4 Rb1 In1 92.70(5) 31_665 . ?
Cl4 Rb1 In1 92.70(5) 32 . ?
Cl4 Rb1 In1 92.70(5) 33_655 . ?
Cl4 Rb1 Rb3 75.51(5) 32 31_665 ?
Cl4 Rb1 Rb3 45.29(5) 31_665 31_665 ?
Cl4 Rb1 Rb3 164.70(5) 33_655 31_665 ?
Cl4 Rb1 Rb4 87.30(5) 33_655 34_665 ?
Cl4 Rb1 Rb4 87.30(5) 32 34_665 ?
Cl4 Rb1 Rb4 87.30(5) 31_665 34_665 ?
Cl4 Rb1 Cl4 119.781(8) 31_665 33_655 ?
Cl4 Rb1 Cl4 119.779(8) 32 33_655 ?
Cl4 Rb1 Cl4 119.782(8) 31_665 32 ?
Cl5 Rb1 In1 129.00(5) 34_665 . ?
Cl5 Rb1 In1 129.00(5) 35_655 . ?
Cl5 Rb1 In1 129.00(5) 36 . ?
Cl5 Rb1 Rb3 130.88(6) 35_655 31_665 ?
Cl5 Rb1 Rb3 47.73(5) 36 31_665 ?
Cl5 Rb1 Rb3 99.41(5) 34_665 31_665 ?
Cl5 Rb1 Rb4 51.00(5) 34_665 34_665 ?
Cl5 Rb1 Rb4 51.00(5) 36 34_665 ?
Cl5 Rb1 Rb4 51.00(5) 35_655 34_665 ?
Cl5 Rb1 Cl4 69.97(7) 35_655 32 ?
Cl5 Rb1 Cl4 60.77(6) 36 32 ?
Cl5 Rb1 Cl4 69.97(7) 34_665 33_655 ?
Cl5 Rb1 Cl4 137.91(8) 36 33_655 ?
Cl5 Rb1 Cl4 60.77(6) 34_665 31_665 ?
Cl5 Rb1 Cl4 60.77(7) 35_655 33_655 ?
Cl5 Rb1 Cl4 69.97(7) 36 31_665 ?
Cl5 Rb1 Cl4 137.91(7) 35_655 31_665 ?
Cl5 Rb1 Cl4 137.91(8) 34_665 32 ?
Cl5 Rb1 Cl5 84.60(7) 36 34_665 ?
Cl5 Rb1 Cl5 84.60(7) 34_665 35_655 ?
Cl5 Rb1 Cl5 84.60(7) 36 35_655 ?
Cl1 Rb2 In1 93.82(5) . 31_665 ?
Cl1 Rb2 In1 35.18(5) 31_665 31_665 ?
Cl1 Rb2 In1 147.33(5) 2_765 31_665 ?
Cl1 Rb2 Cl1 56.90(9) . 2_765 ?
Cl1 Rb2 Cl1 123.91(5) 31_665 2_765 ?
Cl1 Rb2 Cl1 92.99(6) . 31_665 ?
Cl1 Rb2 Cl2 56.82(6) 31_665 31_665 ?
Cl1 Rb2 Cl2 62.43(7) . 31_665 ?
Cl1 Rb2 Cl3 168.57(7) . 33_545 ?
Cl1 Rb2 Cl3 117.47(7) . 32 ?
Cl1 Rb2 Cl3 126.43(6) 31_665 32 ?
Cl1 Rb2 Cl4 82.84(7) . 32 ?
Cl1 Rb2 Cl6 84.70(6) . 36 ?
Cl1 Rb2 Cl6 112.97(7) 31_665 36 ?
Cl2 Rb2 In1 97.26(6) . 31_665 ?
Cl2 Rb2 In1 34.34(5) 33_545 31_665 ?
Cl2 Rb2 In1 34.38(4) 31_665 31_665 ?
Cl2 Rb2 Cl1 66.27(7) . 31_665 ?
Cl2 Rb2 Cl1 173.87(6) 33_545 2_765 ?
Cl2 Rb2 Cl1 60.89(6) 33_545 31_665 ?
Cl2 Rb2 Cl1 119.33(7) 31_665 2_765 ?
Cl2 Rb2 Cl1 120.99(7) 33_545 . ?
Cl2 Rb2 Cl1 61.75(7) . . ?
Cl2 Rb2 Cl1 57.91(6) . 2_765 ?
Cl2 Rb2 Cl2 93.31(7) . 31_665 ?
Cl2 Rb2 Cl2 59.02(9) 33_545 31_665 ?
Cl2 Rb2 Cl2 127.15(5) . 33_545 ?
Cl2 Rb2 Cl3 120.48(7) 33_545 32 ?
Cl2 Rb2 Cl3 62.81(7) 33_545 33_545 ?
Cl2 Rb2 Cl3 92.85(7) 33_545 . ?
Cl2 Rb2 Cl3 65.24(7) . . ?
Cl2 Rb2 Cl3 176.45(6) 31_665 32 ?
Cl2 Rb2 Cl3 126.00(7) . 33_545 ?
Cl2 Rb2 Cl3 89.60(7) . 32 ?
Cl2 Rb2 Cl4 119.80(8) . 32 ?
Cl2 Rb2 Cl4 112.52(7) 33_545 32 ?
Cl2 Rb2 Cl6 63.98(6) 33_545 36 ?
Cl2 Rb2 Cl6 145.92(7) . 36 ?
Cl2 Rb2 Cl6 63.68(6) 31_665 36 ?
Cl3 Rb2 In1 147.10(5) 32 31_665 ?
Cl3 Rb2 In1 93.34(5) 33_545 31_665 ?
Cl3 Rb2 In1 95.10(5) . 31_665 ?
Cl3 Rb2 Cl1 67.64(6) . 31_665 ?
Cl3 Rb2 Cl1 92.70(6) . 2_765 ?
Cl3 Rb2 Cl1 97.99(7) 33_545 31_665 ?
Cl3 Rb2 Cl1 118.03(6) 33_545 2_765 ?
Cl3 Rb2 Cl1 60.75(6) 32 2_765 ?
Cl3 Rb2 Cl1 126.92(7) . . ?
Cl3 Rb2 Cl2 124.38(6) . 31_665 ?
Cl3 Rb2 Cl2 121.69(7) 33_545 31_665 ?
Cl3 Rb2 Cl3 61.14(8) . 33_545 ?
Cl3 Rb2 Cl3 57.67(9) 33_545 32 ?
Cl3 Rb2 Cl3 58.80(8) . 32 ?
Cl3 Rb2 Cl4 123.07(7) . 32 ?
Cl3 Rb2 Cl6 88.08(6) 33_545 36 ?
Cl3 Rb2 Cl6 148.25(7) . 36 ?
Cl4 Rb2 In1 134.41(6) 32 31_665 ?
Cl4 Rb2 Cl1 168.78(7) 32 31_665 ?
Cl4 Rb2 Cl1 62.06(6) 32 2_765 ?
Cl4 Rb2 Cl2 112.25(7) 32 31_665 ?
Cl4 Rb2 Cl3 85.79(7) 32 33_545 ?
Cl4 Rb2 Cl3 64.44(6) 32 32 ?
Cl4 Rb2 Cl6 56.39(6) 32 36 ?
Cl6 Rb2 In1 78.02(5) 36 31_665 ?
Cl6 Rb2 Cl1 109.89(6) 36 2_765 ?
Cl6 Rb2 Cl3 112.80(6) 36 32 ?
Rb1 Rb3 Rb2 149.64(3) 31_665 32 ?
Rb4 Rb3 Rb1 110.07(2) . 31_665 ?
Rb4 Rb3 Rb2 67.45(2) . 32 ?
Cu1 Rb3 Rb1 122.30(3) 4_665 31_665 ?
Cu1 Rb3 Rb2 77.18(3) 4_665 32 ?
Cu1 Rb3 Rb4 123.02(3) 4_665 . ?
Cl1 Rb3 Rb1 47.02(5) 31_665 31_665 ?
Cl1 Rb3 Rb2 103.53(6) 31_665 32 ?
Cl1 Rb3 Rb4 107.88(6) 31_665 . ?
Cl1 Rb3 Cu1 123.28(7) 31_665 4_665 ?
Cl1 Rb3 Cl3 72.31(7) 31_665 . ?
Cl1 Rb3 Cl5 148.94(8) 31_665 3_665 ?
Cl1 Rb3 Cl5 92.00(7) 31_665 6_665 ?
Cl1 Rb3 Cl6 143.41(7) 31_665 5_665 ?
Cl1 Rb3 Cl6 95.31(8) 31_665 6_665 ?
Cl2 Rb3 Rb1 114.39(6) . 31_665 ?
Cl2 Rb3 Rb2 46.47(6) . 32 ?
Cl2 Rb3 Rb4 109.03(6) . . ?
Cl2 Rb3 Cu1 69.48(7) . 4_665 ?
Cl2 Rb3 Cl1 71.83(7) . 31_665 ?
Cl2 Rb3 Cl3 67.87(7) . . ?
Cl2 Rb3 Cl4 132.72(8) . . ?
Cl2 Rb3 Cl5 130.26(8) . 3_665 ?
Cl2 Rb3 Cl5 134.79(8) . 6_665 ?
Cl2 Rb3 Cl6 71.89(7) . 5_665 ?
Cl2 Rb3 Cl6 75.00(7) . 6_665 ?
Cl3 Rb3 Rb1 106.08(6) . 31_665 ?
Cl3 Rb3 Rb2 48.34(5) . 32 ?
Cl3 Rb3 Rb4 48.10(5) . . ?
Cl3 Rb3 Cu1 125.07(6) . 4_665 ?
Cl4 Rb3 Rb1 55.11(6) . 31_665 ?
Cl4 Rb3 Rb2 116.08(6) . 32 ?
Cl4 Rb3 Rb4 55.04(6) . . ?
Cl4 Rb3 Cu1 157.77(7) . 4_665 ?
Cl4 Rb3 Cl1 72.93(8) . 31_665 ?
Cl4 Rb3 Cl3 72.08(7) . . ?
Cl4 Rb3 Cl5 76.39(7) . 6_665 ?
Cl4 Rb3 Cl5 76.25(7) . 3_665 ?
Cl4 Rb3 Cl6 139.01(8) . 5_665 ?
Cl4 Rb3 Cl6 138.90(8) . 6_665 ?
Cl5 Rb3 Rb1 47.58(5) 6_665 31_665 ?
Cl5 Rb3 Rb1 115.19(6) 3_665 31_665 ?
Cl5 Rb3 Rb2 162.26(6) 6_665 32 ?
Cl5 Rb3 Rb2 86.54(6) 3_665 32 ?
Cl5 Rb3 Rb4 48.65(5) 3_665 . ?
Cl5 Rb3 Rb4 116.13(6) 6_665 . ?
Cl5 Rb3 Cu1 87.21(6) 6_665 4_665 ?
Cl5 Rb3 Cu1 87.43(6) 3_665 4_665 ?
Cl5 Rb3 Cl3 94.75(7) 3_665 . ?
Cl5 Rb3 Cl3 147.69(8) 6_665 . ?
Cl5 Rb3 Cl5 84.37(8) 3_665 6_665 ?
Cl5 Rb3 Cl6 64.56(7) 6_665 6_665 ?
Cl5 Rb3 Cl6 110.41(7) 6_665 5_665 ?
Cl5 Rb3 Cl6 110.59(7) 3_665 6_665 ?
Cl5 Rb3 Cl6 64.79(7) 3_665 5_665 ?
Cl6 Rb3 Rb1 155.63(6) 5_665 31_665 ?
Cl6 Rb3 Rb1 87.71(5) 6_665 31_665 ?
Cl6 Rb3 Rb2 51.85(5) 5_665 32 ?
Cl6 Rb3 Rb2 104.90(5) 6_665 32 ?
Cl6 Rb3 Rb4 88.29(5) 5_665 . ?
Cl6 Rb3 Rb4 156.63(6) 6_665 . ?
Cl6 Rb3 Cu1 35.39(5) 5_665 4_665 ?
Cl6 Rb3 Cu1 35.40(5) 6_665 4_665 ?
Cl6 Rb3 Cl3 142.84(7) 6_665 . ?
Cl6 Rb3 Cl3 98.10(7) 5_665 . ?
Cl6 Rb3 Cl6 70.80(10) 6_665 5_665 ?
In2 Rb4 Rb1 180.0 . 28_665 ?
In2 Rb4 Rb3 86.77(2) . 3_665 ?
Rb1 Rb4 Rb3 93.23(2) 28_665 3_665 ?
Cl3 Rb4 In2 37.90(5) . . ?
Cl3 Rb4 In2 37.90(5) 3_665 . ?
Cl3 Rb4 In2 37.90(5) 2_655 . ?
Cl3 Rb4 Rb1 142.10(5) 3_665 28_665 ?
Cl3 Rb4 Rb1 142.10(5) 2_655 28_665 ?
Cl3 Rb4 Rb1 142.10(5) . 28_665 ?
Cl3 Rb4 Rb3 48.91(5) 3_665 3_665 ?
Cl3 Rb4 Rb3 103.86(6) 2_655 3_665 ?
Cl3 Rb4 Rb3 106.51(6) . 3_665 ?
Cl3 Rb4 Cl3 64.28(8) 3_665 . ?
Cl3 Rb4 Cl3 64.28(8) 2_655 . ?
Cl3 Rb4 Cl3 64.28(8) 3_665 2_655 ?
Cl3 Rb4 Cl4 85.65(7) . 3_665 ?
Cl3 Rb4 Cl4 66.77(6) 2_655 2_655 ?
Cl3 Rb4 Cl4 66.77(6) . . ?
Cl3 Rb4 Cl4 85.65(7) 2_655 . ?
Cl3 Rb4 Cl4 85.65(7) 3_665 2_655 ?
Cl3 Rb4 Cl4 66.77(6) 3_665 3_665 ?
Cl3 Rb4 Cl4 129.90(7) 3_665 . ?
Cl3 Rb4 Cl4 129.90(7) 2_655 3_665 ?
Cl3 Rb4 Cl4 129.90(7) . 2_655 ?
Cl3 Rb4 Cl5 152.44(7) . 2_655 ?
Cl3 Rb4 Cl5 152.44(7) 2_655 3_665 ?
Cl3 Rb4 Cl5 94.34(6) . 3_665 ?
Cl3 Rb4 Cl5 152.44(7) 3_665 . ?
Cl3 Rb4 Cl5 123.91(7) 2_655 2_655 ?
Cl3 Rb4 Cl5 94.34(6) 3_665 2_655 ?
Cl3 Rb4 Cl5 94.34(6) 2_655 . ?
Cl3 Rb4 Cl5 123.91(7) . . ?
Cl3 Rb4 Cl5 123.91(7) 3_665 3_665 ?
Cl4 Rb4 In2 94.15(5) 2_655 . ?
Cl4 Rb4 In2 94.15(5) 3_665 . ?
Cl4 Rb4 In2 94.15(5) . . ?
Cl4 Rb4 Rb1 85.85(5) 3_665 28_665 ?
Cl4 Rb4 Rb1 85.85(5) 2_655 28_665 ?
Cl4 Rb4 Rb1 85.85(5) . 28_665 ?
Cl4 Rb4 Rb3 164.95(5) . 3_665 ?
Cl4 Rb4 Rb3 45.52(5) 3_665 3_665 ?
Cl4 Rb4 Rb3 75.36(5) 2_655 3_665 ?
Cl4 Rb4 Cl4 119.482(12) 2_655 . ?
Cl4 Rb4 Cl4 119.482(12) 3_665 . ?
Cl4 Rb4 Cl4 119.482(12) 2_655 3_665 ?
Cl5 Rb4 In2 129.95(5) 3_665 . ?
Cl5 Rb4 In2 129.95(5) 2_655 . ?
Cl5 Rb4 In2 129.95(5) . . ?
Cl5 Rb4 Rb1 50.05(5) 2_655 28_665 ?
Cl5 Rb4 Rb1 50.05(5) . 28_665 ?
Cl5 Rb4 Rb1 50.05(5) 3_665 28_665 ?
Cl5 Rb4 Rb3 129.34(6) . 3_665 ?
Cl5 Rb4 Rb3 47.42(5) 2_655 3_665 ?
Cl5 Rb4 Rb3 98.71(5) 3_665 3_665 ?
Cl5 Rb4 Cl4 135.52(7) 3_665 2_655 ?
Cl5 Rb4 Cl4 60.07(6) 3_665 3_665 ?
Cl5 Rb4 Cl4 60.07(6) . . ?
Cl5 Rb4 Cl4 135.53(7) . 3_665 ?
Cl5 Rb4 Cl4 69.27(7) 3_665 . ?
Cl5 Rb4 Cl4 69.28(7) 2_655 3_665 ?
Cl5 Rb4 Cl4 60.07(6) 2_655 2_655 ?
Cl5 Rb4 Cl4 69.27(7) . 2_655 ?
Cl5 Rb4 Cl4 135.52(7) 2_655 . ?
Cl5 Rb4 Cl5 83.20(7) . 3_665 ?
Cl5 Rb4 Cl5 83.19(7) 2_655 3_665 ?
Cl5 Rb4 Cl5 83.20(7) . 2_655 ?
Rb3 Cu1 Rb3 115.10(3) 5_565 6_655 ?
Rb3 Cu1 Rb3 115.10(3) 4_445 6_655 ?
Rb3 Cu1 Rb3 115.10(3) 4_445 5_565 ?
Cl6 Cu1 Rb3 59.44(8) 3 6_655 ?
Cl6 Cu1 Rb3 59.30(7) 2 5_565 ?
Cl6 Cu1 Rb3 59.30(7) 3 4_445 ?
Cl6 Cu1 Rb3 59.29(7) . 6_655 ?
Cl6 Cu1 Rb3 160.52(12) 2 6_655 ?
Cl6 Cu1 Rb3 160.52(12) 3 5_565 ?
Cl6 Cu1 Rb3 160.51(12) . 4_445 ?
Cl6 Cu1 Rb3 59.44(8) 2 4_445 ?
Cl6 Cu1 Rb3 59.44(7) . 5_565 ?
Cl6 Cu1 Cl6 118.74(4) 2 . ?
Cl6 Cu1 Cl6 118.74(4) 2 3 ?
Cl6 Cu1 Cl6 118.74(4) 3 . ?
In1 Cl1 Rb1 86.54(8) . . ?
In1 Cl1 Rb2 92.41(8) . . ?
In1 Cl1 Rb2 82.26(8) . 3_675 ?
In1 Cl1 Rb2 90.45(8) . 31_665 ?
In1 Cl1 Rb3 172.67(11) . 31_665 ?
Rb1 Cl1 Rb2 100.30(8) . . ?
Rb1 Cl1 Rb2 172.19(10) . 31_665 ?
Rb1 Cl1 Rb2 91.45(7) . 3_675 ?
Rb2 Cl1 Rb2 166.80(8) . 3_675 ?
Rb2 Cl1 Rb2 80.99(6) 31_665 3_675 ?
Rb2 Cl1 Rb2 87.01(6) . 31_665 ?
Rb3 Cl1 Rb1 86.32(7) 31_665 . ?
Rb3 Cl1 Rb2 96.43(7) 31_665 31_665 ?
Rb3 Cl1 Rb2 90.47(8) 31_665 . ?
Rb3 Cl1 Rb2 96.30(7) 31_665 3_675 ?
In1 Cl2 Rb2 94.05(9) . 32 ?
In1 Cl2 Rb2 86.87(8) . 31_665 ?
In1 Cl2 Rb2 97.82(8) . . ?
In1 Cl2 Rb3 156.96(11) . . ?
Rb2 Cl2 Rb2 92.80(8) . 32 ?
Rb2 Cl2 Rb2 86.69(7) . 31_665 ?
Rb2 Cl2 Rb2 179.00(9) 32 31_665 ?
Rb3 Cl2 Rb2 91.97(7) . 32 ?
Rb3 Cl2 Rb2 87.32(7) . 31_665 ?
Rb3 Cl2 Rb2 104.08(8) . . ?
In2 Cl3 Rb2 91.31(8) . 32 ?
In2 Cl3 Rb2 93.44(7) . . ?
In2 Cl3 Rb2 86.11(7) . 33_545 ?
In2 Cl3 Rb3 170.10(10) . . ?
In2 Cl3 Rb4 87.64(8) . . ?
Rb2 Cl3 Rb2 172.20(8) 32 33_545 ?
Rb2 Cl3 Rb2 88.21(6) . 32 ?
Rb2 Cl3 Rb2 84.60(6) . 33_545 ?
Rb3 Cl3 Rb2 96.12(7) . . ?
Rb3 Cl3 Rb2 86.47(7) . 32 ?
Rb3 Cl3 Rb2 97.29(7) . 33_545 ?
Rb4 Cl3 Rb2 95.74(7) . 32 ?
Rb4 Cl3 Rb2 91.52(6) . 33_545 ?
Rb4 Cl3 Rb2 175.88(9) . . ?
Rb4 Cl3 Rb3 82.99(6) . . ?
In3 Cl4 Rb1 98.17(9) . 31_665 ?
In3 Cl4 Rb2 114.79(10) . 33_545 ?
In3 Cl4 Rb3 138.63(11) . . ?
In3 Cl4 Rb4 99.89(9) . . ?
Rb2 Cl4 Rb1 92.04(7) 33_545 31_665 ?
Rb2 Cl4 Rb4 90.52(7) 33_545 . ?
Rb3 Cl4 Rb1 79.60(7) . 31_665 ?
Rb3 Cl4 Rb2 106.58(8) . 33_545 ?
Rb3 Cl4 Rb4 79.45(7) . . ?
Rb4 Cl4 Rb1 158.74(9) . 31_665 ?
In3 Cl5 Rb1 108.15(9) . 28_665 ?
In3 Cl5 Rb3 104.74(9) . 6_655 ?
In3 Cl5 Rb3 105.08(8) . 2_655 ?
In3 Cl5 Rb4 108.22(9) . . ?
Rb1 Cl5 Rb3 84.69(6) 28_665 6_655 ?
Rb1 Cl5 Rb4 78.95(7) 28_665 . ?
Rb3 Cl5 Rb1 145.96(9) 2_655 28_665 ?
Rb3 Cl5 Rb3 93.96(8) 2_655 6_655 ?
Rb3 Cl5 Rb4 83.94(6) 2_655 . ?
Rb3 Cl5 Rb4 146.36(9) 6_655 . ?
In3 Cl6 Rb2 103.28(9) . 30_455 ?
In3 Cl6 Rb3 101.44(9) . 5_565 ?
In3 Cl6 Rb3 101.98(9) . 6_655 ?
Rb3 Cl6 Rb2 84.42(6) 6_655 30_455 ?
Rb3 Cl6 Rb2 83.50(6) 5_565 30_455 ?
Rb3 Cl6 Rb3 155.56(9) 6_655 5_565 ?
Cu1 Cl6 In3 129.65(13) . . ?
Cu1 Cl6 Rb2 127.06(12) . 30_455 ?
Cu1 Cl6 Rb3 85.16(9) . 5_565 ?
Cu1 Cl6 Rb3 85.30(8) . 6_655 ?

_olex2_submission_special_instructions 'No special instructions were received'
_exptl_crystal_recrystallization_method 'From the Melt'
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_mo_rb2cutbcl6data2_0ma
_database_code_depnum_ccdc_archive 'CCDC 2128947'
loop_
_audit_author_name
_audit_author_address
'Jia Lin'
;Shanghai University of Electric Power
China
;
_audit_update_record             
;
2022-02-24 deposited with the CCDC.	2022-06-13 downloaded from the CCDC.
;
_audit_creation_date             2018-01-21
_audit_creation_method           
;
Olex2 1.2
(compiled 2017.01.04 svn.r3372 for OlexSys, GUI svn.r5292)
;
_shelx_SHELXL_version_number     2016/6
_chemical_name_common            ?
_chemical_name_systematic        Rb8CuTb3Cl18
_chemical_formula_moiety         '0.33(Cl216 Cu12 Rb96 Tb36)'
_chemical_formula_sum            'Cl72 Cu4 Rb32 Tb12'
_chemical_formula_weight         7448.64
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Rb Rb -0.9393 2.9676 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Tb Tb -0.1723 4.1537 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      trigonal
_space_group_IT_number           167
_space_group_name_H-M_alt        'R -3 c'
_space_group_name_Hall           '-R 3 2"c'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'
'y, x, -z+1/2'
'x-y, -y, -z+1/2'
'-x, -x+y, -z+1/2'
'x+2/3, y+1/3, z+1/3'
'-y+2/3, x-y+1/3, z+1/3'
'-x+y+2/3, -x+1/3, z+1/3'
'y+2/3, x+1/3, -z+5/6'
'x-y+2/3, -y+1/3, -z+5/6'
'-x+2/3, -x+y+1/3, -z+5/6'
'x+1/3, y+2/3, z+2/3'
'-y+1/3, x-y+2/3, z+2/3'
'-x+y+1/3, -x+2/3, z+2/3'
'y+1/3, x+2/3, -z+7/6'
'x-y+1/3, -y+2/3, -z+7/6'
'-x+1/3, -x+y+2/3, -z+7/6'
'-x, -y, -z'
'y, -x+y, -z'
'x-y, x, -z'
'-y, -x, z-1/2'
'-x+y, y, z-1/2'
'x, x-y, z-1/2'
'-x+2/3, -y+1/3, -z+1/3'
'y+2/3, -x+y+1/3, -z+1/3'
'x-y+2/3, x+1/3, -z+1/3'
'-y+2/3, -x+1/3, z-1/6'
'-x+y+2/3, y+1/3, z-1/6'
'x+2/3, x-y+1/3, z-1/6'
'-x+1/3, -y+2/3, -z+2/3'
'y+1/3, -x+y+2/3, -z+2/3'
'x-y+1/3, x+2/3, -z+2/3'
'-y+1/3, -x+2/3, z+1/6'
'-x+y+1/3, y+2/3, z+1/6'
'x+1/3, x-y+2/3, z+1/6'

_cell_length_a                   13.0330(5)
_cell_length_b                   13.0330(5)
_cell_length_c                   76.493(5)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_volume                     11252.3(11)
_cell_formula_units_Z            3
_cell_measurement_reflns_used    8004
_cell_measurement_temperature    296.15
_cell_measurement_theta_max      25.04
_cell_measurement_theta_min      2.79
_shelx_estimated_absorpt_T_max   ?
_shelx_estimated_absorpt_T_min   ?
_exptl_absorpt_coefficient_mu    17.744
_exptl_absorpt_correction_T_max  0.7452
_exptl_absorpt_correction_T_min  0.4359
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
SADABS-2016/2 (Bruker,2016/2) was used for absorption correction.
wR2(int) was 0.1502 before and 0.0625 after correction.
The Ratio of minimum to maximum transmission is 0.5849.
The λ/2 correction factor is Not present.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            colourless
_exptl_crystal_colour_primary    colourless
_exptl_crystal_density_diffrn    3.298
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       plate
_exptl_crystal_F_000             9912
_exptl_crystal_size_max          0.08
_exptl_crystal_size_mid          0.08
_exptl_crystal_size_min          0.05
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0706
_diffrn_reflns_av_unetI/netI     0.0265
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.999
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       90
_diffrn_reflns_limit_l_min       -90
_diffrn_reflns_number            29355
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.999
_diffrn_reflns_theta_full        25.025
_diffrn_reflns_theta_max         25.025
_diffrn_reflns_theta_min         2.792
_diffrn_ambient_temperature      296.15
_diffrn_detector                 'Bruker Photon100'
_diffrn_detector_area_resol_mean 10.4
_diffrn_detector_type            'CMOS area detector'
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device       'four-circle diffractometer'
_diffrn_measurement_device_type  'D8 Venture'
_diffrn_measurement_method       'ω and φ scans'
_diffrn_radiation_collimation    'focusing mirrors'
_diffrn_radiation_monochromator  'mirror optics'
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   'microfocus sealed X-ray tube'
_diffrn_source_type              'Incoatec I\ms'
_diffrn_standards_number         0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                1805
_reflns_number_total             2224
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT V8.38A (?, 2016)'
_computing_data_collection       ?
_computing_data_reduction        'SAINT V8.38A (?, 2016)'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'XL (Sheldrick, 2008)'
_computing_structure_solution    'XT (Sheldrick, 2015)'
_refine_diff_density_max         4.325
_refine_diff_density_min         -2.244
_refine_diff_density_rms         0.346
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.118
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     92
_refine_ls_number_reflns         2224
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0831
_refine_ls_R_factor_gt           0.0675
_refine_ls_restrained_S_all      1.118
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0836P)²+1708.8916P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1806
_refine_ls_wR_factor_ref         0.1916
_refine_special_details          ?
_olex2_refinement_description    
;
;
_atom_sites_solution_hydrogens   .
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Tb2 Tb 0.666667 0.333333 0.333333 0.0145(4) Uani 1 6 d S T P . .
Tb1 Tb 1.333333 0.666667 0.33097(2) 0.0157(4) Uani 1 3 d S T P . .
Tb3 Tb 0.65792(7) 0.666667 0.416667 0.0166(3) Uani 1 2 d S T P . .
Rb3 Rb 1.03082(17) 0.66553(15) 0.38437(2) 0.0312(5) Uani 1 1 d . . . . .
Rb4 Rb 0.666667 0.333333 0.38831(4) 0.0350(7) Uani 1 3 d S T P . .
Rb1 Rb 1.333333 0.666667 0.27708(4) 0.0348(7) Uani 1 3 d S T P . .
Rb2 Rb 0.99765(17) 0.66803(19) 0.31713(3) 0.0454(6) Uani 1 1 d . . . . .
Cu1 Cu 0.333333 0.666667 0.44061(8) 0.0596(14) Uani 1 3 d S T P . .
Cl5 Cl 0.5332(4) 0.4308(4) 0.41650(6) 0.0331(10) Uani 1 1 d . . . . .
Cl3 Cl 0.8375(4) 0.4896(4) 0.35362(6) 0.0389(11) Uani 1 1 d . . . . .
Cl6 Cl 0.5056(4) 0.6651(4) 0.44131(7) 0.0452(13) Uani 1 1 d . . . . .
Cl4 Cl 0.7824(5) 0.6653(5) 0.39044(6) 0.0499(14) Uani 1 1 d . . . . .
Cl1 Cl 1.3022(6) 0.8139(5) 0.31051(7) 0.0541(15) Uani 1 1 d . . . . .
Cl2 Cl 1.1591(5) 0.6487(6) 0.34985(7) 0.0566(16) Uani 1 1 d . . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Tb2 Rb4 4.206(3) 31_655 ?
Tb2 Rb4 4.205(3) . ?
Tb2 Rb2 4.512(2) 3_665 ?
Tb2 Rb2 4.512(2) 2_655 ?
Tb2 Rb2 4.512(2) . ?
Tb2 Rb2 4.512(2) 32 ?
Tb2 Cl3 2.642(4) 31_655 ?
Tb2 Cl3 2.642(4) . ?
Tb2 Cl3 2.642(4) 32 ?
Tb2 Cl3 2.642(4) 3_665 ?
Tb2 Cl3 2.642(4) 2_655 ?
Tb2 Cl3 2.642(4) 33_545 ?
Tb1 Rb1 4.123(3) . ?
Tb1 Rb2 4.539(2) 32 ?
Tb1 Rb2 4.510(2) 3_775 ?
Tb1 Rb2 4.539(2) 31_765 ?
Tb1 Rb2 4.510(2) . ?
Tb1 Rb2 4.5101(19) 2_755 ?
Tb1 Cl1 2.660(5) 2_755 ?
Tb1 Cl1 2.660(5) 3_775 ?
Tb1 Cl1 2.660(5) . ?
Tb1 Cl2 2.600(5) 3_775 ?
Tb1 Cl2 2.600(5) 2_755 ?
Tb1 Cl2 2.600(5) . ?
Tb3 Cl5 2.663(4) 11_565 ?
Tb3 Cl5 2.663(4) . ?
Tb3 Cl6 2.730(5) 11_565 ?
Tb3 Cl6 2.731(5) . ?
Tb3 Cl4 2.586(5) 11_565 ?
Tb3 Cl4 2.586(5) . ?
Rb3 Rb4 4.5621(18) . ?
Rb3 Rb1 4.5906(18) 31_765 ?
Rb3 Rb2 4.892(3) 32 ?
Rb3 Cu1 3.987(2) 10 ?
Rb3 Cl5 3.357(5) 3_665 ?
Rb3 Cl5 3.393(5) 10 ?
Rb3 Cl3 3.370(5) . ?
Rb3 Cl6 3.480(5) 12_655 ?
Rb3 Cl6 3.460(5) 10 ?
Rb3 Cl4 3.269(5) . ?
Rb3 Cl1 3.256(5) 31_765 ?
Rb3 Cl2 3.191(5) . ?
Rb4 Rb1 4.240(4) 34_665 ?
Rb4 Cl5 3.392(5) 2_655 ?
Rb4 Cl5 3.391(5) . ?
Rb4 Cl5 3.392(5) 3_665 ?
Rb4 Cl3 3.407(5) 3_665 ?
Rb4 Cl3 3.407(5) 2_655 ?
Rb4 Cl3 3.407(5) . ?
Rb4 Cl4 3.807(6) . ?
Rb4 Cl4 3.807(6) 2_655 ?
Rb4 Cl4 3.807(6) 3_665 ?
Rb1 Cl5 3.346(5) 29_655 ?
Rb1 Cl5 3.346(5) 28_665 ?
Rb1 Cl5 3.346(5) 30 ?
Rb1 Cl4 3.835(6) 32 ?
Rb1 Cl4 3.835(6) 31_765 ?
Rb1 Cl4 3.835(6) 33_645 ?
Rb1 Cl1 3.342(6) 3_775 ?
Rb1 Cl1 3.342(6) 2_755 ?
Rb1 Cl1 3.342(6) . ?
Rb2 Cl3 3.954(6) 32 ?
Rb2 Cl3 3.586(6) 33_545 ?
Rb2 Cl3 3.564(5) . ?
Rb2 Cl6 3.846(6) 28_665 ?
Rb2 Cl4 3.492(6) 32 ?
Rb2 Cl1 3.721(6) 31_765 ?
Rb2 Cl1 3.476(7) . ?
Rb2 Cl2 3.950(7) 31_765 ?
Rb2 Cl2 3.517(7) 33_545 ?
Rb2 Cl2 3.360(6) . ?
Cu1 Cl6 2.256(5) 2_665 ?
Cu1 Cl6 2.256(5) 3_565 ?
Cu1 Cl6 2.256(5) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Rb4 Tb2 Rb4 180.0 31_655 . ?
Rb4 Tb2 Rb2 105.95(3) . 2_655 ?
Rb4 Tb2 Rb2 74.05(3) 31_655 3_665 ?
Rb4 Tb2 Rb2 105.95(3) 31_655 32 ?
Rb4 Tb2 Rb2 105.95(3) . . ?
Rb4 Tb2 Rb2 74.05(3) . 32 ?
Rb4 Tb2 Rb2 74.05(3) 31_655 2_655 ?
Rb4 Tb2 Rb2 105.95(3) . 3_665 ?
Rb4 Tb2 Rb2 74.05(3) 31_655 . ?
Rb2 Tb2 Rb2 112.75(2) 3_665 2_655 ?
Rb2 Tb2 Rb2 67.25(2) . 32 ?
Rb2 Tb2 Rb2 112.75(2) 3_665 . ?
Rb2 Tb2 Rb2 112.75(2) . 2_655 ?
Rb2 Tb2 Rb2 67.25(2) 3_665 32 ?
Rb2 Tb2 Rb2 180.00(5) 2_655 32 ?
Cl3 Tb2 Rb4 54.02(10) 33_545 31_655 ?
Cl3 Tb2 Rb4 54.02(10) 32 31_655 ?
Cl3 Tb2 Rb4 125.98(10) . 31_655 ?
Cl3 Tb2 Rb4 125.98(10) 32 . ?
Cl3 Tb2 Rb4 54.02(10) 3_665 . ?
Cl3 Tb2 Rb4 125.98(10) 3_665 31_655 ?
Cl3 Tb2 Rb4 125.98(10) 33_545 . ?
Cl3 Tb2 Rb4 54.02(10) . . ?
Cl3 Tb2 Rb4 54.02(10) 2_655 . ?
Cl3 Tb2 Rb4 125.98(10) 2_655 31_655 ?
Cl3 Tb2 Rb4 125.98(10) 31_655 . ?
Cl3 Tb2 Rb4 54.02(10) 31_655 31_655 ?
Cl3 Tb2 Rb2 127.39(12) 2_655 3_665 ?
Cl3 Tb2 Rb2 52.14(11) 3_665 3_665 ?
Cl3 Tb2 Rb2 127.86(11) 33_545 3_665 ?
Cl3 Tb2 Rb2 52.61(12) 32 3_665 ?
Cl3 Tb2 Rb2 119.39(12) 33_545 32 ?
Cl3 Tb2 Rb2 60.61(12) 32 . ?
Cl3 Tb2 Rb2 127.86(11) 32 2_655 ?
Cl3 Tb2 Rb2 127.85(11) 31_655 . ?
Cl3 Tb2 Rb2 127.39(12) . 2_655 ?
Cl3 Tb2 Rb2 60.61(12) 33_545 2_655 ?
Cl3 Tb2 Rb2 52.14(11) 32 32 ?
Cl3 Tb2 Rb2 119.39(12) 2_655 . ?
Cl3 Tb2 Rb2 52.61(12) 33_545 . ?
Cl3 Tb2 Rb2 60.61(12) 3_665 32 ?
Cl3 Tb2 Rb2 60.61(12) 31_655 3_665 ?
Cl3 Tb2 Rb2 127.39(12) 3_665 . ?
Cl3 Tb2 Rb2 52.14(11) . . ?
Cl3 Tb2 Rb2 52.61(12) 31_655 2_655 ?
Cl3 Tb2 Rb2 127.39(12) 31_655 32 ?
Cl3 Tb2 Rb2 119.39(12) . 3_665 ?
Cl3 Tb2 Rb2 52.61(12) . 32 ?
Cl3 Tb2 Rb2 52.14(11) 2_655 2_655 ?
Cl3 Tb2 Rb2 127.86(11) 2_655 32 ?
Cl3 Tb2 Rb2 119.39(12) 3_665 2_655 ?
Cl3 Tb2 Cl3 91.02(15) 33_545 . ?
Cl3 Tb2 Cl3 88.98(15) 32 31_655 ?
Cl3 Tb2 Cl3 180.0 33_545 3_665 ?
Cl3 Tb2 Cl3 88.98(15) . 3_665 ?
Cl3 Tb2 Cl3 91.02(15) 31_655 3_665 ?
Cl3 Tb2 Cl3 91.02(15) 33_545 2_655 ?
Cl3 Tb2 Cl3 88.99(15) . 2_655 ?
Cl3 Tb2 Cl3 88.98(15) 3_665 2_655 ?
Cl3 Tb2 Cl3 88.98(15) 32 33_545 ?
Cl3 Tb2 Cl3 180.0 32 2_655 ?
Cl3 Tb2 Cl3 88.98(15) 31_655 33_545 ?
Cl3 Tb2 Cl3 91.02(15) 31_655 2_655 ?
Cl3 Tb2 Cl3 91.02(15) 32 . ?
Cl3 Tb2 Cl3 91.02(15) 32 3_665 ?
Cl3 Tb2 Cl3 180.0 31_655 . ?
Rb1 Tb1 Rb2 76.42(3) . . ?
Rb1 Tb1 Rb2 76.42(3) . 2_755 ?
Rb1 Tb1 Rb2 108.23(3) . 31_765 ?
Rb1 Tb1 Rb2 76.42(3) . 3_775 ?
Rb1 Tb1 Rb2 108.23(3) . 32 ?
Rb2 Tb1 Rb2 114.66(2) . 2_755 ?
Rb2 Tb1 Rb2 110.68(3) 31_765 32 ?
Rb2 Tb1 Rb2 67.29(4) 2_755 32 ?
Rb2 Tb1 Rb2 114.66(2) . 3_775 ?
Rb2 Tb1 Rb2 67.29(4) . 31_765 ?
Rb2 Tb1 Rb2 67.03(5) . 32 ?
Rb2 Tb1 Rb2 175.35(3) 2_755 31_765 ?
Rb2 Tb1 Rb2 114.66(2) 3_775 2_755 ?
Rb2 Tb1 Rb2 175.35(3) 3_775 32 ?
Rb2 Tb1 Rb2 67.03(5) 3_775 31_765 ?
Cl1 Tb1 Rb1 53.96(12) . . ?
Cl1 Tb1 Rb1 53.95(12) 2_755 . ?
Cl1 Tb1 Rb1 53.95(12) 3_775 . ?
Cl1 Tb1 Rb2 55.06(12) . 31_765 ?
Cl1 Tb1 Rb2 65.66(15) 2_755 . ?
Cl1 Tb1 Rb2 55.06(12) 2_755 32 ?
Cl1 Tb1 Rb2 50.27(15) . . ?
Cl1 Tb1 Rb2 116.73(15) . 32 ?
Cl1 Tb1 Rb2 129.55(13) . 2_755 ?
Cl1 Tb1 Rb2 129.55(13) 3_775 . ?
Cl1 Tb1 Rb2 116.73(15) 3_775 31_765 ?
Cl1 Tb1 Rb2 65.66(15) . 3_775 ?
Cl1 Tb1 Rb2 50.27(14) 2_755 2_755 ?
Cl1 Tb1 Rb2 132.47(15) 3_775 32 ?
Cl1 Tb1 Rb2 50.27(15) 3_775 3_775 ?
Cl1 Tb1 Rb2 129.55(13) 2_755 3_775 ?
Cl1 Tb1 Rb2 65.66(15) 3_775 2_755 ?
Cl1 Tb1 Rb2 132.47(15) 2_755 31_765 ?
Cl1 Tb1 Cl1 88.89(17) . 3_775 ?
Cl1 Tb1 Cl1 88.89(17) . 2_755 ?
Cl1 Tb1 Cl1 88.89(16) 2_755 3_775 ?
Cl2 Tb1 Rb1 123.73(12) 2_755 . ?
Cl2 Tb1 Rb1 123.73(13) 3_775 . ?
Cl2 Tb1 Rb1 123.73(12) . . ?
Cl2 Tb1 Rb2 50.57(16) . 32 ?
Cl2 Tb1 Rb2 117.68(16) 3_775 . ?
Cl2 Tb1 Rb2 127.75(13) 2_755 31_765 ?
Cl2 Tb1 Rb2 50.57(15) 3_775 31_765 ?
Cl2 Tb1 Rb2 47.61(12) 2_755 2_755 ?
Cl2 Tb1 Rb2 126.94(16) 2_755 . ?
Cl2 Tb1 Rb2 126.93(16) 3_775 2_755 ?
Cl2 Tb1 Rb2 47.61(12) 3_775 3_775 ?
Cl2 Tb1 Rb2 127.75(13) 3_775 32 ?
Cl2 Tb1 Rb2 126.94(16) . 3_775 ?
Cl2 Tb1 Rb2 60.12(16) 2_755 32 ?
Cl2 Tb1 Rb2 117.67(16) . 2_755 ?
Cl2 Tb1 Rb2 117.67(16) 2_755 3_775 ?
Cl2 Tb1 Rb2 47.61(12) . . ?
Cl2 Tb1 Rb2 60.12(16) . 31_765 ?
Cl2 Tb1 Cl1 175.98(19) . 3_775 ?
Cl2 Tb1 Cl1 175.98(19) 3_775 2_755 ?
Cl2 Tb1 Cl1 91.8(2) 2_755 3_775 ?
Cl2 Tb1 Cl1 176.0(2) 2_755 . ?
Cl2 Tb1 Cl1 91.8(2) 3_775 . ?
Cl2 Tb1 Cl1 87.17(18) 3_775 3_775 ?
Cl2 Tb1 Cl1 87.17(18) 2_755 2_755 ?
Cl2 Tb1 Cl1 91.8(2) . 2_755 ?
Cl2 Tb1 Cl1 87.17(18) . . ?
Cl2 Tb1 Cl2 92.15(17) . 3_775 ?
Cl2 Tb1 Cl2 92.14(17) 3_775 2_755 ?
Cl2 Tb1 Cl2 92.15(17) . 2_755 ?
Cl5 Tb3 Cl5 176.2(2) 11_565 . ?
Cl5 Tb3 Cl6 88.79(14) 11_565 . ?
Cl5 Tb3 Cl6 88.80(15) . 11_565 ?
Cl5 Tb3 Cl6 88.43(15) . . ?
Cl5 Tb3 Cl6 88.43(14) 11_565 11_565 ?
Cl6 Tb3 Cl6 87.3(3) . 11_565 ?
Cl4 Tb3 Cl5 91.76(17) 11_565 . ?
Cl4 Tb3 Cl5 90.65(17) 11_565 11_565 ?
Cl4 Tb3 Cl5 91.77(17) . 11_565 ?
Cl4 Tb3 Cl5 90.65(17) . . ?
Cl4 Tb3 Cl6 85.46(17) . 11_565 ?
Cl4 Tb3 Cl6 85.46(17) 11_565 . ?
Cl4 Tb3 Cl6 172.75(18) . . ?
Cl4 Tb3 Cl6 172.74(18) 11_565 11_565 ?
Cl4 Tb3 Cl4 101.8(2) 11_565 . ?
Rb4 Rb3 Rb1 110.61(4) . 31_765 ?
Rb4 Rb3 Rb2 67.44(4) . 32 ?
Rb1 Rb3 Rb2 150.76(6) 31_765 32 ?
Cu1 Rb3 Rb4 123.40(4) 10 . ?
Cu1 Rb3 Rb1 122.57(5) 10 31_765 ?
Cu1 Rb3 Rb2 74.65(7) 10 32 ?
Cl5 Rb3 Rb4 47.79(9) 3_665 . ?
Cl5 Rb3 Rb4 115.32(9) 10 . ?
Cl5 Rb3 Rb1 114.32(9) 3_665 31_765 ?
Cl5 Rb3 Rb1 46.64(8) 10 31_765 ?
Cl5 Rb3 Rb2 86.54(9) 3_665 32 ?
Cl5 Rb3 Rb2 162.21(9) 10 32 ?
Cl5 Rb3 Cu1 90.82(10) 3_665 10 ?
Cl5 Rb3 Cu1 90.50(10) 10 10 ?
Cl5 Rb3 Cl5 83.89(12) 3_665 10 ?
Cl5 Rb3 Cl3 93.66(12) 3_665 . ?
Cl5 Rb3 Cl6 110.89(13) 10 12_655 ?
Cl5 Rb3 Cl6 111.09(13) 3_665 10 ?
Cl5 Rb3 Cl6 66.99(11) 3_665 12_655 ?
Cl5 Rb3 Cl6 66.59(11) 10 10 ?
Cl3 Rb3 Rb4 48.04(9) . . ?
Cl3 Rb3 Rb1 108.43(10) . 31_765 ?
Cl3 Rb3 Rb2 47.14(10) . 32 ?
Cl3 Rb3 Cu1 121.06(12) . 10 ?
Cl3 Rb3 Cl5 148.41(13) . 10 ?
Cl3 Rb3 Cl6 141.29(13) . 10 ?
Cl3 Rb3 Cl6 96.78(14) . 12_655 ?
Cl6 Rb3 Rb4 155.55(11) 10 . ?
Cl6 Rb3 Rb4 89.29(9) 12_655 . ?
Cl6 Rb3 Rb1 88.50(9) 10 31_765 ?
Cl6 Rb3 Rb1 154.42(11) 12_655 31_765 ?
Cl6 Rb3 Rb2 103.36(9) 10 32 ?
Cl6 Rb3 Rb2 51.39(10) 12_655 32 ?
Cl6 Rb3 Cu1 34.35(9) 10 10 ?
Cl6 Rb3 Cu1 34.32(9) 12_655 10 ?
Cl6 Rb3 Cl6 68.50(17) 10 12_655 ?
Cl4 Rb3 Rb4 55.24(11) . . ?
Cl4 Rb3 Rb1 55.37(11) . 31_765 ?
Cl4 Rb3 Rb2 115.61(12) . 32 ?
Cl4 Rb3 Cu1 162.60(13) . 10 ?
Cl4 Rb3 Cl5 76.43(13) . 3_665 ?
Cl4 Rb3 Cl5 76.58(13) . 10 ?
Cl4 Rb3 Cl3 72.26(14) . . ?
Cl4 Rb3 Cl6 140.83(14) . 10 ?
Cl4 Rb3 Cl6 141.13(14) . 12_655 ?
Cl1 Rb3 Rb4 111.46(14) 31_765 . ?
Cl1 Rb3 Rb1 46.68(10) 31_765 31_765 ?
Cl1 Rb3 Rb2 105.37(11) 31_765 32 ?
Cl1 Rb3 Cu1 118.22(14) 31_765 10 ?
Cl1 Rb3 Cl5 150.46(15) 31_765 3_665 ?
Cl1 Rb3 Cl5 90.16(13) 31_765 10 ?
Cl1 Rb3 Cl3 76.57(15) 31_765 . ?
Cl1 Rb3 Cl6 141.08(14) 31_765 12_655 ?
Cl1 Rb3 Cl6 92.67(16) 31_765 10 ?
Cl1 Rb3 Cl4 74.04(15) 31_765 . ?
Cl2 Rb3 Rb4 108.76(14) . . ?
Cl2 Rb3 Rb1 115.79(13) . 31_765 ?
Cl2 Rb3 Rb2 45.86(13) . 32 ?
Cl2 Rb3 Cu1 65.27(14) . 10 ?
Cl2 Rb3 Cl5 135.91(16) . 10 ?
Cl2 Rb3 Cl5 129.75(15) . 3_665 ?
Cl2 Rb3 Cl3 67.36(15) . . ?
Cl2 Rb3 Cl6 69.69(14) . 12_655 ?
Cl2 Rb3 Cl6 73.93(15) . 10 ?
Cl2 Rb3 Cl4 132.09(14) . . ?
Cl2 Rb3 Cl1 72.48(15) . 31_765 ?
Tb2 Rb4 Rb3 86.21(4) . . ?
Tb2 Rb4 Rb1 180.0 . 34_665 ?
Rb1 Rb4 Rb3 93.79(4) 34_665 . ?
Cl5 Rb4 Tb2 129.48(8) 3_665 . ?
Cl5 Rb4 Tb2 129.48(8) 2_655 . ?
Cl5 Rb4 Tb2 129.48(8) . . ?
Cl5 Rb4 Rb3 99.88(8) . . ?
Cl5 Rb4 Rb3 129.40(9) 2_655 . ?
Cl5 Rb4 Rb3 47.14(8) 3_665 . ?
Cl5 Rb4 Rb1 50.52(8) . 34_665 ?
Cl5 Rb4 Rb1 50.52(8) 3_665 34_665 ?
Cl5 Rb4 Rb1 50.52(8) 2_655 34_665 ?
Cl5 Rb4 Cl5 83.89(12) 2_655 3_665 ?
Cl5 Rb4 Cl5 83.89(12) . 3_665 ?
Cl5 Rb4 Cl5 83.89(12) . 2_655 ?
Cl5 Rb4 Cl3 92.37(10) . 2_655 ?
Cl5 Rb4 Cl3 125.13(11) 3_665 3_665 ?
Cl5 Rb4 Cl3 125.13(12) . . ?
Cl5 Rb4 Cl3 92.37(11) 3_665 . ?
Cl5 Rb4 Cl3 150.29(12) 3_665 2_655 ?
Cl5 Rb4 Cl3 150.29(12) 2_655 . ?
Cl5 Rb4 Cl3 125.13(12) 2_655 2_655 ?
Cl5 Rb4 Cl3 92.37(10) 2_655 3_665 ?
Cl5 Rb4 Cl3 150.29(12) . 3_665 ?
Cl5 Rb4 Cl4 62.16(10) . . ?
Cl5 Rb4 Cl4 69.15(11) . 2_655 ?
Cl5 Rb4 Cl4 137.83(13) 2_655 . ?
Cl5 Rb4 Cl4 69.15(11) 3_665 . ?
Cl5 Rb4 Cl4 62.16(10) 2_655 2_655 ?
Cl5 Rb4 Cl4 137.83(13) 3_665 2_655 ?
Cl5 Rb4 Cl4 69.15(11) 2_655 3_665 ?
Cl5 Rb4 Cl4 62.16(10) 3_665 3_665 ?
Cl5 Rb4 Cl4 137.84(13) . 3_665 ?
Cl3 Rb4 Tb2 38.86(8) 3_665 . ?
Cl3 Rb4 Tb2 38.86(8) 2_655 . ?
Cl3 Rb4 Tb2 38.86(8) . . ?
Cl3 Rb4 Rb3 105.24(10) 2_655 . ?
Cl3 Rb4 Rb3 105.08(10) 3_665 . ?
Cl3 Rb4 Rb3 47.35(8) . . ?
Cl3 Rb4 Rb1 141.14(8) . 34_665 ?
Cl3 Rb4 Rb1 141.14(8) 3_665 34_665 ?
Cl3 Rb4 Rb1 141.14(8) 2_655 34_665 ?
Cl3 Rb4 Cl3 65.83(12) 3_665 2_655 ?
Cl3 Rb4 Cl3 65.83(12) 3_665 . ?
Cl3 Rb4 Cl3 65.83(12) 2_655 . ?
Cl3 Rb4 Cl4 83.01(13) 3_665 2_655 ?
Cl3 Rb4 Cl4 129.56(12) 3_665 . ?
Cl3 Rb4 Cl4 83.01(12) . 3_665 ?
Cl3 Rb4 Cl4 65.47(11) 3_665 3_665 ?
Cl3 Rb4 Cl4 65.47(11) 2_655 2_655 ?
Cl3 Rb4 Cl4 129.56(12) 2_655 3_665 ?
Cl3 Rb4 Cl4 129.56(12) . 2_655 ?
Cl3 Rb4 Cl4 83.01(12) 2_655 . ?
Cl3 Rb4 Cl4 65.47(11) . . ?
Cl4 Rb4 Tb2 92.45(8) . . ?
Cl4 Rb4 Tb2 92.46(8) 3_665 . ?
Cl4 Rb4 Tb2 92.46(8) 2_655 . ?
Cl4 Rb4 Rb3 164.42(8) 2_655 . ?
Cl4 Rb4 Rb3 44.87(8) . . ?
Cl4 Rb4 Rb3 75.76(9) 3_665 . ?
Cl4 Rb4 Rb1 87.54(8) 2_655 34_665 ?
Cl4 Rb4 Rb1 87.55(8) . 34_665 ?
Cl4 Rb4 Rb1 87.54(8) 3_665 34_665 ?
Cl4 Rb4 Cl4 119.818(13) 3_665 2_655 ?
Cl4 Rb4 Cl4 119.818(13) 3_665 . ?
Cl4 Rb4 Cl4 119.818(13) 2_655 . ?
Tb1 Rb1 Rb3 85.01(4) . 31_765 ?
Tb1 Rb1 Rb4 180.0 . 28_665 ?
Rb4 Rb1 Rb3 94.99(4) 28_665 31_765 ?
Cl5 Rb1 Tb1 128.53(8) 30 . ?
Cl5 Rb1 Tb1 128.52(8) 28_665 . ?
Cl5 Rb1 Tb1 128.53(8) 29_655 . ?
Cl5 Rb1 Rb3 130.96(9) 30 31_765 ?
Cl5 Rb1 Rb3 47.48(8) 28_665 31_765 ?
Cl5 Rb1 Rb3 100.54(8) 29_655 31_765 ?
Cl5 Rb1 Rb4 51.47(8) 29_655 28_665 ?
Cl5 Rb1 Rb4 51.48(8) 28_665 28_665 ?
Cl5 Rb1 Rb4 51.47(8) 30 28_665 ?
Cl5 Rb1 Cl5 85.30(12) 30 29_655 ?
Cl5 Rb1 Cl5 85.30(12) 28_665 29_655 ?
Cl5 Rb1 Cl5 85.30(12) 28_665 30 ?
Cl5 Rb1 Cl4 62.88(10) 28_665 32 ?
Cl5 Rb1 Cl4 140.26(13) 30 31_765 ?
Cl5 Rb1 Cl4 62.88(10) 29_655 31_765 ?
Cl5 Rb1 Cl4 69.82(11) 28_665 31_765 ?
Cl5 Rb1 Cl4 62.88(10) 30 33_645 ?
Cl5 Rb1 Cl4 140.26(13) 29_655 32 ?
Cl5 Rb1 Cl4 69.82(11) 29_655 33_645 ?
Cl5 Rb1 Cl4 140.26(13) 28_665 33_645 ?
Cl5 Rb1 Cl4 69.82(11) 30 32 ?
Cl4 Rb1 Tb1 90.98(8) 31_765 . ?
Cl4 Rb1 Tb1 90.98(8) 32 . ?
Cl4 Rb1 Tb1 90.98(8) 33_645 . ?
Cl4 Rb1 Rb3 163.72(8) 33_645 31_765 ?
Cl4 Rb1 Rb3 75.95(8) 32 31_765 ?
Cl4 Rb1 Rb3 44.55(8) 31_765 31_765 ?
Cl4 Rb1 Rb4 89.02(8) 33_645 28_665 ?
Cl4 Rb1 Rb4 89.02(8) 31_765 28_665 ?
Cl4 Rb1 Rb4 89.02(8) 32 28_665 ?
Cl4 Rb1 Cl4 119.971(5) 32 33_645 ?
Cl4 Rb1 Cl4 119.973(5) 32 31_765 ?
Cl4 Rb1 Cl4 119.970(6) 31_765 33_645 ?
Cl1 Rb1 Tb1 40.06(9) 3_775 . ?
Cl1 Rb1 Tb1 40.06(9) 2_755 . ?
Cl1 Rb1 Tb1 40.06(9) . . ?
Cl1 Rb1 Rb3 107.55(12) 2_755 31_765 ?
Cl1 Rb1 Rb3 101.77(12) 3_775 31_765 ?
Cl1 Rb1 Rb3 45.15(8) . 31_765 ?
Cl1 Rb1 Rb4 139.94(9) 3_775 28_665 ?
Cl1 Rb1 Rb4 139.94(9) 2_755 28_665 ?
Cl1 Rb1 Rb4 139.94(9) . 28_665 ?
Cl1 Rb1 Cl5 127.10(14) . 29_655 ?
Cl1 Rb1 Cl5 146.67(14) 3_775 28_665 ?
Cl1 Rb1 Cl5 89.51(11) . 28_665 ?
Cl1 Rb1 Cl5 127.10(13) 2_755 28_665 ?
Cl1 Rb1 Cl5 89.51(11) 2_755 30 ?
Cl1 Rb1 Cl5 127.10(13) 3_775 30 ?
Cl1 Rb1 Cl5 146.68(14) 2_755 29_655 ?
Cl1 Rb1 Cl5 89.51(11) 3_775 29_655 ?
Cl1 Rb1 Cl5 146.67(14) . 30 ?
Cl1 Rb1 Cl4 65.98(12) . 31_765 ?
Cl1 Rb1 Cl4 78.53(15) 2_755 33_645 ?
Cl1 Rb1 Cl4 130.18(13) . 33_645 ?
Cl1 Rb1 Cl4 65.98(12) 3_775 33_645 ?
Cl1 Rb1 Cl4 78.53(15) . 32 ?
Cl1 Rb1 Cl4 130.18(13) 3_775 32 ?
Cl1 Rb1 Cl4 65.98(12) 2_755 32 ?
Cl1 Rb1 Cl4 130.18(13) 2_755 31_765 ?
Cl1 Rb1 Cl4 78.53(15) 3_775 31_765 ?
Cl1 Rb1 Cl1 67.74(14) 2_755 3_775 ?
Cl1 Rb1 Cl1 67.74(14) 3_775 . ?
Cl1 Rb1 Cl1 67.74(14) 2_755 . ?
Tb1 Rb2 Tb2 113.08(4) . . ?
Cl3 Rb2 Tb2 35.83(7) 33_545 . ?
Cl3 Rb2 Tb2 35.82(7) . . ?
Cl3 Rb2 Tb2 35.60(6) 32 . ?
Cl3 Rb2 Tb1 93.80(9) . . ?
Cl3 Rb2 Tb1 90.88(7) 32 . ?
Cl3 Rb2 Tb1 147.90(9) 33_545 . ?
Cl3 Rb2 Cl3 63.63(14) . 33_545 ?
Cl3 Rb2 Cl3 59.91(13) . 32 ?
Cl3 Rb2 Cl3 58.58(13) 33_545 32 ?
Cl3 Rb2 Cl6 149.31(12) . 28_665 ?
Cl3 Rb2 Cl6 87.07(11) 33_545 28_665 ?
Cl3 Rb2 Cl1 100.55(14) 33_545 31_765 ?
Cl3 Rb2 Cl1 68.58(12) . 31_765 ?
Cl3 Rb2 Cl2 121.31(11) 33_545 31_765 ?
Cl3 Rb2 Cl2 124.82(12) . 31_765 ?
Cl6 Rb2 Tb2 120.21(9) 28_665 . ?
Cl6 Rb2 Tb1 116.76(9) 28_665 . ?
Cl6 Rb2 Cl3 113.61(11) 28_665 32 ?
Cl6 Rb2 Cl2 61.80(11) 28_665 31_765 ?
Cl4 Rb2 Tb2 91.82(11) 32 . ?
Cl4 Rb2 Tb1 89.46(11) 32 . ?
Cl4 Rb2 Cl3 63.09(12) 32 32 ?
Cl4 Rb2 Cl3 85.18(14) 32 33_545 ?
Cl4 Rb2 Cl3 122.94(13) 32 . ?
Cl4 Rb2 Cl6 58.69(11) 32 28_665 ?
Cl4 Rb2 Cl1 168.43(14) 32 31_765 ?
Cl4 Rb2 Cl2 112.11(12) 32 31_765 ?
Cl4 Rb2 Cl2 112.43(13) 32 33_545 ?
Cl1 Rb2 Tb2 98.70(10) 31_765 . ?
Cl1 Rb2 Tb2 147.90(9) . . ?
Cl1 Rb2 Tb1 90.80(11) 31_765 . ?
Cl1 Rb2 Tb1 36.05(8) . . ?
Cl1 Rb2 Cl3 117.44(11) . 32 ?
Cl1 Rb2 Cl3 128.46(12) 31_765 32 ?
Cl1 Rb2 Cl3 166.39(14) . 33_545 ?
Cl1 Rb2 Cl3 127.37(12) . . ?
Cl1 Rb2 Cl6 83.02(12) . 28_665 ?
Cl1 Rb2 Cl6 111.23(11) 31_765 28_665 ?
Cl1 Rb2 Cl4 81.71(14) . 32 ?
Cl1 Rb2 Cl1 91.75(13) . 31_765 ?
Cl1 Rb2 Cl2 56.33(11) 31_765 31_765 ?
Cl1 Rb2 Cl2 120.55(13) . 33_545 ?
Cl1 Rb2 Cl2 61.38(12) . 31_765 ?
Cl2 Rb2 Tb2 91.04(10) 33_545 . ?
Cl2 Rb2 Tb2 147.29(9) 31_765 . ?
Cl2 Rb2 Tb2 93.13(11) . . ?
Cl2 Rb2 Tb1 147.31(10) 33_545 . ?
Cl2 Rb2 Tb1 89.99(9) 31_765 . ?
Cl2 Rb2 Tb1 34.86(8) . . ?
Cl2 Rb2 Cl3 89.67(15) . 32 ?
Cl2 Rb2 Cl3 175.11(12) 31_765 32 ?
Cl2 Rb2 Cl3 63.38(12) . . ?
Cl2 Rb2 Cl3 61.68(11) 33_545 33_545 ?
Cl2 Rb2 Cl3 126.67(13) . 33_545 ?
Cl2 Rb2 Cl3 120.26(11) 33_545 32 ?
Cl2 Rb2 Cl3 93.88(13) 33_545 . ?
Cl2 Rb2 Cl6 146.18(14) . 28_665 ?
Cl2 Rb2 Cl6 62.29(12) 33_545 28_665 ?
Cl2 Rb2 Cl4 119.56(14) . 32 ?
Cl2 Rb2 Cl1 64.90(14) . 31_765 ?
Cl2 Rb2 Cl1 64.06(13) . . ?
Cl2 Rb2 Cl1 62.87(12) 33_545 31_765 ?
Cl2 Rb2 Cl2 127.63(10) . 33_545 ?
Cl2 Rb2 Cl2 93.79(14) . 31_765 ?
Cl2 Rb2 Cl2 59.88(16) 33_545 31_765 ?
Rb3 Cu1 Rb3 117.48(5) 10_445 11_465 ?
Rb3 Cu1 Rb3 117.48(5) 10_445 12_665 ?
Rb3 Cu1 Rb3 117.48(5) 12_665 11_465 ?
Cl6 Cu1 Rb3 169.4(3) 2_665 10_445 ?
Cl6 Cu1 Rb3 60.45(13) 2_665 11_465 ?
Cl6 Cu1 Rb3 169.4(3) . 11_465 ?
Cl6 Cu1 Rb3 60.45(13) . 12_665 ?
Cl6 Cu1 Rb3 169.4(3) 3_565 12_665 ?
Cl6 Cu1 Rb3 59.92(13) 2_665 12_665 ?
Cl6 Cu1 Rb3 59.92(14) . 10_445 ?
Cl6 Cu1 Rb3 59.92(13) 3_565 11_465 ?
Cl6 Cu1 Rb3 60.45(13) 3_565 10_445 ?
Cl6 Cu1 Cl6 119.94(2) 2_665 3_565 ?
Cl6 Cu1 Cl6 119.94(2) 3_565 . ?
Cl6 Cu1 Cl6 119.94(2) 2_665 . ?
Tb3 Cl5 Rb3 103.87(13) . 10_445 ?
Tb3 Cl5 Rb3 104.20(14) . 2_655 ?
Tb3 Cl5 Rb4 107.69(14) . . ?
Tb3 Cl5 Rb1 107.58(14) . 34_665 ?
Rb3 Cl5 Rb3 94.15(12) 2_655 10_445 ?
Rb3 Cl5 Rb4 85.07(11) 2_655 . ?
Rb4 Cl5 Rb3 147.63(14) . 10_445 ?
Rb1 Cl5 Rb3 85.89(11) 34_665 10_445 ?
Rb1 Cl5 Rb3 147.24(14) 34_665 2_655 ?
Rb1 Cl5 Rb4 78.00(11) 34_665 . ?
Tb2 Cl3 Rb3 171.73(19) . . ?
Tb2 Cl3 Rb4 87.12(12) . . ?
Tb2 Cl3 Rb2 92.05(14) . . ?
Tb2 Cl3 Rb2 83.79(13) . 33_545 ?
Tb2 Cl3 Rb2 91.56(14) . 32 ?
Rb3 Cl3 Rb4 84.61(12) . . ?
Rb3 Cl3 Rb2 96.50(13) . 33_545 ?
Rb3 Cl3 Rb2 96.20(11) . . ?
Rb3 Cl3 Rb2 89.32(12) . 32 ?
Rb4 Cl3 Rb2 90.78(12) . 33_545 ?
Rb4 Cl3 Rb2 173.91(18) . . ?
Rb4 Cl3 Rb2 97.39(13) . 32 ?
Rb2 Cl3 Rb2 88.66(11) . 32 ?
Rb2 Cl3 Rb2 170.39(16) 32 33_545 ?
Rb2 Cl3 Rb2 83.13(11) . 33_545 ?
Tb3 Cl6 Rb3 100.71(14) . 10_445 ?
Tb3 Cl6 Rb3 99.63(14) . 12_665 ?
Tb3 Cl6 Rb2 101.33(15) . 34_665 ?
Rb3 Cl6 Rb3 158.32(17) 10_445 12_665 ?
Rb3 Cl6 Rb2 83.62(12) 12_665 34_665 ?
Rb3 Cl6 Rb2 85.09(13) 10_445 34_665 ?
Cu1 Cl6 Tb3 135.0(3) . . ?
Cu1 Cl6 Rb3 85.73(15) . 10_445 ?
Cu1 Cl6 Rb3 85.23(15) . 12_665 ?
Cu1 Cl6 Rb2 123.7(2) . 34_665 ?
Tb3 Cl4 Rb3 137.3(2) . . ?
Tb3 Cl4 Rb4 98.49(17) . . ?
Tb3 Cl4 Rb1 96.60(16) . 31_765 ?
Tb3 Cl4 Rb2 114.52(18) . 33_545 ?
Rb3 Cl4 Rb4 79.89(12) . . ?
Rb3 Cl4 Rb1 80.08(12) . 31_765 ?
Rb3 Cl4 Rb2 108.19(13) . 33_545 ?
Rb4 Cl4 Rb1 159.96(15) . 31_765 ?
Rb2 Cl4 Rb4 92.00(14) 33_545 . ?
Rb2 Cl4 Rb1 93.66(14) 33_545 31_765 ?
Tb1 Cl1 Rb3 170.8(2) . 31_765 ?
Tb1 Cl1 Rb1 85.99(14) . . ?
Tb1 Cl1 Rb2 93.68(16) . . ?
Tb1 Cl1 Rb2 89.08(15) . 31_765 ?
Rb3 Cl1 Rb1 88.16(13) 31_765 . ?
Rb3 Cl1 Rb2 95.22(13) 31_765 31_765 ?
Rb3 Cl1 Rb2 94.56(16) 31_765 . ?
Rb1 Cl1 Rb2 103.33(18) . . ?
Rb1 Cl1 Rb2 167.7(2) . 31_765 ?
Rb2 Cl1 Rb2 88.25(13) . 31_765 ?
Tb1 Cl2 Rb3 156.5(2) . . ?
Tb1 Cl2 Rb2 85.08(16) . 31_765 ?
Tb1 Cl2 Rb2 94.61(18) . 32 ?
Tb1 Cl2 Rb2 97.53(15) . . ?
Rb3 Cl2 Rb2 93.51(14) . 32 ?
Rb3 Cl2 Rb2 87.03(15) . 31_765 ?
Rb3 Cl2 Rb2 103.99(15) . . ?
Rb2 Cl2 Rb2 93.17(17) . 32 ?
Rb2 Cl2 Rb2 86.21(14) . 31_765 ?
Rb2 Cl2 Rb2 179.26(18) 32 31_765 ?

_olex2_submission_special_instructions 'No special instructions were received'
