# Electronic Supplementary Material (ESI) for Nanoscale.
# This journal is © The Royal Society of Chemistry 2024

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
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data_test_sq
_audit_block_doi                 10.5517/ccdc.csd.cc2jnp0x
_database_code_depnum_ccdc_archive 'CCDC 2343569'
loop_
_audit_author_name
_audit_author_address
AgCu
;Beijing Institute of Technology
China
;
_audit_update_record             
;
2024-03-27 deposited with the CCDC.	2024-05-27 downloaded from the CCDC.
;
_audit_creation_date             2024-03-25
_audit_creation_method           
;
Olex2 1.3
(compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6408)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         
'C195 H231.185 Ag22 Cl Cu O34 P12 S11 Si W9, 2(F6 Sb)'
_chemical_formula_sum            
'C195 H231.18 Ag22 Cl Cu F12 O34 P12 S11 Sb2 Si W9'
_chemical_formula_weight         8469.64
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
W W -0.8490 6.8722 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_H-M_alt        'P 1 21/n 1'
_space_group_name_Hall           '-P 2yn'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'

_cell_length_a                   20.8060(3)
_cell_length_b                   32.6834(5)
_cell_length_c                   41.5251(8)
_cell_angle_alpha                90
_cell_angle_beta                 98.7177(16)
_cell_angle_gamma                90
_cell_volume                     27911.3(8)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    71905
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      25.9660
_cell_measurement_theta_min      2.0620
_shelx_estimated_absorpt_T_max   0.412
_shelx_estimated_absorpt_T_min   0.382
_exptl_absorpt_coefficient_mu    5.681
_exptl_absorpt_correction_T_max  ?
_exptl_absorpt_correction_T_min  ?
_exptl_absorpt_correction_type   ?
_exptl_absorpt_process_details   ?
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            'clear brownish red'
_exptl_crystal_colour_lustre     clear
_exptl_crystal_colour_modifier   brownish
_exptl_crystal_colour_primary    red
_exptl_crystal_density_diffrn    2.016
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             15997
_exptl_crystal_size_max          0.21
_exptl_crystal_size_mid          0.2
_exptl_crystal_size_min          0.19
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0661
_diffrn_reflns_av_unetI/netI     0.0602
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.999
_diffrn_reflns_limit_h_max       24
_diffrn_reflns_limit_h_min       -24
_diffrn_reflns_limit_k_max       38
_diffrn_reflns_limit_k_min       -38
_diffrn_reflns_limit_l_max       49
_diffrn_reflns_limit_l_min       -47
_diffrn_reflns_number            236237
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.999
_diffrn_reflns_theta_full        25.000
_diffrn_reflns_theta_max         25.000
_diffrn_reflns_theta_min         1.934
_diffrn_ambient_temperature      293(2)
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'XtaLAB Synergy R, DW system, HyPix'
_diffrn_measurement_method       ?
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                31327
_reflns_number_total             49117
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       ?
_computing_data_collection       ?
_computing_data_reduction        ?
_computing_molecular_graphics    'Olex2 1.3 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.3 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2018/3 (Sheldrick, 2015)'
_computing_structure_solution    ?
_refine_diff_density_max         6.898
_refine_diff_density_min         -6.663
_refine_diff_density_rms         0.329
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.028
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     2453
_refine_ls_number_reflns         49117
_refine_ls_number_restraints     4635
_refine_ls_R_factor_all          0.1655
_refine_ls_R_factor_gt           0.1165
_refine_ls_restrained_S_all      1.032
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.1600P)²+1407.8883P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2989
_refine_ls_wR_factor_ref         0.3435
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups, All C(H,H) groups
 At 1.5 times of:
  All C(H,H,H) groups
2. Restrained distances
 C322-C323 = C323-C324
 1.5 with sigma of 0.02
 C313-C314 = C314-C315
 1.5 with sigma of 0.02
 C303-C305 = C309-C311 = C319-C321
 2.2 with sigma of 0.02
 C309-C310 = C310-C311
 1.5 with sigma of 0.02
 C326-C327 = C316-C317 = C317-C318
 1.5 with sigma of 0.02
 S2-C311
 2.8 with sigma of 0.02
 C301-C300 = C300-C302
 1.5 with sigma of 0.02
 P18-C316
 1.9 with sigma of 0.02
 P18-C91
 1.8 with sigma of 0.02
 P21-C114
 2.7 with sigma of 0.02
 Ag7-S7
 2.5 with sigma of 0.02
 F131-F86
 2.4 with sigma of 0.02
 C164-C166
 1.54 with sigma of 0.02
 C150-C148
 1.54 with sigma of 0.02
 C320-C319 = C321-C320
 1.54 with sigma of 0.02
 C321-C320 = C320-C319
 1.54 with sigma of 0.02
 C149-C148
 1.54 with sigma of 0.02
 S7-C164
 1.7 with sigma of 0.02
 C153-C152 = C152-C151
 1.54 with sigma of 0.02
 Ag2-S8
 2 with sigma of 0.02
 Sb1-F56 \\sim Sb1-F97 \\sim Sb1-F110 \\sim Sb1-F124 \\sim Sb1-F145 \\sim
Sb1-F213
 with sigma of 0.02
 Sb2-F86 \\sim Sb2-F131 \\sim Sb2-F161 \\sim Sb2-F174 \\sim Sb2-F185 \\sim
Sb2-F134
 with sigma of 0.02
 F56-F97 \\sim F56-F110 \\sim F56-F145 \\sim F56-F213 \\sim F97-F110 \\sim
F97-F124 \\sim F97-F145 ~
 F110-F124 \\sim F110-F213 \\sim F124-F145 \\sim F124-F213 \\sim F145-F213
 with sigma of 0.04
 F86-F131 \\sim F86-F174 \\sim F86-F185 \\sim F86-F134 \\sim F131-F161 \\sim
F131-F174 \\sim F131-F134
 \\sim F161-F174 \\sim F161-F185 \\sim F161-F134 \\sim F174-F185 \\sim F185-F134
 with sigma of 0.04
3. Restrained planarity
 P21, C109, C110, C111, C112, C113, C114
 with sigma of 0.1
 P13, C121, C122, C123, C124, C125, C126
 with sigma of 0.1
 P13, C127, C128, C129, C130, C131, C132
 with sigma of 0.1
 P21, C139, C140, C141, C142, C143, C144
 with sigma of 0.1
 P18, C91, C92, C93, C94, C95, C96
 with sigma of 0.1
4. Rigid bond restraints
 Sb2, F86, F131, F161, F174, F185, F134
 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01
 Sb1, F56, F97, F110, F124, F145, F213
 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01
5. Uiso/Uaniso restraints and constraints
F56 \\sim F86 \\sim F97 \\sim F110 \\sim F124 \\sim F131 \\sim F145 \\sim F161
\\sim F174 \\sim F213 \\sim F185 \\sim F134: within 2A with sigma of 0.01 and
sigma for terminal atoms of 0.02 within 2A
C30A \\sim C30B \\sim C1 \\sim C2 \\sim C3 \\sim C4 \\sim C5 \\sim C6 \\sim C7
\\sim C8 \\sim C9 \\sim C10 \\sim C11 \\sim C12 \\sim C13 \\sim C14 \\sim C15
\\sim C16 \\sim C17 \\sim C18 \\sim C19 \\sim C20 \\sim C21 \\sim C22 \\sim C23
\\sim C24 \\sim C25 \\sim C26 \\sim C27 \\sim C28 \\sim C29 \\sim C30 \\sim C31
\\sim C32 \\sim C33 \\sim C34 \\sim C35 \\sim C36 \\sim C37 \\sim C38 \\sim C39
\\sim C40 \\sim C41 \\sim C42 \\sim C43 \\sim C44 \\sim C45 \\sim C46 \\sim C47
\\sim C48 \\sim C49 \\sim C50 \\sim C51 \\sim C52 \\sim C53 \\sim C54 \\sim C55
\\sim C56 \\sim C57 \\sim C58 \\sim C59 \\sim C60 \\sim C61 \\sim C62 \\sim C63
\\sim C64 \\sim C65 \\sim C66 \\sim C67 \\sim C68 \\sim C69 \\sim C70 \\sim C71
\\sim C72 \\sim C73 \\sim C74 \\sim C75 \\sim C76 \\sim C77 \\sim C78 \\sim C79
\\sim C80 \\sim C81 \\sim C82 \\sim C83 \\sim C84 \\sim C85 \\sim C86 \\sim C87
\\sim C88 \\sim C89 \\sim C90 \\sim C91 \\sim C92 \\sim C93 \\sim C94 \\sim C95
\\sim C96 \\sim C97 \\sim C98 \\sim C99 \\sim C100 \\sim C101 \\sim C102 \\sim
C103 \\sim C104 \\sim C105 \\sim C106 \\sim C107 \\sim C108 \\sim C109 \\sim
C110 \\sim C111 \\sim C112 \\sim C113 \\sim C114 \\sim C115 \\sim C116 \\sim
C117 \\sim C118 \\sim C119 \\sim C120 \\sim C121 \\sim C122 \\sim C123 \\sim
C124 \\sim C125 \\sim C126 \\sim C127 \\sim C128 \\sim C129 \\sim C130 \\sim
C131 \\sim C132 \\sim C133 \\sim C134 \\sim C135 \\sim C136 \\sim C137 \\sim
C138 \\sim C139 \\sim C140 \\sim C141 \\sim C142 \\sim C143 \\sim C144 \\sim
C300 \\sim C301 \\sim C302 \\sim C303 \\sim C304 \\sim C305 \\sim C313 \\sim
C314 \\sim C315 \\sim C316 \\sim C317 \\sim C318 \\sim C319 \\sim C320 \\sim
C321 \\sim C322 \\sim C323 \\sim C324 \\sim C309 \\sim C310 \\sim C311 \\sim
C325 \\sim C326 \\sim C327 \\sim C328 \\sim C329 \\sim C146 \\sim C157 \\sim
C145 \\sim C171 \\sim C201 \\sim C147 \\sim C154 \\sim C156 \\sim C151 \\sim
C148 \\sim C149 \\sim C155 \\sim C152 \\sim C150 \\sim C153 \\sim C161 \\sim
C160 \\sim C159 \\sim C158 \\sim C163 \\sim C162 \\sim C165 \\sim C164 \\sim
C166: within 4A with sigma of 0.01 and sigma for terminal atoms of 0.02 within
4A
Uanis(Sb2) \\sim Ueq, Uanis(Sb1) \\sim Ueq: with sigma of 0.002 and sigma for
terminal atoms of 0.004
Uanis(Ag1A) \\sim Ueq, Uanis(Ag2A) \\sim Ueq, Uanis(Ag3A) \\sim Ueq,
Uanis(Ag1B) \\sim Ueq, Uanis(Ag2B) \\sim Ueq, Uanis(Ag3B) \\sim Ueq, Uanis(Ag4)
\\sim Ueq, Uanis(Ag5A) \\sim Ueq, Uanis(Ag5B) \\sim Ueq, Uanis(Ag6) \\sim Ueq,
Uanis(Ag7) \\sim Ueq, Uanis(Ag8A) \\sim Ueq, Uanis(Ag8B) \\sim Ueq, Uanis(Ag9A)
\\sim Ueq, Uanis(Ag9B) \\sim Ueq, Uanis(Ag10) \\sim Ueq, Uanis(Ag11) \\sim Ueq,
Uanis(Ag12) \\sim Ueq, Uanis(Ag13) \\sim Ueq, Uanis(Ag14) \\sim Ueq,
Uanis(Ag15) \\sim Ueq, Uanis(Ag18) \\sim Ueq, Uanis(Ag19) \\sim Ueq,
Uanis(Ag20) \\sim Ueq, Uanis(Ag35) \\sim Ueq, Uanis(Ag38) \\sim Ueq,
Uanis(Ag39) \\sim Ueq, Uanis(Ag41) \\sim Ueq, Uanis(Ag1) \\sim Ueq, Uanis(Ag2)
\\sim Ueq, Uanis(Ag3) \\sim Ueq, Uanis(S4) \\sim Ueq, Uanis(S10) \\sim Ueq:
with sigma of 0.005 and sigma for terminal atoms of 0.01
Uanis(F145) \\sim Ueq, Uanis(F56) \\sim Ueq, Uanis(F213) \\sim Ueq, Uanis(F124)
\\sim Ueq, Uanis(F97) \\sim Ueq, Uanis(F110) \\sim Ueq: with sigma of 0.001 and
sigma for terminal atoms of 0.002
Uanis(O1) \\sim Ueq, Uanis(O2) \\sim Ueq, Uanis(O3) \\sim Ueq, Uanis(O4) \\sim
Ueq, Uanis(O5) \\sim Ueq, Uanis(O6) \\sim Ueq, Uanis(O17) \\sim Ueq, Uanis(O19)
\\sim Ueq, Uanis(P18) \\sim Ueq, Uanis(P19) \\sim Ueq, Uanis(P20) \\sim Ueq,
Uanis(P21) \\sim Ueq: with sigma of 0.005 and sigma for terminal atoms of 0.01
Uanis(Ag15) \\sim Ueq: with sigma of 0.003 and sigma for terminal atoms of 0.006
Uanis(S9B) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(F185) \\sim Ueq, Uanis(F86) \\sim Ueq, Uanis(F134) \\sim Ueq, Uanis(F131)
\\sim Ueq, Uanis(F174) \\sim Ueq, Uanis(F161) \\sim Ueq: with sigma of 0.01 and
sigma for terminal atoms of 0.02
Uanis(Ag3A) = Uanis(Ag3B)
Uanis(Ag2) = Uanis(Ag41)
Uanis(Cu6A) = Uanis(Cu6B)
Uanis(Ag1) = Uanis(Ag39)
Uanis(Ag5A) = Uanis(Ag5B)
Uanis(Ag2A) = Uanis(Ag2B)
Uanis(Ag1A) = Uanis(Ag1B)
Uanis(Ag9A) = Uanis(Ag9B)
Uanis(Ag8A) = Uanis(Ag8B)
Uanis(S7) = Uanis(S10)
Uanis(S8) = Uanis(S11)
Uanis(C152) = Uanis(C320)
Uanis(S10) = Uanis(S5)
Uanis(F213) = Uanis(F97)
Uanis(F185) = Uanis(F131)
6. Same fragment restrains
{C309, C310, C311, S2} sigma for 1-2: 0.02, 1-3: 0.04
as in
{C325, C326, C327, S4}
7. Others
 Sof(Ag1B)=Sof(Ag2B)=Sof(Ag3B)=1-FVAR(1)
 Sof(Ag1A)=Sof(Ag2A)=Sof(Ag3A)=FVAR(1)
 Sof(C30B)=Sof(H30C)=Sof(H30D)=Sof(P1B)=Sof(Ag9B)=1-FVAR(2)
 Sof(C30A)=Sof(H30A)=Sof(H30B)=Sof(P1A)=Sof(Ag9A)=Sof(H32R)=Sof(H32S)=FVAR(2)
 Sof(Ag8B)=1-FVAR(3)
 Sof(Ag8A)=FVAR(3)
 Sof(Ag5B)=1-FVAR(4)
 Sof(Ag5A)=FVAR(4)
 Fixed Sof: Ag38(0.5) Ag39(0.5) Ag41(0.5) Ag1(0.5) Cu6A(0.5) Ag2(0.5)
 Cu6B(0.5) H152(0.5) Ag3(0.5)
 Fixed X: C313(0.34662)
8.a Ternary CH refined with riding coordinates:
 C300(H300), C304(H304), C314(H314), C320(H320), C323(H323), C310(H310),
 C326(H326), C154(H154), C148(H148), C152(H152), C164(H164)
8.b Secondary CH2 refined with riding coordinates:
 C30A(H30A,H30B), C30B(H30C,H30D), C1(H1A,H1B), C2(H2A,H2B), C3(H3A,H3B),
 C4(H4A,H4B), C5(H5A,H5B), C6(H6A,H6B), C7(H7A,H7B), C8(H8A,H8B), C9(H9A,H9B),
 C10(H10A,H10B), C11(H11A,H11B), C12(H12A,H12B), C316(H31G,H31H), C317(H31I,
 H31J), C318(H31K,H31L), C328(H32P,H32Q), C329(H32R,H32S)
8.c Me refined with riding coordinates:
 C322(H32D,H32E,H32F), C324(H32G,H32H,H32I), C309(H30Q,H30R,H30S)
8.d Aromatic/amide H refined with riding coordinates:
 C14(H14), C15(H15), C16(H16), C17(H17), C18(H18), C20(H20), C21(H21),
 C22(H22), C23(H23), C24(H24), C26(H26), C27(H27), C28(H28), C29(H29), C30(H30),
  C32(H32), C33(H33), C34(H34), C35(H35), C36(H36), C38(H38), C39(H39),
 C40(H40), C41(H41), C42(H42), C44(H44), C45(H45), C46(H46), C47(H47), C48(H48),
  C50(H50), C51(H51), C52(H52), C53(H53), C54(H54), C56(H56), C57(H57),
 C58(H58), C59(H59), C60(H60), C62(H62), C63(H63), C64(H64), C65(H65), C66(H66),
  C68(H68), C69(H69), C70(H70), C71(H71), C72(H72), C74(H74), C75(H75),
 C76(H76), C77(H77), C78(H78), C80(H80), C81(H81), C82(H82), C83(H83), C84(H84),
  C86(H86), C87(H87), C88(H88), C89(H89), C90(H90), C92(H92), C93(H93),
 C94(H94), C95(H95), C96(H96), C98(H98), C99(H99), C100(H100), C101(H101),
 C102(H102), C104(H104), C105(H105), C106(H106), C107(H107), C108(H108),
 C110(H110), C111(H111), C112(H112), C113(H113), C114(H114), C116(H116),
 C117(H117), C118(H118), C119(H119), C120(H120), C122(H122), C123(H123),
 C124(H124), C125(H125), C126(H126), C128(H128), C129(H129), C130(H130),
 C131(H131), C132(H132), C134(H134), C135(H135), C136(H136), C137(H137),
 C138(H138), C139(H139), C140(H140), C141(H141), C142(H142), C143(H143),
 C146(H146), C145(H145), C171(H171), C201(H201), C147(H147), C160(H160),
 C159(H159), C158(H158), C163(H163), C162(H162)
8.e Fitted hexagon refined as free rotating group:
 C13(C14,C15,C16,C17,C18), C19(C20,C21,C22,C23,C24), C25(C26,C27,C28,C29,C30),
 C31(C32,C33,C34,C35,C36), C37(C38,C39,C40,C41,C42), C43(C44,C45,C46,C47,C48),
 C49(C50,C51,C52,C53,C54), C55(C56,C57,C58,C59,C60), C61(C62,C63,C64,C65,C66),
 C67(C68,C69,C70,C71,C72), C73(C74,C75,C76,C77,C78), C79(C80,C81,C82,C83,C84),
 C85(C86,C87,C88,C89,C90), C91(C92,C93,C94,C95,C96), C97(C98,C99,C100,C101,
 C102), C103(C104,C105,C106,C107,C108), C109(C110,C111,C112,C113,C114),
 C115(C116,C117,C118,C119,C120), C121(C122,C123,C124,C125,C126), C127(C128,C129,
 C130,C131,C132), C133(C134,C135,C136,C137,C138), C139(C140,C141,C142,C143,
 C144), C146(C157,C145,C171,C201,C147), C161(C160,C159,C158,C163,C162)
8.f Idealised Me refined as rotating group:
 C301(H30E,H30F,H30G), C302(H30H,H30I,H30J), C303(H30K,H30L,H30M), C305(H30N,
 H30O,H30P), C313(H31A,H31B,H31C), C315(H31D,H31E,H31F), C319(H31M,H31N,H31O),
 C321(H32A,H32B,H32C), C311(H31P,H31Q,H31R), C325(H32J,H32K,H32L), C327(H32M,
 H32N,H32O), C156(H15A,H15B,H15C), C151(H15D,H15E,H15F), C149(H14A,H14B,H14C),
 C155(H15G,H15H,H15I), C150(H15J,H15K,H15L), C153(H15M,H15N,H15O), C165(H16A,
 H16B,H16C), C166(H16D,H16E,H16F)
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
W1 W 0.35913(5) 0.74118(3) 0.72665(2) 0.0513(2) Uani 1 1 d . . . . .
W2 W 0.19805(5) 0.75363(3) 0.70449(3) 0.0538(3) Uani 1 1 d . . . . .
W3 W 0.30341(5) 0.79876(3) 0.66103(3) 0.0526(3) Uani 1 1 d . . . . .
W4 W 0.44999(4) 0.66946(3) 0.67258(2) 0.0480(2) Uani 1 1 d . . . . .
W5 W 0.34695(5) 0.62564(3) 0.71918(3) 0.0537(3) Uani 1 1 d . . . . .
W6 W 0.17378(4) 0.63699(3) 0.69682(3) 0.0506(3) Uani 1 1 d . . . . .
W7 W 0.11319(4) 0.69374(3) 0.63021(3) 0.0546(3) Uani 1 1 d . . . . .
W8 W 0.22180(5) 0.74267(3) 0.58214(3) 0.0578(3) Uani 1 1 d . . . . .
W9 W 0.38525(5) 0.73028(3) 0.60300(2) 0.0513(2) Uani 1 1 d . . . . .
Si1 Si 0.2824(2) 0.69110(17) 0.65495(13) 0.0340(12) Uani 1 1 d . . . . .
Ag1A Ag 0.33326(15) 0.59593(11) 0.63816(9) 0.0806(9) Uani 0.709(2) 1 d . U P A
1
Ag2A Ag 0.28127(17) 0.64347(10) 0.58418(9) 0.0826(9) Uani 0.709(2) 1 d . U P A
1
Ag3A Ag 0.20110(14) 0.60205(10) 0.61914(8) 0.0670(7) Uani 0.709(2) 1 d . U P A
1
Ag1B Ag 0.3457(4) 0.6217(3) 0.6130(2) 0.0806(9) Uani 0.291(2) 1 d . U P A 2
Ag2B Ag 0.2132(4) 0.6315(2) 0.5896(2) 0.0826(9) Uani 0.291(2) 1 d . U P A 2
Ag3B Ag 0.2616(3) 0.5830(2) 0.64313(18) 0.0670(7) Uani 0.291(2) 1 d . U P A 2
Ag4 Ag 0.27974(10) 0.55964(6) 0.58048(6) 0.0710(6) Uani 1 1 d . U . . .
O1 O 0.4100(8) 0.7561(5) 0.7609(4) 0.063(4) Uani 1 1 d . U . . .
O2 O 0.3160(8) 0.8497(5) 0.6546(4) 0.056(4) Uani 1 1 d . U . . .
O3 O 0.1429(8) 0.7763(5) 0.7264(4) 0.060(4) Uani 1 1 d . U . . .
O4 O 0.3594(7) 0.7931(4) 0.7012(3) 0.043(3) Uani 1 1 d . U . . .
O5 O 0.2294(8) 0.8018(5) 0.6841(4) 0.052(4) Uani 1 1 d . U . . .
O6 O 0.2753(7) 0.7574(5) 0.7369(4) 0.051(4) Uani 1 1 d . U . . .
O7 O 0.2837(7) 0.7327(4) 0.6786(3) 0.045(3) Uani 1 1 d . . . . .
O8 O 0.1914(8) 0.6980(4) 0.7156(4) 0.052(4) Uani 1 1 d . . . . .
O9 O 0.3469(8) 0.6853(4) 0.7347(3) 0.046(4) Uani 1 1 d . . . . .
O10 O 0.4237(7) 0.7233(4) 0.6987(3) 0.044(3) Uani 1 1 d . . . . .
O11 O 0.3668(7) 0.7751(4) 0.6385(4) 0.047(3) Uani 1 1 d . . . . .
O12 O 0.2398(7) 0.7846(4) 0.6223(4) 0.048(4) Uani 1 1 d . . . . .
O13 O 0.1434(8) 0.7429(5) 0.6632(4) 0.056(4) Uani 1 1 d . . . . .
O14 O 0.3725(9) 0.6069(5) 0.7583(4) 0.069(5) Uani 1 1 d . . . . .
O15 O 0.4348(11) 0.6431(6) 0.7121(6) 0.089(7) Uani 1 1 d . . . . .
O16 O 0.5317(8) 0.6768(5) 0.6860(5) 0.063(5) Uani 1 1 d . . . . .
O17 O 0.4336(10) 0.7058(6) 0.6385(5) 0.080(5) Uani 1 1 d . U . . .
O18 O 0.4402(8) 0.7617(6) 0.5871(4) 0.063(4) Uani 1 1 d . . . . .
O19 O 0.3093(11) 0.7570(7) 0.5795(6) 0.096(7) Uani 1 1 d . U . . .
O20 O 0.1864(9) 0.7819(6) 0.5566(5) 0.081(6) Uani 1 1 d . . . . .
O21 O 0.1543(10) 0.7278(6) 0.6044(5) 0.085(6) Uani 1 1 d . . . . .
O22 O 0.0340(7) 0.7118(6) 0.6238(5) 0.067(5) Uani 1 1 d . . . . .
O23 O 0.1039(12) 0.6660(5) 0.6706(5) 0.088(7) Uani 1 1 d . . . . .
O24 O 0.1293(9) 0.6243(5) 0.7278(5) 0.070(5) Uani 1 1 d . . . . .
O25 O 0.2585(9) 0.6298(5) 0.7171(6) 0.080(6) Uani 1 1 d . . . . .
O26 O 0.3410(9) 0.6621(6) 0.6712(5) 0.081(6) Uani 1 1 d . . . . .
O27 O 0.2914(8) 0.7068(5) 0.6190(5) 0.068(5) Uani 1 1 d . . . . .
O28 O 0.2106(8) 0.6710(5) 0.6551(5) 0.066(5) Uani 1 1 d . . . . .
O29 O 0.3433(9) 0.5816(5) 0.6949(4) 0.069(5) Uani 1 1 d . . . . .
O30 O 0.4486(8) 0.6250(6) 0.6473(5) 0.076(6) Uani 1 1 d . . . . .
O31 O 0.3823(9) 0.6876(6) 0.5774(4) 0.069(5) Uani 1 1 d . . . . .
O32 O 0.2159(9) 0.6989(5) 0.5557(4) 0.069(5) Uani 1 1 d . . . . .
O33 O 0.1079(8) 0.6512(5) 0.6044(5) 0.076(6) Uani 1 1 d . . . . .
O34 O 0.1674(9) 0.5932(5) 0.6716(5) 0.069(5) Uani 1 1 d . . . . .
C30A C 0.052(7) 0.748(5) 0.513(4) 0.146(4) Uani 0.343(4) 1 d . U P A 1
H30A H 0.074167 0.764529 0.530813 0.175 Uiso 0.343(4) 1 calc R U P A 1
H30B H 0.011644 0.762344 0.504276 0.175 Uiso 0.343(4) 1 calc R U P A 1
P1A P 0.0993(14) 0.7423(12) 0.4835(6) 0.103(10) Uani 0.343(4) 1 d . . P A 1
C30B C 0.039(4) 0.690(2) 0.495(2) 0.144(3) Uani 0.657(4) 1 d . U P A 2
H30C H 0.004044 0.703328 0.480262 0.173 Uiso 0.657(4) 1 calc R U P A 2
H30D H 0.027640 0.661583 0.495510 0.173 Uiso 0.657(4) 1 calc R U P A 2
P1B P 0.1128(10) 0.6925(9) 0.4728(4) 0.142(9) Uani 0.657(4) 1 d . . P A 2
P11 P -0.0627(3) 0.6668(2) 0.5546(2) 0.078(2) Uani 1 1 d . . . . .
P12 P 0.0919(4) 0.5093(2) 0.7266(2) 0.071(2) Uani 1 1 d . . . . .
P13 P 0.3582(4) 0.4953(2) 0.7577(3) 0.093(3) Uani 1 1 d . . . . .
P14 P -0.0053(4) 0.8206(2) 0.6698(2) 0.081(2) Uani 1 1 d . . . . .
P15 P 0.1742(5) 0.8997(3) 0.6004(3) 0.095(3) Uani 1 1 d . . . . .
P16 P 0.4943(4) 0.8709(2) 0.6330(2) 0.075(2) Uani 1 1 d . . . . .
P17 P 0.5791(4) 0.7774(3) 0.7426(2) 0.080(2) Uani 1 1 d . . . . .
S1 S 0.5340(4) 0.6487(3) 0.7757(2) 0.098(3) Uani 1 1 d . . . . .
Ag5A Ag 0.53996(18) 0.57569(11) 0.65553(12) 0.0736(10) Uani 0.696(6) 1 d . U P
A 1
Ag5B Ag 0.5183(4) 0.5687(3) 0.6374(3) 0.0736(10) Uani 0.304(6) 1 d . U P A 2
Ag6 Ag 0.40517(13) 0.51939(8) 0.71285(7) 0.0921(8) Uani 1 1 d . U . . .
Ag7 Ag 0.08816(11) 0.53615(7) 0.67268(6) 0.0760(6) Uani 1 1 d D U . . .
Ag8A Ag 0.4425(3) 0.6421(2) 0.80271(13) 0.0889(12) Uani 0.584(6) 1 d . U P B 1
Ag8B Ag 0.4273(4) 0.6645(3) 0.79563(19) 0.0889(12) Uani 0.416(6) 1 d . U P B 2
Ag9A Ag 0.1972(3) 0.7048(2) 0.49711(16) 0.0706(8) Uani 0.343(4) 1 d . U P A 1
Ag9B Ag 0.21989(18) 0.67819(12) 0.50070(8) 0.0706(8) Uani 0.657(4) 1 d . U P A
2
Ag10 Ag 0.42208(12) 0.69469(10) 0.52619(6) 0.0939(8) Uani 1 1 d . U . . .
Ag11 Ag 0.00618(10) 0.61718(7) 0.58508(7) 0.0832(7) Uani 1 1 d . U . . .
Ag12 Ag 0.32406(12) 0.77874(8) 0.51998(6) 0.0834(7) Uani 1 1 d . U . . .
Ag13 Ag 0.23257(13) 0.84978(8) 0.57569(7) 0.0885(7) Uani 1 1 d . U . . .
Ag14 Ag 0.01261(13) 0.74885(8) 0.67295(9) 0.1061(10) Uani 1 1 d . U . . .
Ag15 Ag 0.08326(17) 0.69595(10) 0.74832(9) 0.1157(10) Uani 1 1 d . U . . .
Ag18 Ag 0.52512(13) 0.59298(9) 0.73878(7) 0.0916(7) Uani 1 1 d . U . . .
Ag19 Ag 0.41037(12) 0.83658(7) 0.59763(6) 0.0789(6) Uani 1 1 d . U . . .
Ag20 Ag -0.00498(13) 0.63033(7) 0.67360(9) 0.1017(9) Uani 1 1 d . U . . .
Ag35 Ag 0.53378(11) 0.71075(8) 0.74351(6) 0.0841(7) Uani 1 1 d . U . . .
Ag38 Ag 0.41559(19) 0.53165(12) 0.61995(10) 0.0601(9) Uani 0.5 1 d . U P A 2
Ag39 Ag 0.1904(3) 0.5982(2) 0.52794(16) 0.0902(14) Uani 0.5 1 d . U P A 2
Ag41 Ag 0.3886(3) 0.5983(2) 0.55830(19) 0.1173(14) Uani 0.5 1 d . U P A 2
C1 C 0.165(2) 0.5262(14) 0.7539(12) 0.133(3) Uani 1 1 d . U . . .
H1A H 0.163813 0.555720 0.756347 0.160 Uiso 1 1 calc R U . . .
H1B H 0.165571 0.514030 0.775190 0.160 Uiso 1 1 calc R U . . .
C2 C 0.225(2) 0.5148(14) 0.7412(12) 0.135(3) Uani 1 1 d . U . . .
H2A H 0.228998 0.531561 0.722368 0.162 Uiso 1 1 calc R U . . .
H2B H 0.221669 0.486474 0.734166 0.162 Uiso 1 1 calc R U . . .
C3 C 0.289(2) 0.5203(14) 0.7678(13) 0.139(3) Uani 1 1 d . U . . .
H3A H 0.280281 0.509836 0.788565 0.167 Uiso 1 1 calc R U . . .
H3B H 0.298626 0.549221 0.770504 0.167 Uiso 1 1 calc R U . . .
C4 C 0.067(2) 0.8517(13) 0.6680(11) 0.122(3) Uani 1 1 d . U . . .
H4A H 0.056958 0.879508 0.673799 0.146 Uiso 1 1 calc R U . . .
H4B H 0.101243 0.841721 0.684343 0.146 Uiso 1 1 calc R U . . .
C5 C 0.091(2) 0.8526(13) 0.6362(11) 0.122(3) Uani 1 1 d . U . . .
H5A H 0.055885 0.859477 0.618800 0.146 Uiso 1 1 calc R U . . .
H5B H 0.108601 0.826229 0.631551 0.146 Uiso 1 1 calc R U . . .
C6 C 0.144(2) 0.8858(13) 0.6399(11) 0.123(3) Uani 1 1 d . U . . .
H6A H 0.180325 0.876325 0.655429 0.148 Uiso 1 1 calc R U . . .
H6B H 0.126784 0.910216 0.648778 0.148 Uiso 1 1 calc R U . . .
C7 C 0.498(2) 0.8645(14) 0.6763(11) 0.127(3) Uani 1 1 d . U . . .
H7A H 0.529316 0.883733 0.687352 0.152 Uiso 1 1 calc R U . . .
H7B H 0.455835 0.871178 0.682162 0.152 Uiso 1 1 calc R U . . .
C8 C 0.516(2) 0.8233(14) 0.6879(11) 0.126(3) Uani 1 1 d . U . . .
H8A H 0.553225 0.814193 0.678304 0.151 Uiso 1 1 calc R U . . .
H8B H 0.480233 0.804762 0.680724 0.151 Uiso 1 1 calc R U . . .
C9 C 0.533(2) 0.8210(14) 0.7250(11) 0.129(3) Uani 1 1 d . U . . .
H9A H 0.492188 0.821710 0.733907 0.154 Uiso 1 1 calc R U . . .
H9B H 0.556656 0.845560 0.732375 0.154 Uiso 1 1 calc R U . . .
C10 C 0.580(2) 0.7015(15) 0.5793(12) 0.134(3) Uani 1 1 d . U . . .
H10A H 0.624965 0.708728 0.579618 0.161 Uiso 1 1 calc R U . . .
H10B H 0.560495 0.722125 0.591686 0.161 Uiso 1 1 calc R U . . .
C11 C 0.577(2) 0.6617(15) 0.5961(12) 0.133(3) Uani 1 1 d . U . . .
H11A H 0.589659 0.640129 0.582251 0.160 Uiso 1 1 calc R U . . .
H11B H 0.532561 0.656426 0.599381 0.160 Uiso 1 1 calc R U . . .
C12 C 0.621(2) 0.6602(15) 0.6287(12) 0.132(3) Uani 1 1 d . U . . .
H12A H 0.601068 0.675777 0.644534 0.159 Uiso 1 1 calc R U . . .
H12B H 0.662137 0.672970 0.626665 0.159 Uiso 1 1 calc R U . . .
C13 C -0.0637(12) 0.8372(9) 0.6364(6) 0.123(3) Uani 1 1 d G U . . .
C14 C -0.0796(13) 0.8784(8) 0.6328(7) 0.124(3) Uani 1 1 d G U . . .
H14 H -0.062107 0.897169 0.648595 0.149 Uiso 1 1 calc R U . . .
C15 C -0.1215(14) 0.8917(6) 0.6055(8) 0.126(3) Uani 1 1 d G U . . .
H15 H -0.132110 0.919279 0.603071 0.151 Uiso 1 1 calc R U . . .
C16 C -0.1476(12) 0.8637(9) 0.5819(6) 0.125(4) Uani 1 1 d G U . . .
H16 H -0.175691 0.872575 0.563646 0.150 Uiso 1 1 calc R U . . .
C17 C -0.1318(13) 0.8225(8) 0.5855(7) 0.127(3) Uani 1 1 d G U . . .
H17 H -0.149267 0.803762 0.569743 0.152 Uiso 1 1 calc R U . . .
C18 C -0.0899(14) 0.8092(6) 0.6128(8) 0.125(3) Uani 1 1 d G U . . .
H18 H -0.079264 0.781652 0.615266 0.150 Uiso 1 1 calc R U . . .
C19 C -0.0327(14) 0.8393(9) 0.7060(6) 0.122(3) Uani 1 1 d G U . . .
C20 C -0.0935(12) 0.8561(9) 0.7074(6) 0.123(3) Uani 1 1 d G U . . .
H20 H -0.123618 0.858564 0.688515 0.148 Uiso 1 1 calc R U . . .
C21 C -0.1094(10) 0.8693(8) 0.7370(8) 0.123(4) Uani 1 1 d G U . . .
H21 H -0.150141 0.880528 0.737980 0.147 Uiso 1 1 calc R U . . .
C22 C -0.0645(14) 0.8656(8) 0.7653(6) 0.123(4) Uani 1 1 d G U . . .
H22 H -0.075084 0.874381 0.785107 0.148 Uiso 1 1 calc R U . . .
C23 C -0.0036(12) 0.8487(9) 0.7639(6) 0.128(3) Uani 1 1 d G U . . .
H23 H 0.026495 0.846272 0.782770 0.154 Uiso 1 1 calc R U . . .
C24 C 0.0123(11) 0.8356(8) 0.7342(8) 0.124(3) Uani 1 1 d G U . . .
H24 H 0.053019 0.824309 0.733306 0.148 Uiso 1 1 calc R U . . .
C25 C -0.1277(12) 0.6895(9) 0.5747(8) 0.129(3) Uani 1 1 d G U . . .
C26 C -0.1758(15) 0.7148(9) 0.5585(6) 0.130(3) Uani 1 1 d G U . . .
H26 H -0.176600 0.720566 0.536539 0.156 Uiso 1 1 calc R U . . .
C27 C -0.2227(12) 0.7314(8) 0.5752(8) 0.129(3) Uani 1 1 d G U . . .
H27 H -0.254929 0.748310 0.564349 0.155 Uiso 1 1 calc R U . . .
C28 C -0.2216(12) 0.7228(9) 0.6080(8) 0.129(3) Uani 1 1 d G U . . .
H28 H -0.252950 0.733895 0.619196 0.155 Uiso 1 1 calc R U . . .
C29 C -0.1734(15) 0.6975(9) 0.6242(6) 0.130(4) Uani 1 1 d G U . . .
H29 H -0.172642 0.691736 0.646233 0.156 Uiso 1 1 calc R U . . .
C30 C -0.1265(12) 0.6809(8) 0.6076(8) 0.130(3) Uani 1 1 d G U . . .
H30 H -0.094313 0.663990 0.618423 0.156 Uiso 1 1 calc R U . . .
C31 C 0.0256(13) 0.5235(9) 0.7477(8) 0.133(3) Uani 1 1 d G U . . .
C32 C 0.0184(13) 0.5651(8) 0.7528(8) 0.135(3) Uani 1 1 d G U . . .
H32 H 0.047824 0.583592 0.746213 0.162 Uiso 1 1 calc R U . . .
C33 C -0.0327(15) 0.5792(7) 0.7678(8) 0.136(3) Uani 1 1 d G U . . .
H33 H -0.037520 0.607098 0.771238 0.164 Uiso 1 1 calc R U . . .
C34 C -0.0767(13) 0.5516(9) 0.7777(7) 0.134(4) Uani 1 1 d G U . . .
H34 H -0.110913 0.561049 0.787722 0.161 Uiso 1 1 calc R U . . .
C35 C -0.0695(13) 0.5100(8) 0.7726(8) 0.134(4) Uani 1 1 d G U . . .
H35 H -0.098963 0.491493 0.779182 0.161 Uiso 1 1 calc R U . . .
C36 C -0.0184(15) 0.4959(7) 0.7576(8) 0.134(3) Uani 1 1 d G U . . .
H36 H -0.013619 0.467985 0.754158 0.161 Uiso 1 1 calc R U . . .
C37 C 0.4914(14) 0.9262(7) 0.6255(8) 0.127(3) Uani 1 1 d G U . . .
C38 C 0.5112(13) 0.9550(10) 0.6497(6) 0.128(3) Uani 1 1 d G U . . .
H38 H 0.525277 0.946553 0.670941 0.153 Uiso 1 1 calc R U . . .
C39 C 0.5098(13) 0.9964(9) 0.6420(7) 0.128(3) Uani 1 1 d G U . . .
H39 H 0.523005 1.015678 0.658115 0.153 Uiso 1 1 calc R U . . .
C40 C 0.4887(14) 1.0091(7) 0.6102(8) 0.128(3) Uani 1 1 d G U . . .
H40 H 0.487813 1.036769 0.605023 0.154 Uiso 1 1 calc R U . . .
C41 C 0.4690(13) 0.9803(10) 0.5860(6) 0.129(3) Uani 1 1 d G U . . .
H41 H 0.454893 0.988735 0.564757 0.155 Uiso 1 1 calc R U . . .
C42 C 0.4704(13) 0.9389(9) 0.5937(7) 0.129(3) Uani 1 1 d G U . . .
H42 H 0.457165 0.919610 0.577582 0.154 Uiso 1 1 calc R U . . .
C43 C 0.5768(11) 0.8567(9) 0.6259(8) 0.127(3) Uani 1 1 d G U . . .
C44 C 0.5821(12) 0.8228(9) 0.6062(8) 0.130(3) Uani 1 1 d G U . . .
H44 H 0.545074 0.808043 0.597812 0.156 Uiso 1 1 calc R U . . .
C45 C 0.6425(15) 0.8109(8) 0.5992(7) 0.133(3) Uani 1 1 d G U . . .
H45 H 0.646039 0.788180 0.586073 0.160 Uiso 1 1 calc R U . . .
C46 C 0.6978(11) 0.8329(9) 0.6118(8) 0.129(3) Uani 1 1 d G U . . .
H46 H 0.738300 0.824950 0.607079 0.155 Uiso 1 1 calc R U . . .
C47 C 0.6926(12) 0.8668(9) 0.6314(7) 0.129(3) Uani 1 1 d G U . . .
H47 H 0.729598 0.881582 0.639825 0.155 Uiso 1 1 calc R U . . .
C48 C 0.6321(15) 0.8787(8) 0.6384(7) 0.128(3) Uani 1 1 d G U . . .
H48 H 0.628633 0.901445 0.651565 0.154 Uiso 1 1 calc R U . . .
C49 C 0.5621(15) 0.7511(8) 0.5218(8) 0.137(3) Uani 1 1 d G U . . .
C50 C 0.5210(11) 0.7845(10) 0.5225(8) 0.136(3) Uani 1 1 d G U . . .
H50 H 0.479703 0.780945 0.527992 0.163 Uiso 1 1 calc R U . . .
C51 C 0.5418(14) 0.8233(8) 0.5150(8) 0.136(3) Uani 1 1 d G U . . .
H51 H 0.514339 0.845692 0.515450 0.164 Uiso 1 1 calc R U . . .
C52 C 0.6036(15) 0.8287(8) 0.5068(8) 0.137(4) Uani 1 1 d G U . . .
H52 H 0.617475 0.854618 0.501764 0.165 Uiso 1 1 calc R U . . .
C53 C 0.6446(11) 0.7952(10) 0.5061(8) 0.137(4) Uani 1 1 d G U . . .
H53 H 0.685973 0.798798 0.500619 0.165 Uiso 1 1 calc R U . . .
C54 C 0.6239(14) 0.7564(8) 0.5136(8) 0.137(3) Uani 1 1 d G U . . .
H54 H 0.651338 0.734051 0.513161 0.164 Uiso 1 1 calc R U . . .
C55 C 0.6921(14) 0.6106(10) 0.6812(6) 0.134(3) Uani 1 1 d G U . . .
C56 C 0.6721(12) 0.6316(9) 0.7070(8) 0.132(3) Uani 1 1 d G U . . .
H56 H 0.633651 0.646560 0.703810 0.159 Uiso 1 1 calc R U . . .
C57 C 0.7097(15) 0.6304(9) 0.7377(7) 0.134(3) Uani 1 1 d G U . . .
H57 H 0.696307 0.644442 0.754998 0.161 Uiso 1 1 calc R U . . .
C58 C 0.7672(14) 0.6080(10) 0.7426(6) 0.135(4) Uani 1 1 d G U . . .
H58 H 0.792304 0.607173 0.763074 0.162 Uiso 1 1 calc R U . . .
C59 C 0.7872(12) 0.5870(9) 0.7167(8) 0.135(4) Uani 1 1 d G U . . .
H59 H 0.825646 0.572024 0.719963 0.162 Uiso 1 1 calc R U . . .
C60 C 0.7496(15) 0.5882(9) 0.6861(7) 0.135(3) Uani 1 1 d G U . . .
H60 H 0.762990 0.574141 0.668774 0.162 Uiso 1 1 calc R U . . .
C61 C 0.6003(16) 0.7924(10) 0.7851(6) 0.131(3) Uani 1 1 d G U . . .
C62 C 0.5503(11) 0.7900(9) 0.8038(8) 0.135(3) Uani 1 1 d G U . . .
H62 H 0.508768 0.782343 0.794120 0.162 Uiso 1 1 calc R U . . .
C63 C 0.5624(13) 0.7991(9) 0.8368(8) 0.135(4) Uani 1 1 d G U . . .
H63 H 0.529000 0.797477 0.849314 0.162 Uiso 1 1 calc R U . . .
C64 C 0.6245(16) 0.8105(9) 0.8512(6) 0.134(4) Uani 1 1 d G U . . .
H64 H 0.632639 0.816553 0.873353 0.161 Uiso 1 1 calc R U . . .
C65 C 0.6745(11) 0.8128(9) 0.8326(8) 0.134(4) Uani 1 1 d G U . . .
H65 H 0.716047 0.820494 0.842199 0.161 Uiso 1 1 calc R U . . .
C66 C 0.6624(13) 0.8038(9) 0.7995(8) 0.132(3) Uani 1 1 d G U . . .
H66 H 0.695816 0.805359 0.787005 0.158 Uiso 1 1 calc R U . . .
C67 C 0.6504(12) 0.7806(10) 0.7229(7) 0.128(3) Uani 1 1 d G U . . .
C68 C 0.6828(14) 0.8172(8) 0.7197(7) 0.128(3) Uani 1 1 d G U . . .
H68 H 0.669187 0.841019 0.728875 0.154 Uiso 1 1 calc R U . . .
C69 C 0.7355(14) 0.8182(8) 0.7027(8) 0.129(3) Uani 1 1 d G U . . .
H69 H 0.757150 0.842719 0.700602 0.155 Uiso 1 1 calc R U . . .
C70 C 0.7558(12) 0.7826(10) 0.6890(7) 0.129(3) Uani 1 1 d G U . . .
H70 H 0.791042 0.783284 0.677654 0.155 Uiso 1 1 calc R U . . .
C71 C 0.7234(14) 0.7460(8) 0.6922(7) 0.129(3) Uani 1 1 d G U . . .
H71 H 0.736970 0.722149 0.682980 0.155 Uiso 1 1 calc R U . . .
C72 C 0.6707(14) 0.7450(8) 0.7091(8) 0.130(3) Uani 1 1 d G U . . .
H72 H 0.649006 0.720449 0.711253 0.155 Uiso 1 1 calc R U . . .
C73 C 0.1063(12) 0.9231(9) 0.5746(7) 0.126(3) Uani 1 1 d G U . . .
C74 C 0.1098(12) 0.9281(9) 0.5417(8) 0.128(4) Uani 1 1 d G U . . .
H74 H 0.145902 0.918734 0.533170 0.154 Uiso 1 1 calc R U . . .
C75 C 0.0592(15) 0.9472(9) 0.5215(6) 0.130(4) Uani 1 1 d G U . . .
H75 H 0.061482 0.950523 0.499421 0.156 Uiso 1 1 calc R U . . .
C76 C 0.0052(12) 0.9612(9) 0.5342(7) 0.129(4) Uani 1 1 d G U . . .
H76 H -0.028679 0.973939 0.520642 0.155 Uiso 1 1 calc R U . . .
C77 C 0.0017(12) 0.9562(9) 0.5671(8) 0.129(4) Uani 1 1 d G U . . .
H77 H -0.034421 0.965567 0.575613 0.154 Uiso 1 1 calc R U . . .
C78 C 0.0523(15) 0.9371(9) 0.5873(6) 0.126(3) Uani 1 1 d G U . . .
H78 H 0.049999 0.933779 0.609363 0.151 Uiso 1 1 calc R U . . .
C79 C 0.6822(14) 0.5834(9) 0.6156(7) 0.134(3) Uani 1 1 d G U . . .
C80 C 0.6790(13) 0.5409(10) 0.6150(7) 0.136(3) Uani 1 1 d G U . . .
H80 H 0.651719 0.527260 0.627178 0.163 Uiso 1 1 calc R U . . .
C81 C 0.7167(15) 0.5188(7) 0.5962(8) 0.136(4) Uani 1 1 d G U . . .
H81 H 0.714515 0.490376 0.595734 0.164 Uiso 1 1 calc R U . . .
C82 C 0.7575(13) 0.5392(9) 0.5779(7) 0.136(4) Uani 1 1 d G U . . .
H82 H 0.782659 0.524390 0.565332 0.163 Uiso 1 1 calc R U . . .
C83 C 0.7607(13) 0.5817(9) 0.5786(7) 0.136(3) Uani 1 1 d G U . . .
H83 H 0.788006 0.595290 0.566375 0.163 Uiso 1 1 calc R U . . .
C84 C 0.7231(15) 0.6038(7) 0.5974(8) 0.135(3) Uani 1 1 d G U . . .
H84 H 0.725210 0.632175 0.597818 0.162 Uiso 1 1 calc R U . . .
C85 C 0.5783(16) 0.6647(8) 0.5116(8) 0.138(3) Uani 1 1 d G U . . .
C86 C 0.5377(11) 0.6458(10) 0.4863(8) 0.140(4) Uani 1 1 d G U . . .
H86 H 0.495267 0.655069 0.480301 0.168 Uiso 1 1 calc R U . . .
C87 C 0.5604(14) 0.6130(10) 0.4698(7) 0.141(4) Uani 1 1 d G U . . .
H87 H 0.533165 0.600405 0.452880 0.170 Uiso 1 1 calc R U . . .
C88 C 0.6237(16) 0.5992(8) 0.4787(8) 0.141(4) Uani 1 1 d G U . . .
H88 H 0.638905 0.577241 0.467731 0.169 Uiso 1 1 calc R U . . .
C89 C 0.6644(11) 0.6180(10) 0.5040(8) 0.139(3) Uani 1 1 d G U . . .
H89 H 0.706747 0.608740 0.510002 0.167 Uiso 1 1 calc R U . . .
C90 C 0.6417(14) 0.6508(10) 0.5205(7) 0.137(3) Uani 1 1 d G U . . .
H90 H 0.668851 0.663404 0.537423 0.165 Uiso 1 1 calc R U . . .
C91 C 0.1087(16) 0.7521(6) 0.8211(4) 0.143(3) Uani 1 1 d DG U . . .
C92 C 0.1516(11) 0.7834(10) 0.8324(7) 0.143(3) Uani 1 1 d G U . . .
H92 H 0.195153 0.781526 0.829796 0.172 Uiso 1 1 calc R U . . .
C93 C 0.1295(15) 0.8173(8) 0.8476(8) 0.144(4) Uani 1 1 d G U . . .
H93 H 0.158213 0.838233 0.855180 0.173 Uiso 1 1 calc R U . . .
C94 C 0.0645(16) 0.8201(7) 0.8515(6) 0.141(4) Uani 1 1 d G U . . .
H94 H 0.049658 0.842815 0.861700 0.169 Uiso 1 1 calc R U . . .
C95 C 0.0216(11) 0.7889(10) 0.8402(8) 0.141(4) Uani 1 1 d G U . . .
H95 H -0.021958 0.790690 0.842835 0.169 Uiso 1 1 calc R U . . .
C96 C 0.0437(15) 0.7549(7) 0.8250(7) 0.143(3) Uani 1 1 d G U . . .
H96 H 0.014981 0.733983 0.817451 0.171 Uiso 1 1 calc R U . . .
C97 C 0.1270(16) 0.6684(9) 0.8301(8) 0.142(3) Uani 1 1 d G U . . .
C98 C 0.1485(15) 0.6740(8) 0.8632(9) 0.143(3) Uani 1 1 d G U . . .
H98 H 0.166505 0.698882 0.870717 0.171 Uiso 1 1 calc R U . . .
C99 C 0.1433(15) 0.6423(11) 0.8850(6) 0.141(4) Uani 1 1 d G U . . .
H99 H 0.157690 0.646059 0.907113 0.169 Uiso 1 1 calc R U . . .
C100 C 0.1164(15) 0.6051(9) 0.8737(8) 0.142(4) Uani 1 1 d G U . . .
H100 H 0.112877 0.583913 0.888338 0.170 Uiso 1 1 calc R U . . .
C101 C 0.0948(14) 0.5995(8) 0.8407(9) 0.141(3) Uani 1 1 d G U . . .
H101 H 0.076878 0.574589 0.833166 0.169 Uiso 1 1 calc R U . . .
C102 C 0.1001(15) 0.6311(11) 0.8189(6) 0.141(3) Uani 1 1 d G U . . .
H102 H 0.085693 0.627412 0.796770 0.170 Uiso 1 1 calc R U . . .
C103 C -0.1101(13) 0.6464(9) 0.5174(7) 0.131(3) Uani 1 1 d G U . . .
C104 C -0.1318(14) 0.6704(7) 0.4904(8) 0.132(3) Uani 1 1 d G U . . .
H104 H -0.120799 0.698002 0.490325 0.159 Uiso 1 1 calc R U . . .
C105 C -0.1700(14) 0.6533(9) 0.4634(7) 0.131(4) Uani 1 1 d G U . . .
H105 H -0.184543 0.669412 0.445255 0.157 Uiso 1 1 calc R U . . .
C106 C -0.1865(13) 0.6121(9) 0.4634(6) 0.130(4) Uani 1 1 d G U . . .
H106 H -0.212078 0.600631 0.445351 0.156 Uiso 1 1 calc R U . . .
C107 C -0.1648(14) 0.5880(7) 0.4905(8) 0.130(4) Uani 1 1 d G U . . .
H107 H -0.175868 0.560440 0.490517 0.156 Uiso 1 1 calc R U . . .
C108 C -0.1266(14) 0.6051(9) 0.5175(7) 0.129(4) Uani 1 1 d G U . . .
H108 H -0.112123 0.589030 0.535587 0.155 Uiso 1 1 calc R U . . .
C109 C 0.3721(8) 0.7078(6) 0.8541(8) 0.149(3) Uani 1 1 d G U . . .
C110 C 0.3564(13) 0.7169(10) 0.8847(8) 0.150(3) Uani 1 1 d G U . . .
H110 H 0.345211 0.696056 0.898009 0.180 Uiso 1 1 calc R U . . .
C111 C 0.3574(15) 0.7573(11) 0.8953(7) 0.150(4) Uani 1 1 d G U . . .
H111 H 0.346933 0.763411 0.915756 0.180 Uiso 1 1 calc R U . . .
C112 C 0.3741(13) 0.7885(8) 0.8754(8) 0.150(4) Uani 1 1 d G U . . .
H112 H 0.374819 0.815471 0.882494 0.180 Uiso 1 1 calc R U . . .
C113 C 0.3898(15) 0.7793(6) 0.8448(8) 0.146(3) Uani 1 1 d G U . . .
H113 H 0.400983 0.800177 0.831485 0.176 Uiso 1 1 calc R U . . .
C114 C 0.3888(13) 0.7390(7) 0.8342(7) 0.149(3) Uani 1 1 d DG U . . .
H114 H 0.399262 0.732823 0.813737 0.179 Uiso 1 1 calc R U . . .
C115 C 0.0913(15) 0.4531(6) 0.7296(8) 0.133(3) Uani 1 1 d G U . . .
C116 C 0.0653(14) 0.4314(9) 0.7019(7) 0.137(3) Uani 1 1 d G U . . .
H116 H 0.047600 0.445288 0.683137 0.165 Uiso 1 1 calc R U . . .
C117 C 0.0658(14) 0.3889(9) 0.7023(7) 0.134(4) Uani 1 1 d G U . . .
H117 H 0.048443 0.374311 0.683806 0.161 Uiso 1 1 calc R U . . .
C118 C 0.0923(14) 0.3681(6) 0.7304(8) 0.134(4) Uani 1 1 d G U . . .
H118 H 0.092633 0.339623 0.730717 0.160 Uiso 1 1 calc R U . . .
C119 C 0.1183(14) 0.3898(9) 0.7582(7) 0.134(4) Uani 1 1 d G U . . .
H119 H 0.135981 0.375913 0.776959 0.161 Uiso 1 1 calc R U . . .
C120 C 0.1178(14) 0.4323(9) 0.7578(7) 0.134(3) Uani 1 1 d G U . . .
H120 H 0.135138 0.446891 0.776290 0.161 Uiso 1 1 calc R U . . .
C121 C 0.4194(12) 0.4968(9) 0.7924(7) 0.144(3) Uani 1 1 d G U . . .
C122 C 0.4202(13) 0.5232(9) 0.8187(9) 0.146(4) Uani 1 1 d G U . . .
H122 H 0.386673 0.541949 0.818999 0.176 Uiso 1 1 calc R U . . .
C123 C 0.4709(17) 0.5215(9) 0.8446(8) 0.150(4) Uani 1 1 d G U . . .
H123 H 0.471430 0.539133 0.862239 0.180 Uiso 1 1 calc R U . . .
C124 C 0.5210(13) 0.4934(10) 0.8443(7) 0.148(4) Uani 1 1 d G U . . .
H124 H 0.554955 0.492257 0.861586 0.178 Uiso 1 1 calc R U . . .
C125 C 0.5202(14) 0.4670(9) 0.8180(9) 0.149(4) Uani 1 1 d G U . . .
H125 H 0.553725 0.448197 0.817692 0.178 Uiso 1 1 calc R U . . .
C126 C 0.4695(17) 0.4687(9) 0.7920(7) 0.146(3) Uani 1 1 d G U . . .
H126 H 0.468969 0.451013 0.774452 0.175 Uiso 1 1 calc R U . . .
C127 C 0.3315(8) 0.4433(6) 0.7553(8) 0.141(3) Uani 1 1 d G U . . .
C128 C 0.3042(13) 0.4251(9) 0.7803(7) 0.140(3) Uani 1 1 d G U . . .
H128 H 0.299797 0.440080 0.798949 0.168 Uiso 1 1 calc R U . . .
C129 C 0.2834(13) 0.3847(10) 0.7776(7) 0.139(4) Uani 1 1 d G U . . .
H129 H 0.265157 0.372574 0.794302 0.167 Uiso 1 1 calc R U . . .
C130 C 0.2900(12) 0.3624(7) 0.7498(9) 0.139(4) Uani 1 1 d G U . . .
H130 H 0.276089 0.335309 0.747890 0.167 Uiso 1 1 calc R U . . .
C131 C 0.3173(15) 0.3805(9) 0.7247(7) 0.142(4) Uani 1 1 d G U . . .
H131 H 0.321662 0.365550 0.706124 0.170 Uiso 1 1 calc R U . . .
C132 C 0.3380(12) 0.4209(10) 0.7275(7) 0.142(3) Uani 1 1 d G U . . .
H132 H 0.356303 0.433056 0.710771 0.171 Uiso 1 1 calc R U . . .
C133 C 0.2248(13) 0.9442(8) 0.6174(7) 0.125(3) Uani 1 1 d G U . . .
C134 C 0.2915(14) 0.9385(7) 0.6254(7) 0.125(3) Uani 1 1 d G U . . .
H134 H 0.310101 0.913737 0.620822 0.151 Uiso 1 1 calc R U . . .
C135 C 0.3304(10) 0.9699(9) 0.6402(7) 0.128(3) Uani 1 1 d G U . . .
H135 H 0.374986 0.966038 0.645605 0.153 Uiso 1 1 calc R U . . .
C136 C 0.3025(13) 1.0069(8) 0.6471(7) 0.126(4) Uani 1 1 d G U . . .
H136 H 0.328532 1.027885 0.656995 0.152 Uiso 1 1 calc R U . . .
C137 C 0.2358(14) 1.0126(7) 0.6390(7) 0.127(4) Uani 1 1 d G U . . .
H137 H 0.217194 1.037431 0.643603 0.153 Uiso 1 1 calc R U . . .
C138 C 0.1969(10) 0.9813(9) 0.6242(7) 0.126(3) Uani 1 1 d G U . . .
H138 H 0.152308 0.985131 0.618820 0.151 Uiso 1 1 calc R U . . .
C139 C 0.3430(13) 0.6135(10) 0.8886(8) 0.153(3) Uani 1 1 d G U . . .
H139 H 0.300414 0.618088 0.878809 0.183 Uiso 1 1 calc R U . . .
C140 C 0.3555(15) 0.5897(10) 0.9166(9) 0.156(4) Uani 1 1 d G U . . .
H140 H 0.321189 0.578370 0.925535 0.187 Uiso 1 1 calc R U . . .
C141 C 0.4192(19) 0.5827(9) 0.9312(7) 0.156(4) Uani 1 1 d G U . . .
H141 H 0.427534 0.566828 0.949887 0.187 Uiso 1 1 calc R U . . .
C142 C 0.4705(13) 0.5996(11) 0.9178(9) 0.155(4) Uani 1 1 d G U . . .
H142 H 0.513105 0.595003 0.927514 0.186 Uiso 1 1 calc R U . . .
C143 C 0.4580(16) 0.6234(9) 0.8898(9) 0.154(3) Uani 1 1 d G U . . .
H143 H 0.492332 0.634721 0.880788 0.184 Uiso 1 1 calc R U . . .
C144 C 0.3943(19) 0.6303(6) 0.8752(6) 0.152(3) Uani 1 1 d G U . . .
C300 C 0.584(3) 0.4996(15) 0.7167(11) 0.156(9) Uani 1 1 d D U . . .
H300 H 0.624027 0.515670 0.722593 0.188 Uiso 1 1 calc R U . . .
C301 C 0.592(3) 0.4768(16) 0.6860(12) 0.165(8) Uani 1 1 d D U . . .
H30E H 0.603853 0.449023 0.691300 0.248 Uiso 1 1 calc R U . . .
H30F H 0.624432 0.489692 0.675637 0.248 Uiso 1 1 calc R U . . .
H30G H 0.550924 0.477130 0.671511 0.248 Uiso 1 1 calc R U . . .
C302 C 0.565(2) 0.4844(16) 0.7479(12) 0.159(6) Uani 1 1 d D U . . .
H30H H 0.523203 0.471670 0.743485 0.238 Uiso 1 1 calc R U . . .
H30I H 0.563544 0.506946 0.762522 0.238 Uiso 1 1 calc R U . . .
H30J H 0.596665 0.464801 0.757566 0.238 Uiso 1 1 calc R U . . .
C303 C 0.610(2) 0.6774(13) 0.8294(13) 0.153(8) Uani 1 1 d D U . . .
H30K H 0.570778 0.680271 0.838948 0.229 Uiso 1 1 calc R U . . .
H30L H 0.618018 0.702346 0.818535 0.229 Uiso 1 1 calc R U . . .
H30M H 0.645670 0.671530 0.846119 0.229 Uiso 1 1 calc R U . . .
C304 C 0.602(2) 0.6458(16) 0.8072(12) 0.139(6) Uani 1 1 d . U . . .
H304 H 0.641775 0.643678 0.797170 0.167 Uiso 1 1 calc R U . . .
C305 C 0.599(3) 0.6101(13) 0.8287(13) 0.156(9) Uani 1 1 d D U . . .
H30N H 0.618975 0.616724 0.850422 0.234 Uiso 1 1 calc R U . . .
H30O H 0.620892 0.587320 0.820756 0.234 Uiso 1 1 calc R U . . .
H30P H 0.554016 0.602966 0.828967 0.234 Uiso 1 1 calc R U . . .
C313 C 0.346620 0.8749(16) 0.4873(11) 0.163(11) Uani 1 1 d D U . . .
H31A H 0.302556 0.876683 0.476441 0.244 Uiso 1 1 calc R U . . .
H31B H 0.363124 0.847915 0.484613 0.244 Uiso 1 1 calc R U . . .
H31C H 0.372881 0.894571 0.478046 0.244 Uiso 1 1 calc R U . . .
C314 C 0.349(3) 0.8837(13) 0.5227(11) 0.151(11) Uani 1 1 d D U . . .
H314 H 0.394964 0.888419 0.530327 0.182 Uiso 1 1 calc R U . . .
C315 C 0.318(3) 0.9235(13) 0.5294(13) 0.153(9) Uani 1 1 d D U . . .
H31D H 0.349235 0.945181 0.529059 0.229 Uiso 1 1 calc R U . . .
H31E H 0.304471 0.922549 0.550488 0.229 Uiso 1 1 calc R U . . .
H31F H 0.281166 0.928521 0.513082 0.229 Uiso 1 1 calc R U . . .
C316 C 0.2302(11) 0.7130(13) 0.8030(13) 0.145(3) Uani 1 1 d D U . . .
H31G H 0.239860 0.733293 0.787419 0.174 Uiso 1 1 calc R U . . .
H31H H 0.250159 0.721616 0.824565 0.174 Uiso 1 1 calc R U . . .
C317 C 0.257(2) 0.6722(12) 0.7951(11) 0.145(3) Uani 1 1 d D U . . .
H31I H 0.222433 0.656704 0.782449 0.174 Uiso 1 1 calc R U . . .
H31J H 0.290012 0.676970 0.781220 0.174 Uiso 1 1 calc R U . . .
C318 C 0.287(2) 0.6464(15) 0.8230(12) 0.146(3) Uani 1 1 d D U . . .
H31K H 0.285348 0.618117 0.815830 0.176 Uiso 1 1 calc R U . . .
H31L H 0.259503 0.648421 0.840007 0.176 Uiso 1 1 calc R U . . .
C319 C 0.3855(18) 0.7554(16) 0.4458(13) 0.158(9) Uani 1 1 d D U . . .
H31M H 0.389865 0.759145 0.423251 0.237 Uiso 1 1 calc R U . . .
H31N H 0.426450 0.746944 0.457726 0.237 Uiso 1 1 calc R U . . .
H31O H 0.372419 0.780761 0.454501 0.237 Uiso 1 1 calc R U . . .
C320 C 0.334(2) 0.7224(13) 0.4486(13) 0.159(7) Uani 1 1 d D U . . .
H320 H 0.342309 0.696589 0.438034 0.190 Uiso 1 1 calc R U . . .
C321 C 0.2802(17) 0.7480(16) 0.4286(13) 0.159(6) Uani 1 1 d D U . . .
H32A H 0.239670 0.733445 0.426540 0.239 Uiso 1 1 calc R U . . .
H32B H 0.291270 0.752926 0.407284 0.239 Uiso 1 1 calc R U . . .
H32C H 0.275967 0.773658 0.439312 0.239 Uiso 1 1 calc R U . . .
C322 C 0.548(2) 0.5426(14) 0.5439(12) 0.147(5) Uani 1 1 d D U . . .
H32D H 0.540419 0.570565 0.549397 0.221 Uiso 1 1 calc R U . . .
H32E H 0.592621 0.535807 0.550455 0.221 Uiso 1 1 calc R U . . .
H32F H 0.536591 0.539023 0.520728 0.221 Uiso 1 1 calc R U . . .
C323 C 0.506(3) 0.5148(15) 0.5612(14) 0.163(9) Uani 1 1 d D U . . .
H323 H 0.467152 0.521519 0.545352 0.196 Uiso 1 1 calc R U . . .
C324 C 0.468(2) 0.4814(14) 0.5758(14) 0.164(7) Uani 1 1 d D U . . .
H32G H 0.440530 0.493511 0.589678 0.247 Uiso 1 1 calc R U . . .
H32H H 0.442424 0.466383 0.558702 0.247 Uiso 1 1 calc R U . . .
H32I H 0.498453 0.463167 0.588429 0.247 Uiso 1 1 calc R U . . .
C309 C -0.089(2) 0.5317(13) 0.6586(9) 0.149(11) Uani 1 1 d D U . . .
H30Q H -0.093465 0.553059 0.673941 0.223 Uiso 1 1 calc R U . . .
H30R H -0.128967 0.516387 0.654423 0.223 Uiso 1 1 calc R U . . .
H30S H -0.054242 0.513798 0.667275 0.223 Uiso 1 1 calc R U . . .
C310 C -0.0751(17) 0.5498(8) 0.6278(9) 0.144(10) Uani 1 1 d D U . . .
H310 H -0.110411 0.567528 0.617525 0.173 Uiso 1 1 calc R U . . .
C311 C -0.0714(19) 0.5104(10) 0.6098(10) 0.154(9) Uani 1 1 d D U . . .
H31P H -0.051924 0.489793 0.624633 0.231 Uiso 1 1 calc R U . . .
H31Q H -0.045558 0.514233 0.592786 0.231 Uiso 1 1 calc R U . . .
H31R H -0.114439 0.501959 0.600522 0.231 Uiso 1 1 calc R U . . .
S2 S 0.0021(4) 0.5764(2) 0.6357(2) 0.085(2) Uani 1 1 d D . . . .
C325 C -0.0828(19) 0.7364(13) 0.7396(10) 0.140(6) Uani 1 1 d D U . . .
H32J H -0.124201 0.741642 0.746370 0.209 Uiso 1 1 calc R U . . .
H32K H -0.073798 0.757441 0.724752 0.209 Uiso 1 1 calc R U . . .
H32L H -0.049497 0.736393 0.758314 0.209 Uiso 1 1 calc R U . . .
C326 C -0.0844(16) 0.6961(12) 0.7232(9) 0.145(8) Uani 1 1 d D U . . .
H326 H -0.095691 0.673024 0.736313 0.174 Uiso 1 1 calc R U . . .
C327 C -0.1357(16) 0.7076(14) 0.6951(10) 0.146(6) Uani 1 1 d D U . . .
H32M H -0.164908 0.727115 0.702307 0.219 Uiso 1 1 calc R U . . .
H32N H -0.159484 0.683557 0.687142 0.219 Uiso 1 1 calc R U . . .
H32O H -0.115375 0.719332 0.678035 0.219 Uiso 1 1 calc R U . . .
S4 S -0.0096(5) 0.6900(3) 0.7063(3) 0.106(3) Uani 1 1 d D U . . .
C328 C -0.018(2) 0.7111(14) 0.5422(13) 0.134(3) Uani 1 1 d . U . . .
H32P H -0.049596 0.728023 0.528452 0.161 Uiso 1 1 calc R U . . .
H32Q H -0.003348 0.726815 0.561651 0.161 Uiso 1 1 calc R U . . .
C329 C 0.036(2) 0.7057(16) 0.5253(14) 0.140(4) Uani 1 1 d . U . . .
H32R H 0.025634 0.686912 0.507176 0.167 Uiso 0.343(4) 1 calc R U P A 1
H32S H 0.073244 0.694925 0.539881 0.167 Uiso 0.343(4) 1 calc R U P A 1
Ag1 Ag 0.1780(3) 0.6037(2) 0.54370(16) 0.0902(14) Uani 0.5 1 d . U P A 1
Cu6A Cu 0.1497(4) 0.5261(3) 0.5813(2) 0.0764(15) Uani 0.5 1 d . . P A 1
Ag2 Ag 0.4170(3) 0.5766(2) 0.57643(19) 0.1173(14) Uani 0.5 1 d D U P A 1
Cu6B Cu 0.1275(4) 0.5459(3) 0.5856(2) 0.0764(15) Uani 0.5 1 d . . P A 2
P18 P 0.1398(7) 0.7087(4) 0.8016(3) 0.120(4) Uani 1 1 d D U . . .
P19 P 0.5372(5) 0.7033(4) 0.5357(3) 0.107(3) Uani 1 1 d . U . . .
P20 P 0.6356(5) 0.6077(3) 0.6437(3) 0.097(3) Uani 1 1 d . U . . .
P21 P 0.3705(7) 0.6585(4) 0.8411(3) 0.137(4) Uani 1 1 d D U . . .
S3 S 0.3286(4) 0.8410(2) 0.5490(2) 0.081(2) Uani 1 1 d . . . . .
S5 S 0.5154(6) 0.5384(4) 0.7013(3) 0.119(2) Uani 1 1 d . . . . .
S6 S 0.3639(7) 0.4914(4) 0.6541(4) 0.132(4) Uani 1 1 d . . . . .
S7 S 0.1446(6) 0.5009(4) 0.6309(3) 0.119(2) Uani 1 1 d D . . . .
S8 S 0.4907(5) 0.5660(4) 0.5890(3) 0.107(2) Uani 1 1 d D . . . .
S10 S 0.0797(6) 0.5786(4) 0.5441(3) 0.119(2) Uani 1 1 d . U . . .
S11 S 0.3218(5) 0.7158(4) 0.4925(3) 0.107(2) Uani 1 1 d . . . . .
Cl25 Cl 0.2604(5) 0.4950(3) 0.5526(2) 0.102(3) Uani 1 1 d . . . . .
S9B S 0.3146(5) 0.6161(3) 0.5176(2) 0.099(3) Uani 1 1 d . U . A 2
C146 C 0.0222(16) 0.6544(10) 0.4213(9) 0.153(4) Uani 1 1 d G U . . .
H146 H -0.011965 0.669622 0.427205 0.184 Uiso 1 1 calc R U . . .
C157 C 0.0851(19) 0.6605(10) 0.4373(8) 0.153(4) Uani 1 1 d G U . . .
C145 C 0.1362(13) 0.6377(11) 0.4284(9) 0.155(4) Uani 1 1 d G U . . .
H145 H 0.178278 0.641765 0.439148 0.186 Uiso 1 1 calc R U . . .
C171 C 0.1242(15) 0.6089(10) 0.4036(9) 0.156(4) Uani 1 1 d G U . . .
H171 H 0.158369 0.593726 0.397704 0.187 Uiso 1 1 calc R U . . .
C201 C 0.0613(18) 0.6029(10) 0.3876(8) 0.156(4) Uani 1 1 d G U . . .
H201 H 0.053293 0.583634 0.371010 0.187 Uiso 1 1 calc R U . . .
C147 C 0.0102(13) 0.6256(11) 0.3965(9) 0.155(4) Uani 1 1 d G U . . .
H147 H -0.031874 0.621582 0.385761 0.186 Uiso 1 1 calc R U . . .
C154 C 0.048(3) 0.5433(16) 0.5099(13) 0.149(9) Uani 1 1 d . U . . .
H154 H 0.011961 0.526605 0.515653 0.178 Uiso 1 1 calc R U . . .
C156 C 0.102(3) 0.5165(16) 0.5012(13) 0.156(8) Uani 1 1 d . U . . .
H15A H 0.138514 0.533177 0.498409 0.234 Uiso 1 1 calc R U . . .
H15B H 0.086925 0.502057 0.481358 0.234 Uiso 1 1 calc R U . . .
H15C H 0.114438 0.497124 0.518440 0.234 Uiso 1 1 calc R U . . .
C151 C 0.238(2) 0.5714(17) 0.4597(13) 0.158(6) Uani 1 1 d D U . . .
H15D H 0.238843 0.565383 0.437191 0.237 Uiso 1 1 calc R U . . .
H15E H 0.213290 0.596022 0.461395 0.237 Uiso 1 1 calc R U . . .
H15F H 0.217458 0.549156 0.469478 0.237 Uiso 1 1 calc R U . . .
C148 C 0.378(2) 0.4398(16) 0.6504(12) 0.151(6) Uani 1 1 d D U . . .
H148 H 0.349314 0.421798 0.660402 0.182 Uiso 1 1 calc R U . . .
C149 C 0.451(2) 0.4316(16) 0.6608(14) 0.157(6) Uani 1 1 d D U . . .
H14A H 0.475803 0.450040 0.649519 0.235 Uiso 1 1 calc R U . . .
H14B H 0.460718 0.403915 0.655549 0.235 Uiso 1 1 calc R U . . .
H14C H 0.462045 0.435769 0.683867 0.235 Uiso 1 1 calc R U . . .
C155 C 0.024(2) 0.5692(16) 0.4775(13) 0.153(6) Uani 1 1 d . U . . .
H15G H 0.001278 0.593031 0.482892 0.229 Uiso 1 1 calc R U . . .
H15H H -0.003685 0.552645 0.462295 0.229 Uiso 1 1 calc R U . . .
H15I H 0.061640 0.577347 0.468004 0.229 Uiso 1 1 calc R U . . .
C152 C 0.3080(18) 0.5772(18) 0.4777(13) 0.159(7) Uani 1 1 d D U . . .
H152 H 0.308123 0.552086 0.490520 0.190 Uiso 0.5 1 calc R U P A 2
C150 C 0.380(3) 0.4320(16) 0.6142(12) 0.161(8) Uani 1 1 d D U . . .
H15J H 0.337359 0.436583 0.602167 0.242 Uiso 1 1 calc R U . . .
H15K H 0.392874 0.404292 0.611213 0.242 Uiso 1 1 calc R U . . .
H15L H 0.410336 0.450371 0.606613 0.242 Uiso 1 1 calc R U . . .
C153 C 0.3833(18) 0.5816(17) 0.4827(13) 0.154(6) Uani 1 1 d D U . . .
H15M H 0.396113 0.604398 0.496728 0.232 Uiso 1 1 calc R U . . .
H15N H 0.397438 0.585966 0.461981 0.232 Uiso 1 1 calc R U . . .
H15O H 0.402806 0.557019 0.492373 0.232 Uiso 1 1 calc R U . . .
Sb1 Sb 0.3810(2) 0.62271(14) 0.38303(11) 0.1617(14) Uani 1 1 d D U . . .
Sb2 Sb 0.1752(3) 0.95602(18) 0.42778(14) 0.1957(19) Uani 1 1 d D U . . .
F56 F 0.3895(13) 0.6276(8) 0.4267(5) 0.194(5) Uani 1 1 d D U . . .
F86 F 0.2359(13) 0.9834(10) 0.4543(7) 0.274(10) Uani 1 1 d D U . . .
F97 F 0.2986(10) 0.6401(8) 0.3798(7) 0.199(4) Uani 1 1 d D U . . .
F110 F 0.3560(13) 0.5714(6) 0.3833(7) 0.199(5) Uani 1 1 d D U . . .
F124 F 0.3767(13) 0.6200(8) 0.3399(5) 0.201(5) Uani 1 1 d D U . . .
F131 F 0.1181(14) 0.9833(11) 0.4486(8) 0.299(9) Uani 1 1 d D U . . .
F145 F 0.4047(13) 0.6760(6) 0.3817(7) 0.202(5) Uani 1 1 d D U . . .
F161 F 0.1083(14) 0.9312(10) 0.4025(7) 0.277(10) Uani 1 1 d D U . . .
F174 F 0.1751(17) 0.9159(9) 0.4576(7) 0.271(10) Uani 1 1 d D U . . .
F213 F 0.4659(10) 0.6096(8) 0.3880(6) 0.199(4) Uani 1 1 d D U . . .
F185 F 0.2329(15) 0.9294(10) 0.4082(8) 0.299(9) Uani 1 1 d D U . . .
C161 C 0.1063(18) 0.7453(8) 0.4545(9) 0.151(4) Uani 1 1 d G U . A 2
C160 C 0.0689(15) 0.7535(10) 0.4246(9) 0.152(4) Uani 1 1 d G U . A 2
H160 H 0.041774 0.733416 0.414111 0.182 Uiso 1 1 calc R U . A 2
C159 C 0.0721(16) 0.7918(11) 0.4103(7) 0.153(4) Uani 1 1 d G U . A 2
H159 H 0.047069 0.797266 0.390244 0.184 Uiso 1 1 calc R U . A 2
C158 C 0.1127(17) 0.8218(9) 0.4259(9) 0.153(4) Uani 1 1 d G U . A 2
H158 H 0.114803 0.847377 0.416374 0.183 Uiso 1 1 calc R U . A 2
C163 C 0.1501(15) 0.8136(10) 0.4559(9) 0.153(4) Uani 1 1 d G U . A 2
H163 H 0.177244 0.833639 0.466373 0.183 Uiso 1 1 calc R U . A 2
C162 C 0.1469(16) 0.7753(11) 0.4702(7) 0.151(4) Uani 1 1 d G U . A 2
H162 H 0.171950 0.769789 0.490242 0.181 Uiso 1 1 calc R U . A 2
F134 F 0.1720(17) 0.9979(8) 0.3998(7) 0.280(10) Uani 1 1 d D U . . .
C165 C 0.175(3) 0.4300(16) 0.6344(14) 0.163(8) Uani 1 1 d . U . . .
H16A H 0.211060 0.448114 0.640304 0.245 Uiso 1 1 calc R U . . .
H16B H 0.187042 0.408488 0.620843 0.245 Uiso 1 1 calc R U . . .
H16C H 0.162258 0.418441 0.653792 0.245 Uiso 1 1 calc R U . . .
C164 C 0.118(2) 0.4537(9) 0.6161(13) 0.151(6) Uani 1 1 d D U . . .
H164 H 0.128336 0.454124 0.593784 0.182 Uiso 1 1 calc R U . . .
C166 C 0.044(2) 0.4564(16) 0.6110(14) 0.161(7) Uani 1 1 d D U . . .
H16D H 0.027743 0.444315 0.629303 0.241 Uiso 1 1 calc R U . . .
H16E H 0.026347 0.441967 0.591496 0.241 Uiso 1 1 calc R U . . .
H16F H 0.030805 0.484561 0.609053 0.241 Uiso 1 1 calc R U . . .
Ag3 Ag 0.2568(3) 0.51601(17) 0.63765(13) 0.0890(14) Uani 0.5 1 d . U P A .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
W1 O1 1.711(17) . ?
W1 O4 2.001(14) . ?
W1 O6 1.932(15) . ?
W1 O7 2.362(15) . ?
W1 O9 1.879(12) . ?
W1 O10 1.990(14) . ?
W2 O3 1.735(15) . ?
W2 O5 1.948(15) . ?
W2 O6 1.938(15) . ?
W2 O7 2.321(14) . ?
W2 O8 1.887(13) . ?
W2 O13 1.939(17) . ?
W3 O2 1.713(15) . ?
W3 O4 1.893(14) . ?
W3 O5 1.934(15) . ?
W3 O7 2.335(13) . ?
W3 O11 1.893(15) . ?
W3 O12 1.978(15) . ?
W4 O10 2.182(14) . ?
W4 O15 1.92(2) . ?
W4 O16 1.725(16) . ?
W4 O17 1.84(2) . ?
W4 O26 2.272(18) . ?
W4 O30 1.790(16) . ?
W5 O9 2.055(13) . ?
W5 O14 1.744(18) . ?
W5 O15 1.98(2) . ?
W5 O25 1.835(19) . ?
W5 O26 2.31(2) . ?
W5 O29 1.753(17) . ?
W6 O8 2.152(13) . ?
W6 O23 1.93(2) . ?
W6 O24 1.746(17) . ?
W6 O25 1.849(18) . ?
W6 O28 2.285(18) . ?
W6 O34 1.768(16) . ?
W7 O13 2.144(16) . ?
W7 O21 1.843(18) . ?
W7 O22 1.733(14) . ?
W7 O23 1.94(2) . ?
W7 O28 2.256(18) . ?
W7 O33 1.747(17) . ?
W8 O12 2.147(15) . ?
W8 O19 1.90(2) . ?
W8 O20 1.753(16) . ?
W8 O21 1.859(18) . ?
W8 O27 2.269(19) . ?
W8 O32 1.797(17) . ?
W9 O11 2.154(14) . ?
W9 O17 1.84(2) . ?
W9 O18 1.741(18) . ?
W9 O19 1.93(2) . ?
W9 O27 2.288(17) . ?
W9 O31 1.750(18) . ?
Si1 O7 1.674(13) . ?
Si1 O26 1.610(19) . ?
Si1 O27 1.62(2) . ?
Si1 O28 1.632(18) . ?
Ag1A Ag2A 2.806(6) . ?
Ag1A Ag3A 2.751(4) . ?
Ag1A Ag4 2.753(4) . ?
Ag1A O26 2.552(19) . ?
Ag1A O29 2.380(18) . ?
Ag1A O30 2.555(18) . ?
Ag1A Ag2 3.370(8) . ?
Ag1A Ag3 3.057(6) . ?
Ag2A Ag3A 2.731(5) . ?
Ag2A Ag4 2.744(4) . ?
Ag2A O27 2.516(17) . ?
Ag2A O31 2.598(17) . ?
Ag2A O32 2.457(17) . ?
Ag2A Ag1 2.835(8) . ?
Ag3A Ag4 2.824(3) . ?
Ag3A O33 2.521(16) . ?
Ag3A O34 2.40(2) . ?
Ag3A Ag1 3.097(7) . ?
Ag3A Cu6A 3.044(9) . ?
Ag3A Ag3 3.094(6) . ?
Ag1B Ag2B 2.797(12) . ?
Ag1B Ag3B 2.626(13) . ?
Ag1B Ag4 2.695(8) . ?
Ag1B O30 2.388(18) . ?
Ag1B Ag38 3.277(9) . ?
Ag1B Ag41 2.675(12) . ?
Ag2B Ag3B 2.789(13) . ?
Ag2B Ag4 2.780(8) . ?
Ag2B O33 2.451(18) . ?
Ag2B Ag39 2.758(11) . ?
Ag3B Ag4 2.791(7) . ?
Ag3B O29 2.531(19) . ?
Ag3B O34 2.459(19) . ?
Ag3B Ag3 2.202(9) . ?
Ag4 Ag39 2.928(7) . ?
Ag4 Ag41 2.865(7) . ?
Ag4 Ag1 2.813(7) . ?
Ag4 Cu6A 2.925(9) . ?
Ag4 Cl25 2.412(7) . ?
Ag4 Ag3 2.871(6) . ?
O14 Ag8A 2.46(2) . ?
O14 Ag8B 2.59(2) . ?
O18 Ag19 2.579(18) . ?
O20 Ag13 2.50(2) . ?
O22 Ag14 2.47(2) . ?
O23 Ag20 2.57(2) . ?
O29 Ag6 2.460(16) . ?
O30 Ag5A 2.476(16) . ?
O30 Ag5B 2.417(18) . ?
O31 Ag10 2.408(17) . ?
O32 Ag9A 2.413(19) . ?
O32 Ag9B 2.395(18) . ?
O33 Ag11 2.417(17) . ?
O34 Ag7 2.494(16) . ?
C30A H30A 0.9700 . ?
C30A H30B 0.9700 . ?
C30A P1A 1.70(15) . ?
C30A C329 1.53(14) . ?
P1A Ag9A 2.37(3) . ?
C30B H30C 0.9700 . ?
C30B H30D 0.9700 . ?
C30B P1B 1.90(8) . ?
C30B C329 1.38(8) . ?
P1B Ag9B 2.396(19) . ?
P1B C157 1.83(3) . ?
P1B C161 1.88(3) . ?
P11 Ag11 2.396(8) . ?
P11 C25 1.85(2) . ?
P11 C103 1.83(2) . ?
P11 C328 1.83(5) . ?
P12 Ag7 2.395(9) . ?
P12 C1 1.84(5) . ?
P12 C31 1.80(2) . ?
P12 C115 1.84(2) . ?
P13 Ag6 2.367(11) . ?
P13 C3 1.76(5) . ?
P13 C121 1.77(3) . ?
P13 C127 1.79(2) . ?
P14 Ag14 2.374(8) . ?
P14 C4 1.82(4) . ?
P14 C13 1.78(2) . ?
P14 C19 1.79(2) . ?
P15 Ag13 2.359(9) . ?
P15 C6 1.90(4) . ?
P15 C73 1.81(2) . ?
P15 C133 1.87(2) . ?
P16 Ag19 2.384(9) . ?
P16 C7 1.80(5) . ?
P16 C37 1.84(2) . ?
P16 C43 1.85(2) . ?
P17 Ag35 2.376(9) . ?
P17 C9 1.81(5) . ?
P17 C61 1.82(2) . ?
P17 C67 1.80(2) . ?
S1 Ag8A 2.360(11) . ?
S1 Ag8B 2.536(13) . ?
S1 Ag18 2.370(10) . ?
S1 Ag35 2.430(11) . ?
S1 C304 1.78(5) . ?
Ag5A P20 2.364(11) . ?
Ag5A S5 2.380(14) . ?
Ag5A S8 2.816(11) . ?
Ag5B Ag38 2.469(11) . ?
Ag5B P20 2.729(14) . ?
Ag5B S5 2.845(17) . ?
Ag5B S8 2.007(16) . ?
Ag6 S5 2.491(13) . ?
Ag6 S6 2.626(15) . ?
Ag7 S2 2.542(8) . ?
Ag7 S7 2.516(10) . ?
Ag8A P21 2.406(15) . ?
Ag8B P21 2.382(16) . ?
Ag9A S11 2.654(13) . ?
Ag9B Ag39 2.950(8) . ?
Ag9B S11 2.520(12) . ?
Ag9B S9B 2.841(8) . ?
Ag10 P19 2.385(11) . ?
Ag10 S11 2.430(11) . ?
Ag11 S2 2.500(10) . ?
Ag11 S10 2.758(12) . ?
Ag12 S3 2.358(9) . ?
Ag12 S11 2.349(11) . ?
Ag13 S3 2.444(9) . ?
Ag14 S4 2.456(11) . ?
Ag15 S4 2.407(12) . ?
Ag15 P18 2.379(14) . ?
Ag18 S5 2.355(11) . ?
Ag19 S3 2.440(9) . ?
Ag20 S2 2.385(9) . ?
Ag20 S4 2.387(11) . ?
Ag38 Ag41 3.342(8) . ?
Ag38 S6 2.314(15) . ?
Ag38 S8 2.443(12) . ?
Ag39 S10 2.576(14) . ?
Ag39 S9B 2.746(14) . ?
Ag41 S8 2.534(12) . ?
Ag41 S9B 2.187(11) . ?
C1 H1A 0.9700 . ?
C1 H1B 0.9700 . ?
C1 C2 1.47(6) . ?
C2 H2A 0.9700 . ?
C2 H2B 0.9700 . ?
C2 C3 1.61(6) . ?
C3 H3A 0.9700 . ?
C3 H3B 0.9700 . ?
C4 H4A 0.9700 . ?
C4 H4B 0.9700 . ?
C4 C5 1.48(5) . ?
C5 H5A 0.9700 . ?
C5 H5B 0.9700 . ?
C5 C6 1.54(5) . ?
C6 H6A 0.9700 . ?
C6 H6B 0.9700 . ?
C7 H7A 0.9700 . ?
C7 H7B 0.9700 . ?
C7 C8 1.46(6) . ?
C8 H8A 0.9700 . ?
C8 H8B 0.9700 . ?
C8 C9 1.53(6) . ?
C9 H9A 0.9700 . ?
C9 H9B 0.9700 . ?
C10 H10A 0.9700 . ?
C10 H10B 0.9700 . ?
C10 C11 1.48(6) . ?
C10 P19 1.89(5) . ?
C11 H11A 0.9700 . ?
C11 H11B 0.9700 . ?
C11 C12 1.52(6) . ?
C12 H12A 0.9700 . ?
C12 H12B 0.9700 . ?
C12 P20 1.84(5) . ?
C13 C14 1.3900 . ?
C13 C18 1.3900 . ?
C14 H14 0.9300 . ?
C14 C15 1.3900 . ?
C15 H15 0.9300 . ?
C15 C16 1.3900 . ?
C16 H16 0.9300 . ?
C16 C17 1.3900 . ?
C17 H17 0.9300 . ?
C17 C18 1.3900 . ?
C18 H18 0.9300 . ?
C19 C20 1.3900 . ?
C19 C24 1.3900 . ?
C20 H20 0.9300 . ?
C20 C21 1.3900 . ?
C21 H21 0.9300 . ?
C21 C22 1.3900 . ?
C22 H22 0.9300 . ?
C22 C23 1.3900 . ?
C23 H23 0.9300 . ?
C23 C24 1.3900 . ?
C24 H24 0.9300 . ?
C25 C26 1.3900 . ?
C25 C30 1.3900 . ?
C26 H26 0.9300 . ?
C26 C27 1.3900 . ?
C27 H27 0.9300 . ?
C27 C28 1.3900 . ?
C28 H28 0.9300 . ?
C28 C29 1.3900 . ?
C29 H29 0.9300 . ?
C29 C30 1.3900 . ?
C30 H30 0.9300 . ?
C31 C32 1.3900 . ?
C31 C36 1.3900 . ?
C32 H32 0.9300 . ?
C32 C33 1.3900 . ?
C33 H33 0.9300 . ?
C33 C34 1.3900 . ?
C34 H34 0.9300 . ?
C34 C35 1.3900 . ?
C35 H35 0.9300 . ?
C35 C36 1.3900 . ?
C36 H36 0.9300 . ?
C37 C38 1.3900 . ?
C37 C42 1.3900 . ?
C38 H38 0.9300 . ?
C38 C39 1.3900 . ?
C39 H39 0.9300 . ?
C39 C40 1.3900 . ?
C40 H40 0.9300 . ?
C40 C41 1.3900 . ?
C41 H41 0.9300 . ?
C41 C42 1.3900 . ?
C42 H42 0.9300 . ?
C43 C44 1.3900 . ?
C43 C48 1.3900 . ?
C44 H44 0.9300 . ?
C44 C45 1.3900 . ?
C45 H45 0.9300 . ?
C45 C46 1.3900 . ?
C46 H46 0.9300 . ?
C46 C47 1.3900 . ?
C47 H47 0.9300 . ?
C47 C48 1.3900 . ?
C48 H48 0.9300 . ?
C49 C50 1.3900 . ?
C49 C54 1.3900 . ?
C49 P19 1.77(3) . ?
C50 H50 0.9300 . ?
C50 C51 1.3900 . ?
C51 H51 0.9300 . ?
C51 C52 1.3900 . ?
C52 H52 0.9300 . ?
C52 C53 1.3900 . ?
C53 H53 0.9300 . ?
C53 C54 1.3900 . ?
C54 H54 0.9300 . ?
C55 C56 1.3900 . ?
C55 C60 1.3900 . ?
C55 P20 1.81(3) . ?
C56 H56 0.9300 . ?
C56 C57 1.3900 . ?
C57 H57 0.9300 . ?
C57 C58 1.3900 . ?
C58 H58 0.9300 . ?
C58 C59 1.3900 . ?
C59 H59 0.9300 . ?
C59 C60 1.3900 . ?
C60 H60 0.9300 . ?
C61 C62 1.3900 . ?
C61 C66 1.3900 . ?
C62 H62 0.9300 . ?
C62 C63 1.3900 . ?
C63 H63 0.9300 . ?
C63 C64 1.3900 . ?
C64 H64 0.9300 . ?
C64 C65 1.3900 . ?
C65 H65 0.9300 . ?
C65 C66 1.3900 . ?
C66 H66 0.9300 . ?
C67 C68 1.3900 . ?
C67 C72 1.3900 . ?
C68 H68 0.9300 . ?
C68 C69 1.3900 . ?
C69 H69 0.9300 . ?
C69 C70 1.3900 . ?
C70 H70 0.9300 . ?
C70 C71 1.3900 . ?
C71 H71 0.9300 . ?
C71 C72 1.3900 . ?
C72 H72 0.9300 . ?
C73 C74 1.3900 . ?
C73 C78 1.3900 . ?
C74 H74 0.9300 . ?
C74 C75 1.3900 . ?
C75 H75 0.9300 . ?
C75 C76 1.3900 . ?
C76 H76 0.9300 . ?
C76 C77 1.3900 . ?
C77 H77 0.9300 . ?
C77 C78 1.3900 . ?
C78 H78 0.9300 . ?
C79 C80 1.3900 . ?
C79 C84 1.3900 . ?
C79 P20 1.81(2) . ?
C80 H80 0.9300 . ?
C80 C81 1.3900 . ?
C81 H81 0.9300 . ?
C81 C82 1.3900 . ?
C82 H82 0.9300 . ?
C82 C83 1.3900 . ?
C83 H83 0.9300 . ?
C83 C84 1.3900 . ?
C84 H84 0.9300 . ?
C85 C86 1.3900 . ?
C85 C90 1.3900 . ?
C85 P19 1.89(2) . ?
C86 H86 0.9300 . ?
C86 C87 1.3900 . ?
C87 H87 0.9300 . ?
C87 C88 1.3900 . ?
C88 H88 0.9300 . ?
C88 C89 1.3900 . ?
C89 H89 0.9300 . ?
C89 C90 1.3900 . ?
C90 H90 0.9300 . ?
C91 C92 1.3900 . ?
C91 C96 1.3900 . ?
C91 P18 1.803(16) . ?
C92 H92 0.9300 . ?
C92 C93 1.3900 . ?
C93 H93 0.9300 . ?
C93 C94 1.3900 . ?
C94 H94 0.9300 . ?
C94 C95 1.3900 . ?
C95 H95 0.9300 . ?
C95 C96 1.3900 . ?
C96 H96 0.9300 . ?
C97 C98 1.3900 . ?
C97 C102 1.3900 . ?
C97 P18 1.82(2) . ?
C98 H98 0.9300 . ?
C98 C99 1.3900 . ?
C99 H99 0.9300 . ?
C99 C100 1.3900 . ?
C100 H100 0.9300 . ?
C100 C101 1.3900 . ?
C101 H101 0.9300 . ?
C101 C102 1.3900 . ?
C102 H102 0.9300 . ?
C103 C104 1.3900 . ?
C103 C108 1.3900 . ?
C104 H104 0.9300 . ?
C104 C105 1.3900 . ?
C105 H105 0.9300 . ?
C105 C106 1.3900 . ?
C106 H106 0.9300 . ?
C106 C107 1.3900 . ?
C107 H107 0.9300 . ?
C107 C108 1.3900 . ?
C108 H108 0.9300 . ?
C109 C110 1.3900 . ?
C109 C114 1.3900 . ?
C109 P21 1.70(2) . ?
C110 H110 0.9300 . ?
C110 C111 1.3900 . ?
C111 H111 0.9300 . ?
C111 C112 1.3900 . ?
C112 H112 0.9300 . ?
C112 C113 1.3900 . ?
C113 H113 0.9300 . ?
C113 C114 1.3900 . ?
C114 H114 0.9300 . ?
C115 C116 1.3900 . ?
C115 C120 1.3900 . ?
C116 H116 0.9300 . ?
C116 C117 1.3900 . ?
C117 H117 0.9300 . ?
C117 C118 1.3900 . ?
C118 H118 0.9300 . ?
C118 C119 1.3900 . ?
C119 H119 0.9300 . ?
C119 C120 1.3900 . ?
C120 H120 0.9300 . ?
C121 C122 1.3900 . ?
C121 C126 1.3900 . ?
C122 H122 0.9300 . ?
C122 C123 1.3900 . ?
C123 H123 0.9300 . ?
C123 C124 1.3900 . ?
C124 H124 0.9300 . ?
C124 C125 1.3900 . ?
C125 H125 0.9300 . ?
C125 C126 1.3900 . ?
C126 H126 0.9300 . ?
C127 C128 1.3900 . ?
C127 C132 1.3900 . ?
C128 H128 0.9300 . ?
C128 C129 1.3900 . ?
C129 H129 0.9300 . ?
C129 C130 1.3900 . ?
C130 H130 0.9300 . ?
C130 C131 1.3900 . ?
C131 H131 0.9300 . ?
C131 C132 1.3900 . ?
C132 H132 0.9300 . ?
C133 C134 1.3900 . ?
C133 C138 1.3900 . ?
C134 H134 0.9300 . ?
C134 C135 1.3900 . ?
C135 H135 0.9300 . ?
C135 C136 1.3900 . ?
C136 H136 0.9300 . ?
C136 C137 1.3900 . ?
C137 H137 0.9300 . ?
C137 C138 1.3900 . ?
C138 H138 0.9300 . ?
C139 H139 0.9300 . ?
C139 C140 1.3900 . ?
C139 C144 1.3900 . ?
C140 H140 0.9300 . ?
C140 C141 1.3900 . ?
C141 H141 0.9300 . ?
C141 C142 1.3900 . ?
C142 H142 0.9300 . ?
C142 C143 1.3900 . ?
C143 H143 0.9300 . ?
C143 C144 1.3900 . ?
C144 P21 1.70(3) . ?
C300 H300 0.9800 . ?
C300 C301 1.50(2) . ?
C300 C302 1.49(2) . ?
C300 S5 1.94(5) . ?
C301 H30E 0.9600 . ?
C301 H30F 0.9600 . ?
C301 H30G 0.9600 . ?
C302 H30H 0.9600 . ?
C302 H30I 0.9600 . ?
C302 H30J 0.9600 . ?
C303 H30K 0.9600 . ?
C303 H30L 0.9600 . ?
C303 H30M 0.9600 . ?
C303 C304 1.38(6) . ?
C304 H304 0.9800 . ?
C304 C305 1.48(6) . ?
C305 H30N 0.9600 . ?
C305 H30O 0.9600 . ?
C305 H30P 0.9600 . ?
C313 H31A 0.9600 . ?
C313 H31B 0.9600 . ?
C313 H31C 0.9600 . ?
C313 C314 1.49(2) . ?
C314 H314 0.9800 . ?
C314 C315 1.49(2) . ?
C314 S3 1.86(5) . ?
C315 H31D 0.9600 . ?
C315 H31E 0.9600 . ?
C315 H31F 0.9600 . ?
C316 H31G 0.9700 . ?
C316 H31H 0.9700 . ?
C316 C317 1.50(2) . ?
C316 P18 1.877(19) . ?
C317 H31I 0.9700 . ?
C317 H31J 0.9700 . ?
C317 C318 1.49(2) . ?
C318 H31K 0.9700 . ?
C318 H31L 0.9700 . ?
C318 P21 1.83(5) . ?
C319 H31M 0.9600 . ?
C319 H31N 0.9600 . ?
C319 H31O 0.9600 . ?
C319 C320 1.541(14) . ?
C320 H320 0.9800 . ?
C320 C321 1.535(14) . ?
C320 S11 1.89(5) . ?
C321 H32A 0.9600 . ?
C321 H32B 0.9600 . ?
C321 H32C 0.9600 . ?
C322 H32D 0.9600 . ?
C322 H32E 0.9600 . ?
C322 H32F 0.9600 . ?
C322 C323 1.52(2) . ?
C323 H323 0.9800 . ?
C323 C324 1.52(2) . ?
C323 S8 2.08(5) . ?
C324 H32G 0.9600 . ?
C324 H32H 0.9600 . ?
C324 H32I 0.9600 . ?
C309 H30Q 0.9600 . ?
C309 H30R 0.9600 . ?
C309 H30S 0.9600 . ?
C309 C310 1.476(19) . ?
C310 H310 0.9800 . ?
C310 C311 1.497(16) . ?
C310 S2 1.81(3) . ?
C311 H31P 0.9600 . ?
C311 H31Q 0.9600 . ?
C311 H31R 0.9600 . ?
C325 H32J 0.9600 . ?
C325 H32K 0.9600 . ?
C325 H32L 0.9600 . ?
C325 C326 1.48(3) . ?
C326 H326 0.9800 . ?
C326 C327 1.503(16) . ?
C326 S4 1.81(3) . ?
C327 H32M 0.9600 . ?
C327 H32N 0.9600 . ?
C327 H32O 0.9600 . ?
C328 H32P 0.9700 . ?
C328 H32Q 0.9700 . ?
C328 C329 1.43(6) . ?
C329 H32R 0.9700 . ?
C329 H32S 0.9700 . ?
Ag1 Cu6A 3.083(11) . ?
Ag1 S10 2.206(14) . ?
Cu6A S7 2.236(15) . ?
Cu6A S10 2.603(15) . ?
Cu6A Ag3 2.995(10) . ?
Ag2 S8 1.582(11) . ?
Cu6B S7 2.375(16) . ?
Cu6B S10 2.140(15) . ?
S6 C148 1.72(5) . ?
S6 Ag3 2.370(14) . ?
S7 C164 1.720(19) . ?
S7 Ag3 2.360(13) . ?
S10 C154 1.87(5) . ?
S9B C152 2.08(6) . ?
C146 H146 0.9300 . ?
C146 C157 1.3900 . ?
C146 C147 1.3900 . ?
C157 C145 1.3900 . ?
C145 H145 0.9300 . ?
C145 C171 1.3900 . ?
C171 H171 0.9300 . ?
C171 C201 1.3900 . ?
C201 H201 0.9300 . ?
C201 C147 1.3900 . ?
C147 H147 0.9300 . ?
C154 H154 0.9800 . ?
C154 C156 1.51(7) . ?
C154 C155 1.60(7) . ?
C156 H15A 0.9600 . ?
C156 H15B 0.9600 . ?
C156 H15C 0.9600 . ?
C151 H15D 0.9600 . ?
C151 H15E 0.9600 . ?
C151 H15F 0.9600 . ?
C151 C152 1.55(2) . ?
C148 H148 0.9800 . ?
C148 C149 1.53(2) . ?
C148 C150 1.53(2) . ?
C149 H14A 0.9600 . ?
C149 H14B 0.9600 . ?
C149 H14C 0.9600 . ?
C155 H15G 0.9600 . ?
C155 H15H 0.9600 . ?
C155 H15I 0.9600 . ?
C152 H152 0.9800 . ?
C152 C153 1.56(2) . ?
C150 H15J 0.9600 . ?
C150 H15K 0.9600 . ?
C150 H15L 0.9600 . ?
C153 H15M 0.9600 . ?
C153 H15N 0.9600 . ?
C153 H15O 0.9600 . ?
Sb1 F56 1.800(19) . ?
Sb1 F97 1.791(19) . ?
Sb1 F110 1.756(19) . ?
Sb1 F124 1.780(19) . ?
Sb1 F145 1.813(19) . ?
Sb1 F213 1.798(19) . ?
Sb2 F86 1.784(18) . ?
Sb2 F131 1.806(18) . ?
Sb2 F161 1.804(18) . ?
Sb2 F174 1.804(19) . ?
Sb2 F185 1.776(18) . ?
Sb2 F134 1.789(19) . ?
C161 C160 1.3900 . ?
C161 C162 1.3900 . ?
C160 H160 0.9300 . ?
C160 C159 1.3900 . ?
C159 H159 0.9300 . ?
C159 C158 1.3900 . ?
C158 H158 0.9300 . ?
C158 C163 1.3900 . ?
C163 H163 0.9300 . ?
C163 C162 1.3900 . ?
C162 H162 0.9300 . ?
C165 H16A 0.9600 . ?
C165 H16B 0.9600 . ?
C165 H16C 0.9600 . ?
C165 C164 1.51(6) . ?
C164 H164 0.9800 . ?
C164 C166 1.54(2) . ?
C166 H16D 0.9600 . ?
C166 H16E 0.9600 . ?
C166 H16F 0.9600 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O1 W1 O4 98.5(7) . . ?
O1 W1 O6 101.7(7) . . ?
O1 W1 O7 170.0(7) . . ?
O1 W1 O9 102.2(7) . . ?
O1 W1 O10 100.5(7) . . ?
O4 W1 O7 73.0(5) . . ?
O6 W1 O4 87.6(6) . . ?
O6 W1 O7 73.3(6) . . ?
O6 W1 O10 157.1(6) . . ?
O9 W1 O4 158.4(6) . . ?
O9 W1 O6 94.4(7) . . ?
O9 W1 O7 86.9(6) . . ?
O9 W1 O10 86.6(6) . . ?
O10 W1 O4 83.4(6) . . ?
O10 W1 O7 83.9(5) . . ?
O3 W2 O5 100.1(7) . . ?
O3 W2 O6 98.8(7) . . ?
O3 W2 O7 170.0(6) . . ?
O3 W2 O8 101.8(7) . . ?
O3 W2 O13 101.2(8) . . ?
O5 W2 O7 72.8(6) . . ?
O6 W2 O5 87.3(7) . . ?
O6 W2 O7 74.2(6) . . ?
O6 W2 O13 159.9(7) . . ?
O8 W2 O5 158.1(6) . . ?
O8 W2 O6 88.6(7) . . ?
O8 W2 O7 85.4(5) . . ?
O8 W2 O13 89.2(7) . . ?
O13 W2 O5 87.3(7) . . ?
O13 W2 O7 85.7(6) . . ?
O2 W3 O4 98.3(7) . . ?
O2 W3 O5 100.3(7) . . ?
O2 W3 O7 170.4(6) . . ?
O2 W3 O11 100.7(7) . . ?
O2 W3 O12 101.5(7) . . ?
O4 W3 O5 89.9(6) . . ?
O4 W3 O7 75.5(5) . . ?
O4 W3 O11 90.8(6) . . ?
O4 W3 O12 160.2(6) . . ?
O5 W3 O7 72.8(6) . . ?
O5 W3 O12 86.0(6) . . ?
O11 W3 O5 158.6(6) . . ?
O11 W3 O7 86.8(6) . . ?
O11 W3 O12 86.1(6) . . ?
O12 W3 O7 84.9(6) . . ?
O10 W4 O26 76.9(6) . . ?
O15 W4 O10 81.5(7) . . ?
O15 W4 O26 71.5(9) . . ?
O16 W4 O10 92.0(6) . . ?
O16 W4 O15 93.8(9) . . ?
O16 W4 O17 102.6(9) . . ?
O16 W4 O26 162.6(8) . . ?
O16 W4 O30 103.4(7) . . ?
O17 W4 O10 80.3(7) . . ?
O17 W4 O15 155.7(9) . . ?
O17 W4 O26 88.9(9) . . ?
O30 W4 O10 164.6(6) . . ?
O30 W4 O15 98.4(10) . . ?
O30 W4 O17 95.0(10) . . ?
O30 W4 O26 88.4(7) . . ?
O9 W5 O26 77.2(6) . . ?
O14 W5 O9 93.2(7) . . ?
O14 W5 O15 94.8(9) . . ?
O14 W5 O25 103.4(10) . . ?
O14 W5 O26 162.8(8) . . ?
O14 W5 O29 103.2(8) . . ?
O15 W5 O9 79.5(7) . . ?
O15 W5 O26 69.7(8) . . ?
O25 W5 O9 84.1(7) . . ?
O25 W5 O15 156.1(8) . . ?
O25 W5 O26 89.9(8) . . ?
O29 W5 O9 163.4(7) . . ?
O29 W5 O15 96.4(9) . . ?
O29 W5 O25 94.5(8) . . ?
O29 W5 O26 86.3(7) . . ?
O8 W6 O28 76.4(6) . . ?
O23 W6 O8 79.8(7) . . ?
O23 W6 O28 69.1(8) . . ?
O24 W6 O8 91.9(7) . . ?
O24 W6 O23 95.5(10) . . ?
O24 W6 O25 102.1(10) . . ?
O24 W6 O28 161.9(7) . . ?
O24 W6 O34 104.1(8) . . ?
O25 W6 O8 81.7(7) . . ?
O25 W6 O23 154.8(9) . . ?
O25 W6 O28 90.0(9) . . ?
O34 W6 O8 163.5(7) . . ?
O34 W6 O23 94.6(9) . . ?
O34 W6 O25 98.4(8) . . ?
O34 W6 O28 87.1(7) . . ?
O13 W7 O28 78.3(6) . . ?
O21 W7 O13 78.6(7) . . ?
O21 W7 O23 154.2(9) . . ?
O21 W7 O28 90.1(9) . . ?
O22 W7 O13 91.3(8) . . ?
O22 W7 O21 102.7(10) . . ?
O22 W7 O23 94.3(10) . . ?
O22 W7 O28 161.7(8) . . ?
O22 W7 O33 101.9(8) . . ?
O23 W7 O13 81.7(7) . . ?
O23 W7 O28 69.5(9) . . ?
O33 W7 O13 166.7(7) . . ?
O33 W7 O21 96.7(10) . . ?
O33 W7 O23 98.7(9) . . ?
O33 W7 O28 89.4(7) . . ?
O12 W8 O27 77.7(6) . . ?
O19 W8 O12 80.3(8) . . ?
O19 W8 O27 69.3(8) . . ?
O20 W8 O12 90.6(8) . . ?
O20 W8 O19 95.9(10) . . ?
O20 W8 O21 102.3(10) . . ?
O20 W8 O27 162.3(8) . . ?
O20 W8 O32 103.3(9) . . ?
O21 W8 O12 80.6(7) . . ?
O21 W8 O19 153.6(10) . . ?
O21 W8 O27 89.0(9) . . ?
O32 W8 O12 166.2(6) . . ?
O32 W8 O19 97.9(10) . . ?
O32 W8 O21 96.3(9) . . ?
O32 W8 O27 88.8(7) . . ?
O11 W9 O27 77.3(6) . . ?
O17 W9 O11 83.1(7) . . ?
O17 W9 O19 155.1(9) . . ?
O17 W9 O27 90.4(8) . . ?
O18 W9 O11 93.2(7) . . ?
O18 W9 O17 104.5(9) . . ?
O18 W9 O19 94.3(9) . . ?
O18 W9 O27 161.3(7) . . ?
O18 W9 O31 101.8(8) . . ?
O19 W9 O11 79.7(8) . . ?
O19 W9 O27 68.3(9) . . ?
O31 W9 O11 164.7(7) . . ?
O31 W9 O17 95.9(9) . . ?
O31 W9 O19 95.9(10) . . ?
O31 W9 O27 87.5(7) . . ?
O26 Si1 O7 106.8(9) . . ?
O26 Si1 O27 112.7(10) . . ?
O26 Si1 O28 113.4(11) . . ?
O27 Si1 O7 106.8(8) . . ?
O27 Si1 O28 111.6(10) . . ?
O28 Si1 O7 104.9(8) . . ?
Ag2A Ag1A Ag2 71.17(16) . . ?
Ag2A Ag1A Ag3 109.29(15) . . ?
Ag3A Ag1A Ag2A 58.85(12) . . ?
Ag3A Ag1A Ag4 61.73(10) . . ?
Ag3A Ag1A Ag2 113.87(17) . . ?
Ag3A Ag1A Ag3 64.13(14) . . ?
Ag4 Ag1A Ag2A 59.16(11) . . ?
Ag4 Ag1A Ag2 56.29(14) . . ?
Ag4 Ag1A Ag3 58.95(13) . . ?
O26 Ag1A Ag2A 86.8(5) . . ?
O26 Ag1A Ag3A 94.1(4) . . ?
O26 Ag1A Ag4 144.8(5) . . ?
O26 Ag1A O30 67.9(6) . . ?
O26 Ag1A Ag2 124.7(5) . . ?
O26 Ag1A Ag3 135.9(5) . . ?
O29 Ag1A Ag2A 149.9(4) . . ?
O29 Ag1A Ag3A 103.5(5) . . ?
O29 Ag1A Ag4 137.7(5) . . ?
O29 Ag1A O26 69.3(7) . . ?
O29 Ag1A O30 89.2(7) . . ?
O29 Ag1A Ag2 137.6(5) . . ?
O29 Ag1A Ag3 78.8(5) . . ?
O30 Ag1A Ag2A 98.8(5) . . ?
O30 Ag1A Ag3A 153.0(5) . . ?
O30 Ag1A Ag4 122.5(5) . . ?
O30 Ag1A Ag2 66.5(5) . . ?
O30 Ag1A Ag3 142.6(4) . . ?
Ag3 Ag1A Ag2 99.39(19) . . ?
Ag1A Ag2A Ag1 112.7(2) . . ?
Ag3A Ag2A Ag1A 59.56(13) . . ?
Ag3A Ag2A Ag4 62.09(11) . . ?
Ag3A Ag2A Ag1 67.59(17) . . ?
Ag4 Ag2A Ag1A 59.45(11) . . ?
Ag4 Ag2A Ag1 60.52(16) . . ?
O27 Ag2A Ag1A 90.4(5) . . ?
O27 Ag2A Ag3A 96.1(4) . . ?
O27 Ag2A Ag4 148.5(5) . . ?
O27 Ag2A O31 66.9(6) . . ?
O27 Ag2A Ag1 135.1(4) . . ?
O31 Ag2A Ag1A 100.0(5) . . ?
O31 Ag2A Ag3A 154.4(4) . . ?
O31 Ag2A Ag4 123.4(4) . . ?
O31 Ag2A Ag1 138.0(5) . . ?
O32 Ag2A Ag1A 155.6(5) . . ?
O32 Ag2A Ag3A 106.4(5) . . ?
O32 Ag2A Ag4 135.1(4) . . ?
O32 Ag2A O27 70.3(6) . . ?
O32 Ag2A O31 86.4(7) . . ?
O32 Ag2A Ag1 74.8(5) . . ?
Ag1A Ag3A Ag4 59.16(10) . . ?
Ag1A Ag3A Ag1 106.68(18) . . ?
Ag1A Ag3A Cu6A 110.3(2) . . ?
Ag1A Ag3A Ag3 62.74(14) . . ?
Ag2A Ag3A Ag1A 61.59(14) . . ?
Ag2A Ag3A Ag4 59.19(10) . . ?
Ag2A Ag3A Ag1 57.81(16) . . ?
Ag2A Ag3A Cu6A 108.99(19) . . ?
Ag2A Ag3A Ag3 110.28(15) . . ?
Ag4 Ag3A Ag1 56.50(15) . . ?
Ag4 Ag3A Cu6A 59.67(17) . . ?
Ag4 Ag3A Ag3 57.82(13) . . ?
O33 Ag3A Ag1A 144.6(4) . . ?
O33 Ag3A Ag2A 93.7(5) . . ?
O33 Ag3A Ag4 131.8(5) . . ?
O33 Ag3A Ag1 75.4(5) . . ?
O33 Ag3A Cu6A 101.4(4) . . ?
O33 Ag3A Ag3 152.2(5) . . ?
O34 Ag3A Ag1A 98.4(5) . . ?
O34 Ag3A Ag2A 145.8(4) . . ?
O34 Ag3A Ag4 136.8(4) . . ?
O34 Ag3A O33 88.7(7) . . ?
O34 Ag3A Ag1 153.7(5) . . ?
O34 Ag3A Cu6A 103.9(4) . . ?
O34 Ag3A Ag3 79.3(4) . . ?
Cu6A Ag3A Ag1 60.3(2) . . ?
Cu6A Ag3A Ag3 58.4(2) . . ?
Ag3 Ag3A Ag1 105.20(19) . . ?
Ag2B Ag1B Ag38 122.2(3) . . ?
Ag3B Ag1B Ag2B 61.8(3) . . ?
Ag3B Ag1B Ag4 63.3(3) . . ?
Ag3B Ag1B Ag38 81.0(3) . . ?
Ag3B Ag1B Ag41 126.8(4) . . ?
Ag4 Ag1B Ag2B 60.8(2) . . ?
Ag4 Ag1B Ag38 63.45(19) . . ?
O30 Ag1B Ag2B 161.6(6) . . ?
O30 Ag1B Ag3B 109.8(7) . . ?
O30 Ag1B Ag4 132.5(5) . . ?
O30 Ag1B Ag38 69.0(5) . . ?
O30 Ag1B Ag41 97.8(6) . . ?
Ag41 Ag1B Ag2B 100.2(3) . . ?
Ag41 Ag1B Ag4 64.5(2) . . ?
Ag41 Ag1B Ag38 67.4(2) . . ?
Ag3B Ag2B Ag1B 56.1(3) . . ?
Ag4 Ag2B Ag1B 57.8(2) . . ?
Ag4 Ag2B Ag3B 60.2(2) . . ?
O33 Ag2B Ag1B 144.6(6) . . ?
O33 Ag2B Ag3B 100.3(6) . . ?
O33 Ag2B Ag4 137.7(6) . . ?
O33 Ag2B Ag39 107.6(6) . . ?
Ag39 Ag2B Ag1B 107.4(4) . . ?
Ag39 Ag2B Ag3B 120.4(3) . . ?
Ag39 Ag2B Ag4 63.8(2) . . ?
Ag1B Ag3B Ag2B 62.1(3) . . ?
Ag1B Ag3B Ag4 59.6(2) . . ?
Ag2B Ag3B Ag4 59.8(2) . . ?
O29 Ag3B Ag1B 90.2(5) . . ?
O29 Ag3B Ag2B 143.3(5) . . ?
O29 Ag3B Ag4 128.2(5) . . ?
O34 Ag3B Ag1B 143.2(5) . . ?
O34 Ag3B Ag2B 95.1(5) . . ?
O34 Ag3B Ag4 135.6(5) . . ?
O34 Ag3B O29 94.4(7) . . ?
Ag3 Ag3B Ag1B 117.0(4) . . ?
Ag3 Ag3B Ag2B 118.5(3) . . ?
Ag3 Ag3B Ag4 69.0(2) . . ?
Ag3 Ag3B O29 94.8(5) . . ?
Ag3 Ag3B O34 99.0(5) . . ?
Ag1A Ag4 Ag3A 59.10(10) . . ?
Ag1A Ag4 Ag1 115.07(17) . . ?
Ag1A Ag4 Cu6A 113.8(2) . . ?
Ag1A Ag4 Ag3 65.82(15) . . ?
Ag2A Ag4 Ag1A 61.40(12) . . ?
Ag2A Ag4 Ag3A 58.72(11) . . ?
Ag2A Ag4 Ag1 61.34(17) . . ?
Ag2A Ag4 Cu6A 112.11(19) . . ?
Ag2A Ag4 Ag3 116.85(16) . . ?
Ag3A Ag4 Cu6A 63.91(18) . . ?
Ag3A Ag4 Ag3 65.82(15) . . ?
Ag1B Ag4 Ag2B 61.4(2) . . ?
Ag1B Ag4 Ag3B 57.2(3) . . ?
Ag1B Ag4 Ag39 105.5(3) . . ?
Ag1B Ag4 Ag41 57.4(3) . . ?
Ag1B Ag4 Ag3 95.5(3) . . ?
Ag2B Ag4 Ag3B 60.1(3) . . ?
Ag2B Ag4 Ag39 57.7(2) . . ?
Ag2B Ag4 Ag41 96.1(2) . . ?
Ag2B Ag4 Ag3 99.1(2) . . ?
Ag3B Ag4 Ag39 114.6(2) . . ?
Ag3B Ag4 Ag41 113.9(2) . . ?
Ag3B Ag4 Ag3 45.7(2) . . ?
Ag41 Ag4 Ag39 90.8(2) . . ?
Ag41 Ag4 Ag3 136.3(2) . . ?
Ag1 Ag4 Ag3A 66.66(16) . . ?
Ag1 Ag4 Cu6A 65.0(2) . . ?
Ag1 Ag4 Ag3 119.85(19) . . ?
Cl25 Ag4 Ag1A 144.1(3) . . ?
Cl25 Ag4 Ag2A 154.3(3) . . ?
Cl25 Ag4 Ag3A 129.3(3) . . ?
Cl25 Ag4 Ag1B 159.2(3) . . ?
Cl25 Ag4 Ag2B 139.0(3) . . ?
Cl25 Ag4 Ag3B 130.5(3) . . ?
Cl25 Ag4 Ag39 88.8(3) . . ?
Cl25 Ag4 Ag41 108.3(3) . . ?
Cl25 Ag4 Ag1 97.5(3) . . ?
Cl25 Ag4 Cu6A 65.8(3) . . ?
Cl25 Ag4 Ag3 85.7(3) . . ?
Ag3 Ag4 Ag39 131.57(19) . . ?
Ag3 Ag4 Cu6A 62.2(2) . . ?
W3 O4 W1 119.8(7) . . ?
W3 O5 W2 121.2(8) . . ?
W1 O6 W2 120.7(8) . . ?
W2 O7 W1 91.8(5) . . ?
W2 O7 W3 93.2(5) . . ?
W3 O7 W1 91.7(5) . . ?
Si1 O7 W1 122.7(8) . . ?
Si1 O7 W2 124.4(8) . . ?
Si1 O7 W3 123.9(8) . . ?
W2 O8 W6 145.0(9) . . ?
W1 O9 W5 149.3(8) . . ?
W1 O10 W4 140.2(7) . . ?
W3 O11 W9 145.7(7) . . ?
W3 O12 W8 142.9(7) . . ?
W2 O13 W7 141.0(8) . . ?
W5 O14 Ag8A 126.6(9) . . ?
W5 O14 Ag8B 110.2(8) . . ?
W4 O15 W5 122.1(13) . . ?
W9 O17 W4 156.1(13) . . ?
W9 O18 Ag19 107.8(8) . . ?
W8 O19 W9 125.2(13) . . ?
W8 O20 Ag13 110.6(9) . . ?
W7 O21 W8 154.1(14) . . ?
W7 O22 Ag14 109.0(9) . . ?
W6 O23 W7 123.5(13) . . ?
W6 O23 Ag20 110.2(8) . . ?
W7 O23 Ag20 117.3(9) . . ?
W5 O25 W6 155.7(14) . . ?
W4 O26 W5 96.3(7) . . ?
W4 O26 Ag1A 94.9(6) . . ?
W5 O26 Ag1A 91.0(7) . . ?
Si1 O26 W4 129.7(13) . . ?
Si1 O26 W5 127.1(11) . . ?
Si1 O26 Ag1A 107.0(9) . . ?
W8 O27 W9 96.7(7) . . ?
W8 O27 Ag2A 92.7(7) . . ?
W9 O27 Ag2A 96.3(6) . . ?
Si1 O27 W8 129.5(9) . . ?
Si1 O27 W9 126.8(10) . . ?
Si1 O27 Ag2A 104.9(8) . . ?
W7 O28 W6 97.3(6) . . ?
Si1 O28 W6 127.7(10) . . ?
Si1 O28 W7 128.6(10) . . ?
W5 O29 Ag1A 113.4(8) . . ?
W5 O29 Ag3B 116.0(8) . . ?
W5 O29 Ag6 122.0(8) . . ?
Ag1A O29 Ag6 115.2(7) . . ?
Ag6 O29 Ag3B 121.7(7) . . ?
W4 O30 Ag1A 108.7(8) . . ?
W4 O30 Ag1B 108.6(8) . . ?
W4 O30 Ag5A 120.3(8) . . ?
W4 O30 Ag5B 139.6(9) . . ?
Ag1B O30 Ag5B 111.8(7) . . ?
Ag5A O30 Ag1A 117.6(7) . . ?
W9 O31 Ag2A 109.4(7) . . ?
W9 O31 Ag10 118.3(9) . . ?
Ag10 O31 Ag2A 122.8(7) . . ?
W8 O32 Ag2A 108.2(7) . . ?
W8 O32 Ag9A 122.5(9) . . ?
W8 O32 Ag9B 143.0(10) . . ?
Ag9A O32 Ag2A 122.5(8) . . ?
W7 O33 Ag3A 112.6(8) . . ?
W7 O33 Ag2B 112.8(8) . . ?
W7 O33 Ag11 122.7(8) . . ?
Ag11 O33 Ag3A 112.9(7) . . ?
Ag11 O33 Ag2B 124.5(7) . . ?
W6 O34 Ag3A 115.7(8) . . ?
W6 O34 Ag3B 113.6(8) . . ?
W6 O34 Ag7 125.8(9) . . ?
Ag3A O34 Ag7 113.0(7) . . ?
Ag3B O34 Ag7 119.0(7) . . ?
H30A C30A H30B 108.4 . . ?
P1A C30A H30A 110.1 . . ?
P1A C30A H30B 110.1 . . ?
C329 C30A H30A 110.1 . . ?
C329 C30A H30B 110.1 . . ?
C329 C30A P1A 108(9) . . ?
C30A P1A Ag9A 117(5) . . ?
H30C C30B H30D 106.3 . . ?
P1B C30B H30C 106.0 . . ?
P1B C30B H30D 106.0 . . ?
C329 C30B H30C 106.0 . . ?
C329 C30B H30D 106.0 . . ?
C329 C30B P1B 125(5) . . ?
C30B P1B Ag9B 121(3) . . ?
C157 P1B C30B 101(3) . . ?
C157 P1B Ag9B 115.7(18) . . ?
C157 P1B C161 101.8(18) . . ?
C161 P1B C30B 102(3) . . ?
C161 P1B Ag9B 112.2(15) . . ?
C25 P11 Ag11 117.0(12) . . ?
C103 P11 Ag11 113.7(11) . . ?
C103 P11 C25 101.0(14) . . ?
C103 P11 C328 106(2) . . ?
C328 P11 Ag11 113.4(15) . . ?
C328 P11 C25 104.2(18) . . ?
C1 P12 Ag7 111.8(15) . . ?
C31 P12 Ag7 116.2(11) . . ?
C31 P12 C1 104.3(19) . . ?
C31 P12 C115 102.0(14) . . ?
C115 P12 Ag7 115.5(12) . . ?
C115 P12 C1 105.8(18) . . ?
C3 P13 Ag6 118.9(16) . . ?
C3 P13 C121 108(2) . . ?
C3 P13 C127 101.4(18) . . ?
C121 P13 Ag6 107.4(7) . . ?
C121 P13 C127 104.5(11) . . ?
C127 P13 Ag6 115.8(13) . . ?
C4 P14 Ag14 115.5(14) . . ?
C13 P14 Ag14 115.3(11) . . ?
C13 P14 C4 105.3(18) . . ?
C13 P14 C19 106.4(14) . . ?
C19 P14 Ag14 111.0(10) . . ?
C19 P14 C4 102.2(17) . . ?
C6 P15 Ag13 118.1(14) . . ?
C73 P15 Ag13 116.2(11) . . ?
C73 P15 C6 106.2(17) . . ?
C73 P15 C133 103.7(14) . . ?
C133 P15 Ag13 113.9(10) . . ?
C133 P15 C6 96.0(17) . . ?
C7 P16 Ag19 118.5(15) . . ?
C7 P16 C37 106.1(18) . . ?
C7 P16 C43 103.4(18) . . ?
C37 P16 Ag19 111.0(11) . . ?
C37 P16 C43 103.1(14) . . ?
C43 P16 Ag19 113.3(11) . . ?
C9 P17 Ag35 122.6(15) . . ?
C9 P17 C61 102.4(19) . . ?
C61 P17 Ag35 105.6(11) . . ?
C67 P17 Ag35 114.6(11) . . ?
C67 P17 C9 101.4(18) . . ?
C67 P17 C61 109.3(15) . . ?
Ag8A S1 Ag18 104.4(4) . . ?
Ag8A S1 Ag35 113.8(5) . . ?
Ag18 S1 Ag8B 112.5(4) . . ?
Ag18 S1 Ag35 106.9(4) . . ?
Ag35 S1 Ag8B 94.6(4) . . ?
C304 S1 Ag8A 104.9(17) . . ?
C304 S1 Ag8B 114.3(17) . . ?
C304 S1 Ag18 114.2(18) . . ?
C304 S1 Ag35 112.4(18) . . ?
O30 Ag5A S8 77.3(5) . . ?
P20 Ag5A O30 109.7(6) . . ?
P20 Ag5A S5 133.0(4) . . ?
P20 Ag5A S8 92.2(4) . . ?
S5 Ag5A O30 101.0(6) . . ?
S5 Ag5A S8 129.6(4) . . ?
O30 Ag5B Ag38 84.7(5) . . ?
O30 Ag5B P20 100.3(6) . . ?
O30 Ag5B S5 90.4(7) . . ?
Ag38 Ag5B P20 168.3(6) . . ?
Ag38 Ag5B S5 87.8(4) . . ?
P20 Ag5B S5 102.6(5) . . ?
S8 Ag5B O30 96.7(7) . . ?
S8 Ag5B Ag38 65.2(5) . . ?
S8 Ag5B P20 103.5(5) . . ?
S8 Ag5B S5 151.2(6) . . ?
O29 Ag6 S5 101.0(6) . . ?
O29 Ag6 S6 85.6(5) . . ?
P13 Ag6 O29 104.7(5) . . ?
P13 Ag6 S5 137.4(4) . . ?
P13 Ag6 S6 120.0(4) . . ?
S5 Ag6 S6 95.1(4) . . ?
O34 Ag7 S2 90.6(5) . . ?
O34 Ag7 S7 87.2(5) . . ?
P12 Ag7 O34 111.3(5) . . ?
P12 Ag7 S2 132.5(3) . . ?
P12 Ag7 S7 121.6(4) . . ?
S7 Ag7 S2 100.4(4) . . ?
S1 Ag8A O14 96.7(5) . . ?
S1 Ag8A P21 157.2(5) . . ?
P21 Ag8A O14 104.0(6) . . ?
S1 Ag8B O14 89.1(5) . . ?
P21 Ag8B O14 100.7(6) . . ?
P21 Ag8B S1 143.6(6) . . ?
O32 Ag9A S11 94.3(6) . . ?
P1A Ag9A O32 106.5(8) . . ?
P1A Ag9A S11 136.5(9) . . ?
O32 Ag9B P1B 104.0(7) . . ?
O32 Ag9B Ag39 81.1(5) . . ?
O32 Ag9B S11 98.2(5) . . ?
O32 Ag9B S9B 95.1(4) . . ?
P1B Ag9B Ag39 97.2(6) . . ?
P1B Ag9B S11 125.4(6) . . ?
P1B Ag9B S9B 144.9(7) . . ?
S11 Ag9B Ag39 135.5(3) . . ?
S11 Ag9B S9B 79.4(4) . . ?
S9B Ag9B Ag39 56.6(3) . . ?
O31 Ag10 S11 99.0(5) . . ?
P19 Ag10 O31 109.7(5) . . ?
P19 Ag10 S11 144.6(4) . . ?
O33 Ag11 S2 96.1(6) . . ?
O33 Ag11 S10 82.9(5) . . ?
P11 Ag11 O33 106.7(5) . . ?
P11 Ag11 S2 135.3(3) . . ?
P11 Ag11 S10 109.1(4) . . ?
S2 Ag11 S10 111.5(3) . . ?
S11 Ag12 S3 178.2(4) . . ?
P15 Ag13 O20 123.6(6) . . ?
P15 Ag13 S3 142.1(3) . . ?
S3 Ag13 O20 93.0(5) . . ?
P14 Ag14 O22 119.0(5) . . ?
P14 Ag14 S4 139.7(3) . . ?
S4 Ag14 O22 98.9(5) . . ?
P18 Ag15 S4 156.6(4) . . ?
S5 Ag18 S1 179.0(4) . . ?
P16 Ag19 O18 112.2(4) . . ?
P16 Ag19 S3 146.7(3) . . ?
S3 Ag19 O18 94.0(4) . . ?
S2 Ag20 O23 99.2(5) . . ?
S2 Ag20 S4 172.9(4) . . ?
S4 Ag20 O23 76.7(5) . . ?
P17 Ag35 S1 143.8(3) . . ?
Ag1B Ag38 Ag41 47.7(2) . . ?
Ag4 Ag38 Ag1B 49.32(14) . . ?
Ag4 Ag38 Ag41 52.05(14) . . ?
Ag5B Ag38 Ag1B 86.4(3) . . ?
Ag5B Ag38 Ag4 132.3(3) . . ?
Ag5B Ag38 Ag41 86.7(3) . . ?
S6 Ag38 Ag1B 108.9(4) . . ?
S6 Ag38 Ag4 91.1(3) . . ?
S6 Ag38 Ag5B 124.2(5) . . ?
S6 Ag38 Ag41 143.1(4) . . ?
S6 Ag38 S8 167.8(4) . . ?
S8 Ag38 Ag1B 81.4(3) . . ?
S8 Ag38 Ag4 100.7(3) . . ?
S8 Ag38 Ag5B 48.2(4) . . ?
S8 Ag38 Ag41 49.0(3) . . ?
Ag2B Ag39 Ag4 58.5(2) . . ?
Ag2B Ag39 Ag9B 89.4(3) . . ?
Ag4 Ag39 Ag9B 121.4(2) . . ?
S10 Ag39 Ag2B 83.7(4) . . ?
S10 Ag39 Ag4 101.0(4) . . ?
S10 Ag39 Ag9B 124.5(4) . . ?
S10 Ag39 S9B 173.5(4) . . ?
S9B Ag39 Ag2B 91.6(3) . . ?
S9B Ag39 Ag4 72.7(2) . . ?
S9B Ag39 Ag9B 59.7(2) . . ?
Ag1B Ag41 Ag4 58.1(2) . . ?
Ag1B Ag41 Ag38 64.9(3) . . ?
Ag4 Ag41 Ag38 61.04(16) . . ?
S8 Ag41 Ag1B 93.1(4) . . ?
S8 Ag41 Ag4 107.4(4) . . ?
S8 Ag41 Ag38 46.7(3) . . ?
S9B Ag41 Ag1B 107.0(4) . . ?
S9B Ag41 Ag4 82.4(4) . . ?
S9B Ag41 Ag38 141.5(4) . . ?
S9B Ag41 S8 159.7(5) . . ?
P12 C1 H1A 109.3 . . ?
P12 C1 H1B 109.3 . . ?
H1A C1 H1B 107.9 . . ?
C2 C1 P12 112(4) . . ?
C2 C1 H1A 109.3 . . ?
C2 C1 H1B 109.3 . . ?
C1 C2 H2A 109.0 . . ?
C1 C2 H2B 109.0 . . ?
C1 C2 C3 113(4) . . ?
H2A C2 H2B 107.8 . . ?
C3 C2 H2A 109.0 . . ?
C3 C2 H2B 109.0 . . ?
P13 C3 H3A 108.7 . . ?
P13 C3 H3B 108.7 . . ?
C2 C3 P13 114(4) . . ?
C2 C3 H3A 108.7 . . ?
C2 C3 H3B 108.7 . . ?
H3A C3 H3B 107.6 . . ?
P14 C4 H4A 108.2 . . ?
P14 C4 H4B 108.2 . . ?
H4A C4 H4B 107.4 . . ?
C5 C4 P14 116(3) . . ?
C5 C4 H4A 108.2 . . ?
C5 C4 H4B 108.2 . . ?
C4 C5 H5A 110.7 . . ?
C4 C5 H5B 110.7 . . ?
C4 C5 C6 105(4) . . ?
H5A C5 H5B 108.8 . . ?
C6 C5 H5A 110.7 . . ?
C6 C5 H5B 110.7 . . ?
P15 C6 H6A 108.7 . . ?
P15 C6 H6B 108.7 . . ?
C5 C6 P15 114(3) . . ?
C5 C6 H6A 108.7 . . ?
C5 C6 H6B 108.7 . . ?
H6A C6 H6B 107.6 . . ?
P16 C7 H7A 108.8 . . ?
P16 C7 H7B 108.8 . . ?
H7A C7 H7B 107.6 . . ?
C8 C7 P16 114(3) . . ?
C8 C7 H7A 108.8 . . ?
C8 C7 H7B 108.8 . . ?
C7 C8 H8A 109.1 . . ?
C7 C8 H8B 109.1 . . ?
C7 C8 C9 113(4) . . ?
H8A C8 H8B 107.8 . . ?
C9 C8 H8A 109.1 . . ?
C9 C8 H8B 109.1 . . ?
P17 C9 H9A 107.8 . . ?
P17 C9 H9B 107.8 . . ?
C8 C9 P17 118(3) . . ?
C8 C9 H9A 107.8 . . ?
C8 C9 H9B 107.8 . . ?
H9A C9 H9B 107.1 . . ?
H10A C10 H10B 107.4 . . ?
C11 C10 H10A 108.4 . . ?
C11 C10 H10B 108.4 . . ?
C11 C10 P19 116(4) . . ?
P19 C10 H10A 108.4 . . ?
P19 C10 H10B 108.4 . . ?
C10 C11 H11A 109.0 . . ?
C10 C11 H11B 109.0 . . ?
C10 C11 C12 113(4) . . ?
H11A C11 H11B 107.8 . . ?
C12 C11 H11A 109.0 . . ?
C12 C11 H11B 109.0 . . ?
C11 C12 H12A 109.1 . . ?
C11 C12 H12B 109.1 . . ?
C11 C12 P20 112(4) . . ?
H12A C12 H12B 107.9 . . ?
P20 C12 H12A 109.1 . . ?
P20 C12 H12B 109.1 . . ?
C14 C13 P14 120.2(19) . . ?
C14 C13 C18 120.0 . . ?
C18 C13 P14 119.6(19) . . ?
C13 C14 H14 120.0 . . ?
C15 C14 C13 120.0 . . ?
C15 C14 H14 120.0 . . ?
C14 C15 H15 120.0 . . ?
C14 C15 C16 120.0 . . ?
C16 C15 H15 120.0 . . ?
C15 C16 H16 120.0 . . ?
C17 C16 C15 120.0 . . ?
C17 C16 H16 120.0 . . ?
C16 C17 H17 120.0 . . ?
C18 C17 C16 120.0 . . ?
C18 C17 H17 120.0 . . ?
C13 C18 H18 120.0 . . ?
C17 C18 C13 120.0 . . ?
C17 C18 H18 120.0 . . ?
C20 C19 P14 125.2(18) . . ?
C20 C19 C24 120.0 . . ?
C24 C19 P14 114.8(18) . . ?
C19 C20 H20 120.0 . . ?
C21 C20 C19 120.0 . . ?
C21 C20 H20 120.0 . . ?
C20 C21 H21 120.0 . . ?
C20 C21 C22 120.0 . . ?
C22 C21 H21 120.0 . . ?
C21 C22 H22 120.0 . . ?
C23 C22 C21 120.0 . . ?
C23 C22 H22 120.0 . . ?
C22 C23 H23 120.0 . . ?
C24 C23 C22 120.0 . . ?
C24 C23 H23 120.0 . . ?
C19 C24 H24 120.0 . . ?
C23 C24 C19 120.0 . . ?
C23 C24 H24 120.0 . . ?
C26 C25 P11 123(2) . . ?
C26 C25 C30 120.0 . . ?
C30 C25 P11 117(2) . . ?
C25 C26 H26 120.0 . . ?
C25 C26 C27 120.0 . . ?
C27 C26 H26 120.0 . . ?
C26 C27 H27 120.0 . . ?
C26 C27 C28 120.0 . . ?
C28 C27 H27 120.0 . . ?
C27 C28 H28 120.0 . . ?
C29 C28 C27 120.0 . . ?
C29 C28 H28 120.0 . . ?
C28 C29 H29 120.0 . . ?
C30 C29 C28 120.0 . . ?
C30 C29 H29 120.0 . . ?
C25 C30 H30 120.0 . . ?
C29 C30 C25 120.0 . . ?
C29 C30 H30 120.0 . . ?
C32 C31 P12 115.7(18) . . ?
C32 C31 C36 120.0 . . ?
C36 C31 P12 124.3(18) . . ?
C31 C32 H32 120.0 . . ?
C33 C32 C31 120.0 . . ?
C33 C32 H32 120.0 . . ?
C32 C33 H33 120.0 . . ?
C32 C33 C34 120.0 . . ?
C34 C33 H33 120.0 . . ?
C33 C34 H34 120.0 . . ?
C35 C34 C33 120.0 . . ?
C35 C34 H34 120.0 . . ?
C34 C35 H35 120.0 . . ?
C36 C35 C34 120.0 . . ?
C36 C35 H35 120.0 . . ?
C31 C36 H36 120.0 . . ?
C35 C36 C31 120.0 . . ?
C35 C36 H36 120.0 . . ?
C38 C37 P16 123(2) . . ?
C38 C37 C42 120.0 . . ?
C42 C37 P16 117(2) . . ?
C37 C38 H38 120.0 . . ?
C39 C38 C37 120.0 . . ?
C39 C38 H38 120.0 . . ?
C38 C39 H39 120.0 . . ?
C38 C39 C40 120.0 . . ?
C40 C39 H39 120.0 . . ?
C39 C40 H40 120.0 . . ?
C39 C40 C41 120.0 . . ?
C41 C40 H40 120.0 . . ?
C40 C41 H41 120.0 . . ?
C42 C41 C40 120.0 . . ?
C42 C41 H41 120.0 . . ?
C37 C42 H42 120.0 . . ?
C41 C42 C37 120.0 . . ?
C41 C42 H42 120.0 . . ?
C44 C43 P16 116.8(18) . . ?
C44 C43 C48 120.0 . . ?
C48 C43 P16 123.2(18) . . ?
C43 C44 H44 120.0 . . ?
C45 C44 C43 120.0 . . ?
C45 C44 H44 120.0 . . ?
C44 C45 H45 120.0 . . ?
C46 C45 C44 120.0 . . ?
C46 C45 H45 120.0 . . ?
C45 C46 H46 120.0 . . ?
C45 C46 C47 120.0 . . ?
C47 C46 H46 120.0 . . ?
C46 C47 H47 120.0 . . ?
C48 C47 C46 120.0 . . ?
C48 C47 H47 120.0 . . ?
C43 C48 H48 120.0 . . ?
C47 C48 C43 120.0 . . ?
C47 C48 H48 120.0 . . ?
C50 C49 C54 120.0 . . ?
C50 C49 P19 118.5(19) . . ?
C54 C49 P19 121.2(19) . . ?
C49 C50 H50 120.0 . . ?
C51 C50 C49 120.0 . . ?
C51 C50 H50 120.0 . . ?
C50 C51 H51 120.0 . . ?
C52 C51 C50 120.0 . . ?
C52 C51 H51 120.0 . . ?
C51 C52 H52 120.0 . . ?
C51 C52 C53 120.0 . . ?
C53 C52 H52 120.0 . . ?
C52 C53 H53 120.0 . . ?
C54 C53 C52 120.0 . . ?
C54 C53 H53 120.0 . . ?
C49 C54 H54 120.0 . . ?
C53 C54 C49 120.0 . . ?
C53 C54 H54 120.0 . . ?
C56 C55 C60 120.0 . . ?
C56 C55 P20 117.4(19) . . ?
C60 C55 P20 122.1(19) . . ?
C55 C56 H56 120.0 . . ?
C57 C56 C55 120.0 . . ?
C57 C56 H56 120.0 . . ?
C56 C57 H57 120.0 . . ?
C58 C57 C56 120.0 . . ?
C58 C57 H57 120.0 . . ?
C57 C58 H58 120.0 . . ?
C57 C58 C59 120.0 . . ?
C59 C58 H58 120.0 . . ?
C58 C59 H59 120.0 . . ?
C58 C59 C60 120.0 . . ?
C60 C59 H59 120.0 . . ?
C55 C60 H60 120.0 . . ?
C59 C60 C55 120.0 . . ?
C59 C60 H60 120.0 . . ?
C62 C61 P17 115.8(19) . . ?
C62 C61 C66 120.0 . . ?
C66 C61 P17 124(2) . . ?
C61 C62 H62 120.0 . . ?
C63 C62 C61 120.0 . . ?
C63 C62 H62 120.0 . . ?
C62 C63 H63 120.0 . . ?
C64 C63 C62 120.0 . . ?
C64 C63 H63 120.0 . . ?
C63 C64 H64 120.0 . . ?
C65 C64 C63 120.0 . . ?
C65 C64 H64 120.0 . . ?
C64 C65 H65 120.0 . . ?
C64 C65 C66 120.0 . . ?
C66 C65 H65 120.0 . . ?
C61 C66 H66 120.0 . . ?
C65 C66 C61 120.0 . . ?
C65 C66 H66 120.0 . . ?
C68 C67 P17 122.5(18) . . ?
C68 C67 C72 120.0 . . ?
C72 C67 P17 117.4(18) . . ?
C67 C68 H68 120.0 . . ?
C67 C68 C69 120.0 . . ?
C69 C68 H68 120.0 . . ?
C68 C69 H69 120.0 . . ?
C70 C69 C68 120.0 . . ?
C70 C69 H69 120.0 . . ?
C69 C70 H70 120.0 . . ?
C69 C70 C71 120.0 . . ?
C71 C70 H70 120.0 . . ?
C70 C71 H71 120.0 . . ?
C70 C71 C72 120.0 . . ?
C72 C71 H71 120.0 . . ?
C67 C72 H72 120.0 . . ?
C71 C72 C67 120.0 . . ?
C71 C72 H72 120.0 . . ?
C74 C73 P15 118.7(18) . . ?
C74 C73 C78 120.0 . . ?
C78 C73 P15 121.2(18) . . ?
C73 C74 H74 120.0 . . ?
C73 C74 C75 120.0 . . ?
C75 C74 H74 120.0 . . ?
C74 C75 H75 120.0 . . ?
C74 C75 C76 120.0 . . ?
C76 C75 H75 120.0 . . ?
C75 C76 H76 120.0 . . ?
C77 C76 C75 120.0 . . ?
C77 C76 H76 120.0 . . ?
C76 C77 H77 120.0 . . ?
C76 C77 C78 120.0 . . ?
C78 C77 H77 120.0 . . ?
C73 C78 H78 120.0 . . ?
C77 C78 C73 120.0 . . ?
C77 C78 H78 120.0 . . ?
C80 C79 C84 120.0 . . ?
C80 C79 P20 114.9(19) . . ?
C84 C79 P20 124.9(19) . . ?
C79 C80 H80 120.0 . . ?
C79 C80 C81 120.0 . . ?
C81 C80 H80 120.0 . . ?
C80 C81 H81 120.0 . . ?
C80 C81 C82 120.0 . . ?
C82 C81 H81 120.0 . . ?
C81 C82 H82 120.0 . . ?
C83 C82 C81 120.0 . . ?
C83 C82 H82 120.0 . . ?
C82 C83 H83 120.0 . . ?
C84 C83 C82 120.0 . . ?
C84 C83 H83 120.0 . . ?
C79 C84 H84 120.0 . . ?
C83 C84 C79 120.0 . . ?
C83 C84 H84 120.0 . . ?
C86 C85 C90 120.0 . . ?
C86 C85 P19 115(2) . . ?
C90 C85 P19 124(2) . . ?
C85 C86 H86 120.0 . . ?
C87 C86 C85 120.0 . . ?
C87 C86 H86 120.0 . . ?
C86 C87 H87 120.0 . . ?
C86 C87 C88 120.0 . . ?
C88 C87 H87 120.0 . . ?
C87 C88 H88 120.0 . . ?
C89 C88 C87 120.0 . . ?
C89 C88 H88 120.0 . . ?
C88 C89 H89 120.0 . . ?
C88 C89 C90 120.0 . . ?
C90 C89 H89 120.0 . . ?
C85 C90 H90 120.0 . . ?
C89 C90 C85 120.0 . . ?
C89 C90 H90 120.0 . . ?
C92 C91 C96 120.0 . . ?
C92 C91 P18 118(2) . . ?
C96 C91 P18 122(2) . . ?
C91 C92 H92 120.0 . . ?
C93 C92 C91 120.0 . . ?
C93 C92 H92 120.0 . . ?
C92 C93 H93 120.0 . . ?
C94 C93 C92 120.0 . . ?
C94 C93 H93 120.0 . . ?
C93 C94 H94 120.0 . . ?
C93 C94 C95 120.0 . . ?
C95 C94 H94 120.0 . . ?
C94 C95 H95 120.0 . . ?
C94 C95 C96 120.0 . . ?
C96 C95 H95 120.0 . . ?
C91 C96 H96 120.0 . . ?
C95 C96 C91 120.0 . . ?
C95 C96 H96 120.0 . . ?
C98 C97 C102 120.0 . . ?
C98 C97 P18 119(2) . . ?
C102 C97 P18 120(2) . . ?
C97 C98 H98 120.0 . . ?
C99 C98 C97 120.0 . . ?
C99 C98 H98 120.0 . . ?
C98 C99 H99 120.0 . . ?
C100 C99 C98 120.0 . . ?
C100 C99 H99 120.0 . . ?
C99 C100 H100 120.0 . . ?
C101 C100 C99 120.0 . . ?
C101 C100 H100 120.0 . . ?
C100 C101 H101 120.0 . . ?
C100 C101 C102 120.0 . . ?
C102 C101 H101 120.0 . . ?
C97 C102 H102 120.0 . . ?
C101 C102 C97 120.0 . . ?
C101 C102 H102 120.0 . . ?
C104 C103 P11 122.9(19) . . ?
C104 C103 C108 120.0 . . ?
C108 C103 P11 117.0(19) . . ?
C103 C104 H104 120.0 . . ?
C103 C104 C105 120.0 . . ?
C105 C104 H104 120.0 . . ?
C104 C105 H105 120.0 . . ?
C104 C105 C106 120.0 . . ?
C106 C105 H105 120.0 . . ?
C105 C106 H106 120.0 . . ?
C107 C106 C105 120.0 . . ?
C107 C106 H106 120.0 . . ?
C106 C107 H107 120.0 . . ?
C108 C107 C106 120.0 . . ?
C108 C107 H107 120.0 . . ?
C103 C108 H108 120.0 . . ?
C107 C108 C103 120.0 . . ?
C107 C108 H108 120.0 . . ?
C110 C109 C114 120.0 . . ?
C110 C109 P21 120.0(17) . . ?
C114 C109 P21 120.0(18) . . ?
C109 C110 H110 120.0 . . ?
C111 C110 C109 120.0 . . ?
C111 C110 H110 120.0 . . ?
C110 C111 H111 120.0 . . ?
C110 C111 C112 120.0 . . ?
C112 C111 H111 120.0 . . ?
C111 C112 H112 120.0 . . ?
C113 C112 C111 120.0 . . ?
C113 C112 H112 120.0 . . ?
C112 C113 H113 120.0 . . ?
C114 C113 C112 120.0 . . ?
C114 C113 H113 120.0 . . ?
C109 C114 H114 120.0 . . ?
C113 C114 C109 120.0 . . ?
C113 C114 H114 120.0 . . ?
C116 C115 P12 117(2) . . ?
C116 C115 C120 120.0 . . ?
C120 C115 P12 123(2) . . ?
C115 C116 H116 120.0 . . ?
C115 C116 C117 120.0 . . ?
C117 C116 H116 120.0 . . ?
C116 C117 H117 120.0 . . ?
C118 C117 C116 120.0 . . ?
C118 C117 H117 120.0 . . ?
C117 C118 H118 120.0 . . ?
C117 C118 C119 120.0 . . ?
C119 C118 H118 120.0 . . ?
C118 C119 H119 120.0 . . ?
C120 C119 C118 120.0 . . ?
C120 C119 H119 120.0 . . ?
C115 C120 H120 120.0 . . ?
C119 C120 C115 120.0 . . ?
C119 C120 H120 120.0 . . ?
C122 C121 P13 125(2) . . ?
C122 C121 C126 120.0 . . ?
C126 C121 P13 115(2) . . ?
C121 C122 H122 120.0 . . ?
C123 C122 C121 120.0 . . ?
C123 C122 H122 120.0 . . ?
C122 C123 H123 120.0 . . ?
C122 C123 C124 120.0 . . ?
C124 C123 H123 120.0 . . ?
C123 C124 H124 120.0 . . ?
C123 C124 C125 120.0 . . ?
C125 C124 H124 120.0 . . ?
C124 C125 H125 120.0 . . ?
C126 C125 C124 120.0 . . ?
C126 C125 H125 120.0 . . ?
C121 C126 H126 120.0 . . ?
C125 C126 C121 120.0 . . ?
C125 C126 H126 120.0 . . ?
C128 C127 P13 121(2) . . ?
C128 C127 C132 120.0 . . ?
C132 C127 P13 118(2) . . ?
C127 C128 H128 120.0 . . ?
C129 C128 C127 120.0 . . ?
C129 C128 H128 120.0 . . ?
C128 C129 H129 120.0 . . ?
C130 C129 C128 120.0 . . ?
C130 C129 H129 120.0 . . ?
C129 C130 H130 120.0 . . ?
C129 C130 C131 120.0 . . ?
C131 C130 H130 120.0 . . ?
C130 C131 H131 120.0 . . ?
C132 C131 C130 120.0 . . ?
C132 C131 H131 120.0 . . ?
C127 C132 H132 120.0 . . ?
C131 C132 C127 120.0 . . ?
C131 C132 H132 120.0 . . ?
C134 C133 P15 118.0(17) . . ?
C134 C133 C138 120.0 . . ?
C138 C133 P15 121.8(17) . . ?
C133 C134 H134 120.0 . . ?
C135 C134 C133 120.0 . . ?
C135 C134 H134 120.0 . . ?
C134 C135 H135 120.0 . . ?
C134 C135 C136 120.0 . . ?
C136 C135 H135 120.0 . . ?
C135 C136 H136 120.0 . . ?
C137 C136 C135 120.0 . . ?
C137 C136 H136 120.0 . . ?
C136 C137 H137 120.0 . . ?
C136 C137 C138 120.0 . . ?
C138 C137 H137 120.0 . . ?
C133 C138 H138 120.0 . . ?
C137 C138 C133 120.0 . . ?
C137 C138 H138 120.0 . . ?
C140 C139 H139 120.0 . . ?
C140 C139 C144 120.0 . . ?
C144 C139 H139 120.0 . . ?
C139 C140 H140 120.0 . . ?
C139 C140 C141 120.0 . . ?
C141 C140 H140 120.0 . . ?
C140 C141 H141 120.0 . . ?
C140 C141 C142 120.0 . . ?
C142 C141 H141 120.0 . . ?
C141 C142 H142 120.0 . . ?
C143 C142 C141 120.0 . . ?
C143 C142 H142 120.0 . . ?
C142 C143 H143 120.0 . . ?
C142 C143 C144 120.0 . . ?
C144 C143 H143 120.0 . . ?
C139 C144 P21 114(2) . . ?
C143 C144 C139 120.0 . . ?
C143 C144 P21 126(2) . . ?
C301 C300 H300 106.6 . . ?
C301 C300 S5 102(3) . . ?
C302 C300 H300 106.6 . . ?
C302 C300 C301 130(5) . . ?
C302 C300 S5 103(3) . . ?
S5 C300 H300 106.6 . . ?
C300 C301 H30E 109.5 . . ?
C300 C301 H30F 109.5 . . ?
C300 C301 H30G 109.5 . . ?
H30E C301 H30F 109.5 . . ?
H30E C301 H30G 109.5 . . ?
H30F C301 H30G 109.5 . . ?
C300 C302 H30H 109.5 . . ?
C300 C302 H30I 109.5 . . ?
C300 C302 H30J 109.5 . . ?
H30H C302 H30I 109.5 . . ?
H30H C302 H30J 109.5 . . ?
H30I C302 H30J 109.5 . . ?
H30K C303 H30L 109.5 . . ?
H30K C303 H30M 109.5 . . ?
H30L C303 H30M 109.5 . . ?
C304 C303 H30K 109.5 . . ?
C304 C303 H30L 109.5 . . ?
C304 C303 H30M 109.5 . . ?
S1 C304 H304 108.7 . . ?
C303 C304 S1 117(4) . . ?
C303 C304 H304 108.7 . . ?
C303 C304 C305 101(4) . . ?
C305 C304 S1 112(4) . . ?
C305 C304 H304 108.7 . . ?
C304 C305 H30N 109.5 . . ?
C304 C305 H30O 109.5 . . ?
C304 C305 H30P 109.5 . . ?
H30N C305 H30O 109.5 . . ?
H30N C305 H30P 109.5 . . ?
H30O C305 H30P 109.5 . . ?
H31A C313 H31B 109.5 . . ?
H31A C313 H31C 109.5 . . ?
H31B C313 H31C 109.5 . . ?
C314 C313 H31A 109.5 . . ?
C314 C313 H31B 109.5 . . ?
C314 C313 H31C 109.5 . . ?
C313 C314 H314 103.1 . . ?
C313 C314 S3 117(3) . . ?
C315 C314 C313 114(4) . . ?
C315 C314 H314 103.1 . . ?
C315 C314 S3 114(3) . . ?
S3 C314 H314 103.1 . . ?
C314 C315 H31D 109.5 . . ?
C314 C315 H31E 109.5 . . ?
C314 C315 H31F 109.5 . . ?
H31D C315 H31E 109.5 . . ?
H31D C315 H31F 109.5 . . ?
H31E C315 H31F 109.5 . . ?
H31G C316 H31H 108.2 . . ?
C317 C316 H31G 109.8 . . ?
C317 C316 H31H 109.8 . . ?
C317 C316 P18 109(3) . . ?
P18 C316 H31G 109.8 . . ?
P18 C316 H31H 109.8 . . ?
C316 C317 H31I 108.0 . . ?
C316 C317 H31J 108.0 . . ?
H31I C317 H31J 107.3 . . ?
C318 C317 C316 117(4) . . ?
C318 C317 H31I 108.0 . . ?
C318 C317 H31J 108.0 . . ?
C317 C318 H31K 108.1 . . ?
C317 C318 H31L 108.1 . . ?
C317 C318 P21 117(4) . . ?
H31K C318 H31L 107.3 . . ?
P21 C318 H31K 108.1 . . ?
P21 C318 H31L 108.1 . . ?
H31M C319 H31N 109.5 . . ?
H31M C319 H31O 109.5 . . ?
H31N C319 H31O 109.5 . . ?
C320 C319 H31M 109.5 . . ?
C320 C319 H31N 109.5 . . ?
C320 C319 H31O 109.5 . . ?
C319 C320 H320 113.1 . . ?
C319 C320 S11 110(4) . . ?
C321 C320 C319 92.1(13) . . ?
C321 C320 H320 113.1 . . ?
C321 C320 S11 113(4) . . ?
S11 C320 H320 113.1 . . ?
C320 C321 H32A 109.5 . . ?
C320 C321 H32B 109.5 . . ?
C320 C321 H32C 109.5 . . ?
H32A C321 H32B 109.5 . . ?
H32A C321 H32C 109.5 . . ?
H32B C321 H32C 109.5 . . ?
H32D C322 H32E 109.5 . . ?
H32D C322 H32F 109.5 . . ?
H32E C322 H32F 109.5 . . ?
C323 C322 H32D 109.5 . . ?
C323 C322 H32E 109.5 . . ?
C323 C322 H32F 109.5 . . ?
C322 C323 H323 91.0 . . ?
C322 C323 S8 86(3) . . ?
C324 C323 C322 171(5) . . ?
C324 C323 H323 91.0 . . ?
C324 C323 S8 103(3) . . ?
S8 C323 H323 91.0 . . ?
C323 C324 H32G 109.5 . . ?
C323 C324 H32H 109.5 . . ?
C323 C324 H32I 109.5 . . ?
H32G C324 H32H 109.5 . . ?
H32G C324 H32I 109.5 . . ?
H32H C324 H32I 109.5 . . ?
H30Q C309 H30R 109.5 . . ?
H30Q C309 H30S 109.5 . . ?
H30R C309 H30S 109.5 . . ?
C310 C309 H30Q 109.5 . . ?
C310 C309 H30R 109.5 . . ?
C310 C309 H30S 109.5 . . ?
C309 C310 H310 112.4 . . ?
C309 C310 C311 96.7(15) . . ?
C309 C310 S2 109(3) . . ?
C311 C310 H310 112.4 . . ?
C311 C310 S2 113(2) . . ?
S2 C310 H310 112.4 . . ?
C310 C311 H31P 109.5 . . ?
C310 C311 H31Q 109.5 . . ?
C310 C311 H31R 109.5 . . ?
H31P C311 H31Q 109.5 . . ?
H31P C311 H31R 109.5 . . ?
H31Q C311 H31R 109.5 . . ?
Ag11 S2 Ag7 132.3(3) . . ?
Ag20 S2 Ag7 95.2(3) . . ?
Ag20 S2 Ag11 100.0(3) . . ?
C310 S2 Ag7 112.7(12) . . ?
C310 S2 Ag11 104.3(13) . . ?
C310 S2 Ag20 109.3(12) . . ?
H32J C325 H32K 109.5 . . ?
H32J C325 H32L 109.5 . . ?
H32K C325 H32L 109.5 . . ?
C326 C325 H32J 109.5 . . ?
C326 C325 H32K 109.5 . . ?
C326 C325 H32L 109.5 . . ?
C325 C326 H326 114.9 . . ?
C325 C326 C327 96(2) . . ?
C325 C326 S4 108(3) . . ?
C327 C326 H326 114.9 . . ?
C327 C326 S4 106(2) . . ?
S4 C326 H326 114.9 . . ?
C326 C327 H32M 109.5 . . ?
C326 C327 H32N 109.5 . . ?
C326 C327 H32O 109.5 . . ?
H32M C327 H32N 109.5 . . ?
H32M C327 H32O 109.5 . . ?
H32N C327 H32O 109.5 . . ?
Ag15 S4 Ag14 98.4(4) . . ?
Ag20 S4 Ag14 106.9(4) . . ?
Ag20 S4 Ag15 112.4(4) . . ?
C326 S4 Ag14 112.2(13) . . ?
C326 S4 Ag15 110.7(13) . . ?
C326 S4 Ag20 115.0(13) . . ?
P11 C328 H32P 107.1 . . ?
P11 C328 H32Q 107.1 . . ?
H32P C328 H32Q 106.8 . . ?
C329 C328 P11 121(4) . . ?
C329 C328 H32P 107.1 . . ?
C329 C328 H32Q 107.1 . . ?
C30A C329 H32R 110.6 . . ?
C30A C329 H32S 110.6 . . ?
C30B C329 C328 130(5) . . ?
C328 C329 C30A 106(7) . . ?
C328 C329 H32R 110.6 . . ?
C328 C329 H32S 110.6 . . ?
H32R C329 H32S 108.7 . . ?
Ag2A Ag1 Ag3A 54.60(15) . . ?
Ag2A Ag1 Cu6A 105.2(3) . . ?
Ag4 Ag1 Ag2A 58.14(16) . . ?
Ag4 Ag1 Ag3A 56.84(14) . . ?
Ag4 Ag1 Cu6A 59.3(2) . . ?
Cu6A Ag1 Ag3A 59.0(2) . . ?
S10 Ag1 Ag2A 141.8(4) . . ?
S10 Ag1 Ag3A 89.3(4) . . ?
S10 Ag1 Ag4 115.4(4) . . ?
S10 Ag1 Cu6A 56.1(4) . . ?
Ag3A Cu6A Ag1 60.7(2) . . ?
Ag4 Cu6A Ag3A 56.42(17) . . ?
Ag4 Cu6A Ag1 55.8(2) . . ?
Ag4 Cu6A Ag3 58.0(2) . . ?
S7 Cu6A Ag3A 83.5(4) . . ?
S7 Cu6A Ag4 108.8(5) . . ?
S7 Cu6A Ag1 144.0(5) . . ?
S7 Cu6A S10 133.6(5) . . ?
S7 Cu6A Ag3 51.2(4) . . ?
S10 Cu6A Ag3A 83.7(3) . . ?
S10 Cu6A Ag4 100.4(4) . . ?
S10 Cu6A Ag1 44.7(3) . . ?
S10 Cu6A Ag3 145.0(4) . . ?
Ag3 Cu6A Ag3A 61.6(2) . . ?
Ag3 Cu6A Ag1 108.0(3) . . ?
Ag4 Ag2 Ag1A 51.17(13) . . ?
S8 Ag2 Ag1A 112.2(5) . . ?
S8 Ag2 Ag4 147.3(6) . . ?
S10 Cu6B S7 160.7(6) . . ?
C91 P18 Ag15 113.3(9) . . ?
C91 P18 C97 100.3(14) . . ?
C91 P18 C316 110.6(19) . . ?
C97 P18 Ag15 112.2(14) . . ?
C97 P18 C316 106.2(19) . . ?
C316 P18 Ag15 113.2(17) . . ?
C10 P19 Ag10 117.7(15) . . ?
C49 P19 Ag10 112.7(12) . . ?
C49 P19 C10 102.8(19) . . ?
C49 P19 C85 103.9(16) . . ?
C85 P19 Ag10 110.9(12) . . ?
C85 P19 C10 107.6(19) . . ?
C12 P20 Ag5A 112.4(15) . . ?
C12 P20 Ag5B 107.6(15) . . ?
C55 P20 Ag5A 107.6(11) . . ?
C55 P20 Ag5B 124.3(11) . . ?
C55 P20 C12 107(2) . . ?
C55 P20 C79 103.7(15) . . ?
C79 P20 Ag5A 119.3(12) . . ?
C79 P20 Ag5B 107.0(12) . . ?
C79 P20 C12 105.7(18) . . ?
C109 P21 Ag8A 116.0(11) . . ?
C109 P21 Ag8B 100.7(11) . . ?
C109 P21 C318 107.8(18) . . ?
C144 P21 Ag8A 107.4(12) . . ?
C144 P21 Ag8B 126.0(14) . . ?
C144 P21 C109 104.9(12) . . ?
C144 P21 C318 111(2) . . ?
C318 P21 Ag8A 109.3(18) . . ?
C318 P21 Ag8B 104.5(17) . . ?
Ag12 S3 Ag13 111.2(3) . . ?
Ag12 S3 Ag19 109.9(3) . . ?
Ag19 S3 Ag13 98.4(3) . . ?
C314 S3 Ag12 110.1(14) . . ?
C314 S3 Ag13 116.7(15) . . ?
C314 S3 Ag19 109.8(18) . . ?
Ag5A S5 Ag6 126.6(5) . . ?
Ag6 S5 Ag5B 114.6(5) . . ?
Ag18 S5 Ag5A 97.6(5) . . ?
Ag18 S5 Ag5B 109.9(5) . . ?
Ag18 S5 Ag6 93.0(4) . . ?
C300 S5 Ag5A 111.1(15) . . ?
C300 S5 Ag5B 114.5(14) . . ?
C300 S5 Ag6 115.4(17) . . ?
C300 S5 Ag18 107.0(17) . . ?
Ag38 S6 Ag6 104.7(5) . . ?
Ag38 S6 Ag3 97.7(5) . . ?
C148 S6 Ag6 112.7(17) . . ?
C148 S6 Ag38 113.5(18) . . ?
C148 S6 Ag3 118.4(16) . . ?
Ag3 S6 Ag6 108.1(5) . . ?
Cu6A S7 Ag7 123.9(5) . . ?
Cu6A S7 Ag3 81.3(5) . . ?
Cu6B S7 Ag7 103.5(4) . . ?
C164 S7 Ag7 120.1(18) . . ?
C164 S7 Cu6A 93(2) . . ?
C164 S7 Cu6B 106(2) . . ?
C164 S7 Ag3 119.0(15) . . ?
Ag3 S7 Ag7 112.3(5) . . ?
Ag3 S7 Cu6B 89.5(5) . . ?
Ag5B S8 Ag38 66.5(4) . . ?
Ag5B S8 Ag41 125.2(5) . . ?
Ag5B S8 C323 123.1(17) . . ?
Ag38 S8 Ag41 84.3(4) . . ?
C323 S8 Ag5A 124.8(17) . . ?
C323 S8 Ag38 94.7(12) . . ?
C323 S8 Ag41 103.8(18) . . ?
Ag2 S8 Ag5A 119.3(6) . . ?
Ag2 S8 C323 102.2(18) . . ?
Ag39 S10 Ag11 130.5(5) . . ?
Ag1 S10 Ag11 115.9(5) . . ?
Ag1 S10 Cu6A 79.3(4) . . ?
Cu6A S10 Ag11 104.3(5) . . ?
Cu6B S10 Ag11 88.0(5) . . ?
Cu6B S10 Ag39 90.5(5) . . ?
C154 S10 Ag11 125.6(18) . . ?
C154 S10 Ag39 100.6(18) . . ?
C154 S10 Ag1 116.5(19) . . ?
C154 S10 Cu6A 98.4(17) . . ?
C154 S10 Cu6B 111.7(18) . . ?
Ag10 S11 Ag9A 133.0(5) . . ?
Ag10 S11 Ag9B 116.7(5) . . ?
Ag12 S11 Ag9A 91.8(4) . . ?
Ag12 S11 Ag9B 108.4(4) . . ?
Ag12 S11 Ag10 90.9(4) . . ?
C320 S11 Ag9A 111.0(14) . . ?
C320 S11 Ag9B 115.1(14) . . ?
C320 S11 Ag10 111.2(14) . . ?
C320 S11 Ag12 112.0(15) . . ?
Ag39 S9B Ag9B 63.7(3) . . ?
Ag41 S9B Ag9B 139.7(4) . . ?
Ag41 S9B Ag39 113.1(5) . . ?
C152 S9B Ag9B 106.3(14) . . ?
C152 S9B Ag39 92.6(12) . . ?
C152 S9B Ag41 114.1(14) . . ?
C157 C146 H146 120.0 . . ?
C157 C146 C147 120.0 . . ?
C147 C146 H146 120.0 . . ?
C146 C157 P1B 129(2) . . ?
C145 C157 P1B 111(2) . . ?
C145 C157 C146 120.0 . . ?
C157 C145 H145 120.0 . . ?
C171 C145 C157 120.0 . . ?
C171 C145 H145 120.0 . . ?
C145 C171 H171 120.0 . . ?
C145 C171 C201 120.0 . . ?
C201 C171 H171 120.0 . . ?
C171 C201 H201 120.0 . . ?
C171 C201 C147 120.0 . . ?
C147 C201 H201 120.0 . . ?
C146 C147 H147 120.0 . . ?
C201 C147 C146 120.0 . . ?
C201 C147 H147 120.0 . . ?
S10 C154 H154 110.8 . . ?
C156 C154 S10 110(4) . . ?
C156 C154 H154 110.8 . . ?
C156 C154 C155 104(5) . . ?
C155 C154 S10 110(3) . . ?
C155 C154 H154 110.8 . . ?
C154 C156 H15A 109.5 . . ?
C154 C156 H15B 109.5 . . ?
C154 C156 H15C 109.5 . . ?
H15A C156 H15B 109.5 . . ?
H15A C156 H15C 109.5 . . ?
H15B C156 H15C 109.5 . . ?
H15D C151 H15E 109.5 . . ?
H15D C151 H15F 109.5 . . ?
H15E C151 H15F 109.5 . . ?
C152 C151 H15D 109.5 . . ?
C152 C151 H15E 109.5 . . ?
C152 C151 H15F 109.5 . . ?
S6 C148 H148 115.0 . . ?
C149 C148 S6 109(4) . . ?
C149 C148 H148 115.0 . . ?
C150 C148 S6 106(4) . . ?
C150 C148 H148 115.0 . . ?
C150 C148 C149 95(4) . . ?
C148 C149 H14A 109.5 . . ?
C148 C149 H14B 109.5 . . ?
C148 C149 H14C 109.5 . . ?
H14A C149 H14B 109.5 . . ?
H14A C149 H14C 109.5 . . ?
H14B C149 H14C 109.5 . . ?
C154 C155 H15G 109.5 . . ?
C154 C155 H15H 109.5 . . ?
C154 C155 H15I 109.5 . . ?
H15G C155 H15H 109.5 . . ?
H15G C155 H15I 109.5 . . ?
H15H C155 H15I 109.5 . . ?
S9B C152 H152 94.8 . . ?
C151 C152 S9B 114(4) . . ?
C151 C152 H152 94.8 . . ?
C151 C152 C153 159(5) . . ?
C153 C152 S9B 84(3) . . ?
C153 C152 H152 94.8 . . ?
C148 C150 H15J 109.5 . . ?
C148 C150 H15K 109.5 . . ?
C148 C150 H15L 109.5 . . ?
H15J C150 H15K 109.5 . . ?
H15J C150 H15L 109.5 . . ?
H15K C150 H15L 109.5 . . ?
C152 C153 H15M 109.5 . . ?
C152 C153 H15N 109.5 . . ?
C152 C153 H15O 109.5 . . ?
H15M C153 H15N 109.5 . . ?
H15M C153 H15O 109.5 . . ?
H15N C153 H15O 109.5 . . ?
F56 Sb1 F145 87.6(10) . . ?
F97 Sb1 F56 89.7(10) . . ?
F97 Sb1 F145 87.4(10) . . ?
F97 Sb1 F213 174.9(11) . . ?
F110 Sb1 F56 93.6(10) . . ?
F110 Sb1 F97 91.3(10) . . ?
F110 Sb1 F124 89.4(10) . . ?
F110 Sb1 F145 178.2(12) . . ?
F110 Sb1 F213 93.3(10) . . ?
F124 Sb1 F56 176.5(11) . . ?
F124 Sb1 F97 92.1(10) . . ?
F124 Sb1 F145 89.4(10) . . ?
F124 Sb1 F213 90.1(10) . . ?
F213 Sb1 F56 87.8(10) . . ?
F213 Sb1 F145 88.0(10) . . ?
F86 Sb2 F131 85.0(9) . . ?
F86 Sb2 F161 174.7(12) . . ?
F86 Sb2 F174 90.8(11) . . ?
F86 Sb2 F134 88.3(11) . . ?
F161 Sb2 F131 89.7(11) . . ?
F161 Sb2 F174 89.6(11) . . ?
F174 Sb2 F131 87.8(11) . . ?
F185 Sb2 F86 93.6(11) . . ?
F185 Sb2 F131 178.5(13) . . ?
F185 Sb2 F161 91.7(11) . . ?
F185 Sb2 F174 91.6(11) . . ?
F185 Sb2 F134 92.3(11) . . ?
F134 Sb2 F131 88.3(11) . . ?
F134 Sb2 F161 90.9(11) . . ?
F134 Sb2 F174 176.0(13) . . ?
C160 C161 P1B 122(2) . . ?
C160 C161 C162 120.0 . . ?
C162 C161 P1B 117(2) . . ?
C161 C160 H160 120.0 . . ?
C161 C160 C159 120.0 . . ?
C159 C160 H160 120.0 . . ?
C160 C159 H159 120.0 . . ?
C158 C159 C160 120.0 . . ?
C158 C159 H159 120.0 . . ?
C159 C158 H158 120.0 . . ?
C163 C158 C159 120.0 . . ?
C163 C158 H158 120.0 . . ?
C158 C163 H163 120.0 . . ?
C158 C163 C162 120.0 . . ?
C162 C163 H163 120.0 . . ?
C161 C162 H162 120.0 . . ?
C163 C162 C161 120.0 . . ?
C163 C162 H162 120.0 . . ?
H16A C165 H16B 109.5 . . ?
H16A C165 H16C 109.5 . . ?
H16B C165 H16C 109.5 . . ?
C164 C165 H16A 109.5 . . ?
C164 C165 H16B 109.5 . . ?
C164 C165 H16C 109.5 . . ?
S7 C164 H164 102.9 . . ?
C165 C164 S7 96(3) . . ?
C165 C164 H164 102.9 . . ?
C165 C164 C166 142(5) . . ?
C166 C164 S7 105(3) . . ?
C166 C164 H164 102.9 . . ?
C164 C166 H16D 109.5 . . ?
C164 C166 H16E 109.5 . . ?
C164 C166 H16F 109.5 . . ?
H16D C166 H16E 109.5 . . ?
H16D C166 H16F 109.5 . . ?
H16E C166 H16F 109.5 . . ?
Ag1A Ag3 Ag3A 53.13(12) . . ?
Ag3B Ag3 Ag4 65.2(2) . . ?
Ag3B Ag3 S6 106.4(4) . . ?
Ag3B Ag3 S7 104.4(4) . . ?
Ag4 Ag3 Ag1A 55.23(12) . . ?
Ag4 Ag3 Ag3A 56.36(11) . . ?
Ag4 Ag3 Cu6A 59.79(19) . . ?
Cu6A Ag3 Ag1A 103.7(2) . . ?
Cu6A Ag3 Ag3A 59.96(19) . . ?
S6 Ag3 Ag1A 79.8(3) . . ?
S6 Ag3 Ag3A 132.9(4) . . ?
S6 Ag3 Ag4 98.0(4) . . ?
S6 Ag3 Cu6A 144.9(5) . . ?
S7 Ag3 Ag1A 133.1(4) . . ?
S7 Ag3 Ag3A 80.5(3) . . ?
S7 Ag3 Ag4 107.0(4) . . ?
S7 Ag3 Cu6A 47.6(4) . . ?
S7 Ag3 S6 146.4(5) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Ag1A Ag2 S8 Ag5A -8.3(8) . . . . ?
Ag1A Ag2 S8 C323 134.0(13) . . . . ?
Ag4 Ag2 S8 Ag5A -60.1(13) . . . . ?
Ag4 Ag2 S8 C323 82.2(16) . . . . ?
O1 W1 O9 W5 -129.9(17) . . . . ?
O2 W3 O4 W1 171.4(8) . . . . ?
O2 W3 O11 W9 -129.6(14) . . . . ?
O3 W2 O8 W6 125.8(14) . . . . ?
O4 W1 O9 W5 32(3) . . . . ?
O4 W3 O11 W9 131.9(14) . . . . ?
O5 W2 O8 W6 -56(3) . . . . ?
O5 W3 O4 W1 71.0(8) . . . . ?
O5 W3 O11 W9 40(3) . . . . ?
O6 W1 O9 W5 127.1(17) . . . . ?
O6 W2 O8 W6 -135.5(15) . . . . ?
O7 W1 O9 W5 54.1(17) . . . . ?
O7 W2 O8 W6 -61.3(14) . . . . ?
O7 W3 O4 W1 -1.2(7) . . . . ?
O7 W3 O11 W9 56.5(14) . . . . ?
O7 Si1 O26 W4 -73.1(14) . . . . ?
O7 Si1 O26 W5 70.5(13) . . . . ?
O7 Si1 O26 Ag1A 175.2(8) . . . . ?
O7 Si1 O27 W8 -69.8(13) . . . . ?
O7 Si1 O27 W9 73.8(12) . . . . ?
O7 Si1 O27 Ag2A -176.3(7) . . . . ?
O7 Si1 O28 W6 -72.7(12) . . . . ?
O7 Si1 O28 W7 72.7(13) . . . . ?
O8 W6 O25 W5 -100(2) . . . . ?
O8 W6 O34 Ag3A 1(3) . . . . ?
O8 W6 O34 Ag3B 43(3) . . . . ?
O8 W6 O34 Ag7 -151(2) . . . . ?
O9 W5 O14 Ag8A -31.1(12) . . . . ?
O9 W5 O14 Ag8B -20.7(9) . . . . ?
O9 W5 O25 W6 100(2) . . . . ?
O9 W5 O29 Ag1A 4(3) . . . . ?
O9 W5 O29 Ag3B -38(3) . . . . ?
O9 W5 O29 Ag6 149(2) . . . . ?
O10 W1 O9 W5 -29.9(17) . . . . ?
O10 W4 O17 W9 -98(3) . . . . ?
O10 W4 O30 Ag1A -21(4) . . . . ?
O10 W4 O30 Ag1B 14(4) . . . . ?
O10 W4 O30 Ag5A -160(2) . . . . ?
O10 W4 O30 Ag5B -166.9(18) . . . . ?
O11 W3 O4 W1 -87.7(8) . . . . ?
O11 W9 O17 W4 97(3) . . . . ?
O11 W9 O18 Ag19 -26.4(7) . . . . ?
O11 W9 O31 Ag2A 4(3) . . . . ?
O11 W9 O31 Ag10 151(2) . . . . ?
O12 W3 O4 W1 -7(2) . . . . ?
O12 W3 O11 W9 -28.6(14) . . . . ?
O12 W8 O19 W9 87.2(14) . . . . ?
O12 W8 O20 Ag13 27.4(9) . . . . ?
O12 W8 O21 W7 -107(3) . . . . ?
O12 W8 O32 Ag2A -10(4) . . . . ?
O12 W8 O32 Ag9A -162(2) . . . . ?
O12 W8 O32 Ag9B -145(2) . . . . ?
O13 W2 O8 W6 24.5(15) . . . . ?
O13 W7 O21 W8 108(3) . . . . ?
O13 W7 O22 Ag14 -28.4(8) . . . . ?
O13 W7 O33 Ag3A 26(4) . . . . ?
O13 W7 O33 Ag2B -15(4) . . . . ?
O13 W7 O33 Ag11 166(3) . . . . ?
O14 W5 O25 W6 -168(2) . . . . ?
O14 W5 O29 Ag1A -167.0(9) . . . . ?
O14 W5 O29 Ag3B 151.4(10) . . . . ?
O14 W5 O29 Ag6 -22.1(13) . . . . ?
O15 W4 O17 W9 -56(4) . . . . ?
O15 W4 O30 Ag1A 67.5(10) . . . . ?
O15 W4 O30 Ag1B 102.0(11) . . . . ?
O15 W4 O30 Ag5A -72.2(13) . . . . ?
O15 W4 O30 Ag5B -78.7(19) . . . . ?
O15 W5 O14 Ag8A 48.6(12) . . . . ?
O15 W5 O14 Ag8B 59.0(9) . . . . ?
O15 W5 O25 W6 53(4) . . . . ?
O15 W5 O29 Ag1A -70.6(10) . . . . ?
O15 W5 O29 Ag3B -112.1(11) . . . . ?
O15 W5 O29 Ag6 74.3(12) . . . . ?
O16 W4 O17 W9 172(3) . . . . ?
O16 W4 O30 Ag1A 163.5(9) . . . . ?
O16 W4 O30 Ag1B -162.0(10) . . . . ?
O16 W4 O30 Ag5A 23.8(14) . . . . ?
O16 W4 O30 Ag5B 17(2) . . . . ?
O17 W4 O30 Ag1A -92.2(10) . . . . ?
O17 W4 O30 Ag1B -57.7(11) . . . . ?
O17 W4 O30 Ag5A 128.1(12) . . . . ?
O17 W4 O30 Ag5B 121.6(18) . . . . ?
O17 W9 O18 Ag19 -110.1(8) . . . . ?
O17 W9 O31 Ag2A 89.4(10) . . . . ?
O17 W9 O31 Ag10 -123.4(11) . . . . ?
O18 W9 O17 W4 -171(3) . . . . ?
O18 W9 O31 Ag2A -164.4(8) . . . . ?
O18 W9 O31 Ag10 -17.1(12) . . . . ?
O19 W8 O20 Ag13 -52.9(11) . . . . ?
O19 W8 O21 W7 -63(4) . . . . ?
O19 W8 O32 Ag2A 71.4(10) . . . . ?
O19 W8 O32 Ag9A -80.2(12) . . . . ?
O19 W8 O32 Ag9B -63.4(16) . . . . ?
O19 W9 O17 W4 51(4) . . . . ?
O19 W9 O18 Ag19 53.5(9) . . . . ?
O19 W9 O31 Ag2A -68.7(10) . . . . ?
O19 W9 O31 Ag10 78.6(11) . . . . ?
O20 W8 O19 W9 176.8(15) . . . . ?
O20 W8 O21 W7 165(3) . . . . ?
O20 W8 O32 Ag2A 169.5(9) . . . . ?
O20 W8 O32 Ag9A 17.8(13) . . . . ?
O20 W8 O32 Ag9B 34.7(17) . . . . ?
O21 W7 O22 Ag14 -107.0(9) . . . . ?
O21 W7 O33 Ag3A 94.5(11) . . . . ?
O21 W7 O33 Ag2B 53.6(12) . . . . ?
O21 W7 O33 Ag11 -125.2(13) . . . . ?
O21 W8 O19 W9 43(3) . . . . ?
O21 W8 O20 Ag13 107.9(10) . . . . ?
O21 W8 O32 Ag2A -86.3(10) . . . . ?
O21 W8 O32 Ag9A 122.1(12) . . . . ?
O21 W8 O32 Ag9B 138.9(16) . . . . ?
O22 W7 O21 W8 -164(3) . . . . ?
O22 W7 O33 Ag3A -160.9(9) . . . . ?
O22 W7 O33 Ag2B 158.1(10) . . . . ?
O22 W7 O33 Ag11 -20.7(14) . . . . ?
O23 W6 O25 W5 -57(3) . . . . ?
O23 W6 O34 Ag3A 69.9(11) . . . . ?
O23 W6 O34 Ag3B 112.5(10) . . . . ?
O23 W6 O34 Ag7 -81.9(13) . . . . ?
O23 W7 O21 W8 67(4) . . . . ?
O23 W7 O22 Ag14 53.4(9) . . . . ?
O23 W7 O33 Ag3A -64.6(11) . . . . ?
O23 W7 O33 Ag2B -105.6(11) . . . . ?
O23 W7 O33 Ag11 75.6(13) . . . . ?
O24 W6 O25 W5 170(2) . . . . ?
O24 W6 O34 Ag3A 166.8(9) . . . . ?
O24 W6 O34 Ag3B -150.6(10) . . . . ?
O24 W6 O34 Ag7 14.9(14) . . . . ?
O25 W5 O14 Ag8A -115.8(11) . . . . ?
O25 W5 O14 Ag8B -105.4(9) . . . . ?
O25 W5 O29 Ag1A 88.1(11) . . . . ?
O25 W5 O29 Ag3B 46.5(11) . . . . ?
O25 W5 O29 Ag6 -127.0(12) . . . . ?
O25 W6 O34 Ag3A -88.4(11) . . . . ?
O25 W6 O34 Ag3B -45.8(11) . . . . ?
O25 W6 O34 Ag7 119.8(12) . . . . ?
O26 W4 O17 W9 -21(3) . . . . ?
O26 W4 O30 Ag1A -3.5(9) . . . . ?
O26 W4 O30 Ag1B 31.0(10) . . . . ?
O26 W4 O30 Ag5A -143.2(12) . . . . ?
O26 W4 O30 Ag5B -149.7(19) . . . . ?
O26 W5 O14 Ag8A 24(3) . . . . ?
O26 W5 O14 Ag8B 35(3) . . . . ?
O26 W5 O25 W6 23(2) . . . . ?
O26 W5 O29 Ag1A -1.5(9) . . . . ?
O26 W5 O29 Ag3B -43.1(9) . . . . ?
O26 W5 O29 Ag6 143.4(11) . . . . ?
O26 Si1 O7 W1 -1.6(13) . . . . ?
O26 Si1 O7 W2 -120.7(11) . . . . ?
O26 Si1 O7 W3 116.6(11) . . . . ?
O26 Si1 O27 W8 173.2(11) . . . . ?
O26 Si1 O27 W9 -43.2(14) . . . . ?
O26 Si1 O27 Ag2A 66.8(11) . . . . ?
O26 Si1 O28 W6 43.5(15) . . . . ?
O26 Si1 O28 W7 -171.1(11) . . . . ?
O27 W8 O19 W9 6.8(12) . . . . ?
O27 W8 O20 Ag13 -21(3) . . . . ?
O27 W8 O21 W7 -29(3) . . . . ?
O27 W8 O32 Ag2A 2.6(8) . . . . ?
O27 W8 O32 Ag9A -149.1(10) . . . . ?
O27 W8 O32 Ag9B -132.2(15) . . . . ?
O27 W9 O17 W4 20(3) . . . . ?
O27 W9 O18 Ag19 32(2) . . . . ?
O27 W9 O31 Ag2A -0.8(8) . . . . ?
O27 W9 O31 Ag10 146.4(10) . . . . ?
O27 Si1 O7 W1 -122.4(9) . . . . ?
O27 Si1 O7 W2 118.5(10) . . . . ?
O27 Si1 O7 W3 -4.2(12) . . . . ?
O27 Si1 O26 W4 43.8(16) . . . . ?
O27 Si1 O26 W5 -172.5(10) . . . . ?
O27 Si1 O26 Ag1A -67.9(12) . . . . ?
O27 Si1 O28 W6 172.1(10) . . . . ?
O27 Si1 O28 W7 -42.5(15) . . . . ?
O28 W6 O25 W5 -23(2) . . . . ?
O28 W6 O34 Ag3A 1.2(9) . . . . ?
O28 W6 O34 Ag3B 43.8(9) . . . . ?
O28 W6 O34 Ag7 -150.6(12) . . . . ?
O28 W7 O21 W8 30(3) . . . . ?
O28 W7 O22 Ag14 26(3) . . . . ?
O28 W7 O33 Ag3A 4.5(9) . . . . ?
O28 W7 O33 Ag2B -36.4(10) . . . . ?
O28 W7 O33 Ag11 144.8(12) . . . . ?
O28 Si1 O7 W1 119.1(10) . . . . ?
O28 Si1 O7 W2 0.0(12) . . . . ?
O28 Si1 O7 W3 -122.7(10) . . . . ?
O28 Si1 O26 W4 171.8(11) . . . . ?
O28 Si1 O26 W5 -44.5(15) . . . . ?
O28 Si1 O26 Ag1A 60.1(13) . . . . ?
O28 Si1 O27 W8 44.3(14) . . . . ?
O28 Si1 O27 W9 -172.2(10) . . . . ?
O28 Si1 O27 Ag2A -62.2(10) . . . . ?
O29 W5 O14 Ag8A 146.3(12) . . . . ?
O29 W5 O14 Ag8B 156.6(9) . . . . ?
O29 W5 O25 W6 -64(2) . . . . ?
O30 W4 O17 W9 68(3) . . . . ?
O31 W9 O17 W4 -67(3) . . . . ?
O31 W9 O18 Ag19 150.5(8) . . . . ?
O32 W8 O19 W9 -78.9(15) . . . . ?
O32 W8 O20 Ag13 -152.5(9) . . . . ?
O32 W8 O21 W7 60(3) . . . . ?
O33 W7 O21 W8 -60(3) . . . . ?
O33 W7 O22 Ag14 153.2(9) . . . . ?
O34 W6 O25 W5 64(2) . . . . ?
P1A C30A C329 C328 -163(6) . . . . ?
C30B P1B C157 C146 30(4) . . . . ?
C30B P1B C157 C145 -144(3) . . . . ?
C30B P1B C161 C160 -86(3) . . . . ?
C30B P1B C161 C162 102(3) . . . . ?
P1B C30B C329 C328 170(5) . . . . ?
P1B C157 C145 C171 175(3) . . . . ?
P1B C161 C160 C159 -172(3) . . . . ?
P1B C161 C162 C163 172(3) . . . . ?
P11 C25 C26 C27 -179(2) . . . . ?
P11 C25 C30 C29 179(2) . . . . ?
P11 C103 C104 C105 -177(2) . . . . ?
P11 C103 C108 C107 177(2) . . . . ?
P11 C328 C329 C30A 169(7) . . . . ?
P11 C328 C329 C30B 66(9) . . . . ?
P12 C1 C2 C3 -167(3) . . . . ?
P12 C31 C32 C33 178(2) . . . . ?
P12 C31 C36 C35 -177(2) . . . . ?
P12 C115 C116 C117 177(2) . . . . ?
P12 C115 C120 C119 -177(2) . . . . ?
P13 C121 C122 C123 -180.0(7) . . . . ?
P13 C121 C126 C125 180.0(7) . . . . ?
P13 C127 C128 C129 179.4(7) . . . . ?
P13 C127 C132 C131 -179.5(7) . . . . ?
P14 C4 C5 C6 171(3) . . . . ?
P14 C13 C14 C15 175(2) . . . . ?
P14 C13 C18 C17 -175(2) . . . . ?
P14 C19 C20 C21 179(2) . . . . ?
P14 C19 C24 C23 -179(2) . . . . ?
P15 C73 C74 C75 -178(2) . . . . ?
P15 C73 C78 C77 178(2) . . . . ?
P15 C133 C134 C135 -175(2) . . . . ?
P15 C133 C138 C137 175(2) . . . . ?
P16 C7 C8 C9 168(3) . . . . ?
P16 C37 C38 C39 178(2) . . . . ?
P16 C37 C42 C41 -178(2) . . . . ?
P16 C43 C44 C45 179(2) . . . . ?
P16 C43 C48 C47 -178(2) . . . . ?
P17 C61 C62 C63 177(2) . . . . ?
P17 C61 C66 C65 -177(2) . . . . ?
P17 C67 C68 C69 -177(2) . . . . ?
P17 C67 C72 C71 177(2) . . . . ?
Ag6 P13 C3 C2 68(3) . . . . ?
Ag6 P13 C121 C122 111.3(12) . . . . ?
Ag6 P13 C121 C126 -68.7(12) . . . . ?
Ag6 P13 C127 C128 178.7(11) . . . . ?
Ag6 P13 C127 C132 -1.8(12) . . . . ?
Ag6 S6 C148 C149 -55(4) . . . . ?
Ag6 S6 C148 C150 -156(3) . . . . ?
Ag7 P12 C1 C2 -57(3) . . . . ?
Ag7 P12 C31 C32 -60.6(18) . . . . ?
Ag7 P12 C31 C36 116.9(16) . . . . ?
Ag7 P12 C115 C116 -23.1(18) . . . . ?
Ag7 P12 C115 C120 154.2(13) . . . . ?
Ag7 S7 C164 C165 -107(3) . . . . ?
Ag7 S7 C164 C166 41(4) . . . . ?
Ag8A S1 C304 C303 -66(4) . . . . ?
Ag8A S1 C304 C305 50(4) . . . . ?
Ag8B S1 C304 C303 -48(5) . . . . ?
Ag8B S1 C304 C305 68(4) . . . . ?
Ag9B P1B C157 C146 162.8(18) . . . . ?
Ag9B P1B C157 C145 -11(2) . . . . ?
Ag9B P1B C161 C160 142.6(17) . . . . ?
Ag9B P1B C161 C162 -30(2) . . . . ?
Ag11 P11 C25 C26 -171.9(12) . . . . ?
Ag11 P11 C25 C30 9.0(17) . . . . ?
Ag11 P11 C103 C104 -153.4(13) . . . . ?
Ag11 P11 C103 C108 29.3(18) . . . . ?
Ag11 P11 C328 C329 52(5) . . . . ?
Ag11 S10 C154 C156 -159(3) . . . . ?
Ag11 S10 C154 C155 87(4) . . . . ?
Ag13 P15 C6 C5 -67(3) . . . . ?
Ag13 P15 C73 C74 -32.1(19) . . . . ?
Ag13 P15 C73 C78 149.9(13) . . . . ?
Ag13 P15 C133 C134 -23.6(18) . . . . ?
Ag13 P15 C133 C138 161.1(13) . . . . ?
Ag14 P14 C4 C5 76(4) . . . . ?
Ag14 P14 C13 C14 178.0(12) . . . . ?
Ag14 P14 C13 C18 -6.6(18) . . . . ?
Ag14 P14 C19 C20 -114.7(15) . . . . ?
Ag14 P14 C19 C24 64.7(15) . . . . ?
Ag18 S1 C304 C303 -180(4) . . . . ?
Ag18 S1 C304 C305 -64(4) . . . . ?
Ag19 P16 C7 C8 68(4) . . . . ?
Ag19 P16 C37 C38 149.7(13) . . . . ?
Ag19 P16 C37 C42 -32.5(16) . . . . ?
Ag19 P16 C43 C44 -12.6(18) . . . . ?
Ag19 P16 C43 C48 165.9(14) . . . . ?
Ag35 P17 C9 C8 -73(4) . . . . ?
Ag35 P17 C61 C62 -54.1(16) . . . . ?
Ag35 P17 C61 C66 123.0(16) . . . . ?
Ag35 P17 C67 C68 179.1(14) . . . . ?
Ag35 P17 C67 C72 2.4(19) . . . . ?
Ag35 S1 C304 C303 58(4) . . . . ?
Ag35 S1 C304 C305 174(3) . . . . ?
Ag38 S6 C148 C149 63(4) . . . . ?
Ag38 S6 C148 C150 -37(4) . . . . ?
Ag39 S10 C154 C156 40(4) . . . . ?
Ag39 S10 C154 C155 -75(4) . . . . ?
C1 P12 C31 C32 63(2) . . . . ?
C1 P12 C31 C36 -120(2) . . . . ?
C1 P12 C115 C116 -147(2) . . . . ?
C1 P12 C115 C120 30(2) . . . . ?
C1 C2 C3 P13 165(3) . . . . ?
C3 P13 C121 C122 -18(2) . . . . ?
C3 P13 C121 C126 162.0(19) . . . . ?
C3 P13 C127 C128 -51(2) . . . . ?
C3 P13 C127 C132 128(2) . . . . ?
C4 P14 C13 C14 -53(2) . . . . ?
C4 P14 C13 C18 121.9(19) . . . . ?
C4 P14 C19 C20 122(2) . . . . ?
C4 P14 C19 C24 -59(2) . . . . ?
C4 C5 C6 P15 -171(3) . . . . ?
C6 P15 C73 C74 -165.8(19) . . . . ?
C6 P15 C73 C78 16(2) . . . . ?
C6 P15 C133 C134 101(2) . . . . ?
C6 P15 C133 C138 -74(2) . . . . ?
C7 P16 C37 C38 20(2) . . . . ?
C7 P16 C37 C42 -162.5(19) . . . . ?
C7 P16 C43 C44 117(2) . . . . ?
C7 P16 C43 C48 -65(2) . . . . ?
C7 C8 C9 P17 -161(3) . . . . ?
C9 P17 C61 C62 75(2) . . . . ?
C9 P17 C61 C66 -108(2) . . . . ?
C9 P17 C67 C68 45(2) . . . . ?
C9 P17 C67 C72 -132(2) . . . . ?
C10 C11 C12 P20 -163(3) . . . . ?
C11 C10 P19 Ag10 65(4) . . . . ?
C11 C10 P19 C49 -170(3) . . . . ?
C11 C10 P19 C85 -61(4) . . . . ?
C11 C12 P20 Ag5A -65(3) . . . . ?
C11 C12 P20 Ag5B -48(3) . . . . ?
C11 C12 P20 C55 177(3) . . . . ?
C11 C12 P20 C79 66(3) . . . . ?
C13 P14 C4 C5 -52(4) . . . . ?
C13 P14 C19 C20 11(2) . . . . ?
C13 P14 C19 C24 -169.2(16) . . . . ?
C13 C14 C15 C16 0.0 . . . . ?
C14 C13 C18 C17 0.0 . . . . ?
C14 C15 C16 C17 0.0 . . . . ?
C15 C16 C17 C18 0.0 . . . . ?
C16 C17 C18 C13 0.0 . . . . ?
C18 C13 C14 C15 0.0 . . . . ?
C19 P14 C4 C5 -163(3) . . . . ?
C19 P14 C13 C14 54.6(19) . . . . ?
C19 P14 C13 C18 -130.1(16) . . . . ?
C19 C20 C21 C22 0.0 . . . . ?
C20 C19 C24 C23 0.0 . . . . ?
C20 C21 C22 C23 0.0 . . . . ?
C21 C22 C23 C24 0.0 . . . . ?
C22 C23 C24 C19 0.0 . . . . ?
C24 C19 C20 C21 0.0 . . . . ?
C25 P11 C103 C104 80.5(19) . . . . ?
C25 P11 C103 C108 -96.8(18) . . . . ?
C25 P11 C328 C329 -180(4) . . . . ?
C25 C26 C27 C28 0.0 . . . . ?
C26 C25 C30 C29 0.0 . . . . ?
C26 C27 C28 C29 0.0 . . . . ?
C27 C28 C29 C30 0.0 . . . . ?
C28 C29 C30 C25 0.0 . . . . ?
C30 C25 C26 C27 0.0 . . . . ?
C31 P12 C1 C2 177(3) . . . . ?
C31 P12 C115 C116 103.8(18) . . . . ?
C31 P12 C115 C120 -78.8(19) . . . . ?
C31 C32 C33 C34 0.0 . . . . ?
C32 C31 C36 C35 0.0 . . . . ?
C32 C33 C34 C35 0.0 . . . . ?
C33 C34 C35 C36 0.0 . . . . ?
C34 C35 C36 C31 0.0 . . . . ?
C36 C31 C32 C33 0.0 . . . . ?
C37 P16 C7 C8 -166(3) . . . . ?
C37 P16 C43 C44 -132.6(18) . . . . ?
C37 P16 C43 C48 46(2) . . . . ?
C37 C38 C39 C40 0.0 . . . . ?
C38 C37 C42 C41 0.0 . . . . ?
C38 C39 C40 C41 0.0 . . . . ?
C39 C40 C41 C42 0.0 . . . . ?
C40 C41 C42 C37 0.0 . . . . ?
C42 C37 C38 C39 0.0 . . . . ?
C43 P16 C7 C8 -58(4) . . . . ?
C43 P16 C37 C38 -88.6(19) . . . . ?
C43 P16 C37 C42 89.1(17) . . . . ?
C43 C44 C45 C46 0.0 . . . . ?
C44 C43 C48 C47 0.0 . . . . ?
C44 C45 C46 C47 0.0 . . . . ?
C45 C46 C47 C48 0.0 . . . . ?
C46 C47 C48 C43 0.0 . . . . ?
C48 C43 C44 C45 0.0 . . . . ?
C49 C50 C51 C52 0.0 . . . . ?
C50 C49 C54 C53 0.0 . . . . ?
C50 C49 P19 Ag10 31(2) . . . . ?
C50 C49 P19 C10 -97(2) . . . . ?
C50 C49 P19 C85 151.4(19) . . . . ?
C50 C51 C52 C53 0.0 . . . . ?
C51 C52 C53 C54 0.0 . . . . ?
C52 C53 C54 C49 0.0 . . . . ?
C54 C49 C50 C51 0.0 . . . . ?
C54 C49 P19 Ag10 -155.4(15) . . . . ?
C54 C49 P19 C10 77(2) . . . . ?
C54 C49 P19 C85 -35(2) . . . . ?
C55 C56 C57 C58 0.0 . . . . ?
C56 C55 C60 C59 0.0 . . . . ?
C56 C55 P20 Ag5A -58.7(18) . . . . ?
C56 C55 P20 Ag5B -64(2) . . . . ?
C56 C55 P20 C12 62(2) . . . . ?
C56 C55 P20 C79 174.0(18) . . . . ?
C56 C57 C58 C59 0.0 . . . . ?
C57 C58 C59 C60 0.0 . . . . ?
C58 C59 C60 C55 0.0 . . . . ?
C60 C55 C56 C57 0.0 . . . . ?
C60 C55 P20 Ag5A 112.6(16) . . . . ?
C60 C55 P20 Ag5B 107.2(17) . . . . ?
C60 C55 P20 C12 -126(2) . . . . ?
C60 C55 P20 C79 -15(2) . . . . ?
C61 P17 C9 C8 170(3) . . . . ?
C61 P17 C67 C68 -63(2) . . . . ?
C61 P17 C67 C72 120.7(18) . . . . ?
C61 C62 C63 C64 0.0 . . . . ?
C62 C61 C66 C65 0.0 . . . . ?
C62 C63 C64 C65 0.0 . . . . ?
C63 C64 C65 C66 0.0 . . . . ?
C64 C65 C66 C61 0.0 . . . . ?
C66 C61 C62 C63 0.0 . . . . ?
C67 P17 C9 C8 57(4) . . . . ?
C67 P17 C61 C62 -177.8(16) . . . . ?
C67 P17 C61 C66 -1(2) . . . . ?
C67 C68 C69 C70 0.0 . . . . ?
C68 C67 C72 C71 0.0 . . . . ?
C68 C69 C70 C71 0.0 . . . . ?
C69 C70 C71 C72 0.0 . . . . ?
C70 C71 C72 C67 0.0 . . . . ?
C72 C67 C68 C69 0.0 . . . . ?
C73 P15 C6 C5 66(3) . . . . ?
C73 P15 C133 C134 -150.9(17) . . . . ?
C73 P15 C133 C138 34(2) . . . . ?
C73 C74 C75 C76 0.0 . . . . ?
C74 C73 C78 C77 0.0 . . . . ?
C74 C75 C76 C77 0.0 . . . . ?
C75 C76 C77 C78 0.0 . . . . ?
C76 C77 C78 C73 0.0 . . . . ?
C78 C73 C74 C75 0.0 . . . . ?
C79 C80 C81 C82 0.0 . . . . ?
C80 C79 C84 C83 0.0 . . . . ?
C80 C79 P20 Ag5A -30(2) . . . . ?
C80 C79 P20 Ag5B -43.4(17) . . . . ?
C80 C79 P20 C12 -158(2) . . . . ?
C80 C79 P20 C55 89.5(19) . . . . ?
C80 C81 C82 C83 0.0 . . . . ?
C81 C82 C83 C84 0.0 . . . . ?
C82 C83 C84 C79 0.0 . . . . ?
C84 C79 C80 C81 0.0 . . . . ?
C84 C79 P20 Ag5A 154.9(14) . . . . ?
C84 C79 P20 Ag5B 141.7(16) . . . . ?
C84 C79 P20 C12 27(3) . . . . ?
C84 C79 P20 C55 -85(2) . . . . ?
C85 C86 C87 C88 0.0 . . . . ?
C86 C85 C90 C89 0.0 . . . . ?
C86 C85 P19 Ag10 16.9(19) . . . . ?
C86 C85 P19 C10 147(2) . . . . ?
C86 C85 P19 C49 -104.4(19) . . . . ?
C86 C87 C88 C89 0.0 . . . . ?
C87 C88 C89 C90 0.0 . . . . ?
C88 C89 C90 C85 0.0 . . . . ?
C90 C85 C86 C87 0.0 . . . . ?
C90 C85 P19 Ag10 -153.8(16) . . . . ?
C90 C85 P19 C10 -24(3) . . . . ?
C90 C85 P19 C49 85(2) . . . . ?
C91 C92 C93 C94 0.0 . . . . ?
C92 C91 C96 C95 0.0 . . . . ?
C92 C91 P18 Ag15 -124.4(13) . . . . ?
C92 C91 P18 C97 115.8(17) . . . . ?
C92 C91 P18 C316 4(2) . . . . ?
C92 C93 C94 C95 0.0 . . . . ?
C93 C94 C95 C96 0.0 . . . . ?
C94 C95 C96 C91 0.0 . . . . ?
C96 C91 C92 C93 0.0 . . . . ?
C96 C91 P18 Ag15 55.7(13) . . . . ?
C96 C91 P18 C97 -64.2(17) . . . . ?
C96 C91 P18 C316 -176(2) . . . . ?
C97 C98 C99 C100 0.0 . . . . ?
C98 C97 C102 C101 0.0 . . . . ?
C98 C97 P18 Ag15 -170.5(13) . . . . ?
C98 C97 P18 C91 -50(2) . . . . ?
C98 C97 P18 C316 65(2) . . . . ?
C98 C99 C100 C101 0.0 . . . . ?
C99 C100 C101 C102 0.0 . . . . ?
C100 C101 C102 C97 0.0 . . . . ?
C102 C97 C98 C99 0.0 . . . . ?
C102 C97 P18 Ag15 14(2) . . . . ?
C102 C97 P18 C91 134.7(19) . . . . ?
C102 C97 P18 C316 -110(2) . . . . ?
C103 P11 C25 C26 -48.0(19) . . . . ?
C103 P11 C25 C30 132.9(17) . . . . ?
C103 P11 C328 C329 -73(5) . . . . ?
C103 C104 C105 C106 0.0 . . . . ?
C104 C103 C108 C107 0.0 . . . . ?
C104 C105 C106 C107 0.0 . . . . ?
C105 C106 C107 C108 0.0 . . . . ?
C106 C107 C108 C103 0.0 . . . . ?
C108 C103 C104 C105 0.0 . . . . ?
C109 C110 C111 C112 0.0 . . . . ?
C110 C109 C114 C113 0.0 . . . . ?
C110 C109 P21 Ag8A -152.2(13) . . . . ?
C110 C109 P21 Ag8B -166.0(13) . . . . ?
C110 C109 P21 C144 -33.9(19) . . . . ?
C110 C109 P21 C318 85(2) . . . . ?
C110 C111 C112 C113 0.0 . . . . ?
C111 C112 C113 C114 0.0 . . . . ?
C112 C113 C114 C109 0.0 . . . . ?
C114 C109 C110 C111 0.0 . . . . ?
C114 C109 P21 Ag8A 28.0(14) . . . . ?
C114 C109 P21 Ag8B 14.3(13) . . . . ?
C114 C109 P21 C144 146.4(19) . . . . ?
C114 C109 P21 C318 -95(2) . . . . ?
C115 P12 C1 C2 69(3) . . . . ?
C115 P12 C31 C32 172.8(18) . . . . ?
C115 P12 C31 C36 -10(2) . . . . ?
C115 C116 C117 C118 0.0 . . . . ?
C116 C115 C120 C119 0.0 . . . . ?
C116 C117 C118 C119 0.0 . . . . ?
C117 C118 C119 C120 0.0 . . . . ?
C118 C119 C120 C115 0.0 . . . . ?
C120 C115 C116 C117 0.0 . . . . ?
C121 P13 C3 C2 -170(3) . . . . ?
C121 P13 C127 C128 60.9(16) . . . . ?
C121 P13 C127 C132 -119.7(16) . . . . ?
C121 C122 C123 C124 0.0 . . . . ?
C122 C121 C126 C125 0.0 . . . . ?
C122 C123 C124 C125 0.0 . . . . ?
C123 C124 C125 C126 0.0 . . . . ?
C124 C125 C126 C121 0.0 . . . . ?
C126 C121 C122 C123 0.0 . . . . ?
C127 P13 C3 C2 -60(3) . . . . ?
C127 P13 C121 C122 -125.3(17) . . . . ?
C127 P13 C121 C126 54.8(16) . . . . ?
C127 C128 C129 C130 0.0 . . . . ?
C128 C127 C132 C131 0.0 . . . . ?
C128 C129 C130 C131 0.0 . . . . ?
C129 C130 C131 C132 0.0 . . . . ?
C130 C131 C132 C127 0.0 . . . . ?
C132 C127 C128 C129 0.0 . . . . ?
C133 P15 C6 C5 172(3) . . . . ?
C133 P15 C73 C74 93.7(18) . . . . ?
C133 P15 C73 C78 -84.3(19) . . . . ?
C133 C134 C135 C136 0.0 . . . . ?
C134 C133 C138 C137 0.0 . . . . ?
C134 C135 C136 C137 0.0 . . . . ?
C135 C136 C137 C138 0.0 . . . . ?
C136 C137 C138 C133 0.0 . . . . ?
C138 C133 C134 C135 0.0 . . . . ?
C139 C140 C141 C142 0.0 . . . . ?
C139 C144 P21 Ag8A -138.0(13) . . . . ?
C139 C144 P21 Ag8B -146.4(15) . . . . ?
C139 C144 P21 C109 98.0(16) . . . . ?
C139 C144 P21 C318 -18(2) . . . . ?
C140 C139 C144 C143 0.0 . . . . ?
C140 C139 C144 P21 180.0(7) . . . . ?
C140 C141 C142 C143 0.0 . . . . ?
C141 C142 C143 C144 0.0 . . . . ?
C142 C143 C144 C139 0.0 . . . . ?
C142 C143 C144 P21 -179.9(8) . . . . ?
C143 C144 P21 Ag8A 42.0(14) . . . . ?
C143 C144 P21 Ag8B 33.6(16) . . . . ?
C143 C144 P21 C109 -82.0(16) . . . . ?
C143 C144 P21 C318 162(2) . . . . ?
C144 C139 C140 C141 0.0 . . . . ?
C313 C314 S3 Ag12 11(4) . . . . ?
C313 C314 S3 Ag13 -117(3) . . . . ?
C313 C314 S3 Ag19 132(3) . . . . ?
C315 C314 S3 Ag12 147(4) . . . . ?
C315 C314 S3 Ag13 19(5) . . . . ?
C315 C314 S3 Ag19 -91(4) . . . . ?
C316 C317 C318 P21 -81(5) . . . . ?
C317 C316 P18 Ag15 -67(4) . . . . ?
C317 C316 P18 C91 165(3) . . . . ?
C317 C316 P18 C97 57(4) . . . . ?
C317 C318 P21 Ag8A -68(4) . . . . ?
C317 C318 P21 Ag8B -48(4) . . . . ?
C317 C318 P21 C109 59(4) . . . . ?
C317 C318 P21 C144 173(3) . . . . ?
C319 C320 S11 Ag9A 141(3) . . . . ?
C319 C320 S11 Ag9B 164(2) . . . . ?
C319 C320 S11 Ag10 -60(3) . . . . ?
C319 C320 S11 Ag12 40(3) . . . . ?
C321 C320 S11 Ag9A 39(3) . . . . ?
C321 C320 S11 Ag9B 62(3) . . . . ?
C321 C320 S11 Ag10 -162(2) . . . . ?
C321 C320 S11 Ag12 -62(3) . . . . ?
C309 C310 S2 Ag7 43(3) . . . . ?
C309 C310 S2 Ag11 -168(2) . . . . ?
C309 C310 S2 Ag20 -62(2) . . . . ?
C311 C310 S2 Ag7 -64(3) . . . . ?
C311 C310 S2 Ag11 86(2) . . . . ?
C311 C310 S2 Ag20 -168(2) . . . . ?
C325 C326 S4 Ag14 -51(3) . . . . ?
C325 C326 S4 Ag15 58(3) . . . . ?
C325 C326 S4 Ag20 -174(2) . . . . ?
C327 C326 S4 Ag14 51(3) . . . . ?
C327 C326 S4 Ag15 159(2) . . . . ?
C327 C326 S4 Ag20 -72(3) . . . . ?
C328 P11 C25 C26 62(2) . . . . ?
C328 P11 C25 C30 -117(2) . . . . ?
C328 P11 C103 C104 -28(2) . . . . ?
C328 P11 C103 C108 155(2) . . . . ?
C329 C30A P1A Ag9A -56(10) . . . . ?
C329 C30B P1B Ag9B 43(8) . . . . ?
C329 C30B P1B C157 172(7) . . . . ?
C329 C30B P1B C161 -83(7) . . . . ?
Ag1 S10 C154 C156 38(4) . . . . ?
Ag1 S10 C154 C155 -77(4) . . . . ?
Cu6A S7 C164 C165 121(3) . . . . ?
Cu6A S7 C164 C166 -91(4) . . . . ?
Cu6A S10 C154 C156 -45(4) . . . . ?
Cu6A S10 C154 C155 -159(3) . . . . ?
Cu6B S7 C164 C165 137(3) . . . . ?
Cu6B S7 C164 C166 -75(4) . . . . ?
Cu6B S10 C154 C156 -55(4) . . . . ?
Cu6B S10 C154 C155 -170(3) . . . . ?
P18 C91 C92 C93 -180.0(7) . . . . ?
P18 C91 C96 C95 180.0(7) . . . . ?
P18 C97 C98 C99 -175(2) . . . . ?
P18 C97 C102 C101 175(2) . . . . ?
P18 C316 C317 C318 -98(5) . . . . ?
P19 C10 C11 C12 171(3) . . . . ?
P19 C49 C50 C51 173(2) . . . . ?
P19 C49 C54 C53 -173(3) . . . . ?
P19 C85 C86 C87 -171(2) . . . . ?
P19 C85 C90 C89 170(2) . . . . ?
P20 C55 C56 C57 171(2) . . . . ?
P20 C55 C60 C59 -171(2) . . . . ?
P20 C79 C80 C81 -175(2) . . . . ?
P20 C79 C84 C83 175(2) . . . . ?
P21 C109 C110 C111 -179.7(7) . . . . ?
P21 C109 C114 C113 179.7(7) . . . . ?
C146 C157 C145 C171 0.0 . . . . ?
C157 P1B C161 C160 18(3) . . . . ?
C157 P1B C161 C162 -154(2) . . . . ?
C157 C146 C147 C201 0.0 . . . . ?
C157 C145 C171 C201 0.0 . . . . ?
C145 C171 C201 C147 0.0 . . . . ?
C171 C201 C147 C146 0.0 . . . . ?
C147 C146 C157 P1B -174(3) . . . . ?
C147 C146 C157 C145 0.0 . . . . ?
C161 P1B C157 C146 -75(3) . . . . ?
C161 P1B C157 C145 111(2) . . . . ?
C161 C160 C159 C158 0.0 . . . . ?
C160 C161 C162 C163 0.0 . . . . ?
C160 C159 C158 C163 0.0 . . . . ?
C159 C158 C163 C162 0.0 . . . . ?
C158 C163 C162 C161 0.0 . . . . ?
C162 C161 C160 C159 0.0 . . . . ?
Ag3 S6 C148 C149 177(3) . . . . ?
Ag3 S6 C148 C150 76(4) . . . . ?
Ag3 S7 C164 C165 39(4) . . . . ?
Ag3 S7 C164 C166 -173(3) . . . . ?

_smtbx_masks_special_details     ?
loop_
_smtbx_masks_void_nr
_smtbx_masks_void_average_x
_smtbx_masks_void_average_y
_smtbx_masks_void_average_z
_smtbx_masks_void_volume
_smtbx_masks_void_count_electrons
_smtbx_masks_void_content
1 -0.134 -0.110 -0.134 5703.6 1294.8 ?
2 -0.060 0.250 0.852 12.8 0.0 ?
3 0.060 0.750 0.148 12.8 0.0 ?
4 0.160 0.984 0.006 16.9 0.0 ?
5 0.340 0.484 0.494 16.9 2.9 ?
6 0.440 0.250 0.352 12.8 0.0 ?
7 0.560 0.750 0.648 12.8 0.0 ?
8 0.660 0.516 0.506 16.9 0.0 ?
9 0.840 0.016 0.994 16.9 2.7 ?

_smtbx_masks_void_probe_radius   1.2
_smtbx_masks_void_truncation_radius 1.2
_platon_squeeze_special_details  ?
_platon_squeeze_void_probe_radius 1.20
_olex2_submission_special_instructions 'No special instructions were received'
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_1213-1_auto_sq
_database_code_depnum_ccdc_archive 'CCDC 2336489'
loop_
_audit_author_name
_audit_author_address
'Jing Zhang'
;Beijing Institute of Technology
China
;
_audit_update_record             
;
2024-02-29 deposited with the CCDC.	2024-05-27 downloaded from the CCDC.
;
_audit_creation_date             2023-12-15
_audit_creation_method           
;
Olex2 1.3
(compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6408)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'Ag16 C242 Co8 O82 P16 S6 Si2 W18, 4(C2 N)'
_chemical_formula_sum            'C250 Ag16 Co8 N4 O82 P16 S6 Si2 W18'
_chemical_formula_weight         10621.26
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
W W -0.8490 6.8722 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   18.6002(2)
_cell_length_b                   22.9769(3)
_cell_length_c                   23.2397(3)
_cell_angle_alpha                67.8510(10)
_cell_angle_beta                 66.9270(10)
_cell_angle_gamma                78.9240(10)
_cell_volume                     8451.8(2)
_cell_formula_units_Z            1
_cell_measurement_reflns_used    46554
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      29.5450
_cell_measurement_theta_min      2.2050
_shelx_estimated_absorpt_T_max   0.328
_shelx_estimated_absorpt_T_min   0.300
_exptl_absorpt_coefficient_mu    7.561
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.65041
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
CrysAlisPro 1.171.42.86a (Rigaku Oxford Diffraction, 2023)
Empirical absorption correction using spherical harmonics,
implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            'clear brownish pink'
_exptl_crystal_colour_lustre     clear
_exptl_crystal_colour_modifier   brownish
_exptl_crystal_colour_primary    pink
_exptl_crystal_density_diffrn    2.087
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             4848
_exptl_crystal_size_max          0.21
_exptl_crystal_size_mid          0.2
_exptl_crystal_size_min          0.19
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0445
_diffrn_reflns_av_unetI/netI     0.0544
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.972
_diffrn_reflns_limit_h_max       21
_diffrn_reflns_limit_h_min       -24
_diffrn_reflns_limit_k_max       29
_diffrn_reflns_limit_k_min       -28
_diffrn_reflns_limit_l_max       30
_diffrn_reflns_limit_l_min       -29
_diffrn_reflns_number            113256
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.972
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         27.499
_diffrn_reflns_theta_min         2.158
_diffrn_ambient_temperature      293(2)
_diffrn_detector_area_resol_mean 10.0000
_diffrn_detector_type            HyPix
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.972
_diffrn_measurement_details      
;
List of Runs (angles in degrees, time in seconds):

  # Type    Start    End  Width  tₑₓₚ   ω     θ     κ     φ   Frames
#--------------------------------------------------------------------------
  1  ω    -86.00 -61.00   0.50    1.50    --  -17.50 152.00 151.00   50
  2  ω     13.00  65.00   0.50    1.50    --  -17.50  19.00 150.00  104
  3  ω    -55.00 -12.00   0.50    1.50    --  -17.50 122.00  -8.00   86
  4  ω    -24.00  58.00   0.50    1.50    --  -17.50  19.00 -90.00  164
  5  ω    -59.00  44.00   0.50    1.50    --   14.06 -57.00-180.00  206
  6  ω    -16.00   9.00   0.50    1.50    --   14.06 -99.00 -30.00   50
  7  ω     19.00  44.00   0.50    1.50    --   14.06 -99.00 -30.00   50
  8  ω     45.00  72.00   0.50    1.50    --   14.06-122.00 -90.00   54
  9  ω     45.00  70.00   0.50    1.50    --   14.06-178.00 -60.00   50
 10  ω     37.00  92.00   0.50    1.50    --   14.06-152.00 109.00  110
 11  ω    -62.00  44.00   0.50    1.50    --   14.06 -57.00  90.00  212
 12  ω    -73.00 -43.00   0.50    1.50    --  -17.50-178.00  30.00   60
 13  ω    -17.00  30.00   0.50    1.50    --  -17.50 -99.00 -90.00   94
;
_diffrn_measurement_device       'four-circle diffractometer'
_diffrn_measurement_device_type  'XtaLAB Synergy R, DW system, HyPix'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                27411
_reflns_number_total             37761
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'CrysAlisPro 1.171.42.86a (Rigaku OD, 2023)'
_computing_data_collection       'CrysAlisPro 1.171.42.86a (Rigaku OD, 2023)'
_computing_data_reduction        'CrysAlisPro 1.171.42.86a (Rigaku OD, 2023)'
_computing_molecular_graphics    'Olex2 1.3 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.3 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2018/3 (Sheldrick, 2015)'
_computing_structure_solution    ?
_refine_diff_density_max         3.227
_refine_diff_density_min         -1.655
_refine_diff_density_rms         0.242
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.021
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1802
_refine_ls_number_reflns         37761
_refine_ls_number_restraints     55
_refine_ls_R_factor_all          0.0796
_refine_ls_R_factor_gt           0.0495
_refine_ls_restrained_S_all      1.021
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0597P)²+109.7717P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1216
_refine_ls_wR_factor_ref         0.1383
_refine_special_details          ?
_olex2_refinement_description    
;
1. Restrained distances
 C124-C61
 1.54 with sigma of 0.02
2. Uiso/Uaniso restraints and constraints
C118 \\sim C79 \\sim C119 \\sim C60 \\sim C121 \\sim C81: within 2A with sigma
of 0.01 and sigma for terminal atoms of 0.02 within 2A
C31 \\sim C110 \\sim C45 \\sim C124 \\sim C61: within 2A with sigma of 0.01 and
sigma for terminal atoms of 0.02 within 2A
Uanis(N2) = Uanis(N1)
3. Others
 Sof(Ag7)=1-FVAR(1)
 Sof(Ag3)=FVAR(1)
4.a Fitted hexagon refined as free rotating group:
 C118(C79,C119,C60,C121,C81)
;
_atom_sites_solution_hydrogens   .
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
W1 W 0.54329(2) 0.24456(2) 0.60046(2) 0.02462(9) Uani 1 1 d . . . . .
W4 W 0.35409(2) 0.49387(2) 0.51489(2) 0.02473(9) Uani 1 1 d . . . . .
W6 W 0.51884(2) 0.39470(2) 0.47318(2) 0.02453(9) Uani 1 1 d . . . . .
W8 W 0.38797(2) 0.26856(2) 0.52544(2) 0.02534(9) Uani 1 1 d . . . . .
W9 W 0.21346(2) 0.44589(2) 0.68628(2) 0.02554(9) Uani 1 1 d . . . . .
W5 W 0.25307(2) 0.22392(2) 0.67828(2) 0.02610(9) Uani 1 1 d . . . . .
W3 W 0.22925(2) 0.36347(2) 0.56787(2) 0.02600(9) Uani 1 1 d . . . . .
W7 W 0.40565(2) 0.19959(2) 0.75167(2) 0.02721(9) Uani 1 1 d . . . . .
W2 W 0.22824(2) 0.30511(2) 0.79662(2) 0.02683(9) Uani 1 1 d . . . . .
Ag2 Ag 0.94903(4) 0.53069(4) 0.18387(4) 0.03546(18) Uani 1 1 d . . . . .
Ag4 Ag 0.20956(5) 0.39577(4) 0.91103(4) 0.03594(18) Uani 1 1 d . . . . .
Ag6 Ag 0.54078(5) 0.17792(4) 0.84446(4) 0.03975(19) Uani 1 1 d . . . . .
Ag8 Ag 0.38202(5) 0.89363(4) 0.30539(4) 0.03930(19) Uani 1 1 d . . . . .
Ag9 Ag 0.88128(5) 0.83767(4) 0.13123(4) 0.0421(2) Uani 1 1 d . . . . .
Ag5 Ag 0.79066(6) 0.43338(4) 0.23919(4) 0.0499(2) Uani 1 1 d . . . . .
Ag1 Ag 0.73189(6) 0.92724(4) 0.16852(4) 0.0493(2) Uani 1 1 d . . . . .
Ag7 Ag 0.7126(5) 0.2254(9) 0.6649(4) 0.090(3) Uani 0.37(2) 1 d . . P A 2
Co1 Co 0.48423(7) 0.45700(6) 0.59218(6) 0.0248(3) Uani 1 1 d . . . . .
Co4 Co 0.51923(7) 0.31170(6) 0.70746(6) 0.0272(3) Uani 1 1 d . . . . .
Co2 Co 0.34506(7) 0.41365(6) 0.75551(6) 0.0264(3) Uani 1 1 d . . . . .
Co3 Co 0.51163(7) 0.43725(6) 0.72309(7) 0.0293(3) Uani 1 1 d . . . . .
Si Si 0.37583(12) 0.34573(9) 0.63632(10) 0.0119(4) Uani 1 1 d . . . . .
S1 S 0.86489(15) 0.51143(12) 0.13821(12) 0.0334(5) Uani 1 1 d . . . . .
P1 P 0.79076(15) 0.33856(12) 0.32667(13) 0.0303(5) Uani 1 1 d . . . . .
S3 S 0.34818(16) 0.85412(13) 0.23926(14) 0.0383(6) Uani 1 1 d . . . . .
P4 P 0.98563(16) 0.80294(13) 0.17305(14) 0.0351(6) Uani 1 1 d . . . . .
P6 P 0.46747(16) 0.17148(13) 0.95540(14) 0.0381(6) Uani 1 1 d . . . . .
P8 P 0.18457(16) 0.30593(14) 1.00762(13) 0.0380(6) Uani 1 1 d . . . . .
P2 P 1.04797(16) 0.54433(14) 0.21720(15) 0.0386(6) Uani 1 1 d . . . . .
S2 S 0.80407(18) 0.90531(15) 0.06695(15) 0.0493(8) Uani 1 1 d . . . . .
P5 P 0.6970(2) 0.98965(16) 0.23785(17) 0.0526(9) Uani 1 1 d . . . . .
P3 P 0.3858(2) 0.94903(14) 0.37158(17) 0.0474(8) Uani 1 1 d . . . . .
P7 P 0.82354(16) 0.28319(16) 0.57347(15) 0.0428(7) Uani 1 1 d . . . . .
O21 O 0.2894(3) 0.4910(3) 0.5999(3) 0.0251(14) Uani 1 1 d . . . . .
O20 O 0.5519(3) 0.5309(3) 0.5520(3) 0.0254(14) Uani 1 1 d . . . . .
O2 O 0.4327(3) 0.5412(3) 0.5155(3) 0.0240(13) Uani 1 1 d . . . . .
O5 O 0.1639(4) 0.3766(3) 0.7625(3) 0.0284(14) Uani 1 1 d . . . . .
O11 O 0.1330(4) 0.4982(3) 0.6861(3) 0.0333(16) Uani 1 1 d . . . . .
O35 O 0.3911(4) 0.1244(3) 0.8086(3) 0.0346(16) Uani 1 1 d . . . . .
O6 O 0.3163(4) 0.5577(3) 0.4642(3) 0.0315(16) Uani 1 1 d . . . . .
O7 O 0.1949(4) 0.1606(3) 0.7154(4) 0.0372(17) Uani 1 1 d . . . . .
O15 O 0.1562(4) 0.2645(3) 0.8682(3) 0.0329(16) Uani 1 1 d . . . . .
O18 O 0.1606(4) 0.3944(4) 0.5307(4) 0.0375(17) Uani 1 1 d . . . . .
O34 O 0.5770(5) 0.5182(4) 0.6677(5) 0.061(2) Uani 1 1 d . . . . .
C29 C 0.6683(6) 0.2547(5) 0.3992(5) 0.036(2) Uani 1 1 d . . . . .
C12 C 0.9865(6) 0.7228(5) 0.2332(5) 0.036(2) Uani 1 1 d . . . . .
C44 C 1.0180(6) 0.6086(5) 0.2518(5) 0.035(2) Uani 1 1 d . . . . .
C17 C 1.0068(6) 0.6720(5) 0.2000(5) 0.035(2) Uani 1 1 d . . . . .
C48 C 0.7311(6) 0.2773(5) 0.3389(5) 0.031(2) Uani 1 1 d . . . . .
C3 C 0.0388(7) 0.2993(6) 1.0042(6) 0.046(3) Uani 1 1 d . . . . .
C33 C 0.7629(6) 0.3550(5) 0.4042(5) 0.036(2) Uani 1 1 d . . . . .
C22 C 0.8092(7) 0.3335(6) 0.4957(6) 0.043(3) Uani 1 1 d . . . . .
C53 C 0.7788(7) 0.3013(6) 0.4632(5) 0.044(3) Uani 1 1 d . . . . .
C55 C 0.9881(7) 0.8293(6) 0.2813(6) 0.049(3) Uani 1 1 d . . . . .
C34 C 1.0799(7) 0.8038(5) 0.1057(6) 0.043(3) Uani 1 1 d . . . . .
C6 C 0.6363(8) 0.1915(6) 0.3491(7) 0.057(3) Uani 1 1 d . . . . .
C23 C 0.2304(6) 0.2324(5) 0.9913(6) 0.045(3) Uani 1 1 d . . . . .
C40 C 0.3598(7) 0.1709(6) 0.9836(6) 0.052(3) Uani 1 1 d . . . . .
C11 C 0.6234(8) 0.9588(6) 0.3228(6) 0.051(3) Uani 1 1 d . . . . .
C43 C 1.0735(7) 0.4801(5) 0.2821(7) 0.048(3) Uani 1 1 d . . . . .
C63 C 1.0809(9) 0.8119(7) 0.0429(6) 0.061(4) Uani 1 1 d . . . . .
C65 C 0.0805(6) 0.2885(5) 1.0468(5) 0.037(2) Uani 1 1 d . . . . .
C67 C 1.0012(6) 0.8513(5) 0.2136(6) 0.041(3) Uani 1 1 d . . . . .
C69 C 0.7758(8) 1.0133(6) 0.2515(7) 0.056(3) Uani 1 1 d . . . . .
C71 C 0.8887(6) 0.3017(5) 0.3147(6) 0.041(3) Uani 1 1 d . . . . .
C35 C 0.3203(6) 0.2367(6) 0.9585(6) 0.050(3) Uani 1 1 d . . . . .
C38 C 0.6220(7) 0.2107(6) 0.4023(6) 0.049(3) Uani 1 1 d . . . . .
C9 C 0.4806(7) 0.9377(5) 0.3837(6) 0.045(3) Uani 1 1 d . . . . .
C16 C 0.0421(7) 0.2682(6) 1.1162(6) 0.049(3) Uani 1 1 d . . . . .
C25 C 0.9049(7) 0.2383(6) 0.3273(7) 0.052(3) Uani 1 1 d . . . . .
C36 C 0.4933(8) 0.0992(5) 1.0138(6) 0.049(3) Uani 1 1 d . . . . .
C8 C 0.3102(8) 0.9333(5) 0.4527(7) 0.052(3) Uani 1 1 d . . . . .
C80 C 0.7980(7) 0.9772(7) 0.3060(7) 0.052(3) Uani 1 1 d . . . . .
C47 C 0.6306(12) 1.1109(7) 0.2328(9) 0.084(6) Uani 1 1 d . . . . .
C27 C 0.5956(8) 1.1326(9) 0.1196(7) 0.073(5) Uani 1 1 d . . . . .
C84 C 1.0194(7) 0.4637(6) 0.3477(7) 0.054(3) Uani 1 1 d . . . . .
C86 C 0.6512(9) 1.0652(6) 0.2022(6) 0.057(4) Uani 1 1 d . . . . .
C88 C 0.4814(6) 0.2377(5) 0.9752(6) 0.045(3) Uani 1 1 d . . . . .
C90 C 0.5108(7) 0.2919(6) 0.9218(7) 0.053(3) Uani 1 1 d . . . . .
C92 C 0.5444(8) 0.9569(6) 0.3156(6) 0.053(3) Uani 1 1 d . . . . .
C94 C 0.5407(16) -0.0138(8) 1.0941(12) 0.098(7) Uani 1 1 d . . . . .
C96 C 0.9914(7) 0.3511(6) 0.6024(6) 0.050(3) Uani 1 1 d . . . . .
C98 C 0.8944(8) 0.2239(6) 0.5491(6) 0.051(3) Uani 1 1 d . . . . .
C100 C -0.0411(8) 0.2884(6) 1.0312(7) 0.055(3) Uani 1 1 d . . . . .
C1 C 0.4595(8) 0.2927(6) 1.0523(7) 0.056(3) Uani 1 1 d . . . . .
C103 C -0.0382(8) 0.2581(6) 1.1417(7) 0.059(4) Uani 1 1 d . . . . .
C39 C 1.1502(7) 0.7922(6) 0.1195(7) 0.056(3) Uani 1 1 d . . . . .
C32 C 1.0031(9) 0.8678(7) 0.3101(8) 0.064(4) Uani 1 1 d . . . . .
C37 C 1.1416(6) 0.5674(6) 0.1507(7) 0.049(3) Uani 1 1 d . . . . .
C2 C 0.4902(7) 0.3465(6) 0.9977(8) 0.057(3) Uani 1 1 d . . . . .
C7 C 0.9273(7) 0.4754(6) 0.0765(6) 0.048(3) Uani 1 1 d . . . . .
C10 C 0.8575(8) 0.9972(7) 0.3157(8) 0.064(4) Uani 1 1 d . . . . .
C13 C 1.0288(7) 0.9122(5) 0.1735(7) 0.049(3) Uani 1 1 d . . . . .
C18 C 0.9852(8) 0.4250(6) 0.1028(7) 0.059(4) Uani 1 1 d . . . . .
C24 C -0.0800(8) 0.2683(7) 1.1007(7) 0.061(4) Uani 1 1 d . . . . .
C28 C 0.6982(8) 0.2162(7) 0.2903(7) 0.056(3) Uani 1 1 d . . . . .
C4 C 0.9733(8) 0.4144(7) 0.5855(6) 0.061(4) Uani 1 1 d . . . . .
C5 C 0.5652(9) 0.0705(6) 0.9914(8) 0.066(4) Uani 1 1 d . . . . .
C15 C 0.5960(12) 1.1705(8) 0.2049(10) 0.092(6) Uani 1 1 d . . . . .
C19 C 0.5791(10) 1.1791(8) 0.1487(8) 0.073(5) Uani 1 1 d . . . . .
C20 C 0.5156(7) 0.3469(6) 0.9326(8) 0.058(4) Uani 1 1 d . . . . .
C120 C 0.2546(11) 0.9306(9) 0.5663(9) 0.086(6) Uani 1 1 d . . . . .
C14 C 0.7454(7) 0.2597(6) 0.2853(6) 0.045(3) Uani 1 1 d . . . . .
C21 C 0.4416(11) 0.0713(6) 1.0786(7) 0.071(4) Uani 1 1 d . . . . .
C26 C 0.9473(7) 0.3099(6) 0.5989(6) 0.053(3) Uani 1 1 d . . . . .
C42 C 0.2386(10) 0.9138(8) 0.4604(7) 0.076(5) Uani 1 1 d . . . . .
C125 C 0.8943(8) 1.0523(7) 0.2711(9) 0.069(4) Uani 1 1 d . . . . .
C83 C 0.4697(16) 0.0144(8) 1.1187(8) 0.099(7) Uani 1 1 d . . . . .
C30 C 0.9044(9) 0.4401(7) 0.5723(8) 0.064(4) Uani 1 1 d . . . . .
C85 C 0.3180(10) 0.9408(8) 0.5063(9) 0.078(5) Uani 1 1 d . . . . .
C62 C 1.1464(11) 0.4447(9) 0.2654(10) 0.095(6) Uani 1 1 d . . . . .
C87 C 1.0314(8) 0.9262(7) 0.2720(8) 0.059(4) Uani 1 1 d . . . . .
C52 C 1.0379(9) 0.4171(7) 0.4012(8) 0.066(4) Uani 1 1 d . . . . .
C89 C 0.8762(10) 0.4483(8) 0.0557(8) 0.076(5) Uani 1 1 d . . . . .
C64 C 0.9640(7) 0.2387(8) 0.4937(8) 0.068(4) Uani 1 1 d . . . . .
C91 C 1.2229(8) 0.7866(7) 0.0700(8) 0.072(4) Uani 1 1 d . . . . .
C46 C 0.9503(7) 0.3415(7) 0.2927(8) 0.067(4) Uani 1 1 d . . . . .
C93 C 1.1533(10) 0.8088(7) -0.0076(7) 0.074(5) Uani 1 1 d . . . . .
C66 C 0.5888(14) 0.0148(9) 1.0321(12) 0.099(7) Uani 1 1 d . . . . .
C95 C 1.1994(8) 0.5892(9) 0.1604(9) 0.086(6) Uani 1 1 d . . . . .
C54 C 1.1543(8) 0.5655(8) 0.0891(7) 0.073(5) Uani 1 1 d . . . . .
C97 C 0.8811(11) 0.1599(7) 0.5863(9) 0.079(5) Uani 1 1 d . . . . .
C68 C 0.8155(11) 1.0670(8) 0.2057(8) 0.083(5) Uani 1 1 d . . . . .
C99 C 0.1759(12) 0.9050(10) 0.5200(9) 0.100(7) Uani 1 1 d . . . . .
C41 C 1.2242(10) 0.7953(8) 0.0055(9) 0.081(5) Uani 1 1 d . . . . .
C101 C 1.0422(9) 0.2499(9) 0.2966(10) 0.088(6) Uani 1 1 d . . . . .
C70 C 1.2268(10) 0.5855(11) 0.0354(10) 0.103(7) Uani 1 1 d . . . . .
C102 C 1.0173(9) 0.1896(10) 0.4780(10) 0.085(6) Uani 1 1 d . . . . .
O1 O 0.4388(3) 0.2938(3) 0.6629(3) 0.0230(13) Uani 1 1 d . . . . .
O19 O 0.6170(4) 0.1997(3) 0.5609(3) 0.0304(15) Uani 1 1 d . . . . .
O3 O 0.4644(4) 0.2403(3) 0.5637(3) 0.0283(14) Uani 1 1 d . . . . .
O4 O 0.1993(3) 0.3997(3) 0.6332(3) 0.0294(15) Uani 1 1 d . . . . .
O37 O 0.4203(4) 0.2359(3) 0.4630(3) 0.0338(16) Uani 1 1 d . . . . .
O8 O 0.3016(4) 0.3228(3) 0.5056(3) 0.0289(14) Uani 1 1 d . . . . .
O9 O 0.5919(4) 0.2683(3) 0.6405(3) 0.0295(15) Uani 1 1 d . . . . .
O12 O 0.3372(3) 0.1925(3) 0.7058(3) 0.0268(14) Uani 1 1 d . . . . .
O13 O 0.5859(4) 0.3991(3) 0.3957(3) 0.0293(15) Uani 1 1 d . . . . .
O29 O 0.4231(3) 0.4059(3) 0.5732(3) 0.0260(14) Uani 1 1 d . . . . .
O41 O 0.3292(3) 0.3136(3) 0.6087(3) 0.0238(13) Uani 1 1 d . . . . .
O32 O 0.1899(4) 0.2851(3) 0.6264(3) 0.0281(14) Uani 1 1 d . . . . .
O42 O 0.4242(4) 0.4732(3) 0.6790(3) 0.0292(15) Uani 1 1 d . . . . .
O24 O 0.3032(3) 0.4320(3) 0.5161(3) 0.0270(14) Uani 1 1 d . . . . .
O10 O 0.4426(4) 0.3585(3) 0.7676(3) 0.0290(14) Uani 1 1 d . . . . .
O36 O 0.6133(4) 0.3008(3) 0.7416(3) 0.0344(16) Uani 1 1 d . . . . .
O14 O 0.2557(4) 0.4721(3) 0.7287(3) 0.0303(15) Uani 1 1 d . . . . .
O30 O 0.4717(4) 0.2273(3) 0.7734(3) 0.0322(15) Uani 1 1 d . . . . .
O16 O 0.2667(4) 0.3489(3) 0.8266(3) 0.0301(15) Uani 1 1 d . . . . .
O38 O 0.6032(4) 0.3933(4) 0.7571(4) 0.0405(18) Uani 1 1 d . . . . .
O17 O 0.3344(4) 0.4458(4) 0.8326(3) 0.0404(18) Uani 1 1 d . . . . .
O22 O 0.3132(3) 0.3701(3) 0.6956(3) 0.0251(14) Uani 1 1 d . . . . .
C56 C 0.4562(8) 0.2372(6) 1.0400(6) 0.049(3) Uani 1 1 d . . . . .
C104 C 0.8796(6) 0.3343(6) 0.5829(6) 0.041(3) Uani 1 1 d . . . . .
O23 O 0.4473(4) 0.3460(3) 0.4781(3) 0.0256(14) Uani 1 1 d . . . . .
O39 O 0.5497(4) 0.3992(3) 0.6446(3) 0.0292(15) Uani 1 1 d . . . . .
O25 O 0.2119(3) 0.2673(3) 0.7378(3) 0.0264(14) Uani 1 1 d . . . . .
O31 O 0.4586(4) 0.4684(3) 0.8044(3) 0.0354(16) Uani 1 1 d . . . . .
C72 C 0.3877(6) 0.4631(5) 0.8422(5) 0.037(2) Uani 1 1 d . . . . .
C105 C 0.6366(6) 0.3422(6) 0.7540(5) 0.039(3) Uani 1 1 d . . . . .
C49 C 0.6339(8) 1.0746(7) 0.1475(6) 0.054(3) Uani 1 1 d . . . . .
C106 C 0.7141(8) 0.3260(7) 0.7664(8) 0.065(4) Uani 1 1 d . . . . .
C73 C 0.8583(8) 0.3991(7) 0.5699(8) 0.057(3) Uani 1 1 d . . . . .
C107 C 0.3653(8) 0.4787(7) 0.9050(6) 0.057(4) Uani 1 1 d . . . . .
O27 O 0.4913(3) 0.1783(3) 0.6789(3) 0.0275(14) Uani 1 1 d . . . . .
O40 O 0.3156(4) 0.2095(3) 0.5932(3) 0.0292(15) Uani 1 1 d . . . . .
O28 O 0.3160(4) 0.2455(3) 0.7915(3) 0.0286(15) Uani 1 1 d . . . . .
C57 C 0.8607(8) 0.9790(8) 0.0153(8) 0.084(6) Uani 1 1 d . . . . .
C108 C 0.2119(7) 0.3086(6) 1.0739(6) 0.049(3) Uani 1 1 d . . . . .
C74 C 0.2221(9) 0.3679(8) 1.0721(7) 0.065(4) Uani 1 1 d . . . . .
C109 C 1.0447(7) 0.9491(7) 0.2041(8) 0.060(4) Uani 1 1 d . . . . .
C31 C 0.2784(9) 0.9098(8) 0.2018(8) 0.077(4) Uani 1 1 d . U . . .
C110 C 0.2388(8) 0.8696(8) 0.1819(8) 0.070(4) Uani 1 1 d . U . . .
C75 C 0.2262(8) 0.2536(9) 1.1218(7) 0.076(5) Uani 1 1 d . . . . .
C111 C 0.9816(8) 0.2122(7) 0.3173(10) 0.078(5) Uani 1 1 d . . . . .
C58 C 0.2429(11) 0.3741(11) 1.1228(9) 0.091(6) Uani 1 1 d . . . . .
C112 C 1.2711(8) 0.6060(10) 0.1083(11) 0.099(7) Uani 1 1 d . . . . .
C76 C 0.8939(10) 1.0005(8) 0.0537(10) 0.093(6) Uani 1 1 d . . . . .
C113 C 0.2464(10) 0.2616(12) 1.1733(8) 0.090(6) Uani 1 1 d . . . . .
C50 C 1.0001(14) 0.1260(13) 0.5192(15) 0.117(9) Uani 1 1 d . . . . .
C114 C 0.2549(12) 0.3214(14) 1.1707(10) 0.116(8) Uani 1 1 d . . . . .
C77 C 0.9317(15) 0.1129(9) 0.5711(11) 0.093(6) Uani 1 1 d . . . . .
C115 C 1.1092(11) 0.3828(9) 0.3867(11) 0.100(7) Uani 1 1 d . . . . .
C59 C 1.2828(8) 0.6051(10) 0.0467(10) 0.092(6) Uani 1 1 d . . . . .
C116 C 1.0281(8) 0.3132(9) 0.2846(11) 0.098(7) Uani 1 1 d . . . . .
C78 C 0.1840(9) 0.9163(7) 0.5727(7) 0.061(4) Uani 1 1 d . . . . .
C117 C 0.8071(10) 1.0320(7) -0.0115(9) 0.096(6) Uani 1 1 d . . . . .
C45 C 0.2324(13) 0.9525(12) 0.2397(12) 0.125(7) Uani 1 1 d . U . . .
C118 C 0.3475(12) 1.0736(5) 0.3747(5) 0.139(5) Uani 1 1 d G U . . .
C79 C 0.3697(10) 1.0348(4) 0.3362(6) 0.103(4) Uani 1 1 d G U . . .
C119 C 0.3865(11) 1.0610(5) 0.2681(6) 0.117(5) Uani 1 1 d G U . . .
C60 C 0.3812(11) 1.1259(5) 0.2384(5) 0.131(6) Uani 1 1 d G U . . .
C121 C 0.3590(12) 1.1647(4) 0.2769(7) 0.131(6) Uani 1 1 d G U . . .
C81 C 0.3421(12) 1.1385(5) 0.3450(7) 0.147(6) Uani 1 1 d G U . . .
C122 C 1.1625(14) 0.3952(11) 0.3196(13) 0.121(8) Uani 1 1 d . . . . .
C51 C 0.8729(11) 1.0865(8) 0.2171(11) 0.090(6) Uani 1 1 d . . . . .
Ag3 Ag 0.70934(19) 0.2456(2) 0.66276(16) 0.0334(9) Uani 0.63(2) 1 d . . P A 1
O26 O 0.4423(3) 0.6715(3) 0.4707(3) 0.0227(13) Uani 1 1 d . . . . .
C123 C 0.5339(14) 0.9218(8) 0.5408(10) 0.086(6) Uani 1 1 d . . . . .
N1 N 0.4724(16) 0.9364(9) 0.5713(14) 0.160(8) Uani 1 1 d . . . . .
C82 C 0.6098(10) 0.9081(7) 0.4963(7) 0.065(4) Uani 1 1 d . . . . .
N2 N 0.8627(16) 0.8961(9) -0.1571(14) 0.160(8) Uani 1 1 d . . . . .
C124 C 0.8993(18) 0.8876(12) -0.1237(14) 0.139(9) Uani 1 1 d D U . . .
C61 C 0.9455(17) 0.8754(12) -0.0785(13) 0.138(9) Uani 1 1 d D U . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
W1 O1 2.312(6) . ?
W1 O19 1.723(7) . ?
W1 O3 1.999(6) . ?
W1 O9 1.792(7) . ?
W1 O27 1.914(6) . ?
W1 O26 1.993(6) 2_666 ?
W4 O21 1.851(6) . ?
W4 O20 1.988(6) 2_666 ?
W4 O2 1.990(6) . ?
W4 O6 1.727(6) . ?
W4 O29 2.422(6) . ?
W4 O24 1.840(7) . ?
W6 O20 1.995(6) 2_666 ?
W6 O2 2.009(6) 2_666 ?
W6 O13 1.720(6) . ?
W6 O29 2.381(6) . ?
W6 O23 1.843(6) . ?
W6 O26 1.833(6) 2_666 ?
W8 O3 1.853(6) . ?
W8 O37 1.729(7) . ?
W8 O8 1.930(6) . ?
W8 O41 2.329(6) . ?
W8 O23 1.979(6) . ?
W8 O40 1.888(6) . ?
W9 O21 1.967(5) . ?
W9 O5 1.917(6) . ?
W9 O11 1.731(7) . ?
W9 O4 2.017(7) . ?
W9 O14 1.786(7) . ?
W9 O22 2.305(6) . ?
W5 O7 1.720(7) . ?
W5 O12 1.839(6) . ?
W5 O41 2.384(6) . ?
W5 O32 2.002(6) . ?
W5 O25 1.846(6) . ?
W5 O40 1.978(7) . ?
W3 O18 1.714(7) . ?
W3 O4 1.849(7) . ?
W3 O8 1.946(6) . ?
W3 O41 2.327(6) . ?
W3 O32 1.873(6) . ?
W3 O24 1.981(6) . ?
W7 O35 1.728(6) . ?
W7 O1 2.338(6) . ?
W7 O12 2.015(6) . ?
W7 O30 1.788(7) . ?
W7 O27 1.962(6) . ?
W7 O28 1.897(7) . ?
W2 O5 1.941(7) . ?
W2 O15 1.731(6) . ?
W2 O16 1.790(7) . ?
W2 O22 2.365(6) . ?
W2 O25 2.010(6) . ?
W2 O28 1.915(7) . ?
Ag2 S1 2.386(3) . ?
Ag2 P2 2.368(3) . ?
Ag4 S1 2.458(3) 2_666 ?
Ag4 P8 2.361(3) . ?
Ag4 O16 2.379(7) . ?
Ag4 O17 2.482(7) . ?
Ag6 S3 2.437(3) 2_666 ?
Ag6 P6 2.359(3) . ?
Ag6 O30 2.315(7) . ?
Ag8 Ag7 3.244(16) 2_666 ?
Ag8 S3 2.369(3) . ?
Ag8 P3 2.364(3) . ?
Ag9 Ag1 3.1572(14) . ?
Ag9 P4 2.376(3) . ?
Ag9 S2 2.405(3) . ?
Ag9 O15 2.569(7) 2_666 ?
Ag5 S1 2.423(3) . ?
Ag5 P1 2.354(3) . ?
Ag5 O14 2.452(7) 2_666 ?
Ag1 S2 2.404(3) . ?
Ag1 P5 2.375(4) . ?
Ag1 O35 2.557(7) 2_666 ?
Ag7 S3 2.308(10) 2_666 ?
Ag7 P7 2.455(8) . ?
Ag7 O9 2.460(11) . ?
Co1 O20 2.011(6) . ?
Co1 O2 2.359(6) 2_666 ?
Co1 O29 2.041(6) . ?
Co1 O42 2.023(7) . ?
Co1 O39 2.013(6) . ?
Co4 O1 2.291(6) . ?
Co4 O9 2.061(7) . ?
Co4 O10 2.031(7) . ?
Co4 O36 2.127(7) . ?
Co4 O30 2.060(6) . ?
Co4 O39 2.018(6) . ?
Co2 Co3 2.9947(17) . ?
Co2 O42 2.022(6) . ?
Co2 O10 2.055(7) . ?
Co2 O14 2.068(7) . ?
Co2 O16 2.040(6) . ?
Co2 O17 2.111(7) . ?
Co2 O22 2.284(6) . ?
Co3 O34 2.106(8) . ?
Co3 O42 2.129(7) . ?
Co3 O10 2.104(6) . ?
Co3 O38 2.083(7) . ?
Co3 O39 2.131(7) . ?
Co3 O31 2.084(7) . ?
Si O1 1.629(6) . ?
Si O29 1.663(6) . ?
Si O41 1.658(6) . ?
Si O22 1.624(7) . ?
S1 C7 1.819(10) . ?
P1 C48 1.830(10) . ?
P1 C33 1.833(11) . ?
P1 C71 1.817(11) . ?
S3 C31 1.867(13) . ?
S3 Ag3 2.584(5) 2_666 ?
P4 C12 1.847(10) . ?
P4 C34 1.834(11) . ?
P4 C67 1.826(12) . ?
P6 C40 1.848(12) . ?
P6 C36 1.826(11) . ?
P6 C88 1.834(13) . ?
P8 C23 1.844(12) . ?
P8 C65 1.838(11) . ?
P8 C108 1.826(13) . ?
P2 C44 1.835(11) . ?
P2 C43 1.813(12) . ?
P2 C37 1.824(11) . ?
S2 C57 1.893(15) . ?
P5 C11 1.864(12) . ?
P5 C69 1.828(14) . ?
P5 C86 1.823(14) . ?
P3 C9 1.848(12) . ?
P3 C8 1.807(15) . ?
P3 C79 1.843(8) . ?
P7 C22 1.832(12) . ?
P7 C98 1.795(15) . ?
P7 C104 1.831(12) . ?
P7 Ag3 2.337(4) . ?
C29 C48 1.414(14) . ?
C29 C38 1.415(15) . ?
C12 C17 1.540(15) . ?
C44 C17 1.541(15) . ?
C48 C14 1.365(15) . ?
C3 C65 1.410(16) . ?
C3 C100 1.399(17) . ?
C33 C53 1.547(14) . ?
C22 C53 1.533(16) . ?
C55 C67 1.393(16) . ?
C55 C32 1.413(18) . ?
C34 C63 1.394(17) . ?
C34 C39 1.419(17) . ?
C6 C38 1.380(18) . ?
C6 C28 1.396(19) . ?
C23 C35 1.548(15) . ?
C40 C35 1.553(16) . ?
C11 C92 1.551(17) . ?
C43 C84 1.410(18) . ?
C43 C62 1.434(19) . ?
C63 C93 1.41(2) . ?
C65 C16 1.409(15) . ?
C67 C13 1.416(16) . ?
C69 C80 1.396(19) . ?
C69 C68 1.393(19) . ?
C71 C25 1.370(16) . ?
C71 C46 1.416(17) . ?
C9 C92 1.519(17) . ?
C16 C103 1.404(17) . ?
C25 C111 1.402(17) . ?
C36 C5 1.366(18) . ?
C36 C21 1.407(18) . ?
C8 C42 1.409(18) . ?
C8 C85 1.39(2) . ?
C80 C10 1.398(18) . ?
C47 C86 1.40(2) . ?
C47 C15 1.43(2) . ?
C27 C19 1.40(2) . ?
C27 C49 1.43(2) . ?
C84 C52 1.415(18) . ?
C86 C49 1.361(17) . ?
C88 C90 1.399(16) . ?
C88 C56 1.386(17) . ?
C90 C20 1.402(19) . ?
C94 C83 1.36(3) . ?
C94 C66 1.35(3) . ?
C96 C4 1.37(2) . ?
C96 C26 1.409(17) . ?
C98 C64 1.408(19) . ?
C98 C97 1.407(19) . ?
C100 C24 1.412(19) . ?
C1 C2 1.408(19) . ?
C1 C56 1.426(18) . ?
C103 C24 1.38(2) . ?
C39 C91 1.411(18) . ?
C32 C87 1.37(2) . ?
C37 C95 1.394(17) . ?
C37 C54 1.375(19) . ?
C2 C20 1.40(2) . ?
C7 C18 1.543(18) . ?
C7 C89 1.53(2) . ?
C10 C125 1.39(2) . ?
C13 C109 1.425(18) . ?
C28 C14 1.398(17) . ?
C4 C30 1.40(2) . ?
C5 C66 1.39(2) . ?
C15 C19 1.40(2) . ?
C120 C85 1.40(2) . ?
C120 C78 1.35(2) . ?
C21 C83 1.43(2) . ?
C26 C104 1.406(16) . ?
C42 C99 1.39(2) . ?
C125 C51 1.37(2) . ?
C30 C73 1.419(19) . ?
C62 C122 1.43(3) . ?
C87 C109 1.39(2) . ?
C52 C115 1.39(2) . ?
C64 C102 1.41(2) . ?
C91 C41 1.43(2) . ?
C46 C116 1.44(2) . ?
C93 C41 1.42(2) . ?
C95 C112 1.40(2) . ?
C54 C70 1.440(19) . ?
C97 C77 1.35(3) . ?
C68 C51 1.38(2) . ?
C99 C78 1.41(2) . ?
C101 C111 1.37(2) . ?
C101 C116 1.36(2) . ?
C70 C59 1.36(2) . ?
C102 C50 1.43(3) . ?
O9 Ag3 2.356(7) . ?
O36 C105 1.281(13) . ?
O36 Ag3 2.544(8) . ?
O38 C105 1.231(13) . ?
O17 C72 1.259(12) . ?
C104 C73 1.411(17) . ?
O31 C72 1.265(12) . ?
C72 C107 1.512(15) . ?
C105 C106 1.529(15) . ?
C57 C76 1.52(3) . ?
C57 C117 1.52(2) . ?
C108 C74 1.39(2) . ?
C108 C75 1.395(19) . ?
C74 C58 1.44(2) . ?
C31 C110 1.57(2) . ?
C31 C45 1.49(3) . ?
C75 C113 1.47(2) . ?
C58 C114 1.35(3) . ?
C112 C59 1.37(3) . ?
C113 C114 1.39(3) . ?
C50 C77 1.35(3) . ?
C115 C122 1.44(3) . ?
C118 C79 1.3900 . ?
C118 C81 1.3900 . ?
C79 C119 1.3900 . ?
C119 C60 1.3900 . ?
C60 C121 1.3900 . ?
C121 C81 1.3900 . ?
C123 N1 1.15(3) . ?
C123 C82 1.45(3) . ?
N2 C124 1.16(3) . ?
C124 C61 1.521(18) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O19 W1 O1 173.3(3) . . ?
O19 W1 O3 97.1(3) . . ?
O19 W1 O9 101.0(3) . . ?
O19 W1 O27 98.6(3) . . ?
O19 W1 O26 101.0(3) . 2_666 ?
O3 W1 O1 82.3(2) . . ?
O9 W1 O1 80.2(3) . . ?
O9 W1 O3 161.4(3) . . ?
O9 W1 O27 94.0(3) . . ?
O9 W1 O26 90.5(3) . 2_666 ?
O27 W1 O1 74.7(2) . . ?
O27 W1 O3 87.6(3) . . ?
O27 W1 O26 158.6(2) . 2_666 ?
O26 W1 O1 85.5(2) 2_666 . ?
O26 W1 O3 81.6(2) 2_666 . ?
O21 W4 O20 154.7(3) . 2_666 ?
O21 W4 O2 92.1(3) . . ?
O21 W4 O29 83.2(2) . . ?
O20 W4 O2 81.3(3) 2_666 . ?
O20 W4 O29 71.7(2) 2_666 . ?
O2 W4 O29 81.3(2) . . ?
O6 W4 O21 104.0(3) . . ?
O6 W4 O20 100.9(3) . 2_666 ?
O6 W4 O2 95.6(3) . . ?
O6 W4 O29 172.3(3) . . ?
O6 W4 O24 98.2(3) . . ?
O24 W4 O21 93.0(3) . . ?
O24 W4 O20 87.5(3) . 2_666 ?
O24 W4 O2 163.6(3) . . ?
O24 W4 O29 83.8(2) . . ?
O20 W6 O2 81.3(3) 2_666 2_666 ?
O20 W6 O29 72.5(2) 2_666 . ?
O2 W6 O29 79.4(2) 2_666 . ?
O13 W6 O20 99.6(3) . 2_666 ?
O13 W6 O2 95.4(3) . 2_666 ?
O13 W6 O29 171.0(3) . . ?
O13 W6 O23 99.4(3) . . ?
O13 W6 O26 103.6(3) . 2_666 ?
O23 W6 O20 87.1(3) . 2_666 ?
O23 W6 O2 162.6(3) . 2_666 ?
O23 W6 O29 84.7(2) . . ?
O26 W6 O20 156.6(3) 2_666 2_666 ?
O26 W6 O2 93.0(3) 2_666 2_666 ?
O26 W6 O29 84.1(2) 2_666 . ?
O26 W6 O23 92.4(3) 2_666 . ?
O3 W8 O8 155.3(3) . . ?
O3 W8 O41 83.6(3) . . ?
O3 W8 O23 83.4(3) . . ?
O3 W8 O40 94.4(3) . . ?
O37 W8 O3 103.0(3) . . ?
O37 W8 O8 100.4(3) . . ?
O37 W8 O41 172.9(3) . . ?
O37 W8 O23 99.7(3) . . ?
O37 W8 O40 100.7(3) . . ?
O8 W8 O41 73.4(2) . . ?
O8 W8 O23 85.0(3) . . ?
O23 W8 O41 83.4(2) . . ?
O40 W8 O8 88.9(3) . . ?
O40 W8 O41 76.0(2) . . ?
O40 W8 O23 159.4(3) . . ?
O21 W9 O4 82.7(3) . . ?
O21 W9 O22 85.7(2) . . ?
O5 W9 O21 158.9(3) . . ?
O5 W9 O4 85.4(3) . . ?
O5 W9 O22 75.6(2) . . ?
O11 W9 O21 99.6(3) . . ?
O11 W9 O5 99.1(3) . . ?
O11 W9 O4 97.7(3) . . ?
O11 W9 O14 100.8(3) . . ?
O11 W9 O22 174.7(3) . . ?
O4 W9 O22 82.5(2) . . ?
O14 W9 O21 91.1(3) . . ?
O14 W9 O5 94.8(3) . . ?
O14 W9 O4 161.2(3) . . ?
O14 W9 O22 79.4(3) . . ?
O7 W5 O12 102.9(3) . . ?
O7 W5 O41 169.2(3) . . ?
O7 W5 O32 99.1(3) . . ?
O7 W5 O25 102.7(3) . . ?
O7 W5 O40 99.0(3) . . ?
O12 W5 O41 84.6(2) . . ?
O12 W5 O32 157.7(3) . . ?
O12 W5 O25 91.8(3) . . ?
O12 W5 O40 88.9(3) . . ?
O32 W5 O41 73.2(2) . . ?
O25 W5 O41 84.5(2) . . ?
O25 W5 O32 86.8(3) . . ?
O25 W5 O40 157.6(3) . . ?
O40 W5 O41 73.2(2) . . ?
O40 W5 O32 84.2(3) . . ?
O18 W3 O4 103.3(3) . . ?
O18 W3 O8 99.2(3) . . ?
O18 W3 O41 172.2(3) . . ?
O18 W3 O32 101.9(3) . . ?
O18 W3 O24 98.4(3) . . ?
O4 W3 O8 155.7(3) . . ?
O4 W3 O41 84.5(3) . . ?
O4 W3 O32 94.7(3) . . ?
O4 W3 O24 84.2(3) . . ?
O8 W3 O41 73.2(2) . . ?
O8 W3 O24 83.5(3) . . ?
O32 W3 O8 89.5(3) . . ?
O32 W3 O41 76.8(2) . . ?
O32 W3 O24 159.4(3) . . ?
O24 W3 O41 82.6(2) . . ?
O35 W7 O1 171.1(3) . . ?
O35 W7 O12 94.7(3) . . ?
O35 W7 O30 101.8(3) . . ?
O35 W7 O27 97.9(3) . . ?
O35 W7 O28 102.1(3) . . ?
O12 W7 O1 83.4(2) . . ?
O30 W7 O1 79.9(3) . . ?
O30 W7 O12 163.4(3) . . ?
O30 W7 O27 92.1(3) . . ?
O30 W7 O28 95.5(3) . . ?
O27 W7 O1 73.3(2) . . ?
O27 W7 O12 84.2(3) . . ?
O28 W7 O1 86.3(2) . . ?
O28 W7 O12 82.3(3) . . ?
O28 W7 O27 156.6(3) . . ?
O5 W2 O22 73.7(2) . . ?
O5 W2 O25 86.0(3) . . ?
O15 W2 O5 98.8(3) . . ?
O15 W2 O16 101.8(3) . . ?
O15 W2 O22 172.5(3) . . ?
O15 W2 O25 95.4(3) . . ?
O15 W2 O28 102.9(3) . . ?
O16 W2 O5 92.9(3) . . ?
O16 W2 O22 79.4(2) . . ?
O16 W2 O25 162.7(3) . . ?
O16 W2 O28 92.7(3) . . ?
O25 W2 O22 83.8(2) . . ?
O28 W2 O5 156.0(3) . . ?
O28 W2 O22 84.4(2) . . ?
O28 W2 O25 81.8(3) . . ?
P2 Ag2 S1 171.41(10) . . ?
S1 Ag4 O17 90.4(2) 2_666 . ?
P8 Ag4 S1 137.56(9) . 2_666 ?
P8 Ag4 O16 101.22(17) . . ?
P8 Ag4 O17 130.4(2) . . ?
O16 Ag4 S1 103.10(17) . 2_666 ?
O16 Ag4 O17 71.2(2) . . ?
P6 Ag6 S3 151.89(10) . 2_666 ?
O30 Ag6 S3 93.81(18) . 2_666 ?
O30 Ag6 P6 113.26(18) . . ?
S3 Ag8 Ag7 45.33(17) . 2_666 ?
P3 Ag8 Ag7 133.8(2) . 2_666 ?
P3 Ag8 S3 165.27(11) . . ?
P4 Ag9 Ag1 130.83(8) . . ?
P4 Ag9 S2 159.26(10) . . ?
P4 Ag9 O15 102.84(17) . 2_666 ?
S2 Ag9 Ag1 48.96(8) . . ?
S2 Ag9 O15 94.60(18) . 2_666 ?
O15 Ag9 Ag1 111.05(15) 2_666 . ?
S1 Ag5 O14 80.18(16) . 2_666 ?
P1 Ag5 S1 148.31(10) . . ?
P1 Ag5 O14 115.55(17) . 2_666 ?
S2 Ag1 Ag9 48.97(8) . . ?
S2 Ag1 O35 94.30(18) . 2_666 ?
P5 Ag1 Ag9 130.53(10) . . ?
P5 Ag1 S2 153.25(11) . . ?
P5 Ag1 O35 107.80(19) . 2_666 ?
O35 Ag1 Ag9 110.10(17) 2_666 . ?
S3 Ag7 Ag8 46.9(3) 2_666 2_666 ?
S3 Ag7 P7 156.1(5) 2_666 . ?
S3 Ag7 O9 94.5(3) 2_666 . ?
P7 Ag7 Ag8 135.8(7) . 2_666 ?
P7 Ag7 O9 109.0(4) . . ?
O9 Ag7 Ag8 73.0(3) . 2_666 ?
O20 Co1 O2 72.2(2) . 2_666 ?
O20 Co1 O29 144.4(3) . . ?
O20 Co1 O42 95.2(3) . . ?
O20 Co1 O39 95.4(2) . . ?
O29 Co1 O2 79.3(2) . 2_666 ?
O42 Co1 O2 167.4(2) . 2_666 ?
O42 Co1 O29 112.0(3) . . ?
O39 Co1 O2 99.6(2) . 2_666 ?
O39 Co1 O29 110.3(3) . . ?
O39 Co1 O42 82.0(3) . . ?
O9 Co4 O1 75.6(2) . . ?
O9 Co4 O36 87.6(3) . . ?
O10 Co4 O1 100.3(2) . . ?
O10 Co4 O9 174.9(3) . . ?
O10 Co4 O36 96.9(3) . . ?
O10 Co4 O30 91.1(3) . . ?
O36 Co4 O1 160.8(3) . . ?
O30 Co4 O1 76.0(2) . . ?
O30 Co4 O9 90.9(3) . . ?
O30 Co4 O36 95.3(3) . . ?
O39 Co4 O1 99.0(2) . . ?
O39 Co4 O9 94.2(3) . . ?
O39 Co4 O10 83.3(3) . . ?
O39 Co4 O36 91.4(3) . . ?
O39 Co4 O30 171.7(3) . . ?
O42 Co2 Co3 45.26(19) . . ?
O42 Co2 O10 83.8(3) . . ?
O42 Co2 O14 89.7(3) . . ?
O42 Co2 O16 174.3(3) . . ?
O42 Co2 O17 99.6(3) . . ?
O42 Co2 O22 97.9(2) . . ?
O10 Co2 Co3 44.60(17) . . ?
O10 Co2 O14 171.7(3) . . ?
O10 Co2 O17 90.1(3) . . ?
O10 Co2 O22 101.0(2) . . ?
O14 Co2 Co3 131.45(18) . . ?
O14 Co2 O17 96.1(3) . . ?
O14 Co2 O22 74.6(3) . . ?
O16 Co2 Co3 136.2(2) . . ?
O16 Co2 O10 95.4(3) . . ?
O16 Co2 O14 90.5(3) . . ?
O16 Co2 O17 86.0(3) . . ?
O16 Co2 O22 76.7(2) . . ?
O17 Co2 Co3 78.6(2) . . ?
O17 Co2 O22 160.1(2) . . ?
O22 Co2 Co3 120.80(16) . . ?
O34 Co3 Co2 132.6(3) . . ?
O34 Co3 O42 93.8(3) . . ?
O34 Co3 O39 95.7(3) . . ?
O42 Co3 Co2 42.41(16) . . ?
O42 Co3 O39 76.9(3) . . ?
O10 Co3 Co2 43.29(18) . . ?
O10 Co3 O34 172.6(3) . . ?
O10 Co3 O42 80.0(2) . . ?
O10 Co3 O39 78.9(2) . . ?
O38 Co3 Co2 137.7(2) . . ?
O38 Co3 O34 88.6(3) . . ?
O38 Co3 O42 171.1(3) . . ?
O38 Co3 O10 96.9(3) . . ?
O38 Co3 O39 94.4(3) . . ?
O38 Co3 O31 90.5(3) . . ?
O39 Co3 Co2 90.90(17) . . ?
O31 Co3 Co2 80.78(19) . . ?
O31 Co3 O34 91.4(3) . . ?
O31 Co3 O42 98.0(3) . . ?
O31 Co3 O10 93.5(3) . . ?
O31 Co3 O39 171.4(3) . . ?
O1 Si O29 109.4(3) . . ?
O1 Si O41 109.2(3) . . ?
O41 Si O29 107.8(3) . . ?
O22 Si O1 110.5(3) . . ?
O22 Si O29 110.2(3) . . ?
O22 Si O41 109.7(3) . . ?
Ag2 S1 Ag4 115.56(11) . 2_666 ?
Ag2 S1 Ag5 95.77(10) . . ?
Ag5 S1 Ag4 116.75(10) . 2_666 ?
C7 S1 Ag2 105.9(4) . . ?
C7 S1 Ag4 110.6(4) . 2_666 ?
C7 S1 Ag5 111.0(4) . . ?
C48 P1 Ag5 116.3(3) . . ?
C48 P1 C33 109.9(5) . . ?
C33 P1 Ag5 109.7(3) . . ?
C71 P1 Ag5 111.3(4) . . ?
C71 P1 C48 104.6(5) . . ?
C71 P1 C33 104.3(5) . . ?
Ag6 S3 Ag3 108.54(13) 2_666 2_666 ?
Ag8 S3 Ag6 114.73(11) . 2_666 ?
Ag8 S3 Ag3 93.27(11) . 2_666 ?
Ag7 S3 Ag8 87.8(4) 2_666 . ?
C31 S3 Ag6 111.2(5) . 2_666 ?
C31 S3 Ag8 111.5(5) . . ?
C31 S3 Ag7 113.3(7) . 2_666 ?
C31 S3 Ag3 116.6(6) . 2_666 ?
C12 P4 Ag9 119.2(4) . . ?
C34 P4 Ag9 111.0(4) . . ?
C34 P4 C12 103.1(5) . . ?
C67 P4 Ag9 116.2(4) . . ?
C67 P4 C12 102.5(5) . . ?
C67 P4 C34 102.9(5) . . ?
C40 P6 Ag6 118.2(5) . . ?
C36 P6 Ag6 111.5(4) . . ?
C36 P6 C40 103.2(6) . . ?
C36 P6 C88 107.4(6) . . ?
C88 P6 Ag6 112.7(4) . . ?
C88 P6 C40 102.7(6) . . ?
C23 P8 Ag4 113.5(4) . . ?
C65 P8 Ag4 112.5(4) . . ?
C65 P8 C23 101.7(5) . . ?
C108 P8 Ag4 116.3(4) . . ?
C108 P8 C23 106.5(6) . . ?
C108 P8 C65 105.0(5) . . ?
C44 P2 Ag2 110.0(4) . . ?
C43 P2 Ag2 118.7(4) . . ?
C43 P2 C44 102.6(5) . . ?
C43 P2 C37 104.5(6) . . ?
C37 P2 Ag2 115.4(4) . . ?
C37 P2 C44 103.9(5) . . ?
Ag1 S2 Ag9 82.07(10) . . ?
C57 S2 Ag9 104.8(5) . . ?
C57 S2 Ag1 100.6(6) . . ?
C11 P5 Ag1 117.4(4) . . ?
C69 P5 Ag1 117.7(5) . . ?
C69 P5 C11 104.1(6) . . ?
C86 P5 Ag1 110.7(5) . . ?
C86 P5 C11 102.6(6) . . ?
C86 P5 C69 102.4(6) . . ?
C9 P3 Ag8 113.0(4) . . ?
C8 P3 Ag8 116.3(4) . . ?
C8 P3 C9 107.1(6) . . ?
C8 P3 C79 100.5(6) . . ?
C79 P3 Ag8 113.3(4) . . ?
C79 P3 C9 105.3(7) . . ?
C22 P7 Ag7 118.4(4) . . ?
C22 P7 Ag3 115.3(4) . . ?
C98 P7 Ag7 105.3(6) . . ?
C98 P7 C22 102.9(6) . . ?
C98 P7 C104 104.2(5) . . ?
C98 P7 Ag3 115.4(4) . . ?
C104 P7 Ag7 123.1(5) . . ?
C104 P7 C22 100.5(5) . . ?
C104 P7 Ag3 116.5(4) . . ?
W4 O21 W9 149.2(4) . . ?
W4 O20 W6 122.3(3) 2_666 2_666 ?
W4 O20 Co1 103.3(3) 2_666 . ?
W6 O20 Co1 104.3(3) 2_666 . ?
W4 O2 W6 161.7(3) . 2_666 ?
W4 O2 Co1 91.9(3) . 2_666 ?
W6 O2 Co1 100.6(2) 2_666 2_666 ?
W9 O5 W2 119.2(3) . . ?
W7 O35 Ag1 117.1(3) . 2_666 ?
W2 O15 Ag9 115.8(3) . 2_666 ?
C48 C29 C38 116.4(10) . . ?
C17 C12 P4 112.0(7) . . ?
C17 C44 P2 111.9(8) . . ?
C12 C17 C44 107.4(9) . . ?
C29 C48 P1 120.5(8) . . ?
C14 C48 P1 116.7(8) . . ?
C14 C48 C29 122.5(10) . . ?
C100 C3 C65 119.6(11) . . ?
C53 C33 P1 117.0(8) . . ?
C53 C22 P7 115.9(8) . . ?
C22 C53 C33 105.3(9) . . ?
C67 C55 C32 119.7(12) . . ?
C63 C34 P4 119.2(10) . . ?
C63 C34 C39 121.2(11) . . ?
C39 C34 P4 119.5(9) . . ?
C38 C6 C28 119.2(12) . . ?
C35 C23 P8 110.2(8) . . ?
C35 C40 P6 113.3(8) . . ?
C92 C11 P5 108.0(8) . . ?
C84 C43 P2 119.4(9) . . ?
C84 C43 C62 120.9(13) . . ?
C62 C43 P2 119.6(12) . . ?
C34 C63 C93 118.9(14) . . ?
C3 C65 P8 117.0(8) . . ?
C16 C65 P8 122.3(9) . . ?
C16 C65 C3 120.6(10) . . ?
C55 C67 P4 121.7(9) . . ?
C55 C67 C13 120.5(11) . . ?
C13 C67 P4 117.7(9) . . ?
C80 C69 P5 120.7(10) . . ?
C68 C69 P5 119.4(12) . . ?
C68 C69 C80 119.8(13) . . ?
C25 C71 P1 123.6(9) . . ?
C25 C71 C46 119.5(11) . . ?
C46 C71 P1 116.9(9) . . ?
C23 C35 C40 109.0(9) . . ?
C6 C38 C29 122.0(11) . . ?
C92 C9 P3 107.9(8) . . ?
C103 C16 C65 118.4(12) . . ?
C71 C25 C111 121.3(12) . . ?
C5 C36 P6 117.3(10) . . ?
C5 C36 C21 119.7(12) . . ?
C21 C36 P6 122.9(11) . . ?
C42 C8 P3 117.2(10) . . ?
C85 C8 P3 124.0(12) . . ?
C85 C8 C42 118.8(14) . . ?
C69 C80 C10 119.4(14) . . ?
C86 C47 C15 121.0(14) . . ?
C19 C27 C49 118.4(13) . . ?
C43 C84 C52 122.1(13) . . ?
C47 C86 P5 120.3(10) . . ?
C49 C86 P5 118.7(11) . . ?
C49 C86 C47 121.0(13) . . ?
C90 C88 P6 117.0(10) . . ?
C56 C88 P6 122.0(9) . . ?
C56 C88 C90 120.6(12) . . ?
C88 C90 C20 120.8(13) . . ?
C9 C92 C11 109.9(10) . . ?
C66 C94 C83 119.4(16) . . ?
C4 C96 C26 121.5(12) . . ?
C64 C98 P7 122.4(10) . . ?
C97 C98 P7 119.7(12) . . ?
C97 C98 C64 117.8(15) . . ?
C3 C100 C24 120.1(13) . . ?
C2 C1 C56 118.5(12) . . ?
C24 C103 C16 121.8(12) . . ?
C91 C39 C34 120.4(14) . . ?
C87 C32 C55 120.6(14) . . ?
C95 C37 P2 121.4(11) . . ?
C54 C37 P2 119.4(9) . . ?
C54 C37 C95 119.2(12) . . ?
C20 C2 C1 121.7(13) . . ?
C18 C7 S1 111.1(8) . . ?
C89 C7 S1 109.3(9) . . ?
C89 C7 C18 112.0(11) . . ?
C125 C10 C80 120.0(15) . . ?
C67 C13 C109 118.1(12) . . ?
C103 C24 C100 119.5(12) . . ?
C6 C28 C14 120.5(12) . . ?
C96 C4 C30 121.2(13) . . ?
C36 C5 C66 121.0(17) . . ?
C19 C15 C47 116.8(16) . . ?
C15 C19 C27 122.7(15) . . ?
C2 C20 C90 118.6(12) . . ?
C78 C120 C85 121.7(15) . . ?
C48 C14 C28 119.4(11) . . ?
C36 C21 C83 116.7(17) . . ?
C104 C26 C96 118.6(12) . . ?
C99 C42 C8 120.5(14) . . ?
C51 C125 C10 119.9(14) . . ?
C94 C83 C21 121.9(18) . . ?
C4 C30 C73 117.6(14) . . ?
C8 C85 C120 119.7(16) . . ?
C122 C62 C43 116.2(18) . . ?
C32 C87 C109 120.5(13) . . ?
C115 C52 C84 117.9(16) . . ?
C102 C64 C98 119.3(16) . . ?
C39 C91 C41 118.6(15) . . ?
C71 C46 C116 118.0(13) . . ?
C63 C93 C41 121.0(14) . . ?
C94 C66 C5 121(2) . . ?
C37 C95 C112 119.8(15) . . ?
C37 C54 C70 120.2(14) . . ?
C77 C97 C98 123.0(19) . . ?
C51 C68 C69 119.7(17) . . ?
C42 C99 C78 119.5(16) . . ?
C93 C41 C91 119.9(14) . . ?
C116 C101 C111 120.1(14) . . ?
C59 C70 C54 119.2(17) . . ?
C64 C102 C50 119.2(17) . . ?
W1 O1 W7 92.0(2) . . ?
Co4 O1 W1 89.6(2) . . ?
Co4 O1 W7 89.1(2) . . ?
Si O1 W1 126.2(3) . . ?
Si O1 W7 124.4(3) . . ?
Si O1 Co4 124.6(3) . . ?
W8 O3 W1 158.1(4) . . ?
W3 O4 W9 156.5(3) . . ?
W8 O8 W3 120.4(3) . . ?
W1 O9 Ag7 130.7(6) . . ?
W1 O9 Co4 114.4(3) . . ?
W1 O9 Ag3 139.6(4) . . ?
Co4 O9 Ag7 110.2(5) . . ?
Co4 O9 Ag3 103.9(3) . . ?
W5 O12 W7 148.2(4) . . ?
W6 O29 W4 93.2(2) . . ?
Co1 O29 W4 97.2(2) . . ?
Co1 O29 W6 98.9(2) . . ?
Si O29 W4 121.5(3) . . ?
Si O29 W6 123.0(3) . . ?
Si O29 Co1 117.2(3) . . ?
W8 O41 W5 90.6(2) . . ?
W3 O41 W8 92.5(2) . . ?
W3 O41 W5 90.6(2) . . ?
Si O41 W8 125.6(3) . . ?
Si O41 W5 122.2(3) . . ?
Si O41 W3 125.2(3) . . ?
W3 O32 W5 119.5(3) . . ?
Co1 O42 Co3 97.9(3) . . ?
Co2 O42 Co1 122.2(3) . . ?
Co2 O42 Co3 92.3(2) . . ?
W4 O24 W3 148.6(4) . . ?
Co4 O10 Co2 127.7(3) . . ?
Co4 O10 Co3 93.4(3) . . ?
Co2 O10 Co3 92.1(3) . . ?
Co4 O36 Ag3 96.0(3) . . ?
C105 O36 Co4 126.9(7) . . ?
C105 O36 Ag3 120.3(6) . . ?
W9 O14 Ag5 124.3(3) . 2_666 ?
W9 O14 Co2 115.2(3) . . ?
Co2 O14 Ag5 120.4(3) . 2_666 ?
W7 O30 Ag6 132.7(3) . . ?
W7 O30 Co4 115.0(3) . . ?
Co4 O30 Ag6 110.2(3) . . ?
W2 O16 Ag4 133.3(3) . . ?
W2 O16 Co2 115.5(3) . . ?
Co2 O16 Ag4 101.3(3) . . ?
C105 O38 Co3 126.0(7) . . ?
Co2 O17 Ag4 96.0(3) . . ?
C72 O17 Ag4 131.4(6) . . ?
C72 O17 Co2 127.9(7) . . ?
W9 O22 W2 90.9(2) . . ?
Co2 O22 W9 90.5(2) . . ?
Co2 O22 W2 88.4(2) . . ?
Si O22 W9 126.1(3) . . ?
Si O22 W2 124.9(3) . . ?
Si O22 Co2 124.9(3) . . ?
C88 C56 C1 119.8(12) . . ?
C26 C104 P7 119.9(9) . . ?
C26 C104 C73 119.5(11) . . ?
C73 C104 P7 120.4(9) . . ?
W6 O23 W8 148.6(3) . . ?
Co1 O39 Co4 122.9(3) . . ?
Co1 O39 Co3 98.1(3) . . ?
Co4 O39 Co3 93.0(3) . . ?
W5 O25 W2 148.9(3) . . ?
C72 O31 Co3 126.1(7) . . ?
O17 C72 O31 126.0(9) . . ?
O17 C72 C107 117.3(10) . . ?
O31 C72 C107 116.8(10) . . ?
O36 C105 C106 116.0(11) . . ?
O38 C105 O36 126.9(10) . . ?
O38 C105 C106 117.1(11) . . ?
C86 C49 C27 120.0(14) . . ?
C104 C73 C30 121.1(12) . . ?
W1 O27 W7 119.4(3) . . ?
W8 O40 W5 120.1(3) . . ?
W7 O28 W2 157.8(4) . . ?
C76 C57 S2 113.4(11) . . ?
C76 C57 C117 108.4(17) . . ?
C117 C57 S2 109.1(11) . . ?
C74 C108 P8 116.7(10) . . ?
C74 C108 C75 121.9(14) . . ?
C75 C108 P8 121.3(12) . . ?
C108 C74 C58 120.1(15) . . ?
C87 C109 C13 120.5(12) . . ?
C110 C31 S3 105.7(10) . . ?
C45 C31 S3 113.2(11) . . ?
C45 C31 C110 122.3(15) . . ?
C108 C75 C113 116.4(17) . . ?
C101 C111 C25 120.2(14) . . ?
C114 C58 C74 119(2) . . ?
C59 C112 C95 120.6(15) . . ?
C114 C113 C75 120.2(17) . . ?
C77 C50 C102 120.3(17) . . ?
C58 C114 C113 122.3(19) . . ?
C97 C77 C50 120(2) . . ?
C52 C115 C122 120.8(17) . . ?
C70 C59 C112 120.8(14) . . ?
C101 C116 C46 120.9(14) . . ?
C120 C78 C99 119.4(15) . . ?
C79 C118 C81 120.0 . . ?
C118 C79 P3 121.9(7) . . ?
C118 C79 C119 120.0 . . ?
C119 C79 P3 117.9(7) . . ?
C60 C119 C79 120.0 . . ?
C119 C60 C121 120.0 . . ?
C81 C121 C60 120.0 . . ?
C121 C81 C118 120.0 . . ?
C62 C122 C115 121.7(18) . . ?
C125 C51 C68 121.1(16) . . ?
P7 Ag3 S3 142.5(2) . 2_666 ?
P7 Ag3 O9 117.0(2) . . ?
P7 Ag3 O36 128.5(3) . . ?
O9 Ag3 S3 90.2(2) . 2_666 ?
O9 Ag3 O36 72.4(2) . . ?
O36 Ag3 S3 82.60(19) . 2_666 ?
W6 O26 W1 149.3(3) 2_666 2_666 ?
N1 C123 C82 174(3) . . ?
N2 C124 C61 179(3) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Ag2 S1 C7 C18 43.5(10) . . . . ?
Ag2 S1 C7 C89 167.6(9) . . . . ?
Ag2 P2 C44 C17 -62.5(7) . . . . ?
Ag2 P2 C43 C84 -69.2(11) . . . . ?
Ag2 P2 C43 C62 107.5(13) . . . . ?
Ag2 P2 C37 C95 166.9(12) . . . . ?
Ag2 P2 C37 C54 -10.6(14) . . . . ?
Ag4 S1 C7 C18 169.4(8) 2_666 . . . ?
Ag4 S1 C7 C89 -66.5(10) 2_666 . . . ?
Ag4 P8 C23 C35 59.8(9) . . . . ?
Ag4 P8 C65 C3 37.0(10) . . . . ?
Ag4 P8 C65 C16 -140.0(9) . . . . ?
Ag4 P8 C108 C74 19.2(11) . . . . ?
Ag4 P8 C108 C75 -157.2(9) . . . . ?
Ag4 O17 C72 O31 154.7(8) . . . . ?
Ag4 O17 C72 C107 -24.7(16) . . . . ?
Ag6 S3 C31 C110 70.2(12) 2_666 . . . ?
Ag6 S3 C31 C45 -153.4(15) 2_666 . . . ?
Ag6 P6 C40 C35 -76.1(10) . . . . ?
Ag6 P6 C36 C5 22.7(12) . . . . ?
Ag6 P6 C36 C21 -154.5(11) . . . . ?
Ag6 P6 C88 C90 19.6(10) . . . . ?
Ag6 P6 C88 C56 -167.4(9) . . . . ?
Ag8 S3 C31 C110 -160.4(9) . . . . ?
Ag8 S3 C31 C45 -24.0(18) . . . . ?
Ag8 P3 C9 C92 56.0(9) . . . . ?
Ag8 P3 C8 C42 -27.3(13) . . . . ?
Ag8 P3 C8 C85 154.3(11) . . . . ?
Ag8 P3 C79 C118 161.2(9) . . . . ?
Ag8 P3 C79 C119 -23.9(11) . . . . ?
Ag9 P4 C12 C17 72.7(8) . . . . ?
Ag9 P4 C34 C63 -11.9(11) . . . . ?
Ag9 P4 C34 C39 172.2(9) . . . . ?
Ag9 P4 C67 C55 113.0(10) . . . . ?
Ag9 P4 C67 C13 -68.2(10) . . . . ?
Ag9 S2 C57 C76 -42.3(13) . . . . ?
Ag9 S2 C57 C117 -163.3(13) . . . . ?
Ag5 S1 C7 C18 -59.3(10) . . . . ?
Ag5 S1 C7 C89 64.8(10) . . . . ?
Ag5 P1 C48 C29 -118.9(8) . . . . ?
Ag5 P1 C48 C14 54.9(10) . . . . ?
Ag5 P1 C33 C53 -165.6(7) . . . . ?
Ag5 P1 C71 C25 -138.7(10) . . . . ?
Ag5 P1 C71 C46 43.1(12) . . . . ?
Ag1 S2 C57 C76 42.2(13) . . . . ?
Ag1 S2 C57 C117 -78.8(14) . . . . ?
Ag1 P5 C11 C92 -65.3(10) . . . . ?
Ag1 P5 C69 C80 -93.0(11) . . . . ?
Ag1 P5 C69 C68 85.1(13) . . . . ?
Ag1 P5 C86 C47 -175.9(12) . . . . ?
Ag1 P5 C86 C49 7.6(12) . . . . ?
Ag7 S3 C31 C110 -63.2(12) 2_666 . . . ?
Ag7 S3 C31 C45 73.2(18) 2_666 . . . ?
Ag7 P7 C22 C53 -55.5(11) . . . . ?
Ag7 P7 C98 C64 174.3(11) . . . . ?
Ag7 P7 C98 C97 -6.1(11) . . . . ?
Ag7 P7 C104 C26 92.5(11) . . . . ?
Ag7 P7 C104 C73 -91.7(12) . . . . ?
Co4 O36 C105 O38 10.4(16) . . . . ?
Co4 O36 C105 C106 -169.8(8) . . . . ?
Co2 O17 C72 O31 4.7(17) . . . . ?
Co2 O17 C72 C107 -174.7(8) . . . . ?
Co3 O38 C105 O36 -14.4(16) . . . . ?
Co3 O38 C105 C106 165.8(9) . . . . ?
Co3 O31 C72 O17 -9.9(17) . . . . ?
Co3 O31 C72 C107 169.6(8) . . . . ?
P1 C48 C14 C28 -175.7(10) . . . . ?
P1 C33 C53 C22 139.3(8) . . . . ?
P1 C71 C25 C111 -179.9(12) . . . . ?
P1 C71 C46 C116 178.3(14) . . . . ?
P4 C12 C17 C44 171.7(6) . . . . ?
P4 C34 C63 C93 -176.2(10) . . . . ?
P4 C34 C39 C91 173.7(10) . . . . ?
P4 C67 C13 C109 -177.1(9) . . . . ?
P6 C40 C35 C23 -173.6(9) . . . . ?
P6 C36 C5 C66 -178.7(13) . . . . ?
P6 C36 C21 C83 179.6(11) . . . . ?
P6 C88 C90 C20 173.3(9) . . . . ?
P6 C88 C56 C1 -172.2(9) . . . . ?
P8 C23 C35 C40 145.1(10) . . . . ?
P8 C65 C16 C103 177.7(9) . . . . ?
P8 C108 C74 C58 179.4(12) . . . . ?
P8 C108 C75 C113 -179.0(10) . . . . ?
P2 C44 C17 C12 -176.8(6) . . . . ?
P2 C43 C84 C52 -175.5(11) . . . . ?
P2 C43 C62 C122 179.3(16) . . . . ?
P2 C37 C95 C112 179.4(15) . . . . ?
P2 C37 C54 C70 178.0(15) . . . . ?
P5 C11 C92 C9 -174.8(8) . . . . ?
P5 C69 C80 C10 -178.8(9) . . . . ?
P5 C69 C68 C51 177.4(14) . . . . ?
P5 C86 C49 C27 178.0(9) . . . . ?
P3 C9 C92 C11 170.7(8) . . . . ?
P3 C8 C42 C99 -175.5(15) . . . . ?
P3 C8 C85 C120 176.5(12) . . . . ?
P3 C79 C119 C60 -175.0(13) . . . . ?
P7 C22 C53 C33 173.6(8) . . . . ?
P7 C98 C64 C102 179.3(12) . . . . ?
P7 C98 C97 C77 -179.8(13) . . . . ?
P7 C104 C73 C30 -175.3(11) . . . . ?
O21 W4 O24 W3 -14.1(7) . . . . ?
O21 W9 O14 Ag5 93.7(3) . . . 2_666 ?
O21 W9 O14 Co2 -89.9(3) . . . . ?
O20 W4 O21 W9 -72.6(10) 2_666 . . . ?
O20 W4 O24 W3 140.5(7) 2_666 . . . ?
O20 W6 O23 W8 -138.0(7) 2_666 . . . ?
O2 W4 O21 W9 -146.5(7) . . . . ?
O2 W4 O24 W3 93.9(11) . . . . ?
O2 W6 O23 W8 -89.6(11) 2_666 . . . ?
O5 W9 O14 Ag5 -106.6(4) . . . 2_666 ?
O5 W9 O14 Co2 69.8(3) . . . . ?
O5 W2 O15 Ag9 109.2(3) . . . 2_666 ?
O5 W2 O16 Ag4 66.0(5) . . . . ?
O5 W2 O16 Co2 -72.5(4) . . . . ?
O11 W9 O14 Ag5 -6.4(4) . . . 2_666 ?
O11 W9 O14 Co2 170.0(3) . . . . ?
O35 W7 O30 Ag6 9.4(5) . . . . ?
O35 W7 O30 Co4 170.6(4) . . . . ?
O35 W7 O28 W2 -137.8(10) . . . . ?
O6 W4 O21 W9 117.2(7) . . . . ?
O6 W4 O24 W3 -118.8(7) . . . . ?
O7 W5 O12 W7 -123.5(6) . . . . ?
O7 W5 O25 W2 123.9(7) . . . . ?
O15 W2 O16 Ag4 -33.7(5) . . . . ?
O15 W2 O16 Co2 -172.2(4) . . . . ?
O18 W3 O4 W9 -130.4(10) . . . . ?
O18 W3 O32 W5 174.4(4) . . . . ?
C29 C48 C14 C28 -2.1(18) . . . . ?
C12 P4 C34 C63 116.9(10) . . . . ?
C12 P4 C34 C39 -59.1(11) . . . . ?
C12 P4 C67 C55 -18.8(11) . . . . ?
C12 P4 C67 C13 160.0(9) . . . . ?
C44 P2 C43 C84 52.2(11) . . . . ?
C44 P2 C43 C62 -131.1(13) . . . . ?
C44 P2 C37 C95 46.4(14) . . . . ?
C44 P2 C37 C54 -131.1(13) . . . . ?
C48 P1 C33 C53 65.3(9) . . . . ?
C48 P1 C71 C25 -12.3(13) . . . . ?
C48 P1 C71 C46 169.5(11) . . . . ?
C48 C29 C38 C6 -1.0(18) . . . . ?
C3 C65 C16 C103 0.9(18) . . . . ?
C3 C100 C24 C103 -1(2) . . . . ?
C33 P1 C48 C29 6.5(10) . . . . ?
C33 P1 C48 C14 -179.7(9) . . . . ?
C33 P1 C71 C25 103.1(12) . . . . ?
C33 P1 C71 C46 -75.1(12) . . . . ?
C22 P7 C98 C64 49.6(12) . . . . ?
C22 P7 C98 C97 -130.8(11) . . . . ?
C22 P7 C104 C26 -133.1(10) . . . . ?
C22 P7 C104 C73 42.7(12) . . . . ?
C55 C67 C13 C109 1.8(18) . . . . ?
C55 C32 C87 C109 1(2) . . . . ?
C34 P4 C12 C17 -50.8(8) . . . . ?
C34 P4 C67 C55 -125.6(10) . . . . ?
C34 P4 C67 C13 53.3(10) . . . . ?
C34 C63 C93 C41 2(2) . . . . ?
C34 C39 C91 C41 3(2) . . . . ?
C6 C28 C14 C48 1(2) . . . . ?
C23 P8 C65 C3 -84.8(10) . . . . ?
C23 P8 C65 C16 98.3(11) . . . . ?
C23 P8 C108 C74 146.9(10) . . . . ?
C23 P8 C108 C75 -29.5(12) . . . . ?
C40 P6 C36 C5 150.6(11) . . . . ?
C40 P6 C36 C21 -26.6(13) . . . . ?
C40 P6 C88 C90 -108.7(9) . . . . ?
C40 P6 C88 C56 64.3(11) . . . . ?
C11 P5 C69 C80 38.8(12) . . . . ?
C11 P5 C69 C68 -143.1(13) . . . . ?
C11 P5 C86 C47 58.1(14) . . . . ?
C11 P5 C86 C49 -118.4(11) . . . . ?
C43 P2 C44 C17 170.2(7) . . . . ?
C43 P2 C37 C95 -60.8(14) . . . . ?
C43 P2 C37 C54 121.7(13) . . . . ?
C43 C84 C52 C115 -6(2) . . . . ?
C43 C62 C122 C115 -1(3) . . . . ?
C63 C34 C39 C91 -2.2(19) . . . . ?
C63 C93 C41 C91 -2(2) . . . . ?
C65 P8 C23 C35 -179.2(8) . . . . ?
C65 P8 C108 C74 -105.8(10) . . . . ?
C65 P8 C108 C75 77.8(11) . . . . ?
C65 C3 C100 C24 1.6(19) . . . . ?
C65 C16 C103 C24 -0.7(19) . . . . ?
C67 P4 C12 C17 -157.4(7) . . . . ?
C67 P4 C34 C63 -136.7(10) . . . . ?
C67 P4 C34 C39 47.3(11) . . . . ?
C67 C55 C32 C87 -1(2) . . . . ?
C67 C13 C109 C87 -1.5(19) . . . . ?
C69 P5 C11 C92 162.7(9) . . . . ?
C69 P5 C86 C47 -49.5(14) . . . . ?
C69 P5 C86 C49 133.9(11) . . . . ?
C69 C80 C10 C125 -0.4(19) . . . . ?
C69 C68 C51 C125 3(3) . . . . ?
C71 P1 C48 C29 118.0(9) . . . . ?
C71 P1 C48 C14 -68.2(10) . . . . ?
C71 P1 C33 C53 -46.3(9) . . . . ?
C71 C25 C111 C101 2(3) . . . . ?
C71 C46 C116 C101 1(3) . . . . ?
C38 C29 C48 P1 175.6(9) . . . . ?
C38 C29 C48 C14 2.2(17) . . . . ?
C38 C6 C28 C14 0(2) . . . . ?
C9 P3 C8 C42 -154.8(11) . . . . ?
C9 P3 C8 C85 26.8(13) . . . . ?
C9 P3 C79 C118 -74.8(11) . . . . ?
C9 P3 C79 C119 100.1(10) . . . . ?
C16 C103 C24 C100 1(2) . . . . ?
C25 C71 C46 C116 0(2) . . . . ?
C36 P6 C40 C35 160.3(10) . . . . ?
C36 P6 C88 C90 142.9(9) . . . . ?
C36 P6 C88 C56 -44.1(11) . . . . ?
C36 C5 C66 C94 2(3) . . . . ?
C36 C21 C83 C94 -4(3) . . . . ?
C8 P3 C9 C92 -174.6(8) . . . . ?
C8 P3 C79 C118 36.4(11) . . . . ?
C8 P3 C79 C119 -148.7(10) . . . . ?
C8 C42 C99 C78 1(3) . . . . ?
C80 C69 C68 C51 -4(3) . . . . ?
C80 C10 C125 C51 -1(2) . . . . ?
C47 C86 C49 C27 1(2) . . . . ?
C47 C15 C19 C27 -1(3) . . . . ?
C84 C43 C62 C122 -4(3) . . . . ?
C84 C52 C115 C122 1(3) . . . . ?
C86 P5 C11 C92 56.3(10) . . . . ?
C86 P5 C69 C80 145.3(11) . . . . ?
C86 P5 C69 C68 -36.5(14) . . . . ?
C86 C47 C15 C19 4(3) . . . . ?
C88 P6 C40 C35 48.7(11) . . . . ?
C88 P6 C36 C5 -101.3(12) . . . . ?
C88 P6 C36 C21 81.5(13) . . . . ?
C88 C90 C20 C2 -0.2(18) . . . . ?
C90 C88 C56 C1 0.5(18) . . . . ?
C96 C4 C30 C73 -7(2) . . . . ?
C96 C26 C104 P7 176.7(10) . . . . ?
C96 C26 C104 C73 0.9(19) . . . . ?
C98 P7 C22 C53 60.1(10) . . . . ?
C98 P7 C104 C26 -26.8(11) . . . . ?
C98 P7 C104 C73 149.0(11) . . . . ?
C98 C64 C102 C50 -1(2) . . . . ?
C98 C97 C77 C50 2(3) . . . . ?
C100 C3 C65 P8 -178.3(9) . . . . ?
C100 C3 C65 C16 -1.3(18) . . . . ?
C1 C2 C20 C90 -0.5(19) . . . . ?
C39 C34 C63 C93 -0.3(19) . . . . ?
C39 C91 C41 C93 -1(2) . . . . ?
C32 C55 C67 P4 178.2(10) . . . . ?
C32 C55 C67 C13 -0.6(19) . . . . ?
C32 C87 C109 C13 0(2) . . . . ?
C37 P2 C44 C17 61.6(8) . . . . ?
C37 P2 C43 C84 160.4(10) . . . . ?
C37 P2 C43 C62 -22.8(14) . . . . ?
C37 C95 C112 C59 4(3) . . . . ?
C37 C54 C70 C59 1(3) . . . . ?
C2 C1 C56 C88 -1.3(19) . . . . ?
C10 C125 C51 C68 0(3) . . . . ?
C28 C6 C38 C29 0(2) . . . . ?
C4 C96 C26 C104 -5(2) . . . . ?
C4 C30 C73 C104 2(2) . . . . ?
C5 C36 C21 C83 2(2) . . . . ?
C15 C47 C86 P5 178.9(14) . . . . ?
C15 C47 C86 C49 -5(3) . . . . ?
C19 C27 C49 C86 1.8(19) . . . . ?
C21 C36 C5 C66 -1(2) . . . . ?
C26 C96 C4 C30 8(2) . . . . ?
C26 C104 C73 C30 0(2) . . . . ?
C42 C8 C85 C120 -2(2) . . . . ?
C42 C99 C78 C120 -5(3) . . . . ?
C83 C94 C66 C5 -4(3) . . . . ?
C85 C8 C42 C99 3(3) . . . . ?
C85 C120 C78 C99 6(3) . . . . ?
C62 C43 C84 C52 8(2) . . . . ?
C52 C115 C122 C62 3(4) . . . . ?
C64 C98 C97 C77 0(2) . . . . ?
C64 C102 C50 C77 3(3) . . . . ?
C46 C71 C25 C111 -2(2) . . . . ?
C66 C94 C83 C21 5(3) . . . . ?
C95 C37 C54 C70 0(3) . . . . ?
C95 C112 C59 C70 -3(4) . . . . ?
C54 C37 C95 C112 -3(3) . . . . ?
C54 C70 C59 C112 0(4) . . . . ?
C97 C98 C64 C102 0(2) . . . . ?
C68 C69 C80 C10 3(2) . . . . ?
C102 C50 C77 C97 -3(3) . . . . ?
O1 W1 O9 Ag7 155.8(5) . . . . ?
O1 W1 O9 Co4 3.0(3) . . . . ?
O1 W1 O9 Ag3 163.1(5) . . . . ?
O1 W7 O30 Ag6 -161.7(5) . . . . ?
O1 W7 O30 Co4 -0.5(3) . . . . ?
O1 W7 O28 W2 39.3(10) . . . . ?
O1 Si O29 W4 178.2(3) . . . . ?
O1 Si O29 W6 59.8(4) . . . . ?
O1 Si O29 Co1 -63.0(4) . . . . ?
O1 Si O41 W8 -57.4(4) . . . . ?
O1 Si O41 W5 60.4(4) . . . . ?
O1 Si O41 W3 177.7(3) . . . . ?
O1 Si O22 W9 177.7(3) . . . . ?
O1 Si O22 W2 -60.2(5) . . . . ?
O1 Si O22 Co2 56.3(5) . . . . ?
O19 W1 O9 Ag7 -17.5(5) . . . . ?
O19 W1 O9 Co4 -170.3(3) . . . . ?
O19 W1 O9 Ag3 -10.2(6) . . . . ?
O3 W1 O9 Ag7 176.6(6) . . . . ?
O3 W1 O9 Co4 23.8(10) . . . . ?
O3 W1 O9 Ag3 -176.1(6) . . . . ?
O3 W8 O40 W5 79.3(4) . . . . ?
O4 W9 O14 Ag5 163.7(6) . . . 2_666 ?
O4 W9 O14 Co2 -19.9(10) . . . . ?
O4 W3 O32 W5 -81.0(4) . . . . ?
O37 W8 O3 W1 131.7(10) . . . . ?
O37 W8 O40 W5 -176.6(4) . . . . ?
O8 W8 O3 W1 -29.3(14) . . . . ?
O8 W8 O40 W5 -76.1(4) . . . . ?
O8 W3 O4 W9 26.8(15) . . . . ?
O8 W3 O32 W5 75.1(4) . . . . ?
O12 W5 O25 W2 20.2(7) . . . . ?
O12 W7 O35 Ag1 -22.2(4) . . . 2_666 ?
O12 W7 O30 Ag6 -165.5(7) . . . . ?
O12 W7 O30 Co4 -4.3(12) . . . . ?
O12 W7 O28 W2 -44.5(10) . . . . ?
O13 W6 O23 W8 122.7(7) . . . . ?
O29 W4 O21 W9 -65.5(7) . . . . ?
O29 W4 O24 W3 68.6(7) . . . . ?
O29 W6 O23 W8 -65.3(7) . . . . ?
O29 Si O1 W1 -56.8(5) . . . . ?
O29 Si O1 W7 179.5(4) . . . . ?
O29 Si O1 Co4 62.7(5) . . . . ?
O29 Si O41 W8 61.3(5) . . . . ?
O29 Si O41 W5 179.1(3) . . . . ?
O29 Si O41 W3 -63.6(4) . . . . ?
O29 Si O22 W9 56.8(5) . . . . ?
O29 Si O22 W2 178.8(3) . . . . ?
O29 Si O22 Co2 -64.7(5) . . . . ?
O41 W8 O3 W1 -50.9(10) . . . . ?
O41 W8 O40 W5 -3.0(3) . . . . ?
O41 W5 O12 W7 64.3(6) . . . . ?
O41 W5 O25 W2 -64.1(7) . . . . ?
O41 W3 O4 W9 50.1(10) . . . . ?
O41 W3 O32 W5 2.3(3) . . . . ?
O41 Si O1 W1 60.9(4) . . . . ?
O41 Si O1 W7 -62.8(5) . . . . ?
O41 Si O1 Co4 -179.5(3) . . . . ?
O41 Si O29 W4 59.6(5) . . . . ?
O41 Si O29 W6 -58.7(4) . . . . ?
O41 Si O29 Co1 178.4(3) . . . . ?
O41 Si O22 W9 -61.8(4) . . . . ?
O41 Si O22 W2 60.2(5) . . . . ?
O41 Si O22 Co2 176.8(3) . . . . ?
O32 W5 O12 W7 66.0(11) . . . . ?
O32 W5 O25 W2 -137.5(7) . . . . ?
O32 W3 O4 W9 126.2(10) . . . . ?
O24 W4 O21 W9 17.9(7) . . . . ?
O24 W3 O4 W9 -33.1(10) . . . . ?
O24 W3 O32 W5 5.1(10) . . . . ?
O30 W7 O35 Ag1 159.2(3) . . . 2_666 ?
O30 W7 O28 W2 118.9(10) . . . . ?
O16 W2 O15 Ag9 -155.9(3) . . . 2_666 ?
O22 W9 O14 Ag5 179.1(4) . . . 2_666 ?
O22 W9 O14 Co2 -4.5(3) . . . . ?
O22 W2 O16 Ag4 138.7(5) . . . . ?
O22 W2 O16 Co2 0.2(3) . . . . ?
O22 Si O1 W1 -178.3(3) . . . . ?
O22 Si O1 W7 58.0(5) . . . . ?
O22 Si O1 Co4 -58.7(4) . . . . ?
O22 Si O29 W4 -60.1(5) . . . . ?
O22 Si O29 W6 -178.5(3) . . . . ?
O22 Si O29 Co1 58.7(4) . . . . ?
O22 Si O41 W8 -178.7(3) . . . . ?
O22 Si O41 W5 -60.9(4) . . . . ?
O22 Si O41 W3 56.5(5) . . . . ?
C56 C88 C90 C20 0.2(18) . . . . ?
C56 C1 C2 C20 1(2) . . . . ?
C104 P7 C22 C53 167.5(9) . . . . ?
C104 P7 C98 C64 -54.9(12) . . . . ?
C104 P7 C98 C97 124.7(11) . . . . ?
O23 W8 O3 W1 33.2(10) . . . . ?
O23 W8 O40 W5 -3.6(10) . . . . ?
O25 W5 O12 W7 -20.0(6) . . . . ?
O25 W2 O15 Ag9 22.5(4) . . . 2_666 ?
O25 W2 O16 Ag4 152.0(7) . . . . ?
O25 W2 O16 Co2 13.5(12) . . . . ?
C49 C27 C19 C15 -2(2) . . . . ?
O27 W1 O9 Ag7 82.1(5) . . . . ?
O27 W1 O9 Co4 -70.7(3) . . . . ?
O27 W1 O9 Ag3 89.4(5) . . . . ?
O27 W7 O35 Ag1 -107.0(4) . . . 2_666 ?
O27 W7 O30 Ag6 -89.1(5) . . . . ?
O27 W7 O30 Co4 72.1(4) . . . . ?
O27 W7 O28 W2 10.6(15) . . . . ?
O40 W8 O3 W1 -126.3(10) . . . . ?
O40 W5 O12 W7 137.5(6) . . . . ?
O40 W5 O25 W2 -71.1(11) . . . . ?
O28 W7 O35 Ag1 60.9(4) . . . 2_666 ?
O28 W7 O30 Ag6 113.0(5) . . . . ?
O28 W7 O30 Co4 -85.8(4) . . . . ?
O28 W2 O15 Ag9 -60.3(4) . . . 2_666 ?
O28 W2 O16 Ag4 -137.4(4) . . . . ?
O28 W2 O16 Co2 84.1(4) . . . . ?
C108 P8 C23 C35 -69.5(9) . . . . ?
C108 P8 C65 C3 164.4(9) . . . . ?
C108 P8 C65 C16 -12.6(11) . . . . ?
C108 C74 C58 C114 2(3) . . . . ?
C108 C75 C113 C114 -4(2) . . . . ?
C74 C108 C75 C113 5(2) . . . . ?
C74 C58 C114 C113 -1(3) . . . . ?
C75 C108 C74 C58 -4(2) . . . . ?
C75 C113 C114 C58 2(3) . . . . ?
C111 C101 C116 C46 0(3) . . . . ?
C116 C101 C111 C25 -1(3) . . . . ?
C78 C120 C85 C8 -3(3) . . . . ?
C118 C79 C119 C60 0.0 . . . . ?
C79 P3 C9 C92 -68.2(9) . . . . ?
C79 P3 C8 C42 95.4(12) . . . . ?
C79 P3 C8 C85 -82.9(13) . . . . ?
C79 C118 C81 C121 0.0 . . . . ?
C79 C119 C60 C121 0.0 . . . . ?
C119 C60 C121 C81 0.0 . . . . ?
C60 C121 C81 C118 0.0 . . . . ?
C81 C118 C79 P3 174.8(13) . . . . ?
C81 C118 C79 C119 0.0 . . . . ?
Ag3 S3 C31 C110 -55.0(11) 2_666 . . . ?
Ag3 S3 C31 C45 81.4(17) 2_666 . . . ?
Ag3 P7 C22 C53 -66.4(9) . . . . ?
Ag3 P7 C98 C64 176.0(10) . . . . ?
Ag3 P7 C98 C97 -4.4(12) . . . . ?
Ag3 P7 C104 C26 101.6(10) . . . . ?
Ag3 P7 C104 C73 -82.6(11) . . . . ?
Ag3 O36 C105 O38 136.7(10) . . . . ?
Ag3 O36 C105 C106 -43.5(12) . . . . ?
O26 W1 O9 Ag7 -118.8(5) 2_666 . . . ?
O26 W1 O9 Co4 88.4(3) 2_666 . . . ?
O26 W1 O9 Ag3 -111.5(5) 2_666 . . . ?
O26 W6 O23 W8 18.5(7) 2_666 . . . ?

_platon_squeeze_details          ?
_platon_squeeze_special_details  ?
loop_
_platon_squeeze_void_nr
_platon_squeeze_void_average_x
_platon_squeeze_void_average_y
_platon_squeeze_void_average_z
_platon_squeeze_void_volume
_platon_squeeze_void_count_electrons
_platon_squeeze_void_content
1 -0.001 -0.001 0.501 1360 274 ' '
2 0.141 0.512 0.558 8 -1 ' '
3 0.141 0.754 0.258 7 0 ' '
4 0.269 0.038 0.075 22 0 ' '
5 0.731 0.961 0.925 23 0 ' '
6 0.859 0.246 0.742 8 0 ' '
7 0.859 0.487 0.442 9 -1 ' '

_platon_squeeze_void_probe_radius 1.20
_olex2_submission_special_instructions 'No special instructions were received'
_oxdiff_exptl_absorpt_empirical_details 
;
Empirical correction (ABSPACK) includes:
- Absorption correction using spherical harmonics
- Frame scaling
;
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_20220928
_database_code_depnum_ccdc_archive 'CCDC 2312087'
loop_
_audit_author_name
_audit_author_address
'Jing Zhang'
;Beijing Institute of Technology
China
;
_audit_update_record             
;
2023-12-05 deposited with the CCDC.	2024-05-27 downloaded from the CCDC.
;
_audit_creation_date             2023-11-13
_audit_creation_method           
;
Olex2 1.3
(compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6408)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         
'C195 H232 Ag24 Cl O52 P12 S11 Si W15, 0.606(O17 W6), C195 H234 Ag24 Cl O41.093 P12 S11 Si W11.364, 2(O Si0.5)'
_chemical_formula_sum            'C390 H466 Ag48 Cl2 O105.39 P24 S22 Si3 W30'
_chemical_formula_weight         19136.95
_chemical_melting_point          ?
_chemical_oxdiff_formula         'Ag Si W O P S'
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
W W -0.8490 6.8722 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   21.7876(2)
_cell_length_b                   21.8079(2)
_cell_length_c                   59.0524(4)
_cell_angle_alpha                86.9110(10)
_cell_angle_beta                 86.8350(10)
_cell_angle_gamma                80.0060(10)
_cell_volume                     27562.3(4)
_cell_formula_units_Z            2
_cell_measurement_reflns_used    171894
_cell_measurement_temperature    180.00(10)
_cell_measurement_theta_max      30.6480
_cell_measurement_theta_min      2.1450
_shelx_estimated_absorpt_T_max   0.855
_shelx_estimated_absorpt_T_min   0.563
_exptl_absorpt_coefficient_mu    8.116
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.52806
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
CrysAlisPro 1.171.40.67a (Rigaku Oxford Diffraction, 2019)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            'clear dark orange'
_exptl_crystal_colour_lustre     clear
_exptl_crystal_colour_modifier   dark
_exptl_crystal_colour_primary    orange
_exptl_crystal_density_diffrn    2.306
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             17826
_exptl_crystal_size_max          0.08
_exptl_crystal_size_mid          0.04
_exptl_crystal_size_min          0.02
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0797
_diffrn_reflns_av_unetI/netI     0.0575
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.999
_diffrn_reflns_limit_h_max       25
_diffrn_reflns_limit_h_min       -25
_diffrn_reflns_limit_k_max       25
_diffrn_reflns_limit_k_min       -25
_diffrn_reflns_limit_l_max       70
_diffrn_reflns_limit_l_min       -68
_diffrn_reflns_number            359565
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.999
_diffrn_reflns_theta_full        25.000
_diffrn_reflns_theta_max         25.000
_diffrn_reflns_theta_min         1.991
_diffrn_ambient_environment      N~2~
_diffrn_ambient_temperature      180.00(10)
_diffrn_detector                 'Hybrid Pixel Array Detector'
_diffrn_detector_area_resol_mean 10.0000
_diffrn_detector_type            HyPix
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_details      
;
List of Runs (angles in degrees, time in seconds):

  # Type    Start    End  Width  tₑₓₚ   ω     θ     κ     φ   Frames
#--------------------------------------------------------------------------
  1  ω    -82.00 -56.00   0.25    2.00    --   -6.91 -18.00 -21.00  104
  2  ω    -20.00  68.00   0.25    2.00    --   -6.91  18.00 146.00  352
  3  ω    -11.00  37.00   0.25    2.00    --    3.47 -99.00  30.00  192
  4  ω     43.00  69.00   0.25    2.00    --    3.47  38.00-180.00  104
  5  ω    -18.00  12.00   0.25    2.00    --   -6.91 -99.00  60.00  120
  6  ω    -18.00  26.00   0.25    2.00    --   -6.91 -99.00 -90.00  176
  7  ω    -17.00  22.00   0.25    2.00    --   -6.91 -99.00-150.00  156
  8  ω     -8.00  26.00   0.25    2.00    --   -6.91 -99.00   0.00  136
  9  ω    -28.00  65.00   0.25    2.00    --   -6.91  77.00-180.00  372
 10  ω    -23.00   2.00   0.25    2.00    --   -6.91 -18.00 -21.00  100
;
_diffrn_measurement_device       'four-circle diffractometer'
_diffrn_measurement_device_type  'XtaLAB Synergy R, DW system, HyPix'
_diffrn_measurement_method       'ω scans'
_diffrn_orient_matrix_type       
'CrysAlisPro convention (1999,Acta A55,543-557)'
_diffrn_orient_matrix_UB_11      -0.0300070000
_diffrn_orient_matrix_UB_12      0.0185562000
_diffrn_orient_matrix_UB_13      0.0013020000
_diffrn_orient_matrix_UB_21      0.0138875000
_diffrn_orient_matrix_UB_22      0.0257567000
_diffrn_orient_matrix_UB_23      0.0025654000
_diffrn_orient_matrix_UB_31      0.0012836000
_diffrn_orient_matrix_UB_32      0.0092610000
_diffrn_orient_matrix_UB_33      -0.0116940000
_diffrn_radiation_monochromator  mirror
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   'Rotating-anode X-ray tube'
_diffrn_source_type              'Rigaku (Mo) X-ray Source'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                88361
_reflns_number_total             96956
_reflns_odcompleteness_completeness 99.89
_reflns_odcompleteness_iscentric 1
_reflns_odcompleteness_theta     26.32
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'CrysAlisPro 1.171.40.67a (Rigaku OD, 2019)'
_computing_data_collection       'CrysAlisPro 1.171.40.67a (Rigaku OD, 2019)'
_computing_data_reduction        'CrysAlisPro 1.171.40.67a (Rigaku OD, 2019)'
_computing_molecular_graphics    'Olex2 1.3 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.3 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2018/3 (Sheldrick, 2015)'
_computing_structure_solution    'SHELXT 2018/2 (Sheldrick, 2018)'
_refine_diff_density_max         5.201
_refine_diff_density_min         -3.544
_refine_diff_density_rms         0.497
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.219
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     6311
_refine_ls_number_reflns         96956
_refine_ls_number_restraints     17199
_refine_ls_R_factor_all          0.1564
_refine_ls_R_factor_gt           0.1503
_refine_ls_restrained_S_all      1.139
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0001P)²+6551.4736P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.3286
_refine_ls_wR_factor_ref         0.3312
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups, All C(H,H) groups
 At 1.5 times of:
  All C(H,H,H) groups
2. Restrained distances
 W3-O1 = W1-O1
 1.9 with sigma of 0.01
 H91A-H376
 2.1 with sigma of 0.01
 C103-C411 = C411-C413
 1.46 with sigma of 0.01
 C103-C413
 2.5 with sigma of 0.01
 C205-C255 = C313-C255
 1.46 with sigma of 0.01
 C226-C158 = C330-C226
 1.48 with sigma of 0.01
 C313-C205
 2.5 with sigma of 0.01
 S24-C219
 1.8 with sigma of 0.01
 C330-C158
 2.5 with sigma of 0.01
 C56-C356 = C56-C352
 1.48 with sigma of 0.01
 O19-O22 = O22-O21
 2.5 with sigma of 0.01
 C381-C19
 2.5 with sigma of 0.01
 C354-C272 = C350-C272
 1.48 with sigma of 0.01
 C19-S24 = S24-C381
 2.6 with sigma of 0.01
 C160-C74 = C346-C74
 1.48 with sigma of 0.01
 Ag23-S21 = Ag21-S21 = Ag41-S21
 2.3 with sigma of 0.01
 C88-C394 = C394-C176
 1.48 with sigma of 0.01
 O20-O19 = O19-O22
 2.5 with sigma of 0.01
 C303-C191 = C191-C189
 1.48 with sigma of 0.01
 C34-C390 = C384-C390
 1.48 with sigma of 0.01
 C39-C201 = C201-C115
 1.48 with sigma of 0.01
 C240-C252 = C328-C240
 1.48 with sigma of 0.01
 C409-C155 = C155-C51
 1.48 with sigma of 0.01
 Si1-O19 = Si1-O22 = Si1-O20 = Si1-O21
 1.5 with sigma of 0.01
 C152-S26 = S26-C70
 2.6 with sigma of 0.01
 W9A-O1B
 1.9 with sigma of 0.01
 C405-C251 = C127-C251
 1.48 with sigma of 0.01
 C19-C219 = C219-C381
 1.48 with sigma of 0.01
 O20-O21 = O21-O22
 2.5 with sigma of 0.01
 C34-S2 = S2-C384
 2.6 with sigma of 0.01
 C407-C101 = C311-C101
 1.48 with sigma of 0.01
 C152-C66 = C70-C66
 1.48 with sigma of 0.01
 C356-S30 = S30-C352
 2.6 with sigma of 0.01
 O40-O43 = O43-O41
 2.5 with sigma of 0.01
 C303-S3 = S3-C189
 2.6 with sigma of 0.01
 O43-O41 = O41-O42
 2.5 with sigma of 0.01
 C407-S23 = S23-C311
 2.6 with sigma of 0.01
 C356-C352
 2.5 with sigma of 0.01
 S2-C390
 1.8 with sigma of 0.01
 C39-S11 = S11-C115
 2.6 with sigma of 0.01
 C127-S13 = S13-C405
 2.6 with sigma of 0.01
 W11A-O28A = W10A-O28A
 1.9 with sigma of 0.01
 C402-C396 = C408-C396
 1.48 with sigma of 0.01
 S25-C409 = C409-C51
 2.6 with sigma of 0.01
 W7A-O39A
 1.9 with sigma of 0.01
 C92-C180 = C182-C92
 1.48 with sigma of 0.01
 C51-C409
 2.5 with sigma of 0.01
 W10A-O27A = W9A-O27A
 1.9 with sigma of 0.01
 C412-C38 = C400-C38
 1.48 with sigma of 0.01
 C127-C405
 2.5 with sigma of 0.01
 C394-C176 = C88-C394
 1.48 with sigma of 0.01
 O40-O42 = O42-O43
 2.5 with sigma of 0.01
 S7-C38 = S29-C396 = S27-C394 = S31-C92 = S15-C1
 1.8 with sigma of 0.01
 C115-C39
 2.5 with sigma of 0.01
 W4-O9 = W2-O9
 1.9 with sigma of 0.01
 C196-C1 = C404-C1
 1.48 with sigma of 0.01
 O42-O43 = O43-O41
 2.5 with sigma of 0.01
 S13-C251
 1.9 with sigma of 0.01
 S23-C101
 1.9 with sigma of 0.01
 C88-S27 = S27-C176
 2.6 with sigma of 0.01
 Si2-O40 = Si2-O41 = Si2-O42 = Si2-O43
 1.5 with sigma of 0.01
 S25-C155
 1.9 with sigma of 0.01
 C180-C182
 2.5 with sigma of 0.01
 W9A-O26A = W11A-O26A
 1.9 with sigma of 0.01
 W10-O30 = W11-O30
 1.9 with sigma of 0.01
 C404-C196
 2.5 with sigma of 0.01
 S3-C191
 1.9 with sigma of 0.01
 O40-O41 = O41-O42
 2.5 with sigma of 0.01
 C77-C99 = C99-C197
 1.48 with sigma of 0.01
 C412-S7 = S7-C400
 2.6 with sigma of 0.01
 C408-C402
 2.5 with sigma of 0.01
 C209-C125 = C125-C95
 1.48 with sigma of 0.01
 W7-O31 = W10-O31
 1.9 with sigma of 0.01
 C239-C13 = C157-C13
 1.48 with sigma of 0.01
 W12A-O30A = W8A-O30A
 1.9 with sigma of 0.01
 C299-C379 = C379-C377
 1.48 with sigma of 0.01
 O33A-W12A_$1
 1.9 with sigma of 0.01
 W7-O25 = W9-O25
 1.9 with sigma of 0.01
 S19-C43
 1.9 with sigma of 0.01
 C63-C43 = C43-C151
 1.48 with sigma of 0.01
 W8-O24 = W9-O24
 1.9 with sigma of 0.01
 C404-S15 = S15-C196
 2.6 with sigma of 0.01
 S9-C99
 1.9 with sigma of 0.01
 W5-O10 = W4-O10
 1.9 with sigma of 0.01
 C72-C68 = C68-C426
 1.48 with sigma of 0.01
 C396-C176
 3.1 with sigma of 0.01
 W7-O23 = O23-W8
 1.9 with sigma of 0.01
 S17-C379
 1.9 with sigma of 0.01
 W7A-O24A = W8A-O24A
 1.9 with sigma of 0.01
 S9-C77 = C77-C197
 2.6 with sigma of 0.01
 C88-C176
 2.5 with sigma of 0.01
 S21-C13
 1.9 with sigma of 0.01
 W3-O11 = W5-O11
 1.9 with sigma of 0.01
 C282-C172 = C386-C282
 1.46 with sigma of 0.01
 W9A-O23A = W7A-O23A
 1.9 with sigma of 0.01
 C239-S21 = S21-C157
 2.6 with sigma of 0.01
 C63-S19 = S19-C151
 2.6 with sigma of 0.01
 W3-O6 = W6-O6
 1.9 with sigma of 0.01
 C419-C107
 2.5 with sigma of 0.01
 W8A-O25A = W9A-O25A
 1.9 with sigma of 0.01
 W4A-O7A = W5A-O7A = W5A-O5 = W6-O5 = W6-O12 = W5-O12
 1.9 with sigma of 0.01
 H133-H34L
 3.2 with sigma of 0.01
 C107-C55
 1.5 with sigma of 0.01
 S24A-C55
 1.8 with sigma of 0.01
 W2-O7 = W3-O7
 1.9 with sigma of 0.01
 W2-O2 = W1-O2
 1.9 with sigma of 0.01
 W1A-O1A = O1A-W2A
 1.9 with sigma of 0.01
 W3A-O10A = O10A-W2A
 1.9 with sigma of 0.01
 O1-O7
 2.7 with sigma of 0.01
 W2-O8 = W6_$2-O8
 1.9 with sigma of 0.01
 W1-O3 = W5_$2-O3
 1.9 with sigma of 0.01
 W4_$2-O4 = W1-O4
 1.9 with sigma of 0.01
 W1A-O2A = W3A-O2A
 1.9 with sigma of 0.01
 W5A-O6A = O6A-W6A
 1.9 with sigma of 0.01
 W5A-O4A = W1A-O4A
 1.9 with sigma of 0.01
 O1A-O4A
 2.7 with sigma of 0.01
 W2A-O8A = W4A-O8A
 1.9 with sigma of 0.01
 W3A-O12A = W4A_$2-O12A
 1.9 with sigma of 0.01
 W3A-O11A = W5A_$2-O11A
 1.9 with sigma of 0.01
 W2A-O10A = W3A-O10A
 1.9 with sigma of 0.01
 W1A-O3A = W6A-O3A
 1.9 with sigma of 0.01
 W1A-O13A
 1.9 with sigma of 0.01
 W3A-O18A
 1.9 with sigma of 0.01
 W2A-O9A
 1.9 with sigma of 0.01
 O9A-O10A = O10A-O1A
 2.7 with sigma of 0.01
 W2A-O17A
 1.9 with sigma of 0.01
 W5A-O14A
 1.9 with sigma of 0.01
 W6A-O15A
 1.9 with sigma of 0.01
 W4A-O16A
 1.9 with sigma of 0.01
 O10_$2-O3 = O3-O4
 2.7 with sigma of 0.01
 O2-O3 = O3-O12_$2
 2.7 with sigma of 0.01
 W3-O15
 1.9 with sigma of 0.01
 W1-O14
 1.9 with sigma of 0.01
 W2-O16
 1.9 with sigma of 0.01
 W6-O13
 1.9 with sigma of 0.01
 W5-O18
 1.9 with sigma of 0.01
 W4-O17
 1.9 with sigma of 0.01
 W11-O28 = W12-O28
 1.9 with sigma of 0.01
 W11-O27 = O27-W9
 1.9 with sigma of 0.01
 W9-O26 = W12-O26
 1.9 with sigma of 0.01
 O26A-O27A = O27A-O23A
 2.7 with sigma of 0.01
 O28A-O27A = O27A-O26A
 2.7 with sigma of 0.01
 O25A-O23A = O23A-O24A
 2.7 with sigma of 0.01
 W12-O29
 1.9 with sigma of 0.01
 W10-O32
 1.9 with sigma of 0.01
 W11-O38
 1.9 with sigma of 0.01
 O32-O30 = O30-O38
 2.7 with sigma of 0.01
 O30-O31 = O31-O29_$1
 2.7 with sigma of 0.01
 O29_$1-O32 = O32-O30
 2.7 with sigma of 0.01
 O27-O30 = O30-O31
 2.7 with sigma of 0.01
 O38-O30 = O30-O32
 2.7 with sigma of 0.01
 W7-O34
 1.9 with sigma of 0.01
 O30-O27 = O27-O25
 2.7 with sigma of 0.01
 O28-O27 = O27-O26
 2.7 with sigma of 0.01
 W7A-O32A = W7A-O33A
 1.9 with sigma of 0.01
 W8A-O31A
 1.9 with sigma of 0.01
 O24A-O31A = O31A_$1-O28A
 2.7 with sigma of 0.01
 O26A-O29A = O29A-O30A
 2.7 with sigma of 0.01
 O24A-O32A = O32A_$1-O28A
 2.7 with sigma of 0.01
 O33A_$1-O29A = O29A-O32A_$1
 2.7 with sigma of 0.01
 O30A-O29A = O29A-O26A
 2.7 with sigma of 0.01
 O32A_$1-O29A = O29A-O33A_$1
 2.7 with sigma of 0.01
 W11A-O37A
 1.9 with sigma of 0.01
 W8A-O35A
 1.9 with sigma of 0.01
 W12A-O36A
 1.9 with sigma of 0.01
 W11A-O29A = W12A-O29A
 2.1 with sigma of 0.01
 W10A-O34A
 1.9 with sigma of 0.01
 W7-O35
 1.9 with sigma of 0.01
 W10-O33
 1.9 with sigma of 0.01
 O32-O33 = O33-O31
 2.7 with sigma of 0.01
 W11-O37
 1.9 with sigma of 0.01
 W9-O36
 1.9 with sigma of 0.01
 W12-O39
 1.9 with sigma of 0.01
 W8A-O31A = O31A_$1-W10A
 1.9 with sigma of 0.01
 W12A_$1-O38A = O38A-W10A
 1.9 with sigma of 0.01
 O23A-O33A = O33A-O38A
 2.7 with sigma of 0.01
 O23A-O27A = O27A-O38A
 2.7 with sigma of 0.01
 Ag23-Ag21
 3.5 with sigma of 0.01
 Ag3-Ag51
 3.5 with sigma of 0.01
 P5-C224
 1.8 with sigma of 0.01
 S27-C394
 1.8 with sigma of 0.01
 S11-C201
 1.9 with sigma of 0.01
 S5-C125
 1.9 with sigma of 0.01
 C378-C265
 3 with sigma of 0.01
 C68-S26A
 1.8 with sigma of 0.01
 C62-C416 = C416-C278
 1.48 with sigma of 0.01
 C265-C380
 3.1 with sigma of 0.01
 P11-C423
 1.6 with sigma of 0.01
 C4-C348 = C4-C344
 1.46 with sigma of 0.01
 P15-C271
 1.7 with sigma of 0.01
 C399-C173 = C85-C399
 1.46 with sigma of 0.01
 H35N-H421 = H421-H35O
 2 with sigma of 0.01
 H38I-H139
 2 with sigma of 0.01
 H41J-H293 = H293-H41K
 2 with sigma of 0.01
 Cl2-C408
 2.5 with sigma of 0.01
 H247-H135
 2.1 with sigma of 0.01
 H17I-H247
 2.2 with sigma of 0.01
 O27A-O1B \\sim O1B-O25A
 with sigma of 0.01
 O23A-O39A \\sim O39A-O32A
 with sigma of 0.01
 C152-C66 \\sim C426-C68
 with sigma of 0.02
 C66-C70 \\sim C68-C72
 with sigma of 0.02
 C152-C70 \\sim C426-C72
 with sigma of 0.04
 O1A-O13A \\sim O13A-O3A
 with sigma of 0.01
 O4A-O13A \\sim O13A-O2A
 with sigma of 0.01
 O2A-O18A \\sim O18A-O11A
 with sigma of 0.01
 O12A-O18A \\sim O18A-O10A
 with sigma of 0.01
 O1A-O17A \\sim O17A-O9A
 with sigma of 0.01
 O10A-O17A \\sim O17A-O8A
 with sigma of 0.01
 O7A-O14A \\sim O14A-O6A
 with sigma of 0.01
 O6A-O15A \\sim O15A-O5A
 with sigma of 0.01
 O8A-O16A \\sim O16A-O7A
 with sigma of 0.01
 O7-O15 \\sim O15-O6
 with sigma of 0.01
 O1-O14 \\sim O14-O3
 with sigma of 0.01
 O7-O16 \\sim O16-O8
 with sigma of 0.01
 O5-O13 \\sim O13-O12
 with sigma of 0.01
 O12-O18 \\sim O18-O11
 with sigma of 0.01
 O10-O17 \\sim O17-O9
 with sigma of 0.01
 O28A-O37A \\sim O37A-O26A
 with sigma of 0.01
 O25A-O35A \\sim O35A-O31A
 with sigma of 0.01
 O29A-O36A \\sim O36A-O30A
 with sigma of 0.01
 O38A-O34A \\sim O34A-O27A
 with sigma of 0.01
 O34-O35 \\sim O35-O25
 with sigma of 0.01
 O30-O37 \\sim O37-O27
 with sigma of 0.01
 O30-O37 \\sim O37-O38
 with sigma of 0.01
 O27-O36 \\sim O36-O24
 with sigma of 0.01
 O25-O36 \\sim O36-O26
 with sigma of 0.01
 O28-O39 \\sim O39-O29
 with sigma of 0.01
 O29A-O37A \\sim O37A-O28A
 with sigma of 0.01
 O28A-O34A \\sim O34A-O38A
 with sigma of 0.01
 O31A_$1-O34A \\sim O34A-O27A
 with sigma of 0.01
 C293-P11 \\sim P11-C297
 with sigma of 0.01
 Ag30-C66 \\sim Ag30-C68
 with sigma of 0.04
 C67-P19 \\sim P19-C33
 with sigma of 0.01
 C211-P11 \\sim P11-C53
 with sigma of 0.01
 C17-P15 \\sim P15-C135
 with sigma of 0.01
3. Restrained planarity
 P5, C372, C380, C382
 with sigma of 0.01
 C211, C423, C53, P11
 with sigma of 0.01
4. Uiso/Uaniso restraints and constraints
All non-hydrogen atoms have similar U: within 2A with sigma of 0.01 and sigma
for terminal atoms of 0.02 within 2A
All non-hydrogen atoms restrained to be isotropic: with sigma of 0.01 and sigma
for terminal atoms of 0.02
Uanis(O21) \\sim Ueq, Uanis(Si1) \\sim Ueq, Uanis(O20) \\sim Ueq, Uanis(O19)
\\sim Ueq, Uanis(O22) \\sim Ueq: with sigma of 0.005 and sigma for terminal
atoms of 0.01
5. Rigid body (RIGU) restrains
 All non-hydrogen atoms
 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01
6. Others
 Sof(W1A)=Sof(W2A)=Sof(W3A)=Sof(W4A)=Sof(W5A)=Sof(W6A)=Sof(O1A)=Sof(O2A)=
 Sof(O3A)=Sof(O4A)=Sof(O5A)=Sof(O6A)=Sof(O7A)=Sof(O8A)=Sof(O9A)=Sof(O10A)=
 Sof(O11A)=Sof(O12A)=Sof(O13A)=Sof(O14A)=Sof(O15A)=Sof(O16A)=Sof(O17A)=
 Sof(O18A)=1-FVAR(1)
 Sof(W1)=Sof(W2)=Sof(W3)=Sof(W4)=Sof(W5)=Sof(W6)=Sof(O1)=Sof(O2)=Sof(O3)=
 Sof(O4)=Sof(O5)=Sof(O6)=Sof(O7)=Sof(O8)=Sof(O9)=Sof(O10)=Sof(O11)=Sof(O12)=
 Sof(O13)=Sof(O14)=Sof(O15)=Sof(O16)=Sof(O17)=Sof(O18)=FVAR(1)
 Sof(W7A)=Sof(W8A)=Sof(W9A)=Sof(W10A)=Sof(W11A)=Sof(W12A)=Sof(O1B)=Sof(O23A)=
 Sof(O24A)=Sof(O25A)=Sof(O26A)=Sof(O27A)=Sof(O28A)=Sof(O29A)=Sof(O30A)=
 Sof(O31A)=Sof(O32A)=Sof(O33A)=Sof(O34A)=Sof(O35A)=Sof(O36A)=Sof(O37A)=
 Sof(O38A)=Sof(O39A)=1-FVAR(2)
 Sof(W7)=Sof(W8)=Sof(W9)=Sof(W10)=Sof(W11)=Sof(W12)=Sof(O23)=Sof(O24)=Sof(O25)=
 Sof(O26)=Sof(O27)=Sof(O28)=Sof(O29)=Sof(O30)=Sof(O31)=Sof(O32)=Sof(O33)=
 Sof(O34)=Sof(O35)=Sof(O36)=Sof(O37)=Sof(O38)=Sof(O39)=FVAR(2)
 Sof(Ag5)=Sof(Ag19)=Sof(Ag21)=Sof(Ag23)=Sof(Ag39)=Sof(S5)=Sof(S9)=Sof(S17)=
 Sof(S19)=Sof(S21)=Sof(C239)=Sof(H23A)=Sof(H23B)=Sof(H23C)=Sof(C125)=Sof(H125)=
 Sof(C63)=Sof(H63A)=Sof(H63B)=Sof(H63C)=Sof(C299)=Sof(H29A)=Sof(H29B)=Sof(H29C)=
 Sof(C151)=Sof(H15K)=Sof(H15L)=Sof(H15M)=Sof(C77)=Sof(H77A)=Sof(H77B)=Sof(H77C)=
 Sof(C157)=Sof(H15N)=Sof(H15O)=Sof(H15P)=Sof(C43)=Sof(H43)=Sof(C377)=Sof(H37D)=
 Sof(H37E)=Sof(H37F)=Sof(C379)=Sof(H379)=Sof(C95)=Sof(H95A)=Sof(H95B)=Sof(H95C)=
 Sof(C197)=Sof(H19G)=Sof(H19H)=Sof(H19I)=Sof(C99)=Sof(H99)=Sof(C13)=Sof(H13)=
 Sof(C209)=Sof(H20I)=Sof(H20J)=Sof(H20K)=1-FVAR(3)
 Sof(Ag3)=Sof(Ag13)=Sof(Ag25)=Sof(Ag49)=Sof(Ag51)=Sof(S3)=Sof(S11)=Sof(S13)=
 Sof(S23)=Sof(S25)=Sof(C115)=Sof(H11D)=Sof(H11E)=Sof(H11F)=Sof(C251)=Sof(H251)=
 Sof(C127)=Sof(H12E)=Sof(H12F)=Sof(H12G)=Sof(C303)=Sof(H30C)=Sof(H30D)=
 Sof(H30E)=Sof(C155)=Sof(H155)=Sof(C311)=Sof(H31A)=Sof(H31B)=Sof(H31C)=Sof(C39)=
 Sof(H39A)=Sof(H39B)=Sof(H39C)=Sof(C189)=Sof(H18G)=Sof(H18H)=Sof(H18I)=
 Sof(C191)=Sof(H191)=Sof(C201)=Sof(H201)=Sof(C101)=Sof(H101)=Sof(C405)=
 Sof(H40L)=Sof(H40M)=Sof(H40N)=Sof(C407)=Sof(H40O)=Sof(H40P)=Sof(H40Q)=Sof(C51)=
 Sof(H51A)=Sof(H51B)=Sof(H51C)=Sof(C409)=Sof(H40R)=Sof(H40S)=Sof(H40T)=FVAR(3)
 Sof(Ag7)=Sof(Ag27)=Sof(Ag29)=Sof(Ag55)=Sof(Ag57)=Sof(S7)=Sof(S15)=Sof(S27)=
 Sof(S29)=Sof(S31)=Sof(C1)=Sof(H1)=Sof(C38)=Sof(H38)=Sof(C88)=Sof(H88A)=
 Sof(H88B)=Sof(H88C)=Sof(C92)=Sof(H92)=Sof(C176)=Sof(H17D)=Sof(H17E)=Sof(H17F)=
 Sof(C180)=Sof(H18A)=Sof(H18B)=Sof(H18C)=Sof(C182)=Sof(H18D)=Sof(H18E)=
 Sof(H18F)=Sof(C196)=Sof(H19A)=Sof(H19B)=Sof(H19C)=Sof(C394)=Sof(H394)=
 Sof(C396)=Sof(H396)=Sof(C400)=Sof(H40A)=Sof(H40B)=Sof(H40C)=Sof(C402)=
 Sof(H40D)=Sof(H40E)=Sof(H40F)=Sof(C404)=Sof(H40G)=Sof(H40H)=Sof(H40I)=
 Sof(C408)=Sof(H40J)=Sof(H40K)=Sof(H2)=Sof(C412)=Sof(H41A)=Sof(H41B)=Sof(H41C)=
 Sof(Ag53)=1-FVAR(4)
 Sof(Ag2)=Sof(Ag15)=Sof(Ag17)=Sof(Ag35)=Sof(Ag45)=Sof(S2)=Sof(S14)=Sof(S28)=
 Sof(S30)=Sof(S32)=Sof(C34)=Sof(H34A)=Sof(H34B)=Sof(H34C)=Sof(C56)=Sof(H56)=
 Sof(C74)=Sof(H74)=Sof(C160)=Sof(H16A)=Sof(H16B)=Sof(H16C)=Sof(C240)=Sof(H240)=
 Sof(C252)=Sof(H25A)=Sof(H25B)=Sof(H25C)=Sof(C272)=Sof(H272)=Sof(C328)=
 Sof(H32E)=Sof(H32F)=Sof(H32G)=Sof(C346)=Sof(H34G)=Sof(H34H)=Sof(H34I)=
 Sof(C350)=Sof(H35A)=Sof(H35B)=Sof(H35C)=Sof(C352)=Sof(H35D)=Sof(H35E)=
 Sof(H35F)=Sof(C354)=Sof(H35G)=Sof(H35H)=Sof(H35I)=Sof(C356)=Sof(H35J)=
 Sof(H35K)=Sof(H35L)=Sof(C384)=Sof(H38A)=Sof(H38B)=Sof(H38C)=Sof(C390)=
 Sof(H390)=Sof(Ag58)=FVAR(4)
 Sof(Ag1A)=Sof(Ag9A)=Sof(S26A)=Sof(C68)=Sof(H68)=Sof(C72)=Sof(H72A)=Sof(H72B)=
 Sof(H72C)=Sof(C426)=Sof(H42A)=Sof(H42B)=Sof(H42C)=1-FVAR(5)
 Sof(Ag9)=Sof(Ag33)=Sof(S26)=Sof(C66)=Sof(H66)=Sof(C70)=Sof(H70A)=Sof(H70B)=
 Sof(H70C)=Sof(C152)=Sof(H15A)=Sof(H15B)=Sof(H15C)=FVAR(5)
 Sof(Ag)=1-FVAR(6)
 Sof(Ag37)=FVAR(6)
 Sof(Ag60)=1-FVAR(7)
 Sof(Ag43)=FVAR(7)
 Sof(Ag61)=1-FVAR(8)
 Sof(Ag44)=FVAR(8)
 Sof(Ag1B)=Sof(Ag62)=Sof(S24A)=Sof(C107)=Sof(H10E)=Sof(H10F)=Sof(H10G)=
 Sof(C55)=Sof(H55)=Sof(C419)=Sof(H41I)=Sof(H41J)=Sof(H41K)=1-FVAR(9)
 Sof(Ag11)=Sof(Ag41)=Sof(S24)=Sof(C219)=Sof(H219)=Sof(C19)=Sof(H19D)=Sof(H19E)=
 Sof(H19F)=Sof(C381)=Sof(H38G)=Sof(H38H)=Sof(H38I)=FVAR(9)
 Fixed Sof: O19(0.25) O20(0.25) O21(0.25) O22(0.25) O40(0.25) O41(0.25)
 O42(0.25) O43(0.25)
 Fixed X: C396(-0.374579) C357(-0.64518) C203(-0.69244) C205(-0.95094) C103(-
 1.23926) C413(-1.20699)
 Fixed Y: C396(1.10682) C357(1.153161) C203(1.09557) C205(0.59489)
 C103(1.325281) C413(1.34072)
 Fixed Z: C396(0.81097) C357(0.528181) C203(0.499469) C205(0.68487)
 C103(0.681141) C413(0.63846)
7.a Riding coordinates:
 C34(H34A,H34B,H34C), C70(H70A,H70B,H70C), C72(H72A,H72B,H72C), C88(H88A,H88B,
 H88C), C98(H98A,H98B,H98C), C152(H15A,H15B,H15C), C158(H15F,H15G,H15H),
 C160(H16A,H16B,H16C), C172(H17A,H17B,H17C), C176(H17D,H17E,H17F), C180(H18A,
 H18B,H18C), C182(H18D,H18E,H18F), C196(H19A,H19B,H19C), C252(H25A,H25B,H25C),
 C328(H32E,H32F,H32G), C330(H33A,H33B,H33C), C346(H34G,H34H,H34I), C348(H34J,
 H34K,H34L), C350(H35A,H35B,H35C), C352(H35D,H35E,H35F), C354(H35G,H35H,H35I),
 C356(H35J,H35K,H35L), C370(H37A,H37B,H37C), C384(H38A,H38B,H38C), C386(H38D,
 H38E,H38F), C400(H40A,H40B,H40C), C402(H40D,H40E,H40F), C404(H40G,H40H,H40I),
 C408(H40J,H40K,H2), C412(H41A,H41B,H41C), C426(H42A,H42B,H42C), C107(H10E,H10F,
 H10G), C115(H11D,H11E,H11F), C239(H23A,H23B,H23C), C63(H63A,H63B,H63C),
 C127(H12E,H12F,H12G), C299(H29A,H29B,H29C), C151(H15K,H15L,H15M), C303(H30C,
 H30D,H30E), C19(H19D,H19E,H19F), C77(H77A,H77B,H77C), C311(H31A,H31B,H31C),
 C39(H39A,H39B,H39C), C313(H31D,H31E,H31F), C157(H15N,H15O,H15P), C357(H35M,
 H35N,H35O), C91(H91A,H91B,H91C), C377(H37D,H37E,H37F), C189(H18G,H18H,H18I),
 C95(H95A,H95B,H95C), C381(H38G,H38H,H38I), C197(H19G,H19H,H19I), C395(H39D,
 H39E,H39F), C397(H39G,H39H,H39I), C405(H40L,H40M,H40N), C203(H20A,H20B,H20C),
 C407(H40O,H40P,H40Q), C51(H51A,H51B,H51C), C409(H40R,H40S,H40T), C205(H20D,
 H20E,H20F), C103(H10J,H10K,H10L), C413(H41F,H41G,H41H), C209(H20I,H20J,H20K),
 C419(H41I,H41J,H41K)
7.b Ternary CH refined with riding coordinates:
 C1(H1), C4(H4), C38(H38), C56(H56), C66(H66), C68(H68), C74(H74), C92(H92),
 C102(H102), C226(H226), C240(H240), C242(H242), C272(H272), C282(H282),
 C390(H390), C394(H394), C396(H396), C219(H219), C55(H55), C125(H125),
 C251(H251), C255(H255), C129(H129), C131(H131), C155(H155), C333(H333),
 C43(H43), C379(H379), C191(H191), C99(H99), C201(H201), C101(H101), C411(H411),
  C13(H13)
7.c Secondary CH2 refined with riding coordinates:
 C24(H24A,H24B), C30(H30A,H30B), C32(H32A,H32B), C60(H60A,H60B), C62(H62A,
 H62B), C64(H64A,H64B), C94(H94A,H94B), C96(H96A,H96B), C100(H10A,H10B),
 C104(H10C,H10D), C122(H12A,H12B), C126(H12C,H12D), C156(H15D,H15E), C248(H24C,
 H24D), C270(H27A,H27B), C276(H27C,H27D), C278(H27E,H27F), C326(H32C,H32D),
 C416(H41D,H41E), C213(H21A,H21B), C215(H21C,H21D), C109(H10H,H10I), C15(H15I,
 H15J), C253(H25D,H25E), C259(H25F,H25G), C277(H27G,H27H), C283(H28A,H28B),
 C307(H30F,H30G), C309(H30H,H30I), C315(H31G,H31H), C79(H79A,H79B), C331(H33D,
 H33E), C85(H85A,H85B), C171(H17G,H17H), C173(H17I,H17J), C399(H39J,H39K),
 C207(H20G,H20H)
7.d Aromatic/amide H refined with riding coordinates:
 C10(H10), C14(H14), C16(H16), C18(H18), C20(H20), C22(H22), C26(H26),
 C28(H28), C36(H36), C42(H42), C44(H44), C46(H46), C48(H48), C50(H50), C52(H52),
  C54(H54), C58(H58), C78(H78), C80(H80), C82(H82), C84(H84), C86(H86),
 C108(H108), C110(H110), C112(H112), C114(H114), C116(H116), C120(H120),
 C124(H124), C130(H130), C132(H132), C134(H134), C136(H136), C138(H138),
 C142(H142), C144(H144), C146(H146), C148(H148), C150(H150), C154(H154),
 C162(H162), C164(H164), C166(H166), C168(H168), C170(H170), C174(H174),
 C186(H186), C188(H188), C190(H190), C192(H192), C194(H194), C200(H200),
 C202(H202), C204(H204), C206(H206), C208(H208), C210(H210), C214(H214),
 C216(H216), C218(H218), C220(H220), C222(H222), C230(H230), C232(H232),
 C234(H234), C236(H236), C238(H238), C244(H244), C246(H246), C250(H250),
 C254(H254), C256(H256), C258(H258), C260(H260), C262(H262), C264(H264),
 C274(H274), C280(H280), C284(H284), C286(H286), C288(H288), C290(H290),
 C292(H292), C296(H296), C298(H298), C300(H300), C304(H304), C306(H306),
 C308(H308), C310(H310), C314(H314), C316(H316), C318(H318), C320(H320),
 C322(H322), C334(H334), C336(H336), C338(H338), C340(H340), C342(H342),
 C358(H358), C360(H360), C364(H364), C366(H366), C368(H368), C372(H372),
 C374(H374), C376(H376), C378(H378), C380(H380), C388(H388), C392(H392),
 C398(H398), C406(H406), C410(H410), C414(H414), C418(H418), C420(H420),
 C422(H422), C27(H27), C221(H221), C111(H111), C7(H7), C225(H225), C113(H113),
 C227(H227), C57(H57), C229(H229), C29(H29), C233(H233), C117(H117), C235(H235),
  C59(H59), C119(H119), C243(H243), C61(H61), C245(H245), C123(H123),
 C247(H247), C31(H31), C249(H249), C257(H257), C65(H65), C261(H261), C33(H33),
 C265(H265), C133(H133), C267(H267), C67(H67), C269(H269), C135(H135), C17(H17),
  C273(H273), C137(H137), C139(H139), C279(H279), C35(H35), C281(H281),
 C71(H71), C143(H143), C287(H287), C9(H9), C289(H289), C145(H145), C291(H291),
 C293(H293), C147(H147), C295(H295), C37(H37), C297(H297), C149(H149),
 C301(H301), C153(H153), C317(H317), C159(H159), C319(H319), C5(H5), C321(H321),
  C161(H161), C81(H81), C163(H163), C327(H327), C41(H41), C329(H329),
 C165(H165), C167(H167), C335(H335), C21(H21), C337(H337), C169(H169),
 C339(H339), C341(H341), C343(H343), C345(H345), C347(H347), C87(H87),
 C349(H349), C351(H351), C11(H11), C353(H353), C177(H177), C355(H355), C89(H89),
  C359(H359), C45(H45), C361(H361), C181(H181), C363(H363), C183(H183),
 C367(H367), C23(H23), C369(H369), C185(H185), C93(H93), C373(H373), C187(H187),
  C375(H375), C47(H47), C383(H383), C3(H3), C385(H385), C387(H387), C97(H97),
 C389(H389), C195(H195), C391(H391), C393(H393), C199(H199), C25(H25),
 C401(H401), C403(H403), C415(H415), C417(H417), C105(H105), C421(H421),
 C211(H211), C53(H53), C425(H425)
7.e Fitted hexagon refined as free rotating group:
 C12(C14,C16,C18,C20,C22), C40(C42,C44,C46,C48,C50), C76(C78,C80,C82,C84,C86),
 C106(C108,C110,C112,C114,C116), C128(C130,C132,C134,C136,C138), C140(C142,C144,
 C146,C148,C150), C184(C186,C188,C190,C192,C194), C198(C200,C202,C204,C206,
 C208), C214(C216,C218,C220,C222,C224), C228(C230,C232,C234,C236,C238),
 C256(C258,C260,C262,C264,C266), C284(C286,C288,C290,C292,C294), C296(C298,C300,
 C302,C304,C306), C312(C314,C316,C318,C320,C322), C332(C334,C336,C338,C340,
 C342), C358(C360,C362,C364,C366,C368), C372(C374,C376,C378,C380,C382), C223(C7,
 C225,C113,C227,C57), C231(C29,C233,C117,C235,C59), C121(C243,C61,C245,C123,
 C247), C263(C33,C265,C133,C267,C67), C135(C271,C17,C273,C137,C275), C285(C143,
 C287,C9,C289,C145), C73(C293,C147,C295,C37,C297), C159(C319,C5,C321,C161,C323),
  C325(C163,C327,C41,C329,C165), C175(C351,C11,C353,C177,C355), C179(C359,C45,
 C361,C181,C363), C365(C183,C367,C23,C369,C185), C371(C93,C373,C187,C375,C47),
 C193(C387,C97,C389,C195,C391), C105(C421,C211,C423,C53,C425)
7.f Idealised Me refined as rotating group:
 C118(H11A,H11B,H11C), C268(H26A,H26B,H26C), C344(H34D,H34E,H34F), C49(H49A,
 H49B,H49C)
;
_atom_sites_solution_hydrogens   mixed
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
W1 W -0.54459(16) 1.49203(14) 0.55819(5) 0.0375(8) Uani 0.501(3) 1 d D U P A 1
W2 W -0.65630(13) 1.49238(14) 0.51695(6) 0.0327(7) Uani 0.501(3) 1 d D U P A 1
W3 W -0.59432(16) 1.62864(15) 0.52496(6) 0.0344(7) Uani 0.501(3) 1 d D U P A 1
W4 W -0.61178(16) 1.49941(16) 0.45865(6) 0.0363(8) Uani 0.501(3) 1 d D U P A 1
W5 W -0.55085(15) 1.63653(15) 0.46679(6) 0.0378(8) Uani 0.501(3) 1 d D U P A 1
W6 W -0.4385(2) 1.6374(2) 0.50736(8) 0.0318(10) Uani 0.501(3) 1 d D U P A 1
O1 O -0.5716(18) 1.5789(6) 0.5517(3) 0.039(3) Uani 0.501(3) 1 d D U P A 1
O2 O -0.6206(8) 1.4810(16) 0.5458(3) 0.036(3) Uani 0.501(3) 1 d D U P A 1
O3 O -0.5099(10) 1.4076(6) 0.5533(4) 0.038(3) Uani 0.501(3) 1 d D U P A 1
O4 O -0.4639(7) 1.5128(14) 0.5593(5) 0.042(3) Uani 0.501(3) 1 d D U P A 1
O5 O -0.412(2) 1.586(2) 0.5333(6) 0.040(3) Uani 0.501(3) 1 d D U P A 1
O6 O -0.5218(8) 1.6647(11) 0.5183(9) 0.040(3) Uani 0.501(3) 1 d D U P A 1
O7 O -0.6547(9) 1.5785(6) 0.5195(7) 0.037(3) Uani 0.501(3) 1 d D U P A 1
O8 O -0.6188(18) 1.4082(7) 0.5135(5) 0.034(4) Uani 0.501(3) 1 d D U P A 1
O9 O -0.6644(10) 1.510(2) 0.48541(17) 0.038(3) Uani 0.501(3) 1 d D U P A 1
O10 O -0.6096(7) 1.5860(6) 0.4597(6) 0.039(3) Uani 0.501(3) 1 d D U P A 1
O11 O -0.5993(15) 1.6556(19) 0.4940(2) 0.039(3) Uani 0.501(3) 1 d D U P A 1
O12 O -0.4873(11) 1.6651(10) 0.4820(4) 0.039(3) Uani 0.501(3) 1 d D U P A 1
O13 O -0.402(2) 1.7085(13) 0.5119(7) 0.049(7) Uani 0.501(3) 1 d D U P A 1
O14 O -0.561(2) 1.4881(9) 0.5900(2) 0.042(5) Uani 0.501(3) 1 d D U P A 1
O15 O -0.6460(10) 1.6953(13) 0.5395(9) 0.045(7) Uani 0.501(3) 1 d D U P A 1
O16 O -0.7392(9) 1.4861(10) 0.5270(9) 0.039(7) Uani 0.501(3) 1 d D U P A 1
O17 O -0.6662(18) 1.493(2) 0.4353(5) 0.048(9) Uani 0.501(3) 1 d D U P A 1
O18 O -0.5795(10) 1.7117(15) 0.4500(8) 0.044(8) Uani 0.501(3) 1 d D U P A 1
W1A W -0.5650(2) 1.62135(16) 0.53568(7) 0.0414(8) Uani 0.499(3) 1 d D U P A 2
W2A W -0.62235(15) 1.47803(16) 0.53986(5) 0.0323(7) Uani 0.499(3) 1 d D U P A 2
W3A W -0.65290(14) 1.58083(16) 0.49205(6) 0.0381(8) Uani 0.499(3) 1 d D U P A 2
W4A W -0.47025(15) 1.39307(15) 0.54651(5) 0.0321(7) Uani 0.499(3) 1 d D U P A 2
W5A W -0.41565(17) 1.5364(2) 0.54547(6) 0.0404(8) Uani 0.499(3) 1 d D U P A 2
W6A W -0.4386(3) 1.6401(3) 0.49738(9) 0.0389(11) Uani 0.499(3) 1 d D U P A 2
O1A O -0.6027(14) 1.5547(8) 0.5491(3) 0.038(3) Uani 0.499(3) 1 d D U P A 2
O2A O -0.6300(15) 1.6288(14) 0.5151(6) 0.039(3) Uani 0.499(3) 1 d D U P A 2
O3A O -0.5022(18) 1.6604(13) 0.5204(7) 0.041(3) Uani 0.499(3) 1 d D U P A 2
O4A O -0.4915(7) 1.5919(12) 0.5517(4) 0.042(3) Uani 0.499(3) 1 d D U P A 2
O5A O -0.492(2) 1.655(2) 0.4700(9) 0.040(4) Uani 0.499(3) 1 d D U P A 2
O6A O -0.3998(15) 1.5994(18) 0.5235(5) 0.040(3) Uani 0.499(3) 1 d D U P A 2
O7A O -0.448(2) 1.4658(12) 0.5579(3) 0.039(4) Uani 0.499(3) 1 d D U P A 2
O8A O -0.5511(9) 1.4362(19) 0.5549(3) 0.034(3) Uani 0.499(3) 1 d D U P A 2
O9A O -0.622(2) 1.4012(8) 0.5260(6) 0.036(4) Uani 0.499(3) 1 d D U P A 2
O10A O -0.6680(9) 1.5219(12) 0.5157(4) 0.037(3) Uani 0.499(3) 1 d D U P A 2
O11A O -0.6467(9) 1.5142(16) 0.4722(7) 0.039(3) Uani 0.499(3) 1 d D U P A 2
O12A O -0.6076(12) 1.6235(13) 0.4698(7) 0.040(3) Uani 0.499(3) 1 d D U P A 2
O13A O -0.6015(6) 1.6855(6) 0.5551(2) 0.046(7) Uani 0.499(3) 1 d D U P A 2
O14A O -0.376(2) 1.5594(18) 0.5709(4) 0.046(8) Uani 0.499(3) 1 d D U P A 2
O15A O -0.401(2) 1.7121(15) 0.4932(8) 0.051(8) Uani 0.499(3) 1 d D U P A 2
O16A O -0.4532(16) 1.3332(19) 0.5708(6) 0.046(9) Uani 0.499(3) 1 d D U P A 2
O17A O -0.6869(7) 1.4711(11) 0.5622(3) 0.044(7) Uani 0.499(3) 1 d D U P A 2
O18A O -0.7354(5) 1.6224(8) 0.4873(3) 0.047(8) Uani 0.499(3) 1 d D U P A 2
W7 W 0.00827(12) 1.04449(13) 0.94175(4) 0.0370(6) Uani 0.606(3) 1 d D U P B 1
W7A W 0.0222(3) 1.1230(2) 0.96078(7) 0.0371(10) Uani 0.394(3) 1 d D U P B 2
W8 W 0.00762(12) 1.15642(11) 0.98300(5) 0.0335(6) Uani 0.606(3) 1 d D U P B 1
W8A W -0.0812(2) 1.15286(19) 1.00808(8) 0.0405(10) Uani 0.394(3) 1 d D U P B 2
W9 W -0.12846(12) 1.09401(13) 0.97492(5) 0.0336(6) Uani 0.606(3) 1 d D U P B 1
W9A W -0.1210(2) 1.0637(2) 0.96392(8) 0.0438(11) Uani 0.394(3) 1 d D U P B 2
W10 W -0.00022(13) 0.88816(13) 0.95879(5) 0.0358(6) Uani 0.606(3) 1 d D U P B 1
W10A W -0.0367(2) 0.9154(2) 0.95466(7) 0.0417(10) Uani 0.394(3) 1 d D U P B 2
W11 W -0.1380(3) 0.9360(3) 0.99927(9) 0.0515(13) Uani 0.606(3) 1 d D U P B 1
W11A W -0.1389(4) 0.9425(3) 0.99116(9) 0.0276(12) Uani 0.394(3) 1 d D U P B 2
W12 W -0.13679(12) 1.05109(12) 1.03304(5) 0.0381(7) Uani 0.606(3) 1 d D U P B 1
W12A W -0.1070(2) 1.02944(19) 1.04635(7) 0.0368(10) Uani 0.394(3) 1 d D U P B 2
O1B O -0.185(2) 1.1018(18) 0.9448(7) 0.049(8) Uani 0.394(3) 1 d D U P B 2
O23 O 0.022(3) 1.1191(17) 0.9544(4) 0.035(3) Uani 0.606(3) 1 d D U P B 1
O23A O -0.0498(6) 1.0962(8) 0.9512(3) 0.039(3) Uani 0.394(3) 1 d D U P B 2
O24 O -0.0780(6) 1.1552(8) 0.9789(7) 0.038(3) Uani 0.606(3) 1 d D U P B 1
O24A O -0.0304(8) 1.1726(8) 0.9835(2) 0.038(3) Uani 0.394(3) 1 d D U P B 2
O25 O -0.0781(6) 1.0587(11) 0.9502(3) 0.040(3) Uani 0.606(3) 1 d D U P B 1
O25A O -0.1300(8) 1.1214(16) 0.9873(4) 0.040(3) Uani 0.394(3) 1 d D U P B 2
O26 O -0.1325(18) 1.1064(8) 1.00699(14) 0.041(3) Uani 0.606(3) 1 d D U P B 1
O26A O -0.1838(6) 1.0190(6) 0.9776(3) 0.037(4) Uani 0.394(3) 1 d D U P B 2
O27 O -0.1558(8) 1.0151(4) 0.9819(3) 0.041(3) Uani 0.606(3) 1 d D U P B 1
O27A O -0.0911(6) 0.9886(4) 0.9464(3) 0.042(3) Uani 0.394(3) 1 d D U P B 2
O28 O -0.1675(13) 0.9784(8) 1.0260(2) 0.047(4) Uani 0.606(3) 1 d D U P B 1
O28A O -0.1035(7) 0.8828(6) 0.9717(2) 0.039(4) Uani 0.394(3) 1 d D U P B 2
O29 O -0.0895(9) 1.1076(8) 1.0441(5) 0.041(3) Uani 0.606(3) 1 d D U P B 1
O29A O -0.1541(10) 0.9950(9) 1.0211(3) 0.045(4) Uani 0.394(3) 1 d D U P B 2
O30 O -0.0792(8) 0.9068(9) 0.9748(3) 0.040(3) Uani 0.606(3) 1 d D U P B 1
O30A O -0.1247(10) 1.1066(7) 1.0296(4) 0.040(3) Uani 0.394(3) 1 d D U P B 2
O31 O -0.0162(9) 0.9644(5) 0.9417(3) 0.041(3) Uani 0.606(3) 1 d D U P B 1
O31A O -0.0198(8) 1.1487(8) 1.0297(3) 0.041(6) Uani 0.394(3) 1 d D U P B 2
O32 O 0.0201(10) 0.8141(8) 0.9775(4) 0.049(5) Uani 0.606(3) 1 d D U P B 1
O32A O 0.0881(9) 1.1203(11) 0.9825(4) 0.036(4) Uani 0.394(3) 1 d D U P B 2
O33 O -0.003(2) 0.8415(8) 0.9331(3) 0.055(7) Uani 0.606(3) 1 d D U P B 1
O33A O 0.0756(7) 1.0570(5) 0.9467(3) 0.038(3) Uani 0.394(3) 1 d D U P B 2
O34 O 0.0901(9) 1.012(2) 0.9512(7) 0.041(4) Uani 0.606(3) 1 d D U P B 1
O34A O -0.0428(7) 0.8700(6) 0.9286(2) 0.054(8) Uani 0.394(3) 1 d D U P B 2
O35 O 0.0157(11) 1.065(2) 0.9103(3) 0.050(8) Uani 0.606(3) 1 d D U P B 1
O35A O -0.124(2) 1.2360(11) 1.0103(9) 0.046(9) Uani 0.394(3) 1 d D U P B 2
O36 O -0.2014(6) 1.1423(6) 0.9632(3) 0.051(7) Uani 0.606(3) 1 d D U P B 1
O36A O -0.169(2) 1.0317(17) 1.0703(8) 0.047(8) Uani 0.394(3) 1 d D U P B 2
O37 O -0.2030(9) 0.9063(9) 0.9854(5) 0.048(6) Uani 0.606(3) 1 d D U P B 1
O37A O -0.2121(7) 0.9094(7) 0.9999(3) 0.046(6) Uani 0.394(3) 1 d D U P B 2
O38 O -0.1140(16) 0.8584(11) 1.0155(5) 0.060(6) Uani 0.606(3) 1 d D U P B 1
O38A O 0.0336(6) 0.9499(9) 0.9434(4) 0.040(4) Uani 0.394(3) 1 d D U P B 2
O39 O -0.2077(10) 1.0800(13) 1.0520(6) 0.044(7) Uani 0.606(3) 1 d D U P B 1
O39A O 0.038(2) 1.187(2) 0.9394(7) 0.044(7) Uani 0.394(3) 1 d D U P B 2
W13 W -0.45302(6) 1.27459(6) 0.90504(2) 0.0191(3) Uani 1 1 d . U . . .
W14 W -0.58358(7) 1.55608(7) 0.89868(2) 0.0295(3) Uani 1 1 d . U . . .
W15 W -0.65116(6) 1.45480(6) 0.85503(2) 0.0241(3) Uani 1 1 d . U . . .
W19 W -0.54583(7) 1.42715(6) 0.93297(2) 0.0235(3) Uani 1 1 d . U . . .
W20 W -0.43376(6) 1.50848(6) 0.91184(2) 0.0216(3) Uani 1 1 d . U . . .
W21 W -0.54631(6) 1.54113(6) 0.83527(2) 0.0225(3) Uani 1 1 d . U . . .
W24 W -0.33684(6) 1.37128(6) 0.88343(2) 0.0186(3) Uani 1 1 d . U . . .
W26 W -0.38129(6) 1.49909(6) 0.85053(2) 0.0201(3) Uani 1 1 d . U . . .
W28 W -0.60119(6) 1.31597(6) 0.89279(2) 0.0233(3) Uani 1 1 d . U . . .
Ag Ag -0.7246(4) 1.4539(6) 0.80341(15) 0.041(3) Uani 0.364(12) 1 d . U P C 2
Ag1A Ag -0.4274(6) 1.1099(4) 0.88377(15) 0.039(2) Uani 0.356(9) 1 d . U P D 2
Ag2 Ag -0.3326(2) 1.2479(2) 0.83095(8) 0.0472(11) Uani 0.709(4) 1 d . U P E 7
Ag4 Ag -0.44670(13) 1.28190(13) 0.80255(4) 0.0303(6) Uani 1 1 d . U . . .
Ag6 Ag -0.63163(14) 1.29692(13) 0.95090(5) 0.0347(6) Uani 1 1 d . U . . .
Ag7 Ag -0.4459(6) 1.3921(6) 0.7742(2) 0.054(3) Uani 0.291(4) 1 d . U P E 8
Ag9 Ag -0.6035(2) 1.1588(3) 0.86948(11) 0.0409(14) Uani 0.644(9) 1 d . U P D 1
Ag9A Ag -0.6198(5) 1.1775(5) 0.8573(2) 0.045(2) Uani 0.356(9) 1 d . U P D 2
Ag10 Ag -0.24330(15) 1.41183(16) 0.92731(5) 0.0399(7) Uani 1 1 d . U . . .
Ag12 Ag -0.45202(15) 1.19620(15) 0.96419(5) 0.0377(7) Uani 1 1 d . U . . .
Ag15 Ag -0.5369(3) 1.3813(3) 0.76999(9) 0.0444(14) Uani 0.709(4) 1 d . U P E 7
Ag17 Ag -0.3812(2) 1.3785(2) 0.78167(8) 0.0450(11) Uani 0.709(4) 1 d . U P E 7
Ag18 Ag -0.49028(16) 1.28087(15) 0.84731(5) 0.0399(7) Uani 1 1 d . U . . .
Ag20 Ag -0.27282(14) 1.43251(15) 0.80186(5) 0.0401(7) Uani 1 1 d . U . . .
Ag24 Ag -0.30811(14) 1.58645(14) 0.89086(6) 0.0413(7) Uani 1 1 d . U . . .
Ag27 Ag -0.3816(6) 1.2031(6) 0.8387(2) 0.051(2) Uani 0.291(4) 1 d . U P E 8
Ag29 Ag -0.2970(7) 1.3136(7) 0.7992(2) 0.051(3) Uani 0.291(4) 1 d . U P E 8
Ag30 Ag -0.55207(16) 1.15186(15) 0.92047(5) 0.0433(7) Uani 1 1 d D U . . .
Ag33 Ag -0.3893(3) 1.1155(2) 0.88257(8) 0.0342(13) Uani 0.644(9) 1 d . U P D 1
Ag34 Ag -0.56637(17) 1.52418(16) 0.77337(6) 0.0483(8) Uani 1 1 d . U . . .
Ag35 Ag -0.5691(2) 1.2623(2) 0.81157(9) 0.0491(12) Uani 0.709(4) 1 d . U P E 7
Ag36 Ag -0.20543(14) 1.45360(17) 0.86495(5) 0.0440(8) Uani 1 1 d . U . . .
Ag37 Ag -0.7118(2) 1.4100(4) 0.79981(9) 0.0433(17) Uani 0.636(12) 1 d . U P C 1
Ag38 Ag -0.64304(16) 1.68424(15) 0.85368(6) 0.0483(8) Uani 1 1 d . U . . .
Ag44 Ag -0.5330(2) 1.3811(2) 0.81969(7) 0.0362(13) Uani 0.803(13) 1 d . U P C 1
Ag45 Ag -0.4510(3) 1.1556(3) 0.82788(12) 0.0751(17) Uani 0.709(4) 1 d . U P E 7
Ag46 Ag -0.75360(17) 1.58073(18) 0.87833(6) 0.0548(9) Uani 1 1 d . U . . .
Ag50 Ag -0.41005(17) 1.3605(2) 0.83142(6) 0.0568(10) Uani 1 1 d . U . . .
Ag54 Ag -0.70875(16) 1.5844(2) 0.81236(5) 0.0540(9) Uani 1 1 d . U . . .
Ag55 Ag -0.5146(7) 1.1755(6) 0.8218(2) 0.060(3) Uani 0.291(4) 1 d . U P E 8
Ag57 Ag -0.5838(6) 1.3283(6) 0.7989(2) 0.057(2) Uani 0.291(4) 1 d . U P E 8
Ag59 Ag -0.20626(18) 1.2990(3) 0.84960(8) 0.0817(15) Uani 1 1 d . U . . .
Ag61 Ag -0.5015(11) 1.4000(8) 0.8195(3) 0.036(4) Uani 0.197(13) 1 d . U P E 2
Cl2 Cl -0.4279(7) 1.2034(7) 0.7747(2) 0.073(4) Uani 1 1 d D U . . .
S2 S -0.5612(10) 1.1518(9) 0.8246(3) 0.069(4) Uani 0.709(4) 1 d D U P E 7
S7 S -0.6134(19) 1.232(2) 0.8113(7) 0.053(5) Uani 0.291(4) 1 d D U P E 8
S8 S -0.2245(4) 1.5000(5) 0.90042(18) 0.038(2) Uani 1 1 d . U . . .
S10 S -0.5628(5) 1.1965(5) 0.95679(16) 0.037(2) Uani 1 1 d . U . . .
S12 S -0.7368(5) 1.6480(5) 0.84434(19) 0.046(2) Uani 1 1 d . U . . .
S14 S -0.3113(9) 1.2881(9) 0.7995(4) 0.049(4) Uani 0.709(4) 1 d . U P E 7
S15 S -0.540(3) 1.363(3) 0.7733(9) 0.050(4) Uani 0.291(4) 1 d D U P E 8
S18 S -0.6791(5) 1.5177(7) 0.78196(19) 0.056(3) Uani 1 1 d . U . . .
S22 S -0.1905(5) 1.3976(7) 0.8311(2) 0.056(3) Uani 1 1 d . U . . .
S26 S -0.5053(8) 1.1016(7) 0.8854(3) 0.037(3) Uani 0.644(9) 1 d D U P D 1
S26A S -0.5445(15) 1.1160(13) 0.8848(5) 0.039(3) Uani 0.356(9) 1 d D U P D 2
S27 S -0.2738(18) 1.2188(17) 0.8289(7) 0.048(5) Uani 0.291(4) 1 d D U P E 8
S28 S -0.4561(8) 1.4335(8) 0.7563(3) 0.048(3) Uani 0.709(4) 1 d . U P E 7
S29 S -0.426(2) 1.104(2) 0.8357(6) 0.066(5) Uani 0.291(4) 1 d D U P E 8
S30 S -0.6233(7) 1.3318(8) 0.7824(3) 0.048(3) Uani 0.709(4) 1 d D U P E 7
S31 S -0.3312(19) 1.3872(19) 0.7732(7) 0.050(5) Uani 0.291(4) 1 d D U P E 8
S32 S -0.3501(8) 1.1442(8) 0.8412(3) 0.054(3) Uani 0.709(4) 1 d . U P E 7
P5 P -0.8071(8) 1.3939(9) 0.8191(3) 0.087(4) Uani 1 1 d D U . . .
P7 P -0.3474(5) 1.6912(5) 0.8780(2) 0.042(2) Uani 1 1 d . U . . .
P9 P -0.3188(7) 1.0803(6) 0.9105(2) 0.060(3) Uani 1 1 d . U . . .
P12 P -0.7192(5) 1.3645(5) 0.96714(17) 0.034(2) Uani 1 1 d . U . . .
P13 P -0.2411(5) 1.3771(5) 0.96667(17) 0.0337(19) Uani 1 1 d . U . . .
P16 P -0.5176(5) 1.6095(5) 0.75874(18) 0.037(2) Uani 1 1 d . U . . .
P17 P -0.2688(5) 1.5288(5) 0.78043(17) 0.034(2) Uani 1 1 d . U . . .
P18 P -0.5826(5) 1.7562(5) 0.86453(19) 0.042(2) Uani 1 1 d . U . . .
P20 P -0.3850(5) 1.1978(5) 0.99421(17) 0.035(2) Uani 1 1 d . U . . .
P21 P -0.7177(10) 1.1738(10) 0.8701(4) 0.100(4) Uani 1 1 d . U . . .
P22 P -0.7998(6) 1.5853(6) 0.9156(2) 0.050(2) Uani 1 1 d . U . . .
P24 P -0.1605(8) 1.2231(8) 0.8754(3) 0.079(3) Uani 1 1 d . U . . .
Si4 Si -0.4986(4) 1.4198(4) 0.87498(14) 0.0140(15) Uani 1 1 d . U . . .
O45 O -0.6353(11) 1.6230(11) 0.9048(4) 0.032(5) Uani 1 1 d . U . . .
O46 O -0.6636(11) 1.2892(11) 0.9078(4) 0.032(5) Uani 1 1 d . U . . .
O48 O -0.3401(10) 1.5586(11) 0.8431(4) 0.027(5) Uani 1 1 d . U . . .
O50 O -0.4239(10) 1.2217(10) 0.9264(3) 0.022(4) Uani 1 1 d . U . . .
O52 O -0.3861(10) 1.3166(10) 0.8987(4) 0.021(3) Uani 1 1 d . U . . .
O54 O -0.5832(10) 1.2684(10) 0.8688(4) 0.022(4) Uani 1 1 d . U . . .
O56 O -0.5378(10) 1.2678(10) 0.9119(4) 0.022(3) Uani 1 1 d . U . . .
O58 O -0.5356(11) 1.4932(11) 0.8118(4) 0.029(4) Uani 1 1 d . U . . .
O60 O -0.3811(10) 1.4286(10) 0.9088(4) 0.023(4) Uani 1 1 d . U . . .
O62 O -0.5480(9) 1.4499(9) 0.8557(4) 0.018(3) Uani 1 1 d . U . . .
O64 O -0.6423(11) 1.4107(11) 0.8304(4) 0.028(4) Uani 1 1 d . U . . .
O66 O -0.4644(10) 1.5348(10) 0.8425(3) 0.019(3) Uani 1 1 d . U . . .
O68 O -0.6415(10) 1.5035(11) 0.8865(4) 0.027(5) Uani 1 1 d . U . . .
O70 O -0.5679(11) 1.4108(11) 0.9604(4) 0.026(4) Uani 1 1 d . U . . .
O72 O -0.5617(12) 1.6179(12) 0.8237(4) 0.035(5) Uani 1 1 d . U . . .
O74 O -0.7314(10) 1.4787(10) 0.8560(4) 0.024(4) Uani 1 1 d . U . . .
O76 O -0.2675(10) 1.3529(10) 0.8983(4) 0.022(4) Uani 1 1 d . U . . .
O78 O -0.5632(10) 1.5720(10) 0.8692(4) 0.023(4) Uani 1 1 d . U . . .
O82 O -0.4144(10) 1.5306(10) 0.8826(4) 0.023(4) Uani 1 1 d . U . . .
O84 O -0.3194(10) 1.4482(10) 0.8687(4) 0.022(3) Uani 1 1 d . U . . .
O88 O -0.5975(10) 1.5039(10) 0.9268(3) 0.020(3) Uani 1 1 d . U . . .
O90 O -0.3649(10) 1.4528(10) 0.8266(4) 0.020(3) Uani 1 1 d . U . . .
O92 O -0.4261(9) 1.4152(10) 0.8663(4) 0.019(3) Uani 1 1 d . U . . .
O94 O -0.4771(10) 1.3533(10) 0.9261(4) 0.021(4) Uani 1 1 d . U . . .
O96 O -0.6406(10) 1.3888(11) 0.8766(4) 0.026(3) Uani 1 1 d . U . . .
O98 O -0.6346(10) 1.5326(10) 0.8407(4) 0.023(3) Uani 1 1 d . U . . .
O100 O -0.3908(11) 1.5504(11) 0.9264(4) 0.028(5) Uani 1 1 d . U . . .
O102 O -0.5094(10) 1.5706(10) 0.9099(4) 0.023(3) Uani 1 1 d . U . . .
O104 O -0.5103(9) 1.3486(9) 0.8827(4) 0.019(3) Uani 1 1 d . U . . .
O105 O -0.4405(10) 1.2277(9) 0.8806(3) 0.017(3) Uani 1 1 d . U . . .
O107 O -0.3193(10) 1.3268(10) 0.8585(4) 0.022(4) Uani 1 1 d . U . . .
O108 O -0.5110(9) 1.4608(9) 0.8971(4) 0.017(3) Uani 1 1 d . U . . .
O109 O -0.4800(10) 1.4712(10) 0.9371(3) 0.021(3) Uani 1 1 d . U . . .
O111 O -0.5946(10) 1.3847(10) 0.9170(3) 0.020(3) Uani 1 1 d . U . . .
C1 C -0.572(3) 1.365(4) 0.7459(10) 0.049(4) Uani 0.291(4) 1 d D U P E 8
H1 H -0.605691 1.401238 0.744108 0.059 Uiso 0.291(4) 1 calc R U P E 8
C4 C -0.7320(18) 1.559(2) 0.7604(7) 0.062(5) Uani 1 1 d D U . . .
H4 H -0.724364 1.602058 0.757588 0.074 Uiso 1 1 calc R U . . .
C6 C -0.547(2) 1.800(2) 0.8410(8) 0.052(4) Uani 1 1 d . U . . .
C8 C -0.3056(18) 1.4176(18) 0.9824(7) 0.036(4) Uani 1 1 d . U . . .
C10 C -0.3104(19) 1.4145(18) 1.0069(7) 0.038(5) Uani 1 1 d . U . . .
H10 H -0.277951 1.393297 1.015344 0.046 Uiso 1 1 calc R U . . .
C12 C -0.3782(13) 1.7468(11) 0.8992(4) 0.044(4) Uani 1 1 d G U . . .
C14 C -0.3733(13) 1.8095(12) 0.8974(4) 0.047(5) Uani 1 1 d G U . . .
H14 H -0.353815 1.825585 0.884547 0.056 Uiso 1 1 calc R U . . .
C16 C -0.3974(14) 1.8484(9) 0.9148(5) 0.050(5) Uani 1 1 d G U . . .
H16 H -0.394122 1.890385 0.913632 0.059 Uiso 1 1 calc R U . . .
C18 C -0.4265(14) 1.8244(11) 0.9340(4) 0.050(5) Uani 1 1 d G U . . .
H18 H -0.442653 1.850378 0.945681 0.060 Uiso 1 1 calc R U . . .
C20 C -0.4314(13) 1.7616(12) 0.9358(4) 0.049(5) Uani 1 1 d G U . . .
H20 H -0.450879 1.745571 0.948645 0.058 Uiso 1 1 calc R U . . .
C22 C -0.4073(13) 1.7228(9) 0.9184(5) 0.045(5) Uani 1 1 d G U . . .
H22 H -0.410572 1.680771 0.919561 0.054 Uiso 1 1 calc R U . . .
C24 C -0.3967(17) 1.5677(18) 0.7763(7) 0.037(5) Uani 1 1 d . U . . .
H24A H -0.387482 1.548440 0.761781 0.044 Uiso 1 1 calc R U . . .
H24B H -0.406866 1.536056 0.787348 0.044 Uiso 1 1 calc R U . . .
C26 C -0.617(2) 1.790(2) 0.7453(8) 0.053(6) Uani 1 1 d . U . . .
H26 H -0.616165 1.823519 0.734980 0.064 Uiso 1 1 calc R U . . .
C28 C -0.294(2) 1.756(2) 0.8419(9) 0.057(5) Uani 1 1 d . U . . .
H28 H -0.331491 1.759308 0.834754 0.068 Uiso 1 1 calc R U . . .
C30 C -0.3371(17) 1.5913(18) 0.7836(7) 0.035(4) Uani 1 1 d . U . . .
H30A H -0.342726 1.603165 0.799284 0.042 Uiso 1 1 calc R U . . .
H30B H -0.330433 1.627706 0.774210 0.042 Uiso 1 1 calc R U . . .
C32 C -0.5162(19) 1.7232(19) 0.8824(7) 0.042(5) Uani 1 1 d . U . . .
H32A H -0.495912 1.756628 0.886848 0.050 Uiso 1 1 calc R U . . .
H32B H -0.531802 1.703279 0.896099 0.050 Uiso 1 1 calc R U . . .
C34 C -0.629(3) 1.131(3) 0.7918(9) 0.066(8) Uani 0.709(4) 1 d D U P E 7
H34A H -0.659499 1.119528 0.802757 0.100 Uiso 0.709(4) 1 d R U P E 7
H34B H -0.632969 1.112598 0.777637 0.100 Uiso 0.709(4) 1 d R U P E 7
H34C H -0.634569 1.175338 0.789607 0.100 Uiso 0.709(4) 1 d R U P E 7
C36 C -0.3557(18) 1.4520(18) 0.9711(7) 0.038(5) Uani 1 1 d . U . . .
H36 H -0.352733 1.453992 0.955351 0.045 Uiso 1 1 calc R U . . .
C38 C -0.647(4) 1.196(4) 0.7893(15) 0.057(6) Uani 0.291(4) 1 d D U P E 8
H38 H -0.679856 1.173486 0.795294 0.068 Uiso 0.291(4) 1 calc R U P E 8
C40 C -0.7928(11) 1.3495(15) 0.9581(5) 0.050(4) Uani 1 1 d G U . . .
C42 C -0.7972(13) 1.3212(16) 0.9379(5) 0.064(6) Uani 1 1 d G U . . .
H42 H -0.761497 1.308697 0.928755 0.076 Uiso 1 1 calc R U . . .
C44 C -0.8549(16) 1.3116(16) 0.9312(5) 0.070(6) Uani 1 1 d G U . . .
H44 H -0.857818 1.292699 0.917695 0.084 Uiso 1 1 calc R U . . .
C46 C -0.9082(12) 1.3303(17) 0.9449(6) 0.068(6) Uani 1 1 d G U . . .
H46 H -0.946849 1.323878 0.940442 0.081 Uiso 1 1 calc R U . . .
C48 C -0.9039(12) 1.3586(16) 0.9651(5) 0.063(6) Uani 1 1 d G U . . .
H48 H -0.939560 1.371055 0.974249 0.075 Uiso 1 1 calc R U . . .
C50 C -0.8462(14) 1.3681(15) 0.9718(4) 0.058(5) Uani 1 1 d G U . . .
H50 H -0.843240 1.387053 0.985310 0.070 Uiso 1 1 calc R U . . .
C52 C -0.415(2) 1.476(2) 1.0063(7) 0.043(5) Uani 1 1 d . U . . .
H52 H -0.451544 1.492562 1.014074 0.052 Uiso 1 1 calc R U . . .
C54 C -0.264(2) 1.546(2) 0.7110(8) 0.052(5) Uani 1 1 d . U . . .
H54 H -0.286712 1.570046 0.699783 0.062 Uiso 1 1 calc R U . . .
C56 C -0.643(2) 1.294(2) 0.7605(6) 0.052(5) Uani 0.709(4) 1 d D U P E 7
H56 H -0.672360 1.267317 0.766830 0.062 Uiso 0.709(4) 1 calc R U P E 7
C58 C -0.187(2) 1.777(2) 0.8422(9) 0.059(6) Uani 1 1 d . U . . .
H58 H -0.153687 1.791029 0.834454 0.071 Uiso 1 1 calc R U . . .
C60 C -0.4544(18) 1.6207(19) 0.7742(7) 0.038(4) Uani 1 1 d . U . . .
H60A H -0.439503 1.657342 0.767519 0.045 Uiso 1 1 calc R U . . .
H60B H -0.470304 1.630542 0.789463 0.045 Uiso 1 1 calc R U . . .
C62 C -0.196(2) 1.164(3) 0.8886(10) 0.074(5) Uani 1 1 d D U . . .
H62A H -0.199770 1.134843 0.877279 0.089 Uiso 1 1 calc R U . . .
H62B H -0.168360 1.142705 0.899802 0.089 Uiso 1 1 calc R U . . .
C64 C -0.763(3) 1.258(3) 0.8672(12) 0.094(6) Uani 1 1 d . U . . .
H64A H -0.806807 1.255694 0.867524 0.113 Uiso 1 1 calc R U . . .
H64B H -0.755419 1.279308 0.880477 0.113 Uiso 1 1 calc R U . . .
C66 C -0.5064(19) 1.0296(19) 0.8842(7) 0.044(4) Uani 0.644(9) 1 d D U P D 1
H66 H -0.531511 1.028497 0.871039 0.052 Uiso 0.644(9) 1 calc R U P D 1
C68 C -0.521(4) 1.0332(16) 0.8821(13) 0.043(4) Uani 0.356(9) 1 d D U P D 2
H68 H -0.503817 1.023140 0.897135 0.052 Uiso 0.356(9) 1 calc R U P D 2
C70 C -0.447(3) 0.9897(14) 0.8774(12) 0.050(7) Uani 0.644(9) 1 d D U P D 1
H70A H -0.430837 1.003372 0.862879 0.076 Uiso 0.644(9) 1 d R U P D 1
H70B H -0.451777 0.946832 0.876908 0.076 Uiso 0.644(9) 1 d R U P D 1
H70C H -0.418797 0.993892 0.888889 0.076 Uiso 0.644(9) 1 d R U P D 1
C72 C -0.473(4) 0.991(4) 0.8689(19) 0.046(8) Uani 0.356(9) 1 d D U P D 2
H72A H -0.483295 0.985164 0.853721 0.069 Uiso 0.356(9) 1 d R U P D 2
H72B H -0.464765 0.951794 0.877101 0.069 Uiso 0.356(9) 1 d R U P D 2
H72C H -0.436255 1.010504 0.868431 0.069 Uiso 0.356(9) 1 d R U P D 2
C74 C -0.291(2) 1.086(3) 0.8221(12) 0.058(5) Uani 0.709(4) 1 d D U P E 7
H74 H -0.291750 1.104550 0.806508 0.070 Uiso 0.709(4) 1 calc R U P E 7
C76 C -0.4193(12) 1.2609(10) 1.0130(4) 0.039(4) Uani 1 1 d G U . . .
C78 C -0.4703(12) 1.3028(12) 1.0053(3) 0.041(5) Uani 1 1 d G U . . .
H78 H -0.485572 1.298565 0.991206 0.049 Uiso 1 1 calc R U . . .
C80 C -0.4986(11) 1.3511(11) 1.0188(4) 0.046(5) Uani 1 1 d G U . . .
H80 H -0.532723 1.379097 1.013723 0.055 Uiso 1 1 calc R U . . .
C82 C -0.4758(12) 1.3574(11) 1.0400(4) 0.045(5) Uani 1 1 d G U . . .
H82 H -0.494742 1.389676 1.048986 0.054 Uiso 1 1 calc R U . . .
C84 C -0.4248(12) 1.3155(12) 1.0476(3) 0.044(5) Uani 1 1 d G U . . .
H84 H -0.409609 1.319725 1.061731 0.053 Uiso 1 1 calc R U . . .
C86 C -0.3966(11) 1.2672(11) 1.0341(4) 0.043(5) Uani 1 1 d G U . . .
H86 H -0.362457 1.239192 1.039214 0.052 Uiso 1 1 calc R U . . .
C88 C -0.185(5) 1.153(4) 0.8046(17) 0.052(9) Uani 0.291(4) 1 d D U P E 8
H88A H -0.166582 1.190079 0.803300 0.078 Uiso 0.291(4) 1 d R U P E 8
H88B H -0.215312 1.155389 0.793100 0.078 Uiso 0.291(4) 1 d R U P E 8
H88C H -0.153842 1.117119 0.802770 0.078 Uiso 0.291(4) 1 d R U P E 8
C90 C -0.377(2) 1.128(2) 1.0130(7) 0.045(4) Uani 1 1 d . U . . .
C92 C -0.311(4) 1.348(6) 0.7471(13) 0.051(6) Uani 0.291(4) 1 d D U P E 8
H92 H -0.316291 1.307105 0.753818 0.061 Uiso 0.291(4) 1 calc R U P E 8
C94 C -0.752(2) 1.5423(19) 0.9404(7) 0.044(5) Uani 1 1 d . U . . .
H94A H -0.711457 1.554289 0.939996 0.053 Uiso 1 1 calc R U . . .
H94B H -0.773628 1.554078 0.954788 0.053 Uiso 1 1 calc R U . . .
C96 C -0.748(3) 1.293(3) 0.8482(12) 0.088(6) Uani 1 1 d . U . . .
H96A H -0.750827 1.269767 0.834725 0.106 Uiso 1 1 calc R U . . .
H96B H -0.706300 1.301010 0.848777 0.106 Uiso 1 1 calc R U . . .
C98 C -0.597(2) 1.192(2) 1.0022(8) 0.058(8) Uani 1 1 d . U . . .
H98A H -0.626226 1.230810 1.001449 0.087 Uiso 1 1 d R U . . .
H98B H -0.555866 1.200720 1.003509 0.087 Uiso 1 1 d R U . . .
H98C H -0.608226 1.167380 1.015239 0.087 Uiso 1 1 d R U . . .
C100 C -0.3042(17) 1.2733(17) 0.9746(6) 0.032(4) Uani 1 1 d . U . . .
H10A H -0.337140 1.304799 0.980594 0.039 Uiso 1 1 calc R U . . .
H10B H -0.312112 1.267616 0.958896 0.039 Uiso 1 1 calc R U . . .
C102 C -0.597(2) 1.158(2) 0.9815(7) 0.045(5) Uani 1 1 d . U . . .
H102 H -0.571688 1.116465 0.983923 0.054 Uiso 1 1 calc R U . . .
C104 C -0.7457(19) 1.4751(18) 0.9384(7) 0.040(5) Uani 1 1 d . U . . .
H10C H -0.713259 1.460293 0.927133 0.049 Uiso 1 1 calc R U . . .
H10D H -0.784573 1.463442 0.934415 0.049 Uiso 1 1 calc R U . . .
C106 C -0.1742(12) 1.3968(14) 0.9798(5) 0.048(4) Uani 1 1 d G U . . .
C108 C -0.1287(14) 1.3516(10) 0.9893(5) 0.055(5) Uani 1 1 d G U . . .
H108 H -0.133685 1.310005 0.990125 0.066 Uiso 1 1 calc R U . . .
C110 C -0.0757(13) 1.3685(13) 0.9975(5) 0.060(6) Uani 1 1 d G U . . .
H110 H -0.045258 1.338255 1.003814 0.072 Uiso 1 1 calc R U . . .
C112 C -0.0683(12) 1.4306(15) 0.9962(6) 0.061(6) Uani 1 1 d G U . . .
H112 H -0.032829 1.441963 1.001677 0.073 Uiso 1 1 calc R U . . .
C114 C -0.1138(15) 1.4758(11) 0.9867(6) 0.062(6) Uani 1 1 d G U . . .
H114 H -0.108825 1.517421 0.985851 0.074 Uiso 1 1 calc R U . . .
C116 C -0.1668(13) 1.4589(12) 0.9785(5) 0.058(5) Uani 1 1 d G U . . .
H116 H -0.197251 1.489173 0.972162 0.070 Uiso 1 1 calc R U . . .
C118 C -0.125(2) 1.562(2) 0.8857(8) 0.054(8) Uani 1 1 d . U . . .
H11A H -0.102642 1.528888 0.876807 0.081 Uiso 1 1 calc R U . . .
H11B H -0.096346 1.587692 0.890067 0.081 Uiso 1 1 calc R U . . .
H11C H -0.156649 1.586664 0.876886 0.081 Uiso 1 1 calc R U . . .
C120 C -0.3654(19) 1.4444(19) 1.0174(7) 0.042(5) Uani 1 1 d . U . . .
H120 H -0.368367 1.442754 1.033229 0.050 Uiso 1 1 calc R U . . .
C122 C -0.7272(19) 1.4479(18) 0.9632(7) 0.040(4) Uani 1 1 d . U . . .
H12A H -0.758649 1.466974 0.974103 0.048 Uiso 1 1 calc R U . . .
H12B H -0.687962 1.460151 0.966468 0.048 Uiso 1 1 calc R U . . .
C124 C -0.493(3) 1.876(3) 0.8264(9) 0.064(6) Uani 1 1 d . U . . .
H124 H -0.485171 1.915288 0.828626 0.077 Uiso 1 1 calc R U . . .
C126 C -0.2397(17) 1.2941(17) 0.9761(6) 0.034(4) Uani 1 1 d . U . . .
H12C H -0.208898 1.267911 0.966702 0.041 Uiso 1 1 calc R U . . .
H12D H -0.226951 1.287933 0.991627 0.041 Uiso 1 1 calc R U . . .
C128 C -0.2090(11) 1.5698(13) 0.7912(4) 0.042(4) Uani 1 1 d G U . . .
C130 C -0.2163(11) 1.5861(13) 0.8137(4) 0.046(5) Uani 1 1 d G U . . .
H130 H -0.250404 1.576978 0.822648 0.055 Uiso 1 1 calc R U . . .
C132 C -0.1727(13) 1.6159(14) 0.8229(3) 0.049(5) Uani 1 1 d G U . . .
H132 H -0.177669 1.626849 0.838025 0.058 Uiso 1 1 calc R U . . .
C134 C -0.1218(12) 1.6295(14) 0.8096(5) 0.050(5) Uani 1 1 d G U . . .
H134 H -0.092644 1.649531 0.815773 0.060 Uiso 1 1 calc R U . . .
C136 C -0.1144(11) 1.6132(14) 0.7871(4) 0.051(5) Uani 1 1 d G U . . .
H136 H -0.080353 1.622342 0.778143 0.061 Uiso 1 1 calc R U . . .
C138 C -0.1580(13) 1.5834(14) 0.7778(3) 0.048(5) Uani 1 1 d G U . . .
H138 H -0.153088 1.572470 0.762765 0.058 Uiso 1 1 calc R U . . .
C140 C -0.0950(17) 1.1716(18) 0.8586(7) 0.083(5) Uani 1 1 d G U . . .
C142 C -0.059(2) 1.126(2) 0.8719(5) 0.085(7) Uani 1 1 d G U . . .
H142 H -0.067543 1.122823 0.887480 0.102 Uiso 1 1 calc R U . . .
C144 C -0.0112(19) 1.0842(18) 0.8618(7) 0.088(7) Uani 1 1 d G U . . .
H144 H 0.012756 1.053519 0.870672 0.105 Uiso 1 1 calc R U . . .
C146 C 0.0012(18) 1.0886(18) 0.8385(7) 0.090(7) Uani 1 1 d G U . . .
H146 H 0.033414 1.060796 0.831748 0.108 Uiso 1 1 calc R U . . .
C148 C -0.035(2) 1.134(2) 0.8252(5) 0.091(7) Uani 1 1 d G U . . .
H148 H -0.026225 1.137376 0.809632 0.109 Uiso 1 1 calc R U . . .
C150 C -0.0826(19) 1.1760(18) 0.8353(7) 0.088(7) Uani 1 1 d G U . . .
H150 H -0.106525 1.206681 0.826439 0.105 Uiso 1 1 calc R U . . .
C152 C -0.543(3) 1.0013(17) 0.9024(10) 0.046(7) Uani 0.644(9) 1 d D U P D 1
H15A H -0.517920 0.996577 0.915444 0.070 Uiso 0.644(9) 1 d R U P D 1
H15B H -0.552020 0.961287 0.898904 0.070 Uiso 0.644(9) 1 d R U P D 1
H15C H -0.581540 1.028977 0.905684 0.070 Uiso 0.644(9) 1 d R U P D 1
C154 C -0.324(2) 1.087(2) 1.0159(8) 0.050(5) Uani 1 1 d . U . . .
H154 H -0.288552 1.093667 1.007101 0.061 Uiso 1 1 calc R U . . .
C156 C -0.3023(18) 1.2121(18) 0.9885(7) 0.036(4) Uani 1 1 d . U . . .
H15D H -0.282751 1.214270 1.002694 0.043 Uiso 1 1 calc R U . . .
H15E H -0.278226 1.178105 0.980158 0.043 Uiso 1 1 calc R U . . .
C158 C -0.825(3) 1.734(3) 0.8199(6) 0.080(10) Uani 1 1 d D U . . .
H15F H -0.869307 1.737066 0.820107 0.119 Uiso 1 1 d R U . . .
H15G H -0.805757 1.698316 0.811377 0.119 Uiso 1 1 d R U . . .
H15H H -0.812777 1.770756 0.812917 0.119 Uiso 1 1 d R U . . .
C160 C -0.316(3) 1.027(3) 0.8219(12) 0.058(8) Uani 0.709(4) 1 d D U P E 7
H16A H -0.351352 1.029681 0.832462 0.088 Uiso 0.709(4) 1 d R U P E 7
H16B H -0.284072 0.993571 0.826702 0.088 Uiso 0.709(4) 1 d R U P E 7
H16C H -0.328212 1.020051 0.807062 0.088 Uiso 0.709(4) 1 d R U P E 7
C162 C -0.4074(19) 1.4822(19) 0.9811(7) 0.041(5) Uani 1 1 d . U . . .
H162 H -0.438066 1.506672 0.972664 0.049 Uiso 1 1 calc R U . . .
C164 C -0.3342(19) 0.9911(19) 0.9741(7) 0.042(5) Uani 1 1 d . U . . .
H164 H -0.307432 0.968755 0.984564 0.050 Uiso 1 1 calc R U . . .
C166 C -0.3992(19) 1.000(2) 0.9783(7) 0.043(5) Uani 1 1 d . U . . .
H166 H -0.416521 0.983789 0.991449 0.051 Uiso 1 1 calc R U . . .
C168 C -0.310(2) 1.017(2) 0.9534(7) 0.045(5) Uani 1 1 d . U . . .
H168 H -0.267463 1.012189 0.950478 0.054 Uiso 1 1 calc R U . . .
C170 C -0.412(2) 1.0573(19) 0.9415(7) 0.042(5) Uani 1 1 d . U . . .
H170 H -0.438561 1.077808 0.930744 0.051 Uiso 1 1 calc R U . . .
C172 C -0.067(2) 1.402(3) 0.8354(8) 0.066(9) Uani 1 1 d D U . . .
H17A H -0.085964 1.429048 0.847136 0.099 Uiso 1 1 d R U . . .
H17B H -0.029404 1.416178 0.829436 0.099 Uiso 1 1 d R U . . .
H17C H -0.056474 1.360338 0.841656 0.099 Uiso 1 1 d R U . . .
C174 C -0.219(2) 1.495(2) 0.7040(9) 0.054(6) Uani 1 1 d . U . . .
H174 H -0.209562 1.485225 0.688846 0.065 Uiso 1 1 calc R U . . .
C176 C -0.248(2) 1.0980(18) 0.8333(17) 0.057(8) Uani 0.291(4) 1 d D U P E 8
H17D H -0.282892 1.110953 0.843476 0.085 Uiso 0.291(4) 1 d R U P E 8
H17E H -0.222211 1.061573 0.839746 0.085 Uiso 0.291(4) 1 d R U P E 8
H17F H -0.261981 1.088583 0.819006 0.085 Uiso 0.291(4) 1 d R U P E 8
C178 C -0.351(2) 1.050(2) 0.9370(8) 0.048(4) Uani 1 1 d . U . . .
C180 C -0.361(4) 1.350(7) 0.731(2) 0.051(7) Uani 0.291(4) 1 d D U P E 8
H18A H -0.348133 1.371252 0.717181 0.076 Uiso 0.291(4) 1 d R U P E 8
H18B H -0.396203 1.376102 0.738021 0.076 Uiso 0.291(4) 1 d R U P E 8
H18C H -0.371923 1.311392 0.727471 0.076 Uiso 0.291(4) 1 d R U P E 8
C182 C -0.247(4) 1.325(7) 0.738(2) 0.050(9) Uani 0.291(4) 1 d D U P E 8
H18D H -0.216580 1.348530 0.742455 0.074 Uiso 0.291(4) 1 d R U P E 8
H18E H -0.248860 1.328770 0.721575 0.074 Uiso 0.291(4) 1 d R U P E 8
H18F H -0.234900 1.282100 0.742535 0.074 Uiso 0.291(4) 1 d R U P E 8
C184 C -0.1301(18) 1.2627(18) 0.8984(6) 0.077(5) Uani 1 1 d G U . . .
C186 C -0.1089(19) 1.3184(18) 0.8929(5) 0.076(6) Uani 1 1 d G U . . .
H186 H -0.112247 1.336095 0.878220 0.091 Uiso 1 1 calc R U . . .
C188 C -0.0827(18) 1.3478(15) 0.9093(7) 0.080(7) Uani 1 1 d G U . . .
H188 H -0.068443 1.385054 0.905635 0.096 Uiso 1 1 calc R U . . .
C190 C -0.0776(18) 1.3214(18) 0.9312(6) 0.081(7) Uani 1 1 d G U . . .
H190 H -0.060082 1.341010 0.942220 0.097 Uiso 1 1 calc R U . . .
C192 C -0.0989(19) 1.2657(18) 0.9367(5) 0.082(7) Uani 1 1 d G U . . .
H192 H -0.095524 1.248005 0.951390 0.098 Uiso 1 1 calc R U . . .
C194 C -0.1251(19) 1.2363(15) 0.9203(7) 0.080(6) Uani 1 1 d G U . . .
H194 H -0.139329 1.199045 0.923975 0.096 Uiso 1 1 calc R U . . .
C196 C -0.519(5) 1.371(6) 0.7296(10) 0.051(11) Uani 0.291(4) 1 d D U P E 8
H19A H -0.491324 1.334241 0.726657 0.077 Uiso 0.291(4) 1 d R U P E 8
H19B H -0.503294 1.400011 0.737167 0.077 Uiso 0.291(4) 1 d R U P E 8
H19C H -0.531724 1.390971 0.714017 0.077 Uiso 0.291(4) 1 d R U P E 8
C198 C -0.2481(15) 1.0211(15) 0.9015(6) 0.071(5) Uani 1 1 d G U . . .
C200 C -0.2571(14) 0.9793(18) 0.8855(6) 0.075(6) Uani 1 1 d G U . . .
H200 H -0.295592 0.982752 0.879085 0.090 Uiso 1 1 calc R U . . .
C202 C -0.2085(18) 0.9323(16) 0.8792(6) 0.076(7) Uani 1 1 d G U . . .
H202 H -0.214434 0.904372 0.868510 0.091 Uiso 1 1 calc R U . . .
C204 C -0.1509(15) 0.9272(16) 0.8888(7) 0.079(7) Uani 1 1 d G U . . .
H204 H -0.118355 0.895733 0.884589 0.094 Uiso 1 1 calc R U . . .
C206 C -0.1419(14) 0.9689(18) 0.9048(6) 0.077(7) Uani 1 1 d G U . . .
H206 H -0.103434 0.965474 0.911243 0.093 Uiso 1 1 calc R U . . .
C208 C -0.1906(18) 1.0159(16) 0.9111(6) 0.075(6) Uani 1 1 d G U . . .
H208 H -0.184591 1.043854 0.921818 0.090 Uiso 1 1 calc R U . . .
C210 C -0.431(2) 1.113(2) 1.0246(8) 0.050(5) Uani 1 1 d . U . . .
H210 H -0.468166 1.141066 1.023290 0.060 Uiso 1 1 calc R U . . .
C212 C -0.245(2) 1.519(2) 0.7504(7) 0.044(4) Uani 1 1 d . U . . .
C214 C -0.913(2) 1.4666(19) 0.8050(7) 0.104(7) Uani 1 1 d G U . . .
H214 H -0.910374 1.437597 0.793821 0.125 Uiso 1 1 calc R U . . .
C216 C -0.9606(19) 1.518(2) 0.8047(8) 0.107(8) Uani 1 1 d G U . . .
H216 H -0.989361 1.523934 0.793381 0.128 Uiso 1 1 calc R U . . .
C218 C -0.9650(18) 1.5618(16) 0.8214(9) 0.108(8) Uani 1 1 d G U . . .
H218 H -0.996655 1.596405 0.821184 0.129 Uiso 1 1 calc R U . . .
C220 C -0.922(2) 1.5535(17) 0.8383(8) 0.107(8) Uani 1 1 d G U . . .
H220 H -0.924962 1.582540 0.849427 0.128 Uiso 1 1 calc R U . . .
C222 C -0.8747(18) 1.502(2) 0.8385(7) 0.104(7) Uani 1 1 d G U . . .
H222 H -0.845974 1.496204 0.849868 0.125 Uiso 1 1 calc R U . . .
C224 C -0.8703(17) 1.4583(16) 0.8219(9) 0.097(6) Uani 1 1 d DG U . . .
C226 C -0.802(2) 1.7124(17) 0.8426(7) 0.060(5) Uani 1 1 d D U . . .
H226 H -0.835124 1.688941 0.847535 0.072 Uiso 1 1 calc R U . . .
C228 C -0.753(2) 1.148(2) 0.8972(7) 0.104(6) Uani 1 1 d G U . . .
C230 C -0.748(2) 1.177(2) 0.9172(9) 0.107(7) Uani 1 1 d G U . . .
H230 H -0.723478 1.208243 0.917284 0.128 Uiso 1 1 calc R U . . .
C232 C -0.778(2) 1.159(2) 0.9372(7) 0.109(8) Uani 1 1 d G U . . .
H232 H -0.774123 1.178282 0.950579 0.130 Uiso 1 1 calc R U . . .
C234 C -0.814(2) 1.113(2) 0.9371(7) 0.109(8) Uani 1 1 d G U . . .
H234 H -0.834453 1.100500 0.950407 0.131 Uiso 1 1 calc R U . . .
C236 C -0.820(2) 1.084(2) 0.9170(9) 0.109(8) Uani 1 1 d G U . . .
H236 H -0.844138 1.052679 0.916940 0.130 Uiso 1 1 calc R U . . .
C238 C -0.790(2) 1.102(2) 0.8971(7) 0.107(7) Uani 1 1 d G U . . .
H238 H -0.793493 1.082639 0.883646 0.129 Uiso 1 1 calc R U . . .
C240 C -0.259(2) 1.266(3) 0.7764(9) 0.049(4) Uani 0.709(4) 1 d D U P E 7
H240 H -0.282823 1.237877 0.769355 0.059 Uiso 0.709(4) 1 calc R U P E 7
C242 C -0.157(2) 1.532(2) 0.9084(8) 0.046(5) Uani 1 1 d . U . . .
H242 H -0.126461 1.496805 0.913717 0.055 Uiso 1 1 calc R U . . .
C244 C -0.517(2) 1.845(2) 0.8457(9) 0.059(5) Uani 1 1 d . U . . .
H244 H -0.511325 1.855102 0.860445 0.070 Uiso 1 1 calc R U . . .
C246 C -0.277(2) 1.561(2) 0.7327(8) 0.047(5) Uani 1 1 d . U . . .
H246 H -0.304840 1.597295 0.736357 0.056 Uiso 1 1 calc R U . . .
C248 C -0.797(3) 1.357(3) 0.8473(11) 0.086(6) Uani 1 1 d . U . . .
H24C H -0.783712 1.385988 0.857080 0.103 Uiso 1 1 calc R U . . .
H24D H -0.837723 1.349154 0.853444 0.103 Uiso 1 1 calc R U . . .
C250 C -0.429(2) 1.061(2) 1.0375(8) 0.053(5) Uani 1 1 d . U . . .
H250 H -0.465637 1.049658 1.044153 0.064 Uiso 1 1 calc R U . . .
C252 C -0.240(3) 1.301(3) 0.7558(9) 0.049(7) Uani 0.709(4) 1 d D U P E 7
H25A H -0.273560 1.307986 0.745464 0.073 Uiso 0.709(4) 1 d R U P E 7
H25B H -0.203530 1.278037 0.748464 0.073 Uiso 0.709(4) 1 d R U P E 7
H25C H -0.231740 1.339966 0.760294 0.073 Uiso 0.709(4) 1 d R U P E 7
C254 C -0.539(2) 1.772(2) 0.8228(9) 0.060(6) Uani 1 1 d . U . . .
H254 H -0.554131 1.734164 0.822625 0.072 Uiso 1 1 calc R U . . .
C256 C -0.6684(14) 1.8643(14) 0.8720(4) 0.055(5) Uani 1 1 d G U . . .
H256 H -0.674278 1.862737 0.856603 0.066 Uiso 1 1 calc R U . . .
C258 C -0.7031(13) 1.9117(13) 0.8845(5) 0.059(6) Uani 1 1 d G U . . .
H258 H -0.732197 1.941862 0.877419 0.070 Uiso 1 1 calc R U . . .
C260 C -0.6943(14) 1.9140(13) 0.9076(5) 0.058(6) Uani 1 1 d G U . . .
H260 H -0.717496 1.945709 0.915895 0.069 Uiso 1 1 calc R U . . .
C262 C -0.6508(15) 1.8689(14) 0.9181(4) 0.057(6) Uani 1 1 d G U . . .
H262 H -0.644876 1.870430 0.933556 0.069 Uiso 1 1 calc R U . . .
C264 C -0.6161(13) 1.8215(12) 0.9057(5) 0.053(5) Uani 1 1 d G U . . .
H264 H -0.586956 1.791305 0.912741 0.063 Uiso 1 1 calc R U . . .
C266 C -0.6249(13) 1.8192(12) 0.8826(5) 0.050(4) Uani 1 1 d G U . . .
C268 C -0.170(2) 1.577(2) 0.9282(8) 0.052(8) Uani 1 1 d . U . . .
H26A H -0.195866 1.615232 0.923302 0.079 Uiso 1 1 calc R U . . .
H26B H -0.131116 1.586278 0.932996 0.079 Uiso 1 1 calc R U . . .
H26C H -0.190702 1.557980 0.940742 0.079 Uiso 1 1 calc R U . . .
C270 C -0.466(2) 1.672(2) 0.8688(8) 0.045(5) Uani 1 1 d . U . . .
H27A H -0.449755 1.638847 0.879509 0.053 Uiso 1 1 calc R U . . .
H27B H -0.487385 1.654589 0.857572 0.053 Uiso 1 1 calc R U . . .
C272 C -0.426(2) 1.404(2) 0.7264(11) 0.050(5) Uani 0.709(4) 1 d D U P E 7
H272 H -0.457413 1.421539 0.715531 0.060 Uiso 0.709(4) 1 calc R U P E 7
C274 C -0.437(2) 1.0346(19) 0.9626(7) 0.042(5) Uani 1 1 d . U . . .
H274 H -0.479654 1.043196 0.965732 0.050 Uiso 1 1 calc R U . . .
C276 C -0.4123(19) 1.695(2) 0.8572(7) 0.044(5) Uani 1 1 d . U . . .
H27C H -0.424826 1.737246 0.851443 0.053 Uiso 1 1 calc R U . . .
H27D H -0.397166 1.669050 0.844501 0.053 Uiso 1 1 calc R U . . .
C278 C -0.289(2) 1.149(2) 0.9191(8) 0.063(5) Uani 1 1 d D U . . .
H27E H -0.323070 1.178012 0.925726 0.075 Uiso 1 1 calc R U . . .
H27F H -0.258905 1.135962 0.930770 0.075 Uiso 1 1 calc R U . . .
C280 C -0.615(2) 1.689(2) 0.7772(8) 0.049(5) Uani 1 1 d . U . . .
H280 H -0.617973 1.656975 0.787892 0.059 Uiso 1 1 calc R U . . .
C282 C -0.109(2) 1.403(2) 0.8171(7) 0.064(5) Uani 1 1 d D U . . .
H282 H -0.112343 1.443969 0.809163 0.076 Uiso 1 1 calc R U . . .
C284 C -0.8974(16) 1.5357(17) 0.9006(5) 0.068(6) Uani 1 1 d G U . . .
H284 H -0.876757 1.539163 0.886527 0.082 Uiso 1 1 calc R U . . .
C286 C -0.9511(17) 1.5090(17) 0.9026(5) 0.073(6) Uani 1 1 d G U . . .
H286 H -0.966299 1.494634 0.889861 0.087 Uiso 1 1 calc R U . . .
C288 C -0.9820(14) 1.5039(17) 0.9237(6) 0.073(6) Uani 1 1 d G U . . .
H288 H -1.017893 1.486004 0.925016 0.088 Uiso 1 1 calc R U . . .
C290 C -0.9593(16) 1.5254(18) 0.9427(5) 0.071(6) Uani 1 1 d G U . . .
H290 H -0.979945 1.521904 0.956837 0.086 Uiso 1 1 calc R U . . .
C292 C -0.9056(16) 1.5520(17) 0.9407(5) 0.067(6) Uani 1 1 d G U . . .
H292 H -0.890403 1.566433 0.953504 0.081 Uiso 1 1 calc R U . . .
C294 C -0.8747(14) 1.5572(16) 0.9197(6) 0.062(5) Uani 1 1 d G U . . .
C296 C -0.7074(15) 1.3314(15) 1.0440(4) 0.060(6) Uani 1 1 d G U . . .
H296 H -0.704885 1.324372 1.059647 0.072 Uiso 1 1 calc R U . . .
C298 C -0.6777(14) 1.3768(14) 1.0329(5) 0.059(6) Uani 1 1 d G U . . .
H298 H -0.655436 1.400096 1.041076 0.070 Uiso 1 1 calc R U . . .
C300 C -0.6814(14) 1.3874(12) 1.0096(5) 0.053(5) Uani 1 1 d G U . . .
H300 H -0.661589 1.417718 1.002106 0.064 Uiso 1 1 calc R U . . .
C302 C -0.7147(14) 1.3526(14) 0.9973(4) 0.046(4) Uani 1 1 d G U . . .
C304 C -0.7444(14) 1.3072(13) 1.0085(5) 0.054(5) Uani 1 1 d G U . . .
H304 H -0.766640 1.283894 1.000278 0.065 Uiso 1 1 calc R U . . .
C306 C -0.7407(14) 1.2966(13) 1.0318(5) 0.058(6) Uani 1 1 d G U . . .
H306 H -0.760488 1.266271 1.039249 0.069 Uiso 1 1 calc R U . . .
C308 C -0.480(3) 1.854(3) 0.8041(10) 0.068(6) Uani 1 1 d . U . . .
H308 H -0.457175 1.873136 0.792745 0.081 Uiso 1 1 calc R U . . .
C310 C -0.571(2) 1.733(2) 0.7440(8) 0.051(5) Uani 1 1 d . U . . .
H310 H -0.541230 1.731380 0.731880 0.062 Uiso 1 1 calc R U . . .
C312 C -0.747(3) 1.130(2) 0.8524(8) 0.109(6) Uani 1 1 d G U . . .
C314 C -0.804(2) 1.151(2) 0.8430(9) 0.112(8) Uani 1 1 d G U . . .
H314 H -0.826858 1.189735 0.846642 0.135 Uiso 1 1 calc R U . . .
C316 C -0.827(2) 1.114(3) 0.8282(9) 0.116(8) Uani 1 1 d G U . . .
H316 H -0.865850 1.128540 0.821877 0.139 Uiso 1 1 calc R U . . .
C318 C -0.793(3) 1.057(2) 0.8227(8) 0.117(8) Uani 1 1 d G U . . .
H318 H -0.809022 1.032191 0.812770 0.140 Uiso 1 1 calc R U . . .
C320 C -0.736(2) 1.036(2) 0.8321(9) 0.116(8) Uani 1 1 d G U . . .
H320 H -0.713203 0.997036 0.828429 0.140 Uiso 1 1 calc R U . . .
C322 C -0.713(2) 1.072(3) 0.8469(9) 0.113(8) Uani 1 1 d G U . . .
H322 H -0.674210 1.058231 0.853193 0.136 Uiso 1 1 calc R U . . .
C324 C -0.566(2) 1.681(2) 0.7593(8) 0.047(4) Uani 1 1 d . U . . .
C326 C -0.508(3) 1.795(3) 0.8012(9) 0.066(6) Uani 1 1 d . U . . .
H32C H -0.538215 1.803805 0.789507 0.079 Uiso 1 1 calc R U . . .
H32D H -0.474950 1.762300 0.795977 0.079 Uiso 1 1 calc R U . . .
C328 C -0.208(3) 1.218(3) 0.7856(11) 0.051(8) Uani 0.709(4) 1 d D U P E 7
H32E H -0.172392 1.237151 0.787769 0.077 Uiso 0.709(4) 1 d R U P E 7
H32F H -0.197662 1.186411 0.774839 0.077 Uiso 0.709(4) 1 d R U P E 7
H32G H -0.222002 1.200711 0.799789 0.077 Uiso 0.709(4) 1 d R U P E 7
C330 C -0.814(3) 1.760(2) 0.8601(7) 0.078(10) Uani 1 1 d D U . . .
H33A H -0.777529 1.777155 0.856248 0.116 Uiso 1 1 d R U . . .
H33B H -0.814609 1.745755 0.875788 0.116 Uiso 1 1 d R U . . .
H33C H -0.850669 1.790575 0.857488 0.116 Uiso 1 1 d R U . . .
C332 C -0.8121(18) 1.6644(14) 0.9262(6) 0.068(5) Uani 1 1 d G U . . .
C334 C -0.7701(16) 1.7034(17) 0.9188(6) 0.073(6) Uani 1 1 d G U . . .
H334 H -0.742286 1.692833 0.906574 0.088 Uiso 1 1 calc R U . . .
C336 C -0.7698(16) 1.7582(16) 0.9298(7) 0.078(7) Uani 1 1 d G U . . .
H336 H -0.741748 1.784279 0.924843 0.094 Uiso 1 1 calc R U . . .
C338 C -0.8114(19) 1.7740(15) 0.9481(6) 0.080(7) Uani 1 1 d G U . . .
H338 H -0.811231 1.810683 0.955376 0.096 Uiso 1 1 calc R U . . .
C340 C -0.8534(17) 1.7351(18) 0.9554(6) 0.079(7) Uani 1 1 d G U . . .
H340 H -0.881252 1.745640 0.967641 0.095 Uiso 1 1 calc R U . . .
C342 C -0.8537(16) 1.6803(16) 0.9445(6) 0.075(6) Uani 1 1 d G U . . .
H342 H -0.881791 1.654194 0.949373 0.090 Uiso 1 1 calc R U . . .
C344 C -0.7982(18) 1.559(3) 0.7655(9) 0.065(9) Uani 1 1 d D U . . .
H34D H -0.802975 1.528461 0.777565 0.098 Uiso 1 1 calc R U . . .
H34E H -0.816911 1.548401 0.752209 0.098 Uiso 1 1 calc R U . . .
H34F H -0.818198 1.599306 0.770069 0.098 Uiso 1 1 calc R U . . .
C346 C -0.226(2) 1.080(3) 0.8296(12) 0.059(7) Uani 0.709(4) 1 d D U P E 7
H34G H -0.219876 1.120807 0.833341 0.088 Uiso 0.709(4) 1 d R U P E 7
H34H H -0.197696 1.065317 0.817371 0.088 Uiso 0.709(4) 1 d R U P E 7
H34I H -0.219906 1.052067 0.842591 0.088 Uiso 0.709(4) 1 d R U P E 7
C348 C -0.719(2) 1.525(2) 0.7398(7) 0.071(9) Uani 1 1 d D U . . .
H34J H -0.721297 1.481046 0.739337 0.106 Uiso 1 1 d R U . . .
H34K H -0.676577 1.530346 0.737847 0.106 Uiso 1 1 d R U . . .
H34L H -0.742867 1.547196 0.727817 0.106 Uiso 1 1 d DR U . . .
C350 C -0.372(3) 1.436(3) 0.7222(11) 0.052(8) Uani 0.709(4) 1 d D U P E 7
H35A H -0.380639 1.475498 0.729136 0.078 Uiso 0.709(4) 1 d R U P E 7
H35B H -0.363579 1.442338 0.706156 0.078 Uiso 0.709(4) 1 d R U P E 7
H35C H -0.335679 1.411058 0.728726 0.078 Uiso 0.709(4) 1 d R U P E 7
C352 C -0.589(2) 1.253(2) 0.7508(7) 0.057(8) Uani 0.709(4) 1 d D U P E 7
H35D H -0.572712 1.271884 0.737222 0.085 Uiso 0.709(4) 1 d R U P E 7
H35E H -0.600162 1.213764 0.747272 0.085 Uiso 0.709(4) 1 d R U P E 7
H35F H -0.556852 1.244874 0.761752 0.085 Uiso 0.709(4) 1 d R U P E 7
C354 C -0.414(3) 1.335(2) 0.7245(11) 0.051(8) Uani 0.709(4) 1 d D U P E 7
H35G H -0.387410 1.318646 0.736466 0.076 Uiso 0.709(4) 1 d R U P E 7
H35H H -0.393740 1.324536 0.710096 0.076 Uiso 0.709(4) 1 d R U P E 7
H35I H -0.452140 1.318097 0.726175 0.076 Uiso 0.709(4) 1 d R U P E 7
C356 C -0.679(3) 1.339(2) 0.7441(6) 0.060(9) Uani 0.709(4) 1 d D U P E 7
H35J H -0.718734 1.355656 0.750623 0.090 Uiso 0.709(4) 1 d R U P E 7
H35K H -0.683744 1.316896 0.730763 0.090 Uiso 0.709(4) 1 d R U P E 7
H35L H -0.655544 1.371596 0.739993 0.090 Uiso 0.709(4) 1 d R U P E 7
C358 C -0.4864(16) 1.5655(15) 0.6937(5) 0.068(6) Uani 1 1 d G U . . .
H358 H -0.501313 1.538668 0.684439 0.081 Uiso 1 1 calc R U . . .
C360 C -0.5076(14) 1.5699(15) 0.7163(6) 0.064(6) Uani 1 1 d G U . . .
H360 H -0.536622 1.545905 0.722150 0.077 Uiso 1 1 calc R U . . .
C362 C -0.4853(15) 1.6100(15) 0.7301(4) 0.055(4) Uani 1 1 d G U . . .
C364 C -0.4419(15) 1.6458(14) 0.7213(5) 0.058(6) Uani 1 1 d G U . . .
H364 H -0.427044 1.672640 0.730482 0.070 Uiso 1 1 calc R U . . .
C366 C -0.4208(14) 1.6415(15) 0.6987(5) 0.064(6) Uani 1 1 d G U . . .
H366 H -0.391734 1.665404 0.692771 0.077 Uiso 1 1 calc R U . . .
C368 C -0.4430(16) 1.6013(17) 0.6849(4) 0.068(6) Uani 1 1 d G U . . .
H368 H -0.428868 1.598419 0.669750 0.081 Uiso 1 1 calc R U . . .
C370 C -0.661(2) 1.148(2) 0.9770(8) 0.056(8) Uani 1 1 d . U . . .
H37A H -0.684193 1.143829 0.991092 0.084 Uiso 1 1 d R U . . .
H37B H -0.658283 1.111189 0.968672 0.084 Uiso 1 1 d R U . . .
H37C H -0.681573 1.183419 0.968212 0.084 Uiso 1 1 d R U . . .
C372 C -0.8888(18) 1.312(2) 0.8185(6) 0.110(7) Uani 1 1 d G U . . .
H372 H -0.903913 1.326460 0.832615 0.132 Uiso 1 1 calc R U . . .
C374 C -0.9149(17) 1.267(2) 0.8087(8) 0.115(8) Uani 1 1 d G U . . .
H374 H -0.947338 1.250526 0.816297 0.138 Uiso 1 1 calc R U . . .
C376 C -0.8923(18) 1.2457(16) 0.7875(7) 0.119(8) Uani 1 1 d G U . . .
H376 H -0.909725 1.215260 0.780962 0.143 Uiso 1 1 calc DR U . . .
C378 C -0.844(2) 1.2701(15) 0.7761(6) 0.119(8) Uani 1 1 d DG U . . .
H378 H -0.828687 1.255929 0.761944 0.143 Uiso 1 1 calc R U . . .
C380 C -0.8177(17) 1.3156(15) 0.7859(6) 0.113(7) Uani 1 1 d DG U . . .
H380 H -0.785262 1.331863 0.778262 0.136 Uiso 1 1 calc R U . . .
C382 C -0.8403(16) 1.3367(13) 0.8071(6) 0.103(6) Uani 1 1 d G U . . .
C384 C -0.545(4) 1.0413(15) 0.8084(11) 0.077(11) Uani 0.709(4) 1 d D U P E 7
H38A H -0.502009 1.035235 0.811708 0.115 Uiso 0.709(4) 1 d R U P E 7
H38B H -0.551139 1.013765 0.796848 0.115 Uiso 0.709(4) 1 d R U P E 7
H38C H -0.569529 1.032475 0.821878 0.115 Uiso 0.709(4) 1 d R U P E 7
C386 C -0.099(3) 1.357(3) 0.7997(9) 0.079(10) Uani 1 1 d D U . . .
H38D H -0.104123 1.316701 0.806427 0.118 Uiso 1 1 d R U . . .
H38E H -0.056783 1.354231 0.793467 0.118 Uiso 1 1 d R U . . .
H38F H -0.127453 1.368221 0.787837 0.118 Uiso 1 1 d R U . . .
C388 C -0.246(2) 1.779(2) 0.8323(9) 0.060(6) Uani 1 1 d . U . . .
H388 H -0.251309 1.798672 0.817954 0.072 Uiso 1 1 calc R U . . .
C390 C -0.566(3) 1.107(2) 0.8003(7) 0.070(6) Uani 0.709(4) 1 d D U P E 7
H390 H -0.535277 1.117184 0.788734 0.084 Uiso 0.709(4) 1 calc R U P E 7
C392 C -0.190(2) 1.461(2) 0.7216(8) 0.055(6) Uani 1 1 d . U . . .
H392 H -0.158450 1.427756 0.717457 0.066 Uiso 1 1 calc R U . . .
C394 C -0.2139(17) 1.151(2) 0.8279(12) 0.052(6) Uani 0.291(4) 1 d D U P E 8
H394 H -0.182851 1.152023 0.839221 0.063 Uiso 0.291(4) 1 calc R U P E 8
C396 C -0.374579 1.106819 0.810970 0.062(6) Uani 0.291(4) 1 d D U P E 8
H396 H -0.351245 1.141369 0.808498 0.074 Uiso 0.291(4) 1 calc R U P E 8
C398 C -0.184(2) 1.752(2) 0.8647(9) 0.058(6) Uani 1 1 d . U . . .
H398 H -0.148930 1.750641 0.872903 0.070 Uiso 1 1 calc R U . . .
C400 C -0.672(7) 1.249(6) 0.7738(15) 0.054(9) Uani 0.291(4) 1 d D U P E 8
H40A H -0.709327 1.270698 0.781300 0.081 Uiso 0.291(4) 1 d R U P E 8
H40B H -0.682807 1.232838 0.760050 0.081 Uiso 0.291(4) 1 d R U P E 8
H40C H -0.643947 1.278148 0.770110 0.081 Uiso 0.291(4) 1 d R U P E 8
C402 C -0.346(6) 1.0485(19) 0.823(2) 0.060(8) Uani 0.291(4) 1 d D U P E 8
H40D H -0.304809 1.057789 0.823338 0.090 Uiso 0.291(4) 1 d R U P E 8
H40E H -0.346309 1.014199 0.813728 0.090 Uiso 0.291(4) 1 d R U P E 8
H40F H -0.360089 1.037719 0.838388 0.090 Uiso 0.291(4) 1 d R U P E 8
C404 C -0.597(5) 1.306(5) 0.7453(16) 0.054(7) Uani 0.291(4) 1 d D U P E 8
H40G H -0.585292 1.281137 0.758745 0.082 Uiso 0.291(4) 1 d R U P E 8
H40H H -0.573972 1.287097 0.732325 0.082 Uiso 0.291(4) 1 d R U P E 8
H40I H -0.640522 1.309806 0.743425 0.082 Uiso 0.291(4) 1 d R U P E 8
C406 C -0.200(2) 1.468(2) 0.7447(8) 0.051(5) Uani 1 1 d . U . . .
H406 H -0.178676 1.440915 0.755554 0.061 Uiso 1 1 calc R U . . .
C408 C -0.423(5) 1.099(3) 0.7951(18) 0.064(12) Uani 0.291(4) 1 d D U P E 8
H40J H -0.451382 1.079535 0.804692 0.096 Uiso 0.291(4) 1 d R U P E 8
H40K H -0.405062 1.072215 0.783332 0.096 Uiso 0.291(4) 1 d R U P E 8
H2 H -0.444862 1.137495 0.788422 0.096 Uiso 0.291(4) 1 d R U P E 8
C410 C -0.236(2) 1.731(2) 0.8738(9) 0.056(5) Uani 1 1 d . U . . .
H410 H -0.235382 1.717060 0.888953 0.067 Uiso 1 1 calc R U . . .
C412 C -0.594(6) 1.155(6) 0.778(2) 0.064(8) Uani 0.291(4) 1 d D U P E 8
H41A H -0.557833 1.174475 0.779154 0.095 Uiso 0.291(4) 1 d R U P E 8
H41B H -0.601053 1.149215 0.762844 0.095 Uiso 0.291(4) 1 d R U P E 8
H41C H -0.587273 1.115365 0.786554 0.095 Uiso 0.291(4) 1 d R U P E 8
C414 C -0.658(2) 1.790(2) 0.7612(8) 0.053(6) Uani 1 1 d . U . . .
H414 H -0.690824 1.823161 0.760929 0.064 Uiso 1 1 calc R U . . .
C416 C -0.258(2) 1.181(2) 0.9001(8) 0.067(6) Uani 1 1 d D U . . .
H41D H -0.287495 1.185703 0.888018 0.080 Uiso 1 1 calc R U . . .
H41E H -0.259374 1.223067 0.905143 0.080 Uiso 1 1 calc R U . . .
C418 C -0.318(2) 1.034(2) 1.0319(8) 0.055(6) Uani 1 1 d . U . . .
H418 H -0.279238 1.010779 1.035526 0.066 Uiso 1 1 calc R U . . .
C420 C -0.371(2) 1.022(2) 1.0408(8) 0.056(6) Uani 1 1 d . U . . .
H420 H -0.370470 0.985816 1.049831 0.067 Uiso 1 1 calc R U . . .
C422 C -0.658(2) 1.746(2) 0.7789(8) 0.052(6) Uani 1 1 d . U . . .
H422 H -0.685552 1.753818 0.791509 0.063 Uiso 1 1 calc R U . . .
C424 C -0.286(2) 1.728(2) 0.8624(8) 0.052(4) Uani 1 1 d . U . . .
C426 C -0.580(4) 1.009(5) 0.886(2) 0.046(7) Uani 0.356(9) 1 d D U P D 2
H42A H -0.603996 0.999919 0.874297 0.068 Uiso 0.356(9) 1 d R U P D 2
H42B H -0.606436 1.033229 0.897277 0.068 Uiso 0.356(9) 1 d R U P D 2
H42C H -0.560426 0.970419 0.893697 0.068 Uiso 0.356(9) 1 d R U P D 2
W16 W -0.99889(6) 0.88199(6) 0.64956(2) 0.0193(3) Uani 1 1 d . U . . .
W17 W -0.81645(6) 1.10260(6) 0.60738(2) 0.0228(3) Uani 1 1 d . U . . .
W18 W -0.77487(6) 0.95414(6) 0.59514(2) 0.0190(3) Uani 1 1 d . U . . .
W22 W -0.87153(6) 0.83756(6) 0.61643(2) 0.0183(3) Uani 1 1 d . U . . .
W23 W -0.92747(6) 1.04685(7) 0.56718(2) 0.0236(3) Uani 1 1 d . U . . .
W25 W -1.04183(6) 1.04701(6) 0.66481(2) 0.0221(3) Uani 1 1 d . U . . .
W27 W -0.95516(6) 1.15191(6) 0.64528(2) 0.0235(3) Uani 1 1 d . U . . .
W29 W -1.05615(7) 1.08465(7) 0.60148(2) 0.0288(3) Uani 1 1 d . U . . .
W30 W -1.00890(6) 0.93473(6) 0.58821(2) 0.0205(3) Uani 1 1 d . U . . .
Ag1 Ag -0.78183(13) 0.94742(13) 0.69733(4) 0.0302(6) Uani 1 1 d . U . . .
Ag1B Ag -0.6774(4) 1.1195(4) 0.64264(15) 0.0434(18) Uani 0.483(9) 1 d . U P F 2
Ag3 Ag -0.7044(4) 0.8793(4) 0.66104(16) 0.052(2) Uani 0.395(4) 1 d D U P E 5
Ag5 Ag -0.8788(3) 0.8815(3) 0.71846(10) 0.0468(13) Uani 0.605(4) 1 d . U P E 6
Ag8 Ag -0.78222(15) 0.99239(16) 0.65285(5) 0.0409(7) Uani 1 1 d . U . . .
Ag11 Ag -0.6158(3) 0.8904(4) 0.61736(10) 0.0363(16) Uani 0.517(9) 1 d . U P F 1
Ag13 Ag -0.7935(6) 0.8095(5) 0.7010(2) 0.056(3) Uani 0.395(4) 1 d . U P E 5
Ag14 Ag -0.91332(15) 0.74334(14) 0.57283(5) 0.0381(7) Uani 1 1 d . U . . .
Ag16 Ag -0.69712(14) 0.95110(15) 0.53580(5) 0.0366(7) Uani 1 1 d . U . . .
Ag19 Ag -0.8792(3) 1.0366(3) 0.72990(11) 0.0435(15) Uani 0.605(4) 1 d . U P E 6
Ag21 Ag -0.7636(3) 1.0710(3) 0.68888(11) 0.0521(14) Uani 0.605(4) 1 d D U P E 6
Ag22 Ag -0.93390(15) 0.77288(14) 0.69785(5) 0.0408(7) Uani 1 1 d . U . . .
Ag23 Ag -0.6550(3) 0.9487(3) 0.67090(13) 0.0741(19) Uani 0.605(4) 1 d D U P E 6
Ag25 Ag -0.8275(5) 1.0839(5) 0.7008(2) 0.065(2) Uani 0.395(4) 1 d . U P E 5
Ag26 Ag -1.08647(14) 0.80852(14) 0.60971(6) 0.0420(7) Uani 1 1 d . U . . .
Ag28 Ag -0.65296(14) 1.05435(16) 0.57900(5) 0.0425(7) Uani 1 1 d . U . . .
Ag31 Ag -0.7939(3) 0.70779(19) 0.64992(7) 0.0838(15) Uani 1 1 d . U . . .
Ag32 Ag -0.95184(17) 0.70621(14) 0.63549(5) 0.0434(8) Uani 1 1 d . U . . .
Ag39 Ag -0.7479(3) 0.8324(3) 0.66921(10) 0.0482(13) Uani 0.605(4) 1 d . U P E 6
Ag40 Ag -1.18520(15) 1.14373(16) 0.64636(6) 0.0476(8) Uani 1 1 d . U . . .
Ag41 Ag -0.6591(3) 1.1036(3) 0.63055(15) 0.0410(16) Uani 0.517(9) 1 d . U P F 1
Ag42 Ag -1.02353(16) 1.06506(17) 0.72743(6) 0.0494(8) Uani 1 1 d . U . . .
Ag43 Ag -0.9116(5) 1.2121(3) 0.70009(11) 0.045(2) Uani 0.528(13) 1 d . U P E 1
Ag47 Ag -0.79782(13) 1.13142(13) 0.54894(5) 0.0334(6) Uani 1 1 d . U . . .
Ag48 Ag -1.0876(2) 1.20898(16) 0.68771(5) 0.0536(9) Uani 1 1 d . U . . .
Ag49 Ag -0.8915(5) 0.9462(4) 0.72616(18) 0.058(2) Uani 0.395(4) 1 d . U P E 5
Ag51 Ag -0.6744(4) 1.0174(4) 0.67871(16) 0.055(2) Uani 0.395(4) 1 d D U P E 5
Ag52 Ag -1.08001(17) 1.25459(17) 0.62199(6) 0.0532(9) Uani 1 1 d . U . . .
Ag53 Ag -0.8999(5) 1.0033(6) 0.68089(19) 0.035(2) Uani 0.291(4) 1 d . U P E 2
Ag56 Ag -0.8579(2) 0.90816(19) 0.66797(6) 0.0646(12) Uani 1 1 d . U . . .
Ag58 Ag -0.8817(2) 1.0333(2) 0.68021(8) 0.0356(10) Uani 0.709(4) 1 d . U P E 1
Ag60 Ag -0.9544(5) 1.2251(3) 0.69670(11) 0.039(2) Uani 0.472(13) 1 d . U P E 2
Ag62 Ag -0.6098(3) 0.9284(5) 0.61612(12) 0.0418(17) Uani 0.483(9) 1 d . U P F 2
Cl1 Cl -0.7054(8) 0.9280(7) 0.7259(3) 0.080(4) Uani 1 1 d . U . G 1
S1 S -1.0003(5) 0.7246(5) 0.60026(18) 0.039(2) Uani 1 1 d . U . . .
S3 S -0.7186(13) 0.7739(13) 0.6713(5) 0.048(4) Uani 0.395(4) 1 d D U P E 5
S4 S -0.6977(5) 1.0620(5) 0.54276(16) 0.035(2) Uani 1 1 d . U . . .
S5 S -0.6456(9) 0.8477(10) 0.6584(3) 0.052(3) Uani 0.605(4) 1 d D U P E 6
S6 S -1.1484(5) 1.2377(5) 0.65589(19) 0.046(2) Uani 1 1 d . U . . .
S9 S -0.9329(9) 0.9566(9) 0.7437(3) 0.051(3) Uani 0.605(4) 1 d D U P E 6
S11 S -0.9004(17) 1.0562(17) 0.7322(6) 0.043(4) Uani 0.395(4) 1 d D U P E 5
S13 S -0.7310(16) 1.1108(16) 0.6879(6) 0.059(4) Uani 0.395(4) 1 d D U P E 5
S16 S -0.8940(7) 0.6923(6) 0.6691(2) 0.058(3) Uani 1 1 d . U . . .
S17 S -0.8184(10) 0.7949(10) 0.7012(4) 0.046(4) Uani 0.605(4) 1 d D U P E 6
S19 S -0.8339(10) 1.1239(10) 0.7174(4) 0.059(4) Uani 0.605(4) 1 d D U P E 6
S20 S -1.0220(7) 1.1794(6) 0.71822(19) 0.057(3) Uani 1 1 d . U . . .
S21 S -0.6609(6) 1.0546(6) 0.6749(4) 0.071(4) Uani 0.605(4) 1 d D U P E 6
S23 S -0.6047(15) 0.9270(17) 0.6622(6) 0.063(5) Uani 0.395(4) 1 d D U P E 5
S24 S -0.6026(9) 1.0071(10) 0.6144(3) 0.039(3) Uani 0.517(9) 1 d D U P F 1
S24A S -0.6169(10) 1.0460(11) 0.6149(4) 0.037(3) Uani 0.483(9) 1 d D U P F 2
S25 S -0.8827(14) 0.8340(14) 0.7266(5) 0.051(4) Uani 0.395(4) 1 d D U P E 5
P1 P -1.1096(5) 1.0167(5) 0.74169(18) 0.035(2) Uani 1 1 d . U . . .
P2 P -1.0861(6) 1.3017(6) 0.5844(2) 0.049(2) Uani 1 1 d . U . . .
P3 P -0.5794(7) 0.8244(8) 0.5897(3) 0.066(3) Uani 1 1 d . U . . .
P4 P -0.8782(5) 0.7405(4) 0.53357(17) 0.0327(19) Uani 1 1 d . U . . .
P6 P -1.2573(5) 1.0823(5) 0.6356(2) 0.044(2) Uani 1 1 d . U . . .
P8 P -0.6991(5) 0.8827(5) 0.50586(17) 0.036(2) Uani 1 1 d . U . . .
P10 P -1.0305(5) 0.7688(4) 0.71888(17) 0.034(2) Uani 1 1 d . U . . .
P11 P -0.6755(12) 1.2214(12) 0.6344(4) 0.128(6) Uani 1 1 d D U . . .
P14 P -0.8648(5) 1.2193(5) 0.53287(17) 0.0331(19) Uani 1 1 d . U . . .
P15 P -0.7295(9) 0.6635(9) 0.6178(4) 0.098(5) Uani 1 1 d D U . . .
P19 P -0.9039(11) 1.3101(10) 0.6809(4) 0.104(5) Uani 1 1 d D U . . .
P23 P -1.1909(5) 0.8480(5) 0.6223(2) 0.041(2) Uani 1 1 d . U . . .
Si3 Si -0.9196(4) 0.9996(4) 0.62511(13) 0.0132(14) Uani 1 1 d . U . . .
O44 O -1.0588(10) 0.8397(10) 0.6565(4) 0.023(4) Uani 1 1 d . U . . .
O47 O -0.7214(10) 0.9245(10) 0.5736(4) 0.023(4) Uani 1 1 d . U . . .
O49 O -1.0047(10) 1.0990(10) 0.5740(4) 0.024(3) Uani 1 1 d . U . . .
O51 O -0.8835(9) 1.0964(10) 0.5827(3) 0.018(3) Uani 1 1 d . U . . .
O53 O -0.9296(10) 0.8808(10) 0.5912(3) 0.019(3) Uani 1 1 d . U . . .
O55 O -1.0293(10) 0.9139(10) 0.6175(4) 0.021(3) Uani 1 1 d . U . . .
O57 O -0.8170(10) 0.8881(10) 0.6011(4) 0.019(3) Uani 1 1 d . U . . .
O59 O -1.0342(10) 0.9641(10) 0.6575(3) 0.019(3) Uani 1 1 d . U . . .
O61 O -0.9469(10) 0.8215(9) 0.6308(4) 0.020(3) Uani 1 1 d . U . . .
O63 O -0.9101(11) 1.0699(11) 0.5396(3) 0.025(4) Uani 1 1 d . U . . .
O65 O -1.0709(10) 1.0114(10) 0.5889(4) 0.021(3) Uani 1 1 d . U . . .
O67 O -0.9631(9) 1.0136(9) 0.6037(3) 0.015(3) Uani 1 1 d . U . . .
O69 O -1.1241(11) 1.1376(11) 0.5945(4) 0.029(5) Uani 1 1 d . U . . .
O71 O -0.9715(10) 0.9807(10) 0.5632(3) 0.021(3) Uani 1 1 d . U . . .
O73 O -0.7688(10) 1.0412(10) 0.5886(4) 0.021(3) Uani 1 1 d . U . . .
O75 O -1.0512(12) 0.8906(11) 0.5733(4) 0.030(5) Uani 1 1 d . U . . .
O77 O -0.8272(10) 0.8197(10) 0.6411(4) 0.022(4) Uani 1 1 d . U . . .
O79 O -0.7298(9) 0.9428(9) 0.6187(3) 0.015(3) Uani 1 1 d . U . . .
O80 O -0.9163(9) 0.9272(9) 0.6332(3) 0.014(3) Uani 1 1 d . U . . .
O81 O -1.0719(10) 1.0644(10) 0.6302(4) 0.020(3) Uani 1 1 d . U . . .
O83 O -0.7691(10) 1.0858(10) 0.6303(4) 0.021(4) Uani 1 1 d . U . . .
O85 O -1.1174(11) 1.0604(11) 0.6773(4) 0.031(5) Uani 1 1 d . U . . .
O86 O -0.9499(9) 1.0494(9) 0.6446(3) 0.018(3) Uani 1 1 d . U . . .
O87 O -0.8535(10) 0.9784(10) 0.5738(3) 0.020(4) Uani 1 1 d . U . . .
O89 O -0.9785(11) 1.2329(10) 0.6443(4) 0.025(4) Uani 1 1 d . U . . .
O91 O -0.7876(11) 1.1619(11) 0.5926(4) 0.031(5) Uani 1 1 d . U . . .
O93 O -0.8521(10) 0.7676(10) 0.6016(4) 0.022(4) Uani 1 1 d . U . . .
O95 O -1.0318(10) 1.1363(10) 0.6595(4) 0.022(4) Uani 1 1 d . U . . .
O97 O -0.8888(11) 1.1411(10) 0.6245(4) 0.025(3) Uani 1 1 d . U . . .
O99 O -0.9512(9) 0.8651(9) 0.6731(3) 0.017(3) Uani 1 1 d . U . . .
O101 O -0.8487(9) 1.0116(9) 0.6164(3) 0.014(3) Uani 1 1 d . U . . .
O103 O -0.9950(10) 1.0346(11) 0.6887(4) 0.025(4) Uani 1 1 d . U . . .
O106 O -1.0037(11) 1.1427(11) 0.6143(4) 0.030(5) Uani 1 1 d . U . . .
O110 O -0.9116(11) 1.1411(11) 0.6695(4) 0.028(4) Uani 1 1 d . U . . .
C213 C -0.7753(17) 0.8017(17) 0.5263(6) 0.031(4) Uani 1 1 d . U . . .
H21A H -0.769965 0.806933 0.542290 0.038 Uiso 1 1 calc R U . . .
H21B H -0.806837 0.835483 0.520885 0.038 Uiso 1 1 calc R U . . .
C107 C -0.496(4) 1.047(3) 0.5979(13) 0.049(7) Uani 0.483(9) 1 d D U P F 2
H10E H -0.481516 1.003643 0.601765 0.074 Uiso 0.483(9) 1 d R U P F 2
H10F H -0.461756 1.069032 0.596785 0.074 Uiso 0.483(9) 1 d R U P F 2
H10G H -0.515866 1.050542 0.583615 0.074 Uiso 0.483(9) 1 d R U P F 2
C215 C -1.1212(18) 0.9539(17) 0.7245(7) 0.034(4) Uani 1 1 d . U . . .
H21C H -1.158997 0.939333 0.730152 0.041 Uiso 1 1 calc R U . . .
H21D H -1.128164 0.970793 0.709109 0.041 Uiso 1 1 calc R U . . .
C27 C -0.9161(18) 0.8097(19) 0.4923(7) 0.037(5) Uani 1 1 d . U . . .
H27 H -0.897944 0.775659 0.484010 0.045 Uiso 1 1 calc R U . . .
C217 C -0.9179(18) 0.8074(18) 0.5172(7) 0.035(4) Uani 1 1 d . U . . .
C109 C -0.7947(17) 0.7380(17) 0.5230(6) 0.031(4) Uani 1 1 d . U . . .
H10H H -0.767743 0.705298 0.531263 0.038 Uiso 1 1 calc R U . . .
H10I H -0.790355 0.728902 0.506996 0.038 Uiso 1 1 calc R U . . .
C219 C -0.5226(11) 1.0180(19) 0.6149(6) 0.046(5) Uani 0.517(9) 1 d D U P F 1
H219 H -0.504562 1.001629 0.629282 0.055 Uiso 0.517(9) 1 calc R U P F 1
C55 C -0.5411(18) 1.066(4) 0.6174(12) 0.045(5) Uani 0.483(9) 1 d D U P F 2
H55 H -0.523666 1.056098 0.632369 0.054 Uiso 0.483(9) 1 calc R U P F 2
C221 C -0.9533(18) 0.8573(18) 0.5283(7) 0.038(5) Uani 1 1 d . U . . .
H221 H -0.956313 0.854378 0.544101 0.046 Uiso 1 1 calc R U . . .
C111 C -1.261(2) 0.796(2) 0.6576(9) 0.058(5) Uani 1 1 d . U . . .
H111 H -1.270323 0.834394 0.664347 0.069 Uiso 1 1 calc R U . . .
C223 C -1.2968(14) 1.0454(15) 0.6585(5) 0.053(4) Uani 1 1 d G U . . .
C7 C -1.3500(14) 1.0199(16) 0.6559(4) 0.059(5) Uani 1 1 d G U . . .
H7 H -1.368353 1.023753 0.641876 0.071 Uiso 1 1 calc R U . . .
C225 C -1.3759(13) 0.9887(16) 0.6741(6) 0.064(6) Uani 1 1 d G U . . .
H225 H -1.411538 0.971620 0.672361 0.077 Uiso 1 1 calc R U . . .
C113 C -1.3485(15) 0.9829(16) 0.6950(5) 0.066(6) Uani 1 1 d G U . . .
H113 H -1.365856 0.962044 0.707232 0.080 Uiso 1 1 calc R U . . .
C227 C -1.2953(15) 1.0084(16) 0.6976(4) 0.064(6) Uani 1 1 d G U . . .
H227 H -1.276987 1.004600 0.711618 0.076 Uiso 1 1 calc R U . . .
C57 C -1.2694(12) 1.0397(15) 0.6794(5) 0.058(5) Uani 1 1 d G U . . .
H57 H -1.233801 1.056734 0.681133 0.070 Uiso 1 1 calc R U . . .
C229 C -1.008(3) 1.490(3) 0.5732(10) 0.072(6) Uani 1 1 d . U . . .
H229 H -0.993592 1.527450 0.571322 0.087 Uiso 1 1 calc R U . . .
C115 C -0.923(4) 1.045(5) 0.7758(7) 0.051(11) Uani 0.395(4) 1 d D U P E 5
H11D H -0.930155 1.077529 0.786528 0.076 Uiso 0.395(4) 1 d R U P E 5
H11E H -0.917955 1.005279 0.783768 0.076 Uiso 0.395(4) 1 d R U P E 5
H11F H -0.957915 1.049509 0.766258 0.076 Uiso 0.395(4) 1 d R U P E 5
C231 C -0.8451(14) 1.2937(11) 0.5396(5) 0.047(4) Uani 1 1 d G U . . .
C29 C -0.7974(14) 1.2937(11) 0.5543(5) 0.057(5) Uani 1 1 d G U . . .
H29 H -0.775874 1.256250 0.560235 0.069 Uiso 1 1 calc R U . . .
C233 C -0.7820(13) 1.3499(14) 0.5602(5) 0.062(6) Uani 1 1 d G U . . .
H233 H -0.750099 1.349911 0.570020 0.075 Uiso 1 1 calc R U . . .
C117 C -0.8142(15) 1.4059(11) 0.5513(6) 0.062(6) Uani 1 1 d G U . . .
H117 H -0.803848 1.443428 0.555261 0.074 Uiso 1 1 calc R U . . .
C235 C -0.8618(14) 1.4058(11) 0.5366(5) 0.058(6) Uani 1 1 d G U . . .
H235 H -0.883373 1.443286 0.530718 0.070 Uiso 1 1 calc R U . . .
C59 C -0.8773(13) 1.3497(14) 0.5308(5) 0.055(5) Uani 1 1 d G U . . .
H59 H -0.909150 1.349626 0.520933 0.066 Uiso 1 1 calc R U . . .
C237 C -0.7621(19) 0.917(2) 0.4879(7) 0.042(4) Uani 1 1 d . U . . .
C119 C -1.288(2) 1.119(2) 0.7559(8) 0.051(5) Uani 1 1 d . U . . .
H119 H -1.321916 1.120102 0.766170 0.061 Uiso 1 1 calc R U . . .
C239 C -0.5408(9) 1.027(5) 0.6675(13) 0.082(12) Uani 0.605(4) 1 d D U P E 6
H23A H -0.566864 1.025365 0.654997 0.123 Uiso 0.605(4) 1 d R U P E 6
H23B H -0.515364 0.986495 0.669987 0.123 Uiso 0.605(4) 1 d R U P E 6
H23C H -0.514464 1.057295 0.664077 0.123 Uiso 0.605(4) 1 d R U P E 6
C15 C -1.0914(17) 0.8361(16) 0.7163(6) 0.032(4) Uani 1 1 d . U . . .
H15I H -1.103999 0.841657 0.700688 0.039 Uiso 1 1 calc R U . . .
H15J H -1.127381 0.829345 0.725879 0.039 Uiso 1 1 calc R U . . .
C241 C -0.855(2) 1.217(2) 0.5017(7) 0.044(4) Uani 1 1 d . U . . .
C121 C -0.768(2) 0.6229(19) 0.5990(6) 0.099(6) Uani 1 1 d G U . . .
C243 C -0.824(2) 0.606(2) 0.6071(6) 0.098(7) Uani 1 1 d G U . . .
H243 H -0.838682 0.613218 0.622058 0.117 Uiso 1 1 calc R U . . .
C61 C -0.8593(17) 0.578(2) 0.5930(8) 0.101(8) Uani 1 1 d G U . . .
H61 H -0.896797 0.566655 0.598390 0.121 Uiso 1 1 calc R U . . .
C245 C -0.8380(18) 0.567(2) 0.5707(8) 0.103(8) Uani 1 1 d G U . . .
H245 H -0.861316 0.548404 0.561187 0.124 Uiso 1 1 calc R U . . .
C123 C -0.7819(17) 0.5840(19) 0.5626(6) 0.104(8) Uani 1 1 d G U . . .
H123 H -0.767721 0.576715 0.547652 0.125 Uiso 1 1 calc R U . . .
C247 C -0.7471(14) 0.6119(14) 0.5767(6) 0.102(7) Uani 1 1 d G U . . .
H247 H -0.709605 0.623279 0.571319 0.123 Uiso 1 1 calc DR U . . .
C31 C -0.9835(19) 0.9096(19) 0.5179(7) 0.040(5) Uani 1 1 d . U . . .
H31 H -1.008724 0.940916 0.525862 0.048 Uiso 1 1 calc R U . . .
C249 C -1.013(3) 1.452(3) 0.5957(10) 0.071(6) Uani 1 1 d . U . . .
H249 H -0.999114 1.467899 0.608360 0.086 Uiso 1 1 calc R U . . .
C125 C -0.585(2) 0.797(2) 0.6762(10) 0.052(5) Uani 0.605(4) 1 d D U P E 6
H125 H -0.605348 0.796917 0.691407 0.062 Uiso 0.605(4) 1 calc R U P E 6
C251 C -0.685(3) 1.151(3) 0.7072(11) 0.064(6) Uani 0.395(4) 1 d D U P E 5
H251 H -0.656739 1.175571 0.698930 0.077 Uiso 0.395(4) 1 calc R U P E 5
C63 C -0.745(3) 1.176(4) 0.7318(12) 0.068(8) Uani 0.605(4) 1 d D U P E 6
H63A H -0.714042 1.142665 0.726092 0.102 Uiso 0.605(4) 1 d R U P E 6
H63B H -0.726982 1.199235 0.741992 0.102 Uiso 0.605(4) 1 d R U P E 6
H63C H -0.762002 1.202255 0.719332 0.102 Uiso 0.605(4) 1 d R U P E 6
C253 C -1.197(2) 0.9118(19) 0.6415(7) 0.043(4) Uani 1 1 d . U . . .
H25D H -1.240379 0.924266 0.646265 0.052 Uiso 1 1 calc R U . . .
H25E H -1.174388 0.896369 0.654973 0.052 Uiso 1 1 calc R U . . .
C127 C -0.652(4) 1.096(4) 0.7199(15) 0.072(10) Uani 0.395(4) 1 d D U P E 5
H12E H -0.649524 1.058371 0.711830 0.108 Uiso 0.395(4) 1 d R U P E 5
H12F H -0.673064 1.091241 0.734430 0.108 Uiso 0.395(4) 1 d R U P E 5
H12G H -0.610334 1.103091 0.722100 0.108 Uiso 0.395(4) 1 d R U P E 5
C255 C -0.8914(13) 0.617(2) 0.6836(7) 0.070(6) Uani 1 1 d D U . . .
H255 H -0.867644 0.589839 0.672330 0.084 Uiso 1 1 calc R U . . .
C2 C -1.245(2) 0.883(2) 0.6007(8) 0.048(4) Uani 1 1 d . U . . .
C257 C -0.9736(19) 0.914(2) 0.4926(7) 0.042(5) Uani 1 1 d . U . . .
H257 H -0.989118 0.950183 0.484424 0.050 Uiso 1 1 calc R U . . .
C129 C -0.656(2) 1.096(2) 0.5184(7) 0.044(5) Uani 1 1 d . U . . .
H129 H -0.615529 1.069492 0.515635 0.053 Uiso 1 1 calc R U . . .
C259 C -1.0679(17) 0.8972(17) 0.7234(7) 0.034(5) Uani 1 1 d . U . . .
H25F H -1.049965 0.889306 0.738191 0.040 Uiso 1 1 calc R U . . .
H25G H -1.035460 0.906737 0.712576 0.040 Uiso 1 1 calc R U . . .
C65 C -1.308(2) 0.872(2) 0.6029(9) 0.055(5) Uani 1 1 d . U . . .
H65 H -1.321217 0.846329 0.614626 0.066 Uiso 1 1 calc R U . . .
C261 C -1.283(2) 0.692(3) 0.6588(9) 0.063(6) Uani 1 1 d . U . . .
H261 H -1.302394 0.661949 0.666738 0.076 Uiso 1 1 calc R U . . .
C131 C -1.062(3) 1.229(2) 0.7425(9) 0.063(5) Uani 1 1 d . U . . .
H131 H -1.102992 1.216509 0.746157 0.075 Uiso 1 1 calc R U . . .
C263 C -0.8702(19) 1.344(2) 0.7013(5) 0.115(7) Uani 1 1 d G U . . .
C33 C -0.8918(19) 1.340(2) 0.7238(5) 0.120(8) Uani 1 1 d DG U . . .
H33 H -0.921930 1.315695 0.727995 0.143 Uiso 1 1 calc R U . . .
C265 C -0.868(2) 1.3726(18) 0.7400(5) 0.123(8) Uani 1 1 d DG U . . .
H265 H -0.882920 1.369849 0.755105 0.148 Uiso 1 1 calc R U . . .
C133 C -0.823(2) 1.4091(19) 0.7337(7) 0.124(9) Uani 1 1 d G U . . .
H133 H -0.807853 1.430840 0.744613 0.149 Uiso 1 1 calc DR U . . .
C267 C -0.802(2) 1.413(2) 0.7112(8) 0.123(8) Uani 1 1 d G U . . .
H267 H -0.771796 1.437678 0.707010 0.148 Uiso 1 1 calc R U . . .
C67 C -0.8253(19) 1.381(2) 0.6950(7) 0.120(8) Uani 1 1 d DG U . . .
H67 H -0.810805 1.383525 0.679900 0.144 Uiso 1 1 calc R U . . .
C269 C -0.839(2) 1.206(2) 0.4562(9) 0.057(6) Uani 1 1 d . U . . .
H269 H -0.834621 1.201900 0.440582 0.068 Uiso 1 1 calc R U . . .
C135 C -0.6245(14) 0.5870(19) 0.6051(5) 0.109(8) Uani 1 1 d DG U . . .
H135 H -0.629776 0.605364 0.590609 0.131 Uiso 1 1 calc DR U . . .
C271 C -0.6674(15) 0.6062(18) 0.6227(4) 0.106(6) Uani 1 1 d DG U . . .
C17 C -0.6596(18) 0.5788(19) 0.6444(5) 0.109(8) Uani 1 1 d DG U . . .
H17 H -0.688321 0.591644 0.656124 0.130 Uiso 1 1 calc R U . . .
C273 C -0.6089(19) 0.5320(18) 0.6484(7) 0.112(8) Uani 1 1 d G U . . .
H273 H -0.603628 0.513598 0.662948 0.134 Uiso 1 1 calc R U . . .
C137 C -0.5660(17) 0.5127(18) 0.6309(8) 0.112(8) Uani 1 1 d G U . . .
H137 H -0.532008 0.481434 0.633603 0.134 Uiso 1 1 calc R U . . .
C275 C -0.5738(15) 0.540(2) 0.6092(7) 0.111(8) Uani 1 1 d G U . . .
C69 C -1.061(2) 1.377(2) 0.5801(9) 0.061(5) Uani 1 1 d . U . . .
C277 C -0.9747(18) 1.2467(19) 0.5612(7) 0.038(5) Uani 1 1 d . U . . .
H27G H -0.959186 1.214986 0.572581 0.046 Uiso 1 1 calc R U . . .
H27H H -0.962523 1.285578 0.564787 0.046 Uiso 1 1 calc R U . . .
C139 C -0.556(2) 0.915(2) 0.5577(7) 0.047(5) Uani 1 1 d . U . . .
H139 H -0.577755 0.943124 0.567894 0.057 Uiso 1 1 calc DR U . . .
C279 C -0.8043(19) 0.967(2) 0.4944(7) 0.044(5) Uani 1 1 d . U . . .
H279 H -0.803420 0.984938 0.508377 0.053 Uiso 1 1 calc R U . . .
C35 C -0.884(2) 1.179(2) 0.4908(8) 0.049(5) Uani 1 1 d . U . . .
H35 H -0.907931 1.153372 0.498952 0.058 Uiso 1 1 calc R U . . .
C281 C -0.9429(19) 0.8655(19) 0.4820(7) 0.040(5) Uani 1 1 d . U . . .
H281 H -0.938843 0.869257 0.466242 0.048 Uiso 1 1 calc R U . . .
C141 C -0.549(2) 0.859(2) 0.5628(8) 0.052(4) Uani 1 1 d . U . . .
C283 C -0.9478(18) 1.2278(19) 0.5381(7) 0.037(4) Uani 1 1 d . U . . .
H28A H -0.967342 1.258382 0.526973 0.045 Uiso 1 1 calc R U . . .
H28B H -0.960146 1.188371 0.535168 0.045 Uiso 1 1 calc R U . . .
C71 C -0.817(2) 0.925(2) 0.4516(7) 0.045(5) Uani 1 1 d . U . . .
H71 H -0.824445 0.908872 0.437953 0.054 Uiso 1 1 calc R U . . .
C285 C -1.1096(15) 0.9842(14) 0.7704(4) 0.050(4) Uani 1 1 d G U . . .
C143 C -1.1451(13) 0.9396(14) 0.7782(5) 0.053(5) Uani 1 1 d G U . . .
H143 H -1.171259 0.925413 0.768507 0.064 Uiso 1 1 calc R U . . .
C287 C -1.1416(14) 0.9160(13) 0.8006(5) 0.060(6) Uani 1 1 d G U . . .
H287 H -1.165322 0.886167 0.805774 0.072 Uiso 1 1 calc R U . . .
C9 C -1.1025(16) 0.9372(15) 0.8151(4) 0.064(6) Uani 1 1 d G U . . .
H9 H -1.100148 0.921455 0.830027 0.076 Uiso 1 1 calc R U . . .
C289 C -1.0670(14) 0.9818(15) 0.8073(5) 0.064(6) Uani 1 1 d G U . . .
H289 H -1.040911 0.995989 0.817013 0.076 Uiso 1 1 calc R U . . .
C145 C -1.0706(14) 1.0054(13) 0.7850(5) 0.059(5) Uani 1 1 d G U . . .
H145 H -1.046847 1.035235 0.779746 0.071 Uiso 1 1 calc R U . . .
C291 C -0.805(2) 1.242(2) 0.4665(9) 0.057(6) Uani 1 1 d . U . . .
H291 H -0.776259 1.262373 0.458008 0.069 Uiso 1 1 calc R U . . .
C73 C -0.6286(18) 1.2503(19) 0.6509(9) 0.135(7) Uani 1 1 d G U . . .
C293 C -0.5693(17) 1.217(2) 0.6549(8) 0.138(9) Uani 1 1 d DG U . . .
H293 H -0.555303 1.179747 0.648066 0.166 Uiso 1 1 calc DR U . . .
C147 C -0.531(2) 1.241(3) 0.6692(9) 0.141(9) Uani 1 1 d G U . . .
H147 H -0.491329 1.218571 0.671829 0.169 Uiso 1 1 calc R U . . .
C295 C -0.552(3) 1.297(3) 0.6794(9) 0.142(9) Uani 1 1 d G U . . .
H295 H -0.526269 1.312374 0.688938 0.170 Uiso 1 1 calc R U . . .
C37 C -0.611(3) 1.330(2) 0.6754(9) 0.142(9) Uani 1 1 d G U . . .
H37 H -0.625185 1.367354 0.682286 0.170 Uiso 1 1 calc R U . . .
C297 C -0.650(2) 1.3065(18) 0.6612(9) 0.139(9) Uani 1 1 d DG U . . .
H297 H -0.689160 1.328532 0.658523 0.167 Uiso 1 1 calc R U . . .
C149 C -1.028(3) 1.460(3) 0.5569(10) 0.071(6) Uani 1 1 d . U . . .
H149 H -1.025405 1.477610 0.542245 0.085 Uiso 1 1 calc R U . . .
C299 C -0.802(3) 0.732(3) 0.7442(10) 0.046(8) Uani 0.605(4) 1 d D U P E 6
H29A H -0.818303 0.766203 0.753854 0.069 Uiso 0.605(4) 1 d R U P E 6
H29B H -0.775843 0.700483 0.752684 0.069 Uiso 0.605(4) 1 d R U P E 6
H29C H -0.836653 0.715413 0.738974 0.069 Uiso 0.605(4) 1 d R U P E 6
C75 C -1.024(2) 0.743(2) 0.7490(7) 0.044(4) Uani 1 1 d . U . . .
C301 C -0.854(2) 0.975(2) 0.4597(8) 0.047(5) Uani 1 1 d . U . . .
H301 H -0.882671 0.998632 0.450278 0.057 Uiso 1 1 calc R U . . .
C151 C -0.764(4) 1.086(3) 0.7516(11) 0.069(11) Uani 0.605(4) 1 d D U P E 6
H15K H -0.793998 1.064686 0.759554 0.104 Uiso 0.605(4) 1 d R U P E 6
H15L H -0.732498 1.091726 0.761603 0.104 Uiso 0.605(4) 1 d R U P E 6
H15M H -0.745328 1.062966 0.738944 0.104 Uiso 0.605(4) 1 d R U P E 6
C303 C -0.660(4) 0.681(3) 0.6957(17) 0.049(9) Uani 0.395(4) 1 d D U P E 5
H30C H -0.657949 0.681419 0.711852 0.073 Uiso 0.395(4) 1 d R U P E 5
H30D H -0.631209 0.646709 0.689922 0.073 Uiso 0.395(4) 1 d R U P E 5
H30E H -0.701519 0.678249 0.691872 0.073 Uiso 0.395(4) 1 d R U P E 5
C19 C -0.526(2) 1.086(2) 0.6124(14) 0.052(7) Uani 0.517(9) 1 d D U P F 1
H19D H -0.529355 1.106973 0.597604 0.079 Uiso 0.517(9) 1 d R U P F 1
H19E H -0.484545 1.085693 0.617484 0.079 Uiso 0.517(9) 1 d R U P F 1
H19F H -0.555895 1.108603 0.622804 0.079 Uiso 0.517(9) 1 d R U P F 1
C305 C -1.183(2) 1.069(2) 0.7406(7) 0.045(4) Uani 1 1 d . U . . .
C153 C -1.231(2) 1.072(2) 0.7592(8) 0.049(5) Uani 1 1 d . U . . .
H153 H -1.226728 1.045135 0.772119 0.059 Uiso 1 1 calc R U . . .
C307 C -1.2254(19) 1.017(2) 0.6180(7) 0.043(5) Uani 1 1 d . U . . .
H30F H -1.258666 0.996348 0.613962 0.052 Uiso 1 1 calc R U . . .
H30G H -1.206064 1.032694 0.604167 0.052 Uiso 1 1 calc R U . . .
C77 C -0.8395(17) 0.911(3) 0.7687(9) 0.056(7) Uani 0.605(4) 1 d D U P E 6
H77A H -0.826770 0.867118 0.767973 0.084 Uiso 0.605(4) 1 d R U P E 6
H77B H -0.819480 0.926078 0.780953 0.084 Uiso 0.605(4) 1 d R U P E 6
H77C H -0.827870 0.931448 0.754693 0.084 Uiso 0.605(4) 1 d R U P E 6
C309 C -1.173(2) 0.968(2) 0.6321(8) 0.044(5) Uani 1 1 d . U . . .
H30H H -1.136864 0.954542 0.621949 0.053 Uiso 1 1 calc R U . . .
H30I H -1.158849 0.988676 0.644414 0.053 Uiso 1 1 calc R U . . .
C155 C -0.858(3) 0.840(3) 0.7567(6) 0.054(6) Uani 0.395(4) 1 d D U P E 5
H155 H -0.856362 0.882943 0.759958 0.064 Uiso 0.395(4) 1 calc R U P E 5
C311 C -0.551(5) 0.927(5) 0.7004(12) 0.060(11) Uani 0.395(4) 1 d D U P E 5
H31A H -0.519192 0.947457 0.692463 0.090 Uiso 0.395(4) 1 d R U P E 5
H31B H -0.535502 0.909737 0.714653 0.090 Uiso 0.395(4) 1 d R U P E 5
H31C H -0.587692 0.957537 0.702923 0.090 Uiso 0.395(4) 1 d R U P E 5
C39 C -0.823(3) 0.987(4) 0.7590(11) 0.051(9) Uani 0.395(4) 1 d D U P E 5
H39A H -0.831100 0.966582 0.745777 0.077 Uiso 0.395(4) 1 d R U P E 5
H39B H -0.827650 0.960362 0.772247 0.077 Uiso 0.395(4) 1 d R U P E 5
H39C H -0.781670 0.996312 0.757757 0.077 Uiso 0.395(4) 1 d R U P E 5
C313 C -0.8520(16) 0.603(3) 0.7031(9) 0.086(10) Uani 1 1 d D U . . .
H31D H -0.848925 0.559440 0.707350 0.128 Uiso 1 1 d R U . . .
H31E H -0.866285 0.627260 0.716010 0.128 Uiso 1 1 d R U . . .
H31F H -0.811835 0.611350 0.697660 0.128 Uiso 1 1 d R U . . .
C157 C -0.597(3) 1.090(4) 0.7062(12) 0.078(10) Uani 0.605(4) 1 d D U P E 6
H15N H -0.624948 1.128352 0.702704 0.117 Uiso 0.605(4) 1 d R U P E 6
H15O H -0.560088 1.099452 0.712314 0.117 Uiso 0.605(4) 1 d R U P E 6
H15P H -0.617488 1.065412 0.717244 0.117 Uiso 0.605(4) 1 d R U P E 6
C315 C -0.7126(18) 0.8015(18) 0.5124(7) 0.035(4) Uani 1 1 d . U . . .
H31G H -0.713570 0.780600 0.498414 0.042 Uiso 1 1 calc R U . . .
H31H H -0.678612 0.778792 0.521061 0.042 Uiso 1 1 calc R U . . .
C79 C -1.0442(19) 1.254(2) 0.5609(7) 0.042(4) Uani 1 1 d . U . . .
H79A H -1.056162 1.213353 0.561965 0.051 Uiso 1 1 calc R U . . .
H79B H -1.057556 1.274060 0.546431 0.051 Uiso 1 1 calc R U . . .
C317 C -0.813(2) 1.248(2) 0.4905(8) 0.054(5) Uani 1 1 d . U . . .
H317 H -0.790629 1.273019 0.498092 0.064 Uiso 1 1 calc R U . . .
C159 C -1.0887(14) 0.6607(12) 0.7223(3) 0.047(5) Uani 1 1 d G U . . .
H159 H -1.079542 0.656984 0.737574 0.057 Uiso 1 1 calc R U . . .
C319 C -1.1198(14) 0.6179(11) 0.7133(4) 0.049(5) Uani 1 1 d G U . . .
H319 H -1.131454 0.585465 0.722460 0.059 Uiso 1 1 calc R U . . .
C5 C -1.1336(13) 0.6235(11) 0.6905(4) 0.048(5) Uani 1 1 d G U . . .
H5 H -1.154395 0.594854 0.684399 0.057 Uiso 1 1 calc R U . . .
C321 C -1.1162(13) 0.6720(13) 0.6767(3) 0.046(5) Uani 1 1 d G U . . .
H321 H -1.125423 0.675763 0.661452 0.055 Uiso 1 1 calc R U . . .
C161 C -1.0851(13) 0.7149(11) 0.6858(4) 0.042(5) Uani 1 1 d G U . . .
H161 H -1.073511 0.747284 0.676566 0.050 Uiso 1 1 calc R U . . .
C323 C -1.0714(13) 0.7092(11) 0.7086(4) 0.040(4) Uani 1 1 d G U . . .
C81 C -1.050(2) 0.764(2) 0.7897(8) 0.051(5) Uani 1 1 d . U . . .
H81 H -1.074834 0.785953 0.800682 0.061 Uiso 1 1 calc R U . . .
C325 C -0.9003(13) 0.6735(11) 0.5207(5) 0.046(4) Uani 1 1 d G U . . .
C163 C -0.9622(12) 0.6653(12) 0.5230(5) 0.054(5) Uani 1 1 d G U . . .
H163 H -0.991812 0.695064 0.530102 0.064 Uiso 1 1 calc R U . . .
C327 C -0.9799(10) 0.6128(14) 0.5148(6) 0.058(6) Uani 1 1 d G U . . .
H327 H -1.021384 0.607415 0.516335 0.069 Uiso 1 1 calc R U . . .
C41 C -0.9357(14) 0.5684(12) 0.5042(5) 0.059(6) Uani 1 1 d G U . . .
H41 H -0.947543 0.533289 0.498678 0.071 Uiso 1 1 calc R U . . .
C329 C -0.8737(13) 0.5765(12) 0.5019(5) 0.058(6) Uani 1 1 d G U . . .
H329 H -0.844131 0.546812 0.494788 0.070 Uiso 1 1 calc R U . . .
C165 C -0.8560(10) 0.6290(14) 0.5101(5) 0.052(5) Uani 1 1 d G U . . .
H165 H -0.814559 0.634461 0.508555 0.062 Uiso 1 1 calc R U . . .
C331 C -0.860(4) 1.303(4) 0.6554(13) 0.108(6) Uani 1 1 d . U . . .
H33D H -0.886985 1.294370 0.643939 0.130 Uiso 1 1 calc R U . . .
H33E H -0.849127 1.343872 0.651265 0.130 Uiso 1 1 calc R U . . .
C83 C -1.228(2) 0.786(2) 0.6383(8) 0.052(4) Uani 1 1 d . U . . .
C333 C -1.033(2) 0.655(2) 0.5919(8) 0.045(5) Uani 1 1 d . U . . .
H333 H -0.997204 0.625643 0.585664 0.054 Uiso 1 1 calc R U . . .
C167 C -1.346(2) 0.900(2) 0.5874(9) 0.058(6) Uani 1 1 d . U . . .
H167 H -1.388784 0.900064 0.589538 0.069 Uiso 1 1 calc R U . . .
C335 C -1.036(3) 1.399(3) 0.5991(10) 0.068(6) Uani 1 1 d . U . . .
H335 H -1.035495 1.377153 0.613121 0.081 Uiso 1 1 calc R U . . .
C21 C -1.051(3) 1.407(3) 0.5598(10) 0.068(6) Uani 1 1 d . U . . .
H21 H -1.061772 1.389840 0.546889 0.081 Uiso 1 1 calc R U . . .
C337 C -1.264(2) 0.933(2) 0.5646(9) 0.054(6) Uani 1 1 d . U . . .
H337 H -1.248642 0.955428 0.552262 0.065 Uiso 1 1 calc R U . . .
C169 C -1.223(2) 0.903(2) 0.5803(8) 0.051(5) Uani 1 1 d . U . . .
H169 H -1.180475 0.896731 0.576834 0.061 Uiso 1 1 calc R U . . .
C339 C -0.492(2) 0.832(2) 0.5261(8) 0.047(5) Uani 1 1 d . U . . .
H339 H -0.472292 0.804466 0.515557 0.056 Uiso 1 1 calc R U . . .
C85 C -0.648(2) 0.791(2) 0.5815(8) 0.065(5) Uani 1 1 d D U . . .
H85A H -0.681722 0.822682 0.576771 0.078 Uiso 1 1 calc R U . . .
H85B H -0.636185 0.761377 0.569510 0.078 Uiso 1 1 calc R U . . .
C341 C -0.500(2) 0.898(2) 0.5208(8) 0.048(5) Uani 1 1 d . U . . .
H341 H -0.485085 0.913340 0.507118 0.058 Uiso 1 1 calc R U . . .
C171 C -0.796(4) 1.252(4) 0.6539(15) 0.114(7) Uani 1 1 d . U . . .
H17G H -0.774828 1.250034 0.667903 0.137 Uiso 1 1 calc R U . . .
H17H H -0.806185 1.211452 0.651488 0.137 Uiso 1 1 calc R U . . .
C343 C -0.513(2) 0.810(2) 0.5469(8) 0.048(5) Uani 1 1 d . U . . .
H343 H -0.506279 0.768019 0.551047 0.058 Uiso 1 1 calc R U . . .
C43 C -0.797(3) 1.148(2) 0.7432(6) 0.062(6) Uani 0.605(4) 1 d D U P E 6
H43 H -0.824584 1.173396 0.754104 0.075 Uiso 0.605(4) 1 calc R U P E 6
C345 C -1.060(2) 0.774(2) 0.7663(8) 0.048(5) Uani 1 1 d . U . . .
H345 H -1.093330 0.804314 0.762230 0.057 Uiso 1 1 calc R U . . .
C173 C -0.715(2) 0.735(2) 0.5940(10) 0.073(8) Uani 1 1 d D U . . .
H17I H -0.703802 0.719520 0.578997 0.087 Uiso 1 1 calc DR U . . .
H17J H -0.751576 0.767560 0.593138 0.087 Uiso 1 1 calc R U . . .
C347 C -0.960(2) 0.686(2) 0.7770(8) 0.053(6) Uani 1 1 d . U . . .
H347 H -0.923949 0.658386 0.780644 0.063 Uiso 1 1 calc R U . . .
C87 C -0.998(2) 0.716(2) 0.7953(8) 0.054(6) Uani 1 1 d . U . . .
H87 H -0.988955 0.705448 0.810400 0.064 Uiso 1 1 calc R U . . .
C349 C -0.974(2) 0.697(2) 0.7536(8) 0.050(5) Uani 1 1 d . U . . .
H349 H -0.951184 0.673501 0.742271 0.060 Uiso 1 1 calc R U . . .
C175 C -1.3213(13) 1.1258(15) 0.6181(5) 0.057(5) Uani 1 1 d G U . . .
C351 C -1.3214(14) 1.1177(14) 0.5949(5) 0.061(6) Uani 1 1 d G U . . .
H351 H -1.290318 1.089175 0.587954 0.073 Uiso 1 1 calc R U . . .
C11 C -1.3681(16) 1.1523(16) 0.5821(4) 0.066(6) Uani 1 1 d G U . . .
H11 H -1.368165 1.146876 0.566549 0.079 Uiso 1 1 calc R U . . .
C353 C -1.4146(14) 1.1950(15) 0.5924(5) 0.067(6) Uani 1 1 d G U . . .
H353 H -1.445759 1.218111 0.583837 0.081 Uiso 1 1 calc R U . . .
C177 C -1.4144(14) 1.2031(14) 0.6156(6) 0.067(6) Uani 1 1 d G U . . .
H177 H -1.445507 1.231646 0.622529 0.080 Uiso 1 1 calc R U . . .
C355 C -1.3678(16) 1.1685(16) 0.6284(4) 0.063(6) Uani 1 1 d G U . . .
H355 H -1.367660 1.173945 0.643934 0.075 Uiso 1 1 calc R U . . .
C89 C -0.533(2) 0.939(2) 0.5373(8) 0.047(5) Uani 1 1 d . U . . .
H89 H -0.538881 0.981375 0.534348 0.057 Uiso 1 1 calc R U . . .
C357 C -0.645180 1.153160 0.528181 0.060(8) Uani 1 1 d . U . . .
H35M H -0.660630 1.185560 0.516640 0.090 Uiso 1 1 d R U . . .
H35N H -0.601440 1.154750 0.529640 0.090 Uiso 1 1 d DR U . . .
H35O H -0.667790 1.160140 0.541840 0.090 Uiso 1 1 d DR U . . .
C179 C -0.6267(11) 0.8736(13) 0.4875(5) 0.046(4) Uani 1 1 d G U . . .
C359 C -0.5873(13) 0.8175(10) 0.4836(5) 0.050(5) Uani 1 1 d G U . . .
H359 H -0.596134 0.780672 0.490663 0.060 Uiso 1 1 calc R U . . .
C45 C -0.5347(12) 0.8163(11) 0.4691(5) 0.053(6) Uani 1 1 d G U . . .
H45 H -0.508291 0.778783 0.466472 0.064 Uiso 1 1 calc R U . . .
C361 C -0.5214(11) 0.8713(13) 0.4585(5) 0.055(6) Uani 1 1 d G U . . .
H361 H -0.486215 0.870575 0.448789 0.066 Uiso 1 1 calc R U . . .
C181 C -0.5608(13) 0.9275(11) 0.4624(5) 0.052(5) Uani 1 1 d G U . . .
H181 H -0.551981 0.964255 0.455296 0.063 Uiso 1 1 calc R U . . .
C363 C -0.6135(12) 0.9286(10) 0.4769(5) 0.048(5) Uani 1 1 d G U . . .
H363 H -0.639825 0.966145 0.479486 0.058 Uiso 1 1 calc R U . . .
C91 C -1.023(2) 1.212(3) 0.7622(8) 0.073(10) Uani 1 1 d . U . . .
H91A H -0.986586 1.230872 0.760093 0.109 Uiso 1 1 d DR U . . .
H91B H -1.011676 1.167722 0.763713 0.109 Uiso 1 1 d R U . . .
H91C H -1.046676 1.227242 0.775633 0.109 Uiso 1 1 d R U . . .
C365 C -1.1642(15) 1.3148(19) 0.5746(6) 0.071(5) Uani 1 1 d G U . . .
C183 C -1.1792(17) 1.3555(17) 0.5560(7) 0.080(6) Uani 1 1 d G U . . .
H183 H -1.152685 1.382925 0.550921 0.096 Uiso 1 1 calc R U . . .
C367 C -1.2340(19) 1.3551(18) 0.5451(6) 0.084(7) Uani 1 1 d G U . . .
H367 H -1.244083 1.382324 0.532617 0.101 Uiso 1 1 calc R U . . .
C23 C -1.2737(15) 1.314(2) 0.5527(7) 0.086(7) Uani 1 1 d G U . . .
H23 H -1.310334 1.313886 0.545335 0.103 Uiso 1 1 calc R U . . .
C369 C -1.2586(17) 1.2735(17) 0.5713(7) 0.083(7) Uani 1 1 d G U . . .
H369 H -1.285188 1.246051 0.576359 0.100 Uiso 1 1 calc R U . . .
C185 C -1.2039(18) 1.2738(17) 0.5822(6) 0.079(6) Uani 1 1 d G U . . .
H185 H -1.193790 1.246652 0.594664 0.095 Uiso 1 1 calc R U . . .
C371 C -0.5187(16) 0.7698(17) 0.6010(7) 0.076(5) Uani 1 1 d G U . . .
C93 C -0.5087(17) 0.7074(19) 0.5956(6) 0.081(6) Uani 1 1 d G U . . .
H93 H -0.535772 0.693047 0.586374 0.097 Uiso 1 1 calc R U . . .
C373 C -0.4581(19) 0.6666(14) 0.6041(7) 0.085(7) Uani 1 1 d G U . . .
H373 H -0.451340 0.624875 0.600557 0.102 Uiso 1 1 calc R U . . .
C187 C -0.4175(16) 0.6881(18) 0.6180(7) 0.087(7) Uani 1 1 d G U . . .
H187 H -0.383698 0.660791 0.623647 0.104 Uiso 1 1 calc R U . . .
C375 C -0.4276(17) 0.7505(19) 0.6233(7) 0.085(7) Uani 1 1 d G U . . .
H375 H -0.400488 0.764878 0.632555 0.102 Uiso 1 1 calc R U . . .
C47 C -0.4782(19) 0.7913(14) 0.6148(7) 0.081(6) Uani 1 1 d G U . . .
H47 H -0.484919 0.833051 0.618373 0.097 Uiso 1 1 calc R U . . .
C377 C -0.722(3) 0.705(3) 0.7134(12) 0.050(8) Uani 0.605(4) 1 d D U P E 6
H37D H -0.744440 0.675666 0.707734 0.075 Uiso 0.605(4) 1 d R U P E 6
H37E H -0.693650 0.684636 0.724454 0.075 Uiso 0.605(4) 1 d R U P E 6
H37F H -0.698380 0.722166 0.701024 0.075 Uiso 0.605(4) 1 d R U P E 6
C189 C -0.607(3) 0.710(5) 0.6660(16) 0.050(9) Uani 0.395(4) 1 d D U P E 5
H18G H -0.632567 0.687317 0.658437 0.074 Uiso 0.395(4) 1 d R U P E 5
H18H H -0.570557 0.682467 0.671227 0.074 Uiso 0.395(4) 1 d R U P E 5
H18I H -0.593367 0.741327 0.655487 0.074 Uiso 0.395(4) 1 d R U P E 5
C379 C -0.767(2) 0.755(3) 0.7244(7) 0.050(4) Uani 0.605(4) 1 d D U P E 6
H379 H -0.742951 0.785370 0.729705 0.060 Uiso 0.605(4) 1 calc R U P E 6
C95 C -0.526(3) 0.819(4) 0.6801(15) 0.059(8) Uani 0.605(4) 1 d D U P E 6
H95A H -0.492373 0.794675 0.671771 0.088 Uiso 0.605(4) 1 d R U P E 6
H95B H -0.518782 0.814515 0.695991 0.088 Uiso 0.605(4) 1 d R U P E 6
H95C H -0.528742 0.862375 0.675221 0.088 Uiso 0.605(4) 1 d R U P E 6
C381 C -0.4907(13) 0.983(3) 0.5957(9) 0.055(9) Uani 0.517(9) 1 d D U P F 1
H38G H -0.469397 0.940374 0.597139 0.083 Uiso 0.517(9) 1 d R U P F 1
H38H H -0.465597 1.006814 0.586239 0.083 Uiso 0.517(9) 1 d R U P F 1
H38I H -0.529947 0.983694 0.588919 0.083 Uiso 0.517(9) 1 d DR U P F 1
C191 C -0.643(2) 0.740(3) 0.6855(11) 0.050(5) Uani 0.395(4) 1 d D U P E 5
H191 H -0.623931 0.766753 0.694874 0.060 Uiso 0.395(4) 1 calc R U P E 5
C383 C -1.193(2) 1.115(2) 0.7233(8) 0.047(5) Uani 1 1 d . U . . .
H383 H -1.160418 1.118654 0.712778 0.056 Uiso 1 1 calc R U . . .
C3 C -1.290(2) 1.160(2) 0.7384(8) 0.051(5) Uani 1 1 d . U . . .
H3 H -1.322502 1.193544 0.738378 0.061 Uiso 1 1 calc R U . . .
C385 C -1.248(2) 1.156(2) 0.7206(8) 0.050(5) Uani 1 1 d . U . . .
H385 H -1.255275 1.180386 0.707289 0.060 Uiso 1 1 calc R U . . .
C193 C -0.975(2) 1.375(2) 0.6749(9) 0.112(6) Uani 1 1 d G U . . .
C387 C -0.968(2) 1.438(3) 0.6734(9) 0.117(8) Uani 1 1 d G U . . .
H387 H -0.930774 1.449220 0.676858 0.140 Uiso 1 1 calc R U . H 2
C97 C -1.018(3) 1.4832(19) 0.6668(9) 0.120(8) Uani 1 1 d G U . . .
H97 H -1.013504 1.524993 0.665844 0.144 Uiso 1 1 calc R U . I 2
C389 C -1.074(2) 1.466(2) 0.6617(9) 0.119(8) Uani 1 1 d G U . . .
H389 H -1.107090 1.496622 0.657271 0.143 Uiso 1 1 calc R U . . .
C195 C -1.080(2) 1.404(3) 0.6631(9) 0.118(8) Uani 1 1 d G U . . .
H195 H -1.117948 1.392478 0.659712 0.141 Uiso 1 1 calc R U . . .
C391 C -1.031(3) 1.3585(19) 0.6697(9) 0.115(8) Uani 1 1 d G U . . .
H391 H -1.035219 1.316704 0.670726 0.138 Uiso 1 1 calc R U . . .
C49 C -1.072(3) 1.293(2) 0.7358(9) 0.064(9) Uani 1 1 d . U . . .
H49A H -1.068595 1.317316 0.748679 0.097 Uiso 1 1 calc R U . . .
H49B H -1.112327 1.305297 0.729781 0.097 Uiso 1 1 calc R U . . .
H49C H -1.040497 1.300799 0.724309 0.097 Uiso 1 1 calc R U . . .
C393 C -1.322(2) 0.931(2) 0.5667(9) 0.057(6) Uani 1 1 d . U . . .
H393 H -1.349165 0.949199 0.555509 0.068 Uiso 1 1 calc R U . . .
C197 C -0.946(3) 0.877(3) 0.7800(14) 0.055(9) Uani 0.605(4) 1 d D U P E 6
H19G H -0.984865 0.896482 0.787189 0.083 Uiso 0.605(4) 1 d R U P E 6
H19H H -0.924365 0.846712 0.790289 0.083 Uiso 0.605(4) 1 d R U P E 6
H19I H -0.954375 0.857942 0.766569 0.083 Uiso 0.605(4) 1 d R U P E 6
C395 C -1.058(2) 0.622(2) 0.6130(8) 0.053(8) Uani 1 1 d . U . . .
H39D H -1.087267 0.650850 0.621504 0.080 Uiso 1 1 d R U . . .
H39E H -1.023717 0.604440 0.622204 0.080 Uiso 1 1 d R U . . .
H39F H -1.078067 0.589240 0.608304 0.080 Uiso 1 1 d R U . . .
C99 C -0.9080(19) 0.926(2) 0.7730(5) 0.054(6) Uani 0.605(4) 1 d D U P E 6
H99 H -0.917697 0.959786 0.783560 0.065 Uiso 0.605(4) 1 calc R U P E 6
C397 C -1.075(2) 0.668(2) 0.5750(8) 0.052(8) Uani 1 1 d . U . . .
H39G H -1.099924 0.636011 0.575521 0.077 Uiso 1 1 d R U . . .
H39H H -1.053284 0.669711 0.560400 0.077 Uiso 1 1 d R U . . .
H39I H -1.101174 0.707671 0.577401 0.077 Uiso 1 1 d R U . . .
C199 C -1.278(2) 0.744(2) 0.6659(9) 0.062(6) Uani 1 1 d . U . . .
H199 H -1.289159 0.747066 0.681249 0.074 Uiso 1 1 calc R U . . .
C399 C -0.663(2) 0.759(2) 0.6030(7) 0.069(7) Uani 1 1 d D U . . .
H39J H -0.629797 0.726262 0.607894 0.083 Uiso 1 1 calc R U . . .
H39K H -0.676100 0.787692 0.615092 0.083 Uiso 1 1 calc R U . . .
C25 C -1.228(2) 0.735(2) 0.6271(9) 0.059(5) Uani 1 1 d . U . . .
H25 H -1.210194 0.731624 0.612451 0.070 Uiso 1 1 calc R U . . .
C401 C -1.256(2) 0.686(3) 0.6381(9) 0.062(6) Uani 1 1 d . U . . .
H401 H -1.255267 0.649838 0.630557 0.074 Uiso 1 1 calc R U . . .
C201 C -0.866(3) 1.047(3) 0.7612(7) 0.046(5) Uani 0.395(4) 1 d D U P E 5
H201 H -0.844385 1.081770 0.764469 0.055 Uiso 0.395(4) 1 calc R U P E 5
C403 C -0.878(2) 1.177(2) 0.4681(8) 0.053(5) Uani 1 1 d . U . . .
H403 H -0.902211 1.153716 0.460702 0.064 Uiso 1 1 calc R U . . .
C101 C -0.565(4) 0.878(3) 0.6865(9) 0.061(7) Uani 0.395(4) 1 d D U P E 5
H101 H -0.588429 0.847818 0.694297 0.073 Uiso 0.395(4) 1 calc R U P E 5
C405 C -0.737(5) 1.189(4) 0.7200(15) 0.068(10) Uani 0.395(4) 1 d D U P E 5
H40L H -0.750664 1.226731 0.711251 0.102 Uiso 0.395(4) 1 d R U P E 5
H40M H -0.723124 1.198901 0.734312 0.102 Uiso 0.395(4) 1 d R U P E 5
H40N H -0.770604 1.166061 0.722551 0.102 Uiso 0.395(4) 1 d R U P E 5
C203 C -0.692440 1.095570 0.499469 0.058(8) Uani 1 1 d . U . . .
H20A H -0.736280 1.104040 0.503510 0.087 Uiso 1 1 d R U . . .
H20B H -0.682000 1.055100 0.493260 0.087 Uiso 1 1 d R U . . .
H20C H -0.682340 1.126510 0.488360 0.087 Uiso 1 1 d R U . . .
C407 C -0.506(3) 0.851(5) 0.6746(18) 0.061(10) Uani 0.395(4) 1 d D U P E 5
H40O H -0.517431 0.839246 0.660120 0.092 Uiso 0.395(4) 1 d R U P E 5
H40P H -0.487971 0.813706 0.683130 0.092 Uiso 0.395(4) 1 d R U P E 5
H40Q H -0.475201 0.877646 0.672170 0.092 Uiso 0.395(4) 1 d R U P E 5
C51 C -0.795(3) 0.801(5) 0.7573(19) 0.050(9) Uani 0.395(4) 1 d D U P E 5
H51A H -0.793059 0.764740 0.748391 0.075 Uiso 0.395(4) 1 d R U P E 5
H51B H -0.787309 0.787630 0.772781 0.075 Uiso 0.395(4) 1 d R U P E 5
H51C H -0.764739 0.825000 0.751411 0.075 Uiso 0.395(4) 1 d R U P E 5
C409 C -0.911(3) 0.818(5) 0.7697(6) 0.056(9) Uani 0.395(4) 1 d D U P E 5
H40R H -0.944043 0.817555 0.759670 0.085 Uiso 0.395(4) 1 d R U P E 5
H40S H -0.925233 0.844775 0.781820 0.085 Uiso 0.395(4) 1 d R U P E 5
H40T H -0.897313 0.776045 0.775820 0.085 Uiso 0.395(4) 1 d R U P E 5
C205 C -0.950940 0.594890 0.684870 0.090(10) Uani 1 1 d D U . . .
H20D H -0.967600 0.605780 0.699430 0.135 Uiso 1 1 d R U . . .
H20E H -0.980200 0.615280 0.673490 0.135 Uiso 1 1 d R U . . .
H20F H -0.945220 0.551080 0.683130 0.135 Uiso 1 1 d R U . . .
C411 C -1.219(2) 1.3020(7) 0.6587(3) 0.061(5) Uani 1 1 d D U . . .
H411 H -1.253181 1.282149 0.654508 0.074 Uiso 1 1 calc R U . . .
C103 C -1.239260 1.325281 0.681141 0.080(10) Uani 1 1 d D U . . .
H10J H -1.253350 1.292480 0.690420 0.120 Uiso 1 1 d R U . . .
H10K H -1.207350 1.340580 0.688650 0.120 Uiso 1 1 d R U . . .
H10L H -1.273650 1.358590 0.678710 0.120 Uiso 1 1 d R U . . .
C413 C -1.206990 1.340721 0.638460 0.088(10) Uani 1 1 d D U . . .
H41F H -1.167660 1.354980 0.638240 0.132 Uiso 1 1 d R U . . .
H41G H -1.208840 1.317680 0.625190 0.132 Uiso 1 1 d R U . . .
H41H H -1.240260 1.375910 0.638620 0.132 Uiso 1 1 d R U . . .
C207 C -0.758(4) 1.271(4) 0.6353(15) 0.121(7) Uani 1 1 d . U . . .
H20G H -0.754156 1.314169 0.636558 0.145 Uiso 1 1 calc R U . . .
H20H H -0.777197 1.267101 0.621198 0.145 Uiso 1 1 calc R U . . .
C415 C -0.850(2) 0.991(2) 0.4784(8) 0.048(5) Uani 1 1 d . U . . .
H415 H -0.881294 1.023568 0.483169 0.058 Uiso 1 1 calc R U . . .
C13 C -0.5814(14) 1.046(4) 0.6877(10) 0.076(6) Uani 0.605(4) 1 d D U P E 6
H13 H -0.579873 1.006283 0.696216 0.091 Uiso 0.605(4) 1 calc R U P E 6
C417 C -0.764(2) 0.896(2) 0.4656(7) 0.044(5) Uani 1 1 d . U . . .
H417 H -0.733532 0.865365 0.459949 0.053 Uiso 1 1 calc R U . . .
C209 C -0.578(4) 0.731(2) 0.6704(13) 0.051(7) Uani 0.605(4) 1 d D U P E 6
H20I H -0.598833 0.706952 0.681688 0.077 Uiso 0.605(4) 1 d R U P E 6
H20J H -0.535063 0.712052 0.668718 0.077 Uiso 0.605(4) 1 d R U P E 6
H20K H -0.597613 0.730623 0.656128 0.077 Uiso 0.605(4) 1 d R U P E 6
C419 C -0.558(2) 1.148(3) 0.6103(10) 0.054(9) Uani 0.483(9) 1 d D U P F 2
H41I H -0.554950 1.166383 0.595150 0.082 Uiso 0.483(9) 1 d R U P F 2
H41J H -0.520240 1.149743 0.617810 0.082 Uiso 0.483(9) 1 d DR U P F 2
H41K H -0.592810 1.171003 0.618530 0.082 Uiso 0.483(9) 1 d DR U P F 2
Si1 Si -0.500000 1.500000 0.500000 0.010(2) Uani 1 2 d DS U P J 3
O19 O -0.5573(15) 1.528(2) 0.5138(8) 0.007(5) Uani 0.25 1 d D U P J 3
O20 O -0.513(2) 1.4502(18) 0.4851(8) 0.010(5) Uani 0.25 1 d D U P J 3
O21 O -0.455(2) 1.474(2) 0.5180(7) 0.008(5) Uani 0.25 1 d D U P J 3
O22 O -0.475(2) 1.5468(19) 0.4841(7) 0.010(5) Uani 0.25 1 d D U P J 3
Si2 Si 0.000000 1.000000 1.000000 0.014(2) Uani 1 2 d DS U P K 4
O40 O -0.0712(4) 1.012(2) 1.0004(8) 0.013(6) Uani 0.25 1 d D U P K 4
O41 O 0.023(2) 1.0587(13) 1.0063(8) 0.018(6) Uani 0.25 1 d D U P K 4
O42 O 0.025(2) 0.983(2) 0.9761(3) 0.016(6) Uani 0.25 1 d D U P K 4
O43 O 0.022(2) 0.9463(15) 1.0169(6) 0.012(6) Uani 0.25 1 d D U P K 4
C105 C -0.5984(19) 1.283(2) 0.5685(3) 0.158(10) Uani 1 1 d G U . . .
H105 H -0.582094 1.295626 0.554557 0.190 Uiso 1 1 calc R U . . .
C421 C -0.6143(10) 1.224(2) 0.5714(4) 0.157(9) Uani 1 1 d G U . . .
H421 H -0.608561 1.197032 0.559350 0.189 Uiso 1 1 calc DR U . . .
C211 C -0.6387(9) 1.2041(17) 0.5923(5) 0.153(9) Uani 1 1 d DG U . . .
H211 H -0.649332 1.164554 0.594186 0.184 Uiso 1 1 calc R U . . .
C423 C -0.6473(10) 1.2437(11) 0.6103(3) 0.145(8) Uani 1 1 d DG U . . .
C53 C -0.631(2) 1.3028(12) 0.6074(4) 0.153(9) Uani 1 1 d DG U . . .
H53 H -0.637171 1.329263 0.619438 0.183 Uiso 1 1 calc R U . . .
C425 C -0.607(3) 1.3222(17) 0.5865(5) 0.157(9) Uani 1 1 d G U . . .
H425 H -0.596399 1.361742 0.584601 0.188 Uiso 1 1 calc R U . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
W1 O1 1.908(10) . ?
W1 O2 1.903(10) . ?
W1 O3 1.895(10) . ?
W1 O4 1.895(10) . ?
W1 O14 1.897(10) . ?
W2 O2 1.900(10) . ?
W2 O7 1.899(10) . ?
W2 O8 1.892(10) . ?
W2 O9 1.893(10) . ?
W2 O16 1.896(10) . ?
W3 O1 1.906(10) . ?
W3 O6 1.897(10) . ?
W3 O7 1.900(10) . ?
W3 O11 1.896(10) . ?
W3 O15 1.892(10) . ?
W4 O4 1.896(10) 2_486 ?
W4 O5 1.89(4) 2_486 ?
W4 O9 1.901(10) . ?
W4 O10 1.902(10) . ?
W4 O17 1.894(10) . ?
W5 O3 1.897(9) 2_486 ?
W5 O10 1.905(9) . ?
W5 O11 1.896(10) . ?
W5 O12 1.900(10) . ?
W5 O18 1.898(10) . ?
W6 O5 1.899(10) . ?
W6 O6 1.898(10) . ?
W6 O8 1.896(10) 2_486 ?
W6 O12 1.897(10) . ?
W6 O13 1.893(10) . ?
O14 C275 1.6(4) 1_565 ?
W1A O1A 1.907(10) . ?
W1A O2A 1.898(10) . ?
W1A O3A 1.898(10) . ?
W1A O4A 1.901(10) . ?
W1A O13A 1.894(10) . ?
W2A O1A 1.910(10) . ?
W2A O8A 1.898(10) . ?
W2A O9A 1.903(10) . ?
W2A O10A 1.905(7) . ?
W2A O17A 1.893(10) . ?
W3A O2A 1.898(10) . ?
W3A O10A 1.900(7) . ?
W3A O11A 1.898(10) . ?
W3A O12A 1.899(10) . ?
W3A O18A 1.896(10) . ?
W4A O5A 1.79(5) 2_486 ?
W4A O7A 1.900(10) . ?
W4A O8A 1.899(10) . ?
W4A O12A 1.893(10) 2_486 ?
W4A O16A 1.894(10) . ?
W5A O4A 1.902(10) . ?
W5A O6A 1.901(10) . ?
W5A O7A 1.900(10) . ?
W5A O11A 1.897(10) 2_486 ?
W5A O14A 1.898(10) . ?
W6A O3A 1.898(10) . ?
W6A O5A 2.03(5) . ?
W6A O6A 1.901(10) . ?
W6A O9A 2.00(4) 2_486 ?
W6A O15A 1.895(10) . ?
W7 O23 1.900(10) . ?
W7 O25 1.896(10) . ?
W7 O31 1.913(9) . ?
W7 O34 1.902(10) . ?
W7 O35 1.895(10) . ?
W7A O23A 1.890(9) . ?
W7A O24A 1.957(9) . ?
W7A O32A 1.969(10) . ?
W7A O33A 1.888(9) . ?
W7A O39A 1.897(10) . ?
W8 O23 1.902(10) . ?
W8 O24 1.900(10) . ?
W8 O32 2.47(2) 2_577 ?
W8 O38 2.29(4) 2_577 ?
W8A O24A 1.856(10) . ?
W8A O25A 1.896(10) . ?
W8A O30A 1.895(10) . ?
W8A O31A 1.889(7) . ?
W8A O35A 1.897(10) . ?
W9 O24 1.901(10) . ?
W9 O25 1.894(10) . ?
W9 O26 1.922(9) . ?
W9 O27 1.934(9) . ?
W9 O36 1.892(10) . ?
W9A O1B 1.896(10) . ?
W9A O23A 1.917(9) . ?
W9A O25A 1.897(10) . ?
W9A O26A 1.933(10) . ?
W9A O27A 1.979(9) . ?
W10 O29 1.971(18) 2_577 ?
W10 O30 1.907(8) . ?
W10 O31 1.886(9) . ?
W10 O32 1.906(9) . ?
W10 O33 1.879(9) . ?
W10A O27A 1.874(9) . ?
W10A O28A 1.940(9) . ?
W10A O31A 1.925(10) 2_577 ?
W10A O34A 1.897(10) . ?
W10A O38A 1.892(10) . ?
W11 O27 1.949(9) . ?
W11 O28 1.898(10) . ?
W11 O30 1.936(9) . ?
W11 O37 1.896(10) . ?
W11 O38 1.905(10) . ?
W11A O26A 1.938(10) . ?
W11A O28A 1.823(10) . ?
W11A O29A 2.138(10) . ?
W11A O32A 2.226(19) 2_577 ?
W11A O37A 1.897(10) . ?
W12 O26 1.912(9) . ?
W12 O28 1.898(10) . ?
W12 O29 1.898(10) . ?
W12 O34 1.81(3) 2_577 ?
W12 O39 1.893(10) . ?
W12A O29A 2.097(10) . ?
W12A O30A 1.896(10) . ?
W12A O33A 1.921(9) 2_577 ?
W12A O36A 1.897(10) . ?
W12A O38A 1.876(9) 2_577 ?
W13 O50 1.73(2) . ?
W13 O52 1.86(2) . ?
W13 O56 1.90(2) . ?
W13 O94 2.15(2) . ?
W13 O104 2.27(2) . ?
W13 O105 1.80(2) . ?
W14 O45 1.72(2) . ?
W14 O68 2.03(2) . ?
W14 O78 1.80(2) . ?
W14 O88 2.00(2) . ?
W14 O102 1.86(2) . ?
W14 O108 2.386(19) . ?
W15 O62 2.23(2) . ?
W15 O64 1.77(2) . ?
W15 O68 2.23(2) . ?
W15 O74 1.73(2) . ?
W15 O96 1.86(2) . ?
W15 O98 1.94(2) . ?
W19 O70 1.70(2) . ?
W19 O88 1.88(2) . ?
W19 O94 2.04(2) . ?
W19 O108 2.33(2) . ?
W19 O109 1.89(2) . ?
W19 O111 1.85(2) . ?
W20 O60 1.92(2) . ?
W20 O82 1.82(2) . ?
W20 O100 1.71(2) . ?
W20 O102 1.95(2) . ?
W20 O108 2.35(2) . ?
W20 O109 1.97(2) . ?
W21 Ag61 3.234(15) . ?
W21 O58 1.76(2) . ?
W21 O62 2.28(2) . ?
W21 O66 1.84(2) . ?
W21 O72 1.76(2) . ?
W21 O78 2.14(2) . ?
W21 O98 1.97(2) . ?
W24 O52 1.90(2) . ?
W24 O60 2.09(2) . ?
W24 O76 1.77(2) . ?
W24 O84 1.93(2) . ?
W24 O92 2.28(2) . ?
W24 O107 1.80(2) . ?
W26 O48 1.73(2) . ?
W26 O66 1.92(2) . ?
W26 O82 2.09(2) . ?
W26 O84 1.93(2) . ?
W26 O90 1.77(2) . ?
W26 O92 2.35(2) . ?
W28 O46 1.75(2) . ?
W28 O54 1.79(2) . ?
W28 O56 1.96(2) . ?
W28 O96 1.90(2) . ?
W28 O104 2.26(2) . ?
W28 O111 2.16(2) . ?
Ag Ag54 3.005(13) . ?
Ag S18 2.162(16) . ?
Ag P5 2.51(2) . ?
Ag O64 2.49(2) . ?
Ag1A S26A 2.53(3) . ?
Ag1A P9 2.878(19) . ?
Ag1A O105 2.53(2) . ?
Ag2 Ag4 3.039(6) . ?
Ag2 Ag50 2.729(7) . ?
Ag2 S14 2.08(2) . ?
Ag2 S32 2.398(18) . ?
Ag2 O107 2.49(2) . ?
Ag4 Ag7 2.857(13) . ?
Ag4 Ag17 2.927(5) . ?
Ag4 Ag18 2.759(4) . ?
Ag4 Ag27 2.934(12) . ?
Ag4 Ag35 2.792(6) . ?
Ag4 Ag44 2.802(4) . ?
Ag4 Ag45 3.077(7) . ?
Ag4 Ag50 2.725(4) . ?
Ag4 Ag57 2.998(14) . ?
Ag4 Ag61 2.853(15) . ?
Ag4 Cl2 2.406(12) . ?
Ag6 S10 2.450(10) . ?
Ag6 P12 2.389(10) . ?
Ag7 S15 2.25(7) . ?
Ag7 S31 2.48(4) . ?
Ag9 Ag30 3.257(7) . ?
Ag9 S26 2.485(18) . ?
Ag9 P21 2.45(2) . ?
Ag9 O54 2.50(2) . ?
Ag9A S26A 2.54(3) . ?
Ag9A P21 2.24(2) . ?
Ag9A O54 2.40(2) . ?
Ag10 S8 2.502(11) . ?
Ag10 P13 2.405(10) . ?
Ag10 O76 2.33(2) . ?
Ag12 S10 2.476(11) . ?
Ag12 P20 2.363(10) . ?
Ag12 O50 2.35(2) . ?
Ag15 Ag34 3.085(7) . ?
Ag15 S28 2.341(17) . ?
Ag15 S30 2.391(17) . ?
Ag17 Ag20 3.132(6) . ?
Ag17 Ag50 2.990(6) . ?
Ag17 S14 2.49(2) . ?
Ag17 S28 2.396(17) . ?
Ag18 Ag27 2.703(12) . ?
Ag18 Ag35 2.882(6) . ?
Ag18 Ag44 2.717(5) . ?
Ag18 Ag45 2.989(7) . ?
Ag18 Ag50 2.766(5) . ?
Ag18 Ag55 2.952(14) . ?
Ag18 Ag61 2.980(18) . ?
Ag18 O54 2.38(2) . ?
Ag18 O104 2.59(2) . ?
Ag18 O105 2.44(2) . ?
Ag20 Ag29 2.748(16) . ?
Ag20 S22 2.549(12) . ?
Ag20 S31 2.51(4) . ?
Ag20 P17 2.406(10) . ?
Ag20 O90 2.41(2) . ?
Ag24 S8 2.450(11) . ?
Ag24 P7 2.395(11) . ?
Ag27 Ag55 3.28(2) . ?
Ag27 S27 2.47(4) . ?
Ag27 S29 2.55(5) . ?
Ag29 Ag50 3.090(13) . ?
Ag29 S27 2.64(4) . ?
Ag29 S31 2.22(4) . ?
Ag30 S10 2.386(11) . ?
Ag30 S26 2.482(17) . ?
Ag30 S26A 2.27(3) . ?
Ag33 S26 2.593(17) . ?
Ag33 P9 2.325(15) . ?
Ag33 O105 2.51(2) . ?
Ag34 S18 2.507(13) . ?
Ag34 P16 2.398(11) . ?
Ag34 O58 2.43(2) . ?
Ag35 Ag45 3.304(8) . ?
Ag35 S2 2.47(2) . ?
Ag35 S30 2.448(17) . ?
Ag36 S8 2.360(11) . ?
Ag36 S22 2.377(14) . ?
Ag36 O84 2.50(2) . ?
Ag37 S18 2.713(16) . ?
Ag37 P5 2.384(18) . ?
Ag37 O64 2.42(2) . ?
Ag38 S12 2.416(12) . ?
Ag38 P18 2.351(12) . ?
Ag44 Ag50 2.758(6) . ?
Ag44 O58 2.45(2) . ?
Ag44 O64 2.41(2) . ?
Ag45 S2 2.43(2) . ?
Ag45 S32 2.35(2) . ?
Ag46 S12 2.470(12) . ?
Ag46 P22 2.368(13) . ?
Ag50 Ag61 2.17(2) . ?
Ag50 O90 2.39(2) . ?
Ag50 O92 2.41(2) . ?
Ag50 O107 2.59(2) . ?
Ag54 S12 2.392(12) . ?
Ag54 S18 2.363(14) . ?
Ag54 O98 2.48(2) . ?
Ag55 S7 2.38(4) . ?
Ag55 S29 2.42(5) . ?
Ag57 S7 2.38(4) . ?
Ag57 S15 1.93(6) . ?
Ag59 S22 2.428(15) . ?
Ag59 S27 2.83(4) . ?
Ag59 P24 2.319(17) . ?
Ag59 O107 2.47(2) . ?
Ag61 O58 2.07(3) . ?
Ag61 O62 2.53(3) . ?
Cl2 H2 1.6995 . ?
S2 C390 1.801(10) . ?
S7 C38 1.800(10) . ?
S8 C242 1.83(4) . ?
S10 C102 1.84(4) . ?
S12 C226 1.82(4) . ?
S14 C240 1.76(6) . ?
S15 C1 1.799(10) . ?
S18 C4 1.85(5) . ?
S22 C282 1.94(5) . ?
S26 C66 1.58(4) . ?
S26A C68 1.802(10) . ?
S27 C394 1.800(7) . ?
S28 C272 1.95(6) . ?
S29 C396 1.802(10) . ?
S30 C56 1.68(5) . ?
S31 C92 1.801(10) . ?
S32 C74 1.99(7) . ?
P5 C224 1.797(10) . ?
P5 C248 1.82(7) . ?
P5 C382 1.75(4) . ?
P7 C12 1.81(2) . ?
P7 C276 1.91(5) . ?
P7 C424 1.86(5) . ?
P9 C178 1.82(5) . ?
P9 C198 1.90(3) . ?
P9 C278 1.84(5) . ?
P12 C40 1.81(2) . ?
P12 C122 1.80(4) . ?
P12 C302 1.79(2) . ?
P13 C8 1.77(4) . ?
P13 C106 1.81(2) . ?
P13 C126 1.86(4) . ?
P16 C60 1.75(4) . ?
P16 C324 1.72(4) . ?
P16 C362 1.80(3) . ?
P17 C30 1.84(4) . ?
P17 C128 1.86(2) . ?
P17 C212 1.83(4) . ?
P18 C6 1.86(5) . ?
P18 C32 1.86(4) . ?
P18 C266 1.87(2) . ?
P20 C76 1.84(2) . ?
P20 C90 1.83(4) . ?
P20 C156 1.89(4) . ?
P21 C64 1.92(7) . ?
P21 C228 1.84(4) . ?
P21 C312 1.67(4) . ?
P22 C94 1.94(4) . ?
P22 C294 1.84(3) . ?
P22 C332 1.84(3) . ?
P24 C62 1.74(6) . ?
P24 C140 1.92(4) . ?
P24 C184 1.86(3) . ?
Si4 O62 1.64(2) . ?
Si4 O92 1.62(2) . ?
Si4 O104 1.65(2) . ?
Si4 O108 1.61(2) . ?
C1 H1 0.9800 . ?
C1 C196 1.481(10) . ?
C1 C404 1.480(10) . ?
C4 H4 0.9800 . ?
C4 C344 1.459(10) . ?
C4 C348 1.458(10) . ?
C6 C244 1.31(7) . ?
C6 C254 1.26(7) . ?
C8 C10 1.44(5) . ?
C8 C36 1.39(5) . ?
C10 H10 0.9300 . ?
C10 C120 1.39(6) . ?
C12 C14 1.3900 . ?
C12 C22 1.3900 . ?
C14 H14 0.9300 . ?
C14 C16 1.3900 . ?
C16 H16 0.9300 . ?
C16 C18 1.3900 . ?
C18 H18 0.9300 . ?
C18 C20 1.3900 . ?
C20 H20 0.9300 . ?
C20 C22 1.3900 . ?
C22 H22 0.9300 . ?
C24 H24A 0.9700 . ?
C24 H24B 0.9700 . ?
C24 C30 1.57(5) . ?
C24 C60 1.56(5) . ?
C26 H26 0.9300 . ?
C26 C310 1.45(6) . ?
C26 C414 1.26(6) . ?
C28 H28 0.9300 . ?
C28 C388 1.32(7) . ?
C28 C424 1.33(7) . ?
C30 H30A 0.9700 . ?
C30 H30B 0.9700 . ?
C32 H32A 0.9700 . ?
C32 H32B 0.9700 . ?
C32 C270 1.63(6) . ?
C34 H34A 0.9600 . ?
C34 H34B 0.9597 . ?
C34 H34C 0.9605 . ?
C34 C390 1.479(10) . ?
C36 H36 0.9300 . ?
C36 C162 1.33(6) . ?
C38 H38 0.9800 . ?
C38 C400 1.480(10) . ?
C38 C412 1.480(10) . ?
C40 C42 1.3900 . ?
C40 C50 1.3900 . ?
C42 H42 0.9300 . ?
C42 C44 1.3900 . ?
C44 H44 0.9300 . ?
C44 C46 1.3900 . ?
C46 H46 0.9300 . ?
C46 C48 1.3900 . ?
C48 H48 0.9300 . ?
C48 C50 1.3900 . ?
C50 H50 0.9300 . ?
C52 H52 0.9300 . ?
C52 C120 1.35(6) . ?
C52 C162 1.49(6) . ?
C54 H54 0.9300 . ?
C54 C174 1.42(6) . ?
C54 C246 1.35(6) . ?
C56 H56 0.9800 . ?
C56 C352 1.481(10) . ?
C56 C356 1.476(10) . ?
C58 H58 0.9300 . ?
C58 C388 1.43(7) . ?
C58 C398 1.40(7) . ?
C60 H60A 0.9700 . ?
C60 H60B 0.9700 . ?
C62 H62A 0.9700 . ?
C62 H62B 0.9700 . ?
C62 C416 1.477(10) . ?
C64 H64A 0.9700 . ?
C64 H64B 0.9700 . ?
C64 C96 1.37(9) . ?
C66 H66 0.9800 . ?
C66 C70 1.477(9) . ?
C66 C152 1.476(9) . ?
C68 H68 0.9800 . ?
C68 C72 1.481(9) . ?
C68 C426 1.479(10) . ?
C70 H70A 0.9604 . ?
C70 H70B 0.9598 . ?
C70 H70C 0.9613 . ?
C72 H72A 0.9578 . ?
C72 H72B 0.9597 . ?
C72 H72C 0.9609 . ?
C74 H74 0.9800 . ?
C74 C160 1.483(10) . ?
C74 C346 1.481(10) . ?
C76 C78 1.3900 . ?
C76 C86 1.3900 . ?
C78 H78 0.9300 . ?
C78 C80 1.3900 . ?
C80 H80 0.9300 . ?
C80 C82 1.3900 . ?
C82 H82 0.9300 . ?
C82 C84 1.3900 . ?
C84 H84 0.9300 . ?
C84 C86 1.3900 . ?
C86 H86 0.9300 . ?
C88 H88A 0.9604 . ?
C88 H88B 0.9615 . ?
C88 H88C 0.9605 . ?
C88 C394 1.480(7) . ?
C90 C154 1.34(6) . ?
C90 C210 1.39(6) . ?
C92 H92 0.9800 . ?
C92 C180 1.480(10) . ?
C92 C182 1.480(11) . ?
C94 H94A 0.9700 . ?
C94 H94B 0.9700 . ?
C94 C104 1.46(6) . ?
C96 H96A 0.9700 . ?
C96 H96B 0.9700 . ?
C96 C248 1.61(9) . ?
C98 H98A 0.9598 . ?
C98 H98B 0.9602 . ?
C98 H98C 0.9586 . ?
C98 C102 1.48(6) . ?
C100 H10A 0.9700 . ?
C100 H10B 0.9700 . ?
C100 C126 1.56(5) . ?
C100 C156 1.53(5) . ?
C102 H102 0.9800 . ?
C102 C370 1.48(6) . ?
C104 H10C 0.9700 . ?
C104 H10D 0.9700 . ?
C104 C122 1.59(6) . ?
C106 C108 1.3900 . ?
C106 C116 1.3900 . ?
C108 H108 0.9300 . ?
C108 C110 1.3900 . ?
C110 H110 0.9300 . ?
C110 C112 1.3900 . ?
C112 H112 0.9300 . ?
C112 C114 1.3900 . ?
C114 H114 0.9300 . ?
C114 C116 1.3900 . ?
C116 H116 0.9300 . ?
C118 H11A 0.9600 . ?
C118 H11B 0.9600 . ?
C118 H11C 0.9600 . ?
C118 C242 1.63(6) . ?
C120 H120 0.9300 . ?
C122 H12A 0.9700 . ?
C122 H12B 0.9700 . ?
C124 H124 0.9300 . ?
C124 C244 1.41(7) . ?
C124 C308 1.42(7) . ?
C126 H12C 0.9700 . ?
C126 H12D 0.9700 . ?
C128 C130 1.3900 . ?
C128 C138 1.3900 . ?
C130 H130 0.9300 . ?
C130 C132 1.3900 . ?
C132 H132 0.9300 . ?
C132 C134 1.3900 . ?
C134 H134 0.9300 . ?
C134 C136 1.3900 . ?
C136 H136 0.9300 . ?
C136 C138 1.3900 . ?
C138 H138 0.9300 . ?
C140 C142 1.3900 . ?
C140 C150 1.3900 . ?
C142 H142 0.9300 . ?
C142 C144 1.3900 . ?
C144 H144 0.9300 . ?
C144 C146 1.3900 . ?
C146 H146 0.9300 . ?
C146 C148 1.3900 . ?
C148 H148 0.9300 . ?
C148 C150 1.3900 . ?
C150 H150 0.9300 . ?
C152 H15A 0.9598 . ?
C152 H15B 0.9609 . ?
C152 H15C 0.9599 . ?
C154 H154 0.9300 . ?
C154 C418 1.44(6) . ?
C156 H15D 0.9700 . ?
C156 H15E 0.9700 . ?
C158 H15F 0.9601 . ?
C158 H15G 0.9603 . ?
C158 H15H 0.9599 . ?
C158 C226 1.479(10) . ?
C160 H16A 0.9609 . ?
C160 H16B 0.9602 . ?
C160 H16C 0.9603 . ?
C162 H162 0.9300 . ?
C164 H164 0.9300 . ?
C164 C166 1.41(6) . ?
C164 C168 1.43(6) . ?
C166 H166 0.9300 . ?
C166 C274 1.37(6) . ?
C168 H168 0.9300 . ?
C168 C178 1.43(6) . ?
C170 H170 0.9300 . ?
C170 C178 1.32(6) . ?
C170 C274 1.43(6) . ?
C172 H17A 0.9602 . ?
C172 H17B 0.9601 . ?
C172 H17C 0.9603 . ?
C172 C282 1.459(10) . ?
C174 H174 0.9300 . ?
C174 C392 1.36(7) . ?
C176 H17D 0.9601 . ?
C176 H17E 0.9596 . ?
C176 H17F 0.9605 . ?
C176 C394 1.480(7) . ?
C180 H18A 0.9600 . ?
C180 H18B 0.9600 . ?
C180 H18C 0.9600 . ?
C182 H18D 0.9607 . ?
C182 H18E 0.9597 . ?
C182 H18F 0.9596 . ?
C184 C186 1.3900 . ?
C184 C194 1.3900 . ?
C186 H186 0.9300 . ?
C186 C188 1.3900 . ?
C188 H188 0.9300 . ?
C188 C190 1.3900 . ?
C190 H190 0.9300 . ?
C190 C192 1.3900 . ?
C192 H192 0.9300 . ?
C192 C194 1.3900 . ?
C194 H194 0.9300 . ?
C196 H19A 0.9385 . ?
C196 H19B 0.9088 . ?
C196 H19C 1.0280 . ?
C198 C200 1.3900 . ?
C198 C208 1.3900 . ?
C200 H200 0.9300 . ?
C200 C202 1.3900 . ?
C202 H202 0.9300 . ?
C202 C204 1.3900 . ?
C204 H204 0.9300 . ?
C204 C206 1.3900 . ?
C206 H206 0.9300 . ?
C206 C208 1.3900 . ?
C208 H208 0.9300 . ?
C210 H210 0.9300 . ?
C210 C250 1.35(6) . ?
C212 C246 1.47(6) . ?
C212 C406 1.41(6) . ?
C214 H214 0.9300 . ?
C214 C216 1.3900 . ?
C214 C224 1.3900 . ?
C216 H216 0.9300 . ?
C216 C218 1.3900 . ?
C218 H218 0.9300 . ?
C218 C220 1.3900 . ?
C220 H220 0.9300 . ?
C220 C222 1.3900 . ?
C222 H222 0.9300 . ?
C222 C224 1.3900 . ?
C226 H226 0.9800 . ?
C226 C330 1.478(10) . ?
C228 C230 1.3900 . ?
C228 C238 1.3900 . ?
C230 H230 0.9300 . ?
C230 C232 1.3900 . ?
C232 H232 0.9300 . ?
C232 C234 1.3900 . ?
C234 H234 0.9300 . ?
C234 C236 1.3900 . ?
C236 H236 0.9300 . ?
C236 C238 1.3900 . ?
C238 H238 0.9300 . ?
C240 H240 0.9800 . ?
C240 C252 1.481(10) . ?
C240 C328 1.482(10) . ?
C242 H242 0.9800 . ?
C242 C268 1.55(6) . ?
C244 H244 0.9300 . ?
C246 H246 0.9300 . ?
C248 H24C 0.9700 . ?
C248 H24D 0.9700 . ?
C250 H250 0.9300 . ?
C250 C420 1.41(7) . ?
C252 H25A 0.9607 . ?
C252 H25B 0.9595 . ?
C252 H25C 0.9600 . ?
C254 H254 0.9300 . ?
C254 C326 1.52(7) . ?
C256 H256 0.9300 . ?
C256 C258 1.3900 . ?
C256 C266 1.3900 . ?
C258 H258 0.9300 . ?
C258 C260 1.3900 . ?
C260 H260 0.9300 . ?
C260 C262 1.3900 . ?
C262 H262 0.9300 . ?
C262 C264 1.3900 . ?
C264 H264 0.9300 . ?
C264 C266 1.3900 . ?
C268 H26A 0.9600 . ?
C268 H26B 0.9600 . ?
C268 H26C 0.9600 . ?
C270 H27A 0.9700 . ?
C270 H27B 0.9700 . ?
C270 C276 1.46(6) . ?
C272 H272 0.9800 . ?
C272 C350 1.481(10) . ?
C272 C354 1.480(10) . ?
C274 H274 0.9300 . ?
C276 H27C 0.9700 . ?
C276 H27D 0.9700 . ?
C278 H27E 0.9700 . ?
C278 H27F 0.9700 . ?
C278 C416 1.480(10) . ?
C280 H280 0.9300 . ?
C280 C324 1.45(6) . ?
C280 C422 1.43(6) . ?
C282 H282 0.9800 . ?
C282 C386 1.460(10) . ?
C284 H284 0.9300 . ?
C284 C286 1.3900 . ?
C284 C294 1.3900 . ?
C286 H286 0.9300 . ?
C286 C288 1.3900 . ?
C288 H288 0.9300 . ?
C288 C290 1.3900 . ?
C290 H290 0.9300 . ?
C290 C292 1.3900 . ?
C292 H292 0.9300 . ?
C292 C294 1.3900 . ?
C296 H296 0.9300 . ?
C296 C298 1.3900 . ?
C296 C306 1.3900 . ?
C298 H298 0.9300 . ?
C298 C300 1.3900 . ?
C300 H300 0.9300 . ?
C300 C302 1.3900 . ?
C302 C304 1.3900 . ?
C304 H304 0.9300 . ?
C304 C306 1.3900 . ?
C306 H306 0.9300 . ?
C308 H308 0.9300 . ?
C308 C326 1.54(7) . ?
C310 H310 0.9300 . ?
C310 C324 1.42(6) . ?
C312 C314 1.3900 . ?
C312 C322 1.3900 . ?
C314 H314 0.9300 . ?
C314 C316 1.3900 . ?
C316 H316 0.9300 . ?
C316 C318 1.3900 . ?
C318 H318 0.9300 . ?
C318 C320 1.3900 . ?
C320 H320 0.9300 . ?
C320 C322 1.3900 . ?
C322 H322 0.9300 . ?
C326 H32C 0.9700 . ?
C326 H32D 0.9700 . ?
C328 H32E 0.9603 . ?
C328 H32F 0.9604 . ?
C328 H32G 0.9586 . ?
C330 H33A 0.9597 . ?
C330 H33B 0.9599 . ?
C330 H33C 0.9598 . ?
C332 C334 1.3900 . ?
C332 C342 1.3900 . ?
C334 H334 0.9300 . ?
C334 C336 1.3900 . ?
C336 H336 0.9300 . ?
C336 C338 1.3900 . ?
C338 H338 0.9300 . ?
C338 C340 1.3900 . ?
C340 H340 0.9300 . ?
C340 C342 1.3900 . ?
C342 H342 0.9300 . ?
C344 H34D 0.9600 . ?
C344 H34E 0.9600 . ?
C344 H34F 0.9600 . ?
C346 H34G 0.9597 . ?
C346 H34H 0.9603 . ?
C346 H34I 0.9599 . ?
C348 H34J 0.9596 . ?
C348 H34K 0.9602 . ?
C348 H34L 0.9606 . ?
C350 H35A 0.9606 . ?
C350 H35B 0.9605 . ?
C350 H35C 0.9597 . ?
C352 H35D 0.9604 . ?
C352 H35E 0.9600 . ?
C352 H35F 0.9595 . ?
C354 H35G 0.9595 . ?
C354 H35H 0.9598 . ?
C354 H35I 0.9605 . ?
C356 H35J 0.9600 . ?
C356 H35K 0.9595 . ?
C356 H35L 0.9602 . ?
C358 H358 0.9300 . ?
C358 C360 1.3900 . ?
C358 C368 1.3900 . ?
C360 H360 0.9300 . ?
C360 C362 1.3900 . ?
C362 C364 1.3900 . ?
C364 H364 0.9300 . ?
C364 C366 1.3900 . ?
C366 H366 0.9300 . ?
C366 C368 1.3900 . ?
C368 H368 0.9300 . ?
C370 H37A 0.9598 . ?
C370 H37B 0.9603 . ?
C370 H37C 0.9602 . ?
C372 H372 0.9300 . ?
C372 C374 1.3900 . ?
C372 C382 1.3900 . ?
C374 H374 0.9300 . ?
C374 C376 1.3900 . ?
C376 H376 0.9300 . ?
C376 C378 1.3900 . ?
C378 H378 0.9300 . ?
C378 C380 1.3900 . ?
C380 H380 0.9300 . ?
C380 C382 1.3900 . ?
C384 H38A 0.9604 . ?
C384 H38B 0.9596 . ?
C384 H38C 0.9599 . ?
C384 C390 1.480(10) . ?
C386 H38D 0.9597 . ?
C386 H38E 0.9602 . ?
C386 H38F 0.9606 . ?
C388 H388 0.9300 . ?
C390 H390 0.9800 . ?
C392 H392 0.9300 . ?
C392 C406 1.39(6) . ?
C394 H394 0.9800 . ?
C396 H396 0.9800 . ?
C396 C402 1.482(10) . ?
C396 C408 1.482(10) . ?
C398 H398 0.9300 . ?
C398 C410 1.36(7) . ?
C400 H40A 0.9599 . ?
C400 H40B 0.9603 . ?
C400 H40C 0.9592 . ?
C402 H40D 0.9597 . ?
C402 H40E 0.9588 . ?
C402 H40F 0.9601 . ?
C404 H40G 0.9591 . ?
C404 H40H 0.9601 . ?
C404 H40I 0.9600 . ?
C406 H406 0.9300 . ?
C408 H40J 0.9599 . ?
C408 H40K 0.9602 . ?
C408 H2 0.9599 . ?
C410 H410 0.9300 . ?
C410 C424 1.32(7) . ?
C412 H41A 0.9606 . ?
C412 H41B 0.9589 . ?
C412 H41C 0.9596 . ?
C414 H414 0.9300 . ?
C414 C422 1.38(6) . ?
C416 H41D 0.9700 . ?
C416 H41E 0.9700 . ?
C418 H418 0.9300 . ?
C418 C420 1.31(7) . ?
C420 H420 0.9300 . ?
C422 H422 0.9300 . ?
C426 H42A 0.9595 . ?
C426 H42B 0.9597 . ?
C426 H42C 0.9601 . ?
W16 O44 1.74(2) . ?
W16 O55 2.08(2) . ?
W16 O59 1.89(2) . ?
W16 O61 1.94(2) . ?
W16 O80 2.338(19) . ?
W16 O99 1.77(2) . ?
W17 O51 2.15(2) . ?
W17 O73 1.91(2) . ?
W17 O83 1.73(2) . ?
W17 O91 1.71(2) . ?
W17 O97 1.92(2) . ?
W17 O101 2.25(2) . ?
W18 O47 1.75(2) . ?
W18 O57 1.85(2) . ?
W18 O73 1.94(2) . ?
W18 O79 1.730(19) . ?
W18 O87 2.16(2) . ?
W18 O101 2.233(19) . ?
W22 O53 2.08(2) . ?
W22 O57 1.92(2) . ?
W22 O61 1.89(2) . ?
W22 O77 1.78(2) . ?
W22 O80 2.280(19) . ?
W22 O93 1.78(2) . ?
W23 O49 1.90(2) . ?
W23 O51 1.87(2) . ?
W23 O63 1.72(2) . ?
W23 O67 2.37(2) . ?
W23 O71 1.90(2) . ?
W23 O87 2.04(2) . ?
W25 Ag53 3.252(10) . ?
W25 O59 1.86(2) . ?
W25 O81 2.17(2) . ?
W25 O85 1.75(2) . ?
W25 O86 2.28(2) . ?
W25 O95 2.00(2) . ?
W25 O103 1.77(2) . ?
W27 O86 2.22(2) . ?
W27 O89 1.75(2) . ?
W27 O95 1.90(2) . ?
W27 O97 1.83(2) . ?
W27 O106 2.20(2) . ?
W27 O110 1.74(2) . ?
W29 O49 1.97(2) . ?
W29 O65 1.88(2) . ?
W29 O67 2.334(19) . ?
W29 O69 1.77(2) . ?
W29 O81 1.76(2) . ?
W29 O106 2.04(2) . ?
W30 O53 1.93(2) . ?
W30 O55 1.81(2) . ?
W30 O65 1.96(2) . ?
W30 O67 2.379(19) . ?
W30 O71 1.96(2) . ?
W30 O75 1.74(2) . ?
Ag1 Ag3 2.953(9) . ?
Ag1 Ag5 2.942(6) . ?
Ag1 Ag8 2.754(4) . ?
Ag1 Ag13 3.058(11) . ?
Ag1 Ag21 2.806(6) . ?
Ag1 Ag25 2.983(11) . ?
Ag1 Ag39 3.044(6) . ?
Ag1 Ag49 2.859(10) . ?
Ag1 Ag53 2.847(10) . ?
Ag1 Ag56 2.730(4) . ?
Ag1 Ag58 2.808(5) . ?
Ag1 Cl1 2.406(13) . ?
Ag1B S24A 2.51(2) . ?
Ag1B P11 2.25(3) . ?
Ag1B O83 2.41(2) . ?
Ag3 Ag8 2.775(9) . ?
Ag3 Ag56 3.300(10) . ?
Ag3 S3 2.41(3) . ?
Ag3 S23 2.57(4) . ?
Ag5 Ag22 3.161(7) . ?
Ag5 Ag56 3.032(7) . ?
Ag5 S9 2.38(2) . ?
Ag5 S17 2.35(2) . ?
Ag8 Ag21 2.891(7) . ?
Ag8 Ag23 3.004(8) . ?
Ag8 Ag51 3.013(9) . ?
Ag8 Ag53 2.956(12) . ?
Ag8 Ag56 2.757(5) . ?
Ag8 Ag58 2.683(6) . ?
Ag8 O79 2.47(2) . ?
Ag8 O83 2.42(2) . ?
Ag11 S24 2.61(2) . ?
Ag11 P3 2.253(17) . ?
Ag11 O79 2.55(2) . ?
Ag13 Ag22 3.310(13) . ?
Ag13 Ag56 3.035(11) . ?
Ag13 S3 2.39(3) . ?
Ag13 S25 2.40(3) . ?
Ag14 S1 2.499(11) . ?
Ag14 P4 2.401(10) . ?
Ag14 O93 2.35(2) . ?
Ag16 S4 2.472(11) . ?
Ag16 P8 2.381(11) . ?
Ag16 O47 2.33(2) . ?
Ag19 Ag42 3.108(8) . ?
Ag19 S9 2.35(2) . ?
Ag19 S19 2.36(2) . ?
Ag21 S19 2.41(2) . ?
Ag21 S21 2.317(10) . ?
Ag22 S16 2.522(12) . ?
Ag22 S17 2.66(2) . ?
Ag22 S25 2.62(3) . ?
Ag22 P10 2.396(10) . ?
Ag22 O99 2.41(2) . ?
Ag23 S5 2.33(2) . ?
Ag23 S21 2.314(10) . ?
Ag25 S11 2.49(4) . ?
Ag25 S13 2.36(4) . ?
Ag26 S1 2.446(11) . ?
Ag26 P23 2.383(11) . ?
Ag28 Ag41 3.270(9) . ?
Ag28 S4 2.386(10) . ?
Ag28 S24 2.50(2) . ?
Ag28 S24A 2.29(2) . ?
Ag31 Ag39 3.330(8) . ?
Ag31 S3 2.76(3) . ?
Ag31 S16 2.467(15) . ?
Ag31 P15 2.44(2) . ?
Ag31 O77 2.46(2) . ?
Ag32 S1 2.369(11) . ?
Ag32 S16 2.386(14) . ?
Ag32 O61 2.53(2) . ?
Ag39 Ag56 2.666(7) . ?
Ag39 S5 2.36(2) . ?
Ag39 S17 2.56(2) . ?
Ag39 O77 2.52(2) . ?
Ag40 S6 2.430(12) . ?
Ag40 P6 2.367(12) . ?
Ag41 S24 2.46(2) . ?
Ag41 P11 2.55(3) . ?
Ag41 O83 2.49(2) . ?
Ag42 S9 2.96(2) . ?
Ag42 S11 2.69(4) . ?
Ag42 S20 2.529(13) . ?
Ag42 P1 2.400(11) . ?
Ag42 O103 2.44(2) . ?
Ag43 S20 2.769(17) . ?
Ag43 P19 2.39(2) . ?
Ag43 O110 2.44(2) . ?
Ag47 S4 2.451(10) . ?
Ag47 P14 2.385(10) . ?
Ag48 Ag60 3.063(11) . ?
Ag48 S6 2.352(12) . ?
Ag48 S20 2.356(13) . ?
Ag48 O95 2.48(2) . ?
Ag49 S11 2.42(4) . ?
Ag49 S25 2.42(3) . ?
Ag49 H39A 1.9230 . ?
Ag51 S13 2.27(4) . ?
Ag51 S23 2.48(4) . ?
Ag52 S6 2.479(12) . ?
Ag52 P2 2.398(13) . ?
Ag52 O89 2.60(2) . ?
Ag53 Ag56 2.271(13) . ?
Ag53 O86 2.54(2) . ?
Ag53 O103 2.10(2) . ?
Ag56 Ag58 2.814(7) . ?
Ag56 O77 2.54(2) . ?
Ag56 O80 2.45(2) . ?
Ag56 O99 2.38(2) . ?
Ag58 O103 2.49(2) . ?
Ag58 O110 2.39(2) . ?
Ag60 S20 2.223(15) . ?
Ag60 P19 2.43(2) . ?
Ag60 O110 2.53(2) . ?
Ag62 S24A 2.54(2) . ?
Ag62 P3 2.786(18) . ?
Ag62 O79 2.57(2) . ?
S1 C333 1.88(4) . ?
S3 C191 1.900(10) . ?
S4 C129 1.85(4) . ?
S5 C125 1.903(10) . ?
S6 C411 1.90(4) . ?
S9 C99 1.900(10) . ?
S11 C201 1.899(10) . ?
S13 C251 1.900(10) . ?
S16 C255 1.80(4) . ?
S17 C379 1.901(10) . ?
S19 C43 1.899(10) . ?
S20 C131 1.92(5) . ?
S21 C13 1.901(10) . ?
S23 C101 1.900(10) . ?
S24 C219 1.801(10) . ?
S24A C55 1.799(10) . ?
S25 C155 1.900(10) . ?
P1 C215 1.81(4) . ?
P1 C285 1.80(2) . ?
P1 C305 1.80(4) . ?
P2 C69 1.83(5) . ?
P2 C79 1.87(4) . ?
P2 C365 1.80(3) . ?
P3 C141 1.85(5) . ?
P3 C85 1.87(6) . ?
P3 C371 1.75(3) . ?
P4 C217 1.82(4) . ?
P4 C109 1.88(4) . ?
P4 C325 1.83(2) . ?
P6 C223 1.79(3) . ?
P6 C307 1.81(4) . ?
P6 C175 1.87(3) . ?
P8 C237 1.81(4) . ?
P8 C315 1.86(4) . ?
P8 C179 1.85(2) . ?
P10 C15 1.81(4) . ?
P10 C75 1.84(4) . ?
P10 C323 1.84(2) . ?
P11 C73 1.67(5) . ?
P11 C207 1.92(9) . ?
P11 C423 1.604(10) . ?
P14 C231 1.82(2) . ?
P14 C241 1.84(4) . ?
P14 C283 1.80(4) . ?
P15 C121 1.79(4) . ?
P15 C271 1.699(10) . ?
P15 C173 2.10(6) . ?
P19 C263 1.71(4) . ?
P19 C331 1.74(8) . ?
P19 C193 1.95(5) . ?
P23 C253 1.83(4) . ?
P23 C2 1.83(5) . ?
P23 C83 1.88(5) . ?
Si3 O67 1.61(2) . ?
Si3 O80 1.62(2) . ?
Si3 O86 1.66(2) . ?
Si3 O101 1.66(2) . ?
C213 H21A 0.9700 . ?
C213 H21B 0.9700 . ?
C213 C109 1.55(5) . ?
C213 C315 1.55(5) . ?
C107 H10E 0.9603 . ?
C107 H10F 0.9610 . ?
C107 H10G 0.9594 . ?
C107 C55 1.498(10) . ?
C215 H21C 0.9700 . ?
C215 H21D 0.9700 . ?
C215 C259 1.54(5) . ?
C27 H27 0.9300 . ?
C27 C217 1.46(5) . ?
C27 C281 1.38(5) . ?
C217 C221 1.39(5) . ?
C109 H10H 0.9700 . ?
C109 H10I 0.9700 . ?
C219 H219 0.9800 . ?
C219 C19 1.481(10) . ?
C219 C381 1.479(10) . ?
C55 H55 0.9800 . ?
C55 C419 1.79(11) . ?
C221 H221 0.9300 . ?
C221 C31 1.35(5) . ?
C111 H111 0.9300 . ?
C111 C83 1.32(7) . ?
C111 C199 1.31(7) . ?
C223 C7 1.3900 . ?
C223 C57 1.3900 . ?
C7 H7 0.9300 . ?
C7 C225 1.3900 . ?
C225 H225 0.9300 . ?
C225 C113 1.3900 . ?
C113 H113 0.9300 . ?
C113 C227 1.3900 . ?
C227 H227 0.9300 . ?
C227 C57 1.3900 . ?
C57 H57 0.9300 . ?
C229 H229 0.9300 . ?
C229 C249 1.53(8) . ?
C229 C149 1.31(8) . ?
C115 H11D 0.9600 . ?
C115 H11E 0.9601 . ?
C115 H11F 0.9602 . ?
C115 C201 1.480(10) . ?
C231 C29 1.3900 . ?
C231 C59 1.3900 . ?
C29 H29 0.9300 . ?
C29 C233 1.3900 . ?
C233 H233 0.9300 . ?
C233 C117 1.3900 . ?
C117 H117 0.9300 . ?
C117 C235 1.3900 . ?
C235 H235 0.9300 . ?
C235 C59 1.3900 . ?
C59 H59 0.9300 . ?
C237 C279 1.36(6) . ?
C237 C417 1.42(6) . ?
C119 H119 0.9300 . ?
C119 C153 1.47(6) . ?
C119 C3 1.33(6) . ?
C239 H23A 0.9606 . ?
C239 H23B 0.9606 . ?
C239 H23C 0.9598 . ?
C239 C13 1.481(10) . ?
C15 H15I 0.9700 . ?
C15 H15J 0.9700 . ?
C15 C259 1.59(5) . ?
C241 C35 1.32(6) . ?
C241 C317 1.37(6) . ?
C121 C243 1.3900 . ?
C121 C247 1.3900 . ?
C243 H243 0.9300 . ?
C243 C61 1.3900 . ?
C61 H61 0.9300 . ?
C61 C245 1.3900 . ?
C245 H245 0.9300 . ?
C245 C123 1.3900 . ?
C123 H123 0.9300 . ?
C123 C247 1.3900 . ?
C247 H247 0.9300 . ?
C31 H31 0.9300 . ?
C31 C257 1.50(6) . ?
C249 H249 0.9300 . ?
C249 C335 1.35(8) . ?
C125 H125 0.9800 . ?
C125 C95 1.480(10) . ?
C125 C209 1.481(10) . ?
C251 H251 0.9800 . ?
C251 C127 1.479(10) . ?
C251 C405 1.480(10) . ?
C63 H63A 0.9601 . ?
C63 H63B 0.9599 . ?
C63 H63C 0.9610 . ?
C63 C43 1.481(10) . ?
C253 H25D 0.9700 . ?
C253 H25E 0.9700 . ?
C253 C309 1.48(6) . ?
C127 H12E 0.9602 . ?
C127 H12F 0.9598 . ?
C127 H12G 0.9600 . ?
C255 H255 0.9800 . ?
C255 C313 1.461(10) . ?
C255 C205 1.460(10) . ?
C2 C65 1.42(6) . ?
C2 C169 1.36(6) . ?
C257 H257 0.9300 . ?
C257 C281 1.31(6) . ?
C129 H129 0.9800 . ?
C129 C357 1.45(5) . ?
C129 C203 1.41(4) . ?
C259 H25F 0.9700 . ?
C259 H25G 0.9700 . ?
C65 H65 0.9300 . ?
C65 C167 1.33(7) . ?
C261 H261 0.9300 . ?
C261 C199 1.27(7) . ?
C261 C401 1.33(7) . ?
C131 H131 0.9800 . ?
C131 C91 1.47(6) . ?
C131 C49 1.43(7) . ?
C263 C33 1.3900 . ?
C263 C67 1.3900 . ?
C33 H33 0.9300 . ?
C33 C265 1.3900 . ?
C265 H265 0.9300 . ?
C265 C133 1.3900 . ?
C133 H133 0.9300 . ?
C133 C267 1.3900 . ?
C267 H267 0.9300 . ?
C267 C67 1.3900 . ?
C67 H67 0.9300 . ?
C269 H269 0.9300 . ?
C269 C291 1.37(7) . ?
C269 C403 1.30(7) . ?
C135 H135 0.9300 . ?
C135 C271 1.3900 . ?
C135 C275 1.3900 . ?
C271 C17 1.3900 . ?
C17 H17 0.9300 . ?
C17 C273 1.3900 . ?
C273 H273 0.9300 . ?
C273 C137 1.3900 . ?
C137 H137 0.9300 . ?
C137 C275 1.3900 . ?
C69 C335 1.41(7) . ?
C69 C21 1.36(7) . ?
C277 H27G 0.9700 . ?
C277 H27H 0.9700 . ?
C277 C283 1.50(5) . ?
C277 C79 1.50(5) . ?
C139 H139 0.9300 . ?
C139 C141 1.24(6) . ?
C139 C89 1.38(6) . ?
C279 H279 0.9300 . ?
C279 C415 1.43(6) . ?
C35 H35 0.9300 . ?
C35 C403 1.34(6) . ?
C281 H281 0.9300 . ?
C141 C343 1.54(6) . ?
C283 H28A 0.9700 . ?
C283 H28B 0.9700 . ?
C71 H71 0.9300 . ?
C71 C301 1.33(6) . ?
C71 C417 1.48(6) . ?
C285 C143 1.3900 . ?
C285 C145 1.3900 . ?
C143 H143 0.9300 . ?
C143 C287 1.3900 . ?
C287 H287 0.9300 . ?
C287 C9 1.3900 . ?
C9 H9 0.9300 . ?
C9 C289 1.3900 . ?
C289 H289 0.9300 . ?
C289 C145 1.3900 . ?
C145 H145 0.9300 . ?
C291 H291 0.9300 . ?
C291 C317 1.43(7) . ?
C73 C293 1.3900 . ?
C73 C297 1.3900 . ?
C293 H293 0.9300 . ?
C293 C147 1.3900 . ?
C147 H147 0.9300 . ?
C147 C295 1.3900 . ?
C295 H295 0.9300 . ?
C295 C37 1.3900 . ?
C37 H37 0.9300 . ?
C37 C297 1.3900 . ?
C297 H297 0.9300 . ?
C149 H149 0.9300 . ?
C149 C21 1.34(7) . ?
C299 H29A 0.9599 . ?
C299 H29B 0.9605 . ?
C299 H29C 0.9598 . ?
C299 C379 1.481(10) . ?
C75 C345 1.37(6) . ?
C75 C349 1.39(6) . ?
C301 H301 0.9300 . ?
C301 C415 1.19(6) . ?
C151 H15K 0.9594 . ?
C151 H15L 0.9601 . ?
C151 H15M 0.9596 . ?
C151 C43 1.481(10) . ?
C303 H30C 0.9571 . ?
C303 H30D 0.9608 . ?
C303 H30E 0.9602 . ?
C303 C191 1.481(10) . ?
C19 H19D 0.9601 . ?
C19 H19E 0.9605 . ?
C19 H19F 0.9592 . ?
C305 C153 1.48(6) . ?
C305 C383 1.40(6) . ?
C153 H153 0.9300 . ?
C307 H30F 0.9700 . ?
C307 H30G 0.9700 . ?
C307 C309 1.66(6) . ?
C77 H77A 0.9597 . ?
C77 H77B 0.9606 . ?
C77 H77C 0.9590 . ?
C77 C99 1.480(10) . ?
C309 H30H 0.9700 . ?
C309 H30I 0.9700 . ?
C155 H155 0.9800 . ?
C155 C51 1.480(10) . ?
C155 C409 1.480(10) . ?
C311 H31A 0.9597 . ?
C311 H31B 0.9592 . ?
C311 H31C 0.9599 . ?
C311 C101 1.480(10) . ?
C39 H39A 0.9589 . ?
C39 H39B 0.9599 . ?
C39 H39C 0.9602 . ?
C39 C201 1.480(10) . ?
C313 H31D 0.9605 . ?
C313 H31E 0.9611 . ?
C313 H31F 0.9598 . ?
C157 H15N 0.9596 . ?
C157 H15O 0.9604 . ?
C157 H15P 0.9613 . ?
C157 C13 1.481(10) . ?
C315 H31G 0.9700 . ?
C315 H31H 0.9700 . ?
C79 H79A 0.9700 . ?
C79 H79B 0.9700 . ?
C317 H317 0.9300 . ?
C159 H159 0.9300 . ?
C159 C319 1.3900 . ?
C159 C323 1.3900 . ?
C319 H319 0.9300 . ?
C319 C5 1.3900 . ?
C5 H5 0.9300 . ?
C5 C321 1.3900 . ?
C321 H321 0.9300 . ?
C321 C161 1.3900 . ?
C161 H161 0.9300 . ?
C161 C323 1.3900 . ?
C81 H81 0.9300 . ?
C81 C345 1.41(6) . ?
C81 C87 1.43(6) . ?
C325 C163 1.3900 . ?
C325 C165 1.3900 . ?
C163 H163 0.9300 . ?
C163 C327 1.3900 . ?
C327 H327 0.9300 . ?
C327 C41 1.3900 . ?
C41 H41 0.9300 . ?
C41 C329 1.3900 . ?
C329 H329 0.9300 . ?
C329 C165 1.3900 . ?
C165 H165 0.9300 . ?
C331 H33D 0.9700 . ?
C331 H33E 0.9700 . ?
C331 C171 1.62(10) . ?
C83 C25 1.31(7) . ?
C333 H333 0.9800 . ?
C333 C395 1.53(6) . ?
C333 C397 1.38(6) . ?
C167 H167 0.9300 . ?
C167 C393 1.48(7) . ?
C335 H335 0.9300 . ?
C21 H21 0.9300 . ?
C337 H337 0.9300 . ?
C337 C169 1.38(6) . ?
C337 C393 1.28(7) . ?
C169 H169 0.9300 . ?
C339 H339 0.9300 . ?
C339 C341 1.43(6) . ?
C339 C343 1.38(6) . ?
C85 H85A 0.9700 . ?
C85 H85B 0.9700 . ?
C85 C399 1.463(10) . ?
C341 H341 0.9300 . ?
C341 C89 1.43(6) . ?
C171 H17G 0.9700 . ?
C171 H17H 0.9700 . ?
C171 C207 1.43(10) . ?
C343 H343 0.9300 . ?
C43 H43 0.9800 . ?
C345 H345 0.9300 . ?
C173 H17I 0.9700 . ?
C173 H17J 0.9700 . ?
C173 C399 1.457(10) . ?
C347 H347 0.9300 . ?
C347 C87 1.44(6) . ?
C347 C349 1.43(6) . ?
C87 H87 0.9300 . ?
C349 H349 0.9300 . ?
C175 C351 1.3900 . ?
C175 C355 1.3900 . ?
C351 H351 0.9300 . ?
C351 C11 1.3900 . ?
C11 H11 0.9300 . ?
C11 C353 1.3900 . ?
C353 H353 0.9300 . ?
C353 C177 1.3900 . ?
C177 H177 0.9300 . ?
C177 C355 1.3900 . ?
C355 H355 0.9300 . ?
C89 H89 0.9300 . ?
C357 H35M 0.9838 . ?
C357 H35N 0.9683 . ?
C357 H35O 0.9272 . ?
C179 C359 1.3900 . ?
C179 C363 1.3900 . ?
C359 H359 0.9300 . ?
C359 C45 1.3900 . ?
C45 H45 0.9300 . ?
C45 C361 1.3900 . ?
C361 H361 0.9300 . ?
C361 C181 1.3900 . ?
C181 H181 0.9300 . ?
C181 C363 1.3900 . ?
C363 H363 0.9300 . ?
C91 H91A 0.9602 . ?
C91 H91B 0.9600 . ?
C91 H91C 0.9598 . ?
C365 C183 1.3900 . ?
C365 C185 1.3900 . ?
C183 H183 0.9300 . ?
C183 C367 1.3900 . ?
C367 H367 0.9300 . ?
C367 C23 1.3900 . ?
C23 H23 0.9300 . ?
C23 C369 1.3900 . ?
C369 H369 0.9300 . ?
C369 C185 1.3900 . ?
C185 H185 0.9300 . ?
C371 C93 1.3900 . ?
C371 C47 1.3900 . ?
C93 H93 0.9300 . ?
C93 C373 1.3900 . ?
C373 H373 0.9300 . ?
C373 C187 1.3900 . ?
C187 H187 0.9300 . ?
C187 C375 1.3900 . ?
C375 H375 0.9300 . ?
C375 C47 1.3900 . ?
C47 H47 0.9300 . ?
C377 H37D 0.9602 . ?
C377 H37E 0.9593 . ?
C377 H37F 0.9608 . ?
C377 C379 1.483(10) . ?
C189 H18G 0.9604 . ?
C189 H18H 0.9600 . ?
C189 H18I 0.9609 . ?
C189 C191 1.480(10) . ?
C379 H379 0.9800 . ?
C95 H95A 0.9595 . ?
C95 H95B 0.9600 . ?
C95 H95C 0.9590 . ?
C381 H38G 0.9600 . ?
C381 H38H 0.9596 . ?
C381 H38I 0.9601 . ?
C191 H191 0.9800 . ?
C383 H383 0.9300 . ?
C383 C385 1.36(6) . ?
C3 H3 0.9300 . ?
C3 C385 1.35(6) . ?
C385 H385 0.9300 . ?
C193 C387 1.3900 . ?
C193 C391 1.3900 . ?
C387 H387 0.9300 . ?
C387 C97 1.3900 . ?
C97 H97 0.9300 . ?
C97 C389 1.3900 . ?
C389 H389 0.9300 . ?
C389 C195 1.3900 . ?
C195 H195 0.9300 . ?
C195 C391 1.3900 . ?
C391 H391 0.9300 . ?
C49 H49A 0.9600 . ?
C49 H49B 0.9600 . ?
C49 H49C 0.9600 . ?
C393 H393 0.9300 . ?
C197 H19G 0.9607 . ?
C197 H19H 0.9604 . ?
C197 H19I 0.9595 . ?
C197 C99 1.480(10) . ?
C395 H39D 0.9590 . ?
C395 H39E 0.9599 . ?
C395 H39F 0.9603 . ?
C99 H99 0.9800 . ?
C397 H39G 0.9595 . ?
C397 H39H 0.9603 . ?
C397 H39I 0.9603 . ?
C199 H199 0.9300 . ?
C399 H39J 0.9700 . ?
C399 H39K 0.9700 . ?
C25 H25 0.9300 . ?
C25 C401 1.43(7) . ?
C401 H401 0.9300 . ?
C201 H201 0.9800 . ?
C403 H403 0.9300 . ?
C101 H101 0.9800 . ?
C101 C407 1.479(10) . ?
C405 H40L 0.9600 . ?
C405 H40M 0.9599 . ?
C405 H40N 0.9596 . ?
C203 H20A 0.9601 . ?
C203 H20B 0.9597 . ?
C203 H20C 0.9602 . ?
C407 H40O 0.9617 . ?
C407 H40P 0.9594 . ?
C407 H40Q 0.9597 . ?
C51 H51A 0.9606 . ?
C51 H51B 0.9597 . ?
C51 H51C 0.9602 . ?
C409 H40R 0.9603 . ?
C409 H40S 0.9603 . ?
C409 H40T 0.9603 . ?
C205 H20D 0.9408 . ?
C205 H20E 0.9861 . ?
C205 H20F 0.9522 . ?
C411 H411 0.9800 . ?
C411 C103 1.464(10) . ?
C411 C413 1.461(10) . ?
C103 H10J 0.9600 . ?
C103 H10K 0.9601 . ?
C103 H10L 0.9599 . ?
C413 H41F 0.9602 . ?
C413 H41G 0.9598 . ?
C413 H41H 0.9599 . ?
C207 H20G 0.9700 . ?
C207 H20H 0.9700 . ?
C415 H415 0.9300 . ?
C13 H13 0.9800 . ?
C417 H417 0.9300 . ?
C209 H20I 0.9604 . ?
C209 H20J 0.9601 . ?
C209 H20K 0.9608 . ?
C419 H41I 0.9603 . ?
C419 H41J 0.9597 . ?
C419 H41K 0.9602 . ?
Si1 O19 1.506(10) 2_486 ?
Si1 O19 1.506(10) . ?
Si1 O20 1.509(10) 2_486 ?
Si1 O20 1.509(10) . ?
Si1 O21 1.504(10) 2_486 ?
Si1 O21 1.504(10) . ?
Si1 O22 1.497(10) . ?
Si1 O22 1.497(10) 2_486 ?
O19 O20 1.69(3) 2_486 ?
O19 O22 1.66(3) 2_486 ?
O20 O21 1.69(3) 2_486 ?
O21 O22 1.66(3) 2_486 ?
Si2 O40 1.526(9) 2_577 ?
Si2 O40 1.526(9) . ?
Si2 O41 1.522(9) 2_577 ?
Si2 O41 1.522(9) . ?
Si2 O42 1.530(9) 2_577 ?
Si2 O42 1.529(9) . ?
Si2 O43 1.528(9) . ?
Si2 O43 1.527(9) 2_577 ?
O40 O41 1.75(2) 2_577 ?
O40 O42 1.77(2) 2_577 ?
O40 O43 1.77(2) 2_577 ?
O41 O42 1.76(2) 2_577 ?
O41 O43 1.75(2) 2_577 ?
O42 O43 1.77(2) 2_577 ?
C105 H105 0.9300 . ?
C105 C421 1.3900 . ?
C105 C425 1.3900 . ?
C421 H421 0.9300 . ?
C421 C211 1.3900 . ?
C211 H211 0.9300 . ?
C211 C423 1.3900 . ?
C423 C53 1.3900 . ?
C53 H53 0.9300 . ?
C53 C425 1.3900 . ?
C425 H425 0.9300 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O2 W1 O1 85.8(14) . . ?
O3 W1 O1 159.3(10) . . ?
O3 W1 O2 90.5(6) . . ?
O3 W1 O4 91.0(6) . . ?
O3 W1 O14 100.5(6) . . ?
O4 W1 O1 85.4(15) . . ?
O4 W1 O2 158.9(12) . . ?
O4 W1 O14 96.3(19) . . ?
O14 W1 O1 100.1(6) . . ?
O14 W1 O2 104.1(19) . . ?
O7 W2 O2 86.0(14) . . ?
O8 W2 O2 84.2(17) . . ?
O8 W2 O7 153.8(15) . . ?
O8 W2 O9 94.2(16) . . ?
O8 W2 O16 102.8(8) . . ?
O9 W2 O2 160.3(12) . . ?
O9 W2 O7 87.0(19) . . ?
O9 W2 O16 102.1(19) . . ?
O16 W2 O2 97.4(17) . . ?
O16 W2 O7 102.5(8) . . ?
O6 W3 O1 101(2) . . ?
O6 W3 O7 155.4(18) . . ?
O7 W3 O1 90.3(6) . . ?
O11 W3 O1 161.0(11) . . ?
O11 W3 O6 75(2) . . ?
O11 W3 O7 87(2) . . ?
O15 W3 O1 97.0(19) . . ?
O15 W3 O6 100.1(7) . . ?
O15 W3 O7 100.0(7) . . ?
O15 W3 O11 102.0(19) . . ?
O4 W4 O9 157.5(12) 2_486 . ?
O4 W4 O10 90.9(14) 2_486 . ?
O5 W4 O4 83.3(19) 2_486 2_486 ?
O5 W4 O9 90.4(19) 2_486 . ?
O5 W4 O10 155.2(16) 2_486 . ?
O5 W4 O17 99.8(19) 2_486 . ?
O9 W4 O10 85.8(19) . . ?
O17 W4 O4 97.5(16) . 2_486 ?
O17 W4 O9 104.8(14) . . ?
O17 W4 O10 104.9(14) . . ?
O3 W5 O10 90.4(5) 2_486 . ?
O3 W5 O12 90.6(6) 2_486 . ?
O3 W5 O18 103.3(16) 2_486 . ?
O11 W5 O3 158.9(10) . 2_486 ?
O11 W5 O10 87.9(19) . . ?
O11 W5 O12 84.1(17) . . ?
O11 W5 O18 97.6(15) . . ?
O12 W5 O10 160.2(11) . . ?
O18 W5 O10 101.6(16) . . ?
O18 W5 O12 97.4(15) . . ?
O6 W6 O5 97(2) . . ?
O8 W6 O5 95.5(19) 2_486 . ?
O8 W6 O6 150(2) 2_486 . ?
O8 W6 O12 86.2(16) 2_486 . ?
O12 W6 O5 156.5(17) . . ?
O12 W6 O6 72(2) . . ?
O13 W6 O5 101.1(9) . . ?
O13 W6 O6 100.8(19) . . ?
O13 W6 O8 104(2) . 2_486 ?
O13 W6 O12 101.3(9) . . ?
W3 O1 W1 134.6(10) . . ?
W2 O2 W1 136.7(12) . . ?
W1 O3 W5 137.0(10) . 2_486 ?
W1 O4 W4 137.2(11) . 2_486 ?
W4 O5 W6 139(3) 2_486 . ?
W3 O6 W6 136.9(12) . . ?
W2 O7 W3 137.0(10) . . ?
W2 O8 W6 136.8(11) . 2_486 ?
W2 O9 W4 136.8(11) . . ?
W4 O10 W5 136.9(10) . . ?
W3 O11 W5 136.0(11) . . ?
W6 O12 W5 136.2(11) . . ?
C275 O14 W1 133(10) 1_565 . ?
O2A W1A O1A 83.8(17) . . ?
O2A W1A O4A 163.0(8) . . ?
O3A W1A O1A 157.3(14) . . ?
O3A W1A O2A 105(2) . . ?
O3A W1A O4A 75(2) . . ?
O4A W1A O1A 90.3(6) . . ?
O13A W1A O1A 99.4(6) . . ?
O13A W1A O2A 98.4(6) . . ?
O13A W1A O3A 99.7(6) . . ?
O13A W1A O4A 98.3(6) . . ?
O8A W2A O1A 88.0(17) . . ?
O8A W2A O9A 86.1(17) . . ?
O8A W2A O10A 156.9(11) . . ?
O9A W2A O1A 165.0(17) . . ?
O9A W2A O10A 90.2(6) . . ?
O10A W2A O1A 89.9(5) . . ?
O17A W2A O1A 97.2(9) . . ?
O17A W2A O8A 101.7(6) . . ?
O17A W2A O9A 97.4(9) . . ?
O17A W2A O10A 101.4(6) . . ?
O2A W3A O10A 86.6(17) . . ?
O2A W3A O12A 90(2) . . ?
O11A W3A O2A 158.1(13) . . ?
O11A W3A O10A 86.1(18) . . ?
O11A W3A O12A 89.1(19) . . ?
O12A W3A O10A 158.8(11) . . ?
O18A W3A O2A 100.8(7) . . ?
O18A W3A O10A 100.6(6) . . ?
O18A W3A O11A 100.8(7) . . ?
O18A W3A O12A 100.5(6) . . ?
O5A W4A O7A 160(2) 2_486 . ?
O5A W4A O8A 88(2) 2_486 . ?
O5A W4A O16A 95(2) 2_486 . ?
O8A W4A O7A 81(2) . . ?
O12A W4A O7A 90.5(19) 2_486 . ?
O12A W4A O8A 158.0(12) 2_486 . ?
O12A W4A O16A 98.5(15) 2_486 . ?
O16A W4A O7A 103.0(15) . . ?
O16A W4A O8A 103.0(15) . . ?
O6A W5A O4A 84.3(17) . . ?
O7A W5A O4A 93.0(17) . . ?
O7A W5A O6A 157.8(13) . . ?
O11A W5A O4A 157.3(15) 2_486 . ?
O11A W5A O6A 83(2) 2_486 . ?
O11A W5A O7A 91.9(17) 2_486 . ?
O11A W5A O14A 107(2) 2_486 . ?
O14A W5A O4A 93.6(18) . . ?
O14A W5A O6A 101.0(7) . . ?
O14A W5A O7A 101.1(7) . . ?
O3A W6A O5A 99(2) . . ?
O3A W6A O6A 78(2) . . ?
O6A W6A O5A 159.5(17) . . ?
O9A W6A O5A 80.5(18) 2_486 . ?
O15A W6A O3A 104.7(19) . . ?
O15A W6A O5A 97.9(13) . . ?
O15A W6A O6A 102.4(13) . . ?
W1A O1A W2A 137.2(10) . . ?
W3A O2A W1A 136.9(11) . . ?
W1A O3A W6A 137.0(12) . . ?
W1A O4A W5A 135.0(11) . . ?
W4A O5A W6A 135(3) 2_486 . ?
W6A O6A W5A 136.8(11) . . ?
W4A O7A W5A 136.4(11) . . ?
W2A O8A W4A 137.2(11) . . ?
W3A O10A W2A 136.1(8) . . ?
W5A O11A W3A 138.5(12) 2_486 . ?
W4A O12A W3A 136.7(11) 2_486 . ?
O23 W7 O31 156.4(8) . . ?
O23 W7 O34 84(3) . . ?
O25 W7 O23 93(2) . . ?
O25 W7 O31 75.0(9) . . ?
O25 W7 O34 146.1(15) . . ?
O34 W7 O31 94.2(17) . . ?
O35 W7 O23 101.1(18) . . ?
O35 W7 O25 107.0(8) . . ?
O35 W7 O31 101.8(17) . . ?
O35 W7 O34 106.7(8) . . ?
O23A W7A O24A 88.9(4) . . ?
O23A W7A O32A 151.5(12) . . ?
O23A W7A O39A 105.8(7) . . ?
O24A W7A O32A 84.3(4) . . ?
O33A W7A O23A 92.1(5) . . ?
O33A W7A O24A 162.0(8) . . ?
O33A W7A O32A 86.3(9) . . ?
O33A W7A O39A 97(2) . . ?
O39A W7A O24A 100(2) . . ?
O39A W7A O32A 102.7(7) . . ?
O23 W8 O32 168.3(8) . 2_577 ?
O23 W8 O38 86(2) . 2_577 ?
O24 W8 O23 85(2) . . ?
O24 W8 O32 88.8(14) . 2_577 ?
O24 W8 O38 169.7(12) . 2_577 ?
O38 W8 O32 98.7(11) 2_577 2_577 ?
O24A W8A O25A 87.8(12) . . ?
O24A W8A O30A 161.4(8) . . ?
O24A W8A O31A 95.4(5) . . ?
O24A W8A O35A 94(2) . . ?
O25A W8A O35A 101.5(7) . . ?
O30A W8A O25A 82.8(13) . . ?
O30A W8A O35A 104(2) . . ?
O31A W8A O25A 156.3(13) . . ?
O31A W8A O30A 87.1(11) . . ?
O31A W8A O35A 101.8(6) . . ?
O24 W9 O26 74.1(15) . . ?
O24 W9 O27 153.6(11) . . ?
O25 W9 O24 94.0(13) . . ?
O25 W9 O26 145.2(14) . . ?
O25 W9 O27 89.8(5) . . ?
O26 W9 O27 88.0(4) . . ?
O36 W9 O24 102.4(6) . . ?
O36 W9 O25 107.8(8) . . ?
O36 W9 O26 106.7(8) . . ?
O36 W9 O27 101.2(5) . . ?
O1B W9A O23A 103(2) . . ?
O1B W9A O25A 101.0(7) . . ?
O1B W9A O26A 85(2) . . ?
O1B W9A O27A 98.0(6) . . ?
O23A W9A O26A 171.0(7) . . ?
O23A W9A O27A 87.3(4) . . ?
O25A W9A O23A 90.2(5) . . ?
O25A W9A O26A 93.7(10) . . ?
O25A W9A O27A 160.9(12) . . ?
O26A W9A O27A 86.4(4) . . ?
O30 W10 O29 150.0(10) . 2_577 ?
O31 W10 O29 88.8(5) . 2_577 ?
O31 W10 O30 91.0(4) . . ?
O31 W10 O32 175.4(9) . . ?
O32 W10 O29 88.1(5) . 2_577 ?
O32 W10 O30 90.0(4) . . ?
O33 W10 O29 96.9(18) . 2_577 ?
O33 W10 O30 113.0(18) . . ?
O33 W10 O31 92.4(6) . . ?
O33 W10 O32 91.3(5) . . ?
O27A W10A O28A 91.2(5) . . ?
O27A W10A O34A 98.2(5) . . ?
O27A W10A O38A 91.6(5) . . ?
O31A W10A O28A 86.7(5) 2_577 . ?
O34A W10A O28A 94.0(4) . . ?
O38A W10A O28A 169.4(8) . . ?
O38A W10A O34A 95.7(5) . . ?
O28 W11 O27 88.9(5) . . ?
O28 W11 O30 157.0(11) . . ?
O28 W11 O38 93.1(11) . . ?
O30 W11 O27 87.4(4) . . ?
O37 W11 O27 90.8(8) . . ?
O37 W11 O28 111.6(12) . . ?
O37 W11 O30 91.2(9) . . ?
O37 W11 O38 92.1(9) . . ?
O38 W11 O27 175.5(11) . . ?
O38 W11 O30 89.2(5) . . ?
O26A W11A O29A 82.2(4) . . ?
O28A W11A O26A 116.6(9) . . ?
O28A W11A O29A 159.5(9) . . ?
O28A W11A O37A 98.1(5) . . ?
O37A W11A O26A 94.3(6) . . ?
O37A W11A O29A 88.1(5) . . ?
O28 W12 O26 111.8(9) . . ?
O29 W12 O26 79.3(11) . . ?
O29 W12 O28 164.3(11) . . ?
O34 W12 O26 141.8(17) 2_577 . ?
O34 W12 O28 74.9(17) 2_577 . ?
O34 W12 O29 89.6(16) 2_577 . ?
O34 W12 O39 106.6(18) 2_577 . ?
O39 W12 O26 110.4(17) . . ?
O39 W12 O28 93.1(6) . . ?
O39 W12 O29 93.2(6) . . ?
O30A W12A O29A 85.0(5) . . ?
O30A W12A O36A 106.6(17) . . ?
O33A W12A O29A 84.3(4) 2_577 . ?
O36A W12A O29A 99.1(15) . . ?
O38A W12A O29A 149.8(9) 2_577 . ?
O38A W12A O30A 91.4(10) 2_577 . ?
O38A W12A O36A 110.6(18) 2_577 . ?
W7 O23 W8 137.1(11) . . ?
W7A O23A W9A 139.4(10) . . ?
W8 O24 W9 136.9(10) . . ?
W8A O24A W7A 133.7(9) . . ?
W9 O25 W7 136.0(10) . . ?
W8A O25A W9A 140.1(12) . . ?
W12 O26 W9 132.6(8) . . ?
W9A O26A W11A 106.0(6) . . ?
W9 O27 W11 144.5(10) . . ?
W10A O27A W9A 129.6(9) . . ?
W11 O28 W12 120.4(8) . . ?
W11A O28A W10A 106.6(7) . . ?
W12 O29 W10 132.0(13) . 2_577 ?
W12A O29A W11A 142.4(11) . . ?
W10 O30 W11 157.4(16) . . ?
W8A O30A W12A 136.5(11) . . ?
W10 O31 W7 137.1(10) . . ?
W10 O32 W8 106.6(9) . 2_577 ?
W12 O34 W7 144(3) 2_577 . ?
W11 O38 W8 106.5(14) . 2_577 ?
W12A O38A W10A 139.9(12) 2_577 . ?
O50 W13 O52 101.1(10) . . ?
O50 W13 O56 95.0(10) . . ?
O50 W13 O94 96.3(9) . . ?
O50 W13 O104 166.9(9) . . ?
O50 W13 O105 102.0(9) . . ?
O52 W13 O56 155.5(9) . . ?
O52 W13 O94 78.0(9) . . ?
O52 W13 O104 87.5(8) . . ?
O56 W13 O94 82.0(9) . . ?
O56 W13 O104 73.8(8) . . ?
O94 W13 O104 75.8(8) . . ?
O105 W13 O52 96.6(9) . . ?
O105 W13 O56 97.9(9) . . ?
O105 W13 O94 161.7(8) . . ?
O105 W13 O104 86.6(8) . . ?
O45 W14 O68 101.0(11) . . ?
O45 W14 O78 101.0(11) . . ?
O45 W14 O88 99.6(11) . . ?
O45 W14 O102 103.0(11) . . ?
O45 W14 O108 170.1(10) . . ?
O68 W14 O108 82.5(8) . . ?
O78 W14 O68 84.9(10) . . ?
O78 W14 O88 156.9(9) . . ?
O78 W14 O102 96.2(10) . . ?
O78 W14 O108 88.5(8) . . ?
O88 W14 O68 80.9(9) . . ?
O88 W14 O108 71.7(8) . . ?
O102 W14 O68 155.3(9) . . ?
O102 W14 O88 89.4(9) . . ?
O102 W14 O108 72.8(8) . . ?
O64 W15 O62 91.1(9) . . ?
O64 W15 O68 168.3(10) . . ?
O64 W15 O96 98.2(10) . . ?
O64 W15 O98 97.7(10) . . ?
O68 W15 O62 77.6(8) . . ?
O74 W15 O62 165.1(9) . . ?
O74 W15 O64 99.7(10) . . ?
O74 W15 O68 92.0(9) . . ?
O74 W15 O96 102.7(10) . . ?
O74 W15 O98 93.7(10) . . ?
O96 W15 O62 85.8(9) . . ?
O96 W15 O68 78.1(9) . . ?
O96 W15 O98 154.8(10) . . ?
O98 W15 O62 74.5(8) . . ?
O98 W15 O68 82.3(9) . . ?
O70 W19 O88 101.8(10) . . ?
O70 W19 O94 102.4(10) . . ?
O70 W19 O108 172.5(9) . . ?
O70 W19 O109 100.7(10) . . ?
O70 W19 O111 102.4(10) . . ?
O88 W19 O94 155.7(9) . . ?
O88 W19 O108 75.0(8) . . ?
O88 W19 O109 88.5(9) . . ?
O94 W19 O108 80.8(8) . . ?
O109 W19 O94 85.6(9) . . ?
O109 W19 O108 72.6(8) . . ?
O111 W19 O88 92.1(9) . . ?
O111 W19 O94 84.1(9) . . ?
O111 W19 O108 84.6(8) . . ?
O111 W19 O109 156.2(9) . . ?
O60 W20 O102 157.3(9) . . ?
O60 W20 O108 85.1(8) . . ?
O60 W20 O109 88.3(9) . . ?
O82 W20 O60 90.6(9) . . ?
O82 W20 O102 87.7(9) . . ?
O82 W20 O108 86.1(9) . . ?
O82 W20 O109 156.9(9) . . ?
O100 W20 O60 104.4(10) . . ?
O100 W20 O82 101.8(11) . . ?
O100 W20 O102 98.1(10) . . ?
O100 W20 O108 167.4(9) . . ?
O100 W20 O109 100.8(10) . . ?
O102 W20 O108 72.2(8) . . ?
O102 W20 O109 84.5(9) . . ?
O109 W20 O108 70.8(8) . . ?
O58 W21 Ag61 35.6(8) . . ?
O58 W21 O62 84.0(9) . . ?
O58 W21 O66 99.0(10) . . ?
O58 W21 O78 161.8(10) . . ?
O58 W21 O98 93.5(10) . . ?
O62 W21 Ag61 51.2(6) . . ?
O66 W21 Ag61 83.6(8) . . ?
O66 W21 O62 87.6(8) . . ?
O66 W21 O78 82.5(9) . . ?
O66 W21 O98 155.7(9) . . ?
O72 W21 Ag61 140.3(9) . . ?
O72 W21 O58 105.4(12) . . ?
O72 W21 O62 165.7(10) . . ?
O72 W21 O66 101.2(11) . . ?
O72 W21 O78 92.0(11) . . ?
O72 W21 O98 95.5(11) . . ?
O78 W21 Ag61 127.7(6) . . ?
O78 W21 O62 77.9(8) . . ?
O98 W21 Ag61 94.8(8) . . ?
O98 W21 O62 73.0(8) . . ?
O98 W21 O78 79.3(9) . . ?
O52 W24 O60 79.9(9) . . ?
O52 W24 O84 156.7(9) . . ?
O52 W24 O92 85.6(8) . . ?
O60 W24 O92 79.4(8) . . ?
O76 W24 O52 101.0(10) . . ?
O76 W24 O60 92.2(9) . . ?
O76 W24 O84 96.9(10) . . ?
O76 W24 O92 168.3(9) . . ?
O76 W24 O107 103.3(10) . . ?
O84 W24 O60 84.6(9) . . ?
O84 W24 O92 74.5(8) . . ?
O107 W24 O52 95.5(10) . . ?
O107 W24 O60 164.5(9) . . ?
O107 W24 O84 94.7(10) . . ?
O107 W24 O92 85.5(9) . . ?
O48 W26 O66 102.6(10) . . ?
O48 W26 O82 96.6(9) . . ?
O48 W26 O84 97.8(10) . . ?
O48 W26 O90 101.3(10) . . ?
O48 W26 O92 169.8(10) . . ?
O66 W26 O82 82.5(9) . . ?
O66 W26 O84 155.2(9) . . ?
O66 W26 O92 85.4(8) . . ?
O82 W26 O92 77.9(8) . . ?
O84 W26 O82 81.2(9) . . ?
O84 W26 O92 73.0(8) . . ?
O90 W26 O66 95.1(9) . . ?
O90 W26 O82 162.0(9) . . ?
O90 W26 O84 94.6(9) . . ?
O90 W26 O92 84.1(9) . . ?
O46 W28 O54 105.9(11) . . ?
O46 W28 O56 94.3(11) . . ?
O46 W28 O96 103.2(11) . . ?
O46 W28 O104 164.7(10) . . ?
O46 W28 O111 93.7(10) . . ?
O54 W28 O56 95.8(9) . . ?
O54 W28 O96 96.6(10) . . ?
O54 W28 O104 84.5(9) . . ?
O54 W28 O111 160.3(9) . . ?
O56 W28 O104 73.1(8) . . ?
O56 W28 O111 80.4(8) . . ?
O96 W28 O56 154.8(9) . . ?
O96 W28 O104 86.3(9) . . ?
O96 W28 O111 80.5(9) . . ?
O111 W28 O104 75.9(8) . . ?
S18 Ag Ag54 51.3(4) . . ?
S18 Ag P5 160.0(7) . . ?
S18 Ag O64 102.1(7) . . ?
P5 Ag Ag54 129.1(6) . . ?
O64 Ag Ag54 90.7(6) . . ?
O64 Ag P5 97.8(8) . . ?
S26A Ag1A P9 144.0(8) . . ?
S26A Ag1A O105 90.5(8) . . ?
O105 Ag1A P9 100.8(7) . . ?
Ag50 Ag2 Ag4 56.07(12) . . ?
S14 Ag2 Ag4 68.1(6) . . ?
S14 Ag2 Ag50 77.9(5) . . ?
S14 Ag2 S32 130.3(7) . . ?
S14 Ag2 O107 104.3(8) . . ?
S32 Ag2 Ag4 95.0(5) . . ?
S32 Ag2 Ag50 131.9(5) . . ?
S32 Ag2 O107 124.8(7) . . ?
O107 Ag2 Ag4 115.1(5) . . ?
O107 Ag2 Ag50 59.3(5) . . ?
Ag2 Ag4 Ag45 71.10(18) . . ?
Ag7 Ag4 Ag27 144.1(4) . . ?
Ag7 Ag4 Ag57 78.9(4) . . ?
Ag17 Ag4 Ag2 84.53(15) . . ?
Ag17 Ag4 Ag45 152.99(19) . . ?
Ag18 Ag4 Ag2 73.59(13) . . ?
Ag18 Ag4 Ag7 124.5(3) . . ?
Ag18 Ag4 Ag17 123.36(15) . . ?
Ag18 Ag4 Ag27 56.6(3) . . ?
Ag18 Ag4 Ag35 62.55(14) . . ?
Ag18 Ag4 Ag44 58.49(12) . . ?
Ag18 Ag4 Ag45 61.32(15) . . ?
Ag18 Ag4 Ag57 77.4(3) . . ?
Ag18 Ag4 Ag61 64.1(4) . . ?
Ag27 Ag4 Ag57 128.9(4) . . ?
Ag35 Ag4 Ag2 130.39(17) . . ?
Ag35 Ag4 Ag17 138.66(18) . . ?
Ag35 Ag4 Ag45 68.32(18) . . ?
Ag50 Ag4 Ag2 56.21(14) . . ?
Ag50 Ag4 Ag7 78.0(3) . . ?
Ag50 Ag4 Ag17 63.76(14) . . ?
Ag50 Ag4 Ag18 60.58(11) . . ?
Ag50 Ag4 Ag27 73.5(3) . . ?
Ag50 Ag4 Ag35 113.45(15) . . ?
Ag50 Ag4 Ag44 59.85(15) . . ?
Ag50 Ag4 Ag45 108.91(19) . . ?
Ag50 Ag4 Ag57 104.1(3) . . ?
Ag50 Ag4 Ag61 45.7(5) . . ?
Cl2 Ag4 Ag2 102.2(4) . . ?
Cl2 Ag4 Ag7 100.7(5) . . ?
Cl2 Ag4 Ag17 102.3(4) . . ?
Cl2 Ag4 Ag18 132.9(4) . . ?
Cl2 Ag4 Ag27 95.3(5) . . ?
Cl2 Ag4 Ag35 92.0(4) . . ?
Cl2 Ag4 Ag44 144.9(4) . . ?
Cl2 Ag4 Ag45 72.8(4) . . ?
Cl2 Ag4 Ag50 153.6(4) . . ?
Cl2 Ag4 Ag57 101.6(5) . . ?
Cl2 Ag4 Ag61 154.5(5) . . ?
P12 Ag6 S10 143.3(3) . . ?
S15 Ag7 Ag4 70.8(15) . . ?
S15 Ag7 S31 161(2) . . ?
S31 Ag7 Ag4 95.7(10) . . ?
S26 Ag9 Ag30 49.0(4) . . ?
S26 Ag9 O54 100.6(6) . . ?
P21 Ag9 Ag30 111.7(6) . . ?
P21 Ag9 S26 147.6(7) . . ?
P21 Ag9 O54 102.3(7) . . ?
O54 Ag9 Ag30 83.5(5) . . ?
P21 Ag9A S26A 109.2(10) . . ?
P21 Ag9A O54 112.5(9) . . ?
O54 Ag9A S26A 86.4(9) . . ?
P13 Ag10 S8 143.1(4) . . ?
O76 Ag10 S8 92.9(6) . . ?
O76 Ag10 P13 124.0(6) . . ?
P20 Ag12 S10 141.6(4) . . ?
O50 Ag12 S10 94.5(6) . . ?
O50 Ag12 P20 122.4(6) . . ?
Ag34 Ag15 Ag4 126.9(2) . . ?
S28 Ag15 Ag4 93.9(5) . . ?
S28 Ag15 Ag34 65.5(4) . . ?
S28 Ag15 S30 176.5(7) . . ?
S30 Ag15 Ag4 89.5(4) . . ?
S30 Ag15 Ag34 112.7(5) . . ?
Ag4 Ag17 Ag20 127.09(18) . . ?
Ag4 Ag17 Ag50 54.83(12) . . ?
Ag50 Ag17 Ag20 79.11(14) . . ?
S14 Ag17 Ag4 65.9(5) . . ?
S14 Ag17 Ag20 73.6(5) . . ?
S14 Ag17 Ag50 67.2(5) . . ?
S28 Ag17 Ag4 102.2(4) . . ?
S28 Ag17 Ag20 125.8(4) . . ?
S28 Ag17 Ag50 122.5(4) . . ?
S28 Ag17 S14 158.0(7) . . ?
Ag4 Ag18 Ag35 59.28(13) . . ?
Ag4 Ag18 Ag45 64.58(15) . . ?
Ag4 Ag18 Ag50 59.10(10) . . ?
Ag4 Ag18 Ag55 65.5(3) . . ?
Ag4 Ag18 Ag61 59.5(3) . . ?
Ag27 Ag18 Ag4 65.0(3) . . ?
Ag27 Ag18 Ag50 76.6(3) . . ?
Ag27 Ag18 Ag55 70.7(4) . . ?
Ag35 Ag18 Ag45 68.46(19) . . ?
Ag44 Ag18 Ag4 61.55(12) . . ?
Ag44 Ag18 Ag50 60.39(17) . . ?
Ag50 Ag18 Ag35 109.48(16) . . ?
Ag50 Ag18 Ag45 110.32(18) . . ?
Ag50 Ag18 Ag55 123.4(3) . . ?
Ag50 Ag18 Ag61 44.2(5) . . ?
O54 Ag18 Ag4 138.7(5) . . ?
O54 Ag18 Ag27 133.0(6) . . ?
O54 Ag18 Ag35 79.5(5) . . ?
O54 Ag18 Ag44 100.8(6) . . ?
O54 Ag18 Ag45 102.3(5) . . ?
O54 Ag18 Ag50 147.3(5) . . ?
O54 Ag18 Ag55 85.0(6) . . ?
O54 Ag18 Ag61 113.5(7) . . ?
O54 Ag18 O104 66.7(7) . . ?
O54 Ag18 O105 82.9(7) . . ?
O104 Ag18 Ag4 142.6(5) . . ?
O104 Ag18 Ag27 122.9(5) . . ?
O104 Ag18 Ag35 132.2(5) . . ?
O104 Ag18 Ag44 91.0(5) . . ?
O104 Ag18 Ag45 149.0(5) . . ?
O104 Ag18 Ag50 86.0(5) . . ?
O104 Ag18 Ag55 150.6(6) . . ?
O104 Ag18 Ag61 86.9(6) . . ?
O105 Ag18 Ag4 129.4(5) . . ?
O105 Ag18 Ag27 64.7(6) . . ?
O105 Ag18 Ag35 141.5(5) . . ?
O105 Ag18 Ag44 155.4(5) . . ?
O105 Ag18 Ag45 82.4(5) . . ?
O105 Ag18 Ag50 103.8(5) . . ?
O105 Ag18 Ag55 102.0(6) . . ?
O105 Ag18 Ag61 142.0(7) . . ?
O105 Ag18 O104 67.9(7) . . ?
S22 Ag20 Ag17 137.1(4) . . ?
S22 Ag20 Ag29 92.3(5) . . ?
S31 Ag20 Ag29 49.8(10) . . ?
S31 Ag20 S22 139.9(10) . . ?
P17 Ag20 Ag17 105.0(3) . . ?
P17 Ag20 Ag29 143.8(4) . . ?
P17 Ag20 S22 117.7(4) . . ?
P17 Ag20 S31 95.4(10) . . ?
O90 Ag20 Ag17 70.4(5) . . ?
O90 Ag20 Ag29 87.3(6) . . ?
O90 Ag20 S22 100.1(6) . . ?
O90 Ag20 S31 91.3(11) . . ?
O90 Ag20 P17 105.4(6) . . ?
P7 Ag24 S8 153.5(4) . . ?
Ag4 Ag27 Ag55 59.5(3) . . ?
Ag18 Ag27 Ag4 58.4(2) . . ?
Ag18 Ag27 Ag55 58.2(3) . . ?
S27 Ag27 Ag4 99.7(10) . . ?
S27 Ag27 Ag18 133.9(10) . . ?
S27 Ag27 Ag55 148.5(11) . . ?
S27 Ag27 S29 127.2(12) . . ?
S29 Ag27 Ag4 100.6(12) . . ?
S29 Ag27 Ag18 97.9(10) . . ?
S29 Ag27 Ag55 47.0(12) . . ?
Ag20 Ag29 Ag50 83.6(4) . . ?
S27 Ag29 Ag20 128.4(11) . . ?
S27 Ag29 Ag50 85.4(9) . . ?
S31 Ag29 Ag20 59.6(11) . . ?
S31 Ag29 Ag50 90.4(11) . . ?
S31 Ag29 S27 170.2(16) . . ?
S10 Ag30 Ag9 146.5(3) . . ?
S10 Ag30 S26 161.7(5) . . ?
S26 Ag30 Ag9 49.1(4) . . ?
S26A Ag30 S10 176.0(8) . . ?
P9 Ag33 S26 124.1(5) . . ?
P9 Ag33 O105 119.6(6) . . ?
O105 Ag33 S26 80.5(6) . . ?
S18 Ag34 Ag15 89.7(4) . . ?
P16 Ag34 Ag15 134.9(3) . . ?
P16 Ag34 S18 130.8(4) . . ?
P16 Ag34 O58 110.6(6) . . ?
O58 Ag34 Ag15 79.7(6) . . ?
O58 Ag34 S18 94.3(6) . . ?
Ag4 Ag35 Ag18 58.17(12) . . ?
Ag4 Ag35 Ag45 59.93(16) . . ?
Ag18 Ag35 Ag45 57.30(17) . . ?
S2 Ag35 Ag4 105.9(5) . . ?
S2 Ag35 Ag18 89.4(5) . . ?
S2 Ag35 Ag45 47.2(5) . . ?
S30 Ag35 Ag4 100.7(4) . . ?
S30 Ag35 Ag18 133.5(4) . . ?
S30 Ag35 Ag45 151.2(5) . . ?
S30 Ag35 S2 137.1(6) . . ?
S8 Ag36 S22 173.9(4) . . ?
S8 Ag36 O84 83.7(6) . . ?
S22 Ag36 O84 92.9(6) . . ?
P5 Ag37 S18 128.9(6) . . ?
P5 Ag37 O64 103.4(8) . . ?
O64 Ag37 S18 89.7(6) . . ?
P18 Ag38 S12 156.5(4) . . ?
Ag18 Ag44 Ag4 59.96(11) . . ?
Ag18 Ag44 Ag50 60.68(14) . . ?
Ag50 Ag44 Ag4 58.67(12) . . ?
O58 Ag44 Ag4 127.9(6) . . ?
O58 Ag44 Ag18 145.6(6) . . ?
O58 Ag44 Ag50 93.4(6) . . ?
O64 Ag44 Ag4 141.8(6) . . ?
O64 Ag44 Ag18 105.8(6) . . ?
O64 Ag44 Ag50 149.4(6) . . ?
O64 Ag44 O58 84.9(8) . . ?
Ag4 Ag45 Ag35 51.75(14) . . ?
Ag18 Ag45 Ag4 54.09(13) . . ?
Ag18 Ag45 Ag35 54.24(15) . . ?
S2 Ag45 Ag4 98.7(5) . . ?
S2 Ag45 Ag18 87.6(5) . . ?
S2 Ag45 Ag35 48.1(5) . . ?
S32 Ag45 Ag4 95.1(5) . . ?
S32 Ag45 Ag18 93.0(5) . . ?
S32 Ag45 Ag35 142.1(5) . . ?
S32 Ag45 S2 163.3(7) . . ?
P22 Ag46 S12 141.3(4) . . ?
Ag2 Ag50 Ag17 89.01(17) . . ?
Ag2 Ag50 Ag18 78.58(17) . . ?
Ag4 Ag50 Ag2 67.72(15) . . ?
Ag4 Ag50 Ag17 61.41(12) . . ?
Ag4 Ag50 Ag18 60.33(11) . . ?
Ag4 Ag50 Ag29 72.3(3) . . ?
Ag4 Ag50 Ag44 61.47(12) . . ?
Ag18 Ag50 Ag17 120.81(15) . . ?
Ag18 Ag50 Ag29 120.3(3) . . ?
Ag44 Ag50 Ag18 58.93(15) . . ?
Ag61 Ag50 Ag4 70.3(5) . . ?
Ag61 Ag50 Ag18 73.2(6) . . ?
Ag61 Ag50 O90 97.5(8) . . ?
Ag61 Ag50 O92 93.9(6) . . ?
Ag61 Ag50 O107 160.6(6) . . ?
O90 Ag50 Ag2 118.4(5) . . ?
O90 Ag50 Ag4 134.5(5) . . ?
O90 Ag50 Ag17 73.4(5) . . ?
O90 Ag50 Ag18 159.6(5) . . ?
O90 Ag50 Ag29 80.1(6) . . ?
O90 Ag50 Ag44 112.0(5) . . ?
O90 Ag50 O92 71.1(7) . . ?
O90 Ag50 O107 82.4(7) . . ?
O92 Ag50 Ag2 118.7(5) . . ?
O92 Ag50 Ag4 150.0(5) . . ?
O92 Ag50 Ag17 142.4(5) . . ?
O92 Ag50 Ag18 91.1(5) . . ?
O92 Ag50 Ag29 135.8(6) . . ?
O92 Ag50 Ag44 97.1(5) . . ?
O92 Ag50 O107 67.6(7) . . ?
O107 Ag50 Ag2 55.8(5) . . ?
O107 Ag50 Ag4 123.2(5) . . ?
O107 Ag50 Ag17 119.3(5) . . ?
O107 Ag50 Ag18 100.4(5) . . ?
O107 Ag50 Ag29 76.1(5) . . ?
O107 Ag50 Ag44 155.1(5) . . ?
S12 Ag54 Ag 132.6(4) . . ?
S12 Ag54 O98 78.0(6) . . ?
S18 Ag54 Ag 45.6(4) . . ?
S18 Ag54 S12 177.3(4) . . ?
S18 Ag54 O98 99.5(6) . . ?
O98 Ag54 Ag 84.3(6) . . ?
Ag4 Ag55 Ag27 54.7(3) . . ?
Ag18 Ag55 Ag4 54.2(2) . . ?
Ag18 Ag55 Ag27 51.1(3) . . ?
S7 Ag55 Ag4 92.1(11) . . ?
S7 Ag55 Ag18 91.5(11) . . ?
S7 Ag55 Ag27 139.2(11) . . ?
S7 Ag55 S29 168.5(15) . . ?
S29 Ag55 Ag4 99.3(10) . . ?
S29 Ag55 Ag18 94.5(13) . . ?
S29 Ag55 Ag27 50.4(12) . . ?
S7 Ag57 Ag4 94.5(11) . . ?
S15 Ag57 Ag4 71(2) . . ?
S15 Ag57 S7 139(2) . . ?
S22 Ag59 S27 121.1(9) . . ?
S22 Ag59 O107 97.8(6) . . ?
P24 Ag59 S22 140.9(6) . . ?
P24 Ag59 S27 94.7(9) . . ?
P24 Ag59 O107 110.7(7) . . ?
O107 Ag59 S27 68.6(9) . . ?
Ag4 Ag61 W21 171.8(9) . . ?
Ag4 Ag61 Ag18 56.4(3) . . ?
Ag18 Ag61 W21 129.0(5) . . ?
Ag50 Ag61 W21 111.6(8) . . ?
Ag50 Ag61 Ag4 64.0(4) . . ?
Ag50 Ag61 Ag18 62.7(4) . . ?
Ag50 Ag61 O62 98.1(8) . . ?
O58 Ag61 W21 29.7(7) . . ?
O58 Ag61 Ag4 146.8(10) . . ?
O58 Ag61 Ag18 155.4(11) . . ?
O58 Ag61 Ag50 127.1(14) . . ?
O58 Ag61 O62 71.8(9) . . ?
O62 Ag61 W21 44.4(5) . . ?
O62 Ag61 Ag4 141.2(8) . . ?
O62 Ag61 Ag18 84.8(7) . . ?
Ag4 Cl2 H2 105.4 . . ?
Ag45 S2 Ag35 84.7(7) . . ?
C390 S2 Ag35 108.3(19) . . ?
C390 S2 Ag45 106(2) . . ?
Ag55 S7 Ag57 99.5(16) . . ?
C38 S7 Ag55 113(3) . . ?
C38 S7 Ag57 112(4) . . ?
Ag24 S8 Ag10 121.8(4) . . ?
Ag36 S8 Ag10 103.8(4) . . ?
Ag36 S8 Ag24 100.1(4) . . ?
C242 S8 Ag10 110.7(15) . . ?
C242 S8 Ag24 108.5(15) . . ?
C242 S8 Ag36 111.2(15) . . ?
Ag6 S10 Ag12 118.5(4) . . ?
Ag30 S10 Ag6 104.4(4) . . ?
Ag30 S10 Ag12 100.5(4) . . ?
C102 S10 Ag6 105.7(15) . . ?
C102 S10 Ag12 107.6(15) . . ?
C102 S10 Ag30 120.9(15) . . ?
Ag38 S12 Ag46 100.7(4) . . ?
Ag54 S12 Ag38 106.2(4) . . ?
Ag54 S12 Ag46 109.2(4) . . ?
C226 S12 Ag38 110.8(17) . . ?
C226 S12 Ag46 109.2(16) . . ?
C226 S12 Ag54 119.2(13) . . ?
Ag2 S14 Ag17 122.5(9) . . ?
C240 S14 Ag2 135.3(18) . . ?
C240 S14 Ag17 100.7(17) . . ?
Ag57 S15 Ag7 125(3) . . ?
C1 S15 Ag7 116(3) . . ?
C1 S15 Ag57 118(4) . . ?
Ag S18 Ag34 132.3(6) . . ?
Ag S18 Ag54 83.1(5) . . ?
Ag34 S18 Ag37 120.0(5) . . ?
Ag54 S18 Ag34 104.2(5) . . ?
Ag54 S18 Ag37 101.1(5) . . ?
C4 S18 Ag 111.3(16) . . ?
C4 S18 Ag34 113.8(14) . . ?
C4 S18 Ag37 114.6(16) . . ?
C4 S18 Ag54 99.1(14) . . ?
Ag36 S22 Ag20 115.0(5) . . ?
Ag36 S22 Ag59 94.9(5) . . ?
Ag59 S22 Ag20 110.0(5) . . ?
C282 S22 Ag20 108.9(14) . . ?
C282 S22 Ag36 109.7(13) . . ?
C282 S22 Ag59 118.0(16) . . ?
Ag9 S26 Ag33 135.2(6) . . ?
Ag30 S26 Ag9 81.9(5) . . ?
Ag30 S26 Ag33 106.5(6) . . ?
C66 S26 Ag9 108(2) . . ?
C66 S26 Ag30 116.3(13) . . ?
C66 S26 Ag33 107.2(16) . . ?
Ag1A S26A Ag9A 126.8(12) . . ?
Ag30 S26A Ag1A 90.3(10) . . ?
Ag30 S26A Ag9A 115.2(12) . . ?
C68 S26A Ag1A 81(3) . . ?
C68 S26A Ag9A 120(3) . . ?
C68 S26A Ag30 117(3) . . ?
Ag27 S27 Ag29 99.2(13) . . ?
Ag27 S27 Ag59 127.3(15) . . ?
Ag29 S27 Ag59 83.1(11) . . ?
C394 S27 Ag27 118(2) . . ?
C394 S27 Ag29 130(3) . . ?
C394 S27 Ag59 98(2) . . ?
Ag15 S28 Ag17 94.9(6) . . ?
C272 S28 Ag15 109.0(15) . . ?
C272 S28 Ag17 104.3(19) . . ?
Ag55 S29 Ag27 82.6(15) . . ?
C396 S29 Ag27 74.9(14) . . ?
C396 S29 Ag55 97.8(18) . . ?
Ag15 S30 Ag35 96.4(6) . . ?
C56 S30 Ag15 108.5(18) . . ?
C56 S30 Ag35 113.7(15) . . ?
Ag7 S31 Ag20 125.2(16) . . ?
Ag29 S31 Ag7 105.1(17) . . ?
Ag29 S31 Ag20 70.6(12) . . ?
C92 S31 Ag7 99(4) . . ?
C92 S31 Ag20 135(4) . . ?
C92 S31 Ag29 102(5) . . ?
Ag45 S32 Ag2 97.1(7) . . ?
C74 S32 Ag2 107.3(18) . . ?
C74 S32 Ag45 109.9(18) . . ?
C224 P5 Ag 98.1(18) . . ?
C224 P5 Ag37 119.5(19) . . ?
C224 P5 C248 106(3) . . ?
C248 P5 Ag 118(2) . . ?
C248 P5 Ag37 114(2) . . ?
C382 P5 Ag 130.5(18) . . ?
C382 P5 Ag37 112.6(17) . . ?
C382 P5 C224 104(2) . . ?
C382 P5 C248 98(3) . . ?
C12 P7 Ag24 117.9(10) . . ?
C12 P7 C276 105.5(17) . . ?
C12 P7 C424 103.1(18) . . ?
C276 P7 Ag24 111.8(14) . . ?
C424 P7 Ag24 111.7(15) . . ?
C424 P7 C276 106(2) . . ?
C178 P9 Ag1A 101.8(16) . . ?
C178 P9 Ag33 116.2(16) . . ?
C178 P9 C198 107.0(19) . . ?
C178 P9 C278 103(2) . . ?
C198 P9 Ag1A 122.1(14) . . ?
C198 P9 Ag33 116.0(14) . . ?
C278 P9 Ag1A 114.1(17) . . ?
C278 P9 Ag33 106.6(17) . . ?
C278 P9 C198 107(2) . . ?
C40 P12 Ag6 112.9(11) . . ?
C122 P12 Ag6 121.3(14) . . ?
C122 P12 C40 102.7(18) . . ?
C302 P12 Ag6 106.2(11) . . ?
C302 P12 C40 110.5(15) . . ?
C302 P12 C122 102.7(17) . . ?
C8 P13 Ag10 110.8(13) . . ?
C8 P13 C106 103.6(17) . . ?
C8 P13 C126 103.9(18) . . ?
C106 P13 Ag10 111.1(11) . . ?
C106 P13 C126 103.3(16) . . ?
C126 P13 Ag10 122.4(13) . . ?
C60 P16 Ag34 113.7(14) . . ?
C60 P16 C362 102.1(18) . . ?
C324 P16 Ag34 113.7(16) . . ?
C324 P16 C60 103(2) . . ?
C324 P16 C362 101.9(19) . . ?
C362 P16 Ag34 120.0(12) . . ?
C30 P17 Ag20 116.9(13) . . ?
C30 P17 C128 98.5(16) . . ?
C128 P17 Ag20 110.9(10) . . ?
C212 P17 Ag20 114.3(14) . . ?
C212 P17 C30 110.4(19) . . ?
C212 P17 C128 103.8(17) . . ?
C6 P18 Ag38 116.1(16) . . ?
C6 P18 C266 103.0(18) . . ?
C32 P18 Ag38 115.4(14) . . ?
C32 P18 C6 104(2) . . ?
C32 P18 C266 101.1(17) . . ?
C266 P18 Ag38 115.2(12) . . ?
C76 P20 Ag12 108.9(9) . . ?
C76 P20 C156 103.1(16) . . ?
C90 P20 Ag12 113.8(15) . . ?
C90 P20 C76 103.9(17) . . ?
C90 P20 C156 104.3(19) . . ?
C156 P20 Ag12 121.1(13) . . ?
C64 P21 Ag9 118(2) . . ?
C64 P21 Ag9A 106(2) . . ?
C228 P21 Ag9 114(2) . . ?
C228 P21 Ag9A 134(2) . . ?
C228 P21 C64 100(3) . . ?
C312 P21 Ag9 115(2) . . ?
C312 P21 Ag9A 106(2) . . ?
C312 P21 C64 108(3) . . ?
C312 P21 C228 100(3) . . ?
C94 P22 Ag46 118.7(14) . . ?
C294 P22 Ag46 116.0(13) . . ?
C294 P22 C94 102.6(18) . . ?
C332 P22 Ag46 112.3(13) . . ?
C332 P22 C94 98.2(19) . . ?
C332 P22 C294 107.0(18) . . ?
C62 P24 Ag59 125(2) . . ?
C62 P24 C140 98(2) . . ?
C62 P24 C184 106(3) . . ?
C140 P24 Ag59 106.0(15) . . ?
C184 P24 Ag59 108.1(15) . . ?
C184 P24 C140 112(2) . . ?
O62 Si4 O104 109.4(11) . . ?
O92 Si4 O62 113.6(11) . . ?
O92 Si4 O104 107.6(11) . . ?
O108 Si4 O62 109.4(11) . . ?
O108 Si4 O92 109.0(12) . . ?
O108 Si4 O104 107.6(11) . . ?
W13 O50 Ag12 137.3(12) . . ?
W13 O52 W24 158.9(13) . . ?
W28 O54 Ag9 122.2(10) . . ?
W28 O54 Ag9A 133.4(11) . . ?
W28 O54 Ag18 115.5(10) . . ?
Ag18 O54 Ag9 112.2(8) . . ?
Ag18 O54 Ag9A 109.6(9) . . ?
W13 O56 W28 118.3(11) . . ?
W21 O58 Ag34 126.3(12) . . ?
W21 O58 Ag44 117.1(11) . . ?
W21 O58 Ag61 114.7(13) . . ?
Ag34 O58 Ag44 111.3(9) . . ?
Ag61 O58 Ag34 118.8(11) . . ?
W20 O60 W24 139.5(12) . . ?
W15 O62 W21 95.2(8) . . ?
W15 O62 Ag61 106.5(10) . . ?
W21 O62 Ag61 84.3(8) . . ?
Si4 O62 W15 130.8(11) . . ?
Si4 O62 W21 125.7(11) . . ?
Si4 O62 Ag61 104.0(11) . . ?
W15 O64 Ag 110.3(11) . . ?
W15 O64 Ag37 130.7(12) . . ?
W15 O64 Ag44 110.1(11) . . ?
Ag44 O64 Ag37 114.4(9) . . ?
W21 O66 W26 160.7(13) . . ?
W14 O68 W15 138.5(12) . . ?
W24 O76 Ag10 123.6(11) . . ?
W14 O78 W21 149.7(12) . . ?
W20 O82 W26 146.0(12) . . ?
W24 O84 Ag36 113.3(9) . . ?
W26 O84 W24 119.9(11) . . ?
W26 O84 Ag36 123.8(10) . . ?
W19 O88 W14 121.4(10) . . ?
W26 O90 Ag20 130.8(11) . . ?
W26 O90 Ag50 111.5(10) . . ?
Ag50 O90 Ag20 109.0(8) . . ?
W24 O92 W26 92.5(7) . . ?
W24 O92 Ag50 99.2(7) . . ?
W26 O92 Ag50 92.9(7) . . ?
Si4 O92 W24 130.7(12) . . ?
Si4 O92 W26 124.7(11) . . ?
Si4 O92 Ag50 108.7(11) . . ?
W19 O94 W13 142.7(11) . . ?
W15 O96 W28 159.0(14) . . ?
W15 O98 W21 116.8(11) . . ?
W15 O98 Ag54 117.0(10) . . ?
W21 O98 Ag54 117.1(10) . . ?
W14 O102 W20 124.3(12) . . ?
W13 O104 Ag18 93.0(7) . . ?
W28 O104 W13 93.8(8) . . ?
W28 O104 Ag18 93.3(7) . . ?
Si4 O104 W13 129.4(12) . . ?
Si4 O104 W28 128.4(11) . . ?
Si4 O104 Ag18 108.5(10) . . ?
W13 O105 Ag1A 122.3(9) . . ?
W13 O105 Ag18 112.5(9) . . ?
W13 O105 Ag33 122.5(9) . . ?
Ag18 O105 Ag1A 117.8(8) . . ?
Ag18 O105 Ag33 124.5(8) . . ?
W24 O107 Ag2 156.3(12) . . ?
W24 O107 Ag50 107.7(9) . . ?
W24 O107 Ag59 112.7(10) . . ?
Ag2 O107 Ag50 64.9(6) . . ?
Ag59 O107 Ag2 86.6(7) . . ?
Ag59 O107 Ag50 129.7(9) . . ?
W19 O108 W14 91.6(7) . . ?
W19 O108 W20 93.2(7) . . ?
W20 O108 W14 90.6(7) . . ?
Si4 O108 W14 123.1(11) . . ?
Si4 O108 W19 125.9(11) . . ?
Si4 O108 W20 122.7(11) . . ?
W19 O109 W20 123.4(11) . . ?
W19 O111 W28 149.3(12) . . ?
S15 C1 H1 110.8 . . ?
C196 C1 S15 104.4(9) . . ?
C196 C1 H1 110.8 . . ?
C404 C1 S15 104.6(9) . . ?
C404 C1 H1 110.8 . . ?
C404 C1 C196 115.1(12) . . ?
S18 C4 H4 110.5 . . ?
C344 C4 S18 115(4) . . ?
C344 C4 H4 110.5 . . ?
C348 C4 S18 107(3) . . ?
C348 C4 H4 110.5 . . ?
C348 C4 C344 103(4) . . ?
C244 C6 P18 120(4) . . ?
C254 C6 P18 112(4) . . ?
C254 C6 C244 125(5) . . ?
C10 C8 P13 123(3) . . ?
C36 C8 P13 120(3) . . ?
C36 C8 C10 117(4) . . ?
C8 C10 H10 121.1 . . ?
C120 C10 C8 118(4) . . ?
C120 C10 H10 121.1 . . ?
C14 C12 P7 124.3(15) . . ?
C14 C12 C22 120.0 . . ?
C22 C12 P7 115.7(15) . . ?
C12 C14 H14 120.0 . . ?
C12 C14 C16 120.0 . . ?
C16 C14 H14 120.0 . . ?
C14 C16 H16 120.0 . . ?
C18 C16 C14 120.0 . . ?
C18 C16 H16 120.0 . . ?
C16 C18 H18 120.0 . . ?
C20 C18 C16 120.0 . . ?
C20 C18 H18 120.0 . . ?
C18 C20 H20 120.0 . . ?
C22 C20 C18 120.0 . . ?
C22 C20 H20 120.0 . . ?
C12 C22 H22 120.0 . . ?
C20 C22 C12 120.0 . . ?
C20 C22 H22 120.0 . . ?
H24A C24 H24B 107.8 . . ?
C30 C24 H24A 109.0 . . ?
C30 C24 H24B 109.0 . . ?
C60 C24 H24A 109.0 . . ?
C60 C24 H24B 109.0 . . ?
C60 C24 C30 113(3) . . ?
C310 C26 H26 122.2 . . ?
C414 C26 H26 122.2 . . ?
C414 C26 C310 116(5) . . ?
C388 C28 H28 121.8 . . ?
C388 C28 C424 116(5) . . ?
C424 C28 H28 121.8 . . ?
P17 C30 H30A 109.8 . . ?
P17 C30 H30B 109.8 . . ?
C24 C30 P17 109(3) . . ?
C24 C30 H30A 109.8 . . ?
C24 C30 H30B 109.8 . . ?
H30A C30 H30B 108.2 . . ?
P18 C32 H32A 109.4 . . ?
P18 C32 H32B 109.4 . . ?
H32A C32 H32B 108.0 . . ?
C270 C32 P18 111(3) . . ?
C270 C32 H32A 109.4 . . ?
C270 C32 H32B 109.4 . . ?
H34A C34 H34B 109.5 . . ?
H34A C34 H34C 109.5 . . ?
H34B C34 H34C 109.5 . . ?
C390 C34 H34A 108.5 . . ?
C390 C34 H34B 109.6 . . ?
C390 C34 H34C 110.3 . . ?
C8 C36 H36 117.4 . . ?
C162 C36 C8 125(4) . . ?
C162 C36 H36 117.4 . . ?
S7 C38 H38 111.9 . . ?
C400 C38 S7 104.5(9) . . ?
C400 C38 H38 111.9 . . ?
C412 C38 S7 104.5(9) . . ?
C412 C38 H38 111.9 . . ?
C412 C38 C400 112(10) . . ?
C42 C40 P12 121.6(18) . . ?
C42 C40 C50 120.0 . . ?
C50 C40 P12 118.4(18) . . ?
C40 C42 H42 120.0 . . ?
C40 C42 C44 120.0 . . ?
C44 C42 H42 120.0 . . ?
C42 C44 H44 120.0 . . ?
C46 C44 C42 120.0 . . ?
C46 C44 H44 120.0 . . ?
C44 C46 H46 120.0 . . ?
C44 C46 C48 120.0 . . ?
C48 C46 H46 120.0 . . ?
C46 C48 H48 120.0 . . ?
C50 C48 C46 120.0 . . ?
C50 C48 H48 120.0 . . ?
C40 C50 H50 120.0 . . ?
C48 C50 C40 120.0 . . ?
C48 C50 H50 120.0 . . ?
C120 C52 H52 121.4 . . ?
C120 C52 C162 117(4) . . ?
C162 C52 H52 121.4 . . ?
C174 C54 H54 117.8 . . ?
C246 C54 H54 117.8 . . ?
C246 C54 C174 124(5) . . ?
S30 C56 H56 106.5 . . ?
C352 C56 S30 111(3) . . ?
C352 C56 H56 106.5 . . ?
C356 C56 S30 111(3) . . ?
C356 C56 H56 106.5 . . ?
C356 C56 C352 115.4(12) . . ?
C388 C58 H58 122.7 . . ?
C398 C58 H58 122.7 . . ?
C398 C58 C388 115(5) . . ?
P16 C60 H60A 107.4 . . ?
P16 C60 H60B 107.4 . . ?
C24 C60 P16 120(3) . . ?
C24 C60 H60A 107.4 . . ?
C24 C60 H60B 107.4 . . ?
H60A C60 H60B 106.9 . . ?
P24 C62 H62A 107.6 . . ?
P24 C62 H62B 107.6 . . ?
H62A C62 H62B 107.0 . . ?
C416 C62 P24 119(4) . . ?
C416 C62 H62A 107.6 . . ?
C416 C62 H62B 107.6 . . ?
P21 C64 H64A 108.1 . . ?
P21 C64 H64B 108.1 . . ?
H64A C64 H64B 107.3 . . ?
C96 C64 P21 117(5) . . ?
C96 C64 H64A 108.1 . . ?
C96 C64 H64B 108.1 . . ?
S26 C66 H66 101.9 . . ?
C70 C66 S26 117(3) . . ?
C70 C66 H66 101.9 . . ?
C152 C66 S26 117(3) . . ?
C152 C66 H66 101.9 . . ?
C152 C66 C70 114(4) . . ?
S26A C68 H68 98.1 . . ?
C72 C68 S26A 137(6) . . ?
C72 C68 H68 98.1 . . ?
C426 C68 S26A 103(6) . . ?
C426 C68 H68 98.1 . . ?
C426 C68 C72 113(5) . . ?
C66 C70 H70A 111.7 . . ?
C66 C70 H70B 111.5 . . ?
C66 C70 H70C 105.1 . . ?
H70A C70 H70B 109.5 . . ?
H70A C70 H70C 109.5 . . ?
H70B C70 H70C 109.5 . . ?
C68 C72 H72A 115.2 . . ?
C68 C72 H72B 108.1 . . ?
C68 C72 H72C 105.0 . . ?
H72A C72 H72B 109.4 . . ?
H72A C72 H72C 109.6 . . ?
H72B C72 H72C 109.4 . . ?
S32 C74 H74 107.6 . . ?
C160 C74 S32 107(4) . . ?
C160 C74 H74 107.6 . . ?
C346 C74 S32 111(5) . . ?
C346 C74 H74 107.6 . . ?
C346 C74 C160 115(6) . . ?
C78 C76 P20 117.4(14) . . ?
C78 C76 C86 120.0 . . ?
C86 C76 P20 122.6(14) . . ?
C76 C78 H78 120.0 . . ?
C76 C78 C80 120.0 . . ?
C80 C78 H78 120.0 . . ?
C78 C80 H80 120.0 . . ?
C78 C80 C82 120.0 . . ?
C82 C80 H80 120.0 . . ?
C80 C82 H82 120.0 . . ?
C84 C82 C80 120.0 . . ?
C84 C82 H82 120.0 . . ?
C82 C84 H84 120.0 . . ?
C82 C84 C86 120.0 . . ?
C86 C84 H84 120.0 . . ?
C76 C86 H86 120.0 . . ?
C84 C86 C76 120.0 . . ?
C84 C86 H86 120.0 . . ?
H88A C88 H88B 109.4 . . ?
H88A C88 H88C 109.5 . . ?
H88B C88 H88C 109.4 . . ?
C394 C88 H88A 106.6 . . ?
C394 C88 H88B 113.0 . . ?
C394 C88 H88C 108.8 . . ?
C154 C90 P20 125(4) . . ?
C154 C90 C210 117(4) . . ?
C210 C90 P20 118(3) . . ?
S31 C92 H92 93.9 . . ?
C180 C92 S31 117(7) . . ?
C180 C92 H92 93.9 . . ?
C182 C92 S31 126(7) . . ?
C182 C92 H92 93.9 . . ?
C182 C92 C180 115.2(12) . . ?
P22 C94 H94A 109.7 . . ?
P22 C94 H94B 109.7 . . ?
H94A C94 H94B 108.2 . . ?
C104 C94 P22 110(3) . . ?
C104 C94 H94A 109.7 . . ?
C104 C94 H94B 109.7 . . ?
C64 C96 H96A 109.9 . . ?
C64 C96 H96B 109.9 . . ?
C64 C96 C248 109(6) . . ?
H96A C96 H96B 108.3 . . ?
C248 C96 H96A 109.9 . . ?
C248 C96 H96B 109.9 . . ?
H98A C98 H98B 109.5 . . ?
H98A C98 H98C 109.6 . . ?
H98B C98 H98C 109.5 . . ?
C102 C98 H98A 110.9 . . ?
C102 C98 H98B 107.5 . . ?
C102 C98 H98C 109.9 . . ?
H10A C100 H10B 108.5 . . ?
C126 C100 H10A 110.2 . . ?
C126 C100 H10B 110.2 . . ?
C156 C100 H10A 110.2 . . ?
C156 C100 H10B 110.2 . . ?
C156 C100 C126 108(3) . . ?
S10 C102 H102 107.8 . . ?
C98 C102 S10 112(3) . . ?
C98 C102 H102 107.8 . . ?
C370 C102 S10 111(3) . . ?
C370 C102 C98 111(4) . . ?
C370 C102 H102 107.8 . . ?
C94 C104 H10C 111.1 . . ?
C94 C104 H10D 111.1 . . ?
C94 C104 C122 103(3) . . ?
H10C C104 H10D 109.1 . . ?
C122 C104 H10C 111.1 . . ?
C122 C104 H10D 111.1 . . ?
C108 C106 P13 122.1(17) . . ?
C108 C106 C116 120.0 . . ?
C116 C106 P13 117.7(17) . . ?
C106 C108 H108 120.0 . . ?
C110 C108 C106 120.0 . . ?
C110 C108 H108 120.0 . . ?
C108 C110 H110 120.0 . . ?
C108 C110 C112 120.0 . . ?
C112 C110 H110 120.0 . . ?
C110 C112 H112 120.0 . . ?
C114 C112 C110 120.0 . . ?
C114 C112 H112 120.0 . . ?
C112 C114 H114 120.0 . . ?
C112 C114 C116 120.0 . . ?
C116 C114 H114 120.0 . . ?
C106 C116 H116 120.0 . . ?
C114 C116 C106 120.0 . . ?
C114 C116 H116 120.0 . . ?
H11A C118 H11B 109.5 . . ?
H11A C118 H11C 109.5 . . ?
H11B C118 H11C 109.5 . . ?
C242 C118 H11A 109.5 . . ?
C242 C118 H11B 109.5 . . ?
C242 C118 H11C 109.5 . . ?
C10 C120 H120 117.8 . . ?
C52 C120 C10 124(4) . . ?
C52 C120 H120 117.8 . . ?
P12 C122 H12A 108.5 . . ?
P12 C122 H12B 108.5 . . ?
C104 C122 P12 115(3) . . ?
C104 C122 H12A 108.5 . . ?
C104 C122 H12B 108.5 . . ?
H12A C122 H12B 107.5 . . ?
C244 C124 H124 115.6 . . ?
C244 C124 C308 129(5) . . ?
C308 C124 H124 115.6 . . ?
P13 C126 H12C 109.1 . . ?
P13 C126 H12D 109.1 . . ?
C100 C126 P13 113(2) . . ?
C100 C126 H12C 109.1 . . ?
C100 C126 H12D 109.1 . . ?
H12C C126 H12D 107.8 . . ?
C130 C128 P17 117.0(15) . . ?
C130 C128 C138 120.0 . . ?
C138 C128 P17 122.9(15) . . ?
C128 C130 H130 120.0 . . ?
C132 C130 C128 120.0 . . ?
C132 C130 H130 120.0 . . ?
C130 C132 H132 120.0 . . ?
C130 C132 C134 120.0 . . ?
C134 C132 H132 120.0 . . ?
C132 C134 H134 120.0 . . ?
C136 C134 C132 120.0 . . ?
C136 C134 H134 120.0 . . ?
C134 C136 H136 120.0 . . ?
C134 C136 C138 120.0 . . ?
C138 C136 H136 120.0 . . ?
C128 C138 H138 120.0 . . ?
C136 C138 C128 120.0 . . ?
C136 C138 H138 120.0 . . ?
C142 C140 P24 114(2) . . ?
C142 C140 C150 120.0 . . ?
C150 C140 P24 126(2) . . ?
C140 C142 H142 120.0 . . ?
C144 C142 C140 120.0 . . ?
C144 C142 H142 120.0 . . ?
C142 C144 H144 120.0 . . ?
C146 C144 C142 120.0 . . ?
C146 C144 H144 120.0 . . ?
C144 C146 H146 120.0 . . ?
C144 C146 C148 120.0 . . ?
C148 C146 H146 120.0 . . ?
C146 C148 H148 120.0 . . ?
C150 C148 C146 120.0 . . ?
C150 C148 H148 120.0 . . ?
C140 C150 H150 120.0 . . ?
C148 C150 C140 120.0 . . ?
C148 C150 H150 120.0 . . ?
C66 C152 H15A 105.2 . . ?
C66 C152 H15B 113.5 . . ?
C66 C152 H15C 109.7 . . ?
H15A C152 H15B 109.4 . . ?
H15A C152 H15C 109.5 . . ?
H15B C152 H15C 109.4 . . ?
C90 C154 H154 117.9 . . ?
C90 C154 C418 124(5) . . ?
C418 C154 H154 117.9 . . ?
P20 C156 H15D 110.0 . . ?
P20 C156 H15E 110.0 . . ?
C100 C156 P20 109(3) . . ?
C100 C156 H15D 110.0 . . ?
C100 C156 H15E 110.0 . . ?
H15D C156 H15E 108.4 . . ?
H15F C158 H15G 109.5 . . ?
H15F C158 H15H 109.5 . . ?
H15G C158 H15H 109.4 . . ?
C226 C158 H15F 109.9 . . ?
C226 C158 H15G 99.7 . . ?
C226 C158 H15H 118.2 . . ?
C74 C160 H16A 108.4 . . ?
C74 C160 H16B 108.7 . . ?
C74 C160 H16C 111.3 . . ?
H16A C160 H16B 109.4 . . ?
H16A C160 H16C 109.5 . . ?
H16B C160 H16C 109.6 . . ?
C36 C162 C52 118(4) . . ?
C36 C162 H162 121.1 . . ?
C52 C162 H162 121.1 . . ?
C166 C164 H164 121.0 . . ?
C166 C164 C168 118(4) . . ?
C168 C164 H164 121.0 . . ?
C164 C166 H166 120.5 . . ?
C274 C166 C164 119(4) . . ?
C274 C166 H166 120.5 . . ?
C164 C168 H168 119.3 . . ?
C178 C168 C164 121(4) . . ?
C178 C168 H168 119.3 . . ?
C178 C170 H170 119.4 . . ?
C178 C170 C274 121(4) . . ?
C274 C170 H170 119.4 . . ?
H17A C172 H17B 109.5 . . ?
H17A C172 H17C 109.4 . . ?
H17B C172 H17C 109.5 . . ?
C282 C172 H17A 110.5 . . ?
C282 C172 H17B 109.1 . . ?
C282 C172 H17C 108.8 . . ?
C54 C174 H174 123.3 . . ?
C392 C174 C54 113(5) . . ?
C392 C174 H174 123.3 . . ?
H17D C176 H17E 109.4 . . ?
H17D C176 H17F 109.5 . . ?
H17E C176 H17F 109.5 . . ?
C394 C176 H17D 109.6 . . ?
C394 C176 H17E 113.8 . . ?
C394 C176 H17F 104.8 . . ?
C168 C178 P9 120(3) . . ?
C170 C178 P9 121(3) . . ?
C170 C178 C168 119(4) . . ?
C92 C180 H18A 107.3 . . ?
C92 C180 H18B 104.2 . . ?
C92 C180 H18C 116.8 . . ?
H18A C180 H18B 109.4 . . ?
H18A C180 H18C 109.4 . . ?
H18B C180 H18C 109.5 . . ?
C92 C182 H18D 113.1 . . ?
C92 C182 H18E 106.3 . . ?
C92 C182 H18F 108.9 . . ?
H18D C182 H18E 109.5 . . ?
H18D C182 H18F 109.5 . . ?
H18E C182 H18F 109.6 . . ?
C186 C184 P24 118(2) . . ?
C186 C184 C194 120.0 . . ?
C194 C184 P24 122(2) . . ?
C184 C186 H186 120.0 . . ?
C188 C186 C184 120.0 . . ?
C188 C186 H186 120.0 . . ?
C186 C188 H188 120.0 . . ?
C186 C188 C190 120.0 . . ?
C190 C188 H188 120.0 . . ?
C188 C190 H190 120.0 . . ?
C192 C190 C188 120.0 . . ?
C192 C190 H190 120.0 . . ?
C190 C192 H192 120.0 . . ?
C190 C192 C194 120.0 . . ?
C194 C192 H192 120.0 . . ?
C184 C194 H194 120.0 . . ?
C192 C194 C184 120.0 . . ?
C192 C194 H194 120.0 . . ?
C1 C196 H19A 115.9 . . ?
C1 C196 H19B 97.0 . . ?
C1 C196 H19C 114.2 . . ?
H19A C196 H19B 116.2 . . ?
H19A C196 H19C 105.6 . . ?
H19B C196 H19C 107.9 . . ?
C200 C198 P9 117(2) . . ?
C200 C198 C208 120.0 . . ?
C208 C198 P9 123(2) . . ?
C198 C200 H200 120.0 . . ?
C198 C200 C202 120.0 . . ?
C202 C200 H200 120.0 . . ?
C200 C202 H202 120.0 . . ?
C204 C202 C200 120.0 . . ?
C204 C202 H202 120.0 . . ?
C202 C204 H204 120.0 . . ?
C206 C204 C202 120.0 . . ?
C206 C204 H204 120.0 . . ?
C204 C206 H206 120.0 . . ?
C204 C206 C208 120.0 . . ?
C208 C206 H206 120.0 . . ?
C198 C208 H208 120.0 . . ?
C206 C208 C198 120.0 . . ?
C206 C208 H208 120.0 . . ?
C90 C210 H210 119.5 . . ?
C250 C210 C90 121(5) . . ?
C250 C210 H210 119.5 . . ?
C246 C212 P17 121(3) . . ?
C406 C212 P17 118(3) . . ?
C406 C212 C246 121(4) . . ?
C216 C214 H214 120.0 . . ?
C216 C214 C224 120.0 . . ?
C224 C214 H214 120.0 . . ?
C214 C216 H216 120.0 . . ?
C214 C216 C218 120.0 . . ?
C218 C216 H216 120.0 . . ?
C216 C218 H218 120.0 . . ?
C220 C218 C216 120.0 . . ?
C220 C218 H218 120.0 . . ?
C218 C220 H220 120.0 . . ?
C218 C220 C222 120.0 . . ?
C222 C220 H220 120.0 . . ?
C220 C222 H222 120.0 . . ?
C220 C222 C224 120.0 . . ?
C224 C222 H222 120.0 . . ?
C214 C224 P5 116(3) . . ?
C222 C224 P5 124(3) . . ?
C222 C224 C214 120.0 . . ?
S12 C226 H226 97.6 . . ?
C158 C226 S12 118(3) . . ?
C158 C226 H226 97.6 . . ?
C158 C226 C330 115.5(11) . . ?
C330 C226 S12 121(3) . . ?
C330 C226 H226 97.6 . . ?
C230 C228 P21 121(3) . . ?
C230 C228 C238 120.0 . . ?
C238 C228 P21 119(3) . . ?
C228 C230 H230 120.0 . . ?
C232 C230 C228 120.00(7) . . ?
C232 C230 H230 120.0 . . ?
C230 C232 H232 120.0 . . ?
C230 C232 C234 120.0 . . ?
C234 C232 H232 120.0 . . ?
C232 C234 H234 120.0 . . ?
C236 C234 C232 120.0 . . ?
C236 C234 H234 120.0 . . ?
C234 C236 H236 120.0 . . ?
C234 C236 C238 120.00(7) . . ?
C238 C236 H236 120.0 . . ?
C228 C238 H238 120.0 . . ?
C236 C238 C228 120.0 . . ?
C236 C238 H238 120.0 . . ?
S14 C240 H240 99.3 . . ?
C252 C240 S14 132(4) . . ?
C252 C240 H240 99.3 . . ?
C252 C240 C328 114(5) . . ?
C328 C240 S14 106(4) . . ?
C328 C240 H240 99.3 . . ?
S8 C242 H242 106.1 . . ?
C118 C242 S8 109(3) . . ?
C118 C242 H242 106.1 . . ?
C268 C242 S8 115(3) . . ?
C268 C242 C118 114(4) . . ?
C268 C242 H242 106.1 . . ?
C6 C244 C124 114(5) . . ?
C6 C244 H244 123.0 . . ?
C124 C244 H244 123.0 . . ?
C54 C246 C212 117(4) . . ?
C54 C246 H246 121.4 . . ?
C212 C246 H246 121.4 . . ?
P5 C248 H24C 108.7 . . ?
P5 C248 H24D 108.7 . . ?
C96 C248 P5 114(5) . . ?
C96 C248 H24C 108.7 . . ?
C96 C248 H24D 108.7 . . ?
H24C C248 H24D 107.6 . . ?
C210 C250 H250 120.7 . . ?
C210 C250 C420 119(5) . . ?
C420 C250 H250 120.7 . . ?
C240 C252 H25A 109.6 . . ?
C240 C252 H25B 110.7 . . ?
C240 C252 H25C 108.2 . . ?
H25A C252 H25B 109.5 . . ?
H25A C252 H25C 109.4 . . ?
H25B C252 H25C 109.5 . . ?
C6 C254 H254 118.2 . . ?
C6 C254 C326 124(5) . . ?
C326 C254 H254 118.2 . . ?
C258 C256 H256 120.0 . . ?
C258 C256 C266 120.0 . . ?
C266 C256 H256 120.0 . . ?
C256 C258 H258 120.0 . . ?
C260 C258 C256 120.0 . . ?
C260 C258 H258 120.0 . . ?
C258 C260 H260 120.0 . . ?
C258 C260 C262 120.0 . . ?
C262 C260 H260 120.0 . . ?
C260 C262 H262 120.0 . . ?
C264 C262 C260 120.0 . . ?
C264 C262 H262 120.0 . . ?
C262 C264 H264 120.0 . . ?
C266 C264 C262 120.0 . . ?
C266 C264 H264 120.0 . . ?
C256 C266 P18 116.6(17) . . ?
C264 C266 P18 123.4(17) . . ?
C264 C266 C256 120.0 . . ?
C242 C268 H26A 109.5 . . ?
C242 C268 H26B 109.5 . . ?
C242 C268 H26C 109.5 . . ?
H26A C268 H26B 109.5 . . ?
H26A C268 H26C 109.5 . . ?
H26B C268 H26C 109.5 . . ?
C32 C270 H27A 108.0 . . ?
C32 C270 H27B 108.0 . . ?
H27A C270 H27B 107.3 . . ?
C276 C270 C32 117(4) . . ?
C276 C270 H27A 108.0 . . ?
C276 C270 H27B 108.0 . . ?
S28 C272 H272 107.8 . . ?
C350 C272 S28 100(4) . . ?
C350 C272 H272 107.8 . . ?
C354 C272 S28 116(4) . . ?
C354 C272 H272 107.8 . . ?
C354 C272 C350 117(5) . . ?
C166 C274 C170 122(4) . . ?
C166 C274 H274 119.2 . . ?
C170 C274 H274 119.2 . . ?
P7 C276 H27C 109.8 . . ?
P7 C276 H27D 109.8 . . ?
C270 C276 P7 110(3) . . ?
C270 C276 H27C 109.8 . . ?
C270 C276 H27D 109.8 . . ?
H27C C276 H27D 108.2 . . ?
P9 C278 H27E 108.9 . . ?
P9 C278 H27F 108.9 . . ?
H27E C278 H27F 107.8 . . ?
C416 C278 P9 113(4) . . ?
C416 C278 H27E 108.9 . . ?
C416 C278 H27F 108.9 . . ?
C324 C280 H280 119.1 . . ?
C422 C280 H280 119.1 . . ?
C422 C280 C324 122(4) . . ?
S22 C282 H282 107.0 . . ?
C172 C282 S22 107(3) . . ?
C172 C282 H282 107.0 . . ?
C172 C282 C386 123(5) . . ?
C386 C282 S22 105(4) . . ?
C386 C282 H282 107.0 . . ?
C286 C284 H284 120.0 . . ?
C286 C284 C294 120.0 . . ?
C294 C284 H284 120.0 . . ?
C284 C286 H286 120.0 . . ?
C288 C286 C284 120.0 . . ?
C288 C286 H286 120.0 . . ?
C286 C288 H288 120.0 . . ?
C286 C288 C290 120.00(5) . . ?
C290 C288 H288 120.0 . . ?
C288 C290 H290 120.0 . . ?
C292 C290 C288 120.0 . . ?
C292 C290 H290 120.0 . . ?
C290 C292 H292 120.0 . . ?
C294 C292 C290 120.0 . . ?
C294 C292 H292 120.0 . . ?
C284 C294 P22 116(2) . . ?
C292 C294 P22 123(2) . . ?
C292 C294 C284 120.00(5) . . ?
C298 C296 H296 120.0 . . ?
C298 C296 C306 120.0 . . ?
C306 C296 H296 120.0 . . ?
C296 C298 H298 120.0 . . ?
C296 C298 C300 120.0 . . ?
C300 C298 H298 120.0 . . ?
C298 C300 H300 120.0 . . ?
C302 C300 C298 120.0 . . ?
C302 C300 H300 120.0 . . ?
C300 C302 P12 120.8(17) . . ?
C300 C302 C304 120.0 . . ?
C304 C302 P12 119.2(17) . . ?
C302 C304 H304 120.0 . . ?
C306 C304 C302 120.0 . . ?
C306 C304 H304 120.0 . . ?
C296 C306 H306 120.0 . . ?
C304 C306 C296 120.0 . . ?
C304 C306 H306 120.0 . . ?
C124 C308 H308 124.7 . . ?
C124 C308 C326 111(5) . . ?
C326 C308 H308 124.7 . . ?
C26 C310 H310 116.9 . . ?
C324 C310 C26 126(4) . . ?
C324 C310 H310 116.9 . . ?
C314 C312 P21 121(4) . . ?
C314 C312 C322 120.0 . . ?
C322 C312 P21 119(4) . . ?
C312 C314 H314 120.0 . . ?
C312 C314 C316 120.0 . . ?
C316 C314 H314 120.0 . . ?
C314 C316 H316 120.0 . . ?
C318 C316 C314 120.0 . . ?
C318 C316 H316 120.0 . . ?
C316 C318 H318 120.0 . . ?
C316 C318 C320 120.0 . . ?
C320 C318 H318 120.0 . . ?
C318 C320 H320 120.0 . . ?
C322 C320 C318 120.0 . . ?
C322 C320 H320 120.0 . . ?
C312 C322 H322 120.0 . . ?
C320 C322 C312 120.0 . . ?
C320 C322 H322 120.0 . . ?
C280 C324 P16 118(3) . . ?
C310 C324 P16 131(4) . . ?
C310 C324 C280 111(4) . . ?
C254 C326 C308 114(5) . . ?
C254 C326 H32C 108.8 . . ?
C254 C326 H32D 108.8 . . ?
C308 C326 H32C 108.8 . . ?
C308 C326 H32D 108.8 . . ?
H32C C326 H32D 107.7 . . ?
C240 C328 H32E 110.4 . . ?
C240 C328 H32F 108.0 . . ?
C240 C328 H32G 110.0 . . ?
H32E C328 H32F 109.5 . . ?
H32E C328 H32G 109.5 . . ?
H32F C328 H32G 109.5 . . ?
C226 C330 H33A 95.0 . . ?
C226 C330 H33B 118.7 . . ?
C226 C330 H33C 113.5 . . ?
H33A C330 H33B 109.5 . . ?
H33A C330 H33C 109.5 . . ?
H33B C330 H33C 109.4 . . ?
C334 C332 P22 118(2) . . ?
C334 C332 C342 120.0 . . ?
C342 C332 P22 120(2) . . ?
C332 C334 H334 120.0 . . ?
C332 C334 C336 120.0 . . ?
C336 C334 H334 120.0 . . ?
C334 C336 H336 120.0 . . ?
C334 C336 C338 120.00(6) . . ?
C338 C336 H336 120.0 . . ?
C336 C338 H338 120.0 . . ?
C340 C338 C336 120.0 . . ?
C340 C338 H338 120.0 . . ?
C338 C340 H340 120.0 . . ?
C342 C340 C338 120.0 . . ?
C342 C340 H340 120.0 . . ?
C332 C342 H342 120.0 . . ?
C340 C342 C332 120.00(5) . . ?
C340 C342 H342 120.0 . . ?
C4 C344 H34D 109.5 . . ?
C4 C344 H34E 109.5 . . ?
C4 C344 H34F 109.5 . . ?
H34D C344 H34E 109.5 . . ?
H34D C344 H34F 109.5 . . ?
H34E C344 H34F 109.5 . . ?
C74 C346 H34G 107.9 . . ?
C74 C346 H34H 109.3 . . ?
C74 C346 H34I 111.2 . . ?
H34G C346 H34H 109.5 . . ?
H34G C346 H34I 109.5 . . ?
H34H C346 H34I 109.5 . . ?
C4 C348 H34J 123.2 . . ?
C4 C348 H34K 94.8 . . ?
C4 C348 H34L 109.1 . . ?
H34J C348 H34K 109.5 . . ?
H34J C348 H34L 109.5 . . ?
H34K C348 H34L 109.4 . . ?
C272 C350 H35A 108.8 . . ?
C272 C350 H35B 110.2 . . ?
C272 C350 H35C 109.4 . . ?
H35A C350 H35B 109.4 . . ?
H35A C350 H35C 109.5 . . ?
H35B C350 H35C 109.5 . . ?
C56 C352 H35D 109.8 . . ?
C56 C352 H35E 109.7 . . ?
C56 C352 H35F 108.8 . . ?
H35D C352 H35E 109.5 . . ?
H35D C352 H35F 109.5 . . ?
H35E C352 H35F 109.5 . . ?
C272 C354 H35G 106.1 . . ?
C272 C354 H35H 110.1 . . ?
C272 C354 H35I 112.2 . . ?
H35G C354 H35H 109.5 . . ?
H35G C354 H35I 109.5 . . ?
H35H C354 H35I 109.3 . . ?
C56 C356 H35J 110.2 . . ?
C56 C356 H35K 108.9 . . ?
C56 C356 H35L 109.3 . . ?
H35J C356 H35K 109.4 . . ?
H35J C356 H35L 109.5 . . ?
H35K C356 H35L 109.5 . . ?
C360 C358 H358 120.0 . . ?
C360 C358 C368 120.0 . . ?
C368 C358 H358 120.0 . . ?
C358 C360 H360 120.0 . . ?
C362 C360 C358 120.0 . . ?
C362 C360 H360 120.0 . . ?
C360 C362 P16 114.0(19) . . ?
C360 C362 C364 120.0 . . ?
C364 C362 P16 126.0(19) . . ?
C362 C364 H364 120.0 . . ?
C362 C364 C366 120.0 . . ?
C366 C364 H364 120.0 . . ?
C364 C366 H366 120.0 . . ?
C364 C366 C368 120.0 . . ?
C368 C366 H366 120.0 . . ?
C358 C368 H368 120.0 . . ?
C366 C368 C358 120.0 . . ?
C366 C368 H368 120.0 . . ?
C102 C370 H37A 109.8 . . ?
C102 C370 H37B 109.0 . . ?
C102 C370 H37C 109.6 . . ?
H37A C370 H37B 109.5 . . ?
H37A C370 H37C 109.5 . . ?
H37B C370 H37C 109.5 . . ?
C374 C372 H372 120.0 . . ?
C374 C372 C382 120.0 . . ?
C382 C372 H372 120.0 . . ?
C372 C374 H374 120.0 . . ?
C372 C374 C376 120.0 . . ?
C376 C374 H374 120.0 . . ?
C374 C376 H376 120.0 . . ?
C378 C376 C374 120.0 . . ?
C378 C376 H376 120.0 . . ?
C376 C378 H378 120.0 . . ?
C380 C378 C376 120.0 . . ?
C380 C378 H378 120.0 . . ?
C378 C380 H380 120.0 . . ?
C378 C380 C382 120.0 . . ?
C382 C380 H380 120.0 . . ?
C372 C382 P5 121(2) . . ?
C380 C382 P5 119(2) . . ?
C380 C382 C372 120.00(6) . . ?
H38A C384 H38B 109.5 . . ?
H38A C384 H38C 109.5 . . ?
H38B C384 H38C 109.4 . . ?
C390 C384 H38A 109.6 . . ?
C390 C384 H38B 109.5 . . ?
C390 C384 H38C 109.3 . . ?
C282 C386 H38D 109.6 . . ?
C282 C386 H38E 108.4 . . ?
C282 C386 H38F 110.5 . . ?
H38D C386 H38E 109.5 . . ?
H38D C386 H38F 109.4 . . ?
H38E C386 H38F 109.4 . . ?
C28 C388 C58 125(5) . . ?
C28 C388 H388 117.3 . . ?
C58 C388 H388 117.3 . . ?
S2 C390 H390 107.6 . . ?
C34 C390 S2 104.6(9) . . ?
C34 C390 C384 124(6) . . ?
C34 C390 H390 107.6 . . ?
C384 C390 S2 104.5(9) . . ?
C384 C390 H390 107.6 . . ?
C174 C392 H392 115.3 . . ?
C174 C392 C406 129(5) . . ?
C406 C392 H392 115.3 . . ?
S27 C394 H394 110.8 . . ?
C88 C394 S27 104.5(8) . . ?
C88 C394 H394 110.8 . . ?
C176 C394 S27 104.4(8) . . ?
C176 C394 C88 115.3(10) . . ?
C176 C394 H394 110.8 . . ?
S29 C396 H396 120.0 . . ?
C402 C396 S29 77(7) . . ?
C402 C396 H396 120.0 . . ?
C408 C396 S29 94(6) . . ?
C408 C396 H396 120.0 . . ?
C408 C396 C402 114.8(12) . . ?
C58 C398 H398 121.5 . . ?
C410 C398 C58 117(5) . . ?
C410 C398 H398 121.5 . . ?
C38 C400 H40A 106.1 . . ?
C38 C400 H40B 108.0 . . ?
C38 C400 H40C 114.2 . . ?
H40A C400 H40B 109.4 . . ?
H40A C400 H40C 109.5 . . ?
H40B C400 H40C 109.4 . . ?
C396 C402 H40D 96.9 . . ?
C396 C402 H40E 108.7 . . ?
C396 C402 H40F 121.8 . . ?
H40D C402 H40E 109.6 . . ?
H40D C402 H40F 109.4 . . ?
H40E C402 H40F 109.4 . . ?
C1 C404 H40G 109.1 . . ?
C1 C404 H40H 102.4 . . ?
C1 C404 H40I 116.4 . . ?
H40G C404 H40H 109.6 . . ?
H40G C404 H40I 109.5 . . ?
H40H C404 H40I 109.5 . . ?
C212 C406 H406 123.0 . . ?
C392 C406 C212 114(4) . . ?
C392 C406 H406 123.0 . . ?
C396 C408 H40J 102.4 . . ?
C396 C408 H40K 110.2 . . ?
C396 C408 H2 115.4 . . ?
H40J C408 H40K 109.5 . . ?
H40J C408 H2 109.5 . . ?
H40K C408 H2 109.5 . . ?
C398 C410 H410 117.9 . . ?
C424 C410 C398 124(5) . . ?
C424 C410 H410 117.9 . . ?
C38 C412 H41A 107.3 . . ?
C38 C412 H41B 111.5 . . ?
C38 C412 H41C 109.6 . . ?
H41A C412 H41B 109.4 . . ?
H41A C412 H41C 109.5 . . ?
H41B C412 H41C 109.5 . . ?
C26 C414 H414 116.6 . . ?
C26 C414 C422 127(5) . . ?
C422 C414 H414 116.6 . . ?
C62 C416 C278 130(5) . . ?
C62 C416 H41D 104.7 . . ?
C62 C416 H41E 104.7 . . ?
C278 C416 H41D 104.7 . . ?
C278 C416 H41E 104.7 . . ?
H41D C416 H41E 105.7 . . ?
C154 C418 H418 123.0 . . ?
C420 C418 C154 114(5) . . ?
C420 C418 H418 123.0 . . ?
C250 C420 H420 117.9 . . ?
C418 C420 C250 124(5) . . ?
C418 C420 H420 117.9 . . ?
C280 C422 H422 121.4 . . ?
C414 C422 C280 117(5) . . ?
C414 C422 H422 121.4 . . ?
C28 C424 P7 122(4) . . ?
C410 C424 P7 116(4) . . ?
C410 C424 C28 122(5) . . ?
C68 C426 H42A 122.0 . . ?
C68 C426 H42B 110.5 . . ?
C68 C426 H42C 94.6 . . ?
H42A C426 H42B 109.5 . . ?
H42A C426 H42C 109.5 . . ?
H42B C426 H42C 109.5 . . ?
O44 W16 O55 96.0(9) . . ?
O44 W16 O59 103.5(10) . . ?
O44 W16 O61 97.9(10) . . ?
O44 W16 O80 168.0(9) . . ?
O44 W16 O99 102.8(10) . . ?
O55 W16 O80 76.5(8) . . ?
O59 W16 O55 83.2(9) . . ?
O59 W16 O61 153.7(9) . . ?
O59 W16 O80 85.2(8) . . ?
O61 W16 O55 79.6(9) . . ?
O61 W16 O80 71.7(8) . . ?
O99 W16 O55 160.9(9) . . ?
O99 W16 O59 95.8(9) . . ?
O99 W16 O61 94.1(9) . . ?
O99 W16 O80 84.4(8) . . ?
O51 W17 O101 75.6(7) . . ?
O73 W17 O51 80.0(8) . . ?
O73 W17 O97 155.6(9) . . ?
O73 W17 O101 72.4(8) . . ?
O83 W17 O51 162.0(9) . . ?
O83 W17 O73 95.3(10) . . ?
O83 W17 O97 95.7(10) . . ?
O83 W17 O101 86.5(9) . . ?
O91 W17 O51 93.7(10) . . ?
O91 W17 O73 92.2(10) . . ?
O91 W17 O83 103.8(11) . . ?
O91 W17 O97 106.1(10) . . ?
O91 W17 O101 162.4(10) . . ?
O97 W17 O51 82.9(9) . . ?
O97 W17 O101 86.6(8) . . ?
O47 W18 O57 100.7(10) . . ?
O47 W18 O73 96.2(10) . . ?
O47 W18 O87 95.9(9) . . ?
O47 W18 O101 165.9(9) . . ?
O57 W18 O73 154.5(9) . . ?
O57 W18 O87 77.7(9) . . ?
O57 W18 O101 87.9(8) . . ?
O73 W18 O87 81.8(9) . . ?
O73 W18 O101 72.2(8) . . ?
O79 W18 O47 102.1(10) . . ?
O79 W18 O57 97.8(9) . . ?
O79 W18 O73 97.2(9) . . ?
O79 W18 O87 161.9(8) . . ?
O79 W18 O101 87.6(8) . . ?
O87 W18 O101 74.9(7) . . ?
O53 W22 O80 78.9(8) . . ?
O57 W22 O53 80.3(9) . . ?
O57 W22 O80 84.9(8) . . ?
O61 W22 O53 83.6(9) . . ?
O61 W22 O57 155.5(9) . . ?
O61 W22 O80 73.9(8) . . ?
O77 W22 O53 165.2(9) . . ?
O77 W22 O57 95.9(10) . . ?
O77 W22 O61 95.0(10) . . ?
O77 W22 O80 86.6(8) . . ?
O93 W22 O53 92.4(9) . . ?
O93 W22 O57 101.3(10) . . ?
O93 W22 O61 97.7(10) . . ?
O93 W22 O77 102.3(10) . . ?
O93 W22 O80 168.4(9) . . ?
O49 W23 O67 73.2(8) . . ?
O49 W23 O71 88.9(10) . . ?
O49 W23 O87 155.3(9) . . ?
O51 W23 O49 92.1(9) . . ?
O51 W23 O67 85.5(8) . . ?
O51 W23 O71 156.9(9) . . ?
O51 W23 O87 84.1(9) . . ?
O63 W23 O49 102.7(10) . . ?
O63 W23 O51 100.2(9) . . ?
O63 W23 O67 173.2(9) . . ?
O63 W23 O71 102.1(10) . . ?
O63 W23 O87 101.9(10) . . ?
O71 W23 O67 72.7(8) . . ?
O71 W23 O87 85.5(9) . . ?
O87 W23 O67 82.2(7) . . ?
O59 W25 Ag53 83.4(7) . . ?
O59 W25 O81 83.0(8) . . ?
O59 W25 O86 87.6(8) . . ?
O59 W25 O95 155.3(9) . . ?
O81 W25 Ag53 127.2(6) . . ?
O81 W25 O86 77.7(8) . . ?
O85 W25 Ag53 137.9(8) . . ?
O85 W25 O59 101.1(10) . . ?
O85 W25 O81 94.7(10) . . ?
O85 W25 O86 167.8(9) . . ?
O85 W25 O95 97.5(10) . . ?
O85 W25 O103 102.4(11) . . ?
O86 W25 Ag53 50.9(6) . . ?
O95 W25 Ag53 93.5(7) . . ?
O95 W25 O81 79.4(8) . . ?
O95 W25 O86 71.9(8) . . ?
O103 W25 Ag53 36.1(8) . . ?
O103 W25 O59 97.4(10) . . ?
O103 W25 O81 162.4(9) . . ?
O103 W25 O86 84.7(9) . . ?
O103 W25 O95 94.3(10) . . ?
O89 W27 O86 165.9(9) . . ?
O89 W27 O95 93.8(10) . . ?
O89 W27 O97 102.6(10) . . ?
O89 W27 O106 92.1(10) . . ?
O95 W27 O86 75.1(8) . . ?
O95 W27 O106 82.3(9) . . ?
O97 W27 O86 85.6(9) . . ?
O97 W27 O95 156.0(9) . . ?
O97 W27 O106 79.7(9) . . ?
O106 W27 O86 78.0(8) . . ?
O110 W27 O86 89.3(9) . . ?
O110 W27 O89 100.9(11) . . ?
O110 W27 O95 97.3(10) . . ?
O110 W27 O97 96.7(11) . . ?
O110 W27 O106 167.0(10) . . ?
O49 W29 O67 72.8(8) . . ?
O49 W29 O106 81.3(10) . . ?
O65 W29 O49 88.0(9) . . ?
O65 W29 O67 73.9(8) . . ?
O65 W29 O106 156.0(9) . . ?
O69 W29 O49 98.1(10) . . ?
O69 W29 O65 101.4(10) . . ?
O69 W29 O67 169.8(9) . . ?
O69 W29 O106 101.3(11) . . ?
O81 W29 O49 156.9(10) . . ?
O81 W29 O65 98.1(10) . . ?
O81 W29 O67 87.4(8) . . ?
O81 W29 O69 102.4(10) . . ?
O81 W29 O106 84.3(10) . . ?
O106 W29 O67 82.4(8) . . ?
O53 W30 O65 158.6(9) . . ?
O53 W30 O67 87.1(7) . . ?
O53 W30 O71 88.9(9) . . ?
O55 W30 O53 88.8(9) . . ?
O55 W30 O65 91.4(9) . . ?
O55 W30 O67 85.3(8) . . ?
O55 W30 O71 156.7(9) . . ?
O65 W30 O67 71.6(8) . . ?
O71 W30 O65 82.6(9) . . ?
O71 W30 O67 71.5(8) . . ?
O75 W30 O53 103.1(10) . . ?
O75 W30 O55 102.1(11) . . ?
O75 W30 O65 97.7(10) . . ?
O75 W30 O67 167.4(9) . . ?
O75 W30 O71 101.0(10) . . ?
Ag3 Ag1 Ag13 69.7(3) . . ?
Ag3 Ag1 Ag25 129.8(3) . . ?
Ag5 Ag1 Ag39 84.15(17) . . ?
Ag8 Ag1 Ag3 58.1(2) . . ?
Ag8 Ag1 Ag5 123.34(16) . . ?
Ag8 Ag1 Ag13 111.5(2) . . ?
Ag8 Ag1 Ag21 62.66(16) . . ?
Ag8 Ag1 Ag25 76.3(2) . . ?
Ag8 Ag1 Ag39 74.88(15) . . ?
Ag8 Ag1 Ag49 124.4(2) . . ?
Ag8 Ag1 Ag53 63.7(3) . . ?
Ag8 Ag1 Ag58 57.68(13) . . ?
Ag21 Ag1 Ag5 137.82(19) . . ?
Ag21 Ag1 Ag39 131.82(19) . . ?
Ag25 Ag1 Ag13 155.1(3) . . ?
Ag49 Ag1 Ag3 142.8(3) . . ?
Ag49 Ag1 Ag13 76.9(3) . . ?
Ag49 Ag1 Ag25 79.4(3) . . ?
Ag56 Ag1 Ag3 70.9(2) . . ?
Ag56 Ag1 Ag5 64.49(15) . . ?
Ag56 Ag1 Ag8 60.36(11) . . ?
Ag56 Ag1 Ag13 63.0(2) . . ?
Ag56 Ag1 Ag21 114.32(17) . . ?
Ag56 Ag1 Ag25 105.4(3) . . ?
Ag56 Ag1 Ag39 54.66(16) . . ?
Ag56 Ag1 Ag49 79.7(2) . . ?
Ag56 Ag1 Ag53 48.0(3) . . ?
Ag56 Ag1 Ag58 61.06(15) . . ?
Cl1 Ag1 Ag8 134.9(5) . . ?
Cl1 Ag1 Ag56 152.0(4) . . ?
Cl1 Ag1 Ag58 144.8(4) . . ?
P11 Ag1B S24A 115.1(8) . . ?
P11 Ag1B O83 113.4(9) . . ?
O83 Ag1B S24A 86.4(7) . . ?
Ag1 Ag3 Ag56 51.42(17) . . ?
Ag8 Ag3 Ag1 57.36(18) . . ?
Ag8 Ag3 Ag56 53.13(18) . . ?
S3 Ag3 Ag1 100.6(8) . . ?
S3 Ag3 Ag8 135.9(8) . . ?
S3 Ag3 Ag56 82.9(7) . . ?
S3 Ag3 S23 128.2(10) . . ?
S23 Ag3 Ag1 100.1(9) . . ?
S23 Ag3 Ag8 94.9(8) . . ?
S23 Ag3 Ag56 144.2(8) . . ?
Ag1 Ag5 Ag22 126.9(2) . . ?
Ag1 Ag5 Ag56 54.37(13) . . ?
Ag56 Ag5 Ag22 78.53(16) . . ?
S9 Ag5 Ag1 101.7(5) . . ?
S9 Ag5 Ag22 126.2(5) . . ?
S9 Ag5 Ag56 123.5(5) . . ?
S17 Ag5 Ag1 83.3(6) . . ?
S17 Ag5 Ag22 55.4(6) . . ?
S17 Ag5 Ag56 69.1(6) . . ?
S17 Ag5 S9 167.1(8) . . ?
Ag1 Ag8 Ag3 64.6(2) . . ?
Ag1 Ag8 Ag21 59.56(15) . . ?
Ag1 Ag8 Ag23 65.00(16) . . ?
Ag1 Ag8 Ag51 65.5(2) . . ?
Ag1 Ag8 Ag53 59.7(2) . . ?
Ag1 Ag8 Ag56 59.40(11) . . ?
Ag3 Ag8 Ag51 72.3(2) . . ?
Ag21 Ag8 Ag23 70.79(18) . . ?
Ag56 Ag8 Ag3 73.2(2) . . ?
Ag56 Ag8 Ag21 110.87(18) . . ?
Ag56 Ag8 Ag23 108.23(19) . . ?
Ag56 Ag8 Ag51 123.3(2) . . ?
Ag56 Ag8 Ag53 46.7(3) . . ?
Ag58 Ag8 Ag1 62.18(13) . . ?
Ag58 Ag8 Ag56 62.28(17) . . ?
O79 Ag8 Ag1 129.3(5) . . ?
O79 Ag8 Ag3 64.9(5) . . ?
O79 Ag8 Ag21 142.2(5) . . ?
O79 Ag8 Ag23 81.2(5) . . ?
O79 Ag8 Ag51 102.7(5) . . ?
O79 Ag8 Ag53 141.8(5) . . ?
O79 Ag8 Ag56 101.6(5) . . ?
O79 Ag8 Ag58 154.2(5) . . ?
O83 Ag8 Ag1 140.4(5) . . ?
O83 Ag8 Ag3 133.1(6) . . ?
O83 Ag8 Ag21 80.8(5) . . ?
O83 Ag8 Ag23 103.0(5) . . ?
O83 Ag8 Ag51 85.4(5) . . ?
O83 Ag8 Ag53 114.5(6) . . ?
O83 Ag8 Ag56 148.7(5) . . ?
O83 Ag8 Ag58 102.2(5) . . ?
O83 Ag8 O79 81.3(7) . . ?
P3 Ag11 S24 122.0(7) . . ?
P3 Ag11 O79 119.7(6) . . ?
O79 Ag11 S24 79.9(6) . . ?
Ag1 Ag13 Ag22 118.0(3) . . ?
Ag56 Ag13 Ag1 53.2(2) . . ?
Ag56 Ag13 Ag22 76.2(3) . . ?
S3 Ag13 Ag1 98.1(8) . . ?
S3 Ag13 Ag22 116.2(8) . . ?
S3 Ag13 Ag56 89.2(8) . . ?
S3 Ag13 S25 168.0(11) . . ?
S25 Ag13 Ag1 89.4(8) . . ?
S25 Ag13 Ag22 51.8(8) . . ?
S25 Ag13 Ag56 87.8(8) . . ?
P4 Ag14 S1 144.1(4) . . ?
O93 Ag14 S1 93.1(6) . . ?
O93 Ag14 P4 122.8(6) . . ?
P8 Ag16 S4 141.6(4) . . ?
O47 Ag16 S4 94.3(6) . . ?
O47 Ag16 P8 122.7(6) . . ?
Ag42 Ag19 Ag1 126.9(2) . . ?
S9 Ag19 Ag1 94.4(5) . . ?
S9 Ag19 Ag42 63.9(5) . . ?
S9 Ag19 S19 174.3(8) . . ?
S19 Ag19 Ag1 91.0(6) . . ?
S19 Ag19 Ag42 111.3(6) . . ?
Ag1 Ag21 Ag8 57.78(13) . . ?
S19 Ag21 Ag1 101.2(5) . . ?
S19 Ag21 Ag8 132.5(5) . . ?
S21 Ag21 Ag1 100.4(4) . . ?
S21 Ag21 Ag8 84.1(5) . . ?
S21 Ag21 S19 143.4(7) . . ?
S16 Ag22 Ag5 134.4(4) . . ?
S16 Ag22 Ag13 91.7(4) . . ?
S16 Ag22 S17 89.8(6) . . ?
S16 Ag22 S25 135.3(8) . . ?
S17 Ag22 Ag5 46.7(5) . . ?
S25 Ag22 Ag13 45.9(7) . . ?
P10 Ag22 Ag5 105.4(3) . . ?
P10 Ag22 Ag13 143.5(4) . . ?
P10 Ag22 S16 119.9(4) . . ?
P10 Ag22 S17 143.4(6) . . ?
P10 Ag22 S25 98.2(7) . . ?
P10 Ag22 O99 106.5(5) . . ?
O99 Ag22 Ag5 69.8(5) . . ?
O99 Ag22 Ag13 83.5(5) . . ?
O99 Ag22 S16 99.9(6) . . ?
O99 Ag22 S17 86.9(7) . . ?
O99 Ag22 S25 89.7(8) . . ?
Ag8 Ag23 Ag1 53.60(13) . . ?
S5 Ag23 Ag1 95.2(6) . . ?
S5 Ag23 Ag8 94.9(5) . . ?
S21 Ag23 Ag1 92.4(3) . . ?
S21 Ag23 Ag8 81.6(5) . . ?
S21 Ag23 S5 167.3(8) . . ?
S11 Ag25 Ag1 87.1(9) . . ?
S13 Ag25 Ag1 93.5(9) . . ?
S13 Ag25 S11 150.7(13) . . ?
P23 Ag26 S1 153.4(4) . . ?
S4 Ag28 Ag41 148.2(3) . . ?
S4 Ag28 S24 160.0(6) . . ?
S24 Ag28 Ag41 48.2(5) . . ?
S24A Ag28 S4 175.9(6) . . ?
S16 Ag31 Ag39 110.1(3) . . ?
S16 Ag31 S3 118.6(7) . . ?
P15 Ag31 Ag39 113.6(5) . . ?
P15 Ag31 S3 104.7(8) . . ?
P15 Ag31 S16 135.7(6) . . ?
P15 Ag31 O77 108.1(7) . . ?
O77 Ag31 Ag39 48.8(5) . . ?
O77 Ag31 S3 71.0(8) . . ?
O77 Ag31 S16 95.1(6) . . ?
S1 Ag32 S16 173.9(5) . . ?
S1 Ag32 O61 83.0(5) . . ?
S16 Ag32 O61 93.4(6) . . ?
Ag1 Ag39 Ag31 147.0(2) . . ?
Ag56 Ag39 Ag1 56.67(14) . . ?
Ag56 Ag39 Ag31 97.1(2) . . ?
S5 Ag39 Ag1 96.2(6) . . ?
S5 Ag39 Ag31 116.9(6) . . ?
S5 Ag39 Ag56 132.2(5) . . ?
S5 Ag39 S17 145.2(7) . . ?
S5 Ag39 O77 123.2(7) . . ?
S17 Ag39 Ag1 78.0(6) . . ?
S17 Ag39 Ag31 74.8(6) . . ?
S17 Ag39 Ag56 72.8(5) . . ?
O77 Ag39 Ag1 114.9(5) . . ?
O77 Ag39 Ag31 47.2(5) . . ?
O77 Ag39 Ag56 58.6(5) . . ?
O77 Ag39 S17 89.5(8) . . ?
P6 Ag40 S6 157.1(4) . . ?
S24 Ag41 Ag28 49.3(5) . . ?
S24 Ag41 P11 151.3(8) . . ?
S24 Ag41 O83 101.1(7) . . ?
P11 Ag41 Ag28 116.6(6) . . ?
O83 Ag41 Ag28 82.6(5) . . ?
O83 Ag41 P11 101.1(8) . . ?
S9 Ag42 Ag19 45.5(4) . . ?
S20 Ag42 Ag19 91.6(4) . . ?
S20 Ag42 S9 135.9(5) . . ?
S20 Ag42 S11 85.1(9) . . ?
P1 Ag42 Ag19 136.4(3) . . ?
P1 Ag42 S9 91.3(5) . . ?
P1 Ag42 S11 140.2(8) . . ?
P1 Ag42 S20 128.4(4) . . ?
P1 Ag42 O103 109.2(6) . . ?
O103 Ag42 Ag19 80.3(5) . . ?
O103 Ag42 S9 88.7(7) . . ?
O103 Ag42 S11 85.5(9) . . ?
O103 Ag42 S20 94.1(6) . . ?
P19 Ag43 S20 124.2(7) . . ?
P19 Ag43 O110 104.3(8) . . ?
O110 Ag43 S20 89.7(7) . . ?
P14 Ag47 S4 143.1(3) . . ?
S6 Ag48 Ag60 131.2(3) . . ?
S6 Ag48 S20 176.9(5) . . ?
S6 Ag48 O95 78.9(6) . . ?
S20 Ag48 Ag60 46.2(4) . . ?
S20 Ag48 O95 98.7(6) . . ?
O95 Ag48 Ag60 82.0(5) . . ?
Ag1 Ag49 H39A 75.6 . . ?
S11 Ag49 Ag1 91.4(9) . . ?
S11 Ag49 S25 170.9(12) . . ?
S11 Ag49 H39A 65.5 . . ?
S25 Ag49 Ag1 93.8(8) . . ?
S25 Ag49 H39A 108.6 . . ?
Ag8 Ag51 Ag1 53.23(16) . . ?
S13 Ag51 Ag1 91.6(9) . . ?
S13 Ag51 Ag8 89.2(9) . . ?
S13 Ag51 S23 168.7(13) . . ?
S23 Ag51 Ag1 97.7(9) . . ?
S23 Ag51 Ag8 91.2(8) . . ?
S6 Ag52 O89 93.9(6) . . ?
P2 Ag52 S6 140.1(4) . . ?
P2 Ag52 O89 123.7(6) . . ?
Ag1 Ag53 W25 171.1(6) . . ?
Ag1 Ag53 Ag8 56.6(2) . . ?
Ag8 Ag53 W25 128.3(4) . . ?
Ag56 Ag53 W25 111.2(5) . . ?
Ag56 Ag53 Ag1 63.3(3) . . ?
Ag56 Ag53 Ag8 62.0(3) . . ?
Ag56 Ag53 O86 97.6(6) . . ?
O86 Ag53 W25 44.3(5) . . ?
O86 Ag53 Ag1 140.8(7) . . ?
O86 Ag53 Ag8 84.3(6) . . ?
O103 Ag53 W25 29.7(6) . . ?
O103 Ag53 Ag1 147.0(8) . . ?
O103 Ag53 Ag8 155.8(8) . . ?
O103 Ag53 Ag56 125.7(9) . . ?
O103 Ag53 O86 72.1(8) . . ?
Ag1 Ag56 Ag3 57.72(18) . . ?
Ag1 Ag56 Ag5 61.14(14) . . ?
Ag1 Ag56 Ag8 60.24(11) . . ?
Ag1 Ag56 Ag13 63.8(2) . . ?
Ag1 Ag56 Ag58 60.84(13) . . ?
Ag8 Ag56 Ag3 53.65(18) . . ?
Ag8 Ag56 Ag5 119.97(17) . . ?
Ag8 Ag56 Ag13 112.1(3) . . ?
Ag8 Ag56 Ag58 57.58(15) . . ?
Ag13 Ag56 Ag3 65.5(3) . . ?
Ag39 Ag56 Ag1 68.67(17) . . ?
Ag39 Ag56 Ag5 89.28(19) . . ?
Ag39 Ag56 Ag8 81.27(19) . . ?
Ag53 Ag56 Ag1 68.7(3) . . ?
Ag53 Ag56 Ag8 71.3(4) . . ?
Ag53 Ag56 O77 160.1(6) . . ?
Ag53 Ag56 O80 92.3(5) . . ?
Ag53 Ag56 O99 95.7(6) . . ?
O77 Ag56 Ag1 126.1(5) . . ?
O77 Ag56 Ag3 71.3(5) . . ?
O77 Ag56 Ag5 120.8(5) . . ?
O77 Ag56 Ag8 103.2(5) . . ?
O77 Ag56 Ag13 81.1(5) . . ?
O77 Ag56 Ag39 57.9(5) . . ?
O77 Ag56 Ag58 155.5(5) . . ?
O80 Ag56 Ag1 149.1(5) . . ?
O80 Ag56 Ag3 116.3(5) . . ?
O80 Ag56 Ag5 140.2(5) . . ?
O80 Ag56 Ag8 91.2(5) . . ?
O80 Ag56 Ag13 145.3(5) . . ?
O80 Ag56 Ag39 121.7(5) . . ?
O80 Ag56 Ag58 95.1(5) . . ?
O80 Ag56 O77 68.4(6) . . ?
O99 Ag56 Ag1 133.3(5) . . ?
O99 Ag56 Ag3 146.4(5) . . ?
O99 Ag56 Ag5 72.6(5) . . ?
O99 Ag56 Ag8 157.4(5) . . ?
O99 Ag56 Ag13 90.3(5) . . ?
O99 Ag56 Ag39 119.3(5) . . ?
O99 Ag56 Ag58 109.6(5) . . ?
O99 Ag56 O77 82.6(7) . . ?
O99 Ag56 O80 70.5(7) . . ?
Ag1 Ag58 Ag56 58.10(13) . . ?
Ag8 Ag58 Ag1 60.14(12) . . ?
Ag8 Ag58 Ag56 60.14(15) . . ?
O103 Ag58 Ag1 127.3(6) . . ?
O103 Ag58 Ag8 146.0(6) . . ?
O103 Ag58 Ag56 94.2(6) . . ?
O110 Ag58 Ag1 142.0(6) . . ?
O110 Ag58 Ag8 105.3(6) . . ?
O110 Ag58 Ag56 149.0(6) . . ?
O110 Ag58 O103 85.4(8) . . ?
S20 Ag60 Ag48 49.9(4) . . ?
S20 Ag60 P19 157.2(7) . . ?
S20 Ag60 O110 101.5(7) . . ?
P19 Ag60 Ag48 125.0(7) . . ?
P19 Ag60 O110 100.7(8) . . ?
O110 Ag60 Ag48 90.2(6) . . ?
S24A Ag62 P3 143.0(7) . . ?
S24A Ag62 O79 89.5(7) . . ?
O79 Ag62 P3 101.5(6) . . ?
Ag26 S1 Ag14 121.2(4) . . ?
Ag32 S1 Ag14 103.5(4) . . ?
Ag32 S1 Ag26 100.7(4) . . ?
C333 S1 Ag14 109.5(15) . . ?
C333 S1 Ag26 109.4(15) . . ?
C333 S1 Ag32 111.8(14) . . ?
Ag3 S3 Ag31 125.4(11) . . ?
Ag13 S3 Ag3 91.2(10) . . ?
Ag13 S3 Ag31 96.1(10) . . ?
C191 S3 Ag3 102(2) . . ?
C191 S3 Ag13 107(2) . . ?
C191 S3 Ag31 126(2) . . ?
Ag28 S4 Ag16 101.4(3) . . ?
Ag28 S4 Ag47 103.3(4) . . ?
Ag47 S4 Ag16 119.2(4) . . ?
C129 S4 Ag16 108.4(15) . . ?
C129 S4 Ag28 118.1(15) . . ?
C129 S4 Ag47 107.0(14) . . ?
Ag23 S5 Ag39 97.1(8) . . ?
C125 S5 Ag23 106.7(19) . . ?
C125 S5 Ag39 112(2) . . ?
Ag40 S6 Ag52 101.0(4) . . ?
Ag48 S6 Ag40 105.6(5) . . ?
Ag48 S6 Ag52 109.9(4) . . ?
C411 S6 Ag40 107.8(13) . . ?
C411 S6 Ag48 118.3(10) . . ?
C411 S6 Ag52 112.4(6) . . ?
Ag5 S9 Ag42 122.0(8) . . ?
Ag19 S9 Ag5 94.7(7) . . ?
Ag19 S9 Ag42 70.6(5) . . ?
C99 S9 Ag5 104.9(16) . . ?
C99 S9 Ag19 111.5(17) . . ?
C99 S9 Ag42 133.0(16) . . ?
Ag25 S11 Ag42 122.8(13) . . ?
Ag49 S11 Ag25 99.0(13) . . ?
Ag49 S11 Ag42 87.2(12) . . ?
C201 S11 Ag25 114(2) . . ?
C201 S11 Ag42 122(2) . . ?
C201 S11 Ag49 97(2) . . ?
Ag51 S13 Ag25 102.3(13) . . ?
C251 S13 Ag25 120(3) . . ?
C251 S13 Ag51 109(3) . . ?
Ag31 S16 Ag22 113.0(6) . . ?
Ag32 S16 Ag22 113.0(5) . . ?
Ag32 S16 Ag31 95.6(4) . . ?
C255 S16 Ag22 106.8(17) . . ?
C255 S16 Ag31 113.9(13) . . ?
C255 S16 Ag32 114.5(12) . . ?
Ag5 S17 Ag22 77.9(7) . . ?
Ag5 S17 Ag39 109.5(8) . . ?
Ag39 S17 Ag22 126.8(9) . . ?
C379 S17 Ag5 104(2) . . ?
C379 S17 Ag22 121(2) . . ?
C379 S17 Ag39 107.9(19) . . ?
Ag19 S19 Ag21 95.9(8) . . ?
C43 S19 Ag19 105.6(18) . . ?
C43 S19 Ag21 117(2) . . ?
Ag42 S20 Ag43 117.6(5) . . ?
Ag48 S20 Ag42 106.6(5) . . ?
Ag48 S20 Ag43 100.8(5) . . ?
Ag60 S20 Ag42 130.1(6) . . ?
Ag60 S20 Ag48 83.9(5) . . ?
C131 S20 Ag42 110.3(17) . . ?
C131 S20 Ag43 115.8(19) . . ?
C131 S20 Ag48 103.9(17) . . ?
C131 S20 Ag60 114.1(18) . . ?
Ag23 S21 Ag21 95.0(4) . . ?
C13 S21 Ag21 136(2) . . ?
C13 S21 Ag23 94(3) . . ?
Ag51 S23 Ag3 85.2(11) . . ?
C101 S23 Ag3 100(3) . . ?
C101 S23 Ag51 108(3) . . ?
Ag28 S24 Ag11 107.1(7) . . ?
Ag41 S24 Ag11 135.1(8) . . ?
Ag41 S24 Ag28 82.5(7) . . ?
C219 S24 Ag11 113.5(15) . . ?
C219 S24 Ag28 112.0(15) . . ?
C219 S24 Ag41 102.1(13) . . ?
Ag1B S24A Ag62 126.4(9) . . ?
Ag28 S24A Ag1B 115.6(9) . . ?
Ag28 S24A Ag62 91.1(8) . . ?
C55 S24A Ag1B 99(2) . . ?
C55 S24A Ag28 116(3) . . ?
C55 S24A Ag62 111(3) . . ?
Ag13 S25 Ag22 82.4(9) . . ?
Ag13 S25 Ag49 99.8(12) . . ?
Ag49 S25 Ag22 124.9(12) . . ?
C155 S25 Ag13 111(2) . . ?
C155 S25 Ag22 148(2) . . ?
C155 S25 Ag49 83(2) . . ?
C215 P1 Ag42 112.2(13) . . ?
C285 P1 Ag42 119.1(11) . . ?
C285 P1 C215 104.9(17) . . ?
C305 P1 Ag42 112.6(15) . . ?
C305 P1 C215 103(2) . . ?
C305 P1 C285 103.6(18) . . ?
C69 P2 Ag52 116.6(18) . . ?
C69 P2 C79 104(2) . . ?
C79 P2 Ag52 116.9(15) . . ?
C365 P2 Ag52 112.4(14) . . ?
C365 P2 C69 105(2) . . ?
C365 P2 C79 100.1(19) . . ?
C141 P3 Ag11 117.0(17) . . ?
C141 P3 Ag62 101.8(17) . . ?
C141 P3 C85 105(2) . . ?
C85 P3 Ag11 106.1(17) . . ?
C85 P3 Ag62 114.8(18) . . ?
C371 P3 Ag11 106.9(16) . . ?
C371 P3 Ag62 111.8(16) . . ?
C371 P3 C141 108(2) . . ?
C371 P3 C85 114(2) . . ?
C217 P4 Ag14 111.3(13) . . ?
C217 P4 C109 101.7(17) . . ?
C217 P4 C325 103.9(16) . . ?
C109 P4 Ag14 124.6(12) . . ?
C325 P4 Ag14 110.1(11) . . ?
C325 P4 C109 103.1(15) . . ?
C223 P6 Ag40 115.5(12) . . ?
C223 P6 C307 102.5(19) . . ?
C223 P6 C175 104.7(16) . . ?
C307 P6 Ag40 115.9(15) . . ?
C307 P6 C175 102.2(18) . . ?
C175 P6 Ag40 114.2(12) . . ?
C237 P8 Ag16 107.6(14) . . ?
C237 P8 C315 104.7(19) . . ?
C237 P8 C179 106.4(17) . . ?
C315 P8 Ag16 120.1(13) . . ?
C179 P8 Ag16 112.6(11) . . ?
C179 P8 C315 104.4(15) . . ?
C15 P10 Ag22 117.3(13) . . ?
C15 P10 C75 109.1(18) . . ?
C15 P10 C323 99.4(16) . . ?
C75 P10 Ag22 116.0(15) . . ?
C75 P10 C323 100.7(16) . . ?
C323 P10 Ag22 111.9(10) . . ?
C73 P11 Ag1B 112.5(19) . . ?
C73 P11 Ag41 118.4(15) . . ?
C73 P11 C207 111(3) . . ?
C207 P11 Ag1B 112(3) . . ?
C207 P11 Ag41 121(3) . . ?
C423 P11 Ag1B 120.6(13) . . ?
C423 P11 Ag41 101.3(12) . . ?
C423 P11 C73 98(2) . . ?
C423 P11 C207 102(3) . . ?
C231 P14 Ag47 113.6(10) . . ?
C231 P14 C241 105.4(18) . . ?
C241 P14 Ag47 108.1(14) . . ?
C283 P14 Ag47 120.1(14) . . ?
C283 P14 C231 105.1(17) . . ?
C283 P14 C241 103.2(19) . . ?
C121 P15 Ag31 115.0(18) . . ?
C121 P15 C173 96(2) . . ?
C271 P15 Ag31 119.1(11) . . ?
C271 P15 C121 98(2) . . ?
C271 P15 C173 117(2) . . ?
C173 P15 Ag31 109.3(17) . . ?
C263 P19 Ag43 100.0(16) . . ?
C263 P19 Ag60 112.1(12) . . ?
C263 P19 C331 113(3) . . ?
C263 P19 C193 100(3) . . ?
C331 P19 Ag43 114(3) . . ?
C331 P19 Ag60 121(3) . . ?
C331 P19 C193 105(3) . . ?
C193 P19 Ag43 124(2) . . ?
C193 P19 Ag60 102(2) . . ?
C253 P23 Ag26 113.4(14) . . ?
C253 P23 C2 101(2) . . ?
C253 P23 C83 106(2) . . ?
C2 P23 Ag26 117.4(15) . . ?
C2 P23 C83 106(2) . . ?
C83 P23 Ag26 111.2(15) . . ?
O67 Si3 O80 108.2(11) . . ?
O67 Si3 O86 107.1(11) . . ?
O67 Si3 O101 107.5(11) . . ?
O80 Si3 O86 114.3(11) . . ?
O80 Si3 O101 109.1(10) . . ?
O86 Si3 O101 110.5(11) . . ?
W18 O47 Ag16 137.3(11) . . ?
W23 O49 W29 121.9(11) . . ?
W23 O51 W17 148.6(11) . . ?
W30 O53 W22 139.9(11) . . ?
W30 O55 W16 147.9(12) . . ?
W18 O57 W22 159.1(13) . . ?
W25 O59 W16 161.4(12) . . ?
W16 O61 Ag32 121.7(10) . . ?
W22 O61 W16 121.6(11) . . ?
W22 O61 Ag32 113.0(9) . . ?
W29 O65 W30 122.8(11) . . ?
W23 O67 W30 91.7(7) . . ?
W29 O67 W23 91.7(7) . . ?
W29 O67 W30 91.4(7) . . ?
Si3 O67 W23 123.7(10) . . ?
Si3 O67 W29 126.6(11) . . ?
Si3 O67 W30 122.0(11) . . ?
W23 O71 W30 124.1(11) . . ?
W17 O73 W18 118.7(11) . . ?
W22 O77 Ag31 114.8(10) . . ?
W22 O77 Ag39 156.8(12) . . ?
W22 O77 Ag56 108.5(9) . . ?
Ag31 O77 Ag39 83.9(7) . . ?
Ag31 O77 Ag56 129.2(9) . . ?
Ag39 O77 Ag56 63.6(5) . . ?
W18 O79 Ag8 113.8(9) . . ?
W18 O79 Ag11 123.2(10) . . ?
W18 O79 Ag62 123.2(9) . . ?
Ag8 O79 Ag11 122.6(8) . . ?
Ag8 O79 Ag62 116.4(8) . . ?
W16 O80 Ag56 92.6(7) . . ?
W22 O80 W16 92.6(7) . . ?
W22 O80 Ag56 96.6(7) . . ?
Si3 O80 W16 126.0(10) . . ?
Si3 O80 W22 131.6(11) . . ?
Si3 O80 Ag56 108.2(10) . . ?
W29 O81 W25 150.2(12) . . ?
W17 O83 Ag1B 136.2(11) . . ?
W17 O83 Ag8 115.2(10) . . ?
W17 O83 Ag41 124.9(10) . . ?
Ag1B O83 Ag8 107.3(8) . . ?
Ag8 O83 Ag41 110.5(8) . . ?
W25 O86 Ag53 84.8(7) . . ?
W27 O86 W25 95.5(8) . . ?
W27 O86 Ag53 106.6(9) . . ?
Si3 O86 W25 124.9(11) . . ?
Si3 O86 W27 130.8(11) . . ?
Si3 O86 Ag53 104.2(10) . . ?
W23 O87 W18 142.5(11) . . ?
W27 O89 Ag52 105.7(10) . . ?
W22 O93 Ag14 122.4(11) . . ?
W25 O95 Ag48 115.4(10) . . ?
W27 O95 W25 117.1(11) . . ?
W27 O95 Ag48 119.6(10) . . ?
W27 O97 W17 161.0(13) . . ?
W16 O99 Ag22 129.5(10) . . ?
W16 O99 Ag56 112.3(9) . . ?
Ag56 O99 Ag22 109.9(8) . . ?
W18 O101 W17 95.4(7) . . ?
Si3 O101 W17 128.3(10) . . ?
Si3 O101 W18 130.5(11) . . ?
W25 O103 Ag42 128.2(11) . . ?
W25 O103 Ag53 114.2(12) . . ?
W25 O103 Ag58 115.2(11) . . ?
Ag42 O103 Ag58 110.3(9) . . ?
Ag53 O103 Ag42 116.8(10) . . ?
W29 O106 W27 139.3(13) . . ?
W27 O110 Ag43 128.7(12) . . ?
W27 O110 Ag58 112.1(11) . . ?
W27 O110 Ag60 109.2(11) . . ?
Ag58 O110 Ag43 114.6(10) . . ?
H21A C213 H21B 108.7 . . ?
C109 C213 H21A 110.5 . . ?
C109 C213 H21B 110.5 . . ?
C109 C213 C315 106(3) . . ?
C315 C213 H21A 110.5 . . ?
C315 C213 H21B 110.5 . . ?
H10E C107 H10F 109.4 . . ?
H10E C107 H10G 109.6 . . ?
H10F C107 H10G 109.4 . . ?
C55 C107 H10E 102.7 . . ?
C55 C107 H10F 112.4 . . ?
C55 C107 H10G 113.1 . . ?
P1 C215 H21C 108.1 . . ?
P1 C215 H21D 108.1 . . ?
H21C C215 H21D 107.3 . . ?
C259 C215 P1 117(3) . . ?
C259 C215 H21C 108.1 . . ?
C259 C215 H21D 108.1 . . ?
C217 C27 H27 122.0 . . ?
C281 C27 H27 122.0 . . ?
C281 C27 C217 116(4) . . ?
C27 C217 P4 122(3) . . ?
C221 C217 P4 120(3) . . ?
C221 C217 C27 118(4) . . ?
P4 C109 H10H 109.8 . . ?
P4 C109 H10I 109.8 . . ?
C213 C109 P4 109(2) . . ?
C213 C109 H10H 109.8 . . ?
C213 C109 H10I 109.8 . . ?
H10H C109 H10I 108.3 . . ?
S24 C219 H219 110.8 . . ?
C19 C219 S24 104.5(9) . . ?
C19 C219 H219 110.8 . . ?
C381 C219 S24 104.5(9) . . ?
C381 C219 H219 110.8 . . ?
C381 C219 C19 115.0(11) . . ?
S24A C55 H55 114.2 . . ?
C107 C55 S24A 114(5) . . ?
C107 C55 H55 114.2 . . ?
C107 C55 C419 99(5) . . ?
C419 C55 S24A 100(4) . . ?
C419 C55 H55 114.2 . . ?
C217 C221 H221 117.6 . . ?
C31 C221 C217 125(4) . . ?
C31 C221 H221 117.6 . . ?
C83 C111 H111 125.2 . . ?
C199 C111 H111 125.2 . . ?
C199 C111 C83 110(5) . . ?
C7 C223 P6 123.3(18) . . ?
C7 C223 C57 120.0 . . ?
C57 C223 P6 116.6(18) . . ?
C223 C7 H7 120.0 . . ?
C223 C7 C225 120.0 . . ?
C225 C7 H7 120.0 . . ?
C7 C225 H225 120.0 . . ?
C113 C225 C7 120.0 . . ?
C113 C225 H225 120.0 . . ?
C225 C113 H113 120.0 . . ?
C227 C113 C225 120.0 . . ?
C227 C113 H113 120.0 . . ?
C113 C227 H227 120.0 . . ?
C113 C227 C57 120.0 . . ?
C57 C227 H227 120.0 . . ?
C223 C57 H57 120.0 . . ?
C227 C57 C223 120.0 . . ?
C227 C57 H57 120.0 . . ?
C249 C229 H229 125.5 . . ?
C149 C229 H229 125.5 . . ?
C149 C229 C249 109(6) . . ?
H11D C115 H11E 109.5 . . ?
H11D C115 H11F 109.5 . . ?
H11E C115 H11F 109.5 . . ?
C201 C115 H11D 112.1 . . ?
C201 C115 H11E 107.6 . . ?
C201 C115 H11F 108.7 . . ?
C29 C231 P14 118.5(17) . . ?
C29 C231 C59 120.0 . . ?
C59 C231 P14 121.5(17) . . ?
C231 C29 H29 120.0 . . ?
C233 C29 C231 120.0 . . ?
C233 C29 H29 120.0 . . ?
C29 C233 H233 120.0 . . ?
C117 C233 C29 120.0 . . ?
C117 C233 H233 120.0 . . ?
C233 C117 H117 120.0 . . ?
C233 C117 C235 120.0 . . ?
C235 C117 H117 120.0 . . ?
C117 C235 H235 120.0 . . ?
C59 C235 C117 120.0 . . ?
C59 C235 H235 120.0 . . ?
C231 C59 H59 120.0 . . ?
C235 C59 C231 120.0 . . ?
C235 C59 H59 120.0 . . ?
C279 C237 P8 121(3) . . ?
C279 C237 C417 118(4) . . ?
C417 C237 P8 120(3) . . ?
C153 C119 H119 119.9 . . ?
C3 C119 H119 119.9 . . ?
C3 C119 C153 120(4) . . ?
H23A C239 H23B 109.4 . . ?
H23A C239 H23C 109.5 . . ?
H23B C239 H23C 109.4 . . ?
C13 C239 H23A 108.3 . . ?
C13 C239 H23B 112.2 . . ?
C13 C239 H23C 107.9 . . ?
P10 C15 H15I 109.5 . . ?
P10 C15 H15J 109.5 . . ?
H15I C15 H15J 108.1 . . ?
C259 C15 P10 111(3) . . ?
C259 C15 H15I 109.5 . . ?
C259 C15 H15J 109.5 . . ?
C35 C241 P14 120(4) . . ?
C35 C241 C317 121(4) . . ?
C317 C241 P14 119(4) . . ?
C243 C121 P15 117(2) . . ?
C243 C121 C247 120.0 . . ?
C247 C121 P15 123(2) . . ?
C121 C243 H243 120.0 . . ?
C121 C243 C61 120.0 . . ?
C61 C243 H243 120.0 . . ?
C243 C61 H61 120.0 . . ?
C245 C61 C243 120.0 . . ?
C245 C61 H61 120.0 . . ?
C61 C245 H245 120.0 . . ?
C61 C245 C123 120.0 . . ?
C123 C245 H245 120.0 . . ?
C245 C123 H123 120.0 . . ?
C245 C123 C247 120.0 . . ?
C247 C123 H123 120.0 . . ?
C121 C247 H247 120.0 . . ?
C123 C247 C121 120.0 . . ?
C123 C247 H247 120.0 . . ?
C221 C31 H31 122.4 . . ?
C221 C31 C257 115(4) . . ?
C257 C31 H31 122.4 . . ?
C229 C249 H249 116.5 . . ?
C335 C249 C229 127(6) . . ?
C335 C249 H249 116.5 . . ?
S5 C125 H125 102.9 . . ?
C95 C125 S5 119(4) . . ?
C95 C125 H125 102.9 . . ?
C95 C125 C209 116(6) . . ?
C209 C125 S5 110(4) . . ?
C209 C125 H125 102.9 . . ?
S13 C251 H251 113.3 . . ?
C127 C251 S13 99.9(8) . . ?
C127 C251 H251 113.3 . . ?
C127 C251 C405 115.4(12) . . ?
C405 C251 S13 99.8(8) . . ?
C405 C251 H251 113.3 . . ?
H63A C63 H63B 109.5 . . ?
H63A C63 H63C 109.4 . . ?
H63B C63 H63C 109.6 . . ?
C43 C63 H63A 109.1 . . ?
C43 C63 H63B 111.5 . . ?
C43 C63 H63C 107.7 . . ?
P23 C253 H25D 108.4 . . ?
P23 C253 H25E 108.4 . . ?
H25D C253 H25E 107.5 . . ?
C309 C253 P23 116(3) . . ?
C309 C253 H25D 108.4 . . ?
C309 C253 H25E 108.4 . . ?
C251 C127 H12E 111.6 . . ?
C251 C127 H12F 109.2 . . ?
C251 C127 H12G 107.6 . . ?
H12E C127 H12F 109.5 . . ?
H12E C127 H12G 109.5 . . ?
H12F C127 H12G 109.5 . . ?
S16 C255 H255 101.1 . . ?
C313 C255 S16 118(3) . . ?
C313 C255 H255 101.1 . . ?
C205 C255 S16 114(2) . . ?
C205 C255 H255 101.1 . . ?
C205 C255 C313 117.5(12) . . ?
C65 C2 P23 119(4) . . ?
C169 C2 P23 120(4) . . ?
C169 C2 C65 119(4) . . ?
C31 C257 H257 120.1 . . ?
C281 C257 C31 120(4) . . ?
C281 C257 H257 120.1 . . ?
S4 C129 H129 108.6 . . ?
C357 C129 S4 100(2) . . ?
C357 C129 H129 108.6 . . ?
C203 C129 S4 106(2) . . ?
C203 C129 H129 108.6 . . ?
C203 C129 C357 124(3) . . ?
C215 C259 C15 112(3) . . ?
C215 C259 H25F 109.2 . . ?
C215 C259 H25G 109.2 . . ?
C15 C259 H25F 109.2 . . ?
C15 C259 H25G 109.2 . . ?
H25F C259 H25G 107.9 . . ?
C2 C65 H65 121.7 . . ?
C167 C65 C2 117(5) . . ?
C167 C65 H65 121.7 . . ?
C199 C261 H261 125.7 . . ?
C199 C261 C401 109(5) . . ?
C401 C261 H261 125.7 . . ?
S20 C131 H131 108.5 . . ?
C91 C131 S20 107(4) . . ?
C91 C131 H131 108.5 . . ?
C49 C131 S20 111(4) . . ?
C49 C131 H131 108.5 . . ?
C49 C131 C91 114(5) . . ?
C33 C263 P19 119.9(4) . . ?
C33 C263 C67 120.0 . . ?
C67 C263 P19 119.9(4) . . ?
C263 C33 H33 120.0 . . ?
C263 C33 C265 120.0 . . ?
C265 C33 H33 120.0 . . ?
C33 C265 H265 120.0 . . ?
C33 C265 C133 120.0 . . ?
C133 C265 H265 120.0 . . ?
C265 C133 H133 120.0 . . ?
C265 C133 C267 120.0 . . ?
C267 C133 H133 120.0 . . ?
C133 C267 H267 120.0 . . ?
C133 C267 C67 120.0 . . ?
C67 C267 H267 120.0 . . ?
C263 C67 H67 120.0 . . ?
C267 C67 C263 120.0 . . ?
C267 C67 H67 120.0 . . ?
C291 C269 H269 119.7 . . ?
C403 C269 H269 119.7 . . ?
C403 C269 C291 121(5) . . ?
C271 C135 H135 120.0 . . ?
C271 C135 C275 120.0 . . ?
C275 C135 H135 120.0 . . ?
C135 C271 P15 120.1(4) . . ?
C135 C271 C17 120.0 . . ?
C17 C271 P15 119.9(4) . . ?
C271 C17 H17 120.0 . . ?
C273 C17 C271 120.0 . . ?
C273 C17 H17 120.0 . . ?
C17 C273 H273 120.0 . . ?
C17 C273 C137 120.0 . . ?
C137 C273 H273 120.0 . . ?
C273 C137 H137 120.0 . . ?
C275 C137 C273 120.0 . . ?
C275 C137 H137 120.0 . . ?
C135 C275 O14 113(3) . 1_545 ?
C137 C275 O14 111(3) . 1_545 ?
C137 C275 C135 120.0 . . ?
C335 C69 P2 115(4) . . ?
C21 C69 P2 126(4) . . ?
C21 C69 C335 117(5) . . ?
H27G C277 H27H 108.4 . . ?
C283 C277 H27G 110.0 . . ?
C283 C277 H27H 110.0 . . ?
C79 C277 H27G 110.0 . . ?
C79 C277 H27H 110.0 . . ?
C79 C277 C283 108(3) . . ?
C141 C139 H139 118.6 . . ?
C141 C139 C89 123(5) . . ?
C89 C139 H139 118.6 . . ?
C237 C279 H279 122.2 . . ?
C237 C279 C415 116(4) . . ?
C415 C279 H279 122.2 . . ?
C241 C35 H35 119.5 . . ?
C241 C35 C403 121(5) . . ?
C403 C35 H35 119.5 . . ?
C27 C281 H281 117.4 . . ?
C257 C281 C27 125(4) . . ?
C257 C281 H281 117.3 . . ?
C139 C141 P3 125(4) . . ?
C139 C141 C343 121(4) . . ?
C343 C141 P3 114(3) . . ?
P14 C283 H28A 107.7 . . ?
P14 C283 H28B 107.7 . . ?
C277 C283 P14 118(3) . . ?
C277 C283 H28A 107.7 . . ?
C277 C283 H28B 107.7 . . ?
H28A C283 H28B 107.1 . . ?
C301 C71 H71 121.9 . . ?
C301 C71 C417 116(4) . . ?
C417 C71 H71 121.9 . . ?
C143 C285 P1 123.6(18) . . ?
C143 C285 C145 120.0 . . ?
C145 C285 P1 116.4(18) . . ?
C285 C143 H143 120.0 . . ?
C285 C143 C287 120.0 . . ?
C287 C143 H143 120.0 . . ?
C143 C287 H287 120.0 . . ?
C9 C287 C143 120.0 . . ?
C9 C287 H287 120.0 . . ?
C287 C9 H9 120.0 . . ?
C287 C9 C289 120.0 . . ?
C289 C9 H9 120.0 . . ?
C9 C289 H289 120.0 . . ?
C145 C289 C9 120.0 . . ?
C145 C289 H289 120.0 . . ?
C285 C145 H145 120.0 . . ?
C289 C145 C285 120.0 . . ?
C289 C145 H145 120.0 . . ?
C269 C291 H291 120.5 . . ?
C269 C291 C317 119(5) . . ?
C317 C291 H291 120.5 . . ?
C293 C73 P11 120.0(4) . . ?
C293 C73 C297 120.0 . . ?
C297 C73 P11 120.0(4) . . ?
C73 C293 H293 120.0 . . ?
C147 C293 C73 120.0 . . ?
C147 C293 H293 120.0 . . ?
C293 C147 H147 120.0 . . ?
C295 C147 C293 120.0 . . ?
C295 C147 H147 120.0 . . ?
C147 C295 H295 120.0 . . ?
C37 C295 C147 120.0 . . ?
C37 C295 H295 120.0 . . ?
C295 C37 H37 120.0 . . ?
C295 C37 C297 120.0 . . ?
C297 C37 H37 120.0 . . ?
C73 C297 H297 120.0 . . ?
C37 C297 C73 120.0 . . ?
C37 C297 H297 120.0 . . ?
C229 C149 H149 117.4 . . ?
C229 C149 C21 125(6) . . ?
C21 C149 H149 117.4 . . ?
H29A C299 H29B 109.5 . . ?
H29A C299 H29C 109.5 . . ?
H29B C299 H29C 109.4 . . ?
C379 C299 H29A 109.9 . . ?
C379 C299 H29B 109.5 . . ?
C379 C299 H29C 109.1 . . ?
C345 C75 P10 124(3) . . ?
C345 C75 C349 121(4) . . ?
C349 C75 P10 115(3) . . ?
C71 C301 H301 118.8 . . ?
C415 C301 C71 122(5) . . ?
C415 C301 H301 118.8 . . ?
H15K C151 H15L 109.5 . . ?
H15K C151 H15M 109.5 . . ?
H15L C151 H15M 109.4 . . ?
C43 C151 H15K 108.5 . . ?
C43 C151 H15L 110.2 . . ?
C43 C151 H15M 109.7 . . ?
H30C C303 H30D 109.7 . . ?
H30C C303 H30E 109.6 . . ?
H30D C303 H30E 109.3 . . ?
C191 C303 H30C 109.2 . . ?
C191 C303 H30D 109.3 . . ?
C191 C303 H30E 109.7 . . ?
C219 C19 H19D 119.8 . . ?
C219 C19 H19E 94.8 . . ?
C219 C19 H19F 112.7 . . ?
H19D C19 H19E 109.4 . . ?
H19D C19 H19F 109.4 . . ?
H19E C19 H19F 109.5 . . ?
C153 C305 P1 123(3) . . ?
C383 C305 P1 120(3) . . ?
C383 C305 C153 116(4) . . ?
C119 C153 C305 115(4) . . ?
C119 C153 H153 122.3 . . ?
C305 C153 H153 122.3 . . ?
P6 C307 H30F 109.7 . . ?
P6 C307 H30G 109.7 . . ?
H30F C307 H30G 108.2 . . ?
C309 C307 P6 110(3) . . ?
C309 C307 H30F 109.7 . . ?
C309 C307 H30G 109.7 . . ?
H77A C77 H77B 109.4 . . ?
H77A C77 H77C 109.5 . . ?
H77B C77 H77C 109.5 . . ?
C99 C77 H77A 109.4 . . ?
C99 C77 H77B 109.0 . . ?
C99 C77 H77C 110.1 . . ?
C253 C309 C307 113(3) . . ?
C253 C309 H30H 109.0 . . ?
C253 C309 H30I 109.0 . . ?
C307 C309 H30H 109.0 . . ?
C307 C309 H30I 109.0 . . ?
H30H C309 H30I 107.8 . . ?
S25 C155 H155 111.0 . . ?
C51 C155 S25 104(6) . . ?
C51 C155 H155 111.0 . . ?
C51 C155 C409 118.9(11) . . ?
C409 C155 S25 99.9(8) . . ?
C409 C155 H155 111.0 . . ?
H31A C311 H31B 109.4 . . ?
H31A C311 H31C 109.5 . . ?
H31B C311 H31C 109.5 . . ?
C101 C311 H31A 109.3 . . ?
C101 C311 H31B 109.7 . . ?
C101 C311 H31C 109.4 . . ?
H39A C39 H39B 109.5 . . ?
H39A C39 H39C 109.5 . . ?
H39B C39 H39C 109.4 . . ?
C201 C39 H39A 111.5 . . ?
C201 C39 H39B 110.4 . . ?
C201 C39 H39C 106.5 . . ?
C255 C313 H31D 108.9 . . ?
C255 C313 H31E 114.5 . . ?
C255 C313 H31F 105.1 . . ?
H31D C313 H31E 109.4 . . ?
H31D C313 H31F 109.5 . . ?
H31E C313 H31F 109.4 . . ?
H15N C157 H15O 109.5 . . ?
H15N C157 H15P 109.4 . . ?
H15O C157 H15P 109.4 . . ?
C13 C157 H15N 116.5 . . ?
C13 C157 H15O 110.8 . . ?
C13 C157 H15P 100.9 . . ?
P8 C315 H31G 109.6 . . ?
P8 C315 H31H 109.6 . . ?
C213 C315 P8 110(3) . . ?
C213 C315 H31G 109.6 . . ?
C213 C315 H31H 109.6 . . ?
H31G C315 H31H 108.1 . . ?
P2 C79 H79A 108.8 . . ?
P2 C79 H79B 108.8 . . ?
C277 C79 P2 114(3) . . ?
C277 C79 H79A 108.8 . . ?
C277 C79 H79B 108.8 . . ?
H79A C79 H79B 107.7 . . ?
C241 C317 C291 117(5) . . ?
C241 C317 H317 121.7 . . ?
C291 C317 H317 121.7 . . ?
C319 C159 H159 120.0 . . ?
C319 C159 C323 120.0 . . ?
C323 C159 H159 120.0 . . ?
C159 C319 H319 120.0 . . ?
C159 C319 C5 120.0 . . ?
C5 C319 H319 120.0 . . ?
C319 C5 H5 120.0 . . ?
C321 C5 C319 120.0 . . ?
C321 C5 H5 120.0 . . ?
C5 C321 H321 120.0 . . ?
C5 C321 C161 120.0 . . ?
C161 C321 H321 120.0 . . ?
C321 C161 H161 120.0 . . ?
C323 C161 C321 120.0 . . ?
C323 C161 H161 120.0 . . ?
C159 C323 P10 123.5(14) . . ?
C161 C323 P10 116.5(14) . . ?
C161 C323 C159 120.0 . . ?
C345 C81 H81 122.2 . . ?
C345 C81 C87 116(4) . . ?
C87 C81 H81 122.2 . . ?
C163 C325 P4 118.4(16) . . ?
C163 C325 C165 120.0 . . ?
C165 C325 P4 121.5(16) . . ?
C325 C163 H163 120.0 . . ?
C327 C163 C325 120.0 . . ?
C327 C163 H163 120.0 . . ?
C163 C327 H327 120.0 . . ?
C163 C327 C41 120.0 . . ?
C41 C327 H327 120.0 . . ?
C327 C41 H41 120.0 . . ?
C327 C41 C329 120.0 . . ?
C329 C41 H41 120.0 . . ?
C41 C329 H329 120.0 . . ?
C41 C329 C165 120.0 . . ?
C165 C329 H329 120.0 . . ?
C325 C165 H165 120.0 . . ?
C329 C165 C325 120.0 . . ?
C329 C165 H165 120.0 . . ?
P19 C331 H33D 107.5 . . ?
P19 C331 H33E 107.5 . . ?
H33D C331 H33E 107.0 . . ?
C171 C331 P19 119(6) . . ?
C171 C331 H33D 107.5 . . ?
C171 C331 H33E 107.5 . . ?
C111 C83 P23 122(4) . . ?
C25 C83 P23 115(4) . . ?
C25 C83 C111 122(5) . . ?
S1 C333 H333 106.5 . . ?
C395 C333 S1 110(3) . . ?
C395 C333 H333 106.5 . . ?
C397 C333 S1 114(3) . . ?
C397 C333 H333 106.5 . . ?
C397 C333 C395 113(4) . . ?
C65 C167 H167 119.4 . . ?
C65 C167 C393 121(5) . . ?
C393 C167 H167 119.4 . . ?
C249 C335 C69 116(6) . . ?
C249 C335 H335 122.0 . . ?
C69 C335 H335 122.0 . . ?
C69 C21 H21 117.3 . . ?
C149 C21 C69 125(6) . . ?
C149 C21 H21 117.3 . . ?
C169 C337 H337 119.4 . . ?
C393 C337 H337 119.4 . . ?
C393 C337 C169 121(5) . . ?
C2 C169 C337 120(5) . . ?
C2 C169 H169 119.9 . . ?
C337 C169 H169 119.9 . . ?
C341 C339 H339 120.0 . . ?
C343 C339 H339 120.0 . . ?
C343 C339 C341 120(4) . . ?
P3 C85 H85A 111.8 . . ?
P3 C85 H85B 111.8 . . ?
H85A C85 H85B 109.5 . . ?
C399 C85 P3 100(3) . . ?
C399 C85 H85A 111.8 . . ?
C399 C85 H85B 111.8 . . ?
C339 C341 H341 121.1 . . ?
C339 C341 C89 118(4) . . ?
C89 C341 H341 121.1 . . ?
C331 C171 H17G 110.0 . . ?
C331 C171 H17H 110.0 . . ?
H17G C171 H17H 108.4 . . ?
C207 C171 C331 108(7) . . ?
C207 C171 H17G 110.0 . . ?
C207 C171 H17H 110.0 . . ?
C141 C343 H343 121.5 . . ?
C339 C343 C141 117(4) . . ?
C339 C343 H343 121.5 . . ?
S19 C43 H43 117.4 . . ?
C63 C43 S19 99.7(8) . . ?
C63 C43 H43 117.4 . . ?
C151 C43 S19 100.0(8) . . ?
C151 C43 C63 102(7) . . ?
C151 C43 H43 117.4 . . ?
C75 C345 C81 126(4) . . ?
C75 C345 H345 117.1 . . ?
C81 C345 H345 117.1 . . ?
P15 C173 H17I 111.2 . . ?
P15 C173 H17J 111.2 . . ?
H17I C173 H17J 109.1 . . ?
C399 C173 P15 103(3) . . ?
C399 C173 H17I 111.2 . . ?
C399 C173 H17J 111.2 . . ?
C87 C347 H347 118.1 . . ?
C349 C347 H347 118.1 . . ?
C349 C347 C87 124(4) . . ?
C81 C87 C347 118(4) . . ?
C81 C87 H87 121.0 . . ?
C347 C87 H87 121.0 . . ?
C75 C349 C347 116(4) . . ?
C75 C349 H349 122.2 . . ?
C347 C349 H349 122.2 . . ?
C351 C175 P6 120.9(18) . . ?
C351 C175 C355 120.0 . . ?
C355 C175 P6 119.0(18) . . ?
C175 C351 H351 120.0 . . ?
C175 C351 C11 120.0 . . ?
C11 C351 H351 120.0 . . ?
C351 C11 H11 120.0 . . ?
C353 C11 C351 120.0 . . ?
C353 C11 H11 120.0 . . ?
C11 C353 H353 120.0 . . ?
C177 C353 C11 120.0 . . ?
C177 C353 H353 120.0 . . ?
C353 C177 H177 120.0 . . ?
C355 C177 C353 120.0 . . ?
C355 C177 H177 120.0 . . ?
C175 C355 H355 120.0 . . ?
C177 C355 C175 120.0 . . ?
C177 C355 H355 120.0 . . ?
C139 C89 C341 121(4) . . ?
C139 C89 H89 119.5 . . ?
C341 C89 H89 119.5 . . ?
C129 C357 H35M 102.8 . . ?
C129 C357 H35N 113.4 . . ?
C129 C357 H35O 111.4 . . ?
H35M C357 H35N 106.8 . . ?
H35M C357 H35O 110.3 . . ?
H35N C357 H35O 111.6 . . ?
C359 C179 P8 125.2(16) . . ?
C359 C179 C363 120.0 . . ?
C363 C179 P8 114.8(16) . . ?
C179 C359 H359 120.0 . . ?
C179 C359 C45 120.0 . . ?
C45 C359 H359 120.0 . . ?
C359 C45 H45 120.0 . . ?
C361 C45 C359 120.0 . . ?
C361 C45 H45 120.0 . . ?
C45 C361 H361 120.0 . . ?
C181 C361 C45 120.0 . . ?
C181 C361 H361 120.0 . . ?
C361 C181 H181 120.0 . . ?
C363 C181 C361 120.0 . . ?
C363 C181 H181 120.0 . . ?
C179 C363 H363 120.0 . . ?
C181 C363 C179 120.0 . . ?
C181 C363 H363 120.0 . . ?
C131 C91 H91A 109.6 . . ?
C131 C91 H91B 109.4 . . ?
C131 C91 H91C 109.4 . . ?
H91A C91 H91B 109.5 . . ?
H91A C91 H91C 109.5 . . ?
H91B C91 H91C 109.5 . . ?
C183 C365 P2 120(2) . . ?
C183 C365 C185 120.0 . . ?
C185 C365 P2 119(2) . . ?
C365 C183 H183 120.0 . . ?
C367 C183 C365 120.0 . . ?
C367 C183 H183 120.0 . . ?
C183 C367 H367 120.0 . . ?
C183 C367 C23 120.0 . . ?
C23 C367 H367 120.0 . . ?
C367 C23 H23 120.0 . . ?
C369 C23 C367 120.0 . . ?
C369 C23 H23 120.0 . . ?
C23 C369 H369 120.0 . . ?
C23 C369 C185 120.0 . . ?
C185 C369 H369 120.0 . . ?
C365 C185 H185 120.0 . . ?
C369 C185 C365 120.0 . . ?
C369 C185 H185 120.0 . . ?
C93 C371 P3 122(3) . . ?
C93 C371 C47 120.0 . . ?
C47 C371 P3 118(3) . . ?
C371 C93 H93 120.0 . . ?
C371 C93 C373 120.0 . . ?
C373 C93 H93 120.0 . . ?
C93 C373 H373 120.0 . . ?
C187 C373 C93 120.0 . . ?
C187 C373 H373 120.0 . . ?
C373 C187 H187 120.0 . . ?
C373 C187 C375 120.0 . . ?
C375 C187 H187 120.0 . . ?
C187 C375 H375 120.0 . . ?
C47 C375 C187 120.0 . . ?
C47 C375 H375 120.0 . . ?
C371 C47 H47 120.0 . . ?
C375 C47 C371 120.0 . . ?
C375 C47 H47 120.0 . . ?
H37D C377 H37E 109.4 . . ?
H37D C377 H37F 109.4 . . ?
H37E C377 H37F 109.5 . . ?
C379 C377 H37D 108.8 . . ?
C379 C377 H37E 108.7 . . ?
C379 C377 H37F 111.0 . . ?
H18G C189 H18H 109.6 . . ?
H18G C189 H18I 109.4 . . ?
H18H C189 H18I 109.5 . . ?
C191 C189 H18G 108.3 . . ?
C191 C189 H18H 109.7 . . ?
C191 C189 H18I 110.5 . . ?
S17 C379 H379 107.9 . . ?
C299 C379 S17 113(4) . . ?
C299 C379 C377 114(5) . . ?
C299 C379 H379 107.9 . . ?
C377 C379 S17 106(4) . . ?
C377 C379 H379 107.9 . . ?
C125 C95 H95A 108.9 . . ?
C125 C95 H95B 108.3 . . ?
C125 C95 H95C 111.2 . . ?
H95A C95 H95B 109.4 . . ?
H95A C95 H95C 109.6 . . ?
H95B C95 H95C 109.4 . . ?
C219 C381 H38G 123.8 . . ?
C219 C381 H38H 112.1 . . ?
C219 C381 H38I 90.4 . . ?
H38G C381 H38H 109.4 . . ?
H38G C381 H38I 109.4 . . ?
H38H C381 H38I 109.5 . . ?
S3 C191 H191 119.2 . . ?
C303 C191 S3 99.8(8) . . ?
C303 C191 H191 119.2 . . ?
C189 C191 S3 99.9(8) . . ?
C189 C191 C303 95(8) . . ?
C189 C191 H191 119.2 . . ?
C305 C383 H383 117.6 . . ?
C385 C383 C305 125(4) . . ?
C385 C383 H383 117.6 . . ?
C119 C3 H3 117.7 . . ?
C119 C3 C385 125(5) . . ?
C385 C3 H3 117.7 . . ?
C383 C385 H385 121.7 . . ?
C3 C385 C383 117(4) . . ?
C3 C385 H385 121.7 . . ?
C387 C193 P19 121(3) . . ?
C387 C193 C391 120.00(5) . . ?
C391 C193 P19 119(3) . . ?
C193 C387 H387 120.0 . . ?
C97 C387 C193 120.00(6) . . ?
C97 C387 H387 120.0 . . ?
C387 C97 H97 120.0 . . ?
C387 C97 C389 120.00(5) . . ?
C389 C97 H97 120.0 . . ?
C97 C389 H389 120.0 . . ?
C195 C389 C97 120.0 . . ?
C195 C389 H389 120.0 . . ?
C389 C195 H195 120.0 . . ?
C391 C195 C389 120.0 . . ?
C391 C195 H195 120.0 . . ?
C193 C391 H391 120.0 . . ?
C195 C391 C193 120.0 . . ?
C195 C391 H391 120.0 . . ?
C131 C49 H49A 109.5 . . ?
C131 C49 H49B 109.5 . . ?
C131 C49 H49C 109.5 . . ?
H49A C49 H49B 109.5 . . ?
H49A C49 H49C 109.5 . . ?
H49B C49 H49C 109.5 . . ?
C167 C393 H393 120.8 . . ?
C337 C393 C167 118(5) . . ?
C337 C393 H393 120.8 . . ?
H19G C197 H19H 109.4 . . ?
H19G C197 H19I 109.5 . . ?
H19H C197 H19I 109.5 . . ?
C99 C197 H19G 109.8 . . ?
C99 C197 H19H 110.9 . . ?
C99 C197 H19I 107.9 . . ?
C333 C395 H39D 110.4 . . ?
C333 C395 H39E 108.9 . . ?
C333 C395 H39F 108.9 . . ?
H39D C395 H39E 109.6 . . ?
H39D C395 H39F 109.5 . . ?
H39E C395 H39F 109.5 . . ?
S9 C99 H99 108.9 . . ?
C77 C99 S9 100.1(8) . . ?
C77 C99 H99 108.9 . . ?
C197 C99 S9 106(4) . . ?
C197 C99 C77 122.8(13) . . ?
C197 C99 H99 108.9 . . ?
C333 C397 H39G 108.4 . . ?
C333 C397 H39H 110.2 . . ?
C333 C397 H39I 109.8 . . ?
H39G C397 H39H 109.5 . . ?
H39G C397 H39I 109.5 . . ?
H39H C397 H39I 109.4 . . ?
C111 C199 H199 111.1 . . ?
C261 C199 C111 138(6) . . ?
C261 C199 H199 111.1 . . ?
C85 C399 H39J 113.0 . . ?
C85 C399 H39K 113.0 . . ?
C173 C399 C85 94(4) . . ?
C173 C399 H39J 113.0 . . ?
C173 C399 H39K 113.0 . . ?
H39J C399 H39K 110.4 . . ?
C83 C25 H25 120.9 . . ?
C83 C25 C401 118(5) . . ?
C401 C25 H25 120.9 . . ?
C261 C401 C25 122(5) . . ?
C261 C401 H401 119.2 . . ?
C25 C401 H401 119.2 . . ?
S11 C201 H201 113.4 . . ?
C115 C201 S11 99.9(8) . . ?
C115 C201 H201 113.4 . . ?
C39 C201 S11 99.9(8) . . ?
C39 C201 C115 115.2(12) . . ?
C39 C201 H201 113.4 . . ?
C269 C403 C35 122(5) . . ?
C269 C403 H403 119.2 . . ?
C35 C403 H403 119.2 . . ?
S23 C101 H101 116.0 . . ?
C311 C101 S23 99.9(8) . . ?
C311 C101 H101 116.0 . . ?
C407 C101 S23 99.9(8) . . ?
C407 C101 C311 107(10) . . ?
C407 C101 H101 116.0 . . ?
C251 C405 H40L 109.0 . . ?
C251 C405 H40M 110.1 . . ?
C251 C405 H40N 109.3 . . ?
H40L C405 H40M 109.5 . . ?
H40L C405 H40N 109.5 . . ?
H40M C405 H40N 109.4 . . ?
C129 C203 H20A 111.9 . . ?
C129 C203 H20B 108.2 . . ?
C129 C203 H20C 108.4 . . ?
H20A C203 H20B 109.5 . . ?
H20A C203 H20C 109.5 . . ?
H20B C203 H20C 109.4 . . ?
C101 C407 H40O 105.0 . . ?
C101 C407 H40P 107.6 . . ?
C101 C407 H40Q 115.7 . . ?
H40O C407 H40P 109.4 . . ?
H40O C407 H40Q 109.4 . . ?
H40P C407 H40Q 109.6 . . ?
C155 C51 H51A 110.9 . . ?
C155 C51 H51B 108.3 . . ?
C155 C51 H51C 109.3 . . ?
H51A C51 H51B 109.5 . . ?
H51A C51 H51C 109.4 . . ?
H51B C51 H51C 109.5 . . ?
C155 C409 H40R 109.1 . . ?
C155 C409 H40S 109.7 . . ?
C155 C409 H40T 109.6 . . ?
H40R C409 H40S 109.5 . . ?
H40R C409 H40T 109.5 . . ?
H40S C409 H40T 109.5 . . ?
C255 C205 H20D 103.2 . . ?
C255 C205 H20E 113.7 . . ?
C255 C205 H20F 111.4 . . ?
H20D C205 H20E 108.9 . . ?
H20D C205 H20F 111.8 . . ?
H20E C205 H20F 107.9 . . ?
S6 C411 H411 103.2 . . ?
C103 C411 S6 119(2) . . ?
C103 C411 H411 103.2 . . ?
C413 C411 S6 99.5(17) . . ?
C413 C411 H411 103.2 . . ?
C413 C411 C103 125.3(11) . . ?
C411 C103 H10J 109.0 . . ?
C411 C103 H10K 113.3 . . ?
C411 C103 H10L 106.0 . . ?
H10J C103 H10K 109.5 . . ?
H10J C103 H10L 109.5 . . ?
H10K C103 H10L 109.5 . . ?
C411 C413 H41F 113.4 . . ?
C411 C413 H41G 109.3 . . ?
C411 C413 H41H 105.7 . . ?
H41F C413 H41G 109.5 . . ?
H41F C413 H41H 109.5 . . ?
H41G C413 H41H 109.5 . . ?
P11 C207 H20G 109.1 . . ?
P11 C207 H20H 109.1 . . ?
C171 C207 P11 113(6) . . ?
C171 C207 H20G 109.1 . . ?
C171 C207 H20H 109.1 . . ?
H20G C207 H20H 107.8 . . ?
C279 C415 H415 116.1 . . ?
C301 C415 C279 128(5) . . ?
C301 C415 H415 116.1 . . ?
S21 C13 H13 100.7 . . ?
C239 C13 S21 99.7(8) . . ?
C239 C13 C157 148(8) . . ?
C239 C13 H13 100.7 . . ?
C157 C13 S21 99.7(8) . . ?
C157 C13 H13 100.7 . . ?
C237 C417 C71 119(4) . . ?
C237 C417 H417 120.7 . . ?
C71 C417 H417 120.7 . . ?
C125 C209 H20I 111.4 . . ?
C125 C209 H20J 110.5 . . ?
C125 C209 H20K 106.4 . . ?
H20I C209 H20J 109.4 . . ?
H20I C209 H20K 109.5 . . ?
H20J C209 H20K 109.5 . . ?
C55 C419 H41I 124.7 . . ?
C55 C419 H41J 84.6 . . ?
C55 C419 H41K 115.4 . . ?
H41I C419 H41J 109.5 . . ?
H41I C419 H41K 109.4 . . ?
H41J C419 H41K 109.5 . . ?
O19 Si1 O20 68.3(10) 2_486 . ?
O19 Si1 O20 111.7(10) . . ?
O21 Si1 O19 102(3) . . ?
O21 Si1 O19 78(3) 2_486 . ?
O21 Si1 O20 68.2(10) 2_486 . ?
O21 Si1 O20 111.8(10) . . ?
O22 Si1 O19 67.2(9) 2_486 . ?
O22 Si1 O19 112.8(9) . . ?
O22 Si1 O20 75(3) 2_486 . ?
O22 Si1 O20 105(3) . . ?
O22 Si1 O21 112.8(9) . . ?
O22 Si1 O21 67.2(9) 2_486 . ?
O40 Si2 O40 180(4) 2_577 . ?
O40 Si2 O42 70.9(8) 2_577 . ?
O40 Si2 O42 109.1(8) . . ?
O40 Si2 O43 109.1(8) . . ?
O40 Si2 O43 70.9(8) 2_577 . ?
O40 Si2 O43 109.1(8) 2_577 2_577 ?
O40 Si2 O43 70.9(8) . 2_577 ?
O41 Si2 O40 70.3(8) 2_577 . ?
O41 Si2 O40 109.7(8) . . ?
O41 Si2 O41 179.994(18) 2_577 . ?
O41 Si2 O42 109.6(7) . . ?
O41 Si2 O42 70.3(7) 2_577 . ?
O41 Si2 O43 70.0(7) 2_577 . ?
O41 Si2 O43 110.0(7) . . ?
O41 Si2 O43 70.0(7) . 2_577 ?
O41 Si2 O43 110.0(7) 2_577 2_577 ?
O43 Si2 O42 70.7(7) 2_577 . ?
O43 Si2 O42 109.3(7) . . ?
O43 Si2 O43 179.99(3) 2_577 . ?
Si2 O40 O43 54.6(5) . 2_577 ?
O41 O40 O43 90.2(9) 2_577 2_577 ?
Si2 O41 O43 55.2(5) . 2_577 ?
Si2 O42 O43 54.6(5) . 2_577 ?
O41 O42 O43 90.2(9) 2_577 2_577 ?
C421 C105 H105 120.0 . . ?
C421 C105 C425 120.0 . . ?
C425 C105 H105 120.0 . . ?
C105 C421 H421 120.0 . . ?
C105 C421 C211 120.0 . . ?
C211 C421 H421 120.0 . . ?
C421 C211 H211 120.0 . . ?
C423 C211 C421 120.0 . . ?
C423 C211 H211 120.0 . . ?
C211 C423 P11 120.1(4) . . ?
C211 C423 C53 120.0 . . ?
C53 C423 P11 119.9(4) . . ?
C423 C53 H53 120.0 . . ?
C425 C53 C423 120.0 . . ?
C425 C53 H53 120.0 . . ?
C105 C425 H425 120.0 . . ?
C53 C425 C105 120.0 . . ?
C53 C425 H425 120.0 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
O1 W1 O3 W5 28(5) . . . 2_486 ?
O1 W1 O4 W4 -109(3) . . . 2_486 ?
O1 W1 O14 C275 -18(32) . . . 1_565 ?
O1 W3 O6 W6 71(5) . . . . ?
O1 W3 O7 W2 -53(3) . . . . ?
O1 W3 O11 W5 -19(9) . . . . ?
O2 W1 O3 W5 108(2) . . . 2_486 ?
O2 W1 O4 W4 -44(4) . . . 2_486 ?
O2 W1 O14 C275 -106(32) . . . 1_565 ?
O2 W2 O7 W3 54(3) . . . . ?
O2 W2 O8 W6 -123(4) . . . 2_486 ?
O2 W2 O9 W4 34(8) . . . . ?
O3 W1 O4 W4 50(3) . . . 2_486 ?
O3 W1 O14 C275 161(32) . . . 1_565 ?
O3 W5 O11 W3 15(8) 2_486 . . . ?
O3 W5 O12 W6 -92(3) 2_486 . . . ?
O4 W1 O3 W5 -51(2) . . . 2_486 ?
O4 W1 O14 C275 69(32) . . . 1_565 ?
O5 W6 O6 W3 -68(5) . . . . ?
O5 W6 O12 W5 -6(6) . . . . ?
O6 W3 O7 W2 66(5) . . . . ?
O6 W3 O11 W5 62(4) . . . . ?
O6 W6 O5 W4 112(4) . . . 2_486 ?
O6 W6 O12 W5 -70(2) . . . . ?
O7 W2 O8 W6 -55(6) . . . 2_486 ?
O7 W2 O9 W4 103(4) . . . . ?
O7 W3 O6 W6 -45(7) . . . . ?
O7 W3 O11 W5 -101(4) . . . . ?
O8 W2 O7 W3 -14(6) . . . . ?
O8 W2 O9 W4 -51(4) . . . . ?
O8 W6 O5 W4 -40(5) 2_486 . . 2_486 ?
O8 W6 O6 W3 46(7) 2_486 . . . ?
O8 W6 O12 W5 89(2) 2_486 . . . ?
O9 W2 O7 W3 -107(3) . . . . ?
O9 W2 O8 W6 37(4) . . . 2_486 ?
O10 W5 O11 W3 101(4) . . . . ?
O10 W5 O12 W6 1(4) . . . . ?
O11 W3 O6 W6 -90(4) . . . . ?
O11 W3 O7 W2 108(3) . . . . ?
O11 W5 O12 W6 68(2) . . . . ?
O12 W5 O11 W3 -61(4) . . . . ?
O12 W6 O5 W4 53(8) . . . 2_486 ?
O12 W6 O6 W3 91(4) . . . . ?
O13 W6 O5 W4 -145(4) . . . 2_486 ?
O13 W6 O6 W3 -171(4) . . . . ?
O13 W6 O12 W5 -168(3) . . . . ?
O14 W1 O3 W5 -148(3) . . . 2_486 ?
O14 W1 O4 W4 151(3) . . . 2_486 ?
O15 W3 O6 W6 171(4) . . . . ?
O15 W3 O7 W2 -150(3) . . . . ?
O15 W3 O11 W5 160(4) . . . . ?
O16 W2 O7 W3 151(3) . . . . ?
O16 W2 O8 W6 140(4) . . . 2_486 ?
O16 W2 O9 W4 -155(4) . . . . ?
O18 W5 O11 W3 -158(4) . . . . ?
O18 W5 O12 W6 165(3) . . . . ?
O1A W1A O2A W3A -67(4) . . . . ?
O1A W1A O3A W6A 33(8) . . . . ?
O1A W2A O8A W4A -108(4) . . . . ?
O2A W1A O3A W6A -78(5) . . . . ?
O2A W3A O10A W2A -53(3) . . . . ?
O2A W3A O11A W5A -39(8) . . . 2_486 ?
O2A W3A O12A W4A 103(4) . . . 2_486 ?
O3A W1A O2A W3A 91(4) . . . . ?
O4A W1A O2A W3A 3(10) . . . . ?
O4A W1A O3A W6A 84(4) . . . . ?
O5A W4A O8A W2A -54(4) 2_486 . . . ?
O5A W6A O3A W1A 78(5) . . . . ?
O6A W6A O3A W1A -81(5) . . . . ?
O7A W4A O8A W2A 110(4) . . . . ?
O9A W2A O8A W4A 58(4) . . . . ?
O9A W6A O3A W1A -7(12) 2_486 . . . ?
O10A W2A O8A W4A -23(7) . . . . ?
O10A W3A O2A W1A 67(4) . . . . ?
O10A W3A O11A W5A -110(4) . . . 2_486 ?
O10A W3A O12A W4A 21(9) . . . 2_486 ?
O11A W3A O2A W1A -4(9) . . . . ?
O11A W3A O10A W2A 106(3) . . . . ?
O11A W3A O12A W4A -56(4) . . . 2_486 ?
O12A W3A O2A W1A -92(4) . . . . ?
O12A W3A O10A W2A 29(6) . . . . ?
O12A W3A O11A W5A 50(4) . . . 2_486 ?
O12A W4A O8A W2A 43(8) 2_486 . . . ?
O13A W1A O2A W3A -166(4) . . . . ?
O13A W1A O3A W6A -180(4) . . . . ?
O15A W6A O3A W1A 179(4) . . . . ?
O16A W4A O8A W2A -149(4) . . . . ?
O17A W2A O8A W4A 155(3) . . . . ?
O18A W3A O2A W1A 167(4) . . . . ?
O18A W3A O10A W2A -153(2) . . . . ?
O18A W3A O11A W5A 150(4) . . . 2_486 ?
O18A W3A O12A W4A -156(4) . . . 2_486 ?
O1B W9A O25A W8A -149(4) . . . . ?
O23 W7 O25 W9 -35(2) . . . . ?
O23 W8 O24 W9 60(4) . . . . ?
O23A W7A O33A W12A -82.5(15) . . . 2_577 ?
O23A W9A O25A W8A -46(3) . . . . ?
O24 W9 O25 W7 35(2) . . . . ?
O24A W7A O23A W9A -47.5(15) . . . . ?
O24A W7A O33A W12A 11(3) . . . 2_577 ?
O24A W8A O25A W9A 54(3) . . . . ?
O24A W8A O30A W12A 42(5) . . . . ?
O24A W8A O31A W10A -100.0(19) . . . 2_577 ?
O25 W7 O23 W8 55(6) . . . . ?
O25A W8A O24A W7A -62.2(17) . . . . ?
O25A W8A O30A W12A 103(2) . . . . ?
O25A W8A O31A W10A -3(4) . . . 2_577 ?
O26 W9 O25 W7 -33(3) . . . . ?
O26 W12 O28 W11 44(2) . . . . ?
O26 W12 O29 W10 -83(2) . . . 2_577 ?
O26A W9A O25A W8A 126(3) . . . . ?
O26A W11A O28A W10A 67.8(12) . . . . ?
O27 W9 O25 W7 -119(2) . . . . ?
O27 W11 O28 W12 -50.8(17) . . . . ?
O27A W9A O25A W8A 36(5) . . . . ?
O27A W10A O38A W12A 118.7(18) . . . 2_577 ?
O28 W12 O29 W10 53(5) . . . 2_577 ?
O28A W10A O27A W9A 80.9(10) . . . . ?
O28A W10A O38A W12A 13(5) . . . 2_577 ?
O29 W10 O31 W7 -47.8(18) 2_577 . . . ?
O29 W12 O28 W11 -89(4) . . . . ?
O29A W11A O28A W10A -87(3) . . . . ?
O29A W12A O30A W8A -99(2) . . . . ?
O30 W10 O31 W7 102.3(19) . . . . ?
O30 W11 O28 W12 30(3) . . . . ?
O30A W8A O24A W7A -3(4) . . . . ?
O30A W8A O25A W9A -110(3) . . . . ?
O30A W8A O31A W10A 61.4(18) . . . 2_577 ?
O31 W7 O23 W8 -4(11) . . . . ?
O31 W7 O25 W9 124(2) . . . . ?
O31A W8A O24A W7A 94.3(15) . . . . ?
O31A W8A O25A W9A -44(5) . . . . ?
O31A W8A O30A W12A -56(2) . . . . ?
O31A W10A O27A W9A -1(3) 2_577 . . . ?
O31A W10A O38A W12A -46.4(18) 2_577 . . 2_577 ?
O32 W8 O24 W9 -110(3) 2_577 . . . ?
O32A W7A O23A W9A 28(2) . . . . ?
O32A W7A O33A W12A 69.0(12) . . . 2_577 ?
O32A W11A O28A W10A -104.9(14) 2_577 . . . ?
O33 W10 O31 W7 -145(2) . . . . ?
O33A W7A O23A W9A 114.5(17) . . . . ?
O33A W12A O30A W8A -41(4) 2_577 . . . ?
O34 W7 O23 W8 -91(6) . . . . ?
O34 W7 O25 W9 49(4) . . . . ?
O34 W12 O28 W11 -96(2) 2_577 . . . ?
O34 W12 O29 W10 60(2) 2_577 . . 2_577 ?
O34A W10A O27A W9A 175.2(9) . . . . ?
O34A W10A O38A W12A -142.8(17) . . . 2_577 ?
O35 W7 O23 W8 163(5) . . . . ?
O35 W7 O25 W9 -138(2) . . . . ?
O35A W8A O24A W7A -163.5(15) . . . . ?
O35A W8A O25A W9A 147(4) . . . . ?
O35A W8A O30A W12A -157.3(19) . . . . ?
O35A W8A O31A W10A 165(3) . . . 2_577 ?
O36 W9 O25 W7 139.4(18) . . . . ?
O36A W12A O30A W8A 163(3) . . . . ?
O37 W11 O28 W12 -141.3(16) . . . . ?
O37A W11A O28A W10A 166.7(10) . . . . ?
O38 W8 O24 W9 26(10) 2_577 . . . ?
O38 W11 O28 W12 125(2) . . . . ?
O38A W10A O27A W9A -88.8(11) . . . . ?
O38A W12A O30A W8A 51(2) 2_577 . . . ?
O39 W12 O28 W11 158(2) . . . . ?
O39 W12 O29 W10 166(2) . . . 2_577 ?
O39A W7A O23A W9A -148(3) . . . . ?
O39A W7A O33A W12A 171.4(12) . . . 2_577 ?
Ag S18 C4 C344 19(4) . . . . ?
Ag S18 C4 C348 -95(3) . . . . ?
Ag P5 C224 C214 101(2) . . . . ?
Ag P5 C224 C222 -73(3) . . . . ?
Ag P5 C248 C96 -79(5) . . . . ?
Ag P5 C382 C372 -175.7(18) . . . . ?
Ag P5 C382 C380 4.3(18) . . . . ?
Ag1A S26A C68 C72 -42(10) . . . . ?
Ag1A S26A C68 C426 169(7) . . . . ?
Ag1A P9 C178 C168 166(3) . . . . ?
Ag1A P9 C178 C170 -14(4) . . . . ?
Ag1A P9 C278 C416 -72(4) . . . . ?
Ag2 S14 C240 C252 -170(5) . . . . ?
Ag2 S14 C240 C328 -24(6) . . . . ?
Ag6 S10 C102 C98 -64(3) . . . . ?
Ag6 S10 C102 C370 60(3) . . . . ?
Ag6 P12 C40 C42 -24(2) . . . . ?
Ag6 P12 C40 C50 157.3(15) . . . . ?
Ag6 P12 C122 C104 73(3) . . . . ?
Ag6 P12 C302 C300 88.9(17) . . . . ?
Ag6 P12 C302 C304 -90.2(16) . . . . ?
Ag7 S15 C1 C196 14(6) . . . . ?
Ag7 S15 C1 C404 136(6) . . . . ?
Ag7 S31 C92 C180 21(12) . . . . ?
Ag7 S31 C92 C182 -174(13) . . . . ?
Ag9 S26 C66 C70 139(4) . . . . ?
Ag9 S26 C66 C152 -81(4) . . . . ?
Ag9 P21 C228 C230 64(3) . . . . ?
Ag9 P21 C228 C238 -120(2) . . . . ?
Ag9 P21 C312 C314 -150(2) . . . . ?
Ag9 P21 C312 C322 29(4) . . . . ?
Ag9A S26A C68 C72 85(11) . . . . ?
Ag9A S26A C68 C426 -64(7) . . . . ?
Ag9A P21 C228 C230 62(4) . . . . ?
Ag9A P21 C228 C238 -122(3) . . . . ?
Ag9A P21 C312 C314 -130(3) . . . . ?
Ag9A P21 C312 C322 50(3) . . . . ?
Ag10 S8 C242 C118 152(3) . . . . ?
Ag10 S8 C242 C268 -79(3) . . . . ?
Ag10 P13 C8 C10 -169(3) . . . . ?
Ag10 P13 C8 C36 14(4) . . . . ?
Ag10 P13 C106 C108 -119.5(17) . . . . ?
Ag10 P13 C106 C116 55.4(18) . . . . ?
Ag10 P13 C126 C100 -75(3) . . . . ?
Ag12 S10 C102 C98 64(3) . . . . ?
Ag12 S10 C102 C370 -172(3) . . . . ?
Ag12 P20 C76 C78 -10.5(17) . . . . ?
Ag12 P20 C76 C86 168.9(13) . . . . ?
Ag12 P20 C90 C154 116(4) . . . . ?
Ag12 P20 C90 C210 -61(4) . . . . ?
Ag12 P20 C156 C100 55(3) . . . . ?
Ag15 S30 C56 C352 53(4) . . . . ?
Ag15 S30 C56 C356 -77(3) . . . . ?
Ag17 S14 C240 C252 25(7) . . . . ?
Ag17 S14 C240 C328 171(4) . . . . ?
Ag20 S31 C92 C180 -157(9) . . . . ?
Ag20 S31 C92 C182 9(18) . . . . ?
Ag20 P17 C30 C24 -59(3) . . . . ?
Ag20 P17 C128 C130 -59.7(16) . . . . ?
Ag20 P17 C128 C138 119.3(15) . . . . ?
Ag20 P17 C212 C246 138(3) . . . . ?
Ag20 P17 C212 C406 -37(4) . . . . ?
Ag24 S8 C242 C118 -72(3) . . . . ?
Ag24 S8 C242 C268 57(4) . . . . ?
Ag24 P7 C12 C14 145.8(14) . . . . ?
Ag24 P7 C12 C22 -32.9(19) . . . . ?
Ag24 P7 C424 C28 129(4) . . . . ?
Ag24 P7 C424 C410 -58(4) . . . . ?
Ag27 S27 C394 C88 122(5) . . . . ?
Ag27 S27 C394 C176 1(5) . . . . ?
Ag27 S29 C396 C402 118(2) . . . . ?
Ag27 S29 C396 C408 -127(3) . . . . ?
Ag29 S27 C394 C88 -9(3) . . . . ?
Ag29 S27 C394 C176 -131(3) . . . . ?
Ag29 S31 C92 C180 128(11) . . . . ?
Ag29 S31 C92 C182 -66(14) . . . . ?
Ag30 S10 C102 C98 178(3) . . . . ?
Ag30 S10 C102 C370 -58(4) . . . . ?
Ag30 S26 C66 C70 -131(4) . . . . ?
Ag30 S26 C66 C152 9(5) . . . . ?
Ag30 S26A C68 C72 -128(10) . . . . ?
Ag30 S26A C68 C426 84(7) . . . . ?
Ag33 S26 C66 C70 -12(5) . . . . ?
Ag33 S26 C66 C152 128(4) . . . . ?
Ag33 P9 C178 C168 168(3) . . . . ?
Ag33 P9 C178 C170 -12(5) . . . . ?
Ag33 P9 C278 C416 -58(4) . . . . ?
Ag34 S18 C4 C344 -177(3) . . . . ?
Ag34 S18 C4 C348 69(3) . . . . ?
Ag34 P16 C60 C24 61(3) . . . . ?
Ag34 P16 C324 C280 30(4) . . . . ?
Ag34 P16 C324 C310 -144(4) . . . . ?
Ag34 P16 C362 C360 19(2) . . . . ?
Ag34 P16 C362 C364 -161.3(16) . . . . ?
Ag35 S2 C390 C34 -62(5) . . . . ?
Ag35 S2 C390 C384 166(4) . . . . ?
Ag35 S30 C56 C352 -53(4) . . . . ?
Ag35 S30 C56 C356 177(3) . . . . ?
Ag36 S8 C242 C118 37(3) . . . . ?
Ag36 S8 C242 C268 166(3) . . . . ?
Ag37 S18 C4 C344 39(4) . . . . ?
Ag37 S18 C4 C348 -74(3) . . . . ?
Ag37 P5 C224 C214 92(3) . . . . ?
Ag37 P5 C224 C222 -82(3) . . . . ?
Ag37 P5 C248 C96 -54(5) . . . . ?
Ag37 P5 C382 C372 167.3(17) . . . . ?
Ag37 P5 C382 C380 -12.7(17) . . . . ?
Ag38 S12 C226 C158 108(4) . . . . ?
Ag38 S12 C226 C330 -46(5) . . . . ?
Ag38 P18 C6 C244 174(4) . . . . ?
Ag38 P18 C6 C254 -24(5) . . . . ?
Ag38 P18 C32 C270 63(3) . . . . ?
Ag38 P18 C266 C256 -71.0(18) . . . . ?
Ag38 P18 C266 C264 107.0(18) . . . . ?
Ag45 S2 C390 C34 -152(4) . . . . ?
Ag45 S2 C390 C384 76(5) . . . . ?
Ag46 S12 C226 C158 -142(4) . . . . ?
Ag46 S12 C226 C330 64(5) . . . . ?
Ag46 P22 C294 C284 0(2) . . . . ?
Ag46 P22 C294 C292 174.8(17) . . . . ?
Ag46 P22 C332 C334 -32(2) . . . . ?
Ag46 P22 C332 C342 161.6(17) . . . . ?
Ag54 S12 C226 C158 -16(5) . . . . ?
Ag54 S12 C226 C330 -169(4) . . . . ?
Ag54 S18 C4 C344 -67(4) . . . . ?
Ag54 S18 C4 C348 179(3) . . . . ?
Ag55 S7 C38 C400 -137(8) . . . . ?
Ag55 S7 C38 C412 -19(10) . . . . ?
Ag55 S29 C396 C402 -162(3) . . . . ?
Ag55 S29 C396 C408 -47(3) . . . . ?
Ag57 S7 C38 C400 -25(9) . . . . ?
Ag57 S7 C38 C412 92(9) . . . . ?
Ag57 S15 C1 C196 -160(6) . . . . ?
Ag57 S15 C1 C404 -39(6) . . . . ?
Ag59 S27 C394 C88 -97(4) . . . . ?
Ag59 S27 C394 C176 141(4) . . . . ?
Ag59 P24 C62 C416 -51(6) . . . . ?
Ag59 P24 C184 C186 -32(2) . . . . ?
Ag59 P24 C184 C194 151.6(19) . . . . ?
Ag61 W21 O58 Ag34 173(3) . . . . ?
Ag61 W21 O66 W26 -24(4) . . . . ?
P7 C12 C14 C16 -179(2) . . . . ?
P7 C12 C22 C20 179(2) . . . . ?
P9 C198 C200 C202 -176(3) . . . . ?
P9 C198 C208 C206 176(3) . . . . ?
P9 C278 C416 C62 -77(7) . . . . ?
P12 C40 C42 C44 -179(3) . . . . ?
P12 C40 C50 C48 179(2) . . . . ?
P12 C302 C304 C306 179(2) . . . . ?
P13 C8 C10 C120 -175(3) . . . . ?
P13 C8 C36 C162 177(3) . . . . ?
P13 C106 C108 C110 175(2) . . . . ?
P13 C106 C116 C114 -175(2) . . . . ?
P16 C362 C364 C366 180(3) . . . . ?
P17 C128 C130 C132 179(2) . . . . ?
P17 C128 C138 C136 -179(2) . . . . ?
P17 C212 C246 C54 -170(3) . . . . ?
P17 C212 C406 C392 174(3) . . . . ?
P18 C6 C244 C124 -178(4) . . . . ?
P18 C6 C254 C326 -177(4) . . . . ?
P18 C32 C270 C276 95(4) . . . . ?
P20 C76 C78 C80 179(2) . . . . ?
P20 C76 C86 C84 -179(2) . . . . ?
P20 C90 C154 C418 176(4) . . . . ?
P20 C90 C210 C250 176(4) . . . . ?
P21 C64 C96 C248 172(5) . . . . ?
P21 C228 C230 C232 176(4) . . . . ?
P21 C228 C238 C236 -177(4) . . . . ?
P21 C312 C314 C316 180(4) . . . . ?
P21 C312 C322 C320 -180(4) . . . . ?
P22 C94 C104 C122 -162(3) . . . . ?
P22 C332 C334 C336 -167(3) . . . . ?
P22 C332 C342 C340 166(3) . . . . ?
P24 C62 C416 C278 -154(5) . . . . ?
P24 C140 C142 C144 178(3) . . . . ?
P24 C140 C150 C148 -178(3) . . . . ?
P24 C184 C186 C188 -176(3) . . . . ?
P24 C184 C194 C192 176(3) . . . . ?
O45 W14 O78 W21 -137(2) . . . . ?
O45 W14 O102 W20 172.1(14) . . . . ?
O46 W28 O54 Ag9 -28.3(15) . . . . ?
O46 W28 O54 Ag9A -6.7(19) . . . . ?
O46 W28 O54 Ag18 -170.9(11) . . . . ?
O48 W26 O90 Ag20 33.6(16) . . . . ?
O48 W26 O90 Ag50 176.8(10) . . . . ?
O50 W13 O52 W24 171(4) . . . . ?
O50 W13 O56 W28 -178.2(12) . . . . ?
O50 W13 O105 Ag1A 21.7(14) . . . . ?
O50 W13 O105 Ag18 171.0(10) . . . . ?
O50 W13 O105 Ag33 -1.5(14) . . . . ?
O52 W13 O50 Ag12 122.0(17) . . . . ?
O52 W13 O56 W28 51(3) . . . . ?
O52 W13 O105 Ag1A 124.6(12) . . . . ?
O52 W13 O105 Ag18 -86.1(10) . . . . ?
O52 W13 O105 Ag33 101.4(12) . . . . ?
O52 W24 O76 Ag10 -98.9(13) . . . . ?
O52 W24 O107 Ag2 18(3) . . . . ?
O52 W24 O107 Ag50 85.6(10) . . . . ?
O52 W24 O107 Ag59 -124.8(10) . . . . ?
O56 W13 O50 Ag12 -39.5(18) . . . . ?
O56 W13 O52 W24 -59(5) . . . . ?
O56 W13 O105 Ag1A -75.2(12) . . . . ?
O56 W13 O105 Ag18 74.1(11) . . . . ?
O56 W13 O105 Ag33 -98.4(12) . . . . ?
O56 W28 O54 Ag9 68.0(13) . . . . ?
O56 W28 O54 Ag9A 89.5(16) . . . . ?
O56 W28 O54 Ag18 -74.7(11) . . . . ?
O58 W21 O66 W26 -56(4) . . . . ?
O60 W20 O82 W26 21(2) . . . . ?
O60 W24 O52 W13 97(4) . . . . ?
O60 W24 O76 Ag10 -18.7(13) . . . . ?
O60 W24 O107 Ag2 -54(5) . . . . ?
O60 W24 O107 Ag50 14(4) . . . . ?
O60 W24 O107 Ag59 163(3) . . . . ?
O62 W15 O64 Ag -139.2(10) . . . . ?
O62 W15 O64 Ag37 -151.5(15) . . . . ?
O62 W15 O64 Ag44 1.9(10) . . . . ?
O62 W15 O96 W28 -29(4) . . . . ?
O62 W21 O58 Ag34 152.4(15) . . . . ?
O62 W21 O58 Ag44 0.7(11) . . . . ?
O62 W21 O58 Ag61 -21.0(14) . . . . ?
O62 W21 O66 W26 27(4) . . . . ?
O62 Si4 O92 W24 -174.3(13) . . . . ?
O62 Si4 O92 W26 54.0(17) . . . . ?
O62 Si4 O92 Ag50 -53.3(13) . . . . ?
O62 Si4 O104 W13 171.7(13) . . . . ?
O62 Si4 O104 W28 -48.7(18) . . . . ?
O62 Si4 O104 Ag18 61.4(12) . . . . ?
O62 Si4 O108 W14 -6.0(16) . . . . ?
O62 Si4 O108 W19 115.0(13) . . . . ?
O62 Si4 O108 W20 -121.8(12) . . . . ?
O64 W15 O96 W28 61(4) . . . . ?
O66 W21 O58 Ag34 -121.0(14) . . . . ?
O66 W21 O58 Ag44 87.3(12) . . . . ?
O66 W21 O58 Ag61 65.6(15) . . . . ?
O66 W26 O90 Ag20 137.5(13) . . . . ?
O66 W26 O90 Ag50 -79.3(10) . . . . ?
O68 W14 O78 W21 -36(2) . . . . ?
O68 W14 O102 W20 6(3) . . . . ?
O68 W15 O64 Ag -154(4) . . . . ?
O68 W15 O64 Ag37 -166(4) . . . . ?
O68 W15 O64 Ag44 -13(5) . . . . ?
O68 W15 O96 W28 -108(4) . . . . ?
O70 W19 O88 W14 168.8(13) . . . . ?
O70 W19 O109 W20 -177.3(13) . . . . ?
O70 W19 O111 W28 -123(2) . . . . ?
O72 W21 O58 Ag34 -16.7(17) . . . . ?
O72 W21 O58 Ag44 -168.4(12) . . . . ?
O72 W21 O58 Ag61 169.9(15) . . . . ?
O72 W21 O66 W26 -164(4) . . . . ?
O74 W15 O64 Ag 30.4(13) . . . . ?
O74 W15 O64 Ag37 18.1(17) . . . . ?
O74 W15 O64 Ag44 171.5(11) . . . . ?
O74 W15 O96 W28 163(4) . . . . ?
O76 W24 O52 W13 -173(4) . . . . ?
O76 W24 O107 Ag2 121(3) . . . . ?
O76 W24 O107 Ag50 -171.7(9) . . . . ?
O76 W24 O107 Ag59 -22.1(12) . . . . ?
O78 W14 O102 W20 -85.2(14) . . . . ?
O78 W21 O58 Ag34 146(2) . . . . ?
O78 W21 O58 Ag44 -6(4) . . . . ?
O78 W21 O58 Ag61 -28(4) . . . . ?
O78 W21 O66 W26 105(4) . . . . ?
O82 W26 O90 Ag20 -141(2) . . . . ?
O82 W26 O90 Ag50 2(4) . . . . ?
O84 W24 O52 W13 48(5) . . . . ?
O84 W24 O76 Ag10 66.2(13) . . . . ?
O84 W24 O107 Ag2 -141(3) . . . . ?
O84 W24 O107 Ag50 -73.5(10) . . . . ?
O84 W24 O107 Ag59 76.1(11) . . . . ?
O84 W26 O90 Ag20 -65.4(14) . . . . ?
O84 W26 O90 Ag50 77.8(10) . . . . ?
O88 W14 O78 W21 16(4) . . . . ?
O88 W14 O102 W20 72.3(14) . . . . ?
O88 W19 O109 W20 -75.5(13) . . . . ?
O88 W19 O111 W28 135(2) . . . . ?
O92 W24 O52 W13 17(4) . . . . ?
O92 W24 O76 Ag10 25(5) . . . . ?
O92 W24 O107 Ag2 -67(3) . . . . ?
O92 W24 O107 Ag50 0.5(9) . . . . ?
O92 W24 O107 Ag59 150.1(10) . . . . ?
O92 W26 O90 Ag20 -137.7(14) . . . . ?
O92 W26 O90 Ag50 5.5(9) . . . . ?
O92 Si4 O62 W15 168.9(13) . . . . ?
O92 Si4 O62 W21 -51.0(17) . . . . ?
O92 Si4 O62 Ag61 42.0(14) . . . . ?
O92 Si4 O104 W13 47.9(18) . . . . ?
O92 Si4 O104 W28 -172.5(13) . . . . ?
O92 Si4 O104 Ag18 -62.4(12) . . . . ?
O92 Si4 O108 W14 118.8(13) . . . . ?
O92 Si4 O108 W19 -120.2(13) . . . . ?
O92 Si4 O108 W20 3.0(16) . . . . ?
O94 W13 O50 Ag12 43.0(18) . . . . ?
O94 W13 O52 W24 -95(4) . . . . ?
O94 W13 O56 W28 86.2(12) . . . . ?
O94 W13 O105 Ag1A -164(2) . . . . ?
O94 W13 O105 Ag18 -14(3) . . . . ?
O94 W13 O105 Ag33 173(2) . . . . ?
O94 W19 O88 W14 -8(3) . . . . ?
O94 W19 O109 W20 80.9(13) . . . . ?
O94 W19 O111 W28 -21(2) . . . . ?
O96 W15 O64 Ag 134.9(11) . . . . ?
O96 W15 O64 Ag37 122.6(15) . . . . ?
O96 W15 O64 Ag44 -84.0(11) . . . . ?
O96 W28 O54 Ag9 -134.0(12) . . . . ?
O96 W28 O54 Ag9A -112.5(16) . . . . ?
O96 W28 O54 Ag18 83.3(12) . . . . ?
O98 W15 O64 Ag -64.7(12) . . . . ?
O98 W15 O64 Ag37 -77.0(16) . . . . ?
O98 W15 O64 Ag44 76.4(11) . . . . ?
O98 W15 O96 W28 -68(5) . . . . ?
O98 W21 O58 Ag34 79.9(15) . . . . ?
O98 W21 O58 Ag44 -71.8(12) . . . . ?
O98 W21 O58 Ag61 -93.4(15) . . . . ?
O98 W21 O66 W26 64(5) . . . . ?
O100 W20 O82 W26 126(2) . . . . ?
O102 W14 O78 W21 119(2) . . . . ?
O102 W20 O82 W26 -136(2) . . . . ?
O104 W13 O50 Ag12 -9(5) . . . . ?
O104 W13 O52 W24 -19(4) . . . . ?
O104 W13 O56 W28 8.7(10) . . . . ?
O104 W13 O105 Ag1A -148.3(12) . . . . ?
O104 W13 O105 Ag18 1.0(9) . . . . ?
O104 W13 O105 Ag33 -171.5(12) . . . . ?
O104 W28 O54 Ag9 140.3(12) . . . . ?
O104 W28 O54 Ag9A 161.9(16) . . . . ?
O104 W28 O54 Ag18 -2.3(10) . . . . ?
O104 Si4 O62 W15 48.7(18) . . . . ?
O104 Si4 O62 W21 -171.3(12) . . . . ?
O104 Si4 O62 Ag61 -78.2(13) . . . . ?
O104 Si4 O92 W24 -53.0(18) . . . . ?
O104 Si4 O92 W26 175.2(12) . . . . ?
O104 Si4 O92 Ag50 67.9(13) . . . . ?
O104 Si4 O108 W14 -124.8(12) . . . . ?
O104 Si4 O108 W19 -3.8(16) . . . . ?
O104 Si4 O108 W20 119.4(12) . . . . ?
O105 W13 O50 Ag12 -138.7(16) . . . . ?
O105 W13 O52 W24 67(4) . . . . ?
O105 W13 O56 W28 -75.3(12) . . . . ?
O107 W24 O52 W13 -68(4) . . . . ?
O107 W24 O76 Ag10 162.7(12) . . . . ?
O108 W14 O78 W21 46(2) . . . . ?
O108 W14 O102 W20 1.3(12) . . . . ?
O108 W19 O88 W14 -4.2(11) . . . . ?
O108 W19 O109 W20 -0.8(11) . . . . ?
O108 W19 O111 W28 60(2) . . . . ?
O108 W20 O82 W26 -64(2) . . . . ?
O108 Si4 O62 W15 -69.0(17) . . . . ?
O108 Si4 O62 W21 71.0(15) . . . . ?
O108 Si4 O62 Ag61 164.1(11) . . . . ?
O108 Si4 O92 W24 63.5(17) . . . . ?
O108 Si4 O92 W26 -68.3(16) . . . . ?
O108 Si4 O92 Ag50 -175.6(10) . . . . ?
O108 Si4 O104 W13 -69.5(16) . . . . ?
O108 Si4 O104 W28 70.2(17) . . . . ?
O108 Si4 O104 Ag18 -179.8(9) . . . . ?
O109 W19 O88 W14 68.2(13) . . . . ?
O109 W19 O111 W28 44(4) . . . . ?
O109 W20 O82 W26 -66(4) . . . . ?
O111 W19 O88 W14 -88.1(13) . . . . ?
O111 W19 O109 W20 16(3) . . . . ?
O111 W28 O54 Ag9 146(2) . . . . ?
O111 W28 O54 Ag9A 167.3(19) . . . . ?
O111 W28 O54 Ag18 3(3) . . . . ?
C6 P18 C32 C270 -66(3) . . . . ?
C6 P18 C266 C256 56(2) . . . . ?
C6 P18 C266 C264 -125(2) . . . . ?
C6 C254 C326 C308 6(8) . . . . ?
C8 P13 C106 C108 122(2) . . . . ?
C8 P13 C106 C116 -64(2) . . . . ?
C8 P13 C126 C100 51(3) . . . . ?
C8 C10 C120 C52 1(6) . . . . ?
C8 C36 C162 C52 -4(6) . . . . ?
C10 C8 C36 C162 0(6) . . . . ?
C12 P7 C424 C28 -104(4) . . . . ?
C12 P7 C424 C410 70(4) . . . . ?
C12 C14 C16 C18 0.0 . . . . ?
C14 C12 C22 C20 0.0 . . . . ?
C14 C16 C18 C20 0.0 . . . . ?
C16 C18 C20 C22 0.0 . . . . ?
C18 C20 C22 C12 0.0 . . . . ?
C22 C12 C14 C16 0.0 . . . . ?
C26 C310 C324 P16 175(4) . . . . ?
C26 C310 C324 C280 0(7) . . . . ?
C26 C414 C422 C280 -12(8) . . . . ?
C30 P17 C128 C130 63.5(19) . . . . ?
C30 P17 C128 C138 -117(2) . . . . ?
C30 P17 C212 C246 4(4) . . . . ?
C30 P17 C212 C406 -171(3) . . . . ?
C30 C24 C60 P16 162(3) . . . . ?
C32 P18 C6 C244 -58(5) . . . . ?
C32 P18 C6 C254 103(4) . . . . ?
C32 P18 C266 C256 164(2) . . . . ?
C32 P18 C266 C264 -18(2) . . . . ?
C32 C270 C276 P7 86(4) . . . . ?
C36 C8 C10 C120 2(6) . . . . ?
C40 P12 C122 C104 -54(3) . . . . ?
C40 P12 C302 C300 -148.4(18) . . . . ?
C40 P12 C302 C304 33(2) . . . . ?
C40 C42 C44 C46 0.0 . . . . ?
C42 C40 C50 C48 0.0 . . . . ?
C42 C44 C46 C48 0.0 . . . . ?
C44 C46 C48 C50 0.0 . . . . ?
C46 C48 C50 C40 0.0 . . . . ?
C50 C40 C42 C44 0.0 . . . . ?
C54 C174 C392 C406 2(8) . . . . ?
C58 C398 C410 C424 5(8) . . . . ?
C60 P16 C324 C280 -93(4) . . . . ?
C60 P16 C324 C310 92(5) . . . . ?
C60 P16 C362 C360 145(2) . . . . ?
C60 P16 C362 C364 -35(3) . . . . ?
C60 C24 C30 P17 -170(3) . . . . ?
C62 P24 C184 C186 -169(2) . . . . ?
C62 P24 C184 C194 15(3) . . . . ?
C64 P21 C228 C230 -63(4) . . . . ?
C64 P21 C228 C238 114(3) . . . . ?
C64 P21 C312 C314 -16(4) . . . . ?
C64 P21 C312 C322 164(3) . . . . ?
C64 C96 C248 P5 -156(5) . . . . ?
C76 P20 C90 C154 -125(4) . . . . ?
C76 P20 C90 C210 57(4) . . . . ?
C76 P20 C156 C100 -67(3) . . . . ?
C76 C78 C80 C82 0.0 . . . . ?
C78 C76 C86 C84 0.0 . . . . ?
C78 C80 C82 C84 0.0 . . . . ?
C80 C82 C84 C86 0.0 . . . . ?
C82 C84 C86 C76 0.0 . . . . ?
C86 C76 C78 C80 0.0 . . . . ?
C90 P20 C76 C78 -132(2) . . . . ?
C90 P20 C76 C86 47(2) . . . . ?
C90 P20 C156 C100 -175(3) . . . . ?
C90 C154 C418 C420 11(7) . . . . ?
C90 C210 C250 C420 5(7) . . . . ?
C94 P22 C294 C284 -131(2) . . . . ?
C94 P22 C294 C292 44(3) . . . . ?
C94 P22 C332 C334 94(2) . . . . ?
C94 P22 C332 C342 -73(2) . . . . ?
C94 C104 C122 P12 177(3) . . . . ?
C106 P13 C8 C10 -50(4) . . . . ?
C106 P13 C8 C36 133(3) . . . . ?
C106 P13 C126 C100 159(3) . . . . ?
C106 C108 C110 C112 0.0 . . . . ?
C108 C106 C116 C114 0.0 . . . . ?
C108 C110 C112 C114 0.0 . . . . ?
C110 C112 C114 C116 0.0 . . . . ?
C112 C114 C116 C106 0.0 . . . . ?
C116 C106 C108 C110 0.0 . . . . ?
C120 C52 C162 C36 6(6) . . . . ?
C122 P12 C40 C42 108(2) . . . . ?
C122 P12 C40 C50 -71(2) . . . . ?
C122 P12 C302 C300 -39(2) . . . . ?
C122 P12 C302 C304 141(2) . . . . ?
C124 C308 C326 C254 -3(7) . . . . ?
C126 P13 C8 C10 58(4) . . . . ?
C126 P13 C8 C36 -119(3) . . . . ?
C126 P13 C106 C108 13(2) . . . . ?
C126 P13 C106 C116 -171.7(19) . . . . ?
C126 C100 C156 P20 164(2) . . . . ?
C128 P17 C30 C24 -178(3) . . . . ?
C128 P17 C212 C246 -101(4) . . . . ?
C128 P17 C212 C406 84(4) . . . . ?
C128 C130 C132 C134 0.0 . . . . ?
C130 C128 C138 C136 0.0 . . . . ?
C130 C132 C134 C136 0.0 . . . . ?
C132 C134 C136 C138 0.0 . . . . ?
C134 C136 C138 C128 0.0 . . . . ?
C138 C128 C130 C132 0.0 . . . . ?
C140 P24 C62 C416 -167(5) . . . . ?
C140 P24 C184 C186 85(3) . . . . ?
C140 P24 C184 C194 -92(3) . . . . ?
C140 C142 C144 C146 0.0 . . . . ?
C142 C140 C150 C148 0.0 . . . . ?
C142 C144 C146 C148 0.0 . . . . ?
C144 C146 C148 C150 0.0 . . . . ?
C146 C148 C150 C140 0.0 . . . . ?
C150 C140 C142 C144 0.0 . . . . ?
C154 C90 C210 C250 -2(7) . . . . ?
C154 C418 C420 C250 -7(8) . . . . ?
C156 P20 C76 C78 119.4(18) . . . . ?
C156 P20 C76 C86 -61(2) . . . . ?
C156 P20 C90 C154 -18(5) . . . . ?
C156 P20 C90 C210 165(4) . . . . ?
C156 C100 C126 P13 -165(3) . . . . ?
C162 C52 C120 C10 -5(6) . . . . ?
C164 C166 C274 C170 4(6) . . . . ?
C164 C168 C178 P9 -179(3) . . . . ?
C164 C168 C178 C170 1(7) . . . . ?
C166 C164 C168 C178 -2(7) . . . . ?
C168 C164 C166 C274 -1(6) . . . . ?
C174 C54 C246 C212 -5(7) . . . . ?
C174 C392 C406 C212 -3(8) . . . . ?
C178 P9 C278 C416 179(4) . . . . ?
C178 C170 C274 C166 -5(7) . . . . ?
C184 P24 C62 C416 76(5) . . . . ?
C184 C186 C188 C190 0.0 . . . . ?
C186 C184 C194 C192 0.0 . . . . ?
C186 C188 C190 C192 0.0 . . . . ?
C188 C190 C192 C194 0.0 . . . . ?
C190 C192 C194 C184 0.0 . . . . ?
C194 C184 C186 C188 0.0 . . . . ?
C198 P9 C178 C168 37(4) . . . . ?
C198 P9 C178 C170 -143(4) . . . . ?
C198 P9 C278 C416 66(4) . . . . ?
C198 C200 C202 C204 0.0 . . . . ?
C200 C198 C208 C206 0.0 . . . . ?
C200 C202 C204 C206 0.0 . . . . ?
C202 C204 C206 C208 0.0 . . . . ?
C204 C206 C208 C198 0.0 . . . . ?
C208 C198 C200 C202 0.0 . . . . ?
C210 C90 C154 C418 -7(7) . . . . ?
C210 C250 C420 C418 0(8) . . . . ?
C212 P17 C30 C24 74(3) . . . . ?
C212 P17 C128 C130 177.1(19) . . . . ?
C212 P17 C128 C138 -4(2) . . . . ?
C214 C216 C218 C220 0.0 . . . . ?
C216 C214 C224 P5 -174(4) . . . . ?
C216 C214 C224 C222 0.0 . . . . ?
C216 C218 C220 C222 0.0 . . . . ?
C218 C220 C222 C224 0.0 . . . . ?
C220 C222 C224 P5 174(4) . . . . ?
C220 C222 C224 C214 0.0 . . . . ?
C224 P5 C248 C96 173(4) . . . . ?
C224 P5 C382 C372 -62(2) . . . . ?
C224 P5 C382 C380 118(2) . . . . ?
C224 C214 C216 C218 0.0 . . . . ?
C228 P21 C312 C314 88(3) . . . . ?
C228 P21 C312 C322 -93(3) . . . . ?
C228 C230 C232 C234 0.0 . . . . ?
C230 C228 C238 C236 0.0 . . . . ?
C230 C232 C234 C236 0.0 . . . . ?
C232 C234 C236 C238 0.0 . . . . ?
C234 C236 C238 C228 0.0 . . . . ?
C238 C228 C230 C232 0.0 . . . . ?
C244 C6 C254 C326 -17(9) . . . . ?
C244 C124 C308 C326 13(8) . . . . ?
C246 C54 C174 C392 2(7) . . . . ?
C246 C212 C406 C392 -1(6) . . . . ?
C248 P5 C224 C214 -137(3) . . . . ?
C248 P5 C224 C222 48(4) . . . . ?
C248 P5 C382 C372 47(3) . . . . ?
C248 P5 C382 C380 -133(3) . . . . ?
C254 C6 C244 C124 23(8) . . . . ?
C256 C258 C260 C262 0.0 . . . . ?
C258 C256 C266 P18 178(2) . . . . ?
C258 C256 C266 C264 0.0 . . . . ?
C258 C260 C262 C264 0.0 . . . . ?
C260 C262 C264 C266 0.0 . . . . ?
C262 C264 C266 P18 -178(2) . . . . ?
C262 C264 C266 C256 0.0 . . . . ?
C266 P18 C6 C244 47(5) . . . . ?
C266 P18 C6 C254 -151(4) . . . . ?
C266 P18 C32 C270 -172(3) . . . . ?
C266 C256 C258 C260 0.0 . . . . ?
C274 C170 C178 P9 -178(3) . . . . ?
C274 C170 C178 C168 2(7) . . . . ?
C276 P7 C12 C14 -88(2) . . . . ?
C276 P7 C12 C22 93(2) . . . . ?
C276 P7 C424 C28 7(5) . . . . ?
C276 P7 C424 C410 -180(4) . . . . ?
C278 P9 C178 C168 -75(4) . . . . ?
C278 P9 C178 C170 105(4) . . . . ?
C284 C286 C288 C290 0.0 . . . . ?
C286 C284 C294 P22 175(3) . . . . ?
C286 C284 C294 C292 0.0 . . . . ?
C286 C288 C290 C292 0.0 . . . . ?
C288 C290 C292 C294 0.0 . . . . ?
C290 C292 C294 P22 -174(3) . . . . ?
C290 C292 C294 C284 0.0 . . . . ?
C294 P22 C332 C334 -160(2) . . . . ?
C294 P22 C332 C342 33(3) . . . . ?
C294 C284 C286 C288 0.0 . . . . ?
C296 C298 C300 C302 0.0 . . . . ?
C298 C296 C306 C304 0.0 . . . . ?
C298 C300 C302 P12 -179(2) . . . . ?
C298 C300 C302 C304 0.0 . . . . ?
C300 C302 C304 C306 0.0 . . . . ?
C302 P12 C40 C42 -143.0(19) . . . . ?
C302 P12 C40 C50 38(2) . . . . ?
C302 P12 C122 C104 -168(3) . . . . ?
C302 C304 C306 C296 0.0 . . . . ?
C306 C296 C298 C300 0.0 . . . . ?
C308 C124 C244 C6 -22(8) . . . . ?
C310 C26 C414 C422 9(8) . . . . ?
C312 P21 C228 C230 -174(3) . . . . ?
C312 P21 C228 C238 3(4) . . . . ?
C312 C314 C316 C318 0.0 . . . . ?
C314 C312 C322 C320 0.0 . . . . ?
C314 C316 C318 C320 0.0 . . . . ?
C316 C318 C320 C322 0.0 . . . . ?
C318 C320 C322 C312 0.0 . . . . ?
C322 C312 C314 C316 0.0 . . . . ?
C324 P16 C60 C24 -176(3) . . . . ?
C324 P16 C362 C360 -108(2) . . . . ?
C324 P16 C362 C364 72(3) . . . . ?
C324 C280 C422 C414 9(7) . . . . ?
C332 P22 C294 C284 126(2) . . . . ?
C332 P22 C294 C292 -59(3) . . . . ?
C332 C334 C336 C338 0.0 . . . . ?
C334 C332 C342 C340 0.0 . . . . ?
C334 C336 C338 C340 0.0 . . . . ?
C336 C338 C340 C342 0.0 . . . . ?
C338 C340 C342 C332 0.0 . . . . ?
C342 C332 C334 C336 0.0 . . . . ?
C358 C360 C362 P16 -180(2) . . . . ?
C358 C360 C362 C364 0.0 . . . . ?
C360 C358 C368 C366 0.0 . . . . ?
C360 C362 C364 C366 0.0 . . . . ?
C362 P16 C60 C24 -70(3) . . . . ?
C362 P16 C324 C280 161(3) . . . . ?
C362 P16 C324 C310 -14(5) . . . . ?
C362 C364 C366 C368 0.0 . . . . ?
C364 C366 C368 C358 0.0 . . . . ?
C368 C358 C360 C362 0.0 . . . . ?
C372 C374 C376 C378 0.0 . . . . ?
C374 C372 C382 P5 180.0(2) . . . . ?
C374 C372 C382 C380 0.0 . . . . ?
C374 C376 C378 C380 0.0 . . . . ?
C376 C378 C380 C382 0.0 . . . . ?
C378 C380 C382 P5 180.0(2) . . . . ?
C378 C380 C382 C372 0.0 . . . . ?
C382 P5 C224 C214 -34(3) . . . . ?
C382 P5 C224 C222 151(3) . . . . ?
C382 P5 C248 C96 65(5) . . . . ?
C382 C372 C374 C376 0.0 . . . . ?
C388 C28 C424 P7 -178(4) . . . . ?
C388 C28 C424 C410 9(8) . . . . ?
C388 C58 C398 C410 3(7) . . . . ?
C398 C58 C388 C28 -5(8) . . . . ?
C398 C410 C424 P7 175(4) . . . . ?
C398 C410 C424 C28 -11(8) . . . . ?
C406 C212 C246 C54 5(7) . . . . ?
C414 C26 C310 C324 -3(8) . . . . ?
C422 C280 C324 P16 -179(4) . . . . ?
C422 C280 C324 C310 -3(6) . . . . ?
C424 P7 C12 C14 22(2) . . . . ?
C424 P7 C12 C22 -156(2) . . . . ?
C424 C28 C388 C58 -1(8) . . . . ?
Ag1B S24A C55 C107 -161(6) . . . . ?
Ag1B S24A C55 C419 -57(3) . . . . ?
Ag1B P11 C73 C293 46(4) . . . . ?
Ag1B P11 C73 C297 -133(2) . . . . ?
Ag1B P11 C423 C211 17(2) . . . . ?
Ag1B P11 C423 C53 -163(2) . . . . ?
Ag3 S3 C191 C303 168(5) . . . . ?
Ag3 S3 C191 C189 -95(6) . . . . ?
Ag3 S23 C101 C311 -130(6) . . . . ?
Ag3 S23 C101 C407 121(7) . . . . ?
Ag11 S24 C219 C19 178(3) . . . . ?
Ag11 S24 C219 C381 57(3) . . . . ?
Ag11 P3 C141 C139 -11(5) . . . . ?
Ag11 P3 C141 C343 168(3) . . . . ?
Ag11 P3 C85 C399 -62(4) . . . . ?
Ag11 P3 C371 C93 143(2) . . . . ?
Ag11 P3 C371 C47 -40(2) . . . . ?
Ag13 S3 C191 C303 73(6) . . . . ?
Ag13 S3 C191 C189 170(6) . . . . ?
Ag14 S1 C333 C395 150(3) . . . . ?
Ag14 S1 C333 C397 -82(4) . . . . ?
Ag14 P4 C217 C27 -166(3) . . . . ?
Ag14 P4 C217 C221 12(4) . . . . ?
Ag14 P4 C109 C213 -71(3) . . . . ?
Ag14 P4 C325 C163 52.1(18) . . . . ?
Ag14 P4 C325 C165 -123.6(16) . . . . ?
Ag16 S4 C129 C357 -164.2(16) . . . . ?
Ag16 S4 C129 C203 66(3) . . . . ?
Ag16 P8 C237 C279 -10(4) . . . . ?
Ag16 P8 C237 C417 163(3) . . . . ?
Ag16 P8 C315 C213 57(3) . . . . ?
Ag16 P8 C179 C359 121.4(16) . . . . ?
Ag16 P8 C179 C363 -59.6(17) . . . . ?
Ag19 S19 C43 C63 151(4) . . . . ?
Ag19 S19 C43 C151 47(5) . . . . ?
Ag21 S19 C43 C63 46(5) . . . . ?
Ag21 S19 C43 C151 -58(5) . . . . ?
Ag22 S16 C255 C313 -60(4) . . . . ?
Ag22 S16 C255 C205 84(3) . . . . ?
Ag22 P10 C15 C259 -57(3) . . . . ?
Ag22 P10 C75 C345 133(4) . . . . ?
Ag22 P10 C75 C349 -38(4) . . . . ?
Ag22 P10 C323 C159 123.1(15) . . . . ?
Ag22 P10 C323 C161 -57.3(16) . . . . ?
Ag25 S11 C201 C115 168(4) . . . . ?
Ag25 S11 C201 C39 -74(4) . . . . ?
Ag26 S1 C333 C395 -75(3) . . . . ?
Ag26 S1 C333 C397 53(4) . . . . ?
Ag26 P23 C253 C309 60(3) . . . . ?
Ag26 P23 C2 C65 141(3) . . . . ?
Ag26 P23 C2 C169 -21(4) . . . . ?
Ag26 P23 C83 C111 135(4) . . . . ?
Ag26 P23 C83 C25 -56(4) . . . . ?
Ag28 S4 C129 C357 -50(3) . . . . ?
Ag28 S4 C129 C203 -179.6(16) . . . . ?
Ag28 S24 C219 C19 57(3) . . . . ?
Ag28 S24 C219 C381 -64(3) . . . . ?
Ag28 S24A C55 C107 -37(7) . . . . ?
Ag28 S24A C55 C419 67(4) . . . . ?
Ag31 S3 C191 C303 -38(6) . . . . ?
Ag31 S3 C191 C189 59(6) . . . . ?
Ag31 S16 C255 C313 66(4) . . . . ?
Ag31 S16 C255 C205 -151(2) . . . . ?
Ag31 P15 C121 C243 -16(2) . . . . ?
Ag31 P15 C121 C247 159(2) . . . . ?
Ag31 P15 C271 C135 -170(2) . . . . ?
Ag31 P15 C271 C17 10(3) . . . . ?
Ag32 S1 C333 C395 36(3) . . . . ?
Ag32 S1 C333 C397 164(3) . . . . ?
Ag32 S16 C255 C313 174(3) . . . . ?
Ag32 S16 C255 C205 -42(4) . . . . ?
Ag40 S6 C411 C103 110(2) . . . . ?
Ag40 S6 C411 C413 -109.9(18) . . . . ?
Ag40 P6 C223 C7 164.7(15) . . . . ?
Ag40 P6 C223 C57 -19(2) . . . . ?
Ag40 P6 C307 C309 62(3) . . . . ?
Ag40 P6 C175 C351 105.6(18) . . . . ?
Ag40 P6 C175 C355 -72(2) . . . . ?
Ag41 S24 C219 C19 -30(3) . . . . ?
Ag41 S24 C219 C381 -151(3) . . . . ?
Ag41 P11 C73 C293 25(4) . . . . ?
Ag41 P11 C73 C297 -153(2) . . . . ?
Ag41 P11 C423 C211 17.5(18) . . . . ?
Ag41 P11 C423 C53 -162.5(18) . . . . ?
Ag42 S11 C201 C115 2(4) . . . . ?
Ag42 S11 C201 C39 120(4) . . . . ?
Ag42 P1 C215 C259 64(3) . . . . ?
Ag42 P1 C285 C143 -159.4(15) . . . . ?
Ag42 P1 C285 C145 19(2) . . . . ?
Ag42 P1 C305 C153 -138(3) . . . . ?
Ag42 P1 C305 C383 32(4) . . . . ?
Ag43 P19 C263 C33 -44(3) . . . . ?
Ag43 P19 C263 C67 142(3) . . . . ?
Ag43 P19 C331 C171 -41(7) . . . . ?
Ag47 S4 C129 C357 66(2) . . . . ?
Ag47 S4 C129 C203 -64(3) . . . . ?
Ag47 P14 C231 C29 -4(2) . . . . ?
Ag47 P14 C231 C59 176.9(15) . . . . ?
Ag47 P14 C241 C35 79(4) . . . . ?
Ag47 P14 C241 C317 -93(4) . . . . ?
Ag47 P14 C283 C277 74(3) . . . . ?
Ag48 S6 C411 C103 -10(3) . . . . ?
Ag48 S6 C411 C413 130.5(14) . . . . ?
Ag49 S11 C201 C115 -89(4) . . . . ?
Ag49 S11 C201 C39 29(4) . . . . ?
Ag51 S23 C101 C311 -42(7) . . . . ?
Ag51 S23 C101 C407 -151(6) . . . . ?
Ag52 S6 C411 C103 -139.5(18) . . . . ?
Ag52 S6 C411 C413 1(2) . . . . ?
Ag52 P2 C69 C335 4(5) . . . . ?
Ag52 P2 C69 C21 169(4) . . . . ?
Ag52 P2 C79 C277 -71(3) . . . . ?
Ag52 P2 C365 C183 163.5(18) . . . . ?
Ag52 P2 C365 C185 -31(2) . . . . ?
Ag53 W25 O59 W16 -24(4) . . . . ?
Ag53 W25 O103 Ag42 169(2) . . . . ?
Ag60 P19 C263 C33 -24(3) . . . . ?
Ag60 P19 C263 C67 162(2) . . . . ?
Ag60 P19 C331 C171 -65(7) . . . . ?
Ag62 S24A C55 C107 64(6) . . . . ?
Ag62 S24A C55 C419 169(3) . . . . ?
Ag62 P3 C141 C139 -14(5) . . . . ?
Ag62 P3 C141 C343 165(3) . . . . ?
Ag62 P3 C85 C399 -75(4) . . . . ?
Ag62 P3 C371 C93 158.7(19) . . . . ?
Ag62 P3 C371 C47 -24(3) . . . . ?
P1 C215 C259 C15 158(3) . . . . ?
P1 C285 C143 C287 179(2) . . . . ?
P1 C285 C145 C289 -179(2) . . . . ?
P1 C305 C153 C119 177(3) . . . . ?
P1 C305 C383 C385 179(4) . . . . ?
P2 C69 C335 C249 176(4) . . . . ?
P2 C69 C21 C149 -175(5) . . . . ?
P2 C365 C183 C367 165(3) . . . . ?
P2 C365 C185 C369 -165(3) . . . . ?
P3 C141 C343 C339 177(3) . . . . ?
P3 C85 C399 C173 -179(4) . . . . ?
P3 C371 C93 C373 177(3) . . . . ?
P3 C371 C47 C375 -177(3) . . . . ?
P4 C217 C221 C31 179(3) . . . . ?
P4 C325 C163 C327 -176(2) . . . . ?
P4 C325 C165 C329 176(2) . . . . ?
P6 C223 C7 C225 176(3) . . . . ?
P6 C223 C57 C227 -176(2) . . . . ?
P6 C307 C309 C253 102(4) . . . . ?
P6 C175 C351 C11 -178(3) . . . . ?
P6 C175 C355 C177 178(3) . . . . ?
P8 C237 C279 C415 178(3) . . . . ?
P8 C237 C417 C71 179(3) . . . . ?
P8 C179 C359 C45 179(2) . . . . ?
P8 C179 C363 C181 -179(2) . . . . ?
P10 C15 C259 C215 -172(3) . . . . ?
P10 C75 C345 C81 -168(4) . . . . ?
P10 C75 C349 C347 166(3) . . . . ?
P11 C73 C293 C147 -178(5) . . . . ?
P11 C73 C297 C37 178(4) . . . . ?
P11 C423 C53 C425 180.0(3) . . . . ?
P14 C231 C29 C233 -179(2) . . . . ?
P14 C231 C59 C235 179(2) . . . . ?
P14 C241 C35 C403 179(4) . . . . ?
P14 C241 C317 C291 176(3) . . . . ?
P15 C121 C243 C61 176(3) . . . . ?
P15 C121 C247 C123 -175(3) . . . . ?
P15 C271 C17 C273 -180(4) . . . . ?
P15 C173 C399 C85 162(4) . . . . ?
P19 C263 C33 C265 -174(4) . . . . ?
P19 C263 C67 C267 174(4) . . . . ?
P19 C331 C171 C207 -158(7) . . . . ?
P19 C193 C387 C97 173(4) . . . . ?
P19 C193 C391 C195 -174(4) . . . . ?
P23 C253 C309 C307 86(4) . . . . ?
P23 C2 C65 C167 177(4) . . . . ?
P23 C2 C169 C337 -175(4) . . . . ?
P23 C83 C25 C401 -179(4) . . . . ?
O44 W16 O59 W25 162(4) . . . . ?
O44 W16 O99 Ag22 30.0(15) . . . . ?
O44 W16 O99 Ag56 174.6(10) . . . . ?
O47 W18 O57 W22 168(3) . . . . ?
O47 W18 O79 Ag8 171.4(10) . . . . ?
O47 W18 O79 Ag11 -2.1(14) . . . . ?
O47 W18 O79 Ag62 21.0(14) . . . . ?
O49 W23 O51 W17 130(2) . . . . ?
O49 W23 O71 W30 -74.4(14) . . . . ?
O49 W29 O65 W30 76.4(13) . . . . ?
O49 W29 O81 W25 16(4) . . . . ?
O51 W17 O83 Ag1B 162(2) . . . . ?
O51 W17 O83 Ag8 -3(4) . . . . ?
O51 W17 O83 Ag41 140(2) . . . . ?
O51 W23 O49 W29 -90.1(14) . . . . ?
O51 W23 O71 W30 18(3) . . . . ?
O53 W22 O61 W16 -85.2(12) . . . . ?
O53 W22 O61 Ag32 116.2(10) . . . . ?
O53 W22 O77 Ag31 163(3) . . . . ?
O53 W22 O77 Ag39 -55(5) . . . . ?
O53 W22 O77 Ag56 10(4) . . . . ?
O53 W22 O93 Ag14 -19.2(13) . . . . ?
O53 W30 O55 W16 24(2) . . . . ?
O55 W16 O59 W25 -103(4) . . . . ?
O55 W16 O99 Ag22 -139(2) . . . . ?
O55 W16 O99 Ag56 6(3) . . . . ?
O57 W18 O47 Ag16 119.9(17) . . . . ?
O57 W18 O79 Ag8 -85.9(11) . . . . ?
O57 W18 O79 Ag11 100.6(12) . . . . ?
O57 W18 O79 Ag62 123.7(12) . . . . ?
O57 W22 O61 W16 -36(3) . . . . ?
O57 W22 O61 Ag32 165.5(17) . . . . ?
O57 W22 O77 Ag31 -122.9(11) . . . . ?
O57 W22 O77 Ag39 19(3) . . . . ?
O57 W22 O77 Ag56 84.3(10) . . . . ?
O57 W22 O93 Ag14 -99.8(12) . . . . ?
O59 W16 O99 Ag22 135.3(13) . . . . ?
O59 W16 O99 Ag56 -80.1(10) . . . . ?
O59 W25 O103 Ag42 -123.0(14) . . . . ?
O59 W25 O103 Ag53 68.0(13) . . . . ?
O59 W25 O103 Ag58 88.1(11) . . . . ?
O61 W16 O59 W25 -54(5) . . . . ?
O61 W16 O99 Ag22 -69.1(13) . . . . ?
O61 W16 O99 Ag56 75.5(10) . . . . ?
O61 W22 O77 Ag31 79.1(11) . . . . ?
O61 W22 O77 Ag39 -139(3) . . . . ?
O61 W22 O77 Ag56 -73.6(10) . . . . ?
O61 W22 O93 Ag14 64.7(13) . . . . ?
O63 W23 O49 W29 168.9(13) . . . . ?
O63 W23 O51 W17 -127(2) . . . . ?
O63 W23 O71 W30 -177.2(13) . . . . ?
O65 W29 O81 W25 120(2) . . . . ?
O65 W30 O55 W16 -134(2) . . . . ?
O67 W23 O49 W29 -5.5(11) . . . . ?
O67 W23 O51 W17 57(2) . . . . ?
O67 W23 O71 W30 -1.7(11) . . . . ?
O67 W29 O65 W30 3.7(11) . . . . ?
O67 W29 O81 W25 47(2) . . . . ?
O67 W30 O55 W16 -63(2) . . . . ?
O67 Si3 O80 W16 -67.8(15) . . . . ?
O67 Si3 O80 W22 68.2(17) . . . . ?
O67 Si3 O80 Ag56 -175.0(9) . . . . ?
O67 Si3 O86 W25 69.8(15) . . . . ?
O67 Si3 O86 W27 -69.3(17) . . . . ?
O67 Si3 O86 Ag53 163.3(10) . . . . ?
O67 Si3 O101 W17 72.0(15) . . . . ?
O67 Si3 O101 W18 -74.5(15) . . . . ?
O69 W29 O65 W30 174.3(13) . . . . ?
O69 W29 O81 W25 -136(2) . . . . ?
O71 W23 O49 W29 66.7(14) . . . . ?
O71 W23 O51 W17 38(4) . . . . ?
O71 W30 O55 W16 -60(4) . . . . ?
O73 W17 O83 Ag1B 88.6(17) . . . . ?
O73 W17 O83 Ag8 -76.8(11) . . . . ?
O73 W17 O83 Ag41 66.6(14) . . . . ?
O73 W18 O47 Ag16 -40.9(18) . . . . ?
O73 W18 O57 W22 -61(5) . . . . ?
O73 W18 O79 Ag8 73.4(10) . . . . ?
O73 W18 O79 Ag11 -100.1(12) . . . . ?
O73 W18 O79 Ag62 -76.9(12) . . . . ?
O75 W30 O55 W16 128(2) . . . . ?
O77 W22 O61 W16 80.0(13) . . . . ?
O77 W22 O61 Ag32 -78.6(11) . . . . ?
O77 W22 O93 Ag14 161.6(12) . . . . ?
O79 W18 O47 Ag16 -139.7(17) . . . . ?
O79 W18 O57 W22 64(4) . . . . ?
O80 W16 O59 W25 -26(4) . . . . ?
O80 W16 O99 Ag22 -140.2(13) . . . . ?
O80 W16 O99 Ag56 4.4(9) . . . . ?
O80 W22 O61 W16 -5.0(11) . . . . ?
O80 W22 O61 Ag32 -163.5(11) . . . . ?
O80 W22 O77 Ag31 152.5(11) . . . . ?
O80 W22 O77 Ag39 -66(3) . . . . ?
O80 W22 O77 Ag56 -0.2(9) . . . . ?
O80 W22 O93 Ag14 22(5) . . . . ?
O80 Si3 O67 W23 -118.6(12) . . . . ?
O80 Si3 O67 W29 118.7(13) . . . . ?
O80 Si3 O67 W30 -1.3(15) . . . . ?
O80 Si3 O86 W25 -50.0(17) . . . . ?
O80 Si3 O86 W27 170.9(13) . . . . ?
O80 Si3 O86 Ag53 43.5(13) . . . . ?
O80 Si3 O101 W17 -171.0(12) . . . . ?
O80 Si3 O101 W18 42.5(17) . . . . ?
O81 W25 O59 W16 105(4) . . . . ?
O81 W25 O103 Ag42 147(2) . . . . ?
O81 W25 O103 Ag53 -22(4) . . . . ?
O81 W25 O103 Ag58 -2(4) . . . . ?
O81 W29 O65 W30 -81.2(14) . . . . ?
O85 W25 O59 W16 -162(4) . . . . ?
O85 W25 O103 Ag42 -19.8(17) . . . . ?
O85 W25 O103 Ag53 171.2(13) . . . . ?
O85 W25 O103 Ag58 -168.8(11) . . . . ?
O86 W25 O59 W16 27(4) . . . . ?
O86 W25 O103 Ag42 150.2(15) . . . . ?
O86 W25 O103 Ag53 -18.8(12) . . . . ?
O86 W25 O103 Ag58 1.2(10) . . . . ?
O86 W27 O89 Ag52 -20(4) . . . . ?
O86 W27 O97 W17 -22(4) . . . . ?
O86 W27 O110 Ag43 -152.4(15) . . . . ?
O86 W27 O110 Ag58 1.9(11) . . . . ?
O86 W27 O110 Ag60 -140.4(10) . . . . ?
O86 Si3 O67 W23 117.8(12) . . . . ?
O86 Si3 O67 W29 -4.9(16) . . . . ?
O86 Si3 O67 W30 -124.9(12) . . . . ?
O86 Si3 O80 W16 51.5(17) . . . . ?
O86 Si3 O80 W22 -172.6(13) . . . . ?
O86 Si3 O80 Ag56 -55.8(13) . . . . ?
O86 Si3 O101 W17 -44.6(17) . . . . ?
O86 Si3 O101 W18 168.9(12) . . . . ?
O87 W18 O47 Ag16 41.4(18) . . . . ?
O87 W18 O57 W22 -98(3) . . . . ?
O87 W18 O79 Ag8 -12(3) . . . . ?
O87 W18 O79 Ag11 174(2) . . . . ?
O87 W18 O79 Ag62 -162(2) . . . . ?
O87 W23 O49 W29 -10(3) . . . . ?
O87 W23 O51 W17 -26(2) . . . . ?
O87 W23 O71 W30 81.6(13) . . . . ?
O89 W27 O97 W17 169(4) . . . . ?
O89 W27 O110 Ag43 17.8(17) . . . . ?
O89 W27 O110 Ag58 172.1(11) . . . . ?
O89 W27 O110 Ag60 29.8(13) . . . . ?
O91 W17 O83 Ag1B -5.0(19) . . . . ?
O91 W17 O83 Ag8 -170.3(11) . . . . ?
O91 W17 O83 Ag41 -27.0(16) . . . . ?
O93 W22 O61 W16 -176.8(12) . . . . ?
O93 W22 O61 Ag32 24.6(11) . . . . ?
O93 W22 O77 Ag31 -20.0(13) . . . . ?
O93 W22 O77 Ag39 122(3) . . . . ?
O93 W22 O77 Ag56 -172.7(10) . . . . ?
O95 W25 O59 W16 60(5) . . . . ?
O95 W25 O103 Ag42 78.8(15) . . . . ?
O95 W25 O103 Ag53 -90.2(13) . . . . ?
O95 W25 O103 Ag58 -70.1(11) . . . . ?
O95 W27 O89 Ag52 -57.1(10) . . . . ?
O95 W27 O97 W17 -59(5) . . . . ?
O95 W27 O110 Ag43 -77.5(15) . . . . ?
O95 W27 O110 Ag58 76.8(11) . . . . ?
O95 W27 O110 Ag60 -65.4(11) . . . . ?
O97 W17 O83 Ag1B -113.2(17) . . . . ?
O97 W17 O83 Ag8 81.5(12) . . . . ?
O97 W17 O83 Ag41 -135.2(13) . . . . ?
O97 W27 O89 Ag52 105.2(10) . . . . ?
O97 W27 O110 Ag43 122.1(15) . . . . ?
O97 W27 O110 Ag58 -83.6(12) . . . . ?
O97 W27 O110 Ag60 134.1(11) . . . . ?
O99 W16 O59 W25 58(4) . . . . ?
O101 W17 O83 Ag1B 160.6(17) . . . . ?
O101 W17 O83 Ag8 -4.8(10) . . . . ?
O101 W17 O83 Ag41 138.6(13) . . . . ?
O101 W18 O47 Ag16 -7(5) . . . . ?
O101 W18 O57 W22 -23(3) . . . . ?
O101 W18 O79 Ag8 1.7(9) . . . . ?
O101 W18 O79 Ag11 -171.8(11) . . . . ?
O101 W18 O79 Ag62 -148.7(12) . . . . ?
O101 Si3 O67 W23 -1.0(15) . . . . ?
O101 Si3 O67 W29 -123.7(13) . . . . ?
O101 Si3 O67 W30 116.3(12) . . . . ?
O101 Si3 O80 W16 175.6(11) . . . . ?
O101 Si3 O80 W22 -48.4(18) . . . . ?
O101 Si3 O80 Ag56 68.4(11) . . . . ?
O101 Si3 O86 W25 -173.4(11) . . . . ?
O101 Si3 O86 W27 47.4(18) . . . . ?
O101 Si3 O86 Ag53 -79.9(11) . . . . ?
O103 W25 O59 W16 -58(4) . . . . ?
O106 W27 O89 Ag52 25.2(10) . . . . ?
O106 W27 O97 W17 -101(4) . . . . ?
O106 W27 O110 Ag43 -165(4) . . . . ?
O106 W27 O110 Ag58 -10(5) . . . . ?
O106 W27 O110 Ag60 -153(4) . . . . ?
O106 W29 O65 W30 13(3) . . . . ?
O106 W29 O81 W25 -36(2) . . . . ?
O110 W27 O89 Ag52 -155.3(10) . . . . ?
O110 W27 O97 W17 66(4) . . . . ?
C215 P1 C285 C143 -33(2) . . . . ?
C215 P1 C285 C145 145.9(19) . . . . ?
C215 P1 C305 C153 101(4) . . . . ?
C215 P1 C305 C383 -89(4) . . . . ?
C27 C217 C221 C31 -4(6) . . . . ?
C217 P4 C109 C213 56(3) . . . . ?
C217 P4 C325 C163 -67(2) . . . . ?
C217 P4 C325 C165 117(2) . . . . ?
C217 C27 C281 C257 -6(6) . . . . ?
C217 C221 C31 C257 -4(6) . . . . ?
C109 P4 C217 C27 60(3) . . . . ?
C109 P4 C217 C221 -123(3) . . . . ?
C109 P4 C325 C163 -173.0(18) . . . . ?
C109 P4 C325 C165 11(2) . . . . ?
C109 C213 C315 P8 159(2) . . . . ?
C221 C31 C257 C281 7(6) . . . . ?
C111 C83 C25 C401 -10(8) . . . . ?
C223 P6 C307 C309 -65(3) . . . . ?
C223 P6 C175 C351 -127(2) . . . . ?
C223 P6 C175 C355 55(2) . . . . ?
C223 C7 C225 C113 0.0 . . . . ?
C7 C223 C57 C227 0.0 . . . . ?
C7 C225 C113 C227 0.0 . . . . ?
C225 C113 C227 C57 0.0 . . . . ?
C113 C227 C57 C223 0.0 . . . . ?
C57 C223 C7 C225 0.0 . . . . ?
C229 C249 C335 C69 -4(9) . . . . ?
C229 C149 C21 C69 3(10) . . . . ?
C231 P14 C241 C35 -159(4) . . . . ?
C231 P14 C241 C317 29(4) . . . . ?
C231 P14 C283 C277 -56(3) . . . . ?
C231 C29 C233 C117 0.0 . . . . ?
C29 C231 C59 C235 0.0 . . . . ?
C29 C233 C117 C235 0.0 . . . . ?
C233 C117 C235 C59 0.0 . . . . ?
C117 C235 C59 C231 0.0 . . . . ?
C59 C231 C29 C233 0.0 . . . . ?
C237 P8 C315 C213 -64(3) . . . . ?
C237 P8 C179 C359 -121(2) . . . . ?
C237 P8 C179 C363 58(2) . . . . ?
C237 C279 C415 C301 -5(8) . . . . ?
C119 C3 C385 C383 -14(8) . . . . ?
C15 P10 C75 C345 -3(4) . . . . ?
C15 P10 C75 C349 -173(3) . . . . ?
C15 P10 C323 C159 -112.3(19) . . . . ?
C15 P10 C323 C161 67.3(19) . . . . ?
C241 P14 C231 C29 -123(2) . . . . ?
C241 P14 C231 C59 59(2) . . . . ?
C241 P14 C283 C277 -166(3) . . . . ?
C241 C35 C403 C269 8(8) . . . . ?
C121 P15 C271 C135 65(3) . . . . ?
C121 P15 C271 C17 -115(3) . . . . ?
C121 C243 C61 C245 0.0 . . . . ?
C243 C121 C247 C123 0.0 . . . . ?
C243 C61 C245 C123 0.0 . . . . ?
C61 C245 C123 C247 0.0 . . . . ?
C245 C123 C247 C121 0.0 . . . . ?
C247 C121 C243 C61 0.0 . . . . ?
C31 C257 C281 C27 -2(7) . . . . ?
C249 C229 C149 C21 3(9) . . . . ?
C253 P23 C2 C65 -94(4) . . . . ?
C253 P23 C2 C169 103(4) . . . . ?
C253 P23 C83 C111 11(5) . . . . ?
C253 P23 C83 C25 -180(4) . . . . ?
C2 P23 C253 C309 -67(4) . . . . ?
C2 P23 C83 C111 -96(5) . . . . ?
C2 P23 C83 C25 73(4) . . . . ?
C2 C65 C167 C393 11(7) . . . . ?
C65 C2 C169 C337 22(7) . . . . ?
C65 C167 C393 C337 -3(8) . . . . ?
C263 P19 C331 C171 73(7) . . . . ?
C263 C33 C265 C133 0.0 . . . . ?
C33 C263 C67 C267 0.0 . . . . ?
C33 C265 C133 C267 0.0 . . . . ?
C265 C133 C267 C67 0.0 . . . . ?
C133 C267 C67 C263 0.0 . . . . ?
C67 C263 C33 C265 0.0 . . . . ?
C269 C291 C317 C241 0(7) . . . . ?
C135 C271 C17 C273 0.0 . . . . ?
C271 P15 C121 C243 111.0(18) . . . . ?
C271 P15 C121 C247 -74(3) . . . . ?
C271 C135 C275 O14 135(4) . . . 1_545 ?
C271 C135 C275 C137 0.0 . . . . ?
C271 C17 C273 C137 0.0 . . . . ?
C17 C273 C137 C275 0.0 . . . . ?
C273 C137 C275 O14 -136(4) . . . 1_545 ?
C273 C137 C275 C135 0.0 . . . . ?
C275 C135 C271 P15 180(4) . . . . ?
C275 C135 C271 C17 0.0 . . . . ?
C69 P2 C79 C277 59(4) . . . . ?
C69 P2 C365 C183 36(3) . . . . ?
C69 P2 C365 C185 -159(3) . . . . ?
C139 C141 C343 C339 -4(7) . . . . ?
C279 C237 C417 C71 -7(6) . . . . ?
C35 C241 C317 C291 4(7) . . . . ?
C281 C27 C217 P4 -174(3) . . . . ?
C281 C27 C217 C221 9(6) . . . . ?
C141 P3 C85 C399 174(4) . . . . ?
C141 P3 C371 C93 -90(3) . . . . ?
C141 P3 C371 C47 87(3) . . . . ?
C141 C139 C89 C341 1(7) . . . . ?
C283 P14 C231 C29 129(2) . . . . ?
C283 P14 C231 C59 -50(2) . . . . ?
C283 P14 C241 C35 -49(4) . . . . ?
C283 P14 C241 C317 139(4) . . . . ?
C283 C277 C79 P2 -161(3) . . . . ?
C71 C301 C415 C279 9(8) . . . . ?
C285 P1 C215 C259 -67(3) . . . . ?
C285 P1 C305 C153 -8(4) . . . . ?
C285 P1 C305 C383 162(4) . . . . ?
C285 C143 C287 C9 0.0 . . . . ?
C143 C285 C145 C289 0.0 . . . . ?
C143 C287 C9 C289 0.0 . . . . ?
C287 C9 C289 C145 0.0 . . . . ?
C9 C289 C145 C285 0.0 . . . . ?
C145 C285 C143 C287 0.0 . . . . ?
C291 C269 C403 C35 -3(8) . . . . ?
C73 P11 C423 C211 138.7(18) . . . . ?
C73 P11 C423 C53 -41.3(18) . . . . ?
C73 C293 C147 C295 0.0 . . . . ?
C293 C73 C297 C37 0.0 . . . . ?
C293 C147 C295 C37 0.0 . . . . ?
C147 C295 C37 C297 0.0 . . . . ?
C295 C37 C297 C73 0.0 . . . . ?
C297 C73 C293 C147 0.0 . . . . ?
C149 C229 C249 C335 -2(9) . . . . ?
C75 P10 C15 C259 77(3) . . . . ?
C75 P10 C323 C159 -1(2) . . . . ?
C75 P10 C323 C161 178.9(19) . . . . ?
C301 C71 C417 C237 10(6) . . . . ?
C305 P1 C215 C259 -175(3) . . . . ?
C305 P1 C285 C143 75(2) . . . . ?
C305 P1 C285 C145 -107(2) . . . . ?
C305 C383 C385 C3 14(7) . . . . ?
C153 C119 C3 C385 11(8) . . . . ?
C153 C305 C383 C385 -11(7) . . . . ?
C307 P6 C223 C7 -68(2) . . . . ?
C307 P6 C223 C57 108(2) . . . . ?
C307 P6 C175 C351 -20(3) . . . . ?
C307 P6 C175 C355 162(2) . . . . ?
C315 P8 C237 C279 118(4) . . . . ?
C315 P8 C237 C417 -68(4) . . . . ?
C315 P8 C179 C359 -10(2) . . . . ?
C315 P8 C179 C363 168.5(18) . . . . ?
C315 C213 C109 P4 -167(2) . . . . ?
C79 P2 C69 C335 -127(4) . . . . ?
C79 P2 C69 C21 39(5) . . . . ?
C79 P2 C365 C183 -72(3) . . . . ?
C79 P2 C365 C185 93(3) . . . . ?
C79 C277 C283 P14 177(3) . . . . ?
C317 C241 C35 C403 -9(7) . . . . ?
C159 C319 C5 C321 0.0 . . . . ?
C319 C159 C323 P10 180(2) . . . . ?
C319 C159 C323 C161 0.0 . . . . ?
C319 C5 C321 C161 0.0 . . . . ?
C5 C321 C161 C323 0.0 . . . . ?
C321 C161 C323 P10 -180(2) . . . . ?
C321 C161 C323 C159 0.0 . . . . ?
C323 P10 C15 C259 -178(2) . . . . ?
C323 P10 C75 C345 -106(4) . . . . ?
C323 P10 C75 C349 83(4) . . . . ?
C323 C159 C319 C5 0.0 . . . . ?
C325 P4 C217 C27 -47(4) . . . . ?
C325 P4 C217 C221 130(3) . . . . ?
C325 P4 C109 C213 163(2) . . . . ?
C325 C163 C327 C41 0.0 . . . . ?
C163 C325 C165 C329 0.0 . . . . ?
C163 C327 C41 C329 0.0 . . . . ?
C327 C41 C329 C165 0.0 . . . . ?
C41 C329 C165 C325 0.0 . . . . ?
C165 C325 C163 C327 0.0 . . . . ?
C331 P19 C263 C33 -165(4) . . . . ?
C331 P19 C263 C67 21(5) . . . . ?
C331 C171 C207 P11 171(5) . . . . ?
C83 P23 C253 C309 -178(3) . . . . ?
C83 P23 C2 C65 16(4) . . . . ?
C83 P23 C2 C169 -146(4) . . . . ?
C83 C111 C199 C261 -18(10) . . . . ?
C83 C25 C401 C261 2(8) . . . . ?
C335 C69 C21 C149 -9(9) . . . . ?
C21 C69 C335 C249 9(8) . . . . ?
C169 C2 C65 C167 -20(7) . . . . ?
C169 C337 C393 C167 5(8) . . . . ?
C339 C341 C89 C139 0(7) . . . . ?
C85 P3 C141 C139 106(5) . . . . ?
C85 P3 C141 C343 -75(4) . . . . ?
C85 P3 C371 C93 26(3) . . . . ?
C85 P3 C371 C47 -157(2) . . . . ?
C341 C339 C343 C141 4(7) . . . . ?
C343 C339 C341 C89 -2(7) . . . . ?
C345 C75 C349 C347 -4(7) . . . . ?
C345 C81 C87 C347 3(7) . . . . ?
C173 P15 C121 C243 -130.8(18) . . . . ?
C173 P15 C121 C247 45(3) . . . . ?
C173 P15 C271 C135 -35(4) . . . . ?
C173 P15 C271 C17 145(3) . . . . ?
C87 C81 C345 C75 -1(7) . . . . ?
C87 C347 C349 C75 7(7) . . . . ?
C349 C75 C345 C81 1(7) . . . . ?
C349 C347 C87 C81 -6(7) . . . . ?
C175 P6 C223 C7 38(2) . . . . ?
C175 P6 C223 C57 -145.7(18) . . . . ?
C175 P6 C307 C309 -173(3) . . . . ?
C175 C351 C11 C353 0.0 . . . . ?
C351 C175 C355 C177 0.0 . . . . ?
C351 C11 C353 C177 0.0 . . . . ?
C11 C353 C177 C355 0.0 . . . . ?
C353 C177 C355 C175 0.0 . . . . ?
C355 C175 C351 C11 0.0 . . . . ?
C89 C139 C141 P3 -180(3) . . . . ?
C89 C139 C141 C343 1(7) . . . . ?
C179 P8 C237 C279 -131(4) . . . . ?
C179 P8 C237 C417 42(4) . . . . ?
C179 P8 C315 C213 -176(2) . . . . ?
C179 C359 C45 C361 0.0 . . . . ?
C359 C179 C363 C181 0.0 . . . . ?
C359 C45 C361 C181 0.0 . . . . ?
C45 C361 C181 C363 0.0 . . . . ?
C361 C181 C363 C179 0.0 . . . . ?
C363 C179 C359 C45 0.0 . . . . ?
C365 P2 C69 C335 129(4) . . . . ?
C365 P2 C69 C21 -66(5) . . . . ?
C365 P2 C79 C277 167(3) . . . . ?
C365 C183 C367 C23 0.0 . . . . ?
C183 C365 C185 C369 0.0 . . . . ?
C183 C367 C23 C369 0.0 . . . . ?
C367 C23 C369 C185 0.0 . . . . ?
C23 C369 C185 C365 0.0 . . . . ?
C185 C365 C183 C367 0.0 . . . . ?
C371 P3 C141 C139 -132(4) . . . . ?
C371 P3 C141 C343 47(4) . . . . ?
C371 P3 C85 C399 56(4) . . . . ?
C371 C93 C373 C187 0.0 . . . . ?
C93 C371 C47 C375 0.0 . . . . ?
C93 C373 C187 C375 0.0 . . . . ?
C373 C187 C375 C47 0.0 . . . . ?
C187 C375 C47 C371 0.0 . . . . ?
C47 C371 C93 C373 0.0 . . . . ?
C383 C305 C153 C119 7(6) . . . . ?
C3 C119 C153 C305 -7(7) . . . . ?
C193 P19 C263 C33 84(3) . . . . ?
C193 P19 C263 C67 -91(3) . . . . ?
C193 P19 C331 C171 -180(6) . . . . ?
C193 C387 C97 C389 0.0 . . . . ?
C387 C193 C391 C195 0.0 . . . . ?
C387 C97 C389 C195 0.0 . . . . ?
C97 C389 C195 C391 0.0 . . . . ?
C389 C195 C391 C193 0.0 . . . . ?
C391 C193 C387 C97 0.0 . . . . ?
C393 C337 C169 C2 -15(8) . . . . ?
C199 C111 C83 P23 -176(4) . . . . ?
C199 C111 C83 C25 16(7) . . . . ?
C199 C261 C401 C25 -1(8) . . . . ?
C401 C261 C199 C111 11(10) . . . . ?
C403 C269 C291 C317 -1(8) . . . . ?
C207 P11 C73 C293 172(4) . . . . ?
C207 P11 C73 C297 -6(4) . . . . ?
C207 P11 C423 C211 -108(3) . . . . ?
C207 P11 C423 C53 72(3) . . . . ?
C417 C237 C279 C415 4(6) . . . . ?
C417 C71 C301 C415 -11(7) . . . . ?
O19 Si1 O20 O19 179.994(6) . . . 2_486 ?
O19 Si1 O20 O21 66(3) . . . 2_486 ?
O19 Si1 O20 O21 -114(3) 2_486 . . 2_486 ?
O19 Si1 O21 O20 -60.2(19) . . . 2_486 ?
O19 Si1 O21 O20 119.8(19) 2_486 . . 2_486 ?
O19 Si1 O21 O22 -122(2) 2_486 . . 2_486 ?
O19 Si1 O21 O22 58(2) . . . 2_486 ?
O19 Si1 O22 O19 -179.992(14) . . . 2_486 ?
O19 Si1 O22 O21 -64(4) . . . 2_486 ?
O19 Si1 O22 O21 116(4) 2_486 . . 2_486 ?
O20 Si1 O19 O20 179.998(3) . . . 2_486 ?
O20 Si1 O19 O22 -118(3) 2_486 . . 2_486 ?
O20 Si1 O19 O22 62(3) . . . 2_486 ?
O20 Si1 O21 O20 180.00(3) . . . 2_486 ?
O20 Si1 O21 O22 -61(3) . . . 2_486 ?
O20 Si1 O21 O22 119(3) 2_486 . . 2_486 ?
O20 Si1 O22 O19 122(2) 2_486 . . 2_486 ?
O20 Si1 O22 O19 -58(2) . . . 2_486 ?
O20 Si1 O22 O21 -122(2) 2_486 . . 2_486 ?
O20 Si1 O22 O21 58(2) . . . 2_486 ?
O21 Si1 O19 O20 -119.9(19) 2_486 . . 2_486 ?
O21 Si1 O19 O20 60.1(19) . . . 2_486 ?
O21 Si1 O19 O22 -58(2) . . . 2_486 ?
O21 Si1 O19 O22 122(2) 2_486 . . 2_486 ?
O21 Si1 O20 O19 -66(3) . . . 2_486 ?
O21 Si1 O20 O19 114(3) 2_486 . . 2_486 ?
O21 Si1 O20 O21 180.00(2) . . . 2_486 ?
O21 Si1 O22 O19 64(4) . . . 2_486 ?
O21 Si1 O22 O19 -116(4) 2_486 . . 2_486 ?
O21 Si1 O22 O21 179.998(5) . . . 2_486 ?
O22 Si1 O19 O20 -62(3) . . . 2_486 ?
O22 Si1 O19 O20 118(3) 2_486 . . 2_486 ?
O22 Si1 O19 O22 180.00(2) . . . 2_486 ?
O22 Si1 O20 O19 -122.9(19) 2_486 . . 2_486 ?
O22 Si1 O20 O19 57.1(19) . . . 2_486 ?
O22 Si1 O20 O21 123(2) 2_486 . . 2_486 ?
O22 Si1 O20 O21 -57(2) . . . 2_486 ?
O22 Si1 O21 O20 61(3) . . . 2_486 ?
O22 Si1 O21 O20 -119(3) 2_486 . . 2_486 ?
O22 Si1 O21 O22 179.999(4) . . . 2_486 ?
O40 Si2 O41 O40 179.998(3) . . . 2_577 ?
O40 Si2 O41 O42 -119.8(10) 2_577 . . 2_577 ?
O40 Si2 O41 O42 60.2(10) . . . 2_577 ?
O40 Si2 O41 O43 -60.0(11) . . . 2_577 ?
O40 Si2 O41 O43 120.0(11) 2_577 . . 2_577 ?
O40 Si2 O42 O40 180.00(3) . . . 2_577 ?
O40 Si2 O42 O41 -59.8(10) . . . 2_577 ?
O40 Si2 O42 O41 120.2(10) 2_577 . . 2_577 ?
O40 Si2 O42 O43 60.8(10) . . . 2_577 ?
O40 Si2 O42 O43 -119.2(10) 2_577 . . 2_577 ?
O40 Si2 O43 O40 179.999(19) . . . 2_577 ?
O40 Si2 O43 O41 59.6(11) . . . 2_577 ?
O40 Si2 O43 O41 -120.4(11) 2_577 . . 2_577 ?
O40 Si2 O43 O42 -60.8(10) . . . 2_577 ?
O40 Si2 O43 O42 119.2(10) 2_577 . . 2_577 ?
O41 Si2 O40 O41 179.994(5) . . . 2_577 ?
O41 Si2 O40 O42 -59.9(10) . . . 2_577 ?
O41 Si2 O40 O42 120.1(10) 2_577 . . 2_577 ?
O41 Si2 O40 O43 59.4(10) . . . 2_577 ?
O41 Si2 O40 O43 -120.6(10) 2_577 . . 2_577 ?
O41 Si2 O42 O40 59.8(10) . . . 2_577 ?
O41 Si2 O42 O40 -120.2(10) 2_577 . . 2_577 ?
O41 Si2 O42 O41 180.001(16) . . . 2_577 ?
O41 Si2 O42 O43 -59.3(10) . . . 2_577 ?
O41 Si2 O42 O43 120.7(10) 2_577 . . 2_577 ?
O41 Si2 O43 O40 -59.6(11) . . . 2_577 ?
O41 Si2 O43 O40 120.4(11) 2_577 . . 2_577 ?
O41 Si2 O43 O41 180.00(3) . . . 2_577 ?
O41 Si2 O43 O42 -120.4(10) 2_577 . . 2_577 ?
O41 Si2 O43 O42 59.6(10) . . . 2_577 ?
O42 Si2 O40 O41 59.9(10) . . . 2_577 ?
O42 Si2 O40 O41 -120.1(10) 2_577 . . 2_577 ?
O42 Si2 O40 O42 180.00(3) . . . 2_577 ?
O42 Si2 O40 O43 -60.7(10) . . . 2_577 ?
O42 Si2 O40 O43 119.3(10) 2_577 . . 2_577 ?
O42 Si2 O41 O40 119.8(10) 2_577 . . 2_577 ?
O42 Si2 O41 O40 -60.2(10) . . . 2_577 ?
O42 Si2 O41 O42 180.000(17) . . . 2_577 ?
O42 Si2 O41 O43 -120.2(10) 2_577 . . 2_577 ?
O42 Si2 O41 O43 59.8(10) . . . 2_577 ?
O42 Si2 O43 O40 60.8(10) . . . 2_577 ?
O42 Si2 O43 O40 -119.2(10) 2_577 . . 2_577 ?
O42 Si2 O43 O41 120.4(10) 2_577 . . 2_577 ?
O42 Si2 O43 O41 -59.6(10) . . . 2_577 ?
O42 Si2 O43 O42 180.00(6) . . . 2_577 ?
O43 Si2 O40 O41 120.6(10) 2_577 . . 2_577 ?
O43 Si2 O40 O41 -59.4(10) . . . 2_577 ?
O43 Si2 O40 O42 60.7(10) . . . 2_577 ?
O43 Si2 O40 O42 -119.3(10) 2_577 . . 2_577 ?
O43 Si2 O40 O43 179.994(19) . . . 2_577 ?
O43 Si2 O41 O40 60.0(11) . . . 2_577 ?
O43 Si2 O41 O40 -120.0(11) 2_577 . . 2_577 ?
O43 Si2 O41 O42 120.2(10) 2_577 . . 2_577 ?
O43 Si2 O41 O42 -59.8(10) . . . 2_577 ?
O43 Si2 O41 O43 180.00(2) . . . 2_577 ?
O43 Si2 O42 O40 -60.8(10) . . . 2_577 ?
O43 Si2 O42 O40 119.2(10) 2_577 . . 2_577 ?
O43 Si2 O42 O41 -120.7(10) 2_577 . . 2_577 ?
O43 Si2 O42 O41 59.3(10) . . . 2_577 ?
O43 Si2 O42 O43 180.00(5) . . . 2_577 ?
C105 C421 C211 C423 0.0 . . . . ?
C421 C105 C425 C53 0.0 . . . . ?
C421 C211 C423 P11 180.0(3) . . . . ?
C421 C211 C423 C53 0.0 . . . . ?
C211 C423 C53 C425 0.0 . . . . ?
C423 P11 C73 C293 -82(3) . . . . ?
C423 P11 C73 C297 100(3) . . . . ?
C423 C53 C425 C105 0.0 . . . . ?
C425 C105 C421 C211 0.0 . . . . ?

