# Electronic Supplementary Material (ESI) for Chemical Science.
# This journal is © The Royal Society of Chemistry 2022

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_Complex_1
_database_code_depnum_ccdc_archive 'CCDC 2150613'
loop_
_audit_author_name
_audit_author_address
'Guang Wu'
;UCSB
United States of America
;
_audit_update_record             
;
2022-02-07 deposited with the CCDC.	2022-04-11 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2014/7
_shelx_SHELXL_version_number     2014/7
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C70 H175 Ni30 O P11 S16'
_chemical_formula_weight         3648.02

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ni Ni 0.3393 1.1124 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_H-M_alt        'P 21/n'
_space_group_name_Hall           '-P 2yn'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'

_cell_length_a                   19.050(6)
_cell_length_b                   33.432(10)
_cell_length_c                   21.256(6)
_cell_angle_alpha                90
_cell_angle_beta                 115.771(4)
_cell_angle_gamma                90
_cell_volume                     12191(6)
_cell_formula_units_Z            4
_cell_measurement_temperature    100(2)
_cell_measurement_reflns_used    9942
_cell_measurement_theta_min      2.18
_cell_measurement_theta_max      25.93

_exptl_crystal_description       plate
_exptl_crystal_colour            black
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    1.988
_exptl_crystal_F_000             7456
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          0.25
_exptl_crystal_size_mid          0.20
_exptl_crystal_size_min          0.05
_exptl_absorpt_coefficient_mu    4.957
_shelx_estimated_absorpt_T_min   0.437
_shelx_estimated_absorpt_T_max   0.523
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_correction_T_min  0.5634
_exptl_absorpt_correction_T_max  0.7454
_exptl_absorpt_process_details   sadabs
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      100(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_source                   ?
_diffrn_measurement_device_type  'Bruker Kappa APEX II'
_diffrn_measurement_method       ?
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            68292
_diffrn_reflns_av_unetI/netI     0.0650
_diffrn_reflns_av_R_equivalents  0.0488
_diffrn_reflns_limit_h_min       -23
_diffrn_reflns_limit_h_max       23
_diffrn_reflns_limit_k_min       -41
_diffrn_reflns_limit_k_max       23
_diffrn_reflns_limit_l_min       -23
_diffrn_reflns_limit_l_max       26
_diffrn_reflns_theta_min         1.218
_diffrn_reflns_theta_max         26.292
_diffrn_reflns_theta_full        25.242
_diffrn_measured_fraction_theta_max 0.964
_diffrn_measured_fraction_theta_full 0.998
_diffrn_reflns_Laue_measured_fraction_max 0.964
_diffrn_reflns_Laue_measured_fraction_full 0.998
_diffrn_reflns_point_group_measured_fraction_max 0.964
_diffrn_reflns_point_group_measured_fraction_full 0.998
_reflns_number_total             23848
_reflns_number_gt                15676
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       ?
_computing_cell_refinement       ?
_computing_data_reduction        ?
_computing_structure_solution    ?
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_molecular_graphics    ?
_computing_publication_material  ?
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.1075P)²+300.0000P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_number_reflns         23848
_refine_ls_number_parameters     769
_refine_ls_number_restraints     1942
_refine_ls_R_factor_all          0.1453
_refine_ls_R_factor_gt           0.0948
_refine_ls_wR_factor_ref         0.2869
_refine_ls_wR_factor_gt          0.2530
_refine_ls_goodness_of_fit_ref   1.173
_refine_ls_restrained_S_all      1.169
_refine_ls_shift/su_max          0.005
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C 0.5208(7) 0.3249(5) 0.4393(13) 0.1055(17) Uani 1 1 d D . . . .
H1A H 0.5184 0.3263 0.3919 0.127 Uiso 1 1 calc R U . . .
H1B H 0.5580 0.3456 0.4683 0.127 Uiso 1 1 calc R U . . .
C2 C 0.5508(13) 0.2849(7) 0.4697(18) 0.137(2) Uani 1 1 d D . . . .
H2A H 0.5652 0.2852 0.5199 0.205 Uiso 1 1 calc R U . . .
H2B H 0.5968 0.2783 0.4623 0.205 Uiso 1 1 calc R U . . .
H2C H 0.5103 0.2647 0.4469 0.205 Uiso 1 1 calc R U . . .
C3 C 0.3632(11) 0.3033(5) 0.3646(10) 0.1055(17) Uani 1 1 d D . . . .
H3A H 0.3690 0.2760 0.3840 0.127 Uiso 1 1 calc R U . . .
H3B H 0.3084 0.3115 0.3498 0.127 Uiso 1 1 calc R U . . .
C4 C 0.378(2) 0.3018(10) 0.3018(9) 0.137(2) Uani 1 1 d D . . . .
H4A H 0.4232 0.2845 0.3111 0.205 Uiso 1 1 calc R U . . .
H4B H 0.3890 0.3288 0.2904 0.205 Uiso 1 1 calc R U . . .
H4C H 0.3322 0.2910 0.2624 0.205 Uiso 1 1 calc R U . . .
C5 C 0.4063(11) 0.3843(4) 0.3882(12) 0.1055(17) Uani 1 1 d D . . . .
H5A H 0.4273 0.4064 0.4223 0.127 Uiso 1 1 calc R U . . .
H5B H 0.4317 0.3851 0.3563 0.127 Uiso 1 1 calc R U . . .
C6 C 0.3107(15) 0.3887(9) 0.3435(16) 0.137(2) Uani 1 1 d D . . . .
H6A H 0.2985 0.4142 0.3183 0.205 Uiso 1 1 calc R U . . .
H6B H 0.2908 0.3666 0.3100 0.205 Uiso 1 1 calc R U . . .
H6C H 0.2864 0.3878 0.3757 0.205 Uiso 1 1 calc R U . . .
C7 C 0.6868(14) 0.4150(3) 0.7125(11) 0.1055(17) Uani 1 1 d D . . . .
H7A H 0.6558 0.4275 0.6663 0.127 Uiso 1 1 calc R U . . .
H7B H 0.6639 0.4241 0.7438 0.127 Uiso 1 1 calc R U . . .
C8 C 0.7630(17) 0.4310(6) 0.7386(18) 0.137(2) Uani 1 1 d D . . . .
H8A H 0.7975 0.4161 0.7803 0.205 Uiso 1 1 calc R U . . .
H8B H 0.7620 0.4592 0.7507 0.205 Uiso 1 1 calc R U . . .
H8C H 0.7822 0.4288 0.7028 0.205 Uiso 1 1 calc R U . . .
C9 C 0.7227(13) 0.3491(7) 0.6496(10) 0.1055(17) Uani 1 1 d D . . . .
H9A H 0.7785 0.3562 0.6756 0.127 Uiso 1 1 calc R U . . .
H9B H 0.7193 0.3199 0.6408 0.127 Uiso 1 1 calc R U . . .
C10 C 0.687(2) 0.3720(11) 0.5779(11) 0.137(2) Uani 1 1 d D . . . .
H10A H 0.7149 0.3649 0.5506 0.205 Uiso 1 1 calc R U . . .
H10B H 0.6316 0.3647 0.5519 0.205 Uiso 1 1 calc R U . . .
H10C H 0.6907 0.4009 0.5866 0.205 Uiso 1 1 calc R U . . .
C11 C 0.7399(12) 0.3434(6) 0.7874(6) 0.1055(17) Uani 1 1 d D . . . .
H11A H 0.7841 0.3625 0.8060 0.127 Uiso 1 1 calc R U . . .
H11B H 0.7133 0.3451 0.8183 0.127 Uiso 1 1 calc R U . . .
C12 C 0.7714(17) 0.3047(8) 0.7943(15) 0.137(2) Uani 1 1 d D . . . .
H12A H 0.7915 0.3008 0.7595 0.205 Uiso 1 1 calc R U . . .
H12B H 0.7306 0.2849 0.7871 0.205 Uiso 1 1 calc R U . . .
H12C H 0.8139 0.3015 0.8413 0.205 Uiso 1 1 calc R U . . .
C13 C -0.0547(12) 0.3090(4) 0.6867(10) 0.1055(17) Uani 1 1 d D . . . .
H13A H -0.0319 0.2924 0.7294 0.127 Uiso 1 1 calc R U . . .
H13B H -0.1052 0.3193 0.6825 0.127 Uiso 1 1 calc R U . . .
C14 C -0.0697(17) 0.2831(6) 0.6259(14) 0.137(2) Uani 1 1 d D . . . .
H14A H -0.1130 0.2650 0.6185 0.205 Uiso 1 1 calc R U . . .
H14B H -0.0229 0.2674 0.6347 0.205 Uiso 1 1 calc R U . . .
H14C H -0.0831 0.2997 0.5843 0.205 Uiso 1 1 calc R U . . .
C15 C -0.0409(10) 0.3763(6) 0.6143(7) 0.1055(17) Uani 1 1 d D . . . .
H15A H -0.0108 0.4004 0.6142 0.127 Uiso 1 1 calc R U . . .
H15B H -0.0414 0.3582 0.5772 0.127 Uiso 1 1 calc R U . . .
C16 C -0.1220(11) 0.3886(10) 0.5962(13) 0.137(2) Uani 1 1 d D . . . .
H16A H -0.1226 0.4066 0.6324 0.205 Uiso 1 1 calc R U . . .
H16B H -0.1535 0.3648 0.5932 0.205 Uiso 1 1 calc R U . . .
H16C H -0.1436 0.4024 0.5511 0.205 Uiso 1 1 calc R U . . .
C17 C -0.0149(13) 0.3832(4) 0.7544(9) 0.1055(17) Uani 1 1 d D . . . .
H17A H -0.0711 0.3801 0.7417 0.127 Uiso 1 1 calc R U . . .
H17B H 0.0143 0.3738 0.8032 0.127 Uiso 1 1 calc R U . . .
C18 C 0.002(2) 0.4263(4) 0.7518(16) 0.137(2) Uani 1 1 d D . . . .
H18A H 0.0440 0.4294 0.7377 0.205 Uiso 1 1 calc R U . . .
H18B H 0.0171 0.4382 0.7980 0.205 Uiso 1 1 calc R U . . .
H18C H -0.0452 0.4397 0.7177 0.205 Uiso 1 1 calc R U . . .
C19 C 0.2983(10) 0.4122(3) 0.9885(10) 0.1055(17) Uani 1 1 d D . . . .
H19A H 0.2947 0.4144 1.0334 0.127 Uiso 1 1 calc R U . . .
H19B H 0.3541 0.4142 0.9988 0.127 Uiso 1 1 calc R U . . .
C20 C 0.2571(18) 0.4466(3) 0.9445(15) 0.137(2) Uani 1 1 d D . . . .
H20A H 0.2730 0.4497 0.9067 0.205 Uiso 1 1 calc R U . . .
H20B H 0.2701 0.4709 0.9730 0.205 Uiso 1 1 calc R U . . .
H20C H 0.2007 0.4419 0.9245 0.205 Uiso 1 1 calc R U . . .
C21 C 0.1715(7) 0.3601(5) 0.9574(12) 0.1055(17) Uani 1 1 d D . . . .
H21A H 0.1812 0.3643 1.0066 0.127 Uiso 1 1 calc R U . . .
H21B H 0.1377 0.3822 0.9295 0.127 Uiso 1 1 calc R U . . .
C22 C 0.1287(12) 0.3218(7) 0.9327(18) 0.137(2) Uani 1 1 d D . . . .
H22A H 0.0798 0.3228 0.9374 0.205 Uiso 1 1 calc R U . . .
H22B H 0.1173 0.3176 0.8835 0.205 Uiso 1 1 calc R U . . .
H22C H 0.1609 0.2996 0.9608 0.205 Uiso 1 1 calc R U . . .
C23 C 0.3249(10) 0.3312(5) 1.0245(8) 0.1055(17) Uani 1 1 d D . . . .
H23A H 0.3083 0.3031 1.0119 0.127 Uiso 1 1 calc R U . . .
H23B H 0.3793 0.3334 1.0306 0.127 Uiso 1 1 calc R U . . .
C24 C 0.3236(18) 0.3401(10) 1.0921(7) 0.137(2) Uani 1 1 d D . . . .
H24A H 0.3442 0.3172 1.1235 0.205 Uiso 1 1 calc R U . . .
H24B H 0.2699 0.3454 1.0845 0.205 Uiso 1 1 calc R U . . .
H24C H 0.3559 0.3637 1.1131 0.205 Uiso 1 1 calc R U . . .
C25 C 0.4837(9) 0.1672(6) 0.6555(9) 0.1055(17) Uani 1 1 d D . . . .
H25A H 0.5167 0.1437 0.6591 0.127 Uiso 1 1 calc R U . . .
H25B H 0.4941 0.1753 0.7035 0.127 Uiso 1 1 calc R U . . .
C26 C 0.4014(11) 0.1552(8) 0.6182(15) 0.137(2) Uani 1 1 d D . . . .
H26A H 0.3747 0.1727 0.5778 0.205 Uiso 1 1 calc R U . . .
H26B H 0.3763 0.1574 0.6497 0.205 Uiso 1 1 calc R U . . .
H26C H 0.3984 0.1275 0.6023 0.205 Uiso 1 1 calc R U . . .
C27 C 0.6200(6) 0.2046(7) 0.6672(8) 0.1055(17) Uani 1 1 d D . . . .
H27A H 0.6339 0.2155 0.7144 0.127 Uiso 1 1 calc R U . . .
H27B H 0.6354 0.1760 0.6727 0.127 Uiso 1 1 calc R U . . .
C28 C 0.6654(8) 0.2259(10) 0.6364(15) 0.137(2) Uani 1 1 d D . . . .
H28A H 0.6382 0.2242 0.5854 0.205 Uiso 1 1 calc R U . . .
H28B H 0.7171 0.2137 0.6527 0.205 Uiso 1 1 calc R U . . .
H28C H 0.6709 0.2541 0.6507 0.205 Uiso 1 1 calc R U . . .
C29 C 0.5039(11) 0.1849(6) 0.5350(6) 0.1055(17) Uani 1 1 d D . . . .
H29A H 0.5494 0.1929 0.5271 0.127 Uiso 1 1 calc R U . . .
H29B H 0.5065 0.1555 0.5415 0.127 Uiso 1 1 calc R U . . .
C30 C 0.4332(15) 0.1942(10) 0.4716(6) 0.137(2) Uani 1 1 d D . . . .
H30A H 0.4359 0.1813 0.4314 0.205 Uiso 1 1 calc R U . . .
H30B H 0.4290 0.2232 0.4645 0.205 Uiso 1 1 calc R U . . .
H30C H 0.3875 0.1843 0.4767 0.205 Uiso 1 1 calc R U . . .
C31 C 0.2287(12) 0.2103(5) 0.9047(5) 0.1055(17) Uani 1 1 d D . . . .
H31A H 0.2815 0.2220 0.9290 0.127 Uiso 1 1 calc R U . . .
H31B H 0.1927 0.2272 0.9156 0.127 Uiso 1 1 calc R U . . .
C32 C 0.230(2) 0.1699(7) 0.9331(10) 0.137(2) Uani 1 1 d D . . . .
H32A H 0.2464 0.1717 0.9836 0.205 Uiso 1 1 calc R U . . .
H32B H 0.1776 0.1582 0.9105 0.205 Uiso 1 1 calc R U . . .
H32C H 0.2665 0.1530 0.9240 0.205 Uiso 1 1 calc R U . . .
C33 C 0.2542(9) 0.1706(5) 0.8007(9) 0.1055(17) Uani 1 1 d D . . . .
H33A H 0.3101 0.1780 0.8218 0.127 Uiso 1 1 calc R U . . .
H33B H 0.2484 0.1476 0.8274 0.127 Uiso 1 1 calc R U . . .
C34 C 0.2319(18) 0.1575(8) 0.7284(11) 0.137(2) Uani 1 1 d D . . . .
H34A H 0.1775 0.1486 0.7075 0.205 Uiso 1 1 calc R U . . .
H34B H 0.2656 0.1353 0.7284 0.205 Uiso 1 1 calc R U . . .
H34C H 0.2378 0.1798 0.7013 0.205 Uiso 1 1 calc R U . . .
C35 C 0.1020(6) 0.1918(6) 0.7770(11) 0.1055(17) Uani 1 1 d D . . . .
H35A H 0.0887 0.1806 0.7301 0.127 Uiso 1 1 calc R U . . .
H35B H 0.1025 0.1692 0.8075 0.127 Uiso 1 1 calc R U . . .
C36 C 0.0397(7) 0.2197(8) 0.7715(18) 0.137(2) Uani 1 1 d D . . . .
H36A H -0.0081 0.2046 0.7616 0.205 Uiso 1 1 calc R U . . .
H36B H 0.0301 0.2387 0.7335 0.205 Uiso 1 1 calc R U . . .
H36C H 0.0557 0.2342 0.8156 0.205 Uiso 1 1 calc R U . . .
C37 C 0.0825(11) 0.2933(5) 0.3587(11) 0.1055(17) Uani 1 1 d D . . . .
H37A H 0.0786 0.2664 0.3767 0.127 Uiso 1 1 calc R U . . .
H37B H 0.0407 0.2952 0.3105 0.127 Uiso 1 1 calc R U . . .
C38 C 0.1582(14) 0.2961(9) 0.3559(16) 0.137(2) Uani 1 1 d D . . . .
H38A H 0.1577 0.3191 0.3271 0.205 Uiso 1 1 calc R U . . .
H38B H 0.1675 0.2716 0.3353 0.205 Uiso 1 1 calc R U . . .
H38C H 0.1998 0.2996 0.4032 0.205 Uiso 1 1 calc R U . . .
C39 C 0.0137(9) 0.3689(5) 0.3468(10) 0.1055(17) Uani 1 1 d D . . . .
H39A H -0.0221 0.3555 0.3030 0.127 Uiso 1 1 calc R U . . .
H39B H -0.0188 0.3848 0.3635 0.127 Uiso 1 1 calc R U . . .
C40 C 0.0630(15) 0.3965(7) 0.3305(16) 0.137(2) Uani 1 1 d D . . . .
H40A H 0.0747 0.4200 0.3610 0.205 Uiso 1 1 calc R U . . .
H40B H 0.0356 0.4050 0.2816 0.205 Uiso 1 1 calc R U . . .
H40C H 0.1117 0.3831 0.3380 0.205 Uiso 1 1 calc R U . . .
C41 C -0.0197(8) 0.3083(5) 0.4194(10) 0.1055(17) Uani 1 1 d D . . . .
H41A H -0.0510 0.3303 0.4256 0.127 Uiso 1 1 calc R U . . .
H41B H -0.0527 0.2949 0.3748 0.127 Uiso 1 1 calc R U . . .
C42 C -0.0029(14) 0.2797(9) 0.4759(15) 0.137(2) Uani 1 1 d D . . . .
H42A H 0.0272 0.2573 0.4703 0.205 Uiso 1 1 calc R U . . .
H42B H -0.0519 0.2696 0.4744 0.205 Uiso 1 1 calc R U . . .
H42C H 0.0274 0.2928 0.5208 0.205 Uiso 1 1 calc R U . . .
C43 C 0.6565(12) 0.3977(4) 1.0445(9) 0.1055(17) Uani 1 1 d D . . . .
H43A H 0.6204 0.4001 1.0666 0.127 Uiso 1 1 calc R U . . .
H43B H 0.7087 0.3914 1.0819 0.127 Uiso 1 1 calc R U . . .
C44 C 0.661(2) 0.4370(4) 1.0142(14) 0.137(2) Uani 1 1 d D . . . .
H44A H 0.7038 0.4368 1.0008 0.205 Uiso 1 1 calc R U . . .
H44B H 0.6693 0.4580 1.0489 0.205 Uiso 1 1 calc R U . . .
H44C H 0.6116 0.4420 0.9729 0.205 Uiso 1 1 calc R U . . .
C45 C 0.6194(11) 0.3159(4) 1.0388(10) 0.1055(17) Uani 1 1 d D . . . .
H45A H 0.6219 0.2902 1.0168 0.127 Uiso 1 1 calc R U . . .
H45B H 0.6659 0.3174 1.0844 0.127 Uiso 1 1 calc R U . . .
C46 C 0.5493(15) 0.3155(9) 1.0518(17) 0.137(2) Uani 1 1 d D . . . .
H46A H 0.5545 0.3359 1.0867 0.205 Uiso 1 1 calc R U . . .
H46B H 0.5437 0.2891 1.0692 0.205 Uiso 1 1 calc R U . . .
H46C H 0.5031 0.3213 1.0082 0.205 Uiso 1 1 calc R U . . .
C47 C 0.7139(9) 0.3435(5) 0.9771(12) 0.1055(17) Uani 1 1 d D . . . .
H47A H 0.7253 0.3651 0.9511 0.127 Uiso 1 1 calc R U . . .
H47B H 0.7573 0.3428 1.0247 0.127 Uiso 1 1 calc R U . . .
C48 C 0.7126(14) 0.3051(7) 0.9424(17) 0.137(2) Uani 1 1 d D . . . .
H48A H 0.6915 0.2842 0.9616 0.205 Uiso 1 1 calc R U . . .
H48B H 0.7657 0.2979 0.9504 0.205 Uiso 1 1 calc R U . . .
H48C H 0.6797 0.3076 0.8921 0.205 Uiso 1 1 calc R U . . .
C49 C 0.3947(10) 0.4738(5) 0.4658(10) 0.1055(17) Uani 1 1 d D . . . .
H49A H 0.4491 0.4717 0.5022 0.127 Uiso 1 1 calc R U . . .
H49B H 0.3751 0.4462 0.4524 0.127 Uiso 1 1 calc R U . . .
C50 C 0.3957(19) 0.4937(9) 0.4042(13) 0.137(2) Uani 1 1 d D . . . .
H50A H 0.3480 0.5095 0.3805 0.205 Uiso 1 1 calc R U . . .
H50B H 0.3985 0.4734 0.3720 0.205 Uiso 1 1 calc R U . . .
H50C H 0.4412 0.5113 0.4191 0.205 Uiso 1 1 calc R U . . .
C51 C 0.3861(9) 0.5454(4) 0.5315(12) 0.1055(17) Uani 1 1 d D . . . .
H51A H 0.4393 0.5405 0.5687 0.127 Uiso 1 1 calc R U . . .
H51B H 0.3916 0.5575 0.4914 0.127 Uiso 1 1 calc R U . . .
C52 C 0.3467(17) 0.5745(5) 0.5579(17) 0.137(2) Uani 1 1 d D . . . .
H52A H 0.2956 0.5813 0.5204 0.205 Uiso 1 1 calc R U . . .
H52B H 0.3786 0.5987 0.5736 0.205 Uiso 1 1 calc R U . . .
H52C H 0.3400 0.5626 0.5971 0.205 Uiso 1 1 calc R U . . .
C53 C 0.2503(8) 0.5119(6) 0.4272(8) 0.1055(17) Uani 1 1 d D . . . .
H53A H 0.2190 0.5294 0.4429 0.127 Uiso 1 1 calc R U . . .
H53B H 0.2669 0.5284 0.3975 0.127 Uiso 1 1 calc R U . . .
C54 C 0.1981(18) 0.4804(8) 0.3827(16) 0.137(2) Uani 1 1 d D . . . .
H54A H 0.2264 0.4637 0.3636 0.205 Uiso 1 1 calc R U . . .
H54B H 0.1532 0.4928 0.3443 0.205 Uiso 1 1 calc R U . . .
H54C H 0.1798 0.4638 0.4106 0.205 Uiso 1 1 calc R U . . .
C55 C 0.4678(12) 0.5440(6) 0.8631(8) 0.1055(17) Uani 1 1 d D . . . .
H55A H 0.4953 0.5700 0.8758 0.127 Uiso 1 1 calc R U . . .
H55B H 0.4114 0.5494 0.8454 0.127 Uiso 1 1 calc R U . . .
C56 C 0.493(2) 0.5195(9) 0.9270(9) 0.137(2) Uani 1 1 d D . . . .
H56A H 0.4925 0.4912 0.9150 0.205 Uiso 1 1 calc R U . . .
H56B H 0.4572 0.5238 0.9484 0.205 Uiso 1 1 calc R U . . .
H56C H 0.5458 0.5273 0.9600 0.205 Uiso 1 1 calc R U . . .
C57 C 0.5893(6) 0.5139(7) 0.8353(8) 0.1055(17) Uani 1 1 d D . . . .
H57A H 0.6138 0.5358 0.8692 0.127 Uiso 1 1 calc R U . . .
H57B H 0.5996 0.4886 0.8620 0.127 Uiso 1 1 calc R U . . .
C58 C 0.6274(10) 0.5118(11) 0.7878(14) 0.137(2) Uani 1 1 d D . . . .
H58A H 0.5942 0.4967 0.7458 0.205 Uiso 1 1 calc R U . . .
H58B H 0.6779 0.4983 0.8116 0.205 Uiso 1 1 calc R U . . .
H58C H 0.6353 0.5389 0.7746 0.205 Uiso 1 1 calc R U . . .
C59 C 0.4785(11) 0.5663(5) 0.7404(8) 0.1055(17) Uani 1 1 d D . . . .
H59A H 0.4822 0.5576 0.6975 0.127 Uiso 1 1 calc R U . . .
H59B H 0.4265 0.5786 0.7260 0.127 Uiso 1 1 calc R U . . .
C60 C 0.5384(17) 0.5973(6) 0.7749(15) 0.137(2) Uani 1 1 d D . . . .
H60A H 0.5787 0.5954 0.7581 0.205 Uiso 1 1 calc R U . . .
H60B H 0.5620 0.5932 0.8256 0.205 Uiso 1 1 calc R U . . .
H60C H 0.5141 0.6238 0.7638 0.205 Uiso 1 1 calc R U . . .
C61 C 0.1444(13) 0.5569(3) 0.6485(9) 0.1055(17) Uani 1 1 d D . . . .
H61A H 0.1020 0.5685 0.6578 0.127 Uiso 1 1 calc R U . . .
H61B H 0.1935 0.5702 0.6804 0.127 Uiso 1 1 calc R U . . .
C62 C 0.129(2) 0.5669(6) 0.5760(11) 0.137(2) Uani 1 1 d D . . . .
H62A H 0.1566 0.5479 0.5595 0.205 Uiso 1 1 calc R U . . .
H62B H 0.1475 0.5941 0.5745 0.205 Uiso 1 1 calc R U . . .
H62C H 0.0730 0.5653 0.5459 0.205 Uiso 1 1 calc R U . . .
C63 C 0.0576(7) 0.4856(5) 0.6099(8) 0.1055(17) Uani 1 1 d D . . . .
H63A H 0.0557 0.4852 0.5625 0.127 Uiso 1 1 calc R U . . .
H63B H 0.0530 0.4576 0.6227 0.127 Uiso 1 1 calc R U . . .
C64 C -0.0109(6) 0.5079(9) 0.6060(16) 0.137(2) Uani 1 1 d D . . . .
H64A H -0.0115 0.5076 0.6518 0.205 Uiso 1 1 calc R U . . .
H64B H -0.0585 0.4953 0.5714 0.205 Uiso 1 1 calc R U . . .
H64C H -0.0081 0.5356 0.5921 0.205 Uiso 1 1 calc R U . . .
C65 C 0.1445(12) 0.5047(6) 0.7519(6) 0.1055(17) Uani 1 1 d D . . . .
H65A H 0.0914 0.5139 0.7427 0.127 Uiso 1 1 calc R U . . .
H65B H 0.1501 0.4770 0.7696 0.127 Uiso 1 1 calc R U . . .
C66 C 0.2017(17) 0.5302(9) 0.8076(8) 0.137(2) Uani 1 1 d D . . . .
H66A H 0.2543 0.5194 0.8217 0.205 Uiso 1 1 calc R U . . .
H66B H 0.1896 0.5305 0.8479 0.205 Uiso 1 1 calc R U . . .
H66C H 0.1993 0.5575 0.7899 0.205 Uiso 1 1 calc R U . . .
C91 C 0.644(5) 0.053(3) 0.631(5) 0.57(3) Uiso 1 1 d D . . . .
H91A H 0.6765 0.0773 0.6456 0.856 Uiso 1 1 calc R U . . .
H91B H 0.6770 0.0295 0.6430 0.856 Uiso 1 1 calc R U . . .
H91C H 0.6109 0.0541 0.5809 0.856 Uiso 1 1 calc R U . . .
C92 C 0.593(5) 0.052(3) 0.669(5) 0.57(3) Uiso 1 1 d D . . . .
H92A H 0.6261 0.0513 0.7203 0.685 Uiso 1 1 calc R U . . .
H92B H 0.5598 0.0760 0.6580 0.685 Uiso 1 1 calc R U . . .
C94 C 0.462(4) 0.025(3) 0.623(4) 0.57(3) Uiso 1 1 d D . . . .
H94A H 0.4553 0.0497 0.6456 0.685 Uiso 1 1 calc R U . . .
H94B H 0.4359 0.0028 0.6344 0.685 Uiso 1 1 calc R U . . .
C95 C 0.426(5) 0.031(4) 0.545(4) 0.57(3) Uiso 1 1 d D . . . .
H95A H 0.3707 0.0370 0.5279 0.856 Uiso 1 1 calc R U . . .
H95B H 0.4521 0.0534 0.5335 0.856 Uiso 1 1 calc R U . . .
H95C H 0.4327 0.0066 0.5224 0.856 Uiso 1 1 calc R U . . .
Ni1 Ni 0.41703(10) 0.33284(5) 0.64899(9) 0.0224(4) Uani 1 1 d . . . . .
Ni2 Ni 0.28449(10) 0.34568(5) 0.63526(8) 0.0216(4) Uani 1 1 d . . . . .
Ni3 Ni 0.26818(10) 0.33408(5) 0.74226(9) 0.0249(4) Uani 1 1 d . . . . .
Ni4 Ni 0.39533(10) 0.35039(5) 0.75025(9) 0.0254(4) Uani 1 1 d . . . . .
Ni5 Ni 0.33642(10) 0.41209(5) 0.68571(9) 0.0259(4) Uani 1 1 d . . . . .
Ni6 Ni 0.55067(10) 0.34226(6) 0.66656(10) 0.0299(4) Uani 1 1 d . . . . .
Ni7 Ni 0.42333(11) 0.33373(5) 0.53601(9) 0.0276(4) Uani 1 1 d . . . . .
Ni8 Ni 0.29032(10) 0.32347(5) 0.52577(9) 0.0253(4) Uani 1 1 d . . . . .
Ni9 Ni 0.53368(11) 0.33827(6) 0.77602(10) 0.0307(4) Uani 1 1 d . . . . .
Ni10 Ni 0.35936(10) 0.39213(5) 0.57833(9) 0.0261(4) Uani 1 1 d . . . . .
Ni11 Ni 0.47312(10) 0.40327(5) 0.69442(9) 0.0273(4) Uani 1 1 d . . . . .
Ni12 Ni 0.47255(11) 0.26828(5) 0.62510(10) 0.0309(4) Uani 1 1 d . . . . .
Ni13 Ni 0.33320(11) 0.27098(5) 0.61401(9) 0.0263(4) Uani 1 1 d . . . . .
Ni14 Ni 0.45240(11) 0.27769(5) 0.73586(9) 0.0292(4) Uani 1 1 d . . . . .
Ni15 Ni 0.16072(10) 0.34905(5) 0.50903(9) 0.0269(4) Uani 1 1 d . . . . .
Ni16 Ni 0.15000(10) 0.32621(5) 0.61607(9) 0.0265(4) Uani 1 1 d . . . . .
Ni17 Ni 0.13284(11) 0.33911(6) 0.72367(10) 0.0345(5) Uani 1 1 d D . . . .
Ni18 Ni 0.26045(12) 0.34600(7) 0.85168(10) 0.0367(5) Uani 1 1 d . . . . .
Ni19 Ni 0.39690(11) 0.33776(6) 0.86765(9) 0.0330(4) Uani 1 1 d . . . . .
Ni20 Ni 0.20262(10) 0.39452(5) 0.67818(9) 0.0273(4) Uani 1 1 d . . . . .
Ni21 Ni 0.31924(10) 0.40024(6) 0.80050(10) 0.0313(4) Uani 1 1 d . . . . .
Ni22 Ni 0.22571(12) 0.27190(6) 0.78256(10) 0.0352(5) Uani 1 1 d D . . . .
Ni23 Ni 0.24355(11) 0.27214(5) 0.67055(9) 0.0278(4) Uani 1 1 d . . . . .
Ni24 Ni 0.36361(11) 0.27823(6) 0.79349(10) 0.0316(4) Uani 1 1 d . . . . .
Ni25 Ni 0.22261(10) 0.41071(5) 0.56992(9) 0.0257(4) Uani 1 1 d . . . . .
Ni26 Ni 0.33011(11) 0.46644(5) 0.58929(11) 0.0347(5) Uani 1 1 d . . . . .
Ni27 Ni 0.44669(11) 0.41718(6) 0.80503(10) 0.0332(4) Uani 1 1 d . . . . .
Ni28 Ni 0.52618(11) 0.36634(6) 0.88346(10) 0.0362(5) Uani 1 1 d . . . . .
Ni29 Ni 0.41076(11) 0.47542(6) 0.72790(11) 0.0384(5) Uani 1 1 d . . . . .
Ni30 Ni 0.24534(11) 0.47026(6) 0.66360(11) 0.0357(5) Uani 1 1 d . . . . .
O1 O 0.545(4) 0.0164(17) 0.648(4) 0.57(3) Uiso 1 1 d D . . . .
P1 P 0.4247(3) 0.33636(13) 0.4335(2) 0.0423(10) Uani 1 1 d D . . . .
P2 P 0.6721(2) 0.36143(15) 0.7019(3) 0.0543(13) Uani 1 1 d D . . . .
P3 P 0.0098(2) 0.35126(15) 0.6979(3) 0.0522(12) Uani 1 1 d D . . . .
P4 P 0.2636(4) 0.36309(18) 0.9521(3) 0.0634(15) Uani 1 1 d D . . . .
P5 P 0.5134(3) 0.20791(14) 0.6155(3) 0.0583(15) Uani 1 1 d D . . . .
P6 P 0.1991(3) 0.21252(15) 0.8109(3) 0.0607(14) Uani 1 1 d D . . . .
P7 P 0.0639(2) 0.33033(14) 0.4117(2) 0.0416(10) Uani 1 1 d D . . . .
P8 P 0.6249(3) 0.35620(15) 0.9842(2) 0.0522(12) Uani 1 1 d D . . . .
P9 P 0.3373(2) 0.49753(15) 0.5040(3) 0.0612(16) Uani 1 1 d D . . . .
P10 P 0.4848(3) 0.52227(18) 0.7930(3) 0.078(2) Uani 1 1 d D . . . .
P11 P 0.1522(2) 0.50417(12) 0.6700(2) 0.0401(10) Uani 1 1 d D . . . .
S1 S 0.4843(2) 0.38675(11) 0.59089(19) 0.0298(8) Uani 1 1 d . . . . .
S2 S 0.3695(2) 0.27436(10) 0.5267(2) 0.0307(8) Uani 1 1 d . . . . .
S3 S 0.2486(2) 0.38306(11) 0.48610(19) 0.0298(8) Uani 1 1 d . . . . .
S4 S 0.2096(2) 0.29022(10) 0.56124(18) 0.0272(7) Uani 1 1 d . . . . .
S5 S 0.3520(2) 0.23681(11) 0.7089(2) 0.0344(8) Uani 1 1 d . . . . .
S6 S 0.1141(2) 0.38560(11) 0.57075(19) 0.0293(8) Uani 1 1 d . . . . .
S7 S 0.1299(2) 0.27910(12) 0.6794(2) 0.0343(8) Uani 1 1 d . . . . .
S8 S 0.1922(2) 0.39325(13) 0.7791(2) 0.0370(9) Uani 1 1 d . . . . .
S9 S 0.3241(2) 0.28892(13) 0.8781(2) 0.0409(9) Uani 1 1 d . . . . .
S10 S 0.4326(2) 0.39881(13) 0.89952(19) 0.0368(9) Uani 1 1 d . . . . .
S11 S 0.5592(2) 0.40073(12) 0.8078(2) 0.0352(9) Uani 1 1 d . . . . .
S12 S 0.5635(2) 0.28663(11) 0.7247(2) 0.0342(8) Uani 1 1 d . . . . .
S13 S 0.4820(2) 0.30478(12) 0.83929(19) 0.0340(8) Uani 1 1 d . . . . .
S14 S 0.3297(2) 0.46231(13) 0.7700(2) 0.0424(10) Uani 1 1 d . . . . .
S15 S 0.2080(2) 0.47561(11) 0.5546(2) 0.0350(9) Uani 1 1 d . . . . .
S16 S 0.4539(2) 0.46611(11) 0.6532(2) 0.0369(9) Uani 1 1 d . . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C1 C2 1.489(7) . ?
C1 P1 1.821(8) . ?
C1 H1A 0.9900 . ?
C1 H1B 0.9900 . ?
C2 H2A 0.9800 . ?
C2 H2B 0.9800 . ?
C2 H2C 0.9800 . ?
C3 C4 1.48(3) . ?
C3 P1 1.801(8) . ?
C3 H3A 0.9900 . ?
C3 H3B 0.9900 . ?
C4 H4A 0.9800 . ?
C4 H4B 0.9800 . ?
C4 H4C 0.9800 . ?
C5 C6 1.65(3) . ?
C5 P1 1.823(8) . ?
C5 H5A 0.9900 . ?
C5 H5B 0.9900 . ?
C6 H6A 0.9800 . ?
C6 H6B 0.9800 . ?
C6 H6C 0.9800 . ?
C7 C8 1.41(3) . ?
C7 P2 1.813(8) . ?
C7 H7A 0.9900 . ?
C7 H7B 0.9900 . ?
C8 H8A 0.9800 . ?
C8 H8B 0.9800 . ?
C8 H8C 0.9800 . ?
C9 C10 1.57(3) . ?
C9 P2 1.807(8) . ?
C9 H9A 0.9900 . ?
C9 H9B 0.9900 . ?
C10 H10A 0.9800 . ?
C10 H10B 0.9800 . ?
C10 H10C 0.9800 . ?
C11 C12 1.41(3) . ?
C11 P2 1.814(8) . ?
C11 H11A 0.9900 . ?
C11 H11B 0.9900 . ?
C12 H12A 0.9800 . ?
C12 H12B 0.9800 . ?
C12 H12C 0.9800 . ?
C13 C14 1.475(9) . ?
C13 P3 1.818(8) . ?
C13 H13A 0.9900 . ?
C13 H13B 0.9900 . ?
C14 H14A 0.9800 . ?
C14 H14B 0.9800 . ?
C14 H14C 0.9800 . ?
C15 C16 1.478(9) . ?
C15 P3 1.817(8) . ?
C15 H15A 0.9900 . ?
C15 H15B 0.9900 . ?
C16 H16A 0.9800 . ?
C16 H16B 0.9800 . ?
C16 H16C 0.9800 . ?
C17 C18 1.480(9) . ?
C17 P3 1.816(8) . ?
C17 H17A 0.9900 . ?
C17 H17B 0.9900 . ?
C18 H18A 0.9800 . ?
C18 H18B 0.9800 . ?
C18 H18C 0.9800 . ?
C19 C20 1.473(9) . ?
C19 P4 1.814(8) . ?
C19 H19A 0.9900 . ?
C19 H19B 0.9900 . ?
C20 H20A 0.9800 . ?
C20 H20B 0.9800 . ?
C20 H20C 0.9800 . ?
C21 C22 1.487(9) . ?
C21 P4 1.809(8) . ?
C21 H21A 0.9900 . ?
C21 H21B 0.9900 . ?
C22 H22A 0.9800 . ?
C22 H22B 0.9800 . ?
C22 H22C 0.9800 . ?
C23 C24 1.478(9) . ?
C23 P4 1.818(8) . ?
C23 H23A 0.9900 . ?
C23 H23B 0.9900 . ?
C24 H24A 0.9800 . ?
C24 H24B 0.9800 . ?
C24 H24C 0.9800 . ?
C25 C26 1.473(9) . ?
C25 P5 1.819(8) . ?
C25 H25A 0.9900 . ?
C25 H25B 0.9900 . ?
C26 H26A 0.9800 . ?
C26 H26B 0.9800 . ?
C26 H26C 0.9800 . ?
C27 C28 1.475(9) . ?
C27 P5 1.845(8) . ?
C27 H27A 0.9900 . ?
C27 H27B 0.9900 . ?
C28 H28A 0.9800 . ?
C28 H28B 0.9800 . ?
C28 H28C 0.9800 . ?
C29 C30 1.464(9) . ?
C29 P5 1.813(8) . ?
C29 H29A 0.9900 . ?
C29 H29B 0.9900 . ?
C30 H30A 0.9800 . ?
C30 H30B 0.9800 . ?
C30 H30C 0.9800 . ?
C31 C32 1.475(9) . ?
C31 P6 1.823(8) . ?
C31 H31A 0.9900 . ?
C31 H31B 0.9900 . ?
C32 H32A 0.9800 . ?
C32 H32B 0.9800 . ?
C32 H32C 0.9800 . ?
C33 C34 1.470(9) . ?
C33 P6 1.820(8) . ?
C33 H33A 0.9900 . ?
C33 H33B 0.9900 . ?
C34 H34A 0.9800 . ?
C34 H34B 0.9800 . ?
C34 H34C 0.9800 . ?
C35 C36 1.473(9) . ?
C35 P6 1.807(8) . ?
C35 H35A 0.9900 . ?
C35 H35B 0.9900 . ?
C36 H36A 0.9800 . ?
C36 H36B 0.9800 . ?
C36 H36C 0.9800 . ?
C37 C38 1.473(9) . ?
C37 P7 1.809(8) . ?
C37 H37A 0.9900 . ?
C37 H37B 0.9900 . ?
C38 H38A 0.9800 . ?
C38 H38B 0.9800 . ?
C38 H38C 0.9800 . ?
C39 C40 1.461(9) . ?
C39 P7 1.826(8) . ?
C39 H39A 0.9900 . ?
C39 H39B 0.9900 . ?
C40 H40A 0.9800 . ?
C40 H40B 0.9800 . ?
C40 H40C 0.9800 . ?
C41 C42 1.458(9) . ?
C41 P7 1.826(8) . ?
C41 H41A 0.9900 . ?
C41 H41B 0.9900 . ?
C42 H42A 0.9800 . ?
C42 H42B 0.9800 . ?
C42 H42C 0.9800 . ?
C43 C44 1.479(9) . ?
C43 P8 1.805(8) . ?
C43 H43A 0.9900 . ?
C43 H43B 0.9900 . ?
C44 H44A 0.9800 . ?
C44 H44B 0.9800 . ?
C44 H44C 0.9800 . ?
C45 C46 1.478(9) . ?
C45 P8 1.811(8) . ?
C45 H45A 0.9900 . ?
C45 H45B 0.9900 . ?
C46 H46A 0.9800 . ?
C46 H46B 0.9800 . ?
C46 H46C 0.9800 . ?
C47 C48 1.478(9) . ?
C47 P8 1.815(8) . ?
C47 H47A 0.9900 . ?
C47 H47B 0.9900 . ?
C48 H48A 0.9800 . ?
C48 H48B 0.9800 . ?
C48 H48C 0.9800 . ?
C49 C50 1.477(9) . ?
C49 P9 1.805(8) . ?
C49 H49A 0.9900 . ?
C49 H49B 0.9900 . ?
C50 H50A 0.9800 . ?
C50 H50B 0.9800 . ?
C50 H50C 0.9800 . ?
C51 C52 1.480(9) . ?
C51 P9 1.814(8) . ?
C51 H51A 0.9900 . ?
C51 H51B 0.9900 . ?
C52 H52A 0.9800 . ?
C52 H52B 0.9800 . ?
C52 H52C 0.9800 . ?
C53 C54 1.475(9) . ?
C53 P9 1.813(8) . ?
C53 H53A 0.9900 . ?
C53 H53B 0.9900 . ?
C54 H54A 0.9800 . ?
C54 H54B 0.9800 . ?
C54 H54C 0.9800 . ?
C55 C56 1.476(9) . ?
C55 P10 1.809(8) . ?
C55 H55A 0.9900 . ?
C55 H55B 0.9900 . ?
C56 H56A 0.9800 . ?
C56 H56B 0.9800 . ?
C56 H56C 0.9800 . ?
C57 C58 1.478(9) . ?
C57 P10 1.815(8) . ?
C57 H57A 0.9900 . ?
C57 H57B 0.9900 . ?
C58 H58A 0.9800 . ?
C58 H58B 0.9800 . ?
C58 H58C 0.9800 . ?
C59 C60 1.478(9) . ?
C59 P10 1.821(8) . ?
C59 H59A 0.9900 . ?
C59 H59B 0.9900 . ?
C60 H60A 0.9800 . ?
C60 H60B 0.9800 . ?
C60 H60C 0.9800 . ?
C61 C62 1.476(9) . ?
C61 P11 1.812(8) . ?
C61 H61A 0.9900 . ?
C61 H61B 0.9900 . ?
C62 H62A 0.9800 . ?
C62 H62B 0.9800 . ?
C62 H62C 0.9800 . ?
C63 C64 1.473(9) . ?
C63 P11 1.807(8) . ?
C63 H63A 0.9900 . ?
C63 H63B 0.9900 . ?
C64 H64A 0.9800 . ?
C64 H64B 0.9800 . ?
C64 H64C 0.9800 . ?
C65 C66 1.480(9) . ?
C65 P11 1.811(8) . ?
C65 H65A 0.9900 . ?
C65 H65B 0.9900 . ?
C66 H66A 0.9800 . ?
C66 H66B 0.9800 . ?
C66 H66C 0.9800 . ?
C91 C92 1.502(10) . ?
C91 H91A 0.9800 . ?
C91 H91B 0.9800 . ?
C91 H91C 0.9800 . ?
C92 O1 1.449(8) . ?
C92 H92A 0.9900 . ?
C92 H92B 0.9900 . ?
C94 O1 1.448(8) . ?
C94 C95 1.504(14) . ?
C94 H94A 0.9900 . ?
C94 H94B 0.9900 . ?
C95 H95A 0.9800 . ?
C95 H95B 0.9800 . ?
C95 H95C 0.9800 . ?
Ni1 Ni6 2.428(3) . ?
Ni1 Ni4 2.433(2) . ?
Ni1 Ni10 2.441(2) . ?
Ni1 Ni2 2.450(2) . ?
Ni1 Ni7 2.456(2) . ?
Ni1 Ni14 2.486(2) . ?
Ni1 Ni13 2.519(3) . ?
Ni1 Ni12 2.550(2) . ?
Ni1 Ni11 2.593(3) . ?
Ni1 Ni9 2.654(3) . ?
Ni1 Ni8 2.699(2) . ?
Ni2 Ni4 2.443(2) . ?
Ni2 S4 2.449(4) . ?
Ni2 Ni3 2.457(2) . ?
Ni2 Ni5 2.477(2) . ?
Ni2 Ni8 2.491(2) . ?
Ni2 Ni16 2.499(2) . ?
Ni2 Ni25 2.573(2) . ?
Ni2 Ni20 2.677(2) . ?
Ni2 Ni15 2.696(2) . ?
Ni2 Ni10 2.722(3) . ?
Ni2 Ni13 2.769(2) . ?
Ni3 Ni4 2.416(3) . ?
Ni3 Ni18 2.427(3) . ?
Ni3 Ni17 2.438(3) . ?
Ni3 Ni20 2.453(3) . ?
Ni3 Ni23 2.492(3) . ?
Ni3 Ni24 2.501(3) . ?
Ni3 Ni22 2.513(3) . ?
Ni3 Ni21 2.515(3) . ?
Ni3 Ni16 2.661(2) . ?
Ni3 Ni19 2.729(3) . ?
Ni3 S8 2.759(4) . ?
Ni4 S13 2.432(4) . ?
Ni4 Ni5 2.461(2) . ?
Ni4 Ni9 2.481(3) . ?
Ni4 Ni27 2.512(3) . ?
Ni4 Ni19 2.518(3) . ?
Ni4 Ni21 2.714(3) . ?
Ni4 Ni14 2.734(3) . ?
Ni4 Ni24 2.741(3) . ?
Ni4 Ni11 2.874(3) . ?
Ni5 Ni25 2.474(2) . ?
Ni5 Ni29 2.488(3) . ?
Ni5 Ni27 2.498(2) . ?
Ni5 S14 2.499(4) . ?
Ni5 Ni30 2.511(2) . ?
Ni5 Ni11 2.546(3) . ?
Ni5 Ni20 2.552(3) . ?
Ni5 Ni10 2.591(3) . ?
Ni5 Ni21 2.629(3) . ?
Ni5 Ni26 2.702(3) . ?
Ni6 S1 2.152(4) . ?
Ni6 S12 2.187(4) . ?
Ni6 P2 2.194(5) . ?
Ni6 Ni9 2.488(3) . ?
Ni6 Ni11 2.730(3) . ?
Ni6 Ni7 2.795(3) . ?
Ni6 Ni12 2.823(3) . ?
Ni7 S1 2.162(4) . ?
Ni7 P1 2.193(4) . ?
Ni7 S2 2.203(4) . ?
Ni7 Ni8 2.471(3) . ?
Ni7 Ni10 2.657(2) . ?
Ni7 Ni12 2.777(3) . ?
Ni8 S3 2.174(4) . ?
Ni8 S2 2.224(4) . ?
Ni8 S4 2.275(4) . ?
Ni8 Ni13 2.435(2) . ?
Ni8 Ni15 2.488(3) . ?
Ni8 Ni10 2.640(3) . ?
Ni9 S11 2.184(5) . ?
Ni9 S12 2.243(4) . ?
Ni9 S13 2.276(4) . ?
Ni9 Ni14 2.466(3) . ?
Ni9 Ni28 2.530(3) . ?
Ni9 Ni11 2.706(3) . ?
Ni10 S3 2.188(4) . ?
Ni10 S1 2.283(4) . ?
Ni10 Ni11 2.505(2) . ?
Ni10 Ni26 2.579(3) . ?
Ni10 Ni25 2.608(3) . ?
Ni11 S16 2.244(4) . ?
Ni11 S11 2.251(4) . ?
Ni11 S1 2.366(4) . ?
Ni11 Ni27 2.651(3) . ?
Ni11 Ni29 2.911(3) . ?
Ni12 S12 2.161(5) . ?
Ni12 S2 2.167(4) . ?
Ni12 P5 2.204(5) . ?
Ni12 Ni13 2.562(3) . ?
Ni12 Ni14 2.564(3) . ?
Ni13 S5 2.208(4) . ?
Ni13 S4 2.218(4) . ?
Ni13 S2 2.247(4) . ?
Ni13 Ni23 2.480(3) . ?
Ni13 Ni14 2.608(3) . ?
Ni14 S13 2.212(4) . ?
Ni14 S5 2.215(4) . ?
Ni14 S12 2.249(4) . ?
Ni14 Ni24 2.483(3) . ?
Ni15 P7 2.181(4) . ?
Ni15 S6 2.239(4) . ?
Ni15 S3 2.246(4) . ?
Ni15 S4 2.251(4) . ?
Ni15 Ni25 2.447(2) . ?
Ni15 Ni16 2.491(3) . ?
Ni16 S6 2.183(4) . ?
Ni16 S7 2.210(4) . ?
Ni16 S4 2.290(4) . ?
Ni16 Ni23 2.447(3) . ?
Ni16 Ni17 2.485(3) . ?
Ni16 Ni20 2.610(3) . ?
Ni17 S8 2.187(5) . ?
Ni17 P3 2.201(4) . ?
Ni17 S7 2.207(5) . ?
Ni17 Ni20 2.693(3) . ?
Ni17 Ni18 2.759(3) . ?
Ni17 Ni22 2.796(3) . ?
Ni18 P4 2.184(5) . ?
Ni18 S8 2.196(5) . ?
Ni18 S9 2.199(5) . ?
Ni18 Ni19 2.486(3) . ?
Ni18 Ni21 2.605(3) . ?
Ni18 Ni22 2.809(3) . ?
Ni19 S10 2.165(5) . ?
Ni19 S9 2.215(5) . ?
Ni19 S13 2.249(4) . ?
Ni19 Ni24 2.445(3) . ?
Ni19 Ni28 2.524(3) . ?
Ni19 Ni21 2.599(3) . ?
Ni20 S6 2.190(4) . ?
Ni20 S8 2.239(4) . ?
Ni20 Ni25 2.549(3) . ?
Ni20 Ni21 2.590(3) . ?
Ni20 Ni30 2.718(3) . ?
Ni21 S14 2.209(5) . ?
Ni21 S10 2.268(4) . ?
Ni21 S8 2.272(4) . ?
Ni21 Ni27 2.454(3) . ?
Ni22 S9 2.156(5) . ?
Ni22 S7 2.173(4) . ?
Ni22 P6 2.197(5) . ?
Ni22 Ni24 2.543(3) . ?
Ni22 Ni23 2.547(3) . ?
Ni23 S5 2.205(4) . ?
Ni23 S4 2.208(4) . ?
Ni23 S7 2.265(4) . ?
Ni23 Ni24 2.628(3) . ?
Ni24 S5 2.203(4) . ?
Ni24 S13 2.217(4) . ?
Ni24 S9 2.259(4) . ?
Ni25 S15 2.194(4) . ?
Ni25 S6 2.238(4) . ?
Ni25 S3 2.246(4) . ?
Ni25 Ni26 2.665(3) . ?
Ni25 Ni30 2.714(3) . ?
Ni26 S15 2.135(4) . ?
Ni26 P9 2.145(6) . ?
Ni26 S16 2.150(4) . ?
Ni26 Ni29 2.682(3) . ?
Ni26 Ni30 2.709(3) . ?
Ni27 S11 2.189(4) . ?
Ni27 S10 2.225(5) . ?
Ni27 Ni28 2.401(3) . ?
Ni27 Ni29 2.444(3) . ?
Ni27 S14 2.521(4) . ?
Ni28 P8 2.176(5) . ?
Ni28 S10 2.236(4) . ?
Ni28 S13 2.267(5) . ?
Ni28 S11 2.277(5) . ?
Ni29 S16 2.104(5) . ?
Ni29 S14 2.140(5) . ?
Ni29 P10 2.158(5) . ?
Ni29 Ni30 2.843(3) . ?
Ni30 S15 2.116(5) . ?
Ni30 S14 2.147(5) . ?
Ni30 P11 2.159(4) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C2 C1 P1 113.8(7) . . ?
C2 C1 H1A 108.8 . . ?
P1 C1 H1A 108.8 . . ?
C2 C1 H1B 108.8 . . ?
P1 C1 H1B 108.8 . . ?
H1A C1 H1B 107.7 . . ?
C1 C2 H2A 109.5 . . ?
C1 C2 H2B 109.5 . . ?
H2A C2 H2B 109.5 . . ?
C1 C2 H2C 109.5 . . ?
H2A C2 H2C 109.5 . . ?
H2B C2 H2C 109.5 . . ?
C4 C3 P1 116.2(16) . . ?
C4 C3 H3A 108.2 . . ?
P1 C3 H3A 108.2 . . ?
C4 C3 H3B 108.2 . . ?
P1 C3 H3B 108.2 . . ?
H3A C3 H3B 107.4 . . ?
C3 C4 H4A 109.5 . . ?
C3 C4 H4B 109.5 . . ?
H4A C4 H4B 109.5 . . ?
C3 C4 H4C 109.5 . . ?
H4A C4 H4C 109.5 . . ?
H4B C4 H4C 109.5 . . ?
C6 C5 P1 107.0(12) . . ?
C6 C5 H5A 110.3 . . ?
P1 C5 H5A 110.3 . . ?
C6 C5 H5B 110.3 . . ?
P1 C5 H5B 110.3 . . ?
H5A C5 H5B 108.6 . . ?
C5 C6 H6A 109.5 . . ?
C5 C6 H6B 109.5 . . ?
H6A C6 H6B 109.5 . . ?
C5 C6 H6C 109.5 . . ?
H6A C6 H6C 109.5 . . ?
H6B C6 H6C 109.5 . . ?
C8 C7 P2 120.0(16) . . ?
C8 C7 H7A 107.3 . . ?
P2 C7 H7A 107.3 . . ?
C8 C7 H7B 107.3 . . ?
P2 C7 H7B 107.3 . . ?
H7A C7 H7B 106.9 . . ?
C7 C8 H8A 109.5 . . ?
C7 C8 H8B 109.5 . . ?
H8A C8 H8B 109.5 . . ?
C7 C8 H8C 109.5 . . ?
H8A C8 H8C 109.5 . . ?
H8B C8 H8C 109.5 . . ?
C10 C9 P2 111.0(14) . . ?
C10 C9 H9A 109.4 . . ?
P2 C9 H9A 109.4 . . ?
C10 C9 H9B 109.4 . . ?
P2 C9 H9B 109.4 . . ?
H9A C9 H9B 108.0 . . ?
C9 C10 H10A 109.5 . . ?
C9 C10 H10B 109.5 . . ?
H10A C10 H10B 109.5 . . ?
C9 C10 H10C 109.5 . . ?
H10A C10 H10C 109.5 . . ?
H10B C10 H10C 109.5 . . ?
C12 C11 P2 119.7(17) . . ?
C12 C11 H11A 107.4 . . ?
P2 C11 H11A 107.4 . . ?
C12 C11 H11B 107.4 . . ?
P2 C11 H11B 107.4 . . ?
H11A C11 H11B 106.9 . . ?
C11 C12 H12A 109.5 . . ?
C11 C12 H12B 109.5 . . ?
H12A C12 H12B 109.5 . . ?
C11 C12 H12C 109.5 . . ?
H12A C12 H12C 109.5 . . ?
H12B C12 H12C 109.5 . . ?
C14 C13 P3 115.7(8) . . ?
C14 C13 H13A 108.4 . . ?
P3 C13 H13A 108.4 . . ?
C14 C13 H13B 108.4 . . ?
P3 C13 H13B 108.4 . . ?
H13A C13 H13B 107.4 . . ?
C13 C14 H14A 109.5 . . ?
C13 C14 H14B 109.5 . . ?
H14A C14 H14B 109.5 . . ?
C13 C14 H14C 109.5 . . ?
H14A C14 H14C 109.5 . . ?
H14B C14 H14C 109.5 . . ?
C16 C15 P3 115.6(7) . . ?
C16 C15 H15A 108.4 . . ?
P3 C15 H15A 108.4 . . ?
C16 C15 H15B 108.4 . . ?
P3 C15 H15B 108.4 . . ?
H15A C15 H15B 107.4 . . ?
C15 C16 H16A 109.5 . . ?
C15 C16 H16B 109.5 . . ?
H16A C16 H16B 109.5 . . ?
C15 C16 H16C 109.5 . . ?
H16A C16 H16C 109.5 . . ?
H16B C16 H16C 109.5 . . ?
C18 C17 P3 115.2(8) . . ?
C18 C17 H17A 108.5 . . ?
P3 C17 H17A 108.5 . . ?
C18 C17 H17B 108.5 . . ?
P3 C17 H17B 108.5 . . ?
H17A C17 H17B 107.5 . . ?
C17 C18 H18A 109.5 . . ?
C17 C18 H18B 109.5 . . ?
H18A C18 H18B 109.5 . . ?
C17 C18 H18C 109.5 . . ?
H18A C18 H18C 109.5 . . ?
H18B C18 H18C 109.5 . . ?
C20 C19 P4 116.1(8) . . ?
C20 C19 H19A 108.3 . . ?
P4 C19 H19A 108.3 . . ?
C20 C19 H19B 108.3 . . ?
P4 C19 H19B 108.3 . . ?
H19A C19 H19B 107.4 . . ?
C19 C20 H20A 109.5 . . ?
C19 C20 H20B 109.5 . . ?
H20A C20 H20B 109.5 . . ?
C19 C20 H20C 109.5 . . ?
H20A C20 H20C 109.5 . . ?
H20B C20 H20C 109.5 . . ?
C22 C21 P4 115.1(8) . . ?
C22 C21 H21A 108.5 . . ?
P4 C21 H21A 108.5 . . ?
C22 C21 H21B 108.5 . . ?
P4 C21 H21B 108.5 . . ?
H21A C21 H21B 107.5 . . ?
C21 C22 H22A 109.5 . . ?
C21 C22 H22B 109.5 . . ?
H22A C22 H22B 109.5 . . ?
C21 C22 H22C 109.5 . . ?
H22A C22 H22C 109.5 . . ?
H22B C22 H22C 109.5 . . ?
C24 C23 P4 115.4(8) . . ?
C24 C23 H23A 108.4 . . ?
P4 C23 H23A 108.4 . . ?
C24 C23 H23B 108.4 . . ?
P4 C23 H23B 108.4 . . ?
H23A C23 H23B 107.5 . . ?
C23 C24 H24A 109.5 . . ?
C23 C24 H24B 109.5 . . ?
H24A C24 H24B 109.5 . . ?
C23 C24 H24C 109.5 . . ?
H24A C24 H24C 109.5 . . ?
H24B C24 H24C 109.5 . . ?
C26 C25 P5 115.3(8) . . ?
C26 C25 H25A 108.4 . . ?
P5 C25 H25A 108.4 . . ?
C26 C25 H25B 108.4 . . ?
P5 C25 H25B 108.4 . . ?
H25A C25 H25B 107.5 . . ?
C25 C26 H26A 109.5 . . ?
C25 C26 H26B 109.5 . . ?
H26A C26 H26B 109.5 . . ?
C25 C26 H26C 109.5 . . ?
H26A C26 H26C 109.5 . . ?
H26B C26 H26C 109.5 . . ?
C28 C27 P5 114.3(8) . . ?
C28 C27 H27A 108.7 . . ?
P5 C27 H27A 108.7 . . ?
C28 C27 H27B 108.7 . . ?
P5 C27 H27B 108.7 . . ?
H27A C27 H27B 107.6 . . ?
C27 C28 H28A 109.5 . . ?
C27 C28 H28B 109.5 . . ?
H28A C28 H28B 109.5 . . ?
C27 C28 H28C 109.5 . . ?
H28A C28 H28C 109.5 . . ?
H28B C28 H28C 109.5 . . ?
C30 C29 P5 116.9(8) . . ?
C30 C29 H29A 108.1 . . ?
P5 C29 H29A 108.1 . . ?
C30 C29 H29B 108.1 . . ?
P5 C29 H29B 108.1 . . ?
H29A C29 H29B 107.3 . . ?
C29 C30 H30A 109.5 . . ?
C29 C30 H30B 109.5 . . ?
H30A C30 H30B 109.5 . . ?
C29 C30 H30C 109.5 . . ?
H30A C30 H30C 109.5 . . ?
H30B C30 H30C 109.5 . . ?
C32 C31 P6 115.3(8) . . ?
C32 C31 H31A 108.5 . . ?
P6 C31 H31A 108.5 . . ?
C32 C31 H31B 108.5 . . ?
P6 C31 H31B 108.5 . . ?
H31A C31 H31B 107.5 . . ?
C31 C32 H32A 109.5 . . ?
C31 C32 H32B 109.5 . . ?
H32A C32 H32B 109.5 . . ?
C31 C32 H32C 109.5 . . ?
H32A C32 H32C 109.5 . . ?
H32B C32 H32C 109.5 . . ?
C34 C33 P6 115.7(8) . . ?
C34 C33 H33A 108.3 . . ?
P6 C33 H33A 108.3 . . ?
C34 C33 H33B 108.3 . . ?
P6 C33 H33B 108.3 . . ?
H33A C33 H33B 107.4 . . ?
C33 C34 H34A 109.5 . . ?
C33 C34 H34B 109.5 . . ?
H34A C34 H34B 109.5 . . ?
C33 C34 H34C 109.5 . . ?
H34A C34 H34C 109.5 . . ?
H34B C34 H34C 109.5 . . ?
C36 C35 P6 116.0(8) . . ?
C36 C35 H35A 108.3 . . ?
P6 C35 H35A 108.3 . . ?
C36 C35 H35B 108.3 . . ?
P6 C35 H35B 108.3 . . ?
H35A C35 H35B 107.4 . . ?
C35 C36 H36A 109.5 . . ?
C35 C36 H36B 109.5 . . ?
H36A C36 H36B 109.5 . . ?
C35 C36 H36C 109.5 . . ?
H36A C36 H36C 109.5 . . ?
H36B C36 H36C 109.5 . . ?
C38 C37 P7 116.2(8) . . ?
C38 C37 H37A 108.2 . . ?
P7 C37 H37A 108.2 . . ?
C38 C37 H37B 108.2 . . ?
P7 C37 H37B 108.2 . . ?
H37A C37 H37B 107.4 . . ?
C37 C38 H38A 109.5 . . ?
C37 C38 H38B 109.5 . . ?
H38A C38 H38B 109.5 . . ?
C37 C38 H38C 109.5 . . ?
H38A C38 H38C 109.5 . . ?
H38B C38 H38C 109.5 . . ?
C40 C39 P7 116.4(8) . . ?
C40 C39 H39A 108.2 . . ?
P7 C39 H39A 108.2 . . ?
C40 C39 H39B 108.2 . . ?
P7 C39 H39B 108.2 . . ?
H39A C39 H39B 107.3 . . ?
C39 C40 H40A 109.5 . . ?
C39 C40 H40B 109.5 . . ?
H40A C40 H40B 109.5 . . ?
C39 C40 H40C 109.5 . . ?
H40A C40 H40C 109.5 . . ?
H40B C40 H40C 109.5 . . ?
C42 C41 P7 116.7(8) . . ?
C42 C41 H41A 108.1 . . ?
P7 C41 H41A 108.1 . . ?
C42 C41 H41B 108.1 . . ?
P7 C41 H41B 108.1 . . ?
H41A C41 H41B 107.3 . . ?
C41 C42 H42A 109.5 . . ?
C41 C42 H42B 109.5 . . ?
H42A C42 H42B 109.5 . . ?
C41 C42 H42C 109.5 . . ?
H42A C42 H42C 109.5 . . ?
H42B C42 H42C 109.5 . . ?
C44 C43 P8 115.9(8) . . ?
C44 C43 H43A 108.3 . . ?
P8 C43 H43A 108.3 . . ?
C44 C43 H43B 108.3 . . ?
P8 C43 H43B 108.3 . . ?
H43A C43 H43B 107.4 . . ?
C43 C44 H44A 109.5 . . ?
C43 C44 H44B 109.5 . . ?
H44A C44 H44B 109.5 . . ?
C43 C44 H44C 109.5 . . ?
H44A C44 H44C 109.5 . . ?
H44B C44 H44C 109.5 . . ?
C46 C45 P8 115.9(8) . . ?
C46 C45 H45A 108.3 . . ?
P8 C45 H45A 108.3 . . ?
C46 C45 H45B 108.3 . . ?
P8 C45 H45B 108.3 . . ?
H45A C45 H45B 107.4 . . ?
C45 C46 H46A 109.5 . . ?
C45 C46 H46B 109.5 . . ?
H46A C46 H46B 109.5 . . ?
C45 C46 H46C 109.5 . . ?
H46A C46 H46C 109.5 . . ?
H46B C46 H46C 109.5 . . ?
C48 C47 P8 115.5(8) . . ?
C48 C47 H47A 108.4 . . ?
P8 C47 H47A 108.4 . . ?
C48 C47 H47B 108.4 . . ?
P8 C47 H47B 108.4 . . ?
H47A C47 H47B 107.5 . . ?
C47 C48 H48A 109.5 . . ?
C47 C48 H48B 109.5 . . ?
H48A C48 H48B 109.5 . . ?
C47 C48 H48C 109.5 . . ?
H48A C48 H48C 109.5 . . ?
H48B C48 H48C 109.5 . . ?
C50 C49 P9 116.4(8) . . ?
C50 C49 H49A 108.2 . . ?
P9 C49 H49A 108.2 . . ?
C50 C49 H49B 108.2 . . ?
P9 C49 H49B 108.2 . . ?
H49A C49 H49B 107.3 . . ?
C49 C50 H50A 109.5 . . ?
C49 C50 H50B 109.5 . . ?
H50A C50 H50B 109.5 . . ?
C49 C50 H50C 109.5 . . ?
H50A C50 H50C 109.5 . . ?
H50B C50 H50C 109.5 . . ?
C52 C51 P9 115.3(8) . . ?
C52 C51 H51A 108.4 . . ?
P9 C51 H51A 108.4 . . ?
C52 C51 H51B 108.4 . . ?
P9 C51 H51B 108.4 . . ?
H51A C51 H51B 107.5 . . ?
C51 C52 H52A 109.5 . . ?
C51 C52 H52B 109.5 . . ?
H52A C52 H52B 109.5 . . ?
C51 C52 H52C 109.5 . . ?
H52A C52 H52C 109.5 . . ?
H52B C52 H52C 109.5 . . ?
C54 C53 P9 119.1(18) . . ?
C54 C53 H53A 107.5 . . ?
P9 C53 H53A 107.5 . . ?
C54 C53 H53B 107.5 . . ?
P9 C53 H53B 107.5 . . ?
H53A C53 H53B 107.0 . . ?
C53 C54 H54A 109.5 . . ?
C53 C54 H54B 109.5 . . ?
H54A C54 H54B 109.5 . . ?
C53 C54 H54C 109.5 . . ?
H54A C54 H54C 109.5 . . ?
H54B C54 H54C 109.5 . . ?
C56 C55 P10 115.7(8) . . ?
C56 C55 H55A 108.4 . . ?
P10 C55 H55A 108.4 . . ?
C56 C55 H55B 108.4 . . ?
P10 C55 H55B 108.4 . . ?
H55A C55 H55B 107.4 . . ?
C55 C56 H56A 109.5 . . ?
C55 C56 H56B 109.5 . . ?
H56A C56 H56B 109.5 . . ?
C55 C56 H56C 109.5 . . ?
H56A C56 H56C 109.5 . . ?
H56B C56 H56C 109.5 . . ?
C58 C57 P10 115.3(8) . . ?
C58 C57 H57A 108.4 . . ?
P10 C57 H57A 108.4 . . ?
C58 C57 H57B 108.4 . . ?
P10 C57 H57B 108.4 . . ?
H57A C57 H57B 107.5 . . ?
C57 C58 H58A 109.5 . . ?
C57 C58 H58B 109.5 . . ?
H58A C58 H58B 109.5 . . ?
C57 C58 H58C 109.5 . . ?
H58A C58 H58C 109.5 . . ?
H58B C58 H58C 109.5 . . ?
C60 C59 P10 115.6(8) . . ?
C60 C59 H59A 108.4 . . ?
P10 C59 H59A 108.4 . . ?
C60 C59 H59B 108.4 . . ?
P10 C59 H59B 108.4 . . ?
H59A C59 H59B 107.4 . . ?
C59 C60 H60A 109.5 . . ?
C59 C60 H60B 109.5 . . ?
H60A C60 H60B 109.5 . . ?
C59 C60 H60C 109.5 . . ?
H60A C60 H60C 109.5 . . ?
H60B C60 H60C 109.5 . . ?
C62 C61 P11 116.2(8) . . ?
C62 C61 H61A 108.2 . . ?
P11 C61 H61A 108.2 . . ?
C62 C61 H61B 108.2 . . ?
P11 C61 H61B 108.2 . . ?
H61A C61 H61B 107.4 . . ?
C61 C62 H62A 109.5 . . ?
C61 C62 H62B 109.5 . . ?
H62A C62 H62B 109.5 . . ?
C61 C62 H62C 109.5 . . ?
H62A C62 H62C 109.5 . . ?
H62B C62 H62C 109.5 . . ?
C64 C63 P11 116.9(8) . . ?
C64 C63 H63A 108.1 . . ?
P11 C63 H63A 108.1 . . ?
C64 C63 H63B 108.1 . . ?
P11 C63 H63B 108.1 . . ?
H63A C63 H63B 107.3 . . ?
C63 C64 H64A 109.5 . . ?
C63 C64 H64B 109.5 . . ?
H64A C64 H64B 109.5 . . ?
C63 C64 H64C 109.5 . . ?
H64A C64 H64C 109.5 . . ?
H64B C64 H64C 109.5 . . ?
C66 C65 P11 115.7(8) . . ?
C66 C65 H65A 108.3 . . ?
P11 C65 H65A 108.3 . . ?
C66 C65 H65B 108.3 . . ?
P11 C65 H65B 108.3 . . ?
H65A C65 H65B 107.4 . . ?
C65 C66 H66A 109.5 . . ?
C65 C66 H66B 109.5 . . ?
H66A C66 H66B 109.5 . . ?
C65 C66 H66C 109.5 . . ?
H66A C66 H66C 109.5 . . ?
H66B C66 H66C 109.5 . . ?
C92 C91 H91A 109.5 . . ?
C92 C91 H91B 109.5 . . ?
H91A C91 H91B 109.5 . . ?
C92 C91 H91C 109.5 . . ?
H91A C91 H91C 109.5 . . ?
H91B C91 H91C 109.5 . . ?
O1 C92 C91 109.7(10) . . ?
O1 C92 H92A 109.7 . . ?
C91 C92 H92A 109.7 . . ?
O1 C92 H92B 109.7 . . ?
C91 C92 H92B 109.7 . . ?
H92A C92 H92B 108.2 . . ?
O1 C94 C95 109.9(13) . . ?
O1 C94 H94A 109.7 . . ?
C95 C94 H94A 109.7 . . ?
O1 C94 H94B 109.7 . . ?
C95 C94 H94B 109.7 . . ?
H94A C94 H94B 108.2 . . ?
C94 C95 H95A 109.5 . . ?
C94 C95 H95B 109.5 . . ?
H95A C95 H95B 109.5 . . ?
C94 C95 H95C 109.5 . . ?
H95A C95 H95C 109.5 . . ?
H95B C95 H95C 109.5 . . ?
Ni6 Ni1 Ni4 113.75(9) . . ?
Ni6 Ni1 Ni10 98.66(8) . . ?
Ni4 Ni1 Ni10 98.30(8) . . ?
Ni6 Ni1 Ni2 162.36(10) . . ?
Ni4 Ni1 Ni2 60.04(7) . . ?
Ni10 Ni1 Ni2 67.64(7) . . ?
Ni6 Ni1 Ni7 69.82(8) . . ?
Ni4 Ni1 Ni7 163.98(9) . . ?
Ni10 Ni1 Ni7 65.71(7) . . ?
Ni2 Ni1 Ni7 111.54(8) . . ?
Ni6 Ni1 Ni14 93.12(8) . . ?
Ni4 Ni1 Ni14 67.50(7) . . ?
Ni10 Ni1 Ni14 164.47(10) . . ?
Ni2 Ni1 Ni14 98.68(8) . . ?
Ni7 Ni1 Ni14 128.49(9) . . ?
Ni6 Ni1 Ni13 129.76(9) . . ?
Ni4 Ni1 Ni13 97.44(8) . . ?
Ni10 Ni1 Ni13 115.28(9) . . ?
Ni2 Ni1 Ni13 67.71(7) . . ?
Ni7 Ni1 Ni13 90.89(8) . . ?
Ni14 Ni1 Ni13 62.79(7) . . ?
Ni6 Ni1 Ni12 69.05(8) . . ?
Ni4 Ni1 Ni12 128.68(9) . . ?
Ni10 Ni1 Ni12 132.81(9) . . ?
Ni2 Ni1 Ni12 128.30(9) . . ?
Ni7 Ni1 Ni12 67.34(7) . . ?
Ni14 Ni1 Ni12 61.20(7) . . ?
Ni13 Ni1 Ni12 60.72(7) . . ?
Ni6 Ni1 Ni11 65.80(7) . . ?
Ni4 Ni1 Ni11 69.67(7) . . ?
Ni10 Ni1 Ni11 59.59(7) . . ?
Ni2 Ni1 Ni11 96.99(8) . . ?
Ni7 Ni1 Ni11 99.54(8) . . ?
Ni14 Ni1 Ni11 117.53(9) . . ?
Ni13 Ni1 Ni11 163.99(9) . . ?
Ni12 Ni1 Ni11 134.70(9) . . ?
Ni6 Ni1 Ni9 58.42(7) . . ?
Ni4 Ni1 Ni9 58.18(7) . . ?
Ni10 Ni1 Ni9 121.61(9) . . ?
Ni2 Ni1 Ni9 118.22(9) . . ?
Ni7 Ni1 Ni9 128.21(9) . . ?
Ni14 Ni1 Ni9 57.22(7) . . ?
Ni13 Ni1 Ni9 119.96(8) . . ?
Ni12 Ni1 Ni9 91.39(8) . . ?
Ni11 Ni1 Ni9 62.08(7) . . ?
Ni6 Ni1 Ni8 126.86(9) . . ?
Ni4 Ni1 Ni8 117.52(9) . . ?
Ni10 Ni1 Ni8 61.57(7) . . ?
Ni2 Ni1 Ni8 57.61(7) . . ?
Ni7 Ni1 Ni8 57.04(7) . . ?
Ni14 Ni1 Ni8 118.28(9) . . ?
Ni13 Ni1 Ni8 55.51(6) . . ?
Ni12 Ni1 Ni8 88.96(8) . . ?
Ni11 Ni1 Ni8 121.11(8) . . ?
Ni9 Ni1 Ni8 174.26(9) . . ?
Ni4 Ni2 S4 134.45(12) . . ?
Ni4 Ni2 Ni1 59.64(7) . . ?
S4 Ni2 Ni1 103.08(11) . . ?
Ni4 Ni2 Ni3 59.07(7) . . ?
S4 Ni2 Ni3 101.68(11) . . ?
Ni1 Ni2 Ni3 113.61(8) . . ?
Ni4 Ni2 Ni5 60.02(7) . . ?
S4 Ni2 Ni5 165.53(12) . . ?
Ni1 Ni2 Ni5 84.76(8) . . ?
Ni3 Ni2 Ni5 85.87(8) . . ?
Ni4 Ni2 Ni8 125.71(9) . . ?
S4 Ni2 Ni8 54.85(10) . . ?
Ni1 Ni2 Ni8 66.23(7) . . ?
Ni3 Ni2 Ni8 153.24(9) . . ?
Ni5 Ni2 Ni8 120.01(9) . . ?
Ni4 Ni2 Ni16 123.97(9) . . ?
S4 Ni2 Ni16 55.13(10) . . ?
Ni1 Ni2 Ni16 154.68(9) . . ?
Ni3 Ni2 Ni16 64.95(7) . . ?
Ni5 Ni2 Ni16 119.49(9) . . ?
Ni8 Ni2 Ni16 103.23(8) . . ?
Ni4 Ni2 Ni25 118.64(9) . . ?
S4 Ni2 Ni25 106.90(11) . . ?
Ni1 Ni2 Ni25 114.77(8) . . ?
Ni3 Ni2 Ni25 114.86(8) . . ?
Ni5 Ni2 Ni25 58.63(7) . . ?
Ni8 Ni2 Ni25 86.78(8) . . ?
Ni16 Ni2 Ni25 86.30(8) . . ?
Ni4 Ni2 Ni20 89.88(8) . . ?
S4 Ni2 Ni20 114.68(11) . . ?
Ni1 Ni2 Ni20 142.10(9) . . ?
Ni3 Ni2 Ni20 56.90(7) . . ?
Ni5 Ni2 Ni20 59.20(7) . . ?
Ni8 Ni2 Ni20 140.30(9) . . ?
Ni16 Ni2 Ni20 60.44(7) . . ?
Ni25 Ni2 Ni20 58.03(7) . . ?
Ni4 Ni2 Ni15 173.86(9) . . ?
S4 Ni2 Ni15 51.62(10) . . ?
Ni1 Ni2 Ni15 122.41(8) . . ?
Ni3 Ni2 Ni15 121.33(9) . . ?
Ni5 Ni2 Ni15 113.90(8) . . ?
Ni8 Ni2 Ni15 57.16(7) . . ?
Ni16 Ni2 Ni15 57.15(7) . . ?
Ni25 Ni2 Ni15 55.28(6) . . ?
Ni20 Ni2 Ni15 85.79(7) . . ?
Ni4 Ni2 Ni10 90.92(8) . . ?
S4 Ni2 Ni10 114.70(11) . . ?
Ni1 Ni2 Ni10 56.02(6) . . ?
Ni3 Ni2 Ni10 143.44(9) . . ?
Ni5 Ni2 Ni10 59.56(7) . . ?
Ni8 Ni2 Ni10 60.66(7) . . ?
Ni16 Ni2 Ni10 140.73(9) . . ?
Ni25 Ni2 Ni10 58.92(7) . . ?
Ni20 Ni2 Ni10 107.40(8) . . ?
Ni15 Ni2 Ni10 86.23(7) . . ?
Ni4 Ni2 Ni13 90.93(7) . . ?
S4 Ni2 Ni13 49.86(10) . . ?
Ni1 Ni2 Ni13 57.34(6) . . ?
Ni3 Ni2 Ni13 101.24(8) . . ?
Ni5 Ni2 Ni13 141.26(9) . . ?
Ni8 Ni2 Ni13 54.86(6) . . ?
Ni16 Ni2 Ni13 97.52(8) . . ?
Ni25 Ni2 Ni13 141.39(9) . . ?
Ni20 Ni2 Ni13 153.11(9) . . ?
Ni15 Ni2 Ni13 94.91(7) . . ?
Ni10 Ni2 Ni13 99.47(7) . . ?
Ni4 Ni3 Ni18 111.86(9) . . ?
Ni4 Ni3 Ni17 162.38(11) . . ?
Ni18 Ni3 Ni17 69.11(8) . . ?
Ni4 Ni3 Ni20 96.09(9) . . ?
Ni18 Ni3 Ni20 99.70(9) . . ?
Ni17 Ni3 Ni20 66.80(8) . . ?
Ni4 Ni3 Ni2 60.19(7) . . ?
Ni18 Ni3 Ni2 161.15(11) . . ?
Ni17 Ni3 Ni2 112.93(9) . . ?
Ni20 Ni3 Ni2 66.09(7) . . ?
Ni4 Ni3 Ni23 98.45(8) . . ?
Ni18 Ni3 Ni23 130.47(10) . . ?
Ni17 Ni3 Ni23 93.07(9) . . ?
Ni20 Ni3 Ni23 115.45(9) . . ?
Ni2 Ni3 Ni23 68.34(7) . . ?
Ni4 Ni3 Ni24 67.74(8) . . ?
Ni18 Ni3 Ni24 92.34(9) . . ?
Ni17 Ni3 Ni24 129.73(10) . . ?
Ni20 Ni3 Ni24 162.71(10) . . ?
Ni2 Ni3 Ni24 99.23(8) . . ?
Ni23 Ni3 Ni24 63.51(8) . . ?
Ni4 Ni3 Ni22 128.65(9) . . ?
Ni18 Ni3 Ni22 69.29(8) . . ?
Ni17 Ni3 Ni22 68.76(8) . . ?
Ni20 Ni3 Ni22 135.16(10) . . ?
Ni2 Ni3 Ni22 129.45(9) . . ?
Ni23 Ni3 Ni22 61.19(8) . . ?
Ni24 Ni3 Ni22 60.97(8) . . ?
Ni4 Ni3 Ni21 66.76(7) . . ?
Ni18 Ni3 Ni21 63.60(8) . . ?
Ni17 Ni3 Ni21 100.05(9) . . ?
Ni20 Ni3 Ni21 62.84(7) . . ?
Ni2 Ni3 Ni21 98.01(9) . . ?
Ni23 Ni3 Ni21 164.09(10) . . ?
Ni24 Ni3 Ni21 112.95(9) . . ?
Ni22 Ni3 Ni21 132.29(10) . . ?
Ni4 Ni3 Ni16 118.44(9) . . ?
Ni18 Ni3 Ni16 127.23(9) . . ?
Ni17 Ni3 Ni16 58.12(7) . . ?
Ni20 Ni3 Ni16 61.21(7) . . ?
Ni2 Ni3 Ni16 58.30(7) . . ?
Ni23 Ni3 Ni16 56.60(7) . . ?
Ni24 Ni3 Ni16 120.08(9) . . ?
Ni22 Ni3 Ni16 90.29(8) . . ?
Ni21 Ni3 Ni16 124.05(9) . . ?
Ni4 Ni3 Ni19 58.23(7) . . ?
Ni18 Ni3 Ni19 57.30(7) . . ?
Ni17 Ni3 Ni19 126.36(9) . . ?
Ni20 Ni3 Ni19 121.97(9) . . ?
Ni2 Ni3 Ni19 118.39(9) . . ?
Ni23 Ni3 Ni19 119.02(9) . . ?
Ni24 Ni3 Ni19 55.53(7) . . ?
Ni22 Ni3 Ni19 89.43(8) . . ?
Ni21 Ni3 Ni19 59.25(7) . . ?
Ni16 Ni3 Ni19 174.85(9) . . ?
Ni4 Ni3 S8 116.89(12) . . ?
Ni18 Ni3 S8 49.61(10) . . ?
Ni17 Ni3 S8 49.31(10) . . ?
Ni20 Ni3 S8 50.48(10) . . ?
Ni2 Ni3 S8 116.29(12) . . ?
Ni23 Ni3 S8 141.91(12) . . ?
Ni24 Ni3 S8 141.59(12) . . ?
Ni22 Ni3 S8 102.12(12) . . ?
Ni21 Ni3 S8 50.80(10) . . ?
Ni16 Ni3 S8 92.21(10) . . ?
Ni19 Ni3 S8 92.87(10) . . ?
Ni3 Ni4 S13 103.53(12) . . ?
Ni3 Ni4 Ni1 115.73(9) . . ?
S13 Ni4 Ni1 102.60(12) . . ?
Ni3 Ni4 Ni2 60.74(7) . . ?
S13 Ni4 Ni2 137.48(13) . . ?
Ni1 Ni4 Ni2 60.32(7) . . ?
Ni3 Ni4 Ni5 87.12(8) . . ?
S13 Ni4 Ni5 161.78(13) . . ?
Ni1 Ni4 Ni5 85.46(8) . . ?
Ni2 Ni4 Ni5 60.67(7) . . ?
Ni3 Ni4 Ni9 156.22(10) . . ?
S13 Ni4 Ni9 55.19(11) . . ?
Ni1 Ni4 Ni9 65.37(7) . . ?
Ni2 Ni4 Ni9 125.69(9) . . ?
Ni5 Ni4 Ni9 116.30(9) . . ?
Ni3 Ni4 Ni27 114.19(9) . . ?
S13 Ni4 Ni27 101.58(12) . . ?
Ni1 Ni4 Ni27 116.28(9) . . ?
Ni2 Ni4 Ni27 120.94(9) . . ?
Ni5 Ni4 Ni27 60.30(7) . . ?
Ni9 Ni4 Ni27 83.14(8) . . ?
Ni3 Ni4 Ni19 67.13(7) . . ?
S13 Ni4 Ni19 54.00(11) . . ?
Ni1 Ni4 Ni19 154.51(10) . . ?
Ni2 Ni4 Ni19 127.83(9) . . ?
Ni5 Ni4 Ni19 119.93(9) . . ?
Ni9 Ni4 Ni19 101.54(8) . . ?
Ni27 Ni4 Ni19 81.68(8) . . ?
Ni3 Ni4 Ni21 58.37(7) . . ?
S13 Ni4 Ni21 112.13(12) . . ?
Ni1 Ni4 Ni21 145.22(9) . . ?
Ni2 Ni4 Ni21 93.22(8) . . ?
Ni5 Ni4 Ni21 60.83(7) . . ?
Ni9 Ni4 Ni21 135.34(9) . . ?
Ni27 Ni4 Ni21 55.85(7) . . ?
Ni19 Ni4 Ni21 59.42(7) . . ?
Ni3 Ni4 Ni14 103.11(9) . . ?
S13 Ni4 Ni14 50.30(10) . . ?
Ni1 Ni4 Ni14 57.17(6) . . ?
Ni2 Ni4 Ni14 92.49(8) . . ?
Ni5 Ni4 Ni14 142.19(9) . . ?
Ni9 Ni4 Ni14 56.19(7) . . ?
Ni27 Ni4 Ni14 138.48(9) . . ?
Ni19 Ni4 Ni14 97.34(8) . . ?
Ni21 Ni4 Ni14 153.70(9) . . ?
Ni3 Ni4 Ni24 57.61(7) . . ?
S13 Ni4 Ni24 50.31(11) . . ?
Ni1 Ni4 Ni24 103.38(8) . . ?
Ni2 Ni4 Ni24 93.33(8) . . ?
Ni5 Ni4 Ni24 144.19(9) . . ?
Ni9 Ni4 Ni24 98.64(8) . . ?
Ni27 Ni4 Ni24 136.49(9) . . ?
Ni19 Ni4 Ni24 55.21(7) . . ?
Ni21 Ni4 Ni24 100.08(8) . . ?
Ni14 Ni4 Ni24 53.94(7) . . ?
Ni3 Ni4 Ni11 142.29(9) . . ?
S13 Ni4 Ni11 114.17(12) . . ?
Ni1 Ni4 Ni11 57.78(7) . . ?
Ni2 Ni4 Ni11 90.17(8) . . ?
Ni5 Ni4 Ni11 56.38(7) . . ?
Ni9 Ni4 Ni11 60.17(7) . . ?
Ni27 Ni4 Ni11 58.51(7) . . ?
Ni19 Ni4 Ni11 136.57(9) . . ?
Ni21 Ni4 Ni11 104.14(8) . . ?
Ni14 Ni4 Ni11 101.49(8) . . ?
Ni24 Ni4 Ni11 155.28(8) . . ?
Ni4 Ni5 Ni25 121.93(9) . . ?
Ni4 Ni5 Ni2 59.31(7) . . ?
Ni25 Ni5 Ni2 62.63(7) . . ?
Ni4 Ni5 Ni29 117.53(9) . . ?
Ni25 Ni5 Ni29 119.32(9) . . ?
Ni2 Ni5 Ni29 167.56(10) . . ?
Ni4 Ni5 Ni27 60.85(7) . . ?
Ni25 Ni5 Ni27 176.05(10) . . ?
Ni2 Ni5 Ni27 120.12(9) . . ?
Ni29 Ni5 Ni27 58.70(8) . . ?
Ni4 Ni5 S14 108.45(13) . . ?
Ni25 Ni5 S14 115.47(12) . . ?
Ni2 Ni5 S14 141.02(14) . . ?
Ni29 Ni5 S14 50.83(12) . . ?
Ni27 Ni5 S14 60.59(11) . . ?
Ni4 Ni5 Ni30 149.77(10) . . ?
Ni25 Ni5 Ni30 65.97(7) . . ?
Ni2 Ni5 Ni30 119.99(9) . . ?
Ni29 Ni5 Ni30 69.33(8) . . ?
Ni27 Ni5 Ni30 110.18(9) . . ?
S14 Ni5 Ni30 50.75(11) . . ?
Ni4 Ni5 Ni11 70.02(7) . . ?
Ni25 Ni5 Ni11 119.76(9) . . ?
Ni2 Ni5 Ni11 97.53(8) . . ?
Ni29 Ni5 Ni11 70.63(8) . . ?
Ni27 Ni5 Ni11 63.39(7) . . ?
S14 Ni5 Ni11 113.28(12) . . ?
Ni30 Ni5 Ni11 134.82(10) . . ?
Ni4 Ni5 Ni20 92.47(8) . . ?
Ni25 Ni5 Ni20 60.92(7) . . ?
Ni2 Ni5 Ni20 64.32(7) . . ?
Ni29 Ni5 Ni20 127.96(9) . . ?
Ni27 Ni5 Ni20 117.10(9) . . ?
S14 Ni5 Ni20 80.71(12) . . ?
Ni30 Ni5 Ni20 64.94(8) . . ?
Ni11 Ni5 Ni20 160.04(10) . . ?
Ni4 Ni5 Ni10 93.70(8) . . ?
Ni25 Ni5 Ni10 61.92(7) . . ?
Ni2 Ni5 Ni10 64.93(7) . . ?
Ni29 Ni5 Ni10 104.42(9) . . ?
Ni27 Ni5 Ni10 121.49(9) . . ?
S14 Ni5 Ni10 152.31(14) . . ?
Ni30 Ni5 Ni10 113.70(9) . . ?
Ni11 Ni5 Ni10 58.35(7) . . ?
Ni20 Ni5 Ni10 115.59(8) . . ?
Ni4 Ni5 Ni21 64.34(7) . . ?
Ni25 Ni5 Ni21 120.78(9) . . ?
Ni2 Ni5 Ni21 94.56(8) . . ?
Ni29 Ni5 Ni21 94.29(9) . . ?
Ni27 Ni5 Ni21 57.12(7) . . ?
S14 Ni5 Ni21 50.94(12) . . ?
Ni30 Ni5 Ni21 86.32(8) . . ?
Ni11 Ni5 Ni21 116.82(8) . . ?
Ni20 Ni5 Ni21 59.98(7) . . ?
Ni10 Ni5 Ni21 156.28(9) . . ?
Ni4 Ni5 Ni26 147.71(9) . . ?
Ni25 Ni5 Ni26 61.79(7) . . ?
Ni2 Ni5 Ni26 113.37(9) . . ?
Ni29 Ni5 Ni26 62.07(8) . . ?
Ni27 Ni5 Ni26 117.68(9) . . ?
S14 Ni5 Ni26 95.33(13) . . ?
Ni30 Ni5 Ni26 62.48(8) . . ?
Ni11 Ni5 Ni26 80.78(8) . . ?
Ni20 Ni5 Ni26 113.16(8) . . ?
Ni10 Ni5 Ni26 58.26(7) . . ?
Ni21 Ni5 Ni26 145.36(9) . . ?
S1 Ni6 S12 153.51(17) . . ?
S1 Ni6 P2 104.10(17) . . ?
S12 Ni6 P2 102.30(17) . . ?
S1 Ni6 Ni1 74.83(12) . . ?
S12 Ni6 Ni1 80.12(12) . . ?
P2 Ni6 Ni1 165.80(18) . . ?
S1 Ni6 Ni9 117.57(13) . . ?
S12 Ni6 Ni9 56.90(12) . . ?
P2 Ni6 Ni9 103.99(17) . . ?
Ni1 Ni6 Ni9 65.34(7) . . ?
S1 Ni6 Ni11 56.49(11) . . ?
S12 Ni6 Ni11 116.79(13) . . ?
P2 Ni6 Ni11 107.25(16) . . ?
Ni1 Ni6 Ni11 60.01(7) . . ?
Ni9 Ni6 Ni11 62.27(7) . . ?
S1 Ni6 Ni7 49.76(11) . . ?
S12 Ni6 Ni7 108.04(14) . . ?
P2 Ni6 Ni7 134.46(17) . . ?
Ni1 Ni6 Ni7 55.57(7) . . ?
Ni9 Ni6 Ni7 120.89(9) . . ?
Ni11 Ni6 Ni7 88.49(7) . . ?
S1 Ni6 Ni12 108.27(13) . . ?
S12 Ni6 Ni12 49.12(12) . . ?
P2 Ni6 Ni12 134.19(15) . . ?
Ni1 Ni6 Ni12 57.52(7) . . ?
Ni9 Ni6 Ni12 88.84(8) . . ?
Ni11 Ni6 Ni12 117.44(8) . . ?
Ni7 Ni6 Ni12 59.24(7) . . ?
S1 Ni7 P1 105.54(17) . . ?
S1 Ni7 S2 155.07(16) . . ?
P1 Ni7 S2 98.82(17) . . ?
S1 Ni7 Ni1 74.06(12) . . ?
P1 Ni7 Ni1 177.50(15) . . ?
S2 Ni7 Ni1 81.83(12) . . ?
S1 Ni7 Ni8 116.79(13) . . ?
P1 Ni7 Ni8 111.89(15) . . ?
S2 Ni7 Ni8 56.48(11) . . ?
Ni1 Ni7 Ni8 66.44(7) . . ?
S1 Ni7 Ni10 55.41(11) . . ?
P1 Ni7 Ni10 120.82(14) . . ?
S2 Ni7 Ni10 115.37(12) . . ?
Ni1 Ni7 Ni10 56.86(6) . . ?
Ni8 Ni7 Ni10 61.85(7) . . ?
S1 Ni7 Ni12 109.59(12) . . ?
P1 Ni7 Ni12 124.28(14) . . ?
S2 Ni7 Ni12 49.98(11) . . ?
Ni1 Ni7 Ni12 57.94(7) . . ?
Ni8 Ni7 Ni12 88.85(8) . . ?
Ni10 Ni7 Ni12 114.64(8) . . ?
S1 Ni7 Ni6 49.46(11) . . ?
P1 Ni7 Ni6 127.06(15) . . ?
S2 Ni7 Ni6 110.48(13) . . ?
Ni1 Ni7 Ni6 54.61(7) . . ?
Ni8 Ni7 Ni6 121.04(9) . . ?
Ni10 Ni7 Ni6 85.22(7) . . ?
Ni12 Ni7 Ni6 60.88(7) . . ?
S3 Ni8 S2 144.27(16) . . ?
S3 Ni8 S4 112.99(15) . . ?
S2 Ni8 S4 100.96(15) . . ?
S3 Ni8 Ni13 154.48(13) . . ?
S2 Ni8 Ni13 57.45(11) . . ?
S4 Ni8 Ni13 56.06(11) . . ?
S3 Ni8 Ni7 95.42(12) . . ?
S2 Ni8 Ni7 55.66(11) . . ?
S4 Ni8 Ni7 148.61(13) . . ?
Ni13 Ni8 Ni7 92.55(8) . . ?
S3 Ni8 Ni15 57.12(11) . . ?
S2 Ni8 Ni15 151.93(14) . . ?
S4 Ni8 Ni15 56.20(11) . . ?
Ni13 Ni8 Ni15 109.73(9) . . ?
Ni7 Ni8 Ni15 151.72(10) . . ?
S3 Ni8 Ni2 86.11(12) . . ?
S2 Ni8 Ni2 121.14(13) . . ?
S4 Ni8 Ni2 61.64(10) . . ?
Ni13 Ni8 Ni2 68.39(7) . . ?
Ni7 Ni8 Ni2 109.69(9) . . ?
Ni15 Ni8 Ni2 65.58(7) . . ?
S3 Ni8 Ni10 53.00(11) . . ?
S2 Ni8 Ni10 115.26(13) . . ?
S4 Ni8 Ni10 124.66(12) . . ?
Ni13 Ni8 Ni10 111.23(9) . . ?
Ni7 Ni8 Ni10 62.54(7) . . ?
Ni15 Ni8 Ni10 92.43(8) . . ?
Ni2 Ni8 Ni10 64.01(7) . . ?
S3 Ni8 Ni1 106.96(12) . . ?
S2 Ni8 Ni1 76.10(12) . . ?
S4 Ni8 Ni1 100.56(11) . . ?
Ni13 Ni8 Ni1 58.49(7) . . ?
Ni7 Ni8 Ni1 56.52(7) . . ?
Ni15 Ni8 Ni1 120.80(8) . . ?
Ni2 Ni8 Ni1 56.16(6) . . ?
Ni10 Ni8 Ni1 54.39(6) . . ?
S11 Ni9 S12 144.80(17) . . ?
S11 Ni9 S13 112.52(17) . . ?
S12 Ni9 S13 100.05(16) . . ?
S11 Ni9 Ni14 156.16(14) . . ?
S12 Ni9 Ni14 56.83(12) . . ?
S13 Ni9 Ni14 55.44(12) . . ?
S11 Ni9 Ni4 89.12(12) . . ?
S12 Ni9 Ni4 119.18(14) . . ?
S13 Ni9 Ni4 61.32(11) . . ?
Ni14 Ni9 Ni4 67.09(8) . . ?
S11 Ni9 Ni6 97.82(14) . . ?
S12 Ni9 Ni6 54.78(11) . . ?
S13 Ni9 Ni6 147.59(14) . . ?
Ni14 Ni9 Ni6 92.16(9) . . ?
Ni4 Ni9 Ni6 110.02(9) . . ?
S11 Ni9 Ni28 57.21(12) . . ?
S12 Ni9 Ni28 148.21(14) . . ?
S13 Ni9 Ni28 55.98(12) . . ?
Ni14 Ni9 Ni28 110.11(10) . . ?
Ni4 Ni9 Ni28 70.56(8) . . ?
Ni6 Ni9 Ni28 154.91(11) . . ?
S11 Ni9 Ni1 110.83(12) . . ?
S12 Ni9 Ni1 74.31(12) . . ?
S13 Ni9 Ni1 100.46(12) . . ?
Ni14 Ni9 Ni1 57.96(7) . . ?
Ni4 Ni9 Ni1 56.45(7) . . ?
Ni6 Ni9 Ni1 56.23(7) . . ?
Ni28 Ni9 Ni1 126.35(9) . . ?
S11 Ni9 Ni11 53.55(11) . . ?
S12 Ni9 Ni11 115.73(13) . . ?
S13 Ni9 Ni11 126.90(12) . . ?
Ni14 Ni9 Ni11 114.16(9) . . ?
Ni4 Ni9 Ni11 67.13(7) . . ?
Ni6 Ni9 Ni11 63.27(7) . . ?
Ni28 Ni9 Ni11 96.03(9) . . ?
Ni1 Ni9 Ni11 57.85(6) . . ?
S3 Ni10 S1 130.05(16) . . ?
S3 Ni10 Ni1 116.06(13) . . ?
S1 Ni10 Ni1 72.35(11) . . ?
S3 Ni10 Ni11 170.84(14) . . ?
S1 Ni10 Ni11 59.02(11) . . ?
Ni1 Ni10 Ni11 63.22(7) . . ?
S3 Ni10 Ni26 93.01(12) . . ?
S1 Ni10 Ni26 108.69(12) . . ?
Ni1 Ni10 Ni26 141.62(10) . . ?
Ni11 Ni10 Ni26 84.03(8) . . ?
S3 Ni10 Ni5 111.03(13) . . ?
S1 Ni10 Ni5 118.92(12) . . ?
Ni1 Ni10 Ni5 82.54(8) . . ?
Ni11 Ni10 Ni5 59.93(7) . . ?
Ni26 Ni10 Ni5 63.03(7) . . ?
S3 Ni10 Ni25 55.01(11) . . ?
S1 Ni10 Ni25 170.43(13) . . ?
Ni1 Ni10 Ni25 113.86(9) . . ?
Ni11 Ni10 Ni25 116.28(9) . . ?
Ni26 Ni10 Ni25 61.84(7) . . ?
Ni5 Ni10 Ni25 56.83(6) . . ?
S3 Ni10 Ni8 52.52(11) . . ?
S1 Ni10 Ni8 106.45(12) . . ?
Ni1 Ni10 Ni8 64.04(7) . . ?
Ni11 Ni10 Ni8 127.20(9) . . ?
Ni26 Ni10 Ni8 142.04(9) . . ?
Ni5 Ni10 Ni8 110.66(9) . . ?
Ni25 Ni10 Ni8 83.05(8) . . ?
S3 Ni10 Ni7 90.01(12) . . ?
S1 Ni10 Ni7 51.22(11) . . ?
Ni1 Ni10 Ni7 57.42(7) . . ?
Ni11 Ni10 Ni7 96.61(8) . . ?
Ni26 Ni10 Ni7 152.56(10) . . ?
Ni5 Ni10 Ni7 139.93(9) . . ?
Ni25 Ni10 Ni7 138.02(9) . . ?
Ni8 Ni10 Ni7 55.61(7) . . ?
S3 Ni10 Ni2 80.32(12) . . ?
S1 Ni10 Ni2 128.60(12) . . ?
Ni1 Ni10 Ni2 56.34(7) . . ?
Ni11 Ni10 Ni2 92.46(8) . . ?
Ni26 Ni10 Ni2 109.50(9) . . ?
Ni5 Ni10 Ni2 55.51(6) . . ?
Ni25 Ni10 Ni2 57.69(6) . . ?
Ni8 Ni10 Ni2 55.33(6) . . ?
Ni7 Ni10 Ni2 97.89(8) . . ?
S16 Ni11 S11 111.86(16) . . ?
S16 Ni11 S1 85.47(15) . . ?
S11 Ni11 S1 131.96(15) . . ?
S16 Ni11 Ni10 80.24(12) . . ?
S11 Ni11 Ni10 164.71(14) . . ?
S1 Ni11 Ni10 55.81(10) . . ?
S16 Ni11 Ni5 82.84(12) . . ?
S11 Ni11 Ni5 109.17(13) . . ?
S1 Ni11 Ni5 117.50(12) . . ?
Ni10 Ni11 Ni5 61.72(7) . . ?
S16 Ni11 Ni1 137.24(13) . . ?
S11 Ni11 Ni1 110.78(13) . . ?
S1 Ni11 Ni1 68.33(11) . . ?
Ni10 Ni11 Ni1 57.19(7) . . ?
Ni5 Ni11 Ni1 80.51(7) . . ?
S16 Ni11 Ni27 96.91(13) . . ?
S11 Ni11 Ni27 52.28(11) . . ?
S1 Ni11 Ni27 173.84(13) . . ?
Ni10 Ni11 Ni27 118.90(9) . . ?
Ni5 Ni11 Ni27 57.42(7) . . ?
Ni1 Ni11 Ni27 106.44(9) . . ?
S16 Ni11 Ni9 162.50(14) . . ?
S11 Ni11 Ni9 51.27(12) . . ?
S1 Ni11 Ni9 102.89(11) . . ?
Ni10 Ni11 Ni9 117.20(9) . . ?
Ni5 Ni11 Ni9 106.09(9) . . ?
Ni1 Ni11 Ni9 60.07(7) . . ?
Ni27 Ni11 Ni9 76.40(8) . . ?
S16 Ni11 Ni6 128.80(14) . . ?
S11 Ni11 Ni6 89.59(12) . . ?
S1 Ni11 Ni6 49.32(10) . . ?
Ni10 Ni11 Ni6 89.61(8) . . ?
Ni5 Ni11 Ni6 134.70(9) . . ?
Ni1 Ni11 Ni6 54.19(7) . . ?
Ni27 Ni11 Ni6 130.74(9) . . ?
Ni9 Ni11 Ni6 54.47(7) . . ?
S16 Ni11 Ni4 135.34(13) . . ?
S11 Ni11 Ni4 78.54(12) . . ?
S1 Ni11 Ni4 120.75(12) . . ?
Ni10 Ni11 Ni4 86.26(8) . . ?
Ni5 Ni11 Ni4 53.60(6) . . ?
Ni1 Ni11 Ni4 52.56(6) . . ?
Ni27 Ni11 Ni4 53.89(7) . . ?
Ni9 Ni11 Ni4 52.69(6) . . ?
Ni6 Ni11 Ni4 93.13(8) . . ?
S16 Ni11 Ni29 45.97(12) . . ?
S11 Ni11 Ni29 87.39(12) . . ?
S1 Ni11 Ni29 129.20(12) . . ?
Ni10 Ni11 Ni29 95.39(8) . . ?
Ni5 Ni11 Ni29 53.74(6) . . ?
Ni1 Ni11 Ni29 134.25(9) . . ?
Ni27 Ni11 Ni29 51.88(7) . . ?
Ni9 Ni11 Ni29 127.91(9) . . ?
Ni6 Ni11 Ni29 171.52(9) . . ?
Ni4 Ni11 Ni29 94.03(8) . . ?
S12 Ni12 S2 157.28(16) . . ?
S12 Ni12 P5 100.7(2) . . ?
S2 Ni12 P5 101.82(19) . . ?
S12 Ni12 Ni1 77.86(12) . . ?
S2 Ni12 Ni1 80.37(11) . . ?
P5 Ni12 Ni1 170.80(16) . . ?
S12 Ni12 Ni13 115.92(13) . . ?
S2 Ni12 Ni13 55.98(11) . . ?
P5 Ni12 Ni13 114.65(18) . . ?
Ni1 Ni12 Ni13 59.05(7) . . ?
S12 Ni12 Ni14 56.07(12) . . ?
S2 Ni12 Ni14 116.11(13) . . ?
P5 Ni12 Ni14 113.39(15) . . ?
Ni1 Ni12 Ni14 58.17(7) . . ?
Ni13 Ni12 Ni14 61.15(7) . . ?
S12 Ni12 Ni7 109.49(13) . . ?
S2 Ni12 Ni7 51.12(11) . . ?
P5 Ni12 Ni7 133.37(15) . . ?
Ni1 Ni12 Ni7 54.72(6) . . ?
Ni13 Ni12 Ni7 83.12(7) . . ?
Ni14 Ni12 Ni7 112.86(8) . . ?
S12 Ni12 Ni6 49.92(11) . . ?
S2 Ni12 Ni6 110.63(12) . . ?
P5 Ni12 Ni6 132.20(18) . . ?
Ni1 Ni12 Ni6 53.43(7) . . ?
Ni13 Ni12 Ni6 112.47(8) . . ?
Ni14 Ni12 Ni6 82.81(8) . . ?
Ni7 Ni12 Ni6 59.89(7) . . ?
S5 Ni13 S4 109.05(16) . . ?
S5 Ni13 S2 142.62(16) . . ?
S4 Ni13 S2 102.03(15) . . ?
S5 Ni13 Ni8 160.59(14) . . ?
S4 Ni13 Ni8 58.31(11) . . ?
S2 Ni13 Ni8 56.54(11) . . ?
S5 Ni13 Ni23 55.75(12) . . ?
S4 Ni13 Ni23 55.74(11) . . ?
S2 Ni13 Ni23 157.47(14) . . ?
Ni8 Ni13 Ni23 106.91(9) . . ?
S5 Ni13 Ni1 108.97(13) . . ?
S4 Ni13 Ni1 107.97(12) . . ?
S2 Ni13 Ni1 79.58(12) . . ?
Ni8 Ni13 Ni1 66.00(7) . . ?
Ni23 Ni13 Ni1 109.02(9) . . ?
S5 Ni13 Ni12 98.51(13) . . ?
S4 Ni13 Ni12 152.41(13) . . ?
S2 Ni13 Ni12 53.07(11) . . ?
Ni8 Ni13 Ni12 94.79(8) . . ?
Ni23 Ni13 Ni12 149.35(10) . . ?
Ni1 Ni13 Ni12 60.23(7) . . ?
S5 Ni13 Ni14 53.98(12) . . ?
S4 Ni13 Ni14 138.74(12) . . ?
S2 Ni13 Ni14 111.58(13) . . ?
Ni8 Ni13 Ni14 123.96(9) . . ?
Ni23 Ni13 Ni14 90.17(8) . . ?
Ni1 Ni13 Ni14 57.98(7) . . ?
Ni12 Ni13 Ni14 59.46(7) . . ?
S5 Ni13 Ni2 104.49(12) . . ?
S4 Ni13 Ni2 57.56(10) . . ?
S2 Ni13 Ni2 109.55(11) . . ?
Ni8 Ni13 Ni2 56.75(7) . . ?
Ni23 Ni13 Ni2 63.68(7) . . ?
Ni1 Ni13 Ni2 54.96(6) . . ?
Ni12 Ni13 Ni2 115.09(8) . . ?
Ni14 Ni13 Ni2 88.24(7) . . ?
S13 Ni14 S5 109.15(17) . . ?
S13 Ni14 S12 101.83(17) . . ?
S5 Ni14 S12 143.27(17) . . ?
S13 Ni14 Ni9 57.94(12) . . ?
S5 Ni14 Ni9 159.79(14) . . ?
S12 Ni14 Ni9 56.58(12) . . ?
S13 Ni14 Ni24 55.99(12) . . ?
S5 Ni14 Ni24 55.58(12) . . ?
S12 Ni14 Ni24 157.66(15) . . ?
Ni9 Ni14 Ni24 106.45(9) . . ?
S13 Ni14 Ni1 107.70(13) . . ?
S5 Ni14 Ni1 109.93(13) . . ?
S12 Ni14 Ni1 77.69(11) . . ?
Ni9 Ni14 Ni1 64.82(7) . . ?
Ni24 Ni14 Ni1 109.77(9) . . ?
S13 Ni14 Ni12 152.55(15) . . ?
S5 Ni14 Ni12 98.30(13) . . ?
S12 Ni14 Ni12 52.87(12) . . ?
Ni9 Ni14 Ni12 95.54(9) . . ?
Ni24 Ni14 Ni12 149.32(10) . . ?
Ni1 Ni14 Ni12 60.63(7) . . ?
S13 Ni14 Ni13 139.29(13) . . ?
S5 Ni14 Ni13 53.76(11) . . ?
S12 Ni14 Ni13 111.08(13) . . ?
Ni9 Ni14 Ni13 123.99(9) . . ?
Ni24 Ni14 Ni13 90.28(9) . . ?
Ni1 Ni14 Ni13 59.22(7) . . ?
Ni12 Ni14 Ni13 59.39(7) . . ?
S13 Ni14 Ni4 57.77(11) . . ?
S5 Ni14 Ni4 103.70(12) . . ?
S12 Ni14 Ni4 109.37(13) . . ?
Ni9 Ni14 Ni4 56.72(7) . . ?
Ni24 Ni14 Ni4 63.18(7) . . ?
Ni1 Ni14 Ni4 55.33(7) . . ?
Ni12 Ni14 Ni4 115.94(8) . . ?
Ni13 Ni14 Ni4 88.32(7) . . ?
P7 Ni15 S6 108.99(16) . . ?
P7 Ni15 S3 110.01(17) . . ?
S6 Ni15 S3 111.95(15) . . ?
P7 Ni15 S4 102.40(17) . . ?
S6 Ni15 S4 111.85(15) . . ?
S3 Ni15 S4 111.20(15) . . ?
P7 Ni15 Ni25 139.28(15) . . ?
S6 Ni15 Ni25 56.84(11) . . ?
S3 Ni15 Ni25 56.99(11) . . ?
S4 Ni15 Ni25 118.32(12) . . ?
P7 Ni15 Ni8 114.47(14) . . ?
S6 Ni15 Ni8 136.49(12) . . ?
S3 Ni15 Ni8 54.40(11) . . ?
S4 Ni15 Ni8 57.12(11) . . ?
Ni25 Ni15 Ni8 89.66(8) . . ?
P7 Ni15 Ni16 114.03(15) . . ?
S6 Ni15 Ni16 54.66(11) . . ?
S3 Ni15 Ni16 135.92(13) . . ?
S4 Ni15 Ni16 57.48(11) . . ?
Ni25 Ni15 Ni16 89.27(8) . . ?
Ni8 Ni15 Ni16 103.55(8) . . ?
P7 Ni15 Ni2 160.90(15) . . ?
S6 Ni15 Ni2 80.66(11) . . ?
S3 Ni15 Ni2 79.93(11) . . ?
S4 Ni15 Ni2 58.51(10) . . ?
Ni25 Ni15 Ni2 59.81(7) . . ?
Ni8 Ni15 Ni2 57.26(7) . . ?
Ni16 Ni15 Ni2 57.44(7) . . ?
S6 Ni16 S7 144.38(16) . . ?
S6 Ni16 S4 112.49(15) . . ?
S7 Ni16 S4 101.01(15) . . ?
S6 Ni16 Ni23 154.75(13) . . ?
S7 Ni16 Ni23 57.93(12) . . ?
S4 Ni16 Ni23 55.44(11) . . ?
S6 Ni16 Ni17 96.15(12) . . ?
S7 Ni16 Ni17 55.70(12) . . ?
S4 Ni16 Ni17 148.46(13) . . ?
Ni23 Ni16 Ni17 93.03(9) . . ?
S6 Ni16 Ni15 56.79(11) . . ?
S7 Ni16 Ni15 151.54(14) . . ?
S4 Ni16 Ni15 55.99(11) . . ?
Ni23 Ni16 Ni15 109.07(9) . . ?
Ni17 Ni16 Ni15 152.04(10) . . ?
S6 Ni16 Ni2 86.39(11) . . ?
S7 Ni16 Ni2 121.54(13) . . ?
S4 Ni16 Ni2 61.32(10) . . ?
Ni23 Ni16 Ni2 68.36(7) . . ?
Ni17 Ni16 Ni2 109.90(9) . . ?
Ni15 Ni16 Ni2 65.41(7) . . ?
S6 Ni16 Ni20 53.49(11) . . ?
S7 Ni16 Ni20 116.47(13) . . ?
S4 Ni16 Ni20 123.41(12) . . ?
Ni23 Ni16 Ni20 111.50(9) . . ?
Ni17 Ni16 Ni20 63.76(8) . . ?
Ni15 Ni16 Ni20 91.58(8) . . ?
Ni2 Ni16 Ni20 63.16(7) . . ?
S6 Ni16 Ni3 108.67(12) . . ?
S7 Ni16 Ni3 75.62(12) . . ?
S4 Ni16 Ni3 100.11(12) . . ?
Ni23 Ni16 Ni3 58.21(7) . . ?
Ni17 Ni16 Ni3 56.44(7) . . ?
Ni15 Ni16 Ni3 121.39(9) . . ?
Ni2 Ni16 Ni3 56.75(6) . . ?
Ni20 Ni16 Ni3 55.46(6) . . ?
S8 Ni17 P3 103.07(18) . . ?
S8 Ni17 S7 153.34(17) . . ?
P3 Ni17 S7 103.58(18) . . ?
S8 Ni17 Ni3 72.99(12) . . ?
P3 Ni17 Ni3 171.82(17) . . ?
S7 Ni17 Ni3 80.53(12) . . ?
S8 Ni17 Ni16 113.30(14) . . ?
P3 Ni17 Ni16 110.81(17) . . ?
S7 Ni17 Ni16 55.84(11) . . ?
Ni3 Ni17 Ni16 65.43(7) . . ?
S8 Ni17 Ni20 53.42(12) . . ?
P3 Ni17 Ni20 114.98(16) . . ?
S7 Ni17 Ni20 113.41(13) . . ?
Ni3 Ni17 Ni20 56.87(7) . . ?
Ni16 Ni17 Ni20 60.39(7) . . ?
S8 Ni17 Ni18 51.12(12) . . ?
P3 Ni17 Ni18 128.03(17) . . ?
S7 Ni17 Ni18 110.18(13) . . ?
Ni3 Ni17 Ni18 55.24(7) . . ?
Ni16 Ni17 Ni18 120.67(9) . . ?
Ni20 Ni17 Ni18 86.32(8) . . ?
S8 Ni17 Ni22 110.22(13) . . ?
P3 Ni17 Ni22 131.13(16) . . ?
S7 Ni17 Ni22 49.78(12) . . ?
Ni3 Ni17 Ni22 56.88(7) . . ?
Ni16 Ni17 Ni22 87.81(8) . . ?
Ni20 Ni17 Ni22 113.49(9) . . ?
Ni18 Ni17 Ni22 60.73(7) . . ?
P4 Ni18 S8 104.8(2) . . ?
P4 Ni18 S9 101.5(2) . . ?
S8 Ni18 S9 153.64(17) . . ?
P4 Ni18 Ni3 172.70(19) . . ?
S8 Ni18 Ni3 73.08(12) . . ?
S9 Ni18 Ni3 81.11(13) . . ?
P4 Ni18 Ni19 108.20(18) . . ?
S8 Ni18 Ni19 116.13(14) . . ?
S9 Ni18 Ni19 56.03(13) . . ?
Ni3 Ni18 Ni19 67.48(8) . . ?
P4 Ni18 Ni21 113.06(18) . . ?
S8 Ni18 Ni21 55.72(12) . . ?
S9 Ni18 Ni21 114.91(14) . . ?
Ni3 Ni18 Ni21 59.85(7) . . ?
Ni19 Ni18 Ni21 61.33(8) . . ?
P4 Ni18 Ni17 128.58(18) . . ?
S8 Ni18 Ni17 50.84(12) . . ?
S9 Ni18 Ni17 109.31(14) . . ?
Ni3 Ni18 Ni17 55.65(7) . . ?
Ni19 Ni18 Ni17 123.08(9) . . ?
Ni21 Ni18 Ni17 90.04(8) . . ?
P4 Ni18 Ni22 129.93(18) . . ?
S8 Ni18 Ni22 109.52(13) . . ?
S9 Ni18 Ni22 49.18(13) . . ?
Ni3 Ni18 Ni22 56.80(7) . . ?
Ni19 Ni18 Ni22 88.18(9) . . ?
Ni21 Ni18 Ni22 116.22(9) . . ?
Ni17 Ni18 Ni22 60.28(7) . . ?
S10 Ni19 S9 142.08(18) . . ?
S10 Ni19 S13 112.40(17) . . ?
S9 Ni19 S13 102.79(18) . . ?
S10 Ni19 Ni24 158.02(15) . . ?
S9 Ni19 Ni24 57.74(13) . . ?
S13 Ni19 Ni24 56.18(12) . . ?
S10 Ni19 Ni18 96.07(13) . . ?
S9 Ni19 Ni18 55.41(13) . . ?
S13 Ni19 Ni18 148.28(15) . . ?
Ni24 Ni19 Ni18 92.26(9) . . ?
S10 Ni19 Ni4 91.08(13) . . ?
S9 Ni19 Ni4 118.99(14) . . ?
S13 Ni19 Ni4 61.05(11) . . ?
Ni24 Ni19 Ni4 67.03(8) . . ?
Ni18 Ni19 Ni4 106.55(9) . . ?
S10 Ni19 Ni28 56.34(12) . . ?
S9 Ni19 Ni28 152.00(15) . . ?
S13 Ni19 Ni28 56.35(12) . . ?
Ni24 Ni19 Ni28 111.02(10) . . ?
Ni18 Ni19 Ni28 151.39(11) . . ?
Ni4 Ni19 Ni28 70.06(8) . . ?
S10 Ni19 Ni21 55.97(12) . . ?
S9 Ni19 Ni21 114.56(14) . . ?
S13 Ni19 Ni21 123.47(13) . . ?
Ni24 Ni19 Ni21 111.97(9) . . ?
Ni18 Ni19 Ni21 61.59(8) . . ?
Ni4 Ni19 Ni21 64.04(7) . . ?
Ni28 Ni19 Ni21 93.34(9) . . ?
S10 Ni19 Ni3 112.01(13) . . ?
S9 Ni19 Ni3 74.25(12) . . ?
S13 Ni19 Ni3 99.35(12) . . ?
Ni24 Ni19 Ni3 57.50(7) . . ?
Ni18 Ni19 Ni3 55.22(7) . . ?
Ni4 Ni19 Ni3 54.64(7) . . ?
Ni28 Ni19 Ni3 123.88(9) . . ?
Ni21 Ni19 Ni3 56.26(7) . . ?
S6 Ni20 S8 130.35(16) . . ?
S6 Ni20 Ni3 116.23(13) . . ?
S8 Ni20 Ni3 71.84(12) . . ?
S6 Ni20 Ni25 55.74(11) . . ?
S8 Ni20 Ni25 168.35(14) . . ?
Ni3 Ni20 Ni25 115.87(9) . . ?
S6 Ni20 Ni5 113.06(13) . . ?
S8 Ni20 Ni5 116.52(13) . . ?
Ni3 Ni20 Ni5 84.33(8) . . ?
Ni25 Ni20 Ni5 58.03(7) . . ?
S6 Ni20 Ni21 172.73(13) . . ?
S8 Ni20 Ni21 55.56(11) . . ?
Ni3 Ni20 Ni21 59.74(7) . . ?
Ni25 Ni20 Ni21 119.41(9) . . ?
Ni5 Ni20 Ni21 61.49(7) . . ?
S6 Ni20 Ni16 53.23(11) . . ?
S8 Ni20 Ni16 107.06(13) . . ?
Ni3 Ni20 Ni16 63.32(7) . . ?
Ni25 Ni20 Ni16 84.52(8) . . ?
Ni5 Ni20 Ni16 112.74(8) . . ?
Ni21 Ni20 Ni16 123.05(9) . . ?
S6 Ni20 Ni2 81.96(11) . . ?
S8 Ni20 Ni2 128.50(13) . . ?
Ni3 Ni20 Ni2 57.01(7) . . ?
Ni25 Ni20 Ni2 58.94(7) . . ?
Ni5 Ni20 Ni2 56.48(6) . . ?
Ni21 Ni20 Ni2 90.84(8) . . ?
Ni16 Ni20 Ni2 56.40(7) . . ?
S6 Ni20 Ni17 90.26(12) . . ?
S8 Ni20 Ni17 51.66(12) . . ?
Ni3 Ni20 Ni17 56.33(7) . . ?
Ni25 Ni20 Ni17 139.57(9) . . ?
Ni5 Ni20 Ni17 140.47(9) . . ?
Ni21 Ni20 Ni17 91.84(8) . . ?
Ni16 Ni20 Ni17 55.85(7) . . ?
Ni2 Ni20 Ni17 98.88(8) . . ?
S6 Ni20 Ni30 98.09(12) . . ?
S8 Ni20 Ni30 106.41(13) . . ?
Ni3 Ni20 Ni30 136.47(9) . . ?
Ni25 Ni20 Ni30 61.94(7) . . ?
Ni5 Ni20 Ni30 56.79(7) . . ?
Ni21 Ni20 Ni30 82.93(8) . . ?
Ni16 Ni20 Ni30 145.65(10) . . ?
Ni2 Ni20 Ni30 106.35(9) . . ?
Ni17 Ni20 Ni30 154.26(9) . . ?
S14 Ni21 S10 96.95(17) . . ?
S14 Ni21 S8 105.19(17) . . ?
S10 Ni21 S8 133.26(17) . . ?
S14 Ni21 Ni27 65.21(13) . . ?
S10 Ni21 Ni27 56.07(12) . . ?
S8 Ni21 Ni27 168.90(15) . . ?
S14 Ni21 Ni3 138.33(14) . . ?
S10 Ni21 Ni3 116.54(13) . . ?
S8 Ni21 Ni3 70.16(12) . . ?
Ni27 Ni21 Ni3 112.74(9) . . ?
S14 Ni21 Ni20 85.55(13) . . ?
S10 Ni21 Ni20 170.08(13) . . ?
S8 Ni21 Ni20 54.37(11) . . ?
Ni27 Ni21 Ni20 117.29(10) . . ?
Ni3 Ni21 Ni20 57.42(7) . . ?
S14 Ni21 Ni19 144.48(14) . . ?
S10 Ni21 Ni19 52.29(12) . . ?
S8 Ni21 Ni19 109.26(14) . . ?
Ni27 Ni21 Ni19 81.18(8) . . ?
Ni3 Ni21 Ni19 64.49(8) . . ?
Ni20 Ni21 Ni19 121.80(9) . . ?
S14 Ni21 Ni18 152.44(15) . . ?
S10 Ni21 Ni18 90.38(14) . . ?
S8 Ni21 Ni18 52.99(12) . . ?
Ni27 Ni21 Ni18 137.90(10) . . ?
Ni3 Ni21 Ni18 56.55(7) . . ?
Ni20 Ni21 Ni18 91.78(9) . . ?
Ni19 Ni21 Ni18 57.08(8) . . ?
S14 Ni21 Ni5 61.49(13) . . ?
S10 Ni21 Ni5 114.33(13) . . ?
S8 Ni21 Ni5 112.41(13) . . ?
Ni27 Ni21 Ni5 58.76(7) . . ?
Ni3 Ni21 Ni5 81.56(8) . . ?
Ni20 Ni21 Ni5 58.53(7) . . ?
Ni19 Ni21 Ni5 111.10(9) . . ?
Ni18 Ni21 Ni5 137.91(10) . . ?
S14 Ni21 Ni4 109.26(14) . . ?
S10 Ni21 Ni4 84.05(12) . . ?
S8 Ni21 Ni4 124.25(13) . . ?
Ni27 Ni21 Ni4 57.89(7) . . ?
Ni3 Ni21 Ni4 54.87(7) . . ?
Ni20 Ni21 Ni4 86.06(8) . . ?
Ni19 Ni21 Ni4 56.54(7) . . ?
Ni18 Ni21 Ni4 97.88(9) . . ?
Ni5 Ni21 Ni4 54.83(6) . . ?
S9 Ni22 S7 157.85(19) . . ?
S9 Ni22 P6 101.0(2) . . ?
S7 Ni22 P6 100.6(2) . . ?
S9 Ni22 Ni3 79.96(13) . . ?
S7 Ni22 Ni3 79.51(12) . . ?
P6 Ni22 Ni3 171.11(19) . . ?
S9 Ni22 Ni24 56.74(13) . . ?
S7 Ni22 Ni24 117.65(13) . . ?
P6 Ni22 Ni24 113.73(18) . . ?
Ni3 Ni22 Ni24 59.29(7) . . ?
S9 Ni22 Ni23 117.69(14) . . ?
S7 Ni22 Ni23 56.69(12) . . ?
P6 Ni22 Ni23 113.53(18) . . ?
Ni3 Ni22 Ni23 59.01(7) . . ?
Ni24 Ni22 Ni23 62.15(7) . . ?
S9 Ni22 Ni17 109.33(15) . . ?
S7 Ni22 Ni17 50.86(12) . . ?
P6 Ni22 Ni17 132.25(18) . . ?
Ni3 Ni22 Ni17 54.37(7) . . ?
Ni24 Ni22 Ni17 113.66(9) . . ?
Ni23 Ni22 Ni17 83.95(8) . . ?
S9 Ni22 Ni18 50.50(13) . . ?
S7 Ni22 Ni18 109.51(14) . . ?
P6 Ni22 Ni18 133.15(18) . . ?
Ni3 Ni22 Ni18 53.91(7) . . ?
Ni24 Ni22 Ni18 83.09(8) . . ?
Ni23 Ni22 Ni18 112.91(9) . . ?
Ni17 Ni22 Ni18 58.99(7) . . ?
S5 Ni23 S4 109.55(15) . . ?
S5 Ni23 S7 143.11(16) . . ?
S4 Ni23 S7 101.87(15) . . ?
S5 Ni23 Ni16 160.56(14) . . ?
S4 Ni23 Ni16 58.66(11) . . ?
S7 Ni23 Ni16 55.78(11) . . ?
S5 Ni23 Ni13 55.88(12) . . ?
S4 Ni23 Ni13 56.13(11) . . ?
S7 Ni23 Ni13 157.88(14) . . ?
Ni16 Ni23 Ni13 107.19(9) . . ?
S5 Ni23 Ni3 108.78(13) . . ?
S4 Ni23 Ni3 107.89(12) . . ?
S7 Ni23 Ni3 78.27(12) . . ?
Ni16 Ni23 Ni3 65.19(7) . . ?
Ni13 Ni23 Ni3 108.86(9) . . ?
S5 Ni23 Ni22 97.86(13) . . ?
S4 Ni23 Ni22 152.54(13) . . ?
S7 Ni23 Ni22 53.28(11) . . ?
Ni16 Ni23 Ni22 94.53(9) . . ?
Ni13 Ni23 Ni22 148.54(10) . . ?
Ni3 Ni23 Ni22 59.80(7) . . ?
S5 Ni23 Ni24 53.37(12) . . ?
S4 Ni23 Ni24 139.06(13) . . ?
S7 Ni23 Ni24 111.08(13) . . ?
Ni16 Ni23 Ni24 123.58(9) . . ?
Ni13 Ni23 Ni24 89.89(9) . . ?
Ni3 Ni23 Ni24 58.41(7) . . ?
Ni22 Ni23 Ni24 58.85(7) . . ?
S5 Ni23 Ni2 104.25(13) . . ?
S4 Ni23 Ni2 57.45(10) . . ?
S7 Ni23 Ni2 108.79(12) . . ?
Ni16 Ni23 Ni2 56.70(7) . . ?
Ni13 Ni23 Ni2 63.23(7) . . ?
Ni3 Ni23 Ni2 55.23(7) . . ?
Ni22 Ni23 Ni2 114.97(9) . . ?
Ni24 Ni23 Ni2 88.55(8) . . ?
S5 Ni24 S13 109.41(16) . . ?
S5 Ni24 S9 143.01(18) . . ?
S13 Ni24 S9 102.40(17) . . ?
S5 Ni24 Ni19 160.69(14) . . ?
S13 Ni24 Ni19 57.44(12) . . ?
S9 Ni24 Ni19 56.02(13) . . ?
S5 Ni24 Ni14 56.03(12) . . ?
S13 Ni24 Ni14 55.82(12) . . ?
S9 Ni24 Ni14 158.15(15) . . ?
Ni19 Ni24 Ni14 106.42(10) . . ?
S5 Ni24 Ni3 108.52(13) . . ?
S13 Ni24 Ni3 107.49(13) . . ?
S9 Ni24 Ni3 78.33(13) . . ?
Ni19 Ni24 Ni3 66.97(8) . . ?
Ni14 Ni24 Ni3 108.22(9) . . ?
S5 Ni24 Ni22 98.02(13) . . ?
S13 Ni24 Ni22 152.48(14) . . ?
S9 Ni24 Ni22 52.95(12) . . ?
Ni19 Ni24 Ni22 95.44(9) . . ?
Ni14 Ni24 Ni22 148.48(10) . . ?
Ni3 Ni24 Ni22 59.74(7) . . ?
S5 Ni24 Ni23 53.43(12) . . ?
S13 Ni24 Ni23 138.36(13) . . ?
S9 Ni24 Ni23 110.89(14) . . ?
Ni19 Ni24 Ni23 125.03(9) . . ?
Ni14 Ni24 Ni23 89.64(9) . . ?
Ni3 Ni24 Ni23 58.08(7) . . ?
Ni22 Ni24 Ni23 58.99(7) . . ?
S5 Ni24 Ni4 103.79(13) . . ?
S13 Ni24 Ni4 57.61(11) . . ?
S9 Ni24 Ni4 109.03(14) . . ?
Ni19 Ni24 Ni4 57.76(7) . . ?
Ni14 Ni24 Ni4 62.88(7) . . ?
Ni3 Ni24 Ni4 54.65(7) . . ?
Ni22 Ni24 Ni4 114.35(9) . . ?
Ni23 Ni24 Ni4 87.61(8) . . ?
S15 Ni25 S6 108.31(15) . . ?
S15 Ni25 S3 110.29(16) . . ?
S6 Ni25 S3 112.03(15) . . ?
S15 Ni25 Ni15 138.90(13) . . ?
S6 Ni25 Ni15 56.90(11) . . ?
S3 Ni25 Ni15 57.00(11) . . ?
S15 Ni25 Ni5 97.43(12) . . ?
S6 Ni25 Ni5 114.33(13) . . ?
S3 Ni25 Ni5 113.37(12) . . ?
Ni15 Ni25 Ni5 123.66(9) . . ?
S15 Ni25 Ni20 106.58(14) . . ?
S6 Ni25 Ni20 54.00(11) . . ?
S3 Ni25 Ni20 143.14(13) . . ?
Ni15 Ni25 Ni20 94.12(8) . . ?
Ni5 Ni25 Ni20 61.05(7) . . ?
S15 Ni25 Ni2 156.16(13) . . ?
S6 Ni25 Ni2 83.50(11) . . ?
S3 Ni25 Ni2 82.70(11) . . ?
Ni15 Ni25 Ni2 64.91(7) . . ?
Ni5 Ni25 Ni2 58.74(7) . . ?
Ni20 Ni25 Ni2 63.03(7) . . ?
S15 Ni25 Ni10 107.72(13) . . ?
S6 Ni25 Ni10 143.96(13) . . ?
S3 Ni25 Ni10 52.96(11) . . ?
Ni15 Ni25 Ni10 94.18(8) . . ?
Ni5 Ni25 Ni10 61.25(7) . . ?
Ni20 Ni25 Ni10 115.12(8) . . ?
Ni2 Ni25 Ni10 63.39(7) . . ?
S15 Ni25 Ni26 51.02(11) . . ?
S6 Ni25 Ni26 155.69(13) . . ?
S3 Ni25 Ni26 89.46(12) . . ?
Ni15 Ni25 Ni26 146.29(10) . . ?
Ni5 Ni25 Ni26 63.33(7) . . ?
Ni20 Ni25 Ni26 114.55(9) . . ?
Ni2 Ni25 Ni26 111.49(8) . . ?
Ni10 Ni25 Ni26 58.55(7) . . ?
S15 Ni25 Ni30 49.70(12) . . ?
S6 Ni25 Ni30 97.05(12) . . ?
S3 Ni25 Ni30 149.79(13) . . ?
Ni15 Ni25 Ni30 153.19(10) . . ?
Ni5 Ni25 Ni30 57.66(7) . . ?
Ni20 Ni25 Ni30 62.11(7) . . ?
Ni2 Ni25 Ni30 109.53(9) . . ?
Ni10 Ni25 Ni30 106.76(8) . . ?
Ni26 Ni25 Ni30 60.46(8) . . ?
S15 Ni26 P9 95.64(18) . . ?
S15 Ni26 S16 161.9(2) . . ?
P9 Ni26 S16 94.67(18) . . ?
S15 Ni26 Ni10 110.66(13) . . ?
P9 Ni26 Ni10 107.14(19) . . ?
S16 Ni26 Ni10 80.30(12) . . ?
S15 Ni26 Ni25 53.00(11) . . ?
P9 Ni26 Ni25 122.35(16) . . ?
S16 Ni26 Ni25 130.71(14) . . ?
Ni10 Ni26 Ni25 59.62(7) . . ?
S15 Ni26 Ni29 112.42(15) . . ?
P9 Ni26 Ni29 131.13(16) . . ?
S16 Ni26 Ni29 50.16(13) . . ?
Ni10 Ni26 Ni29 99.44(8) . . ?
Ni25 Ni26 Ni29 106.42(10) . . ?
S15 Ni26 Ni5 92.36(14) . . ?
P9 Ni26 Ni5 165.62(19) . . ?
S16 Ni26 Ni5 80.93(13) . . ?
Ni10 Ni26 Ni5 58.71(7) . . ?
Ni25 Ni26 Ni5 54.89(6) . . ?
Ni29 Ni26 Ni5 55.03(7) . . ?
S15 Ni26 Ni30 50.10(13) . . ?
P9 Ni26 Ni30 138.00(17) . . ?
S16 Ni26 Ni30 113.58(15) . . ?
Ni10 Ni26 Ni30 107.76(9) . . ?
Ni25 Ni26 Ni30 60.66(7) . . ?
Ni29 Ni26 Ni30 63.65(8) . . ?
Ni5 Ni26 Ni30 55.29(7) . . ?
S11 Ni27 S10 114.04(16) . . ?
S11 Ni27 Ni28 59.26(12) . . ?
S10 Ni27 Ni28 57.66(12) . . ?
S11 Ni27 Ni29 101.75(14) . . ?
S10 Ni27 Ni29 135.80(14) . . ?
Ni28 Ni27 Ni29 159.70(11) . . ?
S11 Ni27 Ni21 152.10(15) . . ?
S10 Ni27 Ni21 57.74(11) . . ?
Ni28 Ni27 Ni21 100.28(10) . . ?
Ni29 Ni27 Ni21 100.01(9) . . ?
S11 Ni27 Ni5 113.06(13) . . ?
S10 Ni27 Ni5 121.29(13) . . ?
Ni28 Ni27 Ni5 130.90(11) . . ?
Ni29 Ni27 Ni5 60.44(7) . . ?
Ni21 Ni27 Ni5 64.12(8) . . ?
S11 Ni27 Ni4 88.21(13) . . ?
S10 Ni27 Ni4 89.86(13) . . ?
Ni28 Ni27 Ni4 72.16(9) . . ?
Ni29 Ni27 Ni4 117.28(10) . . ?
Ni21 Ni27 Ni4 66.26(8) . . ?
Ni5 Ni27 Ni4 58.85(7) . . ?
S11 Ni27 S14 152.63(18) . . ?
S10 Ni27 S14 89.63(16) . . ?
Ni28 Ni27 S14 146.96(15) . . ?
Ni29 Ni27 S14 51.04(12) . . ?
Ni21 Ni27 S14 52.70(12) . . ?
Ni5 Ni27 S14 59.73(11) . . ?
Ni4 Ni27 S14 106.21(13) . . ?
S11 Ni27 Ni11 54.44(11) . . ?
S10 Ni27 Ni11 153.65(15) . . ?
Ni28 Ni27 Ni11 100.72(9) . . ?
Ni29 Ni27 Ni11 69.55(8) . . ?
Ni21 Ni27 Ni11 119.41(9) . . ?
Ni5 Ni27 Ni11 59.19(7) . . ?
Ni4 Ni27 Ni11 67.60(7) . . ?
S14 Ni27 Ni11 109.13(13) . . ?
P8 Ni28 S10 109.33(19) . . ?
P8 Ni28 S13 105.81(18) . . ?
S10 Ni28 S13 109.09(17) . . ?
P8 Ni28 S11 112.78(19) . . ?
S10 Ni28 S11 110.26(17) . . ?
S13 Ni28 S11 109.44(16) . . ?
P8 Ni28 Ni27 143.89(18) . . ?
S10 Ni28 Ni27 57.22(12) . . ?
S13 Ni28 Ni27 110.28(13) . . ?
S11 Ni28 Ni27 55.73(11) . . ?
P8 Ni28 Ni19 116.63(16) . . ?
S10 Ni28 Ni19 53.69(13) . . ?
S13 Ni28 Ni19 55.68(12) . . ?
S11 Ni28 Ni19 130.58(13) . . ?
Ni27 Ni28 Ni19 83.76(9) . . ?
P8 Ni28 Ni9 117.79(17) . . ?
S10 Ni28 Ni9 132.80(13) . . ?
S13 Ni28 Ni9 56.34(12) . . ?
S11 Ni28 Ni9 53.72(12) . . ?
Ni27 Ni28 Ni9 84.37(9) . . ?
Ni19 Ni28 Ni9 100.03(9) . . ?
P8 Ni28 Ni4 160.42(17) . . ?
S10 Ni28 Ni4 80.46(11) . . ?
S13 Ni28 Ni4 54.61(10) . . ?
S11 Ni28 Ni4 77.71(12) . . ?
Ni27 Ni28 Ni4 55.69(7) . . ?
Ni19 Ni28 Ni4 54.87(7) . . ?
Ni9 Ni28 Ni4 53.93(7) . . ?
S16 Ni29 S14 151.05(18) . . ?
S16 Ni29 P10 103.3(2) . . ?
S14 Ni29 P10 105.6(2) . . ?
S16 Ni29 Ni27 107.51(14) . . ?
S14 Ni29 Ni27 66.34(13) . . ?
P10 Ni29 Ni27 103.5(2) . . ?
S16 Ni29 Ni5 87.15(13) . . ?
S14 Ni29 Ni5 64.87(13) . . ?
P10 Ni29 Ni5 163.6(2) . . ?
Ni27 Ni29 Ni5 60.86(8) . . ?
S16 Ni29 Ni26 51.68(12) . . ?
S14 Ni29 Ni26 105.30(14) . . ?
P10 Ni29 Ni26 133.5(2) . . ?
Ni27 Ni29 Ni26 120.48(10) . . ?
Ni5 Ni29 Ni26 62.90(7) . . ?
S16 Ni29 Ni30 110.09(14) . . ?
S14 Ni29 Ni30 48.56(12) . . ?
P10 Ni29 Ni30 129.11(16) . . ?
Ni27 Ni29 Ni30 101.69(10) . . ?
Ni5 Ni29 Ni30 55.72(7) . . ?
Ni26 Ni29 Ni30 58.63(7) . . ?
S16 Ni29 Ni11 50.06(11) . . ?
S14 Ni29 Ni11 112.21(14) . . ?
P10 Ni29 Ni11 122.40(16) . . ?
Ni27 Ni29 Ni11 58.58(7) . . ?
Ni5 Ni29 Ni11 55.63(7) . . ?
Ni26 Ni29 Ni11 74.84(7) . . ?
Ni30 Ni29 Ni11 108.48(8) . . ?
S15 Ni30 S14 154.96(19) . . ?
S15 Ni30 P11 97.50(17) . . ?
S14 Ni30 P11 104.92(18) . . ?
S15 Ni30 Ni5 98.43(13) . . ?
S14 Ni30 Ni5 64.36(12) . . ?
P11 Ni30 Ni5 156.18(17) . . ?
S15 Ni30 Ni26 50.74(12) . . ?
S14 Ni30 Ni26 104.22(15) . . ?
P11 Ni30 Ni26 140.91(16) . . ?
Ni5 Ni30 Ni26 62.23(7) . . ?
S15 Ni30 Ni25 52.26(11) . . ?
S14 Ni30 Ni25 119.34(14) . . ?
P11 Ni30 Ni25 123.94(14) . . ?
Ni5 Ni30 Ni25 56.36(7) . . ?
Ni26 Ni30 Ni25 58.87(7) . . ?
S15 Ni30 Ni20 103.23(13) . . ?
S14 Ni30 Ni20 83.61(14) . . ?
P11 Ni30 Ni20 100.78(15) . . ?
Ni5 Ni30 Ni20 58.26(7) . . ?
Ni26 Ni30 Ni20 107.85(8) . . ?
Ni25 Ni30 Ni20 55.96(7) . . ?
S15 Ni30 Ni29 107.23(14) . . ?
S14 Ni30 Ni29 48.36(14) . . ?
P11 Ni30 Ni29 134.99(14) . . ?
Ni5 Ni30 Ni29 54.96(7) . . ?
Ni26 Ni30 Ni29 57.72(7) . . ?
Ni25 Ni30 Ni29 100.79(8) . . ?
Ni20 Ni30 Ni29 109.03(8) . . ?
C94 O1 C92 113.1(13) . . ?
C3 P1 C1 101.8(5) . . ?
C3 P1 C5 101.7(5) . . ?
C1 P1 C5 100.2(5) . . ?
C3 P1 Ni7 120.0(8) . . ?
C1 P1 Ni7 111.7(8) . . ?
C5 P1 Ni7 118.5(8) . . ?
C9 P2 C7 102.0(5) . . ?
C9 P2 C11 101.6(5) . . ?
C7 P2 C11 101.5(5) . . ?
C9 P2 Ni6 119.2(8) . . ?
C7 P2 Ni6 114.5(8) . . ?
C11 P2 Ni6 115.6(8) . . ?
C17 P3 C15 101.3(5) . . ?
C17 P3 C13 101.0(5) . . ?
C15 P3 C13 100.8(5) . . ?
C17 P3 Ni17 119.9(8) . . ?
C15 P3 Ni17 112.6(6) . . ?
C13 P3 Ni17 118.3(8) . . ?
C21 P4 C19 101.9(5) . . ?
C21 P4 C23 101.4(5) . . ?
C19 P4 C23 100.9(5) . . ?
C21 P4 Ni18 115.5(8) . . ?
C19 P4 Ni18 120.2(8) . . ?
C23 P4 Ni18 114.1(7) . . ?
C29 P5 C25 101.5(5) . . ?
C29 P5 C27 99.7(5) . . ?
C25 P5 C27 99.3(5) . . ?
C29 P5 Ni12 125.6(7) . . ?
C25 P5 Ni12 116.6(8) . . ?
C27 P5 Ni12 110.0(8) . . ?
C35 P6 C33 101.6(5) . . ?
C35 P6 C31 101.3(5) . . ?
C33 P6 C31 100.3(5) . . ?
C35 P6 Ni22 123.8(7) . . ?
C33 P6 Ni22 116.7(8) . . ?
C31 P6 Ni22 109.7(7) . . ?
C37 P7 C39 101.2(5) . . ?
C37 P7 C41 101.2(5) . . ?
C39 P7 C41 99.3(5) . . ?
C37 P7 Ni15 118.3(7) . . ?
C39 P7 Ni15 117.6(7) . . ?
C41 P7 Ni15 116.2(7) . . ?
C43 P8 C45 102.1(5) . . ?
C43 P8 C47 101.7(5) . . ?
C45 P8 C47 101.3(5) . . ?
C43 P8 Ni28 117.2(7) . . ?
C45 P8 Ni28 118.7(7) . . ?
C47 P8 Ni28 113.2(7) . . ?
C49 P9 C53 102.0(5) . . ?
C49 P9 C51 101.9(5) . . ?
C53 P9 C51 101.4(5) . . ?
C49 P9 Ni26 116.1(6) . . ?
C53 P9 Ni26 121.3(8) . . ?
C51 P9 Ni26 111.5(8) . . ?
C55 P10 C57 101.8(5) . . ?
C55 P10 C59 101.2(5) . . ?
C57 P10 C59 101.1(5) . . ?
C55 P10 Ni29 121.2(8) . . ?
C57 P10 Ni29 118.4(8) . . ?
C59 P10 Ni29 110.1(7) . . ?
C63 P11 C65 102.2(5) . . ?
C63 P11 C61 102.0(5) . . ?
C65 P11 C61 101.6(5) . . ?
C63 P11 Ni30 111.7(6) . . ?
C65 P11 Ni30 118.6(8) . . ?
C61 P11 Ni30 118.4(8) . . ?
Ni6 S1 Ni7 80.78(14) . . ?
Ni6 S1 Ni10 112.70(17) . . ?
Ni7 S1 Ni10 73.37(13) . . ?
Ni6 S1 Ni11 74.19(13) . . ?
Ni7 S1 Ni11 116.69(17) . . ?
Ni10 S1 Ni11 65.17(11) . . ?
Ni12 S2 Ni7 78.90(15) . . ?
Ni12 S2 Ni8 113.85(17) . . ?
Ni7 S2 Ni8 67.86(12) . . ?
Ni12 S2 Ni13 70.95(13) . . ?
Ni7 S2 Ni13 105.65(16) . . ?
Ni8 S2 Ni13 66.01(11) . . ?
Ni8 S3 Ni10 74.48(13) . . ?
Ni8 S3 Ni25 103.82(16) . . ?
Ni10 S3 Ni25 72.03(13) . . ?
Ni8 S3 Ni15 68.48(12) . . ?
Ni10 S3 Ni15 113.27(17) . . ?
Ni25 S3 Ni15 66.01(12) . . ?
Ni23 S4 Ni13 68.14(12) . . ?
Ni23 S4 Ni15 128.84(17) . . ?
Ni13 S4 Ni15 128.55(17) . . ?
Ni23 S4 Ni8 123.46(17) . . ?
Ni13 S4 Ni8 65.62(12) . . ?
Ni15 S4 Ni8 66.68(12) . . ?
Ni23 S4 Ni16 65.90(12) . . ?
Ni13 S4 Ni16 123.17(17) . . ?
Ni15 S4 Ni16 66.53(12) . . ?
Ni8 S4 Ni16 117.91(16) . . ?
Ni23 S4 Ni2 73.08(12) . . ?
Ni13 S4 Ni2 72.59(12) . . ?
Ni15 S4 Ni2 69.87(11) . . ?
Ni8 S4 Ni2 63.51(11) . . ?
Ni16 S4 Ni2 63.55(10) . . ?
Ni24 S5 Ni23 73.19(13) . . ?
Ni24 S5 Ni13 109.83(17) . . ?
Ni23 S5 Ni13 68.37(13) . . ?
Ni24 S5 Ni14 68.39(13) . . ?
Ni23 S5 Ni14 109.27(17) . . ?
Ni13 S5 Ni14 72.26(13) . . ?
Ni16 S6 Ni20 73.28(13) . . ?
Ni16 S6 Ni25 103.40(15) . . ?
Ni20 S6 Ni25 70.27(12) . . ?
Ni16 S6 Ni15 68.56(12) . . ?
Ni20 S6 Ni15 111.32(16) . . ?
Ni25 S6 Ni15 66.26(12) . . ?
Ni22 S7 Ni17 79.36(15) . . ?
Ni22 S7 Ni16 113.67(18) . . ?
Ni17 S7 Ni16 68.46(13) . . ?
Ni22 S7 Ni23 70.02(14) . . ?
Ni17 S7 Ni23 106.30(17) . . ?
Ni16 S7 Ni23 66.29(12) . . ?
Ni17 S8 Ni18 78.03(16) . . ?
Ni17 S8 Ni20 74.93(14) . . ?
Ni18 S8 Ni20 114.48(18) . . ?
Ni17 S8 Ni21 116.67(18) . . ?
Ni18 S8 Ni21 71.29(13) . . ?
Ni20 S8 Ni21 70.07(13) . . ?
Ni17 S8 Ni3 57.70(11) . . ?
Ni18 S8 Ni3 57.31(11) . . ?
Ni20 S8 Ni3 57.68(10) . . ?
Ni21 S8 Ni3 59.04(10) . . ?
Ni22 S9 Ni18 80.32(16) . . ?
Ni22 S9 Ni19 115.23(19) . . ?
Ni18 S9 Ni19 68.56(15) . . ?
Ni22 S9 Ni24 70.30(14) . . ?
Ni18 S9 Ni24 105.78(18) . . ?
Ni19 S9 Ni24 66.24(13) . . ?
Ni19 S10 Ni27 97.03(16) . . ?
Ni19 S10 Ni28 69.97(14) . . ?
Ni27 S10 Ni28 65.12(13) . . ?
Ni19 S10 Ni21 71.73(13) . . ?
Ni27 S10 Ni21 66.19(13) . . ?
Ni28 S10 Ni21 111.66(17) . . ?
Ni9 S11 Ni27 98.51(17) . . ?
Ni9 S11 Ni11 75.18(14) . . ?
Ni27 S11 Ni11 73.29(13) . . ?
Ni9 S11 Ni28 69.07(14) . . ?
Ni27 S11 Ni28 65.01(13) . . ?
Ni11 S11 Ni28 118.59(18) . . ?
Ni12 S12 Ni6 80.95(15) . . ?
Ni12 S12 Ni9 115.50(17) . . ?
Ni6 S12 Ni9 68.32(13) . . ?
Ni12 S12 Ni14 71.06(14) . . ?
Ni6 S12 Ni14 107.08(16) . . ?
Ni9 S12 Ni14 66.58(12) . . ?
Ni14 S13 Ni24 68.19(13) . . ?
Ni14 S13 Ni19 124.40(18) . . ?
Ni24 S13 Ni19 66.38(13) . . ?
Ni14 S13 Ni28 132.20(19) . . ?
Ni24 S13 Ni28 131.98(18) . . ?
Ni19 S13 Ni28 67.97(13) . . ?
Ni14 S13 Ni9 66.62(13) . . ?
Ni24 S13 Ni9 123.79(18) . . ?
Ni19 S13 Ni9 117.68(18) . . ?
Ni28 S13 Ni9 67.68(14) . . ?
Ni14 S13 Ni4 71.93(12) . . ?
Ni24 S13 Ni4 72.08(12) . . ?
Ni19 S13 Ni4 64.95(11) . . ?
Ni28 S13 Ni4 75.95(13) . . ?
Ni9 S13 Ni4 63.49(11) . . ?
Ni29 S14 Ni30 83.08(18) . . ?
Ni29 S14 Ni21 119.25(19) . . ?
Ni30 S14 Ni21 107.67(19) . . ?
Ni29 S14 Ni5 64.30(13) . . ?
Ni30 S14 Ni5 64.90(13) . . ?
Ni21 S14 Ni5 67.56(13) . . ?
Ni29 S14 Ni27 62.61(13) . . ?
Ni30 S14 Ni27 123.07(19) . . ?
Ni21 S14 Ni27 62.09(12) . . ?
Ni5 S14 Ni27 59.68(11) . . ?
Ni30 S15 Ni26 79.16(15) . . ?
Ni30 S15 Ni25 78.04(15) . . ?
Ni26 S15 Ni25 75.98(13) . . ?
Ni29 S16 Ni26 78.16(16) . . ?
Ni29 S16 Ni11 83.97(17) . . ?
Ni26 S16 Ni11 101.49(17) . . ?

_refine_diff_density_max         2.484
_refine_diff_density_min         -1.804
_refine_diff_density_rms         0.267


####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_Complex_2
_database_code_depnum_ccdc_archive 'CCDC 2150614'
loop_
_audit_author_name
_audit_author_address
'Guang Wu'
;UCSB
United States of America
;
_audit_update_record             
;
2022-02-07 deposited with the CCDC.	2022-04-11 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2014/7
_shelx_SHELXL_version_number     2014/7
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C65 H162 Ni26 P10 S14'
_chemical_formula_weight         3228.94

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ni Ni 0.3393 1.1124 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_H-M_alt        'P 21/n'
_space_group_name_Hall           '-P 2yn'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'

_cell_length_a                   19.007(15)
_cell_length_b                   25.85(2)
_cell_length_c                   23.475(19)
_cell_angle_alpha                90
_cell_angle_beta                 99.628(7)
_cell_angle_gamma                90
_cell_volume                     11374(16)
_cell_formula_units_Z            4
_cell_measurement_temperature    116(2)
_cell_measurement_reflns_used    1325
_cell_measurement_theta_min      2.34
_cell_measurement_theta_max      18.03

_exptl_crystal_description       plate
_exptl_crystal_colour            black
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    1.886
_exptl_crystal_F_000             6616
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          0.20
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.10
_exptl_absorpt_coefficient_mu    4.615
_shelx_estimated_absorpt_T_min   ?
_shelx_estimated_absorpt_T_max   ?
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_correction_T_min  0.5744
_exptl_absorpt_correction_T_max  0.7450
_exptl_absorpt_process_details   sadabs
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      116(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_source                   ?
_diffrn_measurement_device_type  'Bruker Kappa APEX II'
_diffrn_measurement_method       ?
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            41853
_diffrn_reflns_av_unetI/netI     0.5379
_diffrn_reflns_av_R_equivalents  0.2698
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_h_max       22
_diffrn_reflns_limit_k_min       -29
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_l_min       -27
_diffrn_reflns_limit_l_max       27
_diffrn_reflns_theta_min         1.181
_diffrn_reflns_theta_max         24.406
_diffrn_reflns_theta_full        24.406
_diffrn_measured_fraction_theta_max 0.994
_diffrn_measured_fraction_theta_full 0.994
_diffrn_reflns_Laue_measured_fraction_max 0.994
_diffrn_reflns_Laue_measured_fraction_full 0.994
_diffrn_reflns_point_group_measured_fraction_max 0.994
_diffrn_reflns_point_group_measured_fraction_full 0.994
_reflns_number_total             18613
_reflns_number_gt                4295
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       ?
_computing_cell_refinement       ?
_computing_data_reduction        ?
_computing_structure_solution    ?
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_molecular_graphics    ?
_computing_publication_material  ?
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.1340P)²] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_number_reflns         18613
_refine_ls_number_parameters     652
_refine_ls_number_restraints     2188
_refine_ls_R_factor_all          0.3907
_refine_ls_R_factor_gt           0.1338
_refine_ls_wR_factor_ref         0.3881
_refine_ls_wR_factor_gt          0.2944
_refine_ls_goodness_of_fit_ref   0.919
_refine_ls_restrained_S_all      0.884
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C 1.0405(9) 0.5681(12) 0.3081(11) 0.180(5) Uiso 1 1 d D . . . .
H1A H 1.0171 0.6018 0.2976 0.217 Uiso 1 1 calc R U . . .
H1B H 1.0218 0.5548 0.3422 0.217 Uiso 1 1 calc R U . . .
C2 C 1.1178(12) 0.577(2) 0.325(2) 0.251(7) Uiso 1 1 d D . . . .
H2A H 1.1261 0.6015 0.3572 0.377 Uiso 1 1 calc R U . . .
H2B H 1.1416 0.5442 0.3367 0.377 Uiso 1 1 calc R U . . .
H2C H 1.1369 0.5914 0.2920 0.377 Uiso 1 1 calc R U . . .
C3 C 1.0589(9) 0.4639(10) 0.2747(14) 0.180(5) Uiso 1 1 d D . . . .
H3A H 1.0554 0.4394 0.2419 0.217 Uiso 1 1 calc R U . . .
H3B H 1.1101 0.4718 0.2872 0.217 Uiso 1 1 calc R U . . .
C4 C 1.033(3) 0.4375(15) 0.322(2) 0.251(7) Uiso 1 1 d D . . . .
H4A H 1.0616 0.4062 0.3324 0.377 Uiso 1 1 calc R U . . .
H4B H 1.0380 0.4605 0.3558 0.377 Uiso 1 1 calc R U . . .
H4C H 0.9830 0.4281 0.3103 0.377 Uiso 1 1 calc R U . . .
C5 C 1.0672(8) 0.5457(14) 0.1951(10) 0.180(5) Uiso 1 1 d D . . . .
H5A H 1.0720 0.5838 0.1988 0.217 Uiso 1 1 calc R U . . .
H5B H 1.1156 0.5309 0.2053 0.217 Uiso 1 1 calc R U . . .
C6 C 1.041(3) 0.534(2) 0.1347(9) 0.251(7) Uiso 1 1 d D . . . .
H6A H 1.0736 0.5478 0.1106 0.377 Uiso 1 1 calc R U . . .
H6B H 1.0372 0.4962 0.1296 0.377 Uiso 1 1 calc R U . . .
H6C H 0.9934 0.5493 0.1231 0.377 Uiso 1 1 calc R U . . .
C7 C 0.8390(17) 0.3319(5) 0.1124(10) 0.180(5) Uiso 1 1 d D . . . .
H7A H 0.8643 0.3341 0.1527 0.217 Uiso 1 1 calc R U . . .
H7B H 0.7886 0.3233 0.1139 0.217 Uiso 1 1 calc R U . . .
C8 C 0.870(3) 0.2893(7) 0.084(2) 0.251(7) Uiso 1 1 d D . . . .
H8A H 0.8652 0.2572 0.1056 0.377 Uiso 1 1 calc R U . . .
H8B H 0.8440 0.2856 0.0446 0.377 Uiso 1 1 calc R U . . .
H8C H 0.9201 0.2964 0.0835 0.377 Uiso 1 1 calc R U . . .
C9 C 0.9304(9) 0.3985(10) 0.0617(11) 0.180(5) Uiso 1 1 d D . . . .
H9A H 0.9358 0.3692 0.0356 0.217 Uiso 1 1 calc R U . . .
H9B H 0.9346 0.4308 0.0398 0.217 Uiso 1 1 calc R U . . .
C10 C 0.9900(8) 0.397(3) 0.1102(17) 0.251(7) Uiso 1 1 d D . . . .
H10A H 1.0352 0.3984 0.0955 0.377 Uiso 1 1 calc R U . . .
H10B H 0.9866 0.4262 0.1359 0.377 Uiso 1 1 calc R U . . .
H10C H 0.9878 0.3644 0.1317 0.377 Uiso 1 1 calc R U . . .
C11 C 0.7841(12) 0.3880(9) 0.0104(7) 0.180(5) Uiso 1 1 d D . . . .
H11A H 0.7846 0.3510 -0.0003 0.217 Uiso 1 1 calc R U . . .
H11B H 0.7347 0.3965 0.0154 0.217 Uiso 1 1 calc R U . . .
C12 C 0.800(3) 0.418(2) -0.0383(9) 0.251(7) Uiso 1 1 d D . . . .
H12A H 0.7655 0.4101 -0.0728 0.377 Uiso 1 1 calc R U . . .
H12B H 0.7983 0.4550 -0.0295 0.377 Uiso 1 1 calc R U . . .
H12C H 0.8484 0.4092 -0.0452 0.377 Uiso 1 1 calc R U . . .
C13 C 0.5211(15) 0.5792(9) 0.4949(7) 0.180(5) Uiso 1 1 d D . . . .
H13A H 0.5079 0.5976 0.5285 0.217 Uiso 1 1 calc R U . . .
H13B H 0.4798 0.5575 0.4783 0.217 Uiso 1 1 calc R U . . .
C14 C 0.580(2) 0.5447(17) 0.516(2) 0.251(7) Uiso 1 1 d D . . . .
H14A H 0.5663 0.5209 0.5447 0.377 Uiso 1 1 calc R U . . .
H14B H 0.5933 0.5249 0.4839 0.377 Uiso 1 1 calc R U . . .
H14C H 0.6216 0.5651 0.5343 0.377 Uiso 1 1 calc R U . . .
C15 C 0.6059(12) 0.6670(11) 0.4782(9) 0.180(5) Uiso 1 1 d D . . . .
H15A H 0.6501 0.6460 0.4838 0.217 Uiso 1 1 calc R U . . .
H15B H 0.6130 0.6960 0.4522 0.217 Uiso 1 1 calc R U . . .
C16 C 0.598(2) 0.689(2) 0.5341(15) 0.251(7) Uiso 1 1 d D . . . .
H16A H 0.6400 0.7095 0.5493 0.377 Uiso 1 1 calc R U . . .
H16B H 0.5553 0.7109 0.5294 0.377 Uiso 1 1 calc R U . . .
H16C H 0.5925 0.6608 0.5612 0.377 Uiso 1 1 calc R U . . .
C17 C 0.4562(12) 0.6682(10) 0.4374(9) 0.180(5) Uiso 1 1 d D . . . .
H17A H 0.4136 0.6470 0.4227 0.217 Uiso 1 1 calc R U . . .
H17B H 0.4521 0.6789 0.4772 0.217 Uiso 1 1 calc R U . . .
C18 C 0.453(2) 0.7147(15) 0.402(3) 0.251(7) Uiso 1 1 d D . . . .
H18A H 0.4086 0.7332 0.4035 0.377 Uiso 1 1 calc R U . . .
H18B H 0.4938 0.7370 0.4165 0.377 Uiso 1 1 calc R U . . .
H18C H 0.4551 0.7050 0.3618 0.377 Uiso 1 1 calc R U . . .
C19 C 0.3570(10) 0.4503(9) 0.3212(13) 0.180(5) Uiso 1 1 d D . . . .
H19A H 0.3858 0.4231 0.3063 0.217 Uiso 1 1 calc R U . . .
H19B H 0.3812 0.4590 0.3608 0.217 Uiso 1 1 calc R U . . .
C20 C 0.2873(15) 0.4285(17) 0.325(3) 0.251(7) Uiso 1 1 d D . . . .
H20A H 0.2934 0.3981 0.3505 0.377 Uiso 1 1 calc R U . . .
H20B H 0.2585 0.4544 0.3414 0.377 Uiso 1 1 calc R U . . .
H20C H 0.2631 0.4184 0.2867 0.377 Uiso 1 1 calc R U . . .
C21 C 0.2981(8) 0.5515(10) 0.3040(13) 0.180(5) Uiso 1 1 d D . . . .
H21A H 0.2777 0.5752 0.2724 0.217 Uiso 1 1 calc R U . . .
H21B H 0.2582 0.5308 0.3142 0.217 Uiso 1 1 calc R U . . .
C22 C 0.327(2) 0.5830(19) 0.354(2) 0.251(7) Uiso 1 1 d D . . . .
H22A H 0.2892 0.6048 0.3648 0.377 Uiso 1 1 calc R U . . .
H22B H 0.3459 0.5604 0.3866 0.377 Uiso 1 1 calc R U . . .
H22C H 0.3656 0.6049 0.3445 0.377 Uiso 1 1 calc R U . . .
C23 C 0.3077(10) 0.4868(11) 0.2073(8) 0.180(5) Uiso 1 1 d D . . . .
H23A H 0.3406 0.4684 0.1858 0.217 Uiso 1 1 calc R U . . .
H23B H 0.2715 0.4615 0.2153 0.217 Uiso 1 1 calc R U . . .
C24 C 0.271(3) 0.5268(18) 0.1697(14) 0.251(7) Uiso 1 1 d D . . . .
H24A H 0.2459 0.5108 0.1342 0.377 Uiso 1 1 calc R U . . .
H24B H 0.2369 0.5447 0.1896 0.377 Uiso 1 1 calc R U . . .
H24C H 0.3062 0.5517 0.1599 0.377 Uiso 1 1 calc R U . . .
C25 C 0.9244(11) 0.6550(10) 0.0686(9) 0.180(5) Uiso 1 1 d D . . . .
H25A H 0.9258 0.6731 0.1060 0.217 Uiso 1 1 calc R U . . .
H25B H 0.9634 0.6292 0.0739 0.217 Uiso 1 1 calc R U . . .
C26 C 0.940(2) 0.6930(19) 0.0262(18) 0.251(7) Uiso 1 1 d D . . . .
H26A H 0.9863 0.7089 0.0397 0.377 Uiso 1 1 calc R U . . .
H26B H 0.9404 0.6757 -0.0109 0.377 Uiso 1 1 calc R U . . .
H26C H 0.9027 0.7198 0.0213 0.377 Uiso 1 1 calc R U . . .
C27 C 0.8476(16) 0.5868(8) -0.0146(6) 0.180(5) Uiso 1 1 d D . . . .
H27A H 0.7993 0.5754 -0.0327 0.217 Uiso 1 1 calc R U . . .
H27B H 0.8644 0.6118 -0.0413 0.217 Uiso 1 1 calc R U . . .
C28 C 0.895(3) 0.5418(17) -0.0094(16) 0.251(7) Uiso 1 1 d D . . . .
H28A H 0.8951 0.5267 -0.0476 0.377 Uiso 1 1 calc R U . . .
H28B H 0.9436 0.5526 0.0073 0.377 Uiso 1 1 calc R U . . .
H28C H 0.8782 0.5160 0.0159 0.377 Uiso 1 1 calc R U . . .
C29 C 0.7764(12) 0.6716(8) 0.0282(10) 0.180(5) Uiso 1 1 d D . . . .
H29A H 0.7916 0.6889 -0.0054 0.217 Uiso 1 1 calc R U . . .
H29B H 0.7296 0.6552 0.0142 0.217 Uiso 1 1 calc R U . . .
C30 C 0.766(3) 0.7113(15) 0.070(2) 0.251(7) Uiso 1 1 d D . . . .
H30A H 0.7305 0.7364 0.0518 0.377 Uiso 1 1 calc R U . . .
H30B H 0.7490 0.6952 0.1030 0.377 Uiso 1 1 calc R U . . .
H30C H 0.8112 0.7291 0.0834 0.377 Uiso 1 1 calc R U . . .
C31 C 0.4533(14) 0.7198(8) 0.1304(7) 0.180(5) Uiso 1 1 d D . . . .
H31A H 0.4506 0.6859 0.1106 0.217 Uiso 1 1 calc R U . . .
H31B H 0.4085 0.7386 0.1159 0.217 Uiso 1 1 calc R U . . .
C32 C 0.513(3) 0.749(2) 0.1137(13) 0.251(7) Uiso 1 1 d D . . . .
H32A H 0.5050 0.7529 0.0716 0.377 Uiso 1 1 calc R U . . .
H32B H 0.5151 0.7832 0.1319 0.377 Uiso 1 1 calc R U . . .
H32C H 0.5574 0.7304 0.1265 0.377 Uiso 1 1 calc R U . . .
C33 C 0.4911(13) 0.7688(5) 0.2399(11) 0.180(5) Uiso 1 1 d D . . . .
H33A H 0.4572 0.7966 0.2246 0.217 Uiso 1 1 calc R U . . .
H33B H 0.4912 0.7666 0.2820 0.217 Uiso 1 1 calc R U . . .
C34 C 0.562(2) 0.7846(16) 0.231(3) 0.251(7) Uiso 1 1 d D . . . .
H34A H 0.5607 0.8203 0.2169 0.377 Uiso 1 1 calc R U . . .
H34B H 0.5787 0.7617 0.2028 0.377 Uiso 1 1 calc R U . . .
H34C H 0.5953 0.7824 0.2679 0.377 Uiso 1 1 calc R U . . .
C35 C 0.3628(8) 0.7105(9) 0.2149(12) 0.180(5) Uiso 1 1 d D . . . .
H35A H 0.3588 0.6997 0.2547 0.217 Uiso 1 1 calc R U . . .
H35B H 0.3466 0.7469 0.2104 0.217 Uiso 1 1 calc R U . . .
C36 C 0.3142(11) 0.679(2) 0.174(2) 0.251(7) Uiso 1 1 d D . . . .
H36A H 0.2654 0.6826 0.1820 0.377 Uiso 1 1 calc R U . . .
H36B H 0.3162 0.6896 0.1347 0.377 Uiso 1 1 calc R U . . .
H36C H 0.3285 0.6422 0.1791 0.377 Uiso 1 1 calc R U . . .
C37 C 0.9587(9) 0.6644(10) 0.4275(11) 0.180(5) Uiso 1 1 d D . . . .
H37A H 0.9802 0.6893 0.4575 0.217 Uiso 1 1 calc R U . . .
H37B H 0.9861 0.6318 0.4341 0.217 Uiso 1 1 calc R U . . .
C38 C 0.9679(18) 0.685(2) 0.3712(18) 0.251(7) Uiso 1 1 d D . . . .
H38A H 1.0187 0.6903 0.3706 0.377 Uiso 1 1 calc R U . . .
H38B H 0.9485 0.6602 0.3410 0.377 Uiso 1 1 calc R U . . .
H38C H 0.9425 0.7179 0.3644 0.377 Uiso 1 1 calc R U . . .
C39 C 0.8276(14) 0.7157(6) 0.4337(12) 0.180(5) Uiso 1 1 d D . . . .
H39A H 0.8296 0.7297 0.3947 0.217 Uiso 1 1 calc R U . . .
H39B H 0.7766 0.7119 0.4369 0.217 Uiso 1 1 calc R U . . .
C40 C 0.859(3) 0.7539(10) 0.476(2) 0.251(7) Uiso 1 1 d D . . . .
H40A H 0.8329 0.7866 0.4692 0.377 Uiso 1 1 calc R U . . .
H40B H 0.8559 0.7414 0.5151 0.377 Uiso 1 1 calc R U . . .
H40C H 0.9091 0.7594 0.4728 0.377 Uiso 1 1 calc R U . . .
C41 C 0.8787(15) 0.6369(10) 0.5151(6) 0.180(5) Uiso 1 1 d D . . . .
H41A H 0.9082 0.6053 0.5222 0.217 Uiso 1 1 calc R U . . .
H41B H 0.9061 0.6655 0.5363 0.217 Uiso 1 1 calc R U . . .
C42 C 0.814(2) 0.629(3) 0.5399(13) 0.251(7) Uiso 1 1 d D . . . .
H42A H 0.8271 0.6216 0.5812 0.377 Uiso 1 1 calc R U . . .
H42B H 0.7848 0.6605 0.5346 0.377 Uiso 1 1 calc R U . . .
H42C H 0.7869 0.6001 0.5205 0.377 Uiso 1 1 calc R U . . .
C43 C 0.5466(12) 0.3764(11) 0.0036(7) 0.180(5) Uiso 1 1 d D . . . .
H43A H 0.5811 0.3482 0.0156 0.217 Uiso 1 1 calc R U . . .
H43B H 0.5113 0.3631 -0.0289 0.217 Uiso 1 1 calc R U . . .
C44 C 0.585(3) 0.4189(16) -0.018(2) 0.251(7) Uiso 1 1 d D . . . .
H44A H 0.6077 0.4065 -0.0501 0.377 Uiso 1 1 calc R U . . .
H44B H 0.5516 0.4468 -0.0317 0.377 Uiso 1 1 calc R U . . .
H44C H 0.6218 0.4318 0.0130 0.377 Uiso 1 1 calc R U . . .
C45 C 0.4628(16) 0.3271(8) 0.0775(8) 0.180(5) Uiso 1 1 d D . . . .
H45A H 0.5022 0.3051 0.0970 0.217 Uiso 1 1 calc R U . . .
H45B H 0.4291 0.3323 0.1049 0.217 Uiso 1 1 calc R U . . .
C46 C 0.426(3) 0.2987(13) 0.0275(13) 0.251(7) Uiso 1 1 d D . . . .
H46A H 0.4080 0.2658 0.0404 0.377 Uiso 1 1 calc R U . . .
H46B H 0.3851 0.3193 0.0083 0.377 Uiso 1 1 calc R U . . .
H46C H 0.4584 0.2920 0.0004 0.377 Uiso 1 1 calc R U . . .
C47 C 0.4221(11) 0.4261(10) 0.0299(9) 0.180(5) Uiso 1 1 d D . . . .
H47A H 0.4388 0.4553 0.0083 0.217 Uiso 1 1 calc R U . . .
H47B H 0.3932 0.4033 0.0012 0.217 Uiso 1 1 calc R U . . .
C48 C 0.376(2) 0.447(2) 0.0678(18) 0.251(7) Uiso 1 1 d D . . . .
H48A H 0.3358 0.4655 0.0447 0.377 Uiso 1 1 calc R U . . .
H48B H 0.3569 0.4184 0.0885 0.377 Uiso 1 1 calc R U . . .
H48C H 0.4027 0.4706 0.0957 0.377 Uiso 1 1 calc R U . . .
C49 C 0.8854(12) 0.4433(9) 0.4994(10) 0.180(5) Uiso 1 1 d D . . . .
H49A H 0.8764 0.4281 0.5362 0.217 Uiso 1 1 calc R U . . .
H49B H 0.9241 0.4229 0.4867 0.217 Uiso 1 1 calc R U . . .
C50 C 0.911(2) 0.4960(11) 0.511(2) 0.251(7) Uiso 1 1 d D . . . .
H50A H 0.9545 0.4953 0.5405 0.377 Uiso 1 1 calc R U . . .
H50B H 0.9223 0.5114 0.4755 0.377 Uiso 1 1 calc R U . . .
H50C H 0.8745 0.5166 0.5252 0.377 Uiso 1 1 calc R U . . .
C51 C 0.8192(15) 0.3730(5) 0.4136(9) 0.180(5) Uiso 1 1 d D . . . .
H51A H 0.8030 0.3457 0.4380 0.217 Uiso 1 1 calc R U . . .
H51B H 0.7882 0.3713 0.3754 0.217 Uiso 1 1 calc R U . . .
C52 C 0.892(2) 0.3606(16) 0.406(3) 0.251(7) Uiso 1 1 d D . . . .
H52A H 0.8927 0.3263 0.3882 0.377 Uiso 1 1 calc R U . . .
H52B H 0.9086 0.3864 0.3805 0.377 Uiso 1 1 calc R U . . .
H52C H 0.9235 0.3607 0.4434 0.377 Uiso 1 1 calc R U . . .
C53 C 0.7376(13) 0.4209(9) 0.4902(10) 0.180(5) Uiso 1 1 d D . . . .
H53A H 0.7621 0.4158 0.5305 0.217 Uiso 1 1 calc R U . . .
H53B H 0.7066 0.4517 0.4900 0.217 Uiso 1 1 calc R U . . .
C54 C 0.692(2) 0.3762(19) 0.474(2) 0.251(7) Uiso 1 1 d D . . . .
H54A H 0.6580 0.3725 0.5008 0.377 Uiso 1 1 calc R U . . .
H54B H 0.6657 0.3810 0.4346 0.377 Uiso 1 1 calc R U . . .
H54C H 0.7213 0.3450 0.4752 0.377 Uiso 1 1 calc R U . . .
C55 C 0.6956(12) 0.2765(6) 0.2683(13) 0.180(5) Uiso 1 1 d D . . . .
H55A H 0.6915 0.2454 0.2922 0.217 Uiso 1 1 calc R U . . .
H55B H 0.6898 0.2649 0.2276 0.217 Uiso 1 1 calc R U . . .
C56 C 0.7678(9) 0.2967(17) 0.284(3) 0.251(7) Uiso 1 1 d D . . . .
H56A H 0.8023 0.2699 0.2786 0.377 Uiso 1 1 calc R U . . .
H56B H 0.7739 0.3267 0.2602 0.377 Uiso 1 1 calc R U . . .
H56C H 0.7756 0.3071 0.3251 0.377 Uiso 1 1 calc R U . . .
C57 C 0.6173(16) 0.3170(8) 0.3518(7) 0.180(5) Uiso 1 1 d D . . . .
H57A H 0.6251 0.2808 0.3651 0.217 Uiso 1 1 calc R U . . .
H57B H 0.6574 0.3378 0.3724 0.217 Uiso 1 1 calc R U . . .
C58 C 0.551(2) 0.336(3) 0.3694(13) 0.251(7) Uiso 1 1 d D . . . .
H58A H 0.5351 0.3668 0.3476 0.377 Uiso 1 1 calc R U . . .
H58B H 0.5605 0.3435 0.4108 0.377 Uiso 1 1 calc R U . . .
H58C H 0.5147 0.3087 0.3617 0.377 Uiso 1 1 calc R U . . .
C59 C 0.5441(12) 0.2809(7) 0.2435(11) 0.180(5) Uiso 1 1 d D . . . .
H59A H 0.5012 0.3030 0.2415 0.217 Uiso 1 1 calc R U . . .
H59B H 0.5491 0.2722 0.2033 0.217 Uiso 1 1 calc R U . . .
C60 C 0.531(2) 0.2330(14) 0.273(2) 0.251(7) Uiso 1 1 d D . . . .
H60A H 0.5109 0.2071 0.2441 0.377 Uiso 1 1 calc R U . . .
H60B H 0.4972 0.2396 0.2992 0.377 Uiso 1 1 calc R U . . .
H60C H 0.5760 0.2201 0.2946 0.377 Uiso 1 1 calc R U . . .
C61 C 0.247(7) 0.829(4) 0.345(4) 0.52(4) Uiso 1 1 d D . . . .
C62 C 0.202(7) 0.781(4) 0.329(3) 0.52(4) Uiso 1 1 d D . . . .
C63 C 0.173(8) 0.781(2) 0.265(3) 0.52(4) Uiso 1 1 d D . . . .
C64 C 0.146(8) 0.728(3) 0.246(3) 0.52(4) Uiso 1 1 d D . . . .
C65 C 0.135(8) 0.724(4) 0.181(3) 0.52(4) Uiso 1 1 d D . . . .
Ni1 Ni 0.7696(2) 0.51977(18) 0.19858(17) 0.0433(12) Uani 1 1 d . . . . .
Ni2 Ni 0.7233(2) 0.55023(19) 0.28554(17) 0.0532(14) Uani 1 1 d . . . . .
Ni3 Ni 0.5908(2) 0.56039(19) 0.27052(17) 0.0522(14) Uani 1 1 d . . . . .
Ni4 Ni 0.6445(2) 0.49789(17) 0.21007(16) 0.0405(12) Uani 1 1 d . . . . .
Ni6 Ni 0.8134(2) 0.46049(19) 0.13410(17) 0.0556(14) Uani 1 1 d D . . . .
Ni7 Ni 0.8981(2) 0.5175(3) 0.2173(2) 0.0824(19) Uani 1 1 d D . . . .
Ni8 Ni 0.8497(3) 0.5786(2) 0.2844(2) 0.0809(19) Uani 1 1 d . . . . .
Ni9 Ni 0.6804(2) 0.46313(18) 0.11818(17) 0.0451(13) Uani 1 1 d . . . . .
Ni10 Ni 0.8233(2) 0.4792(2) 0.29192(18) 0.0676(17) Uani 1 1 d . . . . .
Ni11 Ni 0.7464(2) 0.4273(2) 0.21795(17) 0.0540(14) Uani 1 1 d . . . . .
Ni12 Ni 0.8135(2) 0.5706(2) 0.12238(18) 0.0601(15) Uani 1 1 d D . . . .
Ni13 Ni 0.7612(3) 0.6160(2) 0.20472(19) 0.0680(16) Uani 1 1 d . . . . .
Ni14 Ni 0.6770(2) 0.55983(17) 0.12389(17) 0.0452(13) Uani 1 1 d . . . . .
Ni15 Ni 0.8094(3) 0.5929(2) 0.3801(2) 0.093(2) Uani 1 1 d D . . . .
Ni16 Ni 0.6805(3) 0.6165(2) 0.3517(2) 0.0767(18) Uani 1 1 d . . . . .
Ni17 Ni 0.5525(3) 0.5949(2) 0.35650(18) 0.082(2) Uani 1 1 d D . . . .
Ni18 Ni 0.4664(2) 0.5385(2) 0.27255(18) 0.0631(15) Uani 1 1 d D . . . .
Ni19 Ni 0.5086(2) 0.50174(19) 0.18516(17) 0.0539(14) Uani 1 1 d . . . . .
Ni20 Ni 0.6459(3) 0.5177(2) 0.36247(17) 0.0617(15) Uani 1 1 d . . . . .
Ni21 Ni 0.5680(2) 0.46701(19) 0.28831(17) 0.0511(14) Uani 1 1 d . . . . .
Ni22 Ni 0.5144(3) 0.6376(2) 0.24180(19) 0.0763(18) Uani 1 1 d D . . . .
Ni23 Ni 0.6530(3) 0.6401(2) 0.24745(19) 0.0723(17) Uani 1 1 d . . . . .
Ni24 Ni 0.5694(2) 0.58353(19) 0.16648(17) 0.0534(14) Uani 1 1 d . . . . .
Ni25 Ni 0.7793(3) 0.5004(2) 0.38469(18) 0.0788(19) Uani 1 1 d D . . . .
Ni27 Ni 0.6262(2) 0.39731(18) 0.23739(18) 0.0574(14) Uani 1 1 d D . . . .
Ni28 Ni 0.5649(2) 0.42727(19) 0.13981(17) 0.0532(14) Uani 1 1 d D . . . .
P1 P 1.0142(5) 0.5233(6) 0.2482(5) 0.172(9) Uani 1 1 d D . . . .
P2 P 0.8412(5) 0.3958(4) 0.0796(4) 0.078(4) Uani 1 1 d D . . . .
P3 P 0.5341(6) 0.6271(5) 0.4414(4) 0.112(5) Uani 1 1 d D . . . .
P4 P 0.3585(5) 0.5077(5) 0.2762(4) 0.101(5) Uani 1 1 d D . . . .
P5 P 0.8401(4) 0.6205(4) 0.0523(4) 0.059(3) Uani 1 1 d D . . . .
P6 P 0.4569(6) 0.7081(4) 0.2073(4) 0.084(4) Uani 1 1 d D . . . .
P7 P 0.8676(7) 0.6515(4) 0.4383(4) 0.127(6) Uani 1 1 d D . . . .
P8 P 0.5000(5) 0.3898(4) 0.0635(4) 0.064(3) Uani 1 1 d D . . . .
P9 P 0.8051(6) 0.4351(4) 0.4458(4) 0.093(4) Uani 1 1 d D . . . .
P10 P 0.6217(6) 0.3190(4) 0.2752(4) 0.087(4) Uani 1 1 d D . . . .
S1 S 0.8639(5) 0.4347(5) 0.2223(4) 0.077(4) Uani 1 1 d . . . . .
S2 S 0.8802(5) 0.6043(5) 0.1998(4) 0.082(4) Uani 1 1 d . . . . .
S3 S 0.8846(6) 0.5274(5) 0.3606(4) 0.081(4) Uani 1 1 d . . . . .
S4 S 0.7655(6) 0.6402(5) 0.2976(4) 0.091(4) Uani 1 1 d . . . . .
S5 S 0.6550(5) 0.6389(4) 0.1528(4) 0.063(3) Uani 1 1 d . . . . .
S6 S 0.7207(6) 0.5641(5) 0.4246(4) 0.076(4) Uani 1 1 d . . . . .
S7 S 0.5879(7) 0.6673(5) 0.3166(4) 0.094(4) Uani 1 1 d . . . . .
S8 S 0.5276(5) 0.5113(4) 0.3595(4) 0.070(3) Uani 1 1 d . . . . .
S9 S 0.4562(5) 0.5784(4) 0.1871(3) 0.067(3) Uani 1 1 d . . . . .
S10 S 0.5075(5) 0.4211(4) 0.2180(4) 0.059(3) Uani 1 1 d . . . . .
S11 S 0.6698(4) 0.3831(4) 0.1539(4) 0.048(3) Uani 1 1 d . . . . .
S12 S 0.7463(5) 0.5134(4) 0.0705(3) 0.053(3) Uani 1 1 d . . . . .
S13 S 0.5795(5) 0.5128(4) 0.1141(3) 0.052(3) Uani 1 1 d . . . . .
S14 S 0.6975(5) 0.4628(4) 0.2974(3) 0.054(3) Uani 1 1 d . . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C1 C2 1.474(8) . ?
C1 P1 1.826(12) . ?
C1 H1A 0.9900 . ?
C1 H1B 0.9900 . ?
C2 H2A 0.9800 . ?
C2 H2B 0.9800 . ?
C2 H2C 0.9800 . ?
C3 C4 1.458(11) . ?
C3 P1 1.814(12) . ?
C3 H3A 0.9900 . ?
C3 H3B 0.9900 . ?
C4 H4A 0.9800 . ?
C4 H4B 0.9800 . ?
C4 H4C 0.9800 . ?
C5 C6 1.458(11) . ?
C5 P1 1.822(12) . ?
C5 H5A 0.9900 . ?
C5 H5B 0.9900 . ?
C6 H6A 0.9800 . ?
C6 H6B 0.9800 . ?
C6 H6C 0.9800 . ?
C7 C8 1.456(11) . ?
C7 P2 1.826(12) . ?
C7 H7A 0.9900 . ?
C7 H7B 0.9900 . ?
C8 H8A 0.9800 . ?
C8 H8B 0.9800 . ?
C8 H8C 0.9800 . ?
C9 C10 1.466(11) . ?
C9 P2 1.816(12) . ?
C9 H9A 0.9900 . ?
C9 H9B 0.9900 . ?
C10 H10A 0.9800 . ?
C10 H10B 0.9800 . ?
C10 H10C 0.9800 . ?
C11 C12 1.456(11) . ?
C11 P2 1.809(11) . ?
C11 H11A 0.9900 . ?
C11 H11B 0.9900 . ?
C12 H12A 0.9800 . ?
C12 H12B 0.9800 . ?
C12 H12C 0.9800 . ?
C13 C14 1.458(11) . ?
C13 P3 1.810(11) . ?
C13 H13A 0.9900 . ?
C13 H13B 0.9900 . ?
C14 H14A 0.9800 . ?
C14 H14B 0.9800 . ?
C14 H14C 0.9800 . ?
C15 C16 1.461(11) . ?
C15 P3 1.811(12) . ?
C15 H15A 0.9900 . ?
C15 H15B 0.9900 . ?
C16 H16A 0.9800 . ?
C16 H16B 0.9800 . ?
C16 H16C 0.9800 . ?
C17 C18 1.457(11) . ?
C17 P3 1.813(12) . ?
C17 H17A 0.9900 . ?
C17 H17B 0.9900 . ?
C18 H18A 0.9800 . ?
C18 H18B 0.9800 . ?
C18 H18C 0.9800 . ?
C19 C20 1.458(11) . ?
C19 P4 1.825(12) . ?
C19 H19A 0.9900 . ?
C19 H19B 0.9900 . ?
C20 H20A 0.9800 . ?
C20 H20B 0.9800 . ?
C20 H20C 0.9800 . ?
C21 C22 1.460(11) . ?
C21 P4 1.811(12) . ?
C21 H21A 0.9900 . ?
C21 H21B 0.9900 . ?
C22 H22A 0.9800 . ?
C22 H22B 0.9800 . ?
C22 H22C 0.9800 . ?
C23 C24 1.458(11) . ?
C23 P4 1.821(12) . ?
C23 H23A 0.9900 . ?
C23 H23B 0.9900 . ?
C24 H24A 0.9800 . ?
C24 H24B 0.9800 . ?
C24 H24C 0.9800 . ?
C25 C26 1.461(11) . ?
C25 P5 1.818(12) . ?
C25 H25A 0.9900 . ?
C25 H25B 0.9900 . ?
C26 H26A 0.9800 . ?
C26 H26B 0.9800 . ?
C26 H26C 0.9800 . ?
C27 C28 1.466(11) . ?
C27 P5 1.824(11) . ?
C27 H27A 0.9900 . ?
C27 H27B 0.9900 . ?
C28 H28A 0.9800 . ?
C28 H28B 0.9800 . ?
C28 H28C 0.9800 . ?
C29 C30 1.458(11) . ?
C29 P5 1.817(11) . ?
C29 H29A 0.9900 . ?
C29 H29B 0.9900 . ?
C30 H30A 0.9800 . ?
C30 H30B 0.9800 . ?
C30 H30C 0.9800 . ?
C31 C32 1.463(11) . ?
C31 P6 1.820(12) . ?
C31 H31A 0.9900 . ?
C31 H31B 0.9900 . ?
C32 H32A 0.9800 . ?
C32 H32B 0.9800 . ?
C32 H32C 0.9800 . ?
C33 C34 1.460(11) . ?
C33 P6 1.817(11) . ?
C33 H33A 0.9900 . ?
C33 H33B 0.9900 . ?
C34 H34A 0.9800 . ?
C34 H34B 0.9800 . ?
C34 H34C 0.9800 . ?
C35 C36 1.467(11) . ?
C35 P6 1.828(12) . ?
C35 H35A 0.9900 . ?
C35 H35B 0.9900 . ?
C36 H36A 0.9800 . ?
C36 H36B 0.9800 . ?
C36 H36C 0.9800 . ?
C37 C38 1.461(11) . ?
C37 P7 1.822(12) . ?
C37 H37A 0.9900 . ?
C37 H37B 0.9900 . ?
C38 H38A 0.9800 . ?
C38 H38B 0.9800 . ?
C38 H38C 0.9800 . ?
C39 C40 1.459(11) . ?
C39 P7 1.821(12) . ?
C39 H39A 0.9900 . ?
C39 H39B 0.9900 . ?
C40 H40A 0.9800 . ?
C40 H40B 0.9800 . ?
C40 H40C 0.9800 . ?
C41 C42 1.459(11) . ?
C41 P7 1.819(12) . ?
C41 H41A 0.9900 . ?
C41 H41B 0.9900 . ?
C42 H42A 0.9800 . ?
C42 H42B 0.9800 . ?
C42 H42C 0.9800 . ?
C43 C44 1.457(11) . ?
C43 P8 1.816(11) . ?
C43 H43A 0.9900 . ?
C43 H43B 0.9900 . ?
C44 H44A 0.9800 . ?
C44 H44B 0.9800 . ?
C44 H44C 0.9800 . ?
C45 C46 1.462(11) . ?
C45 P8 1.820(12) . ?
C45 H45A 0.9900 . ?
C45 H45B 0.9900 . ?
C46 H46A 0.9800 . ?
C46 H46B 0.9800 . ?
C46 H46C 0.9800 . ?
C47 C48 1.460(11) . ?
C47 P8 1.817(11) . ?
C47 H47A 0.9900 . ?
C47 H47B 0.9900 . ?
C48 H48A 0.9800 . ?
C48 H48B 0.9800 . ?
C48 H48C 0.9800 . ?
C49 C50 1.458(11) . ?
C49 P9 1.821(12) . ?
C49 H49A 0.9900 . ?
C49 H49B 0.9900 . ?
C50 H50A 0.9800 . ?
C50 H50B 0.9800 . ?
C50 H50C 0.9800 . ?
C51 C52 1.461(11) . ?
C51 P9 1.814(12) . ?
C51 H51A 0.9900 . ?
C51 H51B 0.9900 . ?
C52 H52A 0.9800 . ?
C52 H52B 0.9800 . ?
C52 H52C 0.9800 . ?
C53 C54 1.458(11) . ?
C53 P9 1.821(12) . ?
C53 H53A 0.9900 . ?
C53 H53B 0.9900 . ?
C54 H54A 0.9800 . ?
C54 H54B 0.9800 . ?
C54 H54C 0.9800 . ?
C55 C56 1.457(11) . ?
C55 P10 1.812(11) . ?
C55 H55A 0.9900 . ?
C55 H55B 0.9900 . ?
C56 H56A 0.9800 . ?
C56 H56B 0.9800 . ?
C56 H56C 0.9800 . ?
C57 C58 1.464(11) . ?
C57 P10 1.815(12) . ?
C57 H57A 0.9900 . ?
C57 H57B 0.9900 . ?
C58 H58A 0.9800 . ?
C58 H58B 0.9800 . ?
C58 H58C 0.9800 . ?
C59 C60 1.457(11) . ?
C59 P10 1.827(12) . ?
C59 H59A 0.9900 . ?
C59 H59B 0.9900 . ?
C60 H60A 0.9800 . ?
C60 H60B 0.9800 . ?
C60 H60C 0.9800 . ?
C61 C62 1.505(10) . ?
C62 C63 1.508(14) . ?
C63 C64 1.507(14) . ?
C64 C65 1.507(14) . ?
Ni1 Ni6 2.399(6) . ?
Ni1 Ni7 2.409(6) . ?
Ni1 Ni12 2.475(6) . ?
Ni1 Ni2 2.483(6) . ?
Ni1 Ni11 2.486(7) . ?
Ni1 Ni10 2.489(6) . ?
Ni1 Ni14 2.493(6) . ?
Ni1 Ni13 2.499(7) . ?
Ni1 Ni4 2.503(6) . ?
Ni1 Ni9 2.741(6) . ?
Ni1 Ni8 2.768(6) . ?
Ni2 S14 2.338(12) . ?
Ni2 S4 2.461(14) . ?
Ni2 Ni3 2.497(7) . ?
Ni2 Ni4 2.515(6) . ?
Ni2 Ni8 2.517(7) . ?
Ni2 Ni16 2.535(7) . ?
Ni2 Ni10 2.629(7) . ?
Ni2 Ni20 2.650(7) . ?
Ni2 Ni25 2.717(6) . ?
Ni2 Ni13 2.733(7) . ?
Ni2 Ni23 2.753(7) . ?
Ni3 Ni17 2.427(6) . ?
Ni3 Ni18 2.440(7) . ?
Ni3 Ni4 2.479(6) . ?
Ni3 Ni23 2.479(8) . ?
Ni3 Ni24 2.481(6) . ?
Ni3 Ni20 2.493(6) . ?
Ni3 Ni22 2.495(7) . ?
Ni3 Ni21 2.501(7) . ?
Ni3 Ni16 2.748(7) . ?
Ni3 Ni19 2.777(6) . ?
Ni4 S14 2.313(9) . ?
Ni4 S13 2.412(8) . ?
Ni4 Ni9 2.534(6) . ?
Ni4 Ni19 2.553(6) . ?
Ni4 Ni11 2.646(6) . ?
Ni4 Ni21 2.649(6) . ?
Ni4 Ni27 2.715(7) . ?
Ni4 Ni14 2.731(6) . ?
Ni4 Ni24 2.738(6) . ?
Ni6 P2 2.221(9) . ?
Ni6 S1 2.233(10) . ?
Ni6 S12 2.256(10) . ?
Ni6 Ni9 2.495(6) . ?
Ni6 Ni11 2.659(6) . ?
Ni6 Ni7 2.743(7) . ?
Ni6 Ni12 2.861(7) . ?
Ni7 P1 2.211(9) . ?
Ni7 S1 2.246(14) . ?
Ni7 S2 2.296(14) . ?
Ni7 Ni8 2.511(8) . ?
Ni7 Ni10 2.629(7) . ?
Ni7 Ni12 2.870(6) . ?
Ni8 S3 2.236(11) . ?
Ni8 S2 2.260(12) . ?
Ni8 S4 2.315(14) . ?
Ni8 Ni13 2.492(6) . ?
Ni8 Ni15 2.519(8) . ?
Ni8 Ni10 2.630(8) . ?
Ni9 S12 2.233(10) . ?
Ni9 S11 2.253(10) . ?
Ni9 S13 2.296(10) . ?
Ni9 Ni14 2.505(7) . ?
Ni9 Ni28 2.511(6) . ?
Ni9 Ni11 2.634(6) . ?
Ni10 S3 2.211(11) . ?
Ni10 S1 2.238(11) . ?
Ni10 S14 2.451(10) . ?
Ni10 Ni11 2.470(7) . ?
Ni10 Ni25 2.520(7) . ?
Ni11 S1 2.226(11) . ?
Ni11 S11 2.227(10) . ?
Ni11 S14 2.401(9) . ?
Ni11 Ni27 2.527(7) . ?
Ni12 S12 2.185(10) . ?
Ni12 S2 2.213(11) . ?
Ni12 P5 2.215(8) . ?
Ni12 Ni13 2.596(7) . ?
Ni12 Ni14 2.616(7) . ?
Ni13 S4 2.256(11) . ?
Ni13 S5 2.257(10) . ?
Ni13 S2 2.304(12) . ?
Ni13 Ni23 2.513(8) . ?
Ni13 Ni14 2.694(6) . ?
Ni14 S13 2.195(10) . ?
Ni14 S5 2.216(11) . ?
Ni14 S12 2.302(10) . ?
Ni14 Ni24 2.497(6) . ?
Ni15 P7 2.209(9) . ?
Ni15 S6 2.254(13) . ?
Ni15 S3 2.312(13) . ?
Ni15 S4 2.323(12) . ?
Ni15 Ni25 2.467(9) . ?
Ni15 Ni16 2.504(8) . ?
Ni16 S6 2.218(11) . ?
Ni16 S7 2.240(12) . ?
Ni16 S4 2.299(14) . ?
Ni16 Ni23 2.490(7) . ?
Ni16 Ni17 2.517(8) . ?
Ni16 Ni20 2.660(8) . ?
Ni17 S8 2.217(13) . ?
Ni17 P3 2.241(9) . ?
Ni17 S7 2.248(15) . ?
Ni17 Ni20 2.659(7) . ?
Ni17 Ni18 2.758(7) . ?
Ni17 Ni22 2.889(7) . ?
Ni18 P4 2.215(9) . ?
Ni18 S9 2.234(10) . ?
Ni18 S8 2.285(9) . ?
Ni18 Ni19 2.511(6) . ?
Ni18 Ni21 2.653(7) . ?
Ni18 Ni22 2.854(8) . ?
Ni19 S9 2.221(11) . ?
Ni19 S10 2.224(11) . ?
Ni19 S13 2.332(10) . ?
Ni19 Ni24 2.484(7) . ?
Ni19 Ni28 2.524(7) . ?
Ni19 Ni21 2.651(6) . ?
Ni20 S6 2.213(11) . ?
Ni20 S8 2.243(11) . ?
Ni20 S14 2.411(10) . ?
Ni20 Ni21 2.466(7) . ?
Ni20 Ni25 2.541(7) . ?
Ni21 S10 2.195(11) . ?
Ni21 S8 2.262(10) . ?
Ni21 S14 2.438(10) . ?
Ni21 Ni27 2.518(6) . ?
Ni22 S9 2.178(12) . ?
Ni22 S7 2.191(12) . ?
Ni22 P6 2.208(9) . ?
Ni22 Ni24 2.607(7) . ?
Ni22 Ni23 2.617(8) . ?
Ni23 S5 2.229(10) . ?
Ni23 S4 2.262(12) . ?
Ni23 S7 2.309(13) . ?
Ni23 Ni24 2.695(6) . ?
Ni24 S13 2.230(11) . ?
Ni24 S5 2.230(12) . ?
Ni24 S9 2.288(11) . ?
Ni25 P9 2.216(9) . ?
Ni25 S6 2.275(12) . ?
Ni25 S3 2.280(13) . ?
Ni25 S14 2.547(10) . ?
Ni27 P10 2.219(9) . ?
Ni27 S11 2.282(9) . ?
Ni27 S10 2.309(10) . ?
Ni27 S14 2.461(11) . ?
Ni27 Ni28 2.512(6) . ?
Ni28 P8 2.221(8) . ?
Ni28 S11 2.272(9) . ?
Ni28 S10 2.293(10) . ?
Ni28 S13 2.321(11) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C2 C1 P1 115.9(8) . . ?
C2 C1 H1A 108.3 . . ?
P1 C1 H1A 108.3 . . ?
C2 C1 H1B 108.3 . . ?
P1 C1 H1B 108.3 . . ?
H1A C1 H1B 107.4 . . ?
C1 C2 H2A 109.5 . . ?
C1 C2 H2B 109.5 . . ?
H2A C2 H2B 109.5 . . ?
C1 C2 H2C 109.5 . . ?
H2A C2 H2C 109.5 . . ?
H2B C2 H2C 109.5 . . ?
C4 C3 P1 117.5(10) . . ?
C4 C3 H3A 107.9 . . ?
P1 C3 H3A 107.9 . . ?
C4 C3 H3B 107.9 . . ?
P1 C3 H3B 107.9 . . ?
H3A C3 H3B 107.2 . . ?
C3 C4 H4A 109.5 . . ?
C3 C4 H4B 109.5 . . ?
H4A C4 H4B 109.5 . . ?
C3 C4 H4C 109.5 . . ?
H4A C4 H4C 109.5 . . ?
H4B C4 H4C 109.5 . . ?
C6 C5 P1 117.3(10) . . ?
C6 C5 H5A 108.0 . . ?
P1 C5 H5A 108.0 . . ?
C6 C5 H5B 108.0 . . ?
P1 C5 H5B 108.0 . . ?
H5A C5 H5B 107.2 . . ?
C5 C6 H6A 109.5 . . ?
C5 C6 H6B 109.5 . . ?
H6A C6 H6B 109.5 . . ?
C5 C6 H6C 109.5 . . ?
H6A C6 H6C 109.5 . . ?
H6B C6 H6C 109.5 . . ?
C8 C7 P2 117.1(10) . . ?
C8 C7 H7A 108.0 . . ?
P2 C7 H7A 108.0 . . ?
C8 C7 H7B 108.0 . . ?
P2 C7 H7B 108.0 . . ?
H7A C7 H7B 107.3 . . ?
C7 C8 H8A 109.5 . . ?
C7 C8 H8B 109.5 . . ?
H8A C8 H8B 109.5 . . ?
C7 C8 H8C 109.5 . . ?
H8A C8 H8C 109.5 . . ?
H8B C8 H8C 109.5 . . ?
C10 C9 P2 116.6(10) . . ?
C10 C9 H9A 108.2 . . ?
P2 C9 H9A 108.2 . . ?
C10 C9 H9B 108.2 . . ?
P2 C9 H9B 108.2 . . ?
H9A C9 H9B 107.3 . . ?
C9 C10 H10A 109.5 . . ?
C9 C10 H10B 109.5 . . ?
H10A C10 H10B 109.5 . . ?
C9 C10 H10C 109.5 . . ?
H10A C10 H10C 109.5 . . ?
H10B C10 H10C 109.5 . . ?
C12 C11 P2 118.1(10) . . ?
C12 C11 H11A 107.8 . . ?
P2 C11 H11A 107.8 . . ?
C12 C11 H11B 107.8 . . ?
P2 C11 H11B 107.8 . . ?
H11A C11 H11B 107.1 . . ?
C11 C12 H12A 109.5 . . ?
C11 C12 H12B 109.5 . . ?
H12A C12 H12B 109.5 . . ?
C11 C12 H12C 109.5 . . ?
H12A C12 H12C 109.5 . . ?
H12B C12 H12C 109.5 . . ?
C14 C13 P3 118.0(10) . . ?
C14 C13 H13A 107.8 . . ?
P3 C13 H13A 107.8 . . ?
C14 C13 H13B 107.8 . . ?
P3 C13 H13B 107.8 . . ?
H13A C13 H13B 107.2 . . ?
C13 C14 H14A 109.5 . . ?
C13 C14 H14B 109.5 . . ?
H14A C14 H14B 109.5 . . ?
C13 C14 H14C 109.5 . . ?
H14A C14 H14C 109.5 . . ?
H14B C14 H14C 109.5 . . ?
C16 C15 P3 117.7(10) . . ?
C16 C15 H15A 107.9 . . ?
P3 C15 H15A 107.9 . . ?
C16 C15 H15B 107.9 . . ?
P3 C15 H15B 107.9 . . ?
H15A C15 H15B 107.2 . . ?
C15 C16 H16A 109.5 . . ?
C15 C16 H16B 109.5 . . ?
H16A C16 H16B 109.5 . . ?
C15 C16 H16C 109.5 . . ?
H16A C16 H16C 109.5 . . ?
H16B C16 H16C 109.5 . . ?
C18 C17 P3 117.8(10) . . ?
C18 C17 H17A 107.9 . . ?
P3 C17 H17A 107.9 . . ?
C18 C17 H17B 107.9 . . ?
P3 C17 H17B 107.9 . . ?
H17A C17 H17B 107.2 . . ?
C17 C18 H18A 109.5 . . ?
C17 C18 H18B 109.5 . . ?
H18A C18 H18B 109.5 . . ?
C17 C18 H18C 109.5 . . ?
H18A C18 H18C 109.5 . . ?
H18B C18 H18C 109.5 . . ?
C20 C19 P4 117.0(10) . . ?
C20 C19 H19A 108.0 . . ?
P4 C19 H19A 108.0 . . ?
C20 C19 H19B 108.0 . . ?
P4 C19 H19B 108.0 . . ?
H19A C19 H19B 107.3 . . ?
C19 C20 H20A 109.5 . . ?
C19 C20 H20B 109.5 . . ?
H20A C20 H20B 109.5 . . ?
C19 C20 H20C 109.5 . . ?
H20A C20 H20C 109.5 . . ?
H20B C20 H20C 109.5 . . ?
C22 C21 P4 117.5(10) . . ?
C22 C21 H21A 107.9 . . ?
P4 C21 H21A 107.9 . . ?
C22 C21 H21B 107.9 . . ?
P4 C21 H21B 107.9 . . ?
H21A C21 H21B 107.2 . . ?
C21 C22 H22A 109.5 . . ?
C21 C22 H22B 109.5 . . ?
H22A C22 H22B 109.5 . . ?
C21 C22 H22C 109.5 . . ?
H22A C22 H22C 109.5 . . ?
H22B C22 H22C 109.5 . . ?
C24 C23 P4 117.2(10) . . ?
C24 C23 H23A 108.0 . . ?
P4 C23 H23A 108.0 . . ?
C24 C23 H23B 108.0 . . ?
P4 C23 H23B 108.0 . . ?
H23A C23 H23B 107.2 . . ?
C23 C24 H24A 109.5 . . ?
C23 C24 H24B 109.5 . . ?
H24A C24 H24B 109.5 . . ?
C23 C24 H24C 109.5 . . ?
H24A C24 H24C 109.5 . . ?
H24B C24 H24C 109.5 . . ?
C26 C25 P5 117.1(10) . . ?
C26 C25 H25A 108.0 . . ?
P5 C25 H25A 108.0 . . ?
C26 C25 H25B 108.0 . . ?
P5 C25 H25B 108.0 . . ?
H25A C25 H25B 107.3 . . ?
C25 C26 H26A 109.5 . . ?
C25 C26 H26B 109.5 . . ?
H26A C26 H26B 109.5 . . ?
C25 C26 H26C 109.5 . . ?
H26A C26 H26C 109.5 . . ?
H26B C26 H26C 109.5 . . ?
C28 C27 P5 116.2(10) . . ?
C28 C27 H27A 108.2 . . ?
P5 C27 H27A 108.2 . . ?
C28 C27 H27B 108.2 . . ?
P5 C27 H27B 108.2 . . ?
H27A C27 H27B 107.4 . . ?
C27 C28 H28A 109.5 . . ?
C27 C28 H28B 109.5 . . ?
H28A C28 H28B 109.5 . . ?
C27 C28 H28C 109.5 . . ?
H28A C28 H28C 109.5 . . ?
H28B C28 H28C 109.5 . . ?
C30 C29 P5 117.4(10) . . ?
C30 C29 H29A 107.9 . . ?
P5 C29 H29A 107.9 . . ?
C30 C29 H29B 107.9 . . ?
P5 C29 H29B 107.9 . . ?
H29A C29 H29B 107.2 . . ?
C29 C30 H30A 109.5 . . ?
C29 C30 H30B 109.5 . . ?
H30A C30 H30B 109.5 . . ?
C29 C30 H30C 109.5 . . ?
H30A C30 H30C 109.5 . . ?
H30B C30 H30C 109.5 . . ?
C32 C31 P6 116.6(10) . . ?
C32 C31 H31A 108.1 . . ?
P6 C31 H31A 108.1 . . ?
C32 C31 H31B 108.1 . . ?
P6 C31 H31B 108.1 . . ?
H31A C31 H31B 107.3 . . ?
C31 C32 H32A 109.5 . . ?
C31 C32 H32B 109.5 . . ?
H32A C32 H32B 109.5 . . ?
C31 C32 H32C 109.5 . . ?
H32A C32 H32C 109.5 . . ?
H32B C32 H32C 109.5 . . ?
C34 C33 P6 117.2(10) . . ?
C34 C33 H33A 108.0 . . ?
P6 C33 H33A 108.0 . . ?
C34 C33 H33B 108.0 . . ?
P6 C33 H33B 108.0 . . ?
H33A C33 H33B 107.3 . . ?
C33 C34 H34A 109.5 . . ?
C33 C34 H34B 109.5 . . ?
H34A C34 H34B 109.5 . . ?
C33 C34 H34C 109.5 . . ?
H34A C34 H34C 109.5 . . ?
H34B C34 H34C 109.5 . . ?
C36 C35 P6 116.0(10) . . ?
C36 C35 H35A 108.3 . . ?
P6 C35 H35A 108.3 . . ?
C36 C35 H35B 108.3 . . ?
P6 C35 H35B 108.3 . . ?
H35A C35 H35B 107.4 . . ?
C35 C36 H36A 109.5 . . ?
C35 C36 H36B 109.5 . . ?
H36A C36 H36B 109.5 . . ?
C35 C36 H36C 109.5 . . ?
H36A C36 H36C 109.5 . . ?
H36B C36 H36C 109.5 . . ?
C38 C37 P7 116.8(10) . . ?
C38 C37 H37A 108.1 . . ?
P7 C37 H37A 108.1 . . ?
C38 C37 H37B 108.1 . . ?
P7 C37 H37B 108.1 . . ?
H37A C37 H37B 107.3 . . ?
C37 C38 H38A 109.5 . . ?
C37 C38 H38B 109.5 . . ?
H38A C38 H38B 109.5 . . ?
C37 C38 H38C 109.5 . . ?
H38A C38 H38C 109.5 . . ?
H38B C38 H38C 109.5 . . ?
C40 C39 P7 117.3(10) . . ?
C40 C39 H39A 108.0 . . ?
P7 C39 H39A 108.0 . . ?
C40 C39 H39B 108.0 . . ?
P7 C39 H39B 108.0 . . ?
H39A C39 H39B 107.2 . . ?
C39 C40 H40A 109.5 . . ?
C39 C40 H40B 109.5 . . ?
H40A C40 H40B 109.5 . . ?
C39 C40 H40C 109.5 . . ?
H40A C40 H40C 109.5 . . ?
H40B C40 H40C 109.5 . . ?
C42 C41 P7 117.3(10) . . ?
C42 C41 H41A 108.0 . . ?
P7 C41 H41A 108.0 . . ?
C42 C41 H41B 108.0 . . ?
P7 C41 H41B 108.0 . . ?
H41A C41 H41B 107.2 . . ?
C41 C42 H42A 109.5 . . ?
C41 C42 H42B 109.5 . . ?
H42A C42 H42B 109.5 . . ?
C41 C42 H42C 109.5 . . ?
H42A C42 H42C 109.5 . . ?
H42B C42 H42C 109.5 . . ?
C44 C43 P8 117.7(10) . . ?
C44 C43 H43A 107.9 . . ?
P8 C43 H43A 107.9 . . ?
C44 C43 H43B 107.9 . . ?
P8 C43 H43B 107.9 . . ?
H43A C43 H43B 107.2 . . ?
C43 C44 H44A 109.5 . . ?
C43 C44 H44B 109.5 . . ?
H44A C44 H44B 109.5 . . ?
C43 C44 H44C 109.5 . . ?
H44A C44 H44C 109.5 . . ?
H44B C44 H44C 109.5 . . ?
C46 C45 P8 117.0(10) . . ?
C46 C45 H45A 108.1 . . ?
P8 C45 H45A 108.1 . . ?
C46 C45 H45B 108.1 . . ?
P8 C45 H45B 108.1 . . ?
H45A C45 H45B 107.3 . . ?
C45 C46 H46A 109.5 . . ?
C45 C46 H46B 109.5 . . ?
H46A C46 H46B 109.5 . . ?
C45 C46 H46C 109.5 . . ?
H46A C46 H46C 109.5 . . ?
H46B C46 H46C 109.5 . . ?
C48 C47 P8 117.3(10) . . ?
C48 C47 H47A 108.0 . . ?
P8 C47 H47A 108.0 . . ?
C48 C47 H47B 108.0 . . ?
P8 C47 H47B 108.0 . . ?
H47A C47 H47B 107.2 . . ?
C47 C48 H48A 109.5 . . ?
C47 C48 H48B 109.5 . . ?
H48A C48 H48B 109.5 . . ?
C47 C48 H48C 109.5 . . ?
H48A C48 H48C 109.5 . . ?
H48B C48 H48C 109.5 . . ?
C50 C49 P9 117.1(10) . . ?
C50 C49 H49A 108.0 . . ?
P9 C49 H49A 108.0 . . ?
C50 C49 H49B 108.0 . . ?
P9 C49 H49B 108.0 . . ?
H49A C49 H49B 107.3 . . ?
C49 C50 H50A 109.5 . . ?
C49 C50 H50B 109.5 . . ?
H50A C50 H50B 109.5 . . ?
C49 C50 H50C 109.5 . . ?
H50A C50 H50C 109.5 . . ?
H50B C50 H50C 109.5 . . ?
C52 C51 P9 117.2(10) . . ?
C52 C51 H51A 108.0 . . ?
P9 C51 H51A 108.0 . . ?
C52 C51 H51B 108.0 . . ?
P9 C51 H51B 108.0 . . ?
H51A C51 H51B 107.2 . . ?
C51 C52 H52A 109.5 . . ?
C51 C52 H52B 109.5 . . ?
H52A C52 H52B 109.5 . . ?
C51 C52 H52C 109.5 . . ?
H52A C52 H52C 109.5 . . ?
H52B C52 H52C 109.5 . . ?
C54 C53 P9 117.0(10) . . ?
C54 C53 H53A 108.0 . . ?
P9 C53 H53A 108.0 . . ?
C54 C53 H53B 108.0 . . ?
P9 C53 H53B 108.0 . . ?
H53A C53 H53B 107.3 . . ?
C53 C54 H54A 109.5 . . ?
C53 C54 H54B 109.5 . . ?
H54A C54 H54B 109.5 . . ?
C53 C54 H54C 109.5 . . ?
H54A C54 H54C 109.5 . . ?
H54B C54 H54C 109.5 . . ?
C56 C55 P10 118.0(10) . . ?
C56 C55 H55A 107.8 . . ?
P10 C55 H55A 107.8 . . ?
C56 C55 H55B 107.8 . . ?
P10 C55 H55B 107.8 . . ?
H55A C55 H55B 107.1 . . ?
C55 C56 H56A 109.5 . . ?
C55 C56 H56B 109.5 . . ?
H56A C56 H56B 109.5 . . ?
C55 C56 H56C 109.5 . . ?
H56A C56 H56C 109.5 . . ?
H56B C56 H56C 109.5 . . ?
C58 C57 P10 117.1(10) . . ?
C58 C57 H57A 108.0 . . ?
P10 C57 H57A 108.0 . . ?
C58 C57 H57B 108.0 . . ?
P10 C57 H57B 108.0 . . ?
H57A C57 H57B 107.3 . . ?
C57 C58 H58A 109.5 . . ?
C57 C58 H58B 109.5 . . ?
H58A C58 H58B 109.5 . . ?
C57 C58 H58C 109.5 . . ?
H58A C58 H58C 109.5 . . ?
H58B C58 H58C 109.5 . . ?
C60 C59 P10 117.1(10) . . ?
C60 C59 H59A 108.0 . . ?
P10 C59 H59A 108.0 . . ?
C60 C59 H59B 108.0 . . ?
P10 C59 H59B 108.0 . . ?
H59A C59 H59B 107.3 . . ?
C59 C60 H60A 109.5 . . ?
C59 C60 H60B 109.5 . . ?
H60A C60 H60B 109.5 . . ?
C59 C60 H60C 109.5 . . ?
H60A C60 H60C 109.5 . . ?
H60B C60 H60C 109.5 . . ?
C61 C62 C63 111(2) . . ?
C64 C63 C62 111(2) . . ?
C63 C64 C65 111(2) . . ?
Ni6 Ni1 Ni7 69.6(2) . . ?
Ni6 Ni1 Ni12 71.9(2) . . ?
Ni7 Ni1 Ni12 71.96(19) . . ?
Ni6 Ni1 Ni2 158.4(3) . . ?
Ni7 Ni1 Ni2 110.3(2) . . ?
Ni12 Ni1 Ni2 129.4(3) . . ?
Ni6 Ni1 Ni11 65.93(19) . . ?
Ni7 Ni1 Ni11 98.6(2) . . ?
Ni12 Ni1 Ni11 137.3(2) . . ?
Ni2 Ni1 Ni11 93.2(2) . . ?
Ni6 Ni1 Ni10 98.7(2) . . ?
Ni7 Ni1 Ni10 64.91(19) . . ?
Ni12 Ni1 Ni10 136.3(2) . . ?
Ni2 Ni1 Ni10 63.85(19) . . ?
Ni11 Ni1 Ni10 59.52(19) . . ?
Ni6 Ni1 Ni14 95.8(2) . . ?
Ni7 Ni1 Ni14 135.5(2) . . ?
Ni12 Ni1 Ni14 63.55(18) . . ?
Ni2 Ni1 Ni14 98.1(2) . . ?
Ni11 Ni1 Ni14 113.7(2) . . ?
Ni10 Ni1 Ni14 158.7(2) . . ?
Ni6 Ni1 Ni13 134.8(2) . . ?
Ni7 Ni1 Ni13 94.9(2) . . ?
Ni12 Ni1 Ni13 62.9(2) . . ?
Ni2 Ni1 Ni13 66.54(19) . . ?
Ni11 Ni1 Ni13 158.7(2) . . ?
Ni10 Ni1 Ni13 112.9(2) . . ?
Ni14 Ni1 Ni13 65.32(17) . . ?
Ni6 Ni1 Ni4 111.1(2) . . ?
Ni7 Ni1 Ni4 158.1(2) . . ?
Ni12 Ni1 Ni4 129.7(2) . . ?
Ni2 Ni1 Ni4 60.59(17) . . ?
Ni11 Ni1 Ni4 64.04(17) . . ?
Ni10 Ni1 Ni4 93.8(2) . . ?
Ni14 Ni1 Ni4 66.27(17) . . ?
Ni13 Ni1 Ni4 98.5(2) . . ?
Ni6 Ni1 Ni9 57.62(17) . . ?
Ni7 Ni1 Ni9 127.2(2) . . ?
Ni12 Ni1 Ni9 91.76(19) . . ?
Ni2 Ni1 Ni9 118.2(2) . . ?
Ni11 Ni1 Ni9 60.27(16) . . ?
Ni10 Ni1 Ni9 119.8(2) . . ?
Ni14 Ni1 Ni9 56.95(16) . . ?
Ni13 Ni1 Ni9 122.2(2) . . ?
Ni4 Ni1 Ni9 57.57(15) . . ?
Ni6 Ni1 Ni8 127.1(2) . . ?
Ni7 Ni1 Ni8 57.5(2) . . ?
Ni12 Ni1 Ni8 91.3(2) . . ?
Ni2 Ni1 Ni8 56.97(18) . . ?
Ni11 Ni1 Ni8 119.2(2) . . ?
Ni10 Ni1 Ni8 59.8(2) . . ?
Ni14 Ni1 Ni8 121.4(2) . . ?
Ni13 Ni1 Ni8 56.20(18) . . ?
Ni4 Ni1 Ni8 117.6(2) . . ?
Ni9 Ni1 Ni8 175.1(2) . . ?
S14 Ni2 S4 166.0(3) . . ?
S14 Ni2 Ni1 84.3(3) . . ?
S4 Ni2 Ni1 103.9(3) . . ?
S14 Ni2 Ni3 83.8(3) . . ?
S4 Ni2 Ni3 102.6(4) . . ?
Ni1 Ni2 Ni3 113.9(2) . . ?
S14 Ni2 Ni4 56.8(2) . . ?
S4 Ni2 Ni4 137.2(3) . . ?
Ni1 Ni2 Ni4 60.10(17) . . ?
Ni3 Ni2 Ni4 59.30(17) . . ?
S14 Ni2 Ni8 120.1(3) . . ?
S4 Ni2 Ni8 55.4(3) . . ?
Ni1 Ni2 Ni8 67.23(19) . . ?
Ni3 Ni2 Ni8 155.5(3) . . ?
Ni4 Ni2 Ni8 127.3(2) . . ?
S14 Ni2 Ni16 119.0(3) . . ?
S4 Ni2 Ni16 54.8(3) . . ?
Ni1 Ni2 Ni16 155.8(3) . . ?
Ni3 Ni2 Ni16 66.19(19) . . ?
Ni4 Ni2 Ni16 125.5(2) . . ?
Ni8 Ni2 Ni16 102.4(3) . . ?
S14 Ni2 Ni10 58.8(3) . . ?
S4 Ni2 Ni10 115.8(4) . . ?
Ni1 Ni2 Ni10 58.19(16) . . ?
Ni3 Ni2 Ni10 141.6(3) . . ?
Ni4 Ni2 Ni10 90.2(2) . . ?
Ni8 Ni2 Ni10 61.4(2) . . ?
Ni16 Ni2 Ni10 137.7(2) . . ?
S14 Ni2 Ni20 57.4(3) . . ?
S4 Ni2 Ni20 115.4(3) . . ?
Ni1 Ni2 Ni20 140.7(3) . . ?
Ni3 Ni2 Ni20 57.86(17) . . ?
Ni4 Ni2 Ni20 88.6(2) . . ?
Ni8 Ni2 Ni20 137.7(2) . . ?
Ni16 Ni2 Ni20 61.7(2) . . ?
Ni10 Ni2 Ni20 102.6(2) . . ?
S14 Ni2 Ni25 60.0(3) . . ?
S4 Ni2 Ni25 106.1(3) . . ?
Ni1 Ni2 Ni25 114.3(2) . . ?
Ni3 Ni2 Ni25 114.3(2) . . ?
Ni4 Ni2 Ni25 116.7(2) . . ?
Ni8 Ni2 Ni25 84.8(2) . . ?
Ni16 Ni2 Ni25 85.2(2) . . ?
Ni10 Ni2 Ni25 56.22(17) . . ?
Ni20 Ni2 Ni25 56.50(18) . . ?
S14 Ni2 Ni13 140.2(3) . . ?
S4 Ni2 Ni13 51.2(3) . . ?
Ni1 Ni2 Ni13 57.01(18) . . ?
Ni3 Ni2 Ni13 102.3(2) . . ?
Ni4 Ni2 Ni13 92.34(19) . . ?
Ni8 Ni2 Ni13 56.49(18) . . ?
Ni16 Ni2 Ni13 98.8(2) . . ?
Ni10 Ni2 Ni13 101.7(2) . . ?
Ni20 Ni2 Ni13 155.7(2) . . ?
Ni25 Ni2 Ni13 141.2(2) . . ?
S14 Ni2 Ni23 138.9(3) . . ?
S4 Ni2 Ni23 51.0(3) . . ?
Ni1 Ni2 Ni23 102.7(2) . . ?
Ni3 Ni2 Ni23 56.11(19) . . ?
Ni4 Ni2 Ni23 91.47(19) . . ?
Ni8 Ni2 Ni23 99.4(3) . . ?
Ni16 Ni2 Ni23 56.00(18) . . ?
Ni10 Ni2 Ni23 156.2(3) . . ?
Ni20 Ni2 Ni23 101.2(2) . . ?
Ni25 Ni2 Ni23 141.1(2) . . ?
Ni13 Ni2 Ni23 54.52(19) . . ?
Ni17 Ni3 Ni18 69.0(2) . . ?
Ni17 Ni3 Ni4 157.6(2) . . ?
Ni18 Ni3 Ni4 110.7(2) . . ?
Ni17 Ni3 Ni23 95.6(3) . . ?
Ni18 Ni3 Ni23 134.1(3) . . ?
Ni4 Ni3 Ni23 99.2(2) . . ?
Ni17 Ni3 Ni24 135.0(2) . . ?
Ni18 Ni3 Ni24 94.3(2) . . ?
Ni4 Ni3 Ni24 66.99(18) . . ?
Ni23 Ni3 Ni24 65.81(19) . . ?
Ni17 Ni3 Ni20 65.39(19) . . ?
Ni18 Ni3 Ni20 98.5(2) . . ?
Ni4 Ni3 Ni20 93.1(2) . . ?
Ni23 Ni3 Ni20 114.2(2) . . ?
Ni24 Ni3 Ni20 159.2(2) . . ?
Ni17 Ni3 Ni22 71.8(2) . . ?
Ni18 Ni3 Ni22 70.6(2) . . ?
Ni4 Ni3 Ni22 130.1(2) . . ?
Ni23 Ni3 Ni22 63.5(2) . . ?
Ni24 Ni3 Ni22 63.19(18) . . ?
Ni20 Ni3 Ni22 136.8(2) . . ?
Ni17 Ni3 Ni2 110.9(2) . . ?
Ni18 Ni3 Ni2 158.5(3) . . ?
Ni4 Ni3 Ni2 60.72(17) . . ?
Ni23 Ni3 Ni2 67.2(2) . . ?
Ni24 Ni3 Ni2 99.2(2) . . ?
Ni20 Ni3 Ni2 64.14(18) . . ?
Ni22 Ni3 Ni2 130.5(3) . . ?
Ni17 Ni3 Ni21 97.5(2) . . ?
Ni18 Ni3 Ni21 65.0(2) . . ?
Ni4 Ni3 Ni21 64.27(18) . . ?
Ni23 Ni3 Ni21 160.2(3) . . ?
Ni24 Ni3 Ni21 113.1(2) . . ?
Ni20 Ni3 Ni21 59.17(19) . . ?
Ni22 Ni3 Ni21 135.1(3) . . ?
Ni2 Ni3 Ni21 94.2(2) . . ?
Ni17 Ni3 Ni16 57.8(2) . . ?
Ni18 Ni3 Ni16 126.8(2) . . ?
Ni4 Ni3 Ni16 118.3(2) . . ?
Ni23 Ni3 Ni16 56.62(19) . . ?
Ni24 Ni3 Ni16 122.4(3) . . ?
Ni20 Ni3 Ni16 60.77(19) . . ?
Ni22 Ni3 Ni16 91.7(2) . . ?
Ni2 Ni3 Ni16 57.57(18) . . ?
Ni21 Ni3 Ni16 119.9(2) . . ?
Ni17 Ni3 Ni19 126.1(3) . . ?
Ni18 Ni3 Ni19 57.10(17) . . ?
Ni4 Ni3 Ni19 57.79(17) . . ?
Ni23 Ni3 Ni19 121.8(2) . . ?
Ni24 Ni3 Ni19 56.06(17) . . ?
Ni20 Ni3 Ni19 119.1(2) . . ?
Ni22 Ni3 Ni19 90.6(2) . . ?
Ni2 Ni3 Ni19 118.5(2) . . ?
Ni21 Ni3 Ni19 60.05(17) . . ?
Ni16 Ni3 Ni19 176.0(2) . . ?
S14 Ni4 S13 165.9(4) . . ?
S14 Ni4 Ni3 84.7(3) . . ?
S13 Ni4 Ni3 103.6(3) . . ?
S14 Ni4 Ni1 84.4(3) . . ?
S13 Ni4 Ni1 102.1(3) . . ?
Ni3 Ni4 Ni1 113.8(2) . . ?
S14 Ni4 Ni2 57.7(3) . . ?
S13 Ni4 Ni2 136.3(3) . . ?
Ni3 Ni4 Ni2 59.99(18) . . ?
Ni1 Ni4 Ni2 59.31(17) . . ?
S14 Ni4 Ni9 118.4(3) . . ?
S13 Ni4 Ni9 55.2(3) . . ?
Ni3 Ni4 Ni9 156.0(2) . . ?
Ni1 Ni4 Ni9 65.94(16) . . ?
Ni2 Ni4 Ni9 125.2(2) . . ?
S14 Ni4 Ni19 119.5(3) . . ?
S13 Ni4 Ni19 55.9(3) . . ?
Ni3 Ni4 Ni19 66.96(18) . . ?
Ni1 Ni4 Ni19 155.5(2) . . ?
Ni2 Ni4 Ni19 126.9(2) . . ?
Ni9 Ni4 Ni19 103.00(19) . . ?
S14 Ni4 Ni11 57.5(2) . . ?
S13 Ni4 Ni11 115.5(3) . . ?
Ni3 Ni4 Ni11 140.9(2) . . ?
Ni1 Ni4 Ni11 57.67(18) . . ?
Ni2 Ni4 Ni11 88.79(19) . . ?
Ni9 Ni4 Ni11 61.08(16) . . ?
Ni19 Ni4 Ni11 138.1(2) . . ?
S14 Ni4 Ni21 58.4(3) . . ?
S13 Ni4 Ni21 116.2(3) . . ?
Ni3 Ni4 Ni21 58.25(18) . . ?
Ni1 Ni4 Ni21 141.7(2) . . ?
Ni2 Ni4 Ni21 90.29(19) . . ?
Ni9 Ni4 Ni21 137.8(2) . . ?
Ni19 Ni4 Ni21 61.25(16) . . ?
Ni11 Ni4 Ni21 102.9(2) . . ?
S14 Ni4 Ni27 58.0(3) . . ?
S13 Ni4 Ni27 107.9(3) . . ?
Ni3 Ni4 Ni27 114.1(2) . . ?
Ni1 Ni4 Ni27 113.8(2) . . ?
Ni2 Ni4 Ni27 115.7(2) . . ?
Ni9 Ni4 Ni27 85.68(19) . . ?
Ni19 Ni4 Ni27 85.79(19) . . ?
Ni11 Ni4 Ni27 56.23(17) . . ?
Ni21 Ni4 Ni27 55.98(16) . . ?
S14 Ni4 Ni14 140.1(3) . . ?
S13 Ni4 Ni14 50.1(3) . . ?
Ni3 Ni4 Ni14 102.0(2) . . ?
Ni1 Ni4 Ni14 56.69(15) . . ?
Ni2 Ni4 Ni14 91.4(2) . . ?
Ni9 Ni4 Ni14 56.68(16) . . ?
Ni19 Ni4 Ni14 98.81(18) . . ?
Ni11 Ni4 Ni14 101.68(19) . . ?
Ni21 Ni4 Ni14 155.3(2) . . ?
Ni27 Ni4 Ni14 142.2(2) . . ?
S14 Ni4 Ni24 140.4(3) . . ?
S13 Ni4 Ni24 50.8(3) . . ?
Ni3 Ni4 Ni24 56.53(16) . . ?
Ni1 Ni4 Ni24 102.8(2) . . ?
Ni2 Ni4 Ni24 92.3(2) . . ?
Ni9 Ni4 Ni24 99.57(19) . . ?
Ni19 Ni4 Ni24 55.88(17) . . ?
Ni11 Ni4 Ni24 156.0(2) . . ?
Ni21 Ni4 Ni24 101.0(2) . . ?
Ni27 Ni4 Ni24 141.6(2) . . ?
Ni14 Ni4 Ni24 54.35(16) . . ?
P2 Ni6 S1 101.7(4) . . ?
P2 Ni6 S12 103.8(4) . . ?
S1 Ni6 S12 154.4(4) . . ?
P2 Ni6 Ni1 170.1(4) . . ?
S1 Ni6 Ni1 75.3(3) . . ?
S12 Ni6 Ni1 79.2(3) . . ?
P2 Ni6 Ni9 105.5(3) . . ?
S1 Ni6 Ni9 114.5(3) . . ?
S12 Ni6 Ni9 55.8(3) . . ?
Ni1 Ni6 Ni9 68.08(17) . . ?
P2 Ni6 Ni11 111.9(3) . . ?
S1 Ni6 Ni11 53.3(3) . . ?
S12 Ni6 Ni11 113.4(3) . . ?
Ni1 Ni6 Ni11 58.61(18) . . ?
Ni9 Ni6 Ni11 61.35(17) . . ?
P2 Ni6 Ni7 130.3(3) . . ?
S1 Ni6 Ni7 52.4(4) . . ?
S12 Ni6 Ni7 110.1(3) . . ?
Ni1 Ni6 Ni7 55.38(18) . . ?
Ni9 Ni6 Ni7 123.5(2) . . ?
Ni11 Ni6 Ni7 86.7(2) . . ?
P2 Ni6 Ni12 133.6(3) . . ?
S1 Ni6 Ni12 112.3(4) . . ?
S12 Ni6 Ni12 48.8(3) . . ?
Ni1 Ni6 Ni12 55.29(17) . . ?
Ni9 Ni6 Ni12 88.56(19) . . ?
Ni11 Ni6 Ni12 113.6(2) . . ?
Ni7 Ni6 Ni12 61.56(18) . . ?
P1 Ni7 S1 109.3(5) . . ?
P1 Ni7 S2 95.9(5) . . ?
S1 Ni7 S2 154.8(4) . . ?
P1 Ni7 Ni1 169.9(4) . . ?
S1 Ni7 Ni1 74.8(3) . . ?
S2 Ni7 Ni1 80.1(3) . . ?
P1 Ni7 Ni8 101.6(4) . . ?
S1 Ni7 Ni8 115.2(3) . . ?
S2 Ni7 Ni8 55.9(3) . . ?
Ni1 Ni7 Ni8 68.4(2) . . ?
P1 Ni7 Ni10 115.4(4) . . ?
S1 Ni7 Ni10 54.0(3) . . ?
S2 Ni7 Ni10 114.0(4) . . ?
Ni1 Ni7 Ni10 59.01(18) . . ?
Ni8 Ni7 Ni10 61.5(2) . . ?
P1 Ni7 Ni6 134.8(4) . . ?
S1 Ni7 Ni6 52.0(3) . . ?
S2 Ni7 Ni6 110.3(3) . . ?
Ni1 Ni7 Ni6 55.05(17) . . ?
Ni8 Ni7 Ni6 123.5(2) . . ?
Ni10 Ni7 Ni6 87.3(2) . . ?
P1 Ni7 Ni12 128.4(4) . . ?
S1 Ni7 Ni12 111.5(3) . . ?
S2 Ni7 Ni12 49.2(3) . . ?
Ni1 Ni7 Ni12 55.08(17) . . ?
Ni8 Ni7 Ni12 88.3(2) . . ?
Ni10 Ni7 Ni12 113.7(2) . . ?
Ni6 Ni7 Ni12 61.24(17) . . ?
S3 Ni8 S2 142.4(5) . . ?
S3 Ni8 S4 114.8(5) . . ?
S2 Ni8 S4 101.5(5) . . ?
S3 Ni8 Ni13 154.6(4) . . ?
S2 Ni8 Ni13 57.8(3) . . ?
S4 Ni8 Ni13 55.8(3) . . ?
S3 Ni8 Ni7 92.2(4) . . ?
S2 Ni8 Ni7 57.2(4) . . ?
S4 Ni8 Ni7 148.3(3) . . ?
Ni13 Ni8 Ni7 92.6(2) . . ?
S3 Ni8 Ni2 88.6(4) . . ?
S2 Ni8 Ni2 118.7(3) . . ?
S4 Ni8 Ni2 61.1(3) . . ?
Ni13 Ni8 Ni2 66.1(2) . . ?
Ni7 Ni8 Ni2 105.9(2) . . ?
S3 Ni8 Ni15 57.8(3) . . ?
S2 Ni8 Ni15 154.3(5) . . ?
S4 Ni8 Ni15 57.3(3) . . ?
Ni13 Ni8 Ni15 110.1(3) . . ?
Ni7 Ni8 Ni15 148.2(3) . . ?
Ni2 Ni8 Ni15 66.4(2) . . ?
S3 Ni8 Ni10 53.3(3) . . ?
S2 Ni8 Ni10 115.3(4) . . ?
S4 Ni8 Ni10 121.3(4) . . ?
Ni13 Ni8 Ni10 108.5(2) . . ?
Ni7 Ni8 Ni10 61.5(2) . . ?
Ni2 Ni8 Ni10 61.39(19) . . ?
Ni15 Ni8 Ni10 89.6(2) . . ?
S3 Ni8 Ni1 108.1(4) . . ?
S2 Ni8 Ni1 73.3(3) . . ?
S4 Ni8 Ni1 99.6(3) . . ?
Ni13 Ni8 Ni1 56.43(18) . . ?
Ni7 Ni8 Ni1 54.03(18) . . ?
Ni2 Ni8 Ni1 55.80(16) . . ?
Ni15 Ni8 Ni1 121.2(3) . . ?
Ni10 Ni8 Ni1 54.84(17) . . ?
S12 Ni9 S11 144.5(4) . . ?
S12 Ni9 S13 100.8(4) . . ?
S11 Ni9 S13 113.8(4) . . ?
S12 Ni9 Ni6 56.7(3) . . ?
S11 Ni9 Ni6 94.1(3) . . ?
S13 Ni9 Ni6 147.1(3) . . ?
S12 Ni9 Ni14 57.8(3) . . ?
S11 Ni9 Ni14 153.1(3) . . ?
S13 Ni9 Ni14 54.2(3) . . ?
Ni6 Ni9 Ni14 93.1(2) . . ?
S12 Ni9 Ni28 154.1(3) . . ?
S11 Ni9 Ni28 56.7(3) . . ?
S13 Ni9 Ni28 57.5(3) . . ?
Ni6 Ni9 Ni28 149.1(2) . . ?
Ni14 Ni9 Ni28 109.1(2) . . ?
S12 Ni9 Ni4 118.3(3) . . ?
S11 Ni9 Ni4 87.4(3) . . ?
S13 Ni9 Ni4 59.7(2) . . ?
Ni6 Ni9 Ni4 107.0(2) . . ?
Ni14 Ni9 Ni4 65.63(17) . . ?
Ni28 Ni9 Ni4 65.79(17) . . ?
S12 Ni9 Ni11 115.2(3) . . ?
S11 Ni9 Ni11 53.5(3) . . ?
S13 Ni9 Ni11 120.3(3) . . ?
Ni6 Ni9 Ni11 62.40(17) . . ?
Ni14 Ni9 Ni11 108.4(2) . . ?
Ni28 Ni9 Ni11 89.6(2) . . ?
Ni4 Ni9 Ni11 61.56(16) . . ?
S12 Ni9 Ni1 72.5(3) . . ?
S11 Ni9 Ni1 108.5(3) . . ?
S13 Ni9 Ni1 98.4(3) . . ?
Ni6 Ni9 Ni1 54.30(16) . . ?
Ni14 Ni9 Ni1 56.53(16) . . ?
Ni28 Ni9 Ni1 121.3(2) . . ?
Ni4 Ni9 Ni1 56.49(16) . . ?
Ni11 Ni9 Ni1 55.06(17) . . ?
S3 Ni10 S1 128.2(5) . . ?
S3 Ni10 S14 117.3(4) . . ?
S1 Ni10 S14 114.1(4) . . ?
S3 Ni10 Ni11 175.7(4) . . ?
S1 Ni10 Ni11 56.2(3) . . ?
S14 Ni10 Ni11 58.4(2) . . ?
S3 Ni10 Ni1 119.5(4) . . ?
S1 Ni10 Ni1 73.4(3) . . ?
S14 Ni10 Ni1 81.9(3) . . ?
Ni11 Ni10 Ni1 60.19(18) . . ?
S3 Ni10 Ni25 57.2(3) . . ?
S1 Ni10 Ni25 161.3(4) . . ?
S14 Ni10 Ni25 61.6(2) . . ?
Ni11 Ni10 Ni25 118.9(3) . . ?
Ni1 Ni10 Ni25 121.5(2) . . ?
S3 Ni10 Ni7 89.7(4) . . ?
S1 Ni10 Ni7 54.2(4) . . ?
S14 Ni10 Ni7 137.8(3) . . ?
Ni11 Ni10 Ni7 93.3(2) . . ?
Ni1 Ni10 Ni7 56.08(17) . . ?
Ni25 Ni10 Ni7 142.1(3) . . ?
S3 Ni10 Ni2 86.3(4) . . ?
S1 Ni10 Ni2 130.6(3) . . ?
S14 Ni10 Ni2 54.7(3) . . ?
Ni11 Ni10 Ni2 90.1(2) . . ?
Ni1 Ni10 Ni2 57.96(17) . . ?
Ni25 Ni10 Ni2 63.65(18) . . ?
Ni7 Ni10 Ni2 99.5(2) . . ?
S3 Ni10 Ni8 54.2(3) . . ?
S1 Ni10 Ni8 111.1(4) . . ?
S14 Ni10 Ni8 111.8(3) . . ?
Ni11 Ni10 Ni8 125.5(2) . . ?
Ni1 Ni10 Ni8 65.39(19) . . ?
Ni25 Ni10 Ni8 86.6(2) . . ?
Ni7 Ni10 Ni8 57.0(2) . . ?
Ni2 Ni10 Ni8 57.2(2) . . ?
S1 Ni11 S11 127.8(4) . . ?
S1 Ni11 S14 116.5(4) . . ?
S11 Ni11 S14 115.3(4) . . ?
S1 Ni11 Ni10 56.6(3) . . ?
S11 Ni11 Ni10 175.5(3) . . ?
S14 Ni11 Ni10 60.4(3) . . ?
S1 Ni11 Ni1 73.6(4) . . ?
S11 Ni11 Ni1 119.0(3) . . ?
S14 Ni11 Ni1 83.0(3) . . ?
Ni10 Ni11 Ni1 60.29(19) . . ?
S1 Ni11 Ni27 161.6(4) . . ?
S11 Ni11 Ni27 57.0(3) . . ?
S14 Ni11 Ni27 59.9(3) . . ?
Ni10 Ni11 Ni27 119.1(2) . . ?
Ni1 Ni11 Ni27 121.4(2) . . ?
S1 Ni11 Ni9 109.6(3) . . ?
S11 Ni11 Ni9 54.5(3) . . ?
S14 Ni11 Ni9 111.6(3) . . ?
Ni10 Ni11 Ni9 124.9(3) . . ?
Ni1 Ni11 Ni9 64.66(17) . . ?
Ni27 Ni11 Ni9 87.56(19) . . ?
S1 Ni11 Ni4 131.4(4) . . ?
S11 Ni11 Ni4 85.3(3) . . ?
S14 Ni11 Ni4 54.3(2) . . ?
Ni10 Ni11 Ni4 90.8(2) . . ?
Ni1 Ni11 Ni4 58.28(17) . . ?
Ni27 Ni11 Ni4 63.27(18) . . ?
Ni9 Ni11 Ni4 57.36(15) . . ?
S1 Ni11 Ni6 53.5(3) . . ?
S11 Ni11 Ni6 90.3(3) . . ?
S14 Ni11 Ni6 138.3(4) . . ?
Ni10 Ni11 Ni6 92.6(2) . . ?
Ni1 Ni11 Ni6 55.46(17) . . ?
Ni27 Ni11 Ni6 142.4(2) . . ?
Ni9 Ni11 Ni6 56.25(16) . . ?
Ni4 Ni11 Ni6 99.3(2) . . ?
S12 Ni12 S2 157.6(4) . . ?
S12 Ni12 P5 99.5(4) . . ?
S2 Ni12 P5 102.1(4) . . ?
S12 Ni12 Ni1 78.9(3) . . ?
S2 Ni12 Ni1 80.3(3) . . ?
P5 Ni12 Ni1 173.2(3) . . ?
S12 Ni12 Ni13 117.4(3) . . ?
S2 Ni12 Ni13 56.6(3) . . ?
P5 Ni12 Ni13 116.9(3) . . ?
Ni1 Ni12 Ni13 58.99(19) . . ?
S12 Ni12 Ni14 56.4(3) . . ?
S2 Ni12 Ni14 117.7(4) . . ?
P5 Ni12 Ni14 115.0(3) . . ?
Ni1 Ni12 Ni14 58.57(16) . . ?
Ni13 Ni12 Ni14 62.24(17) . . ?
S12 Ni12 Ni6 51.0(3) . . ?
S2 Ni12 Ni6 108.8(4) . . ?
P5 Ni12 Ni6 130.9(3) . . ?
Ni1 Ni12 Ni6 52.85(17) . . ?
Ni13 Ni12 Ni6 111.8(2) . . ?
Ni14 Ni12 Ni6 82.89(18) . . ?
S12 Ni12 Ni7 107.9(3) . . ?
S2 Ni12 Ni7 51.8(3) . . ?
P5 Ni12 Ni7 133.4(3) . . ?
Ni1 Ni12 Ni7 52.96(16) . . ?
Ni13 Ni12 Ni7 82.7(2) . . ?
Ni14 Ni12 Ni7 111.5(2) . . ?
Ni6 Ni12 Ni7 57.20(17) . . ?
S4 Ni13 S5 109.5(4) . . ?
S4 Ni13 S2 102.0(4) . . ?
S5 Ni13 S2 143.6(4) . . ?
S4 Ni13 Ni8 58.1(4) . . ?
S5 Ni13 Ni8 159.7(4) . . ?
S2 Ni13 Ni8 56.1(3) . . ?
S4 Ni13 Ni1 109.8(4) . . ?
S5 Ni13 Ni1 106.9(3) . . ?
S2 Ni13 Ni1 78.1(4) . . ?
Ni8 Ni13 Ni1 67.4(2) . . ?
S4 Ni13 Ni23 56.3(3) . . ?
S5 Ni13 Ni23 55.4(3) . . ?
S2 Ni13 Ni23 158.2(3) . . ?
Ni8 Ni13 Ni23 106.9(2) . . ?
Ni1 Ni13 Ni23 109.5(3) . . ?
S4 Ni13 Ni12 152.6(4) . . ?
S5 Ni13 Ni12 97.8(3) . . ?
S2 Ni13 Ni12 53.3(3) . . ?
Ni8 Ni13 Ni12 95.1(2) . . ?
Ni1 Ni13 Ni12 58.08(18) . . ?
Ni23 Ni13 Ni12 148.2(2) . . ?
S4 Ni13 Ni14 138.7(4) . . ?
S5 Ni13 Ni14 52.3(3) . . ?
S2 Ni13 Ni14 111.5(3) . . ?
Ni8 Ni13 Ni14 124.5(3) . . ?
Ni1 Ni13 Ni14 57.24(16) . . ?
Ni23 Ni13 Ni14 89.1(2) . . ?
Ni12 Ni13 Ni14 59.24(17) . . ?
S4 Ni13 Ni2 58.2(4) . . ?
S5 Ni13 Ni2 102.8(3) . . ?
S2 Ni13 Ni2 109.2(3) . . ?
Ni8 Ni13 Ni2 57.37(19) . . ?
Ni1 Ni13 Ni2 56.45(18) . . ?
Ni23 Ni13 Ni2 63.15(19) . . ?
Ni12 Ni13 Ni2 114.5(2) . . ?
Ni14 Ni13 Ni2 87.6(2) . . ?
S13 Ni14 S5 110.1(4) . . ?
S13 Ni14 S12 101.8(4) . . ?
S5 Ni14 S12 143.3(4) . . ?
S13 Ni14 Ni1 109.1(3) . . ?
S5 Ni14 Ni1 108.4(3) . . ?
S12 Ni14 Ni1 76.4(3) . . ?
S13 Ni14 Ni24 56.3(3) . . ?
S5 Ni14 Ni24 56.1(3) . . ?
S12 Ni14 Ni24 158.0(3) . . ?
Ni1 Ni14 Ni24 110.5(2) . . ?
S13 Ni14 Ni9 58.0(3) . . ?
S5 Ni14 Ni9 160.9(3) . . ?
S12 Ni14 Ni9 55.2(3) . . ?
Ni1 Ni14 Ni9 66.52(17) . . ?
Ni24 Ni14 Ni9 107.2(2) . . ?
S13 Ni14 Ni12 151.5(3) . . ?
S5 Ni14 Ni12 98.3(3) . . ?
S12 Ni14 Ni12 52.3(3) . . ?
Ni1 Ni14 Ni12 57.88(17) . . ?
Ni24 Ni14 Ni12 149.2(2) . . ?
Ni9 Ni14 Ni12 94.1(2) . . ?
S13 Ni14 Ni13 139.8(3) . . ?
S5 Ni14 Ni13 53.7(3) . . ?
S12 Ni14 Ni13 109.7(3) . . ?
Ni1 Ni14 Ni13 57.44(18) . . ?
Ni24 Ni14 Ni13 90.9(2) . . ?
Ni9 Ni14 Ni13 123.9(2) . . ?
Ni12 Ni14 Ni13 58.53(18) . . ?
S13 Ni14 Ni4 57.4(2) . . ?
S5 Ni14 Ni4 103.7(3) . . ?
S12 Ni14 Ni4 108.6(3) . . ?
Ni1 Ni14 Ni4 57.04(16) . . ?
Ni24 Ni14 Ni4 62.97(17) . . ?
Ni9 Ni14 Ni4 57.69(16) . . ?
Ni12 Ni14 Ni4 114.86(19) . . ?
Ni13 Ni14 Ni4 88.61(19) . . ?
P7 Ni15 S6 106.0(5) . . ?
P7 Ni15 S3 111.2(5) . . ?
S6 Ni15 S3 112.6(5) . . ?
P7 Ni15 S4 103.2(5) . . ?
S6 Ni15 S4 111.7(5) . . ?
S3 Ni15 S4 111.6(5) . . ?
P7 Ni15 Ni25 137.2(4) . . ?
S6 Ni15 Ni25 57.4(3) . . ?
S3 Ni15 Ni25 56.9(3) . . ?
S4 Ni15 Ni25 119.5(4) . . ?
P7 Ni15 Ni16 111.4(4) . . ?
S6 Ni15 Ni16 55.3(3) . . ?
S3 Ni15 Ni16 137.4(4) . . ?
S4 Ni15 Ni16 56.7(4) . . ?
Ni25 Ni15 Ni16 91.4(3) . . ?
P7 Ni15 Ni8 117.2(4) . . ?
S6 Ni15 Ni8 136.7(4) . . ?
S3 Ni15 Ni8 54.9(3) . . ?
S4 Ni15 Ni8 56.9(4) . . ?
Ni25 Ni15 Ni8 90.2(3) . . ?
Ni16 Ni15 Ni8 103.2(2) . . ?
P7 Ni15 Ni2 160.2(4) . . ?
S6 Ni15 Ni2 81.5(3) . . ?
S3 Ni15 Ni2 81.5(3) . . ?
S4 Ni15 Ni2 57.2(3) . . ?
Ni25 Ni15 Ni2 62.37(18) . . ?
Ni16 Ni15 Ni2 57.36(18) . . ?
Ni8 Ni15 Ni2 56.76(18) . . ?
S6 Ni16 S7 142.3(5) . . ?
S6 Ni16 S4 113.9(5) . . ?
S7 Ni16 S4 102.8(5) . . ?
S6 Ni16 Ni23 153.8(4) . . ?
S7 Ni16 Ni23 58.1(3) . . ?
S4 Ni16 Ni23 56.2(3) . . ?
S6 Ni16 Ni15 56.6(3) . . ?
S7 Ni16 Ni15 156.1(5) . . ?
S4 Ni16 Ni15 57.7(3) . . ?
Ni23 Ni16 Ni15 110.9(3) . . ?
S6 Ni16 Ni17 92.3(4) . . ?
S7 Ni16 Ni17 56.0(4) . . ?
S4 Ni16 Ni17 149.1(3) . . ?
Ni23 Ni16 Ni17 93.0(2) . . ?
Ni15 Ni16 Ni17 147.5(3) . . ?
S6 Ni16 Ni2 87.4(3) . . ?
S7 Ni16 Ni2 118.9(3) . . ?
S4 Ni16 Ni2 61.0(4) . . ?
Ni23 Ni16 Ni2 66.4(2) . . ?
Ni15 Ni16 Ni2 66.4(2) . . ?
Ni17 Ni16 Ni2 106.8(3) . . ?
S6 Ni16 Ni20 53.0(3) . . ?
S7 Ni16 Ni20 114.0(4) . . ?
S4 Ni16 Ni20 121.1(4) . . ?
Ni23 Ni16 Ni20 108.3(2) . . ?
Ni15 Ni16 Ni20 89.3(2) . . ?
Ni17 Ni16 Ni20 61.7(2) . . ?
Ni2 Ni16 Ni20 61.3(2) . . ?
S6 Ni16 Ni3 107.9(4) . . ?
S7 Ni16 Ni3 72.3(3) . . ?
S4 Ni16 Ni3 99.8(3) . . ?
Ni23 Ni16 Ni3 56.24(18) . . ?
Ni15 Ni16 Ni3 121.5(3) . . ?
Ni17 Ni16 Ni3 54.69(18) . . ?
Ni2 Ni16 Ni3 56.24(17) . . ?
Ni20 Ni16 Ni3 54.88(17) . . ?
S8 Ni17 P3 105.6(5) . . ?
S8 Ni17 S7 155.0(4) . . ?
P3 Ni17 S7 99.4(5) . . ?
S8 Ni17 Ni3 76.3(3) . . ?
P3 Ni17 Ni3 171.6(4) . . ?
S7 Ni17 Ni3 78.9(3) . . ?
S8 Ni17 Ni16 115.5(3) . . ?
P3 Ni17 Ni16 104.7(4) . . ?
S7 Ni17 Ni16 55.7(4) . . ?
Ni3 Ni17 Ni16 67.5(2) . . ?
S8 Ni17 Ni20 53.9(3) . . ?
P3 Ni17 Ni20 115.7(4) . . ?
S7 Ni17 Ni20 113.8(4) . . ?
Ni3 Ni17 Ni20 58.50(17) . . ?
Ni16 Ni17 Ni20 61.8(2) . . ?
S8 Ni17 Ni18 53.3(3) . . ?
P3 Ni17 Ni18 132.0(4) . . ?
S7 Ni17 Ni18 109.0(3) . . ?
Ni3 Ni17 Ni18 55.69(18) . . ?
Ni16 Ni17 Ni18 123.2(2) . . ?
Ni20 Ni17 Ni18 87.3(2) . . ?
S8 Ni17 Ni22 112.4(3) . . ?
P3 Ni17 Ni22 129.4(4) . . ?
S7 Ni17 Ni22 48.6(3) . . ?
Ni3 Ni17 Ni22 55.17(17) . . ?
Ni16 Ni17 Ni22 88.1(2) . . ?
Ni20 Ni17 Ni22 113.4(2) . . ?
Ni18 Ni17 Ni22 60.66(18) . . ?
P4 Ni18 S9 105.0(4) . . ?
P4 Ni18 S8 101.0(4) . . ?
S9 Ni18 S8 154.0(5) . . ?
P4 Ni18 Ni3 172.2(4) . . ?
S9 Ni18 Ni3 79.3(3) . . ?
S8 Ni18 Ni3 74.8(3) . . ?
P4 Ni18 Ni19 108.6(3) . . ?
S9 Ni18 Ni19 55.5(3) . . ?
S8 Ni18 Ni19 115.4(3) . . ?
Ni3 Ni18 Ni19 68.23(18) . . ?
P4 Ni18 Ni21 113.6(4) . . ?
S9 Ni18 Ni21 113.5(3) . . ?
S8 Ni18 Ni21 53.9(3) . . ?
Ni3 Ni18 Ni21 58.63(19) . . ?
Ni19 Ni18 Ni21 61.71(17) . . ?
P4 Ni18 Ni17 127.2(3) . . ?
S9 Ni18 Ni17 110.5(4) . . ?
S8 Ni18 Ni17 51.1(3) . . ?
Ni3 Ni18 Ni17 55.27(18) . . ?
Ni19 Ni18 Ni17 123.5(2) . . ?
Ni21 Ni18 Ni17 86.4(2) . . ?
P4 Ni18 Ni22 132.1(4) . . ?
S9 Ni18 Ni22 48.9(3) . . ?
S8 Ni18 Ni22 111.5(4) . . ?
Ni3 Ni18 Ni22 55.59(19) . . ?
Ni19 Ni18 Ni22 88.5(2) . . ?
Ni21 Ni18 Ni22 113.9(2) . . ?
Ni17 Ni18 Ni22 61.94(19) . . ?
S9 Ni19 S10 143.0(4) . . ?
S9 Ni19 S13 102.7(4) . . ?
S10 Ni19 S13 113.8(4) . . ?
S9 Ni19 Ni24 57.9(3) . . ?
S10 Ni19 Ni24 152.9(3) . . ?
S13 Ni19 Ni24 55.0(3) . . ?
S9 Ni19 Ni18 55.9(3) . . ?
S10 Ni19 Ni18 92.8(3) . . ?
S13 Ni19 Ni18 147.1(4) . . ?
Ni24 Ni19 Ni18 92.5(2) . . ?
S9 Ni19 Ni28 155.9(3) . . ?
S10 Ni19 Ni28 57.3(3) . . ?
S13 Ni19 Ni28 57.0(3) . . ?
Ni24 Ni19 Ni28 109.4(2) . . ?
Ni18 Ni19 Ni28 148.2(2) . . ?
S9 Ni19 Ni4 118.0(4) . . ?
S10 Ni19 Ni4 87.2(3) . . ?
S13 Ni19 Ni4 59.0(2) . . ?
Ni24 Ni19 Ni4 65.82(18) . . ?
Ni18 Ni19 Ni4 106.0(2) . . ?
Ni28 Ni19 Ni4 65.32(17) . . ?
S9 Ni19 Ni21 114.0(3) . . ?
S10 Ni19 Ni21 52.6(3) . . ?
S13 Ni19 Ni21 119.1(3) . . ?
Ni24 Ni19 Ni21 108.0(2) . . ?
Ni18 Ni19 Ni21 61.80(17) . . ?
Ni28 Ni19 Ni21 88.9(2) . . ?
Ni4 Ni19 Ni21 61.16(16) . . ?
S9 Ni19 Ni3 72.4(3) . . ?
S10 Ni19 Ni3 107.4(3) . . ?
S13 Ni19 Ni3 97.2(3) . . ?
Ni24 Ni19 Ni3 55.94(17) . . ?
Ni18 Ni19 Ni3 54.67(17) . . ?
Ni28 Ni19 Ni3 119.6(2) . . ?
Ni4 Ni19 Ni3 55.25(16) . . ?
Ni21 Ni19 Ni3 54.80(17) . . ?
S6 Ni20 S8 126.2(4) . . ?
S6 Ni20 S14 116.8(4) . . ?
S8 Ni20 S14 116.7(4) . . ?
S6 Ni20 Ni21 176.1(4) . . ?
S8 Ni20 Ni21 57.2(3) . . ?
S14 Ni20 Ni21 60.0(3) . . ?
S6 Ni20 Ni3 117.5(4) . . ?
S8 Ni20 Ni3 74.5(3) . . ?
S14 Ni20 Ni3 82.4(3) . . ?
Ni21 Ni20 Ni3 60.56(18) . . ?
S6 Ni20 Ni25 56.7(3) . . ?
S8 Ni20 Ni25 162.4(4) . . ?
S14 Ni20 Ni25 61.9(3) . . ?
Ni21 Ni20 Ni25 120.8(2) . . ?
Ni3 Ni20 Ni25 121.0(2) . . ?
S6 Ni20 Ni2 84.7(3) . . ?
S8 Ni20 Ni2 132.1(3) . . ?
S14 Ni20 Ni2 54.8(3) . . ?
Ni21 Ni20 Ni2 91.4(2) . . ?
Ni3 Ni20 Ni2 57.99(18) . . ?
Ni25 Ni20 Ni2 63.08(19) . . ?
S6 Ni20 Ni17 88.7(3) . . ?
S8 Ni20 Ni17 53.0(3) . . ?
S14 Ni20 Ni17 138.4(3) . . ?
Ni21 Ni20 Ni17 92.6(2) . . ?
Ni3 Ni20 Ni17 56.10(17) . . ?
Ni25 Ni20 Ni17 141.0(3) . . ?
Ni2 Ni20 Ni17 99.7(2) . . ?
S6 Ni20 Ni16 53.2(3) . . ?
S8 Ni20 Ni16 109.3(4) . . ?
S14 Ni20 Ni16 111.8(3) . . ?
Ni21 Ni20 Ni16 124.9(2) . . ?
Ni3 Ni20 Ni16 64.35(19) . . ?
Ni25 Ni20 Ni16 86.3(2) . . ?
Ni2 Ni20 Ni16 57.04(19) . . ?
Ni17 Ni20 Ni16 56.5(2) . . ?
S10 Ni21 S8 129.0(4) . . ?
S10 Ni21 S14 115.9(4) . . ?
S8 Ni21 S14 114.8(4) . . ?
S10 Ni21 Ni20 174.5(3) . . ?
S8 Ni21 Ni20 56.5(3) . . ?
S14 Ni21 Ni20 58.9(3) . . ?
S10 Ni21 Ni3 118.7(3) . . ?
S8 Ni21 Ni3 74.0(3) . . ?
S14 Ni21 Ni3 81.7(3) . . ?
Ni20 Ni21 Ni3 60.27(18) . . ?
S10 Ni21 Ni27 58.2(3) . . ?
S8 Ni21 Ni27 160.5(3) . . ?
S14 Ni21 Ni27 59.5(3) . . ?
Ni20 Ni21 Ni27 117.1(2) . . ?
Ni3 Ni21 Ni27 120.6(2) . . ?
S10 Ni21 Ni4 85.5(3) . . ?
S8 Ni21 Ni4 130.8(4) . . ?
S14 Ni21 Ni4 53.9(2) . . ?
Ni20 Ni21 Ni4 89.7(2) . . ?
Ni3 Ni21 Ni4 57.48(17) . . ?
Ni27 Ni21 Ni4 63.33(18) . . ?
S10 Ni21 Ni19 53.6(3) . . ?
S8 Ni21 Ni19 111.0(3) . . ?
S14 Ni21 Ni19 111.4(3) . . ?
Ni20 Ni21 Ni19 125.4(3) . . ?
Ni3 Ni21 Ni19 65.15(18) . . ?
Ni27 Ni21 Ni19 87.86(19) . . ?
Ni4 Ni21 Ni19 57.59(16) . . ?
S10 Ni21 Ni18 89.7(3) . . ?
S8 Ni21 Ni18 54.7(3) . . ?
S14 Ni21 Ni18 138.0(3) . . ?
Ni20 Ni21 Ni18 93.7(2) . . ?
Ni3 Ni21 Ni18 56.41(19) . . ?
Ni27 Ni21 Ni18 143.1(2) . . ?
Ni4 Ni21 Ni18 99.4(2) . . ?
Ni19 Ni21 Ni18 56.49(16) . . ?
S9 Ni22 S7 155.7(5) . . ?
S9 Ni22 P6 101.2(4) . . ?
S7 Ni22 P6 102.4(4) . . ?
S9 Ni22 Ni3 79.1(3) . . ?
S7 Ni22 Ni3 78.4(3) . . ?
P6 Ni22 Ni3 171.8(4) . . ?
S9 Ni22 Ni24 56.3(3) . . ?
S7 Ni22 Ni24 117.2(4) . . ?
P6 Ni22 Ni24 115.1(3) . . ?
Ni3 Ni22 Ni24 58.14(17) . . ?
S9 Ni22 Ni23 117.0(3) . . ?
S7 Ni22 Ni23 56.6(4) . . ?
P6 Ni22 Ni23 115.5(4) . . ?
Ni3 Ni22 Ni23 58.0(2) . . ?
Ni24 Ni22 Ni23 62.11(19) . . ?
S9 Ni22 Ni18 50.6(3) . . ?
S7 Ni22 Ni18 107.5(4) . . ?
P6 Ni22 Ni18 132.4(4) . . ?
Ni3 Ni22 Ni18 53.77(18) . . ?
Ni24 Ni22 Ni18 82.6(2) . . ?
Ni23 Ni22 Ni18 111.7(2) . . ?
S9 Ni22 Ni17 107.7(3) . . ?
S7 Ni22 Ni17 50.3(4) . . ?
P6 Ni22 Ni17 133.6(3) . . ?
Ni3 Ni22 Ni17 52.98(16) . . ?
Ni24 Ni22 Ni17 111.1(2) . . ?
Ni23 Ni22 Ni17 82.4(2) . . ?
Ni18 Ni22 Ni17 57.41(18) . . ?
S5 Ni23 S4 110.3(5) . . ?
S5 Ni23 S7 143.6(4) . . ?
S4 Ni23 S7 101.8(4) . . ?
S5 Ni23 Ni3 107.1(4) . . ?
S4 Ni23 Ni3 109.4(4) . . ?
S7 Ni23 Ni3 76.7(4) . . ?
S5 Ni23 Ni16 160.1(4) . . ?
S4 Ni23 Ni16 57.6(3) . . ?
S7 Ni23 Ni16 55.5(3) . . ?
Ni3 Ni23 Ni16 67.1(2) . . ?
S5 Ni23 Ni13 56.5(3) . . ?
S4 Ni23 Ni13 56.1(3) . . ?
S7 Ni23 Ni13 157.9(4) . . ?
Ni3 Ni23 Ni13 109.5(3) . . ?
Ni16 Ni23 Ni13 106.3(2) . . ?
S5 Ni23 Ni22 97.7(3) . . ?
S4 Ni23 Ni22 152.0(4) . . ?
S7 Ni23 Ni22 52.4(3) . . ?
Ni3 Ni23 Ni22 58.6(2) . . ?
Ni16 Ni23 Ni22 95.0(2) . . ?
Ni13 Ni23 Ni22 149.1(2) . . ?
S5 Ni23 Ni24 52.8(3) . . ?
S4 Ni23 Ni24 139.6(4) . . ?
S7 Ni23 Ni24 109.8(4) . . ?
Ni3 Ni23 Ni24 57.12(18) . . ?
Ni16 Ni23 Ni24 124.2(3) . . ?
Ni13 Ni23 Ni24 90.5(2) . . ?
Ni22 Ni23 Ni24 58.77(18) . . ?
S5 Ni23 Ni2 103.0(3) . . ?
S4 Ni23 Ni2 57.8(4) . . ?
S7 Ni23 Ni2 108.5(4) . . ?
Ni3 Ni23 Ni2 56.72(19) . . ?
Ni16 Ni23 Ni2 57.57(18) . . ?
Ni13 Ni23 Ni2 62.3(2) . . ?
Ni22 Ni23 Ni2 115.2(3) . . ?
Ni24 Ni23 Ni2 88.2(2) . . ?
S13 Ni24 S5 108.4(4) . . ?
S13 Ni24 S9 103.9(4) . . ?
S5 Ni24 S9 143.4(4) . . ?
S13 Ni24 Ni3 109.3(3) . . ?
S5 Ni24 Ni3 107.1(3) . . ?
S9 Ni24 Ni3 77.4(3) . . ?
S13 Ni24 Ni19 59.0(3) . . ?
S5 Ni24 Ni19 160.8(3) . . ?
S9 Ni24 Ni19 55.3(3) . . ?
Ni3 Ni24 Ni19 68.01(19) . . ?
S13 Ni24 Ni14 55.0(3) . . ?
S5 Ni24 Ni14 55.6(3) . . ?
S9 Ni24 Ni14 158.8(4) . . ?
Ni3 Ni24 Ni14 108.9(2) . . ?
Ni19 Ni24 Ni14 107.4(2) . . ?
S13 Ni24 Ni22 153.6(4) . . ?
S5 Ni24 Ni22 97.9(3) . . ?
S9 Ni24 Ni22 52.4(3) . . ?
Ni3 Ni24 Ni22 58.67(18) . . ?
Ni19 Ni24 Ni22 94.9(2) . . ?
Ni14 Ni24 Ni22 148.4(2) . . ?
S13 Ni24 Ni23 137.6(3) . . ?
S5 Ni24 Ni23 52.8(3) . . ?
S9 Ni24 Ni23 110.3(3) . . ?
Ni3 Ni24 Ni23 57.07(18) . . ?
Ni19 Ni24 Ni23 125.0(2) . . ?
Ni14 Ni24 Ni23 89.4(2) . . ?
Ni22 Ni24 Ni23 59.1(2) . . ?
S13 Ni24 Ni4 57.0(2) . . ?
S5 Ni24 Ni4 103.1(3) . . ?
S9 Ni24 Ni4 108.9(3) . . ?
Ni3 Ni24 Ni4 56.48(16) . . ?
Ni19 Ni24 Ni4 58.30(17) . . ?
Ni14 Ni24 Ni4 62.69(16) . . ?
Ni22 Ni24 Ni4 115.1(2) . . ?
Ni23 Ni24 Ni4 88.07(19) . . ?
P9 Ni25 S6 110.8(4) . . ?
P9 Ni25 S3 106.6(4) . . ?
S6 Ni25 S3 113.0(5) . . ?
P9 Ni25 Ni15 137.6(4) . . ?
S6 Ni25 Ni15 56.6(4) . . ?
S3 Ni25 Ni15 58.1(4) . . ?
P9 Ni25 Ni10 108.9(4) . . ?
S6 Ni25 Ni10 140.3(4) . . ?
S3 Ni25 Ni10 54.6(3) . . ?
Ni15 Ni25 Ni10 93.4(3) . . ?
P9 Ni25 Ni20 111.9(4) . . ?
S6 Ni25 Ni20 54.4(3) . . ?
S3 Ni25 Ni20 141.5(4) . . ?
Ni15 Ni25 Ni20 92.9(2) . . ?
Ni10 Ni25 Ni20 109.0(2) . . ?
P9 Ni25 S14 105.7(4) . . ?
S6 Ni25 S14 109.4(4) . . ?
S3 Ni25 S14 111.1(4) . . ?
Ni15 Ni25 S14 116.7(3) . . ?
Ni10 Ni25 S14 57.8(2) . . ?
Ni20 Ni25 S14 56.6(2) . . ?
P9 Ni25 Ni2 158.2(4) . . ?
S6 Ni25 Ni2 82.0(3) . . ?
S3 Ni25 Ni2 82.9(3) . . ?
Ni15 Ni25 Ni2 64.06(19) . . ?
Ni10 Ni25 Ni2 60.13(18) . . ?
Ni20 Ni25 Ni2 60.41(17) . . ?
S14 Ni25 Ni2 52.6(3) . . ?
P10 Ni27 S11 103.9(4) . . ?
P10 Ni27 S10 102.8(4) . . ?
S11 Ni27 S10 110.9(3) . . ?
P10 Ni27 S14 117.0(4) . . ?
S11 Ni27 S14 111.0(4) . . ?
S10 Ni27 S14 110.9(4) . . ?
P10 Ni27 Ni28 127.1(4) . . ?
S11 Ni27 Ni28 56.3(3) . . ?
S10 Ni27 Ni28 56.6(3) . . ?
S14 Ni27 Ni28 115.9(3) . . ?
P10 Ni27 Ni21 114.5(3) . . ?
S11 Ni27 Ni21 140.7(3) . . ?
S10 Ni27 Ni21 53.9(3) . . ?
S14 Ni27 Ni21 58.6(3) . . ?
Ni28 Ni27 Ni21 92.2(2) . . ?
P10 Ni27 Ni11 116.6(3) . . ?
S11 Ni27 Ni11 54.9(3) . . ?
S10 Ni27 Ni11 140.0(3) . . ?
S14 Ni27 Ni11 57.5(3) . . ?
Ni28 Ni27 Ni11 92.1(2) . . ?
Ni21 Ni27 Ni11 110.4(2) . . ?
P10 Ni27 Ni4 169.7(3) . . ?
S11 Ni27 Ni4 82.6(3) . . ?
S10 Ni27 Ni4 81.8(3) . . ?
S14 Ni27 Ni4 52.8(3) . . ?
Ni28 Ni27 Ni4 63.09(17) . . ?
Ni21 Ni27 Ni4 60.69(18) . . ?
Ni11 Ni27 Ni4 60.50(17) . . ?
P8 Ni28 S11 104.7(4) . . ?
P8 Ni28 S10 109.9(4) . . ?
S11 Ni28 S10 111.9(4) . . ?
P8 Ni28 S13 106.3(4) . . ?
S11 Ni28 S13 112.1(4) . . ?
S10 Ni28 S13 111.6(4) . . ?
P8 Ni28 Ni9 112.6(3) . . ?
S11 Ni28 Ni9 55.9(3) . . ?
S10 Ni28 Ni9 137.5(3) . . ?
S13 Ni28 Ni9 56.6(3) . . ?
P8 Ni28 Ni27 135.4(3) . . ?
S11 Ni28 Ni27 56.7(2) . . ?
S10 Ni28 Ni27 57.2(3) . . ?
S13 Ni28 Ni27 118.3(3) . . ?
Ni9 Ni28 Ni27 90.6(2) . . ?
P8 Ni28 Ni19 117.1(3) . . ?
S11 Ni28 Ni19 138.2(3) . . ?
S10 Ni28 Ni19 54.7(3) . . ?
S13 Ni28 Ni19 57.4(3) . . ?
Ni9 Ni28 Ni19 104.5(2) . . ?
Ni27 Ni28 Ni19 90.9(2) . . ?
P8 Ni28 Ni4 162.3(3) . . ?
S11 Ni28 Ni4 82.2(3) . . ?
S10 Ni28 Ni4 81.5(3) . . ?
S13 Ni28 Ni4 56.2(2) . . ?
Ni9 Ni28 Ni4 57.51(16) . . ?
Ni27 Ni28 Ni4 62.07(17) . . ?
Ni19 Ni28 Ni4 57.86(17) . . ?
C3 P1 C5 103.0(6) . . ?
C3 P1 C1 102.8(6) . . ?
C5 P1 C1 102.4(6) . . ?
C3 P1 Ni7 116.0(6) . . ?
C5 P1 Ni7 115.6(5) . . ?
C1 P1 Ni7 115.2(5) . . ?
C11 P2 C9 103.8(6) . . ?
C11 P2 C7 102.9(6) . . ?
C9 P2 C7 102.7(6) . . ?
C11 P2 Ni6 115.9(5) . . ?
C9 P2 Ni6 115.3(5) . . ?
C7 P2 Ni6 114.5(5) . . ?
C13 P3 C15 103.8(6) . . ?
C13 P3 C17 103.5(6) . . ?
C15 P3 C17 103.6(6) . . ?
C13 P3 Ni17 115.0(5) . . ?
C15 P3 Ni17 114.8(5) . . ?
C17 P3 Ni17 114.8(5) . . ?
C21 P4 C23 103.4(6) . . ?
C21 P4 C19 103.1(6) . . ?
C23 P4 C19 102.5(6) . . ?
C21 P4 Ni18 115.8(5) . . ?
C23 P4 Ni18 115.4(6) . . ?
C19 P4 Ni18 114.8(5) . . ?
C29 P5 C25 103.2(6) . . ?
C29 P5 C27 102.8(6) . . ?
C25 P5 C27 102.9(6) . . ?
C29 P5 Ni12 115.6(5) . . ?
C25 P5 Ni12 115.6(5) . . ?
C27 P5 Ni12 114.9(5) . . ?
C33 P6 C31 103.0(6) . . ?
C33 P6 C35 102.5(6) . . ?
C31 P6 C35 102.5(6) . . ?
C33 P6 Ni22 116.0(5) . . ?
C31 P6 Ni22 115.8(5) . . ?
C35 P6 Ni22 115.1(5) . . ?
C41 P7 C39 103.0(6) . . ?
C41 P7 C37 102.7(6) . . ?
C39 P7 C37 102.8(6) . . ?
C41 P7 Ni15 115.7(6) . . ?
C39 P7 Ni15 115.3(5) . . ?
C37 P7 Ni15 115.4(6) . . ?
C43 P8 C47 103.3(6) . . ?
C43 P8 C45 102.9(6) . . ?
C47 P8 C45 103.0(6) . . ?
C43 P8 Ni28 115.5(5) . . ?
C47 P8 Ni28 115.3(5) . . ?
C45 P8 Ni28 115.0(5) . . ?
C51 P9 C49 103.0(6) . . ?
C51 P9 C53 103.1(6) . . ?
C49 P9 C53 102.6(6) . . ?
C51 P9 Ni25 115.9(6) . . ?
C49 P9 Ni25 115.4(5) . . ?
C53 P9 Ni25 115.1(5) . . ?
C55 P10 C57 103.7(6) . . ?
C55 P10 C59 102.8(6) . . ?
C57 P10 C59 102.8(6) . . ?
C55 P10 Ni27 115.9(5) . . ?
C57 P10 Ni27 115.6(6) . . ?
C59 P10 Ni27 114.3(5) . . ?
Ni11 S1 Ni6 73.2(3) . . ?
Ni11 S1 Ni10 67.2(3) . . ?
Ni6 S1 Ni10 112.2(5) . . ?
Ni11 S1 Ni7 112.2(5) . . ?
Ni6 S1 Ni7 75.5(4) . . ?
Ni10 S1 Ni7 71.8(4) . . ?
Ni12 S2 Ni8 114.2(5) . . ?
Ni12 S2 Ni7 79.0(4) . . ?
Ni8 S2 Ni7 66.9(4) . . ?
Ni12 S2 Ni13 70.1(3) . . ?
Ni8 S2 Ni13 66.2(4) . . ?
Ni7 S2 Ni13 103.7(5) . . ?
Ni10 S3 Ni8 72.5(3) . . ?
Ni10 S3 Ni25 68.3(4) . . ?
Ni8 S3 Ni25 102.9(4) . . ?
Ni10 S3 Ni15 106.8(4) . . ?
Ni8 S3 Ni15 67.2(4) . . ?
Ni25 S3 Ni15 65.0(4) . . ?
Ni13 S4 Ni23 67.6(3) . . ?
Ni13 S4 Ni16 123.0(5) . . ?
Ni23 S4 Ni16 66.2(4) . . ?
Ni13 S4 Ni8 66.1(4) . . ?
Ni23 S4 Ni8 123.0(5) . . ?
Ni16 S4 Ni8 117.1(6) . . ?
Ni13 S4 Ni15 127.6(6) . . ?
Ni23 S4 Ni15 127.5(6) . . ?
Ni16 S4 Ni15 65.6(4) . . ?
Ni8 S4 Ni15 65.8(4) . . ?
Ni13 S4 Ni2 70.7(4) . . ?
Ni23 S4 Ni2 71.2(4) . . ?
Ni16 S4 Ni2 64.3(4) . . ?
Ni8 S4 Ni2 63.5(4) . . ?
Ni15 S4 Ni2 70.3(4) . . ?
Ni14 S5 Ni23 110.7(5) . . ?
Ni14 S5 Ni24 68.4(4) . . ?
Ni23 S5 Ni24 74.4(4) . . ?
Ni14 S5 Ni13 74.1(3) . . ?
Ni23 S5 Ni13 68.1(3) . . ?
Ni24 S5 Ni13 111.2(5) . . ?
Ni20 S6 Ni16 73.8(3) . . ?
Ni20 S6 Ni15 108.7(4) . . ?
Ni16 S6 Ni15 68.1(4) . . ?
Ni20 S6 Ni25 68.9(3) . . ?
Ni16 S6 Ni25 104.7(4) . . ?
Ni15 S6 Ni25 66.0(4) . . ?
Ni22 S7 Ni16 116.5(5) . . ?
Ni22 S7 Ni17 81.2(5) . . ?
Ni16 S7 Ni17 68.2(4) . . ?
Ni22 S7 Ni23 71.0(4) . . ?
Ni16 S7 Ni23 66.4(4) . . ?
Ni17 S7 Ni23 105.8(5) . . ?
Ni17 S8 Ni20 73.2(4) . . ?
Ni17 S8 Ni21 111.7(5) . . ?
Ni20 S8 Ni21 66.4(3) . . ?
Ni17 S8 Ni18 75.5(4) . . ?
Ni20 S8 Ni18 111.3(4) . . ?
Ni21 S8 Ni18 71.4(3) . . ?
Ni22 S9 Ni19 117.1(4) . . ?
Ni22 S9 Ni18 80.6(3) . . ?
Ni19 S9 Ni18 68.6(3) . . ?
Ni22 S9 Ni24 71.4(4) . . ?
Ni19 S9 Ni24 66.9(3) . . ?
Ni18 S9 Ni24 105.9(4) . . ?
Ni21 S10 Ni19 73.7(4) . . ?
Ni21 S10 Ni28 107.7(4) . . ?
Ni19 S10 Ni28 67.9(3) . . ?
Ni21 S10 Ni27 67.9(3) . . ?
Ni19 S10 Ni27 104.6(4) . . ?
Ni28 S10 Ni27 66.2(3) . . ?
Ni11 S11 Ni9 72.0(3) . . ?
Ni11 S11 Ni28 107.4(4) . . ?
Ni9 S11 Ni28 67.4(3) . . ?
Ni11 S11 Ni27 68.1(3) . . ?
Ni9 S11 Ni27 103.9(4) . . ?
Ni28 S11 Ni27 66.9(3) . . ?
Ni12 S12 Ni9 116.1(4) . . ?
Ni12 S12 Ni6 80.2(3) . . ?
Ni9 S12 Ni6 67.5(3) . . ?
Ni12 S12 Ni14 71.3(3) . . ?
Ni9 S12 Ni14 67.1(3) . . ?
Ni6 S12 Ni14 105.6(4) . . ?
Ni14 S13 Ni24 68.7(3) . . ?
Ni14 S13 Ni9 67.8(3) . . ?
Ni24 S13 Ni9 125.7(4) . . ?
Ni14 S13 Ni28 129.5(4) . . ?
Ni24 S13 Ni28 127.8(4) . . ?
Ni9 S13 Ni28 65.9(3) . . ?
Ni14 S13 Ni19 124.9(4) . . ?
Ni24 S13 Ni19 66.0(3) . . ?
Ni9 S13 Ni19 118.7(4) . . ?
Ni28 S13 Ni19 65.7(3) . . ?
Ni14 S13 Ni4 72.5(3) . . ?
Ni24 S13 Ni4 72.2(3) . . ?
Ni9 S13 Ni4 65.1(2) . . ?
Ni28 S13 Ni4 70.7(3) . . ?
Ni19 S13 Ni4 65.1(3) . . ?
Ni4 S14 Ni2 65.5(3) . . ?
Ni4 S14 Ni11 68.3(3) . . ?
Ni2 S14 Ni11 99.3(4) . . ?
Ni4 S14 Ni20 99.7(4) . . ?
Ni2 S14 Ni20 67.8(3) . . ?
Ni11 S14 Ni20 165.7(5) . . ?
Ni4 S14 Ni21 67.7(3) . . ?
Ni2 S14 Ni21 100.1(4) . . ?
Ni11 S14 Ni21 117.7(4) . . ?
Ni20 S14 Ni21 61.1(3) . . ?
Ni4 S14 Ni10 99.8(4) . . ?
Ni2 S14 Ni10 66.5(3) . . ?
Ni11 S14 Ni10 61.2(3) . . ?
Ni20 S14 Ni10 115.8(4) . . ?
Ni21 S14 Ni10 165.2(5) . . ?
Ni4 S14 Ni27 69.2(3) . . ?
Ni2 S14 Ni27 134.7(4) . . ?
Ni11 S14 Ni27 62.6(3) . . ?
Ni20 S14 Ni27 121.6(4) . . ?
Ni21 S14 Ni27 61.9(3) . . ?
Ni10 S14 Ni27 122.5(4) . . ?
Ni4 S14 Ni25 132.9(5) . . ?
Ni2 S14 Ni25 67.4(3) . . ?
Ni11 S14 Ni25 120.5(4) . . ?
Ni20 S14 Ni25 61.6(3) . . ?
Ni21 S14 Ni25 121.6(4) . . ?
Ni10 S14 Ni25 60.5(3) . . ?
Ni27 S14 Ni25 157.9(5) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C61 C62 C63 C64 164(14) . . . . ?
C62 C63 C64 C65 -165(14) . . . . ?
C4 C3 P1 C5 175(4) . . . . ?
C4 C3 P1 C1 69(4) . . . . ?
C4 C3 P1 Ni7 -58(4) . . . . ?
C6 C5 P1 C3 98(4) . . . . ?
C6 C5 P1 C1 -156(4) . . . . ?
C6 C5 P1 Ni7 -30(4) . . . . ?
C2 C1 P1 C3 60(4) . . . . ?
C2 C1 P1 C5 -47(4) . . . . ?
C2 C1 P1 Ni7 -173(4) . . . . ?
C12 C11 P2 C9 -41(3) . . . . ?
C12 C11 P2 C7 -148(3) . . . . ?
C12 C11 P2 Ni6 86(3) . . . . ?
C10 C9 P2 C11 -171(4) . . . . ?
C10 C9 P2 C7 -64(4) . . . . ?
C10 C9 P2 Ni6 61(4) . . . . ?
C8 C7 P2 C11 65(4) . . . . ?
C8 C7 P2 C9 -43(4) . . . . ?
C8 C7 P2 Ni6 -169(4) . . . . ?
C14 C13 P3 C15 -62(4) . . . . ?
C14 C13 P3 C17 -170(3) . . . . ?
C14 C13 P3 Ni17 64(3) . . . . ?
C16 C15 P3 C13 -53(4) . . . . ?
C16 C15 P3 C17 55(4) . . . . ?
C16 C15 P3 Ni17 -179(4) . . . . ?
C18 C17 P3 C13 174(4) . . . . ?
C18 C17 P3 C15 66(4) . . . . ?
C18 C17 P3 Ni17 -60(4) . . . . ?
C22 C21 P4 C23 -169(4) . . . . ?
C22 C21 P4 C19 85(4) . . . . ?
C22 C21 P4 Ni18 -41(4) . . . . ?
C24 C23 P4 C21 46(4) . . . . ?
C24 C23 P4 C19 153(3) . . . . ?
C24 C23 P4 Ni18 -81(3) . . . . ?
C20 C19 P4 C21 53(4) . . . . ?
C20 C19 P4 C23 -54(4) . . . . ?
C20 C19 P4 Ni18 180(4) . . . . ?
C30 C29 P5 C25 -64(4) . . . . ?
C30 C29 P5 C27 -171(3) . . . . ?
C30 C29 P5 Ni12 63(4) . . . . ?
C26 C25 P5 C29 -46(4) . . . . ?
C26 C25 P5 C27 61(4) . . . . ?
C26 C25 P5 Ni12 -173(4) . . . . ?
C28 C27 P5 C29 -179(4) . . . . ?
C28 C27 P5 C25 74(4) . . . . ?
C28 C27 P5 Ni12 -52(4) . . . . ?
C34 C33 P6 C31 -62(3) . . . . ?
C34 C33 P6 C35 -168(3) . . . . ?
C34 C33 P6 Ni22 65(3) . . . . ?
C32 C31 P6 C33 40(3) . . . . ?
C32 C31 P6 C35 146(3) . . . . ?
C32 C31 P6 Ni22 -88(3) . . . . ?
C36 C35 P6 C33 157(3) . . . . ?
C36 C35 P6 C31 50(3) . . . . ?
C36 C35 P6 Ni22 -76(3) . . . . ?
C42 C41 P7 C39 68(4) . . . . ?
C42 C41 P7 C37 175(4) . . . . ?
C42 C41 P7 Ni15 -59(4) . . . . ?
C40 C39 P7 C41 46(4) . . . . ?
C40 C39 P7 C37 -61(4) . . . . ?
C40 C39 P7 Ni15 173(4) . . . . ?
C38 C37 P7 C41 -171(4) . . . . ?
C38 C37 P7 C39 -65(4) . . . . ?
C38 C37 P7 Ni15 62(4) . . . . ?
C44 C43 P8 C47 75(4) . . . . ?
C44 C43 P8 C45 -178(4) . . . . ?
C44 C43 P8 Ni28 -52(4) . . . . ?
C48 C47 P8 C43 -175(4) . . . . ?
C48 C47 P8 C45 78(4) . . . . ?
C48 C47 P8 Ni28 -48(4) . . . . ?
C46 C45 P8 C43 -48(4) . . . . ?
C46 C45 P8 C47 59(4) . . . . ?
C46 C45 P8 Ni28 -174(4) . . . . ?
C52 C51 P9 C49 -37(3) . . . . ?
C52 C51 P9 C53 -143(3) . . . . ?
C52 C51 P9 Ni25 90(3) . . . . ?
C50 C49 P9 C51 148(4) . . . . ?
C50 C49 P9 C53 -105(4) . . . . ?
C50 C49 P9 Ni25 21(4) . . . . ?
C54 C53 P9 C51 -24(3) . . . . ?
C54 C53 P9 C49 -131(3) . . . . ?
C54 C53 P9 Ni25 103(3) . . . . ?
C56 C55 P10 C57 -79(4) . . . . ?
C56 C55 P10 C59 174(4) . . . . ?
C56 C55 P10 Ni27 49(4) . . . . ?
C58 C57 P10 C55 -163(4) . . . . ?
C58 C57 P10 C59 -56(4) . . . . ?
C58 C57 P10 Ni27 69(4) . . . . ?
C60 C59 P10 C55 64(4) . . . . ?
C60 C59 P10 C57 -43(4) . . . . ?
C60 C59 P10 Ni27 -169(4) . . . . ?

_refine_diff_density_max         1.270
_refine_diff_density_min         -1.092
_refine_diff_density_rms         0.211



###END###

# start Validation Reply Form
_vrf_PLAT308_Complex_1           
;
PROBLEM: Single Bonded Metal Atom in Structure (Unusual) Ni1 Check
RESPONSE: This alert is an artefact of the checkcif software. Ni1, Ni3, and Ni5 are bound to 11 other Ni atoms. Ni2 and Ni4 are abound to 11 Ni atoms. It is not an isolated atom. 
;
_vrf_PLAT230_Complex_1           
;
PROBLEM: Hirshfeld Test Diff for P1 --C1 . 12.4 s.u.
RESPONSE: This alert is due to the unresolved positional disorder of the ethyl carbons of the triethylphosphine ligands.
;
_vrf_PLAT341_Complex_1           
;
PROBLEM: Low Bond Precision on C-C Bonds ............... 0.03571 Ang.
RESPONSE: This alert is due to the unresolved positional disorder of the ethyl carbons of the triethylphosphine ligands.
;
_vrf_PLAT601_Complex_1           
;
PROBLEM: Unit Cell Contains Solvent Accessible VOIDS of . 102 Ang**3
RESPONSE: There may be other disordered diethyl ether solvent molecules in the cell, but attempts to model 
;
_vrf_RINTA01_Complex_2           
;
PROBLEM: The value of Rint is greater than 0.25 Rint given 0.270
RESPONSE: Crystals of complex 2 were all highly twinned, limiting the resolution of the data. 
;
_vrf_PLAT020_Complex_2           
;
PROBLEM: The Value of Rint is Greater Than 0.12 ......... 0.270 Report
RESPONSE: Crystals of complex 2 were all highly twinned, limiting the resolution of the data.
;
_vrf_PLAT026_Complex_2           
;
PROBLEM: Ratio Observed / Unique Reflections (too) Low .. 23% Check
RESPONSE: Crystals of complex 2 were all highly twinned, limiting the resolution of the data.
;
_vrf_PLAT201_Complex_2           
;
PROBLEM: Isotropic non-H Atoms in Main Residue(s) ....... C1 C2 C3 C4 C5 etc. 60 Report
RESPONSE: Twinning of the crystals of complex 2 as well as unresolved positional disorder on the carbon atoms of the triethylphosphine ligands precluded anisotropic refinement of the triethylphosphine carbon atoms
;
_vrf_PLAT308_Complex_2           
;
PROBLEM: Single Bonded Metal Atom in Structure (Unusual) Ni1 Check
RESPONSE: This alert is an artefact of the checkcif software. Ni1, Ni2, Ni3, and Ni4 are each bound to 11 other Ni atoms. It is not an isolated atom.
;
_vrf_PLAT084_Complex_2           
;
PROBLEM: High wR2 Value (i.e. > 0.25) ................... 0.39 Report
RESPONSE: Crystals of complex 2 were all highly twinned, limiting the resolution of the data.
;
_vrf_PLAT242_Complex_2           
;
PROBLEM: Low ?MainMol? Ueq as Compared to Neighbors of P2 Check
RESPONSE: Unresolved twinning of the crystals of complex 2 limited the resolution of the data and hampered the refinement of the phosphorous atoms.
;
_vrf_PLAT315_Complex_2           
;
PROBLEM: Singly Bonded Carbon Detected (H-atoms Missing). C61 Check
RESPONSE: Unresolved twinning of the crystals of complex 2 limited the resolution of the data and hampered the refinement of the phosphorous atoms.
;
_vrf_PLAT341_Complex_2           
;
PROBLEM: Low Bond Precision on C-C Bonds ............... 0.05529 Ang.
RESPONSE: Twinning of the crystals of complex 2 as well as unresolved positional disorder on the carbon atoms of the triethylphosphine ligands precluded anisotropic refinement of the triethylphosphine carbon atoms
;
# end Validation Reply Form
