# Electronic Supplementary Material (ESI) for Dalton Transactions.
# This journal is © The Royal Society of Chemistry 2023

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_9biAT
_audit_block_doi                 10.5517/ccdc.csd.cc2dyl43
_database_code_depnum_ccdc_archive 'CCDC 2232965'
loop_
_audit_author_name
_audit_author_address
'Kang Mun Lee'
;Kangwon National University
South Korea
;
_audit_update_record             
;
2022-12-27 deposited with the CCDC.	2023-05-11 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2018/3
_shelx_SHELXL_version_number     2018/3
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         'C44 H46 B20'
_chemical_formula_sum            'C44 H46 B20'
_chemical_formula_weight         791.01

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   11.9622(7)
_cell_length_b                   13.4561(8)
_cell_length_c                   14.6657(9)
_cell_angle_alpha                75.096(2)
_cell_angle_beta                 73.810(2)
_cell_angle_gamma                79.007(2)
_cell_volume                     2172.7(2)
_cell_formula_units_Z            2
_cell_measurement_temperature    296(2)
_cell_measurement_reflns_used    32778
_cell_measurement_theta_min      2.533
_cell_measurement_theta_max      25.403

_exptl_crystal_description       plate
_exptl_crystal_colour            yellow
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    1.209
_exptl_crystal_F_000             820
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          0.078
_exptl_crystal_size_mid          0.074
_exptl_crystal_size_min          0.022
_exptl_absorpt_coefficient_mu    0.061
_shelx_estimated_absorpt_T_min   0.995
_shelx_estimated_absorpt_T_max   0.999
_exptl_absorpt_correction_type   MULTI-SCAN
_exptl_absorpt_correction_T_min  0.6366
_exptl_absorpt_correction_T_max  0.7455
_exptl_absorpt_process_details   ?
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      296(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_source                   'I\^I1/4S 3.0 Microfocus'
_diffrn_measurement_device_type  'PHOTON II 14'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            32778
_diffrn_reflns_av_unetI/netI     0.1020
_diffrn_reflns_av_R_equivalents  0.0929
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_limit_l_max       17
_diffrn_reflns_theta_min         2.533
_diffrn_reflns_theta_max         25.403
_diffrn_reflns_theta_full        25.242
_diffrn_measured_fraction_theta_max 0.988
_diffrn_measured_fraction_theta_full 0.989
_diffrn_reflns_Laue_measured_fraction_max 0.988
_diffrn_reflns_Laue_measured_fraction_full 0.989
_diffrn_reflns_point_group_measured_fraction_max 0.988
_diffrn_reflns_point_group_measured_fraction_full 0.989
_reflns_number_total             7915
_reflns_number_gt                4357
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       'Bruker APEX4'
_computing_cell_refinement       'Bruker APEX4'
_computing_data_reduction        'Bruker APEX4'
_computing_structure_solution    SHELXS
_computing_structure_refinement  SHELXL
_computing_molecular_graphics    ORTEP
_computing_publication_material  CIFTAB
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0844P)²+1.3101P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_number_reflns         7915
_refine_ls_number_parameters     577
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.1536
_refine_ls_R_factor_gt           0.0804
_refine_ls_wR_factor_ref         0.2004
_refine_ls_wR_factor_gt          0.1686
_refine_ls_goodness_of_fit_ref   0.981
_refine_ls_restrained_S_all      0.981
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
B1 B 0.2789(4) 0.5215(3) 0.5945(3) 0.0483(10) Uani 1 1 d . . . . .
H1 H 0.360488 0.549381 0.546465 0.058 Uiso 1 1 calc R U . . .
C2 C 0.1013(3) 0.6641(3) 0.9768(3) 0.0497(9) Uani 1 1 d . . . . .
H2 H 0.030326 0.649653 1.020555 0.060 Uiso 1 1 calc R U . . .
C1 C 0.1229(3) 0.6500(2) 0.8857(2) 0.0416(8) Uani 1 1 d . . . . .
H1A H 0.066265 0.624651 0.868545 0.050 Uiso 1 1 calc R U . . .
B2 B 0.2598(4) 0.3886(3) 0.6222(3) 0.0611(12) Uani 1 1 d . . . . .
H2A H 0.326650 0.330268 0.590744 0.073 Uiso 1 1 calc R U . . .
C3 C 0.1857(3) 0.7006(3) 1.0066(3) 0.0502(9) Uani 1 1 d . . . . .
H3 H 0.172849 0.705774 1.070788 0.060 Uiso 1 1 calc R U . . .
B3 B 0.1746(4) 0.4815(4) 0.5520(3) 0.0610(12) Uani 1 1 d . . . . .
H3A H 0.186687 0.483731 0.474360 0.073 Uiso 1 1 calc R U . . .
C4 C 0.2841(3) 0.7275(2) 0.9415(2) 0.0446(8) Uani 1 1 d . . . . .
H4 H 0.338705 0.752714 0.961216 0.053 Uiso 1 1 calc R U . . .
B4 B 0.1387(4) 0.5976(4) 0.5964(3) 0.0534(11) Uani 1 1 d . . . . .
H4A H 0.127045 0.674120 0.547810 0.064 Uiso 1 1 calc R U . . .
C5 C 0.5033(3) 0.8215(3) 0.6027(3) 0.0549(10) Uani 1 1 d . . . . .
H5 H 0.556584 0.848462 0.622348 0.066 Uiso 1 1 calc R U . . .
B5 B 0.1762(4) 0.3597(3) 0.7429(3) 0.0566(12) Uani 1 1 d . . . . .
H5A H 0.187467 0.282876 0.791059 0.068 Uiso 1 1 calc R U . . .
C6 C 0.5098(3) 0.8367(3) 0.5071(3) 0.0619(11) Uani 1 1 d . . . . .
H6 H 0.565299 0.875441 0.461511 0.074 Uiso 1 1 calc R U . . .
B6 B 0.1081(4) 0.3813(4) 0.6449(4) 0.0643(13) Uani 1 1 d . . . . .
H6A H 0.075088 0.318588 0.628474 0.077 Uiso 1 1 calc R U . . .
C7 C 0.4322(3) 0.7936(3) 0.4771(3) 0.0558(10) Uani 1 1 d . . . . .
H7 H 0.435836 0.804972 0.411071 0.067 Uiso 1 1 calc R U . . .
B7 B 0.0345(4) 0.5092(4) 0.6297(3) 0.0604(12) Uani 1 1 d . . . . .
H7A H -0.046340 0.528607 0.603467 0.072 Uiso 1 1 calc R U . . .
C8 C 0.3522(3) 0.7358(3) 0.5421(2) 0.0476(9) Uani 1 1 d . . . . .
H8 H 0.302747 0.707751 0.519340 0.057 Uiso 1 1 calc R U . . .
B8 B 0.0549(3) 0.5685(3) 0.7172(3) 0.0486(10) Uani 1 1 d . . . . .
H8A H -0.012802 0.625891 0.749380 0.058 Uiso 1 1 calc R U . . .
C9 C 0.2560(3) 0.6583(2) 0.7166(2) 0.0365(7) Uani 1 1 d . . . . .
B9 B 0.1466(3) 0.4763(3) 0.7856(3) 0.0439(9) Uani 1 1 d . . . . .
H9 H 0.142155 0.474870 0.861892 0.053 Uiso 1 1 calc R U . . .
C10 C 0.4051(3) 0.7594(2) 0.7741(2) 0.0401(8) Uani 1 1 d . . . . .
B10 B 0.0371(4) 0.4357(3) 0.7480(3) 0.0564(12) Uani 1 1 d . . . . .
H10 H -0.042279 0.407835 0.800144 0.068 Uiso 1 1 calc R U . . .
C11 C 0.4168(3) 0.7651(2) 0.6748(2) 0.0407(8) Uani 1 1 d . . . . .
B11 B 0.9073(3) 0.8805(3) 0.8063(3) 0.0459(10) Uani 1 1 d . . . . .
H11 H 0.918315 0.796741 0.809455 0.055 Uiso 1 1 calc R U . . .
C12 C 0.3405(3) 0.7161(2) 0.6450(2) 0.0401(8) Uani 1 1 d . . . . .
B12 B 0.8545(3) 0.9324(3) 0.9136(3) 0.0500(10) Uani 1 1 d . . . . .
H12 H 0.833730 0.883365 0.987186 0.060 Uiso 1 1 calc R U . . .
C13 C 0.2285(3) 0.6723(2) 0.8141(2) 0.0353(7) Uani 1 1 d . . . . .
B13 B 1.0019(4) 0.9391(3) 0.8434(3) 0.0560(12) Uani 1 1 d . . . . .
H13 H 1.076072 0.893865 0.872421 0.067 Uiso 1 1 calc R U . . .
C14 C 0.3082(3) 0.7189(2) 0.8428(2) 0.0377(8) Uani 1 1 d . . . . .
B14 B 1.0049(3) 0.9601(3) 0.7192(3) 0.0536(11) Uani 1 1 d . . . . .
H14 H 1.081059 0.929013 0.667687 0.064 Uiso 1 1 calc R U . . .
C15 C 0.2005(3) 0.5788(2) 0.6921(2) 0.0387(8) Uani 1 1 d . . . . .
B15 B 0.9218(4) 1.0811(3) 0.6847(4) 0.0578(12) Uani 1 1 d . . . . .
H15 H 0.943161 1.129354 0.610775 0.069 Uiso 1 1 calc R U . . .
C16 C 0.2759(3) 0.4461(2) 0.7075(2) 0.0444(8) Uani 1 1 d . . . . .
B16 B 1.0096(4) 1.0660(3) 0.7691(4) 0.0633(13) Uani 1 1 d . . . . .
H16 H 1.088468 1.104990 0.750008 0.076 Uiso 1 1 calc R U . . .
C17 C 0.3874(3) 0.4240(2) 0.7409(3) 0.0452(8) Uani 1 1 d . . . . .
B17 B 0.9193(4) 1.0488(3) 0.8871(4) 0.0596(12) Uani 1 1 d . . . . .
H17 H 0.940652 1.076203 0.943968 0.072 Uiso 1 1 calc R U . . .
C18 C 0.3867(3) 0.4073(3) 0.8370(3) 0.0660(11) Uani 1 1 d . . . . .
H18 H 0.315820 0.416080 0.882500 0.079 Uiso 1 1 calc R U . . .
B18 B 0.7717(4) 1.0540(3) 0.8804(3) 0.0526(11) Uani 1 1 d . . . . .
H18A H 0.696468 1.085543 0.932399 0.063 Uiso 1 1 calc R U . . .
C19 C 0.4904(4) 0.3775(3) 0.8678(3) 0.0760(13) Uani 1 1 d . . . . .
H19 H 0.488027 0.367191 0.933493 0.091 Uiso 1 1 calc R U . . .
B19 B 0.7748(3) 1.0715(3) 0.7538(3) 0.0487(10) Uani 1 1 d . . . . .
H19A H 0.700168 1.112009 0.723108 0.058 Uiso 1 1 calc R U . . .
C20 C 0.5931(4) 0.3635(3) 0.8043(4) 0.0751(13) Uani 1 1 d . . . . .
H20 H 0.662048 0.343039 0.825412 0.090 Uiso 1 1 calc R U . . .
B20 B 0.8662(4) 1.1359(3) 0.7899(4) 0.0604(12) Uani 1 1 d . . . . .
H20A H 0.850728 1.220349 0.783772 0.072 Uiso 1 1 calc R U . . .
C21 C 0.5961(4) 0.3796(4) 0.7082(4) 0.0969(16) Uani 1 1 d . . . . .
H21 H 0.667561 0.370535 0.663400 0.116 Uiso 1 1 calc R U . . .
C22 C 0.4938(4) 0.4091(4) 0.6769(3) 0.0818(14) Uani 1 1 d . . . . .
H22 H 0.497047 0.419040 0.611090 0.098 Uiso 1 1 calc R U . . .
C31 C 0.7506(3) 0.7172(3) 0.9095(2) 0.0459(8) Uani 1 1 d . . . . .
H31 H 0.798560 0.742694 0.935941 0.055 Uiso 1 1 calc R U . . .
C32 C 0.7620(3) 0.6144(3) 0.9158(3) 0.0552(10) Uani 1 1 d . . . . .
H32 H 0.818506 0.570826 0.945038 0.066 Uiso 1 1 calc R U . . .
C33 C 0.6907(4) 0.5725(3) 0.8794(3) 0.0689(12) Uani 1 1 d . . . . .
H33 H 0.702425 0.501834 0.880944 0.083 Uiso 1 1 calc R U . . .
C34 C 0.6037(3) 0.6347(3) 0.8414(3) 0.0573(10) Uani 1 1 d . . . . .
H34 H 0.555159 0.605728 0.818463 0.069 Uiso 1 1 calc R U . . .
C35 C 0.3617(3) 0.9722(3) 0.7900(3) 0.0583(10) Uani 1 1 d . . . . .
H35 H 0.309773 0.942523 0.771392 0.070 Uiso 1 1 calc R U . . .
C36 C 0.3354(3) 1.0711(3) 0.7981(4) 0.0799(14) Uani 1 1 d . . . . .
H36 H 0.266372 1.109730 0.784841 0.096 Uiso 1 1 calc R U . . .
C37 C 0.4130(3) 1.1163(3) 0.8269(4) 0.0740(13) Uani 1 1 d . . . . .
H37 H 0.392901 1.183995 0.835684 0.089 Uiso 1 1 calc R U . . .
C38 C 0.5153(3) 1.0634(3) 0.8418(3) 0.0568(10) Uani 1 1 d . . . . .
H38 H 0.564983 1.096034 0.860016 0.068 Uiso 1 1 calc R U . . .
C39 C 0.6592(3) 0.8986(2) 0.8469(2) 0.0397(8) Uani 1 1 d . . . . .
C40 C 0.4889(3) 0.8060(2) 0.8054(2) 0.0399(8) Uani 1 1 d . . . . .
C41 C 0.4676(3) 0.9106(2) 0.8092(2) 0.0419(8) Uani 1 1 d . . . . .
C42 C 0.5513(3) 0.9585(2) 0.8309(2) 0.0418(8) Uani 1 1 d . . . . .
C43 C 0.6674(3) 0.7888(2) 0.8634(2) 0.0391(8) Uani 1 1 d . . . . .
C44 C 0.5856(3) 0.7436(2) 0.8363(2) 0.0410(8) Uani 1 1 d . . . . .
C45 C 0.7667(3) 0.9505(2) 0.8347(2) 0.0424(8) Uani 1 1 d . . . . .
C46 C 0.8628(3) 0.9683(2) 0.7125(3) 0.0460(9) Uani 1 1 d . . . . .
C47 C 0.8330(3) 0.9305(3) 0.6366(3) 0.0475(9) Uani 1 1 d . . . . .
C48 C 0.8615(4) 0.8278(3) 0.6292(3) 0.0733(12) Uani 1 1 d . . . . .
H48 H 0.895281 0.780254 0.675531 0.088 Uiso 1 1 calc R U . . .
C49 C 0.8411(4) 0.7946(4) 0.5550(3) 0.0829(14) Uani 1 1 d . . . . .
H49 H 0.860350 0.724973 0.552053 0.099 Uiso 1 1 calc R U . . .
C50 C 0.7931(4) 0.8625(4) 0.4862(3) 0.0716(12) Uani 1 1 d . . . . .
H50 H 0.781586 0.840310 0.434833 0.086 Uiso 1 1 calc R U . . .
C51 C 0.7620(3) 0.9632(4) 0.4928(3) 0.0677(11) Uani 1 1 d . . . . .
H51 H 0.726478 1.009816 0.447013 0.081 Uiso 1 1 calc R U . . .
C52 C 0.7830(3) 0.9970(3) 0.5673(3) 0.0604(10) Uani 1 1 d . . . . .
H52 H 0.762623 1.066546 0.570098 0.072 Uiso 1 1 calc R U . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
B1 C16 1.701(5) . ?
B1 C15 1.752(5) . ?
B1 B3 1.760(6) . ?
B1 B2 1.773(6) . ?
B1 B4 1.787(6) . ?
B1 H1 1.1000 . ?
C2 C1 1.345(4) . ?
C2 C3 1.412(5) . ?
C2 H2 0.9300 . ?
C1 C13 1.425(4) . ?
C1 H1A 0.9300 . ?
B2 C16 1.700(5) . ?
B2 B5 1.758(7) . ?
B2 B3 1.760(7) . ?
B2 B6 1.768(7) . ?
B2 H2A 1.1000 . ?
C3 C4 1.337(5) . ?
C3 H3 0.9300 . ?
B3 B4 1.778(6) . ?
B3 B7 1.779(7) . ?
B3 B6 1.779(7) . ?
B3 H3A 1.1000 . ?
C4 C14 1.426(4) . ?
C4 H4 0.9300 . ?
B4 C15 1.705(5) . ?
B4 B8 1.761(6) . ?
B4 B7 1.771(6) . ?
B4 H4A 1.1000 . ?
C5 C6 1.345(5) . ?
C5 C11 1.429(5) . ?
C5 H5 0.9300 . ?
B5 C16 1.707(5) . ?
B5 B10 1.772(6) . ?
B5 B9 1.775(5) . ?
B5 B6 1.779(6) . ?
B5 H5A 1.1000 . ?
C6 C7 1.398(5) . ?
C6 H6 0.9300 . ?
B6 B7 1.768(7) . ?
B6 B10 1.778(6) . ?
B6 H6A 1.1000 . ?
C7 C8 1.351(5) . ?
C7 H7 0.9300 . ?
B7 B8 1.766(6) . ?
B7 B10 1.768(7) . ?
B7 H7A 1.1000 . ?
C8 C12 1.435(4) . ?
C8 H8 0.9300 . ?
B8 C15 1.702(5) . ?
B8 B10 1.767(6) . ?
B8 B9 1.790(6) . ?
B8 H8A 1.1000 . ?
C9 C12 1.421(4) . ?
C9 C13 1.427(4) . ?
C9 C15 1.522(4) . ?
B9 C16 1.697(5) . ?
B9 C15 1.752(5) . ?
B9 B10 1.775(5) . ?
B9 H9 1.1000 . ?
C10 C14 1.401(4) . ?
C10 C11 1.407(4) . ?
C10 C40 1.501(4) . ?
B10 H10 1.1000 . ?
C11 C12 1.434(4) . ?
B11 C46 1.704(5) . ?
B11 B14 1.756(6) . ?
B11 C45 1.760(5) . ?
B11 B13 1.762(6) . ?
B11 B12 1.790(6) . ?
B11 H11 1.1000 . ?
B12 C45 1.713(5) . ?
B12 B18 1.771(6) . ?
B12 B13 1.783(6) . ?
B12 B17 1.785(6) . ?
B12 H12 1.1000 . ?
C13 C14 1.438(4) . ?
B13 B14 1.761(6) . ?
B13 B17 1.772(6) . ?
B13 B16 1.777(6) . ?
B13 H13 1.1000 . ?
B14 C46 1.710(5) . ?
B14 B15 1.770(6) . ?
B14 B16 1.777(6) . ?
B14 H14 1.1000 . ?
C15 C16 1.829(4) . ?
B15 C46 1.702(5) . ?
B15 B19 1.777(6) . ?
B15 B16 1.786(6) . ?
B15 B20 1.786(7) . ?
B15 H15 1.1000 . ?
C16 C17 1.499(4) . ?
B16 B17 1.749(7) . ?
B16 B20 1.778(6) . ?
B16 H16 1.1000 . ?
C17 C18 1.367(5) . ?
C17 C22 1.369(5) . ?
B17 B20 1.781(6) . ?
B17 B18 1.783(6) . ?
B17 H17 1.1000 . ?
C18 C19 1.390(5) . ?
C18 H18 0.9300 . ?
B18 C45 1.710(5) . ?
B18 B20 1.771(7) . ?
B18 B19 1.801(6) . ?
B18 H18A 1.1000 . ?
C19 C20 1.333(6) . ?
C19 H19 0.9300 . ?
B19 C46 1.710(5) . ?
B19 C45 1.752(5) . ?
B19 B20 1.774(6) . ?
B19 H19A 1.1000 . ?
C20 C21 1.361(6) . ?
C20 H20 0.9300 . ?
B20 H20A 1.1000 . ?
C21 C22 1.379(6) . ?
C21 H21 0.9300 . ?
C22 H22 0.9300 . ?
C31 C32 1.345(5) . ?
C31 C43 1.431(4) . ?
C31 H31 0.9300 . ?
C32 C33 1.387(5) . ?
C32 H32 0.9300 . ?
C33 C34 1.358(5) . ?
C33 H33 0.9300 . ?
C34 C44 1.426(4) . ?
C34 H34 0.9300 . ?
C35 C36 1.336(5) . ?
C35 C41 1.431(4) . ?
C35 H35 0.9300 . ?
C36 C37 1.405(5) . ?
C36 H36 0.9300 . ?
C37 C38 1.338(5) . ?
C37 H37 0.9300 . ?
C38 C42 1.431(4) . ?
C38 H38 0.9300 . ?
C39 C43 1.423(4) . ?
C39 C42 1.430(4) . ?
C39 C45 1.525(4) . ?
C40 C41 1.396(4) . ?
C40 C44 1.405(4) . ?
C41 C42 1.432(4) . ?
C43 C44 1.433(4) . ?
C45 C46 1.825(5) . ?
C46 C47 1.485(5) . ?
C47 C52 1.363(5) . ?
C47 C48 1.384(5) . ?
C48 C49 1.372(5) . ?
C48 H48 0.9300 . ?
C49 C50 1.354(6) . ?
C49 H49 0.9300 . ?
C50 C51 1.356(6) . ?
C50 H50 0.9300 . ?
C51 C52 1.384(5) . ?
C51 H51 0.9300 . ?
C52 H52 0.9300 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C16 B1 C15 63.9(2) . . ?
C16 B1 B3 106.2(3) . . ?
C15 B1 B3 106.6(3) . . ?
C16 B1 B2 58.5(2) . . ?
C15 B1 B2 110.2(3) . . ?
B3 B1 B2 59.8(2) . . ?
C16 B1 B4 108.4(3) . . ?
C15 B1 B4 57.6(2) . . ?
B3 B1 B4 60.2(2) . . ?
B2 B1 B4 108.5(3) . . ?
C16 B1 H1 121.3 . . ?
C15 B1 H1 120.7 . . ?
B3 B1 H1 123.1 . . ?
B2 B1 H1 121.2 . . ?
B4 B1 H1 122.2 . . ?
C1 C2 C3 120.5(3) . . ?
C1 C2 H2 119.8 . . ?
C3 C2 H2 119.8 . . ?
C2 C1 C13 123.0(3) . . ?
C2 C1 H1A 118.5 . . ?
C13 C1 H1A 118.5 . . ?
C16 B2 B5 59.1(2) . . ?
C16 B2 B3 106.2(3) . . ?
B5 B2 B3 108.8(3) . . ?
C16 B2 B6 106.7(3) . . ?
B5 B2 B6 60.6(3) . . ?
B3 B2 B6 60.6(3) . . ?
C16 B2 B1 58.6(2) . . ?
B5 B2 B1 107.2(3) . . ?
B3 B2 B1 59.7(2) . . ?
B6 B2 B1 107.8(3) . . ?
C16 B2 H2A 123.5 . . ?
B5 B2 H2A 121.5 . . ?
B3 B2 H2A 121.6 . . ?
B6 B2 H2A 121.5 . . ?
B1 B2 H2A 122.4 . . ?
C4 C3 C2 119.3(3) . . ?
C4 C3 H3 120.3 . . ?
C2 C3 H3 120.3 . . ?
B1 B3 B2 60.5(2) . . ?
B1 B3 B4 60.7(2) . . ?
B2 B3 B4 109.5(3) . . ?
B1 B3 B7 107.5(3) . . ?
B2 B3 B7 107.7(3) . . ?
B4 B3 B7 59.7(2) . . ?
B1 B3 B6 107.9(3) . . ?
B2 B3 B6 59.9(3) . . ?
B4 B3 B6 108.3(3) . . ?
B7 B3 B6 59.6(3) . . ?
B1 B3 H3A 121.6 . . ?
B2 B3 H3A 121.1 . . ?
B4 B3 H3A 120.9 . . ?
B7 B3 H3A 122.4 . . ?
B6 B3 H3A 121.9 . . ?
C3 C4 C14 122.1(3) . . ?
C3 C4 H4 118.9 . . ?
C14 C4 H4 118.9 . . ?
C15 B4 B8 58.8(2) . . ?
C15 B4 B7 107.2(3) . . ?
B8 B4 B7 60.0(2) . . ?
C15 B4 B3 107.9(3) . . ?
B8 B4 B3 107.8(3) . . ?
B7 B4 B3 60.2(3) . . ?
C15 B4 B1 60.2(2) . . ?
B8 B4 B1 106.4(3) . . ?
B7 B4 B1 106.6(3) . . ?
B3 B4 B1 59.1(2) . . ?
C15 B4 H4A 122.1 . . ?
B8 B4 H4A 122.5 . . ?
B7 B4 H4A 122.1 . . ?
B3 B4 H4A 121.6 . . ?
B1 B4 H4A 122.8 . . ?
C6 C5 C11 121.8(3) . . ?
C6 C5 H5 119.1 . . ?
C11 C5 H5 119.1 . . ?
C16 B5 B2 58.7(2) . . ?
C16 B5 B10 105.7(3) . . ?
B2 B5 B10 107.6(3) . . ?
C16 B5 B9 58.3(2) . . ?
B2 B5 B9 106.4(3) . . ?
B10 B5 B9 60.1(2) . . ?
C16 B5 B6 105.9(3) . . ?
B2 B5 B6 60.0(3) . . ?
B10 B5 B6 60.1(3) . . ?
B9 B5 B6 107.6(3) . . ?
C16 B5 H5A 123.9 . . ?
B2 B5 H5A 122.3 . . ?
B10 B5 H5A 122.0 . . ?
B9 B5 H5A 122.4 . . ?
B6 B5 H5A 122.0 . . ?
C5 C6 C7 119.3(4) . . ?
C5 C6 H6 120.3 . . ?
C7 C6 H6 120.3 . . ?
B7 B6 B2 107.9(3) . . ?
B7 B6 B10 59.8(3) . . ?
B2 B6 B10 106.9(3) . . ?
B7 B6 B5 108.0(3) . . ?
B2 B6 B5 59.4(3) . . ?
B10 B6 B5 59.8(2) . . ?
B7 B6 B3 60.2(3) . . ?
B2 B6 B3 59.5(3) . . ?
B10 B6 B3 107.1(3) . . ?
B5 B6 B3 107.0(3) . . ?
B7 B6 H6A 121.4 . . ?
B2 B6 H6A 122.3 . . ?
B10 B6 H6A 122.4 . . ?
B5 B6 H6A 122.1 . . ?
B3 B6 H6A 122.3 . . ?
C8 C7 C6 121.2(3) . . ?
C8 C7 H7 119.4 . . ?
C6 C7 H7 119.4 . . ?
B8 B7 B6 108.9(3) . . ?
B8 B7 B10 60.0(2) . . ?
B6 B7 B10 60.4(3) . . ?
B8 B7 B4 59.7(2) . . ?
B6 B7 B4 109.1(3) . . ?
B10 B7 B4 107.9(3) . . ?
B8 B7 B3 107.6(3) . . ?
B6 B7 B3 60.2(3) . . ?
B10 B7 B3 107.6(3) . . ?
B4 B7 B3 60.1(2) . . ?
B8 B7 H7A 121.8 . . ?
B6 B7 H7A 120.7 . . ?
B10 B7 H7A 121.9 . . ?
B4 B7 H7A 121.5 . . ?
B3 B7 H7A 122.1 . . ?
C7 C8 C12 122.5(3) . . ?
C7 C8 H8 118.7 . . ?
C12 C8 H8 118.7 . . ?
C15 B8 B4 59.0(2) . . ?
C15 B8 B7 107.5(3) . . ?
B4 B8 B7 60.3(2) . . ?
C15 B8 B10 108.6(3) . . ?
B4 B8 B10 108.3(3) . . ?
B7 B8 B10 60.0(2) . . ?
C15 B8 B9 60.2(2) . . ?
B4 B8 B9 106.9(3) . . ?
B7 B8 B9 107.2(3) . . ?
B10 B8 B9 59.9(2) . . ?
C15 B8 H8A 121.8 . . ?
B4 B8 H8A 122.2 . . ?
B7 B8 H8A 122.0 . . ?
B10 B8 H8A 121.2 . . ?
B9 B8 H8A 122.4 . . ?
C12 C9 C13 118.4(3) . . ?
C12 C9 C15 121.2(3) . . ?
C13 C9 C15 120.3(3) . . ?
C16 B9 C15 64.0(2) . . ?
C16 B9 B5 58.8(2) . . ?
C15 B9 B5 110.6(3) . . ?
C16 B9 B10 106.0(3) . . ?
C15 B9 B10 106.0(3) . . ?
B5 B9 B10 59.9(2) . . ?
C16 B9 B8 108.1(3) . . ?
C15 B9 B8 57.4(2) . . ?
B5 B9 B8 108.3(3) . . ?
B10 B9 B8 59.4(2) . . ?
C16 B9 H9 121.3 . . ?
C15 B9 H9 120.8 . . ?
B5 B9 H9 120.9 . . ?
B10 B9 H9 123.6 . . ?
B8 B9 H9 122.6 . . ?
C14 C10 C11 119.4(3) . . ?
C14 C10 C40 120.1(3) . . ?
C11 C10 C40 120.2(3) . . ?
B8 B10 B7 60.0(2) . . ?
B8 B10 B5 109.4(3) . . ?
B7 B10 B5 108.3(3) . . ?
B8 B10 B9 60.7(2) . . ?
B7 B10 B9 107.7(3) . . ?
B5 B10 B9 60.0(2) . . ?
B8 B10 B6 108.4(3) . . ?
B7 B10 B6 59.8(3) . . ?
B5 B10 B6 60.1(3) . . ?
B9 B10 B6 107.6(3) . . ?
B8 B10 H10 120.8 . . ?
B7 B10 H10 122.0 . . ?
B5 B10 H10 121.1 . . ?
B9 B10 H10 121.9 . . ?
B6 B10 H10 121.9 . . ?
C10 C11 C5 120.2(3) . . ?
C10 C11 C12 120.3(3) . . ?
C5 C11 C12 119.5(3) . . ?
C46 B11 B14 59.2(2) . . ?
C46 B11 C45 63.5(2) . . ?
B14 B11 C45 110.5(3) . . ?
C46 B11 B13 106.9(3) . . ?
B14 B11 B13 60.1(2) . . ?
C45 B11 B13 106.7(3) . . ?
C46 B11 B12 108.7(3) . . ?
B14 B11 B12 109.1(3) . . ?
C45 B11 B12 57.7(2) . . ?
B13 B11 B12 60.2(2) . . ?
C46 B11 H11 121.0 . . ?
B14 B11 H11 120.7 . . ?
C45 B11 H11 121.0 . . ?
B13 B11 H11 122.9 . . ?
B12 B11 H11 122.0 . . ?
C9 C12 C11 119.6(3) . . ?
C9 C12 C8 124.8(3) . . ?
C11 C12 C8 115.5(3) . . ?
C45 B12 B18 58.8(2) . . ?
C45 B12 B13 107.8(3) . . ?
B18 B12 B13 107.8(3) . . ?
C45 B12 B17 106.9(3) . . ?
B18 B12 B17 60.2(2) . . ?
B13 B12 B17 59.6(2) . . ?
C45 B12 B11 60.3(2) . . ?
B18 B12 B11 106.5(3) . . ?
B13 B12 B11 59.1(2) . . ?
B17 B12 B11 106.0(3) . . ?
C45 B12 H12 122.0 . . ?
B18 B12 H12 122.3 . . ?
B13 B12 H12 121.8 . . ?
B17 B12 H12 122.6 . . ?
B11 B12 H12 122.9 . . ?
C1 C13 C9 125.2(3) . . ?
C1 C13 C14 115.7(3) . . ?
C9 C13 C14 118.9(3) . . ?
B14 B13 B11 59.8(2) . . ?
B14 B13 B17 108.0(3) . . ?
B11 B13 B17 107.8(3) . . ?
B14 B13 B16 60.3(3) . . ?
B11 B13 B16 107.2(3) . . ?
B17 B13 B16 59.1(3) . . ?
B14 B13 B12 109.2(3) . . ?
B11 B13 B12 60.7(2) . . ?
B17 B13 B12 60.3(2) . . ?
B16 B13 B12 107.9(3) . . ?
B14 B13 H13 121.2 . . ?
B11 B13 H13 122.0 . . ?
B17 B13 H13 122.1 . . ?
B16 B13 H13 122.4 . . ?
B12 B13 H13 120.9 . . ?
C10 C14 C4 120.4(3) . . ?
C10 C14 C13 120.6(3) . . ?
C4 C14 C13 118.9(3) . . ?
C46 B14 B11 58.9(2) . . ?
C46 B14 B13 106.7(3) . . ?
B11 B14 B13 60.1(2) . . ?
C46 B14 B15 58.5(2) . . ?
B11 B14 B15 106.9(3) . . ?
B13 B14 B15 108.8(3) . . ?
C46 B14 B16 105.9(3) . . ?
B11 B14 B16 107.5(3) . . ?
B13 B14 B16 60.3(3) . . ?
B15 B14 B16 60.5(2) . . ?
C46 B14 H14 123.7 . . ?
B11 B14 H14 122.3 . . ?
B13 B14 H14 121.3 . . ?
B15 B14 H14 121.8 . . ?
B16 B14 H14 122.0 . . ?
C9 C15 B8 127.1(3) . . ?
C9 C15 B4 126.4(3) . . ?
B8 C15 B4 62.3(2) . . ?
C9 C15 B1 118.2(3) . . ?
B8 C15 B1 110.7(3) . . ?
B4 C15 B1 62.3(2) . . ?
C9 C15 B9 118.6(3) . . ?
B8 C15 B9 62.4(2) . . ?
B4 C15 B9 111.1(3) . . ?
B1 C15 B9 105.2(2) . . ?
C9 C15 C16 116.6(2) . . ?
B8 C15 C16 106.1(2) . . ?
B4 C15 C16 106.4(2) . . ?
B1 C15 C16 56.69(19) . . ?
B9 C15 C16 56.53(18) . . ?
C46 B15 B14 59.0(2) . . ?
C46 B15 B19 58.8(2) . . ?
B14 B15 B19 106.8(3) . . ?
C46 B15 B16 105.9(3) . . ?
B14 B15 B16 60.0(2) . . ?
B19 B15 B16 107.0(3) . . ?
C46 B15 B20 105.9(3) . . ?
B14 B15 B20 107.5(3) . . ?
B19 B15 B20 59.7(2) . . ?
B16 B15 B20 59.7(3) . . ?
C46 B15 H15 123.5 . . ?
B14 B15 H15 122.0 . . ?
B19 B15 H15 122.4 . . ?
B16 B15 H15 122.4 . . ?
B20 B15 H15 122.3 . . ?
C17 C16 B9 119.5(3) . . ?
C17 C16 B2 121.2(3) . . ?
B9 C16 B2 112.8(3) . . ?
C17 C16 B1 117.2(3) . . ?
B9 C16 B1 110.0(3) . . ?
B2 C16 B1 62.8(2) . . ?
C17 C16 B5 122.5(3) . . ?
B9 C16 B5 62.9(2) . . ?
B2 C16 B5 62.1(2) . . ?
B1 C16 B5 113.0(3) . . ?
C17 C16 C15 118.4(2) . . ?
B9 C16 C15 59.45(19) . . ?
B2 C16 C15 110.0(3) . . ?
B1 C16 C15 59.37(19) . . ?
B5 C16 C15 110.1(2) . . ?
B17 B16 B13 60.3(3) . . ?
B17 B16 B14 108.3(3) . . ?
B13 B16 B14 59.4(2) . . ?
B17 B16 B20 60.6(3) . . ?
B13 B16 B20 108.0(3) . . ?
B14 B16 B20 107.6(3) . . ?
B17 B16 B15 109.0(3) . . ?
B13 B16 B15 107.4(3) . . ?
B14 B16 B15 59.6(2) . . ?
B20 B16 B15 60.2(3) . . ?
B17 B16 H16 120.8 . . ?
B13 B16 H16 122.1 . . ?
B14 B16 H16 122.2 . . ?
B20 B16 H16 121.6 . . ?
B15 B16 H16 121.7 . . ?
C18 C17 C22 117.3(3) . . ?
C18 C17 C16 121.7(3) . . ?
C22 C17 C16 120.6(3) . . ?
B16 B17 B13 60.6(3) . . ?
B16 B17 B20 60.5(3) . . ?
B13 B17 B20 108.0(3) . . ?
B16 B17 B18 108.7(3) . . ?
B13 B17 B18 107.7(3) . . ?
B20 B17 B18 59.6(2) . . ?
B16 B17 B12 109.0(3) . . ?
B13 B17 B12 60.2(2) . . ?
B20 B17 B12 107.4(3) . . ?
B18 B17 B12 59.5(2) . . ?
B16 B17 H17 120.7 . . ?
B13 B17 H17 121.6 . . ?
B20 B17 H17 122.0 . . ?
B18 B17 H17 122.0 . . ?
B12 B17 H17 121.8 . . ?
C17 C18 C19 121.0(4) . . ?
C17 C18 H18 119.5 . . ?
C19 C18 H18 119.5 . . ?
C45 B18 B12 58.9(2) . . ?
C45 B18 B20 107.9(3) . . ?
B12 B18 B20 108.4(3) . . ?
C45 B18 B17 107.1(3) . . ?
B12 B18 B17 60.3(2) . . ?
B20 B18 B17 60.1(2) . . ?
C45 B18 B19 59.8(2) . . ?
B12 B18 B19 106.7(3) . . ?
B20 B18 B19 59.5(2) . . ?
B17 B18 B19 106.8(3) . . ?
C45 B18 H18A 122.3 . . ?
B12 B18 H18A 122.0 . . ?
B20 B18 H18A 121.4 . . ?
B17 B18 H18A 122.1 . . ?
B19 B18 H18A 122.7 . . ?
C20 C19 C18 120.7(4) . . ?
C20 C19 H19 119.7 . . ?
C18 C19 H19 119.7 . . ?
C46 B19 C45 63.6(2) . . ?
C46 B19 B20 106.1(3) . . ?
C45 B19 B20 105.9(3) . . ?
C46 B19 B15 58.4(2) . . ?
C45 B19 B15 109.9(3) . . ?
B20 B19 B15 60.4(3) . . ?
C46 B19 B18 108.0(3) . . ?
C45 B19 B18 57.5(2) . . ?
B20 B19 B18 59.4(2) . . ?
B15 B19 B18 108.4(3) . . ?
C46 B19 H19A 121.5 . . ?
C45 B19 H19A 121.1 . . ?
B20 B19 H19A 123.3 . . ?
B15 B19 H19A 121.0 . . ?
B18 B19 H19A 122.5 . . ?
C19 C20 C21 119.4(4) . . ?
C19 C20 H20 120.3 . . ?
C21 C20 H20 120.3 . . ?
B18 B20 B19 61.1(2) . . ?
B18 B20 B16 107.9(3) . . ?
B19 B20 B16 107.5(3) . . ?
B18 B20 B17 60.3(2) . . ?
B19 B20 B17 108.1(3) . . ?
B16 B20 B17 58.9(3) . . ?
B18 B20 B15 109.4(3) . . ?
B19 B20 B15 59.9(2) . . ?
B16 B20 B15 60.1(3) . . ?
B17 B20 B15 107.6(3) . . ?
B18 B20 H20A 120.7 . . ?
B19 B20 H20A 121.6 . . ?
B16 B20 H20A 122.4 . . ?
B17 B20 H20A 122.2 . . ?
B15 B20 H20A 121.3 . . ?
C20 C21 C22 120.3(4) . . ?
C20 C21 H21 119.8 . . ?
C22 C21 H21 119.8 . . ?
C17 C22 C21 121.2(4) . . ?
C17 C22 H22 119.4 . . ?
C21 C22 H22 119.4 . . ?
C32 C31 C43 122.4(3) . . ?
C32 C31 H31 118.8 . . ?
C43 C31 H31 118.8 . . ?
C31 C32 C33 120.9(3) . . ?
C31 C32 H32 119.6 . . ?
C33 C32 H32 119.6 . . ?
C34 C33 C32 120.1(3) . . ?
C34 C33 H33 120.0 . . ?
C32 C33 H33 120.0 . . ?
C33 C34 C44 121.0(3) . . ?
C33 C34 H34 119.5 . . ?
C44 C34 H34 119.5 . . ?
C36 C35 C41 121.8(3) . . ?
C36 C35 H35 119.1 . . ?
C41 C35 H35 119.1 . . ?
C35 C36 C37 119.5(3) . . ?
C35 C36 H36 120.3 . . ?
C37 C36 H36 120.3 . . ?
C38 C37 C36 121.1(3) . . ?
C38 C37 H37 119.5 . . ?
C36 C37 H37 119.5 . . ?
C37 C38 C42 122.5(3) . . ?
C37 C38 H38 118.7 . . ?
C42 C38 H38 118.7 . . ?
C43 C39 C42 117.9(3) . . ?
C43 C39 C45 120.6(3) . . ?
C42 C39 C45 121.1(3) . . ?
C41 C40 C44 119.4(3) . . ?
C41 C40 C10 120.1(3) . . ?
C44 C40 C10 120.4(3) . . ?
C40 C41 C35 120.2(3) . . ?
C40 C41 C42 120.9(3) . . ?
C35 C41 C42 119.0(3) . . ?
C39 C42 C38 124.6(3) . . ?
C39 C42 C41 119.4(3) . . ?
C38 C42 C41 115.9(3) . . ?
C39 C43 C31 124.6(3) . . ?
C39 C43 C44 119.5(3) . . ?
C31 C43 C44 115.9(3) . . ?
C40 C44 C34 120.6(3) . . ?
C40 C44 C43 120.3(3) . . ?
C34 C44 C43 119.0(3) . . ?
C39 C45 B18 127.1(3) . . ?
C39 C45 B12 128.8(3) . . ?
B18 C45 B12 62.3(2) . . ?
C39 C45 B19 115.9(3) . . ?
B18 C45 B19 62.7(2) . . ?
B12 C45 B19 111.6(3) . . ?
C39 C45 B11 119.1(3) . . ?
B18 C45 B11 110.6(3) . . ?
B12 C45 B11 62.0(2) . . ?
B19 C45 B11 105.5(3) . . ?
C39 C45 C46 114.3(2) . . ?
B18 C45 C46 106.9(3) . . ?
B12 C45 C46 106.7(2) . . ?
B19 C45 C46 57.1(2) . . ?
B11 C45 C46 56.74(19) . . ?
C47 C46 B15 121.0(3) . . ?
C47 C46 B11 119.2(3) . . ?
B15 C46 B11 112.5(3) . . ?
C47 C46 B19 118.4(3) . . ?
B15 C46 B19 62.8(2) . . ?
B11 C46 B19 110.0(3) . . ?
C47 C46 B14 121.7(3) . . ?
B15 C46 B14 62.5(2) . . ?
B11 C46 B14 61.9(2) . . ?
B19 C46 B14 112.8(3) . . ?
C47 C46 C45 119.2(3) . . ?
B15 C46 C45 110.0(3) . . ?
B11 C46 C45 59.7(2) . . ?
B19 C46 C45 59.3(2) . . ?
B14 C46 C45 109.5(3) . . ?
C52 C47 C48 117.0(3) . . ?
C52 C47 C46 121.3(3) . . ?
C48 C47 C46 121.6(3) . . ?
C49 C48 C47 121.5(4) . . ?
C49 C48 H48 119.3 . . ?
C47 C48 H48 119.3 . . ?
C50 C49 C48 120.4(4) . . ?
C50 C49 H49 119.8 . . ?
C48 C49 H49 119.8 . . ?
C49 C50 C51 119.4(4) . . ?
C49 C50 H50 120.3 . . ?
C51 C50 H50 120.3 . . ?
C50 C51 C52 120.2(4) . . ?
C50 C51 H51 119.9 . . ?
C52 C51 H51 119.9 . . ?
C47 C52 C51 121.5(4) . . ?
C47 C52 H52 119.3 . . ?
C51 C52 H52 119.3 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C3 C2 C1 C13 -1.2(5) . . . . ?
C15 B1 B2 C16 -39.3(3) . . . . ?
B3 B1 B2 C16 -137.3(3) . . . . ?
B4 B1 B2 C16 -100.7(3) . . . . ?
C16 B1 B2 B5 35.2(3) . . . . ?
C15 B1 B2 B5 -4.1(4) . . . . ?
B3 B1 B2 B5 -102.1(3) . . . . ?
B4 B1 B2 B5 -65.5(4) . . . . ?
C16 B1 B2 B3 137.3(3) . . . . ?
C15 B1 B2 B3 98.0(3) . . . . ?
B4 B1 B2 B3 36.6(3) . . . . ?
C16 B1 B2 B6 99.0(3) . . . . ?
C15 B1 B2 B6 59.7(4) . . . . ?
B3 B1 B2 B6 -38.3(3) . . . . ?
B4 B1 B2 B6 -1.7(4) . . . . ?
C1 C2 C3 C4 4.4(5) . . . . ?
C16 B1 B3 B2 -37.0(3) . . . . ?
C15 B1 B3 B2 -104.0(3) . . . . ?
B4 B1 B3 B2 -139.3(3) . . . . ?
C16 B1 B3 B4 102.3(3) . . . . ?
C15 B1 B3 B4 35.3(3) . . . . ?
B2 B1 B3 B4 139.3(3) . . . . ?
C16 B1 B3 B7 63.9(4) . . . . ?
C15 B1 B3 B7 -3.2(4) . . . . ?
B2 B1 B3 B7 100.9(4) . . . . ?
B4 B1 B3 B7 -38.4(3) . . . . ?
C16 B1 B3 B6 1.0(4) . . . . ?
C15 B1 B3 B6 -66.0(4) . . . . ?
B2 B1 B3 B6 38.0(3) . . . . ?
B4 B1 B3 B6 -101.3(3) . . . . ?
C16 B2 B3 B1 37.1(3) . . . . ?
B5 B2 B3 B1 99.4(3) . . . . ?
B6 B2 B3 B1 137.4(3) . . . . ?
C16 B2 B3 B4 0.0(4) . . . . ?
B5 B2 B3 B4 62.3(4) . . . . ?
B6 B2 B3 B4 100.3(4) . . . . ?
B1 B2 B3 B4 -37.1(3) . . . . ?
C16 B2 B3 B7 -63.4(4) . . . . ?
B5 B2 B3 B7 -1.1(4) . . . . ?
B6 B2 B3 B7 36.9(3) . . . . ?
B1 B2 B3 B7 -100.4(3) . . . . ?
C16 B2 B3 B6 -100.3(3) . . . . ?
B5 B2 B3 B6 -38.0(3) . . . . ?
B1 B2 B3 B6 -137.4(3) . . . . ?
C2 C3 C4 C14 -1.2(5) . . . . ?
B1 B3 B4 C15 -36.7(3) . . . . ?
B2 B3 B4 C15 0.3(4) . . . . ?
B7 B3 B4 C15 99.9(3) . . . . ?
B6 B3 B4 C15 64.0(4) . . . . ?
B1 B3 B4 B8 -98.8(3) . . . . ?
B2 B3 B4 B8 -61.8(4) . . . . ?
B7 B3 B4 B8 37.9(3) . . . . ?
B6 B3 B4 B8 2.0(4) . . . . ?
B1 B3 B4 B7 -136.6(3) . . . . ?
B2 B3 B4 B7 -99.6(4) . . . . ?
B6 B3 B4 B7 -35.9(3) . . . . ?
B2 B3 B4 B1 37.0(3) . . . . ?
B7 B3 B4 B1 136.6(3) . . . . ?
B6 B3 B4 B1 100.7(3) . . . . ?
C16 B1 B4 C15 40.5(2) . . . . ?
B3 B1 B4 C15 139.0(3) . . . . ?
B2 B1 B4 C15 102.6(3) . . . . ?
C16 B1 B4 B8 2.8(4) . . . . ?
C15 B1 B4 B8 -37.7(2) . . . . ?
B3 B1 B4 B8 101.3(3) . . . . ?
B2 B1 B4 B8 64.9(3) . . . . ?
C16 B1 B4 B7 -60.0(3) . . . . ?
C15 B1 B4 B7 -100.6(3) . . . . ?
B3 B1 B4 B7 38.5(3) . . . . ?
B2 B1 B4 B7 2.0(4) . . . . ?
C16 B1 B4 B3 -98.5(3) . . . . ?
C15 B1 B4 B3 -139.0(3) . . . . ?
B2 B1 B4 B3 -36.4(3) . . . . ?
B3 B2 B5 C16 -98.1(3) . . . . ?
B6 B2 B5 C16 -136.1(3) . . . . ?
B1 B2 B5 C16 -35.0(3) . . . . ?
C16 B2 B5 B10 98.0(3) . . . . ?
B3 B2 B5 B10 -0.1(4) . . . . ?
B6 B2 B5 B10 -38.1(3) . . . . ?
B1 B2 B5 B10 63.1(4) . . . . ?
C16 B2 B5 B9 34.9(3) . . . . ?
B3 B2 B5 B9 -63.2(4) . . . . ?
B6 B2 B5 B9 -101.2(3) . . . . ?
B1 B2 B5 B9 0.0(4) . . . . ?
C16 B2 B5 B6 136.1(3) . . . . ?
B3 B2 B5 B6 38.0(3) . . . . ?
B1 B2 B5 B6 101.1(3) . . . . ?
C11 C5 C6 C7 -2.0(6) . . . . ?
C16 B2 B6 B7 62.3(4) . . . . ?
B5 B2 B6 B7 100.7(3) . . . . ?
B3 B2 B6 B7 -37.2(3) . . . . ?
B1 B2 B6 B7 0.7(4) . . . . ?
C16 B2 B6 B10 -0.7(4) . . . . ?
B5 B2 B6 B10 37.7(3) . . . . ?
B3 B2 B6 B10 -100.2(3) . . . . ?
B1 B2 B6 B10 -62.3(4) . . . . ?
C16 B2 B6 B5 -38.4(3) . . . . ?
B3 B2 B6 B5 -138.0(3) . . . . ?
B1 B2 B6 B5 -100.1(3) . . . . ?
C16 B2 B6 B3 99.6(3) . . . . ?
B5 B2 B6 B3 138.0(3) . . . . ?
B1 B2 B6 B3 37.9(3) . . . . ?
C16 B5 B6 B7 -62.5(4) . . . . ?
B2 B5 B6 B7 -100.6(3) . . . . ?
B10 B5 B6 B7 36.8(3) . . . . ?
B9 B5 B6 B7 -1.4(4) . . . . ?
C16 B5 B6 B2 38.0(3) . . . . ?
B10 B5 B6 B2 137.3(3) . . . . ?
B9 B5 B6 B2 99.2(3) . . . . ?
C16 B5 B6 B10 -99.3(3) . . . . ?
B2 B5 B6 B10 -137.3(3) . . . . ?
B9 B5 B6 B10 -38.2(3) . . . . ?
C16 B5 B6 B3 0.9(4) . . . . ?
B2 B5 B6 B3 -37.1(3) . . . . ?
B10 B5 B6 B3 100.2(3) . . . . ?
B9 B5 B6 B3 62.1(4) . . . . ?
B1 B3 B6 B7 100.1(3) . . . . ?
B2 B3 B6 B7 138.4(3) . . . . ?
B4 B3 B6 B7 35.9(3) . . . . ?
B1 B3 B6 B2 -38.3(3) . . . . ?
B4 B3 B6 B2 -102.5(3) . . . . ?
B7 B3 B6 B2 -138.4(3) . . . . ?
B1 B3 B6 B10 61.6(4) . . . . ?
B2 B3 B6 B10 99.9(3) . . . . ?
B4 B3 B6 B10 -2.6(4) . . . . ?
B7 B3 B6 B10 -38.5(3) . . . . ?
B1 B3 B6 B5 -1.2(4) . . . . ?
B2 B3 B6 B5 37.1(3) . . . . ?
B4 B3 B6 B5 -65.4(4) . . . . ?
B7 B3 B6 B5 -101.3(3) . . . . ?
C5 C6 C7 C8 -1.0(6) . . . . ?
B2 B6 B7 B8 -62.9(4) . . . . ?
B10 B6 B7 B8 36.6(3) . . . . ?
B5 B6 B7 B8 -0.1(4) . . . . ?
B3 B6 B7 B8 -99.9(3) . . . . ?
B2 B6 B7 B10 -99.6(3) . . . . ?
B5 B6 B7 B10 -36.8(3) . . . . ?
B3 B6 B7 B10 -136.5(3) . . . . ?
B2 B6 B7 B4 0.6(4) . . . . ?
B10 B6 B7 B4 100.2(3) . . . . ?
B5 B6 B7 B4 63.4(4) . . . . ?
B3 B6 B7 B4 -36.3(3) . . . . ?
B2 B6 B7 B3 36.9(3) . . . . ?
B10 B6 B7 B3 136.5(3) . . . . ?
B5 B6 B7 B3 99.7(3) . . . . ?
C15 B4 B7 B8 36.4(3) . . . . ?
B3 B4 B7 B8 137.6(3) . . . . ?
B1 B4 B7 B8 99.6(3) . . . . ?
C15 B4 B7 B6 -64.8(4) . . . . ?
B8 B4 B7 B6 -101.2(3) . . . . ?
B3 B4 B7 B6 36.4(3) . . . . ?
B1 B4 B7 B6 -1.6(4) . . . . ?
C15 B4 B7 B10 -0.7(4) . . . . ?
B8 B4 B7 B10 -37.2(3) . . . . ?
B3 B4 B7 B10 100.4(3) . . . . ?
B1 B4 B7 B10 62.4(4) . . . . ?
C15 B4 B7 B3 -101.1(3) . . . . ?
B8 B4 B7 B3 -137.6(3) . . . . ?
B1 B4 B7 B3 -38.0(3) . . . . ?
B1 B3 B7 B8 1.2(4) . . . . ?
B2 B3 B7 B8 65.1(4) . . . . ?
B4 B3 B7 B8 -37.7(3) . . . . ?
B6 B3 B7 B8 102.1(3) . . . . ?
B1 B3 B7 B6 -100.9(3) . . . . ?
B2 B3 B7 B6 -37.1(3) . . . . ?
B4 B3 B7 B6 -139.8(3) . . . . ?
B1 B3 B7 B10 -62.0(4) . . . . ?
B2 B3 B7 B10 1.8(4) . . . . ?
B4 B3 B7 B10 -100.9(3) . . . . ?
B6 B3 B7 B10 38.9(3) . . . . ?
B1 B3 B7 B4 38.9(3) . . . . ?
B2 B3 B7 B4 102.7(3) . . . . ?
B6 B3 B7 B4 139.8(3) . . . . ?
C6 C7 C8 C12 0.8(5) . . . . ?
B7 B4 B8 C15 138.4(3) . . . . ?
B3 B4 B8 C15 100.5(3) . . . . ?
B1 B4 B8 C15 38.3(2) . . . . ?
C15 B4 B8 B7 -138.4(3) . . . . ?
B3 B4 B8 B7 -37.9(3) . . . . ?
B1 B4 B8 B7 -100.1(3) . . . . ?
C15 B4 B8 B10 -101.1(3) . . . . ?
B7 B4 B8 B10 37.3(3) . . . . ?
B3 B4 B8 B10 -0.6(4) . . . . ?
B1 B4 B8 B10 -62.7(3) . . . . ?
C15 B4 B8 B9 -37.9(2) . . . . ?
B7 B4 B8 B9 100.5(3) . . . . ?
B3 B4 B8 B9 62.5(3) . . . . ?
B1 B4 B8 B9 0.4(4) . . . . ?
B6 B7 B8 C15 65.0(4) . . . . ?
B10 B7 B8 C15 101.8(3) . . . . ?
B4 B7 B8 C15 -36.6(3) . . . . ?
B3 B7 B8 C15 1.2(4) . . . . ?
B6 B7 B8 B4 101.6(3) . . . . ?
B10 B7 B8 B4 138.4(3) . . . . ?
B3 B7 B8 B4 37.8(3) . . . . ?
B6 B7 B8 B10 -36.8(3) . . . . ?
B4 B7 B8 B10 -138.4(3) . . . . ?
B3 B7 B8 B10 -100.5(3) . . . . ?
B6 B7 B8 B9 1.6(4) . . . . ?
B10 B7 B8 B9 38.4(3) . . . . ?
B4 B7 B8 B9 -100.0(3) . . . . ?
B3 B7 B8 B9 -62.1(4) . . . . ?
B2 B5 B9 C16 -35.1(3) . . . . ?
B10 B5 B9 C16 -136.3(3) . . . . ?
B6 B5 B9 C16 -98.1(3) . . . . ?
C16 B5 B9 C15 39.3(2) . . . . ?
B2 B5 B9 C15 4.2(4) . . . . ?
B10 B5 B9 C15 -97.0(3) . . . . ?
B6 B5 B9 C15 -58.8(4) . . . . ?
C16 B5 B9 B10 136.3(3) . . . . ?
B2 B5 B9 B10 101.2(3) . . . . ?
B6 B5 B9 B10 38.2(3) . . . . ?
C16 B5 B9 B8 100.5(3) . . . . ?
B2 B5 B9 B8 65.4(4) . . . . ?
B10 B5 B9 B8 -35.8(3) . . . . ?
B6 B5 B9 B8 2.4(4) . . . . ?
C15 B8 B9 C16 -40.9(2) . . . . ?
B4 B8 B9 C16 -3.5(3) . . . . ?
B7 B8 B9 C16 59.8(3) . . . . ?
B10 B8 B9 C16 98.3(3) . . . . ?
B4 B8 B9 C15 37.4(2) . . . . ?
B7 B8 B9 C15 100.7(3) . . . . ?
B10 B8 B9 C15 139.2(3) . . . . ?
C15 B8 B9 B5 -103.2(3) . . . . ?
B4 B8 B9 B5 -65.8(3) . . . . ?
B7 B8 B9 B5 -2.5(4) . . . . ?
B10 B8 B9 B5 36.0(3) . . . . ?
C15 B8 B9 B10 -139.2(3) . . . . ?
B4 B8 B9 B10 -101.8(3) . . . . ?
B7 B8 B9 B10 -38.5(3) . . . . ?
C15 B8 B10 B7 -99.9(3) . . . . ?
B4 B8 B10 B7 -37.4(3) . . . . ?
B9 B8 B10 B7 -136.7(3) . . . . ?
C15 B8 B10 B5 0.4(4) . . . . ?
B4 B8 B10 B5 62.9(4) . . . . ?
B7 B8 B10 B5 100.4(4) . . . . ?
B9 B8 B10 B5 -36.3(3) . . . . ?
C15 B8 B10 B9 36.8(3) . . . . ?
B4 B8 B10 B9 99.3(3) . . . . ?
B7 B8 B10 B9 136.7(3) . . . . ?
C15 B8 B10 B6 -63.5(4) . . . . ?
B4 B8 B10 B6 -1.0(4) . . . . ?
B7 B8 B10 B6 36.4(3) . . . . ?
B9 B8 B10 B6 -100.3(3) . . . . ?
B6 B7 B10 B8 139.3(3) . . . . ?
B4 B7 B10 B8 37.1(3) . . . . ?
B3 B7 B10 B8 100.5(3) . . . . ?
B8 B7 B10 B5 -102.4(3) . . . . ?
B6 B7 B10 B5 37.0(3) . . . . ?
B4 B7 B10 B5 -65.3(4) . . . . ?
B3 B7 B10 B5 -1.8(4) . . . . ?
B8 B7 B10 B9 -38.9(3) . . . . ?
B6 B7 B10 B9 100.4(3) . . . . ?
B4 B7 B10 B9 -1.8(4) . . . . ?
B3 B7 B10 B9 61.6(4) . . . . ?
B8 B7 B10 B6 -139.3(3) . . . . ?
B4 B7 B10 B6 -102.3(3) . . . . ?
B3 B7 B10 B6 -38.8(3) . . . . ?
C16 B5 B10 B8 -1.0(4) . . . . ?
B2 B5 B10 B8 -62.6(4) . . . . ?
B9 B5 B10 B8 36.6(3) . . . . ?
B6 B5 B10 B8 -100.6(3) . . . . ?
C16 B5 B10 B7 62.7(3) . . . . ?
B2 B5 B10 B7 1.2(4) . . . . ?
B9 B5 B10 B7 100.4(3) . . . . ?
B6 B5 B10 B7 -36.8(3) . . . . ?
C16 B5 B10 B9 -37.6(3) . . . . ?
B2 B5 B10 B9 -99.2(3) . . . . ?
B6 B5 B10 B9 -137.2(3) . . . . ?
C16 B5 B10 B6 99.6(3) . . . . ?
B2 B5 B10 B6 38.0(3) . . . . ?
B9 B5 B10 B6 137.2(3) . . . . ?
C16 B9 B10 B8 -101.9(3) . . . . ?
C15 B9 B10 B8 -35.0(3) . . . . ?
B5 B9 B10 B8 -139.8(3) . . . . ?
C16 B9 B10 B7 -63.3(3) . . . . ?
C15 B9 B10 B7 3.6(4) . . . . ?
B5 B9 B10 B7 -101.3(3) . . . . ?
B8 B9 B10 B7 38.6(3) . . . . ?
C16 B9 B10 B5 38.0(3) . . . . ?
C15 B9 B10 B5 104.9(3) . . . . ?
B8 B9 B10 B5 139.8(3) . . . . ?
C16 B9 B10 B6 -0.2(4) . . . . ?
C15 B9 B10 B6 66.7(3) . . . . ?
B5 B9 B10 B6 -38.2(3) . . . . ?
B8 B9 B10 B6 101.6(3) . . . . ?
B7 B6 B10 B8 -36.5(3) . . . . ?
B2 B6 B10 B8 64.7(4) . . . . ?
B5 B6 B10 B8 102.3(3) . . . . ?
B3 B6 B10 B8 2.2(4) . . . . ?
B2 B6 B10 B7 101.2(3) . . . . ?
B5 B6 B10 B7 138.8(3) . . . . ?
B3 B6 B10 B7 38.7(3) . . . . ?
B7 B6 B10 B5 -138.8(3) . . . . ?
B2 B6 B10 B5 -37.6(3) . . . . ?
B3 B6 B10 B5 -100.1(3) . . . . ?
B7 B6 B10 B9 -100.6(3) . . . . ?
B2 B6 B10 B9 0.6(4) . . . . ?
B5 B6 B10 B9 38.2(3) . . . . ?
B3 B6 B10 B9 -61.9(4) . . . . ?
C14 C10 C11 C5 169.5(3) . . . . ?
C40 C10 C11 C5 -4.4(4) . . . . ?
C14 C10 C11 C12 -9.3(4) . . . . ?
C40 C10 C11 C12 176.8(3) . . . . ?
C6 C5 C11 C10 -173.7(3) . . . . ?
C6 C5 C11 C12 5.1(5) . . . . ?
C13 C9 C12 C11 15.9(4) . . . . ?
C15 C9 C12 C11 -160.7(3) . . . . ?
C13 C9 C12 C8 -160.0(3) . . . . ?
C15 C9 C12 C8 23.4(4) . . . . ?
C10 C11 C12 C9 -2.4(4) . . . . ?
C5 C11 C12 C9 178.8(3) . . . . ?
C10 C11 C12 C8 173.8(3) . . . . ?
C5 C11 C12 C8 -5.0(4) . . . . ?
C7 C8 C12 C9 178.2(3) . . . . ?
C7 C8 C12 C11 2.2(5) . . . . ?
C46 B11 B12 C45 39.6(2) . . . . ?
B14 B11 B12 C45 102.6(3) . . . . ?
B13 B11 B12 C45 138.8(3) . . . . ?
C46 B11 B12 B18 2.0(4) . . . . ?
B14 B11 B12 B18 65.0(3) . . . . ?
C45 B11 B12 B18 -37.6(2) . . . . ?
B13 B11 B12 B18 101.2(3) . . . . ?
C46 B11 B12 B13 -99.2(3) . . . . ?
B14 B11 B12 B13 -36.2(3) . . . . ?
C45 B11 B12 B13 -138.8(3) . . . . ?
C46 B11 B12 B17 -61.0(3) . . . . ?
B14 B11 B12 B17 2.0(3) . . . . ?
C45 B11 B12 B17 -100.6(3) . . . . ?
B13 B11 B12 B17 38.2(3) . . . . ?
C2 C1 C13 C9 179.7(3) . . . . ?
C2 C1 C13 C14 -4.8(4) . . . . ?
C12 C9 C13 C1 157.7(3) . . . . ?
C15 C9 C13 C1 -25.7(4) . . . . ?
C12 C9 C13 C14 -17.7(4) . . . . ?
C15 C9 C13 C14 158.9(3) . . . . ?
C46 B11 B13 B14 -37.7(3) . . . . ?
C45 B11 B13 B14 -104.4(3) . . . . ?
B12 B11 B13 B14 -139.9(3) . . . . ?
C46 B11 B13 B17 63.2(4) . . . . ?
B14 B11 B13 B17 100.9(3) . . . . ?
C45 B11 B13 B17 -3.5(4) . . . . ?
B12 B11 B13 B17 -39.0(3) . . . . ?
C46 B11 B13 B16 1.0(4) . . . . ?
B14 B11 B13 B16 38.7(3) . . . . ?
C45 B11 B13 B16 -65.7(4) . . . . ?
B12 B11 B13 B16 -101.2(3) . . . . ?
C46 B11 B13 B12 102.2(3) . . . . ?
B14 B11 B13 B12 139.9(3) . . . . ?
C45 B11 B13 B12 35.5(3) . . . . ?
C45 B12 B13 B14 -0.8(4) . . . . ?
B18 B12 B13 B14 -62.8(4) . . . . ?
B17 B12 B13 B14 -100.2(3) . . . . ?
B11 B12 B13 B14 36.1(3) . . . . ?
C45 B12 B13 B11 -36.9(3) . . . . ?
B18 B12 B13 B11 -98.9(3) . . . . ?
B17 B12 B13 B11 -136.4(3) . . . . ?
C45 B12 B13 B17 99.5(3) . . . . ?
B18 B12 B13 B17 37.4(3) . . . . ?
B11 B12 B13 B17 136.4(3) . . . . ?
C45 B12 B13 B16 63.2(4) . . . . ?
B18 B12 B13 B16 1.2(4) . . . . ?
B17 B12 B13 B16 -36.3(3) . . . . ?
B11 B12 B13 B16 100.1(3) . . . . ?
C11 C10 C14 C4 -169.9(3) . . . . ?
C40 C10 C14 C4 4.0(4) . . . . ?
C11 C10 C14 C13 7.4(4) . . . . ?
C40 C10 C14 C13 -178.8(3) . . . . ?
C3 C4 C14 C10 172.3(3) . . . . ?
C3 C4 C14 C13 -5.0(5) . . . . ?
C1 C13 C14 C10 -169.6(3) . . . . ?
C9 C13 C14 C10 6.2(4) . . . . ?
C1 C13 C14 C4 7.6(4) . . . . ?
C9 C13 C14 C4 -176.5(3) . . . . ?
C45 B11 B14 C46 -39.2(3) . . . . ?
B13 B11 B14 C46 -137.1(3) . . . . ?
B12 B11 B14 C46 -100.8(3) . . . . ?
C46 B11 B14 B13 137.1(3) . . . . ?
C45 B11 B14 B13 98.0(3) . . . . ?
B12 B11 B14 B13 36.3(3) . . . . ?
C46 B11 B14 B15 34.8(3) . . . . ?
C45 B11 B14 B15 -4.3(4) . . . . ?
B13 B11 B14 B15 -102.3(3) . . . . ?
B12 B11 B14 B15 -66.0(3) . . . . ?
C46 B11 B14 B16 98.4(3) . . . . ?
C45 B11 B14 B16 59.3(3) . . . . ?
B13 B11 B14 B16 -38.7(3) . . . . ?
B12 B11 B14 B16 -2.4(4) . . . . ?
B11 B13 B14 C46 37.4(3) . . . . ?
B17 B13 B14 C46 -63.0(4) . . . . ?
B16 B13 B14 C46 -99.2(3) . . . . ?
B12 B13 B14 C46 0.9(4) . . . . ?
B17 B13 B14 B11 -100.5(3) . . . . ?
B16 B13 B14 B11 -136.6(3) . . . . ?
B12 B13 B14 B11 -36.5(3) . . . . ?
B11 B13 B14 B15 99.1(3) . . . . ?
B17 B13 B14 B15 -1.3(4) . . . . ?
B16 B13 B14 B15 -37.5(3) . . . . ?
B12 B13 B14 B15 62.6(4) . . . . ?
B11 B13 B14 B16 136.6(3) . . . . ?
B17 B13 B14 B16 36.1(3) . . . . ?
B12 B13 B14 B16 100.1(3) . . . . ?
C12 C9 C15 B8 -130.0(3) . . . . ?
C13 C9 C15 B8 53.5(4) . . . . ?
C12 C9 C15 B4 -49.6(4) . . . . ?
C13 C9 C15 B4 133.8(3) . . . . ?
C12 C9 C15 B1 25.2(4) . . . . ?
C13 C9 C15 B1 -151.3(3) . . . . ?
C12 C9 C15 B9 154.4(3) . . . . ?
C13 C9 C15 B9 -22.1(4) . . . . ?
C12 C9 C15 C16 89.9(3) . . . . ?
C13 C9 C15 C16 -86.7(3) . . . . ?
B4 B8 C15 C9 116.3(4) . . . . ?
B7 B8 C15 C9 153.5(3) . . . . ?
B10 B8 C15 C9 -143.0(3) . . . . ?
B9 B8 C15 C9 -106.4(3) . . . . ?
B7 B8 C15 B4 37.2(3) . . . . ?
B10 B8 C15 B4 100.7(3) . . . . ?
B9 B8 C15 B4 137.3(3) . . . . ?
B4 B8 C15 B1 -40.5(3) . . . . ?
B7 B8 C15 B1 -3.3(4) . . . . ?
B10 B8 C15 B1 60.2(3) . . . . ?
B9 B8 C15 B1 96.8(3) . . . . ?
B4 B8 C15 B9 -137.3(3) . . . . ?
B7 B8 C15 B9 -100.1(3) . . . . ?
B10 B8 C15 B9 -36.6(3) . . . . ?
B4 B8 C15 C16 -100.3(3) . . . . ?
B7 B8 C15 C16 -63.2(3) . . . . ?
B10 B8 C15 C16 0.3(3) . . . . ?
B9 B8 C15 C16 37.0(2) . . . . ?
B8 B4 C15 C9 -117.3(3) . . . . ?
B7 B4 C15 C9 -154.3(3) . . . . ?
B3 B4 C15 C9 142.3(3) . . . . ?
B1 B4 C15 C9 106.0(3) . . . . ?
B7 B4 C15 B8 -37.0(3) . . . . ?
B3 B4 C15 B8 -100.4(3) . . . . ?
B1 B4 C15 B8 -136.7(3) . . . . ?
B8 B4 C15 B1 136.7(3) . . . . ?
B7 B4 C15 B1 99.7(3) . . . . ?
B3 B4 C15 B1 36.3(3) . . . . ?
B8 B4 C15 B9 40.1(3) . . . . ?
B7 B4 C15 B9 3.1(4) . . . . ?
B3 B4 C15 B9 -60.3(4) . . . . ?
B1 B4 C15 B9 -96.5(3) . . . . ?
B8 B4 C15 C16 99.9(3) . . . . ?
B7 B4 C15 C16 62.9(3) . . . . ?
B3 B4 C15 C16 -0.5(4) . . . . ?
B1 B4 C15 C16 -36.7(2) . . . . ?
C16 B1 C15 C9 104.7(3) . . . . ?
B3 B1 C15 C9 -155.0(3) . . . . ?
B2 B1 C15 C9 141.7(3) . . . . ?
B4 B1 C15 C9 -118.6(3) . . . . ?
C16 B1 C15 B8 -96.2(3) . . . . ?
B3 B1 C15 B8 4.1(4) . . . . ?
B2 B1 C15 B8 -59.2(4) . . . . ?
B4 B1 C15 B8 40.5(3) . . . . ?
C16 B1 C15 B4 -136.6(3) . . . . ?
B3 B1 C15 B4 -36.4(3) . . . . ?
B2 B1 C15 B4 -99.7(3) . . . . ?
C16 B1 C15 B9 -30.4(2) . . . . ?
B3 B1 C15 B9 69.8(3) . . . . ?
B2 B1 C15 B9 6.6(3) . . . . ?
B4 B1 C15 B9 106.2(3) . . . . ?
B3 B1 C15 C16 100.2(3) . . . . ?
B2 B1 C15 C16 37.0(3) . . . . ?
B4 B1 C15 C16 136.6(3) . . . . ?
C16 B9 C15 C9 -104.5(3) . . . . ?
B5 B9 C15 C9 -141.6(3) . . . . ?
B10 B9 C15 C9 155.2(3) . . . . ?
B8 B9 C15 C9 119.3(3) . . . . ?
C16 B9 C15 B8 136.2(3) . . . . ?
B5 B9 C15 B8 99.1(3) . . . . ?
B10 B9 C15 B8 35.8(3) . . . . ?
C16 B9 C15 B4 96.1(3) . . . . ?
B5 B9 C15 B4 59.0(3) . . . . ?
B10 B9 C15 B4 -4.2(3) . . . . ?
B8 B9 C15 B4 -40.1(3) . . . . ?
C16 B9 C15 B1 30.5(2) . . . . ?
B5 B9 C15 B1 -6.6(3) . . . . ?
B10 B9 C15 B1 -69.9(3) . . . . ?
B8 B9 C15 B1 -105.7(3) . . . . ?
B5 B9 C15 C16 -37.1(2) . . . . ?
B10 B9 C15 C16 -100.4(3) . . . . ?
B8 B9 C15 C16 -136.2(3) . . . . ?
B11 B14 B15 C46 -35.0(3) . . . . ?
B13 B14 B15 C46 -98.5(3) . . . . ?
B16 B14 B15 C46 -135.8(3) . . . . ?
C46 B14 B15 B19 35.6(3) . . . . ?
B11 B14 B15 B19 0.6(4) . . . . ?
B13 B14 B15 B19 -62.9(4) . . . . ?
B16 B14 B15 B19 -100.3(4) . . . . ?
C46 B14 B15 B16 135.8(3) . . . . ?
B11 B14 B15 B16 100.9(3) . . . . ?
B13 B14 B15 B16 37.4(3) . . . . ?
C46 B14 B15 B20 98.4(3) . . . . ?
B11 B14 B15 B20 63.4(4) . . . . ?
B13 B14 B15 B20 -0.1(4) . . . . ?
B16 B14 B15 B20 -37.5(3) . . . . ?
C15 B9 C16 C17 107.5(3) . . . . ?
B5 B9 C16 C17 -113.8(3) . . . . ?
B10 B9 C16 C17 -152.3(3) . . . . ?
B8 B9 C16 C17 145.3(3) . . . . ?
C15 B9 C16 B2 -100.5(3) . . . . ?
B5 B9 C16 B2 38.2(3) . . . . ?
B10 B9 C16 B2 -0.2(4) . . . . ?
B8 B9 C16 B2 -62.6(3) . . . . ?
C15 B9 C16 B1 -32.4(2) . . . . ?
B5 B9 C16 B1 106.3(3) . . . . ?
B10 B9 C16 B1 67.8(3) . . . . ?
B8 B9 C16 B1 5.4(3) . . . . ?
C15 B9 C16 B5 -138.7(3) . . . . ?
B10 B9 C16 B5 -38.4(3) . . . . ?
B8 B9 C16 B5 -100.9(3) . . . . ?
B5 B9 C16 C15 138.7(3) . . . . ?
B10 B9 C16 C15 100.3(3) . . . . ?
B8 B9 C16 C15 37.9(2) . . . . ?
B5 B2 C16 C17 113.0(3) . . . . ?
B3 B2 C16 C17 -144.5(3) . . . . ?
B6 B2 C16 C17 152.1(3) . . . . ?
B1 B2 C16 C17 -106.9(4) . . . . ?
B5 B2 C16 B9 -38.5(3) . . . . ?
B3 B2 C16 B9 64.0(4) . . . . ?
B6 B2 C16 B9 0.6(4) . . . . ?
B1 B2 C16 B9 101.6(3) . . . . ?
B5 B2 C16 B1 -140.1(3) . . . . ?
B3 B2 C16 B1 -37.6(3) . . . . ?
B6 B2 C16 B1 -101.0(3) . . . . ?
B3 B2 C16 B5 102.5(3) . . . . ?
B6 B2 C16 B5 39.1(3) . . . . ?
B1 B2 C16 B5 140.1(3) . . . . ?
B5 B2 C16 C15 -102.8(3) . . . . ?
B3 B2 C16 C15 -0.3(4) . . . . ?
B6 B2 C16 C15 -63.7(4) . . . . ?
B1 B2 C16 C15 37.3(3) . . . . ?
C15 B1 C16 C17 -108.5(3) . . . . ?
B3 B1 C16 C17 150.6(3) . . . . ?
B2 B1 C16 C17 113.0(3) . . . . ?
B4 B1 C16 C17 -146.1(3) . . . . ?
C15 B1 C16 B9 32.5(2) . . . . ?
B3 B1 C16 B9 -68.5(3) . . . . ?
B2 B1 C16 B9 -106.1(3) . . . . ?
B4 B1 C16 B9 -5.2(3) . . . . ?
C15 B1 C16 B2 138.6(3) . . . . ?
B3 B1 C16 B2 37.6(3) . . . . ?
B4 B1 C16 B2 100.9(3) . . . . ?
C15 B1 C16 B5 100.5(3) . . . . ?
B3 B1 C16 B5 -0.4(4) . . . . ?
B2 B1 C16 B5 -38.0(3) . . . . ?
B4 B1 C16 B5 62.9(3) . . . . ?
B3 B1 C16 C15 -101.0(3) . . . . ?
B2 B1 C16 C15 -138.6(3) . . . . ?
B4 B1 C16 C15 -37.7(2) . . . . ?
B2 B5 C16 C17 -110.9(4) . . . . ?
B10 B5 C16 C17 147.7(3) . . . . ?
B9 B5 C16 C17 109.2(3) . . . . ?
B6 B5 C16 C17 -149.6(3) . . . . ?
B2 B5 C16 B9 139.8(3) . . . . ?
B10 B5 C16 B9 38.5(3) . . . . ?
B6 B5 C16 B9 101.2(3) . . . . ?
B10 B5 C16 B2 -101.4(3) . . . . ?
B9 B5 C16 B2 -139.8(3) . . . . ?
B6 B5 C16 B2 -38.6(3) . . . . ?
B2 B5 C16 B1 38.3(3) . . . . ?
B10 B5 C16 B1 -63.1(4) . . . . ?
B9 B5 C16 B1 -101.5(3) . . . . ?
B6 B5 C16 B1 -0.3(4) . . . . ?
B2 B5 C16 C15 102.6(3) . . . . ?
B10 B5 C16 C15 1.2(4) . . . . ?
B9 B5 C16 C15 -37.2(3) . . . . ?
B6 B5 C16 C15 63.9(3) . . . . ?
C9 C15 C16 C17 -1.2(4) . . . . ?
B8 C15 C16 C17 -149.1(3) . . . . ?
B4 C15 C16 C17 145.8(3) . . . . ?
B1 C15 C16 C17 106.5(3) . . . . ?
B9 C15 C16 C17 -109.4(3) . . . . ?
C9 C15 C16 B9 108.1(3) . . . . ?
B8 C15 C16 B9 -39.7(3) . . . . ?
B4 C15 C16 B9 -104.9(3) . . . . ?
B1 C15 C16 B9 -144.1(3) . . . . ?
C9 C15 C16 B2 -146.5(3) . . . . ?
B8 C15 C16 B2 65.7(3) . . . . ?
B4 C15 C16 B2 0.5(3) . . . . ?
B1 C15 C16 B2 -38.8(3) . . . . ?
B9 C15 C16 B2 105.3(3) . . . . ?
C9 C15 C16 B1 -107.7(3) . . . . ?
B8 C15 C16 B1 104.5(3) . . . . ?
B4 C15 C16 B1 39.3(3) . . . . ?
B9 C15 C16 B1 144.1(3) . . . . ?
C9 C15 C16 B5 146.8(3) . . . . ?
B8 C15 C16 B5 -1.0(3) . . . . ?
B4 C15 C16 B5 -66.2(3) . . . . ?
B1 C15 C16 B5 -105.4(3) . . . . ?
B9 C15 C16 B5 38.7(3) . . . . ?
B14 B13 B16 B17 139.2(3) . . . . ?
B11 B13 B16 B17 100.7(3) . . . . ?
B12 B13 B16 B17 36.8(3) . . . . ?
B11 B13 B16 B14 -38.4(3) . . . . ?
B17 B13 B16 B14 -139.2(3) . . . . ?
B12 B13 B16 B14 -102.4(3) . . . . ?
B14 B13 B16 B20 100.2(3) . . . . ?
B11 B13 B16 B20 61.8(4) . . . . ?
B17 B13 B16 B20 -39.0(3) . . . . ?
B12 B13 B16 B20 -2.2(4) . . . . ?
B14 B13 B16 B15 36.7(3) . . . . ?
B11 B13 B16 B15 -1.7(4) . . . . ?
B17 B13 B16 B15 -102.4(3) . . . . ?
B12 B13 B16 B15 -65.6(4) . . . . ?
C46 B14 B16 B17 63.6(4) . . . . ?
B11 B14 B16 B17 1.9(4) . . . . ?
B13 B14 B16 B17 -36.8(3) . . . . ?
B15 B14 B16 B17 101.8(3) . . . . ?
C46 B14 B16 B13 100.4(3) . . . . ?
B11 B14 B16 B13 38.6(3) . . . . ?
B15 B14 B16 B13 138.5(3) . . . . ?
C46 B14 B16 B20 -0.5(4) . . . . ?
B11 B14 B16 B20 -62.2(4) . . . . ?
B13 B14 B16 B20 -100.9(4) . . . . ?
B15 B14 B16 B20 37.7(3) . . . . ?
C46 B14 B16 B15 -38.2(3) . . . . ?
B11 B14 B16 B15 -99.9(3) . . . . ?
B13 B14 B16 B15 -138.5(3) . . . . ?
C46 B15 B16 B17 -62.2(4) . . . . ?
B14 B15 B16 B17 -100.5(3) . . . . ?
B19 B15 B16 B17 -0.6(4) . . . . ?
B20 B15 B16 B17 37.3(3) . . . . ?
C46 B15 B16 B13 1.7(4) . . . . ?
B14 B15 B16 B13 -36.7(3) . . . . ?
B19 B15 B16 B13 63.3(4) . . . . ?
B20 B15 B16 B13 101.1(4) . . . . ?
C46 B15 B16 B14 38.4(3) . . . . ?
B19 B15 B16 B14 100.0(3) . . . . ?
B20 B15 B16 B14 137.8(3) . . . . ?
C46 B15 B16 B20 -99.4(3) . . . . ?
B14 B15 B16 B20 -137.8(3) . . . . ?
B19 B15 B16 B20 -37.8(3) . . . . ?
B9 C16 C17 C18 13.2(5) . . . . ?
B2 C16 C17 C18 -136.5(4) . . . . ?
B1 C16 C17 C18 150.3(3) . . . . ?
B5 C16 C17 C18 -61.7(4) . . . . ?
C15 C16 C17 C18 82.2(4) . . . . ?
B9 C16 C17 C22 -173.8(3) . . . . ?
B2 C16 C17 C22 36.5(5) . . . . ?
B1 C16 C17 C22 -36.7(5) . . . . ?
B5 C16 C17 C22 111.3(4) . . . . ?
C15 C16 C17 C22 -104.8(4) . . . . ?
B14 B16 B17 B13 36.4(3) . . . . ?
B20 B16 B17 B13 136.7(3) . . . . ?
B15 B16 B17 B13 99.6(3) . . . . ?
B13 B16 B17 B20 -136.7(3) . . . . ?
B14 B16 B17 B20 -100.3(3) . . . . ?
B15 B16 B17 B20 -37.0(3) . . . . ?
B13 B16 B17 B18 -100.3(3) . . . . ?
B14 B16 B17 B18 -63.9(4) . . . . ?
B20 B16 B17 B18 36.4(3) . . . . ?
B15 B16 B17 B18 -0.6(4) . . . . ?
B13 B16 B17 B12 -37.0(3) . . . . ?
B14 B16 B17 B12 -0.7(4) . . . . ?
B20 B16 B17 B12 99.6(3) . . . . ?
B15 B16 B17 B12 62.6(4) . . . . ?
B14 B13 B17 B16 -36.7(3) . . . . ?
B11 B13 B17 B16 -99.8(3) . . . . ?
B12 B13 B17 B16 -139.0(3) . . . . ?
B14 B13 B17 B20 2.2(4) . . . . ?
B11 B13 B17 B20 -60.9(4) . . . . ?
B16 B13 B17 B20 38.9(3) . . . . ?
B12 B13 B17 B20 -100.1(3) . . . . ?
B14 B13 B17 B18 65.2(4) . . . . ?
B11 B13 B17 B18 2.0(4) . . . . ?
B16 B13 B17 B18 101.9(3) . . . . ?
B12 B13 B17 B18 -37.1(3) . . . . ?
B14 B13 B17 B12 102.3(3) . . . . ?
B11 B13 B17 B12 39.2(3) . . . . ?
B16 B13 B17 B12 139.0(3) . . . . ?
C45 B12 B17 B16 -63.9(4) . . . . ?
B18 B12 B17 B16 -101.0(3) . . . . ?
B13 B12 B17 B16 37.2(3) . . . . ?
B11 B12 B17 B16 -0.8(4) . . . . ?
C45 B12 B17 B13 -101.1(3) . . . . ?
B18 B12 B17 B13 -138.2(3) . . . . ?
B11 B12 B17 B13 -38.0(3) . . . . ?
C45 B12 B17 B20 0.1(4) . . . . ?
B18 B12 B17 B20 -36.9(3) . . . . ?
B13 B12 B17 B20 101.2(4) . . . . ?
B11 B12 B17 B20 63.2(4) . . . . ?
C45 B12 B17 B18 37.0(3) . . . . ?
B13 B12 B17 B18 138.2(3) . . . . ?
B11 B12 B17 B18 100.1(3) . . . . ?
C22 C17 C18 C19 0.7(6) . . . . ?
C16 C17 C18 C19 173.9(4) . . . . ?
B13 B12 B18 C45 100.5(3) . . . . ?
B17 B12 B18 C45 137.6(3) . . . . ?
B11 B12 B18 C45 38.3(2) . . . . ?
C45 B12 B18 B20 -100.2(3) . . . . ?
B13 B12 B18 B20 0.3(4) . . . . ?
B17 B12 B18 B20 37.4(3) . . . . ?
B11 B12 B18 B20 -61.9(3) . . . . ?
C45 B12 B18 B17 -137.6(3) . . . . ?
B13 B12 B18 B17 -37.2(3) . . . . ?
B11 B12 B18 B17 -99.3(3) . . . . ?
C45 B12 B18 B19 -37.5(2) . . . . ?
B13 B12 B18 B19 63.0(3) . . . . ?
B17 B12 B18 B19 100.2(3) . . . . ?
B11 B12 B18 B19 0.9(4) . . . . ?
B16 B17 B18 C45 64.4(4) . . . . ?
B13 B17 B18 C45 0.3(4) . . . . ?
B20 B17 B18 C45 101.2(3) . . . . ?
B12 B17 B18 C45 -37.1(3) . . . . ?
B16 B17 B18 B12 101.5(3) . . . . ?
B13 B17 B18 B12 37.4(3) . . . . ?
B20 B17 B18 B12 138.3(3) . . . . ?
B16 B17 B18 B20 -36.8(3) . . . . ?
B13 B17 B18 B20 -100.9(4) . . . . ?
B12 B17 B18 B20 -138.3(3) . . . . ?
B16 B17 B18 B19 1.6(4) . . . . ?
B13 B17 B18 B19 -62.6(4) . . . . ?
B20 B17 B18 B19 38.4(3) . . . . ?
B12 B17 B18 B19 -100.0(3) . . . . ?
C17 C18 C19 C20 -0.6(7) . . . . ?
B14 B15 B19 C46 -35.7(3) . . . . ?
B16 B15 B19 C46 -98.6(3) . . . . ?
B20 B15 B19 C46 -136.5(3) . . . . ?
C46 B15 B19 C45 39.0(3) . . . . ?
B14 B15 B19 C45 3.3(4) . . . . ?
B16 B15 B19 C45 -59.7(4) . . . . ?
B20 B15 B19 C45 -97.5(3) . . . . ?
C46 B15 B19 B20 136.5(3) . . . . ?
B14 B15 B19 B20 100.8(3) . . . . ?
B16 B15 B19 B20 37.8(3) . . . . ?
C46 B15 B19 B18 100.2(3) . . . . ?
B14 B15 B19 B18 64.5(4) . . . . ?
B16 B15 B19 B18 1.6(4) . . . . ?
B20 B15 B19 B18 -36.3(3) . . . . ?
C45 B18 B19 C46 -40.5(2) . . . . ?
B12 B18 B19 C46 -3.4(4) . . . . ?
B20 B18 B19 C46 98.5(3) . . . . ?
B17 B18 B19 C46 59.9(3) . . . . ?
B12 B18 B19 C45 37.1(2) . . . . ?
B20 B18 B19 C45 139.0(3) . . . . ?
B17 B18 B19 C45 100.3(3) . . . . ?
C45 B18 B19 B20 -139.0(3) . . . . ?
B12 B18 B19 B20 -101.9(3) . . . . ?
B17 B18 B19 B20 -38.6(3) . . . . ?
C45 B18 B19 B15 -102.3(3) . . . . ?
B12 B18 B19 B15 -65.2(3) . . . . ?
B20 B18 B19 B15 36.7(3) . . . . ?
B17 B18 B19 B15 -1.9(4) . . . . ?
C18 C19 C20 C21 0.5(7) . . . . ?
C45 B18 B20 B19 36.6(3) . . . . ?
B12 B18 B20 B19 98.9(3) . . . . ?
B17 B18 B20 B19 136.4(3) . . . . ?
C45 B18 B20 B16 -63.9(4) . . . . ?
B12 B18 B20 B16 -1.6(4) . . . . ?
B17 B18 B20 B16 35.9(3) . . . . ?
B19 B18 B20 B16 -100.5(3) . . . . ?
C45 B18 B20 B17 -99.8(3) . . . . ?
B12 B18 B20 B17 -37.5(3) . . . . ?
B19 B18 B20 B17 -136.4(3) . . . . ?
C45 B18 B20 B15 -0.1(4) . . . . ?
B12 B18 B20 B15 62.2(4) . . . . ?
B17 B18 B20 B15 99.7(3) . . . . ?
B19 B18 B20 B15 -36.7(3) . . . . ?
C46 B19 B20 B18 -101.7(3) . . . . ?
C45 B19 B20 B18 -35.2(3) . . . . ?
B15 B19 B20 B18 -139.3(3) . . . . ?
C46 B19 B20 B16 -0.5(4) . . . . ?
C45 B19 B20 B16 66.0(4) . . . . ?
B15 B19 B20 B16 -38.1(3) . . . . ?
B18 B19 B20 B16 101.2(3) . . . . ?
C46 B19 B20 B17 -62.7(4) . . . . ?
C45 B19 B20 B17 3.8(4) . . . . ?
B15 B19 B20 B17 -100.3(3) . . . . ?
B18 B19 B20 B17 39.0(3) . . . . ?
C46 B19 B20 B15 37.6(3) . . . . ?
C45 B19 B20 B15 104.2(3) . . . . ?
B18 B19 B20 B15 139.3(3) . . . . ?
B17 B16 B20 B18 -36.5(3) . . . . ?
B13 B16 B20 B18 2.3(4) . . . . ?
B14 B16 B20 B18 65.1(4) . . . . ?
B15 B16 B20 B18 102.5(3) . . . . ?
B17 B16 B20 B19 -100.9(3) . . . . ?
B13 B16 B20 B19 -62.1(4) . . . . ?
B14 B16 B20 B19 0.6(4) . . . . ?
B15 B16 B20 B19 38.0(3) . . . . ?
B13 B16 B20 B17 38.8(3) . . . . ?
B14 B16 B20 B17 101.5(3) . . . . ?
B15 B16 B20 B17 139.0(3) . . . . ?
B17 B16 B20 B15 -139.0(3) . . . . ?
B13 B16 B20 B15 -100.1(3) . . . . ?
B14 B16 B20 B15 -37.4(3) . . . . ?
B16 B17 B20 B18 139.3(3) . . . . ?
B13 B17 B20 B18 100.4(3) . . . . ?
B12 B17 B20 B18 36.9(3) . . . . ?
B16 B17 B20 B19 100.0(3) . . . . ?
B13 B17 B20 B19 61.0(4) . . . . ?
B18 B17 B20 B19 -39.4(3) . . . . ?
B12 B17 B20 B19 -2.5(4) . . . . ?
B13 B17 B20 B16 -39.0(3) . . . . ?
B18 B17 B20 B16 -139.3(3) . . . . ?
B12 B17 B20 B16 -102.4(3) . . . . ?
B16 B17 B20 B15 36.7(3) . . . . ?
B13 B17 B20 B15 -2.3(4) . . . . ?
B18 B17 B20 B15 -102.7(3) . . . . ?
B12 B17 B20 B15 -65.8(4) . . . . ?
C46 B15 B20 B18 -0.6(4) . . . . ?
B14 B15 B20 B18 -62.4(3) . . . . ?
B19 B15 B20 B18 37.2(3) . . . . ?
B16 B15 B20 B18 -100.0(3) . . . . ?
C46 B15 B20 B19 -37.8(3) . . . . ?
B14 B15 B20 B19 -99.6(3) . . . . ?
B16 B15 B20 B19 -137.2(3) . . . . ?
C46 B15 B20 B16 99.4(3) . . . . ?
B14 B15 B20 B16 37.6(3) . . . . ?
B19 B15 B20 B16 137.2(3) . . . . ?
C46 B15 B20 B17 63.3(3) . . . . ?
B14 B15 B20 B17 1.5(4) . . . . ?
B19 B15 B20 B17 101.1(3) . . . . ?
B16 B15 B20 B17 -36.1(3) . . . . ?
C19 C20 C21 C22 -0.6(8) . . . . ?
C18 C17 C22 C21 -0.7(7) . . . . ?
C16 C17 C22 C21 -174.1(4) . . . . ?
C20 C21 C22 C17 0.7(8) . . . . ?
C43 C31 C32 C33 -1.5(6) . . . . ?
C31 C32 C33 C34 -3.6(6) . . . . ?
C32 C33 C34 C44 1.4(6) . . . . ?
C41 C35 C36 C37 -0.4(7) . . . . ?
C35 C36 C37 C38 3.2(8) . . . . ?
C36 C37 C38 C42 -0.8(7) . . . . ?
C14 C10 C40 C41 -87.7(4) . . . . ?
C11 C10 C40 C41 86.1(4) . . . . ?
C14 C10 C40 C44 88.6(4) . . . . ?
C11 C10 C40 C44 -97.5(4) . . . . ?
C44 C40 C41 C35 -172.0(3) . . . . ?
C10 C40 C41 C35 4.4(5) . . . . ?
C44 C40 C41 C42 9.0(5) . . . . ?
C10 C40 C41 C42 -174.7(3) . . . . ?
C36 C35 C41 C40 176.4(4) . . . . ?
C36 C35 C41 C42 -4.6(6) . . . . ?
C43 C39 C42 C38 160.6(3) . . . . ?
C45 C39 C42 C38 -26.6(5) . . . . ?
C43 C39 C42 C41 -14.6(5) . . . . ?
C45 C39 C42 C41 158.2(3) . . . . ?
C37 C38 C42 C39 -179.4(4) . . . . ?
C37 C38 C42 C41 -4.1(6) . . . . ?
C40 C41 C42 C39 1.2(5) . . . . ?
C35 C41 C42 C39 -177.9(3) . . . . ?
C40 C41 C42 C38 -174.4(3) . . . . ?
C35 C41 C42 C38 6.6(5) . . . . ?
C42 C39 C43 C31 -159.6(3) . . . . ?
C45 C39 C43 C31 27.6(5) . . . . ?
C42 C39 C43 C44 18.0(5) . . . . ?
C45 C39 C43 C44 -154.8(3) . . . . ?
C32 C31 C43 C39 -174.0(3) . . . . ?
C32 C31 C43 C44 8.3(5) . . . . ?
C41 C40 C44 C34 174.3(3) . . . . ?
C10 C40 C44 C34 -2.0(5) . . . . ?
C41 C40 C44 C43 -5.5(5) . . . . ?
C10 C40 C44 C43 178.2(3) . . . . ?
C33 C34 C44 C40 -174.1(4) . . . . ?
C33 C34 C44 C43 5.8(6) . . . . ?
C39 C43 C44 C40 -8.2(5) . . . . ?
C31 C43 C44 C40 169.6(3) . . . . ?
C39 C43 C44 C34 172.0(3) . . . . ?
C31 C43 C44 C34 -10.2(5) . . . . ?
C43 C39 C45 B18 -139.9(3) . . . . ?
C42 C39 C45 B18 47.5(5) . . . . ?
C43 C39 C45 B12 -57.9(4) . . . . ?
C42 C39 C45 B12 129.5(4) . . . . ?
C43 C39 C45 B19 145.9(3) . . . . ?
C42 C39 C45 B19 -26.7(4) . . . . ?
C43 C39 C45 B11 18.2(4) . . . . ?
C42 C39 C45 B11 -154.4(3) . . . . ?
C43 C39 C45 C46 82.3(3) . . . . ?
C42 C39 C45 C46 -90.4(3) . . . . ?
B12 B18 C45 C39 119.3(4) . . . . ?
B20 B18 C45 C39 -139.5(3) . . . . ?
B17 B18 C45 C39 157.1(3) . . . . ?
B19 B18 C45 C39 -103.1(4) . . . . ?
B20 B18 C45 B12 101.1(3) . . . . ?
B17 B18 C45 B12 37.8(3) . . . . ?
B19 B18 C45 B12 137.6(3) . . . . ?
B12 B18 C45 B19 -137.6(3) . . . . ?
B20 B18 C45 B19 -36.5(3) . . . . ?
B17 B18 C45 B19 -99.8(3) . . . . ?
B12 B18 C45 B11 -40.3(3) . . . . ?
B20 B18 C45 B11 60.9(3) . . . . ?
B17 B18 C45 B11 -2.5(4) . . . . ?
B19 B18 C45 B11 97.3(3) . . . . ?
B12 B18 C45 C46 -100.4(3) . . . . ?
B20 B18 C45 C46 0.7(3) . . . . ?
B17 B18 C45 C46 -62.6(3) . . . . ?
B19 B18 C45 C46 37.2(2) . . . . ?
B18 B12 C45 C39 -116.9(4) . . . . ?
B13 B12 C45 C39 142.7(3) . . . . ?
B17 B12 C45 C39 -154.6(3) . . . . ?
B11 B12 C45 C39 106.3(3) . . . . ?
B13 B12 C45 B18 -100.4(3) . . . . ?
B17 B12 C45 B18 -37.7(3) . . . . ?
B11 B12 C45 B18 -136.8(3) . . . . ?
B18 B12 C45 B19 40.1(3) . . . . ?
B13 B12 C45 B19 -60.3(3) . . . . ?
B17 B12 C45 B19 2.4(4) . . . . ?
B11 B12 C45 B19 -96.7(3) . . . . ?
B18 B12 C45 B11 136.8(3) . . . . ?
B13 B12 C45 B11 36.4(3) . . . . ?
B17 B12 C45 B11 99.1(3) . . . . ?
B18 B12 C45 C46 100.7(3) . . . . ?
B13 B12 C45 C46 0.3(3) . . . . ?
B17 B12 C45 C46 63.0(3) . . . . ?
B11 B12 C45 C46 -36.1(2) . . . . ?
C46 B19 C45 C39 -103.3(3) . . . . ?
B20 B19 C45 C39 156.3(3) . . . . ?
B15 B19 C45 C39 -140.0(3) . . . . ?
B18 B19 C45 C39 120.3(3) . . . . ?
C46 B19 C45 B18 136.4(3) . . . . ?
B20 B19 C45 B18 36.0(3) . . . . ?
B15 B19 C45 B18 99.7(3) . . . . ?
C46 B19 C45 B12 96.5(3) . . . . ?
B20 B19 C45 B12 -3.9(4) . . . . ?
B15 B19 C45 B12 59.8(4) . . . . ?
B18 B19 C45 B12 -39.9(3) . . . . ?
C46 B19 C45 B11 30.9(2) . . . . ?
B20 B19 C45 B11 -69.5(3) . . . . ?
B15 B19 C45 B11 -5.8(4) . . . . ?
B18 B19 C45 B11 -105.5(3) . . . . ?
B20 B19 C45 C46 -100.4(3) . . . . ?
B15 B19 C45 C46 -36.7(3) . . . . ?
B18 B19 C45 C46 -136.4(3) . . . . ?
C46 B11 C45 C39 101.4(3) . . . . ?
B14 B11 C45 C39 138.7(3) . . . . ?
B13 B11 C45 C39 -157.7(3) . . . . ?
B12 B11 C45 C39 -121.1(3) . . . . ?
C46 B11 C45 B18 -97.2(3) . . . . ?
B14 B11 C45 B18 -59.9(4) . . . . ?
B13 B11 C45 B18 3.8(4) . . . . ?
B12 B11 C45 B18 40.4(3) . . . . ?
C46 B11 C45 B12 -137.5(3) . . . . ?
B14 B11 C45 B12 -100.3(3) . . . . ?
B13 B11 C45 B12 -36.6(3) . . . . ?
C46 B11 C45 B19 -31.0(2) . . . . ?
B14 B11 C45 B19 6.3(4) . . . . ?
B13 B11 C45 B19 69.9(3) . . . . ?
B12 B11 C45 B19 106.5(3) . . . . ?
B14 B11 C45 C46 37.3(3) . . . . ?
B13 B11 C45 C46 100.9(3) . . . . ?
B12 B11 C45 C46 137.5(3) . . . . ?
B14 B15 C46 C47 -112.3(3) . . . . ?
B19 B15 C46 C47 108.3(3) . . . . ?
B16 B15 C46 C47 -151.1(3) . . . . ?
B20 B15 C46 C47 146.5(3) . . . . ?
B14 B15 C46 B11 37.7(3) . . . . ?
B19 B15 C46 B11 -101.7(3) . . . . ?
B16 B15 C46 B11 -1.1(4) . . . . ?
B20 B15 C46 B11 -63.5(3) . . . . ?
B14 B15 C46 B19 139.4(3) . . . . ?
B16 B15 C46 B19 100.5(3) . . . . ?
B20 B15 C46 B19 38.2(3) . . . . ?
B19 B15 C46 B14 -139.4(3) . . . . ?
B16 B15 C46 B14 -38.8(3) . . . . ?
B20 B15 C46 B14 -101.2(3) . . . . ?
B14 B15 C46 C45 102.2(3) . . . . ?
B19 B15 C46 C45 -37.2(2) . . . . ?
B16 B15 C46 C45 63.4(3) . . . . ?
B20 B15 C46 C45 1.1(3) . . . . ?
B14 B11 C46 C47 112.6(3) . . . . ?
C45 B11 C46 C47 -108.7(3) . . . . ?
B13 B11 C46 C47 150.7(3) . . . . ?
B12 B11 C46 C47 -145.7(3) . . . . ?
B14 B11 C46 B15 -38.0(3) . . . . ?
C45 B11 C46 B15 100.7(3) . . . . ?
B13 B11 C46 B15 0.1(4) . . . . ?
B12 B11 C46 B15 63.7(4) . . . . ?
B14 B11 C46 B19 -105.9(3) . . . . ?
C45 B11 C46 B19 32.8(2) . . . . ?
B13 B11 C46 B19 -67.8(3) . . . . ?
B12 B11 C46 B19 -4.3(4) . . . . ?
C45 B11 C46 B14 138.6(3) . . . . ?
B13 B11 C46 B14 38.0(3) . . . . ?
B12 B11 C46 B14 101.6(3) . . . . ?
B14 B11 C46 C45 -138.6(3) . . . . ?
B13 B11 C46 C45 -100.6(3) . . . . ?
B12 B11 C46 C45 -37.0(2) . . . . ?
C45 B19 C46 C47 108.9(3) . . . . ?
B20 B19 C46 C47 -151.0(3) . . . . ?
B15 B19 C46 C47 -112.4(3) . . . . ?
B18 B19 C46 C47 146.6(3) . . . . ?
C45 B19 C46 B15 -138.7(3) . . . . ?
B20 B19 C46 B15 -38.6(3) . . . . ?
B18 B19 C46 B15 -101.0(3) . . . . ?
C45 B19 C46 B11 -32.9(2) . . . . ?
B20 B19 C46 B11 67.2(4) . . . . ?
B15 B19 C46 B11 105.8(3) . . . . ?
B18 B19 C46 B11 4.8(4) . . . . ?
C45 B19 C46 B14 -99.9(3) . . . . ?
B20 B19 C46 B14 0.2(4) . . . . ?
B15 B19 C46 B14 38.8(3) . . . . ?
B18 B19 C46 B14 -62.2(4) . . . . ?
B20 B19 C46 C45 100.1(3) . . . . ?
B15 B19 C46 C45 138.7(3) . . . . ?
B18 B19 C46 C45 37.7(2) . . . . ?
B11 B14 C46 C47 -108.7(3) . . . . ?
B13 B14 C46 C47 -146.7(3) . . . . ?
B15 B14 C46 C47 111.2(4) . . . . ?
B16 B14 C46 C47 150.2(3) . . . . ?
B11 B14 C46 B15 140.2(3) . . . . ?
B13 B14 C46 B15 102.2(3) . . . . ?
B16 B14 C46 B15 39.1(3) . . . . ?
B13 B14 C46 B11 -38.0(3) . . . . ?
B15 B14 C46 B11 -140.2(3) . . . . ?
B16 B14 C46 B11 -101.1(3) . . . . ?
B11 B14 C46 B19 101.3(3) . . . . ?
B13 B14 C46 B19 63.2(4) . . . . ?
B15 B14 C46 B19 -38.9(3) . . . . ?
B16 B14 C46 B19 0.2(4) . . . . ?
B11 B14 C46 C45 37.3(2) . . . . ?
B13 B14 C46 C45 -0.8(3) . . . . ?
B15 B14 C46 C45 -102.9(3) . . . . ?
B16 B14 C46 C45 -63.8(3) . . . . ?
C39 C45 C46 C47 -1.4(4) . . . . ?
B18 C45 C46 C47 -147.4(3) . . . . ?
B12 C45 C46 C47 147.2(3) . . . . ?
B19 C45 C46 C47 -107.6(3) . . . . ?
B11 C45 C46 C47 108.7(3) . . . . ?
C39 C45 C46 B15 144.9(3) . . . . ?
B18 C45 C46 B15 -1.2(3) . . . . ?
B12 C45 C46 B15 -66.6(3) . . . . ?
B19 C45 C46 B15 38.7(3) . . . . ?
B11 C45 C46 B15 -105.1(3) . . . . ?
C39 C45 C46 B11 -110.1(3) . . . . ?
B18 C45 C46 B11 103.9(3) . . . . ?
B12 C45 C46 B11 38.5(3) . . . . ?
B19 C45 C46 B11 143.7(3) . . . . ?
C39 C45 C46 B19 106.2(3) . . . . ?
B18 C45 C46 B19 -39.8(2) . . . . ?
B12 C45 C46 B19 -105.2(3) . . . . ?
B11 C45 C46 B19 -143.7(3) . . . . ?
C39 C45 C46 B14 -148.3(3) . . . . ?
B18 C45 C46 B14 65.7(3) . . . . ?
B12 C45 C46 B14 0.3(3) . . . . ?
B19 C45 C46 B14 105.5(3) . . . . ?
B11 C45 C46 B14 -38.2(3) . . . . ?
B15 C46 C47 C52 -40.4(5) . . . . ?
B11 C46 C47 C52 171.6(3) . . . . ?
B19 C46 C47 C52 33.3(5) . . . . ?
B14 C46 C47 C52 -115.2(4) . . . . ?
C45 C46 C47 C52 102.1(4) . . . . ?
B15 C46 C47 C48 135.3(4) . . . . ?
B11 C46 C47 C48 -12.8(5) . . . . ?
B19 C46 C47 C48 -151.1(4) . . . . ?
B14 C46 C47 C48 60.4(5) . . . . ?
C45 C46 C47 C48 -82.3(4) . . . . ?
C52 C47 C48 C49 0.4(6) . . . . ?
C46 C47 C48 C49 -175.4(4) . . . . ?
C47 C48 C49 C50 0.7(7) . . . . ?
C48 C49 C50 C51 -2.0(7) . . . . ?
C49 C50 C51 C52 2.3(7) . . . . ?
C48 C47 C52 C51 -0.1(6) . . . . ?
C46 C47 C52 C51 175.7(3) . . . . ?
C50 C51 C52 C47 -1.2(6) . . . . ?

_refine_diff_density_max         0.198
_refine_diff_density_min         -0.196
_refine_diff_density_rms         0.039

