# Electronic Supplementary Material (ESI) for Dalton Transactions.
# This journal is © The Royal Society of Chemistry 2024

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_1_a
_database_code_depnum_ccdc_archive 'CCDC 2350961'
loop_
_audit_author_name
_audit_author_address
'Sujuan Yu'
;Tianjin University of Technology
China
;
_audit_update_record             
;
2024-06-25 deposited with the CCDC.	2024-06-28 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2018/3
_shelx_SHELXL_version_number     2018/3
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         'B4 Li3 Na7 O26 P6'
_chemical_formula_sum            'B4 Li3 Na7 O26 P6'
_chemical_formula_weight         826.81

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Li Li -0.0003 0.0001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      orthorhombic
_space_group_IT_number           29
_space_group_name_H-M_alt        'P c a 21'
_space_group_name_Hall           'P 2c -2ac'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, z+1/2'
'x+1/2, -y, z'
'-x+1/2, y, z+1/2'

_cell_length_a                   6.6568(6)
_cell_length_b                   13.6358(12)
_cell_length_c                   11.3226(12)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_volume                     1027.76(17)
_cell_formula_units_Z            2
_cell_measurement_temperature    298(2)
_cell_measurement_reflns_used    1258
_cell_measurement_theta_min      0.865
_cell_measurement_theta_max      0.893

_exptl_crystal_description       Block
_exptl_crystal_colour            colourless
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    2.672
_exptl_crystal_F_000             808
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          0.18
_exptl_crystal_size_mid          0.16
_exptl_crystal_size_min          0.14
_exptl_absorpt_coefficient_mu    0.808
_shelx_estimated_absorpt_T_min   ?
_shelx_estimated_absorpt_T_max   ?
_exptl_absorpt_correction_type   ?
_exptl_absorpt_correction_T_min  ?
_exptl_absorpt_correction_T_max  ?
_exptl_absorpt_process_details   ?
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      298(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_source                   ?
_diffrn_measurement_device_type  'Bruker APEX-III CCD'
_diffrn_measurement_method       ?
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            4692
_diffrn_reflns_av_unetI/netI     0.0771
_diffrn_reflns_av_R_equivalents  0.0588
_diffrn_reflns_limit_h_min       -6
_diffrn_reflns_limit_h_max       7
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_l_min       -13
_diffrn_reflns_limit_l_max       13
_diffrn_reflns_theta_min         2.988
_diffrn_reflns_theta_max         24.701
_diffrn_reflns_theta_full        24.701
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measured_fraction_theta_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 0.999
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 0.999
_diffrn_reflns_point_group_measured_fraction_full 1.001
_reflns_number_total             1732
_reflns_number_gt                1293
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.888
_reflns_Friedel_fraction_max     1.000
_reflns_Friedel_fraction_full    1.001

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences. Completness statistics refer to single and
 composite reflections containing twin component 1 only.
;

_computing_data_collection       'Bruker SMART'
_computing_cell_refinement       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_refine_special_details          
;
 Refined as a 2-component perfect inversion twin.
;
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0291P)²+1.4245P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   .
_refine_ls_hydrogen_treatment    undef
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_abs_structure_details 
;
 Refined as a perfect inversion twin.
;
_refine_ls_abs_structure_Flack   0.5
_chemical_absolute_configuration ?
_refine_ls_number_reflns         1732
_refine_ls_number_parameters     211
_refine_ls_number_restraints     34
_refine_ls_R_factor_all          0.0773
_refine_ls_R_factor_gt           0.0500
_refine_ls_wR_factor_ref         0.1072
_refine_ls_wR_factor_gt          0.0926
_refine_ls_goodness_of_fit_ref   1.045
_refine_ls_restrained_S_all      1.038
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
P1 P 0.2690(4) 0.74935(18) 0.5600(3) 0.0143(7) Uani 1 1 d . . . . .
Na1 Na 0.8404(15) 0.7508(7) 0.6694(9) 0.030(3) Uani 0.5 1 d D . P . .
Li2 Li 0.227(3) 0.8790(11) 0.801(2) 0.018(4) Uani 1 1 d . U . . .
P2 P 0.7599(4) 0.60206(17) 0.3349(3) 0.0160(8) Uani 1 1 d . . . . .
P3 P 0.7638(4) 0.91888(17) 0.3213(3) 0.0149(7) Uani 1 1 d . . . . .
Na2 Na 0.2281(7) 0.6136(3) 0.8018(5) 0.0246(12) Uani 1 1 d . . . . .
Na3 Na 1.0395(6) 0.4944(3) 0.5731(5) 0.0298(12) Uani 1 1 d . . . . .
Na4 Na 1.0261(7) 1.0039(5) 0.5633(6) 0.0534(16) Uani 1 1 d . . . . .
O1 O 0.8300(11) 0.7663(5) 0.4840(7) 0.0134(17) Uani 1 1 d D U . . .
O2 O 0.9587(9) 0.8522(5) 0.3155(8) 0.0166(18) Uani 1 1 d . . . . .
O3 O 1.1855(10) 0.7615(5) 0.4314(7) 0.0136(16) Uani 1 1 d . U . . .
O4 O 0.9417(9) 0.6759(5) 0.3137(8) 0.0149(17) Uani 1 1 d . U . . .
O5 O 0.4943(9) 0.7775(5) 0.5435(7) 0.0191(19) Uani 1 1 d D . . . .
O6 O 0.7842(11) 0.9976(5) 0.4135(7) 0.020(2) Uani 1 1 d . . . . .
O7 O 0.5924(11) 0.8438(5) 0.3547(7) 0.019(2) Uani 1 1 d . . . . .
O8 O 0.8085(12) 0.5283(5) 0.4268(8) 0.023(2) Uani 1 1 d . . . . .
O9 O 0.5834(11) 0.6710(5) 0.3779(7) 0.021(2) Uani 1 1 d . . . . .
O10 O 0.7015(10) 0.5590(5) 0.2184(8) 0.023(2) Uani 1 1 d . . . . .
O11 O 0.1765(11) 0.8243(6) 0.6417(8) 0.035(2) Uani 1 1 d . . . . .
O12 O 0.2445(12) 0.6458(5) 0.5994(8) 0.039(2) Uani 1 1 d . . . . .
O13 O 0.7218(11) 0.9566(6) 0.2002(8) 0.028(2) Uani 1 1 d . . . . .
B1 B 0.6277(19) 0.7636(9) 0.4435(13) 0.021(3) Uani 1 1 d D . . . .
B2 B 0.972(2) 0.7638(10) 0.3924(12) 0.019(3) Uani 1 1 d . U . . .
Li1A Li 0.854(5) 0.794(4) 0.663(2) 0.030(3) Uani 0.5 1 d D . P . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
P1 O12 1.490(8) . ?
P1 O11 1.510(9) . ?
P1 O5 1.560(7) . ?
P1 O3 1.567(9) 1_455 ?
P1 Li1A 3.06(4) 1_455 ?
P1 Na1 3.110(11) 1_455 ?
P1 Na2 3.316(6) . ?
Na1 Li1A 0.60(5) . ?
Na1 O1 2.110(11) . ?
Na1 O11 2.472(13) 1_655 ?
Na1 O7 2.492(13) 4_655 ?
Na1 O9 2.649(13) 4_655 ?
Na1 O10 2.689(12) 4_655 ?
Na1 O4 2.691(13) 4_655 ?
Na1 O5 2.733(12) . ?
Na1 P2 2.842(10) 4_655 ?
Na1 O13 2.858(13) 4_655 ?
Na1 B1 2.928(17) . ?
Na1 O2 2.935(13) 4_655 ?
Li2 O11 1.98(2) . ?
Li2 O6 2.11(2) 2_675 ?
Li2 O2 2.129(19) 4_655 ?
Li2 O3 2.26(2) 4_655 ?
Li2 O7 2.27(2) 4 ?
Li2 O13 2.536(19) 2_675 ?
Li2 B2 2.75(2) 4_655 ?
Li2 P3 2.767(16) 2_675 ?
Li2 Li1A 3.15(3) 1_455 ?
Li2 Na4 3.45(2) 1_455 ?
Li2 Na2 3.619(16) . ?
P2 O8 1.483(8) . ?
P2 O10 1.496(9) . ?
P2 O9 1.582(8) . ?
P2 O4 1.593(7) . ?
P2 Na2 2.965(4) 2_664 ?
P2 Na2 3.274(6) 4_554 ?
P2 Na3 3.340(7) 3_465 ?
P2 Na2 3.432(6) 4_654 ?
P3 O13 1.491(9) . ?
P3 O6 1.503(8) . ?
P3 O7 1.579(8) . ?
P3 O2 1.586(7) . ?
P3 Li1A 2.59(4) 4_654 ?
P3 Na4 3.335(7) 3_475 ?
P3 Na4 3.406(8) 2_774 ?
P3 Na4 3.449(7) . ?
Na2 O12 2.337(10) . ?
Na2 O4 2.361(7) 4_655 ?
Na2 O9 2.378(8) 4 ?
Na2 O8 2.410(9) 2_665 ?
Na2 O3 2.560(8) 4_655 ?
Na2 O10 2.579(8) 2_665 ?
Na2 B2 3.039(14) 4_655 ?
Na2 Na3 3.305(7) 1_455 ?
Na3 O8 2.307(9) . ?
Na3 O8 2.459(10) 3_565 ?
Na3 O10 2.460(9) 4_655 ?
Na3 O10 2.492(9) 2_765 ?
Na3 O12 2.493(8) 1_655 ?
Na3 O12 2.756(10) 3_565 ?
Na3 Na3 3.3319(5) 3_465 ?
Na3 Na3 3.3320(5) 3_565 ?
Na4 O6 2.341(10) . ?
Na4 O13 2.347(11) 2_775 ?
Na4 O13 2.354(10) 4_655 ?
Na4 O6 2.415(10) 3_575 ?
Na4 O11 2.790(11) 1_655 ?
Na4 O5 2.996(10) 3_575 ?
Na4 Li1A 3.28(5) . ?
Na4 Na4 3.3301(6) 3_475 ?
Na4 Na4 3.3301(6) 3_575 ?
O1 B2 1.403(15) . ?
O1 B1 1.423(14) . ?
O1 Li1A 2.07(3) . ?
O2 B2 1.490(15) . ?
O3 B2 1.491(15) . ?
O4 B2 1.505(15) . ?
O5 B1 1.452(16) . ?
O7 B1 1.504(16) . ?
O7 Li1A 2.30(3) 4_654 ?
O9 B1 1.494(14) . ?
O11 Li1A 2.20(4) 1_455 ?
O13 Li1A 2.31(5) 4_654 ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O12 P1 O11 114.5(6) . . ?
O12 P1 O5 112.0(4) . . ?
O11 P1 O5 107.4(4) . . ?
O12 P1 O3 109.8(5) . 1_455 ?
O11 P1 O3 110.7(5) . 1_455 ?
O5 P1 O3 101.7(5) . 1_455 ?
O12 P1 Li1A 88.7(10) . 1_455 ?
O11 P1 Li1A 42.5(7) . 1_455 ?
O5 P1 Li1A 149.8(8) . 1_455 ?
O3 P1 Li1A 90.8(5) 1_455 1_455 ?
O12 P1 Na1 77.7(4) . 1_455 ?
O11 P1 Na1 51.5(4) . 1_455 ?
O5 P1 Na1 158.2(4) . 1_455 ?
O3 P1 Na1 92.5(3) 1_455 1_455 ?
Li1A P1 Na1 11.2(9) 1_455 1_455 ?
O12 P1 Na2 38.3(4) . . ?
O11 P1 Na2 80.7(4) . . ?
O5 P1 Na2 108.4(4) . . ?
O3 P1 Na2 142.8(3) 1_455 . ?
Li1A P1 Na2 73.9(8) 1_455 . ?
Na1 P1 Na2 66.4(2) 1_455 . ?
Li1A Na1 O1 78(2) . . ?
Li1A Na1 O11 57(4) . 1_655 ?
O1 Na1 O11 82.2(5) . 1_655 ?
Li1A Na1 O7 64(2) . 4_655 ?
O1 Na1 O7 142.4(5) . 4_655 ?
O11 Na1 O7 74.8(4) 1_655 4_655 ?
Li1A Na1 O9 118(2) . 4_655 ?
O1 Na1 O9 159.0(6) . 4_655 ?
O11 Na1 O9 96.1(4) 1_655 4_655 ?
O7 Na1 O9 54.8(3) 4_655 4_655 ?
Li1A Na1 O10 174(2) . 4_655 ?
O1 Na1 O10 107.4(5) . 4_655 ?
O11 Na1 O10 121.0(5) 1_655 4_655 ?
O7 Na1 O10 109.8(4) 4_655 4_655 ?
O9 Na1 O10 55.7(3) 4_655 4_655 ?
Li1A Na1 O4 123(4) . 4_655 ?
O1 Na1 O4 128.2(5) . 4_655 ?
O11 Na1 O4 149.6(5) 1_655 4_655 ?
O7 Na1 O4 78.9(4) 4_655 4_655 ?
O9 Na1 O4 55.7(3) 4_655 4_655 ?
O10 Na1 O4 55.5(3) 4_655 4_655 ?
Li1A Na1 O5 86(3) . . ?
O1 Na1 O5 56.0(4) . . ?
O11 Na1 O5 130.0(5) 1_655 . ?
O7 Na1 O5 121.5(5) 4_655 . ?
O9 Na1 O5 132.9(5) 4_655 . ?
O10 Na1 O5 98.6(4) 4_655 . ?
O4 Na1 O5 77.2(3) 4_655 . ?
Li1A Na1 P2 144(3) . 4_655 ?
O1 Na1 P2 136.0(5) . 4_655 ?
O11 Na1 P2 125.8(4) 1_655 4_655 ?
O7 Na1 P2 81.4(3) 4_655 4_655 ?
O9 Na1 P2 33.2(2) 4_655 4_655 ?
O10 Na1 P2 31.2(2) 4_655 4_655 ?
O4 Na1 P2 33.33(19) 4_655 4_655 ?
O5 Na1 P2 103.9(4) . 4_655 ?
Li1A Na1 O13 22(4) . 4_655 ?
O1 Na1 O13 91.1(4) . 4_655 ?
O11 Na1 O13 75.4(4) 1_655 4_655 ?
O7 Na1 O13 54.8(3) 4_655 4_655 ?
O9 Na1 O13 108.8(4) 4_655 4_655 ?
O10 Na1 O13 156.2(5) 4_655 4_655 ?
O4 Na1 O13 101.4(4) 4_655 4_655 ?
O5 Na1 O13 79.1(3) . 4_655 ?
P2 Na1 O13 125.9(4) 4_655 4_655 ?
Li1A Na1 B1 85.2(19) . . ?
O1 Na1 B1 27.1(4) . . ?
O11 Na1 B1 107.6(5) 1_655 . ?
O7 Na1 B1 142.4(5) 4_655 . ?
O9 Na1 B1 153.6(5) 4_655 . ?
O10 Na1 B1 100.8(4) 4_655 . ?
O4 Na1 B1 102.5(4) 4_655 . ?
O5 Na1 B1 29.5(3) . . ?
P2 Na1 B1 120.3(4) 4_655 . ?
O13 Na1 B1 88.8(4) 4_655 . ?
Li1A Na1 O2 73(4) . 4_655 ?
O1 Na1 O2 119.4(5) . 4_655 ?
O11 Na1 O2 119.6(4) 1_655 4_655 ?
O7 Na1 O2 53.7(3) 4_655 4_655 ?
O9 Na1 O2 79.7(4) 4_655 4_655 ?
O10 Na1 O2 105.8(4) 4_655 4_655 ?
O4 Na1 O2 50.4(3) 4_655 4_655 ?
O5 Na1 O2 70.1(3) . 4_655 ?
P2 Na1 O2 78.8(3) 4_655 4_655 ?
O13 Na1 O2 51.0(3) 4_655 4_655 ?
B1 Na1 O2 97.8(4) . 4_655 ?
O11 Li2 O6 147.6(10) . 2_675 ?
O11 Li2 O2 100.1(10) . 4_655 ?
O6 Li2 O2 97.1(8) 2_675 4_655 ?
O11 Li2 O3 112.0(8) . 4_655 ?
O6 Li2 O3 100.2(10) 2_675 4_655 ?
O2 Li2 O3 64.8(6) 4_655 4_655 ?
O11 Li2 O7 90.3(8) . 4 ?
O6 Li2 O7 88.3(8) 2_675 4 ?
O2 Li2 O7 149.8(10) 4_655 4 ?
O3 Li2 O7 85.0(7) 4_655 4 ?
O11 Li2 O13 87.0(9) . 2_675 ?
O6 Li2 O13 64.7(5) 2_675 2_675 ?
O2 Li2 O13 93.2(7) 4_655 2_675 ?
O3 Li2 O13 152.5(9) 4_655 2_675 ?
O7 Li2 O13 115.7(7) 4 2_675 ?
O11 Li2 B2 104.7(8) . 4_655 ?
O6 Li2 B2 104.6(9) 2_675 4_655 ?
O2 Li2 B2 32.5(4) 4_655 4_655 ?
O3 Li2 B2 32.8(4) 4_655 4_655 ?
O7 Li2 B2 117.5(8) 4 4_655 ?
O13 Li2 B2 125.2(7) 2_675 4_655 ?
O11 Li2 P3 117.2(9) . 2_675 ?
O6 Li2 P3 32.5(3) 2_675 2_675 ?
O2 Li2 P3 98.2(6) 4_655 2_675 ?
O3 Li2 P3 130.2(10) 4_655 2_675 ?
O7 Li2 P3 102.0(7) 4 2_675 ?
O13 Li2 P3 32.3(3) 2_675 2_675 ?
B2 Li2 P3 121.4(7) 4_655 2_675 ?
O11 Li2 Li1A 43.8(8) . 1_455 ?
O6 Li2 Li1A 124.1(11) 2_675 1_455 ?
O2 Li2 Li1A 138.7(12) 4_655 1_455 ?
O3 Li2 Li1A 105.4(10) 4_655 1_455 ?
O7 Li2 Li1A 46.7(8) 4 1_455 ?
O13 Li2 Li1A 102.0(11) 2_675 1_455 ?
B2 Li2 Li1A 123.5(11) 4_655 1_455 ?
P3 Li2 Li1A 115.1(10) 2_675 1_455 ?
O11 Li2 Na1 44.7(5) . 1_455 ?
O6 Li2 Na1 129.5(8) 2_675 1_455 ?
O2 Li2 Na1 132.9(8) 4_655 1_455 ?
O3 Li2 Na1 96.6(6) 4_655 1_455 ?
O7 Li2 Na1 46.2(4) 4 1_455 ?
O13 Li2 Na1 110.8(7) 2_675 1_455 ?
B2 Li2 Na1 114.7(6) 4_655 1_455 ?
P3 Li2 Na1 123.9(6) 2_675 1_455 ?
Li1A Li2 Na1 9.1(8) 1_455 1_455 ?
O11 Li2 Na4 53.9(6) . 1_455 ?
O6 Li2 Na4 93.7(6) 2_675 1_455 ?
O2 Li2 Na4 121.8(9) 4_655 1_455 ?
O3 Li2 Na4 163.9(8) 4_655 1_455 ?
O7 Li2 Na4 87.2(6) 4 1_455 ?
O13 Li2 Na4 42.8(4) 2_675 1_455 ?
B2 Li2 Na4 149.2(9) 4_655 1_455 ?
P3 Li2 Na4 65.3(4) 2_675 1_455 ?
Li1A Li2 Na4 59.4(9) 1_455 1_455 ?
Na1 Li2 Na4 68.0(4) 1_455 1_455 ?
O11 Li2 Na2 68.1(5) . . ?
O6 Li2 Na2 142.5(10) 2_675 . ?
O2 Li2 Na2 80.0(5) 4_655 . ?
O3 Li2 Na2 44.6(3) 4_655 . ?
O7 Li2 Na2 77.8(5) 4 . ?
O13 Li2 Na2 152.3(9) 2_675 . ?
B2 Li2 Na2 55.0(4) 4_655 . ?
P3 Li2 Na2 174.7(9) 2_675 . ?
Li1A Li2 Na2 68.7(9) 1_455 . ?
Na1 Li2 Na2 59.8(3) 1_455 . ?
Na4 Li2 Na2 119.8(6) 1_455 . ?
O8 P2 O10 114.2(4) . . ?
O8 P2 O9 110.4(5) . . ?
O10 P2 O9 108.2(5) . . ?
O8 P2 O4 111.6(5) . . ?
O10 P2 O4 108.3(5) . . ?
O9 P2 O4 103.6(3) . . ?
O8 P2 Na1 176.7(4) . 4_654 ?
O10 P2 Na1 68.7(4) . 4_654 ?
O9 P2 Na1 66.7(4) . 4_654 ?
O4 P2 Na1 68.1(3) . 4_654 ?
O8 P2 Na2 53.9(3) . 2_664 ?
O10 P2 Na2 60.4(3) . 2_664 ?
O9 P2 Na2 130.4(3) . 2_664 ?
O4 P2 Na2 126.0(3) . 2_664 ?
Na1 P2 Na2 129.1(3) 4_654 2_664 ?
O8 P2 Na2 109.2(4) . 4_554 ?
O10 P2 Na2 70.1(3) . 4_554 ?
O9 P2 Na2 43.1(3) . 4_554 ?
O4 P2 Na2 134.9(3) . 4_554 ?
Na1 P2 Na2 70.0(2) 4_654 4_554 ?
Na2 P2 Na2 93.43(14) 2_664 4_554 ?
O8 P2 Na3 42.5(3) . 3_465 ?
O10 P2 Na3 116.3(3) . 3_465 ?
O9 P2 Na3 70.1(3) . 3_465 ?
O4 P2 Na3 134.8(4) . 3_465 ?
Na1 P2 Na3 135.3(2) 4_654 3_465 ?
Na2 P2 Na3 73.94(15) 2_664 3_465 ?
Na2 P2 Na3 71.05(13) 4_554 3_465 ?
O8 P2 Na2 83.7(3) . 4_654 ?
O10 P2 Na2 100.4(3) . 4_654 ?
O9 P2 Na2 138.1(3) . 4_654 ?
O4 P2 Na2 36.9(2) . 4_654 ?
Na1 P2 Na2 97.4(2) 4_654 4_654 ?
Na2 P2 Na2 90.27(13) 2_664 4_654 ?
Na2 P2 Na2 166.1(2) 4_554 4_654 ?
Na3 P2 Na2 122.84(15) 3_465 4_654 ?
O13 P3 O6 114.1(5) . . ?
O13 P3 O7 108.0(5) . . ?
O6 P3 O7 111.3(5) . . ?
O13 P3 O2 108.2(5) . . ?
O6 P3 O2 111.4(5) . . ?
O7 P3 O2 103.3(4) . . ?
O13 P3 Li1A 62.3(10) . 4_654 ?
O6 P3 Li1A 167.4(8) . 4_654 ?
O7 P3 Li1A 61.4(7) . 4_654 ?
O2 P3 Li1A 80.9(9) . 4_654 ?
O13 P3 Li2 65.3(6) . 2_674 ?
O6 P3 Li2 49.1(6) . 2_674 ?
O7 P3 Li2 133.0(5) . 2_674 ?
O2 P3 Li2 123.4(5) . 2_674 ?
Li1A P3 Li2 127.0(11) 4_654 2_674 ?
O13 P3 Na1 71.8(4) . 4_654 ?
O6 P3 Na1 168.9(4) . 4_654 ?
O7 P3 Na1 57.7(4) . 4_654 ?
O2 P3 Na1 73.9(4) . 4_654 ?
Li1A P3 Na1 10.0(10) 4_654 4_654 ?
Li2 P3 Na1 136.9(6) 2_674 4_654 ?
O13 P3 Na4 123.9(4) . 3_475 ?
O6 P3 Na4 41.2(3) . 3_475 ?
O7 P3 Na4 70.5(3) . 3_475 ?
O2 P3 Na4 127.1(4) . 3_475 ?
Li1A P3 Na4 129.2(6) 4_654 3_475 ?
Li2 P3 Na4 76.4(5) 2_674 3_475 ?
Na1 P3 Na4 127.8(2) 4_654 3_475 ?
O13 P3 Na4 35.1(3) . 2_774 ?
O6 P3 Na4 109.7(3) . 2_774 ?
O7 P3 Na4 134.6(4) . 2_774 ?
O2 P3 Na4 78.8(3) . 2_774 ?
Li1A P3 Na4 74.6(8) 4_654 2_774 ?
Li2 P3 Na4 67.1(5) 2_674 2_774 ?
Na1 P3 Na4 80.6(2) 4_654 2_774 ?
Na4 P3 Na4 143.3(2) 3_475 2_774 ?
O13 P3 Na4 135.2(4) . . ?
O6 P3 Na4 33.2(3) . . ?
O7 P3 Na4 113.2(3) . . ?
O2 P3 Na4 79.1(3) . . ?
Li1A P3 Na4 157.3(10) 4_654 . ?
Li2 P3 Na4 73.9(5) 2_674 . ?
Na1 P3 Na4 147.5(2) 4_654 . ?
Na4 P3 Na4 58.76(12) 3_475 . ?
Na4 P3 Na4 111.69(8) 2_774 . ?
O12 Na2 O4 86.8(3) . 4_655 ?
O12 Na2 O9 109.5(3) . 4 ?
O4 Na2 O9 132.3(3) 4_655 4 ?
O12 Na2 O8 137.0(3) . 2_665 ?
O4 Na2 O8 110.5(3) 4_655 2_665 ?
O9 Na2 O8 87.9(3) 4 2_665 ?
O12 Na2 O3 113.8(3) . 4_655 ?
O4 Na2 O3 58.3(3) 4_655 4_655 ?
O9 Na2 O3 74.3(3) 4 4_655 ?
O8 Na2 O3 108.6(3) 2_665 4_655 ?
O12 Na2 O10 78.7(3) . 2_665 ?
O4 Na2 O10 100.4(3) 4_655 2_665 ?
O9 Na2 O10 126.3(3) 4 2_665 ?
O8 Na2 O10 60.1(3) 2_665 2_665 ?
O3 Na2 O10 152.7(3) 4_655 2_665 ?
O12 Na2 P2 108.0(2) . 2_665 ?
O4 Na2 P2 109.0(2) 4_655 2_665 ?
O9 Na2 P2 107.7(2) 4 2_665 ?
O8 Na2 P2 29.8(2) 2_665 2_665 ?
O3 Na2 P2 134.7(3) 4_655 2_665 ?
O10 Na2 P2 30.3(2) 2_665 2_665 ?
O12 Na2 B2 100.0(3) . 4_655 ?
O4 Na2 B2 29.1(3) 4_655 4_655 ?
O9 Na2 B2 103.3(3) 4 4_655 ?
O8 Na2 B2 114.2(4) 2_665 4_655 ?
O3 Na2 B2 29.3(3) 4_655 4_655 ?
O10 Na2 B2 128.2(3) 2_665 4_655 ?
P2 Na2 B2 127.4(3) 2_665 4_655 ?
O12 Na2 P2 99.6(3) . 4 ?
O4 Na2 P2 159.2(2) 4_655 4 ?
O9 Na2 P2 27.02(19) 4 4 ?
O8 Na2 P2 78.1(2) 2_665 4 ?
O3 Na2 P2 101.3(2) 4_655 4 ?
O10 Na2 P2 100.29(19) 2_665 4 ?
P2 Na2 P2 87.98(13) 2_665 4 ?
B2 Na2 P2 130.3(3) 4_655 4 ?
O12 Na2 Na3 48.8(2) . 1_455 ?
O4 Na2 Na3 125.1(3) 4_655 1_455 ?
O9 Na2 Na3 96.6(2) 4 1_455 ?
O8 Na2 Na3 91.5(2) 2_665 1_455 ?
O3 Na2 Na3 157.2(3) 4_655 1_455 ?
O10 Na2 Na3 48.2(2) 2_665 1_455 ?
P2 Na2 Na3 67.76(13) 2_665 1_455 ?
B2 Na2 Na3 147.7(3) 4_655 1_455 ?
P2 Na2 Na3 71.88(13) 4 1_455 ?
O12 Na2 P1 23.3(2) . . ?
O4 Na2 P1 76.7(2) 4_655 . ?
O9 Na2 P1 100.8(2) 4 . ?
O8 Na2 P1 160.3(3) 2_665 . ?
O3 Na2 P1 90.9(2) 4_655 . ?
O10 Na2 P1 101.1(2) 2_665 . ?
P2 Na2 P1 130.96(19) 2_665 . ?
B2 Na2 P1 81.3(3) 4_655 . ?
P2 Na2 P1 101.69(15) 4 . ?
Na3 Na2 P1 70.05(15) 1_455 . ?
O12 Na2 P2 94.0(3) . 4_655 ?
O4 Na2 P2 23.89(16) 4_655 4_655 ?
O9 Na2 P2 147.3(3) 4 4_655 ?
O8 Na2 P2 90.0(2) 2_665 4_655 ?
O3 Na2 P2 75.55(19) 4_655 4_655 ?
O10 Na2 P2 79.49(19) 2_665 4_655 ?
P2 Na2 P2 85.07(13) 2_665 4_655 ?
B2 Na2 P2 48.8(3) 4_655 4_655 ?
P2 Na2 P2 166.1(2) 4 4_655 ?
Na3 Na2 P2 116.11(16) 1_455 4_655 ?
P1 Na2 P2 91.95(13) . 4_655 ?
O8 Na3 O8 91.5(4) . 3_565 ?
O8 Na3 O10 88.5(3) . 4_655 ?
O8 Na3 O10 166.0(3) 3_565 4_655 ?
O8 Na3 O10 173.6(4) . 2_765 ?
O8 Na3 O10 84.5(3) 3_565 2_765 ?
O10 Na3 O10 96.6(4) 4_655 2_765 ?
O8 Na3 O12 106.5(3) . 1_655 ?
O8 Na3 O12 77.6(3) 3_565 1_655 ?
O10 Na3 O12 88.9(3) 4_655 1_655 ?
O10 Na3 O12 77.5(3) 2_765 1_655 ?
O8 Na3 O12 75.0(3) . 3_565 ?
O8 Na3 O12 120.3(3) 3_565 3_565 ?
O10 Na3 O12 73.3(3) 4_655 3_565 ?
O10 Na3 O12 102.7(3) 2_765 3_565 ?
O12 Na3 O12 162.1(4) 1_655 3_565 ?
O8 Na3 Na2 135.8(3) . 1_655 ?
O8 Na3 Na2 108.2(2) 3_565 1_655 ?
O10 Na3 Na2 63.1(2) 4_655 1_655 ?
O10 Na3 Na2 50.5(2) 2_765 1_655 ?
O12 Na3 Na2 44.9(2) 1_655 1_655 ?
O12 Na3 Na2 121.8(3) 3_565 1_655 ?
O8 Na3 Na3 47.6(2) . 3_465 ?
O8 Na3 Na3 137.2(2) 3_565 3_465 ?
O10 Na3 Na3 48.1(2) 4_655 3_465 ?
O10 Na3 Na3 134.8(2) 2_765 3_465 ?
O12 Na3 Na3 120.6(3) 1_655 3_465 ?
O12 Na3 Na3 47.18(18) 3_565 3_465 ?
Na2 Na3 Na3 110.90(15) 1_655 3_465 ?
O8 Na3 Na3 131.0(3) . 3_565 ?
O8 Na3 Na3 43.8(2) 3_565 3_565 ?
O10 Na3 Na3 129.4(2) 4_655 3_565 ?
O10 Na3 Na3 47.3(2) 2_765 3_565 ?
O12 Na3 Na3 54.2(2) 1_655 3_565 ?
O12 Na3 Na3 138.0(3) 3_565 3_565 ?
Na2 Na3 Na3 66.29(13) 1_655 3_565 ?
Na3 Na3 Na3 174.7(3) 3_465 3_565 ?
O8 Na3 P2 78.0(3) . 3_565 ?
O8 Na3 P2 24.02(19) 3_565 3_565 ?
O10 Na3 P2 165.3(3) 4_655 3_565 ?
O10 Na3 P2 96.5(2) 2_765 3_565 ?
O12 Na3 P2 100.5(3) 1_655 3_565 ?
O12 Na3 P2 97.3(2) 3_565 3_565 ?
Na2 Na3 P2 131.25(16) 1_655 3_565 ?
Na3 Na3 P2 117.19(12) 3_465 3_565 ?
Na3 Na3 P2 65.12(10) 3_565 3_565 ?
O8 Na3 Na2 102.3(2) . 3_565 ?
O8 Na3 Na2 147.7(2) 3_565 3_565 ?
O10 Na3 Na2 45.2(2) 4_655 3_565 ?
O10 Na3 Na2 78.8(2) 2_765 3_565 ?
O12 Na3 Na2 124.3(3) 1_655 3_565 ?
O12 Na3 Na2 40.1(2) 3_565 3_565 ?
Na2 Na3 Na2 81.79(19) 1_655 3_565 ?
Na3 Na3 Na2 56.50(11) 3_465 3_565 ?
Na3 Na3 Na2 126.11(13) 3_565 3_565 ?
P2 Na3 Na2 131.88(16) 3_565 3_565 ?
O8 Na3 Na2 66.8(3) . 4_654 ?
O8 Na3 Na2 38.2(2) 3_565 4_654 ?
O10 Na3 Na2 130.7(2) 4_655 4_654 ?
O10 Na3 Na2 112.1(2) 2_765 4_654 ?
O12 Na3 Na2 61.3(2) 1_655 4_654 ?
O12 Na3 Na2 132.3(3) 3_565 4_654 ?
Na2 Na3 Na2 105.54(13) 1_655 4_654 ?
Na3 Na3 Na2 112.75(12) 3_465 4_654 ?
Na3 Na3 Na2 64.78(12) 3_565 4_654 ?
P2 Na3 Na2 48.51(11) 3_565 4_654 ?
Na2 Na3 Na2 169.07(15) 3_565 4_654 ?
O6 Na4 O13 168.2(4) . 2_775 ?
O6 Na4 O13 89.1(3) . 4_655 ?
O13 Na4 O13 97.4(4) 2_775 4_655 ?
O6 Na4 O6 88.8(4) . 3_575 ?
O13 Na4 O6 87.6(3) 2_775 3_575 ?
O13 Na4 O6 163.6(4) 4_655 3_575 ?
O6 Na4 O11 116.5(3) . 1_655 ?
O13 Na4 O11 74.6(3) 2_775 1_655 ?
O13 Na4 O11 78.6(3) 4_655 1_655 ?
O6 Na4 O11 87.8(3) 3_575 1_655 ?
O6 Na4 O5 86.2(3) . 3_575 ?
O13 Na4 O5 82.6(3) 2_775 3_575 ?
O13 Na4 O5 105.8(3) 4_655 3_575 ?
O6 Na4 O5 90.4(3) 3_575 3_575 ?
O11 Na4 O5 157.2(3) 1_655 3_575 ?
O6 Na4 Li1A 88.8(4) . . ?
O13 Na4 Li1A 102.8(5) 2_775 . ?
O13 Na4 Li1A 44.7(7) 4_655 . ?
O6 Na4 Li1A 118.9(7) 3_575 . ?
O11 Na4 Li1A 41.5(6) 1_655 . ?
O5 Na4 Li1A 150.2(7) 3_575 . ?
O6 Na4 Na4 46.5(2) . 3_475 ?
O13 Na4 Na4 136.2(3) 2_775 3_475 ?
O13 Na4 Na4 44.8(3) 4_655 3_475 ?
O6 Na4 Na4 135.3(2) 3_575 3_475 ?
O11 Na4 Na4 109.3(3) 1_655 3_475 ?
O5 Na4 Na4 87.8(3) 3_575 3_475 ?
Li1A Na4 Na4 67.9(6) . 3_475 ?
O6 Na4 Na4 133.3(2) . 3_575 ?
O13 Na4 Na4 45.0(2) 2_775 3_575 ?
O13 Na4 Na4 133.8(3) 4_655 3_575 ?
O6 Na4 Na4 44.6(2) 3_575 3_575 ?
O11 Na4 Na4 67.3(3) 1_655 3_575 ?
O5 Na4 Na4 95.9(3) 3_575 3_575 ?
Li1A Na4 Na4 108.8(7) . 3_575 ?
Na4 Na4 Na4 176.4(5) 3_475 3_575 ?
O6 Na4 P3 75.1(3) . 3_575 ?
O13 Na4 P3 97.5(3) 2_775 3_575 ?
O13 Na4 P3 163.8(3) 4_655 3_575 ?
O6 Na4 P3 24.19(19) 3_575 3_575 ?
O11 Na4 P3 111.6(3) 1_655 3_575 ?
O5 Na4 P3 70.0(2) 3_575 3_575 ?
Li1A Na4 P3 136.4(6) . 3_575 ?
Na4 Na4 P3 118.97(14) 3_475 3_575 ?
Na4 Na4 P3 62.34(12) 3_575 3_575 ?
O6 Na4 P3 156.3(3) . 2_775 ?
O13 Na4 P3 21.4(2) 2_775 2_775 ?
O13 Na4 P3 78.9(3) 4_655 2_775 ?
O6 Na4 P3 108.3(3) 3_575 2_775 ?
O11 Na4 P3 81.4(2) 1_655 2_775 ?
O5 Na4 P3 77.6(2) 3_575 2_775 ?
Li1A Na4 P3 96.7(4) . 2_775 ?
Na4 Na4 P3 114.85(14) 3_475 2_775 ?
Na4 Na4 P3 66.39(11) 3_575 2_775 ?
P3 Na4 P3 114.35(14) 3_575 2_775 ?
O6 Na4 P3 20.58(19) . . ?
O13 Na4 P3 164.5(3) 2_775 . ?
O13 Na4 P3 94.4(3) 4_655 . ?
O6 Na4 P3 78.4(3) 3_575 . ?
O11 Na4 P3 98.0(3) 1_655 . ?
O5 Na4 P3 103.8(2) 3_575 . ?
Li1A Na4 P3 78.7(4) . . ?
Na4 Na4 P3 58.90(11) 3_475 . ?
Na4 Na4 P3 119.69(16) 3_575 . ?
P3 Na4 P3 72.16(16) 3_575 . ?
P3 Na4 P3 173.24(19) 2_775 . ?
B2 O1 B1 113.4(9) . . ?
B2 O1 Li1A 132.7(12) . . ?
B1 O1 Li1A 113.2(12) . . ?
B2 O1 Na1 135.3(8) . . ?
B1 O1 Na1 110.4(8) . . ?
Li1A O1 Na1 16.5(13) . . ?
B2 O2 P3 119.2(7) . . ?
B2 O2 Li2 97.3(8) . 4_654 ?
P3 O2 Li2 135.1(6) . 4_654 ?
B2 O2 Na1 89.3(6) . 4_654 ?
P3 O2 Na1 74.8(4) . 4_654 ?
Li2 O2 Na1 134.6(7) 4_654 4_654 ?
B2 O3 P1 128.0(7) . 1_655 ?
B2 O3 Li2 92.1(8) . 4_654 ?
P1 O3 Li2 126.4(7) 1_655 4_654 ?
B2 O3 Na2 93.5(6) . 4_654 ?
P1 O3 Na2 111.7(4) 1_655 4_654 ?
Li2 O3 Na2 97.2(6) 4_654 4_654 ?
B2 O4 P2 121.0(7) . . ?
B2 O4 Na2 101.3(6) . 4_654 ?
P2 O4 Na2 119.2(4) . 4_654 ?
B2 O4 Na1 98.6(6) . 4_654 ?
P2 O4 Na1 78.5(4) . 4_654 ?
Na2 O4 Na1 138.8(5) 4_654 4_654 ?
B1 O5 P1 130.5(7) . . ?
B1 O5 Na1 82.7(6) . . ?
P1 O5 Na1 135.7(5) . . ?
B1 O5 Na4 98.4(6) . 3_475 ?
P1 O5 Na4 107.7(3) . 3_475 ?
Na1 O5 Na4 92.0(3) . 3_475 ?
P3 O6 Li2 98.4(7) . 2_674 ?
P3 O6 Na4 126.2(5) . . ?
Li2 O6 Na4 115.7(6) 2_674 . ?
P3 O6 Na4 114.7(4) . 3_475 ?
Li2 O6 Na4 113.9(6) 2_674 3_475 ?
Na4 O6 Na4 88.9(4) . 3_475 ?
B1 O7 P3 121.2(6) . . ?
B1 O7 Li2 118.8(8) . 4_554 ?
P3 O7 Li2 118.5(6) . 4_554 ?
B1 O7 Li1A 113.1(13) . 4_654 ?
P3 O7 Li1A 81.5(11) . 4_654 ?
Li2 O7 Li1A 87.3(11) 4_554 4_654 ?
B1 O7 Na1 99.5(6) . 4_654 ?
P3 O7 Na1 89.9(4) . 4_654 ?
Li2 O7 Na1 92.8(7) 4_554 4_654 ?
Li1A O7 Na1 13.7(12) 4_654 4_654 ?
P2 O8 Na3 141.8(5) . . ?
P2 O8 Na2 96.3(4) . 2_664 ?
Na3 O8 Na2 109.1(3) . 2_664 ?
P2 O8 Na3 113.5(4) . 3_465 ?
Na3 O8 Na3 88.6(4) . 3_465 ?
Na2 O8 Na3 102.8(3) 2_664 3_465 ?
B1 O9 P2 120.6(7) . . ?
B1 O9 Na2 129.1(6) . 4_554 ?
P2 O9 Na2 109.9(4) . 4_554 ?
B1 O9 Na1 93.3(7) . 4_654 ?
P2 O9 Na1 80.1(4) . 4_654 ?
Na2 O9 Na1 88.8(4) 4_554 4_654 ?
P2 O10 Na3 154.1(5) . 4_654 ?
P2 O10 Na3 121.1(4) . 2_764 ?
Na3 O10 Na3 84.6(3) 4_654 2_764 ?
P2 O10 Na2 89.3(4) . 2_664 ?
Na3 O10 Na2 92.1(3) 4_654 2_664 ?
Na3 O10 Na2 81.4(3) 2_764 2_664 ?
P2 O10 Na1 80.0(4) . 4_654 ?
Na3 O10 Na1 98.2(4) 4_654 4_654 ?
Na3 O10 Na1 102.7(4) 2_764 4_654 ?
Na2 O10 Na1 169.2(4) 2_664 4_654 ?
P1 O11 Li2 138.0(8) . . ?
P1 O11 Li1A 109.9(11) . 1_455 ?
Li2 O11 Li1A 97.8(10) . 1_455 ?
P1 O11 Na1 99.9(5) . 1_455 ?
Li2 O11 Na1 101.1(7) . 1_455 ?
Li1A O11 Na1 13.3(12) 1_455 1_455 ?
P1 O11 Na4 123.1(5) . 1_455 ?
Li2 O11 Na4 91.2(6) . 1_455 ?
Li1A O11 Na4 81.3(13) 1_455 1_455 ?
Na1 O11 Na4 94.1(4) 1_455 1_455 ?
P1 O12 Na2 118.5(5) . . ?
P1 O12 Na3 144.0(5) . 1_455 ?
Na2 O12 Na3 86.3(3) . 1_455 ?
P1 O12 Na3 123.2(5) . 3_465 ?
Na2 O12 Na3 90.5(3) . 3_465 ?
Na3 O12 Na3 78.6(2) 1_455 3_465 ?
P3 O13 Li1A 82.9(9) . 4_654 ?
P3 O13 Na4 123.5(5) . 2_774 ?
Li1A O13 Na4 104.9(6) 4_654 2_774 ?
P3 O13 Na4 146.2(5) . 4_654 ?
Li1A O13 Na4 89.5(10) 4_654 4_654 ?
Na4 O13 Na4 90.2(4) 2_774 4_654 ?
P3 O13 Li2 82.4(7) . 2_674 ?
Li1A O13 Li2 163.3(9) 4_654 2_674 ?
Na4 O13 Li2 89.9(5) 2_774 2_674 ?
Na4 O13 Li2 98.4(6) 4_654 2_674 ?
P3 O13 Na1 78.5(4) . 4_654 ?
Li1A O13 Na1 5.5(10) 4_654 4_654 ?
Na4 O13 Na1 104.4(4) 2_774 4_654 ?
Na4 O13 Na1 95.0(4) 4_654 4_654 ?
Li2 O13 Na1 160.4(7) 2_674 4_654 ?
O1 B1 O5 108.9(10) . . ?
O1 B1 O9 111.7(9) . . ?
O5 B1 O9 112.2(9) . . ?
O1 B1 O7 110.2(9) . . ?
O5 B1 O7 109.3(9) . . ?
O9 B1 O7 104.5(10) . . ?
O1 B1 Na1 42.5(5) . . ?
O5 B1 Na1 67.8(6) . . ?
O9 B1 Na1 118.7(8) . . ?
O7 B1 Na1 134.6(8) . . ?
O1 B1 Na1 105.0(8) . 4_654 ?
O5 B1 Na1 145.7(8) . 4_654 ?
O9 B1 Na1 58.1(6) . 4_654 ?
O7 B1 Na1 52.1(6) . 4_654 ?
Na1 B1 Na1 146.5(5) . 4_654 ?
O1 B2 O2 111.9(10) . . ?
O1 B2 O3 115.0(10) . . ?
O2 B2 O3 104.2(9) . . ?
O1 B2 O4 111.6(9) . . ?
O2 B2 O4 106.9(9) . . ?
O3 B2 O4 106.6(9) . . ?
O1 B2 Li2 139.1(10) . 4_654 ?
O2 B2 Li2 50.1(6) . 4_654 ?
O3 B2 Li2 55.1(7) . 4_654 ?
O4 B2 Li2 109.1(8) . 4_654 ?
O1 B2 Na2 135.1(8) . 4_654 ?
O2 B2 Na2 112.8(7) . 4_654 ?
O3 B2 Na2 57.2(5) . 4_654 ?
O4 B2 Na2 49.6(5) . 4_654 ?
Li2 B2 Na2 77.2(5) 4_654 4_654 ?
Na1 Li1A O1 85(3) . . ?
Na1 Li1A O11 110(4) . 1_655 ?
O1 Li1A O11 90.0(14) . 1_655 ?
Na1 Li1A O7 102(3) . 4_655 ?
O1 Li1A O7 172(2) . 4_655 ?
O11 Li1A O7 84.2(8) 1_655 4_655 ?
Na1 Li1A O13 153(5) . 4_655 ?
O1 Li1A O13 109.7(18) . 4_655 ?
O11 Li1A O13 93.1(16) 1_655 4_655 ?
O7 Li1A O13 65.3(10) 4_655 4_655 ?
Na1 Li1A P3 122(4) . 4_655 ?
O1 Li1A P3 141(2) . 4_655 ?
O11 Li1A P3 104.5(13) 1_655 4_655 ?
O7 Li1A P3 37.1(6) 4_655 4_655 ?
O13 Li1A P3 34.9(6) 4_655 4_655 ?
Na1 Li1A P1 89(4) . 1_655 ?
O1 Li1A P1 70.0(10) . 1_655 ?
O11 Li1A P1 27.6(5) 1_655 1_655 ?
O7 Li1A P1 106.2(9) 4_655 1_655 ?
O13 Li1A P1 117.2(16) 4_655 1_655 ?
P3 Li1A P1 131.9(12) 4_655 1_655 ?
Na1 Li1A Li2 115(3) . 1_655 ?
O1 Li1A Li2 127.6(17) . 1_655 ?
O11 Li1A Li2 38.4(6) 1_655 1_655 ?
O7 Li1A Li2 45.9(6) 4_655 1_655 ?
O13 Li1A Li2 74.4(10) 4_655 1_655 ?
P3 Li1A Li2 70.0(8) 4_655 1_655 ?
P1 Li1A Li2 63.2(7) 1_655 1_655 ?
Na1 Li1A Na4 161(4) . . ?
O1 Li1A Na4 81.3(13) . . ?
O11 Li1A Na4 57.2(10) 1_655 . ?
O7 Li1A Na4 90.9(13) 4_655 . ?
O13 Li1A Na4 45.8(9) 4_655 . ?
P3 Li1A Na4 76.9(12) 4_655 . ?
P1 Li1A Na4 74.1(9) 1_655 . ?
Li2 Li1A Na4 64.9(8) 1_655 . ?
Na1 Li1A Na4 133(3) . 3_475 ?
O1 Li1A Na4 77.9(11) . 3_475 ?
O11 Li1A Na4 113.8(17) 1_655 3_475 ?
O7 Li1A Na4 99.4(14) 4_655 3_475 ?
O13 Li1A Na4 37.9(6) 4_655 3_475 ?
P3 Li1A Na4 62.8(9) 4_655 3_475 ?
P1 Li1A Na4 124.4(13) 1_655 3_475 ?
Li2 Li1A Na4 110.1(13) 1_655 3_475 ?
Na4 Li1A Na4 56.7(7) . 3_475 ?
Na1 Li1A Na2 55(3) . 1_655 ?
O1 Li1A Na2 109.4(15) . 1_655 ?
O11 Li1A Na2 62.1(9) 1_655 1_655 ?
O7 Li1A Na2 72.7(8) 4_655 1_655 ?
O13 Li1A Na2 133.1(8) 4_655 1_655 ?
P3 Li1A Na2 109.6(7) 4_655 1_655 ?
P1 Li1A Na2 56.1(6) 1_655 1_655 ?
Li2 Li1A Na2 61.4(6) 1_655 1_655 ?
Na4 Li1A Na2 118.2(9) . 1_655 ?
Na4 Li1A Na2 171.0(9) 3_475 1_655 ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
O13 P3 O2 B2 -144.5(8) . . . . ?
O6 P3 O2 B2 89.3(8) . . . . ?
O7 P3 O2 B2 -30.2(9) . . . . ?
Li1A P3 O2 B2 -87.8(11) 4_654 . . . ?
Li2 P3 O2 B2 143.6(9) 2_674 . . . ?
Na1 P3 O2 B2 -80.4(8) 4_654 . . . ?
Na4 P3 O2 B2 45.2(9) 3_475 . . . ?
Na4 P3 O2 B2 -163.7(8) 2_774 . . . ?
Na4 P3 O2 B2 81.3(8) . . . . ?
O13 P3 O2 Li2 75.3(13) . . . 4_654 ?
O6 P3 O2 Li2 -50.9(13) . . . 4_654 ?
O7 P3 O2 Li2 -170.4(12) . . . 4_654 ?
Li1A P3 O2 Li2 132.0(15) 4_654 . . 4_654 ?
Li2 P3 O2 Li2 3.4(10) 2_674 . . 4_654 ?
Na1 P3 O2 Li2 139.3(12) 4_654 . . 4_654 ?
Na4 P3 O2 Li2 -95.0(12) 3_475 . . 4_654 ?
Na4 P3 O2 Li2 56.0(12) 2_774 . . 4_654 ?
Na4 P3 O2 Li2 -58.9(12) . . . 4_654 ?
O13 P3 O2 Na1 -64.0(4) . . . 4_654 ?
O6 P3 O2 Na1 169.7(4) . . . 4_654 ?
O7 P3 O2 Na1 50.2(4) . . . 4_654 ?
Li1A P3 O2 Na1 -7.3(8) 4_654 . . 4_654 ?
Li2 P3 O2 Na1 -136.0(7) 2_674 . . 4_654 ?
Na4 P3 O2 Na1 125.6(3) 3_475 . . 4_654 ?
Na4 P3 O2 Na1 -83.3(3) 2_774 . . 4_654 ?
Na4 P3 O2 Na1 161.8(3) . . . 4_654 ?
O8 P2 O4 B2 -83.2(8) . . . . ?
O10 P2 O4 B2 150.3(8) . . . . ?
O9 P2 O4 B2 35.6(9) . . . . ?
Na1 P2 O4 B2 93.3(8) 4_654 . . . ?
Na2 P2 O4 B2 -143.4(7) 2_664 . . . ?
Na2 P2 O4 B2 70.5(10) 4_554 . . . ?
Na3 P2 O4 B2 -39.6(9) 3_465 . . . ?
Na2 P2 O4 B2 -126.8(11) 4_654 . . . ?
O8 P2 O4 Na2 43.6(7) . . . 4_654 ?
O10 P2 O4 Na2 -82.9(6) . . . 4_654 ?
O9 P2 O4 Na2 162.4(5) . . . 4_654 ?
Na1 P2 O4 Na2 -140.0(6) 4_654 . . 4_654 ?
Na2 P2 O4 Na2 -16.7(7) 2_664 . . 4_654 ?
Na2 P2 O4 Na2 -162.7(3) 4_554 . . 4_654 ?
Na3 P2 O4 Na2 87.2(6) 3_465 . . 4_654 ?
O8 P2 O4 Na1 -176.4(5) . . . 4_654 ?
O10 P2 O4 Na1 57.1(4) . . . 4_654 ?
O9 P2 O4 Na1 -57.6(4) . . . 4_654 ?
Na2 P2 O4 Na1 123.3(4) 2_664 . . 4_654 ?
Na2 P2 O4 Na1 -22.8(5) 4_554 . . 4_654 ?
Na3 P2 O4 Na1 -132.9(4) 3_465 . . 4_654 ?
Na2 P2 O4 Na1 140.0(6) 4_654 . . 4_654 ?
O12 P1 O5 B1 84.5(11) . . . . ?
O11 P1 O5 B1 -149.0(9) . . . . ?
O3 P1 O5 B1 -32.7(10) 1_455 . . . ?
Li1A P1 O5 B1 -145.4(16) 1_455 . . . ?
Na1 P1 O5 B1 -162.5(9) 1_455 . . . ?
Na2 P1 O5 B1 125.2(9) . . . . ?
O12 P1 O5 Na1 -45.0(8) . . . . ?
O11 P1 O5 Na1 81.5(7) . . . . ?
O3 P1 O5 Na1 -162.2(6) 1_455 . . . ?
Li1A P1 O5 Na1 85.0(15) 1_455 . . . ?
Na1 P1 O5 Na1 68.0(12) 1_455 . . . ?
Na2 P1 O5 Na1 -4.3(7) . . . . ?
O12 P1 O5 Na4 -157.2(5) . . . 3_475 ?
O11 P1 O5 Na4 -30.8(6) . . . 3_475 ?
O3 P1 O5 Na4 85.5(4) 1_455 . . 3_475 ?
Li1A P1 O5 Na4 -27.2(16) 1_455 . . 3_475 ?
Na1 P1 O5 Na4 -44.2(12) 1_455 . . 3_475 ?
Na2 P1 O5 Na4 -116.5(3) . . . 3_475 ?
O13 P3 O6 Li2 -6.7(7) . . . 2_674 ?
O7 P3 O6 Li2 -129.1(6) . . . 2_674 ?
O2 P3 O6 Li2 116.3(6) . . . 2_674 ?
Li1A P3 O6 Li2 -77(4) 4_654 . . 2_674 ?
Na1 P3 O6 Li2 -127(2) 4_654 . . 2_674 ?
Na4 P3 O6 Li2 -121.3(7) 3_475 . . 2_674 ?
Na4 P3 O6 Li2 30.9(6) 2_774 . . 2_674 ?
Na4 P3 O6 Li2 130.7(8) . . . 2_674 ?
O13 P3 O6 Na4 -137.4(5) . . . . ?
O7 P3 O6 Na4 100.2(6) . . . . ?
O2 P3 O6 Na4 -14.4(7) . . . . ?
Li1A P3 O6 Na4 152(4) 4_654 . . . ?
Li2 P3 O6 Na4 -130.7(8) 2_674 . . . ?
Na1 P3 O6 Na4 102(2) 4_654 . . . ?
Na4 P3 O6 Na4 108.1(7) 3_475 . . . ?
Na4 P3 O6 Na4 -99.8(5) 2_774 . . . ?
O13 P3 O6 Na4 114.6(5) . . . 3_475 ?
O7 P3 O6 Na4 -7.9(6) . . . 3_475 ?
O2 P3 O6 Na4 -122.5(5) . . . 3_475 ?
Li1A P3 O6 Na4 44(5) 4_654 . . 3_475 ?
Li2 P3 O6 Na4 121.3(7) 2_674 . . 3_475 ?
Na1 P3 O6 Na4 -6(2) 4_654 . . 3_475 ?
Na4 P3 O6 Na4 152.2(3) 2_774 . . 3_475 ?
Na4 P3 O6 Na4 -108.1(7) . . . 3_475 ?
O13 P3 O7 B1 154.7(8) . . . . ?
O6 P3 O7 B1 -79.4(9) . . . . ?
O2 P3 O7 B1 40.2(10) . . . . ?
Li1A P3 O7 B1 111.9(13) 4_654 . . . ?
Li2 P3 O7 B1 -132.7(10) 2_674 . . . ?
Na1 P3 O7 B1 101.1(8) 4_654 . . . ?
Na4 P3 O7 B1 -84.9(8) 3_475 . . . ?
Na4 P3 O7 B1 127.4(8) 2_774 . . . ?
Na4 P3 O7 B1 -43.5(9) . . . . ?
O13 P3 O7 Li2 -39.5(9) . . . 4_554 ?
O6 P3 O7 Li2 86.4(9) . . . 4_554 ?
O2 P3 O7 Li2 -154.0(8) . . . 4_554 ?
Li1A P3 O7 Li2 -82.3(14) 4_654 . . 4_554 ?
Li2 P3 O7 Li2 33.1(8) 2_674 . . 4_554 ?
Na1 P3 O7 Li2 -93.1(8) 4_654 . . 4_554 ?
Na4 P3 O7 Li2 80.9(8) 3_475 . . 4_554 ?
Na4 P3 O7 Li2 -66.8(9) 2_774 . . 4_554 ?
Na4 P3 O7 Li2 122.3(7) . . . 4_554 ?
O13 P3 O7 Li1A 42.7(12) . . . 4_654 ?
O6 P3 O7 Li1A 168.7(11) . . . 4_654 ?
O2 P3 O7 Li1A -71.8(12) . . . 4_654 ?
Li2 P3 O7 Li1A 115.4(13) 2_674 . . 4_654 ?
Na1 P3 O7 Li1A -10.8(11) 4_654 . . 4_654 ?
Na4 P3 O7 Li1A 163.2(11) 3_475 . . 4_654 ?
Na4 P3 O7 Li1A 15.5(12) 2_774 . . 4_654 ?
Na4 P3 O7 Li1A -155.4(11) . . . 4_654 ?
O13 P3 O7 Na1 53.6(5) . . . 4_654 ?
O6 P3 O7 Na1 179.5(4) . . . 4_654 ?
O2 P3 O7 Na1 -60.9(5) . . . 4_654 ?
Li1A P3 O7 Na1 10.8(11) 4_654 . . 4_654 ?
Li2 P3 O7 Na1 126.2(8) 2_674 . . 4_654 ?
Na4 P3 O7 Na1 174.0(4) 3_475 . . 4_654 ?
Na4 P3 O7 Na1 26.3(5) 2_774 . . 4_654 ?
Na4 P3 O7 Na1 -144.6(3) . . . 4_654 ?
O10 P2 O8 Na3 136.0(7) . . . . ?
O9 P2 O8 Na3 -101.9(8) . . . . ?
O4 P2 O8 Na3 12.8(10) . . . . ?
Na2 P2 O8 Na3 132.4(10) 2_664 . . . ?
Na2 P2 O8 Na3 -147.8(7) 4_554 . . . ?
Na3 P2 O8 Na3 -120.7(10) 3_465 . . . ?
Na2 P2 O8 Na3 37.4(8) 4_654 . . . ?
O10 P2 O8 Na2 3.6(6) . . . 2_664 ?
O9 P2 O8 Na2 125.8(4) . . . 2_664 ?
O4 P2 O8 Na2 -119.6(4) . . . 2_664 ?
Na2 P2 O8 Na2 79.9(3) 4_554 . . 2_664 ?
Na3 P2 O8 Na2 106.9(5) 3_465 . . 2_664 ?
Na2 P2 O8 Na2 -94.9(3) 4_654 . . 2_664 ?
O10 P2 O8 Na3 -103.3(5) . . . 3_465 ?
O9 P2 O8 Na3 18.9(6) . . . 3_465 ?
O4 P2 O8 Na3 133.6(4) . . . 3_465 ?
Na2 P2 O8 Na3 -106.9(5) 2_664 . . 3_465 ?
Na2 P2 O8 Na3 -27.0(5) 4_554 . . 3_465 ?
Na2 P2 O8 Na3 158.2(4) 4_654 . . 3_465 ?
O8 P2 O9 B1 90.2(9) . . . . ?
O10 P2 O9 B1 -144.1(9) . . . . ?
O4 P2 O9 B1 -29.4(10) . . . . ?
Na1 P2 O9 B1 -88.0(9) 4_654 . . . ?
Na2 P2 O9 B1 149.6(8) 2_664 . . . ?
Na2 P2 O9 B1 -173.1(11) 4_554 . . . ?
Na3 P2 O9 B1 103.7(9) 3_465 . . . ?
Na2 P2 O9 B1 -13.7(11) 4_654 . . . ?
O8 P2 O9 Na2 -96.7(5) . . . 4_554 ?
O10 P2 O9 Na2 28.9(5) . . . 4_554 ?
O4 P2 O9 Na2 143.7(4) . . . 4_554 ?
Na1 P2 O9 Na2 85.1(4) 4_654 . . 4_554 ?
Na2 P2 O9 Na2 -37.3(6) 2_664 . . 4_554 ?
Na3 P2 O9 Na2 -83.2(3) 3_465 . . 4_554 ?
Na2 P2 O9 Na2 159.4(3) 4_654 . . 4_554 ?
O8 P2 O9 Na1 178.2(4) . . . 4_654 ?
O10 P2 O9 Na1 -56.1(4) . . . 4_654 ?
O4 P2 O9 Na1 58.6(5) . . . 4_654 ?
Na2 P2 O9 Na1 -122.4(4) 2_664 . . 4_654 ?
Na2 P2 O9 Na1 -85.1(4) 4_554 . . 4_654 ?
Na3 P2 O9 Na1 -168.3(3) 3_465 . . 4_654 ?
Na2 P2 O9 Na1 74.3(5) 4_654 . . 4_654 ?
O8 P2 O10 Na3 90.0(12) . . . 4_654 ?
O9 P2 O10 Na3 -33.4(12) . . . 4_654 ?
O4 P2 O10 Na3 -145.0(10) . . . 4_654 ?
Na1 P2 O10 Na3 -88.3(11) 4_654 . . 4_654 ?
Na2 P2 O10 Na3 93.4(11) 2_664 . . 4_654 ?
Na2 P2 O10 Na3 -12.8(10) 4_554 . . 4_654 ?
Na3 P2 O10 Na3 42.8(12) 3_465 . . 4_654 ?
Na2 P2 O10 Na3 177.7(10) 4_654 . . 4_654 ?
O8 P2 O10 Na3 -82.8(6) . . . 2_764 ?
O9 P2 O10 Na3 153.8(4) . . . 2_764 ?
O4 P2 O10 Na3 42.2(6) . . . 2_764 ?
Na1 P2 O10 Na3 98.9(5) 4_654 . . 2_764 ?
Na2 P2 O10 Na3 -79.4(4) 2_664 . . 2_764 ?
Na2 P2 O10 Na3 174.4(5) 4_554 . . 2_764 ?
Na3 P2 O10 Na3 -130.0(4) 3_465 . . 2_764 ?
Na2 P2 O10 Na3 4.9(5) 4_654 . . 2_764 ?
O8 P2 O10 Na2 -3.4(5) . . . 2_664 ?
O9 P2 O10 Na2 -126.7(4) . . . 2_664 ?
O4 P2 O10 Na2 121.6(3) . . . 2_664 ?
Na1 P2 O10 Na2 178.3(3) 4_654 . . 2_664 ?
Na2 P2 O10 Na2 -106.2(3) 4_554 . . 2_664 ?
Na3 P2 O10 Na2 -50.5(3) 3_465 . . 2_664 ?
Na2 P2 O10 Na2 84.4(2) 4_654 . . 2_664 ?
O8 P2 O10 Na1 178.3(5) . . . 4_654 ?
O9 P2 O10 Na1 54.9(4) . . . 4_654 ?
O4 P2 O10 Na1 -56.7(4) . . . 4_654 ?
Na2 P2 O10 Na1 -178.3(3) 2_664 . . 4_654 ?
Na2 P2 O10 Na1 75.5(3) 4_554 . . 4_654 ?
Na3 P2 O10 Na1 131.1(3) 3_465 . . 4_654 ?
Na2 P2 O10 Na1 -94.0(3) 4_654 . . 4_654 ?
O12 P1 O11 Li2 70.4(13) . . . . ?
O5 P1 O11 Li2 -54.6(13) . . . . ?
O3 P1 O11 Li2 -164.8(11) 1_455 . . . ?
Li1A P1 O11 Li2 128.1(18) 1_455 . . . ?
Na1 P1 O11 Li2 119.1(13) 1_455 . . . ?
Na2 P1 O11 Li2 51.9(12) . . . . ?
O12 P1 O11 Li1A -57.7(12) . . . 1_455 ?
O5 P1 O11 Li1A 177.3(11) . . . 1_455 ?
O3 P1 O11 Li1A 67.1(12) 1_455 . . 1_455 ?
Na1 P1 O11 Li1A -9.0(10) 1_455 . . 1_455 ?
Na2 P1 O11 Li1A -76.2(11) . . . 1_455 ?
O12 P1 O11 Na1 -48.7(6) . . . 1_455 ?
O5 P1 O11 Na1 -173.6(5) . . . 1_455 ?
O3 P1 O11 Na1 76.1(5) 1_455 . . 1_455 ?
Li1A P1 O11 Na1 9.0(10) 1_455 . . 1_455 ?
Na2 P1 O11 Na1 -67.2(4) . . . 1_455 ?
O12 P1 O11 Na4 -150.2(5) . . . 1_455 ?
O5 P1 O11 Na4 84.8(6) . . . 1_455 ?
O3 P1 O11 Na4 -25.4(6) 1_455 . . 1_455 ?
Li1A P1 O11 Na4 -92.5(12) 1_455 . . 1_455 ?
Na1 P1 O11 Na4 -101.5(6) 1_455 . . 1_455 ?
Na2 P1 O11 Na4 -168.7(5) . . . 1_455 ?
O11 P1 O12 Na2 -30.4(7) . . . . ?
O5 P1 O12 Na2 92.1(6) . . . . ?
O3 P1 O12 Na2 -155.6(4) 1_455 . . . ?
Li1A P1 O12 Na2 -65.2(6) 1_455 . . . ?
Na1 P1 O12 Na2 -67.4(5) 1_455 . . . ?
O11 P1 O12 Na3 98.1(10) . . . 1_455 ?
O5 P1 O12 Na3 -139.4(9) . . . 1_455 ?
O3 P1 O12 Na3 -27.1(11) 1_455 . . 1_455 ?
Li1A P1 O12 Na3 63.3(10) 1_455 . . 1_455 ?
Na1 P1 O12 Na3 61.1(9) 1_455 . . 1_455 ?
Na2 P1 O12 Na3 128.5(12) . . . 1_455 ?
O11 P1 O12 Na3 -141.9(5) . . . 3_465 ?
O5 P1 O12 Na3 -19.4(8) . . . 3_465 ?
O3 P1 O12 Na3 92.9(6) 1_455 . . 3_465 ?
Li1A P1 O12 Na3 -176.7(6) 1_455 . . 3_465 ?
Na1 P1 O12 Na3 -178.9(6) 1_455 . . 3_465 ?
Na2 P1 O12 Na3 -111.5(7) . . . 3_465 ?
O6 P3 O13 Li1A -166.5(8) . . . 4_654 ?
O7 P3 O13 Li1A -42.3(8) . . . 4_654 ?
O2 P3 O13 Li1A 68.8(8) . . . 4_654 ?
Li2 P3 O13 Li1A -172.1(9) 2_674 . . 4_654 ?
Na1 P3 O13 Li1A 3.4(8) 4_654 . . 4_654 ?
Na4 P3 O13 Li1A -120.4(8) 3_475 . . 4_654 ?
Na4 P3 O13 Li1A 103.2(9) 2_774 . . 4_654 ?
Na4 P3 O13 Li1A 161.7(8) . . . 4_654 ?
O6 P3 O13 Na4 90.3(6) . . . 2_774 ?
O7 P3 O13 Na4 -145.5(5) . . . 2_774 ?
O2 P3 O13 Na4 -34.3(7) . . . 2_774 ?
Li1A P3 O13 Na4 -103.2(9) 4_654 . . 2_774 ?
Li2 P3 O13 Na4 84.8(6) 2_674 . . 2_774 ?
Na1 P3 O13 Na4 -99.7(6) 4_654 . . 2_774 ?
Na4 P3 O13 Na4 136.4(5) 3_475 . . 2_774 ?
Na4 P3 O13 Na4 58.6(8) . . . 2_774 ?
O6 P3 O13 Na4 -88.3(10) . . . 4_654 ?
O7 P3 O13 Na4 35.9(11) . . . 4_654 ?
O2 P3 O13 Na4 147.1(8) . . . 4_654 ?
Li1A P3 O13 Na4 78.2(11) 4_654 . . 4_654 ?
Li2 P3 O13 Na4 -93.8(10) 2_674 . . 4_654 ?
Na1 P3 O13 Na4 81.7(9) 4_654 . . 4_654 ?
Na4 P3 O13 Na4 -42.2(11) 3_475 . . 4_654 ?
Na4 P3 O13 Na4 -178.6(13) 2_774 . . 4_654 ?
Na4 P3 O13 Na4 -120.0(8) . . . 4_654 ?
O6 P3 O13 Li2 5.5(6) . . . 2_674 ?
O7 P3 O13 Li2 129.8(5) . . . 2_674 ?
O2 P3 O13 Li2 -119.1(5) . . . 2_674 ?
Li1A P3 O13 Li2 172.1(9) 4_654 . . 2_674 ?
Na1 P3 O13 Li2 175.5(5) 4_654 . . 2_674 ?
Na4 P3 O13 Li2 51.7(5) 3_475 . . 2_674 ?
Na4 P3 O13 Li2 -84.8(6) 2_774 . . 2_674 ?
Na4 P3 O13 Li2 -26.2(6) . . . 2_674 ?
O6 P3 O13 Na1 -170.0(4) . . . 4_654 ?
O7 P3 O13 Na1 -45.7(4) . . . 4_654 ?
O2 P3 O13 Na1 65.4(4) . . . 4_654 ?
Li1A P3 O13 Na1 -3.4(7) 4_654 . . 4_654 ?
Li2 P3 O13 Na1 -175.5(5) 2_674 . . 4_654 ?
Na4 P3 O13 Na1 -123.8(3) 3_475 . . 4_654 ?
Na4 P3 O13 Na1 99.7(6) 2_774 . . 4_654 ?
Na4 P3 O13 Na1 158.3(4) . . . 4_654 ?
B2 O1 B1 O5 -173.7(9) . . . . ?
Li1A O1 B1 O5 -2.4(18) . . . . ?
Na1 O1 B1 O5 15.1(11) . . . . ?
B2 O1 B1 O9 61.9(13) . . . . ?
Li1A O1 B1 O9 -126.9(17) . . . . ?
Na1 O1 B1 O9 -109.3(10) . . . . ?
B2 O1 B1 O7 -53.8(13) . . . . ?
Li1A O1 B1 O7 117.4(17) . . . . ?
Na1 O1 B1 O7 135.0(8) . . . . ?
B2 O1 B1 Na1 171.2(12) . . . . ?
Li1A O1 B1 Na1 -17.6(14) . . . . ?
B2 O1 B1 Na1 0.8(10) . . . 4_654 ?
Li1A O1 B1 Na1 172.0(16) . . . 4_654 ?
Na1 O1 B1 Na1 -170.4(6) . . . 4_654 ?
P1 O5 B1 O1 -158.1(7) . . . . ?
Na1 O5 B1 O1 -11.0(8) . . . . ?
Na4 O5 B1 O1 79.9(9) 3_475 . . . ?
P1 O5 B1 O9 -34.0(14) . . . . ?
Na1 O5 B1 O9 113.1(9) . . . . ?
Na4 O5 B1 O9 -156.0(8) 3_475 . . . ?
P1 O5 B1 O7 81.5(11) . . . . ?
Na1 O5 B1 O7 -131.4(8) . . . . ?
Na4 O5 B1 O7 -40.5(8) 3_475 . . . ?
P1 O5 B1 Na1 -147.1(8) . . . . ?
Na4 O5 B1 Na1 90.9(3) 3_475 . . . ?
P1 O5 B1 Na1 31.5(19) . . . 4_654 ?
Na1 O5 B1 Na1 178.6(14) . . . 4_654 ?
Na4 O5 B1 Na1 -90.5(13) 3_475 . . 4_654 ?
P2 O9 B1 O1 -14.2(14) . . . . ?
Na2 O9 B1 O1 174.2(6) 4_554 . . . ?
Na1 O9 B1 O1 -94.6(10) 4_654 . . . ?
P2 O9 B1 O5 -136.7(8) . . . . ?
Na2 O9 B1 O5 51.7(13) 4_554 . . . ?
Na1 O9 B1 O5 142.8(9) 4_654 . . . ?
P2 O9 B1 O7 104.9(8) . . . . ?
Na2 O9 B1 O7 -66.7(11) 4_554 . . . ?
Na1 O9 B1 O7 24.5(7) 4_654 . . . ?
P2 O9 B1 Na1 -60.7(11) . . . . ?
Na2 O9 B1 Na1 127.6(6) 4_554 . . . ?
Na1 O9 B1 Na1 -141.2(6) 4_654 . . . ?
P2 O9 B1 Na1 80.4(7) . . . 4_654 ?
Na2 O9 B1 Na1 -91.2(8) 4_554 . . 4_654 ?
P3 O7 B1 O1 -2.1(13) . . . . ?
Li2 O7 B1 O1 -167.9(8) 4_554 . . . ?
Li1A O7 B1 O1 91.9(13) 4_654 . . . ?
Na1 O7 B1 O1 93.6(9) 4_654 . . . ?
P3 O7 B1 O5 117.5(8) . . . . ?
Li2 O7 B1 O5 -48.3(13) 4_554 . . . ?
Li1A O7 B1 O5 -148.5(12) 4_654 . . . ?
Na1 O7 B1 O5 -146.8(8) 4_654 . . . ?
P3 O7 B1 O9 -122.2(8) . . . . ?
Li2 O7 B1 O9 72.0(11) 4_554 . . . ?
Li1A O7 B1 O9 -28.2(13) 4_654 . . . ?
Na1 O7 B1 O9 -26.5(8) 4_654 . . . ?
P3 O7 B1 Na1 40.0(14) . . . . ?
Li2 O7 B1 Na1 -125.8(10) 4_554 . . . ?
Li1A O7 B1 Na1 134.1(13) 4_654 . . . ?
Na1 O7 B1 Na1 135.7(9) 4_654 . . . ?
P3 O7 B1 Na1 -95.7(7) . . . 4_654 ?
Li2 O7 B1 Na1 98.5(9) 4_554 . . 4_654 ?
Li1A O7 B1 Na1 -1.7(10) 4_654 . . 4_654 ?
B1 O1 B2 O2 64.2(12) . . . . ?
Li1A O1 B2 O2 -105(2) . . . . ?
Na1 O1 B2 O2 -127.6(10) . . . . ?
B1 O1 B2 O3 -177.1(9) . . . . ?
Li1A O1 B2 O3 14(2) . . . . ?
Na1 O1 B2 O3 -8.9(17) . . . . ?
B1 O1 B2 O4 -55.5(13) . . . . ?
Li1A O1 B2 O4 135(2) . . . . ?
Na1 O1 B2 O4 112.7(11) . . . . ?
B1 O1 B2 Li2 118.0(13) . . . 4_654 ?
Li1A O1 B2 Li2 -51(3) . . . 4_654 ?
Na1 O1 B2 Li2 -73.8(18) . . . 4_654 ?
B1 O1 B2 Na2 -109.4(11) . . . 4_654 ?
Li1A O1 B2 Na2 82(2) . . . 4_654 ?
Na1 O1 B2 Na2 58.9(16) . . . 4_654 ?
P3 O2 B2 O1 -16.4(13) . . . . ?
Li2 O2 B2 O1 136.5(10) 4_654 . . . ?
Na1 O2 B2 O1 -88.6(9) 4_654 . . . ?
P3 O2 B2 O3 -141.4(7) . . . . ?
Li2 O2 B2 O3 11.6(10) 4_654 . . . ?
Na1 O2 B2 O3 146.5(8) 4_654 . . . ?
P3 O2 B2 O4 106.0(9) . . . . ?
Li2 O2 B2 O4 -101.1(10) 4_654 . . . ?
Na1 O2 B2 O4 33.9(8) 4_654 . . . ?
P3 O2 B2 Li2 -152.9(10) . . . 4_654 ?
Na1 O2 B2 Li2 134.9(7) 4_654 . . 4_654 ?
P3 O2 B2 Na2 158.6(5) . . . 4_654 ?
Li2 O2 B2 Na2 -48.5(9) 4_654 . . 4_654 ?
Na1 O2 B2 Na2 86.5(6) 4_654 . . 4_654 ?
P1 O3 B2 O1 7.8(15) 1_655 . . . ?
Li2 O3 B2 O1 -133.7(11) 4_654 . . . ?
Na2 O3 B2 O1 129.0(9) 4_654 . . . ?
P1 O3 B2 O2 130.7(8) 1_655 . . . ?
Li2 O3 B2 O2 -10.8(10) 4_654 . . . ?
Na2 O3 B2 O2 -108.1(8) 4_654 . . . ?
P1 O3 B2 O4 -116.5(9) 1_655 . . . ?
Li2 O3 B2 O4 102.0(9) 4_654 . . . ?
Na2 O3 B2 O4 4.7(8) 4_654 . . . ?
P1 O3 B2 Li2 141.5(10) 1_655 . . 4_654 ?
Na2 O3 B2 Li2 -97.3(6) 4_654 . . 4_654 ?
P1 O3 B2 Na2 -121.2(8) 1_655 . . 4_654 ?
Li2 O3 B2 Na2 97.3(6) 4_654 . . 4_654 ?
P2 O4 B2 O1 3.0(13) . . . . ?
Na2 O4 B2 O1 -131.6(9) 4_654 . . . ?
Na1 O4 B2 O1 84.7(10) 4_654 . . . ?
P2 O4 B2 O2 -119.7(8) . . . . ?
Na2 O4 B2 O2 105.8(8) 4_654 . . . ?
Na1 O4 B2 O2 -37.9(9) 4_654 . . . ?
P2 O4 B2 O3 129.3(8) . . . . ?
Na2 O4 B2 O3 -5.2(9) 4_654 . . . ?
Na1 O4 B2 O3 -148.9(7) 4_654 . . . ?
P2 O4 B2 Li2 -172.5(7) . . . 4_654 ?
Na2 O4 B2 Li2 52.9(8) 4_654 . . 4_654 ?
Na1 O4 B2 Li2 -90.8(7) 4_654 . . 4_654 ?
P2 O4 B2 Na2 134.5(8) . . . 4_654 ?
Na1 O4 B2 Na2 -143.7(5) 4_654 . . 4_654 ?
O11 Na1 Li1A O1 88.2(19) 1_655 . . . ?
O7 Na1 Li1A O1 176(2) 4_655 . . . ?
O9 Na1 Li1A O1 166.2(17) 4_655 . . . ?
O4 Na1 Li1A O1 -128.2(12) 4_655 . . . ?
O5 Na1 Li1A O1 -56.0(6) . . . . ?
P2 Na1 Li1A O1 -165(4) 4_655 . . . ?
O13 Na1 Li1A O1 -125(5) 4_655 . . . ?
B1 Na1 Li1A O1 -26.5(5) . . . . ?
O2 Na1 Li1A O1 -126.3(12) 4_655 . . . ?
O1 Na1 Li1A O11 -88.2(19) . . . 1_655 ?
O7 Na1 Li1A O11 88.1(16) 4_655 . . 1_655 ?
O9 Na1 Li1A O11 78(3) 4_655 . . 1_655 ?
O4 Na1 Li1A O11 143.5(17) 4_655 . . 1_655 ?
O5 Na1 Li1A O11 -144.2(17) . . . 1_655 ?
P2 Na1 Li1A O11 107(5) 4_655 . . 1_655 ?
O13 Na1 Li1A O11 147(6) 4_655 . . 1_655 ?
B1 Na1 Li1A O11 -114.7(17) . . . 1_655 ?
O2 Na1 Li1A O11 145.5(19) 4_655 . . 1_655 ?
O1 Na1 Li1A O7 -176(2) . . . 4_655 ?
O11 Na1 Li1A O7 -88.1(16) 1_655 . . 4_655 ?
O9 Na1 Li1A O7 -10(4) 4_655 . . 4_655 ?
O4 Na1 Li1A O7 55(3) 4_655 . . 4_655 ?
O5 Na1 Li1A O7 127.7(18) . . . 4_655 ?
P2 Na1 Li1A O7 19(6) 4_655 . . 4_655 ?
O13 Na1 Li1A O7 58(4) 4_655 . . 4_655 ?
B1 Na1 Li1A O7 157.2(19) . . . 4_655 ?
O2 Na1 Li1A O7 57.4(15) 4_655 . . 4_655 ?
O1 Na1 Li1A O13 125(5) . . . 4_655 ?
O11 Na1 Li1A O13 -147(6) 1_655 . . 4_655 ?
O7 Na1 Li1A O13 -58(4) 4_655 . . 4_655 ?
O9 Na1 Li1A O13 -69(6) 4_655 . . 4_655 ?
O4 Na1 Li1A O13 -3(6) 4_655 . . 4_655 ?
O5 Na1 Li1A O13 69(5) . . . 4_655 ?
P2 Na1 Li1A O13 -40(9) 4_655 . . 4_655 ?
B1 Na1 Li1A O13 99(5) . . . 4_655 ?
O2 Na1 Li1A O13 -1(4) 4_655 . . 4_655 ?
O1 Na1 Li1A P3 149(3) . . . 4_655 ?
O11 Na1 Li1A P3 -122(3) 1_655 . . 4_655 ?
O7 Na1 Li1A P3 -34.3(11) 4_655 . . 4_655 ?
O9 Na1 Li1A P3 -44(4) 4_655 . . 4_655 ?
O4 Na1 Li1A P3 21(4) 4_655 . . 4_655 ?
O5 Na1 Li1A P3 93(2) . . . 4_655 ?
P2 Na1 Li1A P3 -15(7) 4_655 . . 4_655 ?
O13 Na1 Li1A P3 24(3) 4_655 . . 4_655 ?
B1 Na1 Li1A P3 123(2) . . . 4_655 ?
O2 Na1 Li1A P3 23.2(18) 4_655 . . 4_655 ?
O1 Na1 Li1A P1 -70.0(8) . . . 1_655 ?
O11 Na1 Li1A P1 18.2(13) 1_655 . . 1_655 ?
O7 Na1 Li1A P1 106.3(17) 4_655 . . 1_655 ?
O9 Na1 Li1A P1 96(2) 4_655 . . 1_655 ?
O4 Na1 Li1A P1 161.8(12) 4_655 . . 1_655 ?
O5 Na1 Li1A P1 -126.0(6) . . . 1_655 ?
P2 Na1 Li1A P1 125(4) 4_655 . . 1_655 ?
O13 Na1 Li1A P1 165(5) 4_655 . . 1_655 ?
B1 Na1 Li1A P1 -96.5(6) . . . 1_655 ?
O2 Na1 Li1A P1 163.7(9) 4_655 . . 1_655 ?
O1 Na1 Li1A Li2 -130(3) . . . 1_655 ?
O11 Na1 Li1A Li2 -41.3(15) 1_655 . . 1_655 ?
O7 Na1 Li1A Li2 46.7(12) 4_655 . . 1_655 ?
O9 Na1 Li1A Li2 37(4) 4_655 . . 1_655 ?
O4 Na1 Li1A Li2 102(3) 4_655 . . 1_655 ?
O5 Na1 Li1A Li2 174(3) . . . 1_655 ?
P2 Na1 Li1A Li2 66(7) 4_655 . . 1_655 ?
O13 Na1 Li1A Li2 105(5) 4_655 . . 1_655 ?
B1 Na1 Li1A Li2 -156(3) . . . 1_655 ?
O2 Na1 Li1A Li2 104(2) 4_655 . . 1_655 ?
O1 Na1 Li1A Na4 -44(7) . . . . ?
O11 Na1 Li1A Na4 44(7) 1_655 . . . ?
O7 Na1 Li1A Na4 132(9) 4_655 . . . ?
O9 Na1 Li1A Na4 122(6) 4_655 . . . ?
O4 Na1 Li1A Na4 -173(6) 4_655 . . . ?
O5 Na1 Li1A Na4 -100(8) . . . . ?
P2 Na1 Li1A Na4 151(5) 4_655 . . . ?
O13 Na1 Li1A Na4 -170(12) 4_655 . . . ?
B1 Na1 Li1A Na4 -71(8) . . . . ?
O2 Na1 Li1A Na4 -171(8) 4_655 . . . ?
O1 Na1 Li1A Na4 69(3) . . . 3_475 ?
O11 Na1 Li1A Na4 157(5) 1_655 . . 3_475 ?
O7 Na1 Li1A Na4 -115(5) 4_655 . . 3_475 ?
O9 Na1 Li1A Na4 -125(2) 4_655 . . 3_475 ?
O4 Na1 Li1A Na4 -60(4) 4_655 . . 3_475 ?
O5 Na1 Li1A Na4 13(3) . . . 3_475 ?
P2 Na1 Li1A Na4 -96(3) 4_655 . . 3_475 ?
O13 Na1 Li1A Na4 -57(6) 4_655 . . 3_475 ?
B1 Na1 Li1A Na4 42(3) . . . 3_475 ?
O2 Na1 Li1A Na4 -58(4) 4_655 . . 3_475 ?
O1 Na1 Li1A Na2 -117.9(14) . . . 1_655 ?
O11 Na1 Li1A Na2 -30(3) 1_655 . . 1_655 ?
O7 Na1 Li1A Na2 58(3) 4_655 . . 1_655 ?
O9 Na1 Li1A Na2 48.3(10) 4_655 . . 1_655 ?
O4 Na1 Li1A Na2 114(2) 4_655 . . 1_655 ?
O5 Na1 Li1A Na2 -173.9(17) . . . 1_655 ?
P2 Na1 Li1A Na2 77(3) 4_655 . . 1_655 ?
O13 Na1 Li1A Na2 117(5) 4_655 . . 1_655 ?
B1 Na1 Li1A Na2 -144.4(16) . . . 1_655 ?
O2 Na1 Li1A Na2 115.8(19) 4_655 . . 1_655 ?

_refine_diff_density_max         0.447
_refine_diff_density_min         -0.478
_refine_diff_density_rms         0.106



