# Electronic Supplementary Material (ESI) for CrystEngComm.
# This journal is © The Royal Society of Chemistry 2023

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
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data_aaa_a
_database_code_depnum_ccdc_archive 'CCDC 2278716'
loop_
_audit_author_name
_audit_author_address
JIANG
;zhejiang normal university
China
;
_audit_update_record             
;
2023-07-03 deposited with the CCDC.	2023-08-28 downloaded from the CCDC.
;
_audit_creation_date             2023-06-07
_audit_creation_method           
;
Olex2 1.5
(compiled 2021.08.20 svn.r13c46975 for OlexSys, GUI svn.r6392)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'Ag45 Br6 C192, 4(F6 Sb)'
_chemical_formula_sum            'C192 Ag45 Br6 F24 Sb4'
_chemical_formula_weight         8582.53
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Br Br -0.2901 2.4595 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   18.711(5)
_cell_length_b                   20.882(6)
_cell_length_c                   21.381(6)
_cell_angle_alpha                110.987(9)
_cell_angle_beta                 114.356(9)
_cell_angle_gamma                99.657(9)
_cell_volume                     6599(3)
_cell_formula_units_Z            1
_cell_measurement_reflns_used    2707
_cell_measurement_temperature    273.15
_cell_measurement_theta_max      15.98
_cell_measurement_theta_min      2.40
_shelx_estimated_absorpt_T_max   0.631
_shelx_estimated_absorpt_T_min   0.586
_exptl_absorpt_coefficient_mu    4.609
_exptl_absorpt_correction_T_max  0.7441
_exptl_absorpt_correction_T_min  0.5679
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
SADABS-2016/2 (Bruker,2016/2) was used for absorption correction.
wR2(int) was 0.1046 before and 0.0799 after correction.
The Ratio of minimum to maximum transmission is 0.7632.
The λ/2 correction factor is Not present.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            yellow
_exptl_crystal_colour_primary    yellow
_exptl_crystal_density_diffrn    2.160
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             3897
_exptl_crystal_size_max          0.13
_exptl_crystal_size_mid          0.12
_exptl_crystal_size_min          0.11
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0954
_diffrn_reflns_av_unetI/netI     0.1117
_diffrn_reflns_Laue_measured_fraction_full 0.994
_diffrn_reflns_Laue_measured_fraction_max 0.994
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       -14
_diffrn_reflns_number            19809
_diffrn_reflns_point_group_measured_fraction_full 0.994
_diffrn_reflns_point_group_measured_fraction_max 0.994
_diffrn_reflns_theta_full        15.990
_diffrn_reflns_theta_max         15.990
_diffrn_reflns_theta_min         2.212
_diffrn_ambient_temperature      273.15
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.994
_diffrn_measured_fraction_theta_max 0.994
_diffrn_measurement_device_type  'BRUKER D8 VENTURE'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_diffrn_source_current           1.4
_diffrn_source_power             0.07
_diffrn_source_voltage           50.0
_diffrn_standards_number         0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                3739
_reflns_number_total             6412
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT V8.38A (Bruker, 2018)'
_computing_data_collection       ?
_computing_data_reduction        'SAINT V8.38A (Bruker, 2018)'
_computing_molecular_graphics    'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2018/3 (Sheldrick, 2015)'
_computing_structure_solution    'SHELXT 2014/5 (Sheldrick, 2014)'
_refine_diff_density_max         2.217
_refine_diff_density_min         -1.127
_refine_diff_density_rms         0.217
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.432
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1222
_refine_ls_number_reflns         6412
_refine_ls_number_restraints     2663
_refine_ls_R_factor_all          0.1824
_refine_ls_R_factor_gt           0.1302
_refine_ls_restrained_S_all      1.186
_refine_ls_shift/su_max          0.058
_refine_ls_shift/su_mean         0.012
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.2000P)²] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.3554
_refine_ls_wR_factor_ref         0.4020
_refine_special_details          ?
_olex2_refinement_description    
;
1. Restrained distances
 Sb2-F3 = Sb2-F4 = Sb2-F6 = Sb2-F8
 1.88 with sigma of 0.02
 Sb2-F5 = Sb2-F7
 1.87 with sigma of 0.02
 Sb1-F1 = Sb1-F2 = Sb1-F10 = Sb1-F12
 1.88 with sigma of 0.02
 Sb1-F9 = Sb1-F11
 1.87 with sigma of 0.02
 C16-C18 = C18-C20
 1.54 with sigma of 0.02
 C36-C38 = C38-C40
 1.54 with sigma of 0.02
 C18-C22 = C18-C24
 1.55 with sigma of 0.02
 C26-C28 = C28-C30
 1.54 with sigma of 0.02
 C28-C32 = C28-C34
 1.55 with sigma of 0.02
 C38-C42 = C38-C44
 1.55 with sigma of 0.02
 C56-C58 = C58-C60
 1.54 with sigma of 0.02
 C66-C68 = C68-C70
 1.54 with sigma of 0.02
 C58-C62 = C58-C64
 1.55 with sigma of 0.02
 C48-C52 = C48-C54
 1.55 with sigma of 0.02
 C46-C48 = C48-C50
 1.54 with sigma of 0.02
 C68-C72 = C68-C74
 1.55 with sigma of 0.02
 C90-C94 = C90-C96
 1.55 with sigma of 0.02
 C88-C90 = C90-C92
 1.54 with sigma of 0.02
 C17-C69 = C69-C35
 1.54 with sigma of 0.02
 C3-C49 = C49-C25
 1.54 with sigma of 0.02
 C49-C51 = C49-C13
 1.55 with sigma of 0.02
 C69-C71 = C69-C9
 1.55 with sigma of 0.02
 C53-C27 = C27-C55
 1.54 with sigma of 0.02
 C27-C7 = C27-C57
 1.55 with sigma of 0.02
 C29-C59 = C59-C15
 1.54 with sigma of 0.02
 C59-C61 = C59-C31
 1.55 with sigma of 0.02
 C63-C2 = C2-C65
 1.54 with sigma of 0.02
 C2-C33 = C2-C67
 1.55 with sigma of 0.02
 C37-C19 = C37-C77
 1.55 with sigma of 0.02
 C73-C37 = C37-C75
 1.54 with sigma of 0.02
 C5-C81 = C81-C41
 1.54 with sigma of 0.02
 C81-C83 = C81-C21
 1.55 with sigma of 0.02
 C43-C87 = C87-C11
 1.54 with sigma of 0.02
 C87-C89 = C87-C45
 1.55 with sigma of 0.02
 C91-C23 = C23-C93
 1.54 with sigma of 0.02
 C23-C47 = C23-C95
 1.55 with sigma of 0.02
 C85-C93
 1.2 with sigma of 0.02
 C26-C32 = C26-C34
 2.52 with sigma of 0.04
 C16-C20
 2.56 with sigma of 0.04
 C16-C22 = C16-C24
 2.52 with sigma of 0.04
 C26-C30
 2.56 with sigma of 0.04
 C36-C40
 2.56 with sigma of 0.04
 C36-C42 = C36-C44
 2.52 with sigma of 0.04
 C46-C50
 2.56 with sigma of 0.04
 C56-C60
 2.56 with sigma of 0.04
 C46-C52 = C46-C54
 2.52 with sigma of 0.04
 C66-C70
 2.56 with sigma of 0.04
 C66-C72 = C66-C74
 2.52 with sigma of 0.04
 C56-C62 = C56-C64
 2.52 with sigma of 0.04
 C88-C92
 2.56 with sigma of 0.04
 C88-C94 = C88-C96
 2.52 with sigma of 0.04
 C29-C15
 2.56 with sigma of 0.04
 C17-C35
 2.56 with sigma of 0.04
 C3-C25
 2.56 with sigma of 0.04
 C53-C55
 2.56 with sigma of 0.04
 C63-C65
 2.56 with sigma of 0.04
 C3-C51 = C3-C13
 2.52 with sigma of 0.04
 C53-C7 = C53-C57
 2.52 with sigma of 0.04
 C29-C61 = C29-C31
 2.52 with sigma of 0.04
 C63-C33 = C63-C67
 2.52 with sigma of 0.04
 C17-C71 = C17-C9
 2.52 with sigma of 0.04
 C73-C75
 2.56 with sigma of 0.04
 C73-C19 = C73-C77
 2.52 with sigma of 0.04
 C5-C41
 2.56 with sigma of 0.04
 C5-C83 = C5-C21
 2.52 with sigma of 0.04
 C43-C89 = C43-C45
 2.52 with sigma of 0.04
 C43-C11
 2.56 with sigma of 0.04
 C91-C93
 2.56 with sigma of 0.04
 C91-C47 = C91-C95
 2.52 with sigma of 0.04
 Sb1-F1 \\sim Sb1-F2 \\sim Sb1-F9 \\sim Sb1-F10 \\sim Sb1-F11 \\sim Sb1-F12
 with sigma of 0.02
 F1-F2 \\sim F1-F9 \\sim F1-F10 \\sim F1-F11 \\sim F2-F9 \\sim F2-F11 \\sim
F2-F12 \\sim F9-F10 \\sim F9-F12 ~
 F10-F11 \\sim F10-F12 \\sim F11-F12
 with sigma of 0.04
 Sb2-F3 \\sim Sb2-F4 \\sim Sb2-F5 \\sim Sb2-F6 \\sim Sb2-F7 \\sim Sb2-F8
 with sigma of 0.02
 F3-F4 \\sim F3-F5 \\sim F3-F6 \\sim F3-F7 \\sim F4-F5 \\sim F4-F7 \\sim F4-F8
\\sim F5-F6 \\sim F5-F8 \\sim F6-F7
 \\sim F6-F8 \\sim F7-F8
 with sigma of 0.04
 C36-C40 \\sim C36-C42 \\sim C36-C44
 with sigma of 0.04
 C38-C40 \\sim C38-C42 \\sim C38-C44 \\sim C38-C36
 with sigma of 0.02
 C40-C42 \\sim C40-C44 \\sim C42-C44
 with sigma of 0.04
 C18-C20 \\sim C18-C22 \\sim C18-C24 \\sim C18-C16
 with sigma of 0.02
 C20-C22 \\sim C20-C24 \\sim C22-C24
 with sigma of 0.04
 C16-C20 \\sim C16-C22 \\sim C16-C24
 with sigma of 0.04
 C28-C30 \\sim C28-C32 \\sim C28-C34 \\sim C28-C26
 with sigma of 0.02
 C30-C32 \\sim C30-C34 \\sim C32-C34
 with sigma of 0.04
 C26-C30 \\sim C26-C32 \\sim C26-C34
 with sigma of 0.04
 C56-C60 \\sim C56-C62 \\sim C56-C64
 with sigma of 0.04
 C48-C50 \\sim C48-C52 \\sim C48-C54 \\sim C48-C46
 with sigma of 0.02
 C60-C62 \\sim C60-C64 \\sim C62-C64
 with sigma of 0.04
 C68-C70 \\sim C68-C72 \\sim C68-C74 \\sim C68-C66
 with sigma of 0.02
 C70-C72 \\sim C70-C74 \\sim C72-C74
 with sigma of 0.04
 C66-C70 \\sim C66-C72 \\sim C66-C74
 with sigma of 0.04
 C50-C52 \\sim C50-C54 \\sim C52-C54
 with sigma of 0.04
 C46-C50 \\sim C46-C52 \\sim C46-C54
 with sigma of 0.04
 C58-C60 \\sim C58-C62 \\sim C58-C64 \\sim C58-C56
 with sigma of 0.02
 C88-C92 \\sim C88-C94 \\sim C88-C96
 with sigma of 0.04
 C90-C92 \\sim C90-C94 \\sim C90-C96 \\sim C90-C88
 with sigma of 0.02
 C92-C94 \\sim C92-C96 \\sim C94-C96
 with sigma of 0.04
 C59-C15 \\sim C59-C61 \\sim C59-C31 \\sim C59-C29
 with sigma of 0.02
 C29-C15 \\sim C29-C61 \\sim C29-C31
 with sigma of 0.04
 C15-C61 \\sim C15-C31 \\sim C61-C31
 with sigma of 0.04
 C2-C65 \\sim C2-C33 \\sim C2-C67 \\sim C2-C63
 with sigma of 0.02
 C17-C35 \\sim C17-C71 \\sim C17-C9
 with sigma of 0.04
 C65-C33 \\sim C65-C67 \\sim C33-C67
 with sigma of 0.04
 C63-C65 \\sim C63-C33 \\sim C63-C67
 with sigma of 0.04
 C69-C35 \\sim C69-C71 \\sim C69-C9 \\sim C69-C17
 with sigma of 0.02
 C35-C71 \\sim C35-C9 \\sim C71-C9
 with sigma of 0.04
 C49-C25 \\sim C49-C51 \\sim C49-C13 \\sim C49-C3
 with sigma of 0.02
 C25-C51 \\sim C25-C13 \\sim C51-C13
 with sigma of 0.04
 C3-C25 \\sim C3-C51 \\sim C3-C13
 with sigma of 0.04
 C27-C55 \\sim C27-C7 \\sim C27-C57 \\sim C27-C53
 with sigma of 0.02
 C55-C7 \\sim C55-C57 \\sim C7-C57
 with sigma of 0.04
 C53-C55 \\sim C53-C7 \\sim C53-C57
 with sigma of 0.04
 C75-C19 \\sim C75-C77 \\sim C19-C77
 with sigma of 0.04
 C37-C75 \\sim C37-C19 \\sim C37-C77 \\sim C37-C73
 with sigma of 0.02
 C73-C75 \\sim C73-C19 \\sim C73-C77
 with sigma of 0.04
 C41-C83 \\sim C41-C21 \\sim C83-C21
 with sigma of 0.04
 C81-C41 \\sim C81-C83 \\sim C81-C21 \\sim C81-C5
 with sigma of 0.02
 C5-C41 \\sim C5-C83 \\sim C5-C21
 with sigma of 0.04
 C43-C11 \\sim C43-C89 \\sim C43-C45
 with sigma of 0.04
 C11-C89 \\sim C11-C45 \\sim C89-C45
 with sigma of 0.04
 C87-C11 \\sim C87-C89 \\sim C87-C45 \\sim C87-C43
 with sigma of 0.02
 C91-C93 \\sim C91-C47 \\sim C91-C95
 with sigma of 0.04
 C93-C47 \\sim C93-C95 \\sim C47-C95
 with sigma of 0.04
 C23-C93 \\sim C23-C47 \\sim C23-C95 \\sim C23-C91
 with sigma of 0.02
2. Uiso/Uaniso restraints and constraints
Sb2 \\sim F3 \\sim F4 \\sim F5 \\sim F6 \\sim F7 \\sim F8: within 2A with sigma
of 0.04 and sigma for terminal atoms of 0.08 within 2A
Sb1 \\sim F1 \\sim F2 \\sim F9 \\sim F10 \\sim F11 \\sim F12: within 2A with
sigma of 0.04 and sigma for terminal atoms of 0.08 within 2A
C26 \\sim C28 \\sim C30 \\sim C32 \\sim C34: within 2A with sigma of 0.04 and
sigma for terminal atoms of 0.08 within 2A
C16 \\sim C18 \\sim C20 \\sim C22 \\sim C24: within 2A with sigma of 0.04 and
sigma for terminal atoms of 0.08 within 2A
C36 \\sim C38 \\sim C40 \\sim C42 \\sim C44: within 2A with sigma of 0.04 and
sigma for terminal atoms of 0.08 within 2A
C56 \\sim C58 \\sim C60 \\sim C62 \\sim C64: within 2A with sigma of 0.04 and
sigma for terminal atoms of 0.08 within 2A
C46 \\sim C48 \\sim C50 \\sim C52 \\sim C54: within 2A with sigma of 0.04 and
sigma for terminal atoms of 0.08 within 2A
C66 \\sim C68 \\sim C70 \\sim C72 \\sim C74: within 2A with sigma of 0.04 and
sigma for terminal atoms of 0.08 within 2A
C88 \\sim C90 \\sim C92 \\sim C94 \\sim C96: within 2A with sigma of 0.04 and
sigma for terminal atoms of 0.08 within 2A
C3 \\sim C49 \\sim C25 \\sim C51 \\sim C13: within 2A with sigma of 0.04 and
sigma for terminal atoms of 0.08 within 2A
C29 \\sim C59 \\sim C15 \\sim C61 \\sim C31: within 2A with sigma of 0.04 and
sigma for terminal atoms of 0.08 within 2A
C53 \\sim C27 \\sim C55 \\sim C7 \\sim C57: within 2A with sigma of 0.04 and
sigma for terminal atoms of 0.08 within 2A
C63 \\sim C2 \\sim C65 \\sim C33 \\sim C67: within 2A with sigma of 0.04 and
sigma for terminal atoms of 0.08 within 2A
C17 \\sim C69 \\sim C35 \\sim C71 \\sim C9: within 2A with sigma of 0.04 and
sigma for terminal atoms of 0.08 within 2A
C73 \\sim C37 \\sim C75 \\sim C19 \\sim C77: within 2A with sigma of 0.04 and
sigma for terminal atoms of 0.08 within 2A
C85: within 2A with sigma of 0.04 and sigma for terminal atoms of 0.08 within 2A
C5 \\sim C81 \\sim C41 \\sim C83 \\sim C21: within 2A with sigma of 0.04 and
sigma for terminal atoms of 0.08 within 2A
C43 \\sim C87 \\sim C11 \\sim C89 \\sim C45: within 2A with sigma of 0.04 and
sigma for terminal atoms of 0.08 within 2A
C91 \\sim C23 \\sim C93 \\sim C47 \\sim C95: within 2A with sigma of 0.04 and
sigma for terminal atoms of 0.08 within 2A
C1 \\sim C4 \\sim C6 \\sim C8 \\sim C10 \\sim C12 \\sim C14 \\sim C16 \\sim C18
\\sim C20 \\sim C22 \\sim C24 \\sim C26 \\sim C28 \\sim C30 \\sim C32 \\sim C34
\\sim C36 \\sim C38 \\sim C40 \\sim C42 \\sim C44 \\sim C46 \\sim C48 \\sim C50
\\sim C52 \\sim C54 \\sim C56 \\sim C58 \\sim C60 \\sim C62 \\sim C64 \\sim C66
\\sim C68 \\sim C70 \\sim C72 \\sim C74 \\sim C76 \\sim C78 \\sim C80 \\sim C82
\\sim C84 \\sim C86 \\sim C88 \\sim C90 \\sim C92 \\sim C94 \\sim C96 \\sim C3
\\sim C49 \\sim C25 \\sim C51 \\sim C13 \\sim C53 \\sim C27 \\sim C55 \\sim C7
\\sim C57 \\sim C29 \\sim C59 \\sim C15 \\sim C61 \\sim C31 \\sim C63 \\sim C2
\\sim C65 \\sim C33 \\sim C67 \\sim C17 \\sim C69 \\sim C35 \\sim C71 \\sim C9
\\sim C73 \\sim C37 \\sim C75 \\sim C19 \\sim C77 \\sim C39 \\sim C79 \\sim C5
\\sim C81 \\sim C41 \\sim C83 \\sim C21 \\sim C85 \\sim C43 \\sim C87 \\sim C11
\\sim C89 \\sim C45 \\sim C91 \\sim C23 \\sim C93 \\sim C47 \\sim C95: within
3.8A with sigma of 0.001 and sigma for terminal atoms of 0.002 within 3.8A
3. Rigid body (RIGU) restrains
 Sb2, F3, F4, F5, F6, F7, F8
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 Sb1, F1, F2, F9, F10, F11, F12
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 C16, C18, C20, C22, C24
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 C36, C38, C40, C42, C44
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 C26, C28, C30, C32, C34
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 C56, C58, C60, C62, C64
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 C46, C48, C50, C52, C54
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 C66, C68, C70, C72, C74
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 C88, C90, C92, C94, C96
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 C3, C49, C25, C51, C13
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 C29, C59, C15, C61, C31
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 C17, C69, C35, C71, C9
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 C53, C27, C55, C7, C57
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 C63, C2, C65, C33, C67
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 C73, C37, C75, C19, C77
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 C5, C81, C41, C83, C21
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 C85
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 C43, C87, C11, C89, C45
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 C91, C23, C93, C47, C95
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
;
_atom_sites_solution_hydrogens   .
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.500000 0.500000 0.500000 0.088(2) Uani 1 2 d S . P . .
Ag4 Ag 0.8369(3) 0.5760(3) 0.5744(4) 0.146(2) Uani 1 1 d . . . . .
Ag6 Ag 0.4012(4) 0.3393(3) 0.6228(3) 0.147(2) Uani 1 1 d . . . . .
Ag8 Ag 0.2838(4) 0.4948(4) 0.6047(3) 0.157(3) Uani 1 1 d . . . . .
Ag10 Ag 0.6967(4) 0.4054(3) 0.6991(4) 0.163(3) Uani 1 1 d . . . . .
Ag12 Ag 0.7583(4) 0.5684(3) 0.8063(4) 0.173(3) Uani 1 1 d . . . . .
Ag14 Ag 0.4350(5) 0.5021(4) 0.7349(4) 0.181(3) Uani 1 1 d . . . . .
Ag16 Ag 0.4265(5) 0.6437(3) 0.7329(4) 0.178(3) Uani 1 1 d . . . . .
Ag18 Ag 0.8341(4) 0.6289(4) 0.7306(4) 0.175(3) Uani 1 1 d . . . . .
Ag20 Ag 0.7529(4) 0.4092(4) 0.5152(5) 0.179(3) Uani 1 1 d . . . . .
Ag22 Ag 0.5552(5) 0.5724(4) 0.6774(3) 0.183(3) Uani 1 1 d . . . . .
Ag23 Ag 0.7970(4) 0.7234(4) 0.6223(5) 0.194(3) Uani 1 1 d . . . . .
Ag3 Ag 0.7402(5) 0.7056(4) 0.8014(4) 0.191(3) Uani 1 1 d . . . . .
Ag13 Ag 0.6693(5) 0.7779(4) 0.5430(4) 0.206(4) Uani 1 1 d . . . . .
Ag7 Ag 0.5877(4) 0.4649(5) 0.7650(4) 0.198(3) Uani 1 1 d . . . . .
Ag15 Ag 0.4104(6) 0.7262(4) 0.6338(4) 0.202(3) Uani 1 1 d . . . . .
Ag2 Ag 0.6391(4) 0.5853(4) 0.4813(5) 0.180(3) Uani 1 1 d . . . . .
Ag17 Ag 0.5816(4) 0.7495(4) 0.7616(4) 0.206(4) Uani 1 1 d . . . . .
Ag9 Ag 0.7006(6) 0.7916(3) 0.6973(4) 0.199(3) Uani 1 1 d . . . . .
Ag19 Ag 0.6757(4) 0.4906(5) 0.5999(4) 0.193(3) Uani 1 1 d . . . . .
Br1 Br 0.4689(5) 0.5764(4) 0.4032(5) 0.147(3) Uani 1 1 d . . . . .
Ag5 Ag 0.5206(5) 0.6651(3) 0.5586(5) 0.199(3) Uani 1 1 d . . . . .
Br3 Br 0.4062(5) 0.5670(5) 0.5664(5) 0.153(3) Uani 1 1 d . . . . .
Ag21 Ag 0.6551(6) 0.2968(4) 0.5347(5) 0.217(4) Uani 1 1 d . . . . .
Br2 Br 0.6572(6) 0.6237(5) 0.6245(5) 0.163(3) Uani 1 1 d . . . . .
Ag11 Ag 0.5224(4) 0.2720(4) 0.5745(7) 0.257(5) Uani 1 1 d . . . . .
Sb2 Sb 0.9282(4) 0.7501(4) 1.2427(4) 0.163(2) Uani 1 1 d D U . . .
F3 F 0.893(3) 0.787(2) 1.173(2) 0.33(2) Uani 1 1 d D U . . .
F4 F 0.8270(18) 0.6688(18) 1.180(2) 0.38(3) Uani 1 1 d D U . . .
F5 F 0.881(3) 0.801(2) 1.296(2) 0.32(2) Uani 1 1 d D U . . .
F6 F 1.0306(17) 0.8307(18) 1.308(2) 0.36(3) Uani 1 1 d D U . . .
F7 F 0.976(3) 0.698(2) 1.191(2) 0.32(2) Uani 1 1 d D U . . .
F8 F 0.964(3) 0.714(3) 1.314(2) 0.36(2) Uani 1 1 d D U . . .
Sb1 Sb 0.6669(4) 1.1648(3) 0.9305(3) 0.150(2) Uani 1 1 d D U . . .
F1 F 0.738(3) 1.2558(14) 0.957(3) 0.37(3) Uani 1 1 d D U . . .
F2 F 0.608(3) 1.142(3) 0.8259(12) 0.40(3) Uani 1 1 d D U . . .
F9 F 0.592(2) 1.208(2) 0.948(3) 0.37(3) Uani 1 1 d D U . . .
F10 F 0.722(3) 1.186(3) 1.0350(12) 0.41(3) Uani 1 1 d D U . . .
F11 F 0.742(2) 1.122(2) 0.915(3) 0.36(3) Uani 1 1 d D U . . .
F12 F 0.595(3) 1.0743(14) 0.906(3) 0.37(3) Uani 1 1 d D U . . .
C1 C 0.397(6) 0.220(5) 0.562(6) 0.209(4) Uani 1 1 d . U . . .
C4 C 0.785(5) 0.834(4) 0.663(5) 0.169(6) Uani 1 1 d . U . . .
C6 C 0.855(5) 0.676(5) 0.850(5) 0.173(6) Uani 1 1 d . U . . .
C8 C 0.466(6) 0.758(5) 0.760(6) 0.228(6) Uani 1 1 d . U . . .
C10 C 0.731(7) 0.817(5) 0.820(6) 0.228(6) Uani 1 1 d . U . . .
C12 C 0.602(5) 0.619(4) 0.800(5) 0.157(8) Uani 1 1 d . U . . .
C14 C 0.885(6) 0.675(5) 0.664(5) 0.189(6) Uani 1 1 d . U . . .
C16 C 1.042(4) 0.687(3) 0.972(4) 0.173(6) Uani 1 1 d D U . . .
C18 C 0.985(3) 0.729(2) 0.987(2) 0.173(6) Uani 1 1 d D U . . .
C20 C 0.966(4) 0.715(4) 1.045(3) 0.173(6) Uani 1 1 d D U . . .
C22 C 0.903(3) 0.702(4) 0.909(3) 0.173(6) Uani 1 1 d D U . . .
C24 C 1.033(4) 0.813(2) 1.022(4) 0.173(6) Uani 1 1 d D U . . .
C26 C 0.919(4) 0.957(3) 0.649(3) 0.169(6) Uani 1 1 d D U . . .
C28 C 0.878(3) 0.966(2) 0.699(3) 0.169(6) Uani 1 1 d D U . . .
C30 C 0.824(3) 1.014(3) 0.689(4) 0.169(6) Uani 1 1 d D U . . .
C32 C 0.947(3) 1.004(3) 0.787(2) 0.169(6) Uani 1 1 d D U . . .
C34 C 0.819(3) 0.890(3) 0.677(4) 0.169(6) Uani 1 1 d D U . . .
C36 C 0.548(4) 0.901(4) 0.947(4) 0.228(6) Uani 1 1 d D U . . .
C38 C 0.460(4) 0.864(3) 0.872(3) 0.228(6) Uani 1 1 d D U . . .
C40 C 0.433(5) 0.918(4) 0.843(4) 0.228(6) Uani 1 1 d D U . . .
C42 C 0.392(4) 0.829(4) 0.885(4) 0.228(6) Uani 1 1 d D U . . .
C44 C 0.460(5) 0.801(3) 0.805(4) 0.228(6) Uani 1 1 d D U . . .
C46 C 0.740(3) 0.724(3) 0.988(3) 0.157(8) Uani 1 1 d D U . . .
C48 C 0.645(3) 0.677(2) 0.941(2) 0.157(8) Uani 1 1 d D U . . .
C50 C 0.595(3) 0.724(3) 0.963(4) 0.157(8) Uani 1 1 d D U . . .
C52 C 0.630(4) 0.613(3) 0.960(3) 0.157(8) Uani 1 1 d D U . . .
C54 C 0.613(4) 0.646(3) 0.853(2) 0.157(8) Uani 1 1 d D U . . .
C56 C 0.466(3) 0.130(4) 0.659(4) 0.209(4) Uani 1 1 d D U . . .
C58 C 0.380(3) 0.119(3) 0.593(3) 0.209(4) Uani 1 1 d D U . . .
C60 C 0.394(5) 0.186(4) 0.577(4) 0.209(4) Uani 1 1 d D U . . .
C62 C 0.315(4) 0.113(4) 0.620(4) 0.209(4) Uani 1 1 d D U . . .
C64 C 0.353(4) 0.044(3) 0.520(3) 0.209(4) Uani 1 1 d D U . . .
C66 C 0.888(4) 0.924(4) 0.999(4) 0.228(6) Uani 1 1 d D U . . .
C68 C 0.814(3) 0.934(2) 0.940(3) 0.228(6) Uani 1 1 d D U . . .
C70 C 0.846(5) 0.991(4) 0.919(4) 0.228(6) Uani 1 1 d D U . . .
C72 C 0.760(4) 0.960(4) 0.975(4) 0.228(6) Uani 1 1 d D U . . .
C74 C 0.757(5) 0.860(3) 0.864(3) 0.228(6) Uani 1 1 d D U . . .
C76 C 0.336(7) 0.550(5) 0.719(6) 0.228(6) Uani 1 1 d . U . . .
C78 C 0.467(6) 0.413(5) 0.761(6) 0.209(5) Uani 1 1 d . U . . .
C80 C 0.786(5) 0.477(5) 0.656(5) 0.172(6) Uani 1 1 d . U . . .
C82 C 0.723(6) 0.466(6) 0.816(6) 0.222(9) Uani 1 1 d . U . . .
C84 C 0.537(5) 0.783(4) 0.600(5) 0.168(6) Uani 1 1 d . U . . .
C86 C 0.654(5) 0.282(5) 0.626(5) 0.208(4) Uani 1 1 d . U . . .
C88 C 1.064(4) 0.820(4) 0.738(4) 0.189(6) Uani 1 1 d D U . . .
C90 C 1.032(3) 0.790(3) 0.782(3) 0.189(6) Uani 1 1 d D U . . .
C92 C 1.017(4) 0.849(3) 0.838(3) 0.189(6) Uani 1 1 d D U . . .
C94 C 1.098(4) 0.765(4) 0.831(4) 0.189(6) Uani 1 1 d D U . . .
C96 C 0.948(3) 0.722(3) 0.722(4) 0.189(6) Uani 1 1 d D U . . .
C3 C 0.648(3) 0.960(3) 0.711(3) 0.168(6) Uani 1 1 d D U . . .
C49 C 0.553(3) 0.913(2) 0.656(3) 0.168(6) Uani 1 1 d D U . . .
C25 C 0.515(3) 0.928(3) 0.586(3) 0.168(6) Uani 1 1 d D U . . .
C51 C 0.505(3) 0.927(3) 0.699(3) 0.168(6) Uani 1 1 d D U . . .
C13 C 0.540(4) 0.830(2) 0.622(4) 0.168(6) Uani 1 1 d D U . . .
C53 C 0.910(4) 0.481(4) 0.972(4) 0.222(9) Uani 1 1 d D U . . .
C27 C 0.818(3) 0.469(3) 0.952(3) 0.222(9) Uani 1 1 d D U . . .
C55 C 0.811(5) 0.530(3) 1.013(4) 0.222(9) Uani 1 1 d D U . . .
C7 C 0.772(4) 0.396(3) 0.944(4) 0.222(9) Uani 1 1 d D U . . .
C57 C 0.763(4) 0.467(4) 0.874(3) 0.222(9) Uani 1 1 d D U . . .
C29 C 0.516(4) 0.302(4) 0.835(4) 0.209(5) Uani 1 1 d D U . . .
C59 C 0.462(3) 0.350(3) 0.836(3) 0.209(5) Uani 1 1 d D U . . .
C15 C 0.459(5) 0.385(4) 0.782(4) 0.209(5) Uani 1 1 d D U . . .
C61 C 0.502(4) 0.413(3) 0.921(3) 0.209(5) Uani 1 1 d D U . . .
C31 C 0.371(3) 0.301(4) 0.807(4) 0.209(5) Uani 1 1 d D U . . .
C63 C 0.325(5) 0.560(4) 0.767(4) 0.228(6) Uani 1 1 d D U . . .
C2 C 0.300(3) 0.583(3) 0.830(3) 0.228(6) Uani 1 1 d D U . . .
C65 C 0.264(5) 0.645(3) 0.834(4) 0.228(6) Uani 1 1 d D U . . .
C33 C 0.376(4) 0.613(4) 0.913(3) 0.228(6) Uani 1 1 d D U . . .
C67 C 0.232(4) 0.516(3) 0.814(4) 0.228(6) Uani 1 1 d D U . . .
C17 C 0.808(4) 0.244(4) 0.751(3) 0.208(4) Uani 1 1 d D U . . .
C69 C 0.730(3) 0.200(3) 0.669(3) 0.208(4) Uani 1 1 d D U . . .
C35 C 0.677(4) 0.247(4) 0.651(4) 0.208(4) Uani 1 1 d D U . . .
C71 C 0.673(4) 0.130(3) 0.659(4) 0.208(4) Uani 1 1 d D U . . .
C9 C 0.756(4) 0.175(4) 0.607(3) 0.208(4) Uani 1 1 d D U . . .
C73 C 0.997(3) 0.543(3) 0.793(3) 0.172(6) Uani 1 1 d D U . . .
C37 C 0.927(3) 0.467(3) 0.733(3) 0.172(6) Uani 1 1 d D U . . .
C75 C 0.842(3) 0.474(4) 0.688(3) 0.172(6) Uani 1 1 d D U . . .
C19 C 0.917(4) 0.424(3) 0.777(4) 0.172(6) Uani 1 1 d D U . . .
C77 C 0.950(4) 0.424(3) 0.674(3) 0.172(6) Uani 1 1 d D U . . .
C39 C 0.826(6) 0.495(6) 0.492(6) 0.206(4) Uani 1 1 d . U . . .
C79 C 0.730(6) 0.640(5) 0.462(5) 0.189(6) Uani 1 1 d . U . . .
C5 C 0.929(4) 0.374(4) 0.450(4) 0.206(4) Uani 1 1 d D U . . .
C81 C 0.869(3) 0.402(3) 0.402(3) 0.206(4) Uani 1 1 d D U . . .
C41 C 0.916(4) 0.445(4) 0.374(4) 0.206(4) Uani 1 1 d D U . . .
C83 C 0.842(4) 0.454(4) 0.453(4) 0.206(4) Uani 1 1 d D U . . .
C21 C 0.790(3) 0.335(3) 0.329(3) 0.206(4) Uani 1 1 d D U . . .
C85 C 0.706(5) 0.286(4) 0.461(5) 0.207(4) Uani 1 1 d D U . . .
C43 C 0.863(4) 0.656(3) 0.394(3) 0.189(6) Uani 1 1 d D U . . .
C87 C 0.842(3) 0.712(3) 0.446(3) 0.189(6) Uani 1 1 d D U . . .
C11 C 0.808(4) 0.761(3) 0.410(4) 0.189(6) Uani 1 1 d D U . . .
C89 C 0.920(3) 0.763(3) 0.527(3) 0.189(6) Uani 1 1 d D U . . .
C45 C 0.773(4) 0.672(4) 0.455(4) 0.189(6) Uani 1 1 d D U . . .
C91 C 0.864(3) 0.210(4) 0.480(4) 0.207(4) Uani 1 1 d D U . . .
C23 C 0.775(3) 0.183(3) 0.468(3) 0.208(4) Uani 1 1 d D U . . .
C93 C 0.730(4) 0.236(4) 0.450(4) 0.207(4) Uani 1 1 d D U . . .
C47 C 0.785(4) 0.185(4) 0.545(3) 0.208(4) Uani 1 1 d D U . . .
C95 C 0.727(4) 0.102(3) 0.401(4) 0.208(4) Uani 1 1 d D U . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 Ag22 3.142(6) 2_666 ?
Ag1 Ag22 3.142(6) . ?
Ag1 Ag2 3.150(5) . ?
Ag1 Ag2 3.150(5) 2_666 ?
Ag1 Br1 2.976(8) . ?
Ag1 Br1 2.976(8) 2_666 ?
Ag1 Ag5 3.109(5) 2_666 ?
Ag1 Ag5 3.109(5) . ?
Ag1 Br3 2.917(9) 2_666 ?
Ag1 Br3 2.917(9) . ?
Ag1 Br2 2.912(9) . ?
Ag1 Br2 2.912(9) 2_666 ?
Ag4 Ag8 3.105(8) 2_666 ?
Ag4 Ag18 3.145(9) . ?
Ag4 Ag20 3.093(9) . ?
Ag4 Ag23 3.197(9) . ?
Ag4 C14 1.96(9) . ?
Ag4 C39 1.86(11) . ?
Ag6 Ag14 3.144(9) . ?
Ag6 Ag13 3.022(10) 2_666 ?
Ag6 Ag7 3.280(9) . ?
Ag6 Ag2 3.085(9) 2_666 ?
Ag6 Ag11 3.184(11) . ?
Ag6 C1 2.33(10) . ?
Ag6 C78 2.40(10) . ?
Ag6 C79 2.60(9) 2_666 ?
Ag8 Ag14 2.973(9) . ?
Ag8 Ag16 3.062(9) . ?
Ag8 Ag2 3.010(10) 2_666 ?
Ag8 C76 1.98(10) . ?
Ag8 C39 2.34(9) 2_666 ?
Ag8 C79 2.57(9) 2_666 ?
Ag10 Ag12 3.014(9) . ?
Ag10 Ag7 3.106(10) . ?
Ag10 Ag19 3.176(10) . ?
Ag10 Ag21 3.090(10) . ?
Ag10 Ag11 3.156(10) . ?
Ag10 C80 2.71(8) . ?
Ag10 C82 2.15(10) . ?
Ag10 C86 2.26(10) . ?
Ag12 Ag18 2.999(9) . ?
Ag12 Ag3 2.973(9) . ?
Ag12 Ag7 3.104(9) . ?
Ag12 C6 2.22(8) . ?
Ag12 C82 2.24(9) . ?
Ag14 Ag16 3.003(9) . ?
Ag14 Ag22 3.346(10) . ?
Ag14 Ag7 2.959(9) . ?
Ag14 C76 2.22(10) . ?
Ag14 C78 2.22(10) . ?
Ag16 Ag15 3.133(10) . ?
Ag16 Ag17 3.016(9) . ?
Ag16 C8 2.16(10) . ?
Ag16 C76 2.20(11) . ?
Ag18 Ag3 3.058(10) . ?
Ag18 Ag19 3.074(10) . ?
Ag18 C6 2.21(8) . ?
Ag18 C14 2.37(8) . ?
Ag20 Ag15 3.178(10) 2_666 ?
Ag20 Ag19 3.005(11) . ?
Ag20 Br3 2.997(10) 2_666 ?
Ag20 Ag21 2.987(10) . ?
Ag20 C80 2.56(8) . ?
Ag20 C39 2.39(9) . ?
Ag20 C85 2.23(7) . ?
Ag22 Ag3 3.265(10) . ?
Ag22 Ag7 3.384(11) . ?
Ag22 Ag17 3.323(10) . ?
Ag22 Br1 2.808(11) 2_666 ?
Ag22 Br3 2.768(11) . ?
Ag22 Br2 2.834(11) . ?
Ag22 C12 2.13(8) . ?
Ag23 Ag13 2.972(10) . ?
Ag23 Ag2 3.114(11) . ?
Ag23 Ag9 3.077(11) . ?
Ag23 C4 2.24(8) . ?
Ag23 C14 2.13(9) . ?
Ag3 Ag17 3.124(10) . ?
Ag3 Ag9 3.269(10) . ?
Ag3 Br2 3.046(11) . ?
Ag3 C6 2.27(8) . ?
Ag3 C10 2.26(10) . ?
Ag13 Ag9 2.997(11) . ?
Ag13 Ag11 3.115(10) 2_666 ?
Ag13 C1 2.09(9) 2_666 ?
Ag13 C4 2.25(8) . ?
Ag7 Br1 3.020(11) 2_666 ?
Ag7 C78 2.29(9) . ?
Ag7 C82 2.30(10) . ?
Ag15 Ag17 3.045(11) . ?
Ag15 Ag5 3.258(12) . ?
Ag15 Ag21 3.104(11) 2_666 ?
Ag15 C8 2.24(10) . ?
Ag15 C85 2.18(8) 2_666 ?
Ag2 Br1 2.857(10) . ?
Ag2 Br3 2.818(10) 2_666 ?
Ag2 Br2 2.725(12) . ?
Ag2 C79 2.14(8) . ?
Ag17 Ag9 3.218(10) . ?
Ag17 C8 2.20(10) . ?
Ag17 C10 2.42(11) . ?
Ag9 Ag5 3.207(11) . ?
Ag9 C4 2.19(8) . ?
Ag9 C10 2.27(10) . ?
Ag19 Br1 2.795(11) 2_666 ?
Ag19 Br3 2.874(11) 2_666 ?
Ag19 Br2 2.746(11) . ?
Ag19 C80 2.05(8) . ?
Br1 Ag5 2.783(12) . ?
Br1 Ag11 2.992(10) 2_666 ?
Ag5 Br3 2.805(11) . ?
Ag5 Br2 2.813(12) . ?
Ag5 C84 2.21(7) . ?
Ag21 Ag11 2.965(12) . ?
Ag21 C86 2.10(9) . ?
Ag21 C85 2.12(8) . ?
Ag11 C1 2.28(9) . ?
Ag11 C86 2.17(9) . ?
Sb2 F3 1.861(14) . ?
Sb2 F4 1.860(14) . ?
Sb2 F5 1.867(14) . ?
Sb2 F6 1.867(15) . ?
Sb2 F7 1.862(14) . ?
Sb2 F8 1.868(14) . ?
Sb1 F1 1.863(14) . ?
Sb1 F2 1.863(14) . ?
Sb1 F9 1.871(14) . ?
Sb1 F10 1.867(14) . ?
Sb1 F11 1.860(14) . ?
Sb1 F12 1.870(14) . ?
C1 C60 0.88(9) . ?
C4 C34 1.10(7) . ?
C6 C22 1.04(8) . ?
C8 C44 1.11(10) . ?
C10 C74 0.90(9) . ?
C12 C54 0.98(8) . ?
C14 C96 1.19(9) . ?
C16 C18 1.550(15) . ?
C18 C20 1.544(15) . ?
C18 C22 1.548(15) . ?
C18 C24 1.550(15) . ?
C26 C28 1.543(15) . ?
C28 C30 1.541(15) . ?
C28 C32 1.545(15) . ?
C28 C34 1.544(15) . ?
C36 C38 1.540(15) . ?
C38 C40 1.538(15) . ?
C38 C42 1.544(15) . ?
C38 C44 1.541(15) . ?
C46 C48 1.544(15) . ?
C48 C50 1.545(15) . ?
C48 C52 1.548(15) . ?
C48 C54 1.545(15) . ?
C56 C58 1.558(15) . ?
C58 C60 1.562(15) . ?
C58 C62 1.562(15) . ?
C58 C64 1.562(15) . ?
C66 C68 1.538(15) . ?
C68 C70 1.542(15) . ?
C68 C72 1.544(15) . ?
C68 C74 1.545(15) . ?
C76 C63 1.08(11) . ?
C78 C15 0.89(9) . ?
C80 C75 1.02(8) . ?
C82 C57 1.13(10) . ?
C84 C13 0.91(8) . ?
C86 C35 1.10(9) . ?
C88 C90 1.547(15) . ?
C90 C92 1.546(15) . ?
C90 C94 1.550(15) . ?
C90 C96 1.550(16) . ?
C3 C49 1.538(15) . ?
C49 C25 1.540(15) . ?
C49 C51 1.541(15) . ?
C49 C13 1.541(15) . ?
C53 C27 1.532(15) . ?
C27 C55 1.536(15) . ?
C27 C7 1.540(15) . ?
C27 C57 1.540(15) . ?
C29 C59 1.552(15) . ?
C59 C15 1.552(15) . ?
C59 C61 1.556(15) . ?
C59 C31 1.550(15) . ?
C63 C2 1.541(15) . ?
C2 C65 1.543(15) . ?
C2 C33 1.542(15) . ?
C2 C67 1.544(15) . ?
C17 C69 1.540(15) . ?
C69 C35 1.543(15) . ?
C69 C71 1.538(15) . ?
C69 C9 1.546(15) . ?
C9 C47 1.68(7) . ?
C73 C37 1.537(15) . ?
C37 C75 1.537(15) . ?
C37 C19 1.542(15) . ?
C37 C77 1.540(15) . ?
C39 C83 1.14(11) . ?
C79 C45 1.05(8) . ?
C5 C81 1.551(15) . ?
C81 C41 1.554(15) . ?
C81 C83 1.554(15) . ?
C81 C21 1.554(15) . ?
C85 C93 1.19(2) . ?
C43 C87 1.539(15) . ?
C87 C11 1.539(15) . ?
C87 C89 1.543(15) . ?
C87 C45 1.541(15) . ?
C91 C23 1.554(15) . ?
C23 C93 1.555(15) . ?
C23 C47 1.560(15) . ?
C23 C95 1.557(15) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Ag22 Ag1 Ag22 180.0(3) 2_666 . ?
Ag22 Ag1 Ag2 71.1(2) 2_666 . ?
Ag22 Ag1 Ag2 108.9(2) . . ?
Ag22 Ag1 Ag2 71.1(2) . 2_666 ?
Ag22 Ag1 Ag2 108.9(2) 2_666 2_666 ?
Ag2 Ag1 Ag2 180.0 2_666 . ?
Br1 Ag1 Ag22 54.6(2) . 2_666 ?
Br1 Ag1 Ag22 125.4(2) 2_666 2_666 ?
Br1 Ag1 Ag22 54.6(2) 2_666 . ?
Br1 Ag1 Ag22 125.4(2) . . ?
Br1 Ag1 Ag2 55.5(2) . . ?
Br1 Ag1 Ag2 124.5(2) 2_666 . ?
Br1 Ag1 Ag2 55.5(2) 2_666 2_666 ?
Br1 Ag1 Ag2 124.5(2) . 2_666 ?
Br1 Ag1 Br1 180.0(2) . 2_666 ?
Br1 Ag1 Ag5 54.4(2) . . ?
Br1 Ag1 Ag5 125.6(2) 2_666 . ?
Br1 Ag1 Ag5 125.6(2) . 2_666 ?
Br1 Ag1 Ag5 54.4(2) 2_666 2_666 ?
Ag5 Ag1 Ag22 71.1(2) 2_666 2_666 ?
Ag5 Ag1 Ag22 108.9(2) 2_666 . ?
Ag5 Ag1 Ag22 108.9(2) . 2_666 ?
Ag5 Ag1 Ag22 71.1(2) . . ?
Ag5 Ag1 Ag2 69.5(2) . . ?
Ag5 Ag1 Ag2 69.5(2) 2_666 2_666 ?
Ag5 Ag1 Ag2 110.5(2) . 2_666 ?
Ag5 Ag1 Ag2 110.5(2) 2_666 . ?
Ag5 Ag1 Ag5 180.0 . 2_666 ?
Br3 Ag1 Ag22 54.2(2) 2_666 2_666 ?
Br3 Ag1 Ag22 125.8(2) 2_666 . ?
Br3 Ag1 Ag22 125.8(2) . 2_666 ?
Br3 Ag1 Ag22 54.2(2) . . ?
Br3 Ag1 Ag2 124.8(2) 2_666 2_666 ?
Br3 Ag1 Ag2 55.2(2) 2_666 . ?
Br3 Ag1 Ag2 124.8(2) . . ?
Br3 Ag1 Ag2 55.2(2) . 2_666 ?
Br3 Ag1 Br1 90.1(2) 2_666 2_666 ?
Br3 Ag1 Br1 89.9(2) 2_666 . ?
Br3 Ag1 Br1 90.1(2) . . ?
Br3 Ag1 Br1 89.9(2) . 2_666 ?
Br3 Ag1 Ag5 124.6(2) 2_666 . ?
Br3 Ag1 Ag5 55.4(2) . . ?
Br3 Ag1 Ag5 55.4(2) 2_666 2_666 ?
Br3 Ag1 Ag5 124.6(2) . 2_666 ?
Br3 Ag1 Br3 180.0 . 2_666 ?
Br2 Ag1 Ag22 124.3(2) . 2_666 ?
Br2 Ag1 Ag22 55.7(2) . . ?
Br2 Ag1 Ag22 124.3(2) 2_666 . ?
Br2 Ag1 Ag22 55.7(2) 2_666 2_666 ?
Br2 Ag1 Ag2 126.8(2) . 2_666 ?
Br2 Ag1 Ag2 53.2(2) . . ?
Br2 Ag1 Ag2 126.8(2) 2_666 . ?
Br2 Ag1 Ag2 53.2(2) 2_666 2_666 ?
Br2 Ag1 Br1 89.4(2) . 2_666 ?
Br2 Ag1 Br1 90.6(2) . . ?
Br2 Ag1 Br1 90.6(2) 2_666 2_666 ?
Br2 Ag1 Br1 89.4(2) 2_666 . ?
Br2 Ag1 Ag5 124.4(2) 2_666 . ?
Br2 Ag1 Ag5 55.6(2) . . ?
Br2 Ag1 Ag5 124.4(2) . 2_666 ?
Br2 Ag1 Ag5 55.6(2) 2_666 2_666 ?
Br2 Ag1 Br3 89.0(2) 2_666 . ?
Br2 Ag1 Br3 91.0(2) . . ?
Br2 Ag1 Br3 91.0(2) 2_666 2_666 ?
Br2 Ag1 Br3 89.0(2) . 2_666 ?
Br2 Ag1 Br2 180.0 2_666 . ?
Ag8 Ag4 Ag18 141.0(3) 2_666 . ?
Ag8 Ag4 Ag23 97.3(3) 2_666 . ?
Ag18 Ag4 Ag23 66.6(2) . . ?
Ag20 Ag4 Ag8 73.5(2) . 2_666 ?
Ag20 Ag4 Ag18 95.5(3) . . ?
Ag20 Ag4 Ag23 139.5(3) . . ?
C14 Ag4 Ag8 136(3) . 2_666 ?
C14 Ag4 Ag18 49(2) . . ?
C14 Ag4 Ag20 144(2) . . ?
C14 Ag4 Ag23 40(3) . . ?
C39 Ag4 Ag8 49(3) . 2_666 ?
C39 Ag4 Ag18 145(3) . . ?
C39 Ag4 Ag20 51(3) . . ?
C39 Ag4 Ag23 145(3) . . ?
C39 Ag4 C14 161(4) . . ?
Ag14 Ag6 Ag7 54.8(2) . . ?
Ag14 Ag6 Ag11 130.2(3) . . ?
Ag13 Ag6 Ag14 147.2(3) 2_666 . ?
Ag13 Ag6 Ag7 135.2(3) 2_666 . ?
Ag13 Ag6 Ag2 72.5(2) 2_666 2_666 ?
Ag13 Ag6 Ag11 60.2(3) 2_666 . ?
Ag2 Ag6 Ag14 75.2(2) 2_666 . ?
Ag2 Ag6 Ag7 97.6(2) 2_666 . ?
Ag2 Ag6 Ag11 96.9(3) 2_666 . ?
Ag11 Ag6 Ag7 78.7(3) . . ?
C1 Ag6 Ag14 169(2) . . ?
C1 Ag6 Ag13 44(2) . 2_666 ?
C1 Ag6 Ag7 116(2) . . ?
C1 Ag6 Ag2 115(2) . 2_666 ?
C1 Ag6 Ag11 46(2) . . ?
C1 Ag6 C78 124(3) . . ?
C1 Ag6 C79 113(3) . 2_666 ?
C78 Ag6 Ag14 45(2) . . ?
C78 Ag6 Ag13 168(2) . 2_666 ?
C78 Ag6 Ag7 44(2) . . ?
C78 Ag6 Ag2 119(2) . 2_666 ?
C78 Ag6 Ag11 113(2) . . ?
C78 Ag6 C79 116(3) . 2_666 ?
C79 Ag6 Ag14 78(2) 2_666 . ?
C79 Ag6 Ag13 74.5(19) 2_666 2_666 ?
C79 Ag6 Ag7 128(2) 2_666 . ?
C79 Ag6 Ag2 43.3(18) 2_666 2_666 ?
C79 Ag6 Ag11 128.3(19) 2_666 . ?
Ag14 Ag8 Ag4 147.3(3) . 2_666 ?
Ag14 Ag8 Ag16 59.7(2) . . ?
Ag14 Ag8 Ag2 78.9(2) . 2_666 ?
Ag16 Ag8 Ag4 135.6(3) . 2_666 ?
Ag2 Ag8 Ag4 69.4(2) 2_666 2_666 ?
Ag2 Ag8 Ag16 104.5(3) 2_666 . ?
C76 Ag8 Ag4 164(3) . 2_666 ?
C76 Ag8 Ag14 48(3) . . ?
C76 Ag8 Ag16 46(3) . . ?
C76 Ag8 Ag2 127(3) . 2_666 ?
C76 Ag8 C39 128(4) . 2_666 ?
C76 Ag8 C79 121(4) . 2_666 ?
C39 Ag8 Ag4 37(3) 2_666 2_666 ?
C39 Ag8 Ag14 173(2) 2_666 . ?
C39 Ag8 Ag16 113(2) 2_666 . ?
C39 Ag8 Ag2 103(3) 2_666 2_666 ?
C39 Ag8 C79 104(3) 2_666 2_666 ?
C79 Ag8 Ag4 70(2) 2_666 2_666 ?
C79 Ag8 Ag14 82(2) 2_666 . ?
C79 Ag8 Ag16 137(2) 2_666 . ?
C79 Ag8 Ag2 44.3(18) 2_666 2_666 ?
Ag12 Ag10 Ag7 60.9(2) . . ?
Ag12 Ag10 Ag19 70.9(2) . . ?
Ag12 Ag10 Ag21 140.9(3) . . ?
Ag12 Ag10 Ag11 137.9(3) . . ?
Ag7 Ag10 Ag19 94.6(3) . . ?
Ag7 Ag10 Ag11 81.7(3) . . ?
Ag21 Ag10 Ag7 133.4(3) . . ?
Ag21 Ag10 Ag19 71.7(2) . . ?
Ag21 Ag10 Ag11 56.7(3) . . ?
Ag11 Ag10 Ag19 95.4(3) . . ?
C80 Ag10 Ag12 72.8(18) . . ?
C80 Ag10 Ag7 124.8(17) . . ?
C80 Ag10 Ag19 39.8(16) . . ?
C80 Ag10 Ag21 71.5(18) . . ?
C80 Ag10 Ag11 121.5(18) . . ?
C82 Ag10 Ag12 48(2) . . ?
C82 Ag10 Ag7 48(3) . . ?
C82 Ag10 Ag19 117(3) . . ?
C82 Ag10 Ag21 171(3) . . ?
C82 Ag10 Ag11 119(3) . . ?
C82 Ag10 C80 116(3) . . ?
C82 Ag10 C86 128(3) . . ?
C86 Ag10 Ag12 176(2) . . ?
C86 Ag10 Ag7 118(2) . . ?
C86 Ag10 Ag19 113(2) . . ?
C86 Ag10 Ag21 43(2) . . ?
C86 Ag10 Ag11 44(2) . . ?
C86 Ag10 C80 110(3) . . ?
Ag10 Ag12 Ag7 61.0(2) . . ?
Ag18 Ag12 Ag10 99.8(3) . . ?
Ag18 Ag12 Ag7 139.8(3) . . ?
Ag3 Ag12 Ag10 140.4(3) . . ?
Ag3 Ag12 Ag18 61.6(2) . . ?
Ag3 Ag12 Ag7 109.2(3) . . ?
C6 Ag12 Ag10 142(2) . . ?
C6 Ag12 Ag18 47(2) . . ?
C6 Ag12 Ag3 49(2) . . ?
C6 Ag12 Ag7 156(2) . . ?
C6 Ag12 C82 149(3) . . ?
C82 Ag12 Ag10 45(3) . . ?
C82 Ag12 Ag18 141(3) . . ?
C82 Ag12 Ag3 155(3) . . ?
C82 Ag12 Ag7 48(3) . . ?
Ag6 Ag14 Ag22 92.0(2) . . ?
Ag8 Ag14 Ag6 88.1(3) . . ?
Ag8 Ag14 Ag16 61.7(2) . . ?
Ag8 Ag14 Ag22 89.2(2) . . ?
Ag16 Ag14 Ag6 140.7(3) . . ?
Ag16 Ag14 Ag22 65.0(2) . . ?
Ag7 Ag14 Ag6 64.9(2) . . ?
Ag7 Ag14 Ag8 140.2(3) . . ?
Ag7 Ag14 Ag16 122.8(3) . . ?
Ag7 Ag14 Ag22 64.6(2) . . ?
C76 Ag14 Ag6 124(2) . . ?
C76 Ag14 Ag8 42(2) . . ?
C76 Ag14 Ag16 47(3) . . ?
C76 Ag14 Ag22 107(3) . . ?
C76 Ag14 Ag7 170(3) . . ?
C76 Ag14 C78 139(4) . . ?
C78 Ag14 Ag6 49(3) . . ?
C78 Ag14 Ag8 131(2) . . ?
C78 Ag14 Ag16 168(3) . . ?
C78 Ag14 Ag22 113(2) . . ?
C78 Ag14 Ag7 50(2) . . ?
Ag8 Ag16 Ag15 98.8(3) . . ?
Ag14 Ag16 Ag8 58.7(2) . . ?
Ag14 Ag16 Ag15 143.4(3) . . ?
Ag14 Ag16 Ag17 117.2(3) . . ?
Ag17 Ag16 Ag8 139.2(3) . . ?
Ag17 Ag16 Ag15 59.3(3) . . ?
C8 Ag16 Ag8 140(3) . . ?
C8 Ag16 Ag14 160(3) . . ?
C8 Ag16 Ag15 46(3) . . ?
C8 Ag16 Ag17 47(3) . . ?
C8 Ag16 C76 147(4) . . ?
C76 Ag16 Ag8 40(3) . . ?
C76 Ag16 Ag14 48(3) . . ?
C76 Ag16 Ag15 133(3) . . ?
C76 Ag16 Ag17 165(3) . . ?
Ag12 Ag18 Ag4 139.7(3) . . ?
Ag12 Ag18 Ag3 58.8(2) . . ?
Ag12 Ag18 Ag19 72.5(2) . . ?
Ag3 Ag18 Ag4 138.5(3) . . ?
Ag3 Ag18 Ag19 94.3(3) . . ?
Ag19 Ag18 Ag4 70.3(2) . . ?
C6 Ag18 Ag4 170(2) . . ?
C6 Ag18 Ag12 48(2) . . ?
C6 Ag18 Ag3 48(2) . . ?
C6 Ag18 Ag19 119(2) . . ?
C6 Ag18 C14 135(3) . . ?
C14 Ag18 Ag4 39(2) . . ?
C14 Ag18 Ag12 176(2) . . ?
C14 Ag18 Ag3 120(2) . . ?
C14 Ag18 Ag19 104(2) . . ?
Ag4 Ag20 Ag15 137.4(3) . 2_666 ?
Ag19 Ag20 Ag4 71.9(2) . . ?
Ag19 Ag20 Ag15 101.0(3) . 2_666 ?
Br3 Ag20 Ag4 83.3(2) 2_666 . ?
Br3 Ag20 Ag15 59.9(2) 2_666 2_666 ?
Br3 Ag20 Ag19 57.2(2) 2_666 . ?
Ag21 Ag20 Ag4 145.4(4) . . ?
Ag21 Ag20 Ag15 60.4(3) . 2_666 ?
Ag21 Ag20 Ag19 75.5(3) . . ?
Ag21 Ag20 Br3 88.8(3) . 2_666 ?
C80 Ag20 Ag4 73.0(19) . . ?
C80 Ag20 Ag15 129.8(18) . 2_666 ?
C80 Ag20 Ag19 42.3(17) . . ?
C80 Ag20 Br3 99.5(17) . 2_666 ?
C80 Ag20 Ag21 75.2(19) . . ?
C39 Ag20 Ag4 37(3) . . ?
C39 Ag20 Ag15 116(2) . 2_666 ?
C39 Ag20 Ag19 106(3) . . ?
C39 Ag20 Br3 90(2) . 2_666 ?
C39 Ag20 Ag21 177(2) . . ?
C39 Ag20 C80 108(3) . . ?
C85 Ag20 Ag4 169(2) . . ?
C85 Ag20 Ag15 43(2) . 2_666 ?
C85 Ag20 Ag19 119(2) . . ?
C85 Ag20 Br3 101(2) . 2_666 ?
C85 Ag20 Ag21 45(2) . . ?
C85 Ag20 C80 115(3) . . ?
C85 Ag20 C39 133(4) . . ?
Ag1 Ag22 Ag14 120.1(2) . . ?
Ag1 Ag22 Ag3 117.4(3) . . ?
Ag1 Ag22 Ag7 117.2(3) . . ?
Ag1 Ag22 Ag17 116.3(3) . . ?
Ag14 Ag22 Ag7 52.17(18) . . ?
Ag3 Ag22 Ag14 122.2(3) . . ?
Ag3 Ag22 Ag7 96.3(2) . . ?
Ag3 Ag22 Ag17 56.59(19) . . ?
Ag17 Ag22 Ag14 100.7(3) . . ?
Ag17 Ag22 Ag7 126.5(3) . . ?
Br1 Ag22 Ag1 59.7(2) 2_666 . ?
Br1 Ag22 Ag14 82.2(3) 2_666 . ?
Br1 Ag22 Ag3 124.1(3) 2_666 . ?
Br1 Ag22 Ag7 57.5(3) 2_666 . ?
Br1 Ag22 Ag17 176.0(3) 2_666 . ?
Br1 Ag22 Br2 94.5(3) 2_666 . ?
Br3 Ag22 Ag1 58.8(2) . . ?
Br3 Ag22 Ag14 85.1(3) . . ?
Br3 Ag22 Ag3 131.4(3) . . ?
Br3 Ag22 Ag7 129.9(3) . . ?
Br3 Ag22 Ag17 81.0(3) . . ?
Br3 Ag22 Br1 96.7(3) . 2_666 ?
Br3 Ag22 Br2 95.8(3) . . ?
Br2 Ag22 Ag1 58.0(2) . . ?
Br2 Ag22 Ag14 176.6(3) . . ?
Br2 Ag22 Ag3 59.4(3) . . ?
Br2 Ag22 Ag7 125.5(3) . . ?
Br2 Ag22 Ag17 82.6(3) . . ?
C12 Ag22 Ag1 175(2) . . ?
C12 Ag22 Ag14 62(2) . . ?
C12 Ag22 Ag3 60(2) . . ?
C12 Ag22 Ag7 60(2) . . ?
C12 Ag22 Ag17 66(2) . . ?
C12 Ag22 Br1 118(2) . 2_666 ?
C12 Ag22 Br3 126(2) . . ?
C12 Ag22 Br2 119(2) . . ?
Ag13 Ag23 Ag4 136.2(4) . . ?
Ag13 Ag23 Ag2 72.8(2) . . ?
Ag13 Ag23 Ag9 59.4(3) . . ?
Ag2 Ag23 Ag4 67.0(2) . . ?
Ag9 Ag23 Ag4 139.2(3) . . ?
Ag9 Ag23 Ag2 95.2(3) . . ?
C4 Ag23 Ag4 173.4(19) . . ?
C4 Ag23 Ag13 49(2) . . ?
C4 Ag23 Ag2 119(2) . . ?
C4 Ag23 Ag9 45(2) . . ?
C14 Ag23 Ag4 37(2) . . ?
C14 Ag23 Ag13 172(2) . . ?
C14 Ag23 Ag2 102(3) . . ?
C14 Ag23 Ag9 127(2) . . ?
C14 Ag23 C4 138(3) . . ?
Ag12 Ag3 Ag18 59.6(2) . . ?
Ag12 Ag3 Ag22 72.6(2) . . ?
Ag12 Ag3 Ag17 129.1(4) . . ?
Ag12 Ag3 Ag9 146.4(3) . . ?
Ag12 Ag3 Br2 89.3(3) . . ?
Ag18 Ag3 Ag22 95.7(3) . . ?
Ag18 Ag3 Ag17 143.6(3) . . ?
Ag18 Ag3 Ag9 93.9(3) . . ?
Ag22 Ag3 Ag9 91.8(2) . . ?
Ag17 Ag3 Ag22 62.6(2) . . ?
Ag17 Ag3 Ag9 60.4(2) . . ?
Br2 Ag3 Ag18 61.1(2) . . ?
Br2 Ag3 Ag22 53.2(2) . . ?
Br2 Ag3 Ag17 82.8(3) . . ?
Br2 Ag3 Ag9 58.2(2) . . ?
C6 Ag3 Ag12 48(2) . . ?
C6 Ag3 Ag18 46(2) . . ?
C6 Ag3 Ag22 119(2) . . ?
C6 Ag3 Ag17 170(2) . . ?
C6 Ag3 Ag9 128(2) . . ?
C6 Ag3 Br2 106(2) . . ?
C10 Ag3 Ag12 170(3) . . ?
C10 Ag3 Ag18 128(3) . . ?
C10 Ag3 Ag22 111(3) . . ?
C10 Ag3 Ag17 50(3) . . ?
C10 Ag3 Ag9 44(3) . . ?
C10 Ag3 Br2 101(3) . . ?
C10 Ag3 C6 130(4) . . ?
Ag6 Ag13 Ag11 62.5(3) 2_666 2_666 ?
Ag23 Ag13 Ag6 97.6(3) . 2_666 ?
Ag23 Ag13 Ag9 62.1(3) . . ?
Ag23 Ag13 Ag11 142.3(3) . 2_666 ?
Ag9 Ag13 Ag6 140.2(3) . 2_666 ?
Ag9 Ag13 Ag11 111.6(4) . 2_666 ?
C1 Ag13 Ag6 50(3) 2_666 2_666 ?
C1 Ag13 Ag23 143(3) 2_666 . ?
C1 Ag13 Ag9 155(3) 2_666 . ?
C1 Ag13 Ag11 47(2) 2_666 2_666 ?
C1 Ag13 C4 147(3) 2_666 . ?
C4 Ag13 Ag6 142(2) . 2_666 ?
C4 Ag13 Ag23 48(2) . . ?
C4 Ag13 Ag9 47(2) . . ?
C4 Ag13 Ag11 154(2) . 2_666 ?
Ag6 Ag7 Ag22 88.9(2) . . ?
Ag10 Ag7 Ag6 98.8(3) . . ?
Ag10 Ag7 Ag22 94.2(3) . . ?
Ag12 Ag7 Ag6 145.2(3) . . ?
Ag12 Ag7 Ag10 58.1(2) . . ?
Ag12 Ag7 Ag22 69.4(2) . . ?
Ag14 Ag7 Ag6 60.3(2) . . ?
Ag14 Ag7 Ag10 147.6(3) . . ?
Ag14 Ag7 Ag12 124.9(4) . . ?
Ag14 Ag7 Ag22 63.3(2) . . ?
Ag14 Ag7 Br1 85.7(3) . 2_666 ?
Br1 Ag7 Ag6 59.0(2) 2_666 . ?
Br1 Ag7 Ag10 61.9(2) 2_666 . ?
Br1 Ag7 Ag12 86.3(3) 2_666 . ?
Br1 Ag7 Ag22 51.6(2) 2_666 . ?
C78 Ag7 Ag6 47(3) . . ?
C78 Ag7 Ag10 136(3) . . ?
C78 Ag7 Ag12 166(3) . . ?
C78 Ag7 Ag14 48(2) . . ?
C78 Ag7 Ag22 109(2) . . ?
C78 Ag7 Br1 104(2) . 2_666 ?
C78 Ag7 C82 137(3) . . ?
C82 Ag7 Ag6 135(3) . . ?
C82 Ag7 Ag10 44(2) . . ?
C82 Ag7 Ag12 46(2) . . ?
C82 Ag7 Ag14 165(3) . . ?
C82 Ag7 Ag22 114(2) . . ?
C82 Ag7 Br1 104(2) . 2_666 ?
Ag16 Ag15 Ag20 91.7(3) . 2_666 ?
Ag16 Ag15 Ag5 98.8(3) . . ?
Ag20 Ag15 Ag5 88.0(2) 2_666 . ?
Ag17 Ag15 Ag16 58.4(2) . . ?
Ag17 Ag15 Ag20 137.4(3) . 2_666 ?
Ag17 Ag15 Ag5 69.7(3) . . ?
Ag17 Ag15 Ag21 132.7(4) . 2_666 ?
Ag21 Ag15 Ag16 143.8(3) 2_666 . ?
Ag21 Ag15 Ag20 56.8(2) 2_666 2_666 ?
Ag21 Ag15 Ag5 66.0(3) 2_666 . ?
C8 Ag15 Ag16 44(2) . . ?
C8 Ag15 Ag20 130(3) . 2_666 ?
C8 Ag15 Ag17 46(3) . . ?
C8 Ag15 Ag5 115(3) . . ?
C8 Ag15 Ag21 173(3) . 2_666 ?
C85 Ag15 Ag16 126(2) 2_666 . ?
C85 Ag15 Ag20 44.6(17) 2_666 2_666 ?
C85 Ag15 Ag17 175(2) 2_666 . ?
C85 Ag15 Ag5 107(2) 2_666 . ?
C85 Ag15 Ag21 43(2) 2_666 2_666 ?
C85 Ag15 C8 138(4) 2_666 . ?
Ag6 Ag2 Ag1 122.2(3) 2_666 . ?
Ag6 Ag2 Ag23 93.4(2) 2_666 . ?
Ag8 Ag2 Ag1 121.5(3) 2_666 . ?
Ag8 Ag2 Ag6 88.6(2) 2_666 2_666 ?
Ag8 Ag2 Ag23 101.2(3) 2_666 . ?
Ag23 Ag2 Ag1 122.2(3) . . ?
Br1 Ag2 Ag1 59.2(2) . . ?
Br1 Ag2 Ag6 63.0(2) . 2_666 ?
Br1 Ag2 Ag8 122.4(3) . 2_666 ?
Br1 Ag2 Ag23 127.6(3) . . ?
Br3 Ag2 Ag1 58.2(2) 2_666 . ?
Br3 Ag2 Ag6 127.8(3) 2_666 2_666 ?
Br3 Ag2 Ag8 63.6(3) 2_666 2_666 ?
Br3 Ag2 Ag23 133.0(3) 2_666 . ?
Br3 Ag2 Br1 94.4(3) 2_666 . ?
Br2 Ag2 Ag1 58.9(2) . . ?
Br2 Ag2 Ag6 131.9(3) . 2_666 ?
Br2 Ag2 Ag8 134.9(3) . 2_666 ?
Br2 Ag2 Ag23 63.4(3) . . ?
Br2 Ag2 Br1 97.1(3) . . ?
Br2 Ag2 Br3 95.0(3) . 2_666 ?
C79 Ag2 Ag1 177(2) . . ?
C79 Ag2 Ag6 56(2) . 2_666 ?
C79 Ag2 Ag8 57(2) . 2_666 ?
C79 Ag2 Ag23 61(2) . . ?
C79 Ag2 Br1 119(2) . . ?
C79 Ag2 Br3 120(2) . 2_666 ?
C79 Ag2 Br2 124(2) . . ?
Ag16 Ag17 Ag22 65.2(2) . . ?
Ag16 Ag17 Ag3 116.6(3) . . ?
Ag16 Ag17 Ag15 62.2(2) . . ?
Ag16 Ag17 Ag9 148.6(3) . . ?
Ag3 Ag17 Ag22 60.8(2) . . ?
Ag3 Ag17 Ag9 62.0(2) . . ?
Ag15 Ag17 Ag22 93.4(2) . . ?
Ag15 Ag17 Ag3 146.4(3) . . ?
Ag15 Ag17 Ag9 100.8(3) . . ?
Ag9 Ag17 Ag22 91.6(2) . . ?
C8 Ag17 Ag16 46(3) . . ?
C8 Ag17 Ag22 109(2) . . ?
C8 Ag17 Ag3 157(3) . . ?
C8 Ag17 Ag15 47(3) . . ?
C8 Ag17 Ag9 141(3) . . ?
C8 Ag17 C10 144(3) . . ?
C10 Ag17 Ag16 158(3) . . ?
C10 Ag17 Ag22 105(2) . . ?
C10 Ag17 Ag3 46(2) . . ?
C10 Ag17 Ag15 140(3) . . ?
C10 Ag17 Ag9 45(2) . . ?
Ag23 Ag9 Ag3 90.1(3) . . ?
Ag23 Ag9 Ag17 139.5(3) . . ?
Ag23 Ag9 Ag5 93.6(3) . . ?
Ag13 Ag9 Ag23 58.6(3) . . ?
Ag13 Ag9 Ag3 142.3(3) . . ?
Ag13 Ag9 Ag17 134.6(4) . . ?
Ag13 Ag9 Ag5 69.5(3) . . ?
Ag17 Ag9 Ag3 57.6(2) . . ?
Ag5 Ag9 Ag3 94.6(2) . . ?
Ag5 Ag9 Ag17 68.3(3) . . ?
C4 Ag9 Ag23 47(2) . . ?
C4 Ag9 Ag3 125(2) . . ?
C4 Ag9 Ag13 48(2) . . ?
C4 Ag9 Ag17 173(2) . . ?
C4 Ag9 Ag5 117(2) . . ?
C4 Ag9 C10 127(4) . . ?
C10 Ag9 Ag23 124(3) . . ?
C10 Ag9 Ag3 44(2) . . ?
C10 Ag9 Ag13 173(2) . . ?
C10 Ag9 Ag17 49(3) . . ?
C10 Ag9 Ag5 116(3) . . ?
Ag10 Ag19 Ag1 122.6(3) . . ?
Ag18 Ag19 Ag1 122.4(3) . . ?
Ag18 Ag19 Ag10 94.8(2) . . ?
Ag20 Ag19 Ag1 118.4(3) . . ?
Ag20 Ag19 Ag10 93.3(3) . . ?
Ag20 Ag19 Ag18 98.9(3) . . ?
Br1 Ag19 Ag1 59.3(2) 2_666 . ?
Br1 Ag19 Ag10 63.3(3) 2_666 . ?
Br1 Ag19 Ag18 130.4(4) 2_666 . ?
Br1 Ag19 Ag20 124.6(4) 2_666 . ?
Br1 Ag19 Br3 94.7(3) 2_666 2_666 ?
Br3 Ag19 Ag1 57.3(2) 2_666 . ?
Br3 Ag19 Ag10 129.6(3) 2_666 . ?
Br3 Ag19 Ag18 129.5(3) 2_666 . ?
Br3 Ag19 Ag20 61.3(3) 2_666 . ?
Br2 Ag19 Ag1 58.3(2) . . ?
Br2 Ag19 Ag10 131.8(4) . . ?
Br2 Ag19 Ag18 64.1(3) . . ?
Br2 Ag19 Ag20 130.9(4) . . ?
Br2 Ag19 Br1 96.7(3) . 2_666 ?
Br2 Ag19 Br3 93.3(3) . 2_666 ?
C80 Ag19 Ag1 175(2) . . ?
C80 Ag19 Ag10 58(2) . . ?
C80 Ag19 Ag18 62(2) . . ?
C80 Ag19 Ag20 57(2) . . ?
C80 Ag19 Br1 121(2) . 2_666 ?
C80 Ag19 Br3 118(2) . 2_666 ?
C80 Ag19 Br2 126(2) . . ?
Ag1 Br1 Ag7 136.6(3) . 2_666 ?
Ag1 Br1 Ag11 137.5(4) . 2_666 ?
Ag22 Br1 Ag1 65.7(2) 2_666 . ?
Ag22 Br1 Ag7 70.9(3) 2_666 2_666 ?
Ag22 Br1 Ag2 80.4(3) 2_666 . ?
Ag22 Br1 Ag11 156.8(4) 2_666 2_666 ?
Ag2 Br1 Ag1 65.3(2) . . ?
Ag2 Br1 Ag7 109.2(3) . 2_666 ?
Ag2 Br1 Ag11 106.7(3) . 2_666 ?
Ag19 Br1 Ag1 66.9(2) 2_666 . ?
Ag19 Br1 Ag22 80.5(3) 2_666 2_666 ?
Ag19 Br1 Ag7 105.1(3) 2_666 2_666 ?
Ag19 Br1 Ag2 132.2(3) 2_666 . ?
Ag19 Br1 Ag11 108.0(3) 2_666 2_666 ?
Ag5 Br1 Ag1 65.2(2) . . ?
Ag5 Br1 Ag22 130.9(3) . 2_666 ?
Ag5 Br1 Ag7 158.2(4) . 2_666 ?
Ag5 Br1 Ag2 78.4(3) . . ?
Ag5 Br1 Ag19 82.0(3) . 2_666 ?
Ag5 Br1 Ag11 72.2(3) . 2_666 ?
Ag11 Br1 Ag7 85.9(4) 2_666 2_666 ?
Ag1 Ag5 Ag15 119.5(3) . . ?
Ag1 Ag5 Ag9 119.7(3) . . ?
Ag9 Ag5 Ag15 96.6(3) . . ?
Br1 Ag5 Ag1 60.4(2) . . ?
Br1 Ag5 Ag15 129.3(3) . . ?
Br1 Ag5 Ag9 129.0(4) . . ?
Br1 Ag5 Br3 96.5(3) . . ?
Br1 Ag5 Br2 96.8(3) . . ?
Br3 Ag5 Ag1 58.9(2) . . ?
Br3 Ag5 Ag15 60.6(3) . . ?
Br3 Ag5 Ag9 128.6(4) . . ?
Br3 Ag5 Br2 95.4(3) . . ?
Br2 Ag5 Ag1 58.7(2) . . ?
Br2 Ag5 Ag15 127.7(4) . . ?
Br2 Ag5 Ag9 61.1(3) . . ?
C84 Ag5 Ag1 179(2) . . ?
C84 Ag5 Ag15 61(2) . . ?
C84 Ag5 Ag9 60(2) . . ?
C84 Ag5 Br1 119(2) . . ?
C84 Ag5 Br3 122(2) . . ?
C84 Ag5 Br2 121(2) . . ?
Ag1 Br3 Ag20 128.1(3) . 2_666 ?
Ag22 Br3 Ag1 67.0(2) . . ?
Ag22 Br3 Ag20 164.4(4) . 2_666 ?
Ag22 Br3 Ag2 81.8(3) . 2_666 ?
Ag22 Br3 Ag19 133.7(4) . 2_666 ?
Ag22 Br3 Ag5 81.4(3) . . ?
Ag2 Br3 Ag1 66.6(2) 2_666 . ?
Ag2 Br3 Ag20 106.9(3) 2_666 2_666 ?
Ag2 Br3 Ag19 80.1(3) 2_666 2_666 ?
Ag19 Br3 Ag1 66.7(2) 2_666 . ?
Ag19 Br3 Ag20 61.5(3) 2_666 2_666 ?
Ag5 Br3 Ag1 65.8(2) . . ?
Ag5 Br3 Ag20 100.8(3) . 2_666 ?
Ag5 Br3 Ag2 132.4(4) . 2_666 ?
Ag5 Br3 Ag19 80.2(3) . 2_666 ?
Ag10 Ag21 Ag15 143.6(3) . 2_666 ?
Ag20 Ag21 Ag10 95.4(3) . . ?
Ag20 Ag21 Ag15 62.9(3) . 2_666 ?
Ag11 Ag21 Ag10 62.8(3) . . ?
Ag11 Ag21 Ag20 140.6(3) . . ?
Ag11 Ag21 Ag15 114.8(4) . 2_666 ?
C86 Ag21 Ag10 47(3) . . ?
C86 Ag21 Ag20 138(3) . . ?
C86 Ag21 Ag15 158(2) . 2_666 ?
C86 Ag21 Ag11 47(2) . . ?
C86 Ag21 C85 148(3) . . ?
C85 Ag21 Ag10 139(2) . . ?
C85 Ag21 Ag20 48.2(18) . . ?
C85 Ag21 Ag15 45(2) . 2_666 ?
C85 Ag21 Ag11 157(2) . . ?
Ag1 Br2 Ag3 133.6(4) . . ?
Ag22 Br2 Ag1 66.3(2) . . ?
Ag22 Br2 Ag3 67.4(3) . . ?
Ag2 Br2 Ag1 67.9(2) . . ?
Ag2 Br2 Ag22 134.1(4) . . ?
Ag2 Br2 Ag3 158.5(4) . . ?
Ag2 Br2 Ag19 84.1(3) . . ?
Ag2 Br2 Ag5 80.1(3) . . ?
Ag19 Br2 Ag1 68.4(2) . . ?
Ag19 Br2 Ag22 80.8(3) . . ?
Ag19 Br2 Ag3 101.7(3) . . ?
Ag19 Br2 Ag5 134.1(4) . . ?
Ag5 Br2 Ag1 65.7(2) . . ?
Ag5 Br2 Ag22 80.1(3) . . ?
Ag5 Br2 Ag3 108.6(4) . . ?
Ag10 Ag11 Ag6 99.8(3) . . ?
Ag13 Ag11 Ag6 57.3(2) 2_666 . ?
Ag13 Ag11 Ag10 146.8(3) 2_666 . ?
Br1 Ag11 Ag6 60.4(2) 2_666 . ?
Br1 Ag11 Ag10 61.6(2) 2_666 . ?
Br1 Ag11 Ag13 85.4(3) 2_666 2_666 ?
Ag21 Ag11 Ag6 145.5(3) . . ?
Ag21 Ag11 Ag10 60.6(2) . . ?
Ag21 Ag11 Ag13 123.5(5) . 2_666 ?
Ag21 Ag11 Br1 85.1(3) . 2_666 ?
C1 Ag11 Ag6 47(3) . . ?
C1 Ag11 Ag10 140(3) . . ?
C1 Ag11 Ag13 42(2) . 2_666 ?
C1 Ag11 Br1 104(3) . 2_666 ?
C1 Ag11 Ag21 160(3) . . ?
C86 Ag11 Ag6 140(3) . . ?
C86 Ag11 Ag10 46(3) . . ?
C86 Ag11 Ag13 163(3) . 2_666 ?
C86 Ag11 Br1 104(3) . 2_666 ?
C86 Ag11 Ag21 45(2) . . ?
C86 Ag11 C1 144(3) . . ?
F3 Sb2 F5 90.3(12) . . ?
F3 Sb2 F6 90.4(12) . . ?
F3 Sb2 F7 91.1(12) . . ?
F3 Sb2 F8 179.0(13) . . ?
F4 Sb2 F3 91.1(12) . . ?
F4 Sb2 F5 89.9(12) . . ?
F4 Sb2 F6 178.5(14) . . ?
F4 Sb2 F7 90.1(12) . . ?
F4 Sb2 F8 89.7(12) . . ?
F5 Sb2 F6 90.1(12) . . ?
F5 Sb2 F8 89.0(12) . . ?
F6 Sb2 F8 88.8(12) . . ?
F7 Sb2 F5 178.6(14) . . ?
F7 Sb2 F6 89.9(12) . . ?
F7 Sb2 F8 89.5(12) . . ?
F1 Sb1 F9 89.9(12) . . ?
F1 Sb1 F10 90.3(12) . . ?
F1 Sb1 F12 178.9(14) . . ?
F2 Sb1 F1 91.3(12) . . ?
F2 Sb1 F9 89.5(12) . . ?
F2 Sb1 F10 177.6(14) . . ?
F2 Sb1 F12 89.5(12) . . ?
F10 Sb1 F9 88.7(12) . . ?
F10 Sb1 F12 88.8(12) . . ?
F11 Sb1 F1 90.2(12) . . ?
F11 Sb1 F2 91.4(12) . . ?
F11 Sb1 F9 179.1(14) . . ?
F11 Sb1 F10 90.4(12) . . ?
F11 Sb1 F12 90.6(12) . . ?
F12 Sb1 F9 89.3(12) . . ?
Ag13 C1 Ag6 86(3) 2_666 . ?
Ag13 C1 Ag11 91(3) 2_666 . ?
Ag11 C1 Ag6 87(3) . . ?
C60 C1 Ag6 128(10) . . ?
C60 C1 Ag13 135(10) . 2_666 ?
C60 C1 Ag11 116(10) . . ?
Ag23 C4 Ag13 83(3) . . ?
Ag9 C4 Ag23 88(3) . . ?
Ag9 C4 Ag13 85(3) . . ?
C34 C4 Ag23 137(7) . . ?
C34 C4 Ag13 110(7) . . ?
C34 C4 Ag9 132(7) . . ?
Ag12 C6 Ag18 85(3) . . ?
Ag12 C6 Ag3 83(3) . . ?
Ag18 C6 Ag3 86(3) . . ?
C22 C6 Ag12 116(8) . . ?
C22 C6 Ag18 143(8) . . ?
C22 C6 Ag3 125(8) . . ?
Ag16 C8 Ag15 91(3) . . ?
Ag16 C8 Ag17 87(4) . . ?
Ag17 C8 Ag15 87(4) . . ?
C44 C8 Ag16 122(10) . . ?
C44 C8 Ag15 129(9) . . ?
C44 C8 Ag17 128(9) . . ?
Ag3 C10 Ag17 84(3) . . ?
Ag3 C10 Ag9 92(3) . . ?
Ag9 C10 Ag17 86(3) . . ?
C74 C10 Ag3 129(10) . . ?
C74 C10 Ag17 119(10) . . ?
C74 C10 Ag9 131(10) . . ?
C54 C12 Ag22 166(8) . . ?
Ag4 C14 Ag18 93(3) . . ?
Ag4 C14 Ag23 103(4) . . ?
Ag23 C14 Ag18 102(3) . . ?
C96 C14 Ag4 144(8) . . ?
C96 C14 Ag18 95(6) . . ?
C96 C14 Ag23 110(7) . . ?
C20 C18 C16 109(2) . . ?
C20 C18 C22 111(2) . . ?
C20 C18 C24 110(2) . . ?
C22 C18 C16 109(2) . . ?
C22 C18 C24 109(2) . . ?
C24 C18 C16 109(2) . . ?
C6 C22 C18 165(8) . . ?
C26 C28 C32 110(2) . . ?
C26 C28 C34 111(2) . . ?
C30 C28 C26 111(2) . . ?
C30 C28 C32 108(2) . . ?
C30 C28 C34 108(2) . . ?
C34 C28 C32 109(2) . . ?
C4 C34 C28 172(7) . . ?
C36 C38 C42 111(2) . . ?
C36 C38 C44 111(2) . . ?
C40 C38 C36 113(2) . . ?
C40 C38 C42 107(3) . . ?
C40 C38 C44 108(3) . . ?
C44 C38 C42 107(3) . . ?
C8 C44 C38 175(9) . . ?
C46 C48 C50 111(2) . . ?
C46 C48 C52 109(2) . . ?
C46 C48 C54 109(2) . . ?
C50 C48 C52 108(2) . . ?
C50 C48 C54 110(2) . . ?
C54 C48 C52 110(2) . . ?
C12 C54 C48 166(8) . . ?
C56 C58 C60 108(2) . . ?
C56 C58 C62 107(2) . . ?
C56 C58 C64 107(2) . . ?
C62 C58 C60 113(2) . . ?
C64 C58 C60 112(2) . . ?
C64 C58 C62 110(2) . . ?
C1 C60 C58 173(10) . . ?
C66 C68 C70 112(2) . . ?
C66 C68 C72 110(2) . . ?
C66 C68 C74 110(2) . . ?
C70 C68 C72 108(3) . . ?
C70 C68 C74 108(3) . . ?
C72 C68 C74 108(3) . . ?
C10 C74 C68 172(10) . . ?
Ag8 C76 Ag14 90(4) . . ?
Ag8 C76 Ag16 94(4) . . ?
Ag14 C76 Ag16 85(4) . . ?
C63 C76 Ag8 145(10) . . ?
C63 C76 Ag14 108(9) . . ?
C63 C76 Ag16 117(9) . . ?
Ag14 C78 Ag6 86(3) . . ?
Ag14 C78 Ag7 82(3) . . ?
Ag7 C78 Ag6 89(3) . . ?
C15 C78 Ag6 110(10) . . ?
C15 C78 Ag14 145(10) . . ?
C15 C78 Ag7 128(10) . . ?
Ag20 C80 Ag10 117(3) . . ?
Ag19 C80 Ag10 82(3) . . ?
Ag19 C80 Ag20 81(3) . . ?
C75 C80 Ag10 97(7) . . ?
C75 C80 Ag20 104(7) . . ?
C75 C80 Ag19 175(9) . . ?
Ag10 C82 Ag12 87(3) . . ?
Ag10 C82 Ag7 89(4) . . ?
Ag12 C82 Ag7 86(3) . . ?
C57 C82 Ag10 135(9) . . ?
C57 C82 Ag12 118(9) . . ?
C57 C82 Ag7 128(8) . . ?
C13 C84 Ag5 170(9) . . ?
Ag21 C86 Ag10 90(3) . . ?
Ag21 C86 Ag11 88(3) . . ?
Ag11 C86 Ag10 91(4) . . ?
C35 C86 Ag10 123(8) . . ?
C35 C86 Ag21 131(10) . . ?
C35 C86 Ag11 123(7) . . ?
C88 C90 C94 110(2) . . ?
C88 C90 C96 109(2) . . ?
C92 C90 C88 111(2) . . ?
C92 C90 C94 108(2) . . ?
C92 C90 C96 110(2) . . ?
C94 C90 C96 109(2) . . ?
C14 C96 C90 165(7) . . ?
C3 C49 C25 111(2) . . ?
C3 C49 C51 111(2) . . ?
C3 C49 C13 110(2) . . ?
C51 C49 C25 109(2) . . ?
C13 C49 C25 107(2) . . ?
C13 C49 C51 108(2) . . ?
C84 C13 C49 172(9) . . ?
C53 C27 C55 113(2) . . ?
C53 C27 C7 113(2) . . ?
C53 C27 C57 113(2) . . ?
C55 C27 C7 105(3) . . ?
C55 C27 C57 106(3) . . ?
C57 C27 C7 105(3) . . ?
C82 C57 C27 180(10) . . ?
C29 C59 C15 110(2) . . ?
C29 C59 C61 109(2) . . ?
C29 C59 C31 108(2) . . ?
C15 C59 C61 109(2) . . ?
C31 C59 C15 110(2) . . ?
C31 C59 C61 111(2) . . ?
C78 C15 C59 167(10) . . ?
C76 C63 C2 169(10) . . ?
C63 C2 C65 113(2) . . ?
C63 C2 C33 112(2) . . ?
C63 C2 C67 111(2) . . ?
C65 C2 C67 107(3) . . ?
C33 C2 C65 106(3) . . ?
C33 C2 C67 108(3) . . ?
C17 C69 C35 111(2) . . ?
C17 C69 C9 111(2) . . ?
C35 C69 C9 108(3) . . ?
C71 C69 C17 111(2) . . ?
C71 C69 C35 108(3) . . ?
C71 C69 C9 108(3) . . ?
C86 C35 C69 156(9) . . ?
C69 C9 C47 155(5) . . ?
C73 C37 C19 108(2) . . ?
C73 C37 C77 111(2) . . ?
C75 C37 C73 111(2) . . ?
C75 C37 C19 110(2) . . ?
C75 C37 C77 108(2) . . ?
C77 C37 C19 109(2) . . ?
C80 C75 C37 177(9) . . ?
Ag4 C39 Ag8 95(4) . 2_666 ?
Ag4 C39 Ag20 92(4) . . ?
Ag8 C39 Ag20 103(3) 2_666 . ?
C83 C39 Ag4 162(9) . . ?
C83 C39 Ag8 99(8) . 2_666 ?
C83 C39 Ag20 96(8) . . ?
Ag8 C79 Ag6 111(3) 2_666 2_666 ?
Ag2 C79 Ag6 81(3) . 2_666 ?
Ag2 C79 Ag8 79(3) . 2_666 ?
C45 C79 Ag6 96(7) . 2_666 ?
C45 C79 Ag8 107(7) . 2_666 ?
C45 C79 Ag2 174(9) . . ?
C5 C81 C41 109(2) . . ?
C5 C81 C83 109(2) . . ?
C5 C81 C21 109(2) . . ?
C41 C81 C83 111(2) . . ?
C21 C81 C41 109(2) . . ?
C21 C81 C83 110(2) . . ?
C39 C83 C81 176(8) . . ?
Ag20 C85 Ag15 92(2) . 2_666 ?
Ag21 C85 Ag20 87(2) . . ?
Ag21 C85 Ag15 93(3) . 2_666 ?
C93 C85 Ag20 141(8) . . ?
C93 C85 Ag15 117(7) . 2_666 ?
C93 C85 Ag21 114(7) . . ?
C43 C87 C11 112(2) . . ?
C43 C87 C89 110(2) . . ?
C43 C87 C45 110(2) . . ?
C11 C87 C89 108(2) . . ?
C11 C87 C45 108(2) . . ?
C45 C87 C89 108(2) . . ?
C79 C45 C87 173(8) . . ?
C91 C23 C47 108(2) . . ?
C91 C23 C95 107(2) . . ?
C93 C23 C91 109(2) . . ?
C93 C23 C47 111(2) . . ?
C93 C23 C95 113(2) . . ?
C95 C23 C47 109(2) . . ?
C85 C93 C23 158(8) . . ?
C23 C47 C9 158(5) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Ag4 C14 C96 C90 91(32) . . . . ?
Ag6 C78 C15 C59 163(47) . . . . ?
Ag8 Ag4 C39 Ag20 -103(4) 2_666 . . . ?
Ag8 Ag4 C39 C83 138(32) 2_666 . . . ?
Ag8 C76 C63 C2 -73(57) . . . . ?
Ag10 C86 C35 C69 -103(22) . . . . ?
Ag12 C6 C22 C18 92(31) . . . . ?
Ag14 C76 C63 C2 169(46) . . . . ?
Ag14 C78 C15 C59 -84(53) . . . . ?
Ag16 C76 C63 C2 75(53) . . . . ?
Ag18 Ag4 C39 Ag8 123(4) . . . 2_666 ?
Ag18 Ag4 C39 Ag20 20(6) . . . . ?
Ag18 Ag4 C39 C83 -98(30) . . . . ?
Ag18 C6 C22 C18 -28(42) . . . . ?
Ag18 C14 C96 C90 -168(27) . . . . ?
Ag20 Ag4 C39 Ag8 103(4) . . . 2_666 ?
Ag20 Ag4 C39 C83 -118(32) . . . . ?
Ag20 C85 C93 C23 74(25) . . . . ?
Ag22 C12 C54 C48 170(13) . . . . ?
Ag23 Ag4 C39 Ag8 -20(6) . . . 2_666 ?
Ag23 Ag4 C39 Ag20 -123(3) . . . . ?
Ag23 Ag4 C39 C83 119(29) . . . . ?
Ag23 C14 C96 C90 -64(31) . . . . ?
Ag3 C6 C22 C18 -168(25) . . . . ?
Ag7 C78 C15 C59 59(59) . . . . ?
Ag15 C85 C93 C23 -150(16) 2_666 . . . ?
Ag21 C86 C35 C69 22(28) . . . . ?
Ag21 C85 C93 C23 -43(23) . . . . ?
Ag11 C86 C35 C69 141(16) . . . . ?
C14 Ag4 C39 Ag8 -112(11) . . . 2_666 ?
C14 Ag4 C39 Ag20 145(10) . . . . ?
C14 Ag4 C39 C83 27(38) . . . . ?
C16 C18 C22 C6 -6(32) . . . . ?
C20 C18 C22 C6 -125(32) . . . . ?
C24 C18 C22 C6 113(32) . . . . ?
C46 C48 C54 C12 67(35) . . . . ?
C50 C48 C54 C12 -171(35) . . . . ?
C52 C48 C54 C12 -53(36) . . . . ?
C76 C63 C2 C65 -14(52) . . . . ?
C76 C63 C2 C33 -133(52) . . . . ?
C76 C63 C2 C67 106(52) . . . . ?
C88 C90 C96 C14 -12(30) . . . . ?
C92 C90 C96 C14 110(30) . . . . ?
C94 C90 C96 C14 -132(30) . . . . ?
C29 C59 C15 C78 -97(52) . . . . ?
C61 C59 C15 C78 23(53) . . . . ?
C31 C59 C15 C78 144(52) . . . . ?
C17 C69 C35 C86 99(22) . . . . ?
C17 C69 C9 C47 -87(12) . . . . ?
C69 C9 C47 C23 -84(18) . . . . ?
C35 C69 C9 C47 35(13) . . . . ?
C71 C69 C35 C86 -139(21) . . . . ?
C71 C69 C9 C47 151(11) . . . . ?
C9 C69 C35 C86 -23(23) . . . . ?
C91 C23 C93 C85 -97(21) . . . . ?
C91 C23 C47 C9 180(13) . . . . ?
C93 C23 C47 C9 60(14) . . . . ?
C47 C23 C93 C85 21(22) . . . . ?
C95 C23 C93 C85 143(20) . . . . ?
C95 C23 C47 C9 -64(14) . . . . ?

_smtbx_masks_special_details     ?
loop_
_smtbx_masks_void_nr
_smtbx_masks_void_average_x
_smtbx_masks_void_average_y
_smtbx_masks_void_average_z
_smtbx_masks_void_volume
_smtbx_masks_void_count_electrons
_smtbx_masks_void_content
1 0.000 0.000 0.500 774.3 109.5 ?
2 0.195 0.875 0.185 12.1 0.0 ?
3 0.321 0.436 0.863 31.2 3.3 ?
4 0.352 0.744 0.216 11.4 0.0 ?
5 0.648 0.256 0.784 11.4 0.0 ?
6 0.679 0.564 0.137 31.2 2.4 ?
7 0.805 0.125 0.815 12.1 0.0 ?

_smtbx_masks_void_probe_radius   1.2
_smtbx_masks_void_truncation_radius 1.2
_olex2_submission_special_instructions 'No special instructions were received'
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_p-1_a
_database_code_depnum_ccdc_archive 'CCDC 2278717'
loop_
_audit_author_name
_audit_author_address
'Zhan-Guo Jiang'
;Zhejiang Normal Univesity
China
;
_audit_update_record             
;
2023-07-03 deposited with the CCDC.	2023-08-28 downloaded from the CCDC.
;
_audit_creation_date             2023-06-08
_audit_creation_method           
;
Olex2 1.5
(compiled 2021.08.20 svn.r13c46975 for OlexSys, GUI svn.r6392)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         '4(F6 Sb), C192 H288 Ag45 Cl6'
_chemical_formula_sum            'C192 H288 Ag45 Cl6 F24 Sb4'
_chemical_formula_weight         8606.06
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   19.854(4)
_cell_length_b                   20.442(4)
_cell_length_c                   20.492(4)
_cell_angle_alpha                102.885(6)
_cell_angle_beta                 116.443(5)
_cell_angle_gamma                108.691(6)
_cell_volume                     6364(2)
_cell_formula_units_Z            1
_cell_measurement_reflns_used    4101
_cell_measurement_temperature    150.00
_cell_measurement_theta_max      21.57
_cell_measurement_theta_min      2.46
_shelx_estimated_absorpt_T_max   ?
_shelx_estimated_absorpt_T_min   ?
_exptl_absorpt_coefficient_mu    3.902
_exptl_absorpt_correction_T_max  0.7449
_exptl_absorpt_correction_T_min  0.6481
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
SADABS-2016/2 (Bruker,2016/2) was used for absorption correction.
wR2(int) was 0.0876 before and 0.0638 after correction.
The Ratio of minimum to maximum transmission is 0.8700.
The λ/2 correction factor is Not present.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            yellow
_exptl_crystal_colour_primary    yellow
_exptl_crystal_density_diffrn    2.245
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             4077
_exptl_crystal_size_max          0.12
_exptl_crystal_size_mid          0.11
_exptl_crystal_size_min          0.1
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0864
_diffrn_reflns_av_unetI/netI     0.0995
_diffrn_reflns_Laue_measured_fraction_full 0.992
_diffrn_reflns_Laue_measured_fraction_max 0.992
_diffrn_reflns_limit_h_max       19
_diffrn_reflns_limit_h_min       -19
_diffrn_reflns_limit_k_max       20
_diffrn_reflns_limit_k_min       -20
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_limit_l_min       -19
_diffrn_reflns_number            35923
_diffrn_reflns_point_group_measured_fraction_full 0.992
_diffrn_reflns_point_group_measured_fraction_max 0.992
_diffrn_reflns_theta_full        20.815
_diffrn_reflns_theta_max         20.815
_diffrn_reflns_theta_min         2.241
_diffrn_ambient_temperature      150.00
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.992
_diffrn_measured_fraction_theta_max 0.992
_diffrn_measurement_device_type  'BRUKER D8 VENTURE'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_diffrn_source_current           1.4
_diffrn_source_power             0.07
_diffrn_source_voltage           50.0
_diffrn_standards_number         0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                6955
_reflns_number_total             13225
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT V8.38A (Bruker, 2018)'
_computing_data_collection       ?
_computing_data_reduction        'SAINT V8.38A (Bruker, 2018)'
_computing_molecular_graphics    'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2018/3 (Sheldrick, 2015)'
_computing_structure_solution    'SHELXT 2014/5 (Sheldrick, 2014)'
_refine_diff_density_max         3.447
_refine_diff_density_min         -2.219
_refine_diff_density_rms         0.281
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.352
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1264
_refine_ls_number_reflns         13225
_refine_ls_number_restraints     1478
_refine_ls_R_factor_all          0.2004
_refine_ls_R_factor_gt           0.1303
_refine_ls_restrained_S_all      1.285
_refine_ls_shift/su_max          0.021
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.2000P)²] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.3589
_refine_ls_wR_factor_ref         0.4174
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.5 times of:
  All C(H,H,H) groups
2. Restrained distances
 C21-C81
 2.5 with sigma of 0.02
 C77-C47
 2.5 with sigma of 0.02
 C15-C75
 1.5 with sigma of 0.02
 C57-C21
 1.5 with sigma of 0.02
 C91-C87
 1.5 with sigma of 0.02
 C6-C8
 1.23 with sigma of 0.02
 C1-C14
 1.23 with sigma of 0.02
 C56-C74
 1.23 with sigma of 0.02
3. Uiso/Uaniso restraints and constraints
C1 \\sim C2 \\sim C3 \\sim C4 \\sim C5 \\sim C6 \\sim C7 \\sim C8 \\sim C9
\\sim C10 \\sim C11 \\sim C12 \\sim C13 \\sim C14 \\sim C15 \\sim C16 \\sim C17
\\sim C18 \\sim C19 \\sim C20 \\sim C21 \\sim C22 \\sim C23 \\sim C24 \\sim C25
\\sim C26 \\sim C27 \\sim C28 \\sim C29 \\sim C30 \\sim C31 \\sim C32 \\sim C33
\\sim C34 \\sim C35 \\sim C36 \\sim C37 \\sim C38 \\sim C39 \\sim C40 \\sim C41
\\sim C42 \\sim C43 \\sim C44 \\sim C45 \\sim C46 \\sim C47 \\sim C48 \\sim C49
\\sim C50 \\sim C51 \\sim C52 \\sim C53 \\sim C54 \\sim C55 \\sim C56 \\sim C57
\\sim C58 \\sim C59 \\sim C60 \\sim C61 \\sim C62 \\sim C63 \\sim C64 \\sim C65
\\sim C66 \\sim C67 \\sim C68 \\sim C69 \\sim C70 \\sim C71 \\sim C72 \\sim C73
\\sim C74 \\sim C75 \\sim C76 \\sim C77 \\sim C78 \\sim C79 \\sim C80 \\sim C81
\\sim C82 \\sim C83 \\sim C84 \\sim C85 \\sim C86 \\sim C87 \\sim C88 \\sim C89
\\sim C90 \\sim C91 \\sim C92 \\sim C93 \\sim C94 \\sim C95 \\sim C96: within
3.8A with sigma of 0.01 and sigma for terminal atoms of 0.02 within 3.8A
F1 \\sim F4 \\sim F5 \\sim F6 \\sim F9 \\sim F12: within 2A with sigma of 0.01
and sigma for terminal atoms of 0.02 within 2A
F2 \\sim F3 \\sim F7 \\sim F8 \\sim F10 \\sim F11: within 2A with sigma of
0.001 and sigma for terminal atoms of 0.002 within 2A
4.a Riding coordinates:
 C24(H24A,H24B,H24C), C47(H47A,H47B,H47C), C53(H53A,H53B,H53C), C77(H77A,H77B,
 H77C), C81(H81A,H81B,H81C), C83(H83A,H83B,H83C)
4.b Idealised Me refined as rotating group:
 C2(H2A,H2B,H2C), C3(H3A,H3B,H3C), C5(H5A,H5B,H5C), C7(H7A,H7B,H7C), C9(H9A,
 H9B,H9C), C11(H11A,H11B,H11C), C13(H13A,H13B,H13C), C17(H17A,H17B,H17C),
 C19(H19A,H19B,H19C), C21(H21A,H21B,H21C), C23(H23A,H23B,H23C), C27(H27A,H27B,
 H27C), C29(H29A,H29B,H29C), C31(H31A,H31B,H31C), C33(H33A,H33B,H33C), C35(H35A,
 H35B,H35C), C37(H37A,H37B,H37C), C39(H39A,H39B,H39C), C41(H41A,H41B,H41C),
 C45(H45A,H45B,H45C), C49(H49A,H49B,H49C), C51(H51A,H51B,H51C), C55(H55A,H55B,
 H55C), C58(H58A,H58B,H58C), C59(H59A,H59B,H59C), C61(H61A,H61B,H61C), C63(H63A,
 H63B,H63C), C65(H65A,H65B,H65C), C67(H67A,H67B,H67C), C69(H69A,H69B,H69C),
 C75(H75A,H75B,H75C), C78(H78A,H78B,H78C), C79(H79A,H79B,H79C), C84(H84A,H84B,
 H84C), C86(H86A,H86B,H86C), C88(H88A,H88B,H88C), C89(H89A,H89B,H89C), C91(H91A,
 H91B,H91C), C93(H93A,H93B,H93C), C94(H94A,H94B,H94C), C95(H95A,H95B,H95C),
 C96(H96A,H96B,H96C)
;
_atom_sites_solution_hydrogens   mixed
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Sb1 Sb 1.0584(2) 0.16668(19) 0.73901(19) 0.0999(11) Uani 1 1 d . . . . .
F1 F 1.1761(19) 0.204(2) 0.792(2) 0.177(15) Uani 1 1 d . . . . .
F4 F 1.056(3) 0.193(2) 0.6569(18) 0.191(16) Uani 1 1 d . . . . .
F5 F 0.947(3) 0.140(5) 0.691(3) 0.38(5) Uani 1 1 d . . . . .
F6 F 1.040(2) 0.0687(15) 0.6862(18) 0.161(13) Uani 1 1 d . . . . .
F9 F 1.069(3) 0.1356(17) 0.821(2) 0.170(14) Uani 1 1 d . . . . .
F12 F 1.076(3) 0.2573(19) 0.793(2) 0.179(15) Uani 1 1 d . . . . .
Sb2 Sb 0.3402(2) -0.15627(19) 0.08208(18) 0.1044(11) Uani 1 1 d . . . . .
F2 F 0.257(4) -0.243(2) 0.065(3) 0.27(3) Uani 1 1 d . . . . .
F3 F 0.341(3) -0.105(2) 0.1701(19) 0.200(17) Uani 1 1 d . . . . .
F7 F 0.409(3) -0.067(3) 0.092(3) 0.22(2) Uani 1 1 d . . . . .
F8 F 0.260(2) -0.133(2) 0.020(2) 0.178(14) Uani 1 1 d . . . . .
F10 F 0.334(3) -0.216(2) -0.005(2) 0.206(18) Uani 1 1 d . . . . .
F11 F 0.432(5) -0.170(4) 0.144(5) 0.62(10) Uani 1 1 d . . . . .
Ag1 Ag 0.500000 0.500000 0.500000 0.0511(9) Uani 1 2 d S . P . .
Ag2 Ag 0.6013(3) 0.4130(2) 0.3026(3) 0.1334(17) Uani 1 1 d . . . . .
Ag3 Ag 0.6877(3) 0.3988(3) 0.6784(3) 0.1255(16) Uani 1 1 d . . . . .
Ag4 Ag 0.2362(2) 0.28051(17) 0.18440(18) 0.0800(10) Uani 1 1 d . . . . .
Ag5 Ag 0.7925(3) 0.4855(2) 0.6307(4) 0.150(2) Uani 1 1 d . . . . .
Ag6 Ag 0.4185(2) 0.2993(2) 0.22235(19) 0.0991(12) Uani 1 1 d . . . . .
Ag7 Ag 0.4459(3) 0.4519(3) 0.3236(2) 0.1257(15) Uani 1 1 d . . . . .
Ag8 Ag 0.2195(2) 0.26644(18) 0.4485(2) 0.0955(11) Uani 1 1 d . . . . .
Ag9 Ag 0.3323(4) 0.2012(2) 0.4537(3) 0.1408(19) Uani 1 1 d . . . . .
Ag10 Ag 0.4772(2) 0.2223(2) 0.4301(3) 0.1064(13) Uani 1 1 d . . . . .
Ag11 Ag 0.8386(3) 0.6228(4) 0.5998(3) 0.161(2) Uani 1 1 d . . . . .
Ag12 Ag 0.5423(3) 0.5293(2) 0.2658(2) 0.0986(11) Uani 1 1 d . . . . .
Ag13 Ag 0.5637(3) 0.3986(3) 0.7286(3) 0.1335(16) Uani 1 1 d . . . . .
Ag14 Ag 0.7235(3) 0.56450(18) 0.8030(2) 0.1178(15) Uani 1 1 d . . . . .
Ag15 Ag 0.5020(3) 0.3680(2) 0.5431(2) 0.1263(16) Uani 1 1 d . . . . .
Ag16 Ag 0.3104(3) 0.20866(19) 0.2999(2) 0.1317(18) Uani 1 1 d . . . . .
Ag17 Ag 0.7345(3) 0.5855(3) 0.4272(2) 0.1303(16) Uani 1 1 d . . . . .
Ag18 Ag 0.3727(3) 0.3036(2) 0.6174(2) 0.1166(14) Uani 1 1 d . . . . .
Ag19 Ag 0.8336(3) 0.6428(3) 0.7458(2) 0.164(2) Uani 1 1 d . . . . .
Ag20 Ag 0.6259(3) 0.4646(3) 0.4792(3) 0.1211(14) Uani 1 1 d . . . . .
Ag21 Ag 0.6651(3) 0.3277(3) 0.5254(2) 0.167(2) Uani 1 1 d . . . . .
Ag22 Ag 0.3156(2) 0.3535(2) 0.3870(2) 0.1183(14) Uani 1 1 d . . . . .
Ag23 Ag 0.5574(3) 0.2877(3) 0.3485(2) 0.1259(16) Uani 1 1 d . . . . .
Cl1 Cl 0.6486(6) 0.5154(5) 0.6272(5) 0.065(2) Uani 1 1 d . . . . .
Cl2 Cl 0.4592(6) 0.3574(5) 0.3942(5) 0.073(3) Uani 1 1 d . . . . .
Cl3 Cl 0.3992(6) 0.4191(5) 0.5521(5) 0.069(2) Uani 1 1 d . . . . .
C1 C 0.692(2) 0.448(2) 0.792(2) 0.076(6) Uani 1 1 d D U . . .
C2 C 1.026(3) 0.736(3) 0.500(3) 0.108(9) Uani 1 1 d . U . . .
H2A H 1.039090 0.695001 0.507691 0.162 Uiso 1 1 calc R U . . .
H2B H 1.073162 0.775774 0.504463 0.162 Uiso 1 1 calc R U . . .
H2C H 0.972974 0.715225 0.447090 0.162 Uiso 1 1 calc R U . . .
C3 C 0.917(3) 0.519(2) 0.911(3) 0.093(8) Uani 1 1 d . U . . .
H3A H 0.972289 0.539847 0.962606 0.140 Uiso 1 1 calc R U . . .
H3B H 0.907592 0.560738 0.901398 0.140 Uiso 1 1 calc R U . . .
H3C H 0.918788 0.489325 0.867255 0.140 Uiso 1 1 calc R U . . .
C4 C 0.535(3) 0.241(2) 0.608(2) 0.080(7) Uani 1 1 d . U . . .
C5 C 0.624(3) 0.081(3) 0.425(3) 0.117(9) Uani 1 1 d . U . . .
H5A H 0.680984 0.113557 0.474797 0.175 Uiso 1 1 calc R U . . .
H5B H 0.616803 0.029639 0.401799 0.175 Uiso 1 1 calc R U . . .
H5C H 0.580066 0.076917 0.435967 0.175 Uiso 1 1 calc R U . . .
C6 C 0.309(3) 0.0706(18) 0.344(2) 0.087(7) Uani 1 1 d D U . . .
C7 C 0.848(3) 0.478(3) 0.406(3) 0.111(9) Uani 1 1 d . U . . .
H7A H 0.795512 0.477886 0.370314 0.166 Uiso 1 1 calc R U . . .
H7B H 0.866285 0.454887 0.373183 0.166 Uiso 1 1 calc R U . . .
H7C H 0.893722 0.530074 0.444878 0.166 Uiso 1 1 calc R U . . .
C8 C 0.344(3) 0.1371(18) 0.358(2) 0.084(6) Uani 1 1 d D U . . .
C9 C 0.195(3) 0.008(2) 0.083(3) 0.108(9) Uani 1 1 d . U . . .
H9A H 0.143146 0.006896 0.043945 0.161 Uiso 1 1 calc R U . . .
H9B H 0.197429 0.013871 0.133282 0.161 Uiso 1 1 calc R U . . .
H9C H 0.194102 -0.040701 0.061211 0.161 Uiso 1 1 calc R U . . .
C10 C 0.146(2) 0.3282(19) 0.137(2) 0.072(7) Uani 1 1 d . U . . .
C11 C 0.268(3) 0.378(3) 0.000(2) 0.103(9) Uani 1 1 d . U . . .
H11A H 0.226850 0.370290 0.015647 0.155 Uiso 1 1 calc R U . . .
H11B H 0.237129 0.350414 -0.058369 0.155 Uiso 1 1 calc R U . . .
H11C H 0.301979 0.432585 0.017432 0.155 Uiso 1 1 calc R U . . .
C12 C 0.887(3) 0.320(2) 0.697(2) 0.076(7) Uani 1 1 d . U . . .
C13 C 0.870(3) 0.508(2) 0.992(2) 0.091(8) Uani 1 1 d . U . . .
H13A H 0.865909 0.475203 1.019203 0.137 Uiso 1 1 calc R U . . .
H13B H 0.831928 0.530742 0.988941 0.137 Uiso 1 1 calc R U . . .
H13C H 0.928811 0.549458 1.021665 0.137 Uiso 1 1 calc R U . . .
C14 C 0.759(2) 0.456(2) 0.846(2) 0.083(7) Uani 1 1 d D U . . .
C15 C 0.506(3) 0.340(3) 0.873(3) 0.109(8) Uani 1 1 d D U . . .
C16 C 0.286(3) 0.149(2) 0.149(3) 0.092(7) Uani 1 1 d . U . . .
C17 C 0.364(3) 0.074(3) 0.164(3) 0.112(9) Uani 1 1 d . U . . .
H17A H 0.380664 0.047953 0.132033 0.168 Uiso 1 1 calc R U . . .
H17B H 0.351203 0.046098 0.192984 0.168 Uiso 1 1 calc R U . . .
H17C H 0.411536 0.126250 0.202085 0.168 Uiso 1 1 calc R U . . .
C18 C 0.282(3) 0.207(2) 0.177(3) 0.094(7) Uani 1 1 d . U . . .
C19 C 0.603(4) 0.346(3) 0.916(3) 0.129(10) Uani 1 1 d . U . . .
H19A H 0.645659 0.395582 0.928179 0.194 Uiso 1 1 calc R U . . .
H19B H 0.602116 0.304866 0.879475 0.194 Uiso 1 1 calc R U . . .
H19C H 0.619369 0.340365 0.966791 0.194 Uiso 1 1 calc R U . . .
C20 C 0.905(3) 0.605(2) 0.701(2) 0.080(7) Uani 1 1 d . U . . .
C21 C 0.119(3) 0.048(3) 0.506(2) 0.138(10) Uani 1 1 d D U . . .
H21A H 0.093507 0.028079 0.533581 0.207 Uiso 1 1 calc R U . . .
H21B H 0.114982 0.006459 0.467800 0.207 Uiso 1 1 calc R U . . .
H21C H 0.088708 0.072517 0.477825 0.207 Uiso 1 1 calc R U . . .
C22 C 0.549(3) 0.187(2) 0.636(2) 0.082(7) Uani 1 1 d . U . . .
C23 C 0.487(3) 0.200(3) 0.037(3) 0.125(9) Uani 1 1 d . U . . .
H23A H 0.442059 0.155994 0.030556 0.187 Uiso 1 1 calc R U . . .
H23B H 0.502704 0.183695 -0.000115 0.187 Uiso 1 1 calc R U . . .
H23C H 0.466856 0.236875 0.026425 0.187 Uiso 1 1 calc R U . . .
C24 C -0.062(3) 0.210(2) -0.015(2) 0.090(8) Uani 1 1 d . U . . .
H24A H -0.101725 0.223510 -0.049901 0.135 Uiso 1 1 d R U . . .
H24B H -0.052885 0.229990 0.037979 0.135 Uiso 1 1 d R U . . .
H24C H -0.099165 0.154770 -0.043001 0.135 Uiso 1 1 d R U . . .
C25 C 0.768(3) 0.435(3) 0.459(2) 0.087(7) Uani 1 1 d . U . . .
C26 C 0.978(3) 0.619(2) 0.751(2) 0.083(7) Uani 1 1 d . U . . .
C27 C 1.081(3) 0.626(2) 0.872(2) 0.096(8) Uani 1 1 d . U . . .
H27A H 1.042567 0.634553 0.886959 0.143 Uiso 1 1 calc R U . . .
H27B H 1.140646 0.661560 0.917414 0.143 Uiso 1 1 calc R U . . .
H27C H 1.069950 0.573547 0.859519 0.143 Uiso 1 1 calc R U . . .
C28 C 0.527(3) 0.280(3) 0.232(3) 0.104(7) Uani 1 1 d . U . . .
C29 C 0.843(3) 0.249(2) 0.700(3) 0.099(9) Uani 1 1 d . U . . .
H29A H 0.793955 0.210930 0.645293 0.148 Uiso 1 1 calc R U . . .
H29B H 0.822672 0.258678 0.734902 0.148 Uiso 1 1 calc R U . . .
H29C H 0.883125 0.229307 0.721402 0.148 Uiso 1 1 calc R U . . .
C30 C 0.615(3) 0.110(2) 0.373(2) 0.083(7) Uani 1 1 d . U . . .
C31 C 1.087(3) 0.589(3) 0.760(3) 0.108(9) Uani 1 1 d . U . . .
H31A H 1.035170 0.541070 0.717549 0.162 Uiso 1 1 calc R U . . .
H31B H 1.128352 0.578581 0.798811 0.162 Uiso 1 1 calc R U . . .
H31C H 1.113176 0.614697 0.735124 0.162 Uiso 1 1 calc R U . . .
C32 C 0.414(3) 0.422(3) 0.206(2) 0.093(7) Uani 1 1 d . U . . .
C33 C 0.278(3) 0.079(3) 0.028(3) 0.113(9) Uani 1 1 d . U . . .
H33A H 0.334836 0.115542 0.044239 0.170 Uiso 1 1 calc R U . . .
H33B H 0.235881 0.094463 -0.001637 0.170 Uiso 1 1 calc R U . . .
H33C H 0.261669 0.027809 -0.006857 0.170 Uiso 1 1 calc R U . . .
C34 C 0.269(3) -0.012(2) 0.329(2) 0.085(7) Uani 1 1 d . U . . .
C35 C 0.485(3) 0.159(2) 0.654(2) 0.100(9) Uani 1 1 d . U . . .
H35A H 0.464468 0.195606 0.661632 0.150 Uiso 1 1 calc R U . . .
H35B H 0.511347 0.152009 0.703613 0.150 Uiso 1 1 calc R U . . .
H35C H 0.436909 0.109609 0.609244 0.150 Uiso 1 1 calc R U . . .
C36 C 0.381(3) 0.389(3) 0.134(2) 0.095(7) Uani 1 1 d . U . . .
C37 C 0.529(4) 0.408(3) 0.947(3) 0.125(10) Uani 1 1 d . U . . .
H37A H 0.477630 0.398668 0.947294 0.187 Uiso 1 1 calc R U . . .
H37B H 0.550607 0.455762 0.942599 0.187 Uiso 1 1 calc R U . . .
H37C H 0.573283 0.411167 0.997334 0.187 Uiso 1 1 calc R U . . .
C38 C 0.518(3) 0.282(2) 0.573(2) 0.085(6) Uani 1 1 d . U . . .
C39 C 0.793(3) 0.336(2) 0.402(3) 0.104(8) Uani 1 1 d . U . . .
H39A H 0.784112 0.309655 0.433745 0.156 Uiso 1 1 calc R U . . .
H39B H 0.834273 0.327365 0.391284 0.156 Uiso 1 1 calc R U . . .
H39C H 0.738759 0.315745 0.350019 0.156 Uiso 1 1 calc R U . . .
C40 C 0.138(3) 0.188(2) 0.273(2) 0.084(7) Uani 1 1 d . U . . .
C41 C 0.692(3) 0.134(3) 0.369(3) 0.115(8) Uani 1 1 d . U . . .
H41A H 0.682471 0.150669 0.326118 0.172 Uiso 1 1 calc R U . . .
H41B H 0.703196 0.090662 0.358608 0.172 Uiso 1 1 calc R U . . .
H41C H 0.742062 0.176411 0.421153 0.172 Uiso 1 1 calc R U . . .
C42 C 0.550(3) 0.265(3) 0.190(3) 0.106(8) Uani 1 1 d . U . . .
C43 C 0.576(3) 0.244(3) 0.135(3) 0.108(8) Uani 1 1 d . U . . .
C44 C 0.598(3) 0.171(2) 0.396(2) 0.083(7) Uani 1 1 d . U . . .
C45 C 0.612(3) 0.309(3) 0.117(3) 0.123(9) Uani 1 1 d . U . . .
H45A H 0.591173 0.345087 0.127943 0.185 Uiso 1 1 calc R U . . .
H45B H 0.592743 0.289246 0.060725 0.185 Uiso 1 1 calc R U . . .
H45C H 0.674568 0.335034 0.152235 0.185 Uiso 1 1 calc R U . . .
C46 C 0.778(2) 0.383(2) 0.651(2) 0.072(7) Uani 1 1 d . U . . .
C47 C 0.689(3) 0.508(3) 0.136(3) 0.149(10) Uani 1 1 d D U . . .
H47A H 0.726146 0.504107 0.115863 0.224 Uiso 1 1 d R U . . .
H47B H 0.653046 0.516817 0.091763 0.224 Uiso 1 1 d R U . . .
H47C H 0.655806 0.456457 0.129653 0.224 Uiso 1 1 d R U . . .
C48 C 0.922(3) 0.715(3) 0.538(3) 0.107(8) Uani 1 1 d . U . . .
C49 C 0.262(3) -0.015(2) 0.403(2) 0.105(9) Uani 1 1 d . U . . .
H49A H 0.202132 -0.035613 0.385506 0.158 Uiso 1 1 calc R U . . .
H49B H 0.296303 0.036412 0.446958 0.158 Uiso 1 1 calc R U . . .
H49C H 0.284197 -0.048521 0.421749 0.158 Uiso 1 1 calc R U . . .
C50 C 0.239(3) 0.157(3) 0.539(3) 0.114(9) Uani 1 1 d . U . . .
C51 C 0.910(3) 0.303(2) 0.631(2) 0.098(8) Uani 1 1 d . U . . .
H51A H 0.935801 0.350700 0.627263 0.147 Uiso 1 1 calc R U . . .
H51B H 0.857599 0.265253 0.578273 0.147 Uiso 1 1 calc R U . . .
H51C H 0.950725 0.283427 0.647664 0.147 Uiso 1 1 calc R U . . .
C52 C 0.201(3) 0.252(2) 0.319(2) 0.090(7) Uani 1 1 d . U . . .
C53 C 0.003(3) 0.268(2) -0.070(2) 0.089(8) Uani 1 1 d . U . . .
H53A H 0.039048 0.323590 -0.039238 0.133 Uiso 1 1 d R U . . .
H53B H -0.052952 0.256220 -0.111588 0.133 Uiso 1 1 d R U . . .
H53C H 0.021088 0.248800 -0.104318 0.133 Uiso 1 1 d R U . . .
C54 C 1.015(3) 0.768(3) 0.560(3) 0.103(8) Uani 1 1 d . U . . .
C55 C 1.117(3) 0.731(2) 0.830(3) 0.102(9) Uani 1 1 d . U . . .
H55A H 1.120516 0.738682 0.785393 0.153 Uiso 1 1 calc R U . . .
H55B H 1.175447 0.752021 0.877288 0.153 Uiso 1 1 calc R U . . .
H55C H 1.087851 0.756281 0.842570 0.153 Uiso 1 1 calc R U . . .
C56 C 0.658(3) 0.510(3) 0.292(3) 0.127(9) Uani 1 1 d D U . . .
C57 C 0.211(3) 0.106(3) 0.567(3) 0.112(9) Uani 1 1 d D U . . .
C58 C 0.630(3) 0.218(2) 0.713(2) 0.089(8) Uani 1 1 d . U . . .
H58A H 0.677750 0.241404 0.707702 0.133 Uiso 1 1 calc R U . . .
H58B H 0.632982 0.177091 0.728993 0.133 Uiso 1 1 calc R U . . .
H58C H 0.634080 0.257531 0.754468 0.133 Uiso 1 1 calc R U . . .
C59 C 0.916(3) 0.452(3) 0.536(3) 0.111(9) Uani 1 1 d . U . . .
H59A H 0.957200 0.505949 0.557983 0.166 Uiso 1 1 calc R U . . .
H59B H 0.941258 0.419898 0.527695 0.166 Uiso 1 1 calc R U . . .
H59C H 0.899751 0.444591 0.573541 0.166 Uiso 1 1 calc R U . . .
C60 C 0.582(3) 0.219(2) 0.416(2) 0.088(7) Uani 1 1 d . U . . .
C61 C 0.183(3) -0.059(2) 0.253(2) 0.105(9) Uani 1 1 d . U . . .
H61A H 0.161309 -0.112503 0.243593 0.158 Uiso 1 1 calc R U . . .
H61B H 0.186057 -0.053489 0.207986 0.158 Uiso 1 1 calc R U . . .
H61C H 0.143555 -0.041202 0.256982 0.158 Uiso 1 1 calc R U . . .
C62 C 0.844(3) 0.466(2) 0.914(2) 0.086(7) Uani 1 1 d . U . . .
C63 C 0.962(3) 0.372(2) 0.775(2) 0.100(9) Uani 1 1 d . U . . .
H63A H 1.001821 0.350871 0.788425 0.150 Uiso 1 1 calc R U . . .
H63B H 0.947160 0.378527 0.814589 0.150 Uiso 1 1 calc R U . . .
H63C H 0.988763 0.421130 0.774797 0.150 Uiso 1 1 calc R U . . .
C64 C 0.048(3) 0.115(2) 0.216(3) 0.092(7) Uani 1 1 d . U . . .
C65 C 1.032(3) 0.843(3) 0.582(3) 0.120(10) Uani 1 1 d . U . . .
H65A H 0.981749 0.846682 0.574465 0.180 Uiso 1 1 calc R U . . .
H65B H 1.047853 0.862096 0.547996 0.180 Uiso 1 1 calc R U . . .
H65C H 1.080452 0.873786 0.638684 0.180 Uiso 1 1 calc R U . . .
C66 C 0.268(3) 0.196(3) 0.509(3) 0.114(9) Uani 1 1 d . U . . .
C67 C 0.324(3) -0.047(2) 0.323(3) 0.110(9) Uani 1 1 d . U . . .
H67A H 0.382067 -0.017127 0.372587 0.164 Uiso 1 1 calc R U . . .
H67B H 0.327585 -0.045526 0.276747 0.164 Uiso 1 1 calc R U . . .
H67C H 0.298872 -0.099779 0.315212 0.164 Uiso 1 1 calc R U . . .
C68 C 0.832(3) 0.429(3) 0.452(2) 0.090(7) Uani 1 1 d . U . . .
C69 C 0.041(3) 0.068(2) 0.267(2) 0.094(8) Uani 1 1 d . U . . .
H69A H 0.096094 0.092248 0.319336 0.141 Uiso 1 1 calc R U . . .
H69B H 0.026409 0.015465 0.237392 0.141 Uiso 1 1 calc R U . . .
H69C H -0.003768 0.067279 0.275974 0.141 Uiso 1 1 calc R U . . .
C70 C 0.856(3) 0.678(3) 0.527(3) 0.111(8) Uani 1 1 d . U . . .
C71 C 0.089(2) 0.2813(18) 0.068(2) 0.068(6) Uani 1 1 d . U . . .
C72 C 0.480(4) 0.345(3) 0.806(3) 0.114(9) Uani 1 1 d . U . . .
C73 C 0.826(3) 0.353(2) 0.673(2) 0.084(7) Uani 1 1 d . U . . .
C74 C 0.705(3) 0.549(3) 0.277(4) 0.133(9) Uani 1 1 d D U . . .
C75 C 0.445(3) 0.261(3) 0.851(3) 0.133(10) Uani 1 1 d D U . . .
H75A H 0.474734 0.242305 0.888973 0.200 Uiso 1 1 calc R U . . .
H75B H 0.424711 0.227140 0.796090 0.200 Uiso 1 1 calc R U . . .
H75C H 0.396563 0.260327 0.852184 0.200 Uiso 1 1 calc R U . . .
C76 C 1.065(3) 0.641(2) 0.803(3) 0.088(7) Uani 1 1 d . U . . .
C77 C 0.832(3) 0.581(3) 0.267(3) 0.148(10) Uani 1 1 d D U . . .
H77A H 0.837233 0.545632 0.291956 0.223 Uiso 1 1 d R U . . .
H77B H 0.877653 0.633282 0.307016 0.223 Uiso 1 1 d R U . . .
H77C H 0.854933 0.573381 0.232426 0.223 Uiso 1 1 d R U . . .
C78 C 0.019(2) 0.1538(19) -0.037(2) 0.082(8) Uani 1 1 d . U . . .
H78A H -0.032102 0.119080 -0.091800 0.124 Uiso 1 1 calc R U . . .
H78B H 0.022006 0.128934 -0.001173 0.124 Uiso 1 1 calc R U . . .
H78C H 0.070452 0.166570 -0.038778 0.124 Uiso 1 1 calc R U . . .
C79 C 0.528(3) 0.042(3) 0.301(3) 0.121(9) Uani 1 1 d . U . . .
H79A H 0.482656 0.044673 0.306757 0.182 Uiso 1 1 calc R U . . .
H79B H 0.528927 -0.005594 0.301017 0.182 Uiso 1 1 calc R U . . .
H79C H 0.518485 0.044186 0.250561 0.182 Uiso 1 1 calc R U . . .
C80 C 0.016(2) 0.2277(19) -0.006(2) 0.071(6) Uani 1 1 d . U . . .
C81 C 0.203(3) 0.160(3) 0.640(3) 0.139(10) Uani 1 1 d D U . . .
H81A H 0.244011 0.213903 0.664216 0.208 Uiso 1 1 d R U . . .
H81B H 0.215431 0.141483 0.682726 0.208 Uiso 1 1 d R U . . .
H81C H 0.144501 0.153283 0.615986 0.208 Uiso 1 1 d R U . . .
C82 C 0.452(3) 0.360(3) 0.741(3) 0.107(8) Uani 1 1 d . U . . .
C83 C 0.246(4) 0.068(3) 0.601(3) 0.140(10) Uani 1 1 d . U . . .
H83A H 0.211746 0.013934 0.561756 0.209 Uiso 1 1 d R U . . .
H83B H 0.248136 0.072324 0.650456 0.209 Uiso 1 1 d R U . . .
H83C H 0.304576 0.087714 0.613566 0.209 Uiso 1 1 d R U . . .
C84 C 0.062(3) 0.070(2) 0.152(2) 0.098(9) Uani 1 1 d . U . . .
H84A H 0.110720 0.105994 0.155048 0.147 Uiso 1 1 calc R U . . .
H84B H 0.009937 0.047426 0.097656 0.147 Uiso 1 1 calc R U . . .
H84C H 0.072629 0.029867 0.165032 0.147 Uiso 1 1 calc R U . . .
C85 C 0.746(4) 0.578(3) 0.237(4) 0.134(9) Uani 1 1 d . U . . .
C86 C 1.085(3) 0.773(3) 0.637(3) 0.116(9) Uani 1 1 d . U . . .
H86A H 1.087294 0.801934 0.683510 0.174 Uiso 1 1 calc R U . . .
H86B H 1.140473 0.798016 0.644042 0.174 Uiso 1 1 calc R U . . .
H86C H 1.072582 0.720845 0.632935 0.174 Uiso 1 1 calc R U . . .
C87 C 0.326(3) 0.348(3) 0.040(2) 0.092(7) Uani 1 1 d D U . . .
C88 C 0.837(3) 0.383(2) 0.900(2) 0.094(8) Uani 1 1 d . U . . .
H88A H 0.776946 0.343737 0.863661 0.141 Uiso 1 1 calc R U . . .
H88B H 0.861831 0.380319 0.952363 0.141 Uiso 1 1 calc R U . . .
H88C H 0.869099 0.375290 0.876883 0.141 Uiso 1 1 calc R U . . .
C89 C 0.618(3) 0.193(3) 0.161(3) 0.123(9) Uani 1 1 d . U . . .
H89A H 0.626395 0.193972 0.211970 0.184 Uiso 1 1 calc R U . . .
H89B H 0.673976 0.212037 0.167350 0.184 Uiso 1 1 calc R U . . .
H89C H 0.580548 0.139661 0.118885 0.184 Uiso 1 1 calc R U . . .
C90 C 0.279(3) 0.079(2) 0.103(3) 0.098(7) Uani 1 1 d . U . . .
C91 C 0.394(3) 0.366(3) 0.024(3) 0.118(9) Uani 1 1 d D U . . .
H91A H 0.426714 0.421068 0.044212 0.177 Uiso 1 1 calc R U . . .
H91B H 0.366622 0.341293 -0.034858 0.177 Uiso 1 1 calc R U . . .
H91C H 0.431728 0.345841 0.050190 0.177 Uiso 1 1 calc R U . . .
C92 C 0.718(3) 0.445(3) 0.471(2) 0.091(7) Uani 1 1 d . U . . .
C93 C 0.271(3) 0.264(3) 0.007(2) 0.116(9) Uani 1 1 d . U . . .
H93A H 0.282719 0.248578 0.050811 0.174 Uiso 1 1 calc R U . . .
H93B H 0.282524 0.236687 -0.029166 0.174 Uiso 1 1 calc R U . . .
H93C H 0.210226 0.251535 -0.024103 0.174 Uiso 1 1 calc R U . . .
C94 C -0.017(3) 0.132(2) 0.184(2) 0.097(9) Uani 1 1 d . U . . .
H94A H 0.006135 0.187296 0.200075 0.145 Uiso 1 1 calc R U . . .
H94B H -0.053510 0.116195 0.204154 0.145 Uiso 1 1 calc R U . . .
H94C H -0.052095 0.104682 0.125008 0.145 Uiso 1 1 calc R U . . .
C95 C 0.738(4) 0.638(3) 0.230(4) 0.146(10) Uani 1 1 d . U . . .
H95A H 0.778283 0.682675 0.282961 0.219 Uiso 1 1 calc R U . . .
H95B H 0.679480 0.627808 0.210680 0.219 Uiso 1 1 calc R U . . .
H95C H 0.751616 0.648652 0.191738 0.219 Uiso 1 1 calc R U . . .
C96 C 0.527(3) 0.119(2) 0.570(2) 0.097(8) Uani 1 1 d . U . . .
H96A H 0.468381 0.098614 0.522925 0.146 Uiso 1 1 calc R U . . .
H96B H 0.529847 0.079045 0.588883 0.146 Uiso 1 1 calc R U . . .
H96C H 0.567372 0.132689 0.554147 0.146 Uiso 1 1 calc R U . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Sb1 F1 1.86(3) . ?
Sb1 F4 1.86(3) . ?
Sb1 F5 1.80(4) . ?
Sb1 F6 1.88(2) . ?
Sb1 F9 1.88(3) . ?
Sb1 F12 1.77(3) . ?
Sb2 F2 1.83(4) . ?
Sb2 F3 1.86(3) . ?
Sb2 F7 1.80(4) . ?
Sb2 F8 1.83(3) . ?
Sb2 F10 1.85(3) . ?
Sb2 F11 1.84(6) . ?
Ag1 Ag7 3.077(3) 2_666 ?
Ag1 Ag7 3.077(3) . ?
Ag1 Ag15 3.026(3) . ?
Ag1 Ag15 3.026(3) 2_666 ?
Ag1 Ag20 2.987(3) 2_666 ?
Ag1 Ag20 2.987(3) . ?
Ag1 Cl1 2.790(9) 2_666 ?
Ag1 Cl1 2.790(9) . ?
Ag1 Cl2 2.820(9) . ?
Ag1 Cl2 2.820(9) 2_666 ?
Ag1 Cl3 2.906(9) . ?
Ag1 Cl3 2.906(9) 2_666 ?
Ag2 Ag6 2.975(6) . ?
Ag2 Ag12 3.064(5) . ?
Ag2 Ag17 3.152(6) . ?
Ag2 Ag20 3.292(6) . ?
Ag2 Ag23 2.929(5) . ?
Ag2 C28 2.33(5) . ?
Ag2 C56 2.05(4) . ?
Ag3 Ag5 2.939(6) . ?
Ag3 Ag13 3.061(6) . ?
Ag3 Ag15 3.210(6) . ?
Ag3 Ag21 2.906(6) . ?
Ag3 C1 2.26(4) . ?
Ag3 C46 2.20(4) . ?
Ag4 Ag6 3.212(5) . ?
Ag4 Ag14 2.928(4) 2_666 ?
Ag4 Ag16 3.123(4) . ?
Ag4 Ag19 2.931(5) 2_666 ?
Ag4 C10 2.26(4) . ?
Ag4 C18 2.01(4) . ?
Ag5 Ag11 2.962(7) . ?
Ag5 Ag19 3.128(7) . ?
Ag5 Ag20 3.180(7) . ?
Ag5 Ag21 2.875(7) . ?
Ag5 C20 2.26(4) . ?
Ag5 C46 2.19(4) . ?
Ag5 C92 2.70(4) . ?
Ag6 Ag7 3.058(5) . ?
Ag6 Ag23 2.947(5) . ?
Ag6 C18 2.34(4) . ?
Ag6 C28 2.24(4) . ?
Ag6 C32 2.63(4) . ?
Ag7 Ag12 2.914(6) . ?
Ag7 Ag14 3.045(6) 2_666 ?
Ag7 Cl1 2.678(10) 2_666 ?
Ag7 Cl2 2.669(10) . ?
Ag7 Cl3 2.781(10) 2_666 ?
Ag7 C32 2.09(4) . ?
Ag8 Ag9 2.928(5) . ?
Ag8 Ag11 3.016(6) 2_666 ?
Ag8 Ag17 3.034(5) 2_666 ?
Ag8 Ag18 3.127(5) . ?
Ag8 Ag22 3.059(5) . ?
Ag8 C52 2.46(4) . ?
Ag8 C66 2.28(5) . ?
Ag8 C70 2.29(4) 2_666 ?
Ag9 Ag10 3.039(5) . ?
Ag9 Ag15 3.270(7) . ?
Ag9 Ag16 3.031(6) . ?
Ag9 Ag18 3.111(6) . ?
Ag9 C8 2.25(4) . ?
Ag9 C66 2.04(4) . ?
Ag10 Ag15 3.074(5) . ?
Ag10 Ag16 3.062(6) . ?
Ag10 Ag21 2.976(6) . ?
Ag10 Ag23 3.019(5) . ?
Ag10 C8 2.15(4) . ?
Ag10 C38 2.52(4) . ?
Ag10 C60 2.24(4) . ?
Ag11 Ag17 2.939(6) . ?
Ag11 Ag19 2.978(6) . ?
Ag11 Ag22 3.363(7) 2_666 ?
Ag11 C20 2.10(4) . ?
Ag11 C70 2.15(5) . ?
Ag12 Ag13 2.958(6) 2_666 ?
Ag12 Ag17 3.328(6) . ?
Ag12 Ag18 3.051(5) 2_666 ?
Ag12 C32 2.29(5) . ?
Ag12 C56 2.30(5) . ?
Ag12 C82 2.27(4) 2_666 ?
Ag13 Ag14 3.222(5) . ?
Ag13 Ag15 3.262(6) . ?
Ag13 Ag18 2.992(6) . ?
Ag13 C1 2.00(4) . ?
Ag13 C82 2.26(5) . ?
Ag14 Ag19 3.098(7) . ?
Ag14 C1 2.20(4) . ?
Ag14 C10 2.32(4) 2_666 ?
Ag15 Cl1 2.849(9) . ?
Ag15 Cl2 2.712(9) . ?
Ag15 Cl3 2.627(10) . ?
Ag15 C38 2.05(4) . ?
Ag16 Ag22 3.042(6) . ?
Ag16 Cl2 2.872(10) . ?
Ag16 C8 2.17(3) . ?
Ag16 C18 2.31(4) . ?
Ag17 Cl3 2.847(10) 2_666 ?
Ag17 C56 2.28(6) . ?
Ag17 C70 2.13(5) . ?
Ag18 C66 2.21(5) . ?
Ag18 C82 2.05(5) . ?
Ag19 Ag22 3.040(6) 2_666 ?
Ag19 C10 2.14(4) 2_666 ?
Ag19 C20 2.24(4) . ?
Ag20 Ag21 3.355(7) . ?
Ag20 Ag23 3.374(6) . ?
Ag20 Cl1 2.748(9) . ?
Ag20 Cl2 2.702(10) . ?
Ag20 Cl3 2.734(10) 2_666 ?
Ag20 C92 2.06(4) . ?
Ag21 Ag23 3.006(6) . ?
Ag21 C46 2.20(4) . ?
Ag21 C60 2.20(4) . ?
Ag22 Cl1 2.661(10) 2_666 ?
Ag22 Cl2 2.763(11) . ?
Ag22 Cl3 2.747(9) . ?
Ag22 C52 2.06(4) . ?
Ag23 C28 2.14(4) . ?
Ag23 C60 2.21(4) . ?
C1 C14 1.216(19) . ?
C2 H2A 0.9800 . ?
C2 H2B 0.9800 . ?
C2 H2C 0.9800 . ?
C2 C54 1.39(5) . ?
C3 H3A 0.9800 . ?
C3 H3B 0.9800 . ?
C3 H3C 0.9800 . ?
C3 C62 1.55(6) . ?
C4 C22 1.39(5) . ?
C4 C38 1.25(5) . ?
C5 H5A 0.9800 . ?
C5 H5B 0.9800 . ?
C5 H5C 0.9800 . ?
C5 C30 1.31(5) . ?
C6 C8 1.209(19) . ?
C6 C34 1.50(5) . ?
C7 H7A 0.9800 . ?
C7 H7B 0.9800 . ?
C7 H7C 0.9800 . ?
C7 C68 1.57(6) . ?
C9 H9A 0.9800 . ?
C9 H9B 0.9800 . ?
C9 H9C 0.9800 . ?
C9 C90 1.63(6) . ?
C10 C71 1.21(4) . ?
C11 H11A 0.9800 . ?
C11 H11B 0.9800 . ?
C11 H11C 0.9800 . ?
C11 C87 1.49(5) . ?
C12 C29 1.47(5) . ?
C12 C51 1.62(5) . ?
C12 C63 1.41(5) . ?
C12 C73 1.51(5) . ?
C13 H13A 0.9800 . ?
C13 H13B 0.9800 . ?
C13 H13C 0.9800 . ?
C13 C62 1.39(5) . ?
C14 C62 1.55(5) . ?
C15 C19 1.68(6) . ?
C15 C37 1.57(6) . ?
C15 C72 1.28(5) . ?
C15 C75 1.49(2) . ?
C16 C18 1.24(5) . ?
C16 C90 1.46(5) . ?
C17 H17A 0.9800 . ?
C17 H17B 0.9800 . ?
C17 H17C 0.9800 . ?
C17 C90 1.63(6) . ?
C19 H19A 0.9800 . ?
C19 H19B 0.9800 . ?
C19 H19C 0.9800 . ?
C20 C26 1.23(5) . ?
C21 H21A 0.9800 . ?
C21 H21B 0.9800 . ?
C21 H21C 0.9800 . ?
C21 C57 1.48(2) . ?
C22 C35 1.45(6) . ?
C22 C58 1.46(5) . ?
C22 C96 1.50(5) . ?
C23 H23A 0.9800 . ?
C23 H23B 0.9800 . ?
C23 H23C 0.9800 . ?
C23 C43 1.72(7) . ?
C24 H24A 0.9541 . ?
C24 H24B 0.9800 . ?
C24 H24C 0.9798 . ?
C24 C80 1.38(5) . ?
C25 C68 1.39(5) . ?
C25 C92 1.20(5) . ?
C26 C76 1.40(5) . ?
C27 H27A 0.9800 . ?
C27 H27B 0.9800 . ?
C27 H27C 0.9800 . ?
C27 C76 1.44(5) . ?
C28 C42 1.16(5) . ?
C29 H29A 0.9800 . ?
C29 H29B 0.9800 . ?
C29 H29C 0.9800 . ?
C30 C41 1.49(6) . ?
C30 C44 1.42(5) . ?
C30 C79 1.54(6) . ?
C31 H31A 0.9800 . ?
C31 H31B 0.9800 . ?
C31 H31C 0.9800 . ?
C31 C76 1.52(5) . ?
C32 C36 1.20(5) . ?
C33 H33A 0.9800 . ?
C33 H33B 0.9800 . ?
C33 H33C 0.9800 . ?
C33 C90 1.52(6) . ?
C34 C49 1.59(5) . ?
C34 C61 1.48(5) . ?
C34 C67 1.52(6) . ?
C35 H35A 0.9800 . ?
C35 H35B 0.9800 . ?
C35 H35C 0.9800 . ?
C36 C87 1.55(5) . ?
C37 H37A 0.9800 . ?
C37 H37B 0.9800 . ?
C37 H37C 0.9800 . ?
C39 H39A 0.9800 . ?
C39 H39B 0.9800 . ?
C39 H39C 0.9800 . ?
C39 C68 1.66(6) . ?
C40 C52 1.24(5) . ?
C40 C64 1.56(6) . ?
C41 H41A 0.9800 . ?
C41 H41B 0.9800 . ?
C41 H41C 0.9800 . ?
C42 C43 1.48(6) . ?
C43 C45 1.49(6) . ?
C43 C89 1.58(6) . ?
C44 C60 1.17(5) . ?
C45 H45A 0.9800 . ?
C45 H45B 0.9800 . ?
C45 H45C 0.9800 . ?
C46 C73 1.26(5) . ?
C47 H47A 1.0104 . ?
C47 H47B 0.9800 . ?
C47 H47C 0.9800 . ?
C47 C85 1.78(7) . ?
C48 C54 1.58(6) . ?
C48 C70 1.18(6) . ?
C49 H49A 0.9800 . ?
C49 H49B 0.9800 . ?
C49 H49C 0.9800 . ?
C50 C57 1.39(6) . ?
C50 C66 1.25(6) . ?
C51 H51A 0.9800 . ?
C51 H51B 0.9800 . ?
C51 H51C 0.9800 . ?
C53 H53A 0.9801 . ?
C53 H53B 0.9633 . ?
C53 H53C 0.9796 . ?
C53 C80 1.66(5) . ?
C54 C65 1.38(6) . ?
C54 C86 1.53(6) . ?
C55 H55A 0.9800 . ?
C55 H55B 0.9800 . ?
C55 H55C 0.9800 . ?
C55 C76 1.60(6) . ?
C56 C74 1.22(2) . ?
C57 C81 1.75(6) . ?
C57 C83 1.32(6) . ?
C58 H58A 0.9800 . ?
C58 H58B 0.9800 . ?
C58 H58C 0.9800 . ?
C59 H59A 0.9800 . ?
C59 H59B 0.9800 . ?
C59 H59C 0.9800 . ?
C59 C68 1.59(6) . ?
C61 H61A 0.9800 . ?
C61 H61B 0.9800 . ?
C61 H61C 0.9800 . ?
C62 C88 1.60(5) . ?
C63 H63A 0.9800 . ?
C63 H63B 0.9800 . ?
C63 H63C 0.9800 . ?
C64 C69 1.60(6) . ?
C64 C84 1.60(5) . ?
C64 C94 1.36(5) . ?
C65 H65A 0.9800 . ?
C65 H65B 0.9800 . ?
C65 H65C 0.9800 . ?
C67 H67A 0.9800 . ?
C67 H67B 0.9800 . ?
C67 H67C 0.9800 . ?
C69 H69A 0.9800 . ?
C69 H69B 0.9800 . ?
C69 H69C 0.9800 . ?
C71 C80 1.38(5) . ?
C72 C82 1.35(5) . ?
C74 C85 1.48(6) . ?
C75 H75A 0.9800 . ?
C75 H75B 0.9800 . ?
C75 H75C 0.9800 . ?
C77 H77A 0.9801 . ?
C77 H77B 0.9800 . ?
C77 H77C 0.9989 . ?
C77 C85 1.51(7) . ?
C78 H78A 0.9800 . ?
C78 H78B 0.9800 . ?
C78 H78C 0.9800 . ?
C78 C80 1.54(5) . ?
C79 H79A 0.9800 . ?
C79 H79B 0.9800 . ?
C79 H79C 0.9800 . ?
C81 H81A 0.9800 . ?
C81 H81B 0.9800 . ?
C81 H81C 0.9800 . ?
C83 H83A 0.9799 . ?
C83 H83B 0.9800 . ?
C83 H83C 0.9799 . ?
C84 H84A 0.9800 . ?
C84 H84B 0.9800 . ?
C84 H84C 0.9800 . ?
C85 C95 1.33(6) . ?
C86 H86A 0.9800 . ?
C86 H86B 0.9800 . ?
C86 H86C 0.9800 . ?
C87 C91 1.48(2) . ?
C87 C93 1.49(6) . ?
C88 H88A 0.9800 . ?
C88 H88B 0.9800 . ?
C88 H88C 0.9800 . ?
C89 H89A 0.9800 . ?
C89 H89B 0.9800 . ?
C89 H89C 0.9800 . ?
C91 H91A 0.9800 . ?
C91 H91B 0.9800 . ?
C91 H91C 0.9800 . ?
C93 H93A 0.9800 . ?
C93 H93B 0.9800 . ?
C93 H93C 0.9800 . ?
C94 H94A 0.9800 . ?
C94 H94B 0.9800 . ?
C94 H94C 0.9800 . ?
C95 H95A 0.9800 . ?
C95 H95B 0.9800 . ?
C95 H95C 0.9800 . ?
C96 H96A 0.9800 . ?
C96 H96B 0.9800 . ?
C96 H96C 0.9800 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
F1 Sb1 F4 89.9(15) . . ?
F1 Sb1 F6 90.1(18) . . ?
F1 Sb1 F9 85.3(15) . . ?
F4 Sb1 F6 92.0(16) . . ?
F4 Sb1 F9 173.1(18) . . ?
F5 Sb1 F1 175(3) . . ?
F5 Sb1 F4 89(2) . . ?
F5 Sb1 F6 95(3) . . ?
F5 Sb1 F9 96(2) . . ?
F6 Sb1 F9 83.1(13) . . ?
F12 Sb1 F1 90.2(19) . . ?
F12 Sb1 F4 91.4(17) . . ?
F12 Sb1 F5 85(3) . . ?
F12 Sb1 F6 176.7(14) . . ?
F12 Sb1 F9 93.6(14) . . ?
F2 Sb2 F3 87.4(19) . . ?
F2 Sb2 F10 88(2) . . ?
F2 Sb2 F11 96(4) . . ?
F7 Sb2 F2 171(2) . . ?
F7 Sb2 F3 90.8(18) . . ?
F7 Sb2 F8 79.9(18) . . ?
F7 Sb2 F10 94.4(19) . . ?
F7 Sb2 F11 93(4) . . ?
F8 Sb2 F2 91(2) . . ?
F8 Sb2 F3 88.2(17) . . ?
F8 Sb2 F10 93.3(16) . . ?
F8 Sb2 F11 172(4) . . ?
F10 Sb2 F3 175(2) . . ?
F11 Sb2 F3 93(3) . . ?
F11 Sb2 F10 86(3) . . ?
Ag7 Ag1 Ag7 180.00(5) . 2_666 ?
Ag15 Ag1 Ag7 71.27(12) . 2_666 ?
Ag15 Ag1 Ag7 108.73(12) . . ?
Ag15 Ag1 Ag7 71.27(12) 2_666 . ?
Ag15 Ag1 Ag7 108.73(12) 2_666 2_666 ?
Ag15 Ag1 Ag15 180.00(16) . 2_666 ?
Ag20 Ag1 Ag7 69.31(12) . . ?
Ag20 Ag1 Ag7 110.69(12) . 2_666 ?
Ag20 Ag1 Ag7 110.69(12) 2_666 . ?
Ag20 Ag1 Ag7 69.31(12) 2_666 2_666 ?
Ag20 Ag1 Ag15 107.77(13) . 2_666 ?
Ag20 Ag1 Ag15 72.23(13) 2_666 2_666 ?
Ag20 Ag1 Ag15 72.23(13) . . ?
Ag20 Ag1 Ag15 107.77(13) 2_666 . ?
Ag20 Ag1 Ag20 180.00(18) . 2_666 ?
Cl1 Ag1 Ag7 54.04(19) . 2_666 ?
Cl1 Ag1 Ag7 54.04(19) 2_666 . ?
Cl1 Ag1 Ag7 125.96(19) 2_666 2_666 ?
Cl1 Ag1 Ag7 125.96(19) . . ?
Cl1 Ag1 Ag15 121.52(19) . 2_666 ?
Cl1 Ag1 Ag15 58.48(19) . . ?
Cl1 Ag1 Ag15 121.52(19) 2_666 . ?
Cl1 Ag1 Ag15 58.48(19) 2_666 2_666 ?
Cl1 Ag1 Ag20 123.31(19) . 2_666 ?
Cl1 Ag1 Ag20 56.69(19) . . ?
Cl1 Ag1 Ag20 56.69(19) 2_666 2_666 ?
Cl1 Ag1 Ag20 123.31(19) 2_666 . ?
Cl1 Ag1 Cl1 180.0(4) 2_666 . ?
Cl1 Ag1 Cl2 93.5(3) . . ?
Cl1 Ag1 Cl2 93.5(3) 2_666 2_666 ?
Cl1 Ag1 Cl2 86.5(3) . 2_666 ?
Cl1 Ag1 Cl2 86.5(3) 2_666 . ?
Cl1 Ag1 Cl3 90.5(3) 2_666 2_666 ?
Cl1 Ag1 Cl3 89.5(3) . 2_666 ?
Cl1 Ag1 Cl3 90.5(3) . . ?
Cl1 Ag1 Cl3 89.5(3) 2_666 . ?
Cl2 Ag1 Ag7 53.60(19) 2_666 2_666 ?
Cl2 Ag1 Ag7 126.40(19) 2_666 . ?
Cl2 Ag1 Ag7 126.40(19) . 2_666 ?
Cl2 Ag1 Ag7 53.60(19) . . ?
Cl2 Ag1 Ag15 124.87(19) 2_666 . ?
Cl2 Ag1 Ag15 124.87(19) . 2_666 ?
Cl2 Ag1 Ag15 55.13(19) . . ?
Cl2 Ag1 Ag15 55.13(19) 2_666 2_666 ?
Cl2 Ag1 Ag20 55.4(2) . . ?
Cl2 Ag1 Ag20 55.4(2) 2_666 2_666 ?
Cl2 Ag1 Ag20 124.6(2) 2_666 . ?
Cl2 Ag1 Ag20 124.6(2) . 2_666 ?
Cl2 Ag1 Cl2 180.0 2_666 . ?
Cl2 Ag1 Cl3 91.2(2) . 2_666 ?
Cl2 Ag1 Cl3 88.8(2) 2_666 2_666 ?
Cl2 Ag1 Cl3 88.8(2) . . ?
Cl2 Ag1 Cl3 91.2(2) 2_666 . ?
Cl3 Ag1 Ag7 55.3(2) . 2_666 ?
Cl3 Ag1 Ag7 124.7(2) . . ?
Cl3 Ag1 Ag7 124.7(2) 2_666 2_666 ?
Cl3 Ag1 Ag7 55.3(2) 2_666 . ?
Cl3 Ag1 Ag15 127.5(2) 2_666 . ?
Cl3 Ag1 Ag15 52.5(2) 2_666 2_666 ?
Cl3 Ag1 Ag15 52.5(2) . . ?
Cl3 Ag1 Ag15 127.5(2) . 2_666 ?
Cl3 Ag1 Ag20 124.7(2) . . ?
Cl3 Ag1 Ag20 124.7(2) 2_666 2_666 ?
Cl3 Ag1 Ag20 55.3(2) . 2_666 ?
Cl3 Ag1 Ag20 55.3(2) 2_666 . ?
Cl3 Ag1 Cl3 180.0 . 2_666 ?
Ag6 Ag2 Ag12 88.40(17) . . ?
Ag6 Ag2 Ag17 140.61(17) . . ?
Ag6 Ag2 Ag20 90.70(14) . . ?
Ag12 Ag2 Ag17 64.72(13) . . ?
Ag12 Ag2 Ag20 92.67(14) . . ?
Ag17 Ag2 Ag20 64.08(15) . . ?
Ag23 Ag2 Ag6 59.88(14) . . ?
Ag23 Ag2 Ag12 139.39(18) . . ?
Ag23 Ag2 Ag17 124.1(2) . . ?
Ag23 Ag2 Ag20 65.39(15) . . ?
C28 Ag2 Ag6 48.0(11) . . ?
C28 Ag2 Ag12 128.7(12) . . ?
C28 Ag2 Ag17 166.6(12) . . ?
C28 Ag2 Ag20 110.5(10) . . ?
C28 Ag2 Ag23 46.4(11) . . ?
C56 Ag2 Ag6 132.4(16) . . ?
C56 Ag2 Ag12 48.8(14) . . ?
C56 Ag2 Ag17 46.1(16) . . ?
C56 Ag2 Ag20 108.5(16) . . ?
C56 Ag2 Ag23 167.5(16) . . ?
C56 Ag2 C28 141.1(19) . . ?
Ag5 Ag3 Ag13 142.79(18) . . ?
Ag5 Ag3 Ag15 100.02(17) . . ?
Ag13 Ag3 Ag15 62.64(14) . . ?
Ag21 Ag3 Ag5 58.93(18) . . ?
Ag21 Ag3 Ag13 133.9(2) . . ?
Ag21 Ag3 Ag15 75.03(16) . . ?
C1 Ag3 Ag5 125.4(10) . . ?
C1 Ag3 Ag13 40.9(9) . . ?
C1 Ag3 Ag15 100.5(9) . . ?
C1 Ag3 Ag21 174.7(10) . . ?
C46 Ag3 Ag5 47.7(10) . . ?
C46 Ag3 Ag13 169.2(10) . . ?
C46 Ag3 Ag15 123.1(10) . . ?
C46 Ag3 Ag21 48.8(10) . . ?
C46 Ag3 C1 136.1(14) . . ?
Ag14 Ag4 Ag6 94.45(15) 2_666 . ?
Ag14 Ag4 Ag16 136.03(14) 2_666 . ?
Ag14 Ag4 Ag19 63.83(17) 2_666 2_666 ?
Ag16 Ag4 Ag6 67.38(14) . . ?
Ag19 Ag4 Ag6 139.64(14) 2_666 . ?
Ag19 Ag4 Ag16 103.83(18) 2_666 . ?
C10 Ag4 Ag6 141.7(10) . . ?
C10 Ag4 Ag14 51.1(9) . 2_666 ?
C10 Ag4 Ag16 147.8(10) . . ?
C10 Ag4 Ag19 46.6(9) . 2_666 ?
C18 Ag4 Ag6 46.5(13) . . ?
C18 Ag4 Ag14 139.7(12) . 2_666 ?
C18 Ag4 Ag16 47.7(12) . . ?
C18 Ag4 Ag19 150.4(12) . 2_666 ?
C18 Ag4 C10 155.7(15) . . ?
Ag3 Ag5 Ag11 143.0(2) . . ?
Ag3 Ag5 Ag19 92.7(2) . . ?
Ag3 Ag5 Ag20 90.78(16) . . ?
Ag11 Ag5 Ag19 58.46(17) . . ?
Ag11 Ag5 Ag20 71.12(17) . . ?
Ag19 Ag5 Ag20 94.77(16) . . ?
Ag21 Ag5 Ag3 59.96(17) . . ?
Ag21 Ag5 Ag11 132.2(3) . . ?
Ag21 Ag5 Ag19 145.3(2) . . ?
Ag21 Ag5 Ag20 67.08(17) . . ?
C20 Ag5 Ag3 129.9(10) . . ?
C20 Ag5 Ag11 45.0(10) . . ?
C20 Ag5 Ag19 45.6(9) . . ?
C20 Ag5 Ag20 114.7(10) . . ?
C20 Ag5 Ag21 168.8(9) . . ?
C20 Ag5 C92 109.7(14) . . ?
C46 Ag5 Ag3 48.2(9) . . ?
C46 Ag5 Ag11 168.8(10) . . ?
C46 Ag5 Ag19 128.1(10) . . ?
C46 Ag5 Ag20 114.7(10) . . ?
C46 Ag5 Ag21 49.4(10) . . ?
C46 Ag5 C20 130.6(15) . . ?
C46 Ag5 C92 108.5(14) . . ?
C92 Ag5 Ag3 116.6(10) . . ?
C92 Ag5 Ag11 69.3(10) . . ?
C92 Ag5 Ag19 120.7(9) . . ?
C92 Ag5 Ag20 39.9(8) . . ?
C92 Ag5 Ag21 63.9(10) . . ?
Ag2 Ag6 Ag4 143.76(16) . . ?
Ag2 Ag6 Ag7 73.14(14) . . ?
Ag7 Ag6 Ag4 71.26(13) . . ?
Ag23 Ag6 Ag2 59.28(14) . . ?
Ag23 Ag6 Ag4 133.65(16) . . ?
Ag23 Ag6 Ag7 99.29(15) . . ?
C18 Ag6 Ag2 171.3(11) . . ?
C18 Ag6 Ag4 38.5(11) . . ?
C18 Ag6 Ag7 106.4(11) . . ?
C18 Ag6 Ag23 112.7(11) . . ?
C18 Ag6 C32 110.4(15) . . ?
C28 Ag6 Ag2 50.7(13) . . ?
C28 Ag6 Ag4 165.5(13) . . ?
C28 Ag6 Ag7 122.9(13) . . ?
C28 Ag6 Ag23 46.4(11) . . ?
C28 Ag6 C18 127.3(17) . . ?
C28 Ag6 C32 118.1(15) . . ?
C32 Ag6 Ag2 75.4(10) . . ?
C32 Ag6 Ag4 73.9(9) . . ?
C32 Ag6 Ag7 42.2(8) . . ?
C32 Ag6 Ag23 129.1(10) . . ?
Ag6 Ag7 Ag1 122.59(15) . . ?
Ag12 Ag7 Ag1 126.63(18) . . ?
Ag12 Ag7 Ag6 89.63(14) . . ?
Ag12 Ag7 Ag14 94.67(15) . 2_666 ?
Ag14 Ag7 Ag1 119.74(16) 2_666 . ?
Ag14 Ag7 Ag6 95.31(15) 2_666 . ?
Cl1 Ag7 Ag1 57.51(19) 2_666 . ?
Cl1 Ag7 Ag6 131.2(3) 2_666 . ?
Cl1 Ag7 Ag12 132.0(3) 2_666 . ?
Cl1 Ag7 Ag14 62.3(2) 2_666 2_666 ?
Cl1 Ag7 Cl3 95.7(3) 2_666 2_666 ?
Cl2 Ag7 Ag1 58.3(2) . . ?
Cl2 Ag7 Ag6 64.5(2) . . ?
Cl2 Ag7 Ag12 133.3(3) . . ?
Cl2 Ag7 Ag14 124.3(3) . 2_666 ?
Cl2 Ag7 Cl1 91.9(3) . 2_666 ?
Cl2 Ag7 Cl3 97.4(3) . 2_666 ?
Cl3 Ag7 Ag1 59.24(19) 2_666 . ?
Cl3 Ag7 Ag6 127.7(3) 2_666 . ?
Cl3 Ag7 Ag12 67.4(2) 2_666 . ?
Cl3 Ag7 Ag14 131.2(3) 2_666 2_666 ?
C32 Ag7 Ag1 177.8(13) . . ?
C32 Ag7 Ag6 57.8(12) . . ?
C32 Ag7 Ag12 51.3(13) . . ?
C32 Ag7 Ag14 62.0(12) . 2_666 ?
C32 Ag7 Cl1 124.2(12) . 2_666 ?
C32 Ag7 Cl2 122.3(12) . . ?
C32 Ag7 Cl3 118.7(13) . 2_666 ?
Ag9 Ag8 Ag11 143.89(17) . 2_666 ?
Ag9 Ag8 Ag17 127.48(19) . 2_666 ?
Ag9 Ag8 Ag18 61.73(15) . . ?
Ag9 Ag8 Ag22 76.76(14) . . ?
Ag11 Ag8 Ag17 58.13(16) 2_666 2_666 ?
Ag11 Ag8 Ag18 126.44(17) 2_666 . ?
Ag11 Ag8 Ag22 67.21(14) 2_666 . ?
Ag17 Ag8 Ag18 70.97(14) 2_666 . ?
Ag17 Ag8 Ag22 91.62(15) 2_666 . ?
Ag22 Ag8 Ag18 100.84(15) . . ?
C52 Ag8 Ag9 80.2(10) . . ?
C52 Ag8 Ag11 71.8(10) . 2_666 ?
C52 Ag8 Ag17 123.3(9) . 2_666 ?
C52 Ag8 Ag18 134.0(10) . . ?
C52 Ag8 Ag22 42.2(10) . . ?
C66 Ag8 Ag9 44.1(11) . . ?
C66 Ag8 Ag11 168.5(13) . 2_666 ?
C66 Ag8 Ag17 110.8(13) . 2_666 ?
C66 Ag8 Ag18 44.8(14) . . ?
C66 Ag8 Ag22 118.9(12) . . ?
C66 Ag8 C52 119.6(16) . . ?
C66 Ag8 C70 125.4(18) . 2_666 ?
C70 Ag8 Ag9 167.5(13) 2_666 . ?
C70 Ag8 Ag11 45.2(13) 2_666 2_666 ?
C70 Ag8 Ag17 44.5(13) 2_666 2_666 ?
C70 Ag8 Ag18 106.3(12) 2_666 . ?
C70 Ag8 Ag22 110.6(14) 2_666 . ?
C70 Ag8 C52 112.1(17) 2_666 . ?
Ag8 Ag9 Ag10 141.14(16) . . ?
Ag8 Ag9 Ag15 93.94(14) . . ?
Ag8 Ag9 Ag16 92.68(19) . . ?
Ag8 Ag9 Ag18 62.28(13) . . ?
Ag10 Ag9 Ag15 58.18(14) . . ?
Ag10 Ag9 Ag18 119.6(2) . . ?
Ag16 Ag9 Ag10 60.59(15) . . ?
Ag16 Ag9 Ag15 84.14(14) . . ?
Ag16 Ag9 Ag18 139.95(16) . . ?
Ag18 Ag9 Ag15 68.31(15) . . ?
C8 Ag9 Ag8 133.1(10) . . ?
C8 Ag9 Ag10 44.9(10) . . ?
C8 Ag9 Ag15 100.4(9) . . ?
C8 Ag9 Ag16 45.7(9) . . ?
C8 Ag9 Ag18 163.0(11) . . ?
C66 Ag9 Ag8 50.9(13) . . ?
C66 Ag9 Ag10 159.8(15) . . ?
C66 Ag9 Ag15 112.4(15) . . ?
C66 Ag9 Ag16 139.2(14) . . ?
C66 Ag9 Ag18 45.0(15) . . ?
C66 Ag9 C8 146.9(18) . . ?
Ag9 Ag10 Ag15 64.68(14) . . ?
Ag9 Ag10 Ag16 59.57(15) . . ?
Ag16 Ag10 Ag15 87.04(14) . . ?
Ag21 Ag10 Ag9 136.5(2) . . ?
Ag21 Ag10 Ag15 76.16(16) . . ?
Ag21 Ag10 Ag16 138.57(18) . . ?
Ag21 Ag10 Ag23 60.17(16) . . ?
Ag23 Ag10 Ag9 142.72(17) . . ?
Ag23 Ag10 Ag15 100.49(16) . . ?
Ag23 Ag10 Ag16 86.93(16) . . ?
C8 Ag10 Ag9 47.8(11) . . ?
C8 Ag10 Ag15 109.3(11) . . ?
C8 Ag10 Ag16 45.2(9) . . ?
C8 Ag10 Ag21 174.3(10) . . ?
C8 Ag10 Ag23 119.3(10) . . ?
C8 Ag10 C38 107.0(15) . . ?
C8 Ag10 C60 127.7(15) . . ?
C38 Ag10 Ag9 62.7(10) . . ?
C38 Ag10 Ag15 41.5(8) . . ?
C38 Ag10 Ag16 115.0(9) . . ?
C38 Ag10 Ag21 75.7(10) . . ?
C38 Ag10 Ag23 129.2(10) . . ?
C60 Ag10 Ag9 169.5(11) . . ?
C60 Ag10 Ag15 122.3(11) . . ?
C60 Ag10 Ag16 125.8(10) . . ?
C60 Ag10 Ag21 47.2(11) . . ?
C60 Ag10 Ag23 46.8(10) . . ?
C60 Ag10 C38 116.3(14) . . ?
Ag5 Ag11 Ag8 145.0(2) . 2_666 ?
Ag5 Ag11 Ag19 63.55(19) . . ?
Ag5 Ag11 Ag22 89.55(16) . 2_666 ?
Ag8 Ag11 Ag22 57.00(13) 2_666 2_666 ?
Ag17 Ag11 Ag5 111.9(3) . . ?
Ag17 Ag11 Ag8 61.24(14) . 2_666 ?
Ag17 Ag11 Ag19 143.2(2) . . ?
Ag17 Ag11 Ag22 87.51(16) . 2_666 ?
Ag19 Ag11 Ag8 100.4(2) . 2_666 ?
Ag19 Ag11 Ag22 56.92(14) . 2_666 ?
C20 Ag11 Ag5 49.4(11) . . ?
C20 Ag11 Ag8 142.0(11) . 2_666 ?
C20 Ag11 Ag17 156.6(11) . . ?
C20 Ag11 Ag19 48.5(10) . . ?
C20 Ag11 Ag22 104.4(10) . 2_666 ?
C20 Ag11 C70 143.0(17) . . ?
C70 Ag11 Ag5 152.0(13) . . ?
C70 Ag11 Ag8 49.3(12) . 2_666 ?
C70 Ag11 Ag17 46.4(13) . . ?
C70 Ag11 Ag19 144.3(13) . . ?
C70 Ag11 Ag22 104.6(12) . 2_666 ?
Ag2 Ag12 Ag17 58.92(14) . . ?
Ag7 Ag12 Ag2 73.91(14) . . ?
Ag7 Ag12 Ag13 72.90(14) . 2_666 ?
Ag7 Ag12 Ag17 95.28(15) . . ?
Ag7 Ag12 Ag18 101.38(15) . 2_666 ?
Ag13 Ag12 Ag2 146.69(17) 2_666 . ?
Ag13 Ag12 Ag17 121.87(16) 2_666 . ?
Ag13 Ag12 Ag18 59.71(14) 2_666 2_666 ?
Ag18 Ag12 Ag2 125.70(18) 2_666 . ?
Ag18 Ag12 Ag17 68.06(14) 2_666 . ?
C32 Ag12 Ag2 78.4(11) . . ?
C32 Ag12 Ag7 45.4(9) . . ?
C32 Ag12 Ag13 80.3(11) . 2_666 ?
C32 Ag12 Ag17 130.2(10) . . ?
C32 Ag12 Ag18 136.0(10) . 2_666 ?
C32 Ag12 C56 116.1(17) . . ?
C56 Ag12 Ag2 42.0(10) . . ?
C56 Ag12 Ag7 113.3(10) . . ?
C56 Ag12 Ag13 162.4(14) . 2_666 ?
C56 Ag12 Ag17 43.1(14) . . ?
C56 Ag12 Ag18 102.7(14) . 2_666 ?
C82 Ag12 Ag2 160.0(13) 2_666 . ?
C82 Ag12 Ag7 120.5(12) 2_666 . ?
C82 Ag12 Ag13 49.1(12) 2_666 2_666 ?
C82 Ag12 Ag17 103.7(13) 2_666 . ?
C82 Ag12 Ag18 42.2(11) 2_666 2_666 ?
C82 Ag12 C32 121.5(17) 2_666 . ?
C82 Ag12 C56 119.0(17) 2_666 . ?
Ag3 Ag13 Ag14 65.20(15) . . ?
Ag3 Ag13 Ag15 60.92(15) . . ?
Ag12 Ag13 Ag3 142.77(18) 2_666 . ?
Ag12 Ag13 Ag14 90.23(17) 2_666 . ?
Ag12 Ag13 Ag15 95.13(15) 2_666 . ?
Ag12 Ag13 Ag18 61.69(14) 2_666 . ?
Ag14 Ag13 Ag15 92.98(15) . . ?
Ag18 Ag13 Ag3 124.2(2) . . ?
Ag18 Ag13 Ag14 144.19(18) . . ?
Ag18 Ag13 Ag15 69.80(15) . . ?
C1 Ag13 Ag3 47.7(10) . . ?
C1 Ag13 Ag12 127.8(10) . 2_666 ?
C1 Ag13 Ag14 42.1(10) . . ?
C1 Ag13 Ag15 105.1(11) . . ?
C1 Ag13 Ag18 170.2(10) . . ?
C1 Ag13 C82 142.8(16) . . ?
C82 Ag13 Ag3 162.4(12) . . ?
C82 Ag13 Ag12 49.4(11) . 2_666 ?
C82 Ag13 Ag14 132.4(12) . . ?
C82 Ag13 Ag15 112.1(11) . . ?
C82 Ag13 Ag18 43.2(12) . . ?
Ag4 Ag14 Ag7 75.43(14) 2_666 2_666 ?
Ag4 Ag14 Ag13 141.72(18) 2_666 . ?
Ag4 Ag14 Ag19 58.14(14) 2_666 . ?
Ag7 Ag14 Ag13 67.58(14) 2_666 . ?
Ag7 Ag14 Ag19 97.83(15) 2_666 . ?
Ag19 Ag14 Ag13 135.26(18) . . ?
C1 Ag14 Ag4 179.1(10) . 2_666 ?
C1 Ag14 Ag7 103.9(10) . 2_666 ?
C1 Ag14 Ag13 37.7(9) . . ?
C1 Ag14 Ag19 121.6(10) . . ?
C1 Ag14 C10 131.2(13) . 2_666 ?
C10 Ag14 Ag4 49.3(9) 2_666 2_666 ?
C10 Ag14 Ag7 122.6(9) 2_666 2_666 ?
C10 Ag14 Ag13 168.9(9) 2_666 . ?
C10 Ag14 Ag19 43.8(9) 2_666 . ?
Ag1 Ag15 Ag3 115.08(16) . . ?
Ag1 Ag15 Ag9 123.83(16) . . ?
Ag1 Ag15 Ag10 122.62(16) . . ?
Ag1 Ag15 Ag13 116.35(14) . . ?
Ag3 Ag15 Ag9 121.00(16) . . ?
Ag3 Ag15 Ag13 56.44(11) . . ?
Ag10 Ag15 Ag3 89.51(15) . . ?
Ag10 Ag15 Ag9 57.14(11) . . ?
Ag10 Ag15 Ag13 120.27(15) . . ?
Ag13 Ag15 Ag9 97.33(16) . . ?
Cl1 Ag15 Ag1 56.62(19) . . ?
Cl1 Ag15 Ag3 58.8(2) . . ?
Cl1 Ag15 Ag9 177.2(3) . . ?
Cl1 Ag15 Ag10 125.3(3) . . ?
Cl1 Ag15 Ag13 80.2(2) . . ?
Cl2 Ag15 Ag1 58.6(2) . . ?
Cl2 Ag15 Ag3 122.5(3) . . ?
Cl2 Ag15 Ag9 87.8(2) . . ?
Cl2 Ag15 Ag10 64.4(2) . . ?
Cl2 Ag15 Ag13 174.5(3) . . ?
Cl2 Ag15 Cl1 94.6(3) . . ?
Cl3 Ag15 Ag1 61.4(2) . . ?
Cl3 Ag15 Ag3 131.9(3) . . ?
Cl3 Ag15 Ag9 83.0(2) . . ?
Cl3 Ag15 Ag10 135.1(3) . . ?
Cl3 Ag15 Ag13 81.3(2) . . ?
Cl3 Ag15 Cl1 95.2(3) . . ?
Cl3 Ag15 Cl2 97.2(3) . . ?
C38 Ag15 Ag1 172.4(13) . . ?
C38 Ag15 Ag3 59.2(12) . . ?
C38 Ag15 Ag9 61.8(12) . . ?
C38 Ag15 Ag10 54.6(11) . . ?
C38 Ag15 Ag13 65.6(11) . . ?
C38 Ag15 Cl1 118.0(12) . . ?
C38 Ag15 Cl2 119.1(12) . . ?
C38 Ag15 Cl3 126.0(13) . . ?
Ag9 Ag16 Ag4 139.4(2) . . ?
Ag9 Ag16 Ag10 59.84(14) . . ?
Ag9 Ag16 Ag22 75.53(15) . . ?
Ag10 Ag16 Ag4 143.59(18) . . ?
Ag22 Ag16 Ag4 67.88(13) . . ?
Ag22 Ag16 Ag10 101.46(14) . . ?
Cl2 Ag16 Ag4 84.0(2) . . ?
Cl2 Ag16 Ag9 89.7(2) . . ?
Cl2 Ag16 Ag10 62.9(2) . . ?
Cl2 Ag16 Ag22 55.6(2) . . ?
C8 Ag16 Ag4 168.5(10) . . ?
C8 Ag16 Ag9 47.9(11) . . ?
C8 Ag16 Ag10 44.5(10) . . ?
C8 Ag16 Ag22 122.1(10) . . ?
C8 Ag16 Cl2 106.3(10) . . ?
C8 Ag16 C18 131.8(16) . . ?
C18 Ag16 Ag4 40.0(11) . . ?
C18 Ag16 Ag9 175.3(11) . . ?
C18 Ag16 Ag10 123.8(11) . . ?
C18 Ag16 Ag22 105.7(11) . . ?
C18 Ag16 Cl2 94.7(11) . . ?
Ag2 Ag17 Ag12 56.35(13) . . ?
Ag8 Ag17 Ag2 149.33(17) 2_666 . ?
Ag8 Ag17 Ag12 106.03(16) 2_666 . ?
Ag11 Ag17 Ag2 118.9(2) . . ?
Ag11 Ag17 Ag8 60.63(15) . 2_666 ?
Ag11 Ag17 Ag12 147.44(18) . . ?
Cl3 Ag17 Ag2 83.9(2) 2_666 . ?
Cl3 Ag17 Ag8 65.5(2) 2_666 2_666 ?
Cl3 Ag17 Ag11 86.9(2) 2_666 . ?
Cl3 Ag17 Ag12 61.0(2) 2_666 . ?
C56 Ag17 Ag2 40.5(10) . . ?
C56 Ag17 Ag8 144.0(13) . 2_666 ?
C56 Ag17 Ag11 155.1(13) . . ?
C56 Ag17 Ag12 43.7(13) . . ?
C56 Ag17 Cl3 101.2(12) . 2_666 ?
C70 Ag17 Ag2 155.7(14) . . ?
C70 Ag17 Ag8 49.0(12) . 2_666 ?
C70 Ag17 Ag11 46.8(14) . . ?
C70 Ag17 Ag12 147.4(14) . . ?
C70 Ag17 Cl3 111.2(12) . 2_666 ?
C70 Ag17 C56 143.5(17) . . ?
Ag9 Ag18 Ag8 55.99(13) . . ?
Ag12 Ag18 Ag8 110.80(16) 2_666 . ?
Ag12 Ag18 Ag9 142.01(17) 2_666 . ?
Ag13 Ag18 Ag8 140.92(18) . . ?
Ag13 Ag18 Ag9 106.9(2) . . ?
Ag13 Ag18 Ag12 58.60(14) . 2_666 ?
C66 Ag18 Ag8 46.8(12) . . ?
C66 Ag18 Ag9 41.0(12) . . ?
C66 Ag18 Ag12 155.6(13) . 2_666 ?
C66 Ag18 Ag13 143.4(12) . . ?
C82 Ag18 Ag8 153.6(12) . . ?
C82 Ag18 Ag9 150.0(13) . . ?
C82 Ag18 Ag12 48.1(12) . 2_666 ?
C82 Ag18 Ag13 49.0(14) . . ?
C82 Ag18 C66 147.7(18) . . ?
Ag4 Ag19 Ag5 143.7(2) 2_666 . ?
Ag4 Ag19 Ag11 133.6(2) 2_666 . ?
Ag4 Ag19 Ag14 58.03(12) 2_666 . ?
Ag4 Ag19 Ag22 70.39(14) 2_666 2_666 ?
Ag11 Ag19 Ag5 57.98(16) . . ?
Ag11 Ag19 Ag14 141.6(2) . . ?
Ag11 Ag19 Ag22 67.93(16) . 2_666 ?
Ag14 Ag19 Ag5 92.2(2) . . ?
Ag22 Ag19 Ag5 92.71(16) 2_666 . ?
Ag22 Ag19 Ag14 92.39(15) 2_666 . ?
C10 Ag19 Ag4 49.9(10) 2_666 2_666 ?
C10 Ag19 Ag5 126.5(9) 2_666 . ?
C10 Ag19 Ag11 169.7(11) 2_666 . ?
C10 Ag19 Ag14 48.4(10) 2_666 . ?
C10 Ag19 Ag22 118.9(10) 2_666 2_666 ?
C10 Ag19 C20 129.5(15) 2_666 . ?
C20 Ag19 Ag4 170.1(11) . 2_666 ?
C20 Ag19 Ag5 46.1(10) . . ?
C20 Ag19 Ag11 44.8(11) . . ?
C20 Ag19 Ag14 130.5(11) . . ?
C20 Ag19 Ag22 111.6(11) . 2_666 ?
Ag1 Ag20 Ag2 120.98(15) . . ?
Ag1 Ag20 Ag5 120.17(16) . . ?
Ag1 Ag20 Ag21 119.78(17) . . ?
Ag1 Ag20 Ag23 119.01(16) . . ?
Ag2 Ag20 Ag21 98.34(15) . . ?
Ag2 Ag20 Ag23 52.11(10) . . ?
Ag5 Ag20 Ag2 118.76(16) . . ?
Ag5 Ag20 Ag21 52.12(12) . . ?
Ag5 Ag20 Ag23 99.43(15) . . ?
Ag21 Ag20 Ag23 53.06(11) . . ?
Cl1 Ag20 Ag1 58.0(2) . . ?
Cl1 Ag20 Ag2 176.9(3) . . ?
Cl1 Ag20 Ag5 62.1(2) . . ?
Cl1 Ag20 Ag21 84.5(2) . . ?
Cl1 Ag20 Ag23 131.0(2) . . ?
Cl2 Ag20 Ag1 59.2(2) . . ?
Cl2 Ag20 Ag2 84.3(2) . . ?
Cl2 Ag20 Ag5 131.5(3) . . ?
Cl2 Ag20 Ag21 84.6(3) . . ?
Cl2 Ag20 Ag23 59.8(2) . . ?
Cl2 Ag20 Cl1 97.2(3) . . ?
Cl2 Ag20 Cl3 97.7(3) . 2_666 ?
Cl3 Ag20 Ag1 60.9(2) 2_666 . ?
Cl3 Ag20 Ag2 83.0(2) 2_666 . ?
Cl3 Ag20 Ag5 125.3(3) 2_666 . ?
Cl3 Ag20 Ag21 177.4(3) 2_666 . ?
Cl3 Ag20 Ag23 129.1(2) 2_666 . ?
Cl3 Ag20 Cl1 94.1(3) 2_666 . ?
C92 Ag20 Ag1 176.9(13) . . ?
C92 Ag20 Ag2 61.4(11) . . ?
C92 Ag20 Ag5 57.4(11) . . ?
C92 Ag20 Ag21 60.7(13) . . ?
C92 Ag20 Ag23 63.9(13) . . ?
C92 Ag20 Cl1 119.5(12) . . ?
C92 Ag20 Cl2 123.7(13) . . ?
C92 Ag20 Cl3 118.5(13) . 2_666 ?
Ag3 Ag21 Ag10 97.6(2) . . ?
Ag3 Ag21 Ag20 87.95(15) . . ?
Ag3 Ag21 Ag23 142.6(2) . . ?
Ag5 Ag21 Ag3 61.12(16) . . ?
Ag5 Ag21 Ag10 142.3(2) . . ?
Ag5 Ag21 Ag20 60.80(16) . . ?
Ag5 Ag21 Ag23 116.5(3) . . ?
Ag10 Ag21 Ag20 89.72(15) . . ?
Ag10 Ag21 Ag23 60.63(14) . . ?
Ag23 Ag21 Ag20 63.80(15) . . ?
C46 Ag21 Ag3 48.7(9) . . ?
C46 Ag21 Ag5 48.8(10) . . ?
C46 Ag21 Ag10 139.3(10) . . ?
C46 Ag21 Ag20 108.1(10) . . ?
C46 Ag21 Ag23 160.0(10) . . ?
C60 Ag21 Ag3 139.7(11) . . ?
C60 Ag21 Ag5 158.9(11) . . ?
C60 Ag21 Ag10 48.6(11) . . ?
C60 Ag21 Ag20 109.5(11) . . ?
C60 Ag21 Ag23 47.1(11) . . ?
C60 Ag21 C46 141.6(15) . . ?
Ag1 Ag22 Ag11 114.81(16) . 2_666 ?
Ag8 Ag22 Ag1 124.44(15) . . ?
Ag8 Ag22 Ag11 55.79(12) . 2_666 ?
Ag16 Ag22 Ag1 114.91(17) . . ?
Ag16 Ag22 Ag8 89.94(15) . . ?
Ag16 Ag22 Ag11 129.78(19) . 2_666 ?
Ag19 Ag22 Ag1 120.51(18) 2_666 . ?
Ag19 Ag22 Ag8 98.08(17) 2_666 . ?
Ag19 Ag22 Ag11 55.15(13) 2_666 2_666 ?
Ag19 Ag22 Ag16 103.23(16) 2_666 . ?
Cl1 Ag22 Ag1 56.3(2) 2_666 . ?
Cl1 Ag22 Ag8 137.1(3) 2_666 . ?
Cl1 Ag22 Ag11 83.9(2) 2_666 2_666 ?
Cl1 Ag22 Ag16 130.9(2) 2_666 . ?
Cl1 Ag22 Ag19 64.2(2) 2_666 2_666 ?
Cl1 Ag22 Cl2 90.2(3) 2_666 . ?
Cl1 Ag22 Cl3 95.8(3) 2_666 . ?
Cl2 Ag22 Ag1 56.2(2) . . ?
Cl2 Ag22 Ag8 127.6(2) . . ?
Cl2 Ag22 Ag11 171.0(3) . 2_666 ?
Cl2 Ag22 Ag16 59.1(2) . . ?
Cl2 Ag22 Ag19 127.7(2) . 2_666 ?
Cl3 Ag22 Ag1 58.3(2) . . ?
Cl3 Ag22 Ag8 66.3(2) . . ?
Cl3 Ag22 Ag11 80.7(2) . 2_666 ?
Cl3 Ag22 Ag16 121.1(3) . . ?
Cl3 Ag22 Ag19 131.8(3) . 2_666 ?
Cl3 Ag22 Cl2 93.3(3) . . ?
C52 Ag22 Ag1 174.4(13) . . ?
C52 Ag22 Ag8 53.1(11) . . ?
C52 Ag22 Ag11 68.5(11) . 2_666 ?
C52 Ag22 Ag16 61.3(11) . . ?
C52 Ag22 Ag19 65.0(13) . 2_666 ?
C52 Ag22 Cl1 129.2(13) . 2_666 ?
C52 Ag22 Cl2 120.4(12) . . ?
C52 Ag22 Cl3 119.3(12) . . ?
Ag2 Ag23 Ag6 60.84(14) . . ?
Ag2 Ag23 Ag10 145.09(18) . . ?
Ag2 Ag23 Ag20 62.50(15) . . ?
Ag2 Ag23 Ag21 115.9(2) . . ?
Ag6 Ag23 Ag10 102.64(17) . . ?
Ag6 Ag23 Ag20 89.59(14) . . ?
Ag6 Ag23 Ag21 145.75(18) . . ?
Ag10 Ag23 Ag20 88.63(14) . . ?
Ag21 Ag23 Ag10 59.20(16) . . ?
Ag21 Ag23 Ag20 63.14(15) . . ?
C28 Ag23 Ag2 51.9(13) . . ?
C28 Ag23 Ag6 49.1(11) . . ?
C28 Ag23 Ag10 141.4(14) . . ?
C28 Ag23 Ag20 113.0(12) . . ?
C28 Ag23 Ag21 158.9(14) . . ?
C28 Ag23 C60 137.0(15) . . ?
C60 Ag23 Ag2 156.4(12) . . ?
C60 Ag23 Ag6 142.7(12) . . ?
C60 Ag23 Ag10 47.8(11) . . ?
C60 Ag23 Ag20 108.6(10) . . ?
C60 Ag23 Ag21 46.8(11) . . ?
Ag1 Cl1 Ag15 64.9(2) . . ?
Ag7 Cl1 Ag1 68.5(2) 2_666 . ?
Ag7 Cl1 Ag15 80.0(3) 2_666 . ?
Ag7 Cl1 Ag20 133.7(4) 2_666 . ?
Ag20 Cl1 Ag1 65.27(19) . . ?
Ag20 Cl1 Ag15 78.6(2) . . ?
Ag22 Cl1 Ag1 71.1(2) 2_666 . ?
Ag22 Cl1 Ag7 86.0(3) 2_666 2_666 ?
Ag22 Cl1 Ag15 136.0(4) 2_666 . ?
Ag22 Cl1 Ag20 81.8(3) 2_666 . ?
Ag1 Cl2 Ag16 134.0(4) . . ?
Ag7 Cl2 Ag1 68.1(2) . . ?
Ag7 Cl2 Ag15 134.4(4) . . ?
Ag7 Cl2 Ag16 113.1(3) . . ?
Ag7 Cl2 Ag20 79.9(3) . . ?
Ag7 Cl2 Ag22 84.2(3) . . ?
Ag15 Cl2 Ag1 66.3(2) . . ?
Ag15 Cl2 Ag16 98.3(3) . . ?
Ag15 Cl2 Ag22 79.8(3) . . ?
Ag20 Cl2 Ag1 65.5(2) . . ?
Ag20 Cl2 Ag15 81.8(3) . . ?
Ag20 Cl2 Ag16 158.9(4) . . ?
Ag20 Cl2 Ag22 134.7(4) . . ?
Ag22 Cl2 Ag1 69.2(2) . . ?
Ag22 Cl2 Ag16 65.3(2) . . ?
Ag7 Cl3 Ag1 65.5(2) 2_666 . ?
Ag7 Cl3 Ag17 110.4(3) 2_666 2_666 ?
Ag15 Cl3 Ag1 66.1(2) . . ?
Ag15 Cl3 Ag7 82.2(3) . 2_666 ?
Ag15 Cl3 Ag17 154.3(4) . 2_666 ?
Ag15 Cl3 Ag20 130.0(4) . 2_666 ?
Ag15 Cl3 Ag22 81.6(3) . . ?
Ag17 Cl3 Ag1 139.3(4) 2_666 . ?
Ag20 Cl3 Ag1 63.9(2) 2_666 . ?
Ag20 Cl3 Ag7 77.4(3) 2_666 2_666 ?
Ag20 Cl3 Ag17 75.6(3) 2_666 2_666 ?
Ag20 Cl3 Ag22 80.5(3) 2_666 . ?
Ag22 Cl3 Ag1 68.2(2) . . ?
Ag22 Cl3 Ag7 133.6(4) . 2_666 ?
Ag22 Cl3 Ag17 102.7(3) . 2_666 ?
Ag13 C1 Ag3 91.5(14) . . ?
Ag13 C1 Ag14 100.1(14) . . ?
Ag14 C1 Ag3 98.9(15) . . ?
C14 C1 Ag3 104(3) . . ?
C14 C1 Ag13 150(4) . . ?
C14 C1 Ag14 103(3) . . ?
H2A C2 H2B 109.5 . . ?
H2A C2 H2C 109.5 . . ?
H2B C2 H2C 109.5 . . ?
C54 C2 H2A 109.5 . . ?
C54 C2 H2B 109.5 . . ?
C54 C2 H2C 109.5 . . ?
H3A C3 H3B 109.5 . . ?
H3A C3 H3C 109.5 . . ?
H3B C3 H3C 109.5 . . ?
C62 C3 H3A 109.5 . . ?
C62 C3 H3B 109.5 . . ?
C62 C3 H3C 109.5 . . ?
C38 C4 C22 172(4) . . ?
H5A C5 H5B 109.5 . . ?
H5A C5 H5C 109.5 . . ?
H5B C5 H5C 109.5 . . ?
C30 C5 H5A 109.5 . . ?
C30 C5 H5B 109.5 . . ?
C30 C5 H5C 109.5 . . ?
C8 C6 C34 178(5) . . ?
H7A C7 H7B 109.5 . . ?
H7A C7 H7C 109.5 . . ?
H7B C7 H7C 109.5 . . ?
C68 C7 H7A 109.5 . . ?
C68 C7 H7B 109.5 . . ?
C68 C7 H7C 109.5 . . ?
Ag10 C8 Ag9 87.4(13) . . ?
Ag10 C8 Ag16 90.3(12) . . ?
Ag16 C8 Ag9 86.4(13) . . ?
C6 C8 Ag9 106(3) . . ?
C6 C8 Ag10 132(3) . . ?
C6 C8 Ag16 136(3) . . ?
H9A C9 H9B 109.5 . . ?
H9A C9 H9C 109.5 . . ?
H9B C9 H9C 109.5 . . ?
C90 C9 H9A 109.5 . . ?
C90 C9 H9B 109.5 . . ?
C90 C9 H9C 109.5 . . ?
Ag4 C10 Ag14 79.6(12) . 2_666 ?
Ag19 C10 Ag4 83.5(12) 2_666 . ?
Ag19 C10 Ag14 87.9(12) 2_666 2_666 ?
C71 C10 Ag4 105(3) . . ?
C71 C10 Ag14 134(3) . 2_666 ?
C71 C10 Ag19 138(3) . 2_666 ?
H11A C11 H11B 109.5 . . ?
H11A C11 H11C 109.5 . . ?
H11B C11 H11C 109.5 . . ?
C87 C11 H11A 109.5 . . ?
C87 C11 H11B 109.5 . . ?
C87 C11 H11C 109.5 . . ?
C29 C12 C51 110(3) . . ?
C29 C12 C73 108(3) . . ?
C63 C12 C29 109(4) . . ?
C63 C12 C51 110(3) . . ?
C63 C12 C73 110(3) . . ?
C73 C12 C51 110(3) . . ?
H13A C13 H13B 109.5 . . ?
H13A C13 H13C 109.5 . . ?
H13B C13 H13C 109.5 . . ?
C62 C13 H13A 109.5 . . ?
C62 C13 H13B 109.5 . . ?
C62 C13 H13C 109.5 . . ?
C1 C14 C62 179(4) . . ?
C37 C15 C19 96(4) . . ?
C72 C15 C19 113(4) . . ?
C72 C15 C37 118(4) . . ?
C72 C15 C75 104(4) . . ?
C75 C15 C19 106(4) . . ?
C75 C15 C37 119(4) . . ?
C18 C16 C90 171(5) . . ?
H17A C17 H17B 109.5 . . ?
H17A C17 H17C 109.5 . . ?
H17B C17 H17C 109.5 . . ?
C90 C17 H17A 109.5 . . ?
C90 C17 H17B 109.5 . . ?
C90 C17 H17C 109.5 . . ?
Ag4 C18 Ag6 95.0(17) . . ?
Ag4 C18 Ag16 92.4(16) . . ?
Ag16 C18 Ag6 98.3(17) . . ?
C16 C18 Ag4 160(4) . . ?
C16 C18 Ag6 99(3) . . ?
C16 C18 Ag16 100(3) . . ?
C15 C19 H19A 109.5 . . ?
C15 C19 H19B 109.5 . . ?
C15 C19 H19C 109.5 . . ?
H19A C19 H19B 109.5 . . ?
H19A C19 H19C 109.5 . . ?
H19B C19 H19C 109.5 . . ?
Ag11 C20 Ag5 85.5(15) . . ?
Ag11 C20 Ag19 86.6(14) . . ?
Ag19 C20 Ag5 88.3(14) . . ?
C26 C20 Ag5 122(3) . . ?
C26 C20 Ag11 140(3) . . ?
C26 C20 Ag19 119(3) . . ?
H21A C21 H21B 109.5 . . ?
H21A C21 H21C 109.5 . . ?
H21B C21 H21C 109.5 . . ?
C57 C21 H21A 109.5 . . ?
C57 C21 H21B 109.5 . . ?
C57 C21 H21C 109.5 . . ?
C4 C22 C35 107(4) . . ?
C4 C22 C58 115(3) . . ?
C4 C22 C96 111(3) . . ?
C35 C22 C58 103(4) . . ?
C35 C22 C96 104(3) . . ?
C58 C22 C96 116(3) . . ?
H23A C23 H23B 109.5 . . ?
H23A C23 H23C 109.5 . . ?
H23B C23 H23C 109.5 . . ?
C43 C23 H23A 109.5 . . ?
C43 C23 H23B 109.5 . . ?
C43 C23 H23C 109.5 . . ?
H24A C24 H24B 108.3 . . ?
H24A C24 H24C 97.8 . . ?
H24B C24 H24C 109.5 . . ?
C80 C24 H24A 121.7 . . ?
C80 C24 H24B 109.4 . . ?
C80 C24 H24C 109.3 . . ?
C92 C25 C68 175(5) . . ?
C20 C26 C76 172(5) . . ?
H27A C27 H27B 109.5 . . ?
H27A C27 H27C 109.5 . . ?
H27B C27 H27C 109.5 . . ?
C76 C27 H27A 109.5 . . ?
C76 C27 H27B 109.5 . . ?
C76 C27 H27C 109.5 . . ?
Ag6 C28 Ag2 81.3(13) . . ?
Ag23 C28 Ag2 81.7(16) . . ?
Ag23 C28 Ag6 84.5(14) . . ?
C42 C28 Ag2 107(4) . . ?
C42 C28 Ag6 138(4) . . ?
C42 C28 Ag23 137(4) . . ?
C12 C29 H29A 109.5 . . ?
C12 C29 H29B 109.5 . . ?
C12 C29 H29C 109.5 . . ?
H29A C29 H29B 109.5 . . ?
H29A C29 H29C 109.5 . . ?
H29B C29 H29C 109.5 . . ?
C5 C30 C41 110(4) . . ?
C5 C30 C44 106(4) . . ?
C5 C30 C79 96(4) . . ?
C41 C30 C79 121(4) . . ?
C44 C30 C41 115(4) . . ?
C44 C30 C79 106(4) . . ?
H31A C31 H31B 109.5 . . ?
H31A C31 H31C 109.5 . . ?
H31B C31 H31C 109.5 . . ?
C76 C31 H31A 109.5 . . ?
C76 C31 H31B 109.5 . . ?
C76 C31 H31C 109.5 . . ?
Ag7 C32 Ag6 80.0(12) . . ?
Ag7 C32 Ag12 83.4(16) . . ?
Ag12 C32 Ag6 117.7(17) . . ?
C36 C32 Ag6 90(3) . . ?
C36 C32 Ag7 164(4) . . ?
C36 C32 Ag12 112(3) . . ?
H33A C33 H33B 109.5 . . ?
H33A C33 H33C 109.5 . . ?
H33B C33 H33C 109.5 . . ?
C90 C33 H33A 109.5 . . ?
C90 C33 H33B 109.5 . . ?
C90 C33 H33C 109.5 . . ?
C6 C34 C49 108(3) . . ?
C6 C34 C67 110(4) . . ?
C61 C34 C6 113(3) . . ?
C61 C34 C49 110(4) . . ?
C61 C34 C67 107(4) . . ?
C67 C34 C49 109(3) . . ?
C22 C35 H35A 109.5 . . ?
C22 C35 H35B 109.5 . . ?
C22 C35 H35C 109.5 . . ?
H35A C35 H35B 109.5 . . ?
H35A C35 H35C 109.5 . . ?
H35B C35 H35C 109.5 . . ?
C32 C36 C87 172(5) . . ?
C15 C37 H37A 109.5 . . ?
C15 C37 H37B 109.5 . . ?
C15 C37 H37C 109.5 . . ?
H37A C37 H37B 109.5 . . ?
H37A C37 H37C 109.5 . . ?
H37B C37 H37C 109.5 . . ?
Ag15 C38 Ag10 83.8(13) . . ?
C4 C38 Ag10 110(3) . . ?
C4 C38 Ag15 166(3) . . ?
H39A C39 H39B 109.5 . . ?
H39A C39 H39C 109.5 . . ?
H39B C39 H39C 109.5 . . ?
C68 C39 H39A 109.5 . . ?
C68 C39 H39B 109.5 . . ?
C68 C39 H39C 109.5 . . ?
C52 C40 C64 168(4) . . ?
C30 C41 H41A 109.5 . . ?
C30 C41 H41B 109.5 . . ?
C30 C41 H41C 109.5 . . ?
H41A C41 H41B 109.5 . . ?
H41A C41 H41C 109.5 . . ?
H41B C41 H41C 109.5 . . ?
C28 C42 C43 178(7) . . ?
C42 C43 C23 108(4) . . ?
C42 C43 C45 112(4) . . ?
C42 C43 C89 107(3) . . ?
C45 C43 C23 87(4) . . ?
C45 C43 C89 126(4) . . ?
C89 C43 C23 115(4) . . ?
C60 C44 C30 178(5) . . ?
C43 C45 H45A 109.5 . . ?
C43 C45 H45B 109.5 . . ?
C43 C45 H45C 109.5 . . ?
H45A C45 H45B 109.5 . . ?
H45A C45 H45C 109.5 . . ?
H45B C45 H45C 109.5 . . ?
Ag3 C46 Ag21 82.5(13) . . ?
Ag5 C46 Ag3 84.1(13) . . ?
Ag5 C46 Ag21 81.8(13) . . ?
C73 C46 Ag3 134(3) . . ?
C73 C46 Ag5 135(3) . . ?
C73 C46 Ag21 121(3) . . ?
H47A C47 H47B 92.8 . . ?
H47A C47 H47C 107.6 . . ?
H47B C47 H47C 109.5 . . ?
C85 C47 H47A 114.4 . . ?
C85 C47 H47B 119.1 . . ?
C85 C47 H47C 111.6 . . ?
C70 C48 C54 175(5) . . ?
C34 C49 H49A 109.5 . . ?
C34 C49 H49B 109.5 . . ?
C34 C49 H49C 109.5 . . ?
H49A C49 H49B 109.5 . . ?
H49A C49 H49C 109.5 . . ?
H49B C49 H49C 109.5 . . ?
C66 C50 C57 170(5) . . ?
C12 C51 H51A 109.5 . . ?
C12 C51 H51B 109.5 . . ?
C12 C51 H51C 109.5 . . ?
H51A C51 H51B 109.5 . . ?
H51A C51 H51C 109.5 . . ?
H51B C51 H51C 109.5 . . ?
Ag22 C52 Ag8 84.7(14) . . ?
C40 C52 Ag8 101(3) . . ?
C40 C52 Ag22 171(4) . . ?
H53A C53 H53B 108.8 . . ?
H53A C53 H53C 109.5 . . ?
H53B C53 H53C 98.4 . . ?
C80 C53 H53A 109.5 . . ?
C80 C53 H53B 120.5 . . ?
C80 C53 H53C 109.4 . . ?
C2 C54 C48 110(4) . . ?
C2 C54 C86 105(4) . . ?
C65 C54 C2 117(5) . . ?
C65 C54 C48 111(4) . . ?
C65 C54 C86 102(4) . . ?
C86 C54 C48 111(4) . . ?
H55A C55 H55B 109.5 . . ?
H55A C55 H55C 109.5 . . ?
H55B C55 H55C 109.5 . . ?
C76 C55 H55A 109.5 . . ?
C76 C55 H55B 109.5 . . ?
C76 C55 H55C 109.5 . . ?
Ag2 C56 Ag12 89.2(16) . . ?
Ag2 C56 Ag17 93.4(18) . . ?
Ag17 C56 Ag12 93.2(19) . . ?
C74 C56 Ag2 153(5) . . ?
C74 C56 Ag12 114(4) . . ?
C74 C56 Ag17 98(4) . . ?
C21 C57 C81 100(3) . . ?
C50 C57 C21 111(4) . . ?
C50 C57 C81 103(4) . . ?
C83 C57 C21 105(5) . . ?
C83 C57 C50 130(5) . . ?
C83 C57 C81 104(4) . . ?
C22 C58 H58A 109.5 . . ?
C22 C58 H58B 109.5 . . ?
C22 C58 H58C 109.5 . . ?
H58A C58 H58B 109.5 . . ?
H58A C58 H58C 109.5 . . ?
H58B C58 H58C 109.5 . . ?
H59A C59 H59B 109.5 . . ?
H59A C59 H59C 109.5 . . ?
H59B C59 H59C 109.5 . . ?
C68 C59 H59A 109.5 . . ?
C68 C59 H59B 109.5 . . ?
C68 C59 H59C 109.5 . . ?
Ag21 C60 Ag10 84.2(14) . . ?
Ag21 C60 Ag23 86.1(15) . . ?
Ag23 C60 Ag10 85.4(15) . . ?
C44 C60 Ag10 135(4) . . ?
C44 C60 Ag21 129(4) . . ?
C44 C60 Ag23 121(3) . . ?
C34 C61 H61A 109.5 . . ?
C34 C61 H61B 109.5 . . ?
C34 C61 H61C 109.5 . . ?
H61A C61 H61B 109.5 . . ?
H61A C61 H61C 109.5 . . ?
H61B C61 H61C 109.5 . . ?
C3 C62 C14 107(3) . . ?
C3 C62 C88 112(3) . . ?
C13 C62 C3 100(4) . . ?
C13 C62 C14 115(3) . . ?
C13 C62 C88 113(3) . . ?
C14 C62 C88 109(3) . . ?
C12 C63 H63A 109.5 . . ?
C12 C63 H63B 109.5 . . ?
C12 C63 H63C 109.5 . . ?
H63A C63 H63B 109.5 . . ?
H63A C63 H63C 109.5 . . ?
H63B C63 H63C 109.5 . . ?
C40 C64 C69 106(3) . . ?
C40 C64 C84 100(3) . . ?
C69 C64 C84 107(3) . . ?
C94 C64 C40 113(4) . . ?
C94 C64 C69 114(4) . . ?
C94 C64 C84 115(4) . . ?
C54 C65 H65A 109.5 . . ?
C54 C65 H65B 109.5 . . ?
C54 C65 H65C 109.5 . . ?
H65A C65 H65B 109.5 . . ?
H65A C65 H65C 109.5 . . ?
H65B C65 H65C 109.5 . . ?
Ag9 C66 Ag8 85.0(16) . . ?
Ag9 C66 Ag18 94(2) . . ?
Ag18 C66 Ag8 88.4(18) . . ?
C50 C66 Ag8 128(4) . . ?
C50 C66 Ag9 143(4) . . ?
C50 C66 Ag18 102(4) . . ?
C34 C67 H67A 109.5 . . ?
C34 C67 H67B 109.5 . . ?
C34 C67 H67C 109.5 . . ?
H67A C67 H67B 109.5 . . ?
H67A C67 H67C 109.5 . . ?
H67B C67 H67C 109.5 . . ?
C7 C68 C39 114(3) . . ?
C7 C68 C59 115(4) . . ?
C25 C68 C7 106(4) . . ?
C25 C68 C39 105(4) . . ?
C25 C68 C59 113(3) . . ?
C59 C68 C39 104(3) . . ?
C64 C69 H69A 109.5 . . ?
C64 C69 H69B 109.5 . . ?
C64 C69 H69C 109.5 . . ?
H69A C69 H69B 109.5 . . ?
H69A C69 H69C 109.5 . . ?
H69B C69 H69C 109.5 . . ?
Ag11 C70 Ag8 85.5(16) . 2_666 ?
Ag17 C70 Ag8 86.5(17) . 2_666 ?
Ag17 C70 Ag11 86.8(19) . . ?
C48 C70 Ag8 122(4) . 2_666 ?
C48 C70 Ag11 125(5) . . ?
C48 C70 Ag17 136(4) . . ?
C10 C71 C80 170(4) . . ?
C15 C72 C82 170(5) . . ?
C46 C73 C12 175(4) . . ?
C56 C74 C85 165(7) . . ?
C15 C75 H75A 109.5 . . ?
C15 C75 H75B 109.5 . . ?
C15 C75 H75C 109.5 . . ?
H75A C75 H75B 109.5 . . ?
H75A C75 H75C 109.5 . . ?
H75B C75 H75C 109.5 . . ?
C26 C76 C27 110(4) . . ?
C26 C76 C31 109(4) . . ?
C26 C76 C55 107(4) . . ?
C27 C76 C31 104(4) . . ?
C27 C76 C55 110(4) . . ?
C31 C76 C55 117(4) . . ?
H77A C77 H77B 109.5 . . ?
H77A C77 H77C 105.9 . . ?
H77B C77 H77C 98.2 . . ?
C85 C77 H77A 109.3 . . ?
C85 C77 H77B 108.7 . . ?
C85 C77 H77C 124.3 . . ?
H78A C78 H78B 109.5 . . ?
H78A C78 H78C 109.5 . . ?
H78B C78 H78C 109.5 . . ?
C80 C78 H78A 109.5 . . ?
C80 C78 H78B 109.5 . . ?
C80 C78 H78C 109.5 . . ?
C30 C79 H79A 109.5 . . ?
C30 C79 H79B 109.5 . . ?
C30 C79 H79C 109.5 . . ?
H79A C79 H79B 109.5 . . ?
H79A C79 H79C 109.5 . . ?
H79B C79 H79C 109.5 . . ?
C24 C80 C53 97(3) . . ?
C24 C80 C78 111(3) . . ?
C71 C80 C24 118(3) . . ?
C71 C80 C53 108(3) . . ?
C71 C80 C78 112(3) . . ?
C78 C80 C53 111(3) . . ?
C57 C81 H81A 109.8 . . ?
C57 C81 H81B 108.4 . . ?
C57 C81 H81C 110.1 . . ?
H81A C81 H81B 109.5 . . ?
H81A C81 H81C 109.5 . . ?
H81B C81 H81C 109.5 . . ?
Ag13 C82 Ag12 81.5(16) . 2_666 ?
Ag18 C82 Ag12 89.6(15) . 2_666 ?
Ag18 C82 Ag13 87.8(15) . . ?
C72 C82 Ag12 129(4) . 2_666 ?
C72 C82 Ag13 104(4) . . ?
C72 C82 Ag18 140(4) . . ?
C57 C83 H83A 107.7 . . ?
C57 C83 H83B 111.6 . . ?
C57 C83 H83C 109.1 . . ?
H83A C83 H83B 109.5 . . ?
H83A C83 H83C 109.5 . . ?
H83B C83 H83C 109.5 . . ?
C64 C84 H84A 109.5 . . ?
C64 C84 H84B 109.5 . . ?
C64 C84 H84C 109.5 . . ?
H84A C84 H84B 109.5 . . ?
H84A C84 H84C 109.5 . . ?
H84B C84 H84C 109.5 . . ?
C74 C85 C47 109(5) . . ?
C74 C85 C77 115(5) . . ?
C77 C85 C47 98(4) . . ?
C95 C85 C47 105(5) . . ?
C95 C85 C74 110(5) . . ?
C95 C85 C77 119(5) . . ?
C54 C86 H86A 109.5 . . ?
C54 C86 H86B 109.5 . . ?
C54 C86 H86C 109.5 . . ?
H86A C86 H86B 109.5 . . ?
H86A C86 H86C 109.5 . . ?
H86B C86 H86C 109.5 . . ?
C11 C87 C36 114(4) . . ?
C11 C87 C93 106(4) . . ?
C91 C87 C11 110(3) . . ?
C91 C87 C36 102(3) . . ?
C91 C87 C93 112(4) . . ?
C93 C87 C36 114(3) . . ?
C62 C88 H88A 109.5 . . ?
C62 C88 H88B 109.5 . . ?
C62 C88 H88C 109.5 . . ?
H88A C88 H88B 109.5 . . ?
H88A C88 H88C 109.5 . . ?
H88B C88 H88C 109.5 . . ?
C43 C89 H89A 109.5 . . ?
C43 C89 H89B 109.5 . . ?
C43 C89 H89C 109.5 . . ?
H89A C89 H89B 109.5 . . ?
H89A C89 H89C 109.5 . . ?
H89B C89 H89C 109.5 . . ?
C9 C90 C17 108(4) . . ?
C16 C90 C9 107(4) . . ?
C16 C90 C17 106(4) . . ?
C16 C90 C33 112(4) . . ?
C33 C90 C9 114(4) . . ?
C33 C90 C17 110(4) . . ?
C87 C91 H91A 109.5 . . ?
C87 C91 H91B 109.5 . . ?
C87 C91 H91C 109.5 . . ?
H91A C91 H91B 109.5 . . ?
H91A C91 H91C 109.5 . . ?
H91B C91 H91C 109.5 . . ?
Ag20 C92 Ag5 82.7(12) . . ?
C25 C92 Ag5 103(3) . . ?
C25 C92 Ag20 174(4) . . ?
C87 C93 H93A 109.5 . . ?
C87 C93 H93B 109.5 . . ?
C87 C93 H93C 109.5 . . ?
H93A C93 H93B 109.5 . . ?
H93A C93 H93C 109.5 . . ?
H93B C93 H93C 109.5 . . ?
C64 C94 H94A 109.5 . . ?
C64 C94 H94B 109.5 . . ?
C64 C94 H94C 109.5 . . ?
H94A C94 H94B 109.5 . . ?
H94A C94 H94C 109.5 . . ?
H94B C94 H94C 109.5 . . ?
C85 C95 H95A 109.5 . . ?
C85 C95 H95B 109.5 . . ?
C85 C95 H95C 109.5 . . ?
H95A C95 H95B 109.5 . . ?
H95A C95 H95C 109.5 . . ?
H95B C95 H95C 109.5 . . ?
C22 C96 H96A 109.5 . . ?
C22 C96 H96B 109.5 . . ?
C22 C96 H96C 109.5 . . ?
H96A C96 H96B 109.5 . . ?
H96A C96 H96C 109.5 . . ?
H96B C96 H96C 109.5 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Ag2 C56 C74 C85 55(29) . . . . ?
Ag12 C56 C74 C85 -94(22) . . . . ?
Ag17 C56 C74 C85 169(21) . . . . ?
C15 C72 C82 Ag12 24(38) . . . 2_666 ?
C15 C72 C82 Ag13 114(34) . . . . ?
C15 C72 C82 Ag18 -141(32) . . . . ?
C19 C15 C72 C82 -124(34) . . . . ?
C37 C15 C72 C82 -12(37) . . . . ?
C52 C40 C64 C69 -107(20) . . . . ?
C52 C40 C64 C84 142(19) . . . . ?
C52 C40 C64 C94 18(21) . . . . ?
C56 C74 C85 C47 4(24) . . . . ?
C56 C74 C85 C77 -106(23) . . . . ?
C56 C74 C85 C95 118(22) . . . . ?
C57 C50 C66 Ag8 145(29) . . . . ?
C57 C50 C66 Ag9 -5(38) . . . . ?
C57 C50 C66 Ag18 -118(32) . . . . ?
C64 C40 C52 Ag8 80(20) . . . . ?
C66 C50 C57 C21 -93(32) . . . . ?
C66 C50 C57 C81 161(31) . . . . ?
C66 C50 C57 C83 39(35) . . . . ?
C75 C15 C72 C82 122(34) . . . . ?

_smtbx_masks_special_details     ?
loop_
_smtbx_masks_void_nr
_smtbx_masks_void_average_x
_smtbx_masks_void_average_y
_smtbx_masks_void_average_z
_smtbx_masks_void_volume
_smtbx_masks_void_count_electrons
_smtbx_masks_void_content
1 0.156 0.879 0.470 21.0 1.0 ?
2 0.500 1.000 1.000 433.4 179.6 ?
3 0.218 0.574 0.922 14.7 0.4 ?
4 0.212 0.791 0.178 10.9 0.0 ?
5 0.782 0.426 0.078 14.7 0.0 ?
6 0.788 0.209 0.822 10.9 0.0 ?
7 0.844 0.121 0.530 21.0 1.3 ?

_smtbx_masks_void_probe_radius   1.2
_smtbx_masks_void_truncation_radius 1.2
_olex2_submission_special_instructions 'No special instructions were received'
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_910_a
_database_code_depnum_ccdc_archive 'CCDC 2278735'
loop_
_audit_author_name
_audit_author_address
'Zhan-Guo Jiang'
;Zhejiang Normal Univesity
China
;
_audit_update_record             
;
2023-07-03 deposited with the CCDC.	2023-08-28 downloaded from the CCDC.
;
_audit_creation_date             2023-06-07
_audit_creation_method           
;
Olex2 1.5
(compiled 2021.08.20 svn.r13c46975 for OlexSys, GUI svn.r6392)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C360 H540 Ag148 Br30 S26'
_chemical_formula_sum            'C360 H540 Ag148 Br30 S26'
_chemical_formula_weight         24063.51
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Br Br -0.2901 2.4595 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      tetragonal
_space_group_IT_number           128
_space_group_name_H-M_alt        'P 4/m n c'
_space_group_name_Hall           '-P 4 2n'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, z'
'-y, x, z'
'y, -x, z'
'-x+1/2, y+1/2, -z+1/2'
'x+1/2, -y+1/2, -z+1/2'
'y+1/2, x+1/2, -z+1/2'
'-y+1/2, -x+1/2, -z+1/2'
'-x, -y, -z'
'x, y, -z'
'y, -x, -z'
'-y, x, -z'
'x-1/2, -y-1/2, z-1/2'
'-x-1/2, y-1/2, z-1/2'
'-y-1/2, -x-1/2, z-1/2'
'y-1/2, x-1/2, z-1/2'

_cell_length_a                   30.517(4)
_cell_length_b                   30.517(4)
_cell_length_c                   35.190(6)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_volume                     32773(11)
_cell_formula_units_Z            2
_cell_measurement_reflns_used    7359
_cell_measurement_temperature    150.0
_cell_measurement_theta_max      17.96
_cell_measurement_theta_min      2.21
_shelx_estimated_absorpt_T_max   0.574
_shelx_estimated_absorpt_T_min   0.521
_exptl_absorpt_coefficient_mu    6.242
_exptl_absorpt_correction_T_max  0.574
_exptl_absorpt_correction_T_min  0.521
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   ?
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            red
_exptl_crystal_colour_primary    red
_exptl_crystal_density_diffrn    2.439
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             22244
_exptl_crystal_size_max          0.12
_exptl_crystal_size_mid          0.11
_exptl_crystal_size_min          0.1
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0919
_diffrn_reflns_av_unetI/netI     0.0565
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.999
_diffrn_reflns_limit_h_max       25
_diffrn_reflns_limit_h_min       -27
_diffrn_reflns_limit_k_max       27
_diffrn_reflns_limit_k_min       -27
_diffrn_reflns_limit_l_max       31
_diffrn_reflns_limit_l_min       -31
_diffrn_reflns_number            58977
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.999
_diffrn_reflns_theta_full        18.847
_diffrn_reflns_theta_max         18.847
_diffrn_reflns_theta_min         0.883
_diffrn_ambient_temperature      150.0
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'BRUKER D8 VENTURE'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_diffrn_standards_number         0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                4408
_reflns_number_total             6603
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       ?
_computing_data_collection       ?
_computing_data_reduction        ?
_computing_molecular_graphics    'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2018/3 (Sheldrick, 2015)'
_computing_structure_solution    'SHELXT 2014/5 (Sheldrick, 2014)'
_refine_diff_density_max         5.209
_refine_diff_density_min         -2.025
_refine_diff_density_rms         0.470
_refine_ls_extinction_coef       0.00025(4)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     'SHELXL-2018/3 (Sheldrick 2018)'
_refine_ls_goodness_of_fit_ref   1.511
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     671
_refine_ls_number_reflns         6603
_refine_ls_number_restraints     1148
_refine_ls_R_factor_all          0.1586
_refine_ls_R_factor_gt           0.1233
_refine_ls_restrained_S_all      1.388
_refine_ls_shift/su_max          0.090
_refine_ls_shift/su_mean         0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.2000P)²] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.3418
_refine_ls_wR_factor_ref         0.3783
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.5 times of:
  All C(H,H,H) groups
2. Restrained distances
 C20-C22 = C22-C24
 1.54 with sigma of 0.02
 C32-C36 = C32-C38
 1.55 with sigma of 0.02
 C17-C35 = C35-C9
 1.54 with sigma of 0.02
 C35-C37 = C35-C19
 1.55 with sigma of 0.02
 C30-C32 = C32-C34
 1.54 with sigma of 0.02
 C22-C26 = C22-C28
 1.55 with sigma of 0.02
 C40-C42 = C42-C44
 1.54 with sigma of 0.02
 C42-C46 = C42-C48
 1.55 with sigma of 0.02
 C50-C52 = C52-C54
 1.54 with sigma of 0.02
 C52-C27 = C52-C7
 1.55 with sigma of 0.02
 C29-C15 = C15-C31
 1.54 with sigma of 0.02
 C15-C2 = C15-C33
 1.55 with sigma of 0.02
 C39-C5 = C5-C41
 1.54 with sigma of 0.02
 C5-C21 = C5-C43
 1.55 with sigma of 0.02
 C25-C51 = C51-C13
 1.54 with sigma of 0.02
 C23-C47 = C47-C3
 1.54 with sigma of 0.02
 C47-C49
 1.55 with sigma of 0.02
 C51-C53
 1.55 with sigma of 0.02
 C4-C37
 1.2 with sigma of 0.02
 C30-C36 = C30-C38
 2.52 with sigma of 0.04
 C17-C37 = C17-C19
 2.52 with sigma of 0.04
 C30-C34
 2.56 with sigma of 0.04
 C17-C9
 2.56 with sigma of 0.04
 C40-C46 = C40-C48
 2.52 with sigma of 0.04
 C20-C26 = C20-C28
 2.52 with sigma of 0.04
 C29-C2 = C29-C33
 2.52 with sigma of 0.04
 C50-C27 = C50-C7
 2.52 with sigma of 0.04
 C20-C24
 2.56 with sigma of 0.04
 C40-C44
 2.56 with sigma of 0.04
 C50-C54
 2.56 with sigma of 0.04
 C29-C31
 2.56 with sigma of 0.04
 C39-C41
 2.56 with sigma of 0.04
 C39-C21 = C39-C43
 2.52 with sigma of 0.04
 C25-C13
 2.56 with sigma of 0.04
 C25-C53
 2.52 with sigma of 0.04
 C23-C3
 2.56 with sigma of 0.04
 C23-C49
 2.52 with sigma of 0.04
 C32-C34 \\sim C32-C36 \\sim C32-C38 \\sim C32-C30
 with sigma of 0.02
 C34-C36 \\sim C34-C38 \\sim C36-C38
 with sigma of 0.04
 C30-C34 \\sim C30-C36 \\sim C30-C38
 with sigma of 0.04
 C35-C9 \\sim C35-C37 \\sim C35-C19 \\sim C35-C17
 with sigma of 0.02
 C9-C37 \\sim C9-C19 \\sim C37-C19
 with sigma of 0.04
 C17-C9 \\sim C17-C37 \\sim C17-C19
 with sigma of 0.04
 C22-C24 \\sim C22-C26 \\sim C22-C28 \\sim C22-C20
 with sigma of 0.02
 C24-C26 \\sim C24-C28 \\sim C26-C28
 with sigma of 0.04
 C20-C24 \\sim C20-C26 \\sim C20-C28
 with sigma of 0.04
 C42-C44 \\sim C42-C46 \\sim C42-C48 \\sim C42-C40
 with sigma of 0.02
 C44-C46 \\sim C44-C48 \\sim C46-C48
 with sigma of 0.04
 C40-C44 \\sim C40-C46 \\sim C40-C48
 with sigma of 0.04
 C52-C54 \\sim C52-C27 \\sim C52-C7 \\sim C52-C50
 with sigma of 0.02
 C54-C27 \\sim C54-C7 \\sim C27-C7
 with sigma of 0.04
 C50-C54 \\sim C50-C27 \\sim C50-C7
 with sigma of 0.04
 C15-C31 \\sim C15-C2 \\sim C15-C33 \\sim C15-C29
 with sigma of 0.02
 C31-C2 \\sim C31-C33 \\sim C2-C33
 with sigma of 0.04
 C29-C31 \\sim C29-C2 \\sim C29-C33
 with sigma of 0.04
 C41-C21 \\sim C41-C43 \\sim C21-C43
 with sigma of 0.04
 C39-C41 \\sim C39-C21 \\sim C39-C43
 with sigma of 0.04
 C5-C41 \\sim C5-C21 \\sim C5-C43 \\sim C5-C39
 with sigma of 0.02
 C47-C3 \\sim C47-C49 \\sim C47-C23
 with sigma of 0.02
 C25-C13 \\sim C25-C53
 with sigma of 0.04
 C23-C3 \\sim C23-C49
 with sigma of 0.04
 C51-C13 \\sim C51-C53 \\sim C51-C25
 with sigma of 0.02
3. Uiso/Uaniso restraints and constraints
C1 \\sim C2 \\sim C3 \\sim C4 \\sim C5 \\sim C6 \\sim C7 \\sim C8 \\sim C9
\\sim C10 \\sim C12 \\sim C13 \\sim C14 \\sim C15 \\sim C16 \\sim C17 \\sim C18
\\sim C19 \\sim C20 \\sim C21 \\sim C22 \\sim C23 \\sim C24 \\sim C25 \\sim C26
\\sim C27 \\sim C28 \\sim C29 \\sim C30 \\sim C31 \\sim C32 \\sim C33 \\sim C34
\\sim C35 \\sim C36 \\sim C37 \\sim C38 \\sim C39 \\sim C40 \\sim C41 \\sim C42
\\sim C43 \\sim C44 \\sim C46 \\sim C47 \\sim C48 \\sim C49 \\sim C50 \\sim C51
\\sim C52 \\sim C53 \\sim C54: within 3.8A with sigma of 0.001 and sigma for
terminal atoms of 0.002 within 3.8A
C30 \\sim C32 \\sim C34 \\sim C36 \\sim C38: within 2A with sigma of 0.04 and
sigma for terminal atoms of 0.08 within 2A
C9 \\sim C17 \\sim C19 \\sim C35 \\sim C37: within 2A with sigma of 0.04 and
sigma for terminal atoms of 0.08 within 2A
C7 \\sim C27 \\sim C50 \\sim C52 \\sim C54: within 2A with sigma of 0.04 and
sigma for terminal atoms of 0.08 within 2A
C20 \\sim C22 \\sim C24 \\sim C26 \\sim C28: within 2A with sigma of 0.04 and
sigma for terminal atoms of 0.08 within 2A
C40 \\sim C42 \\sim C44 \\sim C46 \\sim C48: within 2A with sigma of 0.04 and
sigma for terminal atoms of 0.08 within 2A
C2 \\sim C15 \\sim C29 \\sim C31 \\sim C33: within 2A with sigma of 0.04 and
sigma for terminal atoms of 0.08 within 2A
C5 \\sim C21 \\sim C39 \\sim C41 \\sim C43: within 2A with sigma of 0.04 and
sigma for terminal atoms of 0.08 within 2A
C13 \\sim C25 \\sim C51 \\sim C53: within 2A with sigma of 0.04 and sigma for
terminal atoms of 0.08 within 2A
C3 \\sim C23 \\sim C47 \\sim C49: within 2A with sigma of 0.04 and sigma for
terminal atoms of 0.08 within 2A
4. Rigid body (RIGU) restrains
 C30, C32, C34, C36, C38
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 C9, C17, C19, C35, C37
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 C20, C22, C24, C26, C28
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 C2, C15, C29, C31, C33
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 C40, C42, C44, C46, C48
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 C7, C27, C50, C52, C54
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 C5, C21, C39, C41, C43
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 C13, C25, C51, C53
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 C3, C23, C47, C49
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
5. Others
 Fixed Sof: C9(0.5) H9A(0.5) H9B(0.5) H9C(0.5) C17(0.5) H17A(0.5) H17B(0.5)
 H17C(0.5) C19(0.5) H19A(0.5) H19B(0.5) H19C(0.5) H23A(0.5) H23B(0.5) H23C(0.5)
 H25A(0.5) H25B(0.5) H25C(0.5)
 Fixed X: C9(0.91414) C17(0.976969) C19(0.95515)
 Fixed Y: C9(0.625701) C17(0.572929) C19(0.59107)
 Fixed Z: C9(0.513161) C17(0.5265) C19(0.45912)
6.a Riding coordinates:
 C2(H2A,H2B,H2C), C7(H7A,H7B,H7C), C9(H9A,H9B,H9C), C17(H17A,H17B,H17C),
 C19(H19A,H19B,H19C), C21(H21A,H21B,H21C), C23(H23A,H23B,H23C), C24(H24A,H24B,
 H24C), C25(H25A,H25B,H25C), C26(H26A,H26B,H26C), C27(H27A,H27B,H27C), C28(H28A,
 H28B,H28C), C29(H29A,H29B,H29C), C33(H33A,H33B,H33C), C34(H34A,H34B,H34C),
 C36(H36A,H36B,H36C), C38(H38A,H38B,H38C), C39(H39A,H39B,H39C), C40(H40A,H40B,
 H40C), C43(H43A,H43B,H43C), C44(H44A,H44B,H44C), C48(H48A,H48B,H48C), C49(H49A,
 H49B,H49C), C50(H50A,H50B,H50C), C53(H53A,H53B,H53C)
;
_atom_sites_solution_hydrogens   difmap
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.76477(13) 0.41823(15) 0.500000 0.0927(16) Uani 1 2 d S T P . .
Ag2 Ag 0.62817(15) 0.41276(15) 0.500000 0.0967(16) Uani 1 2 d S T P . .
Ag3 Ag 0.45920(16) 0.31014(19) 0.35985(16) 0.172(2) Uani 1 1 d . . . . .
Ag4 Ag 0.61513(14) 0.36161(11) 0.42870(13) 0.1177(14) Uani 1 1 d . . . . .
Ag5 Ag 0.44935(13) 0.45113(13) 0.32932(12) 0.1161(14) Uani 1 1 d . . . . .
Ag6 Ag 0.43006(14) 0.49637(13) 0.23206(12) 0.1254(15) Uani 1 1 d . . . . .
Ag7 Ag 0.85264(14) 0.45387(15) 0.500000 0.0945(15) Uani 1 2 d S T P . .
Ag8 Ag 0.50265(12) 0.39847(15) 0.38871(12) 0.1218(15) Uani 1 1 d . . . . .
Ag9 Ag 0.49469(12) 0.23755(10) 0.40698(11) 0.1034(13) Uani 1 1 d . . . . .
Ag10 Ag 0.80785(12) 0.40552(13) 0.41982(16) 0.1404(19) Uani 1 1 d . . . . .
Ag11 Ag 0.59036(16) 0.27021(13) 0.43964(18) 0.162(2) Uani 1 1 d . . . . .
Ag12 Ag 0.67501(18) 0.3070(2) 0.500000 0.133(2) Uani 1 2 d S T P . .
Ag13 Ag 0.3757(2) 0.3475(2) 0.32532(19) 0.200(3) Uani 1 1 d . . . . .
Ag14 Ag 0.65956(13) 0.51300(17) 0.54191(12) 0.1353(17) Uani 1 1 d . . . . .
Ag15 Ag 0.60432(15) 0.20327(15) 0.500000 0.0967(16) Uani 1 2 d S T P . .
Ag16 Ag 0.39053(15) 0.41579(16) 0.25918(12) 0.1359(16) Uani 1 1 d . . . . .
Ag17 Ag 0.53412(12) 0.16495(11) 0.44957(11) 0.1018(13) Uani 1 1 d . . . . .
Ag18 Ag 0.72875(15) 0.36455(15) 0.37623(13) 0.1331(16) Uani 1 1 d . . . . .
Ag19 Ag 0.55066(13) 0.43497(14) 0.45378(11) 0.1156(14) Uani 1 1 d . . . . .
Ag20 Ag 0.76023(16) 0.32485(15) 0.45540(14) 0.1408(17) Uani 1 1 d . . . . .
Ag21 Ag 0.33673(17) 0.42995(17) 0.34332(13) 0.1497(18) Uani 1 1 d . . . . .
Br1 Br 0.37125(15) 0.51435(17) 0.29473(14) 0.1044(16) Uani 1 1 d . . . . .
Br2 Br 0.500000 0.500000 0.4232(5) 0.148(5) Uani 1 4 d S T P . .
Br3 Br 0.74874(16) 0.50714(16) 0.500000 0.0709(16) Uani 1 2 d S T P . .
Br4 Br 0.70052(12) 0.41109(13) 0.44562(12) 0.0793(13) Uani 1 1 d . . . . .
Br5 Br 0.66704(16) 0.29900(15) 0.39663(16) 0.1078(17) Uani 1 1 d . . . . .
S1 S 0.6020(4) 0.3343(4) 0.500000 0.071(4) Uani 1 2 d S T P . .
S2 S 0.5986(4) 0.4904(4) 0.500000 0.074(4) Uani 1 2 d S T P . .
S3 S 0.500000 0.500000 0.2945(6) 0.072(5) Uani 1 4 d S T P . .
S4 S 0.4220(3) 0.4148(3) 0.3871(3) 0.077(3) Uani 1 1 d . . . . .
S5 S 0.5283(3) 0.3079(3) 0.3948(3) 0.077(3) Uani 1 1 d . . . . .
C1 C 0.8244(19) 0.472(3) 0.406(2) 0.190(6) Uani 1 1 d . U . . .
C2 C 0.9406(14) 0.4554(19) 0.4179(11) 0.190(6) Uani 1 1 d D U . . .
H2A H 0.950384 0.484872 0.424895 0.285 Uiso 1 1 d R U . . .
H2B H 0.966124 0.437122 0.411955 0.285 Uiso 1 1 d R U . . .
H2C H 0.924494 0.442372 0.439235 0.285 Uiso 1 1 d R U . . .
C3 C 0.858(2) 0.354(3) 0.500000 0.195(4) Uani 1 2 d DS TU P . .
C4 C 0.8809(17) 0.5163(15) 0.500000 0.109(5) Uani 1 2 d DS TU P . .
C5 C 0.4249(15) 0.2117(14) 0.2785(15) 0.265(6) Uani 1 1 d D U . . .
C6 C 0.829(3) 0.387(3) 0.500000 0.195(4) Uani 1 2 d S TU P . .
C7 C 0.7915(17) 0.2702(18) 0.3194(14) 0.195(4) Uani 1 1 d D U . . .
H7A H 0.800431 0.244841 0.304206 0.292 Uiso 1 1 d R U . . .
H7B H 0.799891 0.297221 0.306266 0.292 Uiso 1 1 d R U . . .
H7C H 0.759641 0.269681 0.322976 0.292 Uiso 1 1 d R U . . .
C8 C 0.427(3) 0.567(3) 0.203(4) 0.280(6) Uani 1 1 d . U . . .
C9 C 0.914140 0.625701 0.513161 0.109(5) Uani 0.5 1 d D U P A -1
H9A H 0.916460 0.628380 0.540840 0.163 Uiso 0.5 1 d R U P A -1
H9B H 0.883200 0.623660 0.505920 0.163 Uiso 0.5 1 d R U P A -1
H9C H 0.927300 0.651490 0.501110 0.163 Uiso 0.5 1 d R U P A -1
C10 C 0.409(3) 0.280(3) 0.322(3) 0.265(6) Uani 1 1 d . U . . .
C12 C 0.604(2) 0.196(2) 0.4395(19) 0.159(5) Uani 1 1 d . U . . .
C13 C 0.735(3) 0.243(3) 0.500000 0.323(7) Uani 1 2 d DS TU P . .
C14 C 0.795(2) 0.346(2) 0.406(2) 0.195(4) Uani 1 1 d . U . . .
C15 C 0.9110(9) 0.4582(14) 0.3825(11) 0.190(6) Uani 1 1 d D U . . .
C16 C 0.332(2) 0.393(2) 0.2946(19) 0.169(6) Uani 1 1 d . U . . .
C17 C 0.976969 0.572929 0.526500 0.109(5) Uani 0.5 1 d D U P A -1
H17A H 0.978800 0.541070 0.529600 0.163 Uiso 0.5 1 d R U P A -1
H17B H 0.972310 0.586670 0.551340 0.163 Uiso 0.5 1 d R U P A -1
H17C H 1.004320 0.583860 0.515410 0.163 Uiso 0.5 1 d R U P A -1
C18 C 0.741(4) 0.289(5) 0.500000 0.323(7) Uani 1 2 d S TU P . .
C19 C 0.955150 0.591070 0.459120 0.109(5) Uani 0.5 1 d D U P A -1
H19A H 0.980430 0.610860 0.459460 0.163 Uiso 0.5 1 d R U P A -1
H19B H 0.931780 0.603900 0.443590 0.163 Uiso 0.5 1 d R U P A -1
H19C H 0.963880 0.562790 0.448310 0.163 Uiso 0.5 1 d R U P A -1
C20 C 0.3114(16) 0.3841(18) 0.2692(13) 0.169(6) Uani 1 1 d D U . . .
C21 C 0.442(2) 0.177(2) 0.3059(19) 0.265(6) Uani 1 1 d D U . . .
H21A H 0.467901 0.162442 0.295317 0.398 Uiso 1 1 d R U . . .
H21B H 0.418801 0.154962 0.309897 0.398 Uiso 1 1 d R U . . .
H21C H 0.449411 0.190522 0.330217 0.398 Uiso 1 1 d R U . . .
C22 C 0.2793(12) 0.3790(11) 0.2362(10) 0.169(6) Uani 1 1 d D U . . .
C23 C 0.9387(19) 0.335(2) 0.500000 0.195(4) Uani 1 2 d DS TU P . .
H23A H 0.953104 0.327101 0.523940 0.292 Uiso 0.5 1 d R U P B -1
H23B H 0.937854 0.366831 0.497370 0.292 Uiso 0.5 1 d R U P B -1
H23C H 0.954994 0.322201 0.478690 0.292 Uiso 0.5 1 d R U P B -1
C24 C 0.2545(16) 0.4208(13) 0.2264(14) 0.169(6) Uani 1 1 d D U . . .
H24A H 0.249584 0.437699 0.249768 0.254 Uiso 1 1 d R U . . .
H24B H 0.226174 0.413359 0.214988 0.254 Uiso 1 1 d R U . . .
H24C H 0.271644 0.438399 0.208528 0.254 Uiso 1 1 d R U . . .
C25 C 0.7997(19) 0.192(3) 0.500000 0.323(7) Uani 1 2 d DS TU P . .
H25A H 0.812110 0.210277 0.479620 0.485 Uiso 0.5 1 d R U P C -1
H25B H 0.807720 0.161497 0.495860 0.485 Uiso 0.5 1 d R U P C -1
H25C H 0.811370 0.202037 0.524530 0.485 Uiso 0.5 1 d R U P C -1
C26 C 0.2442(14) 0.3445(14) 0.2444(15) 0.169(6) Uani 1 1 d D U . . .
H26A H 0.257411 0.315318 0.243165 0.254 Uiso 1 1 d R U . . .
H26B H 0.220951 0.346838 0.225265 0.254 Uiso 1 1 d R U . . .
H26C H 0.231711 0.349238 0.269715 0.254 Uiso 1 1 d R U . . .
C27 C 0.8005(18) 0.2277(16) 0.3821(16) 0.195(4) Uani 1 1 d D U . . .
H27A H 0.788787 0.237601 0.406573 0.292 Uiso 1 1 d R U . . .
H27B H 0.825087 0.207631 0.386523 0.292 Uiso 1 1 d R U . . .
H27C H 0.777517 0.212501 0.367873 0.292 Uiso 1 1 d R U . . .
C28 C 0.3033(17) 0.3643(17) 0.2002(11) 0.169(6) Uani 1 1 d D U . . .
H28A H 0.317776 0.389758 0.188847 0.254 Uiso 1 1 d R U . . .
H28B H 0.282326 0.351918 0.182067 0.254 Uiso 1 1 d R U . . .
H28C H 0.325316 0.342108 0.206687 0.254 Uiso 1 1 d R U . . .
C29 C 0.9269(15) 0.4948(16) 0.3558(14) 0.190(6) Uani 1 1 d D U . . .
H29A H 0.911196 0.522048 0.361494 0.285 Uiso 1 1 d R U . . .
H29B H 0.921196 0.486189 0.329465 0.285 Uiso 1 1 d R U . . .
H29C H 0.958446 0.499419 0.359345 0.285 Uiso 1 1 d R U . . .
C30 C 0.409(2) 0.563(2) 0.1741(19) 0.280(6) Uani 1 1 d D U . . .
C31 C 0.8639(11) 0.466(2) 0.3969(15) 0.190(6) Uani 1 1 d D U . . .
C32 C 0.3857(14) 0.5545(13) 0.1366(16) 0.280(6) Uani 1 1 d D U . . .
C33 C 0.9117(15) 0.4134(14) 0.3625(16) 0.190(6) Uani 1 1 d D U . . .
H33A H 0.941317 0.400949 0.363471 0.285 Uiso 1 1 d R U . . .
H33B H 0.902747 0.417029 0.335981 0.285 Uiso 1 1 d R U . . .
H33C H 0.891257 0.393539 0.375391 0.285 Uiso 1 1 d R U . . .
C34 C 0.387(2) 0.5913(18) 0.1072(18) 0.280(6) Uani 1 1 d D U . . .
H34A H 0.406703 0.614170 0.115995 0.420 Uiso 1 1 d R U . . .
H34B H 0.357053 0.603680 0.104535 0.420 Uiso 1 1 d R U . . .
H34C H 0.396453 0.580110 0.082585 0.420 Uiso 1 1 d R U . . .
C35 C 0.9385(5) 0.5844(5) 0.500000 0.109(5) Uani 1 2 d DS TU P . .
C36 C 0.3366(15) 0.545(2) 0.140(2) 0.280(6) Uani 1 1 d D U . . .
H36A H 0.326826 0.548216 0.166095 0.420 Uiso 1 1 d R U . . .
H36B H 0.329906 0.515846 0.130425 0.420 Uiso 1 1 d R U . . .
H36C H 0.321466 0.567056 0.123915 0.420 Uiso 1 1 d R U . . .
C37 C 0.9049(9) 0.5468(11) 0.500000 0.109(5) Uani 1 2 d DS TU P A .
C38 C 0.403(2) 0.5150(18) 0.1141(19) 0.280(6) Uani 1 1 d D U . . .
H38A H 0.423544 0.526044 0.095332 0.420 Uiso 1 1 d R U . . .
H38B H 0.378084 0.500724 0.100962 0.420 Uiso 1 1 d R U . . .
H38C H 0.417114 0.493764 0.130742 0.420 Uiso 1 1 d R U . . .
C39 C 0.4570(19) 0.221(2) 0.2463(18) 0.265(6) Uani 1 1 d D U . . .
H39A H 0.486837 0.220754 0.256624 0.398 Uiso 1 1 d R U . . .
H39B H 0.450877 0.249604 0.234954 0.398 Uiso 1 1 d R U . . .
H39C H 0.454287 0.198104 0.226864 0.398 Uiso 1 1 d R U . . .
C40 C 0.6639(12) 0.1759(15) 0.3601(13) 0.160(5) Uani 1 1 d D U . . .
H40A H 0.667667 0.177146 0.332509 0.239 Uiso 1 1 d R U . . .
H40B H 0.681307 0.151726 0.370479 0.239 Uiso 1 1 d R U . . .
H40C H 0.673797 0.203596 0.371409 0.239 Uiso 1 1 d R U . . .
C41 C 0.415(2) 0.253(2) 0.302(2) 0.265(6) Uani 1 1 d D U . . .
C42 C 0.6150(12) 0.1688(10) 0.3694(9) 0.159(5) Uani 1 1 d D U . . .
C43 C 0.3817(17) 0.193(2) 0.263(2) 0.265(6) Uani 1 1 d D U . . .
H43A H 0.367323 0.215112 0.247517 0.398 Uiso 1 1 d R U . . .
H43B H 0.362423 0.185312 0.284697 0.398 Uiso 1 1 d R U . . .
H43C H 0.387683 0.166792 0.248227 0.398 Uiso 1 1 d R U . . .
C44 C 0.5869(14) 0.1924(15) 0.3391(13) 0.160(5) Uani 1 1 d D U . . .
H44A H 0.603358 0.216980 0.328177 0.239 Uiso 1 1 d R U . . .
H44B H 0.560208 0.203440 0.351197 0.239 Uiso 1 1 d R U . . .
H44C H 0.579138 0.171710 0.318917 0.239 Uiso 1 1 d R U . . .
C46 C 0.6062(17) 0.1877(17) 0.4097(11) 0.159(5) Uani 1 1 d D U . . .
C47 C 0.8916(19) 0.316(2) 0.500000 0.195(4) Uani 1 2 d DS TU P . .
C48 C 0.6055(16) 0.1189(11) 0.3699(14) 0.160(5) Uani 1 1 d D U . . .
H48A H 0.620399 0.104762 0.348456 0.239 Uiso 1 1 d R U . . .
H48B H 0.573889 0.114042 0.367846 0.239 Uiso 1 1 d R U . . .
H48C H 0.616269 0.106302 0.393766 0.239 Uiso 1 1 d R U . . .
C49 C 0.8856(18) 0.2918(18) 0.5383(12) 0.195(4) Uani 1 1 d D U . . .
H49A H 0.878033 0.312536 0.558568 0.292 Uiso 1 1 d R U . . .
H49B H 0.912823 0.276606 0.544908 0.292 Uiso 1 1 d R U . . .
H49C H 0.861913 0.270386 0.535418 0.292 Uiso 1 1 d R U . . .
C50 C 0.8655(13) 0.2651(18) 0.3526(17) 0.195(4) Uani 1 1 d D U . . .
H50A H 0.871782 0.237203 0.339868 0.292 Uiso 1 1 d R U . . .
H50B H 0.880082 0.265623 0.377418 0.292 Uiso 1 1 d R U . . .
H50C H 0.876472 0.289323 0.336968 0.292 Uiso 1 1 d R U . . .
C51 C 0.749(2) 0.194(3) 0.500000 0.323(7) Uani 1 2 d DS TU P . .
C52 C 0.8152(14) 0.2687(11) 0.3587(11) 0.195(4) Uani 1 1 d D U . . .
C53 C 0.7337(19) 0.184(3) 0.5414(12) 0.323(7) Uani 1 1 d D U . . .
H53A H 0.749697 0.204238 0.558093 0.485 Uiso 1 1 d R U . . .
H53B H 0.740077 0.153788 0.548843 0.485 Uiso 1 1 d R U . . .
H53C H 0.702197 0.189558 0.543603 0.485 Uiso 1 1 d R U . . .
C54 C 0.8040(19) 0.3114(15) 0.3811(17) 0.195(4) Uani 1 1 d D U . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 Ag7 2.894(6) . ?
Ag1 Ag10 3.137(5) 10_556 ?
Ag1 Ag10 3.137(5) . ?
Ag1 Ag20 3.256(6) 10_556 ?
Ag1 Ag20 3.256(6) . ?
Ag1 Br3 2.757(7) . ?
Ag1 Br4 2.749(5) . ?
Ag1 Br4 2.749(5) 10_556 ?
Ag1 C6 2.17(11) . ?
Ag2 Ag4 2.982(5) 10_556 ?
Ag2 Ag4 2.982(5) . ?
Ag2 Ag19 2.950(5) . ?
Ag2 Ag19 2.950(5) 10_556 ?
Ag2 Br4 2.922(5) . ?
Ag2 Br4 2.922(5) 10_556 ?
Ag2 S1 2.525(13) . ?
Ag2 S2 2.535(13) . ?
Ag3 Ag8 3.171(7) . ?
Ag3 Ag9 2.972(6) . ?
Ag3 Ag13 3.045(7) . ?
Ag3 Ag18 3.176(6) 4_565 ?
Ag3 Br1 3.063(7) 3_655 ?
Ag3 S5 2.441(11) . ?
Ag3 C10 2.22(10) . ?
Ag4 Ag11 2.915(5) . ?
Ag4 Ag14 3.347(6) 11_566 ?
Ag4 Ag19 3.108(5) . ?
Ag4 Br4 3.070(5) . ?
Ag4 Br5 2.726(6) . ?
Ag4 S1 2.674(6) . ?
Ag4 S4 2.524(11) 3_655 ?
Ag5 Ag5 3.038(5) 4_565 ?
Ag5 Ag5 3.038(5) 3_655 ?
Ag5 Ag8 2.961(6) 4_565 ?
Ag5 Ag8 3.098(6) . ?
Ag5 Ag16 3.237(6) . ?
Ag5 Br1 2.941(6) 3_655 ?
Ag5 S3 2.474(10) . ?
Ag5 S4 2.461(11) . ?
Ag6 Ag6 3.022(6) 4_565 ?
Ag6 Ag6 3.023(6) 3_655 ?
Ag6 Ag16 2.901(6) . ?
Ag6 Br1 2.896(6) . ?
Ag6 C8 2.34(9) 3_655 ?
Ag6 C8 2.40(9) . ?
Ag7 Ag17 3.071(5) 3_655 ?
Ag7 Ag17 3.071(5) 12_656 ?
Ag7 C4 2.09(3) . ?
Ag7 C6 2.18(10) . ?
Ag8 Ag14 3.033(6) 11_566 ?
Ag8 Ag19 2.938(6) . ?
Ag8 Ag21 3.214(6) 3_655 ?
Ag8 S4 2.620(10) 3_655 ?
Ag8 S4 2.513(10) . ?
Ag8 S5 2.879(10) . ?
Ag9 Ag10 3.087(6) 4_565 ?
Ag9 Ag11 3.292(7) . ?
Ag9 Ag17 2.933(5) . ?
Ag9 S5 2.418(10) . ?
Ag9 C1 2.01(6) 4_565 ?
Ag10 Ag18 3.122(7) . ?
Ag10 Ag20 3.121(6) . ?
Ag10 C1 2.16(8) . ?
Ag10 C14 1.92(7) . ?
Ag10 C31 2.65(5) . ?
Ag11 Ag14 3.254(6) 11_566 ?
Ag11 Ag15 2.978(6) . ?
Ag11 Br5 2.922(7) . ?
Ag11 S1 2.908(10) . ?
Ag11 S5 2.722(11) . ?
Ag11 C12 2.31(6) . ?
Ag12 Ag20 3.086(7) 10_556 ?
Ag12 Ag20 3.086(7) . ?
Ag12 S1 2.378(14) . ?
Ag12 C13 2.67(7) . ?
Ag12 C18 2.09(11) . ?
Ag13 Ag16 3.157(7) . ?
Ag13 Ag18 2.956(7) 4_565 ?
Ag13 Ag21 2.855(8) . ?
Ag13 C10 2.29(10) . ?
Ag13 C16 2.20(7) . ?
Ag14 Ag14 2.950(8) 10_556 ?
Ag14 Ag19 3.109(6) 12_656 ?
Ag14 S2 2.471(11) . ?
Ag14 S5 2.483(11) 12_656 ?
Ag15 Ag17 3.018(5) . ?
Ag15 Ag17 3.018(5) 10_556 ?
Ag15 C12 2.14(7) . ?
Ag15 C12 2.14(7) 10_556 ?
Ag16 C8 2.39(11) 3_655 ?
Ag16 C16 2.28(7) . ?
Ag16 C20 2.63(5) . ?
Ag17 C1 2.46(8) 4_565 ?
Ag17 C4 2.32(4) 11_566 ?
Ag17 C12 2.36(7) . ?
Ag17 C46 2.70(5) . ?
Ag18 Ag20 3.186(6) . ?
Ag18 Br4 2.953(6) . ?
Ag18 Br5 2.840(7) . ?
Ag18 C10 2.37(11) 3_655 ?
Ag18 C14 2.36(7) . ?
Ag19 Ag19 3.253(8) 10_556 ?
Ag19 Br2 2.736(7) . ?
Ag19 S2 2.661(11) 11_566 ?
Ag19 S2 2.766(11) . ?
Ag19 S4 2.603(11) 3_655 ?
Ag20 Ag20 3.139(10) 10_556 ?
Ag20 C14 2.13(8) . ?
Ag20 C18 2.00(10) . ?
Ag21 S5 2.383(11) 4_565 ?
Ag21 C16 2.06(7) . ?
C1 C31 1.26(6) . ?
C2 H2A 0.9801 . ?
C2 H2B 0.9800 . ?
C2 H2C 0.9800 . ?
C2 C15 1.541(14) . ?
C3 C6 1.34(11) . ?
C3 C47 1.548(15) . ?
C4 C37 1.19(2) . ?
C5 C21 1.527(14) . ?
C5 C39 1.525(14) . ?
C5 C41 1.528(14) . ?
C5 C43 1.532(14) . ?
C7 H7A 0.9800 . ?
C7 H7B 0.9799 . ?
C7 H7C 0.9798 . ?
C7 C52 1.562(14) . ?
C8 C30 1.16(11) . ?
C9 H9A 0.9800 . ?
C9 H9B 0.9800 . ?
C9 H9C 0.9801 . ?
C9 C35 1.536(11) . ?
C10 C41 1.11(12) . ?
C12 C46 1.08(7) . ?
C13 C18 1.42(16) . ?
C13 C51 1.552(15) . ?
C14 C54 1.40(8) . ?
C15 C29 1.539(14) . ?
C15 C31 1.541(14) . ?
C15 C33 1.539(14) . ?
C16 C20 1.13(7) . ?
C17 H17A 0.9800 . ?
C17 H17B 0.9799 . ?
C17 H17C 0.9799 . ?
C17 C35 1.539(10) . ?
C19 H19A 0.9798 . ?
C19 H19B 0.9801 . ?
C19 H19C 0.9801 . ?
C19 C35 1.539(6) . ?
C20 C22 1.527(14) . ?
C21 H21A 0.9798 . ?
C21 H21B 0.9801 . ?
C21 H21C 0.9801 . ?
C22 C24 1.525(14) . ?
C22 C26 1.529(14) . ?
C22 C28 1.529(14) . ?
C23 H23A 0.9800 . ?
C23 H23B 0.9800 . ?
C23 H23C 0.9801 . ?
C23 C47 1.547(15) . ?
C24 H24A 0.9800 . ?
C24 H24B 0.9798 . ?
C24 H24C 0.9796 . ?
C25 H25A 0.9798 . ?
C25 H25B 0.9801 . ?
C25 H25C 0.9801 . ?
C25 C51 1.553(15) . ?
C26 H26A 0.9795 . ?
C26 H26B 0.9797 . ?
C26 H26C 0.9801 . ?
C27 H27A 0.9799 . ?
C27 H27B 0.9800 . ?
C27 H27C 0.9799 . ?
C27 C52 1.562(14) . ?
C28 H28A 0.9798 . ?
C28 H28B 0.9801 . ?
C28 H28C 0.9801 . ?
C29 H29A 0.9801 . ?
C29 H29B 0.9803 . ?
C29 H29C 0.9799 . ?
C30 C32 1.528(14) . ?
C32 C34 1.527(14) . ?
C32 C36 1.528(14) . ?
C32 C38 1.530(14) . ?
C33 H33A 0.9803 . ?
C33 H33B 0.9799 . ?
C33 H33C 0.9799 . ?
C34 H34A 0.9799 . ?
C34 H34B 0.9800 . ?
C34 H34C 0.9799 . ?
C35 C37 1.537(12) . ?
C36 H36A 0.9795 . ?
C36 H36B 0.9799 . ?
C36 H36C 0.9803 . ?
C38 H38A 0.9799 . ?
C38 H38B 0.9800 . ?
C38 H38C 0.9802 . ?
C39 H39A 0.9800 . ?
C39 H39B 0.9800 . ?
C39 H39C 0.9802 . ?
C40 H40A 0.9800 . ?
C40 H40B 0.9794 . ?
C40 H40C 0.9799 . ?
C40 C42 1.545(14) . ?
C42 C44 1.546(14) . ?
C42 C46 1.553(14) . ?
C42 C48 1.550(14) . ?
C43 H43A 0.9800 . ?
C43 H43B 0.9798 . ?
C43 H43C 0.9800 . ?
C44 H44A 0.9800 . ?
C44 H44B 0.9798 . ?
C44 H44C 0.9803 . ?
C47 C49 1.550(15) . ?
C47 C49 1.550(15) 10_556 ?
C48 H48A 0.9798 . ?
C48 H48B 0.9800 . ?
C48 H48C 0.9797 . ?
C49 H49A 0.9797 . ?
C49 H49B 0.9800 . ?
C49 H49C 0.9800 . ?
C50 H50A 0.9799 . ?
C50 H50B 0.9804 . ?
C50 H50C 0.9799 . ?
C50 C52 1.556(14) . ?
C51 C53 1.559(15) 10_556 ?
C51 C53 1.559(15) . ?
C52 C54 1.561(14) . ?
C53 H53A 0.9802 . ?
C53 H53B 0.9804 . ?
C53 H53C 0.9800 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Ag7 Ag1 Ag10 70.01(11) . 10_556 ?
Ag7 Ag1 Ag10 70.01(11) . . ?
Ag7 Ag1 Ag20 111.62(16) . 10_556 ?
Ag7 Ag1 Ag20 111.62(16) . . ?
Ag10 Ag1 Ag10 128.2(2) 10_556 . ?
Ag10 Ag1 Ag20 110.07(17) . 10_556 ?
Ag10 Ag1 Ag20 110.07(17) 10_556 . ?
Ag10 Ag1 Ag20 58.40(12) 10_556 10_556 ?
Ag10 Ag1 Ag20 58.40(12) . . ?
Ag20 Ag1 Ag20 57.63(18) 10_556 . ?
Br3 Ag1 Ag7 78.14(18) . . ?
Br3 Ag1 Ag10 101.31(13) . . ?
Br3 Ag1 Ag10 101.31(13) . 10_556 ?
Br3 Ag1 Ag20 148.62(11) . . ?
Br3 Ag1 Ag20 148.62(11) . 10_556 ?
Br4 Ag1 Ag7 133.70(12) 10_556 . ?
Br4 Ag1 Ag7 133.70(12) . . ?
Br4 Ag1 Ag10 70.30(12) . . ?
Br4 Ag1 Ag10 156.27(18) . 10_556 ?
Br4 Ag1 Ag10 156.28(18) 10_556 . ?
Br4 Ag1 Ag10 70.30(12) 10_556 10_556 ?
Br4 Ag1 Ag20 103.64(18) 10_556 . ?
Br4 Ag1 Ag20 103.65(18) . 10_556 ?
Br4 Ag1 Ag20 64.20(14) . . ?
Br4 Ag1 Ag20 64.19(14) 10_556 10_556 ?
Br4 Ag1 Br3 87.22(15) . . ?
Br4 Ag1 Br3 87.22(15) 10_556 . ?
Br4 Ag1 Br4 88.3(2) 10_556 . ?
C6 Ag1 Ag7 48(3) . . ?
C6 Ag1 Ag10 64.5(2) . . ?
C6 Ag1 Ag10 64.5(2) . 10_556 ?
C6 Ag1 Ag20 69(2) . 10_556 ?
C6 Ag1 Ag20 69(2) . . ?
C6 Ag1 Br3 127(3) . . ?
C6 Ag1 Br4 127.1(13) . . ?
C6 Ag1 Br4 127.1(13) . 10_556 ?
Ag4 Ag2 Ag4 114.6(2) . 10_556 ?
Ag19 Ag2 Ag4 118.51(19) . 10_556 ?
Ag19 Ag2 Ag4 63.20(12) 10_556 10_556 ?
Ag19 Ag2 Ag4 118.51(19) 10_556 . ?
Ag19 Ag2 Ag4 63.21(12) . . ?
Ag19 Ag2 Ag19 66.93(18) 10_556 . ?
Br4 Ag2 Ag4 130.00(19) 10_556 . ?
Br4 Ag2 Ag4 62.65(12) 10_556 10_556 ?
Br4 Ag2 Ag4 130.01(19) . 10_556 ?
Br4 Ag2 Ag4 62.65(12) . . ?
Br4 Ag2 Ag19 104.40(12) . . ?
Br4 Ag2 Ag19 166.17(19) 10_556 . ?
Br4 Ag2 Ag19 166.17(19) . 10_556 ?
Br4 Ag2 Ag19 104.40(12) 10_556 10_556 ?
Br4 Ag2 Br4 81.8(2) . 10_556 ?
S1 Ag2 Ag4 57.40(11) . 10_556 ?
S1 Ag2 Ag4 57.40(11) . . ?
S1 Ag2 Ag19 88.0(3) . . ?
S1 Ag2 Ag19 88.0(3) . 10_556 ?
S1 Ag2 Br4 102.8(3) . 10_556 ?
S1 Ag2 Br4 102.8(3) . . ?
S1 Ag2 S2 140.7(5) . . ?
S2 Ag2 Ag4 116.22(15) . 10_556 ?
S2 Ag2 Ag4 116.22(15) . . ?
S2 Ag2 Ag19 60.0(3) . 10_556 ?
S2 Ag2 Ag19 60.0(3) . . ?
S2 Ag2 Br4 106.6(3) . . ?
S2 Ag2 Br4 106.6(3) . 10_556 ?
Ag8 Ag3 Ag18 129.8(3) . 4_565 ?
Ag9 Ag3 Ag8 107.61(16) . . ?
Ag9 Ag3 Ag13 143.8(2) . . ?
Ag9 Ag3 Ag18 87.23(16) . 4_565 ?
Ag9 Ag3 Br1 140.8(3) . 3_655 ?
Ag13 Ag3 Ag8 99.2(2) . . ?
Ag13 Ag3 Ag18 56.69(17) . 4_565 ?
Ag13 Ag3 Br1 72.19(19) . 3_655 ?
Br1 Ag3 Ag8 67.16(15) 3_655 . ?
Br1 Ag3 Ag18 127.1(2) 3_655 4_565 ?
S5 Ag3 Ag8 60.1(2) . . ?
S5 Ag3 Ag9 51.9(2) . . ?
S5 Ag3 Ag13 159.1(3) . . ?
S5 Ag3 Ag18 133.1(3) . 4_565 ?
S5 Ag3 Br1 99.6(3) . 3_655 ?
C10 Ag3 Ag8 146(2) . . ?
C10 Ag3 Ag9 106(2) . . ?
C10 Ag3 Ag13 49(3) . . ?
C10 Ag3 Ag18 48(3) . 4_565 ?
C10 Ag3 Br1 89(2) . 3_655 ?
C10 Ag3 S5 152(3) . . ?
Ag2 Ag4 Ag14 88.01(16) . 11_566 ?
Ag2 Ag4 Ag19 57.89(13) . . ?
Ag2 Ag4 Br4 57.72(14) . . ?
Ag11 Ag4 Ag2 115.1(2) . . ?
Ag11 Ag4 Ag14 62.17(14) . 11_566 ?
Ag11 Ag4 Ag19 119.17(19) . . ?
Ag11 Ag4 Br4 131.69(18) . . ?
Ag19 Ag4 Ag14 57.44(13) . 11_566 ?
Br4 Ag4 Ag14 145.63(18) . 11_566 ?
Br4 Ag4 Ag19 97.35(15) . . ?
Br5 Ag4 Ag2 129.6(2) . . ?
Br5 Ag4 Ag11 62.28(16) . . ?
Br5 Ag4 Ag14 122.26(17) . 11_566 ?
Br5 Ag4 Ag19 171.9(2) . . ?
Br5 Ag4 Br4 86.09(17) . . ?
S1 Ag4 Ag2 52.7(3) . . ?
S1 Ag4 Ag11 62.5(3) . . ?
S1 Ag4 Ag14 60.7(3) . 11_566 ?
S1 Ag4 Ag19 82.2(3) . . ?
S1 Ag4 Br4 95.7(3) . . ?
S1 Ag4 Br5 104.9(3) . . ?
S4 Ag4 Ag2 98.9(3) 3_655 . ?
S4 Ag4 Ag11 132.9(3) 3_655 . ?
S4 Ag4 Ag14 89.0(3) 3_655 11_566 ?
S4 Ag4 Ag19 53.9(3) 3_655 . ?
S4 Ag4 Br4 93.5(3) 3_655 . ?
S4 Ag4 Br5 118.8(3) 3_655 . ?
S4 Ag4 S1 135.9(4) 3_655 . ?
Ag5 Ag5 Ag5 90.003(1) 4_565 3_655 ?
Ag5 Ag5 Ag8 57.70(14) 3_655 . ?
Ag5 Ag5 Ag8 120.62(12) 4_565 . ?
Ag5 Ag5 Ag16 123.27(14) 3_655 . ?
Ag5 Ag5 Ag16 110.06(15) 4_565 . ?
Ag8 Ag5 Ag5 122.19(11) 4_565 3_655 ?
Ag8 Ag5 Ag5 62.16(13) 4_565 4_565 ?
Ag8 Ag5 Ag8 92.65(18) 4_565 . ?
Ag8 Ag5 Ag16 113.96(17) 4_565 . ?
Ag8 Ag5 Ag16 129.25(17) . . ?
Br1 Ag5 Ag5 66.96(18) 3_655 3_655 ?
Br1 Ag5 Ag5 145.28(14) 3_655 4_565 ?
Br1 Ag5 Ag8 152.17(18) 3_655 4_565 ?
Br1 Ag5 Ag8 69.60(15) 3_655 . ?
Br1 Ag5 Ag16 67.49(16) 3_655 . ?
S3 Ag5 Ag5 52.12(18) . 4_565 ?
S3 Ag5 Ag5 52.12(18) . 3_655 ?
S3 Ag5 Ag8 108.6(3) . . ?
S3 Ag5 Ag8 113.0(3) . 4_565 ?
S3 Ag5 Ag16 99.7(4) . . ?
S3 Ag5 Br1 93.4(2) . 3_655 ?
S4 Ag5 Ag5 109.3(3) . 3_655 ?
S4 Ag5 Ag5 117.2(3) . 4_565 ?
S4 Ag5 Ag8 52.2(2) . . ?
S4 Ag5 Ag8 56.9(2) . 4_565 ?
S4 Ag5 Ag16 106.9(3) . . ?
S4 Ag5 Br1 95.5(3) . 3_655 ?
S4 Ag5 S3 153.3(5) . . ?
Ag6 Ag6 Ag6 89.999(1) 4_565 3_655 ?
Ag16 Ag6 Ag6 155.26(15) . 4_565 ?
Ag16 Ag6 Ag6 75.01(18) . 3_655 ?
Br1 Ag6 Ag6 105.91(17) . 4_565 ?
Br1 Ag6 Ag6 125.96(15) . 3_655 ?
Br1 Ag6 Ag16 69.65(17) . . ?
C8 Ag6 Ag6 130(2) 3_655 4_565 ?
C8 Ag6 Ag6 51(2) 3_655 3_655 ?
C8 Ag6 Ag6 50(2) . 4_565 ?
C8 Ag6 Ag6 129(2) . 3_655 ?
C8 Ag6 Ag16 53(3) 3_655 . ?
C8 Ag6 Ag16 153(2) . . ?
C8 Ag6 Br1 98(3) . . ?
C8 Ag6 Br1 122(2) 3_655 . ?
C8 Ag6 C8 129(6) 3_655 . ?
Ag1 Ag7 Ag17 97.92(15) . 3_655 ?
Ag1 Ag7 Ag17 97.92(15) . 12_656 ?
Ag17 Ag7 Ag17 70.59(17) 12_656 3_655 ?
C4 Ag7 Ag1 136.4(17) . . ?
C4 Ag7 Ag17 49.1(11) . 12_656 ?
C4 Ag7 Ag17 49.1(11) . 3_655 ?
C4 Ag7 C6 175(3) . . ?
C6 Ag7 Ag1 48(3) . . ?
C6 Ag7 Ag17 133.8(17) . 12_656 ?
C6 Ag7 Ag17 133.8(17) . 3_655 ?
Ag3 Ag8 Ag21 67.06(17) . 3_655 ?
Ag5 Ag8 Ag3 90.31(16) . . ?
Ag5 Ag8 Ag3 114.76(19) 3_655 . ?
Ag5 Ag8 Ag5 60.13(15) 3_655 . ?
Ag5 Ag8 Ag14 145.56(18) 3_655 11_566 ?
Ag5 Ag8 Ag21 107.75(17) . 3_655 ?
Ag5 Ag8 Ag21 69.62(15) 3_655 3_655 ?
Ag14 Ag8 Ag3 78.76(16) 11_566 . ?
Ag14 Ag8 Ag5 154.26(19) 11_566 . ?
Ag14 Ag8 Ag21 89.49(16) 11_566 3_655 ?
Ag19 Ag8 Ag3 141.30(19) . . ?
Ag19 Ag8 Ag5 126.23(18) . . ?
Ag19 Ag8 Ag5 96.53(17) . 3_655 ?
Ag19 Ag8 Ag14 62.74(14) . 11_566 ?
Ag19 Ag8 Ag21 106.87(16) . 3_655 ?
S4 Ag8 Ag3 75.6(3) . . ?
S4 Ag8 Ag3 128.9(3) 3_655 . ?
S4 Ag8 Ag5 50.7(3) . . ?
S4 Ag8 Ag5 110.3(3) . 3_655 ?
S4 Ag8 Ag5 110.4(3) 3_655 . ?
S4 Ag8 Ag5 51.9(3) 3_655 3_655 ?
S4 Ag8 Ag14 103.7(3) . 11_566 ?
S4 Ag8 Ag14 94.4(3) 3_655 11_566 ?
S4 Ag8 Ag19 55.5(3) 3_655 . ?
S4 Ag8 Ag19 115.5(3) . . ?
S4 Ag8 Ag21 62.2(2) 3_655 3_655 ?
S4 Ag8 Ag21 137.1(3) . 3_655 ?
S4 Ag8 S4 152.5(4) . 3_655 ?
S4 Ag8 S5 117.3(3) . . ?
S4 Ag8 S5 90.2(3) 3_655 . ?
S5 Ag8 Ag3 47.3(2) . . ?
S5 Ag8 Ag5 133.7(3) . . ?
S5 Ag8 Ag5 115.2(3) . 3_655 ?
S5 Ag8 Ag14 49.6(2) . 11_566 ?
S5 Ag8 Ag19 99.8(3) . . ?
S5 Ag8 Ag21 45.6(2) . 3_655 ?
Ag3 Ag9 Ag10 95.46(16) . 4_565 ?
Ag3 Ag9 Ag11 107.00(14) . . ?
Ag10 Ag9 Ag11 150.1(2) 4_565 . ?
Ag17 Ag9 Ag3 176.2(2) . . ?
Ag17 Ag9 Ag10 87.01(14) . 4_565 ?
Ag17 Ag9 Ag11 71.73(13) . . ?
S5 Ag9 Ag3 52.6(3) . . ?
S5 Ag9 Ag10 143.0(3) . 4_565 ?
S5 Ag9 Ag11 54.4(3) . . ?
S5 Ag9 Ag17 126.0(3) . . ?
C1 Ag9 Ag3 124(2) 4_565 . ?
C1 Ag9 Ag10 44(2) 4_565 4_565 ?
C1 Ag9 Ag11 126(2) 4_565 . ?
C1 Ag9 Ag17 56(2) 4_565 . ?
C1 Ag9 S5 167(2) 4_565 . ?
Ag9 Ag10 Ag1 80.48(14) 3_655 . ?
Ag9 Ag10 Ag18 86.21(15) 3_655 . ?
Ag9 Ag10 Ag20 123.03(15) 3_655 . ?
Ag18 Ag10 Ag1 99.64(15) . . ?
Ag20 Ag10 Ag1 62.71(15) . . ?
Ag20 Ag10 Ag18 61.39(15) . . ?
C1 Ag10 Ag1 100.8(19) . . ?
C1 Ag10 Ag9 40.4(15) . 3_655 ?
C1 Ag10 Ag18 116.5(17) . . ?
C1 Ag10 Ag20 161.1(17) . . ?
C1 Ag10 C31 28.2(17) . . ?
C14 Ag10 Ag1 105(2) . . ?
C14 Ag10 Ag9 135(2) . 3_655 ?
C14 Ag10 Ag18 49(2) . . ?
C14 Ag10 Ag20 42(2) . . ?
C14 Ag10 C1 152(3) . . ?
C14 Ag10 C31 136(3) . . ?
C31 Ag10 Ag1 117.3(11) . . ?
C31 Ag10 Ag9 68.2(10) . 3_655 ?
C31 Ag10 Ag18 129.1(12) . . ?
C31 Ag10 Ag20 167.2(11) . . ?
Ag4 Ag11 Ag9 118.26(18) . . ?
Ag4 Ag11 Ag14 65.44(14) . 11_566 ?
Ag4 Ag11 Ag15 135.5(3) . . ?
Ag4 Ag11 Br5 55.69(15) . . ?
Ag14 Ag11 Ag9 68.01(14) 11_566 . ?
Ag15 Ag11 Ag9 99.68(16) . . ?
Ag15 Ag11 Ag14 114.4(2) . 11_566 ?
Br5 Ag11 Ag9 128.3(3) . . ?
Br5 Ag11 Ag14 119.10(17) . 11_566 ?
Br5 Ag11 Ag15 117.5(2) . . ?
S1 Ag11 Ag4 54.7(2) . . ?
S1 Ag11 Ag9 124.5(3) . . ?
S1 Ag11 Ag14 60.0(3) . 11_566 ?
S1 Ag11 Ag15 85.6(3) . . ?
S1 Ag11 Br5 94.5(3) . . ?
S5 Ag11 Ag4 72.5(2) . . ?
S5 Ag11 Ag9 46.2(2) . . ?
S5 Ag11 Ag14 48.1(2) . 11_566 ?
S5 Ag11 Ag15 143.5(3) . . ?
S5 Ag11 Br5 97.5(3) . . ?
S5 Ag11 S1 103.0(3) . . ?
C12 Ag11 Ag4 153.3(17) . . ?
C12 Ag11 Ag9 82.2(17) . . ?
C12 Ag11 Ag14 141.3(17) . 11_566 ?
C12 Ag11 Ag15 45.6(17) . . ?
C12 Ag11 Br5 98.6(17) . . ?
C12 Ag11 S1 129.8(18) . . ?
C12 Ag11 S5 122.8(18) . . ?
Ag20 Ag12 Ag20 61.1(2) . 10_556 ?
S1 Ag12 Ag20 136.7(3) . 10_556 ?
S1 Ag12 Ag20 136.7(3) . . ?
S1 Ag12 C13 154(3) . . ?
C13 Ag12 Ag20 63(2) . 10_556 ?
C13 Ag12 Ag20 63(2) . . ?
C18 Ag12 Ag20 40(3) . 10_556 ?
C18 Ag12 Ag20 40(3) . . ?
C18 Ag12 S1 175(4) . . ?
C18 Ag12 C13 32(5) . . ?
Ag3 Ag13 Ag16 114.9(2) . . ?
Ag18 Ag13 Ag3 63.89(15) 4_565 . ?
Ag18 Ag13 Ag16 169.4(3) 4_565 . ?
Ag21 Ag13 Ag3 126.2(3) . . ?
Ag21 Ag13 Ag16 68.97(18) . . ?
Ag21 Ag13 Ag18 120.8(3) . 4_565 ?
C10 Ag13 Ag3 47(2) . . ?
C10 Ag13 Ag16 119(3) . . ?
C10 Ag13 Ag18 52(3) . 4_565 ?
C10 Ag13 Ag21 170(3) . . ?
C16 Ag13 Ag3 159.3(19) . . ?
C16 Ag13 Ag16 46.3(18) . . ?
C16 Ag13 Ag18 136.4(19) . 4_565 ?
C16 Ag13 Ag21 45.9(17) . . ?
C16 Ag13 C10 144(3) . . ?
Ag8 Ag14 Ag4 74.66(13) 12_656 12_656 ?
Ag8 Ag14 Ag11 107.43(17) 12_656 12_656 ?
Ag8 Ag14 Ag19 57.15(14) 12_656 12_656 ?
Ag11 Ag14 Ag4 52.39(12) 12_656 12_656 ?
Ag14 Ag14 Ag4 108.00(11) 10_556 12_656 ?
Ag14 Ag14 Ag8 143.62(11) 10_556 12_656 ?
Ag14 Ag14 Ag11 101.51(14) 10_556 12_656 ?
Ag14 Ag14 Ag19 92.80(11) 10_556 12_656 ?
Ag19 Ag14 Ag4 57.42(12) 12_656 12_656 ?
Ag19 Ag14 Ag11 109.46(18) 12_656 12_656 ?
S2 Ag14 Ag4 107.4(3) . 12_656 ?
S2 Ag14 Ag8 90.7(2) . 12_656 ?
S2 Ag14 Ag11 144.8(3) . 12_656 ?
S2 Ag14 Ag14 53.4(2) . 10_556 ?
S2 Ag14 Ag19 55.6(3) . 12_656 ?
S2 Ag14 S5 152.7(4) . 12_656 ?
S5 Ag14 Ag4 68.0(3) 12_656 12_656 ?
S5 Ag14 Ag8 62.0(3) 12_656 12_656 ?
S5 Ag14 Ag11 54.7(3) 12_656 12_656 ?
S5 Ag14 Ag14 153.8(2) 12_656 10_556 ?
S5 Ag14 Ag19 104.9(3) 12_656 12_656 ?
Ag11 Ag15 Ag11 91.0(3) . 10_556 ?
Ag11 Ag15 Ag17 75.22(14) 10_556 10_556 ?
Ag11 Ag15 Ag17 75.22(14) . . ?
Ag11 Ag15 Ag17 125.72(19) . 10_556 ?
Ag11 Ag15 Ag17 125.72(19) 10_556 . ?
Ag17 Ag15 Ag17 72.03(18) . 10_556 ?
C12 Ag15 Ag11 141.3(16) . 10_556 ?
C12 Ag15 Ag11 50.4(16) 10_556 10_556 ?
C12 Ag15 Ag11 50.4(16) . . ?
C12 Ag15 Ag11 141.3(16) 10_556 . ?
C12 Ag15 Ag17 122.8(18) 10_556 . ?
C12 Ag15 Ag17 51.2(18) . . ?
C12 Ag15 Ag17 122.8(18) . 10_556 ?
C12 Ag15 Ag17 51.2(18) 10_556 10_556 ?
C12 Ag15 C12 168(3) . 10_556 ?
Ag6 Ag16 Ag5 74.79(15) . . ?
Ag6 Ag16 Ag13 149.5(2) . . ?
Ag13 Ag16 Ag5 74.77(18) . . ?
C8 Ag16 Ag5 106(2) 3_655 . ?
C8 Ag16 Ag6 51.5(19) 3_655 . ?
C8 Ag16 Ag13 142(2) 3_655 . ?
C8 Ag16 C20 131(2) 3_655 . ?
C16 Ag16 Ag5 96.8(17) . . ?
C16 Ag16 Ag6 139.8(17) . . ?
C16 Ag16 Ag13 44.2(17) . . ?
C16 Ag16 C8 157(3) . 3_655 ?
C16 Ag16 C20 25.4(17) . . ?
C20 Ag16 Ag5 122.0(10) . . ?
C20 Ag16 Ag6 137.6(11) . . ?
C20 Ag16 Ag13 61.7(10) . . ?
Ag9 Ag17 Ag7 95.75(14) . 11_566 ?
Ag9 Ag17 Ag15 107.40(15) . . ?
Ag15 Ag17 Ag7 107.10(14) . 11_566 ?
C1 Ag17 Ag7 76.9(18) 4_565 11_566 ?
C1 Ag17 Ag9 42.6(13) 4_565 . ?
C1 Ag17 Ag15 149.6(13) 4_565 . ?
C1 Ag17 C46 105(2) 4_565 . ?
C4 Ag17 Ag7 42.8(8) 11_566 11_566 ?
C4 Ag17 Ag9 138.5(8) 11_566 . ?
C4 Ag17 Ag15 87.2(13) 11_566 . ?
C4 Ag17 C1 112(2) 11_566 4_565 ?
C4 Ag17 C12 125(2) 11_566 . ?
C4 Ag17 C46 138.0(14) 11_566 . ?
C12 Ag17 Ag7 151.3(16) . 11_566 ?
C12 Ag17 Ag9 89.6(16) . . ?
C12 Ag17 Ag15 44.8(16) . . ?
C12 Ag17 C1 123(2) . 4_565 ?
C12 Ag17 C46 23.5(17) . . ?
C46 Ag17 Ag7 174.2(9) . 11_566 ?
C46 Ag17 Ag9 82.8(11) . . ?
C46 Ag17 Ag15 68.2(10) . . ?
Ag3 Ag18 Ag20 128.11(19) 3_655 . ?
Ag10 Ag18 Ag3 90.80(17) . 3_655 ?
Ag10 Ag18 Ag20 59.29(16) . . ?
Ag13 Ag18 Ag3 59.42(17) 3_655 3_655 ?
Ag13 Ag18 Ag10 149.4(2) 3_655 . ?
Ag13 Ag18 Ag20 144.2(2) 3_655 . ?
Br4 Ag18 Ag3 66.65(15) . 3_655 ?
Br4 Ag18 Ag10 68.08(14) . . ?
Br4 Ag18 Ag13 102.5(2) . 3_655 ?
Br4 Ag18 Ag20 63.12(14) . . ?
Br5 Ag18 Ag3 116.0(2) . 3_655 ?
Br5 Ag18 Ag10 132.1(2) . . ?
Br5 Ag18 Ag13 73.3(2) . 3_655 ?
Br5 Ag18 Ag20 73.21(18) . . ?
Br5 Ag18 Br4 86.35(18) . . ?
C10 Ag18 Ag3 44(2) 3_655 3_655 ?
C10 Ag18 Ag10 105(2) 3_655 . ?
C10 Ag18 Ag13 50(2) 3_655 3_655 ?
C10 Ag18 Ag20 164(2) 3_655 . ?
C10 Ag18 Br4 111(2) 3_655 . ?
C10 Ag18 Br5 122(2) 3_655 . ?
C14 Ag18 Ag3 128.5(17) . 3_655 ?
C14 Ag18 Ag10 37.9(17) . . ?
C14 Ag18 Ag13 168(2) . 3_655 ?
C14 Ag18 Ag20 41.9(19) . . ?
C14 Ag18 Br4 90(2) . . ?
C14 Ag18 Br5 106.7(17) . . ?
C14 Ag18 C10 127(3) . 3_655 ?
Ag2 Ag19 Ag4 58.90(12) . . ?
Ag2 Ag19 Ag14 93.23(17) . 11_566 ?
Ag2 Ag19 Ag19 56.53(9) . 10_556 ?
Ag4 Ag19 Ag14 65.14(14) . 11_566 ?
Ag4 Ag19 Ag19 106.50(11) . 10_556 ?
Ag8 Ag19 Ag2 137.96(18) . . ?
Ag8 Ag19 Ag4 79.71(14) . . ?
Ag8 Ag19 Ag14 60.12(15) . 11_566 ?
Ag8 Ag19 Ag19 141.21(12) . 10_556 ?
Ag14 Ag19 Ag19 87.20(11) 11_566 10_556 ?
Br2 Ag19 Ag2 146.8(2) . . ?
Br2 Ag19 Ag4 140.2(3) . . ?
Br2 Ag19 Ag8 71.7(3) . . ?
Br2 Ag19 Ag14 118.90(18) . 11_566 ?
Br2 Ag19 Ag19 113.2(3) . 10_556 ?
Br2 Ag19 S2 95.0(3) . . ?
S2 Ag19 Ag2 97.4(3) 11_566 . ?
S2 Ag19 Ag2 52.5(3) . . ?
S2 Ag19 Ag4 109.5(3) 11_566 . ?
S2 Ag19 Ag4 105.8(3) . . ?
S2 Ag19 Ag8 89.2(2) 11_566 . ?
S2 Ag19 Ag8 162.6(2) . . ?
S2 Ag19 Ag14 50.0(3) 11_566 11_566 ?
S2 Ag19 Ag14 137.3(2) . 11_566 ?
S2 Ag19 Ag19 52.32(19) 11_566 10_556 ?
S2 Ag19 Ag19 53.98(18) . 10_556 ?
S2 Ag19 Br2 97.4(3) 11_566 . ?
S2 Ag19 S2 104.0(3) 11_566 . ?
S4 Ag19 Ag2 97.9(3) 3_655 . ?
S4 Ag19 Ag4 51.5(2) 3_655 . ?
S4 Ag19 Ag8 56.0(2) 3_655 . ?
S4 Ag19 Ag14 93.0(3) 3_655 11_566 ?
S4 Ag19 Ag19 154.4(2) 3_655 10_556 ?
S4 Ag19 Br2 89.1(4) 3_655 . ?
S4 Ag19 S2 114.2(3) 3_655 . ?
S4 Ag19 S2 140.6(3) 3_655 11_566 ?
Ag10 Ag20 Ag1 58.89(13) . . ?
Ag10 Ag20 Ag18 59.32(16) . . ?
Ag10 Ag20 Ag20 113.65(13) . 10_556 ?
Ag12 Ag20 Ag1 86.88(16) . . ?
Ag12 Ag20 Ag10 137.39(19) . . ?
Ag12 Ag20 Ag18 104.94(18) . . ?
Ag12 Ag20 Ag20 59.44(11) . 10_556 ?
Ag18 Ag20 Ag1 95.83(15) . . ?
Ag20 Ag20 Ag1 61.18(9) 10_556 . ?
Ag20 Ag20 Ag18 150.97(11) 10_556 . ?
C14 Ag20 Ag1 96.1(19) . . ?
C14 Ag20 Ag10 37.2(19) . . ?
C14 Ag20 Ag12 153(2) . . ?
C14 Ag20 Ag18 48(2) . . ?
C14 Ag20 Ag20 144(2) . 10_556 ?
C18 Ag20 Ag1 96(3) . . ?
C18 Ag20 Ag10 152(4) . . ?
C18 Ag20 Ag12 42(3) . . ?
C18 Ag20 Ag18 144(3) . . ?
C18 Ag20 Ag20 38(4) . 10_556 ?
C18 Ag20 C14 161(4) . . ?
Ag13 Ag21 Ag8 115.5(2) . 4_565 ?
S5 Ag21 Ag8 59.7(3) 4_565 4_565 ?
S5 Ag21 Ag13 142.6(3) 4_565 . ?
C16 Ag21 Ag8 144(2) . 4_565 ?
C16 Ag21 Ag13 50.1(19) . . ?
C16 Ag21 S5 154(2) . 4_565 ?
Ag5 Br1 Ag3 95.5(2) 4_565 4_565 ?
Ag6 Br1 Ag3 175.6(2) . 4_565 ?
Ag6 Br1 Ag5 82.70(16) . 4_565 ?
Ag19 Br2 Ag19 133.7(6) . 2_665 ?
Ag19 Br2 Ag19 81.1(2) . 4_565 ?
Ag19 Br2 Ag19 81.1(2) 4_565 2_665 ?
Ag19 Br2 Ag19 133.7(6) 3_655 4_565 ?
Ag19 Br2 Ag19 81.1(2) 3_655 2_665 ?
Ag19 Br2 Ag19 81.1(2) . 3_655 ?
Ag1 Br4 Ag2 94.68(16) . . ?
Ag1 Br4 Ag4 141.22(19) . . ?
Ag1 Br4 Ag18 113.93(16) . . ?
Ag2 Br4 Ag4 59.62(13) . . ?
Ag2 Br4 Ag18 140.38(19) . . ?
Ag18 Br4 Ag4 81.41(16) . . ?
Ag4 Br5 Ag11 62.03(16) . . ?
Ag4 Br5 Ag18 89.79(18) . . ?
Ag18 Br5 Ag11 150.9(2) . . ?
Ag2 S1 Ag4 69.9(3) . . ?
Ag2 S1 Ag4 69.9(3) . 10_556 ?
Ag2 S1 Ag11 132.6(2) . . ?
Ag2 S1 Ag11 132.6(2) . 10_556 ?
Ag4 S1 Ag4 139.5(5) . 10_556 ?
Ag4 S1 Ag11 156.0(5) 10_556 . ?
Ag4 S1 Ag11 62.80(14) . . ?
Ag4 S1 Ag11 156.0(5) . 10_556 ?
Ag4 S1 Ag11 62.79(14) 10_556 10_556 ?
Ag11 S1 Ag11 93.8(4) . 10_556 ?
Ag12 S1 Ag2 92.1(5) . . ?
Ag12 S1 Ag4 88.2(3) . 10_556 ?
Ag12 S1 Ag4 88.2(3) . . ?
Ag12 S1 Ag11 83.1(4) . 10_556 ?
Ag12 S1 Ag11 83.1(4) . . ?
Ag2 S2 Ag19 67.5(3) . 10_556 ?
Ag2 S2 Ag19 141.5(2) . 12_656 ?
Ag2 S2 Ag19 67.5(3) . . ?
Ag2 S2 Ag19 141.5(2) . 3_655 ?
Ag14 S2 Ag2 89.6(4) . . ?
Ag14 S2 Ag2 89.6(4) 10_556 . ?
Ag14 S2 Ag14 73.3(4) 10_556 . ?
Ag14 S2 Ag19 102.6(2) 10_556 . ?
Ag14 S2 Ag19 156.9(5) . . ?
Ag14 S2 Ag19 117.5(5) . 3_655 ?
Ag14 S2 Ag19 117.5(5) 10_556 12_656 ?
Ag14 S2 Ag19 74.5(3) . 12_656 ?
Ag14 S2 Ag19 74.5(3) 10_556 3_655 ?
Ag14 S2 Ag19 156.9(5) 10_556 10_556 ?
Ag14 S2 Ag19 102.6(2) . 10_556 ?
Ag19 S2 Ag19 75.4(4) 12_656 3_655 ?
Ag19 S2 Ag19 81.9(3) 3_655 . ?
Ag19 S2 Ag19 81.9(3) 12_656 10_556 ?
Ag19 S2 Ag19 125.3(5) 3_655 10_556 ?
Ag19 S2 Ag19 72.0(4) . 10_556 ?
Ag19 S2 Ag19 125.3(5) 12_656 . ?
Ag5 S3 Ag5 75.8(4) . 4_565 ?
Ag5 S3 Ag5 75.8(4) . 3_655 ?
Ag5 S3 Ag5 75.8(4) 2_665 4_565 ?
Ag5 S3 Ag5 120.5(8) 4_565 3_655 ?
Ag5 S3 Ag5 120.5(8) . 2_665 ?
Ag5 S3 Ag5 75.8(4) 2_665 3_655 ?
Ag4 S4 Ag8 97.8(4) 4_565 4_565 ?
Ag4 S4 Ag19 74.6(3) 4_565 4_565 ?
Ag5 S4 Ag4 152.8(5) . 4_565 ?
Ag5 S4 Ag8 71.2(3) . 4_565 ?
Ag5 S4 Ag8 77.0(3) . . ?
Ag5 S4 Ag19 120.7(4) . 4_565 ?
Ag8 S4 Ag4 129.0(4) . 4_565 ?
Ag8 S4 Ag8 117.3(4) . 4_565 ?
Ag8 S4 Ag19 84.9(3) . 4_565 ?
Ag19 S4 Ag8 68.5(3) 4_565 4_565 ?
Ag3 S5 Ag8 72.6(3) . . ?
Ag3 S5 Ag11 154.8(4) . . ?
Ag3 S5 Ag14 106.2(4) . 11_566 ?
Ag9 S5 Ag3 75.4(3) . . ?
Ag9 S5 Ag8 138.6(4) . . ?
Ag9 S5 Ag11 79.4(3) . . ?
Ag9 S5 Ag14 96.7(4) . 11_566 ?
Ag11 S5 Ag8 129.6(4) . . ?
Ag14 S5 Ag8 68.4(3) 11_566 . ?
Ag14 S5 Ag11 77.2(3) 11_566 . ?
Ag21 S5 Ag3 94.0(4) 3_655 . ?
Ag21 S5 Ag8 74.6(3) 3_655 . ?
Ag21 S5 Ag9 133.6(5) 3_655 . ?
Ag21 S5 Ag11 102.9(4) 3_655 . ?
Ag21 S5 Ag14 129.4(4) 3_655 11_566 ?
Ag9 C1 Ag10 96(3) 3_655 . ?
Ag9 C1 Ag17 81(2) 3_655 3_655 ?
Ag10 C1 Ag17 128(3) . 3_655 ?
C31 C1 Ag9 163(7) . 3_655 ?
C31 C1 Ag10 98(5) . . ?
C31 C1 Ag17 98(5) . 3_655 ?
H2A C2 H2B 109.5 . . ?
H2A C2 H2C 109.5 . . ?
H2B C2 H2C 109.5 . . ?
C15 C2 H2A 109.2 . . ?
C15 C2 H2B 108.9 . . ?
C15 C2 H2C 110.3 . . ?
C6 C3 C47 179(8) . . ?
Ag7 C4 Ag17 88.0(10) . 3_655 ?
Ag7 C4 Ag17 88.0(10) . 12_656 ?
Ag17 C4 Ag17 100(2) 3_655 12_656 ?
C37 C4 Ag7 166(5) . . ?
C37 C4 Ag17 101(2) . 12_656 ?
C37 C4 Ag17 101(2) . 3_655 ?
C21 C5 C41 107(2) . . ?
C21 C5 C43 105(2) . . ?
C39 C5 C21 112(2) . . ?
C39 C5 C41 112(2) . . ?
C39 C5 C43 111(2) . . ?
C41 C5 C43 109(3) . . ?
Ag1 C6 Ag7 83(4) . . ?
C3 C6 Ag1 159(8) . . ?
C3 C6 Ag7 118(8) . . ?
H7A C7 H7B 109.5 . . ?
H7A C7 H7C 109.5 . . ?
H7B C7 H7C 109.5 . . ?
C52 C7 H7A 109.4 . . ?
C52 C7 H7B 108.8 . . ?
C52 C7 H7C 110.2 . . ?
Ag6 C8 Ag6 79(3) 4_565 . ?
Ag6 C8 Ag16 76(3) 4_565 4_565 ?
Ag16 C8 Ag6 98(5) 4_565 . ?
C30 C8 Ag6 144(10) . 4_565 ?
C30 C8 Ag6 106(7) . . ?
C30 C8 Ag16 136(7) . 4_565 ?
H9A C9 H9B 109.5 . . ?
H9A C9 H9C 109.5 . . ?
H9B C9 H9C 109.5 . . ?
C35 C9 H9A 109.5 . . ?
C35 C9 H9B 109.6 . . ?
C35 C9 H9C 109.3 . . ?
Ag3 C10 Ag13 85(4) . . ?
Ag3 C10 Ag18 87(4) . 4_565 ?
Ag13 C10 Ag18 79(4) . 4_565 ?
C41 C10 Ag3 125(9) . . ?
C41 C10 Ag13 142(9) . . ?
C41 C10 Ag18 121(8) . 4_565 ?
Ag11 C12 Ag17 103(2) . . ?
Ag15 C12 Ag11 84(2) . . ?
Ag15 C12 Ag17 84(2) . . ?
C46 C12 Ag11 104(6) . . ?
C46 C12 Ag15 172(6) . . ?
C46 C12 Ag17 96(5) . . ?
C18 C13 Ag12 51(5) . . ?
C18 C13 C51 156(10) . . ?
C51 C13 Ag12 153(6) . . ?
Ag10 C14 Ag18 93(3) . . ?
Ag10 C14 Ag20 101(4) . . ?
Ag20 C14 Ag18 90(3) . . ?
C54 C14 Ag10 146(6) . . ?
C54 C14 Ag18 93(5) . . ?
C54 C14 Ag20 113(5) . . ?
C2 C15 C31 107(2) . . ?
C29 C15 C2 110(2) . . ?
C29 C15 C31 112(2) . . ?
C33 C15 C2 108(2) . . ?
C33 C15 C29 111(2) . . ?
C33 C15 C31 108(2) . . ?
Ag13 C16 Ag16 90(3) . . ?
Ag21 C16 Ag13 84(3) . . ?
Ag21 C16 Ag16 104(3) . . ?
C20 C16 Ag13 125(6) . . ?
C20 C16 Ag16 95(5) . . ?
C20 C16 Ag21 146(6) . . ?
H17A C17 H17B 109.5 . . ?
H17A C17 H17C 109.5 . . ?
H17B C17 H17C 109.5 . . ?
C35 C17 H17A 109.6 . . ?
C35 C17 H17B 109.4 . . ?
C35 C17 H17C 109.3 . . ?
Ag20 C18 Ag12 98(4) 10_556 . ?
Ag20 C18 Ag12 98(4) . . ?
Ag20 C18 Ag20 103(7) . 10_556 ?
C13 C18 Ag12 98(9) . . ?
C13 C18 Ag20 126(4) . . ?
C13 C18 Ag20 126(4) . 10_556 ?
H19A C19 H19B 109.5 . . ?
H19A C19 H19C 109.5 . . ?
H19B C19 H19C 109.5 . . ?
C35 C19 H19A 109.3 . . ?
C35 C19 H19B 109.5 . . ?
C35 C19 H19C 109.6 . . ?
C16 C20 Ag16 60(5) . . ?
C16 C20 C22 171(6) . . ?
C22 C20 Ag16 122(2) . . ?
C5 C21 H21A 110.3 . . ?
C5 C21 H21B 108.7 . . ?
C5 C21 H21C 109.4 . . ?
H21A C21 H21B 109.5 . . ?
H21A C21 H21C 109.5 . . ?
H21B C21 H21C 109.5 . . ?
C20 C22 C26 112(2) . . ?
C20 C22 C28 111(2) . . ?
C24 C22 C20 114(2) . . ?
C24 C22 C26 106(2) . . ?
C24 C22 C28 107(2) . . ?
C26 C22 C28 107(2) . . ?
H23A C23 H23B 109.5 . . ?
H23A C23 H23C 109.5 . . ?
H23B C23 H23C 109.5 . . ?
C47 C23 H23A 109.2 . . ?
C47 C23 H23B 110.2 . . ?
C47 C23 H23C 109.1 . . ?
C22 C24 H24A 109.1 . . ?
C22 C24 H24B 109.6 . . ?
C22 C24 H24C 109.7 . . ?
H24A C24 H24B 109.5 . . ?
H24A C24 H24C 109.5 . . ?
H24B C24 H24C 109.5 . . ?
H25A C25 H25B 109.5 . . ?
H25A C25 H25C 109.5 . . ?
H25B C25 H25C 109.5 . . ?
C51 C25 H25A 111.3 . . ?
C51 C25 H25B 106.6 . . ?
C51 C25 H25C 110.5 . . ?
C22 C26 H26A 109.2 . . ?
C22 C26 H26B 109.2 . . ?
C22 C26 H26C 110.1 . . ?
H26A C26 H26B 109.5 . . ?
H26A C26 H26C 109.5 . . ?
H26B C26 H26C 109.5 . . ?
H27A C27 H27B 109.5 . . ?
H27A C27 H27C 109.4 . . ?
H27B C27 H27C 109.5 . . ?
C52 C27 H27A 108.7 . . ?
C52 C27 H27B 111.4 . . ?
C52 C27 H27C 108.3 . . ?
C22 C28 H28A 108.7 . . ?
C22 C28 H28B 109.8 . . ?
C22 C28 H28C 109.8 . . ?
H28A C28 H28B 109.5 . . ?
H28A C28 H28C 109.5 . . ?
H28B C28 H28C 109.5 . . ?
C15 C29 H29A 109.7 . . ?
C15 C29 H29B 109.1 . . ?
C15 C29 H29C 109.7 . . ?
H29A C29 H29B 109.4 . . ?
H29A C29 H29C 109.5 . . ?
H29B C29 H29C 109.4 . . ?
C8 C30 C32 177(8) . . ?
C1 C31 Ag10 54(5) . . ?
C1 C31 C15 175(5) . . ?
C15 C31 Ag10 126(3) . . ?
C30 C32 C38 115(2) . . ?
C34 C32 C30 117(2) . . ?
C34 C32 C36 101(3) . . ?
C34 C32 C38 103(3) . . ?
C36 C32 C30 116(2) . . ?
C36 C32 C38 103(3) . . ?
C15 C33 H33A 109.9 . . ?
C15 C33 H33B 109.3 . . ?
C15 C33 H33C 109.2 . . ?
H33A C33 H33B 109.5 . . ?
H33A C33 H33C 109.5 . . ?
H33B C33 H33C 109.5 . . ?
C32 C34 H34A 108.7 . . ?
C32 C34 H34B 109.5 . . ?
C32 C34 H34C 110.2 . . ?
H34A C34 H34B 109.5 . . ?
H34A C34 H34C 109.5 . . ?
H34B C34 H34C 109.4 . . ?
C9 C35 C17 111.9(7) . . ?
C9 C35 C19 109.4(7) . . ?
C9 C35 C37 106.8(16) . . ?
C17 C35 C19 110.2(8) . . ?
C37 C35 C17 109.8(12) . . ?
C37 C35 C19 108.6(7) . . ?
C32 C36 H36A 110.6 . . ?
C32 C36 H36B 110.4 . . ?
C32 C36 H36C 107.4 . . ?
H36A C36 H36B 109.5 . . ?
H36A C36 H36C 109.5 . . ?
H36B C36 H36C 109.5 . . ?
C4 C37 C35 176(4) . . ?
C32 C38 H38A 107.3 . . ?
C32 C38 H38B 109.8 . . ?
C32 C38 H38C 111.3 . . ?
H38A C38 H38B 109.5 . . ?
H38A C38 H38C 109.5 . . ?
H38B C38 H38C 109.5 . . ?
C5 C39 H39A 108.7 . . ?
C5 C39 H39B 110.2 . . ?
C5 C39 H39C 109.5 . . ?
H39A C39 H39B 109.5 . . ?
H39A C39 H39C 109.5 . . ?
H39B C39 H39C 109.5 . . ?
H40A C40 H40B 109.5 . . ?
H40A C40 H40C 109.5 . . ?
H40B C40 H40C 109.5 . . ?
C42 C40 H40A 109.1 . . ?
C42 C40 H40B 109.8 . . ?
C42 C40 H40C 109.5 . . ?
C10 C41 C5 174(9) . . ?
C40 C42 C44 108.9(19) . . ?
C40 C42 C46 107.9(19) . . ?
C40 C42 C48 108.7(19) . . ?
C44 C42 C46 111(2) . . ?
C44 C42 C48 111(2) . . ?
C48 C42 C46 109(2) . . ?
C5 C43 H43A 109.0 . . ?
C5 C43 H43B 109.9 . . ?
C5 C43 H43C 109.4 . . ?
H43A C43 H43B 109.5 . . ?
H43A C43 H43C 109.5 . . ?
H43B C43 H43C 109.5 . . ?
C42 C44 H44A 110.2 . . ?
C42 C44 H44B 108.7 . . ?
C42 C44 H44C 109.5 . . ?
H44A C44 H44B 109.5 . . ?
H44A C44 H44C 109.4 . . ?
H44B C44 H44C 109.5 . . ?
C12 C46 Ag17 61(5) . . ?
C12 C46 C42 169(6) . . ?
C42 C46 Ag17 121(3) . . ?
C3 C47 C49 106(3) . 10_556 ?
C3 C47 C49 106(3) . . ?
C23 C47 C3 110(2) . . ?
C23 C47 C49 107(2) . 10_556 ?
C23 C47 C49 107(2) . . ?
C49 C47 C49 121(6) 10_556 . ?
C42 C48 H48A 109.7 . . ?
C42 C48 H48B 109.3 . . ?
C42 C48 H48C 109.4 . . ?
H48A C48 H48B 109.5 . . ?
H48A C48 H48C 109.5 . . ?
H48B C48 H48C 109.5 . . ?
C47 C49 H49A 110.6 . . ?
C47 C49 H49B 109.4 . . ?
C47 C49 H49C 108.4 . . ?
H49A C49 H49B 109.5 . . ?
H49A C49 H49C 109.5 . . ?
H49B C49 H49C 109.5 . . ?
H50A C50 H50B 109.5 . . ?
H50A C50 H50C 109.5 . . ?
H50B C50 H50C 109.5 . . ?
C52 C50 H50A 108.5 . . ?
C52 C50 H50B 108.8 . . ?
C52 C50 H50C 111.2 . . ?
C13 C51 C25 108(2) . . ?
C13 C51 C53 96(5) . 10_556 ?
C13 C51 C53 96(5) . . ?
C25 C51 C53 107(2) . 10_556 ?
C25 C51 C53 107(2) . . ?
C53 C51 C53 138(8) . 10_556 ?
C7 C52 C27 111(2) . . ?
C50 C52 C7 110(2) . . ?
C50 C52 C27 107(2) . . ?
C50 C52 C54 110(2) . . ?
C54 C52 C7 109(2) . . ?
C54 C52 C27 110(2) . . ?
C51 C53 H53A 106.8 . . ?
C51 C53 H53B 112.2 . . ?
C51 C53 H53C 109.4 . . ?
H53A C53 H53B 109.5 . . ?
H53A C53 H53C 109.5 . . ?
H53B C53 H53C 109.5 . . ?
C14 C54 C52 171(6) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Ag9 C1 C31 Ag10 -142(24) 3_655 . . . ?
Ag11 C12 C46 Ag17 -105(4) . . . . ?
Ag11 C12 C46 C42 152(33) . . . . ?
Ag12 C13 C18 Ag20 105(8) . . . 10_556 ?
Ag12 C13 C18 Ag20 -105(8) . . . . ?
Ag12 C13 C51 C25 180.0 . . . . ?
Ag12 C13 C51 C53 -70(3) . . . . ?
Ag12 C13 C51 C53 70(3) . . . 10_556 ?
Ag13 C16 C20 Ag16 -93(6) . . . . ?
Ag16 C20 C22 C24 -83(3) . . . . ?
Ag16 C20 C22 C26 157(3) . . . . ?
Ag16 C20 C22 C28 38(3) . . . . ?
Ag17 C1 C31 Ag10 130(4) 3_655 . . . ?
Ag17 C12 C46 C42 -103(34) . . . . ?
Ag21 C16 C20 Ag16 122(11) . . . . ?
C2 C15 C31 Ag10 -84(3) . . . . ?
C18 C13 C51 C25 0.0 . . . . ?
C18 C13 C51 C53 110(3) . . . . ?
C18 C13 C51 C53 -110(3) . . . 10_556 ?
C29 C15 C31 Ag10 155(3) . . . . ?
C33 C15 C31 Ag10 32(4) . . . . ?
C40 C42 C46 Ag17 -162(3) . . . . ?
C40 C42 C46 C12 -66(35) . . . . ?
C44 C42 C46 Ag17 79(3) . . . . ?
C44 C42 C46 C12 175(35) . . . . ?
C48 C42 C46 Ag17 -44(3) . . . . ?
C48 C42 C46 C12 52(36) . . . . ?
C51 C13 C18 Ag12 180.0 . . . . ?
C51 C13 C18 Ag20 -75(8) . . . 10_556 ?
C51 C13 C18 Ag20 75(8) . . . . ?

_smtbx_masks_special_details     ?
loop_
_smtbx_masks_void_nr
_smtbx_masks_void_average_x
_smtbx_masks_void_average_y
_smtbx_masks_void_average_z
_smtbx_masks_void_volume
_smtbx_masks_void_count_electrons
_smtbx_masks_void_content
1 -0.779 -0.185 -0.126 12690.0 15263.2 ?
2 0.000 0.500 0.000 35.2 22.6 ?
3 0.000 0.500 0.500 35.2 22.6 ?
4 0.500 0.000 0.500 35.2 22.6 ?
5 0.500 0.000 0.000 35.2 22.6 ?

_smtbx_masks_void_probe_radius   1.2
_smtbx_masks_void_truncation_radius 1.2
_olex2_submission_special_instructions 'No special instructions were received'
