# Electronic Supplementary Material (ESI) for Journal of Materials Chemistry C.
# This journal is © The Royal Society of Chemistry 2024

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
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data_r20181029c1
_database_code_depnum_ccdc_archive 'CCDC 2299704'
loop_
_audit_author_name
_audit_author_address
'Jie HAN'
;Nankai University
China
;
_audit_update_record             
;
2023-10-07 deposited with the CCDC.	2024-01-22 downloaded from the CCDC.
;
_audit_creation_date             2023-10-07
_audit_creation_method           
;
Olex2 1.5
(compiled 2023.08.24 svn.re1ec1418 for OlexSys, GUI svn.r6817)
;
_shelx_SHELXL_version_number     2019/2
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C34 H26 O'
_chemical_formula_sum            'C34 H26 O'
_chemical_formula_weight         450.55
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_H-M_alt        'P 1 21/c 1'
_space_group_name_Hall           '-P 2ybc'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'

_cell_length_a                   9.6418(19)
_cell_length_b                   26.613(5)
_cell_length_c                   9.4683(19)
_cell_angle_alpha                90
_cell_angle_beta                 98.63(3)
_cell_angle_gamma                90
_cell_volume                     2402.0(8)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    4759
_cell_measurement_temperature    113(2)
_cell_measurement_theta_max      27.8984
_cell_measurement_theta_min      2.2694
_shelx_estimated_absorpt_T_max   0.991
_shelx_estimated_absorpt_T_min   0.986
_exptl_absorpt_coefficient_mu    0.073
_exptl_absorpt_correction_T_max  1
_exptl_absorpt_correction_T_min  0.7957
_exptl_absorpt_correction_type   MULTI-SCAN
_exptl_absorpt_process_details   crystalclear
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            colourless
_exptl_crystal_colour_primary    colourless
_exptl_crystal_density_diffrn    1.246
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             952
_exptl_crystal_size_max          0.2
_exptl_crystal_size_mid          0.18
_exptl_crystal_size_min          0.12
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0627
_diffrn_reflns_av_unetI/netI     0.0619
_diffrn_reflns_Laue_measured_fraction_full 0.997
_diffrn_reflns_Laue_measured_fraction_max 0.996
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       34
_diffrn_reflns_limit_k_min       -35
_diffrn_reflns_limit_l_max       12
_diffrn_reflns_limit_l_min       -12
_diffrn_reflns_number            23569
_diffrn_reflns_point_group_measured_fraction_full 0.997
_diffrn_reflns_point_group_measured_fraction_max 0.996
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         27.902
_diffrn_reflns_theta_min         2.914
_diffrn_ambient_temperature      113(2)
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type  'rigaku saturn'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                4731
_reflns_number_total             5725
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       crystalclear
_computing_data_collection       crystalclear
_computing_data_reduction        crystalclear
_computing_molecular_graphics    'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2019/2 (Sheldrick, 2015)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_refine_diff_density_max         0.263
_refine_diff_density_min         -0.186
_refine_diff_density_rms         0.047
_refine_ls_extinction_coef       0.0074(14)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     'SHELXL-2019/2 (Sheldrick 2019)'
_refine_ls_goodness_of_fit_ref   1.127
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     319
_refine_ls_number_reflns         5725
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0784
_refine_ls_R_factor_gt           0.0634
_refine_ls_restrained_S_all      1.127
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0558P)²+0.4705P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1373
_refine_ls_wR_factor_ref         0.1465
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups
 At 1.5 times of:
  All C(H,H,H) groups
2.a Aromatic/amide H refined with riding coordinates:
 C3(H3), C4(H4), C5(H5), C6(H6), C10(H10), C11(H11), C12(H12), C13(H13),
 C20(H20), C21(H21), C24(H24), C25(H25), C26(H26), C27(H27), C28(H28), C30(H30),
  C31(H31), C32(H32), C33(H33), C34(H34)
2.b Idealised Me refined as rotating group:
 C18(H18A,H18B,H18C), C19(H19A,H19B,H19C)
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
O1 O 0.49657(11) 0.62493(4) 0.56151(12) 0.0287(3) Uani 1 1 d . . . . .
C1 C 0.62759(16) 0.54561(6) 0.75297(17) 0.0264(3) Uani 1 1 d . . . . .
C2 C 0.72411(16) 0.52665(6) 0.88320(18) 0.0286(4) Uani 1 1 d . . . . .
C3 C 0.74435(17) 0.47725(6) 0.9275(2) 0.0341(4) Uani 1 1 d . . . . .
H3 H 0.700265 0.450672 0.870620 0.041 Uiso 1 1 calc R U . . .
C4 C 0.82964(18) 0.46689(7) 1.0559(2) 0.0391(4) Uani 1 1 d . . . . .
H4 H 0.843897 0.433127 1.087271 0.047 Uiso 1 1 calc R U . . .
C5 C 0.89390(19) 0.50583(7) 1.1380(2) 0.0394(4) Uani 1 1 d . . . . .
H5 H 0.950540 0.498460 1.226544 0.047 Uiso 1 1 calc R U . . .
C6 C 0.87706(18) 0.55555(7) 1.09323(19) 0.0353(4) Uani 1 1 d . . . . .
H6 H 0.922499 0.581904 1.150054 0.042 Uiso 1 1 calc R U . . .
C7 C 0.79234(15) 0.56621(6) 0.96345(17) 0.0276(3) Uani 1 1 d . . . . .
C8 C 0.74894(15) 0.61362(6) 0.88707(17) 0.0258(3) Uani 1 1 d . . . . .
C9 C 0.78961(16) 0.66469(6) 0.91827(17) 0.0277(3) Uani 1 1 d . . . . .
C10 C 0.89498(18) 0.67898(7) 1.03190(19) 0.0348(4) Uani 1 1 d . . . . .
H10 H 0.940582 0.653854 1.093394 0.042 Uiso 1 1 calc R U . . .
C11 C 0.93236(19) 0.72818(7) 1.0549(2) 0.0415(4) Uani 1 1 d . . . . .
H11 H 1.003624 0.736832 1.131531 0.050 Uiso 1 1 calc R U . . .
C12 C 0.86621(19) 0.76590(7) 0.9660(2) 0.0413(4) Uani 1 1 d . . . . .
H12 H 0.892951 0.800016 0.982293 0.050 Uiso 1 1 calc R U . . .
C13 C 0.76313(18) 0.75368(6) 0.8558(2) 0.0354(4) Uani 1 1 d . . . . .
H13 H 0.718208 0.779655 0.797065 0.042 Uiso 1 1 calc R U . . .
C14 C 0.72192(16) 0.70323(6) 0.82729(17) 0.0277(3) Uani 1 1 d . . . . .
C15 C 0.61740(16) 0.69042(6) 0.70877(17) 0.0267(3) Uani 1 1 d . . . . .
C16 C 0.58692(15) 0.64023(6) 0.67972(16) 0.0241(3) Uani 1 1 d . . . . .
C17 C 0.65220(15) 0.60201(6) 0.76829(17) 0.0245(3) Uani 1 1 d . . . . .
C18 C 0.66951(18) 0.52485(6) 0.61382(19) 0.0336(4) Uani 1 1 d . . . . .
H18A H 0.768510 0.532406 0.610842 0.050 Uiso 1 1 calc R U . . .
H18B H 0.611398 0.540525 0.531812 0.050 Uiso 1 1 calc R U . . .
H18C H 0.655355 0.488378 0.610127 0.050 Uiso 1 1 calc R U . . .
C19 C 0.47413(17) 0.53166(7) 0.7638(2) 0.0346(4) Uani 1 1 d . . . . .
H19A H 0.463681 0.495032 0.761131 0.052 Uiso 1 1 calc R U . . .
H19B H 0.411802 0.546547 0.683392 0.052 Uiso 1 1 calc R U . . .
H19C H 0.449501 0.544556 0.853763 0.052 Uiso 1 1 calc R U . . .
C20 C 0.53959(17) 0.72739(6) 0.61533(18) 0.0316(4) Uani 1 1 d . . . . .
H20 H 0.563957 0.761918 0.625893 0.038 Uiso 1 1 calc R U . . .
C21 C 0.43502(17) 0.71353(6) 0.51554(18) 0.0318(4) Uani 1 1 d . . . . .
H21 H 0.383695 0.738972 0.459905 0.038 Uiso 1 1 calc R U . . .
C22 C 0.39343(16) 0.65963(6) 0.48584(17) 0.0270(3) Uani 1 1 d . . . . .
C23 C 0.39489(16) 0.65066(6) 0.32677(17) 0.0263(3) Uani 1 1 d . . . . .
C24 C 0.51009(17) 0.62898(6) 0.27773(19) 0.0317(4) Uani 1 1 d . . . . .
H24 H 0.585925 0.616500 0.344172 0.038 Uiso 1 1 calc R U . . .
C25 C 0.5148(2) 0.62548(7) 0.1323(2) 0.0381(4) Uani 1 1 d . . . . .
H25 H 0.593418 0.610284 0.099951 0.046 Uiso 1 1 calc R U . . .
C26 C 0.4061(2) 0.64388(7) 0.0341(2) 0.0389(4) Uani 1 1 d . . . . .
H26 H 0.410412 0.641718 -0.065285 0.047 Uiso 1 1 calc R U . . .
C27 C 0.29097(19) 0.66551(7) 0.08181(19) 0.0360(4) Uani 1 1 d . . . . .
H27 H 0.215693 0.678075 0.014857 0.043 Uiso 1 1 calc R U . . .
C28 C 0.28521(17) 0.66886(6) 0.22668(18) 0.0307(4) Uani 1 1 d . . . . .
H28 H 0.205744 0.683718 0.258386 0.037 Uiso 1 1 calc R U . . .
C29 C 0.25343(16) 0.64610(6) 0.53561(17) 0.0287(4) Uani 1 1 d . . . . .
C30 C 0.20998(18) 0.67116(7) 0.64993(18) 0.0351(4) Uani 1 1 d . . . . .
H30 H 0.263239 0.698707 0.692693 0.042 Uiso 1 1 calc R U . . .
C31 C 0.08896(19) 0.65625(8) 0.70240(19) 0.0415(5) Uani 1 1 d . . . . .
H31 H 0.060292 0.673730 0.780610 0.050 Uiso 1 1 calc R U . . .
C32 C 0.0105(2) 0.61640(8) 0.6418(2) 0.0437(5) Uani 1 1 d . . . . .
H32 H -0.071661 0.606232 0.678296 0.052 Uiso 1 1 calc R U . . .
C33 C 0.0524(2) 0.59125(7) 0.5274(2) 0.0437(5) Uani 1 1 d . . . . .
H33 H -0.001600 0.563885 0.484609 0.052 Uiso 1 1 calc R U . . .
C34 C 0.17336(18) 0.60591(6) 0.4748(2) 0.0361(4) Uani 1 1 d . . . . .
H34 H 0.201601 0.588331 0.396523 0.043 Uiso 1 1 calc R U . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
O1 C16 1.3728(18) . ?
O1 C22 1.4633(18) . ?
C1 C2 1.515(2) . ?
C1 C17 1.523(2) . ?
C1 C18 1.538(2) . ?
C1 C19 1.544(2) . ?
C2 C3 1.385(2) . ?
C2 C7 1.403(2) . ?
C3 H3 0.9500 . ?
C3 C4 1.389(2) . ?
C4 H4 0.9500 . ?
C4 C5 1.385(3) . ?
C5 H5 0.9500 . ?
C5 C6 1.391(3) . ?
C6 H6 0.9500 . ?
C6 C7 1.399(2) . ?
C7 C8 1.483(2) . ?
C8 C9 1.433(2) . ?
C8 C17 1.384(2) . ?
C9 C10 1.416(2) . ?
C9 C14 1.432(2) . ?
C10 H10 0.9500 . ?
C10 C11 1.367(3) . ?
C11 H11 0.9500 . ?
C11 C12 1.401(3) . ?
C12 H12 0.9500 . ?
C12 C13 1.368(3) . ?
C13 H13 0.9500 . ?
C13 C14 1.414(2) . ?
C14 C15 1.432(2) . ?
C15 C16 1.386(2) . ?
C15 C20 1.454(2) . ?
C16 C17 1.406(2) . ?
C18 H18A 0.9800 . ?
C18 H18B 0.9800 . ?
C18 H18C 0.9800 . ?
C19 H19A 0.9800 . ?
C19 H19B 0.9800 . ?
C19 H19C 0.9800 . ?
C20 H20 0.9500 . ?
C20 C21 1.326(2) . ?
C21 H21 0.9500 . ?
C21 C22 1.504(2) . ?
C22 C23 1.527(2) . ?
C22 C29 1.538(2) . ?
C23 C24 1.392(2) . ?
C23 C28 1.397(2) . ?
C24 H24 0.9500 . ?
C24 C25 1.387(2) . ?
C25 H25 0.9500 . ?
C25 C26 1.381(3) . ?
C26 H26 0.9500 . ?
C26 C27 1.385(3) . ?
C27 H27 0.9500 . ?
C27 C28 1.384(2) . ?
C28 H28 0.9500 . ?
C29 C30 1.389(2) . ?
C29 C34 1.392(2) . ?
C30 H30 0.9500 . ?
C30 C31 1.393(3) . ?
C31 H31 0.9500 . ?
C31 C32 1.377(3) . ?
C32 H32 0.9500 . ?
C32 C33 1.385(3) . ?
C33 H33 0.9500 . ?
C33 C34 1.391(2) . ?
C34 H34 0.9500 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C16 O1 C22 120.89(12) . . ?
C2 C1 C17 100.53(13) . . ?
C2 C1 C18 111.67(13) . . ?
C2 C1 C19 110.09(13) . . ?
C17 C1 C18 112.24(13) . . ?
C17 C1 C19 111.58(13) . . ?
C18 C1 C19 110.39(14) . . ?
C3 C2 C1 127.16(15) . . ?
C3 C2 C7 120.99(16) . . ?
C7 C2 C1 111.81(14) . . ?
C2 C3 H3 120.3 . . ?
C2 C3 C4 119.44(17) . . ?
C4 C3 H3 120.3 . . ?
C3 C4 H4 120.0 . . ?
C5 C4 C3 119.93(17) . . ?
C5 C4 H4 120.0 . . ?
C4 C5 H5 119.4 . . ?
C4 C5 C6 121.25(17) . . ?
C6 C5 H5 119.4 . . ?
C5 C6 H6 120.4 . . ?
C5 C6 C7 119.10(17) . . ?
C7 C6 H6 120.4 . . ?
C2 C7 C8 107.42(14) . . ?
C6 C7 C2 119.22(15) . . ?
C6 C7 C8 133.29(16) . . ?
C9 C8 C7 131.15(15) . . ?
C17 C8 C7 108.21(14) . . ?
C17 C8 C9 120.63(14) . . ?
C10 C9 C8 123.64(15) . . ?
C10 C9 C14 118.35(15) . . ?
C14 C9 C8 117.99(14) . . ?
C9 C10 H10 119.3 . . ?
C11 C10 C9 121.33(17) . . ?
C11 C10 H10 119.3 . . ?
C10 C11 H11 119.8 . . ?
C10 C11 C12 120.38(17) . . ?
C12 C11 H11 119.8 . . ?
C11 C12 H12 120.0 . . ?
C13 C12 C11 120.06(17) . . ?
C13 C12 H12 120.0 . . ?
C12 C13 H13 119.3 . . ?
C12 C13 C14 121.50(17) . . ?
C14 C13 H13 119.3 . . ?
C9 C14 C15 120.28(14) . . ?
C13 C14 C9 118.38(15) . . ?
C13 C14 C15 121.33(15) . . ?
C14 C15 C20 123.62(14) . . ?
C16 C15 C14 119.22(14) . . ?
C16 C15 C20 117.16(14) . . ?
O1 C16 C15 122.49(14) . . ?
O1 C16 C17 116.38(13) . . ?
C15 C16 C17 121.08(14) . . ?
C8 C17 C1 111.96(13) . . ?
C8 C17 C16 120.66(14) . . ?
C16 C17 C1 127.37(14) . . ?
C1 C18 H18A 109.5 . . ?
C1 C18 H18B 109.5 . . ?
C1 C18 H18C 109.5 . . ?
H18A C18 H18B 109.5 . . ?
H18A C18 H18C 109.5 . . ?
H18B C18 H18C 109.5 . . ?
C1 C19 H19A 109.5 . . ?
C1 C19 H19B 109.5 . . ?
C1 C19 H19C 109.5 . . ?
H19A C19 H19B 109.5 . . ?
H19A C19 H19C 109.5 . . ?
H19B C19 H19C 109.5 . . ?
C15 C20 H20 119.6 . . ?
C21 C20 C15 120.86(15) . . ?
C21 C20 H20 119.6 . . ?
C20 C21 H21 118.3 . . ?
C20 C21 C22 123.44(15) . . ?
C22 C21 H21 118.3 . . ?
O1 C22 C21 111.57(13) . . ?
O1 C22 C23 106.14(12) . . ?
O1 C22 C29 105.39(12) . . ?
C21 C22 C23 106.96(13) . . ?
C21 C22 C29 112.81(13) . . ?
C23 C22 C29 113.84(13) . . ?
C24 C23 C22 121.32(14) . . ?
C24 C23 C28 118.58(15) . . ?
C28 C23 C22 119.80(14) . . ?
C23 C24 H24 119.8 . . ?
C25 C24 C23 120.34(16) . . ?
C25 C24 H24 119.8 . . ?
C24 C25 H25 119.7 . . ?
C26 C25 C24 120.66(17) . . ?
C26 C25 H25 119.7 . . ?
C25 C26 H26 120.3 . . ?
C25 C26 C27 119.45(17) . . ?
C27 C26 H26 120.3 . . ?
C26 C27 H27 119.9 . . ?
C28 C27 C26 120.22(17) . . ?
C28 C27 H27 119.9 . . ?
C23 C28 H28 119.6 . . ?
C27 C28 C23 120.74(16) . . ?
C27 C28 H28 119.6 . . ?
C30 C29 C22 120.51(15) . . ?
C30 C29 C34 118.56(16) . . ?
C34 C29 C22 120.72(14) . . ?
C29 C30 H30 119.7 . . ?
C29 C30 C31 120.54(18) . . ?
C31 C30 H30 119.7 . . ?
C30 C31 H31 119.7 . . ?
C32 C31 C30 120.54(17) . . ?
C32 C31 H31 119.7 . . ?
C31 C32 H32 120.3 . . ?
C31 C32 C33 119.46(18) . . ?
C33 C32 H32 120.3 . . ?
C32 C33 H33 119.9 . . ?
C32 C33 C34 120.24(19) . . ?
C34 C33 H33 119.9 . . ?
C29 C34 H34 119.7 . . ?
C33 C34 C29 120.67(17) . . ?
C33 C34 H34 119.7 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
O1 C16 C17 C1 -4.0(2) . . . . ?
O1 C16 C17 C8 177.59(13) . . . . ?
O1 C22 C23 C24 -22.04(19) . . . . ?
O1 C22 C23 C28 164.37(13) . . . . ?
O1 C22 C29 C30 93.40(16) . . . . ?
O1 C22 C29 C34 -81.41(18) . . . . ?
C1 C2 C3 C4 -175.33(15) . . . . ?
C1 C2 C7 C6 175.09(14) . . . . ?
C1 C2 C7 C8 -2.31(17) . . . . ?
C2 C1 C17 C8 0.79(16) . . . . ?
C2 C1 C17 C16 -177.78(14) . . . . ?
C2 C3 C4 C5 -0.2(3) . . . . ?
C2 C7 C8 C9 -177.76(15) . . . . ?
C2 C7 C8 C17 2.76(17) . . . . ?
C3 C2 C7 C6 -2.8(2) . . . . ?
C3 C2 C7 C8 179.76(14) . . . . ?
C3 C4 C5 C6 -1.3(3) . . . . ?
C4 C5 C6 C7 0.7(3) . . . . ?
C5 C6 C7 C2 1.4(2) . . . . ?
C5 C6 C7 C8 177.94(16) . . . . ?
C6 C7 C8 C9 5.4(3) . . . . ?
C6 C7 C8 C17 -174.12(17) . . . . ?
C7 C2 C3 C4 2.3(2) . . . . ?
C7 C8 C9 C10 5.2(3) . . . . ?
C7 C8 C9 C14 -176.28(15) . . . . ?
C7 C8 C17 C1 -2.18(17) . . . . ?
C7 C8 C17 C16 176.49(13) . . . . ?
C8 C9 C10 C11 178.30(16) . . . . ?
C8 C9 C14 C13 -178.92(14) . . . . ?
C8 C9 C14 C15 -0.3(2) . . . . ?
C9 C8 C17 C1 178.27(13) . . . . ?
C9 C8 C17 C16 -3.1(2) . . . . ?
C9 C10 C11 C12 0.3(3) . . . . ?
C9 C14 C15 C16 -2.7(2) . . . . ?
C9 C14 C15 C20 177.20(14) . . . . ?
C10 C9 C14 C13 -0.3(2) . . . . ?
C10 C9 C14 C15 178.34(15) . . . . ?
C10 C11 C12 C13 0.3(3) . . . . ?
C11 C12 C13 C14 -0.8(3) . . . . ?
C12 C13 C14 C9 0.8(3) . . . . ?
C12 C13 C14 C15 -177.79(17) . . . . ?
C13 C14 C15 C16 175.90(15) . . . . ?
C13 C14 C15 C20 -4.2(2) . . . . ?
C14 C9 C10 C11 -0.2(3) . . . . ?
C14 C15 C16 O1 -174.58(13) . . . . ?
C14 C15 C16 C17 2.9(2) . . . . ?
C14 C15 C20 C21 -173.66(16) . . . . ?
C15 C16 C17 C1 178.41(14) . . . . ?
C15 C16 C17 C8 0.0(2) . . . . ?
C15 C20 C21 C22 -3.2(3) . . . . ?
C16 O1 C22 C21 21.47(19) . . . . ?
C16 O1 C22 C23 137.63(13) . . . . ?
C16 O1 C22 C29 -101.30(15) . . . . ?
C16 C15 C20 C21 6.2(2) . . . . ?
C17 C1 C2 C3 178.78(15) . . . . ?
C17 C1 C2 C7 1.01(16) . . . . ?
C17 C8 C9 C10 -175.39(15) . . . . ?
C17 C8 C9 C14 3.2(2) . . . . ?
C18 C1 C2 C3 -62.0(2) . . . . ?
C18 C1 C2 C7 120.23(15) . . . . ?
C18 C1 C17 C8 -118.01(15) . . . . ?
C18 C1 C17 C16 63.4(2) . . . . ?
C19 C1 C2 C3 61.0(2) . . . . ?
C19 C1 C2 C7 -116.78(15) . . . . ?
C19 C1 C17 C8 117.48(15) . . . . ?
C19 C1 C17 C16 -61.1(2) . . . . ?
C20 C15 C16 O1 5.5(2) . . . . ?
C20 C15 C16 C17 -177.00(14) . . . . ?
C20 C21 C22 O1 -10.1(2) . . . . ?
C20 C21 C22 C23 -125.78(17) . . . . ?
C20 C21 C22 C29 108.30(19) . . . . ?
C21 C22 C23 C24 97.20(17) . . . . ?
C21 C22 C23 C28 -76.39(17) . . . . ?
C21 C22 C29 C30 -28.6(2) . . . . ?
C21 C22 C29 C34 156.62(15) . . . . ?
C22 O1 C16 C15 -20.4(2) . . . . ?
C22 O1 C16 C17 162.03(13) . . . . ?
C22 C23 C24 C25 -173.92(15) . . . . ?
C22 C23 C28 C27 173.65(15) . . . . ?
C22 C29 C30 C31 -174.81(15) . . . . ?
C22 C29 C34 C33 174.94(16) . . . . ?
C23 C22 C29 C30 -150.70(15) . . . . ?
C23 C22 C29 C34 34.5(2) . . . . ?
C23 C24 C25 C26 0.7(3) . . . . ?
C24 C23 C28 C27 -0.1(2) . . . . ?
C24 C25 C26 C27 -0.7(3) . . . . ?
C25 C26 C27 C28 0.3(3) . . . . ?
C26 C27 C28 C23 0.1(3) . . . . ?
C28 C23 C24 C25 -0.3(2) . . . . ?
C29 C22 C23 C24 -137.50(15) . . . . ?
C29 C22 C23 C28 48.91(19) . . . . ?
C29 C30 C31 C32 0.1(3) . . . . ?
C30 C29 C34 C33 0.0(3) . . . . ?
C30 C31 C32 C33 -0.4(3) . . . . ?
C31 C32 C33 C34 0.5(3) . . . . ?
C32 C33 C34 C29 -0.3(3) . . . . ?
C34 C29 C30 C31 0.1(2) . . . . ?

_olex2_submission_special_instructions 'No special instructions were received'
