# Supplementary Information (SI) for Dalton Transactions.
# This journal is © The Royal Society of Chemistry 2024

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
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data_lcy03-5_pl
_database_code_depnum_ccdc_archive 'CCDC 2360227'
loop_
_audit_author_name
_audit_author_address
'Junseong Lee'
;Chonnam National University
South Korea
;
_audit_update_record             
;
2024-06-03 deposited with the CCDC.	2024-08-29 downloaded from the CCDC.
;
_audit_creation_date             2021-11-30
_audit_creation_method           
;
Olex2 1.5
(compiled 2021.11.18 svn.ra9532c28 for OlexSys, GUI svn.r6429)
;
_shelxl_version_number           2014-3
_chemical_name_common            ?
_chemical_name_systematic        
;
 ?
;
_chemical_formula_moiety         'C52 H32 F6 N4 Si Zn, 4(C H Cl3)'
_chemical_formula_sum            'C56 H36 Cl12 F6 N4 Si Zn'
_chemical_formula_weight         1397.75
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Zn Zn 0.2839 1.4301 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      tetragonal
_space_group_IT_number           142
_space_group_name_H-M_alt        'I 41/a c d'
_space_group_name_Hall           '-I 4bd 2c'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-y+1/4, x+3/4, z+1/4'
'-x+1/2, -y, z+1/2'
'y+1/4, -x+1/4, z+3/4'
'x, -y, -z+1/2'
'y+1/4, x+3/4, -z+3/4'
'-x+1/2, y, -z'
'-y+1/4, -x+1/4, -z+1/4'
'x+1/2, y+1/2, z+1/2'
'-y+3/4, x+5/4, z+3/4'
'-x+1, -y+1/2, z+1'
'y+3/4, -x+3/4, z+5/4'
'x+1/2, -y+1/2, -z+1'
'y+3/4, x+5/4, -z+5/4'
'-x+1, y+1/2, -z+1/2'
'-y+3/4, -x+3/4, -z+3/4'
'-x, -y, -z'
'y-1/4, -x-3/4, -z-1/4'
'x-1/2, y, -z-1/2'
'-y-1/4, x-1/4, -z-3/4'
'-x, y, z-1/2'
'-y-1/4, -x-3/4, z-3/4'
'x-1/2, -y, z'
'y-1/4, x-1/4, z-1/4'
'-x+1/2, -y+1/2, -z+1/2'
'y+1/4, -x-1/4, -z+1/4'
'x, y+1/2, -z'
'-y+1/4, x+1/4, -z-1/4'
'-x+1/2, y+1/2, z'
'-y+1/4, -x-1/4, z-1/4'
'x, -y+1/2, z+1/2'
'y+1/4, x+1/4, z+1/4'

_cell_length_a                   28.0983(6)
_cell_length_b                   28.0983(6)
_cell_length_c                   14.9330(3)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_volume                     11789.8(6)
_cell_formula_units_Z            8
_cell_measurement_reflns_used    7490
_cell_measurement_temperature    100
_cell_measurement_theta_max      25.512
_cell_measurement_theta_min      2.895
_shelx_estimated_absorpt_T_max   0.903
_shelx_estimated_absorpt_T_min   0.903
_exptl_absorpt_coefficient_mu    1.042
_exptl_absorpt_correction_T_max  0.7452
_exptl_absorpt_correction_T_min  0.5185
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
SADABS-2014/2 (Bruker,2014/2) was used for absorption correction.
wR2(int) was 0.1014 before and 0.0639 after correction.
The Ratio of minimum to maximum transmission is 0.6958.
The λ/2 correction factor is 0.00150.
;
_exptl_crystal_colour            ?
_exptl_crystal_density_diffrn    1.575
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             5616
_exptl_crystal_size_max          0.1
_exptl_crystal_size_mid          0.1
_exptl_crystal_size_min          0.1
_exptl_special_details           
;
 ?
;
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.3365
_diffrn_reflns_av_unetI/netI     0.0854
_diffrn_reflns_Laue_measured_fraction_full 0.998
_diffrn_reflns_Laue_measured_fraction_max 0.998
_diffrn_reflns_limit_h_max       33
_diffrn_reflns_limit_h_min       -34
_diffrn_reflns_limit_k_max       34
_diffrn_reflns_limit_k_min       -34
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_number            77527
_diffrn_reflns_point_group_measured_fraction_full 0.998
_diffrn_reflns_point_group_measured_fraction_max 0.998
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         25.731
_diffrn_reflns_theta_min         2.118
_diffrn_ambient_temperature      100
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_diffrn_source_current           30.0
_diffrn_source_power             1.5
_diffrn_source_voltage           50.0
_diffrn_standards_number         0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                1088
_reflns_number_total             2815
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT v8.34A (Bruker, 2013)'
_computing_data_collection       ?
_computing_data_reduction        'SAINT v8.34A (Bruker, 2013)'
_computing_molecular_graphics    'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_structure_refinement  'XL  (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS-1997  (Sheldrick, 2008)'
_refine_diff_density_max         0.990
_refine_diff_density_min         -0.664
_refine_diff_density_rms         0.118
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.028
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     186
_refine_ls_number_reflns         2815
_refine_ls_number_restraints     6
_refine_ls_R_factor_all          0.2037
_refine_ls_R_factor_gt           0.0785
_refine_ls_restrained_S_all      1.028
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.1214P)²+62.6277P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2041
_refine_ls_wR_factor_ref         0.2773
_refine_special_details          
;
 ?
;
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups
2. Uiso/Uaniso restraints and constraints
Uanis(C8) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
3.a Ternary CH refined with riding coordinates:
 C17(H17)
3.b Aromatic/amide H refined with riding coordinates:
 C2(H2), C15(H15), C1(H1), C5(H5), C12(H12), C7(H7), C8(H8), C16(H16)
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Zn1 Zn 0.0000 0.2500 0.1250 0.0225(5) Uani 1 4 d S T P . .
Si1 Si 0.0000 0.2500 -0.1250 0.0247(9) Uani 1 4 d S T P . .
F1 F 0.0000 0.2500 -0.0121(4) 0.0347(14) Uani 1 2 d S T P . .
F2 F 0.05894(15) 0.24354(18) -0.1244(5) 0.0438(13) Uani 1 1 d . . . . .
N1 N 0.0544(2) 0.1956(2) 0.1250 0.028(2) Uani 1 2 d S T P . .
N2 N -0.0537(2) 0.1963(2) 0.1250 0.026(2) Uani 1 2 d S T P . .
C14 C 0.3757(3) -0.1257(3) 0.1250 0.029(3) Uani 1 2 d S T P . .
C4 C 0.1619(3) 0.0881(3) 0.1250 0.026(3) Uani 1 2 d S T P . .
C2 C 0.0873(4) 0.1244(4) 0.0624(7) 0.039(3) Uani 1 1 d . . . . .
H2 H 0.0852 0.0994 0.0198 0.047 Uiso 1 1 calc R U . . .
C13 C 0.3385(3) -0.0885(3) 0.1250 0.034(3) Uani 1 2 d S T P . .
C15 C -0.0895(3) 0.1975(3) 0.0664(7) 0.031(2) Uani 1 1 d . . . . .
H15 H -0.0905 0.2227 0.0239 0.038 Uiso 1 1 calc R U . . .
C3 C 0.1245(3) 0.1255(3) 0.1250 0.035(3) Uani 1 2 d S T P . .
C1 C 0.0539(3) 0.1602(3) 0.0640(7) 0.031(2) Uani 1 1 d . . . . .
H1 H 0.0293 0.1600 0.0202 0.037 Uiso 1 1 calc R U . . .
C6 C 0.2450(3) 0.0666(3) 0.1310(8) 0.030(2) Uani 1 1 d . . . . .
C9 C 0.3171(3) -0.0054(3) 0.1314(8) 0.030(2) Uani 1 1 d . . . . .
C5 C 0.2093(3) 0.1014(3) 0.1336(7) 0.031(2) Uani 1 1 d . . . . .
H5 H 0.2175 0.1339 0.1412 0.038 Uiso 1 1 calc R U . . .
C12 C 0.3513(3) -0.0410(3) 0.1306(8) 0.031(2) Uani 1 1 d . . . . .
H12 H 0.3840 -0.0327 0.1340 0.038 Uiso 1 1 calc R U . . .
C10 C 0.2686(3) -0.0186(3) 0.1250 0.027(3) Uani 1 2 d S T P . .
C11 C 0.2325(3) 0.0175(3) 0.1250 0.029(3) Uani 1 2 d S T P . .
C7 C 0.2948(3) 0.0786(3) 0.1366(8) 0.040(3) Uani 1 1 d . . . . .
H7 H 0.3038 0.1111 0.1405 0.048 Uiso 1 1 calc R U . . .
C8 C 0.3292(3) 0.0447(3) 0.1362(8) 0.038(2) Uani 1 1 d . U . . .
H8 H 0.3617 0.0539 0.1393 0.046 Uiso 1 1 calc R U . . .
C16 C -0.1246(3) 0.1643(3) 0.0649(7) 0.032(2) Uani 1 1 d . . . . .
H16 H -0.1498 0.1671 0.0227 0.038 Uiso 1 1 calc R U . . .
Cl3 Cl -0.03647(11) 0.04269(12) 0.3728(3) 0.0832(11) Uani 1 1 d . . . . .
Cl1 Cl 0.04379(12) 0.07413(14) 0.4739(2) 0.0831(12) Uani 1 1 d . . . . .
C17 C 0.0118(3) 0.0826(4) 0.3750(9) 0.054(3) Uani 1 1 d . . . . .
H17 H -0.0005 0.1160 0.3731 0.065 Uiso 1 1 calc R U . . .
Cl2 Cl 0.04763(13) 0.07239(15) 0.2811(3) 0.0912(13) Uani 1 1 d . . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Zn1 F1 2.048(6) 14_444 ?
Zn1 F1 2.048(6) . ?
Zn1 N1 2.163(9) 11_454 ?
Zn1 N1 2.163(9) . ?
Zn1 N2 2.133(8) 11_454 ?
Zn1 N2 2.134(8) . ?
Si1 F1 1.685(6) . ?
Si1 F1 1.685(6) 18_565 ?
Si1 F2 1.666(4) . ?
Si1 F2 1.666(4) 28 ?
Si1 F2 1.666(4) 18_565 ?
Si1 F2 1.666(4) 11_454 ?
N1 C1 1.348(10) 8 ?
N1 C1 1.348(10) . ?
N2 C15 1.335(10) 14_444 ?
N2 C15 1.335(10) . ?
C14 C13 1.479(15) . ?
C14 C16 1.407(10) 23_655 ?
C14 C16 1.407(10) 26 ?
C4 C3 1.484(14) . ?
C4 C5 1.389(9) 8 ?
C4 C5 1.389(9) . ?
C2 H2 0.9500 . ?
C2 C3 1.403(11) . ?
C2 C1 1.377(13) . ?
C13 C12 1.384(9) 8 ?
C13 C12 1.384(9) . ?
C15 H15 0.9500 . ?
C15 C16 1.358(12) . ?
C3 C2 1.403(11) 8 ?
C1 H1 0.9500 . ?
C6 C5 1.401(11) . ?
C6 C11 1.425(9) . ?
C6 C7 1.442(11) . ?
C9 C12 1.389(11) . ?
C9 C10 1.416(9) . ?
C9 C8 1.449(11) . ?
C5 H5 0.9500 . ?
C12 H12 0.9500 . ?
C10 C9 1.416(9) 8 ?
C10 C11 1.435(13) . ?
C11 C6 1.425(9) 8 ?
C7 H7 0.9500 . ?
C7 C8 1.358(10) . ?
C8 H8 0.9500 . ?
C16 C14 1.407(10) 20_556 ?
C16 H16 0.9500 . ?
Cl3 C17 1.760(9) . ?
Cl1 C17 1.745(13) . ?
C17 H17 1.0000 . ?
C17 Cl2 1.750(12) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
F1 Zn1 F1 180.0 14_444 . ?
F1 Zn1 N1 90.0 14_444 . ?
F1 Zn1 N1 90.0 . . ?
F1 Zn1 N1 90.0 . 11_454 ?
F1 Zn1 N1 90.0 14_444 11_454 ?
F1 Zn1 N2 90.0 14_444 11_454 ?
F1 Zn1 N2 90.0 . 11_454 ?
F1 Zn1 N2 90.0 14_444 . ?
F1 Zn1 N2 90.0 . . ?
N1 Zn1 N1 180.0(2) 11_454 . ?
N2 Zn1 N1 90.0 . 11_454 ?
N2 Zn1 N1 90.0 . . ?
N2 Zn1 N1 89.999(1) 11_454 . ?
N2 Zn1 N1 90.001(1) 11_454 11_454 ?
N2 Zn1 N2 180.0 11_454 . ?
F1 Si1 F1 180.0 . 18_565 ?
F2 Si1 F1 90.3(3) 28 . ?
F2 Si1 F1 90.3(3) . 18_565 ?
F2 Si1 F1 89.7(3) 11_454 . ?
F2 Si1 F1 90.3(3) 11_454 18_565 ?
F2 Si1 F1 89.7(3) . . ?
F2 Si1 F1 90.3(3) 18_565 . ?
F2 Si1 F1 89.7(3) 18_565 18_565 ?
F2 Si1 F1 89.7(3) 28 18_565 ?
F2 Si1 F2 90.002(4) 18_565 11_454 ?
F2 Si1 F2 90.004(4) 18_565 . ?
F2 Si1 F2 90.000(4) 28 . ?
F2 Si1 F2 179.4(6) 28 18_565 ?
F2 Si1 F2 90.002(4) 28 11_454 ?
F2 Si1 F2 179.4(6) 11_454 . ?
Si1 F1 Zn1 180.0 . . ?
C1 N1 Zn1 120.8(5) 8 . ?
C1 N1 Zn1 120.8(5) . . ?
C1 N1 C1 118.3(10) 8 . ?
C15 N2 Zn1 121.0(5) 14_444 . ?
C15 N2 Zn1 121.0(5) . . ?
C15 N2 C15 117.9(10) 14_444 . ?
C16 C14 C13 122.7(5) 26 . ?
C16 C14 C13 122.7(5) 23_655 . ?
C16 C14 C16 114.6(11) 23_655 26 ?
C5 C4 C3 119.2(5) . . ?
C5 C4 C3 119.2(5) 8 . ?
C5 C4 C5 121.5(10) . 8 ?
C3 C2 H2 120.6 . . ?
C1 C2 H2 120.6 . . ?
C1 C2 C3 118.8(10) . . ?
C12 C13 C14 119.8(5) . . ?
C12 C13 C14 119.8(5) 8 . ?
C12 C13 C12 120.3(10) 8 . ?
N2 C15 H15 118.6 . . ?
N2 C15 C16 122.7(9) . . ?
C16 C15 H15 118.6 . . ?
C2 C3 C4 120.8(6) 8 . ?
C2 C3 C4 120.8(6) . . ?
C2 C3 C2 118.4(12) . 8 ?
N1 C1 C2 122.8(9) . . ?
N1 C1 H1 118.6 . . ?
C2 C1 H1 118.6 . . ?
C5 C6 C11 120.0(8) . . ?
C5 C6 C7 122.0(8) . . ?
C11 C6 C7 118.0(8) . . ?
C12 C9 C10 118.5(7) . . ?
C12 C9 C8 122.5(8) . . ?
C10 C9 C8 119.0(8) . . ?
C4 C5 C6 119.8(8) . . ?
C4 C5 H5 120.1 . . ?
C6 C5 H5 120.1 . . ?
C13 C12 C9 121.1(8) . . ?
C13 C12 H12 119.5 . . ?
C9 C12 H12 119.5 . . ?
C9 C10 C9 120.6(10) 8 . ?
C9 C10 C11 119.7(5) 8 . ?
C9 C10 C11 119.7(5) . . ?
C6 C11 C6 118.8(10) . 8 ?
C6 C11 C10 120.6(5) . . ?
C6 C11 C10 120.6(5) 8 . ?
C6 C7 H7 119.1 . . ?
C8 C7 C6 121.8(9) . . ?
C8 C7 H7 119.1 . . ?
C9 C8 H8 119.5 . . ?
C7 C8 C9 120.9(9) . . ?
C7 C8 H8 119.5 . . ?
C14 C16 H16 119.5 20_556 . ?
C15 C16 C14 121.0(9) . 20_556 ?
C15 C16 H16 119.5 . . ?
Cl3 C17 H17 109.3 . . ?
Cl1 C17 Cl3 109.0(7) . . ?
Cl1 C17 H17 109.3 . . ?
Cl1 C17 Cl2 111.1(6) . . ?
Cl2 C17 Cl3 108.9(7) . . ?
Cl2 C17 H17 109.3 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Zn1 N1 C1 C2 -178.9(7) . . . . ?
Zn1 N2 C15 C16 -179.3(7) . . . . ?
N2 C15 C16 C14 -1.5(14) . . . 20_556 ?
C14 C13 C12 C9 -179.6(9) . . . . ?
C15 N2 C15 C16 0.7(7) 14_444 . . . ?
C3 C4 C5 C6 -178.1(8) . . . . ?
C3 C2 C1 N1 -2.2(14) . . . . ?
C1 N1 C1 C2 1.1(7) 8 . . . ?
C1 C2 C3 C4 -179.0(7) . . . . ?
C1 C2 C3 C2 1.1(7) . . . 8 ?
C6 C7 C8 C9 -1(2) . . . . ?
C9 C10 C11 C6 0.2(10) 8 . . 8 ?
C9 C10 C11 C6 0.2(10) . . . . ?
C9 C10 C11 C6 -179.8(10) . . . 8 ?
C9 C10 C11 C6 -179.8(10) 8 . . . ?
C5 C4 C3 C2 135.3(7) . . . . ?
C5 C4 C3 C2 -44.7(7) 8 . . . ?
C5 C4 C3 C2 135.3(7) 8 . . 8 ?
C5 C4 C3 C2 -44.7(7) . . . 8 ?
C5 C4 C5 C6 1.9(8) 8 . . . ?
C5 C6 C11 C6 1.9(8) . . . 8 ?
C5 C6 C11 C10 -178.1(8) . . . . ?
C5 C6 C7 C8 178.4(12) . . . . ?
C12 C13 C12 C9 0.4(9) 8 . . . ?
C12 C9 C10 C9 0.4(9) . . . 8 ?
C12 C9 C10 C11 -179.6(9) . . . . ?
C12 C9 C8 C7 179.8(13) . . . . ?
C10 C9 C12 C13 -0.8(17) . . . . ?
C10 C9 C8 C7 1.3(19) . . . . ?
C11 C6 C5 C4 -3.7(16) . . . . ?
C11 C6 C7 C8 -0.1(19) . . . . ?
C7 C6 C5 C4 177.8(9) . . . . ?
C7 C6 C11 C6 -179.6(13) . . . 8 ?
C7 C6 C11 C10 0.4(13) . . . . ?
C8 C9 C12 C13 -179.4(10) . . . . ?
C8 C9 C10 C9 179.0(13) . . . 8 ?
C8 C9 C10 C11 -1.0(13) . . . . ?
C16 C14 C13 C12 -134.7(7) 23_655 . . . ?
C16 C14 C13 C12 -134.7(7) 26 . . 8 ?
C16 C14 C13 C12 45.3(7) 23_655 . . 8 ?
C16 C14 C13 C12 45.3(7) 26 . . . ?

_olex2_submission_special_instructions 'No special instructions were received'
