# Electronic Supplementary Material (ESI) for Dalton Transactions.
# This journal is © The Royal Society of Chemistry 2023

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_Cs3AlF6_HT
_database_code_depnum_ccdc_archive 'CCDC 2193505'
loop_
_audit_author_name
_audit_author_address
'Gregory Morrison'
;University of South Carolina
United States of America
;
_audit_update_record             
;
2022-07-28 deposited with the CCDC.	2023-05-19 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2018/3
_shelx_SHELXL_version_number     2018/3
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'Al Cs3 F6'
_chemical_formula_weight         539.71

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
F F -0.0002 0.0031 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Al Al 0.0115 0.0165 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cs Cs -1.7794 0.8050 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      cubic
_space_group_IT_number           225
_space_group_name_H-M_alt        'F m -3 m'
_space_group_name_Hall           '-F 4 2 3'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, z'
'-x, y, -z'
'x, -y, -z'
'z, x, y'
'z, -x, -y'
'-z, -x, y'
'-z, x, -y'
'y, z, x'
'-y, z, -x'
'y, -z, -x'
'-y, -z, x'
'y, x, -z'
'-y, -x, -z'
'y, -x, z'
'-y, x, z'
'x, z, -y'
'-x, z, y'
'-x, -z, -y'
'x, -z, y'
'z, y, -x'
'z, -y, x'
'-z, y, x'
'-z, -y, -x'
'x, y+1/2, z+1/2'
'-x, -y+1/2, z+1/2'
'-x, y+1/2, -z+1/2'
'x, -y+1/2, -z+1/2'
'z, x+1/2, y+1/2'
'z, -x+1/2, -y+1/2'
'-z, -x+1/2, y+1/2'
'-z, x+1/2, -y+1/2'
'y, z+1/2, x+1/2'
'-y, z+1/2, -x+1/2'
'y, -z+1/2, -x+1/2'
'-y, -z+1/2, x+1/2'
'y, x+1/2, -z+1/2'
'-y, -x+1/2, -z+1/2'
'y, -x+1/2, z+1/2'
'-y, x+1/2, z+1/2'
'x, z+1/2, -y+1/2'
'-x, z+1/2, y+1/2'
'-x, -z+1/2, -y+1/2'
'x, -z+1/2, y+1/2'
'z, y+1/2, -x+1/2'
'z, -y+1/2, x+1/2'
'-z, y+1/2, x+1/2'
'-z, -y+1/2, -x+1/2'
'x+1/2, y, z+1/2'
'-x+1/2, -y, z+1/2'
'-x+1/2, y, -z+1/2'
'x+1/2, -y, -z+1/2'
'z+1/2, x, y+1/2'
'z+1/2, -x, -y+1/2'
'-z+1/2, -x, y+1/2'
'-z+1/2, x, -y+1/2'
'y+1/2, z, x+1/2'
'-y+1/2, z, -x+1/2'
'y+1/2, -z, -x+1/2'
'-y+1/2, -z, x+1/2'
'y+1/2, x, -z+1/2'
'-y+1/2, -x, -z+1/2'
'y+1/2, -x, z+1/2'
'-y+1/2, x, z+1/2'
'x+1/2, z, -y+1/2'
'-x+1/2, z, y+1/2'
'-x+1/2, -z, -y+1/2'
'x+1/2, -z, y+1/2'
'z+1/2, y, -x+1/2'
'z+1/2, -y, x+1/2'
'-z+1/2, y, x+1/2'
'-z+1/2, -y, -x+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, -y+1/2, z'
'-x+1/2, y+1/2, -z'
'x+1/2, -y+1/2, -z'
'z+1/2, x+1/2, y'
'z+1/2, -x+1/2, -y'
'-z+1/2, -x+1/2, y'
'-z+1/2, x+1/2, -y'
'y+1/2, z+1/2, x'
'-y+1/2, z+1/2, -x'
'y+1/2, -z+1/2, -x'
'-y+1/2, -z+1/2, x'
'y+1/2, x+1/2, -z'
'-y+1/2, -x+1/2, -z'
'y+1/2, -x+1/2, z'
'-y+1/2, x+1/2, z'
'x+1/2, z+1/2, -y'
'-x+1/2, z+1/2, y'
'-x+1/2, -z+1/2, -y'
'x+1/2, -z+1/2, y'
'z+1/2, y+1/2, -x'
'z+1/2, -y+1/2, x'
'-z+1/2, y+1/2, x'
'-z+1/2, -y+1/2, -x'
'-x, -y, -z'
'x, y, -z'
'x, -y, z'
'-x, y, z'
'-z, -x, -y'
'-z, x, y'
'z, x, -y'
'z, -x, y'
'-y, -z, -x'
'y, -z, x'
'-y, z, x'
'y, z, -x'
'-y, -x, z'
'y, x, z'
'-y, x, -z'
'y, -x, -z'
'-x, -z, y'
'x, -z, -y'
'x, z, y'
'-x, z, -y'
'-z, -y, x'
'-z, y, -x'
'z, -y, -x'
'z, y, x'
'-x, -y+1/2, -z+1/2'
'x, y+1/2, -z+1/2'
'x, -y+1/2, z+1/2'
'-x, y+1/2, z+1/2'
'-z, -x+1/2, -y+1/2'
'-z, x+1/2, y+1/2'
'z, x+1/2, -y+1/2'
'z, -x+1/2, y+1/2'
'-y, -z+1/2, -x+1/2'
'y, -z+1/2, x+1/2'
'-y, z+1/2, x+1/2'
'y, z+1/2, -x+1/2'
'-y, -x+1/2, z+1/2'
'y, x+1/2, z+1/2'
'-y, x+1/2, -z+1/2'
'y, -x+1/2, -z+1/2'
'-x, -z+1/2, y+1/2'
'x, -z+1/2, -y+1/2'
'x, z+1/2, y+1/2'
'-x, z+1/2, -y+1/2'
'-z, -y+1/2, x+1/2'
'-z, y+1/2, -x+1/2'
'z, -y+1/2, -x+1/2'
'z, y+1/2, x+1/2'
'-x+1/2, -y, -z+1/2'
'x+1/2, y, -z+1/2'
'x+1/2, -y, z+1/2'
'-x+1/2, y, z+1/2'
'-z+1/2, -x, -y+1/2'
'-z+1/2, x, y+1/2'
'z+1/2, x, -y+1/2'
'z+1/2, -x, y+1/2'
'-y+1/2, -z, -x+1/2'
'y+1/2, -z, x+1/2'
'-y+1/2, z, x+1/2'
'y+1/2, z, -x+1/2'
'-y+1/2, -x, z+1/2'
'y+1/2, x, z+1/2'
'-y+1/2, x, -z+1/2'
'y+1/2, -x, -z+1/2'
'-x+1/2, -z, y+1/2'
'x+1/2, -z, -y+1/2'
'x+1/2, z, y+1/2'
'-x+1/2, z, -y+1/2'
'-z+1/2, -y, x+1/2'
'-z+1/2, y, -x+1/2'
'z+1/2, -y, -x+1/2'
'z+1/2, y, x+1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, y+1/2, -z'
'x+1/2, -y+1/2, z'
'-x+1/2, y+1/2, z'
'-z+1/2, -x+1/2, -y'
'-z+1/2, x+1/2, y'
'z+1/2, x+1/2, -y'
'z+1/2, -x+1/2, y'
'-y+1/2, -z+1/2, -x'
'y+1/2, -z+1/2, x'
'-y+1/2, z+1/2, x'
'y+1/2, z+1/2, -x'
'-y+1/2, -x+1/2, z'
'y+1/2, x+1/2, z'
'-y+1/2, x+1/2, -z'
'y+1/2, -x+1/2, -z'
'-x+1/2, -z+1/2, y'
'x+1/2, -z+1/2, -y'
'x+1/2, z+1/2, y'
'-x+1/2, z+1/2, -y'
'-z+1/2, -y+1/2, x'
'-z+1/2, y+1/2, -x'
'z+1/2, -y+1/2, -x'
'z+1/2, y+1/2, x'

_cell_length_a                   9.3433(3)
_cell_length_b                   9.3433(3)
_cell_length_c                   9.3433(3)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_volume                     815.64(8)
_cell_formula_units_Z            4
_cell_measurement_temperature    623(2)
_cell_measurement_reflns_used    2231
_cell_measurement_theta_min      2.5352
_cell_measurement_theta_max      16.2454

_exptl_crystal_description       polyhedron
_exptl_crystal_colour            colorless
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    4.395
_exptl_crystal_F_000             928
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          0.02
_exptl_crystal_size_mid          0.02
_exptl_crystal_size_min          0.01
_exptl_absorpt_coefficient_mu    3.106
_shelx_estimated_absorpt_T_min   ?
_shelx_estimated_absorpt_T_max   ?
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_correction_T_min  0.8304
_exptl_absorpt_correction_T_max  0.9531
_exptl_absorpt_process_details   
'SADABS 2016/2: Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D. (2015). J. Appl. Cryst.'
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      623(2)
_diffrn_radiation_wavelength     0.41328
_diffrn_radiation_type           synchrotron
_diffrn_source                   synchrotron
_diffrn_measurement_device_type  'Huber 3-circle with Pilatus3X 1M'
_diffrn_measurement_method       ?
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            11945
_diffrn_reflns_av_unetI/netI     0.0146
_diffrn_reflns_av_R_equivalents  0.1004
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_l_min       -15
_diffrn_reflns_limit_l_max       15
_diffrn_reflns_theta_min         2.195
_diffrn_reflns_theta_max         19.862
_diffrn_reflns_theta_full        14.357
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measured_fraction_theta_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 1.000
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 1.000
_diffrn_reflns_point_group_measured_fraction_full 1.000
_reflns_number_total             131
_reflns_number_gt                88
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       'SAINT v8.40B (Bruker, 2013)'
_computing_cell_refinement       'Bruker APEX3 v2019.11-0 (Bruker, 2019)'
_computing_data_reduction        ?
_computing_structure_solution    'SHELXT 2018/2 (Sheldrick, 2018)'
_computing_structure_refinement  'SHELXL-2018/3 (Sheldrick, 2018)'
_computing_molecular_graphics    ?
_computing_publication_material  ?
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0508P)²+28.6465P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   .
_refine_ls_hydrogen_treatment    undef
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_number_reflns         131
_refine_ls_number_parameters     7
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0679
_refine_ls_R_factor_gt           0.0527
_refine_ls_wR_factor_ref         0.1579
_refine_ls_wR_factor_gt          0.1489
_refine_ls_goodness_of_fit_ref   1.148
_refine_ls_restrained_S_all      1.148
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Cs01 Cs 0.250000 0.250000 0.250000 0.0667(9) Uani 1 24 d S T P . .
Cs02 Cs 0.500000 0.000000 0.500000 0.0662(10) Uani 1 48 d S T P . .
Al03 Al 0.500000 0.500000 0.500000 0.0271(17) Uani 1 48 d S T P . .
F004 F 0.500000 0.3076(12) 0.500000 0.086(4) Uani 1 8 d S T P . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Cs01 F004 3.3470(18) . ?
Cs01 F004 3.3470(18) 5 ?
Cs01 F004 3.3470(18) 9 ?
Cs01 F004 3.3470(18) 77_445 ?
Cs01 F004 3.3470(18) 33_544 ?
Cs01 F004 3.3470(18) 49_454 ?
Cs01 F004 3.3470(18) 177_556 ?
Cs01 F004 3.3470(18) 153_565 ?
Cs01 F004 3.3470(18) 149_565 ?
Cs01 F004 3.3470(18) 125_655 ?
Cs01 F004 3.3470(18) 169_556 ?
Cs01 F004 3.3470(18) 121_655 ?
Cs02 F004 2.874(11) . ?
Cs02 F004 2.874(11) 177_556 ?
Cs02 F004 2.874(11) 81_545 ?
Cs02 F004 2.874(11) 125_655 ?
Cs02 F004 2.874(11) 29_545 ?
Cs02 F004 2.874(11) 97_656 ?
Al03 F004 1.797(11) 105_666 ?
Al03 F004 1.797(11) 9 ?
Al03 F004 1.797(11) 101_666 ?
Al03 F004 1.797(11) 5 ?
Al03 F004 1.797(11) 97_666 ?
Al03 F004 1.797(11) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
F004 Cs01 F004 44.6(3) . 5 ?
F004 Cs01 F004 44.6(3) . 9 ?
F004 Cs01 F004 44.6(3) 5 9 ?
F004 Cs01 F004 119.15(3) . 77_445 ?
F004 Cs01 F004 161.5(4) 5 77_445 ?
F004 Cs01 F004 119.15(3) 9 77_445 ?
F004 Cs01 F004 119.15(3) . 33_544 ?
F004 Cs01 F004 119.15(3) 5 33_544 ?
F004 Cs01 F004 161.5(4) 9 33_544 ?
F004 Cs01 F004 74.8(3) 77_445 33_544 ?
F004 Cs01 F004 161.5(4) . 49_454 ?
F004 Cs01 F004 119.15(3) 5 49_454 ?
F004 Cs01 F004 119.15(3) 9 49_454 ?
F004 Cs01 F004 74.8(3) 77_445 49_454 ?
F004 Cs01 F004 74.8(3) 33_544 49_454 ?
F004 Cs01 F004 74.8(3) . 177_556 ?
F004 Cs01 F004 119.15(3) 5 177_556 ?
F004 Cs01 F004 91.48(6) 9 177_556 ?
F004 Cs01 F004 44.6(3) 77_445 177_556 ?
F004 Cs01 F004 91.48(6) 33_544 177_556 ?
F004 Cs01 F004 119.15(3) 49_454 177_556 ?
F004 Cs01 F004 119.15(3) . 153_565 ?
F004 Cs01 F004 74.8(3) 5 153_565 ?
F004 Cs01 F004 91.48(6) 9 153_565 ?
F004 Cs01 F004 119.15(3) 77_445 153_565 ?
F004 Cs01 F004 91.48(6) 33_544 153_565 ?
F004 Cs01 F004 44.6(3) 49_454 153_565 ?
F004 Cs01 F004 161.5(4) 177_556 153_565 ?
F004 Cs01 F004 119.15(3) . 149_565 ?
F004 Cs01 F004 91.48(6) 5 149_565 ?
F004 Cs01 F004 74.8(3) 9 149_565 ?
F004 Cs01 F004 91.48(6) 77_445 149_565 ?
F004 Cs01 F004 119.15(3) 33_544 149_565 ?
F004 Cs01 F004 44.6(3) 49_454 149_565 ?
F004 Cs01 F004 119.15(3) 177_556 149_565 ?
F004 Cs01 F004 44.6(3) 153_565 149_565 ?
F004 Cs01 F004 74.8(3) . 125_655 ?
F004 Cs01 F004 91.48(6) 5 125_655 ?
F004 Cs01 F004 119.15(3) 9 125_655 ?
F004 Cs01 F004 91.48(6) 77_445 125_655 ?
F004 Cs01 F004 44.6(3) 33_544 125_655 ?
F004 Cs01 F004 119.15(3) 49_454 125_655 ?
F004 Cs01 F004 74.8(3) 177_556 125_655 ?
F004 Cs01 F004 119.15(3) 153_565 125_655 ?
F004 Cs01 F004 161.5(4) 149_565 125_655 ?
F004 Cs01 F004 91.48(6) . 169_556 ?
F004 Cs01 F004 119.15(3) 5 169_556 ?
F004 Cs01 F004 74.8(3) 9 169_556 ?
F004 Cs01 F004 44.6(3) 77_445 169_556 ?
F004 Cs01 F004 119.15(3) 33_544 169_556 ?
F004 Cs01 F004 91.48(6) 49_454 169_556 ?
F004 Cs01 F004 44.6(3) 177_556 169_556 ?
F004 Cs01 F004 119.15(3) 153_565 169_556 ?
F004 Cs01 F004 74.8(3) 149_565 169_556 ?
F004 Cs01 F004 119.15(3) 125_655 169_556 ?
F004 Cs01 F004 91.48(6) . 121_655 ?
F004 Cs01 F004 74.8(3) 5 121_655 ?
F004 Cs01 F004 119.15(3) 9 121_655 ?
F004 Cs01 F004 119.15(3) 77_445 121_655 ?
F004 Cs01 F004 44.6(3) 33_544 121_655 ?
F004 Cs01 F004 91.48(6) 49_454 121_655 ?
F004 Cs01 F004 119.15(3) 177_556 121_655 ?
F004 Cs01 F004 74.8(3) 153_565 121_655 ?
F004 Cs01 F004 119.15(3) 149_565 121_655 ?
F004 Cs01 F004 44.6(3) 125_655 121_655 ?
F004 Cs01 F004 161.5(4) 169_556 121_655 ?
F004 Cs02 F004 90.0 . 177_556 ?
F004 Cs02 F004 90.000(1) . 81_545 ?
F004 Cs02 F004 180.0 177_556 81_545 ?
F004 Cs02 F004 90.0 . 125_655 ?
F004 Cs02 F004 90.000(1) 177_556 125_655 ?
F004 Cs02 F004 90.0 81_545 125_655 ?
F004 Cs02 F004 90.0 . 29_545 ?
F004 Cs02 F004 90.000(1) 177_556 29_545 ?
F004 Cs02 F004 90.0 81_545 29_545 ?
F004 Cs02 F004 180.0 125_655 29_545 ?
F004 Cs02 F004 180.0 . 97_656 ?
F004 Cs02 F004 90.000(1) 177_556 97_656 ?
F004 Cs02 F004 90.0 81_545 97_656 ?
F004 Cs02 F004 90.000(1) 125_655 97_656 ?
F004 Cs02 F004 90.0 29_545 97_656 ?
F004 Cs02 Cs01 54.7 . 49 ?
F004 Cs02 Cs01 125.264(1) 177_556 49 ?
F004 Cs02 Cs01 54.7 81_545 49 ?
F004 Cs02 Cs01 125.3 125_655 49 ?
F004 Cs02 Cs01 54.736(1) 29_545 49 ?
F004 Cs02 Cs01 125.3 97_656 49 ?
F004 Cs02 Cs01 125.3 . 145 ?
F004 Cs02 Cs01 54.736(1) 177_556 145 ?
F004 Cs02 Cs01 125.3 81_545 145 ?
F004 Cs02 Cs01 54.7 125_655 145 ?
F004 Cs02 Cs01 125.264(1) 29_545 145 ?
F004 Cs02 Cs01 54.7 97_656 145 ?
Cs01 Cs02 Cs01 180.0 49 145 ?
F004 Cs02 Cs01 125.3 . 25_545 ?
F004 Cs02 Cs01 54.7 177_556 25_545 ?
F004 Cs02 Cs01 125.3 81_545 25_545 ?
F004 Cs02 Cs01 125.3 125_655 25_545 ?
F004 Cs02 Cs01 54.736(1) 29_545 25_545 ?
F004 Cs02 Cs01 54.7 97_656 25_545 ?
Cs01 Cs02 Cs01 109.5 49 25_545 ?
Cs01 Cs02 Cs01 70.5 145 25_545 ?
F004 Cs02 Cs01 54.7 . 121_655 ?
F004 Cs02 Cs01 125.3 177_556 121_655 ?
F004 Cs02 Cs01 54.7 81_545 121_655 ?
F004 Cs02 Cs01 54.7 125_655 121_655 ?
F004 Cs02 Cs01 125.264(1) 29_545 121_655 ?
F004 Cs02 Cs01 125.3 97_656 121_655 ?
Cs01 Cs02 Cs01 70.5 49 121_655 ?
Cs01 Cs02 Cs01 109.5 145 121_655 ?
Cs01 Cs02 Cs01 180.0 25_545 121_655 ?
F004 Cs02 Cs01 54.7 . . ?
F004 Cs02 Cs01 54.7 177_556 . ?
F004 Cs02 Cs01 125.3 81_545 . ?
F004 Cs02 Cs01 54.7 125_655 . ?
F004 Cs02 Cs01 125.3 29_545 . ?
F004 Cs02 Cs01 125.3 97_656 . ?
Cs01 Cs02 Cs01 109.5 49 . ?
Cs01 Cs02 Cs01 70.5 145 . ?
Cs01 Cs02 Cs01 109.5 25_545 . ?
Cs01 Cs02 Cs01 70.5 121_655 . ?
F004 Cs02 Cs01 125.264(1) . 73_545 ?
F004 Cs02 Cs01 125.264(1) 177_556 73_545 ?
F004 Cs02 Cs01 54.7 81_545 73_545 ?
F004 Cs02 Cs01 54.7 125_655 73_545 ?
F004 Cs02 Cs01 125.3 29_545 73_545 ?
F004 Cs02 Cs01 54.7 97_656 73_545 ?
Cs01 Cs02 Cs01 109.471(1) 49 73_545 ?
Cs01 Cs02 Cs01 70.5 145 73_545 ?
Cs01 Cs02 Cs01 109.5 25_545 73_545 ?
Cs01 Cs02 Cs01 70.5 121_655 73_545 ?
Cs01 Cs02 Cs01 109.5 . 73_545 ?
F004 Al03 F004 180.0 105_666 9 ?
F004 Al03 F004 90.000(1) 105_666 101_666 ?
F004 Al03 F004 90.000(1) 9 101_666 ?
F004 Al03 F004 90.000(1) 105_666 5 ?
F004 Al03 F004 90.000(1) 9 5 ?
F004 Al03 F004 180.0 101_666 5 ?
F004 Al03 F004 90.000(2) 105_666 97_666 ?
F004 Al03 F004 90.000(1) 9 97_666 ?
F004 Al03 F004 90.000(1) 101_666 97_666 ?
F004 Al03 F004 90.0 5 97_666 ?
F004 Al03 F004 90.000(1) 105_666 . ?
F004 Al03 F004 90.000(2) 9 . ?
F004 Al03 F004 90.0 101_666 . ?
F004 Al03 F004 90.000(1) 5 . ?
F004 Al03 F004 180.0 97_666 . ?
F004 Al03 Cs01 125.3 105_666 . ?
F004 Al03 Cs01 54.736(1) 9 . ?
F004 Al03 Cs01 125.264(1) 101_666 . ?
F004 Al03 Cs01 54.736(1) 5 . ?
F004 Al03 Cs01 125.264(1) 97_666 . ?
F004 Al03 Cs01 54.736(1) . . ?
F004 Al03 Cs01 54.7 105_666 97_666 ?
F004 Al03 Cs01 125.264(1) 9 97_666 ?
F004 Al03 Cs01 54.736(1) 101_666 97_666 ?
F004 Al03 Cs01 125.264(1) 5 97_666 ?
F004 Al03 Cs01 54.736(1) 97_666 97_666 ?
F004 Al03 Cs01 125.264(1) . 97_666 ?
Cs01 Al03 Cs01 180.0 . 97_666 ?
F004 Al03 Cs01 54.7 105_666 73 ?
F004 Al03 Cs01 125.264(1) 9 73 ?
F004 Al03 Cs01 125.264(1) 101_666 73 ?
F004 Al03 Cs01 54.736(1) 5 73 ?
F004 Al03 Cs01 54.736(1) 97_666 73 ?
F004 Al03 Cs01 125.264(1) . 73 ?
Cs01 Al03 Cs01 109.5 . 73 ?
Cs01 Al03 Cs01 70.5 97_666 73 ?
F004 Al03 Cs01 125.3 105_666 169_556 ?
F004 Al03 Cs01 54.736(1) 9 169_556 ?
F004 Al03 Cs01 54.736(1) 101_666 169_556 ?
F004 Al03 Cs01 125.264(1) 5 169_556 ?
F004 Al03 Cs01 125.264(1) 97_666 169_556 ?
F004 Al03 Cs01 54.736(1) . 169_556 ?
Cs01 Al03 Cs01 70.5 . 169_556 ?
Cs01 Al03 Cs01 109.5 97_666 169_556 ?
Cs01 Al03 Cs01 180.0 73 169_556 ?
F004 Al03 Cs01 54.7 105_666 121_655 ?
F004 Al03 Cs01 125.264(1) 9 121_655 ?
F004 Al03 Cs01 125.264(1) 101_666 121_655 ?
F004 Al03 Cs01 54.7 5 121_655 ?
F004 Al03 Cs01 125.264(1) 97_666 121_655 ?
F004 Al03 Cs01 54.736(1) . 121_655 ?
Cs01 Al03 Cs01 70.5 . 121_655 ?
Cs01 Al03 Cs01 109.5 97_666 121_655 ?
Cs01 Al03 Cs01 70.5 73 121_655 ?
Cs01 Al03 Cs01 109.5 169_556 121_655 ?
F004 Al03 Cs01 54.736(1) 105_666 49 ?
F004 Al03 Cs01 125.3 9 49 ?
F004 Al03 Cs01 54.7 101_666 49 ?
F004 Al03 Cs01 125.264(1) 5 49 ?
F004 Al03 Cs01 125.264(1) 97_666 49 ?
F004 Al03 Cs01 54.736(2) . 49 ?
Cs01 Al03 Cs01 109.5 . 49 ?
Cs01 Al03 Cs01 70.5 97_666 49 ?
Cs01 Al03 Cs01 109.5 73 49 ?
Cs01 Al03 Cs01 70.5 169_556 49 ?
Cs01 Al03 Cs01 70.5 121_655 49 ?
Al03 F004 Cs02 180.0 . . ?
Al03 F004 Cs01 99.26(19) . . ?
Cs02 F004 Cs01 80.74(19) . . ?
Al03 F004 Cs01 99.26(19) . 49 ?
Cs02 F004 Cs01 80.74(19) . 49 ?
Cs01 F004 Cs01 161.5(4) . 49 ?
Al03 F004 Cs01 99.26(19) . 169_556 ?
Cs02 F004 Cs01 80.74(19) . 169_556 ?
Cs01 F004 Cs01 88.52(6) . 169_556 ?
Cs01 F004 Cs01 88.52(6) 49 169_556 ?
Al03 F004 Cs01 99.26(19) . 121_655 ?
Cs02 F004 Cs01 80.74(19) . 121_655 ?
Cs01 F004 Cs01 88.52(6) . 121_655 ?
Cs01 F004 Cs01 88.52(6) 49 121_655 ?
Cs01 F004 Cs01 161.5(4) 169_556 121_655 ?

_refine_diff_density_max         1.758
_refine_diff_density_min         -1.332
_refine_diff_density_rms         0.199



####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_Cs3AlF6_C2_m
_database_code_depnum_ccdc_archive 'CCDC 2193507'
loop_
_audit_author_name
_audit_author_address
'Gregory Morrison'
;University of South Carolina
United States of America
;
_audit_update_record             
;
2022-07-28 deposited with the CCDC.	2023-05-19 downloaded from the CCDC.
;
_audit_creation_date             2022-01-12
_audit_creation_method           
;
Olex2 1.2
(compiled May 18 2018 14:05:52 for OlexSys, GUI svn.r5506)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         '0.08(Al12 Cs36 F72)'
_chemical_formula_sum            'Al Cs3 F6'
_chemical_formula_weight         539.71
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Al Al 0.0645 0.0514 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cs Cs -0.3680 2.1192 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           12
_space_group_name_H-M_alt        'C 1 2/m 1'
_space_group_name_Hall           '-C 2y'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z'
'-x, -y, -z'
'x, -y, z'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z'

_cell_length_a                   11.2739(2)
_cell_length_b                   19.5018(4)
_cell_length_c                   11.3248(2)
_cell_angle_alpha                90
_cell_angle_beta                 109.6410(10)
_cell_angle_gamma                90
_cell_volume                     2345.02(8)
_cell_formula_units_Z            12
_cell_measurement_reflns_used    9264
_cell_measurement_temperature    300.00
_cell_measurement_theta_max      36.2454
_cell_measurement_theta_min      3.2991
_shelx_estimated_absorpt_T_max   0.603
_shelx_estimated_absorpt_T_min   0.603
_exptl_absorpt_coefficient_mu    14.061
_exptl_absorpt_correction_T_max  0.7471
_exptl_absorpt_correction_T_min  0.6507
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
SADABS-2016/2 (Bruker,2016) was used for absorption correction.
wR2(int) was 0.1122 before and 0.0580 after correction.
The Ratio of minimum to maximum transmission is 0.8710.
The λ/2 correction factor is Not present.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    4.586
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       polyhedron
_exptl_crystal_F_000             2784
_exptl_crystal_size_max          0.04
_exptl_crystal_size_mid          0.04
_exptl_crystal_size_min          0.04
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0374
_diffrn_reflns_av_unetI/netI     0.0117
_diffrn_reflns_Laue_measured_fraction_full 0.998
_diffrn_reflns_Laue_measured_fraction_max 0.999
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_k_max       30
_diffrn_reflns_limit_k_min       -30
_diffrn_reflns_limit_l_max       17
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_number            108074
_diffrn_reflns_point_group_measured_fraction_full 0.998
_diffrn_reflns_point_group_measured_fraction_max 0.999
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         33.142
_diffrn_reflns_theta_min         2.184
_diffrn_ambient_temperature      300.0
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'Bruker D8 Quest'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   'microfocus sealed X-ray tube'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                4298
_reflns_number_total             4590
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences. Completness statistics refer to single and
 composite reflections containing twin component 1 only.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT v8.34A (Bruker, 2013)'
_computing_data_collection       'Bruker APEX3 v2016.5-0 (Bruker, 2016)'
_computing_data_reduction        'SAINT v8.34A (Bruker, 013)'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    'SHELXT 2018/2 (Sheldrick, 2018)'
_refine_diff_density_max         3.972
_refine_diff_density_min         -2.609
_refine_diff_density_rms         0.199
_refine_ls_extinction_coef       0.000148(14)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     'SHELXL-2018/3 (Sheldrick 2018)'
_refine_ls_goodness_of_fit_ref   1.166
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     166
_refine_ls_number_reflns         4590
_refine_ls_number_restraints     2
_refine_ls_R_factor_all          0.0273
_refine_ls_R_factor_gt           0.0244
_refine_ls_restrained_S_all      1.165
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0242P)²+18.9315P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0586
_refine_ls_wR_factor_ref         0.0619
_refine_special_details          
;
 Refined as a 2-component twin.
;
_olex2_refinement_description    
;
1. Twinned data refinement
 Scales: 0.9415(13)
 0.0585(13)
2. Uiso/Uaniso restraints and constraints
Uanis(F2A) = Uanis(F2B) = Uanis(F2C)
Uanis(Cs1A) = Uanis(Cs1B)
Uanis(F1A) = Uanis(F1B)
3. Others
 2*[Sof(Cs1A)+Sof(Cs1B)+Sof(F1A)+Sof(F2A)+Sof(F2C)]+1*[Sof(F1B)+Sof(F2B)]=1
 with esd of 0.001
 2*[Sof(Cs1A)+Sof(Cs1B)+Sof(F1A)+Sof(F2A)+Sof(F2C)]+1*[Sof(F1B)+Sof(F2B)]=1
 with esd of 0.001
 Sof(Cs1A)=1-FVAR(1)
 Sof(Cs1B)=Sof(F1A)=Sof(F2A)=Sof(F2C)=FVAR(1)
 Sof(F1B)=0.5*FVAR(3)
 Sof(F2B)=FVAR(2)
;
_atom_sites_solution_hydrogens   .
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Cs1A Cs 0.63952(11) 0.68949(6) 0.85473(10) 0.02180(13) Uani 0.685(4) 1 d . . .
. .
Cs1B Cs 0.6297(2) 0.67719(11) 0.8651(2) 0.02180(13) Uani 0.315(4) 1 d . . . . .
Cs2 Cs 0.35484(3) 0.500000 0.57122(3) 0.02420(7) Uani 1 2 d S T P . .
Cs3 Cs 0.79277(3) 1.000000 1.21052(3) 0.02485(7) Uani 1 2 d S T P . .
Cs4 Cs 0.28282(2) 0.64406(2) 0.77842(2) 0.02494(6) Uani 1 1 d . . . . .
Cs5 Cs -0.08368(4) 0.500000 0.14290(3) 0.02811(7) Uani 1 2 d S T P . .
Cs6 Cs 0.62593(2) 0.83220(2) 0.37939(2) 0.02601(5) Uani 1 1 d . . . . .
Al1 Al 0.500000 0.83413(6) 1.000000 0.0130(2) Uani 1 2 d S T P . .
Al2 Al 0.500000 0.500000 1.000000 0.0152(3) Uani 1 4 d S T P . .
Al3 Al 0.000000 0.500000 0.500000 0.0140(3) Uani 1 4 d S T P . .
Al4 Al 0.500000 0.67271(7) 0.500000 0.0132(2) Uani 1 2 d S T P . .
F1A F 0.4602(17) 0.4815(13) 0.835(2) 0.069(6) Uani 0.315(4) 1 d . . . . .
F1B F 0.421(3) 0.500000 0.835(4) 0.069(6) Uani 0.370(8) 2 d S T P . .
F2A F 0.5469(14) 0.5811(7) 0.9622(13) 0.059(2) Uani 0.315(4) 1 d . . . . .
F2B F 0.6132(12) 0.5641(7) 0.9840(11) 0.059(2) Uani 0.370(8) 1 d . . . . .
F2C F 0.6588(12) 0.5272(6) 1.0288(12) 0.059(2) Uani 0.315(4) 1 d . . . . .
F3 F 0.0975(3) 0.500000 0.3988(3) 0.0305(7) Uani 1 2 d S T P . .
F4 F 0.1000(3) 0.56511(14) 0.5967(3) 0.0359(6) Uani 1 1 d . . . . .
F5 F 0.4026(2) 0.60616(12) 0.3995(2) 0.0285(5) Uani 1 1 d . . . . .
F6 F 0.5991(2) 0.73864(11) 0.5988(2) 0.0260(4) Uani 1 1 d . . . . .
F7 F 0.4004(2) 0.67169(13) 0.5959(2) 0.0296(5) Uani 1 1 d . . . . .
F8 F 0.4029(2) 0.76783(12) 0.9020(2) 0.0311(5) Uani 1 1 d . . . . .
F9 F 0.4018(3) 0.83498(13) 1.0981(3) 0.0306(5) Uani 1 1 d . . . . .
F10 F 0.6001(2) 0.89954(13) 1.0980(2) 0.0310(5) Uani 1 1 d . . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Cs1A F2A 2.810(12) . ?
Cs1A F2B 2.916(13) . ?
Cs1A F2C 3.696(12) . ?
Cs1A F5 3.200(3) 2_656 ?
Cs1A F6 2.939(3) . ?
Cs1A F7 3.266(3) . ?
Cs1A F8 3.271(3) . ?
Cs1A F8 3.322(3) 2_657 ?
Cs1A F8 2.954(3) 8_565 ?
Cs1A F9 2.953(3) 2_657 ?
Cs1A F9 3.330(3) 8_565 ?
Cs1A F10 3.296(3) 7_667 ?
Cs1B F2A 2.507(12) . ?
Cs1B F2B 2.623(13) . ?
Cs1B F2C 3.419(12) . ?
Cs1B F5 3.209(4) 2_656 ?
Cs1B F6 3.154(3) . ?
Cs1B F7 3.270(4) . ?
Cs1B F8 3.153(4) 8_565 ?
Cs1B F8 3.249(4) . ?
Cs1B F8 3.297(4) 2_657 ?
Cs1B F9 3.314(4) 8_565 ?
Cs1B F9 3.141(3) 2_657 ?
Cs1B F10 3.292(4) 7_667 ?
Cs2 F1A 2.84(2) . ?
Cs2 F1A 2.84(2) 6_565 ?
Cs2 F1B 2.83(4) . ?
Cs2 F3 2.902(4) . ?
Cs2 F4 3.242(3) . ?
Cs2 F4 3.242(3) 6_565 ?
Cs2 F5 3.010(2) . ?
Cs2 F5 3.010(2) 6_565 ?
Cs2 F5 3.356(3) 2_656 ?
Cs2 F5 3.356(3) 5_666 ?
Cs2 F7 3.385(3) 6_565 ?
Cs2 F7 3.385(3) . ?
Cs3 F1A 3.019(15) 7_667 ?
Cs3 F1A 3.019(15) 4_657 ?
Cs3 F1B 3.44(3) 7_667 ?
Cs3 F2A 3.460(15) 4_657 ?
Cs3 F2B 3.018(12) 7_667 ?
Cs3 F2B 3.018(12) 4_657 ?
Cs3 F2C 2.986(12) 7_667 ?
Cs3 F2C 2.986(12) 4_657 ?
Cs3 F5 2.936(2) 8_566 ?
Cs3 F5 2.936(2) 3_556 ?
Cs3 F10 2.884(2) 6_575 ?
Cs3 F10 2.884(2) . ?
Cs4 F1A 3.09(2) 6_565 ?
Cs4 F1A 3.69(2) . ?
Cs4 F1B 3.172(17) . ?
Cs4 F2A 3.246(17) . ?
Cs4 F2A 3.167(13) 2_657 ?
Cs4 F2B 2.987(11) 2_657 ?
Cs4 F2C 3.071(12) 2_657 ?
Cs4 F4 2.829(2) . ?
Cs4 F6 3.290(2) 8_465 ?
Cs4 F7 2.857(2) . ?
Cs4 F8 2.889(2) . ?
Cs4 F9 2.900(2) 7_567 ?
Cs5 F2B 3.514(14) 6_464 ?
Cs5 F2C 2.803(14) 1_454 ?
Cs5 F2C 2.803(14) 6_464 ?
Cs5 F3 2.931(4) . ?
Cs5 F4 3.272(3) 5_566 ?
Cs5 F4 3.272(3) 2_556 ?
Cs5 F9 3.254(3) 3_444 ?
Cs5 F9 3.254(3) 8_464 ?
Cs5 F10 3.016(3) 3_444 ?
Cs5 F10 3.016(3) 8_464 ?
Cs5 F10 3.313(3) 4_546 ?
Cs5 F10 3.313(3) 7_566 ?
Cs6 F3 3.3025(5) 3 ?
Cs6 F4 3.322(3) 7_566 ?
Cs6 F4 3.261(3) 8_565 ?
Cs6 F5 3.278(3) 8_565 ?
Cs6 F6 3.178(2) . ?
Cs6 F6 3.201(3) 2_656 ?
Cs6 F6 3.327(3) 7_666 ?
Cs6 F7 3.166(3) 2_656 ?
Cs6 F7 3.239(3) 8_565 ?
Cs6 F8 3.338(3) 2_656 ?
Cs6 F9 3.336(3) 1_554 ?
Cs6 F10 3.367(3) 1_554 ?
Al1 F8 1.812(2) 2_657 ?
Al1 F8 1.812(2) . ?
Al1 F9 1.813(2) . ?
Al1 F9 1.813(2) 2_657 ?
Al1 F10 1.814(2) . ?
Al1 F10 1.814(2) 2_657 ?
Al2 F1A 1.81(2) 5_667 ?
Al2 F1A 1.81(2) . ?
Al2 F1B 1.78(4) 5_667 ?
Al2 F1B 1.78(4) . ?
Al2 F2A 1.765(12) 6_565 ?
Al2 F2A 1.765(12) . ?
Al2 F2A 1.765(12) 2_657 ?
Al2 F2A 1.765(12) 5_667 ?
Al2 F2C 1.789(11) 2_657 ?
Al2 F2C 1.789(11) 6_565 ?
Al2 F2C 1.789(11) . ?
Al2 F2C 1.789(11) 5_667 ?
Al3 F3 1.836(3) 5_566 ?
Al3 F3 1.836(3) . ?
Al3 F4 1.803(2) . ?
Al3 F4 1.803(2) 2_556 ?
Al3 F4 1.803(2) 5_566 ?
Al3 F4 1.803(2) 6_565 ?
Al4 F5 1.829(2) . ?
Al4 F5 1.829(2) 2_656 ?
Al4 F6 1.820(2) . ?
Al4 F6 1.820(2) 2_656 ?
Al4 F7 1.805(2) 2_656 ?
Al4 F7 1.805(2) . ?
F1A F1A 0.72(5) 6_565 ?
F1A F1B 0.57(3) . ?
F2A F2A 1.57(3) 2_657 ?
F2A F2B 0.778(18) . ?
F2A F2C 1.62(2) . ?
F2B F2C 0.930(17) . ?
F2C F2C 1.06(2) 6_565 ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
F2A Cs1A F2B 15.5(3) . . ?
F2A Cs1A F2C 24.3(4) . . ?
F2A Cs1A F5 92.5(3) . 2_656 ?
F2A Cs1A F6 135.7(3) . . ?
F2A Cs1A F7 89.7(3) . . ?
F2A Cs1A F8 80.7(3) . . ?
F2A Cs1A F8 129.1(3) . 8_565 ?
F2A Cs1A F8 79.0(3) . 2_657 ?
F2A Cs1A F9 122.7(3) . 2_657 ?
F2A Cs1A F9 83.7(3) . 8_565 ?
F2A Cs1A F10 88.5(4) . 7_667 ?
F2B Cs1A F2C 8.8(3) . . ?
F2B Cs1A F5 90.9(2) . 2_656 ?
F2B Cs1A F6 139.5(2) . . ?
F2B Cs1A F7 99.7(2) . . ?
F2B Cs1A F8 94.8(3) . . ?
F2B Cs1A F8 84.4(2) . 2_657 ?
F2B Cs1A F8 114.3(3) . 8_565 ?
F2B Cs1A F9 131.8(2) . 2_657 ?
F2B Cs1A F9 71.1(2) . 8_565 ?
F2B Cs1A F10 73.3(3) . 7_667 ?
F5 Cs1A F2C 90.53(19) 2_656 . ?
F5 Cs1A F7 46.39(6) 2_656 . ?
F5 Cs1A F8 120.14(7) 2_656 . ?
F5 Cs1A F8 163.85(8) 2_656 2_657 ?
F5 Cs1A F9 119.60(7) 2_656 8_565 ?
F5 Cs1A F10 74.53(6) 2_656 7_667 ?
F6 Cs1A F2C 140.08(19) . . ?
F6 Cs1A F5 49.56(6) . 2_656 ?
F6 Cs1A F7 48.85(6) . . ?
F6 Cs1A F8 84.27(7) . 8_565 ?
F6 Cs1A F8 130.53(7) . 2_657 ?
F6 Cs1A F8 98.30(8) . . ?
F6 Cs1A F9 83.31(7) . 2_657 ?
F6 Cs1A F9 131.54(7) . 8_565 ?
F6 Cs1A F10 99.58(8) . 7_667 ?
F7 Cs1A F2C 105.7(2) . . ?
F7 Cs1A F8 119.19(7) . 2_657 ?
F7 Cs1A F8 73.99(6) . . ?
F7 Cs1A F9 164.36(7) . 8_565 ?
F7 Cs1A F10 120.74(7) . 7_667 ?
F8 Cs1A F2C 102.6(2) . . ?
F8 Cs1A F2C 87.2(2) 2_657 . ?
F8 Cs1A F2C 105.6(2) 8_565 . ?
F8 Cs1A F5 98.19(8) 8_565 2_656 ?
F8 Cs1A F7 131.96(8) 8_565 . ?
F8 Cs1A F8 131.61(5) 8_565 . ?
F8 Cs1A F8 45.31(8) . 2_657 ?
F8 Cs1A F8 97.82(7) 8_565 2_657 ?
F8 Cs1A F9 48.05(6) 8_565 8_565 ?
F8 Cs1A F9 73.43(6) 2_657 8_565 ?
F8 Cs1A F9 118.53(7) . 8_565 ?
F8 Cs1A F10 161.89(8) . 7_667 ?
F8 Cs1A F10 48.16(6) 8_565 7_667 ?
F9 Cs1A F2C 135.3(2) 2_657 . ?
F9 Cs1A F2C 63.85(19) 8_565 . ?
F9 Cs1A F5 131.77(8) 2_657 2_656 ?
F9 Cs1A F7 97.58(8) 2_657 . ?
F9 Cs1A F8 48.29(6) 2_657 . ?
F9 Cs1A F8 48.14(6) 2_657 2_657 ?
F9 Cs1A F8 84.63(8) 2_657 8_565 ?
F9 Cs1A F9 97.93(7) 2_657 8_565 ?
F9 Cs1A F10 131.51(8) 2_657 7_667 ?
F10 Cs1A F2C 64.7(2) 7_667 . ?
F10 Cs1A F8 118.44(7) 7_667 2_657 ?
F10 Cs1A F9 45.20(6) 7_667 8_565 ?
F2A Cs1B F2B 17.3(4) . . ?
F2A Cs1B F2C 26.4(5) . . ?
F2A Cs1B F5 98.3(3) . 2_656 ?
F2A Cs1B F6 140.0(3) . . ?
F2A Cs1B F7 95.2(3) . . ?
F2A Cs1B F8 133.4(4) . 8_565 ?
F2A Cs1B F8 83.8(3) . 2_657 ?
F2A Cs1B F8 85.7(4) . . ?
F2A Cs1B F9 126.8(4) . 2_657 ?
F2A Cs1B F9 88.8(4) . 8_565 ?
F2A Cs1B F10 94.0(4) . 7_667 ?
F2B Cs1B F2C 9.2(4) . . ?
F2B Cs1B F5 96.4(3) . 2_656 ?
F2B Cs1B F6 143.8(3) . . ?
F2B Cs1B F7 106.3(3) . . ?
F2B Cs1B F8 116.9(3) . 8_565 ?
F2B Cs1B F8 89.6(3) . 2_657 ?
F2B Cs1B F8 101.3(3) . . ?
F2B Cs1B F9 136.4(3) . 2_657 ?
F2B Cs1B F9 74.8(3) . 8_565 ?
F2B Cs1B F10 77.0(3) . 7_667 ?
F5 Cs1B F2C 95.6(2) 2_656 . ?
F5 Cs1B F7 46.29(7) 2_656 . ?
F5 Cs1B F8 120.52(10) 2_656 . ?
F5 Cs1B F8 166.02(11) 2_656 2_657 ?
F5 Cs1B F9 119.78(10) 2_656 8_565 ?
F5 Cs1B F10 74.46(8) 2_656 7_667 ?
F6 Cs1B F2C 143.4(2) . . ?
F6 Cs1B F5 47.91(7) . 2_656 ?
F6 Cs1B F7 47.38(7) . . ?
F6 Cs1B F8 94.49(10) . . ?
F6 Cs1B F8 123.73(9) . 2_657 ?
F6 Cs1B F9 124.26(9) . 8_565 ?
F6 Cs1B F10 95.36(9) . 7_667 ?
F7 Cs1B F2C 112.3(2) . . ?
F7 Cs1B F8 119.85(10) . 2_657 ?
F7 Cs1B F9 165.93(11) . 8_565 ?
F7 Cs1B F10 120.75(10) . 7_667 ?
F8 Cs1B F2C 107.9(2) 8_565 . ?
F8 Cs1B F2C 109.4(2) . . ?
F8 Cs1B F2C 92.4(2) 2_657 . ?
F8 Cs1B F5 94.01(10) 8_565 2_656 ?
F8 Cs1B F6 77.63(8) 8_565 . ?
F8 Cs1B F7 124.45(9) 8_565 . ?
F8 Cs1B F7 74.23(8) . . ?
F8 Cs1B F8 45.66(8) . 2_657 ?
F8 Cs1B F8 94.48(10) 8_565 2_657 ?
F8 Cs1B F8 125.01(8) 8_565 . ?
F8 Cs1B F9 73.96(8) 2_657 8_565 ?
F8 Cs1B F9 46.96(7) 8_565 8_565 ?
F8 Cs1B F9 119.62(10) . 8_565 ?
F8 Cs1B F10 46.91(7) 8_565 7_667 ?
F8 Cs1B F10 164.93(11) . 7_667 ?
F9 Cs1B F2C 67.2(2) 8_565 . ?
F9 Cs1B F2C 139.5(2) 2_657 . ?
F9 Cs1B F5 124.37(10) 2_657 2_656 ?
F9 Cs1B F6 76.93(8) 2_657 . ?
F9 Cs1B F7 93.83(10) 2_657 . ?
F9 Cs1B F8 47.24(7) 2_657 . ?
F9 Cs1B F8 47.20(7) 2_657 2_657 ?
F9 Cs1B F8 78.36(8) 2_657 8_565 ?
F9 Cs1B F9 94.59(9) 2_657 8_565 ?
F9 Cs1B F10 124.71(10) 2_657 7_667 ?
F10 Cs1B F2C 68.1(2) 7_667 . ?
F10 Cs1B F8 119.30(10) 7_667 2_657 ?
F10 Cs1B F9 45.34(7) 7_667 8_565 ?
F1A Cs2 F1A 14.6(10) 6_565 . ?
F1A Cs2 F3 132.6(3) 6_565 . ?
F1A Cs2 F3 132.6(3) . . ?
F1A Cs2 F4 85.8(3) . 6_565 ?
F1A Cs2 F4 91.5(3) . . ?
F1A Cs2 F4 85.8(3) 6_565 . ?
F1A Cs2 F4 91.5(3) 6_565 6_565 ?
F1A Cs2 F5 119.3(5) 6_565 . ?
F1A Cs2 F5 86.3(4) . 2_656 ?
F1A Cs2 F5 77.2(4) . 5_666 ?
F1A Cs2 F5 131.6(4) . . ?
F1A Cs2 F5 86.3(4) 6_565 5_666 ?
F1A Cs2 F5 131.6(4) 6_565 6_565 ?
F1A Cs2 F5 119.3(5) . 6_565 ?
F1A Cs2 F5 77.2(4) 6_565 2_656 ?
F1A Cs2 F7 92.3(5) 6_565 6_565 ?
F1A Cs2 F7 92.3(5) . . ?
F1A Cs2 F7 77.8(5) . 6_565 ?
F1A Cs2 F7 77.8(5) 6_565 . ?
F1B Cs2 F1A 11.6(6) . 6_565 ?
F1B Cs2 F1A 11.6(6) . . ?
F1B Cs2 F3 124.1(7) . . ?
F1B Cs2 F4 80.4(6) . 6_565 ?
F1B Cs2 F4 80.4(6) . . ?
F1B Cs2 F5 88.8(5) . 2_656 ?
F1B Cs2 F5 129.9(3) . . ?
F1B Cs2 F5 88.8(5) . 5_666 ?
F1B Cs2 F5 129.9(3) . 6_565 ?
F1B Cs2 F7 86.22(10) . 6_565 ?
F1B Cs2 F7 86.22(10) . . ?
F3 Cs2 F4 49.03(7) . 6_565 ?
F3 Cs2 F4 49.03(7) . . ?
F3 Cs2 F5 85.45(7) . . ?
F3 Cs2 F5 131.56(5) . 2_656 ?
F3 Cs2 F5 85.45(7) . 6_565 ?
F3 Cs2 F5 131.56(5) . 5_666 ?
F3 Cs2 F7 98.35(5) . . ?
F3 Cs2 F7 98.35(5) . 6_565 ?
F4 Cs2 F4 46.12(9) 6_565 . ?
F4 Cs2 F5 117.82(6) 6_565 5_666 ?
F4 Cs2 F5 117.82(6) . 2_656 ?
F4 Cs2 F5 161.80(7) . 5_666 ?
F4 Cs2 F5 161.80(7) 6_565 2_656 ?
F4 Cs2 F7 119.65(6) . 6_565 ?
F4 Cs2 F7 119.65(6) 6_565 . ?
F4 Cs2 F7 73.73(6) 6_565 6_565 ?
F4 Cs2 F7 73.73(6) . . ?
F5 Cs2 F4 133.10(6) . 6_565 ?
F5 Cs2 F4 133.10(6) 6_565 . ?
F5 Cs2 F4 98.30(7) . . ?
F5 Cs2 F4 98.30(7) 6_565 6_565 ?
F5 Cs2 F5 86.91(9) . 6_565 ?
F5 Cs2 F5 99.87(6) 6_565 2_656 ?
F5 Cs2 F5 47.37(8) . 2_656 ?
F5 Cs2 F5 47.37(8) 6_565 5_666 ?
F5 Cs2 F5 99.87(6) . 5_666 ?
F5 Cs2 F5 76.18(8) 2_656 5_666 ?
F5 Cs2 F7 46.98(6) 6_565 6_565 ?
F5 Cs2 F7 44.40(6) 5_666 6_565 ?
F5 Cs2 F7 132.73(6) . 6_565 ?
F5 Cs2 F7 46.98(6) . . ?
F5 Cs2 F7 120.40(6) 5_666 . ?
F5 Cs2 F7 44.40(6) 2_656 . ?
F5 Cs2 F7 120.40(6) 2_656 6_565 ?
F5 Cs2 F7 132.73(6) 6_565 . ?
F7 Cs2 F7 163.16(9) . 6_565 ?
F1A Cs3 F1A 13.8(9) 7_667 4_657 ?
F1A Cs3 F1B 7.0(5) 4_657 7_667 ?
F1A Cs3 F1B 7.0(5) 7_667 7_667 ?
F1A Cs3 F2A 43.2(5) 4_657 4_657 ?
F1A Cs3 F2A 33.1(5) 7_667 4_657 ?
F1B Cs3 F2A 38.7(5) 7_667 4_657 ?
F2B Cs3 F1A 49.8(5) 7_667 7_667 ?
F2B Cs3 F1A 41.9(5) 4_657 7_667 ?
F2B Cs3 F1A 41.9(5) 7_667 4_657 ?
F2B Cs3 F1A 49.8(5) 4_657 4_657 ?
F2B Cs3 F1B 46.5(6) 4_657 7_667 ?
F2B Cs3 F1B 46.5(6) 7_667 7_667 ?
F2B Cs3 F2A 11.4(3) 4_657 4_657 ?
F2B Cs3 F2A 53.0(2) 7_667 4_657 ?
F2B Cs3 F2B 48.9(5) 7_667 4_657 ?
F2C Cs3 F1A 53.6(5) 7_667 7_667 ?
F2C Cs3 F1A 50.5(5) 4_657 7_667 ?
F2C Cs3 F1A 53.6(5) 4_657 4_657 ?
F2C Cs3 F1A 50.5(5) 7_667 4_657 ?
F2C Cs3 F1B 52.8(7) 4_657 7_667 ?
F2C Cs3 F1B 52.8(7) 7_667 7_667 ?
F2C Cs3 F2A 27.9(4) 4_657 4_657 ?
F2C Cs3 F2A 43.8(3) 7_667 4_657 ?
F2C Cs3 F2B 17.8(3) 7_667 7_667 ?
F2C Cs3 F2B 36.4(4) 7_667 4_657 ?
F2C Cs3 F2B 17.8(3) 4_657 4_657 ?
F2C Cs3 F2B 36.4(4) 4_657 7_667 ?
F2C Cs3 F2C 20.5(5) 7_667 4_657 ?
F5 Cs3 F1A 81.5(4) 3_556 7_667 ?
F5 Cs3 F1A 91.2(5) 3_556 4_657 ?
F5 Cs3 F1A 91.2(5) 8_566 7_667 ?
F5 Cs3 F1A 81.5(4) 8_566 4_657 ?
F5 Cs3 F1B 85.6(5) 8_566 7_667 ?
F5 Cs3 F1B 85.6(5) 3_556 7_667 ?
F5 Cs3 F2A 124.2(2) 8_566 4_657 ?
F5 Cs3 F2A 85.3(3) 3_556 4_657 ?
F5 Cs3 F2B 94.3(3) 3_556 4_657 ?
F5 Cs3 F2B 131.2(2) 8_566 4_657 ?
F5 Cs3 F2B 131.2(2) 3_556 7_667 ?
F5 Cs3 F2B 94.3(3) 8_566 7_667 ?
F5 Cs3 F2C 112.0(3) 8_566 7_667 ?
F5 Cs3 F2C 128.74(19) 8_566 4_657 ?
F5 Cs3 F2C 112.0(3) 3_556 4_657 ?
F5 Cs3 F2C 128.74(19) 3_556 7_667 ?
F5 Cs3 F5 89.69(10) 3_556 8_566 ?
F10 Cs3 F1A 116.4(5) 6_575 7_667 ?
F10 Cs3 F1A 127.4(4) . 7_667 ?
F10 Cs3 F1A 127.4(4) 6_575 4_657 ?
F10 Cs3 F1A 116.4(5) . 4_657 ?
F10 Cs3 F1B 122.6(4) 6_575 7_667 ?
F10 Cs3 F1B 122.6(4) . 7_667 ?
F10 Cs3 F2A 84.2(2) 6_575 4_657 ?
F10 Cs3 F2A 121.3(3) . 4_657 ?
F10 Cs3 F2B 110.9(3) 6_575 7_667 ?
F10 Cs3 F2B 110.9(3) . 4_657 ?
F10 Cs3 F2B 78.1(2) . 7_667 ?
F10 Cs3 F2B 78.1(2) 6_575 4_657 ?
F10 Cs3 F2C 79.6(2) 6_575 4_657 ?
F10 Cs3 F2C 93.4(3) . 4_657 ?
F10 Cs3 F2C 79.6(2) . 7_667 ?
F10 Cs3 F2C 93.4(3) 6_575 7_667 ?
F10 Cs3 F5 150.64(7) . 3_556 ?
F10 Cs3 F5 85.04(7) . 8_566 ?
F10 Cs3 F5 150.64(7) 6_575 8_566 ?
F10 Cs3 F5 85.04(7) 6_575 3_556 ?
F10 Cs3 F10 85.57(11) . 6_575 ?
F1A Cs4 F1A 6.9(5) 6_565 . ?
F1A Cs4 F1B 10.4(7) 6_565 . ?
F1A Cs4 F2A 34.6(5) 6_565 . ?
F1A Cs4 F2A 49.6(5) 6_565 2_657 ?
F1A Cs4 F6 155.3(4) 6_565 8_465 ?
F1B Cs4 F1A 4.1(7) . . ?
F1B Cs4 F2A 41.6(7) . . ?
F1B Cs4 F6 154.9(7) . 8_465 ?
F2A Cs4 F1A 51.8(4) 2_657 . ?
F2A Cs4 F1A 40.2(4) . . ?
F2A Cs4 F1B 50.6(8) 2_657 . ?
F2A Cs4 F2A 28.3(4) 2_657 . ?
F2A Cs4 F6 154.4(2) 2_657 8_465 ?
F2A Cs4 F6 155.6(2) . 8_465 ?
F2B Cs4 F1A 50.9(4) 2_657 . ?
F2B Cs4 F1A 50.9(4) 2_657 6_565 ?
F2B Cs4 F1B 48.5(7) 2_657 . ?
F2B Cs4 F2A 14.1(3) 2_657 2_657 ?
F2B Cs4 F2A 39.4(3) 2_657 . ?
F2B Cs4 F2C 17.6(3) 2_657 2_657 ?
F2B Cs4 F6 153.4(2) 2_657 8_465 ?
F2C Cs4 F1A 42.6(3) 2_657 . ?
F2C Cs4 F1A 45.2(4) 2_657 6_565 ?
F2C Cs4 F1B 39.2(7) 2_657 . ?
F2C Cs4 F2A 48.1(3) 2_657 . ?
F2C Cs4 F2A 30.1(4) 2_657 2_657 ?
F2C Cs4 F6 153.6(2) 2_657 8_465 ?
F4 Cs4 F1A 89.0(5) . 6_565 ?
F4 Cs4 F1A 83.0(4) . . ?
F4 Cs4 F1B 81.6(7) . . ?
F4 Cs4 F2A 123.2(2) . . ?
F4 Cs4 F2A 122.0(3) . 2_657 ?
F4 Cs4 F2B 109.9(3) . 2_657 ?
F4 Cs4 F2C 92.5(3) . 2_657 ?
F4 Cs4 F6 77.02(7) . 8_465 ?
F4 Cs4 F7 88.75(8) . . ?
F4 Cs4 F8 156.27(8) . . ?
F4 Cs4 F9 87.83(8) . 7_567 ?
F6 Cs4 F1A 153.7(4) 8_465 . ?
F7 Cs4 F1A 86.1(3) . . ?
F7 Cs4 F1A 82.7(3) . 6_565 ?
F7 Cs4 F1B 89.9(6) . . ?
F7 Cs4 F2A 89.2(2) . . ?
F7 Cs4 F2A 117.4(3) . 2_657 ?
F7 Cs4 F2B 127.8(2) . 2_657 ?
F7 Cs4 F2C 127.9(2) . 2_657 ?
F7 Cs4 F6 76.74(7) . 8_465 ?
F7 Cs4 F8 86.40(8) . . ?
F7 Cs4 F9 154.83(7) . 7_567 ?
F8 Cs4 F1A 119.7(3) . . ?
F8 Cs4 F1A 113.4(5) . 6_565 ?
F8 Cs4 F1B 121.6(7) . . ?
F8 Cs4 F2A 80.5(3) . 2_657 ?
F8 Cs4 F2A 80.0(2) . . ?
F8 Cs4 F2B 91.2(3) . 2_657 ?
F8 Cs4 F2C 108.8(3) . 2_657 ?
F8 Cs4 F6 79.27(7) . 8_465 ?
F8 Cs4 F9 86.78(8) . 7_567 ?
F9 Cs4 F1A 122.1(3) 7_567 6_565 ?
F9 Cs4 F1A 118.2(3) 7_567 . ?
F9 Cs4 F1B 114.2(6) 7_567 . ?
F9 Cs4 F2A 113.3(2) 7_567 . ?
F9 Cs4 F2A 85.2(2) 7_567 2_657 ?
F9 Cs4 F2B 76.5(2) 7_567 2_657 ?
F9 Cs4 F2C 77.2(2) 7_567 2_657 ?
F9 Cs4 F6 78.19(7) 7_567 8_465 ?
F2C Cs5 F2B 11.0(3) 6_464 6_464 ?
F2C Cs5 F2B 32.1(3) 1_454 6_464 ?
F2C Cs5 F2C 21.8(5) 6_464 1_454 ?
F2C Cs5 F3 136.5(3) 1_454 . ?
F2C Cs5 F3 136.5(3) 6_464 . ?
F2C Cs5 F4 97.2(2) 6_464 2_556 ?
F2C Cs5 F4 97.2(2) 1_454 5_566 ?
F2C Cs5 F4 88.8(3) 6_464 5_566 ?
F2C Cs5 F4 88.8(3) 1_454 2_556 ?
F2C Cs5 F9 75.6(2) 1_454 8_464 ?
F2C Cs5 F9 97.2(2) 1_454 3_444 ?
F2C Cs5 F9 97.2(2) 6_464 8_464 ?
F2C Cs5 F9 75.6(2) 6_464 3_444 ?
F2C Cs5 F10 135.1(2) 1_454 3_444 ?
F2C Cs5 F10 88.3(3) 6_464 7_566 ?
F2C Cs5 F10 88.3(3) 1_454 4_546 ?
F2C Cs5 F10 75.3(2) 1_454 7_566 ?
F2C Cs5 F10 135.1(2) 6_464 8_464 ?
F2C Cs5 F10 75.3(2) 6_464 4_546 ?
F2C Cs5 F10 117.6(2) 1_454 8_464 ?
F2C Cs5 F10 117.6(2) 6_464 3_444 ?
F3 Cs5 F2B 137.8(2) . 6_464 ?
F3 Cs5 F4 48.74(7) . 5_566 ?
F3 Cs5 F4 48.74(7) . 2_556 ?
F3 Cs5 F9 97.82(5) . 3_444 ?
F3 Cs5 F9 97.82(5) . 8_464 ?
F3 Cs5 F10 129.91(6) . 4_546 ?
F3 Cs5 F10 82.91(7) . 8_464 ?
F3 Cs5 F10 82.91(7) . 3_444 ?
F3 Cs5 F10 129.91(6) . 7_566 ?
F4 Cs5 F2B 89.08(19) 5_566 6_464 ?
F4 Cs5 F2B 105.1(2) 2_556 6_464 ?
F4 Cs5 F4 45.66(9) 2_556 5_566 ?
F4 Cs5 F10 165.26(7) 2_556 4_546 ?
F4 Cs5 F10 120.54(6) 5_566 4_546 ?
F4 Cs5 F10 120.54(6) 2_556 7_566 ?
F4 Cs5 F10 165.26(7) 5_566 7_566 ?
F9 Cs5 F2B 65.09(19) 3_444 6_464 ?
F9 Cs5 F2B 106.42(19) 8_464 6_464 ?
F9 Cs5 F4 120.62(6) 3_444 2_556 ?
F9 Cs5 F4 75.03(6) 3_444 5_566 ?
F9 Cs5 F4 120.62(6) 8_464 5_566 ?
F9 Cs5 F4 75.03(6) 8_464 2_556 ?
F9 Cs5 F9 163.09(9) 3_444 8_464 ?
F9 Cs5 F10 45.62(6) 8_464 7_566 ?
F9 Cs5 F10 45.62(6) 3_444 4_546 ?
F9 Cs5 F10 118.07(6) 3_444 7_566 ?
F9 Cs5 F10 118.07(6) 8_464 4_546 ?
F10 Cs5 F2B 90.75(19) 7_566 6_464 ?
F10 Cs5 F2B 65.9(2) 4_546 6_464 ?
F10 Cs5 F2B 138.57(19) 8_464 6_464 ?
F10 Cs5 F2B 106.71(19) 3_444 6_464 ?
F10 Cs5 F4 98.61(7) 3_444 5_566 ?
F10 Cs5 F4 130.83(6) 8_464 5_566 ?
F10 Cs5 F4 98.61(7) 8_464 2_556 ?
F10 Cs5 F4 130.83(6) 3_444 2_556 ?
F10 Cs5 F9 48.14(6) 8_464 8_464 ?
F10 Cs5 F9 48.14(6) 3_444 3_444 ?
F10 Cs5 F9 128.14(6) 3_444 8_464 ?
F10 Cs5 F9 128.14(6) 8_464 3_444 ?
F10 Cs5 F10 95.55(7) 8_464 4_546 ?
F10 Cs5 F10 95.55(7) 3_444 7_566 ?
F10 Cs5 F10 47.82(8) 8_464 7_566 ?
F10 Cs5 F10 47.82(8) 3_444 4_546 ?
F10 Cs5 F10 81.01(10) 8_464 3_444 ?
F10 Cs5 F10 72.51(8) 4_546 7_566 ?
F3 Cs6 F4 45.82(7) 3 7_566 ?
F3 Cs6 F6 121.02(7) 3 7_666 ?
F3 Cs6 F8 117.11(7) 3 2_656 ?
F3 Cs6 F9 89.33(8) 3 1_554 ?
F3 Cs6 F10 72.37(7) 3 1_554 ?
F4 Cs6 F3 46.06(7) 8_565 3 ?
F4 Cs6 F4 45.77(8) 8_565 7_566 ?
F4 Cs6 F5 92.69(7) 8_565 8_565 ?
F4 Cs6 F6 164.86(6) 7_566 7_666 ?
F4 Cs6 F6 121.12(6) 8_565 7_666 ?
F4 Cs6 F8 118.25(6) 7_566 2_656 ?
F4 Cs6 F8 161.21(6) 8_565 2_656 ?
F4 Cs6 F9 73.30(6) 7_566 1_554 ?
F4 Cs6 F9 118.64(6) 8_565 1_554 ?
F4 Cs6 F10 90.99(7) 7_566 1_554 ?
F4 Cs6 F10 118.26(6) 8_565 1_554 ?
F5 Cs6 F3 75.13(7) 8_565 3 ?
F5 Cs6 F4 120.72(6) 8_565 7_566 ?
F5 Cs6 F6 46.05(6) 8_565 7_666 ?
F5 Cs6 F8 89.39(6) 8_565 2_656 ?
F5 Cs6 F9 117.27(6) 8_565 1_554 ?
F5 Cs6 F10 72.57(6) 8_565 1_554 ?
F6 Cs6 F3 117.56(7) 2_656 3 ?
F6 Cs6 F3 118.68(7) . 3 ?
F6 Cs6 F4 90.29(7) . 7_566 ?
F6 Cs6 F4 72.92(6) . 8_565 ?
F6 Cs6 F4 91.00(7) 2_656 8_565 ?
F6 Cs6 F4 71.83(6) 2_656 7_566 ?
F6 Cs6 F5 164.53(6) 2_656 8_565 ?
F6 Cs6 F5 119.64(6) . 8_565 ?
F6 Cs6 F6 47.65(8) . 2_656 ?
F6 Cs6 F6 92.00(6) . 7_666 ?
F6 Cs6 F6 120.034(14) 2_656 7_666 ?
F6 Cs6 F7 73.30(6) . 8_565 ?
F6 Cs6 F7 120.57(6) 2_656 8_565 ?
F6 Cs6 F8 121.76(6) . 2_656 ?
F6 Cs6 F8 72.77(6) 7_666 2_656 ?
F6 Cs6 F8 91.94(6) 2_656 2_656 ?
F6 Cs6 F9 117.74(6) 7_666 1_554 ?
F6 Cs6 F9 121.02(6) . 1_554 ?
F6 Cs6 F9 73.57(6) 2_656 1_554 ?
F6 Cs6 F10 164.38(6) . 1_554 ?
F6 Cs6 F10 118.46(6) 2_656 1_554 ?
F6 Cs6 F10 90.81(6) 7_666 1_554 ?
F7 Cs6 F3 93.56(8) 8_565 3 ?
F7 Cs6 F3 163.71(7) 2_656 3 ?
F7 Cs6 F4 119.44(6) 2_656 7_566 ?
F7 Cs6 F4 120.37(6) 2_656 8_565 ?
F7 Cs6 F4 75.44(6) 8_565 8_565 ?
F7 Cs6 F4 121.06(6) 8_565 7_566 ?
F7 Cs6 F5 118.15(6) 2_656 8_565 ?
F7 Cs6 F5 46.48(6) 8_565 8_565 ?
F7 Cs6 F6 72.28(6) 2_656 7_666 ?
F7 Cs6 F6 47.87(6) 2_656 2_656 ?
F7 Cs6 F6 45.95(6) 8_565 7_666 ?
F7 Cs6 F6 47.68(6) 2_656 . ?
F7 Cs6 F7 90.23(7) 2_656 8_565 ?
F7 Cs6 F8 74.38(6) 2_656 2_656 ?
F7 Cs6 F8 118.39(6) 8_565 2_656 ?
F7 Cs6 F9 161.37(6) 8_565 1_554 ?
F7 Cs6 F9 92.12(7) 2_656 1_554 ?
F7 Cs6 F10 118.82(6) 8_565 1_554 ?
F7 Cs6 F10 119.24(6) 2_656 1_554 ?
F8 Cs6 F10 45.05(6) 2_656 1_554 ?
F9 Cs6 F8 45.16(6) 1_554 2_656 ?
F9 Cs6 F10 45.02(6) 1_554 1_554 ?
Cs1A Al1 Cs1A 166.31(5) 8_465 7_667 ?
Cs1A Al1 Cs1A 104.62(3) 2_657 7_667 ?
Cs1A Al1 Cs1A 64.74(3) . 7_667 ?
Cs1A Al1 Cs1A 86.01(5) 2_657 . ?
Cs1A Al1 Cs1A 64.74(3) 2_657 8_465 ?
Cs1A Al1 Cs1A 104.62(3) . 8_465 ?
Cs1A Al1 Cs5 103.95(2) . 7_566 ?
Cs1A Al1 Cs5 103.95(2) 2_657 3_556 ?
Cs1A Al1 Cs5 84.75(2) 8_465 3_556 ?
Cs1A Al1 Cs5 106.89(2) 8_465 7_566 ?
Cs1A Al1 Cs5 168.70(3) . 3_556 ?
Cs1A Al1 Cs5 168.70(3) 2_657 7_566 ?
Cs1A Al1 Cs5 106.89(2) 7_667 3_556 ?
Cs1A Al1 Cs5 84.75(2) 7_667 7_566 ?
Cs5 Al1 Cs5 66.72(2) 3_556 7_566 ?
F8 Al1 Cs1A 57.73(9) 2_657 2_657 ?
F8 Al1 Cs1A 59.36(9) . 2_657 ?
F8 Al1 Cs1A 59.36(9) 2_657 . ?
F8 Al1 Cs1A 47.32(9) . 8_465 ?
F8 Al1 Cs1A 47.32(9) 2_657 7_667 ?
F8 Al1 Cs1A 120.52(9) 2_657 8_465 ?
F8 Al1 Cs1A 57.73(9) . . ?
F8 Al1 Cs1A 120.52(9) . 7_667 ?
F8 Al1 Cs5 132.05(9) . 3_556 ?
F8 Al1 Cs5 121.46(9) . 7_566 ?
F8 Al1 Cs5 132.05(9) 2_657 7_566 ?
F8 Al1 Cs5 121.46(9) 2_657 3_556 ?
F8 Al1 F8 88.98(18) 2_657 . ?
F8 Al1 F9 89.95(13) . 2_657 ?
F8 Al1 F9 90.80(13) . . ?
F8 Al1 F9 90.79(13) 2_657 2_657 ?
F8 Al1 F9 89.95(13) 2_657 . ?
F8 Al1 F10 178.80(13) . . ?
F8 Al1 F10 90.20(12) 2_657 . ?
F8 Al1 F10 178.80(13) 2_657 2_657 ?
F8 Al1 F10 90.20(12) . 2_657 ?
F9 Al1 Cs1A 47.52(9) 2_657 . ?
F9 Al1 Cs1A 47.53(9) . 2_657 ?
F9 Al1 Cs1A 133.52(10) . . ?
F9 Al1 Cs1A 120.78(9) 2_657 8_465 ?
F9 Al1 Cs1A 133.52(10) 2_657 2_657 ?
F9 Al1 Cs1A 59.37(9) 2_657 7_667 ?
F9 Al1 Cs1A 120.78(9) . 7_667 ?
F9 Al1 Cs1A 59.37(9) . 8_465 ?
F9 Al1 Cs5 56.75(9) . 3_556 ?
F9 Al1 Cs5 56.75(9) 2_657 7_566 ?
F9 Al1 Cs5 122.22(10) 2_657 3_556 ?
F9 Al1 Cs5 122.22(10) . 7_566 ?
F9 Al1 F9 178.96(18) . 2_657 ?
F9 Al1 F10 89.19(13) . 2_657 ?
F9 Al1 F10 90.07(13) . . ?
F9 Al1 F10 89.19(13) 2_657 . ?
F9 Al1 F10 90.08(13) 2_657 2_657 ?
F10 Al1 Cs1A 121.08(9) . . ?
F10 Al1 Cs1A 133.88(9) . 8_465 ?
F10 Al1 Cs1A 133.88(9) 2_657 7_667 ?
F10 Al1 Cs1A 120.82(9) 2_657 . ?
F10 Al1 Cs1A 58.29(9) 2_657 8_465 ?
F10 Al1 Cs1A 58.30(9) . 7_667 ?
F10 Al1 Cs1A 120.82(9) . 2_657 ?
F10 Al1 Cs1A 121.07(9) 2_657 2_657 ?
F10 Al1 Cs5 58.64(9) 2_657 3_556 ?
F10 Al1 Cs5 58.64(9) . 7_566 ?
F10 Al1 Cs5 49.14(9) . 3_556 ?
F10 Al1 Cs5 49.15(9) 2_657 7_566 ?
F10 Al1 F10 90.64(18) 2_657 . ?
F1A Al2 F1A 180.0(15) . 5_667 ?
F1B Al2 F1A 161.6(10) 5_667 . ?
F1B Al2 F1A 18.4(10) . . ?
F1B Al2 F1A 161.6(10) . 5_667 ?
F1B Al2 F1A 18.3(10) 5_667 5_667 ?
F1B Al2 F1B 179.998(10) . 5_667 ?
F1B Al2 F2C 72.0(10) . 2_657 ?
F1B Al2 F2C 72.0(10) 5_667 6_565 ?
F1B Al2 F2C 108.0(10) 5_667 5_667 ?
F1B Al2 F2C 108.0(10) 5_667 2_657 ?
F1B Al2 F2C 108.0(10) . . ?
F1B Al2 F2C 72.0(10) 5_667 . ?
F1B Al2 F2C 108.0(10) . 6_565 ?
F1B Al2 F2C 72.0(10) . 5_667 ?
F2A Al2 F1A 85.4(9) . . ?
F2A Al2 F1A 85.4(9) 5_667 5_667 ?
F2A Al2 F1A 63.9(9) 2_657 5_667 ?
F2A Al2 F1A 94.6(9) 5_667 . ?
F2A Al2 F1A 116.1(9) 6_565 5_667 ?
F2A Al2 F1A 116.1(9) 2_657 . ?
F2A Al2 F1A 94.6(9) . 5_667 ?
F2A Al2 F1A 63.9(9) 6_565 . ?
F2A Al2 F1B 99.7(6) . 5_667 ?
F2A Al2 F1B 99.7(6) 5_667 . ?
F2A Al2 F1B 99.7(6) 6_565 5_667 ?
F2A Al2 F1B 80.3(6) 2_657 5_667 ?
F2A Al2 F1B 80.3(6) 6_565 . ?
F2A Al2 F1B 99.7(6) 2_657 . ?
F2A Al2 F1B 80.3(6) . . ?
F2A Al2 F1B 80.3(6) 5_667 5_667 ?
F2A Al2 F2A 127.3(10) . 6_565 ?
F2A Al2 F2A 180.0 . 5_667 ?
F2A Al2 F2A 127.3(10) 5_667 2_657 ?
F2A Al2 F2A 52.7(10) . 2_657 ?
F2A Al2 F2A 180.0 6_565 2_657 ?
F2A Al2 F2A 52.7(10) 5_667 6_565 ?
F2A Al2 F2C 54.2(7) . . ?
F2A Al2 F2C 125.8(7) 2_657 6_565 ?
F2A Al2 F2C 125.8(7) 6_565 2_657 ?
F2A Al2 F2C 125.8(7) 5_667 . ?
F2A Al2 F2C 93.1(7) . 2_657 ?
F2A Al2 F2C 86.9(7) 6_565 . ?
F2A Al2 F2C 86.9(7) 2_657 5_667 ?
F2A Al2 F2C 93.1(7) 2_657 . ?
F2A Al2 F2C 54.2(7) 5_667 5_667 ?
F2A Al2 F2C 125.8(7) . 5_667 ?
F2A Al2 F2C 86.9(7) 5_667 2_657 ?
F2A Al2 F2C 86.9(7) . 6_565 ?
F2A Al2 F2C 54.2(7) 2_657 2_657 ?
F2A Al2 F2C 93.1(7) 5_667 6_565 ?
F2A Al2 F2C 54.2(7) 6_565 6_565 ?
F2A Al2 F2C 93.1(7) 6_565 5_667 ?
F2C Al2 F1A 89.2(7) 2_657 . ?
F2C Al2 F1A 89.2(7) 6_565 5_667 ?
F2C Al2 F1A 97.6(6) 5_667 5_667 ?
F2C Al2 F1A 97.6(6) . . ?
F2C Al2 F1A 82.4(6) . 5_667 ?
F2C Al2 F1A 90.8(7) 2_657 5_667 ?
F2C Al2 F1A 82.4(6) 5_667 . ?
F2C Al2 F1A 90.8(7) 6_565 . ?
F2C Al2 F2C 145.5(9) 5_667 6_565 ?
F2C Al2 F2C 180.0(8) 6_565 2_657 ?
F2C Al2 F2C 34.5(9) 6_565 . ?
F2C Al2 F2C 145.5(9) 2_657 . ?
F2C Al2 F2C 180.0 5_667 . ?
F2C Al2 F2C 34.5(9) 5_667 2_657 ?
Cs2 Al3 Cs2 180.0 . 5_566 ?
Cs2 Al3 Cs5 95.280(8) 5_566 5_566 ?
Cs2 Al3 Cs5 95.280(8) . . ?
Cs2 Al3 Cs5 84.720(8) 5_566 . ?
Cs2 Al3 Cs5 84.720(8) . 5_566 ?
Cs2 Al3 Cs6 113.416(4) . 4_546 ?
Cs2 Al3 Cs6 113.416(4) 5_566 8_465 ?
Cs2 Al3 Cs6 66.584(4) . 8_465 ?
Cs2 Al3 Cs6 66.584(4) 5_566 4_546 ?
Cs5 Al3 Cs5 180.000(12) . 5_566 ?
Cs5 Al3 Cs6 68.165(4) 5_566 4_546 ?
Cs5 Al3 Cs6 68.165(5) . 8_465 ?
Cs5 Al3 Cs6 111.835(5) 5_566 8_465 ?
Cs5 Al3 Cs6 111.835(5) . 4_546 ?
Cs6 Al3 Cs6 180.0 4_546 8_465 ?
F3 Al3 Cs2 132.47(11) . 5_566 ?
F3 Al3 Cs2 47.53(11) . . ?
F3 Al3 Cs2 132.47(11) 5_566 . ?
F3 Al3 Cs2 47.53(11) 5_566 5_566 ?
F3 Al3 Cs5 132.25(11) 5_566 . ?
F3 Al3 Cs5 47.75(11) 5_566 5_566 ?
F3 Al3 Cs5 132.25(11) . 5_566 ?
F3 Al3 Cs5 47.75(11) . . ?
F3 Al3 Cs6 124.816(4) . 4_546 ?
F3 Al3 Cs6 55.184(4) . 8_465 ?
F3 Al3 Cs6 55.184(5) 5_566 4_546 ?
F3 Al3 Cs6 124.816(5) 5_566 8_465 ?
F3 Al3 F3 180.0 . 5_566 ?
F4 Al3 Cs2 58.23(10) 5_566 5_566 ?
F4 Al3 Cs2 58.23(10) 2_556 5_566 ?
F4 Al3 Cs2 121.77(10) 5_566 . ?
F4 Al3 Cs2 121.77(10) 6_565 5_566 ?
F4 Al3 Cs2 121.77(10) 2_556 . ?
F4 Al3 Cs2 121.77(10) . 5_566 ?
F4 Al3 Cs2 58.23(10) . . ?
F4 Al3 Cs2 58.23(10) 6_565 . ?
F4 Al3 Cs5 58.48(9) 6_565 5_566 ?
F4 Al3 Cs5 121.52(9) 6_565 . ?
F4 Al3 Cs5 121.52(9) 5_566 5_566 ?
F4 Al3 Cs5 121.52(9) 2_556 5_566 ?
F4 Al3 Cs5 121.52(9) . . ?
F4 Al3 Cs5 58.48(9) . 5_566 ?
F4 Al3 Cs5 58.48(9) 5_566 . ?
F4 Al3 Cs5 58.48(9) 2_556 . ?
F4 Al3 Cs6 53.71(9) 5_566 4_546 ?
F4 Al3 Cs6 124.34(10) 2_556 4_546 ?
F4 Al3 Cs6 126.29(9) 5_566 8_465 ?
F4 Al3 Cs6 55.66(10) 2_556 8_465 ?
F4 Al3 Cs6 53.71(9) . 8_465 ?
F4 Al3 Cs6 55.66(10) 6_565 4_546 ?
F4 Al3 Cs6 126.29(9) . 4_546 ?
F4 Al3 Cs6 124.34(10) 6_565 8_465 ?
F4 Al3 F3 90.24(12) 5_566 . ?
F4 Al3 F3 89.76(12) . . ?
F4 Al3 F3 90.24(12) 2_556 . ?
F4 Al3 F3 89.76(12) 6_565 . ?
F4 Al3 F3 90.24(12) 6_565 5_566 ?
F4 Al3 F3 89.76(12) 2_556 5_566 ?
F4 Al3 F3 90.24(12) . 5_566 ?
F4 Al3 F3 89.76(12) 5_566 5_566 ?
F4 Al3 F4 180.0 5_566 . ?
F4 Al3 F4 90.48(19) 2_556 . ?
F4 Al3 F4 90.48(19) 5_566 6_565 ?
F4 Al3 F4 89.52(19) 5_566 2_556 ?
F4 Al3 F4 180.0 6_565 2_556 ?
F4 Al3 F4 89.52(19) 6_565 . ?
Cs1A Al4 Cs1A 170.13(5) 2_656 . ?
Cs1A Al4 Cs1B 4.31(3) 2_656 2_656 ?
Cs1A Al4 Cs1B 173.37(6) . 2_656 ?
Cs1A Al4 Cs1B 173.37(6) 2_656 . ?
Cs1A Al4 Cs1B 4.31(3) . . ?
Cs1A Al4 Cs6 68.11(2) 2_656 . ?
Cs1A Al4 Cs6 68.11(2) . 2_656 ?
Cs1A Al4 Cs6 103.53(3) 2_656 2_656 ?
Cs1A Al4 Cs6 103.53(3) . . ?
Cs1B Al4 Cs1B 177.43(8) . 2_656 ?
Cs6 Al4 Cs1B 69.96(4) . 2_656 ?
Cs6 Al4 Cs1B 107.84(4) . . ?
Cs6 Al4 Cs1B 69.97(4) 2_656 . ?
Cs6 Al4 Cs1B 107.84(4) 2_656 2_656 ?
Cs6 Al4 Cs6 72.42(2) . 2_656 ?
F5 Al4 Cs1A 57.00(8) . 2_656 ?
F5 Al4 Cs1A 131.82(9) 2_656 2_656 ?
F5 Al4 Cs1A 57.00(8) 2_656 . ?
F5 Al4 Cs1A 131.81(9) . . ?
F5 Al4 Cs1B 127.51(9) . . ?
F5 Al4 Cs1B 127.51(9) 2_656 2_656 ?
F5 Al4 Cs1B 54.75(8) 2_656 . ?
F5 Al4 Cs1B 54.75(8) . 2_656 ?
F5 Al4 Cs6 124.59(8) . . ?
F5 Al4 Cs6 125.27(9) 2_656 . ?
F5 Al4 Cs6 125.27(9) . 2_656 ?
F5 Al4 Cs6 124.59(8) 2_656 2_656 ?
F5 Al4 F5 89.59(17) 2_656 . ?
F6 Al4 Cs1A 122.62(9) . 2_656 ?
F6 Al4 Cs1A 122.62(9) 2_656 . ?
F6 Al4 Cs1A 48.66(8) . . ?
F6 Al4 Cs1A 48.66(8) 2_656 2_656 ?
F6 Al4 Cs1B 124.80(9) 2_656 . ?
F6 Al4 Cs1B 52.96(8) 2_656 2_656 ?
F6 Al4 Cs1B 52.96(8) . . ?
F6 Al4 Cs1B 124.79(9) . 2_656 ?
F6 Al4 Cs6 55.61(8) . 2_656 ?
F6 Al4 Cs6 54.90(8) 2_656 2_656 ?
F6 Al4 Cs6 54.90(8) . . ?
F6 Al4 Cs6 55.61(8) 2_656 . ?
F6 Al4 F5 90.15(11) . 2_656 ?
F6 Al4 F5 179.00(12) . . ?
F6 Al4 F5 90.15(11) 2_656 . ?
F6 Al4 F5 179.00(12) 2_656 2_656 ?
F6 Al4 F6 90.12(16) . 2_656 ?
F7 Al4 Cs1A 59.05(9) 2_656 2_656 ?
F7 Al4 Cs1A 59.05(9) . . ?
F7 Al4 Cs1A 121.07(9) . 2_656 ?
F7 Al4 Cs1A 121.07(9) 2_656 . ?
F7 Al4 Cs1B 56.59(10) 2_656 2_656 ?
F7 Al4 Cs1B 56.59(10) . . ?
F7 Al4 Cs1B 123.44(10) . 2_656 ?
F7 Al4 Cs1B 123.44(10) 2_656 . ?
F7 Al4 Cs6 126.84(10) . . ?
F7 Al4 Cs6 54.42(9) . 2_656 ?
F7 Al4 Cs6 54.42(9) 2_656 . ?
F7 Al4 Cs6 126.84(10) 2_656 2_656 ?
F7 Al4 F5 90.10(12) . . ?
F7 Al4 F5 90.10(12) 2_656 2_656 ?
F7 Al4 F5 89.01(12) 2_656 . ?
F7 Al4 F5 89.00(12) . 2_656 ?
F7 Al4 F6 90.03(12) . 2_656 ?
F7 Al4 F6 90.86(12) . . ?
F7 Al4 F6 90.86(12) 2_656 2_656 ?
F7 Al4 F6 90.03(12) 2_656 . ?
F7 Al4 F7 178.74(19) 2_656 . ?
Cs1B F1A Cs4 175.7(7) 6_565 . ?
Cs2 F1A Cs1B 103.3(6) . 6_565 ?
Cs2 F1A Cs3 83.7(5) . 7_667 ?
Cs2 F1A Cs4 82.6(6) . 6_565 ?
Cs2 F1A Cs4 72.4(5) . . ?
Cs3 F1A Cs1B 68.1(4) 7_667 6_565 ?
Cs3 F1A Cs4 129.0(7) 7_667 6_565 ?
Cs3 F1A Cs4 110.2(7) 7_667 . ?
Cs4 F1A Cs1B 67.9(5) 6_565 6_565 ?
Cs4 F1A Cs4 111.7(5) 6_565 . ?
Al2 F1A Cs1B 97.7(9) . 6_565 ?
Al2 F1A Cs2 158.9(12) . . ?
Al2 F1A Cs3 103.3(8) . 7_667 ?
Al2 F1A Cs4 106.9(8) . 6_565 ?
Al2 F1A Cs4 86.5(8) . . ?
F1A F1A Cs1B 149.5(3) 6_565 6_565 ?
F1A F1A Cs2 82.7(5) 6_565 . ?
F1A F1A Cs3 83.1(5) 6_565 7_667 ?
F1A F1A Cs4 142.4(4) 6_565 6_565 ?
F1A F1A Cs4 30.7(3) 6_565 . ?
F1A F1A Al2 78.5(8) 6_565 . ?
F1B F1A Cs1B 159(4) . 6_565 ?
F1B F1A Cs2 83(6) . . ?
F1B F1A Cs3 133(4) . 7_667 ?
F1B F1A Cs4 24(4) . . ?
F1B F1A Cs4 93(4) . 6_565 ?
F1B F1A Al2 78(6) . . ?
F1B F1A F1A 51(4) . 6_565 ?
Cs2 F1B Cs3 76.6(7) . 7_667 ?
Cs2 F1B Cs4 81.3(8) . 6_565 ?
Cs2 F1B Cs4 81.3(8) . . ?
Cs4 F1B Cs3 113.0(5) 6_565 7_667 ?
Cs4 F1B Cs3 113.0(5) . 7_667 ?
Cs4 F1B Cs4 124.7(12) 6_565 . ?
Al2 F1B Cs2 166.2(16) . . ?
Al2 F1B Cs3 89.7(13) . 7_667 ?
Al2 F1B Cs4 104.6(8) . . ?
Al2 F1B Cs4 104.6(8) . 6_565 ?
F1A F1B Cs2 85(6) 6_565 . ?
F1A F1B Cs2 85(6) . . ?
F1A F1B Cs3 40(4) . 7_667 ?
F1A F1B Cs3 40(4) 6_565 7_667 ?
F1A F1B Cs4 76(4) 6_565 . ?
F1A F1B Cs4 76(4) . 6_565 ?
F1A F1B Cs4 152(4) . . ?
F1A F1B Cs4 152(4) 6_565 6_565 ?
F1A F1B Al2 84(7) . . ?
F1A F1B Al2 84(7) 6_565 . ?
F1A F1B F1A 78(7) 6_565 . ?
Cs1A F2A Cs1B 101.0(4) . 2_657 ?
Cs1A F2A Cs3 76.0(3) . 7_667 ?
Cs1A F2A Cs4 85.0(3) . 2_657 ?
Cs1A F2A Cs4 80.3(4) . . ?
Cs1B F2A Cs1A 0.44(9) . . ?
Cs1B F2A Cs1B 101.4(5) . 2_657 ?
Cs1B F2A Cs3 75.6(3) . 7_667 ?
Cs1B F2A Cs4 85.3(3) . 2_657 ?
Cs1B F2A Cs4 80.4(4) . . ?
Cs3 F2A Cs1B 176.6(5) 7_667 2_657 ?
Cs4 F2A Cs1B 65.4(3) 2_657 2_657 ?
Cs4 F2A Cs1B 67.1(3) . 2_657 ?
Cs4 F2A Cs3 115.6(4) 2_657 7_667 ?
Cs4 F2A Cs3 110.6(4) . 7_667 ?
Cs4 F2A Cs4 126.0(5) 2_657 . ?
Al2 F2A Cs1A 164.6(7) . . ?
Al2 F2A Cs1B 164.2(8) . . ?
Al2 F2A Cs1B 93.8(5) . 2_657 ?
Al2 F2A Cs3 89.0(6) . 7_667 ?
Al2 F2A Cs4 102.1(5) . . ?
Al2 F2A Cs4 105.1(6) . 2_657 ?
F2A F2A Cs1A 130.8(4) 2_657 . ?
F2A F2A Cs1B 131.2(4) 2_657 . ?
F2A F2A Cs1B 30.4(2) 2_657 2_657 ?
F2A F2A Cs3 152.2(3) 2_657 7_667 ?
F2A F2A Cs4 78.7(10) 2_657 2_657 ?
F2A F2A Cs4 73.0(10) 2_657 . ?
F2A F2A Al2 63.6(5) 2_657 . ?
F2A F2A F2C 108.0(11) 2_657 . ?
F2B F2A Cs1A 90.0(15) . . ?
F2B F2A Cs1B 89.9(15) . . ?
F2B F2A Cs1B 132.3(17) . 2_657 ?
F2B F2A Cs3 49.9(14) . 7_667 ?
F2B F2A Cs4 160.1(18) . . ?
F2B F2A Cs4 69.7(14) . 2_657 ?
F2B F2A Al2 82.9(17) . . ?
F2B F2A F2A 125(2) . 2_657 ?
F2B F2A F2C 20.2(13) . . ?
F2C F2A Cs1A 110.2(7) . . ?
F2C F2A Cs1B 123.5(8) . 2_657 ?
F2C F2A Cs1B 110.0(7) . . ?
F2C F2A Cs3 59.6(6) . 7_667 ?
F2C F2A Cs4 161.2(7) . . ?
F2C F2A Cs4 71.7(6) . 2_657 ?
F2C F2A Al2 63.6(6) . . ?
Cs1A F2B Cs3 82.0(3) . 7_667 ?
Cs1A F2B Cs4 86.5(3) . 2_657 ?
Cs1A F2B Cs5 108.1(3) . 1_656 ?
Cs1B F2B Cs1A 1.67(8) . . ?
Cs1B F2B Cs3 82.6(3) . 7_667 ?
Cs1B F2B Cs4 87.1(3) . 2_657 ?
Cs1B F2B Cs5 109.7(3) . 1_656 ?
Cs3 F2B Cs5 72.9(3) 7_667 1_656 ?
Cs4 F2B Cs3 138.2(4) 2_657 7_667 ?
Cs4 F2B Cs5 72.8(3) 2_657 1_656 ?
Al2 F2B Cs1A 144.2(7) . . ?
Al2 F2B Cs1B 142.5(7) . . ?
Al2 F2B Cs3 102.5(5) . 7_667 ?
Al2 F2B Cs4 110.0(5) . 2_657 ?
Al2 F2B Cs5 107.2(6) . 1_656 ?
F2A F2B Cs1A 74.5(16) . . ?
F2A F2B Cs1B 72.9(16) . . ?
F2A F2B Cs3 118.8(16) . 7_667 ?
F2A F2B Cs4 96.2(15) . 2_657 ?
F2A F2B Cs5 168.3(17) . 1_656 ?
F2A F2B Al2 72.3(13) . . ?
F2A F2B F2C 143(2) . . ?
F2C F2B Cs1A 142.4(12) . . ?
F2C F2B Cs1B 144.0(13) . . ?
F2C F2B Cs3 79.2(12) . 7_667 ?
F2C F2B Cs4 86.3(11) . 2_657 ?
F2C F2B Cs5 35.0(9) . 1_656 ?
F2C F2B Al2 72.2(10) . . ?
Cs1B F2C Cs1A 2.01(6) . . ?
Cs3 F2C Cs1A 70.4(2) 7_667 . ?
Cs3 F2C Cs1B 70.9(3) 7_667 . ?
Cs3 F2C Cs4 135.7(3) 7_667 2_657 ?
Cs4 F2C Cs1A 72.8(2) 2_657 . ?
Cs4 F2C Cs1B 73.1(3) 2_657 . ?
Cs5 F2C Cs1A 105.9(3) 1_656 . ?
Cs5 F2C Cs1B 107.9(3) 1_656 . ?
Cs5 F2C Cs3 84.7(4) 1_656 7_667 ?
Cs5 F2C Cs4 82.6(3) 1_656 2_657 ?
Al2 F2C Cs1A 106.3(6) . . ?
Al2 F2C Cs1B 104.3(6) . . ?
Al2 F2C Cs3 105.0(5) . 7_667 ?
Al2 F2C Cs4 108.2(6) . 2_657 ?
Al2 F2C Cs5 147.8(6) . 1_656 ?
F2A F2C Cs1A 45.5(5) . . ?
F2A F2C Cs1B 43.5(5) . . ?
F2A F2C Cs3 92.5(7) . 7_667 ?
F2A F2C Cs4 78.2(7) . 2_657 ?
F2A F2C Cs5 149.4(7) . 1_656 ?
F2A F2C Al2 62.1(6) . . ?
F2B F2C Cs1A 28.8(9) . . ?
F2B F2C Cs1B 26.8(9) . . ?
F2B F2C Cs3 83.0(11) . 7_667 ?
F2B F2C Cs4 76.1(10) . 2_657 ?
F2B F2C Cs5 134.0(11) . 1_656 ?
F2B F2C Al2 78.1(12) . . ?
F2B F2C F2A 16.8(10) . . ?
F2B F2C F2C 140.7(10) . 6_565 ?
F2C F2C Cs1A 148.91(19) 6_565 . ?
F2C F2C Cs1B 148.8(2) 6_565 . ?
F2C F2C Cs3 79.8(2) 6_565 7_667 ?
F2C F2C Cs4 137.9(2) 6_565 2_657 ?
F2C F2C Cs5 79.1(2) 6_565 1_656 ?
F2C F2C Al2 72.8(4) 6_565 . ?
F2C F2C F2A 130.5(5) 6_565 . ?
Cs2 F3 Cs3 73.87(7) . 3_444 ?
Cs2 F3 Cs5 150.72(13) . . ?
Cs2 F3 Cs6 86.99(6) . 8_465 ?
Cs2 F3 Cs6 86.99(6) . 3_445 ?
Cs5 F3 Cs3 76.85(8) . 3_444 ?
Cs5 F3 Cs6 89.15(6) . 3_445 ?
Cs5 F3 Cs6 89.15(6) . 8_465 ?
Cs6 F3 Cs3 82.31(6) 8_465 3_444 ?
Cs6 F3 Cs3 82.31(6) 3_445 3_444 ?
Cs6 F3 Cs6 164.51(12) 8_465 3_445 ?
Al3 F3 Cs2 104.65(15) . . ?
Al3 F3 Cs3 178.52(17) . 3_444 ?
Al3 F3 Cs5 104.62(14) . . ?
Al3 F3 Cs6 97.66(6) . 8_465 ?
Al3 F3 Cs6 97.66(6) . 3_445 ?
Cs2 F4 Cs5 104.37(8) . 5_566 ?
Cs2 F4 Cs6 165.98(9) . 7_566 ?
Cs2 F4 Cs6 82.32(7) . 8_465 ?
Cs4 F4 Cs2 80.04(7) . . ?
Cs4 F4 Cs5 78.66(7) . 5_566 ?
Cs4 F4 Cs6 90.21(7) . 7_566 ?
Cs4 F4 Cs6 89.22(7) . 8_465 ?
Cs5 F4 Cs6 83.31(7) 5_566 7_566 ?
Cs6 F4 Cs5 164.75(9) 8_465 5_566 ?
Cs6 F4 Cs6 87.54(7) 8_465 7_566 ?
Al3 F4 Cs2 93.55(11) . . ?
Al3 F4 Cs4 168.18(15) . . ?
Al3 F4 Cs5 93.50(11) . 5_566 ?
Al3 F4 Cs6 99.82(11) . 8_465 ?
Al3 F4 Cs6 97.71(11) . 7_566 ?
Cs1A F5 Cs1B 5.43(3) 2_656 2_656 ?
Cs1A F5 Cs2 105.76(8) 2_656 5_666 ?
Cs1A F5 Cs6 84.33(6) 2_656 8_465 ?
Cs1B F5 Cs2 101.04(8) 2_656 5_666 ?
Cs1B F5 Cs6 88.28(7) 2_656 8_465 ?
Cs2 F5 Cs1A 157.81(8) . 2_656 ?
Cs2 F5 Cs1B 155.68(9) . 2_656 ?
Cs2 F5 Cs2 80.13(6) . 5_666 ?
Cs2 F5 Cs6 85.67(7) . 8_465 ?
Cs3 F5 Cs1A 78.66(6) 3_444 2_656 ?
Cs3 F5 Cs1B 74.69(7) 3_444 2_656 ?
Cs3 F5 Cs2 82.11(6) 3_444 . ?
Cs3 F5 Cs2 76.52(6) 3_444 5_666 ?
Cs3 F5 Cs6 92.84(6) 3_444 8_465 ?
Cs6 F5 Cs2 163.25(8) 8_465 5_666 ?
Al4 F5 Cs1A 94.36(9) . 2_656 ?
Al4 F5 Cs1B 97.51(10) . 2_656 ?
Al4 F5 Cs2 94.44(10) . 5_666 ?
Al4 F5 Cs2 106.65(10) . . ?
Al4 F5 Cs3 166.39(14) . 3_444 ?
Al4 F5 Cs6 98.12(10) . 8_465 ?
Cs1A F6 Cs1B 4.04(6) . . ?
Cs1A F6 Cs4 76.14(6) . 8_565 ?
Cs1A F6 Cs6 87.68(6) . 7_666 ?
Cs1A F6 Cs6 88.53(7) . 2_656 ?
Cs1A F6 Cs6 159.11(8) . . ?
Cs1B F6 Cs4 80.18(7) . 8_565 ?
Cs1B F6 Cs6 88.36(8) . 7_666 ?
Cs1B F6 Cs6 163.15(9) . . ?
Cs1B F6 Cs6 88.73(8) . 2_656 ?
Cs4 F6 Cs6 82.27(5) 8_565 7_666 ?
Cs6 F6 Cs4 83.03(5) . 8_565 ?
Cs6 F6 Cs4 84.65(5) 2_656 8_565 ?
Cs6 F6 Cs6 88.00(6) . 7_666 ?
Cs6 F6 Cs6 91.11(6) . 2_656 ?
Cs6 F6 Cs6 166.90(7) 2_656 7_666 ?
Al4 F6 Cs1A 103.63(10) . . ?
Al4 F6 Cs1B 99.60(10) . . ?
Al4 F6 Cs4 178.92(12) . 8_565 ?
Al4 F6 Cs6 97.16(9) . . ?
Al4 F6 Cs6 96.67(9) . 7_666 ?
Al4 F6 Cs6 96.41(9) . 2_656 ?
Cs1A F7 Cs1B 5.33(3) . . ?
Cs1A F7 Cs2 103.64(8) . . ?
Cs1B F7 Cs2 99.20(8) . . ?
Cs4 F7 Cs1A 79.30(6) . . ?
Cs4 F7 Cs1B 75.24(7) . . ?
Cs4 F7 Cs2 77.21(6) . . ?
Cs4 F7 Cs6 92.42(7) . 2_656 ?
Cs4 F7 Cs6 89.17(7) . 8_465 ?
Cs6 F7 Cs1A 83.64(7) 2_656 . ?
Cs6 F7 Cs1A 166.42(8) 8_465 . ?
Cs6 F7 Cs1B 87.33(8) 2_656 . ?
Cs6 F7 Cs1B 164.00(9) 8_465 . ?
Cs6 F7 Cs2 80.47(6) 8_465 . ?
Cs6 F7 Cs2 165.76(8) 2_656 . ?
Cs6 F7 Cs6 89.76(7) 2_656 8_465 ?
Al4 F7 Cs1A 92.65(10) . . ?
Al4 F7 Cs1B 95.96(11) . . ?
Al4 F7 Cs2 93.97(10) . . ?
Al4 F7 Cs4 166.13(14) . . ?
Al4 F7 Cs6 100.02(10) . 8_465 ?
Al4 F7 Cs6 97.94(11) . 2_656 ?
Cs1A F8 Cs1A 82.18(7) 8_465 2_657 ?
Cs1A F8 Cs1A 158.02(9) 8_465 . ?
Cs1A F8 Cs1A 105.88(8) . 2_657 ?
Cs1A F8 Cs1B 101.36(9) . 2_657 ?
Cs1A F8 Cs1B 156.42(9) 8_465 . ?
Cs1A F8 Cs1B 4.30(5) 8_465 8_465 ?
Cs1A F8 Cs1B 85.44(8) 8_465 2_657 ?
Cs1A F8 Cs6 87.22(7) 8_465 2_656 ?
Cs1A F8 Cs6 165.86(8) 2_657 2_656 ?
Cs1A F8 Cs6 80.93(7) . 2_656 ?
Cs1B F8 Cs1A 5.33(3) . . ?
Cs1B F8 Cs1A 162.00(9) 8_465 . ?
Cs1B F8 Cs1A 81.95(8) 8_465 2_657 ?
Cs1B F8 Cs1A 5.24(3) 2_657 2_657 ?
Cs1B F8 Cs1A 101.27(9) . 2_657 ?
Cs1B F8 Cs1B 85.52(9) 8_465 2_657 ?
Cs1B F8 Cs1B 96.63(9) . 2_657 ?
Cs1B F8 Cs1B 160.68(11) 8_465 . ?
Cs1B F8 Cs6 164.64(9) 2_657 2_656 ?
Cs1B F8 Cs6 88.17(8) 8_465 2_656 ?
Cs1B F8 Cs6 84.83(8) . 2_656 ?
Cs4 F8 Cs1A 82.46(7) . 8_465 ?
Cs4 F8 Cs1A 80.96(7) . 2_657 ?
Cs4 F8 Cs1A 78.79(6) . . ?
Cs4 F8 Cs1B 77.26(7) . 2_657 ?
Cs4 F8 Cs1B 86.68(8) . 8_465 ?
Cs4 F8 Cs1B 75.16(7) . . ?
Cs4 F8 Cs6 88.41(6) . 2_656 ?
Al1 F8 Cs1A 94.32(10) . . ?
Al1 F8 Cs1A 92.64(10) . 2_657 ?
Al1 F8 Cs1A 105.87(11) . 8_465 ?
Al1 F8 Cs1B 95.71(11) . 2_657 ?
Al1 F8 Cs1B 97.32(11) . . ?
Al1 F8 Cs1B 101.58(11) . 8_465 ?
Al1 F8 Cs4 168.82(14) . . ?
Al1 F8 Cs6 99.27(10) . 2_656 ?
Cs1A F9 Cs1A 82.07(7) 2_657 8_465 ?
Cs1A F9 Cs1B 85.14(8) 2_657 8_465 ?
Cs1A F9 Cs1B 4.48(5) 2_657 2_657 ?
Cs1A F9 Cs5 157.65(9) 2_657 3_556 ?
Cs1A F9 Cs6 85.78(7) 2_657 1_556 ?
Cs1A F9 Cs6 164.81(8) 8_465 1_556 ?
Cs1B F9 Cs1A 5.23(3) 8_465 8_465 ?
Cs1B F9 Cs1A 82.01(8) 2_657 8_465 ?
Cs1B F9 Cs1B 85.41(9) 2_657 8_465 ?
Cs1B F9 Cs5 161.84(9) 2_657 3_556 ?
Cs1B F9 Cs6 163.83(9) 8_465 1_556 ?
Cs1B F9 Cs6 86.58(8) 2_657 1_556 ?
Cs4 F9 Cs1A 82.28(6) 7_567 2_657 ?
Cs4 F9 Cs1A 80.67(7) 7_567 8_465 ?
Cs4 F9 Cs1B 76.82(7) 7_567 8_465 ?
Cs4 F9 Cs1B 86.71(7) 7_567 2_657 ?
Cs4 F9 Cs5 78.00(6) 7_567 3_556 ?
Cs4 F9 Cs6 88.72(7) 7_567 1_556 ?
Cs5 F9 Cs1A 104.78(8) 3_556 8_465 ?
Cs5 F9 Cs1B 100.35(8) 3_556 8_465 ?
Cs5 F9 Cs6 83.38(6) 3_556 1_556 ?
Al1 F9 Cs1A 105.55(11) . 2_657 ?
Al1 F9 Cs1A 92.69(10) . 8_465 ?
Al1 F9 Cs1B 95.97(11) . 8_465 ?
Al1 F9 Cs1B 101.07(11) . 2_657 ?
Al1 F9 Cs4 169.05(14) . 7_567 ?
Al1 F9 Cs5 95.48(10) . 3_556 ?
Al1 F9 Cs6 99.34(11) . 1_556 ?
Cs1A F10 Cs5 104.21(8) 7_667 7_566 ?
Cs1A F10 Cs6 81.48(6) 7_667 1_556 ?
Cs1B F10 Cs1A 5.28(3) 7_667 7_667 ?
Cs1B F10 Cs5 99.59(8) 7_667 7_566 ?
Cs1B F10 Cs6 85.44(7) 7_667 1_556 ?
Cs3 F10 Cs1A 77.80(6) . 7_667 ?
Cs3 F10 Cs1B 74.06(7) . 7_667 ?
Cs3 F10 Cs5 86.69(6) . 3_556 ?
Cs3 F10 Cs5 77.73(6) . 7_566 ?
Cs3 F10 Cs6 91.96(7) . 1_556 ?
Cs5 F10 Cs1A 159.99(9) 3_556 7_667 ?
Cs5 F10 Cs1B 158.84(9) 3_556 7_667 ?
Cs5 F10 Cs5 84.45(7) 3_556 7_566 ?
Cs5 F10 Cs6 166.65(8) 7_566 1_556 ?
Cs5 F10 Cs6 86.54(7) 3_556 1_556 ?
Al1 F10 Cs1A 93.78(10) . 7_667 ?
Al1 F10 Cs1B 96.71(11) . 7_667 ?
Al1 F10 Cs3 165.74(14) . . ?
Al1 F10 Cs5 93.49(10) . 7_566 ?
Al1 F10 Cs5 103.80(11) . 3_556 ?
Al1 F10 Cs6 98.22(10) . 1_556 ?

_olex2_submission_special_instructions 'No special instructions were received'
loop_
_twin_individual_id
_twin_individual_mass_fraction_refined
1 0.9415(13)
2 0.0585(13)

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_Rb3GaF6
_database_code_depnum_ccdc_archive 'CCDC 2193515'
loop_
_audit_author_name
_audit_author_address
'Hunter B. Tisdale'
;University of South Carolina
United States of America
;
_audit_update_record             
;
2022-07-28 deposited with the CCDC.	2023-05-19 downloaded from the CCDC.
;
#==============================================================================
# CHEMICAL DATA

_chemical_name_systematic        
;
    ?
;
_chemical_name_common            Rb3GaF6
_chemical_formula_structural     'Rb3 Ga F6'
_chemical_formula_analytical     ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'F6 Ga1 Rb3'
_chemical_formula_weight         440.117
_chemical_melting_point          ?
_chemical_compound_source        ?

#==============================================================================
# CRYSTAL DATA

_space_group_crystal_system      tetragonal
_space_group_name_H-M_alt        'I 41/a Z'
_space_group_name_Hall           '-I 4ad'
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 x,y,z
2 1/2+x,y,1/2-z
3 3/4-y,1/4+x,1/4+z
4 3/4+y,3/4-x,3/4+z
5 1/2+x,1/2+y,1/2+z
6 1+x,1/2+y,1-z
7 5/4-y,3/4+x,3/4+z
8 5/4+y,5/4-x,5/4+z
9 -x,-y,-z
10 -1/2-x,-y,-1/2+z
11 -3/4+y,-1/4-x,-1/4-z
12 -3/4-y,-3/4+x,-3/4-z
13 -1/2-x,-1/2-y,-1/2-z
14 -1-x,-1/2-y,-1+z
15 -5/4+y,-3/4-x,-3/4-z
16 -5/4-y,-5/4+x,-5/4-z

_cell_length_a                   19.7947(4)
_cell_length_b                   19.7947(4)
_cell_length_c                   35.7471(8)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_volume                     14006.7(5)
_cell_formula_units_Z            80
_cell_measurement_temperature    ?
_rigaku_reference_intensity_ratio 4.79

#==============================================================================
# ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_Wyckoff_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
Rb1 Rb e 0 0.25 0.371194 0.012665 Uiso 1
Rb2 Rb f 0.898404 0.441909 0.510562 0.012665 Uiso 1
Rb3 Rb f 0.186951 0.322881 0.498693 0.012665 Uiso 1
Rb4 Rb f 0.082665 0.562619 0.371688 0.012665 Uiso 1
Rb5 Rb f 0.196966 0.325047 0.373590 0.012665 Uiso 1
Rb6 Rb e 0 0.25 0.510412 0.012665 Uiso 1
Rb7 Rb f 0.899895 0.456743 0.364969 0.012665 Uiso 1
Rb8 Rb f 0.928 0.09 0.3212 0.012665 Uiso 1
Rb9 Rb f 0.864226 0.331509 0.433565 0.012665 Uiso 1
Rb10 Rb b 0 0.25 0.625 0.012665 Uiso 1
Rb11 Rb f 0.695113 0.835993 0.742724 0.012665 Uiso 1
Rb12 Rb f 0.166455 0.683395 0.301793 0.012665 Uiso 1
Rb13 Rb f 0.736428 0.529902 0.308391 0.012665 Uiso 1
Rb14 Rb f 0.101470 0.046889 0.255106 0.012665 Uiso 1
Rb15 Rb e 0 0.25 0.997656 0.012665 Uiso 1
Rb16 Rb f 0.095040 0.053533 0.119578 0.012665 Uiso 1
Rb17 Rb a 0 0.25 0.125 0.012665 Uiso 1
Rb18 Rb f 0.070441 0.902266 0.935948 0.012665 Uiso 1
Ga1 Ga f 0.056679 0.395883 0.438881 0.012665 Uiso 1
Ga2 Ga f 0.643432 0.704929 0.807272 0.012665 Uiso 1
Ga3 Ga f 0.547268 0.896269 0.181622 0.012665 Uiso 1
Ga4 Ga f 0.257215 0.502345 0.061058 0.012665 Uiso 1
Ga5 Ga f 0.553275 0.893573 0.686577 0.012665 Uiso 1
F1 F f 0.1071 0.4247 0.4788 0.012665 Uiso 1
F2 F f 0.9833 0.3784 0.3967 0.012665 Uiso 1
F3 F f 0.7363 0.74 0.8148 0.012665 Uiso 1
F4 F f 0.5551 0.6493 0.8112 0.012665 Uiso 1
F5 F f 0.6362 0.9374 0.1814 0.012665 Uiso 1
F6 F f 0.0219 0.4921 0.4381 0.012665 Uiso 1
F7 F f 0.0982 0.3151 0.4299 0.012665 Uiso 1
F8 F f 0.6062 0.7838 0.8145 0.012665 Uiso 1
F9 F f 0.6871 0.6064 0.8127 0.012665 Uiso 1
F10 F f 0.505 0.9846 0.1863 0.012665 Uiso 1
F11 F f 0.5536 0.9122 0.2413 0.012665 Uiso 1
F12 F f 0.9809 0.3707 0.4743 0.012665 Uiso 1
F13 F f 0.1198 0.4263 0.3959 0.012665 Uiso 1
F14 F f 0.6506 0.696 0.8675 0.012665 Uiso 1
F15 F f 0.6603 0.6919 0.7582 0.012665 Uiso 1
F16 F f 0.4682 0.8479 0.1861 0.012665 Uiso 1
F17 F f 0.5977 0.8136 0.1867 0.012665 Uiso 1
F18 F f 0.5488 0.8889 0.134 0.012665 Uiso 1
F19 F f 0.2788 0.5946 0.064 0.012665 Uiso 1
F20 F f 0.1621 0.5333 0.0623 0.012665 Uiso 1
F21 F f 0.2579 0.501 0.1156 0.012665 Uiso 1
F22 F f 0.225 0.4016 0.0684 0.012665 Uiso 1
F23 F f 0.337 0.4669 0.0626 0.012665 Uiso 1
F24 F f 0.2609 0.4951 0.0092 0.012665 Uiso 1
F25 F f 0.6287 0.9555 0.6879 0.012665 Uiso 1
F26 F f 0.4958 0.982 0.6918 0.012665 Uiso 1
F27 F f 0.5616 0.9008 0.7461 0.012665 Uiso 1
F28 F f 0.4679 0.8537 0.7054 0.012665 Uiso 1
F29 F f 0.5997 0.8121 0.6869 0.012665 Uiso 1
F30 F f 0.5259 0.8938 0.636 0.012665 Uiso 1
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_Cs3AlF6_HT_CCDC1
_database_code_depnum_ccdc_archive 'CCDC 2193514'
loop_
_audit_author_name
_audit_author_address
'Hunter B. Tisdale'
;University of South Carolina
United States of America
;
_audit_update_record             
;
2023-05-17 deposited with the CCDC.	2023-05-19 downloaded from the CCDC.
;
#==============================================================================
# CHEMICAL DATA

_chemical_name_systematic        
;
    ?
;
_chemical_name_common            Fm-3m
_chemical_formula_structural     'Al Cs3 F6'
_chemical_formula_analytical     ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'Al Cs3 F6'
_chemical_formula_weight         539.688
_chemical_melting_point          ?
_chemical_compound_source        ?

#==============================================================================
# CRYSTAL DATA

_space_group_crystal_system      cubic
_space_group_name_H-M_alt        'F m -3 m'
_space_group_name_Hall           '-F 4 2 3'
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 x,y,z
2 z,x,y
3 y,z,x
4 x,z,y
5 y,x,z
6 z,y,x
7 x,-y,-z
8 z,-x,-y
9 y,-z,-x
10 x,-z,-y
11 y,-x,-z
12 z,-y,-x
13 -x,y,-z
14 -z,x,-y
15 -y,z,-x
16 -x,z,-y
17 -y,x,-z
18 -z,y,-x
19 -x,-y,z
20 -z,-x,y
21 -y,-z,x
22 -x,-z,y
23 -y,-x,z
24 -z,-y,x
25 x,1/2+y,1/2+z
26 z,1/2+x,1/2+y
27 y,1/2+z,1/2+x
28 x,1/2+z,1/2+y
29 y,1/2+x,1/2+z
30 z,1/2+y,1/2+x
31 x,1/2-y,1/2-z
32 z,1/2-x,1/2-y
33 y,1/2-z,1/2-x
34 x,1/2-z,1/2-y
35 y,1/2-x,1/2-z
36 z,1/2-y,1/2-x
37 -x,1/2+y,1/2-z
38 -z,1/2+x,1/2-y
39 -y,1/2+z,1/2-x
40 -x,1/2+z,1/2-y
41 -y,1/2+x,1/2-z
42 -z,1/2+y,1/2-x
43 -x,1/2-y,1/2+z
44 -z,1/2-x,1/2+y
45 -y,1/2-z,1/2+x
46 -x,1/2-z,1/2+y
47 -y,1/2-x,1/2+z
48 -z,1/2-y,1/2+x
49 1/2+x,1/2+y,z
50 1/2+z,1/2+x,y
51 1/2+y,1/2+z,x
52 1/2+x,1/2+z,y
53 1/2+y,1/2+x,z
54 1/2+z,1/2+y,x
55 1/2+x,1/2-y,-z
56 1/2+z,1/2-x,-y
57 1/2+y,1/2-z,-x
58 1/2+x,1/2-z,-y
59 1/2+y,1/2-x,-z
60 1/2+z,1/2-y,-x
61 1/2-x,1/2+y,-z
62 1/2-z,1/2+x,-y
63 1/2-y,1/2+z,-x
64 1/2-x,1/2+z,-y
65 1/2-y,1/2+x,-z
66 1/2-z,1/2+y,-x
67 1/2-x,1/2-y,z
68 1/2-z,1/2-x,y
69 1/2-y,1/2-z,x
70 1/2-x,1/2-z,y
71 1/2-y,1/2-x,z
72 1/2-z,1/2-y,x
73 1/2+x,y,1/2+z
74 1/2+z,x,1/2+y
75 1/2+y,z,1/2+x
76 1/2+x,z,1/2+y
77 1/2+y,x,1/2+z
78 1/2+z,y,1/2+x
79 1/2+x,-y,1/2-z
80 1/2+z,-x,1/2-y
81 1/2+y,-z,1/2-x
82 1/2+x,-z,1/2-y
83 1/2+y,-x,1/2-z
84 1/2+z,-y,1/2-x
85 1/2-x,y,1/2-z
86 1/2-z,x,1/2-y
87 1/2-y,z,1/2-x
88 1/2-x,z,1/2-y
89 1/2-y,x,1/2-z
90 1/2-z,y,1/2-x
91 1/2-x,-y,1/2+z
92 1/2-z,-x,1/2+y
93 1/2-y,-z,1/2+x
94 1/2-x,-z,1/2+y
95 1/2-y,-x,1/2+z
96 1/2-z,-y,1/2+x
97 -x,-y,-z
98 -z,-x,-y
99 -y,-z,-x
100 -x,-z,-y
101 -y,-x,-z
102 -z,-y,-x
103 -x,y,z
104 -z,x,y
105 -y,z,x
106 -x,z,y
107 -y,x,z
108 -z,y,x
109 x,-y,z
110 z,-x,y
111 y,-z,x
112 x,-z,y
113 y,-x,z
114 z,-y,x
115 x,y,-z
116 z,x,-y
117 y,z,-x
118 x,z,-y
119 y,x,-z
120 z,y,-x
121 -x,-1/2-y,-1/2-z
122 -z,-1/2-x,-1/2-y
123 -y,-1/2-z,-1/2-x
124 -x,-1/2-z,-1/2-y
125 -y,-1/2-x,-1/2-z
126 -z,-1/2-y,-1/2-x
127 -x,-1/2+y,-1/2+z
128 -z,-1/2+x,-1/2+y
129 -y,-1/2+z,-1/2+x
130 -x,-1/2+z,-1/2+y
131 -y,-1/2+x,-1/2+z
132 -z,-1/2+y,-1/2+x
133 x,-1/2-y,-1/2+z
134 z,-1/2-x,-1/2+y
135 y,-1/2-z,-1/2+x
136 x,-1/2-z,-1/2+y
137 y,-1/2-x,-1/2+z
138 z,-1/2-y,-1/2+x
139 x,-1/2+y,-1/2-z
140 z,-1/2+x,-1/2-y
141 y,-1/2+z,-1/2-x
142 x,-1/2+z,-1/2-y
143 y,-1/2+x,-1/2-z
144 z,-1/2+y,-1/2-x
145 -1/2-x,-1/2-y,-z
146 -1/2-z,-1/2-x,-y
147 -1/2-y,-1/2-z,-x
148 -1/2-x,-1/2-z,-y
149 -1/2-y,-1/2-x,-z
150 -1/2-z,-1/2-y,-x
151 -1/2-x,-1/2+y,z
152 -1/2-z,-1/2+x,y
153 -1/2-y,-1/2+z,x
154 -1/2-x,-1/2+z,y
155 -1/2-y,-1/2+x,z
156 -1/2-z,-1/2+y,x
157 -1/2+x,-1/2-y,z
158 -1/2+z,-1/2-x,y
159 -1/2+y,-1/2-z,x
160 -1/2+x,-1/2-z,y
161 -1/2+y,-1/2-x,z
162 -1/2+z,-1/2-y,x
163 -1/2+x,-1/2+y,-z
164 -1/2+z,-1/2+x,-y
165 -1/2+y,-1/2+z,-x
166 -1/2+x,-1/2+z,-y
167 -1/2+y,-1/2+x,-z
168 -1/2+z,-1/2+y,-x
169 -1/2-x,-y,-1/2-z
170 -1/2-z,-x,-1/2-y
171 -1/2-y,-z,-1/2-x
172 -1/2-x,-z,-1/2-y
173 -1/2-y,-x,-1/2-z
174 -1/2-z,-y,-1/2-x
175 -1/2-x,y,-1/2+z
176 -1/2-z,x,-1/2+y
177 -1/2-y,z,-1/2+x
178 -1/2-x,z,-1/2+y
179 -1/2-y,x,-1/2+z
180 -1/2-z,y,-1/2+x
181 -1/2+x,-y,-1/2+z
182 -1/2+z,-x,-1/2+y
183 -1/2+y,-z,-1/2+x
184 -1/2+x,-z,-1/2+y
185 -1/2+y,-x,-1/2+z
186 -1/2+z,-y,-1/2+x
187 -1/2+x,y,-1/2-z
188 -1/2+z,x,-1/2-y
189 -1/2+y,z,-1/2-x
190 -1/2+x,z,-1/2-y
191 -1/2+y,x,-1/2-z
192 -1/2+z,y,-1/2-x

_cell_length_a                   9.3232(2)
_cell_length_b                   9.3232(2)
_cell_length_c                   9.3232(2)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_volume                     810.40(4)
_cell_formula_units_Z            4
_cell_measurement_temperature    ?
_rigaku_reference_intensity_ratio 10.05

#==============================================================================
# ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_Wyckoff_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
Cs1 Cs c 0.75 0.75 0.75 0.0553(6) Uiso 1
Cs2 Cs a 0 0.5 0.5 0.0567(9) Uiso 1
Al1 Al b 0.5 0.5 0.5 0.038(3) Uiso 1
F1 F e 0.6933(8) 0.5 0.5 0.081(3) Uiso 1
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_Cs3GaF6_HT
_database_code_depnum_ccdc_archive 'CCDC 2193516'
loop_
_audit_author_name
_audit_author_address
'Hunter B. Tisdale'
;University of South Carolina
United States of America
;
_audit_update_record             
;
2023-05-17 deposited with the CCDC.	2023-05-19 downloaded from the CCDC.
;
#==============================================================================
# CHEMICAL DATA

_chemical_name_systematic        
;
    ?
;
_chemical_name_common            Fm-3m
_chemical_formula_structural     'Ga Cs3 F6'
_chemical_formula_analytical     ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'Ga Cs3 F6'
_chemical_formula_weight         582.43
_chemical_melting_point          ?
_chemical_compound_source        ?

#==============================================================================
# CRYSTAL DATA

_space_group_crystal_system      cubic
_space_group_name_H-M_alt        'F m -3 m'
_space_group_name_Hall           '-F 4 2 3'
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 x,y,z
2 z,x,y
3 y,z,x
4 x,z,y
5 y,x,z
6 z,y,x
7 x,-y,-z
8 z,-x,-y
9 y,-z,-x
10 x,-z,-y
11 y,-x,-z
12 z,-y,-x
13 -x,y,-z
14 -z,x,-y
15 -y,z,-x
16 -x,z,-y
17 -y,x,-z
18 -z,y,-x
19 -x,-y,z
20 -z,-x,y
21 -y,-z,x
22 -x,-z,y
23 -y,-x,z
24 -z,-y,x
25 x,1/2+y,1/2+z
26 z,1/2+x,1/2+y
27 y,1/2+z,1/2+x
28 x,1/2+z,1/2+y
29 y,1/2+x,1/2+z
30 z,1/2+y,1/2+x
31 x,1/2-y,1/2-z
32 z,1/2-x,1/2-y
33 y,1/2-z,1/2-x
34 x,1/2-z,1/2-y
35 y,1/2-x,1/2-z
36 z,1/2-y,1/2-x
37 -x,1/2+y,1/2-z
38 -z,1/2+x,1/2-y
39 -y,1/2+z,1/2-x
40 -x,1/2+z,1/2-y
41 -y,1/2+x,1/2-z
42 -z,1/2+y,1/2-x
43 -x,1/2-y,1/2+z
44 -z,1/2-x,1/2+y
45 -y,1/2-z,1/2+x
46 -x,1/2-z,1/2+y
47 -y,1/2-x,1/2+z
48 -z,1/2-y,1/2+x
49 1/2+x,1/2+y,z
50 1/2+z,1/2+x,y
51 1/2+y,1/2+z,x
52 1/2+x,1/2+z,y
53 1/2+y,1/2+x,z
54 1/2+z,1/2+y,x
55 1/2+x,1/2-y,-z
56 1/2+z,1/2-x,-y
57 1/2+y,1/2-z,-x
58 1/2+x,1/2-z,-y
59 1/2+y,1/2-x,-z
60 1/2+z,1/2-y,-x
61 1/2-x,1/2+y,-z
62 1/2-z,1/2+x,-y
63 1/2-y,1/2+z,-x
64 1/2-x,1/2+z,-y
65 1/2-y,1/2+x,-z
66 1/2-z,1/2+y,-x
67 1/2-x,1/2-y,z
68 1/2-z,1/2-x,y
69 1/2-y,1/2-z,x
70 1/2-x,1/2-z,y
71 1/2-y,1/2-x,z
72 1/2-z,1/2-y,x
73 1/2+x,y,1/2+z
74 1/2+z,x,1/2+y
75 1/2+y,z,1/2+x
76 1/2+x,z,1/2+y
77 1/2+y,x,1/2+z
78 1/2+z,y,1/2+x
79 1/2+x,-y,1/2-z
80 1/2+z,-x,1/2-y
81 1/2+y,-z,1/2-x
82 1/2+x,-z,1/2-y
83 1/2+y,-x,1/2-z
84 1/2+z,-y,1/2-x
85 1/2-x,y,1/2-z
86 1/2-z,x,1/2-y
87 1/2-y,z,1/2-x
88 1/2-x,z,1/2-y
89 1/2-y,x,1/2-z
90 1/2-z,y,1/2-x
91 1/2-x,-y,1/2+z
92 1/2-z,-x,1/2+y
93 1/2-y,-z,1/2+x
94 1/2-x,-z,1/2+y
95 1/2-y,-x,1/2+z
96 1/2-z,-y,1/2+x
97 -x,-y,-z
98 -z,-x,-y
99 -y,-z,-x
100 -x,-z,-y
101 -y,-x,-z
102 -z,-y,-x
103 -x,y,z
104 -z,x,y
105 -y,z,x
106 -x,z,y
107 -y,x,z
108 -z,y,x
109 x,-y,z
110 z,-x,y
111 y,-z,x
112 x,-z,y
113 y,-x,z
114 z,-y,x
115 x,y,-z
116 z,x,-y
117 y,z,-x
118 x,z,-y
119 y,x,-z
120 z,y,-x
121 -x,-1/2-y,-1/2-z
122 -z,-1/2-x,-1/2-y
123 -y,-1/2-z,-1/2-x
124 -x,-1/2-z,-1/2-y
125 -y,-1/2-x,-1/2-z
126 -z,-1/2-y,-1/2-x
127 -x,-1/2+y,-1/2+z
128 -z,-1/2+x,-1/2+y
129 -y,-1/2+z,-1/2+x
130 -x,-1/2+z,-1/2+y
131 -y,-1/2+x,-1/2+z
132 -z,-1/2+y,-1/2+x
133 x,-1/2-y,-1/2+z
134 z,-1/2-x,-1/2+y
135 y,-1/2-z,-1/2+x
136 x,-1/2-z,-1/2+y
137 y,-1/2-x,-1/2+z
138 z,-1/2-y,-1/2+x
139 x,-1/2+y,-1/2-z
140 z,-1/2+x,-1/2-y
141 y,-1/2+z,-1/2-x
142 x,-1/2+z,-1/2-y
143 y,-1/2+x,-1/2-z
144 z,-1/2+y,-1/2-x
145 -1/2-x,-1/2-y,-z
146 -1/2-z,-1/2-x,-y
147 -1/2-y,-1/2-z,-x
148 -1/2-x,-1/2-z,-y
149 -1/2-y,-1/2-x,-z
150 -1/2-z,-1/2-y,-x
151 -1/2-x,-1/2+y,z
152 -1/2-z,-1/2+x,y
153 -1/2-y,-1/2+z,x
154 -1/2-x,-1/2+z,y
155 -1/2-y,-1/2+x,z
156 -1/2-z,-1/2+y,x
157 -1/2+x,-1/2-y,z
158 -1/2+z,-1/2-x,y
159 -1/2+y,-1/2-z,x
160 -1/2+x,-1/2-z,y
161 -1/2+y,-1/2-x,z
162 -1/2+z,-1/2-y,x
163 -1/2+x,-1/2+y,-z
164 -1/2+z,-1/2+x,-y
165 -1/2+y,-1/2+z,-x
166 -1/2+x,-1/2+z,-y
167 -1/2+y,-1/2+x,-z
168 -1/2+z,-1/2+y,-x
169 -1/2-x,-y,-1/2-z
170 -1/2-z,-x,-1/2-y
171 -1/2-y,-z,-1/2-x
172 -1/2-x,-z,-1/2-y
173 -1/2-y,-x,-1/2-z
174 -1/2-z,-y,-1/2-x
175 -1/2-x,y,-1/2+z
176 -1/2-z,x,-1/2+y
177 -1/2-y,z,-1/2+x
178 -1/2-x,z,-1/2+y
179 -1/2-y,x,-1/2+z
180 -1/2-z,y,-1/2+x
181 -1/2+x,-y,-1/2+z
182 -1/2+z,-x,-1/2+y
183 -1/2+y,-z,-1/2+x
184 -1/2+x,-z,-1/2+y
185 -1/2+y,-x,-1/2+z
186 -1/2+z,-y,-1/2+x
187 -1/2+x,y,-1/2-z
188 -1/2+z,x,-1/2-y
189 -1/2+y,z,-1/2-x
190 -1/2+x,z,-1/2-y
191 -1/2+y,x,-1/2-z
192 -1/2+z,y,-1/2-x

_cell_length_a                   9.4478(3)
_cell_length_b                   9.4478(3)
_cell_length_c                   9.4478(3)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_volume                     843.32(5)
_cell_formula_units_Z            4
_cell_measurement_temperature    ?
_rigaku_reference_intensity_ratio 11.01

#==============================================================================
# ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_Wyckoff_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
Cs1 Cs c 0.75 0.75 0.75 0.0657(9) Uiso 1
Cs2 Cs a 0 0.5 0.5 0.0668(12) Uiso 1
Ga1 Ga b 0.5 0.5 0.5 0.057(2) Uiso 1
F1 F e 0.7035(10) 0.5 0.5 0.136(4) Uiso 1
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_Cs3GaF6_C2_m_MDS
_database_code_depnum_ccdc_archive 'CCDC 2239383'
loop_
_audit_author_name
_audit_author_address
'Mark D. Smith'
;University of South Carolina
United States of America
;
_audit_update_record             
;
2023-02-01 deposited with the CCDC.	2023-05-19 downloaded from the CCDC.
;
_audit_creation_date             2023-02-01
_audit_creation_method           
;
Olex2 1.2
(compiled May 18 2018 14:05:52 for OlexSys, GUI svn.r5506)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         '0.08(Cs36 F72 Ga12)'
_chemical_formula_sum            'Cs3 F6 Ga'
_chemical_formula_weight         582.45
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ga Ga 0.2307 1.6083 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cs Cs -0.3680 2.1192 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           12
_space_group_name_H-M_alt        'C 1 2/m 1'
_space_group_name_Hall           '-C 2y'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z'
'-x, -y, -z'
'x, -y, z'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z'

_cell_length_a                   11.396(6)
_cell_length_b                   19.760(11)
_cell_length_c                   11.453(6)
_cell_angle_alpha                90
_cell_angle_beta                 109.72(2)
_cell_angle_gamma                90
_cell_volume                     2428(2)
_cell_formula_units_Z            12
_cell_measurement_reflns_used    9799
_cell_measurement_temperature    301(2)
_cell_measurement_theta_min      3.623
_cell_measurement_theta_max      32.543
_shelx_estimated_absorpt_T_max   0.731
_shelx_estimated_absorpt_T_min   0.433
_exptl_absorpt_coefficient_mu    16.730
_exptl_absorpt_correction_T_min  0.1852
_exptl_absorpt_correction_T_max  0.2686
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
; 
Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D., 
 J. Appl. Cryst. 48 (2015) 3-10. 
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    4.780
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       irregular
_exptl_crystal_F_000             3000
_exptl_crystal_size_max          0.06
_exptl_crystal_size_mid          0.03
_exptl_crystal_size_min          0.02
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0487
_diffrn_reflns_av_unetI/netI     0.0146
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 1.000
_diffrn_reflns_limit_h_max       16
_diffrn_reflns_limit_h_min       -16
_diffrn_reflns_limit_k_max       27
_diffrn_reflns_limit_k_min       -27
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       -16
_diffrn_reflns_number            82746
_diffrn_reflns_point_group_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 1.000
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         30.027
_diffrn_reflns_theta_min         1.889
_diffrn_ambient_temperature      301(2)
_diffrn_detector_area_resol_mean 7.39
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type  'Bruker D8 QUEST'
_diffrn_measurement_method       'ω and φ scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   'microfocus sealed X-ray tube'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                3270
_reflns_number_total             3663
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences. Completness statistics refer to single and
 composite reflections containing twin component 1 only.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_data_collection       'Bruker APEX3 v2019.1-0 (Bruker, 2019)'
_computing_cell_refinement       'SAINT+ Ver. 8.40B (Bruker, 2019)'
_computing_data_reduction        'SAINT+ Ver. 8.40B (Bruker, 2019)'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    'XT (Sheldrick, 2015)'
_refine_diff_density_max         3.399
_refine_diff_density_min         -2.781
_refine_diff_density_rms         0.214
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.154
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     158
_refine_ls_number_reflns         3663
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0337
_refine_ls_R_factor_gt           0.0278
_refine_ls_restrained_S_all      1.154
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0238P)²+33.5978P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0629
_refine_ls_wR_factor_ref         0.0675
_refine_special_details          
;
 Refined as a 2-component twin.
;
_olex2_refinement_description    
;
1. Twinned data refinement
 Scales: 0.9160(18)
 0.0840(18)
2. Others
 Fixed Sof: F1A(0.25) F1B(0.25) F2A(0.25) F2B(0.25) F2C(0.25) F2D(0.25)
;
_atom_sites_solution_hydrogens   .
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Cs1 Cs 0.13714(4) 0.81334(2) 0.85662(4) 0.03316(9) Uani 1 1 d . . . . .
Cs2 Cs 0.14571(5) 1.000000 0.43087(5) 0.02771(11) Uani 1 2 d S T P . .
Cs3 Cs 0.20565(5) 1.000000 0.79001(5) 0.02740(11) Uani 1 2 d S T P . .
Cs4 Cs 0.21569(3) 0.85695(2) 0.22020(3) 0.02790(9) Uani 1 1 d . . . . .
Cs5 Cs 0.41717(6) 1.000000 0.14297(5) 0.03230(12) Uani 1 2 d S T P . .
Cs6 Cs 0.12621(3) 0.66799(2) 0.37980(4) 0.02995(9) Uani 1 1 d . . . . .
Ga1 Ga 0.000000 0.66579(4) 0.000000 0.01551(13) Uani 1 2 d S T P . .
Ga2 Ga 0.000000 1.000000 0.000000 0.01707(19) Uani 1 4 d S T P . .
Ga3 Ga 0.500000 1.000000 0.500000 0.01703(19) Uani 1 4 d S T P . .
Ga4 Ga 0.000000 0.82667(4) 0.500000 0.01636(14) Uani 1 2 d S T P . .
F1A F 0.0356(16) 0.9768(9) 0.1685(15) 0.037(4) Uiso 0.25 1 d . . . . .
F1B F 0.0771(14) 0.9922(16) 0.1737(13) 0.041(4) Uiso 0.25 1 d . . . . .
F2A F 0.038(2) 0.9114(10) -0.0348(18) 0.051(4) Uiso 0.25 1 d . . . . .
F2B F 0.0885(17) 0.9269(8) -0.0322(14) 0.031(3) Uiso 0.25 1 d . . . . .
F2C F 0.1393(16) 0.9450(9) 0.0000(16) 0.035(3) Uiso 0.25 1 d . . . . .
F2D F 0.1666(16) 0.9773(9) 0.0333(17) 0.048(4) Uiso 0.25 1 d . . . . .
F3 F 0.3998(5) 1.000000 0.6049(5) 0.0344(11) Uani 1 2 d S T P . .
F4 F 0.3970(4) 0.9330(2) 0.4005(4) 0.0453(10) Uani 1 1 d . . . . .
F5 F 0.1002(4) 0.89541(18) 0.6039(3) 0.0336(8) Uani 1 1 d . . . . .
F6 F 0.1023(3) 0.75863(17) 0.6022(3) 0.0309(7) Uani 1 1 d . . . . .
F7 F 0.1026(3) 0.8278(2) 0.4013(4) 0.0350(8) Uani 1 1 d . . . . .
F8 F 0.1000(3) 0.73415(19) 0.1011(4) 0.0371(8) Uani 1 1 d . . . . .
F9 F -0.1016(4) 0.6648(2) 0.1005(4) 0.0371(8) Uani 1 1 d . . . . .
F10 F 0.1029(3) 0.59859(19) 0.1012(4) 0.0375(8) Uani 1 1 d . . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Cs1 Cs3 3.898(2) . ?
Cs1 Cs4 3.9884(17) 7_566 ?
Cs1 Cs4 3.911(2) 2_556 ?
Cs1 Ga1 3.922(2) 7_566 ?
Cs1 Ga1 3.9208(15) 1_556 ?
Cs1 Ga4 3.858(2) . ?
Cs1 F1A 3.743(17) 2_556 ?
Cs1 F2A 2.745(18) 1_556 ?
Cs1 F2B 2.728(16) 1_556 ?
Cs1 F2C 3.072(18) 1_556 ?
Cs1 F2D 3.774(18) 1_556 ?
Cs1 F5 3.219(4) . ?
Cs1 F6 3.006(4) . ?
Cs1 F7 3.290(4) 2_556 ?
Cs1 F8 3.297(4) 2_556 ?
Cs1 F8 3.019(4) 7_566 ?
Cs1 F8 3.357(4) 1_556 ?
Cs1 F9 3.353(5) 8_566 ?
Cs1 F9 3.025(4) 2_556 ?
Cs1 F10 3.327(4) 7_566 ?
Cs2 Cs3 3.949(2) 5_576 ?
Cs2 Cs3 3.936(2) . ?
Cs2 Cs4 3.9681(15) . ?
Cs2 Cs4 3.9681(15) 6_575 ?
Cs2 Ga3 3.843(2) . ?
Cs2 Ga4 4.0004(18) . ?
Cs2 Ga4 4.0004(18) 5_576 ?
Cs2 F1A 2.875(17) 6_575 ?
Cs2 F1A 2.875(17) . ?
Cs2 F1B 2.785(14) . ?
Cs2 F1B 2.785(14) 6_575 ?
Cs2 F3 2.909(5) . ?
Cs2 F4 3.278(5) 6_575 ?
Cs2 F4 3.278(5) . ?
Cs2 F5 3.027(4) 6_575 ?
Cs2 F5 3.027(4) . ?
Cs2 F5 3.396(4) 5_576 ?
Cs2 F5 3.396(4) 2_556 ?
Cs2 F7 3.438(4) 6_575 ?
Cs2 F7 3.438(4) . ?
Cs3 Ga2 3.8834(16) 1_556 ?
Cs3 F1A 2.980(17) 2_556 ?
Cs3 F1A 2.980(17) 5_576 ?
Cs3 F1B 3.389(15) 5_576 ?
Cs3 F1B 3.389(15) 2_556 ?
Cs3 F2A 3.65(2) 6_576 ?
Cs3 F2A 3.65(2) 1_556 ?
Cs3 F2B 3.138(17) 6_576 ?
Cs3 F2B 3.138(17) 1_556 ?
Cs3 F2C 2.961(16) 1_556 ?
Cs3 F2C 2.961(16) 6_576 ?
Cs3 F2D 3.000(18) 1_556 ?
Cs3 F2D 3.000(18) 6_576 ?
Cs3 F3 3.543(5) . ?
Cs3 F5 2.921(3) 6_575 ?
Cs3 F5 2.920(3) . ?
Cs3 F10 2.876(4) 4_556 ?
Cs3 F10 2.876(4) 7_566 ?
Cs4 Cs5 3.9263(15) . ?
Cs4 Ga2 4.0260(15) . ?
Cs4 F1A 3.058(17) . ?
Cs4 F1B 3.06(3) . ?
Cs4 F1B 3.33(3) 6_575 ?
Cs4 F2A 3.13(2) . ?
Cs4 F2A 3.14(2) 2 ?
Cs4 F2B 3.678(19) 2 ?
Cs4 F2B 3.089(15) . ?
Cs4 F2C 2.943(16) . ?
Cs4 F2D 3.121(17) . ?
Cs4 F4 2.813(4) . ?
Cs4 F6 3.287(3) 7_566 ?
Cs4 F7 2.846(3) . ?
Cs4 F8 2.877(4) . ?
Cs4 F9 2.885(3) 8_565 ?
Cs5 Ga1 3.9176(17) 7_565 ?
Cs5 Ga1 3.9176(17) 3 ?
Cs5 Ga3 3.874(2) . ?
Cs5 F2C 3.224(19) 6_575 ?
Cs5 F2C 3.224(19) . ?
Cs5 F2D 2.740(18) . ?
Cs5 F2D 2.740(18) 6_575 ?
Cs5 F3 2.937(5) 5_676 ?
Cs5 F4 3.311(5) . ?
Cs5 F4 3.311(5) 6_575 ?
Cs5 F9 3.289(4) 8_565 ?
Cs5 F9 3.289(4) 3 ?
Cs5 F10 3.031(4) 8_565 ?
Cs5 F10 3.351(4) 7_565 ?
Cs5 F10 3.351(4) 4 ?
Cs5 F10 3.031(4) 3 ?
Cs6 Ga1 4.095(2) . ?
Cs6 Ga3 4.0398(16) 3_445 ?
Cs6 Ga4 3.8899(16) . ?
Cs6 Ga4 4.012(2) 7_566 ?
Cs6 F3 3.3426(19) 7_566 ?
Cs6 F4 3.359(5) 8_465 ?
Cs6 F4 3.292(5) 7_566 ?
Cs6 F5 3.306(4) 7_566 ?
Cs6 F6 3.359(4) 7_566 ?
Cs6 F6 3.200(4) . ?
Cs6 F6 3.224(4) 2_556 ?
Cs6 F7 3.186(4) . ?
Cs6 F7 3.258(4) 7_566 ?
Cs6 F8 3.368(5) . ?
Cs6 F9 3.372(5) . ?
Cs6 F10 3.401(4) . ?
Ga1 F8 1.890(3) . ?
Ga1 F8 1.890(3) 2 ?
Ga1 F9 1.889(3) 2 ?
Ga1 F9 1.889(3) . ?
Ga1 F10 1.888(3) 2 ?
Ga1 F10 1.888(3) . ?
Ga2 F2A 1.877(19) 5_575 ?
Ga2 F2A 1.877(19) 2 ?
Ga2 F2A 1.877(19) 6_575 ?
Ga2 F2A 1.877(19) . ?
Ga2 F2B 1.868(15) 6_575 ?
Ga2 F2B 1.868(15) 5_575 ?
Ga2 F2B 1.868(15) 2 ?
Ga2 F2B 1.868(15) . ?
Ga2 F2D 1.861(17) 6_575 ?
Ga2 F2D 1.861(17) . ?
Ga2 F2D 1.861(17) 2 ?
Ga2 F2D 1.861(17) 5_575 ?
Ga3 F3 1.917(5) 5_676 ?
Ga3 F3 1.917(5) . ?
Ga3 F4 1.877(4) 5_676 ?
Ga3 F4 1.877(4) . ?
Ga3 F4 1.877(4) 6_575 ?
Ga3 F4 1.877(4) 2_656 ?
Ga4 F5 1.910(3) . ?
Ga4 F5 1.910(3) 2_556 ?
Ga4 F6 1.902(3) . ?
Ga4 F6 1.902(3) 2_556 ?
Ga4 F7 1.881(3) . ?
Ga4 F7 1.881(3) 2_556 ?
F1A F1A 0.92(3) 6_575 ?
F1A F1B 0.76(3) 6_575 ?
F1A F1B 0.55(2) . ?
F1B F1B 0.31(6) 6_575 ?
F2A F2A 1.35(4) 2 ?
F2A F2B 0.65(2) . ?
F2A F2C 1.28(3) . ?
F2B F2C 0.674(19) . ?
F2B F2D 1.38(2) . ?
F2C F2D 1.59(3) 6_575 ?
F2C F2D 0.76(2) . ?
F2D F2D 0.90(3) 6_575 ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Cs3 Cs1 Cs4 90.35(2) . 2_556 ?
Cs3 Cs1 Cs4 128.92(3) . 7_566 ?
Cs3 Cs1 Ga1 74.334(17) . 7_566 ?
Cs3 Cs1 Ga1 156.927(18) . 1_556 ?
Cs4 Cs1 Cs4 127.823(16) 2_556 7_566 ?
Cs4 Cs1 Ga1 158.38(2) 2_556 7_566 ?
Cs4 Cs1 Ga1 74.53(3) 2_556 1_556 ?
Ga1 Cs1 Cs4 73.84(4) 1_556 7_566 ?
Ga1 Cs1 Cs4 73.66(3) 7_566 7_566 ?
Ga1 Cs1 Ga1 114.57(2) 1_556 7_566 ?
Ga4 Cs1 Cs3 76.386(17) . . ?
Ga4 Cs1 Cs4 82.78(2) . 7_566 ?
Ga4 Cs1 Cs4 74.24(2) . 2_556 ?
Ga4 Cs1 Ga1 114.70(2) . 1_556 ?
Ga4 Cs1 Ga1 115.42(2) . 7_566 ?
F1A Cs1 Cs3 45.8(3) 2_556 . ?
F1A Cs1 Cs4 163.9(3) 2_556 7_566 ?
F1A Cs1 Cs4 47.0(3) 2_556 2_556 ?
F1A Cs1 Ga1 113.6(3) 2_556 1_556 ?
F1A Cs1 Ga1 113.2(3) 2_556 7_566 ?
F1A Cs1 Ga4 81.1(3) 2_556 . ?
F1A Cs1 F2D 41.4(4) 2_556 1_556 ?
F2A Cs1 Cs3 64.0(4) 1_556 . ?
F2A Cs1 Cs4 52.8(5) 1_556 2_556 ?
F2A Cs1 Cs4 164.6(4) 1_556 7_566 ?
F2A Cs1 Ga1 105.9(5) 1_556 7_566 ?
F2A Cs1 Ga1 92.9(4) 1_556 1_556 ?
F2A Cs1 Ga4 110.5(4) 1_556 . ?
F2A Cs1 F1A 30.6(5) 1_556 2_556 ?
F2A Cs1 F2C 24.5(5) 1_556 1_556 ?
F2A Cs1 F2D 29.2(5) 1_556 1_556 ?
F2A Cs1 F5 95.9(4) 1_556 . ?
F2A Cs1 F6 138.9(4) 1_556 . ?
F2A Cs1 F7 90.0(4) 1_556 2_556 ?
F2A Cs1 F8 133.3(5) 1_556 7_566 ?
F2A Cs1 F8 76.3(4) 1_556 1_556 ?
F2A Cs1 F8 77.5(5) 1_556 2_556 ?
F2A Cs1 F9 85.3(5) 1_556 8_566 ?
F2A Cs1 F9 120.9(4) 1_556 2_556 ?
F2A Cs1 F10 92.8(5) 1_556 7_566 ?
F2B Cs1 Cs3 53.0(4) 1_556 . ?
F2B Cs1 Cs4 164.6(4) 1_556 7_566 ?
F2B Cs1 Cs4 64.4(4) 1_556 2_556 ?
F2B Cs1 Ga1 104.1(4) 1_556 1_556 ?
F2B Cs1 Ga1 94.0(4) 1_556 7_566 ?
F2B Cs1 Ga4 111.4(3) 1_556 . ?
F2B Cs1 F1A 30.9(4) 1_556 2_556 ?
F2B Cs1 F2A 13.6(4) 1_556 1_556 ?
F2B Cs1 F2C 11.5(4) 1_556 1_556 ?
F2B Cs1 F2D 16.0(5) 1_556 1_556 ?
F2B Cs1 F5 91.1(3) 1_556 . ?
F2B Cs1 F6 140.1(3) 1_556 . ?
F2B Cs1 F7 96.3(4) 1_556 2_556 ?
F2B Cs1 F8 90.9(4) 1_556 2_556 ?
F2B Cs1 F8 121.9(4) 1_556 7_566 ?
F2B Cs1 F8 83.8(3) 1_556 1_556 ?
F2B Cs1 F9 76.6(4) 1_556 8_566 ?
F2B Cs1 F9 131.5(4) 1_556 2_556 ?
F2B Cs1 F10 79.2(4) 1_556 7_566 ?
F2C Cs1 Cs3 48.5(3) 1_556 . ?
F2C Cs1 Cs4 75.9(3) 1_556 2_556 ?
F2C Cs1 Cs4 154.7(3) 1_556 7_566 ?
F2C Cs1 Ga1 82.5(3) 1_556 7_566 ?
F2C Cs1 Ga1 109.8(3) 1_556 1_556 ?
F2C Cs1 Ga4 115.8(3) 1_556 . ?
F2C Cs1 F1A 38.7(4) 1_556 2_556 ?
F2C Cs1 F2D 4.7(4) 1_556 1_556 ?
F2C Cs1 F5 91.7(3) 1_556 . ?
F2C Cs1 F7 105.1(3) 1_556 2_556 ?
F2C Cs1 F8 85.9(3) 1_556 1_556 ?
F2C Cs1 F8 100.5(3) 1_556 2_556 ?
F2C Cs1 F9 66.5(3) 1_556 8_566 ?
F2C Cs1 F10 68.5(3) 1_556 7_566 ?
F2D Cs1 Cs3 46.0(3) 1_556 . ?
F2D Cs1 Cs4 80.2(3) 1_556 2_556 ?
F2D Cs1 Cs4 151.0(3) 1_556 7_566 ?
F2D Cs1 Ga1 78.2(3) 1_556 7_566 ?
F2D Cs1 Ga1 112.9(3) 1_556 1_556 ?
F2D Cs1 Ga4 116.1(3) 1_556 . ?
F5 Cs1 Cs3 47.27(6) . . ?
F5 Cs1 Cs4 82.77(7) . 2_556 ?
F5 Cs1 Cs4 99.43(7) . 7_566 ?
F5 Cs1 Ga1 143.28(6) . 1_556 ?
F5 Cs1 Ga1 97.06(7) . 7_566 ?
F5 Cs1 Ga4 29.59(6) . . ?
F5 Cs1 F1A 65.8(3) . 2_556 ?
F5 Cs1 F2D 90.6(3) . 1_556 ?
F5 Cs1 F7 48.09(9) . 2_556 ?
F5 Cs1 F8 165.89(10) . 1_556 ?
F5 Cs1 F8 120.42(9) . 2_556 ?
F5 Cs1 F9 119.62(9) . 8_566 ?
F5 Cs1 F10 72.96(9) . 7_566 ?
F6 Cs1 Cs3 96.91(7) . . ?
F6 Cs1 Cs4 53.87(6) . 7_566 ?
F6 Cs1 Cs4 94.12(7) . 2_556 ?
F6 Cs1 Ga1 102.66(7) . 7_566 ?
F6 Cs1 Ga1 101.40(8) . 1_556 ?
F6 Cs1 Ga4 28.91(6) . . ?
F6 Cs1 F1A 110.0(3) . 2_556 ?
F6 Cs1 F2C 142.9(3) . 1_556 ?
F6 Cs1 F2D 141.9(3) . 1_556 ?
F6 Cs1 F5 51.34(9) . . ?
F6 Cs1 F7 50.44(9) . 2_556 ?
F6 Cs1 F8 97.18(11) . 2_556 ?
F6 Cs1 F8 80.96(10) . 7_566 ?
F6 Cs1 F8 128.92(10) . 1_556 ?
F6 Cs1 F9 80.05(10) . 2_556 ?
F6 Cs1 F9 130.05(9) . 8_566 ?
F6 Cs1 F10 98.56(10) . 7_566 ?
F7 Cs1 Cs3 84.41(7) 2_556 . ?
F7 Cs1 Cs4 99.14(7) 2_556 7_566 ?
F7 Cs1 Cs4 45.54(6) 2_556 2_556 ?
F7 Cs1 Ga1 96.48(7) 2_556 1_556 ?
F7 Cs1 Ga1 143.66(6) 2_556 7_566 ?
F7 Cs1 Ga4 29.15(6) 2_556 . ?
F7 Cs1 F1A 66.4(3) 2_556 2_556 ?
F7 Cs1 F2D 107.7(3) 2_556 1_556 ?
F7 Cs1 F8 72.52(9) 2_556 2_556 ?
F7 Cs1 F8 119.27(9) 2_556 1_556 ?
F7 Cs1 F9 166.36(9) 2_556 8_566 ?
F7 Cs1 F10 120.93(9) 2_556 7_566 ?
F8 Cs1 Cs3 134.92(6) 2_556 . ?
F8 Cs1 Cs3 94.13(8) 7_566 . ?
F8 Cs1 Cs3 133.97(6) 1_556 . ?
F8 Cs1 Cs4 83.16(7) 1_556 2_556 ?
F8 Cs1 Cs4 45.94(7) 7_566 7_566 ?
F8 Cs1 Cs4 46.07(6) 2_556 2_556 ?
F8 Cs1 Cs4 88.37(7) 1_556 7_566 ?
F8 Cs1 Cs4 173.70(7) 7_566 2_556 ?
F8 Cs1 Cs4 93.35(8) 2_556 7_566 ?
F8 Cs1 Ga1 28.79(6) 1_556 1_556 ?
F8 Cs1 Ga1 28.73(6) 2_556 1_556 ?
F8 Cs1 Ga1 96.42(7) 1_556 7_566 ?
F8 Cs1 Ga1 27.92(7) 7_566 7_566 ?
F8 Cs1 Ga1 142.09(6) 2_556 7_566 ?
F8 Cs1 Ga1 102.47(8) 7_566 1_556 ?
F8 Cs1 Ga4 102.51(8) 7_566 . ?
F8 Cs1 Ga4 97.39(7) 2_556 . ?
F8 Cs1 Ga4 142.63(6) 1_556 . ?
F8 Cs1 F1A 138.5(3) 7_566 2_556 ?
F8 Cs1 F1A 104.8(3) 1_556 2_556 ?
F8 Cs1 F1A 89.1(3) 2_556 2_556 ?
F8 Cs1 F2C 110.4(3) 7_566 1_556 ?
F8 Cs1 F2D 106.1(3) 7_566 1_556 ?
F8 Cs1 F2D 104.9(3) 2_556 1_556 ?
F8 Cs1 F2D 88.1(3) 1_556 1_556 ?
F8 Cs1 F5 97.03(11) 7_566 . ?
F8 Cs1 F7 130.51(10) 7_566 2_556 ?
F8 Cs1 F8 96.84(10) 7_566 1_556 ?
F8 Cs1 F8 46.82(11) 2_556 1_556 ?
F8 Cs1 F8 130.33(6) 7_566 2_556 ?
F8 Cs1 F9 81.50(10) 7_566 2_556 ?
F8 Cs1 F9 49.62(9) 7_566 8_566 ?
F8 Cs1 F9 118.69(9) 2_556 8_566 ?
F8 Cs1 F10 49.65(10) 7_566 7_566 ?
F8 Cs1 F10 163.86(10) 2_556 7_566 ?
F9 Cs1 Cs3 175.00(6) 2_556 . ?
F9 Cs1 Cs3 82.02(7) 8_566 . ?
F9 Cs1 Cs4 93.82(7) 2_556 2_556 ?
F9 Cs1 Cs4 88.34(7) 8_566 7_566 ?
F9 Cs1 Cs4 135.69(6) 8_566 2_556 ?
F9 Cs1 Cs4 46.09(7) 2_556 7_566 ?
F9 Cs1 Ga1 96.55(7) 8_566 1_556 ?
F9 Cs1 Ga1 27.94(6) 2_556 1_556 ?
F9 Cs1 Ga1 102.35(8) 2_556 7_566 ?
F9 Cs1 Ga1 28.75(6) 8_566 7_566 ?
F9 Cs1 Ga4 102.09(8) 2_556 . ?
F9 Cs1 Ga4 143.31(6) 8_566 . ?
F9 Cs1 F1A 104.4(3) 8_566 2_556 ?
F9 Cs1 F1A 138.9(3) 2_556 2_556 ?
F9 Cs1 F2C 135.4(3) 2_556 1_556 ?
F9 Cs1 F2D 63.2(3) 8_566 1_556 ?
F9 Cs1 F2D 137.6(3) 2_556 1_556 ?
F9 Cs1 F5 130.58(10) 2_556 . ?
F9 Cs1 F7 96.54(11) 2_556 2_556 ?
F9 Cs1 F8 72.03(9) 8_566 1_556 ?
F9 Cs1 F8 49.80(9) 2_556 2_556 ?
F9 Cs1 F8 49.53(9) 2_556 1_556 ?
F9 Cs1 F9 96.86(10) 2_556 8_566 ?
F9 Cs1 F10 130.17(10) 2_556 7_566 ?
F10 Cs1 Cs3 46.08(6) 7_566 . ?
F10 Cs1 Cs4 93.05(8) 7_566 7_566 ?
F10 Cs1 Cs4 135.62(7) 7_566 2_556 ?
F10 Cs1 Ga1 28.72(6) 7_566 7_566 ?
F10 Cs1 Ga1 142.12(6) 7_566 1_556 ?
F10 Cs1 Ga4 98.10(7) 7_566 . ?
F10 Cs1 F1A 88.8(3) 7_566 2_556 ?
F10 Cs1 F2D 63.8(3) 7_566 1_556 ?
F10 Cs1 F8 118.65(9) 7_566 1_556 ?
F10 Cs1 F9 46.76(9) 7_566 8_566 ?
Cs3 Cs2 Cs3 116.76(3) . 5_576 ?
Cs3 Cs2 Cs4 129.48(2) . . ?
Cs3 Cs2 Cs4 88.79(3) 5_576 6_575 ?
Cs3 Cs2 Cs4 88.79(3) 5_576 . ?
Cs3 Cs2 Cs4 129.48(2) . 6_575 ?
Cs3 Cs2 Ga4 74.359(16) . 5_576 ?
Cs3 Cs2 Ga4 74.359(16) . . ?
Cs3 Cs2 Ga4 74.21(2) 5_576 . ?
Cs3 Cs2 Ga4 74.21(2) 5_576 5_576 ?
Cs4 Cs2 Cs4 90.85(4) . 6_575 ?
Cs4 Cs2 Ga4 72.09(4) 6_575 5_576 ?
Cs4 Cs2 Ga4 155.820(18) 6_575 . ?
Cs4 Cs2 Ga4 72.09(4) . . ?
Cs4 Cs2 Ga4 155.820(18) . 5_576 ?
Ga3 Cs2 Cs3 154.10(2) . 5_576 ?
Ga3 Cs2 Cs3 89.14(3) . . ?
Ga3 Cs2 Cs4 73.294(19) . . ?
Ga3 Cs2 Cs4 73.29(2) . 6_575 ?
Ga3 Cs2 Ga4 115.888(19) . 5_576 ?
Ga3 Cs2 Ga4 115.888(19) . . ?
Ga4 Cs2 Ga4 117.78(4) . 5_576 ?
F1A Cs2 Cs3 162.3(3) . . ?
F1A Cs2 Cs3 48.7(3) . 5_576 ?
F1A Cs2 Cs3 48.7(3) 6_575 5_576 ?
F1A Cs2 Cs3 162.3(3) 6_575 . ?
F1A Cs2 Cs4 65.5(3) 6_575 . ?
F1A Cs2 Cs4 65.5(3) . 6_575 ?
F1A Cs2 Cs4 50.0(3) 6_575 6_575 ?
F1A Cs2 Cs4 50.0(3) . . ?
F1A Cs2 Ga3 105.8(3) 6_575 . ?
F1A Cs2 Ga3 105.8(3) . . ?
F1A Cs2 Ga4 106.2(3) . 5_576 ?
F1A Cs2 Ga4 90.4(3) 6_575 5_576 ?
F1A Cs2 Ga4 90.4(3) . . ?
F1A Cs2 Ga4 106.2(3) 6_575 . ?
F1A Cs2 F1A 18.4(7) 6_575 . ?
F1A Cs2 F3 134.3(4) . . ?
F1A Cs2 F3 134.3(4) 6_575 . ?
F1A Cs2 F4 92.4(4) 6_575 . ?
F1A Cs2 F4 85.0(4) . . ?
F1A Cs2 F4 92.4(4) . 6_575 ?
F1A Cs2 F4 85.0(4) 6_575 6_575 ?
F1A Cs2 F5 133.0(4) 6_575 . ?
F1A Cs2 F5 85.6(3) . 5_576 ?
F1A Cs2 F5 74.3(3) . 2_556 ?
F1A Cs2 F5 117.7(3) . . ?
F1A Cs2 F5 85.6(4) 6_575 2_556 ?
F1A Cs2 F5 117.7(3) 6_575 6_575 ?
F1A Cs2 F5 74.3(3) 6_575 5_576 ?
F1A Cs2 F5 133.0(3) . 6_575 ?
F1A Cs2 F7 93.3(3) . 6_575 ?
F1A Cs2 F7 75.0(3) 6_575 6_575 ?
F1A Cs2 F7 75.0(3) . . ?
F1A Cs2 F7 93.3(3) 6_575 . ?
F1B Cs2 Cs3 57.4(3) . 5_576 ?
F1B Cs2 Cs3 57.4(3) 6_575 5_576 ?
F1B Cs2 Cs3 173.3(4) . . ?
F1B Cs2 Cs3 173.3(4) 6_575 . ?
F1B Cs2 Cs4 50.2(6) . . ?
F1B Cs2 Cs4 55.8(6) 6_575 . ?
F1B Cs2 Cs4 50.2(6) 6_575 6_575 ?
F1B Cs2 Cs4 55.8(6) . 6_575 ?
F1B Cs2 Ga3 96.8(3) . . ?
F1B Cs2 Ga3 96.8(3) 6_575 . ?
F1B Cs2 Ga4 100.1(6) 6_575 5_576 ?
F1B Cs2 Ga4 105.6(6) . 5_576 ?
F1B Cs2 Ga4 100.1(6) . . ?
F1B Cs2 Ga4 105.6(6) 6_575 . ?
F1B Cs2 F1A 11.0(5) 6_575 6_575 ?
F1B Cs2 F1A 15.4(6) 6_575 . ?
F1B Cs2 F1A 15.4(6) . 6_575 ?
F1B Cs2 F1A 11.0(5) . . ?
F1B Cs2 F1B 6.3(13) 6_575 . ?
F1B Cs2 F3 125.7(3) . . ?
F1B Cs2 F3 125.7(3) 6_575 . ?
F1B Cs2 F4 79.0(4) 6_575 6_575 ?
F1B Cs2 F4 81.6(4) . 6_575 ?
F1B Cs2 F4 79.0(4) . . ?
F1B Cs2 F4 81.6(4) 6_575 . ?
F1B Cs2 F5 89.1(5) 6_575 2_556 ?
F1B Cs2 F5 127.3(6) . . ?
F1B Cs2 F5 85.2(5) 6_575 5_576 ?
F1B Cs2 F5 132.9(6) . 6_575 ?
F1B Cs2 F5 132.9(6) 6_575 . ?
F1B Cs2 F5 85.2(5) . 2_556 ?
F1B Cs2 F5 89.1(5) . 5_576 ?
F1B Cs2 F5 127.3(6) 6_575 6_575 ?
F1B Cs2 F7 82.0(7) 6_575 6_575 ?
F1B Cs2 F7 82.0(7) . . ?
F1B Cs2 F7 88.3(7) . 6_575 ?
F1B Cs2 F7 88.3(7) 6_575 . ?
F3 Cs2 Cs3 60.15(10) . . ?
F3 Cs2 Cs3 176.92(9) . 5_576 ?
F3 Cs2 Cs4 93.37(7) . . ?
F3 Cs2 Cs4 93.37(7) . 6_575 ?
F3 Cs2 Ga3 28.98(10) . . ?
F3 Cs2 Ga4 104.36(5) . . ?
F3 Cs2 Ga4 104.36(5) . 5_576 ?
F3 Cs2 F4 50.91(11) . . ?
F3 Cs2 F4 50.91(11) . 6_575 ?
F3 Cs2 F5 132.20(8) . 5_576 ?
F3 Cs2 F5 132.20(8) . 2_556 ?
F3 Cs2 F5 84.39(10) . . ?
F3 Cs2 F5 84.39(10) . 6_575 ?
F3 Cs2 F7 98.25(7) . . ?
F3 Cs2 F7 98.25(7) . 6_575 ?
F4 Cs2 Cs3 131.71(7) . 5_576 ?
F4 Cs2 Cs3 105.14(8) 6_575 . ?
F4 Cs2 Cs3 131.71(7) 6_575 5_576 ?
F4 Cs2 Cs3 105.14(8) . . ?
F4 Cs2 Cs4 82.01(8) 6_575 . ?
F4 Cs2 Cs4 44.43(6) 6_575 6_575 ?
F4 Cs2 Cs4 44.43(6) . . ?
F4 Cs2 Cs4 82.01(8) . 6_575 ?
F4 Cs2 Ga3 29.21(6) . . ?
F4 Cs2 Ga3 29.21(6) 6_575 . ?
F4 Cs2 Ga4 143.37(7) . 5_576 ?
F4 Cs2 Ga4 96.39(8) 6_575 5_576 ?
F4 Cs2 Ga4 96.39(8) . . ?
F4 Cs2 Ga4 143.37(7) 6_575 . ?
F4 Cs2 F4 47.62(14) . 6_575 ?
F4 Cs2 F5 161.67(10) 6_575 2_556 ?
F4 Cs2 F5 117.25(10) 6_575 5_576 ?
F4 Cs2 F5 117.25(10) . 2_556 ?
F4 Cs2 F5 161.66(10) . 5_576 ?
F4 Cs2 F7 119.33(9) . 6_575 ?
F4 Cs2 F7 119.33(9) 6_575 . ?
F4 Cs2 F7 71.99(9) 6_575 6_575 ?
F4 Cs2 F7 71.99(9) . . ?
F5 Cs2 Cs3 93.37(7) 6_575 5_576 ?
F5 Cs2 Cs3 46.10(6) 2_556 5_576 ?
F5 Cs2 Cs3 88.16(6) 5_576 . ?
F5 Cs2 Cs3 47.42(7) 6_575 . ?
F5 Cs2 Cs3 46.10(6) 5_576 5_576 ?
F5 Cs2 Cs3 88.16(6) 2_556 . ?
F5 Cs2 Cs3 47.42(7) . . ?
F5 Cs2 Cs3 93.37(7) . 5_576 ?
F5 Cs2 Cs4 79.77(7) 2_556 . ?
F5 Cs2 Cs4 91.47(8) 6_575 6_575 ?
F5 Cs2 Cs4 133.59(6) 5_576 . ?
F5 Cs2 Cs4 133.59(6) 2_556 6_575 ?
F5 Cs2 Cs4 91.47(8) . . ?
F5 Cs2 Cs4 79.77(7) 5_576 6_575 ?
F5 Cs2 Cs4 176.86(6) 6_575 . ?
F5 Cs2 Cs4 176.86(6) . 6_575 ?
F5 Cs2 Ga3 105.38(8) . . ?
F5 Cs2 Ga3 142.40(6) 5_576 . ?
F5 Cs2 Ga3 105.38(8) 6_575 . ?
F5 Cs2 Ga3 142.40(6) 2_556 . ?
F5 Cs2 Ga4 27.32(6) . . ?
F5 Cs2 Ga4 99.38(7) 5_576 . ?
F5 Cs2 Ga4 27.32(6) 6_575 5_576 ?
F5 Cs2 Ga4 28.46(6) 2_556 . ?
F5 Cs2 Ga4 106.30(8) . 5_576 ?
F5 Cs2 Ga4 106.31(8) 6_575 . ?
F5 Cs2 Ga4 99.38(7) 2_556 5_576 ?
F5 Cs2 Ga4 28.46(6) 5_576 5_576 ?
F5 Cs2 F4 98.20(11) 6_575 6_575 ?
F5 Cs2 F4 133.94(10) . 6_575 ?
F5 Cs2 F4 133.94(10) 6_575 . ?
F5 Cs2 F4 98.20(11) . . ?
F5 Cs2 F5 86.13(14) . 6_575 ?
F5 Cs2 F5 49.03(12) 6_575 5_576 ?
F5 Cs2 F5 100.10(9) . 5_576 ?
F5 Cs2 F5 100.10(9) 6_575 2_556 ?
F5 Cs2 F5 49.03(12) . 2_556 ?
F5 Cs2 F5 74.98(12) 2_556 5_576 ?
F5 Cs2 F7 45.68(8) 5_576 6_575 ?
F5 Cs2 F7 48.58(9) . . ?
F5 Cs2 F7 133.62(9) . 6_575 ?
F5 Cs2 F7 120.40(9) 5_576 . ?
F5 Cs2 F7 120.40(9) 2_556 6_575 ?
F5 Cs2 F7 133.62(9) 6_575 . ?
F5 Cs2 F7 48.58(9) 6_575 6_575 ?
F5 Cs2 F7 45.68(8) 2_556 . ?
F7 Cs2 Cs3 94.10(6) . . ?
F7 Cs2 Cs3 94.10(6) 6_575 . ?
F7 Cs2 Cs3 81.76(7) . 5_576 ?
F7 Cs2 Cs3 81.76(7) 6_575 5_576 ?
F7 Cs2 Cs4 134.14(6) . 6_575 ?
F7 Cs2 Cs4 44.48(6) 6_575 6_575 ?
F7 Cs2 Cs4 134.14(6) 6_575 . ?
F7 Cs2 Cs4 44.48(6) . . ?
F7 Cs2 Ga3 97.21(6) 6_575 . ?
F7 Cs2 Ga3 97.21(6) . . ?
F7 Cs2 Ga4 144.27(6) . 5_576 ?
F7 Cs2 Ga4 144.27(6) 6_575 . ?
F7 Cs2 Ga4 28.01(5) . . ?
F7 Cs2 Ga4 28.01(5) 6_575 5_576 ?
F7 Cs2 F7 163.50(14) . 6_575 ?
Cs1 Cs3 Cs1 142.21(3) . 6_575 ?
Ga2 Cs3 Cs1 71.109(15) 1_556 . ?
Ga2 Cs3 Cs1 71.109(15) 1_556 6_575 ?
F1A Cs3 Cs1 64.3(3) 5_576 6_575 ?
F1A Cs3 Cs1 64.3(3) 2_556 . ?
F1A Cs3 Cs1 81.8(3) 5_576 . ?
F1A Cs3 Cs1 81.8(3) 2_556 6_575 ?
F1A Cs3 Ga2 28.2(3) 2_556 1_556 ?
F1A Cs3 Ga2 28.2(3) 5_576 1_556 ?
F1A Cs3 F1A 17.7(7) 2_556 5_576 ?
F1A Cs3 F1B 11.6(6) 2_556 5_576 ?
F1A Cs3 F1B 6.6(7) 2_556 2_556 ?
F1A Cs3 F1B 11.6(6) 5_576 2_556 ?
F1A Cs3 F1B 6.6(7) 5_576 5_576 ?
F1A Cs3 F2A 45.8(4) 2_556 6_576 ?
F1A Cs3 F2A 32.4(5) 2_556 1_556 ?
F1A Cs3 F2A 32.4(5) 5_576 6_576 ?
F1A Cs3 F2A 45.8(4) 5_576 1_556 ?
F1A Cs3 F2B 49.4(4) 5_576 1_556 ?
F1A Cs3 F2B 49.4(4) 2_556 6_576 ?
F1A Cs3 F2B 37.7(5) 5_576 6_576 ?
F1A Cs3 F2B 37.7(4) 2_556 1_556 ?
F1A Cs3 F2D 56.0(4) 5_576 1_556 ?
F1A Cs3 F2D 52.8(5) 2_556 1_556 ?
F1A Cs3 F2D 52.8(5) 5_576 6_576 ?
F1A Cs3 F2D 56.0(4) 2_556 6_576 ?
F1A Cs3 F3 153.1(3) 5_576 . ?
F1A Cs3 F3 153.1(3) 2_556 . ?
F1B Cs3 Cs1 70.8(5) 2_556 . ?
F1B Cs3 Cs1 76.0(5) 5_576 . ?
F1B Cs3 Cs1 76.0(5) 2_556 6_575 ?
F1B Cs3 Cs1 70.8(5) 5_576 6_575 ?
F1B Cs3 Ga2 29.1(2) 2_556 1_556 ?
F1B Cs3 Ga2 29.1(2) 5_576 1_556 ?
F1B Cs3 F1B 5.2(11) 2_556 5_576 ?
F1B Cs3 F2A 42.1(5) 2_556 6_576 ?
F1B Cs3 F2A 42.1(5) 5_576 1_556 ?
F1B Cs3 F2A 38.2(5) 2_556 1_556 ?
F1B Cs3 F2A 38.2(5) 5_576 6_576 ?
F1B Cs3 F3 152.2(3) 2_556 . ?
F1B Cs3 F3 152.2(3) 5_576 . ?
F2A Cs3 Cs1 99.7(3) 6_576 . ?
F2A Cs3 Cs1 42.5(3) 6_576 6_575 ?
F2A Cs3 Cs1 42.5(3) 1_556 . ?
F2A Cs3 Cs1 99.7(3) 1_556 6_575 ?
F2A Cs3 Ga2 28.6(3) 1_556 1_556 ?
F2A Cs3 Ga2 28.6(3) 6_576 1_556 ?
F2A Cs3 F2A 57.3(6) 6_576 1_556 ?
F2B Cs3 Cs1 44.0(3) 1_556 . ?
F2B Cs3 Cs1 44.0(3) 6_576 6_575 ?
F2B Cs3 Cs1 98.7(3) 1_556 6_575 ?
F2B Cs3 Cs1 98.7(3) 6_576 . ?
F2B Cs3 Ga2 28.4(3) 6_576 1_556 ?
F2B Cs3 Ga2 28.4(3) 1_556 1_556 ?
F2B Cs3 F1B 43.0(5) 1_556 2_556 ?
F2B Cs3 F1B 43.0(5) 6_576 5_576 ?
F2B Cs3 F1B 46.4(5) 1_556 5_576 ?
F2B Cs3 F1B 46.4(5) 6_576 2_556 ?
F2B Cs3 F2A 56.5(3) 6_576 1_556 ?
F2B Cs3 F2A 56.5(3) 1_556 6_576 ?
F2B Cs3 F2A 6.6(5) 6_576 6_576 ?
F2B Cs3 F2A 6.6(5) 1_556 1_556 ?
F2B Cs3 F2B 54.8(6) 6_576 1_556 ?
F2B Cs3 F3 151.2(3) 1_556 . ?
F2B Cs3 F3 151.2(3) 6_576 . ?
F2C Cs3 Cs1 51.0(4) 1_556 . ?
F2C Cs3 Cs1 93.8(3) 1_556 6_575 ?
F2C Cs3 Cs1 93.8(3) 6_576 . ?
F2C Cs3 Cs1 51.0(4) 6_576 6_575 ?
F2C Cs3 Ga2 28.8(3) 6_576 1_556 ?
F2C Cs3 Ga2 28.8(3) 1_556 1_556 ?
F2C Cs3 F1A 46.5(5) 6_576 5_576 ?
F2C Cs3 F1A 54.9(5) 1_556 5_576 ?
F2C Cs3 F1A 54.9(5) 6_576 2_556 ?
F2C Cs3 F1A 46.5(5) 1_556 2_556 ?
F2C Cs3 F1B 53.3(5) 1_556 5_576 ?
F2C Cs3 F1B 50.9(5) 1_556 2_556 ?
F2C Cs3 F1B 53.3(5) 6_576 2_556 ?
F2C Cs3 F1B 50.9(5) 6_576 5_576 ?
F2C Cs3 F2A 18.8(5) 1_556 1_556 ?
F2C Cs3 F2A 53.5(5) 1_556 6_576 ?
F2C Cs3 F2A 53.5(5) 6_576 1_556 ?
F2C Cs3 F2A 18.8(5) 6_576 6_576 ?
F2C Cs3 F2B 12.2(4) 1_556 1_556 ?
F2C Cs3 F2B 50.3(4) 1_556 6_576 ?
F2C Cs3 F2B 50.3(4) 6_576 1_556 ?
F2C Cs3 F2B 12.2(4) 6_576 6_576 ?
F2C Cs3 F2C 43.1(7) 6_576 1_556 ?
F2C Cs3 F2D 14.5(4) 1_556 1_556 ?
F2C Cs3 F2D 30.9(6) 1_556 6_576 ?
F2C Cs3 F2D 30.9(6) 6_576 1_556 ?
F2C Cs3 F2D 14.5(4) 6_576 6_576 ?
F2C Cs3 F3 150.3(3) 1_556 . ?
F2C Cs3 F3 150.3(3) 6_576 . ?
F2D Cs3 Cs1 81.8(3) 6_576 . ?
F2D Cs3 Cs1 81.8(3) 1_556 6_575 ?
F2D Cs3 Cs1 64.8(3) 1_556 . ?
F2D Cs3 Cs1 64.8(3) 6_576 6_575 ?
F2D Cs3 Ga2 27.8(3) 1_556 1_556 ?
F2D Cs3 Ga2 27.8(3) 6_576 1_556 ?
F2D Cs3 F1B 55.5(4) 6_576 5_576 ?
F2D Cs3 F1B 56.5(4) 6_576 2_556 ?
F2D Cs3 F1B 56.5(4) 1_556 5_576 ?
F2D Cs3 F1B 55.5(4) 1_556 2_556 ?
F2D Cs3 F2A 45.0(5) 1_556 6_576 ?
F2D Cs3 F2A 45.0(5) 6_576 1_556 ?
F2D Cs3 F2A 31.7(5) 6_576 6_576 ?
F2D Cs3 F2A 31.7(5) 1_556 1_556 ?
F2D Cs3 F2B 25.8(4) 6_576 6_576 ?
F2D Cs3 F2B 40.3(5) 1_556 6_576 ?
F2D Cs3 F2B 40.3(5) 6_576 1_556 ?
F2D Cs3 F2B 25.8(4) 1_556 1_556 ?
F2D Cs3 F2D 17.2(7) 6_576 1_556 ?
F2D Cs3 F3 150.9(3) 1_556 . ?
F2D Cs3 F3 150.9(3) 6_576 . ?
F3 Cs3 Cs1 108.893(15) . . ?
F3 Cs3 Cs1 108.893(15) . 6_575 ?
F3 Cs3 Ga2 178.63(9) . 1_556 ?
F3 Cs3 F2A 151.3(3) . 6_576 ?
F3 Cs3 F2A 151.3(3) . 1_556 ?
F5 Cs3 Cs1 54.06(8) 6_575 6_575 ?
F5 Cs3 Cs1 138.77(8) . 6_575 ?
F5 Cs3 Cs1 138.77(8) 6_575 . ?
F5 Cs3 Cs1 54.06(8) . . ?
F5 Cs3 Ga2 105.44(8) . 1_556 ?
F5 Cs3 Ga2 105.44(8) 6_575 1_556 ?
F5 Cs3 F1A 80.4(3) 6_575 5_576 ?
F5 Cs3 F1A 92.9(3) . 5_576 ?
F5 Cs3 F1A 80.4(3) . 2_556 ?
F5 Cs3 F1A 92.9(3) 6_575 2_556 ?
F5 Cs3 F1B 87.0(4) 6_575 2_556 ?
F5 Cs3 F1B 87.0(4) . 5_576 ?
F5 Cs3 F1B 83.3(4) 6_575 5_576 ?
F5 Cs3 F1B 83.3(4) . 2_556 ?
F5 Cs3 F2A 84.2(3) . 1_556 ?
F5 Cs3 F2A 84.2(3) 6_575 6_576 ?
F5 Cs3 F2A 125.2(3) . 6_576 ?
F5 Cs3 F2A 125.2(3) 6_575 1_556 ?
F5 Cs3 F2B 89.3(3) . 1_556 ?
F5 Cs3 F2B 89.3(3) 6_575 6_576 ?
F5 Cs3 F2B 129.7(3) 6_575 1_556 ?
F5 Cs3 F2B 129.7(3) . 6_576 ?
F5 Cs3 F2C 100.2(4) 6_575 6_576 ?
F5 Cs3 F2C 134.2(3) . 6_576 ?
F5 Cs3 F2C 100.2(4) . 1_556 ?
F5 Cs3 F2C 134.2(3) 6_575 1_556 ?
F5 Cs3 F2D 114.7(4) 6_575 6_576 ?
F5 Cs3 F2D 129.1(3) . 6_576 ?
F5 Cs3 F2D 114.7(4) . 1_556 ?
F5 Cs3 F2D 129.1(3) 6_575 1_556 ?
F5 Cs3 F3 75.49(10) 6_575 . ?
F5 Cs3 F3 75.49(10) . . ?
F5 Cs3 F5 90.09(15) . 6_575 ?
F10 Cs3 Cs1 56.43(8) 7_566 . ?
F10 Cs3 Cs1 56.43(8) 4_556 6_575 ?
F10 Cs3 Cs1 136.78(9) 7_566 6_575 ?
F10 Cs3 Cs1 136.78(9) 4_556 . ?
F10 Cs3 Ga2 105.05(9) 7_566 1_556 ?
F10 Cs3 Ga2 105.05(9) 4_556 1_556 ?
F10 Cs3 F1A 115.6(3) 4_556 5_576 ?
F10 Cs3 F1A 115.6(3) 7_566 2_556 ?
F10 Cs3 F1A 129.9(3) 4_556 2_556 ?
F10 Cs3 F1A 129.9(3) 7_566 5_576 ?
F10 Cs3 F1B 126.2(5) 4_556 2_556 ?
F10 Cs3 F1B 122.0(5) 4_556 5_576 ?
F10 Cs3 F1B 122.0(5) 7_566 2_556 ?
F10 Cs3 F1B 126.2(5) 7_566 5_576 ?
F10 Cs3 F2A 123.2(3) 7_566 6_576 ?
F10 Cs3 F2A 84.2(3) 4_556 6_576 ?
F10 Cs3 F2A 123.2(3) 4_556 1_556 ?
F10 Cs3 F2A 84.2(3) 7_566 1_556 ?
F10 Cs3 F2B 80.4(3) 4_556 6_576 ?
F10 Cs3 F2B 80.4(3) 7_566 1_556 ?
F10 Cs3 F2B 117.2(3) 7_566 6_576 ?
F10 Cs3 F2B 117.2(3) 4_556 1_556 ?
F10 Cs3 F2C 105.1(4) 7_566 6_576 ?
F10 Cs3 F2C 76.3(3) 4_556 6_576 ?
F10 Cs3 F2C 105.1(4) 4_556 1_556 ?
F10 Cs3 F2C 76.3(3) 7_566 1_556 ?
F10 Cs3 F2D 79.9(3) 7_566 1_556 ?
F10 Cs3 F2D 91.6(4) 7_566 6_576 ?
F10 Cs3 F2D 79.9(3) 4_556 6_576 ?
F10 Cs3 F2D 91.6(4) 4_556 1_556 ?
F10 Cs3 F3 73.97(11) 7_566 . ?
F10 Cs3 F3 73.97(11) 4_556 . ?
F10 Cs3 F5 149.39(11) 4_556 . ?
F10 Cs3 F5 84.38(11) 7_566 . ?
F10 Cs3 F5 149.39(11) 7_566 6_575 ?
F10 Cs3 F5 84.38(11) 4_556 6_575 ?
F10 Cs3 F10 85.26(17) 4_556 7_566 ?
Cs1 Cs4 Cs1 63.684(16) 7_566 1_554 ?
Cs1 Cs4 Cs1 82.41(2) 2_556 1_554 ?
Cs1 Cs4 Cs1 103.97(3) 2_556 7_566 ?
Cs1 Cs4 Cs2 83.77(3) 2_556 . ?
Cs1 Cs4 Cs5 137.98(2) 2_556 . ?
Cs1 Cs4 Ga2 131.87(3) 7_566 . ?
Cs1 Cs4 Ga2 69.50(3) 2_556 . ?
Cs2 Cs4 Cs1 139.243(19) . 1_554 ?
Cs2 Cs4 Cs1 157.062(17) . 7_566 ?
Cs2 Cs4 Ga2 71.05(4) . . ?
Cs5 Cs4 Cs1 103.67(4) . 7_566 ?
Cs5 Cs4 Cs1 82.22(3) . 1_554 ?
Cs5 Cs4 Cs2 82.93(4) . . ?
Cs5 Cs4 Ga2 68.49(4) . . ?
Ga2 Cs4 Cs1 68.19(3) . 1_554 ?
F1A Cs4 Cs1 156.3(3) . 7_566 ?
F1A Cs4 Cs1 93.7(3) . 1_554 ?
F1A Cs4 Cs1 63.6(3) . 2_556 ?
F1A Cs4 Cs2 46.1(3) . . ?
F1A Cs4 Cs5 78.7(3) . . ?
F1A Cs4 Ga2 26.7(3) . . ?
F1A Cs4 F1B 10.3(4) . . ?
F1A Cs4 F1B 12.8(4) . 6_575 ?
F1A Cs4 F2A 36.9(5) . 2 ?
F1A Cs4 F2A 51.1(5) . . ?
F1A Cs4 F2B 32.6(4) . 2 ?
F1A Cs4 F2B 53.1(4) . . ?
F1A Cs4 F2D 47.5(4) . . ?
F1A Cs4 F6 154.1(3) . 7_566 ?
F1B Cs4 Cs1 95.6(2) 6_575 1_554 ?
F1B Cs4 Cs1 158.7(2) 6_575 7_566 ?
F1B Cs4 Cs1 76.4(3) 6_575 2_556 ?
F1B Cs4 Cs1 158.4(3) . 7_566 ?
F1B Cs4 Cs1 94.9(3) . 1_554 ?
F1B Cs4 Cs1 73.9(4) . 2_556 ?
F1B Cs4 Cs2 44.4(3) . . ?
F1B Cs4 Cs2 43.8(2) 6_575 . ?
F1B Cs4 Cs5 66.5(3) 6_575 . ?
F1B Cs4 Cs5 68.8(4) . . ?
F1B Cs4 Ga2 26.8(3) . . ?
F1B Cs4 Ga2 27.8(3) 6_575 . ?
F1B Cs4 F1B 2.6(5) . 6_575 ?
F1B Cs4 F2A 43.9(5) . 2 ?
F1B Cs4 F2A 53.4(4) . . ?
F1B Cs4 F2B 42.9(4) 6_575 2 ?
F1B Cs4 F2B 52.7(4) . . ?
F1B Cs4 F2B 40.6(4) . 2 ?
F1B Cs4 F2D 41.6(4) . . ?
F1B Cs4 F6 153.6(3) . 7_566 ?
F2A Cs4 Cs1 42.6(3) . 1_554 ?
F2A Cs4 Cs1 119.9(4) 2 7_566 ?
F2A Cs4 Cs1 62.8(4) 2 1_554 ?
F2A Cs4 Cs1 64.7(4) . 2_556 ?
F2A Cs4 Cs1 105.8(3) . 7_566 ?
F2A Cs4 Cs1 44.2(3) 2 2_556 ?
F2A Cs4 Cs2 80.8(4) 2 . ?
F2A Cs4 Cs2 97.0(3) . . ?
F2A Cs4 Cs5 94.3(3) 2 . ?
F2A Cs4 Cs5 77.7(4) . . ?
F2A Cs4 Ga2 26.9(3) 2 . ?
F2A Cs4 Ga2 26.9(3) . . ?
F2A Cs4 F1B 46.2(5) 2 6_575 ?
F2A Cs4 F1B 54.6(4) . 6_575 ?
F2A Cs4 F2A 24.9(7) . 2 ?
F2A Cs4 F2B 6.1(4) 2 2 ?
F2A Cs4 F2B 30.5(4) . 2 ?
F2A Cs4 F6 154.2(4) 2 7_566 ?
F2A Cs4 F6 153.0(4) . 7_566 ?
F2B Cs4 Cs1 105.7(3) . 7_566 ?
F2B Cs4 Cs1 76.5(4) . 2_556 ?
F2B Cs4 Cs1 124.9(2) 2 7_566 ?
F2B Cs4 Cs1 42.0(2) 2 2_556 ?
F2B Cs4 Cs1 42.4(3) . 1_554 ?
F2B Cs4 Cs1 68.9(2) 2 1_554 ?
F2B Cs4 Cs2 97.1(3) . . ?
F2B Cs4 Cs2 75.2(2) 2 . ?
F2B Cs4 Cs5 65.9(4) . . ?
F2B Cs4 Cs5 96.0(2) 2 . ?
F2B Cs4 Ga2 27.6(2) 2 . ?
F2B Cs4 Ga2 26.5(3) . . ?
F2B Cs4 F1B 53.3(4) . 6_575 ?
F2B Cs4 F2A 11.9(4) . . ?
F2B Cs4 F2A 34.9(5) . 2 ?
F2B Cs4 F2B 39.8(5) . 2 ?
F2B Cs4 F2D 25.6(4) . . ?
F2B Cs4 F6 152.7(3) . 7_566 ?
F2C Cs4 Cs1 109.5(3) . 7_566 ?
F2C Cs4 Cs1 87.3(4) . 2_556 ?
F2C Cs4 Cs1 49.1(4) . 1_554 ?
F2C Cs4 Cs2 92.2(3) . . ?
F2C Cs4 Cs5 53.7(4) . . ?
F2C Cs4 Ga2 26.7(3) . . ?
F2C Cs4 F1A 52.5(4) . . ?
F2C Cs4 F1B 49.3(4) . . ?
F2C Cs4 F1B 49.2(4) . 6_575 ?
F2C Cs4 F2A 43.9(5) . 2 ?
F2C Cs4 F2A 24.0(5) . . ?
F2C Cs4 F2B 12.5(4) . . ?
F2C Cs4 F2B 47.8(4) . 2 ?
F2C Cs4 F2D 13.9(4) . . ?
F2C Cs4 F6 152.0(3) . 7_566 ?
F2D Cs4 Cs1 94.6(3) . 2_556 ?
F2D Cs4 Cs1 62.0(3) . 1_554 ?
F2D Cs4 Cs1 118.9(3) . 7_566 ?
F2D Cs4 Cs2 81.3(3) . . ?
F2D Cs4 Cs5 43.9(3) . . ?
F2D Cs4 Ga2 26.5(3) . . ?
F2D Cs4 F1B 40.8(4) . 6_575 ?
F2D Cs4 F2A 35.8(5) . . ?
F2D Cs4 F2A 50.5(5) . 2 ?
F2D Cs4 F2B 52.9(4) . 2 ?
F2D Cs4 F6 152.0(3) . 7_566 ?
F4 Cs4 Cs1 110.69(10) . 7_566 ?
F4 Cs4 Cs1 136.69(10) . 2_556 ?
F4 Cs4 Cs1 136.21(10) . 1_554 ?
F4 Cs4 Cs2 54.66(10) . . ?
F4 Cs4 Cs5 55.95(10) . . ?
F4 Cs4 Ga2 103.10(10) . . ?
F4 Cs4 F1A 90.4(3) . . ?
F4 Cs4 F1B 82.5(4) . . ?
F4 Cs4 F1B 80.2(3) . 6_575 ?
F4 Cs4 F2A 126.4(4) . 2 ?
F4 Cs4 F2A 125.8(4) . . ?
F4 Cs4 F2B 122.9(3) . 2 ?
F4 Cs4 F2B 116.4(4) . . ?
F4 Cs4 F2C 104.2(4) . . ?
F4 Cs4 F2D 90.8(4) . . ?
F4 Cs4 F6 76.31(12) . 7_566 ?
F4 Cs4 F7 88.52(13) . . ?
F4 Cs4 F8 154.76(12) . . ?
F4 Cs4 F9 87.67(13) . 8_565 ?
F6 Cs4 Cs1 111.85(7) 7_566 2_556 ?
F6 Cs4 Cs1 111.29(7) 7_566 1_554 ?
F6 Cs4 Cs1 47.61(7) 7_566 7_566 ?
F6 Cs4 Cs2 109.45(7) 7_566 . ?
F6 Cs4 Cs5 110.17(8) 7_566 . ?
F6 Cs4 Ga2 178.56(7) 7_566 . ?
F6 Cs4 F1B 152.5(3) 7_566 6_575 ?
F6 Cs4 F2B 153.7(2) 7_566 2 ?
F7 Cs4 Cs1 55.63(9) . 2_556 ?
F7 Cs4 Cs1 135.22(9) . 1_554 ?
F7 Cs4 Cs1 108.52(8) . 7_566 ?
F7 Cs4 Cs2 57.84(8) . . ?
F7 Cs4 Cs5 138.85(8) . . ?
F7 Cs4 Ga2 105.53(9) . . ?
F7 Cs4 F1A 81.9(3) . . ?
F7 Cs4 F1B 89.5(3) . 6_575 ?
F7 Cs4 F1B 88.3(3) . . ?
F7 Cs4 F2A 91.3(4) . 2 ?
F7 Cs4 F2A 116.0(4) . . ?
F7 Cs4 F2B 126.0(3) . . ?
F7 Cs4 F2B 86.2(3) . 2 ?
F7 Cs4 F2C 131.9(3) . . ?
F7 Cs4 F2D 129.3(3) . . ?
F7 Cs4 F6 75.80(11) . 7_566 ?
F7 Cs4 F8 85.81(12) . . ?
F7 Cs4 F9 153.24(11) . 8_565 ?
F8 Cs4 Cs1 54.93(9) . 1_554 ?
F8 Cs4 Cs1 48.95(8) . 7_566 ?
F8 Cs4 Cs1 55.63(8) . 2_556 ?
F8 Cs4 Cs2 137.33(9) . . ?
F8 Cs4 Cs5 135.22(9) . . ?
F8 Cs4 Ga2 102.12(9) . . ?
F8 Cs4 F1A 113.0(3) . . ?
F8 Cs4 F1B 121.8(4) . . ?
F8 Cs4 F1B 124.2(3) . 6_575 ?
F8 Cs4 F2A 78.4(4) . 2 ?
F8 Cs4 F2A 78.4(4) . . ?
F8 Cs4 F2B 86.5(3) . . ?
F8 Cs4 F2B 81.3(3) . 2 ?
F8 Cs4 F2C 97.8(4) . . ?
F8 Cs4 F2D 111.7(4) . . ?
F8 Cs4 F6 78.45(11) . 7_566 ?
F8 Cs4 F9 86.43(12) . 8_565 ?
F9 Cs4 Cs1 135.41(9) 8_565 2_556 ?
F9 Cs4 Cs1 54.81(9) 8_565 1_554 ?
F9 Cs4 Cs1 49.06(8) 8_565 7_566 ?
F9 Cs4 Cs2 136.09(8) 8_565 . ?
F9 Cs4 Cs5 55.23(8) 8_565 . ?
F9 Cs4 Ga2 101.13(9) 8_565 . ?
F9 Cs4 F1A 124.6(3) 8_565 . ?
F9 Cs4 F1B 115.9(3) 8_565 6_575 ?
F9 Cs4 F1B 117.4(3) 8_565 . ?
F9 Cs4 F2A 87.3(4) 8_565 . ?
F9 Cs4 F2A 112.1(4) 8_565 2 ?
F9 Cs4 F2B 78.9(3) 8_565 . ?
F9 Cs4 F2B 117.8(3) 8_565 2 ?
F9 Cs4 F2C 74.5(3) 8_565 . ?
F9 Cs4 F2D 77.2(3) 8_565 . ?
F9 Cs4 F6 77.56(11) 8_565 7_566 ?
Cs3 Cs5 Cs3 115.52(3) 1_554 5_676 ?
Cs4 Cs5 Cs3 91.68(3) 6_575 1_554 ?
Cs4 Cs5 Cs3 91.68(3) . 1_554 ?
Cs4 Cs5 Cs3 127.82(2) 6_575 5_676 ?
Cs4 Cs5 Cs3 127.82(2) . 5_676 ?
Cs4 Cs5 Cs4 92.10(4) 6_575 . ?
Ga1 Cs5 Cs3 73.85(2) 3 1_554 ?
Ga1 Cs5 Cs3 73.85(2) 7_565 1_554 ?
Ga1 Cs5 Cs3 72.136(17) 3 5_676 ?
Ga1 Cs5 Cs3 72.136(18) 7_565 5_676 ?
Ga1 Cs5 Cs4 74.57(4) 3 6_575 ?
Ga1 Cs5 Cs4 159.70(2) 7_565 6_575 ?
Ga1 Cs5 Cs4 74.57(4) 7_565 . ?
Ga1 Cs5 Cs4 159.70(2) 3 . ?
Ga1 Cs5 Ga1 113.49(4) 7_565 3 ?
Ga3 Cs5 Cs3 158.16(2) . 1_554 ?
Ga3 Cs5 Cs3 86.32(3) . 5_676 ?
Ga3 Cs5 Cs4 73.44(2) . . ?
Ga3 Cs5 Cs4 73.44(2) . 6_575 ?
Ga3 Cs5 Ga1 115.72(2) . 7_565 ?
Ga3 Cs5 Ga1 115.72(2) . 3 ?
F2C Cs5 Cs3 47.5(3) 6_575 1_554 ?
F2C Cs5 Cs3 151.9(3) 6_575 5_676 ?
F2C Cs5 Cs3 151.9(3) . 5_676 ?
F2C Cs5 Cs3 47.5(3) . 1_554 ?
F2C Cs5 Cs4 78.9(3) . 6_575 ?
F2C Cs5 Cs4 47.4(3) 6_575 6_575 ?
F2C Cs5 Cs4 47.4(3) . . ?
F2C Cs5 Cs4 78.9(3) 6_575 . ?
F2C Cs5 Ga1 113.8(3) . 3 ?
F2C Cs5 Ga1 80.8(3) . 7_565 ?
F2C Cs5 Ga1 80.8(3) 6_575 3 ?
F2C Cs5 Ga1 113.8(3) 6_575 7_565 ?
F2C Cs5 Ga3 112.6(3) . . ?
F2C Cs5 Ga3 112.6(3) 6_575 . ?
F2C Cs5 F2C 39.4(6) . 6_575 ?
F2C Cs5 F4 88.0(3) 6_575 6_575 ?
F2C Cs5 F4 103.6(3) . 6_575 ?
F2C Cs5 F4 88.0(3) . . ?
F2C Cs5 F4 103.6(3) 6_575 . ?
F2C Cs5 F9 65.6(3) . 8_565 ?
F2C Cs5 F9 104.8(3) 6_575 8_565 ?
F2C Cs5 F9 65.6(3) 6_575 3 ?
F2C Cs5 F9 104.8(3) . 3 ?
F2C Cs5 F10 89.6(3) 6_575 7_565 ?
F2C Cs5 F10 89.6(3) . 4 ?
F2C Cs5 F10 66.5(3) . 7_565 ?
F2C Cs5 F10 66.5(3) 6_575 4 ?
F2D Cs5 Cs3 161.7(4) 6_575 5_676 ?
F2D Cs5 Cs3 161.7(4) . 5_676 ?
F2D Cs5 Cs3 49.4(4) 6_575 1_554 ?
F2D Cs5 Cs3 49.4(4) . 1_554 ?
F2D Cs5 Cs4 52.2(4) . . ?
F2D Cs5 Cs4 67.9(4) . 6_575 ?
F2D Cs5 Cs4 52.2(4) 6_575 6_575 ?
F2D Cs5 Cs4 67.9(4) 6_575 . ?
F2D Cs5 Ga1 91.9(4) . 7_565 ?
F2D Cs5 Ga1 91.9(4) 6_575 3 ?
F2D Cs5 Ga1 107.8(4) 6_575 7_565 ?
F2D Cs5 Ga1 107.8(4) . 3 ?
F2D Cs5 Ga3 109.2(4) . . ?
F2D Cs5 Ga3 109.2(4) 6_575 . ?
F2D Cs5 F2C 29.5(5) 6_575 . ?
F2D Cs5 F2C 29.5(5) . 6_575 ?
F2D Cs5 F2C 11.2(4) 6_575 6_575 ?
F2D Cs5 F2C 11.2(4) . . ?
F2D Cs5 F2D 18.8(7) . 6_575 ?
F2D Cs5 F3 137.3(4) . 5_676 ?
F2D Cs5 F3 137.3(4) 6_575 5_676 ?
F2D Cs5 F4 88.2(4) 6_575 6_575 ?
F2D Cs5 F4 95.7(4) . 6_575 ?
F2D Cs5 F4 95.7(4) 6_575 . ?
F2D Cs5 F4 88.2(4) . . ?
F2D Cs5 F9 95.1(4) . 3 ?
F2D Cs5 F9 95.1(4) 6_575 8_565 ?
F2D Cs5 F9 76.4(4) 6_575 3 ?
F2D Cs5 F9 76.4(4) . 8_565 ?
F2D Cs5 F10 135.1(4) 6_575 8_565 ?
F2D Cs5 F10 75.8(4) 6_575 4 ?
F2D Cs5 F10 86.9(4) 6_575 7_565 ?
F2D Cs5 F10 135.1(4) . 3 ?
F2D Cs5 F10 75.8(4) . 7_565 ?
F2D Cs5 F10 119.8(4) 6_575 3 ?
F2D Cs5 F10 119.8(4) . 8_565 ?
F2D Cs5 F10 86.9(4) . 4 ?
F3 Cs5 Cs3 173.13(9) 5_676 1_554 ?
F3 Cs5 Cs3 57.61(10) 5_676 5_676 ?
F3 Cs5 Cs4 93.09(7) 5_676 . ?
F3 Cs5 Cs4 93.09(7) 5_676 6_575 ?
F3 Cs5 Ga1 102.68(5) 5_676 3 ?
F3 Cs5 Ga1 102.68(5) 5_676 7_565 ?
F3 Cs5 Ga3 28.71(9) 5_676 . ?
F3 Cs5 F2C 138.5(3) 5_676 . ?
F3 Cs5 F2C 138.5(3) 5_676 6_575 ?
F3 Cs5 F4 50.50(11) 5_676 6_575 ?
F3 Cs5 F4 50.50(11) 5_676 . ?
F3 Cs5 F9 97.73(8) 5_676 3 ?
F3 Cs5 F9 97.73(8) 5_676 8_565 ?
F3 Cs5 F10 81.55(10) 5_676 8_565 ?
F3 Cs5 F10 81.55(10) 5_676 3 ?
F3 Cs5 F10 130.25(9) 5_676 4 ?
F3 Cs5 F10 130.25(9) 5_676 7_565 ?
F4 Cs5 Cs3 135.28(7) 6_575 1_554 ?
F4 Cs5 Cs3 135.28(7) . 1_554 ?
F4 Cs5 Cs3 102.51(8) . 5_676 ?
F4 Cs5 Cs3 102.51(8) 6_575 5_676 ?
F4 Cs5 Cs4 44.75(6) 6_575 6_575 ?
F4 Cs5 Cs4 82.26(8) . 6_575 ?
F4 Cs5 Cs4 44.75(6) . . ?
F4 Cs5 Cs4 82.26(8) 6_575 . ?
F4 Cs5 Ga1 143.66(6) 6_575 7_565 ?
F4 Cs5 Ga1 97.88(8) 6_575 3 ?
F4 Cs5 Ga1 97.88(8) . 7_565 ?
F4 Cs5 Ga1 143.66(6) . 3 ?
F4 Cs5 Ga3 28.96(6) . . ?
F4 Cs5 Ga3 28.96(6) 6_575 . ?
F4 Cs5 F4 47.12(14) . 6_575 ?
F4 Cs5 F10 165.88(10) . 4 ?
F4 Cs5 F10 165.88(10) 6_575 7_565 ?
F4 Cs5 F10 120.34(10) 6_575 4 ?
F4 Cs5 F10 120.34(10) . 7_565 ?
F9 Cs5 Cs3 82.06(7) 3 1_554 ?
F9 Cs5 Cs3 92.27(7) 3 5_676 ?
F9 Cs5 Cs3 92.27(7) 8_565 5_676 ?
F9 Cs5 Cs3 82.06(8) 8_565 1_554 ?
F9 Cs5 Cs4 46.10(6) 3 6_575 ?
F9 Cs5 Cs4 137.07(7) 8_565 6_575 ?
F9 Cs5 Cs4 46.10(6) 8_565 . ?
F9 Cs5 Cs4 137.07(7) 3 . ?
F9 Cs5 Ga1 141.18(7) 8_565 3 ?
F9 Cs5 Ga1 28.73(6) 3 3 ?
F9 Cs5 Ga1 28.73(6) 8_565 7_565 ?
F9 Cs5 Ga1 141.18(7) 3 7_565 ?
F9 Cs5 Ga3 97.85(7) 8_565 . ?
F9 Cs5 Ga3 97.85(7) 3 . ?
F9 Cs5 F4 73.45(10) 8_565 . ?
F9 Cs5 F4 73.45(10) 3 6_575 ?
F9 Cs5 F4 120.45(10) 8_565 6_575 ?
F9 Cs5 F4 120.45(10) 3 . ?
F9 Cs5 F9 163.91(15) 8_565 3 ?
F9 Cs5 F10 47.04(9) 8_565 7_565 ?
F9 Cs5 F10 118.00(9) 8_565 4 ?
F9 Cs5 F10 118.00(9) 3 7_565 ?
F9 Cs5 F10 47.04(9) 3 4 ?
F10 Cs5 Cs3 45.52(6) 4 1_554 ?
F10 Cs5 Cs3 44.46(7) 8_565 5_676 ?
F10 Cs5 Cs3 85.89(7) 7_565 5_676 ?
F10 Cs5 Cs3 93.21(8) 3 1_554 ?
F10 Cs5 Cs3 45.52(6) 7_565 1_554 ?
F10 Cs5 Cs3 93.21(8) 8_565 1_554 ?
F10 Cs5 Cs3 85.89(7) 4 5_676 ?
F10 Cs5 Cs3 44.46(7) 3 5_676 ?
F10 Cs5 Cs4 136.54(6) 7_565 6_575 ?
F10 Cs5 Cs4 93.76(8) 3 6_575 ?
F10 Cs5 Cs4 83.63(7) 4 6_575 ?
F10 Cs5 Cs4 136.54(6) 4 . ?
F10 Cs5 Cs4 172.26(7) 3 . ?
F10 Cs5 Cs4 83.63(7) 7_565 . ?
F10 Cs5 Cs4 172.26(7) 8_565 6_575 ?
F10 Cs5 Cs4 93.76(8) 8_565 . ?
F10 Cs5 Ga1 101.05(9) 8_565 3 ?
F10 Cs5 Ga1 95.49(7) 7_565 3 ?
F10 Cs5 Ga1 28.78(6) 4 3 ?
F10 Cs5 Ga1 27.99(6) 8_565 7_565 ?
F10 Cs5 Ga1 95.49(8) 4 7_565 ?
F10 Cs5 Ga1 101.05(9) 3 7_565 ?
F10 Cs5 Ga1 28.78(6) 7_565 7_565 ?
F10 Cs5 Ga1 27.99(6) 3 3 ?
F10 Cs5 Ga3 143.54(6) 7_565 . ?
F10 Cs5 Ga3 143.54(6) 4 . ?
F10 Cs5 Ga3 103.44(8) 3 . ?
F10 Cs5 Ga3 103.44(8) 8_565 . ?
F10 Cs5 F2C 139.0(3) 3 . ?
F10 Cs5 F2C 108.8(3) 3 6_575 ?
F10 Cs5 F2C 139.0(3) 8_565 6_575 ?
F10 Cs5 F2C 108.8(3) 8_565 . ?
F10 Cs5 F4 131.28(10) 8_565 6_575 ?
F10 Cs5 F4 131.28(10) 3 . ?
F10 Cs5 F4 98.39(11) 3 6_575 ?
F10 Cs5 F4 98.39(11) 8_565 . ?
F10 Cs5 F9 128.84(10) 3 8_565 ?
F10 Cs5 F9 49.80(9) 8_565 8_565 ?
F10 Cs5 F9 128.84(10) 8_565 3 ?
F10 Cs5 F9 49.80(9) 3 3 ?
F10 Cs5 F10 79.97(15) 3 8_565 ?
F10 Cs5 F10 49.42(12) 8_565 7_565 ?
F10 Cs5 F10 95.54(10) 8_565 4 ?
F10 Cs5 F10 95.54(10) 3 7_565 ?
F10 Cs5 F10 71.08(13) 7_565 4 ?
F10 Cs5 F10 49.42(12) 3 4 ?
Cs1 Cs6 Cs4 52.80(3) 2_556 . ?
Cs2 Cs6 Cs1 170.632(13) 7_566 2_556 ?
Cs2 Cs6 Cs4 54.479(16) 7_566 7_566 ?
Cs2 Cs6 Cs4 132.22(3) 7_566 . ?
Cs4 Cs6 Cs1 132.921(17) 7_566 2_556 ?
Cs4 Cs6 Cs4 117.358(18) 7_566 . ?
Ga1 Cs6 Cs1 55.06(2) . 2_556 ?
Ga1 Cs6 Cs2 117.45(2) . 7_566 ?
Ga1 Cs6 Cs4 67.51(2) . . ?
Ga1 Cs6 Cs4 171.931(15) . 7_566 ?
Ga3 Cs6 Cs1 120.14(3) 3_445 2_556 ?
Ga3 Cs6 Cs2 54.61(3) 3_445 7_566 ?
Ga3 Cs6 Cs4 172.894(12) 3_445 . ?
Ga3 Cs6 Cs4 67.444(18) 3_445 7_566 ?
Ga3 Cs6 Ga1 108.39(2) 3_445 . ?
Ga4 Cs6 Cs1 55.32(3) . 2_556 ?
Ga4 Cs6 Cs1 128.53(2) 7_566 2_556 ?
Ga4 Cs6 Cs2 57.23(2) 7_566 7_566 ?
Ga4 Cs6 Cs2 132.32(3) . 7_566 ?
Ga4 Cs6 Cs4 68.10(2) 7_566 7_566 ?
Ga4 Cs6 Cs4 77.86(2) . 7_566 ?
Ga4 Cs6 Cs4 68.30(4) . . ?
Ga4 Cs6 Cs4 75.73(2) 7_566 . ?
Ga4 Cs6 Ga1 108.45(2) 7_566 . ?
Ga4 Cs6 Ga1 110.19(2) . . ?
Ga4 Cs6 Ga3 108.97(4) . 3_445 ?
Ga4 Cs6 Ga3 111.32(2) 7_566 3_445 ?
Ga4 Cs6 Ga4 109.51(2) . 7_566 ?
F3 Cs6 Cs1 129.10(9) 7_566 2_556 ?
F3 Cs6 Cs2 42.24(9) 7_566 7_566 ?
F3 Cs6 Cs4 153.70(8) 7_566 . ?
F3 Cs6 Cs4 81.06(9) 7_566 7_566 ?
F3 Cs6 Ga1 92.27(9) 7_566 . ?
F3 Cs6 Ga3 28.12(8) 7_566 3_445 ?
F3 Cs6 Ga4 137.06(8) 7_566 . ?
F3 Cs6 Ga4 96.35(9) 7_566 7_566 ?
F3 Cs6 F4 47.26(11) 7_566 8_465 ?
F3 Cs6 F6 121.43(10) 7_566 7_566 ?
F3 Cs6 F8 117.01(11) 7_566 . ?
F3 Cs6 F9 88.73(11) 7_566 . ?
F3 Cs6 F10 70.64(11) 7_566 . ?
F4 Cs6 Cs1 131.04(8) 7_566 2_556 ?
F4 Cs6 Cs1 92.67(7) 8_465 2_556 ?
F4 Cs6 Cs2 81.86(7) 8_465 7_566 ?
F4 Cs6 Cs2 48.74(8) 7_566 7_566 ?
F4 Cs6 Cs4 40.32(6) 7_566 7_566 ?
F4 Cs6 Cs4 85.06(7) 8_465 7_566 ?
F4 Cs6 Cs4 156.44(6) 7_566 . ?
F4 Cs6 Cs4 145.46(6) 8_465 . ?
F4 Cs6 Ga1 93.78(8) 8_465 . ?
F4 Cs6 Ga1 135.68(7) 7_566 . ?
F4 Cs6 Ga3 27.48(6) 8_465 3_445 ?
F4 Cs6 Ga3 27.31(6) 7_566 3_445 ?
F4 Cs6 Ga4 94.80(8) 7_566 . ?
F4 Cs6 Ga4 95.95(8) 7_566 7_566 ?
F4 Cs6 Ga4 138.80(6) 8_465 7_566 ?
F4 Cs6 Ga4 93.72(8) 8_465 . ?
F4 Cs6 F3 47.64(11) 7_566 7_566 ?
F4 Cs6 F4 47.20(12) 7_566 8_465 ?
F4 Cs6 F5 92.56(10) 7_566 7_566 ?
F4 Cs6 F6 121.66(9) 7_566 7_566 ?
F4 Cs6 F6 166.95(8) 8_465 7_566 ?
F4 Cs6 F8 162.85(8) 7_566 . ?
F4 Cs6 F8 118.37(9) 8_465 . ?
F4 Cs6 F9 71.80(9) 8_465 . ?
F4 Cs6 F9 118.62(9) 7_566 . ?
F4 Cs6 F10 90.59(11) 8_465 . ?
F4 Cs6 F10 118.15(10) 7_566 . ?
F5 Cs6 Cs1 136.15(7) 7_566 2_556 ?
F5 Cs6 Cs2 44.32(7) 7_566 7_566 ?
F5 Cs6 Cs4 89.92(7) 7_566 . ?
F5 Cs6 Cs4 81.37(7) 7_566 7_566 ?
F5 Cs6 Ga1 92.43(7) 7_566 . ?
F5 Cs6 Ga3 96.13(7) 7_566 3_445 ?
F5 Cs6 Ga4 137.71(6) 7_566 . ?
F5 Cs6 Ga4 28.21(6) 7_566 7_566 ?
F5 Cs6 F3 73.69(10) 7_566 7_566 ?
F5 Cs6 F4 120.78(10) 7_566 8_465 ?
F5 Cs6 F6 47.84(9) 7_566 7_566 ?
F5 Cs6 F8 88.91(10) 7_566 . ?
F5 Cs6 F9 117.13(9) 7_566 . ?
F5 Cs6 F10 70.95(8) 7_566 . ?
F6 Cs6 Cs1 100.37(7) 7_566 2_556 ?
F6 Cs6 Cs1 43.44(7) 2_556 2_556 ?
F6 Cs6 Cs1 84.28(7) . 2_556 ?
F6 Cs6 Cs2 103.23(7) . 7_566 ?
F6 Cs6 Cs2 139.18(7) 2_556 7_566 ?
F6 Cs6 Cs2 85.14(7) 7_566 7_566 ?
F6 Cs6 Cs4 48.77(6) . 7_566 ?
F6 Cs6 Cs4 82.03(7) 2_556 . ?
F6 Cs6 Cs4 87.13(7) . . ?
F6 Cs6 Cs4 92.99(7) 2_556 7_566 ?
F6 Cs6 Cs4 47.57(6) 7_566 . ?
F6 Cs6 Cs4 86.49(6) 7_566 7_566 ?
F6 Cs6 Ga1 139.28(6) . . ?
F6 Cs6 Ga1 94.13(7) 2_556 . ?
F6 Cs6 Ga1 93.20(6) 7_566 . ?
F6 Cs6 Ga3 92.67(7) 2_556 3_445 ?
F6 Cs6 Ga3 93.03(7) . 3_445 ?
F6 Cs6 Ga3 139.48(6) 7_566 3_445 ?
F6 Cs6 Ga4 29.14(6) 2_556 . ?
F6 Cs6 Ga4 94.46(7) . 7_566 ?
F6 Cs6 Ga4 29.09(6) . . ?
F6 Cs6 Ga4 94.20(7) 7_566 . ?
F6 Cs6 Ga4 28.16(6) 7_566 7_566 ?
F6 Cs6 Ga4 138.64(6) 2_556 7_566 ?
F6 Cs6 F3 117.42(10) 2_556 7_566 ?
F6 Cs6 F3 118.77(11) . 7_566 ?
F6 Cs6 F4 70.21(10) 2_556 8_465 ?
F6 Cs6 F4 89.96(11) . 8_465 ?
F6 Cs6 F4 71.37(10) . 7_566 ?
F6 Cs6 F4 90.75(11) 2_556 7_566 ?
F6 Cs6 F5 166.79(8) 2_556 7_566 ?
F6 Cs6 F5 119.94(9) . 7_566 ?
F6 Cs6 F6 91.92(10) . 7_566 ?
F6 Cs6 F6 120.22(4) 2_556 7_566 ?
F6 Cs6 F6 49.52(11) . 2_556 ?
F6 Cs6 F7 120.91(9) 2_556 7_566 ?
F6 Cs6 F7 71.73(9) . 7_566 ?
F6 Cs6 F8 122.21(9) . . ?
F6 Cs6 F8 91.70(10) 2_556 . ?
F6 Cs6 F8 71.09(8) 7_566 . ?
F6 Cs6 F9 117.68(9) 7_566 . ?
F6 Cs6 F9 121.36(9) . . ?
F6 Cs6 F9 71.99(9) 2_556 . ?
F6 Cs6 F10 166.45(8) . . ?
F6 Cs6 F10 90.58(9) 7_566 . ?
F6 Cs6 F10 118.36(9) 2_556 . ?
F7 Cs6 Cs1 48.57(8) . 2_556 ?
F7 Cs6 Cs1 137.28(7) 7_566 2_556 ?
F7 Cs6 Cs2 51.66(7) 7_566 7_566 ?
F7 Cs6 Cs2 140.78(8) . 7_566 ?
F7 Cs6 Cs4 39.89(6) . . ?
F7 Cs6 Cs4 92.67(7) . 7_566 ?
F7 Cs6 Cs4 90.31(7) 7_566 . ?
F7 Cs6 Cs4 40.88(6) 7_566 7_566 ?
F7 Cs6 Ga1 94.82(7) . . ?
F7 Cs6 Ga1 136.03(6) 7_566 . ?
F7 Cs6 Ga3 137.66(6) . 3_445 ?
F7 Cs6 Ga3 96.49(7) 7_566 3_445 ?
F7 Cs6 Ga4 27.58(6) 7_566 7_566 ?
F7 Cs6 Ga4 28.69(6) . . ?
F7 Cs6 Ga4 93.15(7) . 7_566 ?
F7 Cs6 Ga4 94.31(7) 7_566 . ?
F7 Cs6 F3 165.71(10) . 7_566 ?
F7 Cs6 F3 93.60(11) 7_566 7_566 ?
F7 Cs6 F4 120.76(10) . 7_566 ?
F7 Cs6 F4 121.28(9) 7_566 8_465 ?
F7 Cs6 F4 119.72(10) . 8_465 ?
F7 Cs6 F4 74.18(10) 7_566 7_566 ?
F7 Cs6 F5 48.30(9) 7_566 7_566 ?
F7 Cs6 F5 118.28(9) . 7_566 ?
F7 Cs6 F6 70.57(9) . 7_566 ?
F7 Cs6 F6 49.72(9) . 2_556 ?
F7 Cs6 F6 49.58(9) . . ?
F7 Cs6 F6 47.71(9) 7_566 7_566 ?
F7 Cs6 F7 89.89(10) . 7_566 ?
F7 Cs6 F8 118.50(9) 7_566 . ?
F7 Cs6 F8 72.89(9) . . ?
F7 Cs6 F9 163.18(8) 7_566 . ?
F7 Cs6 F9 91.93(10) . . ?
F7 Cs6 F10 119.07(9) 7_566 . ?
F7 Cs6 F10 119.37(9) . . ?
F8 Cs6 Cs1 48.32(7) . 2_556 ?
F8 Cs6 Cs2 128.30(7) . 7_566 ?
F8 Cs6 Cs4 156.24(6) . 7_566 ?
F8 Cs6 Cs4 40.55(6) . . ?
F8 Cs6 Ga1 27.17(6) . . ?
F8 Cs6 Ga3 135.56(6) . 3_445 ?
F8 Cs6 Ga4 95.59(7) . . ?
F8 Cs6 Ga4 93.41(7) . 7_566 ?
F8 Cs6 F9 46.73(9) . . ?
F8 Cs6 F10 46.63(9) . . ?
F9 Cs6 Cs1 43.66(7) . 2_556 ?
F9 Cs6 Cs2 127.01(7) . 7_566 ?
F9 Cs6 Cs4 80.50(7) . . ?
F9 Cs6 Cs4 155.49(6) . 7_566 ?
F9 Cs6 Ga1 27.16(6) . . ?
F9 Cs6 Ga3 93.40(7) . 3_445 ?
F9 Cs6 Ga4 135.61(6) . 7_566 ?
F9 Cs6 Ga4 95.30(7) . . ?
F9 Cs6 F10 46.46(9) . . ?
F10 Cs6 Cs1 82.17(7) . 2_556 ?
F10 Cs6 Cs2 90.25(6) . 7_566 ?
F10 Cs6 Cs4 144.73(6) . 7_566 ?
F10 Cs6 Cs4 84.75(7) . . ?
F10 Cs6 Ga1 27.21(6) . . ?
F10 Cs6 Ga3 93.69(7) . 3_445 ?
F10 Cs6 Ga4 137.40(6) . . ?
F10 Cs6 Ga4 94.02(7) . 7_566 ?
Cs1 Ga1 Cs1 65.43(2) 2_556 8_464 ?
Cs1 Ga1 Cs1 105.04(3) 2_556 7_566 ?
Cs1 Ga1 Cs1 65.43(2) 1_554 7_566 ?
Cs1 Ga1 Cs1 83.91(4) 1_554 2_556 ?
Cs1 Ga1 Cs1 167.93(3) 7_566 8_464 ?
Cs1 Ga1 Cs1 105.04(3) 1_554 8_464 ?
Cs5 Ga1 Cs1 169.495(15) 7_565 2_556 ?
Cs5 Ga1 Cs1 83.93(2) 3_445 8_464 ?
Cs5 Ga1 Cs1 106.36(2) 7_565 8_464 ?
Cs5 Ga1 Cs1 105.10(4) 3_445 2_556 ?
Cs5 Ga1 Cs1 169.495(15) 3_445 1_554 ?
Cs5 Ga1 Cs1 83.93(2) 7_565 7_566 ?
Cs5 Ga1 Cs1 106.36(2) 3_445 7_566 ?
Cs5 Ga1 Cs1 105.10(4) 7_565 1_554 ?
Cs5 Ga1 Cs5 66.51(4) 7_565 3_445 ?
F8 Ga1 Cs1 48.40(12) . 7_566 ?
F8 Ga1 Cs1 58.81(13) 2 2_556 ?
F8 Ga1 Cs1 48.40(12) 2 8_464 ?
F8 Ga1 Cs1 56.98(13) . 2_556 ?
F8 Ga1 Cs1 120.91(12) . 8_464 ?
F8 Ga1 Cs1 56.98(13) 2 1_554 ?
F8 Ga1 Cs1 120.91(12) 2 7_566 ?
F8 Ga1 Cs1 58.81(13) . 1_554 ?
F8 Ga1 Cs5 121.47(13) 2 7_565 ?
F8 Ga1 Cs5 121.47(13) . 3_445 ?
F8 Ga1 Cs5 132.31(12) . 7_565 ?
F8 Ga1 Cs5 132.31(12) 2 3_445 ?
F8 Ga1 F8 88.8(2) 2 . ?
F9 Ga1 Cs1 132.52(12) 2 2_556 ?
F9 Ga1 Cs1 132.53(12) . 1_554 ?
F9 Ga1 Cs1 121.51(14) 2 8_464 ?
F9 Ga1 Cs1 121.51(14) . 7_566 ?
F9 Ga1 Cs1 58.63(14) . 8_464 ?
F9 Ga1 Cs1 58.63(14) 2 7_566 ?
F9 Ga1 Cs1 48.63(12) 2 1_554 ?
F9 Ga1 Cs1 48.63(12) . 2_556 ?
F9 Ga1 Cs5 122.02(12) 2 3_445 ?
F9 Ga1 Cs5 56.84(12) . 3_445 ?
F9 Ga1 Cs5 122.01(12) . 7_565 ?
F9 Ga1 Cs5 56.84(12) 2 7_565 ?
F9 Ga1 F8 90.79(18) . 2 ?
F9 Ga1 F8 90.04(18) . . ?
F9 Ga1 F8 90.79(18) 2 . ?
F9 Ga1 F8 90.04(18) 2 2 ?
F9 Ga1 F9 178.8(2) . 2 ?
F10 Ga1 Cs1 121.27(13) 2 1_554 ?
F10 Ga1 Cs1 132.82(12) 2 7_566 ?
F10 Ga1 Cs1 121.81(12) . 1_554 ?
F10 Ga1 Cs1 132.83(12) . 8_464 ?
F10 Ga1 Cs1 121.26(13) . 2_556 ?
F10 Ga1 Cs1 57.87(12) 2 8_464 ?
F10 Ga1 Cs1 57.87(12) . 7_566 ?
F10 Ga1 Cs1 121.81(12) 2 2_556 ?
F10 Ga1 Cs5 58.72(13) . 7_565 ?
F10 Ga1 Cs5 48.91(12) . 3_445 ?
F10 Ga1 Cs5 48.91(12) 2 7_565 ?
F10 Ga1 Cs5 58.72(13) 2 3_445 ?
F10 Ga1 F8 178.78(18) 2 . ?
F10 Ga1 F8 178.78(18) . 2 ?
F10 Ga1 F8 90.32(17) 2 2 ?
F10 Ga1 F8 90.32(17) . . ?
F10 Ga1 F9 89.15(18) . 2 ?
F10 Ga1 F9 90.04(18) . . ?
F10 Ga1 F9 90.04(18) 2 2 ?
F10 Ga1 F9 89.15(18) 2 . ?
F10 Ga1 F10 90.6(3) . 2 ?
F2A Ga2 F2A 42.3(12) . 2 ?
F2A Ga2 F2A 180.0 6_575 2 ?
F2A Ga2 F2A 137.7(12) 2 5_575 ?
F2A Ga2 F2A 137.7(12) . 6_575 ?
F2A Ga2 F2A 180.0(13) . 5_575 ?
F2A Ga2 F2A 42.3(12) 6_575 5_575 ?
F2B Ga2 F2A 59.9(10) 5_575 6_575 ?
F2B Ga2 F2A 120.1(10) 6_575 . ?
F2B Ga2 F2A 19.9(6) 5_575 5_575 ?
F2B Ga2 F2A 59.9(10) 2 . ?
F2B Ga2 F2A 59.9(10) 6_575 5_575 ?
F2B Ga2 F2A 160.1(6) . 5_575 ?
F2B Ga2 F2A 19.9(6) . . ?
F2B Ga2 F2A 160.1(6) 6_575 2 ?
F2B Ga2 F2A 19.9(6) 6_575 6_575 ?
F2B Ga2 F2A 19.9(6) 2 2 ?
F2B Ga2 F2A 120.1(10) 2 5_575 ?
F2B Ga2 F2A 120.1(10) 5_575 2 ?
F2B Ga2 F2A 160.1(6) 2 6_575 ?
F2B Ga2 F2A 59.9(10) . 2 ?
F2B Ga2 F2A 120.1(10) . 6_575 ?
F2B Ga2 F2A 160.1(6) 5_575 . ?
F2B Ga2 F2B 78.7(11) 2 . ?
F2B Ga2 F2B 180.0 6_575 2 ?
F2B Ga2 F2B 101.3(11) 2 5_575 ?
F2B Ga2 F2B 180.0(13) 5_575 . ?
F2B Ga2 F2B 78.7(11) 6_575 5_575 ?
F2B Ga2 F2B 101.3(11) 6_575 . ?
F2D Ga2 F2A 118.1(8) 5_575 . ?
F2D Ga2 F2A 61.9(8) 2 2 ?
F2D Ga2 F2A 88.7(9) . 6_575 ?
F2D Ga2 F2A 61.9(8) . . ?
F2D Ga2 F2A 91.3(9) . 2 ?
F2D Ga2 F2A 61.9(8) 6_575 6_575 ?
F2D Ga2 F2A 118.1(8) 6_575 2 ?
F2D Ga2 F2A 91.3(9) 6_575 5_575 ?
F2D Ga2 F2A 88.7(9) 5_575 2 ?
F2D Ga2 F2A 118.1(8) 2 6_575 ?
F2D Ga2 F2A 88.7(9) 6_575 . ?
F2D Ga2 F2A 61.9(8) 5_575 5_575 ?
F2D Ga2 F2A 91.3(9) 2 . ?
F2D Ga2 F2A 118.1(8) . 5_575 ?
F2D Ga2 F2A 91.3(9) 5_575 6_575 ?
F2D Ga2 F2A 88.7(9) 2 5_575 ?
F2D Ga2 F2B 110.8(9) 2 . ?
F2D Ga2 F2B 43.3(7) 2 2 ?
F2D Ga2 F2B 69.2(9) 2 5_575 ?
F2D Ga2 F2B 136.7(7) 5_575 . ?
F2D Ga2 F2B 110.8(9) . 2 ?
F2D Ga2 F2B 43.3(7) . . ?
F2D Ga2 F2B 69.2(9) 6_575 . ?
F2D Ga2 F2B 43.3(7) 6_575 6_575 ?
F2D Ga2 F2B 69.2(9) 5_575 2 ?
F2D Ga2 F2B 136.7(7) 2 6_575 ?
F2D Ga2 F2B 110.8(9) 6_575 5_575 ?
F2D Ga2 F2B 110.8(9) 5_575 6_575 ?
F2D Ga2 F2B 43.3(7) 5_575 5_575 ?
F2D Ga2 F2B 69.2(9) . 6_575 ?
F2D Ga2 F2B 136.7(7) 6_575 2 ?
F2D Ga2 F2B 136.7(7) . 5_575 ?
F2D Ga2 F2D 27.9(11) 2 5_575 ?
F2D Ga2 F2D 180.0 5_575 . ?
F2D Ga2 F2D 180.0 6_575 2 ?
F2D Ga2 F2D 27.9(11) 6_575 . ?
F2D Ga2 F2D 152.1(11) 2 . ?
F2D Ga2 F2D 152.1(11) 6_575 5_575 ?
Cs2 Ga3 Cs2 180.0 . 5_676 ?
Cs2 Ga3 Cs5 94.72(2) . 5_676 ?
Cs2 Ga3 Cs5 85.28(2) 5_676 5_676 ?
Cs2 Ga3 Cs5 94.72(3) 5_676 . ?
Cs2 Ga3 Cs5 85.28(3) . . ?
Cs2 Ga3 Cs6 66.428(18) . 4_556 ?
Cs2 Ga3 Cs6 66.428(18) 5_676 8_565 ?
Cs2 Ga3 Cs6 113.572(18) . 8_565 ?
Cs2 Ga3 Cs6 113.572(18) 5_676 4_556 ?
Cs5 Ga3 Cs5 180.0 . 5_676 ?
Cs5 Ga3 Cs6 111.824(19) 5_676 8_565 ?
Cs5 Ga3 Cs6 68.176(18) . 8_565 ?
Cs5 Ga3 Cs6 111.824(18) . 4_556 ?
Cs5 Ga3 Cs6 68.176(19) 5_676 4_556 ?
Cs6 Ga3 Cs6 180.0 4_556 8_565 ?
F3 Ga3 Cs2 132.67(16) 5_676 . ?
F3 Ga3 Cs2 47.33(16) 5_676 5_676 ?
F3 Ga3 Cs2 47.33(16) . . ?
F3 Ga3 Cs2 132.67(16) . 5_676 ?
F3 Ga3 Cs5 132.61(16) . . ?
F3 Ga3 Cs5 47.39(16) . 5_676 ?
F3 Ga3 Cs5 47.39(16) 5_676 . ?
F3 Ga3 Cs5 132.61(16) 5_676 5_676 ?
F3 Ga3 Cs6 55.279(19) 5_676 8_565 ?
F3 Ga3 Cs6 124.721(19) 5_676 4_556 ?
F3 Ga3 Cs6 124.72(2) . 8_565 ?
F3 Ga3 Cs6 55.28(2) . 4_556 ?
F3 Ga3 F3 180.0(3) . 5_676 ?
F4 Ga3 Cs2 121.54(14) 5_676 . ?
F4 Ga3 Cs2 58.45(14) . . ?
F4 Ga3 Cs2 58.46(14) 2_656 5_676 ?
F4 Ga3 Cs2 121.54(14) 6_575 5_676 ?
F4 Ga3 Cs2 121.54(14) 2_656 . ?
F4 Ga3 Cs2 58.46(14) 5_676 5_676 ?
F4 Ga3 Cs2 121.54(14) . 5_676 ?
F4 Ga3 Cs2 58.46(14) 6_575 . ?
F4 Ga3 Cs5 58.64(14) 2_656 5_676 ?
F4 Ga3 Cs5 121.36(14) 6_575 5_676 ?
F4 Ga3 Cs5 58.64(14) 5_676 5_676 ?
F4 Ga3 Cs5 121.36(14) . 5_676 ?
F4 Ga3 Cs5 58.64(14) 6_575 . ?
F4 Ga3 Cs5 121.36(14) 2_656 . ?
F4 Ga3 Cs5 58.64(14) . . ?
F4 Ga3 Cs5 121.36(14) 5_676 . ?
F4 Ga3 Cs6 55.63(14) . 8_565 ?
F4 Ga3 Cs6 126.44(14) 2_656 4_556 ?
F4 Ga3 Cs6 53.56(14) 2_656 8_565 ?
F4 Ga3 Cs6 124.37(14) . 4_556 ?
F4 Ga3 Cs6 126.44(14) 6_575 8_565 ?
F4 Ga3 Cs6 124.37(14) 5_676 8_565 ?
F4 Ga3 Cs6 53.56(14) 6_575 4_556 ?
F4 Ga3 Cs6 55.63(14) 5_676 4_556 ?
F4 Ga3 F3 89.86(18) 2_656 5_676 ?
F4 Ga3 F3 89.86(18) 5_676 5_676 ?
F4 Ga3 F3 90.14(18) 6_575 5_676 ?
F4 Ga3 F3 90.14(18) 5_676 . ?
F4 Ga3 F3 89.86(18) . . ?
F4 Ga3 F3 90.14(18) 2_656 . ?
F4 Ga3 F3 90.14(18) . 5_676 ?
F4 Ga3 F3 89.86(18) 6_575 . ?
F4 Ga3 F4 89.6(3) 6_575 . ?
F4 Ga3 F4 180.0 5_676 . ?
F4 Ga3 F4 89.6(3) 5_676 2_656 ?
F4 Ga3 F4 90.4(3) 2_656 . ?
F4 Ga3 F4 90.4(3) 5_676 6_575 ?
F4 Ga3 F4 180.0 6_575 2_656 ?
Cs1 Ga4 Cs1 172.17(3) . 2_556 ?
Cs1 Ga4 Cs2 102.77(2) 2_556 5_576 ?
Cs1 Ga4 Cs2 102.77(2) . . ?
Cs1 Ga4 Cs2 84.02(2) . 5_576 ?
Cs1 Ga4 Cs2 84.02(2) 2_556 . ?
Cs1 Ga4 Cs6 104.69(3) 2_556 2_556 ?
Cs1 Ga4 Cs6 104.69(3) . . ?
Cs1 Ga4 Cs6 68.68(2) . 2_556 ?
Cs1 Ga4 Cs6 68.68(2) 2_556 . ?
Cs2 Ga4 Cs2 62.22(4) 5_576 . ?
Cs6 Ga4 Cs2 113.10(4) . . ?
Cs6 Ga4 Cs2 113.10(4) 2_556 5_576 ?
Cs6 Ga4 Cs2 171.091(13) 2_556 . ?
Cs6 Ga4 Cs2 171.091(12) . 5_576 ?
Cs6 Ga4 Cs6 72.58(4) 2_556 . ?
F5 Ga4 Cs1 56.32(11) . . ?
F5 Ga4 Cs1 130.66(11) . 2_556 ?
F5 Ga4 Cs1 56.32(11) 2_556 2_556 ?
F5 Ga4 Cs1 130.66(11) 2_556 . ?
F5 Ga4 Cs2 57.90(12) 2_556 . ?
F5 Ga4 Cs2 57.90(12) . 5_576 ?
F5 Ga4 Cs2 46.65(11) 2_556 5_576 ?
F5 Ga4 Cs2 46.65(11) . . ?
F5 Ga4 Cs6 125.38(13) 2_556 2_556 ?
F5 Ga4 Cs6 125.38(12) . . ?
F5 Ga4 Cs6 124.57(12) . 2_556 ?
F5 Ga4 Cs6 124.57(12) 2_556 . ?
F5 Ga4 F5 89.3(2) 2_556 . ?
F6 Ga4 Cs1 49.82(11) 2_556 2_556 ?
F6 Ga4 Cs1 49.82(11) . . ?
F6 Ga4 Cs1 123.28(11) 2_556 . ?
F6 Ga4 Cs1 123.28(11) . 2_556 ?
F6 Ga4 Cs2 121.18(12) . . ?
F6 Ga4 Cs2 133.84(11) 2_556 . ?
F6 Ga4 Cs2 121.19(12) 2_556 5_576 ?
F6 Ga4 Cs2 133.84(11) . 5_576 ?
F6 Ga4 Cs6 55.63(12) 2_556 . ?
F6 Ga4 Cs6 54.89(11) . . ?
F6 Ga4 Cs6 55.63(12) . 2_556 ?
F6 Ga4 Cs6 54.89(11) 2_556 2_556 ?
F6 Ga4 F5 90.32(16) 2_556 2_556 ?
F6 Ga4 F5 178.87(18) . 2_556 ?
F6 Ga4 F5 178.87(17) 2_556 . ?
F6 Ga4 F5 90.32(16) . . ?
F6 Ga4 F6 90.0(2) . 2_556 ?
F7 Ga4 Cs1 58.44(13) . 2_556 ?
F7 Ga4 Cs1 121.67(13) . . ?
F7 Ga4 Cs1 121.67(13) 2_556 2_556 ?
F7 Ga4 Cs1 58.44(13) 2_556 . ?
F7 Ga4 Cs2 59.14(12) 2_556 5_576 ?
F7 Ga4 Cs2 119.51(12) . 5_576 ?
F7 Ga4 Cs2 59.14(12) . . ?
F7 Ga4 Cs2 119.51(12) 2_556 . ?
F7 Ga4 Cs6 54.39(12) 2_556 2_556 ?
F7 Ga4 Cs6 126.97(12) 2_556 . ?
F7 Ga4 Cs6 54.40(12) . . ?
F7 Ga4 Cs6 126.97(12) . 2_556 ?
F7 Ga4 F5 90.21(18) . . ?
F7 Ga4 F5 90.21(18) 2_556 2_556 ?
F7 Ga4 F5 88.82(17) . 2_556 ?
F7 Ga4 F5 88.82(17) 2_556 . ?
F7 Ga4 F6 90.86(17) . 2_556 ?
F7 Ga4 F6 90.11(17) . . ?
F7 Ga4 F6 90.86(17) 2_556 . ?
F7 Ga4 F6 90.11(17) 2_556 2_556 ?
F7 Ga4 F7 178.6(2) . 2_556 ?
Cs2 F1A Cs1 104.5(5) . 2_556 ?
Cs2 F1A Cs3 84.8(4) . 5_576 ?
Cs2 F1A Cs4 83.9(4) . . ?
Cs3 F1A Cs1 69.8(3) 5_576 2_556 ?
Cs3 F1A Cs4 133.1(6) 5_576 . ?
Cs4 F1A Cs1 69.4(3) . 2_556 ?
Ga2 F1A Cs1 101.8(6) . 2_556 ?
Ga2 F1A Cs2 153.7(8) . . ?
Ga2 F1A Cs3 103.5(7) . 5_576 ?
Ga2 F1A Cs4 106.5(7) . . ?
F1A F1A Cs1 149.6(3) 6_575 2_556 ?
F1A F1A Cs2 80.8(3) 6_575 . ?
F1A F1A Cs3 81.2(3) 6_575 5_576 ?
F1A F1A Cs4 140.8(3) 6_575 . ?
F1A F1A Ga2 76.0(5) 6_575 . ?
F1B F1A Cs1 154(4) . 2_556 ?
F1B F1A Cs1 173.6(18) 6_575 2_556 ?
F1B F1A Cs2 75.6(19) 6_575 . ?
F1B F1A Cs2 75(3) . . ?
F1B F1A Cs3 135(4) . 5_576 ?
F1B F1A Cs3 116.4(19) 6_575 5_576 ?
F1B F1A Cs4 85(4) . . ?
F1B F1A Cs4 104.4(17) 6_575 . ?
F1B F1A Ga2 78.3(19) 6_575 . ?
F1B F1A Ga2 82(3) . . ?
F1B F1A F1A 56(4) . 6_575 ?
F1B F1A F1A 36.7(17) 6_575 6_575 ?
F1B F1A F1B 20(5) . 6_575 ?
Cs2 F1B Cs3 78.9(4) . 5_576 ?
Cs2 F1B Cs4 85.4(6) . . ?
Cs2 F1B Cs4 80.4(6) . 6_575 ?
Cs4 F1B Cs3 118.3(8) . 5_576 ?
Cs4 F1B Cs3 111.0(8) 6_575 5_576 ?
Cs4 F1B Cs4 124.4(5) . 6_575 ?
Ga2 F1B Cs2 166.7(12) . . ?
Ga2 F1B Cs3 90.1(5) . 5_576 ?
Ga2 F1B Cs4 106.5(10) . . ?
Ga2 F1B Cs4 97.0(10) . 6_575 ?
F1A F1B Cs2 89(2) 6_575 . ?
F1A F1B Cs2 94(3) . . ?
F1A F1B Cs3 51.9(16) 6_575 5_576 ?
F1A F1B Cs3 39(4) . 5_576 ?
F1A F1B Cs4 85(4) . . ?
F1A F1B Cs4 149(4) . 6_575 ?
F1A F1B Cs4 170(2) 6_575 . ?
F1A F1B Cs4 62.8(17) 6_575 6_575 ?
F1A F1B Ga2 78(2) 6_575 . ?
F1A F1B Ga2 82(3) . . ?
F1A F1B F1A 87(5) . 6_575 ?
F1B F1B Cs2 86.8(7) 6_575 . ?
F1B F1B Cs3 87.4(6) 6_575 5_576 ?
F1B F1B Cs4 150.9(3) 6_575 . ?
F1B F1B Cs4 26.5(3) 6_575 6_575 ?
F1B F1B Ga2 85.3(10) 6_575 . ?
F1B F1B F1A 36.7(17) 6_575 6_575 ?
F1B F1B F1A 124(4) 6_575 . ?
Cs1 F2A Cs3 73.5(4) 1_554 1_554 ?
Cs1 F2A Cs4 86.7(5) 1_554 . ?
Cs1 F2A Cs4 83.0(5) 1_554 2 ?
Cs4 F2A Cs3 112.5(6) . 1_554 ?
Cs4 F2A Cs3 109.0(5) 2 1_554 ?
Cs4 F2A Cs4 132.2(7) . 2 ?
Ga2 F2A Cs1 156.0(10) . 1_554 ?
Ga2 F2A Cs3 82.5(7) . 1_554 ?
Ga2 F2A Cs4 103.9(8) . 2 ?
Ga2 F2A Cs4 104.2(8) . . ?
F2A F2A Cs1 135.0(5) 2 1_554 ?
F2A F2A Cs3 151.3(3) 2 1_554 ?
F2A F2A Cs4 77.2(17) 2 2 ?
F2A F2A Cs4 77.9(16) 2 . ?
F2A F2A Ga2 68.9(6) 2 . ?
F2B F2A Cs1 82(2) . 1_554 ?
F2B F2A Cs3 34(2) . 1_554 ?
F2B F2A Cs4 143(3) . 2 ?
F2B F2A Cs4 80(2) . . ?
F2B F2A Ga2 79(2) . . ?
F2B F2A F2A 135(3) . 2 ?
F2B F2A F2C 15(2) . . ?
F2C F2A Cs1 92.2(12) . 1_554 ?
F2C F2A Cs3 48.3(10) . 1_554 ?
F2C F2A Cs4 156.9(14) . 2 ?
F2C F2A Cs4 69.7(11) . . ?
F2C F2A Ga2 72.4(11) . . ?
F2C F2A F2A 120(2) . 2 ?
Cs1 F2B Cs3 83.0(4) 1_554 1_554 ?
Cs1 F2B Cs4 73.6(4) 1_554 2 ?
Cs1 F2B Cs4 87.9(4) 1_554 . ?
Cs3 F2B Cs4 108.4(4) 1_554 2 ?
Cs4 F2B Cs3 130.2(6) . 1_554 ?
Cs4 F2B Cs4 115.6(5) . 2 ?
Ga2 F2B Cs1 159.4(9) . 1_554 ?
Ga2 F2B Cs3 98.5(6) . 1_554 ?
Ga2 F2B Cs4 86.6(6) . 2 ?
Ga2 F2B Cs4 106.0(6) . . ?
F2A F2B Cs1 85(2) . 1_554 ?
F2A F2B Cs3 139(3) . 1_554 ?
F2A F2B Cs4 88(3) . . ?
F2A F2B Cs4 31(2) . 2 ?
F2A F2B Ga2 81(2) . . ?
F2A F2B F2C 150(4) . . ?
F2A F2B F2D 141(3) . . ?
F2C F2B Cs1 115(2) . 1_554 ?
F2C F2B Cs3 69(2) . 1_554 ?
F2C F2B Cs4 170(2) . 2 ?
F2C F2B Cs4 71(2) . . ?
F2C F2B Ga2 85(2) . . ?
F2C F2B F2D 16.5(19) . . ?
F2D F2B Cs1 130.8(12) . 1_554 ?
F2D F2B Cs3 71.5(10) . 1_554 ?
F2D F2B Cs4 154.1(11) . 2 ?
F2D F2B Cs4 78.5(10) . . ?
F2D F2B Ga2 68.1(9) . . ?
Cs1 F2C Cs5 112.7(5) 1_554 . ?
Cs3 F2C Cs1 80.5(4) 1_554 1_554 ?
Cs3 F2C Cs5 79.2(4) 1_554 . ?
Cs4 F2C Cs1 84.5(4) . 1_554 ?
Cs4 F2C Cs3 146.1(6) . 1_554 ?
Cs4 F2C Cs5 78.9(4) . . ?
Ga2 F2C Cs1 128.4(8) . 1_554 ?
Ga2 F2C Cs3 103.3(6) . 1_554 ?
Ga2 F2C Cs4 109.9(6) . . ?
Ga2 F2C Cs5 118.6(8) . . ?
F2A F2C Cs1 63.3(11) . 1_554 ?
F2A F2C Cs3 113.0(13) . 1_554 ?
F2A F2C Cs4 86.3(11) . . ?
F2A F2C Cs5 165.1(13) . . ?
F2A F2C Ga2 68.4(11) . . ?
F2A F2C F2D 131.4(17) . 6_575 ?
F2B F2C Cs1 54(2) . 1_554 ?
F2B F2C Cs3 99(2) . 1_554 ?
F2B F2C Cs4 96(2) . . ?
F2B F2C Cs5 166(2) . . ?
F2B F2C Ga2 75(2) . . ?
F2B F2C F2A 14.7(19) . . ?
F2B F2C F2D 149(4) . . ?
F2B F2C F2D 135(3) . 6_575 ?
F2D F2C Cs1 155.9(12) 6_575 1_554 ?
F2D F2C Cs1 156(2) . 1_554 ?
F2D F2C Cs3 86(2) . 1_554 ?
F2D F2C Cs3 75.9(10) 6_575 1_554 ?
F2D F2C Cs4 97(2) . . ?
F2D F2C Cs4 112.9(10) 6_575 . ?
F2D F2C Cs5 58.1(8) 6_575 . ?
F2D F2C Cs5 44.8(19) . . ?
F2D F2C Ga2 73.9(19) . . ?
F2D F2C Ga2 63.2(10) 6_575 . ?
F2D F2C F2A 141(3) . . ?
F2D F2C F2D 17.6(13) . 6_575 ?
Cs3 F2D Cs1 69.2(4) 1_554 1_554 ?
Cs3 F2D Cs4 134.6(6) 1_554 . ?
Cs4 F2D Cs1 71.1(3) . 1_554 ?
Cs5 F2D Cs1 106.1(5) . 1_554 ?
Cs5 F2D Cs3 86.7(5) . 1_554 ?
Cs5 F2D Cs4 83.8(5) . . ?
Ga2 F2D Cs1 101.4(7) . 1_554 ?
Ga2 F2D Cs3 103.5(7) . 1_554 ?
Ga2 F2D Cs4 105.0(7) . . ?
Ga2 F2D Cs5 152.6(9) . . ?
F2B F2D Cs1 33.2(9) . 1_554 ?
F2B F2D Cs3 82.7(10) . 1_554 ?
F2B F2D Cs4 75.9(9) . . ?
F2B F2D Cs5 138.6(12) . . ?
F2B F2D Ga2 68.6(10) . . ?
F2B F2D F2C 122.0(15) . 6_575 ?
F2C F2D Cs1 136.6(11) 6_575 1_554 ?
F2C F2D Cs1 19.3(18) . 1_554 ?
F2C F2D Cs3 80(2) . 1_554 ?
F2C F2D Cs3 73.2(9) 6_575 1_554 ?
F2C F2D Cs4 151.3(12) 6_575 . ?
F2C F2D Cs4 69.5(19) . . ?
F2C F2D Cs5 92.4(10) 6_575 . ?
F2C F2D Cs5 124(2) . . ?
F2C F2D Ga2 83(2) . . ?
F2C F2D Ga2 67.3(10) 6_575 . ?
F2C F2D F2B 14.7(17) . . ?
F2C F2D F2C 133(3) . 6_575 ?
F2C F2D F2D 148(2) . 6_575 ?
F2D F2D Cs1 149.1(3) 6_575 1_554 ?
F2D F2D Cs3 81.4(3) 6_575 1_554 ?
F2D F2D Cs4 139.6(3) 6_575 . ?
F2D F2D Cs5 80.6(4) 6_575 . ?
F2D F2D Ga2 76.1(5) 6_575 . ?
F2D F2D F2B 136.3(9) 6_575 . ?
F2D F2D F2C 14.7(9) 6_575 6_575 ?
Cs2 F3 Cs3 74.45(11) . . ?
Cs2 F3 Cs5 152.41(18) . 5_676 ?
Cs2 F3 Cs6 87.17(9) . 7_566 ?
Cs2 F3 Cs6 87.17(9) . 4_556 ?
Cs5 F3 Cs3 77.96(12) 5_676 . ?
Cs5 F3 Cs6 89.68(9) 5_676 4_556 ?
Cs5 F3 Cs6 89.68(9) 5_676 7_566 ?
Cs6 F3 Cs3 83.36(8) 7_566 . ?
Cs6 F3 Cs3 83.36(8) 4_556 . ?
Cs6 F3 Cs6 166.54(16) 7_566 4_556 ?
Ga3 F3 Cs2 103.7(2) . . ?
Ga3 F3 Cs3 178.1(2) . . ?
Ga3 F3 Cs5 103.9(2) . 5_676 ?
Ga3 F3 Cs6 96.60(8) . 4_556 ?
Ga3 F3 Cs6 96.60(8) . 7_566 ?
Cs2 F4 Cs5 105.01(13) . . ?
Cs2 F4 Cs6 167.28(14) . 8_565 ?
Cs2 F4 Cs6 82.26(11) . 7_566 ?
Cs4 F4 Cs2 80.91(11) . . ?
Cs4 F4 Cs5 79.30(11) . . ?
Cs4 F4 Cs6 90.48(11) . 7_566 ?
Cs4 F4 Cs6 91.53(12) . 8_565 ?
Cs5 F4 Cs6 83.41(11) . 8_565 ?
Cs6 F4 Cs5 166.18(13) 7_566 . ?
Cs6 F4 Cs6 87.63(11) 7_566 8_565 ?
Ga3 F4 Cs2 92.33(16) . . ?
Ga3 F4 Cs4 167.4(2) . . ?
Ga3 F4 Cs5 92.40(16) . . ?
Ga3 F4 Cs6 96.89(16) . 8_565 ?
Ga3 F4 Cs6 99.12(17) . 7_566 ?
Cs1 F5 Cs2 105.33(11) . 5_576 ?
Cs1 F5 Cs6 85.62(9) . 7_566 ?
Cs2 F5 Cs1 158.97(12) . . ?
Cs2 F5 Cs2 79.90(9) . 5_576 ?
Cs2 F5 Cs6 85.93(10) . 7_566 ?
Cs3 F5 Cs1 78.67(9) . . ?
Cs3 F5 Cs2 76.99(9) . 5_576 ?
Cs3 F5 Cs2 82.85(10) . . ?
Cs3 F5 Cs6 94.54(10) . 7_566 ?
Cs6 F5 Cs2 164.24(12) 7_566 5_576 ?
Ga4 F5 Cs1 94.08(13) . . ?
Ga4 F5 Cs2 106.03(15) . . ?
Ga4 F5 Cs2 93.64(14) . 5_576 ?
Ga4 F5 Cs3 166.0(2) . . ?
Ga4 F5 Cs6 96.88(14) . 7_566 ?
Cs1 F6 Cs4 78.52(8) . 7_566 ?
Cs1 F6 Cs6 88.16(9) . 7_566 ?
Cs1 F6 Cs6 89.03(10) . 2_556 ?
Cs1 F6 Cs6 162.58(12) . . ?
Cs4 F6 Cs6 83.47(9) 7_566 7_566 ?
Cs6 F6 Cs4 85.94(9) 2_556 7_566 ?
Cs6 F6 Cs4 84.16(9) . 7_566 ?
Cs6 F6 Cs6 91.57(10) . 2_556 ?
Cs6 F6 Cs6 88.08(10) . 7_566 ?
Cs6 F6 Cs6 169.39(11) 2_556 7_566 ?
Ga4 F6 Cs1 101.27(14) . . ?
Ga4 F6 Cs4 178.81(18) . 7_566 ?
Ga4 F6 Cs6 95.23(14) . 2_556 ?
Ga4 F6 Cs6 95.36(14) . 7_566 ?
Ga4 F6 Cs6 96.01(13) . . ?
Cs1 F7 Cs2 102.83(11) 2_556 . ?
Cs4 F7 Cs1 78.83(10) . 2_556 ?
Cs4 F7 Cs2 77.69(9) . . ?
Cs4 F7 Cs6 94.22(10) . . ?
Cs4 F7 Cs6 90.60(10) . 7_566 ?
Cs6 F7 Cs1 84.87(10) . 2_556 ?
Cs6 F7 Cs1 167.91(11) 7_566 2_556 ?
Cs6 F7 Cs2 80.34(9) 7_566 . ?
Cs6 F7 Cs2 167.32(12) . . ?
Cs6 F7 Cs6 90.11(10) . 7_566 ?
Ga4 F7 Cs1 92.41(14) . 2_556 ?
Ga4 F7 Cs2 92.85(14) . . ?
Ga4 F7 Cs4 165.2(2) . . ?
Ga4 F7 Cs6 99.13(15) . 7_566 ?
Ga4 F7 Cs6 96.92(14) . . ?
Cs1 F8 Cs1 160.45(13) 7_566 2_556 ?
Cs1 F8 Cs1 83.16(10) 7_566 1_554 ?
Cs1 F8 Cs1 103.98(11) 2_556 1_554 ?
Cs1 F8 Cs6 167.32(12) 1_554 . ?
Cs1 F8 Cs6 87.79(10) 7_566 . ?
Cs1 F8 Cs6 81.96(10) 2_556 . ?
Cs4 F8 Cs1 85.11(10) . 7_566 ?
Cs4 F8 Cs1 78.30(10) . 2_556 ?
Cs4 F8 Cs1 80.54(10) . 1_554 ?
Cs4 F8 Cs6 89.89(10) . . ?
Ga1 F8 Cs1 94.28(14) . 2_556 ?
Ga1 F8 Cs1 92.40(15) . 1_554 ?
Ga1 F8 Cs1 103.68(16) . 7_566 ?
Ga1 F8 Cs4 168.1(2) . . ?
Ga1 F8 Cs6 98.37(15) . . ?
Cs1 F9 Cs1 83.14(10) 2_556 8_464 ?
Cs1 F9 Cs5 160.43(13) 2_556 3_445 ?
Cs1 F9 Cs6 166.16(12) 8_464 . ?
Cs1 F9 Cs6 86.01(10) 2_556 . ?
Cs4 F9 Cs1 84.85(9) 8_465 2_556 ?
Cs4 F9 Cs1 80.49(10) 8_465 8_464 ?
Cs4 F9 Cs5 78.67(9) 8_465 3_445 ?
Cs4 F9 Cs6 90.02(11) 8_465 . ?
Cs5 F9 Cs1 104.23(11) 3_445 8_464 ?
Cs5 F9 Cs6 83.53(10) 3_445 . ?
Ga1 F9 Cs1 92.61(15) . 8_464 ?
Ga1 F9 Cs1 103.43(15) . 2_556 ?
Ga1 F9 Cs4 168.6(2) . 8_465 ?
Ga1 F9 Cs5 94.43(14) . 3_445 ?
Ga1 F9 Cs6 98.26(16) . . ?
Cs1 F10 Cs5 103.42(11) 7_566 7_565 ?
Cs1 F10 Cs6 82.47(9) 7_566 . ?
Cs3 F10 Cs1 77.49(10) 7_566 7_566 ?
Cs3 F10 Cs5 87.95(10) 7_566 3_445 ?
Cs3 F10 Cs5 78.24(10) 7_566 7_565 ?
Cs3 F10 Cs6 93.38(10) 7_566 . ?
Cs5 F10 Cs1 161.46(13) 3_445 7_566 ?
Cs5 F10 Cs5 84.46(10) 3_445 7_565 ?
Cs5 F10 Cs6 87.04(10) 3_445 . ?
Cs5 F10 Cs6 168.25(12) 7_565 . ?
Ga1 F10 Cs1 93.42(14) . 7_566 ?
Ga1 F10 Cs3 164.9(2) . 7_566 ?
Ga1 F10 Cs5 103.10(15) . 3_445 ?
Ga1 F10 Cs5 92.49(15) . 7_565 ?
Ga1 F10 Cs6 97.34(15) . . ?

_olex2_submission_special_instructions 'No special instructions were received'
loop_
_twin_individual_id
_twin_individual_mass_fraction_refined
1 0.9160(18)
2 0.0840(18)

####################################################################### 
# 
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# Crystallographic Data Centre (CCDC).
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# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
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# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_Rb3AlF6_Fddd
_database_code_depnum_ccdc_archive 'CCDC 2193510'
loop_
_audit_author_name
_audit_author_address
'Gregory Morrison'
;University of South Carolina
United States of America
;
_audit_update_record             
;
2022-07-28 deposited with the CCDC.	2023-05-19 downloaded from the CCDC.
;
_audit_creation_date             2022-02-14
_audit_creation_method           
;
Olex2 1.2
(compiled May 18 2018 14:05:52 for OlexSys, GUI svn.r5506)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         '0.02(Al48 F288 Rb144)'
_chemical_formula_sum            'Al F6 Rb3'
_chemical_formula_weight         397.39
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Al Al 0.0645 0.0514 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Rb Rb -0.9393 2.9676 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      orthorhombic
_space_group_IT_number           70
_space_group_name_H-M_alt        'F d d d'
_space_group_name_Hall           '-F 2uv 2vw'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+3/4, -y+3/4, z'
'-x+3/4, y, -z+3/4'
'x, -y+3/4, -z+3/4'
'x, y+1/2, z+1/2'
'-x+3/4, -y+5/4, z+1/2'
'-x+3/4, y+1/2, -z+5/4'
'x, -y+5/4, -z+5/4'
'x+1/2, y, z+1/2'
'-x+5/4, -y+3/4, z+1/2'
'-x+5/4, y, -z+5/4'
'x+1/2, -y+3/4, -z+5/4'
'x+1/2, y+1/2, z'
'-x+5/4, -y+5/4, z'
'-x+5/4, y+1/2, -z+3/4'
'x+1/2, -y+5/4, -z+3/4'
'-x, -y, -z'
'x-3/4, y-3/4, -z'
'x-3/4, -y, z-3/4'
'-x, y-3/4, z-3/4'
'-x, -y+1/2, -z+1/2'
'x-3/4, y-1/4, -z+1/2'
'x-3/4, -y+1/2, z-1/4'
'-x, y-1/4, z-1/4'
'-x+1/2, -y, -z+1/2'
'x-1/4, y-3/4, -z+1/2'
'x-1/4, -y, z-1/4'
'-x+1/2, y-3/4, z-1/4'
'-x+1/2, -y+1/2, -z'
'x-1/4, y-1/4, -z'
'x-1/4, -y+1/2, z-3/4'
'-x+1/2, y-1/4, z-3/4'

_cell_length_a                   12.4412(11)
_cell_length_b                   17.6466(16)
_cell_length_c                   37.201(4)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_volume                     8167.4(13)
_cell_formula_units_Z            48
_cell_measurement_reflns_used    9087
_cell_measurement_temperature    299(2)
_cell_measurement_theta_max      37.1263
_cell_measurement_theta_min      2.5549
_shelx_estimated_absorpt_T_max   0.246
_shelx_estimated_absorpt_T_min   0.165
_exptl_absorpt_coefficient_mu    21.650
_exptl_absorpt_correction_T_max  0.7482
_exptl_absorpt_correction_T_min  0.3919
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
SADABS-2016/2 (Bruker,2016) was used for absorption correction.
wR2(int) was 0.1568 before and 0.0873 after correction.
The Ratio of minimum to maximum transmission is 0.5238.
The λ/2 correction factor is Not present.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    3.878
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       shard
_exptl_crystal_F_000             8544
_exptl_crystal_size_max          0.13
_exptl_crystal_size_mid          0.1
_exptl_crystal_size_min          0.09
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0742
_diffrn_reflns_av_unetI/netI     0.0269
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.999
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_k_max       25
_diffrn_reflns_limit_k_min       -25
_diffrn_reflns_limit_l_max       53
_diffrn_reflns_limit_l_min       -53
_diffrn_reflns_number            133061
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.999
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         30.504
_diffrn_reflns_theta_min         2.190
_diffrn_ambient_temperature      299.37
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'Bruker D8 Quest'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   'microfocus sealed X-ray tube'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                2704
_reflns_number_total             3134
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT v8.34A (Bruker, 2013)'
_computing_data_collection       'Bruker APEX3 v2016.5-0 (Bruker, 2016)'
_computing_data_reduction        'SAINT v8.34A (Bruker, 013)'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    'ShelXT (Sheldrick, 2015)'
_refine_diff_density_max         1.712
_refine_diff_density_min         -0.863
_refine_diff_density_rms         0.132
_refine_ls_extinction_coef       0.000011(3)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     'SHELXL-2018/3 (Sheldrick 2018)'
_refine_ls_goodness_of_fit_ref   1.069
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     162
_refine_ls_number_reflns         3134
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0306
_refine_ls_R_factor_gt           0.0252
_refine_ls_restrained_S_all      1.069
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0253P)²+96.4949P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0612
_refine_ls_wR_factor_ref         0.0643
_refine_special_details          ?
_olex2_refinement_description    
;
1. Uiso/Uaniso restraints and constraints
Uanis(Rb1A) = Uanis(Rb1B)
Uanis(Rb2A) = Uanis(Rb2B)
2. Others
 Sof(Rb1A)=1-FVAR(1)
 Sof(Rb1B)=FVAR(1)
 Sof(Rb2A)=1-FVAR(2)
 Sof(Rb2B)=FVAR(2)
 Fixed Sof: F9(0.5) F10A(0.5) F10B(0.5)
;
_atom_sites_solution_hydrogens   .
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Rb1A Rb 0.62919(12) 0.48160(12) 0.52996(7) 0.0208(3) Uani 0.668(8) 1 d . . . .
.
Rb1B Rb 0.6294(3) 0.49285(18) 0.53683(8) 0.0208(3) Uani 0.332(8) 1 d . . . . .
Rb2A Rb 0.9126(2) 0.48342(12) 0.62418(2) 0.0209(2) Uani 0.819(12) 1 d . . . . .
Rb2B Rb 0.8925(6) 0.4948(4) 0.62454(12) 0.0209(2) Uani 0.181(12) 1 d . . . . .
Rb3 Rb 0.87919(2) 0.49786(2) 0.45917(2) 0.02468(8) Uani 1 1 d . . . . .
Rb4 Rb 0.84330(2) 0.62426(2) 0.55326(2) 0.02232(8) Uani 1 1 d . . . . .
Rb5 Rb 0.375000 0.58317(2) 0.375000 0.02208(9) Uani 1 2 d S T P . .
Al1 Al 0.625000 0.625000 0.45802(3) 0.01049(18) Uani 1 2 d S T P . .
Al2 Al 1.125000 0.625000 0.625000 0.0120(3) Uani 1 4 d S T P . .
Al3 Al 0.875000 0.375000 0.53867(3) 0.01133(19) Uani 1 2 d S T P . .
Al4 Al 0.375000 0.375000 0.375000 0.0120(3) Uani 1 4 d S T P . .
F1 F 0.72681(17) 0.62592(13) 0.49254(5) 0.0328(4) Uani 1 1 d . . . . .
F2 F 0.52245(17) 0.62307(13) 0.42380(5) 0.0329(5) Uani 1 1 d . . . . .
F3 F 0.62301(19) 0.72697(11) 0.45764(6) 0.0327(5) Uani 1 1 d . . . . .
F4 F 1.02244(18) 0.62483(14) 0.59109(6) 0.0375(5) Uani 1 1 d . . . . .
F5 F 0.77166(15) 0.37494(11) 0.50426(5) 0.0237(4) Uani 1 1 d . . . . .
F6 F 1.125000 0.52143(15) 0.625000 0.0286(6) Uani 1 2 d S T P . .
F7 F 0.97836(15) 0.37370(12) 0.57348(5) 0.0265(4) Uani 1 1 d . . . . .
F8 F 0.87589(16) 0.47702(10) 0.53910(5) 0.0268(4) Uani 1 1 d . . . . .
F9 F 0.3774(7) 0.3274(5) 0.41656(17) 0.091(3) Uani 0.5 1 d . . . . .
F10A F 0.2726(7) 0.4381(5) 0.3865(4) 0.113(5) Uani 0.5 1 d . . . . .
F10B F 0.4718(9) 0.4420(5) 0.3897(4) 0.134(6) Uani 0.5 1 d . . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Rb1A Al3 3.6050(17) . ?
Rb1A F1 2.788(3) 30_556 ?
Rb1A F1 3.162(3) 14 ?
Rb1A F1 3.146(3) . ?
Rb1A F2 3.151(3) 17_666 ?
Rb1A F3 2.788(3) 14 ?
Rb1A F3 3.221(3) 30_556 ?
Rb1A F5 2.756(3) . ?
Rb1A F7 3.036(2) 2_655 ?
Rb1A F8 3.089(3) . ?
Rb1A F9 2.611(6) 18_666 ?
Rb1A F10B 3.510(17) 17_666 ?
Rb1B F1 3.114(4) . ?
Rb1B F1 3.134(4) 14 ?
Rb1B F1 3.009(4) 30_556 ?
Rb1B F2 3.146(4) 17_666 ?
Rb1B F3 2.994(4) 14 ?
Rb1B F3 3.208(4) 30_556 ?
Rb1B F5 2.988(4) . ?
Rb1B F7 3.037(4) 2_655 ?
Rb1B F8 3.081(4) . ?
Rb1B F9 2.287(6) 18_666 ?
Rb1B F10A 3.332(16) 17_666 ?
Rb1B F10B 3.220(17) 17_666 ?
Rb2A Al2 3.6367(9) . ?
Rb2A F2 3.159(3) 19_666 ?
Rb2A F2 2.802(3) 32_656 ?
Rb2A F3 3.138(2) 32_656 ?
Rb2A F4 3.100(3) . ?
Rb2A F4 3.130(3) 8 ?
Rb2A F6 2.726(2) . ?
Rb2A F7 3.195(2) 2_655 ?
Rb2A F7 2.824(3) . ?
Rb2A F8 3.200(2) . ?
Rb2A F10A 2.717(8) 17_666 ?
Rb2A F10B 2.775(12) 19_666 ?
Rb2B Rb4 3.554(6) . ?
Rb2B F2 3.148(5) 19_666 ?
Rb2B F2 3.015(7) 32_656 ?
Rb2B F3 3.113(5) 32_656 ?
Rb2B F4 3.071(5) . ?
Rb2B F4 3.090(5) 8 ?
Rb2B F6 2.931(6) . ?
Rb2B F7 3.200(5) 2_655 ?
Rb2B F7 3.052(7) . ?
Rb2B F8 3.200(5) . ?
Rb2B F10A 2.406(11) 17_666 ?
Rb2B F10B 2.464(15) 19_666 ?
Rb3 F1 3.200(2) . ?
Rb3 F2 3.237(2) 14 ?
Rb3 F3 3.169(2) 14 ?
Rb3 F4 3.111(2) 17_766 ?
Rb3 F4 3.158(3) 30_556 ?
Rb3 F5 3.0052(19) 2_655 ?
Rb3 F5 3.051(2) . ?
Rb3 F5 3.166(2) 18_666 ?
Rb3 F6 3.1501(5) 17_766 ?
Rb3 F7 3.123(2) 17_766 ?
Rb3 F8 2.997(2) . ?
Rb3 F8 3.080(2) 17_766 ?
Rb4 F1 2.6839(19) . ?
Rb4 F3 2.6893(19) 29_666 ?
Rb4 F4 2.636(2) . ?
Rb4 F5 3.0827(17) 18_666 ?
Rb4 F8 2.6820(18) . ?
Rb4 F9 3.087(10) 17_666 ?
Rb4 F9 3.026(9) 18_666 ?
Rb4 F10A 2.882(8) 17_666 ?
Rb4 F10B 2.866(9) 18_666 ?
Rb5 F2 2.6751(18) . ?
Rb5 F2 2.6751(18) 3 ?
Rb5 F6 3.322(3) 18_566 ?
Rb5 F7 2.7412(18) 18_566 ?
Rb5 F7 2.7412(18) 28_665 ?
Rb5 F9 3.227(9) 4 ?
Rb5 F9 3.227(9) 2 ?
Rb5 F10A 2.891(9) . ?
Rb5 F10A 2.892(9) 3 ?
Rb5 F10B 2.820(8) . ?
Rb5 F10B 2.820(8) 3 ?
Al1 F1 1.804(2) . ?
Al1 F1 1.804(2) 14 ?
Al1 F2 1.8028(19) . ?
Al1 F2 1.803(2) 14 ?
Al1 F3 1.7997(19) . ?
Al1 F3 1.7996(19) 14 ?
Al2 F4 1.7945(19) 11_655 ?
Al2 F4 1.7945(19) 8 ?
Al2 F4 1.7944(19) . ?
Al2 F4 1.7945(19) 14_655 ?
Al2 F6 1.828(3) . ?
Al2 F6 1.828(3) 14_655 ?
Al3 F5 1.8143(19) . ?
Al3 F5 1.8143(19) 2_655 ?
Al3 F7 1.8249(19) 2_655 ?
Al3 F7 1.8250(19) . ?
Al3 F8 1.8003(18) 2_655 ?
Al3 F8 1.8003(18) . ?
Al4 F9 1.760(5) . ?
Al4 F9 1.760(5) 3 ?
Al4 F9 1.760(5) 2 ?
Al4 F9 1.760(5) 4 ?
Al4 F10A 1.746(6) 4 ?
Al4 F10A 1.746(6) . ?
Al4 F10A 1.746(6) 3 ?
Al4 F10A 1.746(6) 2 ?
Al4 F10B 1.775(7) 4 ?
Al4 F10B 1.775(7) 3 ?
Al4 F10B 1.775(7) . ?
Al4 F10B 1.775(7) 2 ?
F9 F9 1.682(17) 2 ?
F9 F10A 1.694(14) 2 ?
F9 F10B 1.624(16) 2 ?
F10A F10B 0.983(15) 3 ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
F1 Rb1A Al3 97.74(6) . . ?
F1 Rb1A Al3 143.93(6) 14 . ?
F1 Rb1A Al3 104.76(8) 30_556 . ?
F1 Rb1A F1 132.16(8) 30_556 . ?
F1 Rb1A F1 96.67(8) 30_556 14 ?
F1 Rb1A F1 47.36(7) . 14 ?
F1 Rb1A F2 50.56(6) 30_556 17_666 ?
F1 Rb1A F2 161.28(10) . 17_666 ?
F1 Rb1A F3 70.77(6) 14 30_556 ?
F1 Rb1A F3 83.06(10) 30_556 14 ?
F1 Rb1A F3 117.76(7) . 30_556 ?
F1 Rb1A F3 49.70(6) 30_556 30_556 ?
F1 Rb1A F7 98.49(9) 30_556 2_655 ?
F1 Rb1A F8 133.72(10) 30_556 . ?
F1 Rb1A F10B 101.77(18) . 17_666 ?
F1 Rb1A F10B 85.42(15) 14 17_666 ?
F1 Rb1A F10B 105.60(16) 30_556 17_666 ?
F2 Rb1A Al3 98.80(6) 17_666 . ?
F2 Rb1A F1 117.17(7) 17_666 14 ?
F2 Rb1A F3 46.74(6) 17_666 30_556 ?
F2 Rb1A F10B 63.00(17) 17_666 17_666 ?
F3 Rb1A Al3 103.41(8) 14 . ?
F3 Rb1A Al3 144.41(6) 30_556 . ?
F3 Rb1A F1 50.40(6) 14 14 ?
F3 Rb1A F1 50.55(6) 14 . ?
F3 Rb1A F2 132.43(10) 14 17_666 ?
F3 Rb1A F3 97.77(8) 14 30_556 ?
F3 Rb1A F7 132.91(10) 14 2_655 ?
F3 Rb1A F8 97.06(8) 14 . ?
F3 Rb1A F10B 62.21(13) 30_556 17_666 ?
F3 Rb1A F10B 135.82(16) 14 17_666 ?
F5 Rb1A Al3 29.47(4) . . ?
F5 Rb1A F1 82.90(10) . 30_556 ?
F5 Rb1A F1 131.19(9) . 14 ?
F5 Rb1A F1 98.69(8) . . ?
F5 Rb1A F2 100.03(8) . 17_666 ?
F5 Rb1A F3 81.42(9) . 14 ?
F5 Rb1A F3 131.96(10) . 30_556 ?
F5 Rb1A F7 52.52(6) . 2_655 ?
F5 Rb1A F8 51.79(6) . . ?
F5 Rb1A F10B 141.95(14) . 17_666 ?
F7 Rb1A Al3 30.38(4) 2_655 . ?
F7 Rb1A F1 120.40(7) 2_655 . ?
F7 Rb1A F1 164.80(11) 2_655 14 ?
F7 Rb1A F2 72.52(6) 2_655 17_666 ?
F7 Rb1A F3 119.06(7) 2_655 30_556 ?
F7 Rb1A F8 49.09(6) 2_655 . ?
F7 Rb1A F10B 89.43(14) 2_655 17_666 ?
F8 Rb1A Al3 29.95(4) . . ?
F8 Rb1A F1 71.72(6) . . ?
F8 Rb1A F1 118.93(7) . 14 ?
F8 Rb1A F2 121.29(7) . 17_666 ?
F8 Rb1A F3 165.14(10) . 30_556 ?
F8 Rb1A F10B 105.78(14) . 17_666 ?
F9 Rb1A Al3 106.0(2) 18_666 . ?
F9 Rb1A F1 79.5(2) 18_666 14 ?
F9 Rb1A F1 131.0(2) 18_666 30_556 ?
F9 Rb1A F1 79.4(2) 18_666 . ?
F9 Rb1A F2 87.6(2) 18_666 17_666 ?
F9 Rb1A F3 124.4(2) 18_666 14 ?
F9 Rb1A F3 84.2(2) 18_666 30_556 ?
F9 Rb1A F5 135.4(2) 18_666 . ?
F9 Rb1A F7 89.7(2) 18_666 2_655 ?
F9 Rb1A F8 86.6(2) 18_666 . ?
F9 Rb1A F10B 25.8(2) 18_666 17_666 ?
F10B Rb1A Al3 115.30(13) 17_666 . ?
F1 Rb1B F1 92.87(11) 30_556 14 ?
F1 Rb1B F1 124.79(11) 30_556 . ?
F1 Rb1B F1 47.84(8) . 14 ?
F1 Rb1B F2 49.04(7) 30_556 17_666 ?
F1 Rb1B F2 166.01(14) . 17_666 ?
F1 Rb1B F2 118.18(12) 14 17_666 ?
F1 Rb1B F3 48.42(8) 30_556 30_556 ?
F1 Rb1B F3 119.13(12) . 30_556 ?
F1 Rb1B F3 71.29(9) 14 30_556 ?
F1 Rb1B F7 93.80(11) 30_556 2_655 ?
F1 Rb1B F8 125.15(12) 30_556 . ?
F1 Rb1B F10A 91.97(16) . 17_666 ?
F1 Rb1B F10A 142.42(18) 30_556 17_666 ?
F1 Rb1B F10A 109.51(16) 14 17_666 ?
F1 Rb1B F10B 109.4(2) . 17_666 ?
F1 Rb1B F10B 91.01(17) 14 17_666 ?
F1 Rb1B F10B 107.83(18) 30_556 17_666 ?
F2 Rb1B F3 46.88(7) 17_666 30_556 ?
F2 Rb1B F10A 93.39(15) 17_666 17_666 ?
F2 Rb1B F10B 66.56(18) 17_666 17_666 ?
F3 Rb1B F1 76.03(9) 14 30_556 ?
F3 Rb1B F1 49.24(7) 14 14 ?
F3 Rb1B F1 49.39(8) 14 . ?
F3 Rb1B F2 124.61(12) 14 17_666 ?
F3 Rb1B F3 93.95(11) 14 30_556 ?
F3 Rb1B F7 124.61(12) 14 2_655 ?
F3 Rb1B F8 93.04(11) 14 . ?
F3 Rb1B F10A 109.95(14) 30_556 17_666 ?
F3 Rb1B F10A 141.31(18) 14 17_666 ?
F3 Rb1B F10B 65.68(15) 30_556 17_666 ?
F3 Rb1B F10B 140.13(19) 14 17_666 ?
F5 Rb1B F1 123.44(12) . 14 ?
F5 Rb1B F1 94.58(11) . . ?
F5 Rb1B F1 75.46(9) . 30_556 ?
F5 Rb1B F2 95.26(11) . 17_666 ?
F5 Rb1B F3 74.39(9) . 14 ?
F5 Rb1B F3 123.65(12) . 30_556 ?
F5 Rb1B F7 50.59(7) . 2_655 ?
F5 Rb1B F8 50.08(7) . . ?
F5 Rb1B F10A 112.61(15) . 17_666 ?
F5 Rb1B F10B 145.48(19) . 17_666 ?
F7 Rb1B F1 121.42(13) 2_655 . ?
F7 Rb1B F1 169.15(14) 2_655 14 ?
F7 Rb1B F2 72.58(9) 2_655 17_666 ?
F7 Rb1B F3 119.44(12) 2_655 30_556 ?
F7 Rb1B F8 49.15(7) 2_655 . ?
F7 Rb1B F10A 69.51(14) 2_655 17_666 ?
F7 Rb1B F10B 95.08(17) 2_655 17_666 ?
F8 Rb1B F1 72.26(9) . . ?
F8 Rb1B F1 120.07(12) . 14 ?
F8 Rb1B F2 121.73(12) . 17_666 ?
F8 Rb1B F3 168.51(13) . 30_556 ?
F8 Rb1B F10A 69.21(13) . 17_666 ?
F8 Rb1B F10B 113.46(16) . 17_666 ?
F9 Rb1B F1 135.7(3) 18_666 30_556 ?
F9 Rb1B F1 85.0(3) 18_666 14 ?
F9 Rb1B F1 85.0(2) 18_666 . ?
F9 Rb1B F2 93.7(2) 18_666 17_666 ?
F9 Rb1B F3 129.0(3) 18_666 14 ?
F9 Rb1B F3 89.9(3) 18_666 30_556 ?
F9 Rb1B F5 140.1(3) 18_666 . ?
F9 Rb1B F7 96.2(3) 18_666 2_655 ?
F9 Rb1B F8 92.8(3) 18_666 . ?
F9 Rb1B F10A 28.0(3) 18_666 17_666 ?
F9 Rb1B F10B 28.3(3) 18_666 17_666 ?
F10B Rb1B F10A 44.49(15) 17_666 17_666 ?
F2 Rb2A Al2 105.22(8) 32_656 . ?
F2 Rb2A Al2 143.60(4) 19_666 . ?
F2 Rb2A F2 50.27(7) 32_656 19_666 ?
F2 Rb2A F3 50.50(6) 32_656 32_656 ?
F2 Rb2A F4 133.95(10) 32_656 . ?
F2 Rb2A F4 99.07(8) 32_656 8 ?
F2 Rb2A F7 71.94(5) 19_666 2_655 ?
F2 Rb2A F7 83.11(10) 32_656 . ?
F2 Rb2A F7 97.82(8) 32_656 2_655 ?
F2 Rb2A F8 131.93(10) 32_656 . ?
F2 Rb2A F8 118.56(6) 19_666 . ?
F3 Rb2A Al2 96.85(4) 32_656 . ?
F3 Rb2A F2 47.35(5) 32_656 19_666 ?
F3 Rb2A F7 119.02(6) 32_656 2_655 ?
F3 Rb2A F8 163.16(9) 32_656 . ?
F4 Rb2A Al2 29.54(4) . . ?
F4 Rb2A Al2 29.56(4) 8 . ?
F4 Rb2A F2 118.38(6) 8 19_666 ?
F4 Rb2A F2 162.60(11) . 19_666 ?
F4 Rb2A F3 118.97(7) . 32_656 ?
F4 Rb2A F3 71.47(6) 8 32_656 ?
F4 Rb2A F4 47.79(7) . 8 ?
F4 Rb2A F7 163.01(11) 8 2_655 ?
F4 Rb2A F7 118.93(6) . 2_655 ?
F4 Rb2A F8 119.93(6) 8 . ?
F4 Rb2A F8 72.45(5) . . ?
F6 Rb2A Al2 29.15(5) . . ?
F6 Rb2A F2 132.45(9) . 19_666 ?
F6 Rb2A F2 83.35(10) . 32_656 ?
F6 Rb2A F3 97.75(6) . 32_656 ?
F6 Rb2A F4 51.62(6) . . ?
F6 Rb2A F4 51.36(6) . 8 ?
F6 Rb2A F7 84.00(10) . . ?
F6 Rb2A F7 133.17(10) . 2_655 ?
F6 Rb2A F8 99.10(6) . . ?
F6 Rb2A F10B 135.25(19) . 19_666 ?
F7 Rb2A Al2 105.43(8) . . ?
F7 Rb2A Al2 144.12(4) 2_655 . ?
F7 Rb2A F2 98.18(8) . 19_666 ?
F7 Rb2A F3 132.60(10) . 32_656 ?
F7 Rb2A F4 134.21(10) . 8 ?
F7 Rb2A F4 99.14(8) . . ?
F7 Rb2A F7 50.13(7) . 2_655 ?
F7 Rb2A F8 49.95(5) . . ?
F7 Rb2A F8 46.90(5) 2_655 . ?
F8 Rb2A Al2 97.83(4) . . ?
F10A Rb2A Al2 105.5(2) 17_666 . ?
F10A Rb2A F2 134.06(19) 17_666 32_656 ?
F10A Rb2A F2 85.47(17) 17_666 19_666 ?
F10A Rb2A F3 92.5(3) 17_666 32_656 ?
F10A Rb2A F4 84.56(18) 17_666 . ?
F10A Rb2A F4 91.3(3) 17_666 8 ?
F10A Rb2A F6 134.3(2) 17_666 . ?
F10A Rb2A F7 75.5(3) 17_666 2_655 ?
F10A Rb2A F7 119.8(3) 17_666 . ?
F10A Rb2A F8 75.6(3) 17_666 . ?
F10A Rb2A F10B 20.6(3) 17_666 19_666 ?
F10B Rb2A Al2 107.1(2) 19_666 . ?
F10B Rb2A F2 116.0(3) 19_666 32_656 ?
F10B Rb2A F2 71.8(3) 19_666 19_666 ?
F10B Rb2A F3 71.9(3) 19_666 32_656 ?
F10B Rb2A F4 94.5(3) 19_666 . ?
F10B Rb2A F4 84.75(18) 19_666 8 ?
F10B Rb2A F7 86.21(19) 19_666 2_655 ?
F10B Rb2A F7 135.4(2) 19_666 . ?
F10B Rb2A F8 95.8(3) 19_666 . ?
F2 Rb2B Rb4 166.4(3) 32_656 . ?
F2 Rb2B Rb4 141.0(2) 19_666 . ?
F2 Rb2B F2 48.88(10) 32_656 19_666 ?
F2 Rb2B F3 49.19(9) 32_656 32_656 ?
F2 Rb2B F4 95.47(16) 32_656 8 ?
F2 Rb2B F4 126.4(2) 32_656 . ?
F2 Rb2B F7 75.92(19) 32_656 . ?
F2 Rb2B F7 93.47(17) 32_656 2_655 ?
F2 Rb2B F7 72.02(10) 19_666 2_655 ?
F2 Rb2B F8 118.87(14) 19_666 . ?
F2 Rb2B F8 123.8(2) 32_656 . ?
F3 Rb2B Rb4 142.7(2) 32_656 . ?
F3 Rb2B F2 47.63(8) 32_656 19_666 ?
F3 Rb2B F7 119.65(14) 32_656 2_655 ?
F3 Rb2B F8 166.48(16) 32_656 . ?
F4 Rb2B Rb4 85.41(13) 8 . ?
F4 Rb2B Rb4 46.18(8) . . ?
F4 Rb2B F2 119.96(15) 8 19_666 ?
F4 Rb2B F2 168.30(17) . 19_666 ?
F4 Rb2B F3 72.33(11) 8 32_656 ?
F4 Rb2B F3 120.68(15) . 32_656 ?
F4 Rb2B F4 48.35(10) . 8 ?
F4 Rb2B F7 119.67(15) . 2_655 ?
F4 Rb2B F7 168.01(17) 8 2_655 ?
F4 Rb2B F8 72.82(11) . . ?
F4 Rb2B F8 121.17(15) 8 . ?
F6 Rb2B Rb4 94.07(12) . . ?
F6 Rb2B F2 76.37(19) . 32_656 ?
F6 Rb2B F2 124.8(2) . 19_666 ?
F6 Rb2B F3 94.10(16) . 32_656 ?
F6 Rb2B F4 50.40(10) . . ?
F6 Rb2B F4 50.31(10) . 8 ?
F6 Rb2B F7 124.9(2) . 2_655 ?
F6 Rb2B F7 76.73(19) . . ?
F6 Rb2B F8 94.88(16) . . ?
F7 Rb2B Rb4 92.63(12) . . ?
F7 Rb2B Rb4 84.04(12) 2_655 . ?
F7 Rb2B F2 93.79(17) . 19_666 ?
F7 Rb2B F3 124.7(2) . 32_656 ?
F7 Rb2B F4 94.96(17) . . ?
F7 Rb2B F4 126.6(2) . 8 ?
F7 Rb2B F7 48.52(10) . 2_655 ?
F7 Rb2B F8 48.39(9) . . ?
F7 Rb2B F8 46.86(8) 2_655 . ?
F8 Rb2B Rb4 46.43(7) . . ?
F10A Rb2B Rb4 53.7(2) 17_666 . ?
F10A Rb2B F2 139.0(3) 17_666 32_656 ?
F10A Rb2B F2 91.2(3) 17_666 19_666 ?
F10A Rb2B F3 99.6(4) 17_666 32_656 ?
F10A Rb2B F4 98.7(4) 17_666 8 ?
F10A Rb2B F4 90.7(3) 17_666 . ?
F10A Rb2B F6 139.8(3) 17_666 . ?
F10A Rb2B F7 79.6(4) 17_666 2_655 ?
F10A Rb2B F7 122.5(4) 17_666 . ?
F10A Rb2B F8 79.8(3) 17_666 . ?
F10A Rb2B F10B 23.2(3) 17_666 19_666 ?
F10B Rb2B Rb4 74.4(4) 19_666 . ?
F10B Rb2B F2 75.9(3) 19_666 19_666 ?
F10B Rb2B F2 119.0(4) 19_666 32_656 ?
F10B Rb2B F3 76.4(4) 19_666 32_656 ?
F10B Rb2B F4 102.0(4) 19_666 . ?
F10B Rb2B F4 91.1(3) 19_666 8 ?
F10B Rb2B F6 140.9(3) 19_666 . ?
F10B Rb2B F7 91.5(3) 19_666 2_655 ?
F10B Rb2B F7 139.6(3) 19_666 . ?
F10B Rb2B F8 102.5(4) 19_666 . ?
F1 Rb3 F2 46.81(5) . 14 ?
F3 Rb3 F1 47.28(5) 14 . ?
F3 Rb3 F2 46.93(5) 14 14 ?
F4 Rb3 F1 163.23(5) 17_766 . ?
F4 Rb3 F1 117.77(5) 30_556 . ?
F4 Rb3 F2 118.33(5) 17_766 14 ?
F4 Rb3 F2 89.88(6) 30_556 14 ?
F4 Rb3 F3 118.44(5) 17_766 14 ?
F4 Rb3 F3 70.70(5) 30_556 14 ?
F4 Rb3 F4 48.03(7) 17_766 30_556 ?
F4 Rb3 F5 167.66(5) 30_556 18_666 ?
F4 Rb3 F5 122.07(5) 17_766 18_666 ?
F4 Rb3 F6 48.24(6) 17_766 17_766 ?
F4 Rb3 F7 92.76(6) 17_766 17_766 ?
F5 Rb3 F1 91.66(6) . . ?
F5 Rb3 F1 70.41(5) 18_666 . ?
F5 Rb3 F1 122.40(5) 2_655 . ?
F5 Rb3 F2 117.92(5) . 14 ?
F5 Rb3 F2 166.78(5) 2_655 14 ?
F5 Rb3 F2 90.15(5) 18_666 14 ?
F5 Rb3 F3 117.56(5) 18_666 14 ?
F5 Rb3 F3 71.06(5) . 14 ?
F5 Rb3 F3 121.16(5) 2_655 14 ?
F5 Rb3 F4 90.42(6) 2_655 30_556 ?
F5 Rb3 F4 69.66(5) . 30_556 ?
F5 Rb3 F4 70.86(5) 2_655 17_766 ?
F5 Rb3 F4 90.47(6) . 17_766 ?
F5 Rb3 F5 92.36(5) 2_655 18_666 ?
F5 Rb3 F5 50.24(6) 2_655 . ?
F5 Rb3 F5 120.853(14) . 18_666 ?
F5 Rb3 F6 118.93(6) 2_655 17_766 ?
F5 Rb3 F6 117.55(5) . 17_766 ?
F5 Rb3 F7 168.13(5) . 17_766 ?
F5 Rb3 F7 120.49(5) 2_655 17_766 ?
F5 Rb3 F8 71.70(5) 2_655 17_766 ?
F5 Rb3 F8 121.65(5) . 17_766 ?
F6 Rb3 F1 116.88(5) 17_766 . ?
F6 Rb3 F2 70.26(5) 17_766 14 ?
F6 Rb3 F3 88.91(4) 17_766 14 ?
F6 Rb3 F4 47.96(6) 17_766 30_556 ?
F6 Rb3 F5 120.86(5) 17_766 18_666 ?
F7 Rb3 F1 88.54(6) 17_766 . ?
F7 Rb3 F2 70.24(5) 17_766 14 ?
F7 Rb3 F3 116.94(5) 17_766 14 ?
F7 Rb3 F4 120.49(5) 17_766 30_556 ?
F7 Rb3 F5 48.34(5) 17_766 18_666 ?
F7 Rb3 F6 72.62(5) 17_766 17_766 ?
F8 Rb3 F1 118.44(5) 17_766 . ?
F8 Rb3 F1 72.16(5) . . ?
F8 Rb3 F2 118.80(5) . 14 ?
F8 Rb3 F2 118.93(5) 17_766 14 ?
F8 Rb3 F3 91.23(5) . 14 ?
F8 Rb3 F3 163.66(5) 17_766 14 ?
F8 Rb3 F4 121.83(5) 17_766 30_556 ?
F8 Rb3 F4 119.82(5) . 30_556 ?
F8 Rb3 F4 73.95(5) 17_766 17_766 ?
F8 Rb3 F4 121.08(5) . 17_766 ?
F8 Rb3 F5 50.29(5) . . ?
F8 Rb3 F5 70.62(5) . 18_666 ?
F8 Rb3 F5 50.45(5) . 2_655 ?
F8 Rb3 F5 48.33(5) 17_766 18_666 ?
F8 Rb3 F6 166.63(6) . 17_766 ?
F8 Rb3 F6 93.02(4) 17_766 17_766 ?
F8 Rb3 F7 48.87(5) 17_766 17_766 ?
F8 Rb3 F7 118.86(5) . 17_766 ?
F8 Rb3 F8 90.60(5) . 17_766 ?
Rb1B Rb4 Rb2B 132.06(13) . 8 ?
Rb2B Rb4 Rb1B 80.73(9) . . ?
Rb2B Rb4 Rb2B 80.02(14) . 8 ?
F1 Rb4 Rb1B 57.47(7) . . ?
F1 Rb4 Rb2B 135.52(9) . 8 ?
F1 Rb4 Rb2B 136.71(9) . . ?
F1 Rb4 F3 86.94(7) . 29_666 ?
F1 Rb4 F5 78.72(6) . 18_666 ?
F1 Rb4 F9 79.79(13) . 17_666 ?
F1 Rb4 F9 80.56(15) . 18_666 ?
F1 Rb4 F10A 112.8(3) . 17_666 ?
F1 Rb4 F10B 109.5(3) . 18_666 ?
F3 Rb4 Rb1B 136.22(7) 29_666 . ?
F3 Rb4 Rb2B 57.22(10) 29_666 8 ?
F3 Rb4 Rb2B 135.52(9) 29_666 . ?
F3 Rb4 F5 77.25(6) 29_666 18_666 ?
F3 Rb4 F9 117.46(18) 29_666 18_666 ?
F3 Rb4 F9 85.62(15) 29_666 17_666 ?
F3 Rb4 F10A 124.6(2) 29_666 17_666 ?
F3 Rb4 F10B 77.67(17) 29_666 18_666 ?
F4 Rb4 Rb1B 136.20(8) . . ?
F4 Rb4 Rb2B 57.22(10) . . ?
F4 Rb4 Rb2B 56.98(10) . 8 ?
F4 Rb4 F1 154.94(7) . . ?
F4 Rb4 F3 86.85(7) . 29_666 ?
F4 Rb4 F5 76.23(7) . 18_666 ?
F4 Rb4 F8 88.89(7) . . ?
F4 Rb4 F9 123.84(14) . 17_666 ?
F4 Rb4 F9 123.60(16) . 18_666 ?
F4 Rb4 F10A 90.5(3) . 17_666 ?
F4 Rb4 F10B 92.8(3) . 18_666 ?
F5 Rb4 Rb1B 114.76(6) 18_666 . ?
F5 Rb4 Rb2B 113.37(13) 18_666 . ?
F5 Rb4 Rb2B 113.17(13) 18_666 8 ?
F5 Rb4 F9 153.09(10) 18_666 17_666 ?
F8 Rb4 Rb1B 56.75(7) . . ?
F8 Rb4 Rb2B 59.83(11) . . ?
F8 Rb4 Rb2B 138.05(8) . 8 ?
F8 Rb4 F1 85.81(7) . . ?
F8 Rb4 F3 153.20(7) . 29_666 ?
F8 Rb4 F5 76.04(6) . 18_666 ?
F8 Rb4 F9 118.28(17) . 17_666 ?
F8 Rb4 F9 86.68(16) . 18_666 ?
F8 Rb4 F10A 81.84(18) . 17_666 ?
F8 Rb4 F10B 129.00(17) . 18_666 ?
F9 Rb4 Rb1B 65.18(18) 17_666 . ?
F9 Rb4 Rb1B 39.38(11) 18_666 . ?
F9 Rb4 Rb2B 92.84(15) 18_666 8 ?
F9 Rb4 Rb2B 72.66(19) 17_666 8 ?
F9 Rb4 Rb2B 93.41(16) 17_666 . ?
F9 Rb4 Rb2B 72.5(2) 18_666 . ?
F9 Rb4 F5 153.82(10) 18_666 18_666 ?
F9 Rb4 F9 31.9(3) 18_666 17_666 ?
F10A Rb4 Rb1B 60.9(3) 17_666 . ?
F10A Rb4 Rb2B 42.3(2) 17_666 . ?
F10A Rb4 Rb2B 75.5(3) 17_666 8 ?
F10A Rb4 F5 154.29(13) 17_666 18_666 ?
F10A Rb4 F9 51.54(17) 17_666 17_666 ?
F10A Rb4 F9 33.2(3) 17_666 18_666 ?
F10B Rb4 Rb1B 90.3(2) 18_666 . ?
F10B Rb4 Rb2B 78.9(3) 18_666 . ?
F10B Rb4 Rb2B 43.0(3) 18_666 8 ?
F10B Rb4 F5 153.09(16) 18_666 18_666 ?
F10B Rb4 F9 31.4(3) 18_666 17_666 ?
F10B Rb4 F9 51.1(2) 18_666 18_666 ?
F10B Rb4 F10A 47.20(18) 18_666 17_666 ?
F2 Rb5 Rb1B 58.81(7) 3 27_565 ?
F2 Rb5 Rb1B 135.82(8) . 27_565 ?
F2 Rb5 F2 149.48(10) 3 . ?
F2 Rb5 F6 74.74(5) 3 18_566 ?
F2 Rb5 F6 74.74(5) . 18_566 ?
F2 Rb5 F7 87.10(7) . 28_665 ?
F2 Rb5 F7 85.02(7) . 18_566 ?
F2 Rb5 F7 85.02(7) 3 28_665 ?
F2 Rb5 F7 87.10(7) 3 18_566 ?
F2 Rb5 F9 123.35(16) . 4 ?
F2 Rb5 F9 84.97(14) 3 4 ?
F2 Rb5 F9 123.35(16) 3 2 ?
F2 Rb5 F9 84.97(14) . 2 ?
F2 Rb5 F10A 91.8(3) 3 . ?
F2 Rb5 F10A 91.8(3) . 3 ?
F2 Rb5 F10A 115.8(3) . . ?
F2 Rb5 F10A 115.8(3) 3 3 ?
F2 Rb5 F10B 131.08(19) 3 . ?
F2 Rb5 F10B 131.08(19) . 3 ?
F2 Rb5 F10B 78.91(16) 3 3 ?
F2 Rb5 F10B 78.92(16) . . ?
F6 Rb5 Rb1B 112.24(5) 18_566 27_565 ?
F7 Rb5 Rb1B 56.04(7) 28_665 27_565 ?
F7 Rb5 Rb1B 139.12(7) 18_566 27_565 ?
F7 Rb5 F6 74.87(5) 18_566 18_566 ?
F7 Rb5 F6 74.88(5) 28_665 18_566 ?
F7 Rb5 F7 149.75(9) 28_665 18_566 ?
F7 Rb5 F9 83.56(13) 18_566 2 ?
F7 Rb5 F9 124.76(15) 18_566 4 ?
F7 Rb5 F9 124.76(15) 28_665 2 ?
F7 Rb5 F9 83.56(13) 28_665 4 ?
F7 Rb5 F10A 128.92(19) 28_665 . ?
F7 Rb5 F10A 80.43(17) 28_665 3 ?
F7 Rb5 F10A 80.43(17) 18_566 . ?
F7 Rb5 F10A 128.92(19) 18_566 3 ?
F7 Rb5 F10B 112.3(4) 28_665 3 ?
F7 Rb5 F10B 94.7(3) 28_665 . ?
F7 Rb5 F10B 94.7(3) 18_566 3 ?
F7 Rb5 F10B 112.3(4) 18_566 . ?
F9 Rb5 Rb1B 39.13(10) 4 27_565 ?
F9 Rb5 Rb1B 96.39(10) 2 27_565 ?
F9 Rb5 F6 151.37(9) 2 18_566 ?
F9 Rb5 F6 151.37(9) 4 18_566 ?
F9 Rb5 F9 57.26(17) 4 2 ?
F10A Rb5 Rb1B 79.0(3) . 27_565 ?
F10A Rb5 Rb1B 61.4(3) 3 27_565 ?
F10A Rb5 F6 152.28(11) 3 18_566 ?
F10A Rb5 F6 152.28(11) . 18_566 ?
F10A Rb5 F9 31.5(3) . 2 ?
F10A Rb5 F9 31.5(3) 3 4 ?
F10A Rb5 F9 45.4(2) . 4 ?
F10A Rb5 F9 45.4(2) 3 2 ?
F10A Rb5 F10A 55.4(2) . 3 ?
F10B Rb5 Rb1B 59.5(3) 3 27_565 ?
F10B Rb5 Rb1B 80.7(3) . 27_565 ?
F10B Rb5 F6 152.02(14) 3 18_566 ?
F10B Rb5 F6 152.02(14) . 18_566 ?
F10B Rb5 F9 30.2(3) 3 4 ?
F10B Rb5 F9 46.7(2) 3 2 ?
F10B Rb5 F9 30.2(3) . 2 ?
F10B Rb5 F9 46.7(2) . 4 ?
F10B Rb5 F10A 51.50(19) 3 3 ?
F10B Rb5 F10A 19.8(3) . 3 ?
F10B Rb5 F10A 51.50(19) . . ?
F10B Rb5 F10A 19.8(3) 3 . ?
F10B Rb5 F10B 56.0(3) . 3 ?
Rb1A Al1 Rb1A 86.81(10) . 14 ?
Rb1A Al1 Rb1A 166.14(9) 18_666 17_666 ?
Rb1A Al1 Rb1A 104.41(4) . 18_666 ?
Rb1A Al1 Rb1A 64.90(5) 14 18_666 ?
Rb1A Al1 Rb1A 64.90(5) . 17_666 ?
Rb1A Al1 Rb1A 104.41(4) 14 17_666 ?
Rb1A Al1 Rb2A 104.84(5) 14 28_665 ?
Rb1A Al1 Rb2A 166.51(7) 14 27_565 ?
Rb1A Al1 Rb2A 166.51(7) . 28_665 ?
Rb1A Al1 Rb2A 104.84(5) . 27_565 ?
Rb2A Al1 Rb1A 104.89(6) 27_565 18_666 ?
Rb2A Al1 Rb1A 104.89(6) 28_665 17_666 ?
Rb2A Al1 Rb1A 86.96(7) 28_665 18_666 ?
Rb2A Al1 Rb1A 86.96(7) 27_565 17_666 ?
Rb2A Al1 Rb2A 64.54(5) 27_565 28_665 ?
F1 Al1 Rb1A 46.41(8) 14 17_666 ?
F1 Al1 Rb1A 58.60(8) . . ?
F1 Al1 Rb1A 121.18(8) . 17_666 ?
F1 Al1 Rb1A 121.18(8) 14 18_666 ?
F1 Al1 Rb1A 59.11(9) 14 . ?
F1 Al1 Rb1A 59.11(9) . 14 ?
F1 Al1 Rb1A 58.60(8) 14 14 ?
F1 Al1 Rb1A 46.41(8) . 18_666 ?
F1 Al1 Rb2A 121.16(8) . 27_565 ?
F1 Al1 Rb2A 133.34(9) . 28_665 ?
F1 Al1 Rb2A 121.16(8) 14 28_665 ?
F1 Al1 Rb2A 133.34(9) 14 27_565 ?
F1 Al1 F1 89.22(15) 14 . ?
F2 Al1 Rb1A 58.12(8) 14 18_666 ?
F2 Al1 Rb1A 121.07(8) 14 . ?
F2 Al1 Rb1A 120.67(8) . . ?
F2 Al1 Rb1A 134.31(9) . 18_666 ?
F2 Al1 Rb1A 134.31(9) 14 17_666 ?
F2 Al1 Rb1A 58.12(8) . 17_666 ?
F2 Al1 Rb1A 120.67(8) 14 14 ?
F2 Al1 Rb1A 121.07(8) . 14 ?
F2 Al1 Rb2A 47.38(9) . 28_665 ?
F2 Al1 Rb2A 58.86(9) . 27_565 ?
F2 Al1 Rb2A 58.85(9) 14 28_665 ?
F2 Al1 Rb2A 47.38(9) 14 27_565 ?
F2 Al1 F1 90.33(10) . 14 ?
F2 Al1 F1 90.33(10) 14 . ?
F2 Al1 F1 179.27(11) 14 14 ?
F2 Al1 F1 179.27(11) . . ?
F2 Al1 F2 90.13(15) . 14 ?
F3 Al1 Rb1A 133.85(9) 14 14 ?
F3 Al1 Rb1A 119.78(8) 14 18_666 ?
F3 Al1 Rb1A 133.86(9) . . ?
F3 Al1 Rb1A 47.05(9) . 14 ?
F3 Al1 Rb1A 47.05(9) 14 . ?
F3 Al1 Rb1A 60.35(8) 14 17_666 ?
F3 Al1 Rb1A 119.78(8) . 17_666 ?
F3 Al1 Rb1A 60.35(8) . 18_666 ?
F3 Al1 Rb2A 58.20(8) . 28_665 ?
F3 Al1 Rb2A 120.91(9) . 27_565 ?
F3 Al1 Rb2A 58.20(8) 14 27_565 ?
F3 Al1 Rb2A 120.91(9) 14 28_665 ?
F3 Al1 F1 90.28(11) . 14 ?
F3 Al1 F1 90.36(11) 14 14 ?
F3 Al1 F1 90.28(11) 14 . ?
F3 Al1 F1 90.36(11) . . ?
F3 Al1 F2 90.21(11) 14 14 ?
F3 Al1 F2 90.21(11) . . ?
F3 Al1 F2 89.16(11) . 14 ?
F3 Al1 F2 89.16(11) 14 . ?
F3 Al1 F3 179.10(15) 14 . ?
Rb2A Al2 Rb2A 179.04(3) 14_655 . ?
Rb2A Al2 Rb2A 86.80(11) 8 . ?
Rb2A Al2 Rb2A 179.04(3) 8 11_655 ?
Rb2A Al2 Rb2A 93.21(11) 11_655 . ?
Rb2A Al2 Rb2A 93.21(11) 14_655 8 ?
Rb2A Al2 Rb2A 86.80(11) 14_655 11_655 ?
Rb2A Al2 Rb2B 98.14(18) 8 14_655 ?
Rb2A Al2 Rb2B 98.14(18) 11_655 . ?
Rb2A Al2 Rb2B 4.94(8) 14_655 14_655 ?
Rb2A Al2 Rb2B 175.01(8) . 14_655 ?
Rb2A Al2 Rb2B 4.94(8) . . ?
Rb2A Al2 Rb2B 175.01(8) 14_655 . ?
Rb2A Al2 Rb2B 81.86(18) 8 . ?
Rb2A Al2 Rb2B 81.86(18) 11_655 14_655 ?
Rb2B Al2 Rb2B 179.47(14) . 14_655 ?
F4 Al2 Rb2A 58.42(8) 11_655 11_655 ?
F4 Al2 Rb2A 58.42(9) . . ?
F4 Al2 Rb2A 121.42(8) 11_655 . ?
F4 Al2 Rb2A 59.36(9) 14_655 11_655 ?
F4 Al2 Rb2A 59.36(9) 11_655 14_655 ?
F4 Al2 Rb2A 121.42(8) . 11_655 ?
F4 Al2 Rb2A 121.42(8) 14_655 8 ?
F4 Al2 Rb2A 120.79(9) 8 11_655 ?
F4 Al2 Rb2A 58.42(9) 14_655 14_655 ?
F4 Al2 Rb2A 120.79(9) . 14_655 ?
F4 Al2 Rb2A 59.36(9) . 8 ?
F4 Al2 Rb2A 120.79(9) 11_655 8 ?
F4 Al2 Rb2A 59.36(9) 8 . ?
F4 Al2 Rb2A 58.42(8) 8 8 ?
F4 Al2 Rb2A 120.79(9) 14_655 . ?
F4 Al2 Rb2A 121.42(9) 8 14_655 ?
F4 Al2 Rb2B 55.87(12) . . ?
F4 Al2 Rb2B 123.68(12) . 14_655 ?
F4 Al2 Rb2B 123.98(12) 8 14_655 ?
F4 Al2 Rb2B 123.98(12) 11_655 . ?
F4 Al2 Rb2B 56.46(12) 11_655 14_655 ?
F4 Al2 Rb2B 56.46(12) 8 . ?
F4 Al2 Rb2B 123.68(12) 14_655 . ?
F4 Al2 Rb2B 55.87(12) 14_655 14_655 ?
F4 Al2 F4 90.64(16) 11_655 8 ?
F4 Al2 F4 89.36(16) . 8 ?
F4 Al2 F4 179.80(16) . 11_655 ?
F4 Al2 F4 90.64(16) . 14_655 ?
F4 Al2 F4 179.81(16) 8 14_655 ?
F4 Al2 F4 89.36(16) 11_655 14_655 ?
F4 Al2 F6 90.10(8) 8 . ?
F4 Al2 F6 90.10(8) 11_655 14_655 ?
F4 Al2 F6 89.90(8) 14_655 14_655 ?
F4 Al2 F6 89.90(8) . . ?
F4 Al2 F6 89.90(8) 8 14_655 ?
F4 Al2 F6 90.10(8) . 14_655 ?
F4 Al2 F6 89.90(8) 11_655 . ?
F4 Al2 F6 90.10(8) 14_655 . ?
F6 Al2 Rb2A 46.61(5) 14_655 14_655 ?
F6 Al2 Rb2A 133.40(5) 14_655 . ?
F6 Al2 Rb2A 46.60(5) . . ?
F6 Al2 Rb2A 46.61(5) 14_655 8 ?
F6 Al2 Rb2A 133.39(5) 14_655 11_655 ?
F6 Al2 Rb2A 133.39(5) . 14_655 ?
F6 Al2 Rb2A 46.61(5) . 11_655 ?
F6 Al2 Rb2A 133.39(5) . 8 ?
F6 Al2 Rb2B 51.54(13) . . ?
F6 Al2 Rb2B 128.46(13) . 14_655 ?
F6 Al2 Rb2B 51.54(13) 14_655 14_655 ?
F6 Al2 Rb2B 128.46(13) 14_655 . ?
F6 Al2 F6 180.0 14_655 . ?
Rb1A Al3 Rb1A 169.68(9) 2_655 . ?
Rb1A Al3 Rb1B 4.87(4) . . ?
Rb1A Al3 Rb1B 4.87(4) 2_655 2_655 ?
Rb1A Al3 Rb1B 173.24(8) . 2_655 ?
Rb1A Al3 Rb1B 173.24(8) 2_655 . ?
Rb1A Al3 Rb3 68.35(3) . . ?
Rb1A Al3 Rb3 102.94(5) 2_655 . ?
Rb1A Al3 Rb3 102.94(5) . 2_655 ?
Rb1A Al3 Rb3 68.35(3) 2_655 2_655 ?
Rb1B Al3 Rb1B 177.87(10) 2_655 . ?
Rb3 Al3 Rb1B 70.38(5) . . ?
Rb3 Al3 Rb1B 107.81(5) 2_655 . ?
Rb3 Al3 Rb1B 107.80(5) . 2_655 ?
Rb3 Al3 Rb1B 70.38(5) 2_655 2_655 ?
Rb3 Al3 Rb3 72.50(2) . 2_655 ?
F5 Al3 Rb1A 122.51(8) . 2_655 ?
F5 Al3 Rb1A 48.37(8) . . ?
F5 Al3 Rb1A 122.51(8) 2_655 . ?
F5 Al3 Rb1A 48.37(8) 2_655 2_655 ?
F5 Al3 Rb1B 53.23(8) 2_655 2_655 ?
F5 Al3 Rb1B 124.91(9) 2_655 . ?
F5 Al3 Rb1B 53.23(8) . . ?
F5 Al3 Rb1B 124.91(9) . 2_655 ?
F5 Al3 Rb3 54.59(6) 2_655 . ?
F5 Al3 Rb3 56.04(7) 2_655 2_655 ?
F5 Al3 Rb3 54.59(6) . 2_655 ?
F5 Al3 Rb3 56.04(7) . . ?
F5 Al3 F5 90.25(13) . 2_655 ?
F5 Al3 F7 90.07(9) . 2_655 ?
F5 Al3 F7 179.18(10) 2_655 2_655 ?
F5 Al3 F7 179.18(10) . . ?
F5 Al3 F7 90.07(9) 2_655 . ?
F7 Al3 Rb1A 57.28(7) . 2_655 ?
F7 Al3 Rb1A 131.92(8) 2_655 2_655 ?
F7 Al3 Rb1A 57.28(7) 2_655 . ?
F7 Al3 Rb1A 131.92(8) . . ?
F7 Al3 Rb1B 54.81(8) 2_655 . ?
F7 Al3 Rb1B 127.06(9) . . ?
F7 Al3 Rb1B 54.81(8) . 2_655 ?
F7 Al3 Rb1B 127.06(9) 2_655 2_655 ?
F7 Al3 Rb3 125.08(6) 2_655 . ?
F7 Al3 Rb3 125.08(6) . 2_655 ?
F7 Al3 Rb3 124.72(7) 2_655 2_655 ?
F7 Al3 Rb3 124.72(7) . . ?
F7 Al3 F7 89.62(13) 2_655 . ?
F8 Al3 Rb1A 58.95(7) 2_655 2_655 ?
F8 Al3 Rb1A 121.15(7) 2_655 . ?
F8 Al3 Rb1A 58.95(7) . . ?
F8 Al3 Rb1A 121.16(7) . 2_655 ?
F8 Al3 Rb1B 56.14(8) 2_655 2_655 ?
F8 Al3 Rb1B 56.14(8) . . ?
F8 Al3 Rb1B 123.89(8) 2_655 . ?
F8 Al3 Rb1B 123.89(8) . 2_655 ?
F8 Al3 Rb3 54.27(7) . . ?
F8 Al3 Rb3 126.75(8) . 2_655 ?
F8 Al3 Rb3 126.75(8) 2_655 . ?
F8 Al3 Rb3 54.27(7) 2_655 2_655 ?
F8 Al3 F5 90.64(9) . . ?
F8 Al3 F5 90.08(9) . 2_655 ?
F8 Al3 F5 90.64(9) 2_655 2_655 ?
F8 Al3 F5 90.08(9) 2_655 . ?
F8 Al3 F7 90.11(10) . . ?
F8 Al3 F7 90.11(10) 2_655 2_655 ?
F8 Al3 F7 89.16(10) 2_655 . ?
F8 Al3 F7 89.16(10) . 2_655 ?
F8 Al3 F8 178.98(15) . 2_655 ?
F9 Al4 F9 57.1(6) 2 . ?
F9 Al4 F9 122.9(6) 3 . ?
F9 Al4 F9 57.1(6) 3 4 ?
F9 Al4 F9 122.9(6) 2 4 ?
F9 Al4 F9 178.0(6) 3 2 ?
F9 Al4 F9 178.0(6) 4 . ?
F9 Al4 F10B 86.6(5) . 4 ?
F9 Al4 F10B 54.7(6) . 2 ?
F9 Al4 F10B 86.6(5) 2 3 ?
F9 Al4 F10B 54.7(6) 4 3 ?
F9 Al4 F10B 127.0(7) 2 4 ?
F9 Al4 F10B 54.7(6) 2 . ?
F9 Al4 F10B 92.0(6) 3 3 ?
F9 Al4 F10B 86.6(5) 4 . ?
F9 Al4 F10B 54.7(6) 3 4 ?
F9 Al4 F10B 92.0(6) . . ?
F9 Al4 F10B 92.0(6) 4 4 ?
F9 Al4 F10B 86.6(5) 3 2 ?
F9 Al4 F10B 92.0(6) 2 2 ?
F9 Al4 F10B 127.0(7) 4 2 ?
F9 Al4 F10B 127.0(7) 3 . ?
F9 Al4 F10B 127.0(7) . 3 ?
F10A Al4 F9 95.8(5) 4 4 ?
F10A Al4 F9 120.5(6) 4 2 ?
F10A Al4 F9 57.8(5) . 2 ?
F10A Al4 F9 57.8(5) 3 4 ?
F10A Al4 F9 85.6(4) 3 2 ?
F10A Al4 F9 120.5(6) 2 4 ?
F10A Al4 F9 120.5(6) 3 . ?
F10A Al4 F9 95.8(5) 3 3 ?
F10A Al4 F9 95.8(5) . . ?
F10A Al4 F9 85.6(4) 2 3 ?
F10A Al4 F9 95.8(5) 2 2 ?
F10A Al4 F9 120.5(6) . 3 ?
F10A Al4 F9 57.8(5) 4 3 ?
F10A Al4 F9 85.6(4) 4 . ?
F10A Al4 F9 85.6(4) . 4 ?
F10A Al4 F9 57.8(5) 2 . ?
F10A Al4 F10A 86.3(8) 3 2 ?
F10A Al4 F10A 100.7(6) 4 2 ?
F10A Al4 F10A 151.5(9) 4 3 ?
F10A Al4 F10A 86.3(8) 4 . ?
F10A Al4 F10A 100.7(6) 3 . ?
F10A Al4 F10A 151.5(9) 2 . ?
F10A Al4 F10B 32.4(5) 2 4 ?
F10A Al4 F10B 175.1(9) 2 3 ?
F10A Al4 F10B 175.1(9) 3 2 ?
F10A Al4 F10B 175.1(9) . 4 ?
F10A Al4 F10B 89.7(4) 4 4 ?
F10A Al4 F10B 89.7(4) . . ?
F10A Al4 F10B 81.6(3) 3 4 ?
F10A Al4 F10B 175.1(9) 4 . ?
F10A Al4 F10B 32.4(5) . 3 ?
F10A Al4 F10B 81.6(3) . 2 ?
F10A Al4 F10B 32.4(5) 4 2 ?
F10A Al4 F10B 81.6(3) 2 . ?
F10A Al4 F10B 89.7(4) 2 2 ?
F10A Al4 F10B 81.6(3) 4 3 ?
F10A Al4 F10B 89.7(4) 3 3 ?
F10A Al4 F10B 32.4(5) 3 . ?
F10B Al4 F10B 94.6(8) . 4 ?
F10B Al4 F10B 144.0(10) . 2 ?
F10B Al4 F10B 144.0(10) 4 3 ?
F10B Al4 F10B 96.4(5) 2 4 ?
F10B Al4 F10B 96.4(5) . 3 ?
F10B Al4 F10B 94.6(8) 2 3 ?
Rb1A F1 Rb1A 83.33(8) 18_666 14 ?
Rb1A F1 Rb1A 106.73(11) . 14 ?
Rb1A F1 Rb1A 159.52(10) 18_666 . ?
Rb1A F1 Rb1B 87.14(9) 18_666 14 ?
Rb1A F1 Rb1B 4.68(8) 18_666 18_666 ?
Rb1A F1 Rb1B 158.12(9) 18_666 . ?
Rb1A F1 Rb3 80.14(7) . . ?
Rb1A F1 Rb3 87.31(7) 18_666 . ?
Rb1A F1 Rb3 168.32(8) 14 . ?
Rb1B F1 Rb1A 163.59(9) 18_666 . ?
Rb1B F1 Rb1A 5.87(5) 14 14 ?
Rb1B F1 Rb1A 82.97(9) 18_666 14 ?
Rb1B F1 Rb1A 5.90(5) . . ?
Rb1B F1 Rb1A 101.71(12) 14 . ?
Rb1B F1 Rb1A 101.79(12) . 14 ?
Rb1B F1 Rb1B 87.13(11) 18_666 14 ?
Rb1B F1 Rb1B 96.61(12) . 14 ?
Rb1B F1 Rb1B 162.70(13) 18_666 . ?
Rb1B F1 Rb3 167.26(9) 14 . ?
Rb1B F1 Rb3 84.46(8) . . ?
Rb1B F1 Rb3 88.27(9) 18_666 . ?
Rb4 F1 Rb1A 83.84(8) . 18_666 ?
Rb4 F1 Rb1A 80.06(7) . . ?
Rb4 F1 Rb1A 82.15(7) . 14 ?
Rb4 F1 Rb1B 78.07(8) . 14 ?
Rb4 F1 Rb1B 88.42(9) . 18_666 ?
Rb4 F1 Rb1B 75.92(8) . . ?
Rb4 F1 Rb3 89.94(6) . . ?
Al1 F1 Rb1A 105.65(10) . 18_666 ?
Al1 F1 Rb1A 91.58(10) . 14 ?
Al1 F1 Rb1A 92.10(9) . . ?
Al1 F1 Rb1B 95.54(10) . . ?
Al1 F1 Rb1B 100.99(11) . 18_666 ?
Al1 F1 Rb1B 94.87(11) . 14 ?
Al1 F1 Rb3 97.67(9) . . ?
Al1 F1 Rb4 168.02(12) . . ?
Rb1A F2 Rb2A 107.51(10) 17_666 27_565 ?
Rb1A F2 Rb3 80.88(7) 17_666 14 ?
Rb1B F2 Rb1A 5.89(5) 17_666 17_666 ?
Rb1B F2 Rb2A 102.52(11) 17_666 27_565 ?
Rb1B F2 Rb2B 97.26(17) 17_666 27_565 ?
Rb1B F2 Rb3 85.31(8) 17_666 14 ?
Rb2A F2 Rb1A 159.98(9) 28_665 17_666 ?
Rb2A F2 Rb1B 158.70(11) 28_665 17_666 ?
Rb2A F2 Rb2A 82.49(8) 28_665 27_565 ?
Rb2A F2 Rb2B 86.50(14) 28_665 27_565 ?
Rb2A F2 Rb2B 4.74(10) 28_665 28_665 ?
Rb2A F2 Rb3 86.95(6) 28_665 14 ?
Rb2A F2 Rb3 167.90(7) 27_565 14 ?
Rb2B F2 Rb1A 163.64(14) 28_665 17_666 ?
Rb2B F2 Rb1A 102.39(17) 27_565 17_666 ?
Rb2B F2 Rb1B 163.12(15) 28_665 17_666 ?
Rb2B F2 Rb2A 5.83(10) 27_565 27_565 ?
Rb2B F2 Rb2A 82.81(11) 28_665 27_565 ?
Rb2B F2 Rb2B 87.1(2) 28_665 27_565 ?
Rb2B F2 Rb3 167.90(11) 27_565 14 ?
Rb2B F2 Rb3 87.16(10) 28_665 14 ?
Rb5 F2 Rb1A 78.79(7) . 17_666 ?
Rb5 F2 Rb1B 74.52(8) . 17_666 ?
Rb5 F2 Rb2A 79.95(7) . 27_565 ?
Rb5 F2 Rb2A 86.19(8) . 28_665 ?
Rb5 F2 Rb2B 75.90(13) . 27_565 ?
Rb5 F2 Rb2B 90.91(14) . 28_665 ?
Rb5 F2 Rb3 93.52(6) . 14 ?
Al1 F2 Rb1A 92.82(9) . 17_666 ?
Al1 F2 Rb1B 96.22(10) . 17_666 ?
Al1 F2 Rb2A 104.36(11) . 28_665 ?
Al1 F2 Rb2A 91.91(9) . 27_565 ?
Al1 F2 Rb2B 95.04(14) . 27_565 ?
Al1 F2 Rb2B 99.63(16) . 28_665 ?
Al1 F2 Rb3 96.43(9) . 14 ?
Al1 F2 Rb5 165.82(12) . . ?
Rb1A F3 Rb1A 82.23(8) 14 18_666 ?
Rb1A F3 Rb1B 4.96(7) 14 14 ?
Rb1A F3 Rb1B 85.69(9) 14 18_666 ?
Rb1A F3 Rb2A 160.69(9) 14 28_665 ?
Rb1A F3 Rb2B 158.61(13) 14 28_665 ?
Rb1A F3 Rb3 86.35(7) 14 14 ?
Rb1B F3 Rb1A 5.76(5) 18_666 18_666 ?
Rb1B F3 Rb1A 82.20(9) 14 18_666 ?
Rb1B F3 Rb1B 86.05(11) 14 18_666 ?
Rb1B F3 Rb2A 164.94(10) 14 28_665 ?
Rb1B F3 Rb2B 163.45(13) 14 28_665 ?
Rb1B F3 Rb3 87.00(9) 14 14 ?
Rb2A F3 Rb1A 106.29(9) 28_665 18_666 ?
Rb2A F3 Rb1B 101.58(10) 28_665 18_666 ?
Rb2A F3 Rb3 82.69(7) 28_665 14 ?
Rb2B F3 Rb1A 101.58(16) 28_665 18_666 ?
Rb2B F3 Rb1B 96.68(16) 28_665 18_666 ?
Rb2B F3 Rb2A 5.87(10) 28_665 28_665 ?
Rb2B F3 Rb3 86.70(13) 28_665 14 ?
Rb3 F3 Rb1A 166.74(8) 14 18_666 ?
Rb3 F3 Rb1B 166.11(9) 14 18_666 ?
Rb4 F3 Rb1A 80.95(7) 29_666 18_666 ?
Rb4 F3 Rb1A 83.74(8) 29_666 14 ?
Rb4 F3 Rb1B 88.64(8) 29_666 14 ?
Rb4 F3 Rb1B 76.67(8) 29_666 18_666 ?
Rb4 F3 Rb2A 80.64(7) 29_666 28_665 ?
Rb4 F3 Rb2B 76.20(14) 29_666 28_665 ?
Rb4 F3 Rb3 91.16(6) 29_666 14 ?
Al1 F3 Rb1A 104.76(11) . 14 ?
Al1 F3 Rb1A 90.61(9) . 18_666 ?
Al1 F3 Rb1B 94.19(10) . 18_666 ?
Al1 F3 Rb1B 99.80(11) . 14 ?
Al1 F3 Rb2A 92.64(9) . 28_665 ?
Al1 F3 Rb2B 96.28(14) . 28_665 ?
Al1 F3 Rb3 98.84(9) . 14 ?
Al1 F3 Rb4 167.19(12) . 29_666 ?
Rb2A F4 Rb2A 106.68(13) . 8 ?
Rb2A F4 Rb3 83.02(7) 8 18_666 ?
Rb2A F4 Rb3 166.89(8) . 18_666 ?
Rb2A F4 Rb3 81.49(8) . 17_766 ?
Rb2B F4 Rb2A 5.87(11) 8 8 ?
Rb2B F4 Rb2A 5.94(10) . . ?
Rb2B F4 Rb2A 101.8(2) 8 . ?
Rb2B F4 Rb2A 101.5(2) . 8 ?
Rb2B F4 Rb2B 96.5(3) . 8 ?
Rb2B F4 Rb3 166.62(12) 8 17_766 ?
Rb2B F4 Rb3 167.20(11) . 18_666 ?
Rb2B F4 Rb3 86.02(15) . 17_766 ?
Rb2B F4 Rb3 87.31(14) 8 18_666 ?
Rb3 F4 Rb2A 167.43(8) 17_766 8 ?
Rb3 F4 Rb3 87.55(6) 17_766 18_666 ?
Rb4 F4 Rb2A 81.62(8) . 8 ?
Rb4 F4 Rb2A 80.58(8) . . ?
Rb4 F4 Rb2B 77.36(14) . 8 ?
Rb4 F4 Rb2B 76.60(14) . . ?
Rb4 F4 Rb3 90.53(6) . 17_766 ?
Rb4 F4 Rb3 92.41(6) . 18_666 ?
Al2 F4 Rb2A 92.04(9) . . ?
Al2 F4 Rb2A 91.08(9) . 8 ?
Al2 F4 Rb2B 95.21(14) . . ?
Al2 F4 Rb2B 94.59(14) . 8 ?
Al2 F4 Rb3 96.66(9) . 18_666 ?
Al2 F4 Rb3 98.28(9) . 17_766 ?
Al2 F4 Rb4 167.59(14) . . ?
Rb1A F5 Rb1B 4.51(8) . . ?
Rb1A F5 Rb3 89.27(6) . . ?
Rb1A F5 Rb3 88.55(6) . 30_556 ?
Rb1A F5 Rb3 161.78(8) . 2_655 ?
Rb1A F5 Rb4 77.32(7) . 30_556 ?
Rb1B F5 Rb3 89.29(9) . . ?
Rb1B F5 Rb3 89.28(8) . 30_556 ?
Rb1B F5 Rb3 166.28(9) . 2_655 ?
Rb1B F5 Rb4 81.82(8) . 30_556 ?
Rb3 F5 Rb3 91.47(5) 2_655 . ?
Rb3 F5 Rb3 170.20(6) . 30_556 ?
Rb3 F5 Rb3 87.65(5) 2_655 30_556 ?
Rb3 F5 Rb4 86.37(5) . 30_556 ?
Rb3 F5 Rb4 84.56(5) 2_655 30_556 ?
Rb4 F5 Rb3 83.83(5) 30_556 30_556 ?
Al3 F5 Rb1A 102.16(9) . . ?
Al3 F5 Rb1B 97.67(10) . . ?
Al3 F5 Rb3 94.40(8) . . ?
Al3 F5 Rb3 95.93(7) . 2_655 ?
Al3 F5 Rb3 95.39(7) . 30_556 ?
Al3 F5 Rb4 179.07(10) . 30_556 ?
Rb2A F6 Rb2A 151.51(16) 11_655 . ?
Rb2A F6 Rb2B 156.5(2) . 11_655 ?
Rb2A F6 Rb2B 156.5(2) 11_655 . ?
Rb2A F6 Rb2B 5.01(10) 11_655 11_655 ?
Rb2A F6 Rb2B 5.01(10) . . ?
Rb2A F6 Rb3 90.03(3) 11_655 17_766 ?
Rb2A F6 Rb3 90.03(3) . 19_666 ?
Rb2A F6 Rb3 86.92(3) . 17_766 ?
Rb2A F6 Rb3 86.92(3) 11_655 19_666 ?
Rb2A F6 Rb5 75.76(8) . 30_656 ?
Rb2A F6 Rb5 75.76(8) 11_655 30_656 ?
Rb2B F6 Rb2B 161.5(3) . 11_655 ?
Rb2B F6 Rb3 87.74(9) 11_655 19_666 ?
Rb2B F6 Rb3 87.74(9) . 17_766 ?
Rb2B F6 Rb3 90.27(9) 11_655 17_766 ?
Rb2B F6 Rb3 90.27(9) . 19_666 ?
Rb2B F6 Rb5 80.76(15) . 30_656 ?
Rb2B F6 Rb5 80.76(15) 11_655 30_656 ?
Rb3 F6 Rb3 167.60(10) 17_766 19_666 ?
Rb3 F6 Rb5 83.80(5) 17_766 30_656 ?
Rb3 F6 Rb5 83.80(5) 19_666 30_656 ?
Al2 F6 Rb2A 104.24(8) . . ?
Al2 F6 Rb2A 104.24(8) . 11_655 ?
Al2 F6 Rb2B 99.24(15) . . ?
Al2 F6 Rb2B 99.24(15) . 11_655 ?
Al2 F6 Rb3 96.20(5) . 17_766 ?
Al2 F6 Rb3 96.20(5) . 19_666 ?
Al2 F6 Rb5 180.0 . 30_656 ?
Rb1A F7 Rb1B 6.11(5) 2_655 2_655 ?
Rb1A F7 Rb2A 105.86(10) 2_655 2_655 ?
Rb1A F7 Rb2B 101.02(16) 2_655 2_655 ?
Rb1A F7 Rb2B 164.77(14) 2_655 . ?
Rb1A F7 Rb3 84.58(7) 2_655 17_766 ?
Rb1B F7 Rb2A 100.63(10) 2_655 2_655 ?
Rb1B F7 Rb2B 95.62(16) 2_655 2_655 ?
Rb1B F7 Rb2B 163.26(15) 2_655 . ?
Rb1B F7 Rb3 89.21(8) 2_655 17_766 ?
Rb2A F7 Rb1A 160.90(9) . 2_655 ?
Rb2A F7 Rb1B 158.91(11) . 2_655 ?
Rb2A F7 Rb2A 81.50(7) . 2_655 ?
Rb2A F7 Rb2B 85.14(12) . 2_655 ?
Rb2A F7 Rb2B 4.42(9) . . ?
Rb2A F7 Rb2B 5.76(10) 2_655 2_655 ?
Rb2A F7 Rb3 85.79(6) . 17_766 ?
Rb2B F7 Rb2A 81.63(10) . 2_655 ?
Rb2B F7 Rb2B 85.59(19) . 2_655 ?
Rb2B F7 Rb3 86.14(10) . 17_766 ?
Rb3 F7 Rb2A 166.05(7) 17_766 2_655 ?
Rb3 F7 Rb2B 166.31(10) 17_766 2_655 ?
Rb5 F7 Rb1A 79.90(7) 30_656 2_655 ?
Rb5 F7 Rb1B 75.48(8) 30_656 2_655 ?
Rb5 F7 Rb2A 84.52(7) 30_656 . ?
Rb5 F7 Rb2A 78.36(7) 30_656 2_655 ?
Rb5 F7 Rb2B 74.16(13) 30_656 2_655 ?
Rb5 F7 Rb2B 88.88(13) 30_656 . ?
Rb5 F7 Rb3 94.79(6) 30_656 17_766 ?
Al3 F7 Rb1A 92.33(8) . 2_655 ?
Al3 F7 Rb1B 95.78(10) . 2_655 ?
Al3 F7 Rb2A 92.27(9) . 2_655 ?
Al3 F7 Rb2A 105.14(10) . . ?
Al3 F7 Rb2B 100.72(15) . . ?
Al3 F7 Rb2B 95.65(14) . 2_655 ?
Al3 F7 Rb3 96.59(8) . 17_766 ?
Al3 F7 Rb5 165.55(11) . 30_656 ?
Rb1A F8 Rb2A 104.47(9) . . ?
Rb1A F8 Rb2B 99.84(15) . . ?
Rb1B F8 Rb1A 6.01(5) . . ?
Rb1B F8 Rb2A 99.56(10) . . ?
Rb1B F8 Rb2B 94.74(16) . . ?
Rb2A F8 Rb2B 5.75(10) . . ?
Rb3 F8 Rb1A 168.97(8) 17_766 . ?
Rb3 F8 Rb1A 84.32(7) . . ?
Rb3 F8 Rb1B 166.51(9) 17_766 . ?
Rb3 F8 Rb1B 88.58(8) . . ?
Rb3 F8 Rb2A 167.23(7) . . ?
Rb3 F8 Rb2A 80.39(6) 17_766 . ?
Rb3 F8 Rb2B 166.56(11) . . ?
Rb3 F8 Rb2B 84.34(13) 17_766 . ?
Rb3 F8 Rb3 89.40(5) . 17_766 ?
Rb4 F8 Rb1A 81.15(7) . . ?
Rb4 F8 Rb1B 76.53(8) . . ?
Rb4 F8 Rb2A 78.07(7) . . ?
Rb4 F8 Rb2B 73.74(13) . . ?
Rb4 F8 Rb3 94.47(6) . . ?
Rb4 F8 Rb3 90.34(5) . 17_766 ?
Al3 F8 Rb1A 91.09(8) . . ?
Al3 F8 Rb1B 94.84(9) . . ?
Al3 F8 Rb2A 92.58(9) . . ?
Al3 F8 Rb2B 96.15(14) . . ?
Al3 F8 Rb3 98.64(8) . 17_766 ?
Al3 F8 Rb3 96.54(8) . . ?
Al3 F8 Rb4 165.83(11) . . ?
Rb1A F9 Rb1B 101.7(2) 30_556 17_666 ?
Rb1A F9 Rb4 83.50(19) 30_556 30_556 ?
Rb1A F9 Rb4 84.8(2) 30_556 17_666 ?
Rb1A F9 Rb5 78.3(2) 30_556 2 ?
Rb1B F9 Rb1A 0.37(12) 30_556 30_556 ?
Rb1B F9 Rb1B 102.0(3) 30_556 17_666 ?
Rb1B F9 Rb4 83.5(2) 30_556 30_556 ?
Rb1B F9 Rb4 85.1(2) 30_556 17_666 ?
Rb1B F9 Rb5 77.9(3) 30_556 2 ?
Rb4 F9 Rb1B 64.04(19) 17_666 17_666 ?
Rb4 F9 Rb1B 66.61(18) 30_556 17_666 ?
Rb4 F9 Rb4 125.4(3) 30_556 17_666 ?
Rb4 F9 Rb5 114.1(3) 17_666 2 ?
Rb4 F9 Rb5 115.2(3) 30_556 2 ?
Rb5 F9 Rb1B 178.1(3) 2 17_666 ?
Al4 F9 Rb1A 168.2(5) . 30_556 ?
Al4 F9 Rb1B 90.1(3) . 17_666 ?
Al4 F9 Rb1B 167.8(5) . 30_556 ?
Al4 F9 Rb4 99.9(4) . 17_666 ?
Al4 F9 Rb4 102.1(3) . 30_556 ?
Al4 F9 Rb5 89.9(3) . 2 ?
F9 F9 Rb1A 130.3(2) 2 30_556 ?
F9 F9 Rb1B 28.66(9) 2 17_666 ?
F9 F9 Rb1B 130.7(2) 2 30_556 ?
F9 F9 Rb4 76.0(5) 2 30_556 ?
F9 F9 Rb4 72.1(6) 2 17_666 ?
F9 F9 Rb5 151.26(11) 2 2 ?
F9 F9 Al4 61.5(3) 2 . ?
F9 F9 F10A 100.8(6) 2 2 ?
F10A F9 Rb1A 113.1(6) 2 30_556 ?
F10A F9 Rb1B 112.8(6) 2 30_556 ?
F10A F9 Rb1B 118.3(5) 2 17_666 ?
F10A F9 Rb4 159.7(5) 2 17_666 ?
F10A F9 Rb4 68.7(4) 2 30_556 ?
F10A F9 Rb5 63.2(4) 2 2 ?
F10A F9 Al4 60.7(4) 2 . ?
F10B F9 Rb1A 109.8(5) 2 30_556 ?
F10B F9 Rb1B 117.5(5) 2 17_666 ?
F10B F9 Rb1B 109.7(6) 2 30_556 ?
F10B F9 Rb4 163.8(5) 2 30_556 ?
F10B F9 Rb4 66.8(4) 2 17_666 ?
F10B F9 Rb5 60.9(4) 2 2 ?
F10B F9 Al4 63.1(4) 2 . ?
F10B F9 F9 100.6(7) 2 2 ?
F10B F9 F10A 96.8(5) 2 2 ?
Rb1B F10A Rb4 176.4(2) 17_666 24_655 ?
Rb2A F10A Rb1B 104.5(3) 17_666 17_666 ?
Rb2A F10A Rb4 83.38(16) 17_666 17_666 ?
Rb2A F10A Rb4 72.2(3) 17_666 24_655 ?
Rb2A F10A Rb5 84.31(19) 17_666 . ?
Rb2B F10A Rb1B 106.2(4) 17_666 17_666 ?
Rb2B F10A Rb2A 1.75(13) 17_666 17_666 ?
Rb2B F10A Rb4 70.4(4) 17_666 24_655 ?
Rb2B F10A Rb4 83.9(2) 17_666 17_666 ?
Rb2B F10A Rb5 85.1(2) 17_666 . ?
Rb4 F10A Rb1B 70.0(3) 17_666 17_666 ?
Rb4 F10A Rb4 110.4(3) 17_666 24_655 ?
Rb4 F10A Rb5 132.4(5) 17_666 . ?
Rb5 F10A Rb1B 69.0(3) . 17_666 ?
Rb5 F10A Rb4 109.0(3) . 24_655 ?
Al4 F10A Rb1B 100.2(5) . 17_666 ?
Al4 F10A Rb2A 155.2(8) . 17_666 ?
Al4 F10A Rb2B 153.5(8) . 17_666 ?
Al4 F10A Rb4 108.2(3) . 17_666 ?
Al4 F10A Rb4 83.2(5) . 24_655 ?
Al4 F10A Rb5 101.9(3) . . ?
F9 F10A Rb1B 39.3(4) 2 17_666 ?
F9 F10A Rb2A 143.3(7) 2 17_666 ?
F9 F10A Rb2B 145.0(7) 2 17_666 ?
F9 F10A Rb4 78.1(5) 2 17_666 ?
F9 F10A Rb4 144.2(5) 2 24_655 ?
F9 F10A Rb5 85.2(5) 2 . ?
F9 F10A Al4 61.5(3) 2 . ?
F10B F10A Rb1B 143.1(11) 3 17_666 ?
F10B F10A Rb2A 83.0(9) 3 17_666 ?
F10B F10A Rb2B 81.7(10) 3 17_666 ?
F10B F10A Rb4 36.3(10) 3 24_655 ?
F10B F10A Rb4 146.7(13) 3 17_666 ?
F10B F10A Rb5 76.0(8) 3 . ?
F10B F10A Al4 75.4(7) 3 . ?
F10B F10A F9 127.9(9) 3 2 ?
Rb1B F10B Rb1A 2.45(8) 17_666 17_666 ?
Rb2A F10B Rb1A 107.6(3) 27_565 17_666 ?
Rb2A F10B Rb1B 110.0(3) 27_565 17_666 ?
Rb2A F10B Rb4 84.31(19) 27_565 30_556 ?
Rb2A F10B Rb5 84.6(3) 27_565 . ?
Rb2B F10B Rb1A 109.3(3) 27_565 17_666 ?
Rb2B F10B Rb1B 111.7(3) 27_565 17_666 ?
Rb2B F10B Rb2A 1.74(12) 27_565 27_565 ?
Rb2B F10B Rb4 84.5(2) 27_565 30_556 ?
Rb2B F10B Rb5 85.6(3) 27_565 . ?
Rb4 F10B Rb1A 73.7(3) 30_556 17_666 ?
Rb4 F10B Rb1B 74.2(3) 30_556 17_666 ?
Rb5 F10B Rb1A 70.9(3) . 17_666 ?
Rb5 F10B Rb1B 71.5(3) . 17_666 ?
Rb5 F10B Rb4 137.5(4) . 30_556 ?
Al4 F10B Rb1A 106.0(7) . 17_666 ?
Al4 F10B Rb1B 103.6(7) . 17_666 ?
Al4 F10B Rb2A 146.3(9) . 27_565 ?
Al4 F10B Rb2B 144.6(9) . 27_565 ?
Al4 F10B Rb4 108.0(4) . 30_556 ?
Al4 F10B Rb5 103.8(3) . . ?
F9 F10B Rb1A 44.4(5) 2 17_666 ?
F9 F10B Rb1B 42.0(5) 2 17_666 ?
F9 F10B Rb2A 151.4(7) 2 27_565 ?
F9 F10B Rb2B 153.0(7) 2 27_565 ?
F9 F10B Rb4 81.8(6) 2 30_556 ?
F9 F10B Rb5 88.9(6) 2 . ?
F9 F10B Al4 62.2(4) 2 . ?
F10A F10B Rb1A 154.1(11) 3 17_666 ?
F10A F10B Rb1B 153.8(11) 3 17_666 ?
F10A F10B Rb2A 76.4(10) 3 27_565 ?
F10A F10B Rb2B 75.1(10) 3 27_565 ?
F10A F10B Rb4 132.0(13) 3 30_556 ?
F10A F10B Rb5 84.2(9) 3 . ?
F10A F10B Al4 72.2(6) 3 . ?
F10A F10B F9 130.6(8) 3 2 ?

_olex2_submission_special_instructions 'No special instructions were received'

# start Validation Reply Form
_vrf_PLAT215_Rb3AlF6_Fddd        
;
PROBLEM: Disordered F10A      has ADP max/min Ratio .....        6.0 Note  
RESPONSE: The Al4 octahedron adopts a range of orientations.  The F9 and F10a/b
locations are the most reasonable average orientations of the octahedra.  
Further decomposing these fluorine atoms into further locations did not lead 
to stable, physically meaningful models.
;
_vrf_PLAT242_Rb3AlF6_Fddd        
;
PROBLEM: Low    'MainMol' Ueq as Compared to Neighbors of        Al4 Check 
RESPONSE: The Al4 octahedron adopts a range of orientations.  The F9 and F10a/b
locations are the most reasonable average orientations of the octahedra.  
Further decomposing these fluorine atoms into further locations did not lead 
to stable, physically meaningful models.
;
# end Validation Reply Form
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_Cs3GaF6_C2_m
_database_code_depnum_ccdc_archive 'CCDC 2193506'
loop_
_audit_author_name
_audit_author_address
'Gregory Morrison'
;University of South Carolina
United States of America
;
_audit_update_record             
;
2022-07-28 deposited with the CCDC.	2023-05-19 downloaded from the CCDC.
;
_audit_creation_date             2022-01-12
_audit_creation_method           
;
Olex2 1.2
(compiled May 18 2018 14:05:52 for OlexSys, GUI svn.r5506)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         '0.08(Cs36 F72 Ga12)'
_chemical_formula_sum            'Cs3 F6 Ga'
_chemical_formula_weight         582.45
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ga Ga 0.2307 1.6083 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cs Cs -0.3680 2.1192 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           12
_space_group_name_H-M_alt        'C 1 2/m 1'
_space_group_name_Hall           '-C 2y'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z'
'-x, -y, -z'
'x, -y, z'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z'

_cell_length_a                   11.3996(3)
_cell_length_b                   19.7132(4)
_cell_length_c                   11.4551(4)
_cell_angle_alpha                90
_cell_angle_beta                 109.7000(10)
_cell_angle_gamma                90
_cell_volume                     2423.55(12)
_cell_formula_units_Z            12
_cell_measurement_reflns_used    9626
_cell_measurement_temperature    300(2)
_cell_measurement_theta_max      36.1275
_cell_measurement_theta_min      3.2644
_shelx_estimated_absorpt_T_max   0.554
_shelx_estimated_absorpt_T_min   0.387
_exptl_absorpt_coefficient_mu    16.760
_exptl_absorpt_correction_T_max  0.7471
_exptl_absorpt_correction_T_min  0.6246
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
SADABS-2016/2 (Bruker,2016) was used for absorption correction.
wR2(int) was 0.0971 before and 0.0580 after correction.
The Ratio of minimum to maximum transmission is 0.8360.
The λ/2 correction factor is Not present.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    4.789
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       polyhedron
_exptl_crystal_F_000             3000
_exptl_crystal_size_max          0.07
_exptl_crystal_size_mid          0.05
_exptl_crystal_size_min          0.04
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0376
_diffrn_reflns_av_unetI/netI     0.0134
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.999
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_k_max       30
_diffrn_reflns_limit_k_min       -30
_diffrn_reflns_limit_l_max       17
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_number            102291
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.999
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         33.137
_diffrn_reflns_theta_min         2.161
_diffrn_ambient_temperature      299.94
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'Bruker D8 Quest'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   'microfocus sealed X-ray tube'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                4466
_reflns_number_total             4759
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences. Completness statistics refer to single and
 composite reflections containing twin component 1 only.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT v8.34A (Bruker, 2013)'
_computing_data_collection       'Bruker APEX3 v2016.5-0 (Bruker, 2016)'
_computing_data_reduction        'SAINT v8.34A (Bruker, 013)'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    'ShelXT (Sheldrick, 2015)'
_refine_diff_density_max         4.065
_refine_diff_density_min         -3.099
_refine_diff_density_rms         0.243
_refine_ls_extinction_coef       0.000159(14)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     'SHELXL-2018/3 (Sheldrick 2018)'
_refine_ls_goodness_of_fit_ref   1.160
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     166
_refine_ls_number_reflns         4759
_refine_ls_number_restraints     1
_refine_ls_R_factor_all          0.0307
_refine_ls_R_factor_gt           0.0281
_refine_ls_restrained_S_all      1.159
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0291P)²+25.0230P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0685
_refine_ls_wR_factor_ref         0.0717
_refine_special_details          
;
 Refined as a 2-component twin.
;
_olex2_refinement_description    
;
1. Twinned data refinement
 Scales: 0.9297(14)
 0.0703(14)
2. Uiso/Uaniso restraints and constraints
Uanis(F2A) = Uanis(F2B) = Uanis(F2C)
Uanis(Cs1A) = Uanis(Cs1B)
Uanis(F1A) = Uanis(F1B)
3. Others
 2*[Sof(Cs1A)+Sof(Cs1B)+Sof(F1A)+Sof(F2A)+Sof(F2C)]+1*[Sof(F1B)+Sof(F2B)]=1
 with esd of 0.001
 Sof(Cs1A)=1-FVAR(1)
 Sof(Cs1B)=Sof(F1A)=Sof(F2A)=Sof(F2C)=FVAR(1)
 Sof(F1B)=0.5*FVAR(3)
 Sof(F2B)=FVAR(2)
;
_atom_sites_solution_hydrogens   .
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Cs1A Cs 0.64015(10) 0.30972(6) 0.85365(10) 0.02317(14) Uani 0.686(4) 1 d . . .
. .
Cs1B Cs 0.6296(2) 0.32274(11) 0.8644(2) 0.02317(14) Uani 0.314(4) 1 d . . . . .
Cs2 Cs 0.14572(4) 0.000000 0.43094(4) 0.02601(8) Uani 1 2 d S T P . .
Cs3 Cs 1.29435(4) 0.500000 1.20995(3) 0.02566(8) Uani 1 2 d S T P . .
Cs4 Cs 0.78423(2) 0.14308(2) 0.77987(2) 0.02593(6) Uani 1 1 d . . . . .
Cs5 Cs 0.91771(5) 0.500000 1.14316(4) 0.03057(9) Uani 1 2 d S T P . .
Cs6 Cs 0.87380(3) 0.33198(2) 0.62028(3) 0.02833(6) Uani 1 1 d . . . . .
Ga1 Ga 1.000000 0.33417(3) 1.000000 0.01375(9) Uani 1 2 d S T P . .
Ga2 Ga 0.000000 0.000000 0.000000 0.01565(13) Uani 1 4 d S T P . .
Ga3 Ga 0.500000 0.000000 0.500000 0.01518(13) Uani 1 4 d S T P . .
Ga4 Ga 1.000000 0.17331(3) 0.500000 0.01429(9) Uani 1 2 d S T P . .
F1A F 0.0407(14) 0.0188(12) 0.1695(17) 0.064(6) Uani 0.314(4) 1 d . . . . .
F1B F 0.085(3) 0.000000 0.171(3) 0.064(6) Uani 0.373(7) 2 d S T P . .
F2A F -0.0474(14) 0.0845(7) 0.0392(14) 0.0542(19) Uani 0.314(4) 1 d . . . . .
F2B F -0.1140(12) 0.0658(6) 0.0171(11) 0.0542(19) Uani 0.373(7) 1 d . . . . .
F2C F 0.1651(12) 0.0292(7) 0.0302(13) 0.0542(19) Uani 0.314(4) 1 d . . . . .
F3 F 0.3995(4) 0.000000 0.6048(4) 0.0336(8) Uani 1 2 d S T P . .
F4 F 0.6031(3) 0.06695(18) 0.5992(3) 0.0442(8) Uani 1 1 d . . . . .
F5 F 0.8998(3) 0.10465(14) 0.3963(3) 0.0318(6) Uani 1 1 d . . . . .
F6 F 1.1022(3) 0.24132(14) 0.6019(3) 0.0290(5) Uani 1 1 d . . . . .
F7 F 0.8975(3) 0.17213(16) 0.5988(3) 0.0335(6) Uani 1 1 d . . . . .
F8 F 0.9001(3) 0.26587(15) 0.8992(3) 0.0354(6) Uani 1 1 d . . . . .
F9 F 1.1015(3) 0.33503(16) 0.8996(3) 0.0356(6) Uani 1 1 d . . . . .
F10 F 1.1033(3) 0.40154(15) 1.1011(3) 0.0356(6) Uani 1 1 d . . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Cs1A F2A 2.802(12) 7_556 ?
Cs1A F2B 2.933(11) 7_556 ?
Cs1A F2C 3.724(14) 8_556 ?
Cs1A F5 3.221(3) 7_656 ?
Cs1A F6 2.946(3) 8_455 ?
Cs1A F7 3.295(4) 8_455 ?
Cs1A F8 3.308(3) 8_455 ?
Cs1A F8 2.960(3) . ?
Cs1A F8 3.365(4) 7_657 ?
Cs1A F9 3.362(4) 2_757 ?
Cs1A F9 2.961(3) 8_455 ?
Cs1A F10 3.328(3) 2_757 ?
Cs1B F2A 2.478(12) 7_556 ?
Cs1B F2B 2.621(11) 7_556 ?
Cs1B F2C 3.432(14) 8_556 ?
Cs1B F5 3.226(4) 7_656 ?
Cs1B F6 3.179(4) 8_455 ?
Cs1B F7 3.292(4) 8_455 ?
Cs1B F8 3.178(4) . ?
Cs1B F8 3.279(4) 8_455 ?
Cs1B F8 3.335(4) 7_657 ?
Cs1B F9 3.344(5) 2_757 ?
Cs1B F9 3.166(4) 8_455 ?
Cs1B F10 3.322(4) 2_757 ?
Cs2 F1A 2.850(19) . ?
Cs2 F1A 2.850(19) 6 ?
Cs2 F1B 2.82(3) . ?
Cs2 F3 2.908(4) . ?
Cs2 F4 3.275(4) 5_656 ?
Cs2 F4 3.275(4) 2_656 ?
Cs2 F5 3.022(3) 2_656 ?
Cs2 F5 3.022(3) 5_656 ?
Cs2 F5 3.395(3) 6_455 ?
Cs2 F5 3.395(3) 1_455 ?
Cs2 F7 3.429(3) 2_656 ?
Cs2 F7 3.429(3) 5_656 ?
Cs3 F1A 3.019(13) 8_656 ?
Cs3 F1A 3.019(14) 3_656 ?
Cs3 F1B 3.49(2) 3_656 ?
Cs3 F2A 3.498(16) 8_656 ?
Cs3 F2B 3.034(13) 8_656 ?
Cs3 F2B 3.034(13) 3_656 ?
Cs3 F2C 2.995(13) 7_656 ?
Cs3 F2C 2.995(13) 4_656 ?
Cs3 F5 2.920(3) 3_556 ?
Cs3 F5 2.920(3) 8_556 ?
Cs3 F10 2.870(3) . ?
Cs3 F10 2.870(3) 6_565 ?
Cs4 F1A 3.088(19) 2_656 ?
Cs4 F1A 3.71(2) 5_656 ?
Cs4 F1B 3.152(13) 5_656 ?
Cs4 F2A 3.162(15) 1_656 ?
Cs4 F2A 3.231(16) 2_656 ?
Cs4 F2B 2.988(13) 1_656 ?
Cs4 F2C 3.044(12) 2_656 ?
Cs4 F4 2.814(3) . ?
Cs4 F6 3.287(2) 8_455 ?
Cs4 F7 2.846(3) . ?
Cs4 F8 2.873(3) . ?
Cs4 F9 2.887(3) 8_455 ?
Cs5 F2B 3.571(14) 7_556 ?
Cs5 F2C 2.790(13) 3_556 ?
Cs5 F2C 2.790(13) 8_556 ?
Cs5 F3 2.936(4) 7_657 ?
Cs5 F4 3.314(4) 4_657 ?
Cs5 F4 3.314(4) 7_657 ?
Cs5 F9 3.285(3) 5_767 ?
Cs5 F9 3.285(3) 2_757 ?
Cs5 F10 3.027(3) . ?
Cs5 F10 3.027(3) 6_565 ?
Cs5 F10 3.347(4) 5_767 ?
Cs5 F10 3.347(4) 2_757 ?
Cs6 F3 3.3351(6) 3 ?
Cs6 F4 3.359(4) 8 ?
Cs6 F4 3.287(4) 7_656 ?
Cs6 F5 3.305(3) 7_656 ?
Cs6 F6 3.358(3) 8_455 ?
Cs6 F6 3.196(3) 2_756 ?
Cs6 F6 3.224(3) . ?
Cs6 F7 3.262(3) 7_656 ?
Cs6 F7 3.179(3) . ?
Cs6 F8 3.369(4) . ?
Cs6 F9 3.373(4) . ?
Cs6 F10 3.402(4) 2_757 ?
Ga1 F8 1.886(3) . ?
Ga1 F8 1.886(3) 2_757 ?
Ga1 F9 1.887(3) . ?
Ga1 F9 1.886(3) 2_757 ?
Ga1 F10 1.890(3) . ?
Ga1 F10 1.890(3) 2_757 ?
Ga2 F1A 1.875(18) . ?
Ga2 F1A 1.875(18) 6 ?
Ga2 F1A 1.875(18) 5 ?
Ga2 F1A 1.875(18) 2 ?
Ga2 F1B 1.87(3) 5 ?
Ga2 F1B 1.87(3) . ?
Ga2 F2A 1.852(12) . ?
Ga2 F2A 1.852(12) 6 ?
Ga2 F2A 1.852(12) 5 ?
Ga2 F2A 1.852(12) 2 ?
Ga2 F2C 1.885(14) . ?
Ga2 F2C 1.885(14) 5 ?
Ga3 F3 1.919(4) 5_656 ?
Ga3 F3 1.919(4) . ?
Ga3 F4 1.875(3) 2_656 ?
Ga3 F4 1.875(3) 5_656 ?
Ga3 F4 1.875(3) 6 ?
Ga3 F4 1.875(3) . ?
Ga4 F5 1.906(3) . ?
Ga4 F5 1.906(3) 2_756 ?
Ga4 F6 1.897(3) . ?
Ga4 F6 1.897(3) 2_756 ?
Ga4 F7 1.881(3) 2_756 ?
Ga4 F7 1.881(3) . ?
F1A F1A 0.74(5) 6 ?
F1A F1B 0.62(2) . ?
F2A F2A 1.62(3) 2 ?
F2A F2B 0.805(17) . ?
F2A F2C 1.70(2) 2 ?
F2B F2C 0.970(16) 2 ?
F2C F2C 1.15(3) 6 ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
F2A Cs1A F2B 15.9(3) 7_556 7_556 ?
F2A Cs1A F2C 25.6(4) 7_556 8_556 ?
F2A Cs1A F5 92.2(3) 7_556 7_656 ?
F2A Cs1A F6 137.0(3) 7_556 8_455 ?
F2A Cs1A F7 88.8(3) 7_556 8_455 ?
F2A Cs1A F8 130.0(3) 7_556 . ?
F2A Cs1A F8 77.4(3) 7_556 7_657 ?
F2A Cs1A F8 79.2(3) 7_556 8_455 ?
F2A Cs1A F9 122.6(3) 7_556 8_455 ?
F2A Cs1A F9 82.8(3) 7_556 2_757 ?
F2A Cs1A F10 88.2(3) 7_556 2_757 ?
F2B Cs1A F2C 9.7(3) 7_556 8_556 ?
F2B Cs1A F5 90.1(3) 7_556 7_656 ?
F2B Cs1A F6 140.7(3) 7_556 8_455 ?
F2B Cs1A F7 99.1(2) 7_556 8_455 ?
F2B Cs1A F8 83.1(3) 7_556 7_657 ?
F2B Cs1A F8 114.9(3) 7_556 . ?
F2B Cs1A F8 93.9(3) 7_556 8_455 ?
F2B Cs1A F9 132.1(3) 7_556 8_455 ?
F2B Cs1A F9 70.2(3) 7_556 2_757 ?
F2B Cs1A F10 72.5(3) 7_556 2_757 ?
F5 Cs1A F2C 89.9(2) 7_656 8_556 ?
F5 Cs1A F7 47.99(7) 7_656 8_455 ?
F5 Cs1A F8 119.98(8) 7_656 8_455 ?
F5 Cs1A F8 164.04(9) 7_656 7_657 ?
F5 Cs1A F9 119.40(8) 7_656 2_757 ?
F5 Cs1A F10 72.96(7) 7_656 2_757 ?
F6 Cs1A F2C 141.4(2) 8_455 8_556 ?
F6 Cs1A F5 51.57(7) 8_455 7_656 ?
F6 Cs1A F7 50.76(7) 8_455 8_455 ?
F6 Cs1A F8 83.14(8) 8_455 . ?
F6 Cs1A F8 98.31(9) 8_455 8_455 ?
F6 Cs1A F8 130.99(8) 8_455 7_657 ?
F6 Cs1A F9 132.20(8) 8_455 2_757 ?
F6 Cs1A F9 82.15(9) 8_455 8_455 ?
F6 Cs1A F10 99.75(9) 8_455 2_757 ?
F7 Cs1A F2C 106.0(2) 8_455 8_556 ?
F7 Cs1A F8 118.79(8) 8_455 7_657 ?
F7 Cs1A F8 72.34(7) 8_455 8_455 ?
F7 Cs1A F9 164.74(9) 8_455 2_757 ?
F7 Cs1A F10 120.67(8) 8_455 2_757 ?
F8 Cs1A F2C 85.86(19) 7_657 8_556 ?
F8 Cs1A F2C 105.3(2) . 8_556 ?
F8 Cs1A F2C 102.38(19) 8_455 8_556 ?
F8 Cs1A F5 98.21(10) . 7_656 ?
F8 Cs1A F7 132.81(9) . 8_455 ?
F8 Cs1A F8 46.61(9) 8_455 7_657 ?
F8 Cs1A F8 132.30(6) . 8_455 ?
F8 Cs1A F8 97.75(9) . 7_657 ?
F8 Cs1A F9 83.54(9) . 8_455 ?
F8 Cs1A F9 118.10(8) 8_455 2_757 ?
F8 Cs1A F9 49.74(8) . 2_757 ?
F8 Cs1A F10 161.92(9) 8_455 2_757 ?
F8 Cs1A F10 49.92(8) . 2_757 ?
F9 Cs1A F2C 62.1(2) 2_757 8_556 ?
F9 Cs1A F2C 135.56(19) 8_455 8_556 ?
F9 Cs1A F5 132.69(9) 8_455 7_656 ?
F9 Cs1A F7 97.55(9) 8_455 8_455 ?
F9 Cs1A F8 49.69(8) 8_455 7_657 ?
F9 Cs1A F8 71.80(7) 2_757 7_657 ?
F9 Cs1A F8 50.01(8) 8_455 8_455 ?
F9 Cs1A F9 97.72(9) 8_455 2_757 ?
F9 Cs1A F10 132.21(9) 8_455 2_757 ?
F10 Cs1A F2C 63.22(19) 2_757 8_556 ?
F10 Cs1A F8 118.15(8) 2_757 7_657 ?
F10 Cs1A F9 46.64(7) 2_757 2_757 ?
F2A Cs1B F2B 17.9(4) 7_556 7_556 ?
F2A Cs1B F2C 28.0(4) 7_556 8_556 ?
F2A Cs1B F5 98.5(4) 7_556 7_656 ?
F2A Cs1B F6 141.6(4) 7_556 8_455 ?
F2A Cs1B F7 94.7(4) 7_556 8_455 ?
F2A Cs1B F8 134.5(4) 7_556 . ?
F2A Cs1B F8 82.4(4) 7_556 7_657 ?
F2A Cs1B F8 84.4(4) 7_556 8_455 ?
F2A Cs1B F9 88.1(4) 7_556 2_757 ?
F2A Cs1B F9 126.8(4) 7_556 8_455 ?
F2A Cs1B F10 94.1(4) 7_556 2_757 ?
F2B Cs1B F2C 10.2(4) 7_556 8_556 ?
F2B Cs1B F5 95.9(3) 7_556 7_656 ?
F2B Cs1B F6 145.2(3) 7_556 8_455 ?
F2B Cs1B F7 106.2(3) 7_556 8_455 ?
F2B Cs1B F8 88.6(3) 7_556 7_657 ?
F2B Cs1B F8 117.6(3) 7_556 . ?
F2B Cs1B F8 100.8(3) 7_556 8_455 ?
F2B Cs1B F9 136.9(3) 7_556 8_455 ?
F2B Cs1B F9 74.0(3) 7_556 2_757 ?
F2B Cs1B F10 76.4(3) 7_556 2_757 ?
F5 Cs1B F2C 95.2(2) 7_656 8_556 ?
F5 Cs1B F7 47.98(8) 7_656 8_455 ?
F5 Cs1B F8 120.72(11) 7_656 8_455 ?
F5 Cs1B F8 167.73(12) 7_656 7_657 ?
F5 Cs1B F9 119.81(11) 7_656 2_757 ?
F5 Cs1B F10 72.99(9) 7_656 2_757 ?
F6 Cs1B F2C 144.8(2) 8_455 8_556 ?
F6 Cs1B F5 49.75(8) 8_455 7_656 ?
F6 Cs1B F7 49.16(8) 8_455 8_455 ?
F6 Cs1B F8 123.78(10) 8_455 7_657 ?
F6 Cs1B F8 94.34(11) 8_455 8_455 ?
F6 Cs1B F9 124.37(10) 8_455 2_757 ?
F6 Cs1B F10 95.27(10) 8_455 2_757 ?
F7 Cs1B F2C 113.2(2) 8_455 8_556 ?
F7 Cs1B F8 119.78(11) 8_455 7_657 ?
F7 Cs1B F9 167.73(11) 8_455 2_757 ?
F7 Cs1B F10 120.97(11) 8_455 2_757 ?
F8 Cs1B F2C 109.6(2) 8_455 8_556 ?
F8 Cs1B F2C 91.2(2) 7_657 8_556 ?
F8 Cs1B F2C 107.6(2) . 8_556 ?
F8 Cs1B F5 93.79(11) . 7_656 ?
F8 Cs1B F6 76.12(9) . 8_455 ?
F8 Cs1B F7 124.78(10) . 8_455 ?
F8 Cs1B F7 72.74(9) 8_455 8_455 ?
F8 Cs1B F8 94.20(11) . 7_657 ?
F8 Cs1B F8 47.05(10) 8_455 7_657 ?
F8 Cs1B F8 125.24(8) . 8_455 ?
F8 Cs1B F9 119.45(11) 8_455 2_757 ?
F8 Cs1B F9 48.51(8) . 2_757 ?
F8 Cs1B F9 72.40(9) 7_657 2_757 ?
F8 Cs1B F10 48.53(8) . 2_757 ?
F8 Cs1B F10 166.28(12) 8_455 2_757 ?
F9 Cs1B F2C 139.8(2) 8_455 8_556 ?
F9 Cs1B F2C 65.5(2) 2_757 8_556 ?
F9 Cs1B F5 124.78(11) 8_455 7_656 ?
F9 Cs1B F6 75.43(9) 8_455 8_455 ?
F9 Cs1B F7 93.65(11) 8_455 8_455 ?
F9 Cs1B F8 48.67(8) 8_455 7_657 ?
F9 Cs1B F8 48.87(8) 8_455 8_455 ?
F9 Cs1B F8 76.88(9) 8_455 . ?
F9 Cs1B F9 94.17(11) 8_455 2_757 ?
F9 Cs1B F10 124.90(11) 8_455 2_757 ?
F10 Cs1B F2C 66.7(2) 2_757 8_556 ?
F10 Cs1B F8 119.23(11) 2_757 7_657 ?
F10 Cs1B F9 46.83(8) 2_757 2_757 ?
F1A Cs2 F1A 15.0(9) 6 . ?
F1A Cs2 F3 133.5(3) 6 . ?
F1A Cs2 F3 133.5(3) . . ?
F1A Cs2 F4 90.8(3) 6 2_656 ?
F1A Cs2 F4 90.8(3) . 5_656 ?
F1A Cs2 F4 84.8(3) . 2_656 ?
F1A Cs2 F4 84.8(3) 6 5_656 ?
F1A Cs2 F5 119.7(5) 6 5_656 ?
F1A Cs2 F5 85.3(3) . 6_455 ?
F1A Cs2 F5 119.7(5) . 2_656 ?
F1A Cs2 F5 76.1(4) . 1_455 ?
F1A Cs2 F5 85.3(3) 6 1_455 ?
F1A Cs2 F5 132.3(4) . 5_656 ?
F1A Cs2 F5 76.1(4) 6 6_455 ?
F1A Cs2 F5 132.3(4) 6 2_656 ?
F1A Cs2 F7 76.8(5) . 2_656 ?
F1A Cs2 F7 91.7(5) 6 2_656 ?
F1A Cs2 F7 76.8(5) 6 5_656 ?
F1A Cs2 F7 91.7(5) . 5_656 ?
F1B Cs2 F1A 12.5(5) . . ?
F1B Cs2 F1A 12.5(5) . 6 ?
F1B Cs2 F3 123.9(5) . . ?
F1B Cs2 F4 78.6(5) . 5_656 ?
F1B Cs2 F4 78.6(5) . 2_656 ?
F1B Cs2 F5 88.7(4) . 6_455 ?
F1B Cs2 F5 131.0(2) . 5_656 ?
F1B Cs2 F5 131.0(2) . 2_656 ?
F1B Cs2 F5 88.7(4) . 1_455 ?
F1B Cs2 F7 85.36(8) . 2_656 ?
F1B Cs2 F7 85.36(8) . 5_656 ?
F3 Cs2 F4 50.86(8) . 5_656 ?
F3 Cs2 F4 50.86(8) . 2_656 ?
F3 Cs2 F5 84.39(8) . 2_656 ?
F3 Cs2 F5 132.22(6) . 1_455 ?
F3 Cs2 F5 132.22(6) . 6_455 ?
F3 Cs2 F5 84.39(8) . 5_656 ?
F3 Cs2 F7 98.31(6) . 2_656 ?
F3 Cs2 F7 98.31(6) . 5_656 ?
F4 Cs2 F4 47.53(12) 2_656 5_656 ?
F4 Cs2 F5 161.72(8) 5_656 1_455 ?
F4 Cs2 F5 117.37(7) 5_656 6_455 ?
F4 Cs2 F5 117.37(7) 2_656 1_455 ?
F4 Cs2 F5 161.72(8) 2_656 6_455 ?
F4 Cs2 F7 72.07(7) 5_656 5_656 ?
F4 Cs2 F7 119.32(8) 2_656 5_656 ?
F4 Cs2 F7 119.32(8) 5_656 2_656 ?
F4 Cs2 F7 72.07(7) 2_656 2_656 ?
F5 Cs2 F4 133.89(8) 2_656 5_656 ?
F5 Cs2 F4 98.23(9) 5_656 5_656 ?
F5 Cs2 F4 133.89(8) 5_656 2_656 ?
F5 Cs2 F4 98.23(9) 2_656 2_656 ?
F5 Cs2 F5 74.85(9) 6_455 1_455 ?
F5 Cs2 F5 100.03(7) 5_656 1_455 ?
F5 Cs2 F5 49.03(9) 5_656 6_455 ?
F5 Cs2 F5 86.10(11) 2_656 5_656 ?
F5 Cs2 F5 100.03(7) 2_656 6_455 ?
F5 Cs2 F5 49.03(9) 2_656 1_455 ?
F5 Cs2 F7 45.71(7) 6_455 5_656 ?
F5 Cs2 F7 48.62(7) 5_656 5_656 ?
F5 Cs2 F7 133.63(7) 2_656 5_656 ?
F5 Cs2 F7 48.62(7) 2_656 2_656 ?
F5 Cs2 F7 120.29(7) 6_455 2_656 ?
F5 Cs2 F7 133.63(7) 5_656 2_656 ?
F5 Cs2 F7 120.29(7) 1_455 5_656 ?
F5 Cs2 F7 45.71(7) 1_455 2_656 ?
F7 Cs2 F7 163.38(11) 5_656 2_656 ?
F1A Cs3 F1A 14.1(9) 3_656 8_656 ?
F1A Cs3 F1B 7.2(5) 3_656 3_656 ?
F1A Cs3 F1B 7.2(5) 8_656 3_656 ?
F1A Cs3 F2A 34.3(5) 8_656 8_656 ?
F1A Cs3 F2A 44.9(4) 3_656 8_656 ?
F1A Cs3 F2B 51.3(4) 8_656 3_656 ?
F1A Cs3 F2B 51.3(4) 3_656 8_656 ?
F1A Cs3 F2B 43.1(5) 3_656 3_656 ?
F1A Cs3 F2B 43.1(5) 8_656 8_656 ?
F1B Cs3 F2A 40.4(4) 3_656 8_656 ?
F2B Cs3 F1B 48.1(5) 3_656 3_656 ?
F2B Cs3 F1B 48.1(5) 8_656 3_656 ?
F2B Cs3 F2A 11.6(3) 8_656 8_656 ?
F2B Cs3 F2A 55.1(3) 3_656 8_656 ?
F2B Cs3 F2B 50.6(4) 8_656 3_656 ?
F2C Cs3 F1A 52.8(4) 4_656 3_656 ?
F2C Cs3 F1A 56.2(4) 7_656 3_656 ?
F2C Cs3 F1A 56.2(4) 4_656 8_656 ?
F2C Cs3 F1A 52.8(4) 7_656 8_656 ?
F2C Cs3 F1B 55.7(6) 4_656 3_656 ?
F2C Cs3 F1B 55.7(6) 7_656 3_656 ?
F2C Cs3 F2A 46.3(4) 4_656 8_656 ?
F2C Cs3 F2A 29.1(3) 7_656 8_656 ?
F2C Cs3 F2B 18.5(3) 7_656 8_656 ?
F2C Cs3 F2B 38.3(4) 7_656 3_656 ?
F2C Cs3 F2B 18.5(3) 4_656 3_656 ?
F2C Cs3 F2B 38.3(4) 4_656 8_656 ?
F2C Cs3 F2C 22.1(5) 7_656 4_656 ?
F5 Cs3 F1A 91.4(4) 8_556 3_656 ?
F5 Cs3 F1A 81.4(4) 3_556 3_656 ?
F5 Cs3 F1A 81.4(4) 8_556 8_656 ?
F5 Cs3 F1A 91.4(4) 3_556 8_656 ?
F5 Cs3 F1B 85.3(4) 8_556 3_656 ?
F5 Cs3 F1B 85.3(4) 3_556 3_656 ?
F5 Cs3 F2A 84.8(2) 8_556 8_656 ?
F5 Cs3 F2A 125.6(2) 3_556 8_656 ?
F5 Cs3 F2B 94.2(3) 3_556 3_656 ?
F5 Cs3 F2B 132.5(2) 8_556 3_656 ?
F5 Cs3 F2B 94.2(2) 8_556 8_656 ?
F5 Cs3 F2B 132.5(2) 3_556 8_656 ?
F5 Cs3 F2C 112.5(3) 8_556 7_656 ?
F5 Cs3 F2C 130.9(3) 8_556 4_656 ?
F5 Cs3 F2C 112.5(3) 3_556 4_656 ?
F5 Cs3 F2C 130.9(3) 3_556 7_656 ?
F5 Cs3 F5 89.90(12) 3_556 8_556 ?
F10 Cs3 F1A 128.7(4) 6_565 8_656 ?
F10 Cs3 F1A 128.7(4) . 3_656 ?
F10 Cs3 F1A 117.3(5) . 8_656 ?
F10 Cs3 F1A 117.3(5) 6_565 3_656 ?
F10 Cs3 F1B 124.0(3) . 3_656 ?
F10 Cs3 F1B 124.0(3) 6_565 3_656 ?
F10 Cs3 F2A 83.9(2) . 8_656 ?
F10 Cs3 F2A 122.5(3) 6_565 8_656 ?
F10 Cs3 F2B 78.0(2) 6_565 3_656 ?
F10 Cs3 F2B 78.0(2) . 8_656 ?
F10 Cs3 F2B 111.7(3) . 3_656 ?
F10 Cs3 F2B 111.7(3) 6_565 8_656 ?
F10 Cs3 F2C 78.5(3) . 7_656 ?
F10 Cs3 F2C 78.5(3) 6_565 4_656 ?
F10 Cs3 F2C 93.5(3) 6_565 7_656 ?
F10 Cs3 F2C 93.5(3) . 4_656 ?
F10 Cs3 F5 149.37(9) . 3_556 ?
F10 Cs3 F5 149.37(9) 6_565 8_556 ?
F10 Cs3 F5 84.54(9) 6_565 3_556 ?
F10 Cs3 F5 84.54(9) . 8_556 ?
F10 Cs3 F10 85.12(13) . 6_565 ?
F1A Cs4 F1A 7.0(5) 2_656 5_656 ?
F1A Cs4 F1B 11.3(5) 2_656 5_656 ?
F1A Cs4 F2A 52.0(4) 2_656 1_656 ?
F1A Cs4 F2A 36.3(5) 2_656 2_656 ?
F1A Cs4 F6 154.0(3) 2_656 8_455 ?
F1B Cs4 F1A 4.7(5) 5_656 5_656 ?
F1B Cs4 F2A 53.5(6) 5_656 1_656 ?
F1B Cs4 F2A 44.3(6) 5_656 2_656 ?
F1B Cs4 F6 153.2(6) 5_656 8_455 ?
F2A Cs4 F1A 42.0(4) 2_656 5_656 ?
F2A Cs4 F1A 54.1(4) 1_656 5_656 ?
F2A Cs4 F2A 29.3(5) 1_656 2_656 ?
F2A Cs4 F6 154.3(2) 2_656 8_455 ?
F2A Cs4 F6 153.2(2) 1_656 8_455 ?
F2B Cs4 F1A 52.9(4) 1_656 2_656 ?
F2B Cs4 F1A 52.8(3) 1_656 5_656 ?
F2B Cs4 F1B 50.7(6) 1_656 5_656 ?
F2B Cs4 F2A 40.7(3) 1_656 2_656 ?
F2B Cs4 F2A 14.7(3) 1_656 1_656 ?
F2B Cs4 F2C 18.5(3) 1_656 2_656 ?
F2B Cs4 F6 152.7(2) 1_656 8_455 ?
F2C Cs4 F1A 47.6(4) 2_656 2_656 ?
F2C Cs4 F1A 44.8(4) 2_656 5_656 ?
F2C Cs4 F1B 41.3(6) 2_656 5_656 ?
F2C Cs4 F2A 50.7(3) 2_656 2_656 ?
F2C Cs4 F2A 31.8(4) 2_656 1_656 ?
F2C Cs4 F6 152.0(2) 2_656 8_455 ?
F4 Cs4 F1A 89.0(4) . 2_656 ?
F4 Cs4 F1A 83.0(3) . 5_656 ?
F4 Cs4 F1B 80.8(6) . 5_656 ?
F4 Cs4 F2A 125.0(3) . 2_656 ?
F4 Cs4 F2A 124.0(3) . 1_656 ?
F4 Cs4 F2B 111.1(3) . 1_656 ?
F4 Cs4 F2C 92.7(3) . 2_656 ?
F4 Cs4 F6 76.13(9) . 8_455 ?
F4 Cs4 F7 88.40(10) . . ?
F4 Cs4 F8 154.82(10) . . ?
F4 Cs4 F9 87.76(11) . 8_455 ?
F6 Cs4 F1A 152.7(3) 8_455 5_656 ?
F7 Cs4 F1A 86.3(3) . 5_656 ?
F7 Cs4 F1A 82.7(3) . 2_656 ?
F7 Cs4 F1B 90.3(5) . 5_656 ?
F7 Cs4 F2A 89.3(2) . 2_656 ?
F7 Cs4 F2A 118.5(3) . 1_656 ?
F7 Cs4 F2B 129.3(2) . 1_656 ?
F7 Cs4 F2C 130.2(3) . 2_656 ?
F7 Cs4 F6 75.82(9) . 8_455 ?
F7 Cs4 F8 85.89(10) . . ?
F7 Cs4 F9 153.30(9) . 8_455 ?
F8 Cs4 F1A 120.9(3) . 5_656 ?
F8 Cs4 F1A 114.5(4) . 2_656 ?
F8 Cs4 F1B 123.7(5) . 5_656 ?
F8 Cs4 F2A 79.9(3) . 1_656 ?
F8 Cs4 F2A 79.5(3) . 2_656 ?
F8 Cs4 F2B 91.2(3) . 1_656 ?
F8 Cs4 F2C 109.6(3) . 2_656 ?
F8 Cs4 F6 78.69(8) . 8_455 ?
F8 Cs4 F9 86.43(10) . 8_455 ?
F9 Cs4 F1A 123.6(3) 8_455 2_656 ?
F9 Cs4 F1A 119.4(2) 8_455 5_656 ?
F9 Cs4 F1B 115.1(5) 8_455 5_656 ?
F9 Cs4 F2A 114.3(3) 8_455 2_656 ?
F9 Cs4 F2A 85.1(2) 8_455 1_656 ?
F9 Cs4 F2B 76.4(2) 8_455 1_656 ?
F9 Cs4 F2C 76.4(3) 8_455 2_656 ?
F9 Cs4 F6 77.61(9) 8_455 8_455 ?
F2C Cs5 F2B 10.5(3) 8_556 7_556 ?
F2C Cs5 F2B 33.5(3) 3_556 7_556 ?
F2C Cs5 F2C 23.8(6) 8_556 3_556 ?
F2C Cs5 F3 137.3(3) 3_556 7_657 ?
F2C Cs5 F3 137.3(3) 8_556 7_657 ?
F2C Cs5 F4 87.6(3) 3_556 4_657 ?
F2C Cs5 F4 87.6(3) 8_556 7_657 ?
F2C Cs5 F4 97.0(3) 8_556 4_657 ?
F2C Cs5 F4 97.0(3) 3_556 7_657 ?
F2C Cs5 F9 97.4(3) 3_556 2_757 ?
F2C Cs5 F9 73.8(3) 3_556 5_767 ?
F2C Cs5 F9 97.4(3) 8_556 5_767 ?
F2C Cs5 F9 73.8(3) 8_556 2_757 ?
F2C Cs5 F10 117.5(3) 8_556 . ?
F2C Cs5 F10 73.8(3) 3_556 5_767 ?
F2C Cs5 F10 117.5(3) 3_556 6_565 ?
F2C Cs5 F10 73.8(3) 8_556 2_757 ?
F2C Cs5 F10 136.5(3) 3_556 . ?
F2C Cs5 F10 87.7(3) 3_556 2_757 ?
F2C Cs5 F10 87.7(3) 8_556 5_767 ?
F2C Cs5 F10 136.5(3) 8_556 6_565 ?
F3 Cs5 F2B 138.5(2) 7_657 7_556 ?
F3 Cs5 F4 50.53(8) 7_657 7_657 ?
F3 Cs5 F4 50.53(8) 7_657 4_657 ?
F3 Cs5 F9 97.82(6) 7_657 2_757 ?
F3 Cs5 F9 97.82(6) 7_657 5_767 ?
F3 Cs5 F10 130.47(7) 7_657 2_757 ?
F3 Cs5 F10 81.62(8) 7_657 6_565 ?
F3 Cs5 F10 81.62(8) 7_657 . ?
F3 Cs5 F10 130.47(7) 7_657 5_767 ?
F4 Cs5 F2B 88.0(2) 7_657 7_556 ?
F4 Cs5 F2B 104.74(19) 4_657 7_556 ?
F4 Cs5 F4 46.94(12) 4_657 7_657 ?
F4 Cs5 F10 120.47(7) 7_657 2_757 ?
F4 Cs5 F10 120.47(7) 4_657 5_767 ?
F4 Cs5 F10 165.73(9) 7_657 5_767 ?
F4 Cs5 F10 165.73(9) 4_657 2_757 ?
F9 Cs5 F2B 63.88(19) 2_757 7_556 ?
F9 Cs5 F2B 106.2(2) 5_767 7_556 ?
F9 Cs5 F4 120.39(8) 5_767 7_657 ?
F9 Cs5 F4 73.58(8) 2_757 7_657 ?
F9 Cs5 F4 73.58(8) 5_767 4_657 ?
F9 Cs5 F4 120.39(8) 2_757 4_657 ?
F9 Cs5 F9 163.75(12) 2_757 5_767 ?
F9 Cs5 F10 47.07(7) 5_767 5_767 ?
F9 Cs5 F10 47.07(7) 2_757 2_757 ?
F9 Cs5 F10 117.85(7) 2_757 5_767 ?
F9 Cs5 F10 117.85(7) 5_767 2_757 ?
F10 Cs5 F2B 64.91(18) 2_757 7_556 ?
F10 Cs5 F2B 89.8(2) 5_767 7_556 ?
F10 Cs5 F2B 139.4(2) 6_565 7_556 ?
F10 Cs5 F2B 107.08(17) . 7_556 ?
F10 Cs5 F4 98.63(9) 6_565 4_657 ?
F10 Cs5 F4 131.37(8) 6_565 7_657 ?
F10 Cs5 F4 131.37(8) . 4_657 ?
F10 Cs5 F4 98.63(9) . 7_657 ?
F10 Cs5 F9 128.77(8) . 5_767 ?
F10 Cs5 F9 128.77(8) 6_565 2_757 ?
F10 Cs5 F9 49.94(7) . 2_757 ?
F10 Cs5 F9 49.94(7) 6_565 5_767 ?
F10 Cs5 F10 95.49(8) . 5_767 ?
F10 Cs5 F10 70.90(10) 2_757 5_767 ?
F10 Cs5 F10 49.59(9) . 2_757 ?
F10 Cs5 F10 79.78(12) 6_565 . ?
F10 Cs5 F10 95.49(8) 6_565 2_757 ?
F10 Cs5 F10 49.59(9) 6_565 5_767 ?
F3 Cs6 F4 47.37(9) 3 8 ?
F3 Cs6 F6 121.32(8) 3 8_455 ?
F3 Cs6 F8 116.95(8) 3 . ?
F3 Cs6 F9 88.82(9) 3 . ?
F3 Cs6 F10 70.68(8) 3 2_757 ?
F4 Cs6 F3 47.65(9) 7_656 3 ?
F4 Cs6 F4 47.21(10) 7_656 8 ?
F4 Cs6 F5 92.54(8) 7_656 7_656 ?
F4 Cs6 F6 121.50(7) 7_656 8_455 ?
F4 Cs6 F8 162.80(7) 7_656 . ?
F4 Cs6 F8 118.35(7) 8 . ?
F4 Cs6 F9 71.88(7) 8 . ?
F4 Cs6 F9 118.70(7) 7_656 . ?
F4 Cs6 F10 118.21(7) 7_656 2_757 ?
F4 Cs6 F10 90.73(9) 8 2_757 ?
F5 Cs6 F3 73.73(8) 7_656 3 ?
F5 Cs6 F4 120.91(7) 7_656 8 ?
F5 Cs6 F6 47.70(6) 7_656 8_455 ?
F5 Cs6 F8 88.94(8) 7_656 . ?
F5 Cs6 F9 117.21(7) 7_656 . ?
F5 Cs6 F10 70.99(7) 7_656 2_757 ?
F6 Cs6 F3 117.37(8) . 3 ?
F6 Cs6 F3 118.72(8) 2_756 3 ?
F6 Cs6 F4 166.87(6) 8_455 8 ?
F6 Cs6 F4 70.05(7) . 8 ?
F6 Cs6 F4 71.31(8) 2_756 7_656 ?
F6 Cs6 F4 90.64(9) . 7_656 ?
F6 Cs6 F4 89.83(9) 2_756 8 ?
F6 Cs6 F5 119.86(7) 2_756 7_656 ?
F6 Cs6 F5 166.72(6) . 7_656 ?
F6 Cs6 F6 91.93(8) 2_756 8_455 ?
F6 Cs6 F6 120.351(15) . 8_455 ?
F6 Cs6 F6 49.46(9) 2_756 . ?
F6 Cs6 F7 71.75(7) 2_756 7_656 ?
F6 Cs6 F7 120.88(7) . 7_656 ?
F6 Cs6 F8 122.31(7) 2_756 . ?
F6 Cs6 F8 71.26(7) 8_455 . ?
F6 Cs6 F8 91.83(8) . . ?
F6 Cs6 F9 72.04(7) . . ?
F6 Cs6 F9 121.35(7) 2_756 . ?
F6 Cs6 F9 117.75(7) 8_455 . ?
F6 Cs6 F10 166.48(6) 2_756 2_757 ?
F6 Cs6 F10 118.46(7) . 2_757 ?
F6 Cs6 F10 90.58(7) 8_455 2_757 ?
F7 Cs6 F3 165.68(8) . 3 ?
F7 Cs6 F3 93.52(9) 7_656 3 ?
F7 Cs6 F4 120.71(8) . 7_656 ?
F7 Cs6 F4 74.11(7) 7_656 7_656 ?
F7 Cs6 F4 121.23(7) 7_656 8 ?
F7 Cs6 F4 119.59(8) . 8 ?
F7 Cs6 F5 48.20(7) 7_656 7_656 ?
F7 Cs6 F5 118.25(7) . 7_656 ?
F7 Cs6 F6 70.68(7) . 8_455 ?
F7 Cs6 F6 49.74(7) . . ?
F7 Cs6 F6 49.59(7) . 2_756 ?
F7 Cs6 F6 47.62(7) 7_656 8_455 ?
F7 Cs6 F7 89.95(8) . 7_656 ?
F7 Cs6 F8 72.97(7) . . ?
F7 Cs6 F8 118.58(7) 7_656 . ?
F7 Cs6 F9 163.17(7) 7_656 . ?
F7 Cs6 F9 91.87(8) . . ?
F7 Cs6 F10 119.36(7) . 2_757 ?
F7 Cs6 F10 119.02(7) 7_656 2_757 ?
F8 Cs6 F9 46.63(7) . . ?
F8 Cs6 F10 46.53(7) . 2_757 ?
F9 Cs6 F10 46.50(7) . 2_757 ?
Cs1A Ga1 Cs1A 64.62(3) 8 2_757 ?
Cs1A Ga1 Cs1A 86.69(4) 8 7_657 ?
Cs1A Ga1 Cs1A 64.62(3) 7_657 . ?
Cs1A Ga1 Cs1A 104.42(2) 7_657 2_757 ?
Cs1A Ga1 Cs1A 104.42(2) 8 . ?
Cs1A Ga1 Cs1A 165.81(4) 2_757 . ?
Cs1A Ga1 Cs5 168.25(2) 8 . ?
Cs1A Ga1 Cs5 106.801(19) . 5_767 ?
Cs1A Ga1 Cs5 103.70(2) 7_657 . ?
Cs1A Ga1 Cs5 85.26(2) 2_757 5_767 ?
Cs1A Ga1 Cs5 106.800(19) 2_757 . ?
Cs1A Ga1 Cs5 103.70(2) 8 5_767 ?
Cs1A Ga1 Cs5 85.26(2) . . ?
Cs1A Ga1 Cs5 168.25(2) 7_657 5_767 ?
Cs5 Ga1 Cs5 66.571(13) 5_767 . ?
F8 Ga1 Cs1A 120.33(10) . 2_757 ?
F8 Ga1 Cs1A 57.84(10) . 8 ?
F8 Ga1 Cs1A 59.59(11) 2_757 8 ?
F8 Ga1 Cs1A 47.05(10) 2_757 2_757 ?
F8 Ga1 Cs1A 120.33(10) 2_757 . ?
F8 Ga1 Cs1A 59.59(11) . 7_657 ?
F8 Ga1 Cs1A 57.84(10) 2_757 7_657 ?
F8 Ga1 Cs1A 47.05(10) . . ?
F8 Ga1 Cs5 132.30(10) . . ?
F8 Ga1 Cs5 132.30(10) 2_757 5_767 ?
F8 Ga1 Cs5 121.38(11) . 5_767 ?
F8 Ga1 Cs5 121.38(11) 2_757 . ?
F8 Ga1 F8 88.9(2) . 2_757 ?
F8 Ga1 F9 90.69(15) . 2_757 ?
F8 Ga1 F9 90.05(15) . . ?
F8 Ga1 F9 90.69(15) 2_757 . ?
F8 Ga1 F9 90.05(15) 2_757 2_757 ?
F8 Ga1 F10 90.22(14) 2_757 . ?
F8 Ga1 F10 178.73(14) . . ?
F8 Ga1 F10 178.73(14) 2_757 2_757 ?
F8 Ga1 F10 90.21(14) . 2_757 ?
F9 Ga1 Cs1A 133.85(10) 2_757 8 ?
F9 Ga1 Cs1A 133.85(10) . 7_657 ?
F9 Ga1 Cs1A 120.73(11) 2_757 2_757 ?
F9 Ga1 Cs1A 120.73(11) . . ?
F9 Ga1 Cs1A 47.18(10) . 8 ?
F9 Ga1 Cs1A 59.42(11) . 2_757 ?
F9 Ga1 Cs1A 47.18(10) 2_757 7_657 ?
F9 Ga1 Cs1A 59.42(11) 2_757 . ?
F9 Ga1 Cs5 122.09(10) 2_757 5_767 ?
F9 Ga1 Cs5 122.09(10) . . ?
F9 Ga1 Cs5 56.89(10) . 5_767 ?
F9 Ga1 Cs5 56.89(10) 2_757 . ?
F9 Ga1 F9 179.0(2) 2_757 . ?
F9 Ga1 F10 90.20(15) 2_757 . ?
F9 Ga1 F10 90.20(15) . 2_757 ?
F9 Ga1 F10 89.08(15) 2_757 2_757 ?
F9 Ga1 F10 89.08(15) . . ?
F10 Ga1 Cs1A 58.41(10) . 2_757 ?
F10 Ga1 Cs1A 120.91(10) 2_757 7_657 ?
F10 Ga1 Cs1A 120.56(11) 2_757 8 ?
F10 Ga1 Cs1A 58.41(10) 2_757 . ?
F10 Ga1 Cs1A 120.56(11) . 7_657 ?
F10 Ga1 Cs1A 134.21(10) 2_757 2_757 ?
F10 Ga1 Cs1A 120.91(10) . 8 ?
F10 Ga1 Cs1A 134.21(10) . . ?
F10 Ga1 Cs5 48.97(10) 2_757 5_767 ?
F10 Ga1 Cs5 58.77(11) 2_757 . ?
F10 Ga1 Cs5 58.77(11) . 5_767 ?
F10 Ga1 Cs5 48.97(10) . . ?
F10 Ga1 F10 90.7(2) 2_757 . ?
F1A Ga2 F1A 180.0(14) 6 2 ?
F1A Ga2 F1A 157.1(15) . 2 ?
F1A Ga2 F1A 22.9(15) 5 2 ?
F1A Ga2 F1A 180.0(3) . 5 ?
F1A Ga2 F1A 157.1(15) 5 6 ?
F1A Ga2 F1A 22.9(15) . 6 ?
F1A Ga2 F2C 90.7(6) 6 5 ?
F1A Ga2 F2C 89.3(6) 6 . ?
F1A Ga2 F2C 97.7(6) . 5 ?
F1A Ga2 F2C 82.3(6) 5 5 ?
F1A Ga2 F2C 90.7(6) 2 . ?
F1A Ga2 F2C 82.3(6) . . ?
F1A Ga2 F2C 97.7(6) 5 . ?
F1A Ga2 F2C 89.3(6) 2 5 ?
F1B Ga2 F1A 161.0(7) 5 . ?
F1B Ga2 F1A 161.0(7) 5 6 ?
F1B Ga2 F1A 161.0(7) . 5 ?
F1B Ga2 F1A 161.0(7) . 2 ?
F1B Ga2 F1A 19.0(7) . 6 ?
F1B Ga2 F1A 19.0(7) 5 2 ?
F1B Ga2 F1A 19.0(7) . . ?
F1B Ga2 F1A 19.0(7) 5 5 ?
F1B Ga2 F1B 180.0 . 5 ?
F1B Ga2 F2C 108.9(8) 5 . ?
F1B Ga2 F2C 71.1(8) 5 5 ?
F1B Ga2 F2C 71.1(8) . . ?
F1B Ga2 F2C 108.9(8) . 5 ?
F2A Ga2 F1A 85.3(8) . 6 ?
F2A Ga2 F1A 85.3(8) 6 . ?
F2A Ga2 F1A 64.0(9) 6 6 ?
F2A Ga2 F1A 116.0(9) 6 2 ?
F2A Ga2 F1A 116.0(9) 5 . ?
F2A Ga2 F1A 64.0(9) 2 2 ?
F2A Ga2 F1A 116.0(9) 2 6 ?
F2A Ga2 F1A 64.0(9) . . ?
F2A Ga2 F1A 94.7(8) 2 . ?
F2A Ga2 F1A 64.0(9) 5 5 ?
F2A Ga2 F1A 94.7(8) 5 6 ?
F2A Ga2 F1A 116.0(9) . 5 ?
F2A Ga2 F1A 85.3(8) 5 2 ?
F2A Ga2 F1A 94.7(8) 6 5 ?
F2A Ga2 F1A 85.3(8) 2 5 ?
F2A Ga2 F1A 94.7(8) . 2 ?
F2A Ga2 F1B 99.4(6) 2 . ?
F2A Ga2 F1B 99.4(6) 6 5 ?
F2A Ga2 F1B 80.6(6) 5 5 ?
F2A Ga2 F1B 99.4(6) 5 . ?
F2A Ga2 F1B 80.6(6) 2 5 ?
F2A Ga2 F1B 80.6(6) . . ?
F2A Ga2 F1B 99.4(6) . 5 ?
F2A Ga2 F1B 80.6(6) 6 . ?
F2A Ga2 F2A 128.1(10) 6 . ?
F2A Ga2 F2A 180.0 5 . ?
F2A Ga2 F2A 51.9(10) 2 . ?
F2A Ga2 F2A 180.0(9) 6 2 ?
F2A Ga2 F2A 51.9(10) 6 5 ?
F2A Ga2 F2A 128.1(10) 2 5 ?
F2A Ga2 F2C 92.1(6) 5 5 ?
F2A Ga2 F2C 87.9(6) 5 . ?
F2A Ga2 F2C 54.2(6) 6 5 ?
F2A Ga2 F2C 87.9(6) . 5 ?
F2A Ga2 F2C 92.1(6) . . ?
F2A Ga2 F2C 125.8(6) 6 . ?
F2A Ga2 F2C 54.2(6) 2 . ?
F2A Ga2 F2C 125.8(6) 2 5 ?
F2C Ga2 F2C 180.0 . 5 ?
Cs2 Ga3 Cs2 180.0 5_656 . ?
Cs2 Ga3 Cs5 94.649(9) 5_656 3_444 ?
Cs2 Ga3 Cs5 85.351(9) 5_656 7_657 ?
Cs2 Ga3 Cs5 94.649(9) . 7_657 ?
Cs2 Ga3 Cs5 85.351(9) . 3_444 ?
Cs2 Ga3 Cs6 66.390(5) 5_656 4_646 ?
Cs2 Ga3 Cs6 66.390(5) . 8_455 ?
Cs2 Ga3 Cs6 113.610(5) 5_656 8_455 ?
Cs2 Ga3 Cs6 113.610(5) . 4_646 ?
Cs5 Ga3 Cs5 180.0 7_657 3_444 ?
Cs5 Ga3 Cs6 111.903(5) 7_657 4_646 ?
Cs5 Ga3 Cs6 68.097(5) 7_657 8_455 ?
Cs5 Ga3 Cs6 111.903(5) 3_444 8_455 ?
Cs5 Ga3 Cs6 68.097(5) 3_444 4_646 ?
Cs6 Ga3 Cs6 180.0 4_646 8_455 ?
F3 Ga3 Cs2 132.72(13) . 5_656 ?
F3 Ga3 Cs2 132.73(13) 5_656 . ?
F3 Ga3 Cs2 47.28(13) . . ?
F3 Ga3 Cs2 47.27(13) 5_656 5_656 ?
F3 Ga3 Cs5 47.37(13) 5_656 3_444 ?
F3 Ga3 Cs5 132.63(13) 5_656 7_657 ?
F3 Ga3 Cs5 132.63(13) . 3_444 ?
F3 Ga3 Cs5 47.37(13) . 7_657 ?
F3 Ga3 Cs6 124.792(5) 5_656 8_455 ?
F3 Ga3 Cs6 55.208(5) . 8_455 ?
F3 Ga3 Cs6 124.792(5) . 4_646 ?
F3 Ga3 Cs6 55.208(5) 5_656 4_646 ?
F3 Ga3 F3 180.0 5_656 . ?
F4 Ga3 Cs2 121.68(12) 2_656 5_656 ?
F4 Ga3 Cs2 121.68(12) 6 . ?
F4 Ga3 Cs2 58.32(12) 2_656 . ?
F4 Ga3 Cs2 58.32(12) 5_656 . ?
F4 Ga3 Cs2 121.68(12) . . ?
F4 Ga3 Cs2 121.68(12) 5_656 5_656 ?
F4 Ga3 Cs2 58.32(12) 6 5_656 ?
F4 Ga3 Cs2 58.32(12) . 5_656 ?
F4 Ga3 Cs5 58.73(12) 2_656 3_444 ?
F4 Ga3 Cs5 121.27(12) 6 3_444 ?
F4 Ga3 Cs5 121.27(12) 5_656 7_657 ?
F4 Ga3 Cs5 121.27(12) . 3_444 ?
F4 Ga3 Cs5 58.73(12) 5_656 3_444 ?
F4 Ga3 Cs5 58.73(12) 6 7_657 ?
F4 Ga3 Cs5 121.27(12) 2_656 7_657 ?
F4 Ga3 Cs5 58.73(12) . 7_657 ?
F4 Ga3 Cs6 55.79(12) 5_656 4_646 ?
F4 Ga3 Cs6 124.21(12) 5_656 8_455 ?
F4 Ga3 Cs6 55.79(12) . 8_455 ?
F4 Ga3 Cs6 53.57(12) 6 4_646 ?
F4 Ga3 Cs6 126.43(12) 6 8_455 ?
F4 Ga3 Cs6 126.43(12) 2_656 4_646 ?
F4 Ga3 Cs6 124.21(12) . 4_646 ?
F4 Ga3 Cs6 53.57(12) 2_656 8_455 ?
F4 Ga3 F3 89.70(15) 6 5_656 ?
F4 Ga3 F3 90.30(15) 5_656 5_656 ?
F4 Ga3 F3 90.29(15) . . ?
F4 Ga3 F3 90.30(15) 2_656 5_656 ?
F4 Ga3 F3 89.70(15) 2_656 . ?
F4 Ga3 F3 89.71(15) . 5_656 ?
F4 Ga3 F3 89.70(15) 5_656 . ?
F4 Ga3 F3 90.30(15) 6 . ?
F4 Ga3 F4 180.0(2) 6 2_656 ?
F4 Ga3 F4 89.5(2) 6 . ?
F4 Ga3 F4 90.5(2) 5_656 6 ?
F4 Ga3 F4 90.5(2) 2_656 . ?
F4 Ga3 F4 180.0 5_656 . ?
F4 Ga3 F4 89.5(2) 5_656 2_656 ?
Cs1A Ga4 Cs1A 169.99(4) 8 7_656 ?
Cs1A Ga4 Cs1B 4.58(3) 7_656 7_656 ?
Cs1A Ga4 Cs1B 173.39(5) 7_656 8 ?
Cs1A Ga4 Cs1B 173.39(5) 8 7_656 ?
Cs1A Ga4 Cs1B 4.58(3) 8 8 ?
Cs1A Ga4 Cs6 103.43(2) 8 2_756 ?
Cs1A Ga4 Cs6 103.43(2) 7_656 . ?
Cs1A Ga4 Cs6 68.121(17) 7_656 2_756 ?
Cs1A Ga4 Cs6 68.121(17) 8 . ?
Cs1B Ga4 Cs1B 177.73(7) 8 7_656 ?
Cs6 Ga4 Cs1B 70.06(4) 2_756 7_656 ?
Cs6 Ga4 Cs1B 70.06(4) . 8 ?
Cs6 Ga4 Cs1B 108.01(3) . 7_656 ?
Cs6 Ga4 Cs1B 108.01(3) 2_756 8 ?
Cs6 Ga4 Cs6 72.729(13) 2_756 . ?
F5 Ga4 Cs1A 131.98(9) 2_756 7_656 ?
F5 Ga4 Cs1A 131.98(9) . 8 ?
F5 Ga4 Cs1A 56.97(9) . 7_656 ?
F5 Ga4 Cs1A 56.97(9) 2_756 8 ?
F5 Ga4 Cs1B 127.41(9) . 8 ?
F5 Ga4 Cs1B 54.60(10) . 7_656 ?
F5 Ga4 Cs1B 54.59(10) 2_756 8 ?
F5 Ga4 Cs1B 127.41(10) 2_756 7_656 ?
F5 Ga4 Cs6 124.51(9) . 2_756 ?
F5 Ga4 Cs6 125.24(10) . . ?
F5 Ga4 Cs6 125.24(10) 2_756 2_756 ?
F5 Ga4 Cs6 124.51(9) 2_756 . ?
F5 Ga4 F5 89.52(18) 2_756 . ?
F6 Ga4 Cs1A 122.59(9) . 7_656 ?
F6 Ga4 Cs1A 122.59(9) 2_756 8 ?
F6 Ga4 Cs1A 48.56(9) . 8 ?
F6 Ga4 Cs1A 48.56(9) 2_756 7_656 ?
F6 Ga4 Cs1B 124.89(10) . 7_656 ?
F6 Ga4 Cs1B 53.13(9) . 8 ?
F6 Ga4 Cs1B 124.89(10) 2_756 8 ?
F6 Ga4 Cs1B 53.13(9) 2_756 7_656 ?
F6 Ga4 Cs6 54.90(9) 2_756 . ?
F6 Ga4 Cs6 54.90(9) . 2_756 ?
F6 Ga4 Cs6 55.75(9) 2_756 2_756 ?
F6 Ga4 Cs6 55.74(9) . . ?
F6 Ga4 F5 90.21(12) 2_756 . ?
F6 Ga4 F5 178.87(14) 2_756 2_756 ?
F6 Ga4 F5 178.87(14) . . ?
F6 Ga4 F5 90.21(12) . 2_756 ?
F6 Ga4 F6 90.09(17) 2_756 . ?
F7 Ga4 Cs1A 120.97(10) . 7_656 ?
F7 Ga4 Cs1A 59.17(10) . 8 ?
F7 Ga4 Cs1A 59.18(10) 2_756 7_656 ?
F7 Ga4 Cs1A 120.97(10) 2_756 8 ?
F7 Ga4 Cs1B 123.50(11) 2_756 8 ?
F7 Ga4 Cs1B 56.54(11) . 8 ?
F7 Ga4 Cs1B 123.50(11) . 7_656 ?
F7 Ga4 Cs1B 56.54(11) 2_756 7_656 ?
F7 Ga4 Cs6 127.07(10) 2_756 . ?
F7 Ga4 Cs6 54.35(10) 2_756 2_756 ?
F7 Ga4 Cs6 127.07(10) . 2_756 ?
F7 Ga4 Cs6 54.34(10) . . ?
F7 Ga4 F5 90.16(14) . . ?
F7 Ga4 F5 88.83(14) 2_756 . ?
F7 Ga4 F5 88.83(14) . 2_756 ?
F7 Ga4 F5 90.16(14) 2_756 2_756 ?
F7 Ga4 F6 90.08(14) . 2_756 ?
F7 Ga4 F6 90.08(14) 2_756 . ?
F7 Ga4 F6 90.92(14) 2_756 2_756 ?
F7 Ga4 F6 90.92(14) . . ?
F7 Ga4 F7 178.6(2) . 2_756 ?
Cs1B F1A Cs4 177.2(5) 7_556 5_656 ?
Cs2 F1A Cs1B 104.2(6) . 7_556 ?
Cs2 F1A Cs3 84.6(4) . 3_344 ?
Cs2 F1A Cs4 73.1(5) . 5_656 ?
Cs2 F1A Cs4 83.7(5) . 2_656 ?
Cs3 F1A Cs1B 68.3(4) 3_344 7_556 ?
Cs3 F1A Cs4 130.1(7) 3_344 2_656 ?
Cs3 F1A Cs4 110.5(6) 3_344 5_656 ?
Cs4 F1A Cs1B 68.0(5) 2_656 7_556 ?
Cs4 F1A Cs4 112.0(4) 2_656 5_656 ?
Ga2 F1A Cs1B 97.1(8) . 7_556 ?
Ga2 F1A Cs2 158.7(12) . . ?
Ga2 F1A Cs3 102.5(6) . 3_344 ?
Ga2 F1A Cs4 105.7(7) . 2_656 ?
Ga2 F1A Cs4 85.6(7) . 5_656 ?
F1A F1A Cs1B 149.4(3) 6 7_556 ?
F1A F1A Cs2 82.5(5) 6 . ?
F1A F1A Cs3 82.9(5) 6 3_344 ?
F1A F1A Cs4 142.5(4) 6 2_656 ?
F1A F1A Cs4 30.5(2) 6 5_656 ?
F1A F1A Ga2 78.6(7) 6 . ?
F1B F1A Cs1B 157(3) . 7_556 ?
F1B F1A Cs2 81(5) . . ?
F1B F1A Cs3 135(3) . 3_344 ?
F1B F1A Cs4 90(3) . 2_656 ?
F1B F1A Cs4 25(3) . 5_656 ?
F1B F1A Ga2 80(4) . . ?
F1B F1A F1A 53(3) . 6 ?
Cs2 F1B Cs3 76.9(6) . 3_344 ?
Cs2 F1B Cs4 83.1(7) . 2_656 ?
Cs2 F1B Cs4 83.1(7) . 5_656 ?
Cs4 F1B Cs3 113.0(4) 5_656 3_344 ?
Cs4 F1B Cs3 113.0(4) 2_656 3_344 ?
Cs4 F1B Cs4 127.0(9) 2_656 5_656 ?
Ga2 F1B Cs2 164.3(12) . . ?
Ga2 F1B Cs3 87.5(9) . 3_344 ?
Ga2 F1B Cs4 103.4(7) . 5_656 ?
Ga2 F1B Cs4 103.4(7) . 2_656 ?
F1A F1B Cs2 87(4) 6 . ?
F1A F1B Cs2 87(4) . . ?
F1A F1B Cs3 38(3) . 3_344 ?
F1A F1B Cs3 38(3) 6 3_344 ?
F1A F1B Cs4 151(3) . 5_656 ?
F1A F1B Cs4 78(3) . 2_656 ?
F1A F1B Cs4 151(3) 6 2_656 ?
F1A F1B Cs4 78(3) 6 5_656 ?
F1A F1B Ga2 81(5) . . ?
F1A F1B Ga2 81(5) 6 . ?
F1A F1B F1A 74(6) . 6 ?
Cs1A F2A Cs1B 102.7(4) 7_556 8_454 ?
Cs1A F2A Cs3 76.5(3) 7_556 3_344 ?
Cs1A F2A Cs4 86.6(4) 7_556 1_454 ?
Cs1A F2A Cs4 81.9(4) 7_556 2_656 ?
Cs1B F2A Cs1A 0.58(9) 7_556 7_556 ?
Cs1B F2A Cs1B 103.3(5) 7_556 8_454 ?
Cs1B F2A Cs3 76.0(4) 7_556 3_344 ?
Cs1B F2A Cs4 81.9(4) 7_556 2_656 ?
Cs1B F2A Cs4 87.0(4) 7_556 1_454 ?
Cs3 F2A Cs1B 178.3(5) 3_344 8_454 ?
Cs4 F2A Cs1B 67.6(3) 2_656 8_454 ?
Cs4 F2A Cs1B 65.6(3) 1_454 8_454 ?
Cs4 F2A Cs3 115.8(5) 1_454 3_344 ?
Cs4 F2A Cs3 110.7(4) 2_656 3_344 ?
Cs4 F2A Cs4 127.6(5) 1_454 2_656 ?
Ga2 F2A Cs1A 163.6(8) . 7_556 ?
Ga2 F2A Cs1B 93.2(5) . 8_454 ?
Ga2 F2A Cs1B 163.1(8) . 7_556 ?
Ga2 F2A Cs3 87.4(6) . 3_344 ?
Ga2 F2A Cs4 103.6(6) . 1_454 ?
Ga2 F2A Cs4 101.1(6) . 2_656 ?
F2A F2A Cs1A 131.5(4) 2 7_556 ?
F2A F2A Cs1B 132.0(4) 2 7_556 ?
F2A F2A Cs1B 29.3(2) 2 8_454 ?
F2A F2A Cs3 151.1(3) 2 3_344 ?
F2A F2A Cs4 77.7(10) 2 1_454 ?
F2A F2A Cs4 73.0(10) 2 2_656 ?
F2A F2A Ga2 64.1(5) 2 . ?
F2A F2A F2C 108.0(11) 2 2 ?
F2B F2A Cs1A 91.4(13) . 7_556 ?
F2B F2A Cs1B 91.2(13) . 7_556 ?
F2B F2A Cs1B 132.5(17) . 8_454 ?
F2B F2A Cs3 49.2(15) . 3_344 ?
F2B F2A Cs4 159.9(18) . 2_656 ?
F2B F2A Cs4 70.3(16) . 1_454 ?
F2B F2A Ga2 80.4(14) . . ?
F2B F2A F2A 124(2) . 2 ?
F2B F2A F2C 17.9(11) . 2 ?
F2C F2A Cs1A 109.1(8) 2 7_556 ?
F2C F2A Cs1B 108.9(8) 2 7_556 ?
F2C F2A Cs1B 122.9(8) 2 8_454 ?
F2C F2A Cs3 58.8(6) 2 3_344 ?
F2C F2A Cs4 160.6(9) 2 2_656 ?
F2C F2A Cs4 70.3(7) 2 1_454 ?
F2C F2A Ga2 63.9(7) 2 . ?
Cs1A F2B Cs3 82.6(3) 7_556 3_344 ?
Cs1A F2B Cs4 87.6(3) 7_556 1_454 ?
Cs1A F2B Cs5 108.5(3) 7_556 7_556 ?
Cs1B F2B Cs1A 1.84(8) 7_556 7_556 ?
Cs1B F2B Cs3 83.2(3) 7_556 3_344 ?
Cs1B F2B Cs4 88.3(3) 7_556 1_454 ?
Cs1B F2B Cs5 110.3(3) 7_556 7_556 ?
Cs3 F2B Cs5 73.0(3) 3_344 7_556 ?
Cs4 F2B Cs3 139.2(4) 1_454 3_344 ?
Cs4 F2B Cs5 72.9(3) 1_454 7_556 ?
Ga2 F2B Cs1A 144.7(6) . 7_556 ?
Ga2 F2B Cs1B 142.9(7) . 7_556 ?
Ga2 F2B Cs3 101.5(5) . 3_344 ?
Ga2 F2B Cs4 109.0(5) . 1_454 ?
Ga2 F2B Cs5 106.2(5) . 7_556 ?
F2A F2B Cs1A 72.7(12) . 7_556 ?
F2A F2B Cs1B 71.0(12) . 7_556 ?
F2A F2B Cs3 119.2(17) . 3_344 ?
F2A F2B Cs4 95.0(17) . 1_454 ?
F2A F2B Cs5 167.6(18) . 7_556 ?
F2A F2B Ga2 74.8(12) . . ?
F2A F2B F2C 147.4(19) . 2 ?
F2C F2B Cs1A 139.5(12) 2 7_556 ?
F2C F2B Cs1B 141.3(12) 2 7_556 ?
F2C F2B Cs3 78.5(11) 2 3_344 ?
F2C F2B Cs4 84.0(11) 2 1_454 ?
F2C F2B Cs5 31.5(10) 2 7_556 ?
F2C F2B Ga2 74.7(10) 2 . ?
Cs1B F2C Cs1A 2.26(6) 8_454 8_454 ?
Cs3 F2C Cs1A 70.9(3) 7_656 8_454 ?
Cs3 F2C Cs1B 71.4(3) 7_656 8_454 ?
Cs3 F2C Cs4 138.4(5) 7_656 2_656 ?
Cs4 F2C Cs1A 73.8(3) 2_656 8_454 ?
Cs4 F2C Cs1B 74.1(3) 2_656 8_454 ?
Cs5 F2C Cs1A 107.8(4) 3_444 8_454 ?
Cs5 F2C Cs1B 110.0(4) 3_444 8_454 ?
Cs5 F2C Cs3 86.1(3) 3_444 7_656 ?
Cs5 F2C Cs4 84.4(4) 3_444 2_656 ?
Ga2 F2C Cs1A 105.8(5) . 8_454 ?
Ga2 F2C Cs1B 103.5(5) . 8_454 ?
Ga2 F2C Cs3 103.1(5) . 7_656 ?
Ga2 F2C Cs4 107.1(4) . 2_656 ?
Ga2 F2C Cs5 146.4(7) . 3_444 ?
F2A F2C Cs1A 45.3(5) 2 8_454 ?
F2A F2C Cs1B 43.1(5) 2 8_454 ?
F2A F2C Cs3 92.0(7) 2 7_656 ?
F2A F2C Cs4 77.9(7) 2 2_656 ?
F2A F2C Cs5 151.1(9) 2 3_444 ?
F2A F2C Ga2 61.9(6) 2 . ?
F2B F2C Cs1A 30.8(9) 2 8_454 ?
F2B F2C Cs1B 28.5(9) 2 8_454 ?
F2B F2C Cs3 83.0(12) 2 7_656 ?
F2B F2C Cs4 77.5(11) 2 2_656 ?
F2B F2C Cs5 138.1(13) 2 3_444 ?
F2B F2C Ga2 75.5(10) 2 . ?
F2B F2C F2A 14.8(9) 2 2 ?
F2B F2C F2C 138.1(11) 2 6 ?
F2C F2C Cs1A 148.52(19) 6 8_454 ?
F2C F2C Cs1B 148.3(2) 6 8_454 ?
F2C F2C Cs3 78.9(3) 6 7_656 ?
F2C F2C Cs4 137.6(3) 6 2_656 ?
F2C F2C Cs5 78.1(3) 6 3_444 ?
F2C F2C Ga2 72.2(4) 6 . ?
F2C F2C F2A 129.8(7) 6 2 ?
Cs2 F3 Cs3 74.49(9) . 7_657 ?
Cs2 F3 Cs5 152.38(15) . 7_657 ?
Cs2 F3 Cs6 87.21(7) . 8_455 ?
Cs2 F3 Cs6 87.21(7) . 3_445 ?
Cs5 F3 Cs3 77.89(9) 7_657 7_657 ?
Cs5 F3 Cs6 89.64(7) 7_657 3_445 ?
Cs5 F3 Cs6 89.64(7) 7_657 8_455 ?
Cs6 F3 Cs3 83.36(7) 3_445 7_657 ?
Cs6 F3 Cs3 83.36(7) 8_455 7_657 ?
Cs6 F3 Cs6 166.56(13) 3_445 8_455 ?
Ga3 F3 Cs2 103.73(16) . . ?
Ga3 F3 Cs3 178.22(19) . 7_657 ?
Ga3 F3 Cs5 103.89(16) . 7_657 ?
Ga3 F3 Cs6 96.60(7) . 3_445 ?
Ga3 F3 Cs6 96.60(7) . 8_455 ?
Cs2 F4 Cs5 105.13(11) 5_656 7_657 ?
Cs2 F4 Cs6 167.33(12) 5_656 8_455 ?
Cs2 F4 Cs6 82.26(9) 5_656 7_656 ?
Cs4 F4 Cs2 80.89(9) . 5_656 ?
Cs4 F4 Cs5 79.19(8) . 7_657 ?
Cs4 F4 Cs6 91.53(9) . 8_455 ?
Cs4 F4 Cs6 90.64(9) . 7_656 ?
Cs5 F4 Cs6 83.18(9) 7_657 8_455 ?
Cs6 F4 Cs5 166.13(11) 7_656 7_657 ?
Cs6 F4 Cs6 87.73(9) 7_656 8_455 ?
Ga3 F4 Cs2 92.53(13) . 5_656 ?
Ga3 F4 Cs4 167.4(2) . . ?
Ga3 F4 Cs5 92.35(13) . 7_657 ?
Ga3 F4 Cs6 99.12(14) . 7_656 ?
Ga3 F4 Cs6 96.72(13) . 8_455 ?
Cs1A F5 Cs1B 5.77(3) 7_656 7_656 ?
Cs1A F5 Cs2 106.62(9) 7_656 1_655 ?
Cs1A F5 Cs6 84.43(8) 7_656 7_656 ?
Cs1B F5 Cs2 101.64(10) 7_656 1_655 ?
Cs1B F5 Cs6 88.72(9) 7_656 7_656 ?
Cs2 F5 Cs1A 159.35(10) 5_656 7_656 ?
Cs2 F5 Cs1B 157.22(10) 5_656 7_656 ?
Cs2 F5 Cs2 79.97(7) 5_656 1_655 ?
Cs2 F5 Cs6 85.91(8) 5_656 7_656 ?
Cs3 F5 Cs1A 79.66(7) 3_444 7_656 ?
Cs3 F5 Cs1B 75.41(8) 3_444 7_656 ?
Cs3 F5 Cs2 82.95(7) 3_444 5_656 ?
Cs3 F5 Cs2 77.07(7) 3_444 1_655 ?
Cs3 F5 Cs6 94.42(8) 3_444 7_656 ?
Cs6 F5 Cs2 164.27(10) 7_656 1_655 ?
Ga4 F5 Cs1A 93.28(11) . 7_656 ?
Ga4 F5 Cs1B 96.61(12) . 7_656 ?
Ga4 F5 Cs2 93.49(11) . 1_655 ?
Ga4 F5 Cs2 106.01(11) . 5_656 ?
Ga4 F5 Cs3 165.86(16) . 3_444 ?
Ga4 F5 Cs6 97.07(11) . 7_656 ?
Cs1A F6 Cs1B 4.24(5) 8 8 ?
Cs1A F6 Cs4 77.04(7) 8 8 ?
Cs1A F6 Cs6 87.92(7) 8 8 ?
Cs1A F6 Cs6 88.87(8) 8 . ?
Cs1A F6 Cs6 161.25(10) 8 2_756 ?
Cs1B F6 Cs4 81.28(8) 8 8 ?
Cs1B F6 Cs6 88.97(9) 8 . ?
Cs1B F6 Cs6 88.59(8) 8 8 ?
Cs1B F6 Cs6 165.49(10) 8 2_756 ?
Cs4 F6 Cs6 83.32(6) 8 8 ?
Cs6 F6 Cs4 84.30(6) 2_756 8 ?
Cs6 F6 Cs4 85.98(7) . 8 ?
Cs6 F6 Cs6 91.71(7) 2_756 . ?
Cs6 F6 Cs6 169.26(9) . 8 ?
Cs6 F6 Cs6 88.07(8) 2_756 8 ?
Ga4 F6 Cs1A 102.57(11) . 8 ?
Ga4 F6 Cs1B 98.34(11) . 8 ?
Ga4 F6 Cs4 178.81(14) . 8 ?
Ga4 F6 Cs6 96.04(10) . 2_756 ?
Ga4 F6 Cs6 95.14(11) . . ?
Ga4 F6 Cs6 95.55(11) . 8 ?
Cs1A F7 Cs2 104.19(9) 8 5_656 ?
Cs1B F7 Cs1A 5.65(3) 8 8 ?
Cs1B F7 Cs2 99.56(9) 8 5_656 ?
Cs4 F7 Cs1A 80.09(8) . 8 ?
Cs4 F7 Cs1B 75.73(8) . 8 ?
Cs4 F7 Cs2 77.76(7) . 5_656 ?
Cs4 F7 Cs6 90.59(8) . 7_656 ?
Cs4 F7 Cs6 94.12(8) . . ?
Cs6 F7 Cs1A 83.78(8) . 8 ?
Cs6 F7 Cs1A 168.38(10) 7_656 8 ?
Cs6 F7 Cs1B 87.76(9) . 8 ?
Cs6 F7 Cs1B 165.94(10) 7_656 8 ?
Cs6 F7 Cs2 167.24(10) . 5_656 ?
Cs6 F7 Cs2 80.31(7) 7_656 5_656 ?
Cs6 F7 Cs6 90.05(8) . 7_656 ?
Ga4 F7 Cs1A 91.47(11) . 8 ?
Ga4 F7 Cs1B 94.99(12) . 8 ?
Ga4 F7 Cs2 92.87(11) . 5_656 ?
Ga4 F7 Cs4 165.30(17) . . ?
Ga4 F7 Cs6 99.06(12) . 7_656 ?
Ga4 F7 Cs6 96.92(11) . . ?
Cs1A F8 Cs1A 106.73(10) 8 7_657 ?
Cs1A F8 Cs1A 82.25(9) . 7_657 ?
Cs1A F8 Cs1A 159.41(11) . 8 ?
Cs1A F8 Cs1B 85.77(10) . 7_657 ?
Cs1A F8 Cs1B 4.50(5) . . ?
Cs1A F8 Cs1B 102.00(10) 8 7_657 ?
Cs1A F8 Cs1B 157.88(10) . 8 ?
Cs1A F8 Cs6 167.26(10) 7_657 . ?
Cs1A F8 Cs6 87.48(8) . . ?
Cs1A F8 Cs6 80.72(8) 8 . ?
Cs1B F8 Cs1A 81.94(9) . 7_657 ?
Cs1B F8 Cs1A 5.63(3) 8 8 ?
Cs1B F8 Cs1A 163.44(11) . 8 ?
Cs1B F8 Cs1A 101.95(10) 8 7_657 ?
Cs1B F8 Cs1A 5.53(3) 7_657 7_657 ?
Cs1B F8 Cs1B 85.80(11) . 7_657 ?
Cs1B F8 Cs1B 97.08(11) 8 7_657 ?
Cs1B F8 Cs1B 162.31(12) . 8 ?
Cs1B F8 Cs6 88.40(9) . . ?
Cs1B F8 Cs6 166.39(10) 7_657 . ?
Cs1B F8 Cs6 84.86(9) 8 . ?
Cs4 F8 Cs1A 83.66(8) . . ?
Cs4 F8 Cs1A 81.71(8) . 7_657 ?
Cs4 F8 Cs1A 79.49(8) . 8 ?
Cs4 F8 Cs1B 77.80(9) . 7_657 ?
Cs4 F8 Cs1B 75.59(8) . 8 ?
Cs4 F8 Cs1B 88.06(9) . . ?
Cs4 F8 Cs6 89.72(8) . . ?
Ga1 F8 Cs1A 93.30(11) . 8 ?
Ga1 F8 Cs1A 91.51(12) . 7_657 ?
Ga1 F8 Cs1A 105.15(13) . . ?
Ga1 F8 Cs1B 100.67(13) . . ?
Ga1 F8 Cs1B 96.50(12) . 8 ?
Ga1 F8 Cs1B 94.72(13) . 7_657 ?
Ga1 F8 Cs4 168.15(16) . . ?
Ga1 F8 Cs6 98.45(12) . . ?
Cs1A F9 Cs1A 82.28(9) 8 2_757 ?
Cs1A F9 Cs1B 85.59(10) 8 2_757 ?
Cs1A F9 Cs1B 4.72(5) 8 8 ?
Cs1A F9 Cs5 159.04(10) 8 5_767 ?
Cs1A F9 Cs6 166.13(10) 2_757 . ?
Cs1A F9 Cs6 85.83(9) 8 . ?
Cs1B F9 Cs1A 82.17(9) 8 2_757 ?
Cs1B F9 Cs1A 5.54(3) 2_757 2_757 ?
Cs1B F9 Cs1B 85.83(11) 8 2_757 ?
Cs1B F9 Cs5 163.32(11) 8 5_767 ?
Cs1B F9 Cs6 86.57(10) 8 . ?
Cs1B F9 Cs6 165.54(10) 2_757 . ?
Cs4 F9 Cs1A 83.41(8) 8 8 ?
Cs4 F9 Cs1A 81.58(8) 8 2_757 ?
Cs4 F9 Cs1B 77.48(9) 8 2_757 ?
Cs4 F9 Cs1B 88.06(9) 8 8 ?
Cs4 F9 Cs5 78.68(7) 8 5_767 ?
Cs4 F9 Cs6 89.99(8) 8 . ?
Cs5 F9 Cs1A 105.53(10) 5_767 2_757 ?
Cs5 F9 Cs1B 100.90(10) 5_767 2_757 ?
Cs5 F9 Cs6 83.39(8) 5_767 . ?
Ga1 F9 Cs1A 91.69(12) . 2_757 ?
Ga1 F9 Cs1A 104.97(13) . 8 ?
Ga1 F9 Cs1B 95.16(13) . 2_757 ?
Ga1 F9 Cs1B 100.25(12) . 8 ?
Ga1 F9 Cs4 168.56(17) . 8 ?
Ga1 F9 Cs5 94.36(11) . 5_767 ?
Ga1 F9 Cs6 98.29(13) . . ?
Cs1A F10 Cs5 104.89(10) 2_757 5_767 ?
Cs1A F10 Cs6 81.32(8) 2_757 2_757 ?
Cs1B F10 Cs1A 5.60(3) 2_757 2_757 ?
Cs1B F10 Cs5 100.08(10) 2_757 5_767 ?
Cs1B F10 Cs6 85.55(9) 2_757 2_757 ?
Cs3 F10 Cs1A 78.56(7) . 2_757 ?
Cs3 F10 Cs1B 74.54(8) . 2_757 ?
Cs3 F10 Cs5 88.04(8) . . ?
Cs3 F10 Cs5 78.51(8) . 5_767 ?
Cs3 F10 Cs6 93.32(8) . 2_757 ?
Cs5 F10 Cs1A 161.54(10) . 2_757 ?
Cs5 F10 Cs1B 160.54(10) . 2_757 ?
Cs5 F10 Cs5 84.51(8) . 5_767 ?
Cs5 F10 Cs6 168.32(10) 5_767 2_757 ?
Cs5 F10 Cs6 86.90(8) . 2_757 ?
Ga1 F10 Cs1A 92.66(11) . 2_757 ?
Ga1 F10 Cs1B 95.80(12) . 2_757 ?
Ga1 F10 Cs3 165.09(17) . . ?
Ga1 F10 Cs5 92.36(12) . 5_767 ?
Ga1 F10 Cs5 102.94(12) . . ?
Ga1 F10 Cs6 97.28(12) . 2_757 ?

