# Supplementary Information (SI) for Organic & Biomolecular Chemistry.
# This journal is © The Royal Society of Chemistry 2024

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
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data_mo_gs_ab_cho_0m
_database_code_depnum_ccdc_archive 'CCDC 2344684'
loop_
_audit_author_name
_audit_author_address
Anil
;IITH
India
;
_audit_update_record             
;
2024-03-31 deposited with the CCDC.	2024-08-09 downloaded from the CCDC.
;
_audit_creation_date             2024-01-08
_audit_creation_method           
;
Olex2 1.5-alpha
(compiled 2023.11.24 svn.r209d9fb2 for OlexSys, GUI svn.r6869)
;
_shelx_SHELXL_version_number     2019/1
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C23 H18 O4 S'
_chemical_formula_sum            'C23 H18 O4 S'
_chemical_formula_weight         390.43
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_H-M_alt        'P 1 21/n 1'
_space_group_name_Hall           '-P 2yn'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'

_cell_length_a                   8.3863(19)
_cell_length_b                   18.506(3)
_cell_length_c                   12.780(2)
_cell_angle_alpha                90
_cell_angle_beta                 108.742(7)
_cell_angle_gamma                90
_cell_volume                     1878.3(6)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    3715
_cell_measurement_temperature    149.00
_cell_measurement_theta_max      24.88
_cell_measurement_theta_min      2.58
_shelx_estimated_absorpt_T_max   0.998
_shelx_estimated_absorpt_T_min   0.991
_exptl_absorpt_coefficient_mu    0.200
_exptl_absorpt_correction_T_max  0.7454
_exptl_absorpt_correction_T_min  0.5069
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
SADABS-2016/2 (Bruker,2016/2) was used for absorption correction.
wR2(int) was 0.1683 before and 0.0788 after correction.
The Ratio of minimum to maximum transmission is 0.6800.
The λ/2 correction factor is Not present.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            'metallic light colourless'
_exptl_crystal_colour_lustre     metallic
_exptl_crystal_colour_modifier   light
_exptl_crystal_colour_primary    colourless
_exptl_crystal_density_diffrn    1.381
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             816
_exptl_crystal_size_max          0.045
_exptl_crystal_size_mid          0.036
_exptl_crystal_size_min          0.012
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0981
_diffrn_reflns_av_unetI/netI     0.0593
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 1.000
_diffrn_reflns_limit_h_max       9
_diffrn_reflns_limit_h_min       -9
_diffrn_reflns_limit_k_max       22
_diffrn_reflns_limit_k_min       -21
_diffrn_reflns_limit_l_max       15
_diffrn_reflns_limit_l_min       -15
_diffrn_reflns_number            22124
_diffrn_reflns_point_group_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 1.000
_diffrn_reflns_theta_full        24.995
_diffrn_reflns_theta_max         24.995
_diffrn_reflns_theta_min         2.201
_diffrn_ambient_temperature      149.00
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type  'Bruker APEX-IV Photon II'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_diffrn_source_current           1.4
_diffrn_source_power             0.07
_diffrn_source_voltage           50.0
_diffrn_standards_number         0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                2495
_reflns_number_total             3304
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT V8.40B (?, 2016)'
_computing_data_collection       ?
_computing_data_reduction        'SAINT V8.40B (?, 2016)'
_computing_molecular_graphics    'Olex2 1.5-alpha (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.5-alpha (Dolomanov et al., 2009)'
_computing_structure_refinement  'XL  (Sheldrick, 2008)'
_computing_structure_solution    'SHELXT 2018/2 (Sheldrick, 2018)'
_refine_diff_density_max         0.223
_refine_diff_density_min         -0.229
_refine_diff_density_rms         0.051
_refine_ls_extinction_coef       0.0041(8)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     'SHELXL-2019/1 (Sheldrick 2019)'
_refine_ls_goodness_of_fit_ref   1.015
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     256
_refine_ls_number_reflns         3304
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0659
_refine_ls_R_factor_gt           0.0421
_refine_ls_restrained_S_all      1.015
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0348P)²+0.7827P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0895
_refine_ls_wR_factor_ref         0.1004
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups
 At 1.5 times of:
  All C(H,H,H) groups
2.a Aromatic/amide H refined with riding coordinates:
 C3(H3), C4(H4), C9(H9), C10(H10), C13(H13), C14(H14), C15(H15), C16(H16),
 C19(H19), C20(H20), C21(H21), C22(H22)
2.b Idealised Me refined as rotating group:
 C1(H1A,H1B,H1C), C12(H12A,H12B,H12C)
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
S1 S 0.06283(8) 0.18722(3) 0.65487(4) 0.02570(18) Uani 1 1 d . . . . .
O1 O 0.8426(2) 0.24715(9) 0.87254(12) 0.0336(4) Uani 1 1 d . . . . .
O2 O -0.2153(2) 0.46651(9) 0.44908(13) 0.0425(5) Uani 1 1 d . . . . .
O3 O 0.31243(19) 0.09312(7) 0.47194(11) 0.0226(4) Uani 1 1 d . . . . .
O4 O 0.2461(2) 0.02831(8) 0.31943(12) 0.0275(4) Uani 1 1 d . . . . .
C1 C 0.9842(3) 0.20210(14) 0.92565(19) 0.0369(6) Uani 1 1 d . . . . .
H1A H 0.948072 0.161884 0.962601 0.055 Uiso 1 1 calc R U . . .
H1B H 1.070009 0.230514 0.980371 0.055 Uiso 1 1 calc R U . . .
H1C H 1.031358 0.183056 0.870337 0.055 Uiso 1 1 calc R U . . .
C2 C 0.7109(3) 0.21687(12) 0.79119(17) 0.0249(5) Uani 1 1 d . . . . .
C3 C 0.5751(3) 0.26228(12) 0.74426(18) 0.0275(6) Uani 1 1 d . . . . .
H3 H 0.580822 0.311407 0.766766 0.033 Uiso 1 1 calc R U . . .
C4 C 0.4323(3) 0.23701(11) 0.66555(17) 0.0243(5) Uani 1 1 d . . . . .
H4 H 0.339173 0.268414 0.635442 0.029 Uiso 1 1 calc R U . . .
C5 C 0.4235(3) 0.16511(11) 0.62951(17) 0.0212(5) Uani 1 1 d . . . . .
C6 C 0.2706(3) 0.13497(11) 0.54934(17) 0.0202(5) Uani 1 1 d . . . . .
C7 C 0.1101(3) 0.14037(11) 0.54801(17) 0.0212(5) Uani 1 1 d . . . . .
C8 C -0.0199(3) 0.27058(11) 0.59127(17) 0.0215(5) Uani 1 1 d . . . . .
C9 C -0.0686(3) 0.32132(12) 0.65441(17) 0.0243(5) Uani 1 1 d . . . . .
H9 H -0.056464 0.310661 0.729289 0.029 Uiso 1 1 calc R U . . .
C10 C -0.1346(3) 0.38729(12) 0.61054(18) 0.0278(6) Uani 1 1 d . . . . .
H10 H -0.168415 0.421522 0.654663 0.033 Uiso 1 1 calc R U . . .
C11 C -0.1510(3) 0.40300(12) 0.50122(18) 0.0281(6) Uani 1 1 d . . . . .
C12 C -0.2491(4) 0.52247(13) 0.5139(2) 0.0464(7) Uani 1 1 d . . . . .
H12A H -0.339988 0.507507 0.541890 0.070 Uiso 1 1 calc R U . . .
H12B H -0.283219 0.566057 0.468726 0.070 Uiso 1 1 calc R U . . .
H12C H -0.147476 0.532702 0.576289 0.070 Uiso 1 1 calc R U . . .
C13 C -0.0374(3) 0.28692(12) 0.48116(17) 0.0262(5) Uani 1 1 d . . . . .
H13 H -0.004838 0.252564 0.436615 0.031 Uiso 1 1 calc R U . . .
C14 C -0.1019(3) 0.35299(12) 0.43735(18) 0.0280(6) Uani 1 1 d . . . . .
H14 H -0.112641 0.364115 0.362832 0.034 Uiso 1 1 calc R U . . .
C15 C 0.7068(3) 0.14628(12) 0.75438(17) 0.0253(5) Uani 1 1 d . . . . .
H15 H 0.800833 0.115300 0.784143 0.030 Uiso 1 1 calc R U . . .
C16 C 0.5637(3) 0.12143(12) 0.67355(17) 0.0235(5) Uani 1 1 d . . . . .
H16 H 0.561613 0.073220 0.647579 0.028 Uiso 1 1 calc R U . . .
C17 C 0.1941(3) 0.05840(11) 0.38617(17) 0.0216(5) Uani 1 1 d . . . . .
C18 C 0.0201(3) 0.06186(11) 0.38457(17) 0.0209(5) Uani 1 1 d . . . . .
C19 C -0.1028(3) 0.02392(12) 0.30267(18) 0.0276(6) Uani 1 1 d . . . . .
H19 H -0.072287 -0.003136 0.248830 0.033 Uiso 1 1 calc R U . . .
C20 C -0.2673(3) 0.02589(12) 0.30035(19) 0.0315(6) Uani 1 1 d . . . . .
H20 H -0.350927 0.000378 0.244532 0.038 Uiso 1 1 calc R U . . .
C21 C -0.3122(3) 0.06524(12) 0.37965(19) 0.0301(6) Uani 1 1 d . . . . .
H21 H -0.426253 0.065886 0.377973 0.036 Uiso 1 1 calc R U . . .
C22 C -0.1927(3) 0.10317(12) 0.46040(18) 0.0260(5) Uani 1 1 d . . . . .
H22 H -0.225038 0.130212 0.513477 0.031 Uiso 1 1 calc R U . . .
C23 C -0.0236(3) 0.10208(11) 0.46469(17) 0.0211(5) Uani 1 1 d . . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
S1 C7 1.767(2) . ?
S1 C8 1.778(2) . ?
O1 C1 1.431(3) . ?
O1 C2 1.370(3) . ?
O2 C11 1.373(3) . ?
O2 C12 1.411(3) . ?
O3 C6 1.387(2) . ?
O3 C17 1.378(3) . ?
O4 C17 1.211(2) . ?
C1 H1A 0.9800 . ?
C1 H1B 0.9800 . ?
C1 H1C 0.9800 . ?
C2 C3 1.387(3) . ?
C2 C15 1.385(3) . ?
C3 H3 0.9500 . ?
C3 C4 1.375(3) . ?
C4 H4 0.9500 . ?
C4 C5 1.402(3) . ?
C5 C6 1.470(3) . ?
C5 C16 1.389(3) . ?
C6 C7 1.344(3) . ?
C7 C23 1.458(3) . ?
C8 C9 1.382(3) . ?
C8 C13 1.400(3) . ?
C9 H9 0.9500 . ?
C9 C10 1.383(3) . ?
C10 H10 0.9500 . ?
C10 C11 1.390(3) . ?
C11 C14 1.381(3) . ?
C12 H12A 0.9800 . ?
C12 H12B 0.9800 . ?
C12 H12C 0.9800 . ?
C13 H13 0.9500 . ?
C13 C14 1.381(3) . ?
C14 H14 0.9500 . ?
C15 H15 0.9500 . ?
C15 C16 1.386(3) . ?
C16 H16 0.9500 . ?
C17 C18 1.454(3) . ?
C18 C19 1.399(3) . ?
C18 C23 1.407(3) . ?
C19 H19 0.9500 . ?
C19 C20 1.371(3) . ?
C20 H20 0.9500 . ?
C20 C21 1.395(3) . ?
C21 H21 0.9500 . ?
C21 C22 1.378(3) . ?
C22 H22 0.9500 . ?
C22 C23 1.401(3) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C7 S1 C8 102.94(10) . . ?
C2 O1 C1 117.73(18) . . ?
C11 O2 C12 117.70(19) . . ?
C17 O3 C6 123.03(17) . . ?
O1 C1 H1A 109.5 . . ?
O1 C1 H1B 109.5 . . ?
O1 C1 H1C 109.5 . . ?
H1A C1 H1B 109.5 . . ?
H1A C1 H1C 109.5 . . ?
H1B C1 H1C 109.5 . . ?
O1 C2 C3 115.5(2) . . ?
O1 C2 C15 124.7(2) . . ?
C15 C2 C3 119.8(2) . . ?
C2 C3 H3 119.6 . . ?
C4 C3 C2 120.7(2) . . ?
C4 C3 H3 119.6 . . ?
C3 C4 H4 119.8 . . ?
C3 C4 C5 120.3(2) . . ?
C5 C4 H4 119.8 . . ?
C4 C5 C6 122.1(2) . . ?
C16 C5 C4 118.1(2) . . ?
C16 C5 C6 119.80(19) . . ?
O3 C6 C5 110.20(18) . . ?
C7 C6 O3 120.9(2) . . ?
C7 C6 C5 128.8(2) . . ?
C6 C7 S1 119.95(17) . . ?
C6 C7 C23 120.4(2) . . ?
C23 C7 S1 119.44(17) . . ?
C9 C8 S1 117.87(16) . . ?
C9 C8 C13 119.0(2) . . ?
C13 C8 S1 123.12(17) . . ?
C8 C9 H9 119.4 . . ?
C8 C9 C10 121.2(2) . . ?
C10 C9 H9 119.4 . . ?
C9 C10 H10 120.3 . . ?
C9 C10 C11 119.3(2) . . ?
C11 C10 H10 120.3 . . ?
O2 C11 C10 124.3(2) . . ?
O2 C11 C14 115.6(2) . . ?
C14 C11 C10 120.1(2) . . ?
O2 C12 H12A 109.5 . . ?
O2 C12 H12B 109.5 . . ?
O2 C12 H12C 109.5 . . ?
H12A C12 H12B 109.5 . . ?
H12A C12 H12C 109.5 . . ?
H12B C12 H12C 109.5 . . ?
C8 C13 H13 120.0 . . ?
C14 C13 C8 120.0(2) . . ?
C14 C13 H13 120.0 . . ?
C11 C14 H14 119.8 . . ?
C13 C14 C11 120.4(2) . . ?
C13 C14 H14 119.8 . . ?
C2 C15 H15 120.4 . . ?
C2 C15 C16 119.2(2) . . ?
C16 C15 H15 120.4 . . ?
C5 C16 H16 119.1 . . ?
C15 C16 C5 121.8(2) . . ?
C15 C16 H16 119.1 . . ?
O3 C17 C18 116.95(18) . . ?
O4 C17 O3 116.4(2) . . ?
O4 C17 C18 126.7(2) . . ?
C19 C18 C17 118.9(2) . . ?
C19 C18 C23 120.5(2) . . ?
C23 C18 C17 120.6(2) . . ?
C18 C19 H19 120.1 . . ?
C20 C19 C18 119.8(2) . . ?
C20 C19 H19 120.1 . . ?
C19 C20 H20 119.9 . . ?
C19 C20 C21 120.2(2) . . ?
C21 C20 H20 119.9 . . ?
C20 C21 H21 119.7 . . ?
C22 C21 C20 120.6(2) . . ?
C22 C21 H21 119.7 . . ?
C21 C22 H22 119.8 . . ?
C21 C22 C23 120.4(2) . . ?
C23 C22 H22 119.8 . . ?
C18 C23 C7 118.0(2) . . ?
C22 C23 C7 123.6(2) . . ?
C22 C23 C18 118.5(2) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
S1 C7 C23 C18 -176.35(15) . . . . ?
S1 C7 C23 C22 3.5(3) . . . . ?
S1 C8 C9 C10 -179.77(18) . . . . ?
S1 C8 C13 C14 -179.67(18) . . . . ?
O1 C2 C3 C4 -176.86(19) . . . . ?
O1 C2 C15 C16 178.1(2) . . . . ?
O2 C11 C14 C13 -179.2(2) . . . . ?
O3 C6 C7 S1 174.22(14) . . . . ?
O3 C6 C7 C23 0.0(3) . . . . ?
O3 C17 C18 C19 -176.36(17) . . . . ?
O3 C17 C18 C23 3.0(3) . . . . ?
O4 C17 C18 C19 4.0(3) . . . . ?
O4 C17 C18 C23 -176.65(19) . . . . ?
C1 O1 C2 C3 178.47(19) . . . . ?
C1 O1 C2 C15 -1.9(3) . . . . ?
C2 C3 C4 C5 -1.6(3) . . . . ?
C2 C15 C16 C5 -0.9(3) . . . . ?
C3 C2 C15 C16 -2.3(3) . . . . ?
C3 C4 C5 C6 177.2(2) . . . . ?
C3 C4 C5 C16 -1.6(3) . . . . ?
C4 C5 C6 O3 137.03(19) . . . . ?
C4 C5 C6 C7 -46.8(3) . . . . ?
C4 C5 C16 C15 2.8(3) . . . . ?
C5 C6 C7 S1 -1.6(3) . . . . ?
C5 C6 C7 C23 -175.77(19) . . . . ?
C6 O3 C17 O4 174.37(17) . . . . ?
C6 O3 C17 C18 -5.3(3) . . . . ?
C6 C5 C16 C15 -175.95(19) . . . . ?
C6 C7 C23 C18 -2.1(3) . . . . ?
C6 C7 C23 C22 177.8(2) . . . . ?
C7 S1 C8 C9 -179.23(18) . . . . ?
C7 S1 C8 C13 0.7(2) . . . . ?
C8 S1 C7 C6 103.74(18) . . . . ?
C8 S1 C7 C23 -82.01(17) . . . . ?
C8 C9 C10 C11 -0.5(4) . . . . ?
C8 C13 C14 C11 -0.6(4) . . . . ?
C9 C8 C13 C14 0.2(3) . . . . ?
C9 C10 C11 O2 179.7(2) . . . . ?
C9 C10 C11 C14 0.1(4) . . . . ?
C10 C11 C14 C13 0.4(4) . . . . ?
C12 O2 C11 C10 7.5(4) . . . . ?
C12 O2 C11 C14 -172.9(2) . . . . ?
C13 C8 C9 C10 0.3(3) . . . . ?
C15 C2 C3 C4 3.5(3) . . . . ?
C16 C5 C6 O3 -44.3(3) . . . . ?
C16 C5 C6 C7 131.9(2) . . . . ?
C17 O3 C6 C5 -179.58(16) . . . . ?
C17 O3 C6 C7 3.9(3) . . . . ?
C17 C18 C19 C20 179.4(2) . . . . ?
C17 C18 C23 C7 0.5(3) . . . . ?
C17 C18 C23 C22 -179.35(19) . . . . ?
C18 C19 C20 C21 -0.4(3) . . . . ?
C19 C18 C23 C7 179.90(18) . . . . ?
C19 C18 C23 C22 0.0(3) . . . . ?
C19 C20 C21 C22 0.7(3) . . . . ?
C20 C21 C22 C23 -0.7(3) . . . . ?
C21 C22 C23 C7 -179.54(19) . . . . ?
C21 C22 C23 C18 0.3(3) . . . . ?
C23 C18 C19 C20 0.0(3) . . . . ?

_olex2_exptl_crystal_mounting_method 'Nylon loop used'
_olex2_submission_special_instructions 'No special instructions were received'
