# Electronic Supplementary Material (ESI) for Physical Chemistry Chemical Physics.
# This journal is © the Owner Societies 2024

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_AgBr2_4pica_final
_database_code_depnum_ccdc_archive 'CCDC 2298748'
loop_
_audit_author_name
_audit_author_address
'Caterina Zuffa'
;University of Bologna
Italy
;
_audit_update_record             
;
2023-10-02 deposited with the CCDC.	2024-01-03 downloaded from the CCDC.
;
# start Validation Reply Form
_vrf_PLAT602_AgBr2_4pica_final   
;
PROBLEM: Solvent Accessible VOID(S) in Structure ........          ! Check
RESPONSE: No void detected with Mercury.
;
# Added during the CSD deposition process: Monday 02 October 2023 02:51 PM
# end Validation Reply Form



#==============================================================================
# Chemical + Structural + Crystal Information
#==============================================================================
_chemical_formula_moiety         'C6 H8 Ag2 Br2 N2'
# Note: _chemical_formula_sum/_weight/_cell_formula_units_Z need to be 
# recalculated if any one is changed
_chemical_formula_sum            'C6 H8 Ag2 Br2 N2'
_chemical_formula_weight         483.68
_cell_formula_units_Z            8
_pd_char_colour                  whitish #ITC Vol G p.233-234
_exptl_crystal_density_diffrn    3.088
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_cell_measurement_temperature    293 #Experiment temperature in K

#==============================================================================
# Instrument + Refinement Information
#==============================================================================
_diffrn_ambient_temperature      293 #Experiment temperature in K
_diffrn_measurement_device_type  Xpert-PRO
_diffrn_radiation_probe          x-ray
_diffrn_radiation_wavelength     1.535
_diffrn_radiation_type           'Cu K\a' #ITC Vol G p.227
_pd_proc_ls_prof_R_factor        0.0448
_pd_proc_ls_prof_wR_factor       0.0607
_pd_proc_ls_prof_wR_expected     0.0562
_refine_ls_R_I_factor            0.0337
_refine_ls_goodness_of_fit_all   1.08003
_refine_ls_shift/su_max          0.00175644498
_refine_ls_number_parameters     0.000000
_refine_ls_number_restraints     ? #How many restraints used
_refine_diff_density_max         ? #Highest Fourier peak
_refine_diff_density_min         ? #Deepest Fourier hole
_refine_ls_hydrogen_treatment    constr
_pd_spec_mount_mode              transmission
_pd_proc_ls_background_function  Chebyschev
_computing_cell_refinement       
;
 TOPAS-Academic v. 5.0
;
_computing_data_reduction        ?
_computing_structure_solution    
;
 TOPAS-Academic v. 5.0
;
_computing_structure_refinement  
;
 TOPAS-Academic v. 5.0
;

#==============================================================================
# Phase Information
#==============================================================================
_cell_length_a                   14.282(1)
_cell_length_b                   22.011(1)
_cell_length_c                   6.624(1)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_volume                     2082.39918
_symmetry_cell_setting           Orthorhombic #Crystal system
_symmetry_space_group_name_H-M   Pbca
_symmetry_space_group_name_Hall  ? #Get from checkCIF
_space_group_IT_number           61
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z '
'-x, y+1/2, -z+1/2 '
'-x+1/2, -y, z+1/2 '
'-x+1/2, y+1/2, z '
'x, -y+1/2, z+1/2 '
'-x, -y, -z '
'x+1/2, -y+1/2, -z '
'x+1/2, y, -z+1/2 '

# Atomic coordinates & thermal parameters
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_symmetry_multiplicity
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_B_iso_or_equiv
Ag1 Ag 8 -20.4059(3) 5.35745(14) 39.5060(10) 1 4.161025
Br1 Br 8 -20.2217(3) 5.3175(2) 39.5450(10) 1 3.178013
Ag2 Ag 8 -20.3369(3) 5.2474(4) 39.2905(7) 1 4.161025
Br2 Br 8 -20.4279(4) 5.33203(19) 39.0408(11) 1 3.178013
N2 N 8 -20.5626(17) 5.3166(5) 39.543(6) 1 3
C1 C 8 -20.635(3) 5.3496(9) 39.429(8) 1 3
C2 C 8 -20.632(4) 5.4173(8) 39.462(10) 1 3
C3 C 8 -20.597(4) 5.4404(9) 39.640(11) 1 3
C4 C 8 -20.665(7) 5.4578(13) 39.322(14) 1 3
C6 C 8 -20.595(5) 5.5013(11) 39.688(13) 1 3
C5 C 8 -20.662(8) 5.5191(12) 39.364(17) 1 3
N1 N 8 -20.627(6) 5.5403(9) 39.548(16) 1 3
H21 H 8 -20.5713 5.2715 39.517 1 6
H22 H 8 -20.572 5.3248 39.692 1 6
H1 H 8 -20.7032 5.3328 39.476 1 6
H2 H 8 -20.625 5.3406 39.269 1 6
H3 H 8 -20.569 5.4084 39.750 1 6
H4 H 8 -20.694 5.4418 39.179 1 6
H5 H 8 -20.686 5.5515 39.25 1 6
H6 H 8 -20.568 5.5171 39.833 1 6

# Molecular Geometry
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_1
_geom_bond_site_symmetry_2
Ag1 N1 2.33(5) 1_555 6_-361684

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_2
_geom_angle_site_symmetry_3
C1 C2 C3 120.010565000000(4) 1_555 1_555 1_555


#==============================================================================
# PD Data Block - Obs + Calc
#==============================================================================
_pd_proc_2theta_range_min        6.00307 #Lowest value in column 2 below
_pd_proc_2theta_range_max        74.96807 #Lowest value in column 2 below
_pd_proc_2theta_range_inc        0.013
_pd_meas_number_of_points        
5306 #This is the last number in column 1 below

loop_
_pd_proc_point_id
_pd_meas_2theta_scan
_pd_proc_intensity_total
_pd_calc_intensity_total
_pd_proc_ls_weight
1 6.00307 354.19627 349.69003 0.00286
2 6.01607 353.67127 353.43997 0.00283
3 6.02907 353.14765 357.20999 0.00280
4 6.04207 352.62542 349.69003 0.00286
5 6.05507 352.10459 361.00000 0.00277
6 6.06807 351.58514 342.25000 0.00292
7 6.08107 351.06709 331.24002 0.00302
8 6.09407 350.55045 334.88998 0.00299
9 6.10707 350.03520 342.25000 0.00292
10 6.12007 349.52136 338.56000 0.00295
11 6.13307 349.00892 342.25000 0.00292
12 6.14607 348.49791 349.69003 0.00286
13 6.15907 347.98834 338.56000 0.00295
14 6.17207 347.48019 349.69003 0.00286
15 6.18507 346.97348 338.56000 0.00295
16 6.19807 346.46824 342.25000 0.00292
17 6.21107 345.96449 342.25000 0.00292
18 6.22407 345.46221 345.96002 0.00289
19 6.23707 344.96142 327.61002 0.00305
20 6.25007 344.46215 345.96002 0.00289
21 6.26307 343.96446 327.61002 0.00305
22 6.27607 343.46830 331.24002 0.00302
23 6.28907 342.97369 334.88998 0.00299
24 6.30207 342.48066 342.25000 0.00292
25 6.31507 341.98933 353.43997 0.00283
26 6.32807 341.49964 331.24002 0.00302
27 6.34107 341.01159 331.24002 0.00302
28 6.35407 340.52521 331.24002 0.00302
29 6.36707 340.04068 327.61002 0.00305
30 6.38007 339.55794 327.61002 0.00305
31 6.39307 339.07699 327.61002 0.00305
32 6.40607 338.59786 334.88998 0.00299
33 6.41907 338.12075 334.88998 0.00299
34 6.43207 337.64570 331.24002 0.00302
35 6.44507 337.17267 334.88998 0.00299
36 6.45807 336.70170 342.25000 0.00292
37 6.47107 336.23298 334.88998 0.00299
38 6.48407 335.76680 327.61002 0.00305
39 6.49707 335.30298 327.61002 0.00305
40 6.51007 334.84163 338.56000 0.00295
41 6.52307 334.38286 338.56000 0.00295
42 6.53607 333.92746 331.24002 0.00302
43 6.54907 333.47504 331.24002 0.00302
44 6.56207 333.02579 342.25000 0.00292
45 6.57507 332.57987 342.25000 0.00292
46 6.58807 332.13851 327.61002 0.00305
47 6.60107 331.70156 320.40997 0.00312
48 6.61407 331.26922 316.83997 0.00316
49 6.62707 330.84190 327.61002 0.00305
50 6.64007 330.42147 327.61002 0.00305
51 6.65307 330.00929 327.61002 0.00305
52 6.66607 329.60586 327.61002 0.00305
53 6.67907 329.21293 324.00000 0.00309
54 6.69207 328.83495 327.61002 0.00305
55 6.70507 328.48653 327.61002 0.00305
56 6.71807 328.18392 324.00000 0.00309
57 6.73107 327.91981 324.00000 0.00309
58 6.74407 327.67932 324.00000 0.00309
59 6.75707 327.27870 331.24002 0.00302
60 6.77007 326.86915 327.61002 0.00305
61 6.78307 326.45836 324.00000 0.00309
62 6.79607 326.05048 320.40997 0.00312
63 6.80907 325.64634 320.40997 0.00312
64 6.82207 325.24562 313.29004 0.00319
65 6.83507 324.84831 313.29004 0.00319
66 6.84807 324.45452 324.00000 0.00309
67 6.86107 324.06507 320.40997 0.00312
68 6.87407 323.68017 320.40997 0.00312
69 6.88707 323.29951 320.40997 0.00312
70 6.90007 322.92329 320.40997 0.00312
71 6.91307 322.55225 334.88998 0.00299
72 6.92607 322.18752 331.24002 0.00302
73 6.93907 321.82836 313.29004 0.00319
74 6.95207 321.47506 313.29004 0.00319
75 6.96507 321.12814 320.40997 0.00312
76 6.97807 320.79052 320.40997 0.00312
77 6.99107 320.46068 324.00000 0.00309
78 7.00407 320.13923 327.61002 0.00305
79 7.01707 319.82679 320.40997 0.00312
80 7.03007 319.52796 316.83997 0.00316
81 7.04307 319.24230 316.83997 0.00316
82 7.05607 318.97072 316.83997 0.00316
83 7.06907 318.71516 316.83997 0.00316
84 7.08207 318.48414 309.76001 0.00323
85 7.09507 318.28927 313.29004 0.00319
86 7.10807 318.14555 316.83997 0.00316
87 7.12107 318.05242 320.40997 0.00312
88 7.13407 317.99749 327.61002 0.00305
89 7.14707 317.81356 331.24002 0.00302
90 7.16007 317.62268 324.00000 0.00309
91 7.17307 317.44431 320.40997 0.00312
92 7.18607 317.28549 338.56000 0.00295
93 7.19907 317.15951 324.00000 0.00309
94 7.21207 317.06622 331.24002 0.00302
95 7.22507 317.01582 342.25000 0.00292
96 7.23807 317.01952 338.56000 0.00295
97 7.25107 317.13107 345.96002 0.00289
98 7.26407 317.36694 345.96002 0.00289
99 7.27707 317.74399 334.88998 0.00299
100 7.29007 318.28630 331.24002 0.00302
101 7.30307 319.08225 320.40997 0.00312
102 7.31607 320.18551 327.61002 0.00305
103 7.32907 321.59563 327.61002 0.00305
104 7.34207 323.35635 338.56000 0.00295
105 7.35507 325.58660 334.88998 0.00299
106 7.36807 328.41701 342.25000 0.00292
107 7.38107 331.66669 353.43997 0.00283
108 7.39407 335.41220 349.69003 0.00286
109 7.40707 339.78634 357.20999 0.00280
110 7.42007 345.22479 364.81003 0.00274
111 7.43307 351.51970 361.00000 0.00277
112 7.44607 358.69301 364.81003 0.00274
113 7.45907 366.77700 380.25000 0.00263
114 7.47207 376.32722 384.16000 0.00260
115 7.48507 386.99647 392.03998 0.00255
116 7.49807 398.81457 404.01001 0.00248
117 7.51107 411.86790 400.00000 0.00250
118 7.52407 426.57133 428.49002 0.00233
119 7.53707 442.99103 432.63995 0.00231
120 7.55007 460.94435 441.00000 0.00227
121 7.56307 480.50887 462.25000 0.00216
122 7.57607 502.02343 488.41000 0.00205
123 7.58907 525.99547 475.23996 0.00210
124 7.60207 552.01476 524.40997 0.00191
125 7.61507 580.20047 529.00000 0.00189
126 7.62807 610.74323 571.20996 0.00175
127 7.64107 644.90661 600.25000 0.00167
128 7.65407 681.92357 615.03998 0.00163
129 7.66707 721.99813 655.36005 0.00153
130 7.68007 765.34230 723.60999 0.00138
131 7.69307 813.68714 767.29004 0.00130
132 7.70607 866.59929 800.88995 0.00125
133 7.71907 924.13486 858.48993 0.00116
134 7.73207 986.67785 894.00995 0.00112
135 7.74507 1056.25644 973.44006 0.00103
136 7.75807 1133.71236 1030.40991 0.00097
137 7.77107 1218.64473 1135.69006 0.00088
138 7.78407 1311.80361 1225.00000 0.00082
139 7.79707 1415.49179 1317.68994 0.00076
140 7.81007 1533.76311 1428.83997 0.00070
141 7.82307 1665.33899 1568.15991 0.00064
142 7.83607 1811.95605 1738.89001 0.00058
143 7.84907 1976.00147 1874.88989 0.00053
144 7.86207 2170.66013 2052.08984 0.00049
145 7.87507 2393.31802 2284.83984 0.00044
146 7.88807 2649.34545 2540.16016 0.00039
147 7.90107 2944.67491 2883.69019 0.00035
148 7.91407 3312.63444 3237.61011 0.00031
149 7.92707 3766.78953 3721.00000 0.00027
150 7.94007 4331.64113 4303.35986 0.00023
151 7.95307 5046.08033 5083.69043 0.00020
152 7.96607 6056.46725 6162.25000 0.00016
153 7.97907 7639.59025 7673.75977 0.00013
154 7.99207 9686.74635 9623.60938 0.00010
155 8.00507 11651.94450 11342.25000 0.00009
156 8.01807 12137.71462 11406.24023 0.00009
157 8.03107 8849.49376 8949.16016 0.00011
158 8.04407 5479.82479 5372.89063 0.00019
159 8.05707 2815.03229 2641.96021 0.00038
160 8.07007 1359.10246 1281.63989 0.00078
161 8.08307 914.11582 745.28998 0.00134
162 8.09607 683.42908 547.56000 0.00183
163 8.10907 572.46158 449.44003 0.00222
164 8.12207 506.45178 400.00000 0.00250
165 8.13507 464.71628 372.48996 0.00268
166 8.14807 433.20924 361.00000 0.00277
167 8.16107 408.69194 342.25000 0.00292
168 8.17407 389.40531 331.24002 0.00302
169 8.18707 374.62388 331.24002 0.00302
170 8.20007 362.76303 324.00000 0.00309
171 8.21307 352.79654 316.83997 0.00316
172 8.22607 344.39829 313.29004 0.00319
173 8.23907 337.40863 306.25000 0.00327
174 8.25207 331.61724 302.75998 0.00330
175 8.26507 326.54664 309.76001 0.00323
176 8.27807 322.09784 306.25000 0.00327
177 8.29107 318.18982 302.75998 0.00330
178 8.30407 314.86190 295.84003 0.00338
179 8.31707 311.85774 295.84003 0.00338
180 8.33007 309.14039 292.41000 0.00342
181 8.34307 306.67480 292.41000 0.00342
182 8.35607 304.48921 292.41000 0.00342
183 8.36907 302.48629 289.00000 0.00346
184 8.38207 300.63260 289.00000 0.00346
185 8.39507 298.91291 295.84003 0.00338
186 8.40807 297.33660 295.84003 0.00338
187 8.42107 295.87545 292.41000 0.00342
188 8.43407 294.49905 289.00000 0.00346
189 8.44707 293.19965 292.41000 0.00342
190 8.46007 291.97747 292.41000 0.00342
191 8.47307 290.82966 292.41000 0.00342
192 8.48607 289.73038 295.84003 0.00338
193 8.49907 288.67429 289.00000 0.00346
194 8.51207 287.65679 289.00000 0.00346
195 8.52507 286.67759 292.41000 0.00342
196 8.53807 285.71052 289.00000 0.00346
197 8.55107 284.73832 285.60999 0.00350
198 8.56407 283.74737 285.60999 0.00350
199 8.57707 282.74924 282.23996 0.00354
200 8.59007 281.85343 289.00000 0.00346
201 8.60307 280.99196 282.23996 0.00354
202 8.61607 280.14980 275.56000 0.00363
203 8.62907 279.42438 275.56000 0.00363
204 8.64207 278.71344 285.60999 0.00350
205 8.65507 278.10399 289.00000 0.00346
206 8.66807 277.59100 278.89001 0.00359
207 8.68107 277.10036 275.56000 0.00363
208 8.69407 276.62244 275.56000 0.00363
209 8.70707 276.15362 295.84003 0.00338
210 8.72007 275.69338 278.89001 0.00359
211 8.73307 275.24138 278.89001 0.00359
212 8.74607 274.79926 285.60999 0.00350
213 8.75907 274.36360 272.25000 0.00367
214 8.77207 273.93399 272.25000 0.00367
215 8.78507 273.50999 289.00000 0.00346
216 8.79807 273.09232 289.00000 0.00346
217 8.81107 272.67903 285.60999 0.00350
218 8.82407 272.26928 278.89001 0.00359
219 8.83707 271.86253 289.00000 0.00346
220 8.85007 271.45822 285.60999 0.00350
221 8.86307 271.05461 285.60999 0.00350
222 8.87607 270.65018 285.60999 0.00350
223 8.88907 270.24327 299.28998 0.00334
224 8.90207 269.83057 295.84003 0.00338
225 8.91507 269.39934 285.60999 0.00350
226 8.92807 268.93291 299.28998 0.00334
227 8.94107 268.43982 299.28998 0.00334
228 8.95407 267.93612 302.75998 0.00330
229 8.96707 267.60454 313.29004 0.00319
230 8.98007 267.28657 309.76001 0.00323
231 8.99307 266.97480 324.00000 0.00309
232 9.00607 266.66502 349.69003 0.00286
233 9.01907 266.35744 345.96002 0.00289
234 9.03207 266.05164 372.48996 0.00268
235 9.04507 265.74747 408.04004 0.00245
236 9.05807 265.44484 388.09003 0.00258
237 9.07107 265.14377 368.64001 0.00271
238 9.08407 264.84403 331.24002 0.00302
239 9.09707 264.54544 302.75998 0.00330
240 9.11007 264.24788 285.60999 0.00350
241 9.12307 263.95123 275.56000 0.00363
242 9.13607 263.65520 272.25000 0.00367
243 9.14907 263.35964 275.56000 0.00363
244 9.16207 263.06437 262.44003 0.00381
245 9.17507 262.76919 265.68997 0.00376
246 9.18807 262.47322 275.56000 0.00363
247 9.20107 262.17641 278.89001 0.00359
248 9.21407 261.87835 268.95999 0.00372
249 9.22707 261.57856 262.44003 0.00381
250 9.24007 261.27463 268.95999 0.00372
251 9.25307 260.96530 278.89001 0.00359
252 9.26607 260.64791 275.56000 0.00363
253 9.27907 260.31980 268.95999 0.00372
254 9.29207 259.97346 259.21002 0.00386
255 9.30507 259.59159 259.21002 0.00386
256 9.31807 259.18319 259.21002 0.00386
257 9.33107 258.79681 265.68997 0.00376
258 9.34407 258.55509 268.95999 0.00372
259 9.35707 258.29753 265.68997 0.00376
260 9.37007 258.05752 272.25000 0.00367
261 9.38307 257.81837 265.68997 0.00376
262 9.39607 257.58006 272.25000 0.00367
263 9.40907 257.34260 282.23996 0.00354
264 9.42207 257.10599 272.25000 0.00367
265 9.43507 256.87023 268.95999 0.00372
266 9.44807 256.63531 262.44003 0.00381
267 9.46107 256.40124 265.68997 0.00376
268 9.47407 256.16800 268.95999 0.00372
269 9.48707 255.93560 265.68997 0.00376
270 9.50007 255.70405 262.44003 0.00381
271 9.51307 255.47333 256.00000 0.00391
272 9.52607 255.24344 256.00000 0.00391
273 9.53907 255.01439 262.44003 0.00381
274 9.55207 254.78617 262.44003 0.00381
275 9.56507 254.55878 249.64000 0.00401
276 9.57807 254.33223 249.64000 0.00401
277 9.59107 254.10650 256.00000 0.00391
278 9.60407 253.88160 259.21002 0.00386
279 9.61707 253.65752 262.44003 0.00381
280 9.63007 253.43427 259.21002 0.00386
281 9.64307 253.21185 256.00000 0.00391
282 9.65607 252.99025 256.00000 0.00391
283 9.66907 252.76948 262.44003 0.00381
284 9.68207 252.54953 259.21002 0.00386
285 9.69507 252.33041 262.44003 0.00381
286 9.70807 252.11211 262.44003 0.00381
287 9.72107 251.89464 262.44003 0.00381
288 9.73407 251.67801 256.00000 0.00391
289 9.74707 251.46221 256.00000 0.00391
290 9.76007 251.24726 256.00000 0.00391
291 9.77307 251.03318 249.64000 0.00401
292 9.78607 250.82004 249.64000 0.00401
293 9.79907 250.60790 256.00000 0.00391
294 9.81207 250.39678 262.44003 0.00381
295 9.82507 250.18657 256.00000 0.00391
296 9.83807 249.97641 256.00000 0.00391
297 9.85107 249.76687 249.64000 0.00401
298 9.86407 249.55810 256.00000 0.00391
299 9.87707 249.35011 249.64000 0.00401
300 9.89007 249.14292 249.64000 0.00401
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1542 26.03607 261.84124 275.56000 0.00363
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1544 26.06207 258.50734 275.56000 0.00363
1545 26.07507 256.53722 268.95999 0.00372
1546 26.08807 254.66455 252.80998 0.00396
1547 26.10107 252.98475 252.80998 0.00396
1548 26.11407 251.51937 249.64000 0.00401
1549 26.12707 250.29854 256.00000 0.00391
1550 26.14007 249.42514 262.44003 0.00381
1551 26.15307 248.80732 246.48999 0.00406
1552 26.16607 248.36556 249.64000 0.00401
1553 26.17907 248.05472 249.64000 0.00401
1554 26.19207 247.83421 237.15999 0.00422
1555 26.20507 247.58152 246.48999 0.00406
1556 26.21807 247.29785 249.64000 0.00401
1557 26.23107 246.98804 249.64000 0.00401
1558 26.24407 246.66745 240.25000 0.00416
1559 26.25707 246.36673 240.25000 0.00416
1560 26.27007 246.10259 240.25000 0.00416
1561 26.28307 245.87994 237.15999 0.00422
1562 26.29607 245.70380 234.09001 0.00427
1563 26.30907 245.59692 252.80998 0.00396
1564 26.32207 245.54608 246.48999 0.00406
1565 26.33507 245.55002 243.36002 0.00411
1566 26.34807 245.60734 243.36002 0.00411
1567 26.36107 245.72764 246.48999 0.00406
1568 26.37407 245.90189 249.64000 0.00401
1569 26.38707 246.12891 240.25000 0.00416
1570 26.40007 246.40598 243.36002 0.00411
1571 26.41307 246.73779 246.48999 0.00406
1572 26.42607 247.12815 246.48999 0.00406
1573 26.43907 247.59732 246.48999 0.00406
1574 26.45207 248.14666 252.80998 0.00396
1575 26.46507 248.79299 262.44003 0.00381
1576 26.47807 249.56464 262.44003 0.00381
1577 26.49107 250.54546 259.21002 0.00386
1578 26.50407 251.78389 262.44003 0.00381
1579 26.51707 253.32609 262.44003 0.00381
1580 26.53007 255.25293 268.95999 0.00372
1581 26.54307 257.77500 275.56000 0.00363
1582 26.55607 261.12789 275.56000 0.00363
1583 26.56907 265.40872 282.23996 0.00354
1584 26.58207 270.86704 289.00000 0.00346
1585 26.59507 278.01625 295.84003 0.00338
1586 26.60807 288.10721 302.75998 0.00330
1587 26.62107 301.17051 313.29004 0.00319
1588 26.63407 317.40395 331.24002 0.00302
1589 26.64707 337.04663 349.69003 0.00286
1590 26.66007 358.47303 368.64001 0.00271
1591 26.67307 376.30166 388.09003 0.00258
1592 26.68607 387.69163 400.00000 0.00250
1593 26.69907 391.08091 400.00000 0.00250
1594 26.71207 384.49164 392.03998 0.00255
1595 26.72507 378.06399 384.16000 0.00260
1596 26.73807 374.67269 388.09003 0.00258
1597 26.75107 377.22785 384.16000 0.00260
1598 26.76407 385.58929 392.03998 0.00255
1599 26.77707 398.83943 404.01001 0.00248
1600 26.79007 418.22823 416.15997 0.00240
1601 26.80307 446.17173 445.21002 0.00225
1602 26.81607 482.24184 484.00000 0.00207
1603 26.82907 523.30488 533.61005 0.00187
1604 26.84207 565.72126 561.69006 0.00178
1605 26.85507 604.67347 600.25000 0.00167
1606 26.86807 629.45435 630.01001 0.00159
1607 26.88107 639.13223 640.08997 0.00156
1608 26.89407 633.03116 620.01001 0.00161
1609 26.90707 611.44119 580.81000 0.00172
1610 26.92007 576.52171 556.96002 0.00180
1611 26.93307 538.44672 524.40997 0.00191
1612 26.94607 499.18045 488.41000 0.00205
1613 26.95907 460.52150 462.25000 0.00216
1614 26.97207 424.84907 420.25000 0.00238
1615 26.98507 392.82663 372.48996 0.00268
1616 26.99807 364.46638 349.69003 0.00286
1617 27.01107 339.94573 324.00000 0.00309
1618 27.02407 320.16478 309.76001 0.00323
1619 27.03707 304.65258 299.28998 0.00334
1620 27.05007 292.29777 285.60999 0.00350
1621 27.06307 282.79732 282.23996 0.00354
1622 27.07607 276.07040 275.56000 0.00363
1623 27.08907 271.89213 272.25000 0.00367
1624 27.10207 269.27395 272.25000 0.00367
1625 27.11507 268.04187 272.25000 0.00367
1626 27.12807 268.09993 275.56000 0.00363
1627 27.14107 269.83135 265.68997 0.00376
1628 27.15407 272.90070 275.56000 0.00363
1629 27.16707 277.44189 282.23996 0.00354
1630 27.18007 283.65000 278.89001 0.00359
1631 27.19307 292.65836 278.89001 0.00359
1632 27.20607 303.87298 295.84003 0.00338
1633 27.21907 317.07250 295.84003 0.00338
1634 27.23207 332.05479 313.29004 0.00319
1635 27.24507 348.03890 345.96002 0.00289
1636 27.25807 362.81122 361.00000 0.00277
1637 27.27107 374.97945 392.03998 0.00255
1638 27.28407 383.31644 400.00000 0.00250
1639 27.29707 384.25208 408.04004 0.00245
1640 27.31007 379.48302 416.15997 0.00240
1641 27.32307 370.66564 404.01001 0.00248
1642 27.33607 358.92752 376.35999 0.00266
1643 27.34907 345.67674 380.25000 0.00263
1644 27.36207 332.50852 349.69003 0.00286
1645 27.37507 319.88508 331.24002 0.00302
1646 27.38807 308.09121 313.29004 0.00319
1647 27.40107 297.73113 313.29004 0.00319
1648 27.41407 288.94398 299.28998 0.00334
1649 27.42707 281.55996 289.00000 0.00346
1650 27.44007 275.54321 289.00000 0.00346
1651 27.45307 271.10091 265.68997 0.00376
1652 27.46607 268.07196 265.68997 0.00376
1653 27.47907 266.22930 268.95999 0.00372
1654 27.49207 265.47466 272.25000 0.00367
1655 27.50507 265.82229 265.68997 0.00376
1656 27.51807 267.17329 272.25000 0.00367
1657 27.53107 269.63150 275.56000 0.00363
1658 27.54407 273.10435 285.60999 0.00350
1659 27.55707 277.54161 285.60999 0.00350
1660 27.57007 282.93392 278.89001 0.00359
1661 27.58307 289.84375 289.00000 0.00346
1662 27.59607 298.08922 299.28998 0.00334
1663 27.60907 308.02744 309.76001 0.00323
1664 27.62207 320.12537 313.29004 0.00319
1665 27.63507 336.10156 338.56000 0.00295
1666 27.64807 356.86977 342.25000 0.00292
1667 27.66107 382.37495 353.43997 0.00283
1668 27.67407 412.51804 384.16000 0.00260
1669 27.68707 447.33812 416.15997 0.00240
1670 27.70007 484.02873 445.21002 0.00225
1671 27.71307 518.30511 475.23996 0.00210
1672 27.72607 547.08928 510.76001 0.00196
1673 27.73907 566.69153 538.24005 0.00186
1674 27.75207 568.52387 547.56000 0.00183
1675 27.76507 558.11845 538.24005 0.00186
1676 27.77807 537.98706 524.40997 0.00191
1677 27.79107 510.80617 506.25000 0.00198
1678 27.80407 480.03041 484.00000 0.00207
1679 27.81707 449.45831 457.95999 0.00218
1680 27.83007 420.00153 445.21002 0.00225
1681 27.84307 392.32403 420.25000 0.00238
1682 27.85607 367.70127 392.03998 0.00255
1683 27.86907 346.55150 372.48996 0.00268
1684 27.88207 328.48359 349.69003 0.00286
1685 27.89507 313.43981 331.24002 0.00302
1686 27.90807 301.70678 320.40997 0.00312
1687 27.92107 293.29610 306.25000 0.00327
1688 27.93407 287.37168 302.75998 0.00330
1689 27.94707 283.75549 299.28998 0.00334
1690 27.96007 282.35371 295.84003 0.00338
1691 27.97307 283.32595 299.28998 0.00334
1692 27.98607 286.73211 306.25000 0.00327
1693 27.99907 292.63501 306.25000 0.00327
1694 28.01207 301.24380 309.76001 0.00323
1695 28.02507 312.99510 316.83997 0.00316
1696 28.03807 330.29612 334.88998 0.00299
1697 28.05107 352.70797 364.81003 0.00274
1698 28.06407 380.58396 380.25000 0.00263
1699 28.07707 414.40146 408.04004 0.00245
1700 28.09007 457.55787 453.68997 0.00220
1701 28.10307 505.51421 501.75998 0.00199
1702 28.11607 556.26312 542.88995 0.00184
1703 28.12907 607.93203 600.25000 0.00167
1704 28.14207 652.68688 660.49005 0.00151
1705 28.15507 684.08738 707.56000 0.00141
1706 28.16807 699.99371 745.28998 0.00134
1707 28.18107 698.40250 756.25000 0.00132
1708 28.19407 674.23703 739.84003 0.00135
1709 28.20707 638.88993 686.44006 0.00146
1710 28.22007 597.75256 630.01001 0.00159
1711 28.23307 553.79106 595.35999 0.00168
1712 28.24607 510.26175 566.43994 0.00177
1713 28.25907 469.31701 515.29004 0.00194
1714 28.27207 431.40566 466.56003 0.00214
1715 28.28507 396.91115 416.15997 0.00240
1716 28.29807 367.40849 372.48996 0.00268
1717 28.31107 342.81716 353.43997 0.00283
1718 28.32407 322.10076 327.61002 0.00305
1719 28.33707 305.03141 320.40997 0.00312
1720 28.35007 291.95526 302.75998 0.00330
1721 28.36307 282.24503 292.41000 0.00342
1722 28.37607 274.71570 285.60999 0.00350
1723 28.38907 269.04314 268.95999 0.00372
1724 28.40207 265.06504 275.56000 0.00363
1725 28.41507 262.37204 265.68997 0.00376
1726 28.42807 260.40296 272.25000 0.00367
1727 28.44107 259.03295 265.68997 0.00376
1728 28.45407 258.18740 256.00000 0.00391
1729 28.46707 257.86969 262.44003 0.00381
1730 28.48007 257.95052 252.80998 0.00396
1731 28.49307 258.48137 259.21002 0.00386
1732 28.50607 259.54519 262.44003 0.00381
1733 28.51907 261.58107 272.25000 0.00367
1734 28.53207 264.51173 256.00000 0.00391
1735 28.54507 268.44691 265.68997 0.00376
1736 28.55807 273.48546 282.23996 0.00354
1737 28.57107 280.10877 275.56000 0.00363
1738 28.58407 287.73028 278.89001 0.00359
1739 28.59707 295.88962 299.28998 0.00334
1740 28.61007 304.15677 299.28998 0.00334
1741 28.62307 311.46647 316.83997 0.00316
1742 28.63607 316.39030 316.83997 0.00316
1743 28.64907 318.69782 324.00000 0.00309
1744 28.66207 318.23412 334.88998 0.00299
1745 28.67507 314.72316 342.25000 0.00292
1746 28.68807 309.12377 320.40997 0.00312
1747 28.70107 302.85999 316.83997 0.00316
1748 28.71407 296.35621 316.83997 0.00316
1749 28.72707 289.94285 299.28998 0.00334
1750 28.74007 284.01283 302.75998 0.00330
1751 28.75307 278.58857 282.23996 0.00354
1752 28.76607 273.62838 282.23996 0.00354
1753 28.77907 269.12927 278.89001 0.00359
1754 28.79207 265.32231 268.95999 0.00372
1755 28.80507 261.94633 262.44003 0.00381
1756 28.81807 258.82569 268.95999 0.00372
1757 28.83107 256.10320 272.25000 0.00367
1758 28.84407 253.87076 259.21002 0.00386
1759 28.85707 252.01497 259.21002 0.00386
1760 28.87007 250.44417 252.80998 0.00396
1761 28.88307 249.13471 259.21002 0.00386
1762 28.89607 248.06212 246.48999 0.00406
1763 28.90907 247.17794 252.80998 0.00396
1764 28.92207 246.43447 246.48999 0.00406
1765 28.93507 245.81346 256.00000 0.00391
1766 28.94807 245.29181 252.80998 0.00396
1767 28.96107 244.85946 252.80998 0.00396
1768 28.97407 244.50134 249.64000 0.00401
1769 28.98707 244.21054 240.25000 0.00416
1770 29.00007 243.97009 243.36002 0.00411
1771 29.01307 243.77412 243.36002 0.00411
1772 29.02607 243.61446 246.48999 0.00406
1773 29.03907 243.48694 234.09001 0.00427
1774 29.05207 243.38452 240.25000 0.00416
1775 29.06507 243.30683 246.48999 0.00406
1776 29.07807 243.25104 246.48999 0.00406
1777 29.09107 243.21224 243.36002 0.00411
1778 29.10407 243.20551 237.15999 0.00422
1779 29.11707 243.21448 237.15999 0.00422
1780 29.13007 243.20529 237.15999 0.00422
1781 29.14307 243.18109 243.36002 0.00411
1782 29.15607 243.16464 249.64000 0.00401
1783 29.16907 243.15937 246.48999 0.00406
1784 29.18207 243.16608 240.25000 0.00416
1785 29.19507 243.18112 240.25000 0.00416
1786 29.20807 243.19782 243.36002 0.00411
1787 29.22107 243.22036 259.21002 0.00386
1788 29.23407 243.25319 252.80998 0.00396
1789 29.24707 243.30042 240.25000 0.00416
1790 29.26007 243.36092 243.36002 0.00411
1791 29.27307 243.43718 240.25000 0.00416
1792 29.28607 243.53313 240.25000 0.00416
1793 29.29907 243.65762 246.48999 0.00406
1794 29.31207 243.81281 246.48999 0.00406
1795 29.32507 244.00604 240.25000 0.00416
1796 29.33807 244.24719 246.48999 0.00406
1797 29.35107 244.57907 246.48999 0.00406
1798 29.36407 245.00619 246.48999 0.00406
1799 29.37707 245.55159 256.00000 0.00391
1800 29.39007 246.24454 252.80998 0.00396
1801 29.40307 247.17581 259.21002 0.00386
1802 29.41607 248.35329 249.64000 0.00401
1803 29.42907 249.76766 256.00000 0.00391
1804 29.44207 251.44565 259.21002 0.00386
1805 29.45507 253.38794 249.64000 0.00401
1806 29.46807 255.46889 259.21002 0.00386
1807 29.48107 257.55295 256.00000 0.00391
1808 29.49407 259.64051 252.80998 0.00396
1809 29.50707 261.59171 259.21002 0.00386
1810 29.52007 263.19130 259.21002 0.00386
1811 29.53307 264.72367 268.95999 0.00372
1812 29.54607 266.60539 268.95999 0.00372
1813 29.55907 269.11913 278.89001 0.00359
1814 29.57207 272.51682 275.56000 0.00363
1815 29.58507 277.12099 275.56000 0.00363
1816 29.59807 283.45243 265.68997 0.00376
1817 29.61107 291.66809 285.60999 0.00350
1818 29.62407 301.21006 292.41000 0.00342
1819 29.63707 311.73408 295.84003 0.00338
1820 29.65007 322.69869 306.25000 0.00327
1821 29.66307 332.30430 313.29004 0.00319
1822 29.67607 339.52357 320.40997 0.00312
1823 29.68907 343.68878 327.61002 0.00305
1824 29.70207 343.97138 324.00000 0.00309
1825 29.71507 339.27771 324.00000 0.00309
1826 29.72807 332.39540 316.83997 0.00316
1827 29.74107 324.07719 316.83997 0.00316
1828 29.75407 315.02405 302.75998 0.00330
1829 29.76707 305.98442 306.25000 0.00327
1830 29.78007 297.32097 299.28998 0.00334
1831 29.79307 289.16392 285.60999 0.00350
1832 29.80607 281.60799 275.56000 0.00363
1833 29.81907 275.01188 275.56000 0.00363
1834 29.83207 269.34342 268.95999 0.00372
1835 29.84507 264.49715 256.00000 0.00391
1836 29.85807 260.46481 278.89001 0.00359
1837 29.87107 257.36931 262.44003 0.00381
1838 29.88407 255.05923 259.21002 0.00386
1839 29.89707 253.31805 272.25000 0.00367
1840 29.91007 252.07454 275.56000 0.00363
1841 29.92307 251.27409 268.95999 0.00372
1842 29.93607 250.80969 259.21002 0.00386
1843 29.94907 250.51918 259.21002 0.00386
1844 29.96207 250.31868 246.48999 0.00406
1845 29.97507 250.18355 259.21002 0.00386
1846 29.98807 250.10417 249.64000 0.00401
1847 30.00107 250.03415 252.80998 0.00396
1848 30.01407 249.98748 246.48999 0.00406
1849 30.02707 250.01215 240.25000 0.00416
1850 30.04007 250.17185 249.64000 0.00401
1851 30.05307 250.48186 249.64000 0.00401
1852 30.06607 250.98072 252.80998 0.00396
1853 30.07907 251.70656 246.48999 0.00406
1854 30.09207 252.78300 252.80998 0.00396
1855 30.10507 254.31359 252.80998 0.00396
1856 30.11807 256.28675 259.21002 0.00386
1857 30.13107 258.71462 265.68997 0.00376
1858 30.14407 261.63393 265.68997 0.00376
1859 30.15707 265.03518 265.68997 0.00376
1860 30.17007 268.56245 272.25000 0.00367
1861 30.18307 271.98213 282.23996 0.00354
1862 30.19607 275.05431 282.23996 0.00354
1863 30.20907 277.08127 275.56000 0.00363
1864 30.22207 277.93150 282.23996 0.00354
1865 30.23507 277.74207 278.89001 0.00359
1866 30.24807 276.62636 268.95999 0.00372
1867 30.26107 274.76776 268.95999 0.00372
1868 30.27407 272.63672 272.25000 0.00367
1869 30.28707 270.47904 272.25000 0.00367
1870 30.30007 268.38654 265.68997 0.00376
1871 30.31307 266.43338 272.25000 0.00367
1872 30.32607 264.74904 262.44003 0.00381
1873 30.33907 263.32242 272.25000 0.00367
1874 30.35207 262.18897 265.68997 0.00376
1875 30.36507 261.39142 259.21002 0.00386
1876 30.37807 261.01466 262.44003 0.00381
1877 30.39107 261.00284 262.44003 0.00381
1878 30.40407 261.32851 265.68997 0.00376
1879 30.41707 262.01566 265.68997 0.00376
1880 30.43007 263.02148 265.68997 0.00376
1881 30.44307 264.29336 268.95999 0.00372
1882 30.45607 265.74097 268.95999 0.00372
1883 30.46907 267.26244 275.56000 0.00363
1884 30.48207 268.77418 275.56000 0.00363
1885 30.49507 270.27474 278.89001 0.00359
1886 30.50807 271.70596 278.89001 0.00359
1887 30.52107 273.06972 268.95999 0.00372
1888 30.53407 274.48677 268.95999 0.00372
1889 30.54707 276.13586 278.89001 0.00359
1890 30.56007 278.04041 278.89001 0.00359
1891 30.57307 280.37065 275.56000 0.00363
1892 30.58607 283.21592 285.60999 0.00350
1893 30.59907 286.74970 289.00000 0.00346
1894 30.61207 291.04867 285.60999 0.00350
1895 30.62507 296.43362 289.00000 0.00346
1896 30.63807 303.07726 299.28998 0.00334
1897 30.65107 311.12253 306.25000 0.00327
1898 30.66407 320.74006 320.40997 0.00312
1899 30.67707 332.17132 327.61002 0.00305
1900 30.69007 345.39166 338.56000 0.00295
1901 30.70307 360.33682 364.81003 0.00274
1902 30.71607 377.61958 380.25000 0.00263
1903 30.72907 397.13890 404.01001 0.00248
1904 30.74207 418.90386 428.49002 0.00233
1905 30.75507 443.90111 449.44003 0.00222
1906 30.76807 476.75100 484.00000 0.00207
1907 30.78107 517.80742 529.00000 0.00189
1908 30.79407 568.84926 580.81000 0.00172
1909 30.80707 633.06371 660.49005 0.00151
1910 30.82007 724.97919 761.76001 0.00131
1911 30.83307 849.97429 900.00000 0.00111
1912 30.84607 1016.97862 1089.00000 0.00092
1913 30.85907 1237.20794 1369.00000 0.00073
1914 30.87207 1545.94389 1713.96008 0.00058
1915 30.88507 1927.08578 2070.25000 0.00048
1916 30.89807 2287.24211 2401.00000 0.00042
1917 30.91107 2540.01036 2570.48999 0.00039
1918 30.92407 2508.97416 2520.04004 0.00040
1919 30.93707 2180.95656 2275.29004 0.00044
1920 30.95007 1868.80490 1953.64001 0.00051
1921 30.96307 1645.78204 1738.89001 0.00058
1922 30.97607 1560.37351 1592.01013 0.00063
1923 30.98907 1507.11949 1513.21008 0.00066
1924 31.00207 1386.74866 1317.68994 0.00076
1925 31.01507 1207.53915 1095.60986 0.00091
1926 31.02807 986.56560 894.00995 0.00112
1927 31.04107 807.74094 707.56000 0.00141
1928 31.05407 676.92808 590.48999 0.00169
1929 31.06707 582.53395 501.75998 0.00199
1930 31.08007 516.56670 445.21002 0.00225
1931 31.09307 472.33301 408.04004 0.00245
1932 31.10607 439.00709 400.00000 0.00250
1933 31.11907 412.29899 372.48996 0.00268
1934 31.13207 390.63962 353.43997 0.00283
1935 31.14507 373.17027 342.25000 0.00292
1936 31.15807 359.16974 327.61002 0.00305
1937 31.17107 347.53294 327.61002 0.00305
1938 31.18407 338.05079 320.40997 0.00312
1939 31.19707 330.50787 309.76001 0.00323
1940 31.21007 324.98165 316.83997 0.00316
1941 31.22307 321.07008 320.40997 0.00312
1942 31.23607 318.74564 324.00000 0.00309
1943 31.24907 318.03432 316.83997 0.00316
1944 31.26207 319.09656 316.83997 0.00316
1945 31.27507 322.01382 338.56000 0.00295
1946 31.28807 327.41213 349.69003 0.00286
1947 31.30107 336.38987 364.81003 0.00274
1948 31.31407 349.48340 372.48996 0.00268
1949 31.32707 367.63099 392.03998 0.00255
1950 31.34007 392.82664 424.36002 0.00236
1951 31.35307 429.95353 462.25000 0.00216
1952 31.36607 478.65071 492.84003 0.00203
1953 31.37907 540.22699 556.96002 0.00180
1954 31.39207 615.90071 630.01001 0.00159
1955 31.40507 712.10485 723.60999 0.00138
1956 31.41807 818.95941 795.24005 0.00126
1957 31.43107 931.70096 888.03998 0.00113
1958 31.44407 1044.98823 1004.89008 0.00100
1959 31.45707 1143.06659 1122.25000 0.00089
1960 31.47007 1211.63474 1232.00989 0.00081
1961 31.48307 1247.10056 1260.25000 0.00079
1962 31.49607 1246.69593 1232.00989 0.00081
1963 31.50907 1204.71636 1197.15991 0.00084
1964 31.52207 1136.61179 1128.95984 0.00089
1965 31.53507 1057.32412 1056.25000 0.00095
1966 31.54807 972.28678 992.25000 0.00101
1967 31.56107 886.47767 912.04004 0.00110
1968 31.57407 804.07013 829.43994 0.00121
1969 31.58707 725.83274 745.28998 0.00134
1970 31.60007 652.66862 650.25000 0.00154
1971 31.61307 585.43750 576.00000 0.00174
1972 31.62607 528.27028 519.83997 0.00192
1973 31.63907 478.39836 462.25000 0.00216
1974 31.65207 435.66949 420.25000 0.00238
1975 31.66507 399.86494 388.09003 0.00258
1976 31.67807 372.42578 361.00000 0.00277
1977 31.69107 350.87683 345.96002 0.00289
1978 31.70407 333.89907 331.24002 0.00302
1979 31.71707 320.88748 313.29004 0.00319
1980 31.73007 311.66277 306.25000 0.00327
1981 31.74307 305.10826 295.84003 0.00338
1982 31.75607 300.21575 299.28998 0.00334
1983 31.76907 296.70088 302.75998 0.00330
1984 31.78207 294.33105 295.84003 0.00338
1985 31.79507 292.88951 285.60999 0.00350
1986 31.80807 292.01448 282.23996 0.00354
1987 31.82107 291.70388 285.60999 0.00350
1988 31.83407 291.91796 285.60999 0.00350
1989 31.84707 292.68425 292.41000 0.00342
1990 31.86007 293.91830 299.28998 0.00334
1991 31.87307 295.71544 302.75998 0.00330
1992 31.88607 298.34490 299.28998 0.00334
1993 31.89907 301.88178 306.25000 0.00327
1994 31.91207 306.50494 316.83997 0.00316
1995 31.92507 312.47224 334.88998 0.00299
1996 31.93807 320.88112 349.69003 0.00286
1997 31.95107 332.28934 361.00000 0.00277
1998 31.96407 347.28318 380.25000 0.00263
1999 31.97707 366.66125 396.00998 0.00253
2000 31.99007 392.48899 416.15997 0.00240
2001 32.00307 427.56637 462.25000 0.00216
2002 32.01607 471.57388 510.76001 0.00196
2003 32.02907 525.33758 571.20996 0.00175
2004 32.04207 590.18004 635.04004 0.00157
2005 32.05507 669.27429 718.23993 0.00139
2006 32.06807 758.29749 812.25000 0.00123
2007 32.08107 854.69178 912.04004 0.00110
2008 32.09407 957.33216 1017.60999 0.00098
2009 32.10707 1063.54658 1128.95984 0.00089
2010 32.12007 1164.62438 1232.00989 0.00081
2011 32.13307 1258.49838 1303.20984 0.00077
2012 32.14607 1343.65141 1361.61011 0.00073
2013 32.15907 1422.58328 1391.28992 0.00072
2014 32.17207 1483.13645 1436.41016 0.00070
2015 32.18507 1535.98703 1466.88989 0.00068
2016 32.19807 1580.38735 1497.69006 0.00067
2017 32.21107 1607.38397 1536.64001 0.00065
2018 32.22407 1605.86857 1560.25000 0.00064
2019 32.23707 1575.46854 1560.25000 0.00064
2020 32.25007 1515.14823 1497.69006 0.00067
2021 32.26307 1423.68611 1398.76013 0.00071
2022 32.27607 1311.04912 1288.81006 0.00078
2023 32.28907 1195.73085 1169.64001 0.00085
2024 32.30207 1081.08913 1082.41016 0.00092
2025 32.31507 970.92554 998.56000 0.00100
2026 32.32807 868.69159 906.01001 0.00110
2027 32.34107 776.40212 806.56000 0.00124
2028 32.35407 692.39064 707.56000 0.00141
2029 32.36707 616.89230 650.25000 0.00154
2030 32.38007 551.79847 556.96002 0.00180
2031 32.39307 497.30799 506.25000 0.00198
2032 32.40607 451.23246 453.68997 0.00220
2033 32.41907 412.75493 416.15997 0.00240
2034 32.43207 381.75956 380.25000 0.00263
2035 32.44507 358.39716 357.20999 0.00280
2036 32.45807 339.88356 342.25000 0.00292
2037 32.47107 325.22010 327.61002 0.00305
2038 32.48407 313.69128 316.83997 0.00316
2039 32.49707 305.19414 313.29004 0.00319
2040 32.51007 298.25424 275.56000 0.00363
2041 32.52307 292.32226 292.41000 0.00342
2042 32.53607 287.25350 275.56000 0.00363
2043 32.54907 283.00133 275.56000 0.00363
2044 32.56207 279.33207 272.25000 0.00367
2045 32.57507 276.08040 278.89001 0.00359
2046 32.58807 273.20927 265.68997 0.00376
2047 32.60107 270.68301 262.44003 0.00381
2048 32.61407 268.50028 262.44003 0.00381
2049 32.62707 266.60143 262.44003 0.00381
2050 32.64007 265.02538 252.80998 0.00396
2051 32.65307 263.74707 246.48999 0.00406
2052 32.66607 262.78042 246.48999 0.00406
2053 32.67907 262.09836 243.36002 0.00411
2054 32.69207 261.73077 256.00000 0.00391
2055 32.70507 261.59397 246.48999 0.00406
2056 32.71807 261.62483 249.64000 0.00401
2057 32.73107 261.76897 249.64000 0.00401
2058 32.74407 261.91831 246.48999 0.00406
2059 32.75707 261.90302 256.00000 0.00391
2060 32.77007 261.71669 256.00000 0.00391
2061 32.78307 261.35919 262.44003 0.00381
2062 32.79607 260.79402 249.64000 0.00401
2063 32.80907 260.10498 246.48999 0.00406
2064 32.82207 259.43715 256.00000 0.00391
2065 32.83507 258.82556 252.80998 0.00396
2066 32.84807 258.27759 249.64000 0.00401
2067 32.86107 257.82181 249.64000 0.00401
2068 32.87407 257.42424 246.48999 0.00406
2069 32.88707 257.05732 249.64000 0.00401
2070 32.90007 256.75626 249.64000 0.00401
2071 32.91307 256.63444 249.64000 0.00401
2072 32.92607 256.68941 249.64000 0.00401
2073 32.93907 256.96734 256.00000 0.00391
2074 32.95207 257.59257 252.80998 0.00396
2075 32.96507 258.68486 252.80998 0.00396
2076 32.97807 260.67737 259.21002 0.00386
2077 32.99107 263.66273 262.44003 0.00381
2078 33.00407 267.91052 272.25000 0.00367
2079 33.01707 273.71371 272.25000 0.00367
2080 33.03007 282.09406 285.60999 0.00350
2081 33.04307 293.50287 299.28998 0.00334
2082 33.05607 307.85773 313.29004 0.00319
2083 33.06907 325.24723 327.61002 0.00305
2084 33.08207 345.91346 345.96002 0.00289
2085 33.09507 369.39377 368.64001 0.00271
2086 33.10807 393.32999 408.04004 0.00245
2087 33.12107 416.17069 445.21002 0.00225
2088 33.13407 436.25109 475.23996 0.00210
2089 33.14707 448.80750 497.28998 0.00201
2090 33.16007 453.22296 501.75998 0.00199
2091 33.17307 450.41474 492.84003 0.00203
2092 33.18607 441.19745 484.00000 0.00207
2093 33.19907 426.77181 462.25000 0.00216
2094 33.21207 410.13735 441.00000 0.00227
2095 33.22507 393.05493 428.49002 0.00233
2096 33.23807 376.05419 408.04004 0.00245
2097 33.25107 359.50696 384.16000 0.00260
2098 33.26407 343.96817 361.00000 0.00277
2099 33.27707 329.43977 334.88998 0.00299
2100 33.29007 316.08044 313.29004 0.00319
2101 33.30307 304.03945 306.25000 0.00327
2102 33.31607 293.79344 282.23996 0.00354
2103 33.32907 285.28078 268.95999 0.00372
2104 33.34207 278.20680 268.95999 0.00372
2105 33.35507 272.51898 262.44003 0.00381
2106 33.36807 268.27944 252.80998 0.00396
2107 33.38107 265.55198 256.00000 0.00391
2108 33.39407 263.84207 259.21002 0.00386
2109 33.40707 263.08339 252.80998 0.00396
2110 33.42007 263.46930 256.00000 0.00391
2111 33.43307 265.09972 268.95999 0.00372
2112 33.44607 267.95593 272.25000 0.00367
2113 33.45907 272.20592 268.95999 0.00372
2114 33.47207 278.75836 285.60999 0.00350
2115 33.48507 288.41608 285.60999 0.00350
2116 33.49807 301.47154 292.41000 0.00342
2117 33.51107 318.47383 313.29004 0.00319
2118 33.52407 340.93061 342.25000 0.00292
2119 33.53707 370.38336 361.00000 0.00277
2120 33.55007 405.20513 376.35999 0.00266
2121 33.56307 444.75219 420.25000 0.00238
2122 33.57607 488.27756 457.95999 0.00218
2123 33.58907 532.43023 524.40997 0.00191
2124 33.60207 572.24536 585.64001 0.00171
2125 33.61507 604.67757 630.01001 0.00159
2126 33.62807 626.80561 645.15997 0.00155
2127 33.64107 630.03836 681.21002 0.00147
2128 33.65407 619.79281 681.21002 0.00147
2129 33.66707 599.70113 660.49005 0.00151
2130 33.68007 572.37272 630.01001 0.00159
2131 33.69307 540.94689 585.64001 0.00171
2132 33.70607 509.09300 538.24005 0.00186
2133 33.71907 477.69084 538.24005 0.00186
2134 33.73207 447.18456 501.75998 0.00199
2135 33.74507 418.13077 462.25000 0.00216
2136 33.75807 391.31966 420.25000 0.00238
2137 33.77107 366.68040 380.25000 0.00263
2138 33.78407 344.40320 361.00000 0.00277
2139 33.79707 324.79098 334.88998 0.00299
2140 33.81007 308.74968 309.76001 0.00323
2141 33.82307 295.17662 295.84003 0.00338
2142 33.83607 283.93588 278.89001 0.00359
2143 33.84907 274.84560 262.44003 0.00381
2144 33.86207 268.24421 259.21002 0.00386
2145 33.87507 263.10811 256.00000 0.00391
2146 33.88807 259.09944 249.64000 0.00401
2147 33.90107 255.99731 262.44003 0.00381
2148 33.91407 253.72601 256.00000 0.00391
2149 33.92707 251.90666 240.25000 0.00416
2150 33.94007 250.33403 243.36002 0.00411
2151 33.95307 248.99510 237.15999 0.00422
2152 33.96607 247.86305 246.48999 0.00406
2153 33.97907 246.89492 246.48999 0.00406
2154 33.99207 246.04002 237.15999 0.00422
2155 34.00507 245.29319 222.00999 0.00450
2156 34.01807 244.64894 231.03999 0.00433
2157 34.03107 244.11436 228.01001 0.00439
2158 34.04407 243.67099 228.01001 0.00439
2159 34.05707 243.32382 225.00000 0.00444
2160 34.07007 243.06761 219.04001 0.00457
2161 34.08307 242.91375 225.00000 0.00444
2162 34.09607 242.86239 222.00999 0.00450
2163 34.10907 242.93965 222.00999 0.00450
2164 34.12207 243.14985 228.01001 0.00439
2165 34.13507 243.50698 219.04001 0.00457
2166 34.14807 244.03195 222.00999 0.00450
2167 34.16107 244.77395 228.01001 0.00439
2168 34.17407 245.86117 228.01001 0.00439
2169 34.18707 247.36554 231.03999 0.00433
2170 34.20007 249.40337 246.48999 0.00406
2171 34.21307 252.11273 246.48999 0.00406
2172 34.22607 256.11623 243.36002 0.00411
2173 34.23907 261.71989 259.21002 0.00386
2174 34.25207 269.22538 262.44003 0.00381
2175 34.26507 279.01773 268.95999 0.00372
2176 34.27807 292.03951 282.23996 0.00354
2177 34.29107 309.07144 299.28998 0.00334
2178 34.30407 329.63155 320.40997 0.00312
2179 34.31707 353.36336 342.25000 0.00292
2180 34.33007 379.85843 364.81003 0.00274
2181 34.34307 407.58289 400.00000 0.00250
2182 34.35607 433.99170 432.63995 0.00231
2183 34.36907 456.79211 462.25000 0.00216
2184 34.38207 474.10348 484.00000 0.00207
2185 34.39507 482.35382 497.28998 0.00201
2186 34.40807 481.20668 501.75998 0.00199
2187 34.42107 473.00436 497.28998 0.00201
2188 34.43407 459.37519 470.89005 0.00212
2189 34.44707 441.99316 449.44003 0.00222
2190 34.46007 422.66346 441.00000 0.00227
2191 34.47307 402.87788 416.15997 0.00240
2192 34.48607 383.35157 392.03998 0.00255
2193 34.49907 364.35919 380.25000 0.00263
2194 34.51207 346.40847 368.64001 0.00271
2195 34.52507 329.74565 345.96002 0.00289
2196 34.53807 314.39367 320.40997 0.00312
2197 34.55107 300.47893 299.28998 0.00334
2198 34.56407 288.25960 278.89001 0.00359
2199 34.57707 278.00028 272.25000 0.00367
2200 34.59007 269.31617 265.68997 0.00376
2201 34.60307 262.04246 252.80998 0.00396
2202 34.61607 256.07843 246.48999 0.00406
2203 34.62907 251.52558 237.15999 0.00422
2204 34.64207 248.00262 228.01001 0.00439
2205 34.65507 245.21149 231.03999 0.00433
2206 34.66807 243.02403 225.00000 0.00444
2207 34.68107 241.36517 222.00999 0.00450
2208 34.69407 240.12624 219.04001 0.00457
2209 34.70707 239.14289 222.00999 0.00450
2210 34.72007 238.36242 225.00000 0.00444
2211 34.73307 237.75320 216.09000 0.00463
2212 34.74607 237.30666 213.16000 0.00469
2213 34.75907 236.97321 216.09000 0.00463
2214 34.77207 236.74572 210.25000 0.00476
2215 34.78507 236.62532 213.16000 0.00469
2216 34.79807 236.61254 219.04001 0.00457
2217 34.81107 236.71174 213.16000 0.00469
2218 34.82407 236.93813 210.25000 0.00476
2219 34.83707 237.29413 207.35999 0.00482
2220 34.85007 237.77613 210.25000 0.00476
2221 34.86307 238.38634 216.09000 0.00463
2222 34.87607 239.18542 219.04001 0.00457
2223 34.88907 240.14956 219.04001 0.00457
2224 34.90207 241.35482 228.01001 0.00439
2225 34.91507 242.82870 219.04001 0.00457
2226 34.92807 244.68294 216.09000 0.00463
2227 34.94107 246.91440 228.01001 0.00439
2228 34.95407 249.58837 225.00000 0.00444
2229 34.96707 252.60888 234.09001 0.00427
2230 34.98007 255.88441 243.36002 0.00411
2231 34.99307 259.26554 234.09001 0.00427
2232 35.00607 262.64522 249.64000 0.00401
2233 35.01907 265.86315 268.95999 0.00372
2234 35.03207 268.79504 272.25000 0.00367
2235 35.04507 271.57378 262.44003 0.00381
2236 35.05807 274.67545 282.23996 0.00354
2237 35.07107 278.09125 275.56000 0.00363
2238 35.08407 281.93348 289.00000 0.00346
2239 35.09707 286.24822 295.84003 0.00338
2240 35.11007 290.68084 295.84003 0.00338
2241 35.12307 294.59640 302.75998 0.00330
2242 35.13607 297.61598 320.40997 0.00312
2243 35.14907 299.40303 316.83997 0.00316
2244 35.16207 298.82306 302.75998 0.00330
2245 35.17507 296.73091 306.25000 0.00327
2246 35.18807 293.54810 306.25000 0.00327
2247 35.20107 289.65357 306.25000 0.00327
2248 35.21407 285.46124 299.28998 0.00334
2249 35.22707 281.39116 285.60999 0.00350
2250 35.24007 277.44841 285.60999 0.00350
2251 35.25307 273.63453 285.60999 0.00350
2252 35.26607 269.79022 265.68997 0.00376
2253 35.27907 265.95510 265.68997 0.00376
2254 35.29207 262.14411 272.25000 0.00367
2255 35.30507 258.40065 265.68997 0.00376
2256 35.31807 254.83822 246.48999 0.00406
2257 35.33107 251.65988 243.36002 0.00411
2258 35.34407 248.81166 237.15999 0.00422
2259 35.35707 246.30355 240.25000 0.00416
2260 35.37007 244.17251 246.48999 0.00406
2261 35.38307 242.42950 234.09001 0.00427
2262 35.39607 240.94687 237.15999 0.00422
2263 35.40907 239.70568 231.03999 0.00433
2264 35.42207 238.70400 231.03999 0.00433
2265 35.43507 237.94721 225.00000 0.00444
2266 35.44807 237.34201 225.00000 0.00444
2267 35.46107 236.87503 225.00000 0.00444
2268 35.47407 236.54208 225.00000 0.00444
2269 35.48707 236.34504 231.03999 0.00433
2270 35.50007 236.23551 228.01001 0.00439
2271 35.51307 236.20559 225.00000 0.00444
2272 35.52607 236.25112 237.15999 0.00422
2273 35.53907 236.37447 243.36002 0.00411
2274 35.55207 236.55438 237.15999 0.00422
2275 35.56507 236.79014 225.00000 0.00444
2276 35.57807 237.08038 228.01001 0.00439
2277 35.59107 237.43226 228.01001 0.00439
2278 35.60407 237.84244 225.00000 0.00444
2279 35.61707 238.32829 234.09001 0.00427
2280 35.63007 238.89461 237.15999 0.00422
2281 35.64307 239.56236 228.01001 0.00439
2282 35.65607 240.34814 225.00000 0.00444
2283 35.66907 241.34196 225.00000 0.00444
2284 35.68207 242.57151 225.00000 0.00444
2285 35.69507 244.09250 219.04001 0.00457
2286 35.70807 245.96869 219.04001 0.00457
2287 35.72107 248.40639 228.01001 0.00439
2288 35.73407 251.47424 228.01001 0.00439
2289 35.74707 255.15456 231.03999 0.00433
2290 35.76007 259.48589 237.15999 0.00422
2291 35.77307 264.54012 243.36002 0.00411
2292 35.78607 270.14105 252.80998 0.00396
2293 35.79907 275.91003 256.00000 0.00391
2294 35.81207 281.64393 265.68997 0.00376
2295 35.82507 286.95613 275.56000 0.00363
2296 35.83807 290.94563 282.23996 0.00354
2297 35.85107 293.70605 289.00000 0.00346
2298 35.86407 295.36859 299.28998 0.00334
2299 35.87707 296.01640 299.28998 0.00334
2300 35.89007 295.80627 292.41000 0.00342
2301 35.90307 295.63918 295.84003 0.00338
2302 35.91607 296.01204 295.84003 0.00338
2303 35.92907 297.30330 299.28998 0.00334
2304 35.94207 299.82148 313.29004 0.00319
2305 35.95507 303.90045 313.29004 0.00319
2306 35.96807 310.60332 324.00000 0.00309
2307 35.98107 321.24092 334.88998 0.00299
2308 35.99407 336.33529 334.88998 0.00299
2309 36.00707 356.83972 349.69003 0.00286
2310 36.02007 385.04799 372.48996 0.00268
2311 36.03307 424.04242 404.01001 0.00248
2312 36.04607 472.39031 441.00000 0.00227
2313 36.05907 530.17287 492.84003 0.00203
2314 36.07207 597.86160 561.69006 0.00178
2315 36.08507 674.04573 615.03998 0.00163
2316 36.09807 751.42696 686.44006 0.00146
2317 36.11107 825.83424 778.40997 0.00128
2318 36.12407 892.46690 858.48993 0.00116
2319 36.13707 934.99696 918.08997 0.00109
2320 36.15007 955.80693 942.49005 0.00106
2321 36.16307 956.04610 954.81000 0.00105
2322 36.17607 937.03712 912.04004 0.00110
2323 36.18907 900.77641 888.03998 0.00113
2324 36.20207 860.81176 852.64001 0.00117
2325 36.21507 821.65567 841.00000 0.00119
2326 36.22807 784.88990 789.61005 0.00127
2327 36.24107 752.42448 772.83997 0.00129
2328 36.25407 724.51178 712.89001 0.00140
2329 36.26707 701.13506 707.56000 0.00141
2330 36.28007 680.72940 691.68994 0.00145
2331 36.29307 663.27724 660.49005 0.00151
2332 36.30607 648.87072 640.08997 0.00156
2333 36.31907 635.04876 625.00000 0.00160
2334 36.33207 619.51314 635.04004 0.00157
2335 36.34507 606.08086 635.04004 0.00157
2336 36.35807 599.18534 615.03998 0.00163
2337 36.37107 599.01683 625.00000 0.00160
2338 36.38407 607.64752 630.01001 0.00159
2339 36.39707 627.77767 635.04004 0.00157
2340 36.41007 662.65651 665.63995 0.00150
2341 36.42307 710.24127 702.25000 0.00142
2342 36.43607 766.38441 756.25000 0.00132
2343 36.44907 828.29438 812.25000 0.00123
2344 36.46207 892.00478 900.00000 0.00111
2345 36.47507 945.53093 967.21002 0.00103
2346 36.48807 983.39578 998.56000 0.00100
2347 36.50107 1002.47137 1043.28992 0.00096
2348 36.51407 999.54268 1036.84009 0.00096
2349 36.52707 967.96262 1011.23993 0.00099
2350 36.54007 922.77949 973.44006 0.00103
2351 36.55307 870.17694 924.15997 0.00108
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5197 73.55107 239.46088 210.25000 0.00476
5198 73.56407 233.10796 210.25000 0.00476
5199 73.57707 227.63476 210.25000 0.00476
5200 73.59007 223.10172 201.64000 0.00496
5201 73.60307 219.18718 201.64000 0.00496
5202 73.61607 215.83284 201.64000 0.00496
5203 73.62907 212.98996 201.64000 0.00496
5204 73.64207 210.73049 193.20999 0.00518
5205 73.65507 208.82187 196.00000 0.00510
5206 73.66807 207.21821 196.00000 0.00510
5207 73.68107 205.89347 193.20999 0.00518
5208 73.69407 204.84943 196.00000 0.00510
5209 73.70707 204.00281 196.00000 0.00510
5210 73.72007 203.30973 196.00000 0.00510
5211 73.73307 202.75636 196.00000 0.00510
5212 73.74607 202.32678 196.00000 0.00510
5213 73.75907 202.00117 190.44000 0.00525
5214 73.77207 201.77056 184.96001 0.00541
5215 73.78507 201.62177 187.68999 0.00533
5216 73.79807 201.53263 193.20999 0.00518
5217 73.81107 201.52690 193.20999 0.00518
5218 73.82407 201.62493 184.96001 0.00541
5219 73.83707 201.80842 184.96001 0.00541
5220 73.85007 202.07128 190.44000 0.00525
5221 73.86307 202.44938 187.68999 0.00533
5222 73.87607 202.93059 198.81001 0.00503
5223 73.88907 203.46146 198.81001 0.00503
5224 73.90207 204.00140 193.20999 0.00518
5225 73.91507 204.52451 198.81001 0.00503
5226 73.92807 204.95075 198.81001 0.00503
5227 73.94107 205.21293 198.81001 0.00503
5228 73.95407 205.32501 198.81001 0.00503
5229 73.96707 205.32772 201.64000 0.00496
5230 73.98007 205.21548 210.25000 0.00476
5231 73.99307 205.00109 210.25000 0.00476
5232 74.00607 204.76502 204.49001 0.00489
5233 74.01907 204.53531 207.35999 0.00482
5234 74.03207 204.31083 207.35999 0.00482
5235 74.04507 204.12010 204.49001 0.00489
5236 74.05807 203.99492 201.64000 0.00496
5237 74.07107 203.93614 196.00000 0.00510
5238 74.08407 203.94132 198.81001 0.00503
5239 74.09707 204.02633 201.64000 0.00496
5240 74.11007 204.16944 204.49001 0.00489
5241 74.12307 204.34112 201.64000 0.00496
5242 74.13607 204.53473 196.00000 0.00510
5243 74.14907 204.75317 207.35999 0.00482
5244 74.16207 204.97779 207.35999 0.00482
5245 74.17507 205.26801 207.35999 0.00482
5246 74.18807 205.64358 204.49001 0.00489
5247 74.20107 206.11931 213.16000 0.00469
5248 74.21407 206.70601 207.35999 0.00482
5249 74.22707 207.48572 207.35999 0.00482
5250 74.24007 208.44962 196.00000 0.00510
5251 74.25307 209.54456 201.64000 0.00496
5252 74.26607 210.73893 207.35999 0.00482
5253 74.27907 212.00942 207.35999 0.00482
5254 74.29207 213.21905 207.35999 0.00482
5255 74.30507 214.28051 207.35999 0.00482
5256 74.31807 215.12399 210.25000 0.00476
5257 74.33107 215.64397 210.25000 0.00476
5258 74.34407 215.64746 201.64000 0.00496
5259 74.35707 215.31730 207.35999 0.00482
5260 74.37007 214.71440 216.09000 0.00463
5261 74.38307 213.90966 219.04001 0.00457
5262 74.39607 213.00796 216.09000 0.00463
5263 74.40907 212.21448 210.25000 0.00476
5264 74.42207 211.59288 213.16000 0.00469
5265 74.43507 211.20110 207.35999 0.00482
5266 74.44807 211.17216 210.25000 0.00476
5267 74.46107 211.47440 207.35999 0.00482
5268 74.47407 212.06060 219.04001 0.00457
5269 74.48707 212.89941 216.09000 0.00463
5270 74.50007 214.02257 216.09000 0.00463
5271 74.51307 215.26586 222.00999 0.00450
5272 74.52607 216.49187 210.25000 0.00476
5273 74.53907 217.67622 219.04001 0.00457
5274 74.55207 218.74812 216.09000 0.00463
5275 74.56507 219.55574 231.03999 0.00433
5276 74.57807 220.05399 225.00000 0.00444
5277 74.59107 220.25546 234.09001 0.00427
5278 74.60407 220.06949 219.04001 0.00457
5279 74.61707 219.36166 231.03999 0.00433
5280 74.63007 218.35116 228.01001 0.00439
5281 74.64307 217.09845 228.01001 0.00439
5282 74.65607 215.68288 219.04001 0.00457
5283 74.66907 214.21867 222.00999 0.00450
5284 74.68207 212.92793 222.00999 0.00450
5285 74.69507 211.83558 213.16000 0.00469
5286 74.70807 210.99306 210.25000 0.00476
5287 74.72107 210.48840 216.09000 0.00463
5288 74.73407 210.32411 219.04001 0.00457
5289 74.74707 210.41980 210.25000 0.00476
5290 74.76007 210.77324 219.04001 0.00457
5291 74.77307 211.37783 213.16000 0.00469
5292 74.78607 212.12737 222.00999 0.00450
5293 74.79907 212.90473 219.04001 0.00457
5294 74.81207 213.70319 216.09000 0.00463
5295 74.82507 214.49066 216.09000 0.00463
5296 74.83807 215.11172 216.09000 0.00463
5297 74.85107 215.59400 222.00999 0.00450
5298 74.86407 216.02274 216.09000 0.00463
5299 74.87707 216.40026 216.09000 0.00463
5300 74.89007 216.67638 216.09000 0.00463
5301 74.90307 216.91403 216.09000 0.00463
5302 74.91607 217.09173 216.09000 0.00463
5303 74.92907 217.06410 213.16000 0.00469
5304 74.94207 216.79647 219.04001 0.00457
5305 74.95507 216.35823 216.09000 0.00463
5306 74.96807 215.67066 213.16000 0.00469

#==============================================================================
# Reflections Data Block
#==============================================================================
_reflns_number_total             548
_reflns_limit_h_min              0 #All of these - see table below
_reflns_limit_h_max              11
_reflns_limit_k_min              0
_reflns_limit_k_max              17
_reflns_limit_l_min              0
_reflns_limit_l_max              5
_reflns_d_resolution_high        11.00025 #Look in column 4 below
_reflns_d_resolution_low         1.25971
_chemical_name_systematic        '[(AgBr)2(4-pica)]n'
_exptl_crystal_colour            powder
_chemical_melting_point          426
_chemical_properties_physical    Light-sensitive
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_AgBr2_3pica_final
_database_code_depnum_ccdc_archive 'CCDC 2298749'
loop_
_audit_author_name
_audit_author_address
'Caterina Zuffa'
;University of Bologna
Italy
;
_audit_update_record             
;
2023-10-02 deposited with the CCDC.	2024-01-03 downloaded from the CCDC.
;
_audit_creation_date             2022-07-28
_audit_creation_method           
;
Olex2 1.5
(compiled 2022.04.07 svn.rca3783a0 for OlexSys, GUI svn.r6498)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        '[(AgBr)2(3-pica)]n'
_chemical_formula_moiety         'C6 H8 Ag2 Br2 N2'
_chemical_formula_sum            'C6 H8 Ag2 Br2 N2'
_chemical_formula_weight         483.68
_chemical_melting_point          379
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Br Br -0.2901 2.4595 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           15
_space_group_name_H-M_alt        'C 1 2/c 1'
_space_group_name_Hall           '-C 2yc'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'

_cell_length_a                   24.605(3)
_cell_length_b                   6.2851(5)
_cell_length_c                   14.3050(12)
_cell_angle_alpha                90
_cell_angle_beta                 110.938(9)
_cell_angle_gamma                90
_cell_volume                     2066.2(3)
_cell_formula_units_Z            8
_cell_measurement_reflns_used    844
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      22.5590
_cell_measurement_theta_min      4.0300
_shelx_estimated_absorpt_T_max   ?
_shelx_estimated_absorpt_T_min   ?
_exptl_absorpt_coefficient_mu    11.474
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.16766
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
CrysAlisPro 1.171.38.46 (Rigaku Oxford Diffraction, 2015)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    3.110
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       plate
_exptl_crystal_F_000             1776
_exptl_crystal_size_max          0.167
_exptl_crystal_size_mid          0.143
_exptl_crystal_size_min          0.076
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0698
_diffrn_reflns_av_unetI/netI     0.1454
_diffrn_reflns_Laue_measured_fraction_full 0.998
_diffrn_reflns_Laue_measured_fraction_max 0.857
_diffrn_reflns_limit_h_max       33
_diffrn_reflns_limit_h_min       -32
_diffrn_reflns_limit_k_max       4
_diffrn_reflns_limit_k_min       -8
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_limit_l_min       -18
_diffrn_reflns_number            4378
_diffrn_reflns_point_group_measured_fraction_full 0.998
_diffrn_reflns_point_group_measured_fraction_max 0.857
_diffrn_reflns_theta_full        25.000
_diffrn_reflns_theta_max         28.984
_diffrn_reflns_theta_min         3.360
_diffrn_ambient_temperature      293(2)
_diffrn_detector                 'CCD plate'
_diffrn_detector_area_resol_mean 16.1340
_diffrn_detector_type            Sapphire3
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.857
_diffrn_measurement_details      
;
List of Runs (angles in degrees, time in seconds):

  # Type    Start    End  Width  tₑₓₚ   ω     θ     κ     φ   Frames
#--------------------------------------------------------------------------
  1  ω    -78.00 -47.00   1.00  125.00    --  -16.36 -77.00 -30.00   31
  2  ω    -24.00  24.00   1.00  125.00    --  -16.36 -99.00-120.00   48
  3  ω    -84.00  -4.00   1.00  125.00    --  -16.36 -57.00  90.00   80
  4  ω     38.00  92.00   1.00  125.00    --   17.61-178.00 -60.00   54
;
_diffrn_measurement_device       'four-circle diffractometer'
_diffrn_measurement_device_type  'Xcalibur, Sapphire3'
_diffrn_measurement_method       'ω scans'
_diffrn_orient_matrix_type       
'CrysAlisPro convention (1999,Acta A55,543-557)'
_diffrn_orient_matrix_UB_11      -0.0294315000
_diffrn_orient_matrix_UB_12      0.0299935000
_diffrn_orient_matrix_UB_13      0.0190226000
_diffrn_orient_matrix_UB_21      0.0376815000
_diffrn_orient_matrix_UB_22      0.0646579000
_diffrn_orient_matrix_UB_23      0.0159743000
_diffrn_orient_matrix_UB_31      -0.0177319000
_diffrn_orient_matrix_UB_32      0.0875812000
_diffrn_orient_matrix_UB_33      -0.0182871000
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   'fine-focus sealed X-ray tube'
_diffrn_source_type              'Enhance (Mo) X-ray Source'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                1170
_reflns_number_total             2359
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'CrysAlisPro 1.171.38.46 (Rigaku OD, 2015)'
_computing_data_collection       'CrysAlisPro 1.171.38.46 (Rigaku OD, 2015)'
_computing_data_reduction        'CrysAlisPro 1.171.38.46 (Rigaku OD, 2015)'
_computing_molecular_graphics    'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2018/3 (Sheldrick, 2015)'
_computing_structure_solution    'SHELXT 2014/5 (Sheldrick, 2014)'
_refine_diff_density_max         0.951
_refine_diff_density_min         -0.827
_refine_diff_density_rms         0.206
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.991
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     110
_refine_ls_number_reflns         2359
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.1742
_refine_ls_R_factor_gt           0.0726
_refine_ls_restrained_S_all      0.991
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0259P)²] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0977
_refine_ls_wR_factor_ref         0.1277
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups, All C(H,H) groups, All N(H,H) groups
2.a Secondary CH2 refined with riding coordinates:
 N2(H2A,H2B), C7(H7A,H7B)
2.b Aromatic/amide H refined with riding coordinates:
 C5(H5), C4(H4), C6(H6), C2(H2)
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag3 Ag -0.500000 0.0739(3) -0.250000 0.0583(5) Uani 1 2 d S T P . .
Ag2 Ag -0.500000 0.5626(3) -0.250000 0.0679(6) Uani 1 2 d S T P . .
Ag1 Ag -0.62051(6) 0.9848(2) -0.21264(9) 0.0665(4) Uani 1 1 d . . . . .
Br1 Br -0.58744(6) 0.8171(2) -0.36493(10) 0.0469(4) Uani 1 1 d . . . . .
Br2 Br -0.53620(6) 0.3179(2) -0.12788(10) 0.0490(4) Uani 1 1 d . . . . .
N2 N -0.5989(4) 0.7995(18) -0.0743(7) 0.046(3) Uani 1 1 d . . . . .
H2A H -0.567780 0.721583 -0.069170 0.055 Uiso 1 1 calc R U . . .
H2B H -0.587845 0.891934 -0.023841 0.055 Uiso 1 1 calc R U . . .
N1 N -0.8030(5) 0.6943(19) -0.1928(7) 0.043(3) Uani 1 1 d . . . . .
C3 C -0.7014(6) 0.746(2) -0.0972(9) 0.034(3) Uani 1 1 d . . . . .
C5 C -0.7716(6) 1.016(2) -0.1092(9) 0.045(4) Uani 1 1 d . . . . .
H5 H -0.781170 1.151508 -0.093773 0.054 Uiso 1 1 calc R U . . .
C4 C -0.7147(6) 0.946(2) -0.0730(9) 0.048(4) Uani 1 1 d . . . . .
H4 H -0.685359 1.034289 -0.032318 0.058 Uiso 1 1 calc R U . . .
C6 C -0.8130(6) 0.884(2) -0.1671(9) 0.037(3) Uani 1 1 d . . . . .
H6 H -0.851317 0.932363 -0.190258 0.045 Uiso 1 1 calc R U . . .
C2 C -0.7464(6) 0.628(2) -0.1570(10) 0.044(4) Uani 1 1 d . . . . .
H2 H -0.738300 0.492187 -0.174859 0.052 Uiso 1 1 calc R U . . .
C7 C -0.6406(6) 0.658(2) -0.0567(10) 0.056(4) Uani 1 1 d . . . . .
H7A H -0.629573 0.634315 0.014705 0.067 Uiso 1 1 calc R U . . .
H7B H -0.639787 0.521832 -0.088052 0.067 Uiso 1 1 calc R U . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag3 Ag2 3.071(2) . ?
Ag3 Ag2 3.214(2) 1_545 ?
Ag3 Ag1 3.2443(12) 2_444 ?
Ag3 Ag1 3.2443(12) 1_545 ?
Ag3 Br1 2.7221(17) 1_545 ?
Ag3 Br1 2.7221(17) 2_444 ?
Ag3 Br2 2.7033(16) 2_454 ?
Ag3 Br2 2.7033(16) . ?
Ag2 Br1 2.7134(18) . ?
Ag2 Br1 2.7134(18) 2_454 ?
Ag2 Br2 2.7060(16) . ?
Ag2 Br2 2.7060(16) 2_454 ?
Ag1 Br1 2.7904(17) . ?
Ag1 Br2 2.891(2) 1_565 ?
Ag1 N2 2.192(10) . ?
Ag1 N1 2.300(10) 4_354 ?
N2 H2A 0.8900 . ?
N2 H2B 0.8900 . ?
N2 C7 1.446(14) . ?
N1 C6 1.300(15) . ?
N1 C2 1.366(15) . ?
C3 C4 1.376(17) . ?
C3 C2 1.355(17) . ?
C3 C7 1.502(17) . ?
C5 H5 0.9300 . ?
C5 C4 1.381(16) . ?
C5 C6 1.343(16) . ?
C4 H4 0.9300 . ?
C6 H6 0.9300 . ?
C2 H2 0.9300 . ?
C7 H7A 0.9700 . ?
C7 H7B 0.9700 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Ag2 Ag3 Ag2 180.0 . 1_545 ?
Ag2 Ag3 Ag1 80.06(4) 1_545 1_545 ?
Ag2 Ag3 Ag1 99.94(4) . 2_444 ?
Ag2 Ag3 Ag1 80.06(4) 1_545 2_444 ?
Ag2 Ag3 Ag1 99.94(4) . 1_545 ?
Ag1 Ag3 Ag1 160.11(7) 1_545 2_444 ?
Br1 Ag3 Ag2 126.37(4) 1_545 . ?
Br1 Ag3 Ag2 53.63(4) 2_444 1_545 ?
Br1 Ag3 Ag2 126.37(4) 2_444 . ?
Br1 Ag3 Ag2 53.63(4) 1_545 1_545 ?
Br1 Ag3 Ag1 54.93(4) 1_545 1_545 ?
Br1 Ag3 Ag1 54.93(4) 2_444 2_444 ?
Br1 Ag3 Ag1 111.70(5) 2_444 1_545 ?
Br1 Ag3 Ag1 111.70(5) 1_545 2_444 ?
Br1 Ag3 Br1 107.25(8) 1_545 2_444 ?
Br2 Ag3 Ag2 55.45(4) . . ?
Br2 Ag3 Ag2 124.55(4) 2_454 1_545 ?
Br2 Ag3 Ag2 124.55(4) . 1_545 ?
Br2 Ag3 Ag2 55.45(4) 2_454 . ?
Br2 Ag3 Ag1 57.31(4) 2_454 2_444 ?
Br2 Ag3 Ag1 137.39(5) 2_454 1_545 ?
Br2 Ag3 Ag1 57.31(4) . 1_545 ?
Br2 Ag3 Ag1 137.39(5) . 2_444 ?
Br2 Ag3 Br1 108.54(4) 2_454 1_545 ?
Br2 Ag3 Br1 110.78(4) . 1_545 ?
Br2 Ag3 Br1 110.78(4) 2_454 2_444 ?
Br2 Ag3 Br1 108.54(4) . 2_444 ?
Br2 Ag3 Br2 110.89(8) 2_454 . ?
Ag3 Ag2 Ag3 180.0 . 1_565 ?
Br1 Ag2 Ag3 53.88(4) 2_454 1_565 ?
Br1 Ag2 Ag3 53.88(4) . 1_565 ?
Br1 Ag2 Ag3 126.12(4) . . ?
Br1 Ag2 Ag3 126.12(4) 2_454 . ?
Br1 Ag2 Br1 107.75(9) . 2_454 ?
Br2 Ag2 Ag3 124.64(4) . 1_565 ?
Br2 Ag2 Ag3 124.64(4) 2_454 1_565 ?
Br2 Ag2 Ag3 55.36(4) . . ?
Br2 Ag2 Ag3 55.36(4) 2_454 . ?
Br2 Ag2 Br1 108.45(4) . 2_454 ?
Br2 Ag2 Br1 110.70(4) 2_454 2_454 ?
Br2 Ag2 Br1 108.46(4) 2_454 . ?
Br2 Ag2 Br1 110.71(4) . . ?
Br2 Ag2 Br2 110.73(8) 2_454 . ?
Br1 Ag1 Ag3 52.98(4) . 1_565 ?
Br1 Ag1 Br2 103.60(5) . 1_565 ?
Br2 Ag1 Ag3 51.90(4) 1_565 1_565 ?
N2 Ag1 Ag3 107.4(2) . 1_565 ?
N2 Ag1 Br1 117.4(3) . . ?
N2 Ag1 Br2 95.7(3) . 1_565 ?
N2 Ag1 N1 135.9(3) . 4_354 ?
N1 Ag1 Ag3 114.1(3) 4_354 1_565 ?
N1 Ag1 Br1 99.4(2) 4_354 . ?
N1 Ag1 Br2 98.4(3) 4_354 1_565 ?
Ag3 Br1 Ag1 72.09(4) 1_565 . ?
Ag2 Br1 Ag3 72.50(5) . 1_565 ?
Ag2 Br1 Ag1 97.99(5) . . ?
Ag3 Br2 Ag2 69.19(5) . . ?
Ag3 Br2 Ag1 70.80(4) . 1_545 ?
Ag2 Br2 Ag1 119.55(6) . 1_545 ?
Ag1 N2 H2A 106.9 . . ?
Ag1 N2 H2B 106.9 . . ?
H2A N2 H2B 106.7 . . ?
C7 N2 Ag1 121.7(8) . . ?
C7 N2 H2A 106.9 . . ?
C7 N2 H2B 106.9 . . ?
C6 N1 Ag1 119.6(10) . 4_344 ?
C6 N1 C2 116.6(12) . . ?
C2 N1 Ag1 123.7(10) . 4_344 ?
C4 C3 C7 122.2(13) . . ?
C2 C3 C4 116.5(13) . . ?
C2 C3 C7 121.3(13) . . ?
C4 C5 H5 120.7 . . ?
C6 C5 H5 120.7 . . ?
C6 C5 C4 118.7(14) . . ?
C3 C4 C5 119.8(14) . . ?
C3 C4 H4 120.1 . . ?
C5 C4 H4 120.1 . . ?
N1 C6 C5 124.2(13) . . ?
N1 C6 H6 117.9 . . ?
C5 C6 H6 117.9 . . ?
N1 C2 H2 117.9 . . ?
C3 C2 N1 124.2(13) . . ?
C3 C2 H2 117.9 . . ?
N2 C7 C3 112.2(11) . . ?
N2 C7 H7A 109.2 . . ?
N2 C7 H7B 109.2 . . ?
C3 C7 H7A 109.2 . . ?
C3 C7 H7B 109.2 . . ?
H7A C7 H7B 107.9 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Ag1 N2 C7 C3 -37.1(14) . . . . ?
Ag1 N1 C6 C5 177.6(9) 4_344 . . . ?
Ag1 N1 C2 C3 -176.6(9) 4_344 . . . ?
C4 C3 C2 N1 -0.7(18) . . . . ?
C4 C3 C7 N2 -52.9(15) . . . . ?
C4 C5 C6 N1 -0.9(19) . . . . ?
C6 N1 C2 C3 0.3(17) . . . . ?
C6 C5 C4 C3 0.5(18) . . . . ?
C2 N1 C6 C5 0.5(18) . . . . ?
C2 C3 C4 C5 0.3(17) . . . . ?
C2 C3 C7 N2 129.4(12) . . . . ?
C7 C3 C4 C5 -177.5(11) . . . . ?
C7 C3 C2 N1 177.1(10) . . . . ?

_olex2_submission_special_instructions 'No special instructions were received'
_oxdiff_exptl_absorpt_empirical_details 
;
Empirical correction (ABSPACK) includes:
- Absorption correction using spherical harmonics
- Frame scaling
;
_oxdiff_exptl_absorpt_empirical_full_max 3.229
_oxdiff_exptl_absorpt_empirical_full_min 0.360
_chemical_compound_source        'solvothermal synthesis'
_chemical_properties_physical    Light-sensitive
_exptl_crystal_preparation       Luminescent
