# Supplementary Information (SI) for Inorganic Chemistry Frontiers.
# This journal is © the Partner Organisations 2024

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_LHY010
_database_code_depnum_ccdc_archive 'CCDC 2329960'
loop_
_audit_author_name
_audit_author_address
'Hongyang Li'
;University of Science and Technology Liaoning
China
;
_audit_update_record             
;
2024-03-14 deposited with the CCDC.	2024-08-18 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2018/3
_shelx_SHELXL_version_number     2018/3
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C12.75 H15 As1.94 N12 Na6 O6.75 Re4 S2.06'
_chemical_formula_weight         1538.49

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
As As 0.0499 2.0058 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Re Re -1.0185 7.2310 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   9.4363(3)
_cell_length_b                   10.2986(2)
_cell_length_c                   17.6142(4)
_cell_angle_alpha                93.9220(10)
_cell_angle_beta                 98.5850(10)
_cell_angle_gamma                104.0900(10)
_cell_volume                     1631.84(7)
_cell_formula_units_Z            2
_cell_measurement_temperature    150(2)
_cell_measurement_reflns_used    5361
_cell_measurement_theta_min      2.95
_cell_measurement_theta_max      27.43

_exptl_crystal_description       block
_exptl_crystal_colour            'clear dark brown'
_exptl_crystal_colour_lustre     clear
_exptl_crystal_colour_modifier   dark
_exptl_crystal_colour_primary    brown
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    3.131
_exptl_crystal_F_000             1385
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          0.040
_exptl_crystal_size_mid          0.020
_exptl_crystal_size_min          0.010
_exptl_absorpt_coefficient_mu    17.005
_shelx_estimated_absorpt_T_min   0.549
_shelx_estimated_absorpt_T_max   0.848
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_correction_T_min  0.5942
_exptl_absorpt_correction_T_max  0.7456
_exptl_absorpt_process_details   
;
 SADABS 2016/2: Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D.,
 J. Appl. Cryst. 48 (2015) 3-10
;
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      150(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_source                   'fine-focus sealed tube'
_diffrn_radiation_monochromator  graphite
_diffrn_measurement_device_type  'Bruker Nonius X8Apex CCD area-detector'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_detector_area_resol_mean 25
_diffrn_reflns_number            19758
_diffrn_reflns_av_unetI/netI     0.0583
_diffrn_reflns_av_R_equivalents  0.0454
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_l_min       -22
_diffrn_reflns_limit_l_max       22
_diffrn_reflns_theta_min         2.816
_diffrn_reflns_theta_max         27.489
_diffrn_reflns_theta_full        25.242
_diffrn_measured_fraction_theta_max 0.993
_diffrn_measured_fraction_theta_full 0.995
_diffrn_reflns_Laue_measured_fraction_max 0.993
_diffrn_reflns_Laue_measured_fraction_full 0.995
_diffrn_reflns_point_group_measured_fraction_max 0.993
_diffrn_reflns_point_group_measured_fraction_full 0.995
_reflns_number_total             7443
_reflns_number_gt                6210
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       ?
_computing_cell_refinement       ?
_computing_data_reduction        ?
_computing_structure_solution    ?
_computing_structure_refinement  'SHELXL-2018/3 (Sheldrick, 2018)'
_computing_molecular_graphics    ?
_computing_publication_material  ?
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0130P)²] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_number_reflns         7443
_refine_ls_number_parameters     424
_refine_ls_number_restraints     12
_refine_ls_R_factor_all          0.0417
_refine_ls_R_factor_gt           0.0320
_refine_ls_wR_factor_ref         0.0600
_refine_ls_wR_factor_gt          0.0568
_refine_ls_goodness_of_fit_ref   1.045
_refine_ls_restrained_S_all      1.046
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Re1 Re 0.72675(3) 0.71569(3) 0.82362(2) 0.00937(7) Uani 1 1 d . . . . .
Re2 Re 0.70050(3) 0.48612(3) 0.72359(2) 0.00919(7) Uani 1 1 d . . . . .
Re3 Re 0.69773(3) 0.72885(3) 0.66444(2) 0.00914(7) Uani 1 1 d . . . . .
Re4 Re 0.45710(3) 0.59435(3) 0.72682(2) 0.00943(7) Uani 1 1 d . . . . .
As1 As 0.91144(12) 0.68462(10) 0.74420(6) 0.0122(3) Uani 0.466(5) 1 d . . P A 1
As2 As 0.56871(13) 0.83407(11) 0.74901(6) 0.0116(4) Uani 0.387(5) 1 d . . P A 1
As3 As 0.56922(11) 0.49203(9) 0.83241(5) 0.0113(3) Uani 0.566(5) 1 d . . P A 1
As4 As 0.53062(12) 0.51011(9) 0.60907(6) 0.0124(3) Uani 0.521(5) 1 d . . P A 1
S1 S 0.91144(12) 0.68462(10) 0.74420(6) 0.0122(3) Uani 0.534(5) 1 d . . P A 1
S2 S 0.56871(13) 0.83407(11) 0.74901(6) 0.0116(4) Uani 0.613(5) 1 d . . P A 1
S3 S 0.56922(11) 0.49203(9) 0.83241(5) 0.0113(3) Uani 0.434(5) 1 d . . P A 1
S4 S 0.53062(12) 0.51011(9) 0.60907(6) 0.0124(3) Uani 0.479(5) 1 d . . P A 1
Na1 Na 1.000000 0.500000 0.500000 0.0177(9) Uani 1 2 d S . P . .
Na2 Na 1.1173(3) 0.4956(3) 0.92515(16) 0.0181(6) Uani 1 1 d . . . . .
Na3 Na 1.0578(3) 1.1777(3) 0.79349(17) 0.0235(7) Uani 1 1 d . . . . .
Na4 Na 0.0335(3) 0.2150(3) 0.59005(16) 0.0174(6) Uani 1 1 d . . . . .
Na5 Na 0.6532(3) 1.1074(3) 0.57732(17) 0.0222(7) Uani 1 1 d . . . . .
Na6 Na 0.8301(4) 0.1975(3) 0.94218(17) 0.0248(7) Uani 1 1 d . . . . .
Na7 Na 0.500000 1.000000 1.000000 0.0270(11) Uani 1 2 d S . P . .
O1 O 1.2717(9) 1.0785(7) 0.7831(4) 0.0251(17) Uani 0.75 1 d . . P . .
H1 H 1.352519 1.088993 0.813199 0.030 Uiso 0.75 1 calc R U P . .
O1W O 1.2449(6) 0.3238(5) 0.8983(3) 0.0211(12) Uani 1 1 d . . . . .
O2W O 0.7602(6) 0.1025(5) 1.0561(3) 0.0241(13) Uani 1 1 d . . . . .
O3W O 1.3051(6) 0.6425(5) 1.0156(3) 0.0201(12) Uani 1 1 d . . . . .
O4W O 0.4319(7) 0.9183(6) 1.1198(3) 0.0347(15) Uani 1 1 d . . . . .
O5W O 0.2419(9) 0.1271(8) 0.5774(4) 0.062(2) Uani 1 1 d . . . . .
O6W O -0.1736(6) 0.1240(5) 0.4941(3) 0.0195(12) Uani 1 1 d . . . . .
N11 N 0.9513(7) 0.6427(6) 0.9642(3) 0.0157(13) Uani 1 1 d . . . . .
N12 N 0.9401(7) 1.0184(6) 0.8778(3) 0.0200(15) Uani 1 1 d . . . . .
N13 N 0.5858(7) 0.7934(6) 0.9729(3) 0.0196(14) Uani 1 1 d . . . . .
N21 N 0.9051(7) 0.3387(6) 0.8362(3) 0.0181(14) Uani 1 1 d . . . . .
N22 N 0.8827(7) 0.3747(6) 0.6022(3) 0.0184(14) Uani 1 1 d . . . . .
N23 N 0.5219(7) 0.1708(6) 0.6867(4) 0.0234(15) Uani 1 1 d . . . . .
N31 N 0.8945(7) 1.0393(6) 0.6695(3) 0.0191(14) Uani 1 1 d . . . . .
N32 N 0.5183(7) 0.8508(6) 0.5265(3) 0.0175(14) Uani 1 1 d . . . . .
N33 N 0.8609(7) 0.6759(6) 0.5190(3) 0.0167(13) Uani 1 1 d . U . . .
N41 N 0.2442(7) 0.6615(6) 0.8449(3) 0.0189(14) Uani 1 1 d . . . . .
N42 N 0.2026(7) 0.3146(6) 0.7102(4) 0.0238(16) Uani 1 1 d . . . . .
N43 N 0.2031(7) 0.6616(6) 0.6003(3) 0.0188(14) Uani 1 1 d . . . . .
C1 C 1.2368(14) 0.9608(12) 0.7433(7) 0.041(3) Uani 0.75 1 d . U P . .
H1B H 1.207314 0.890718 0.776992 0.062 Uiso 0.75 1 calc R U P . .
H1A H 1.322687 0.947385 0.721658 0.062 Uiso 0.75 1 calc R U P . .
H1C H 1.154255 0.955561 0.701266 0.062 Uiso 0.75 1 calc R U P . .
C11 C 0.8716(8) 0.6676(6) 0.9127(4) 0.0122(15) Uani 1 1 d . . . . .
C12 C 0.8677(8) 0.9115(7) 0.8569(4) 0.0161(16) Uani 1 1 d . . . . .
C13 C 0.6323(8) 0.7695(7) 0.9193(4) 0.0155(16) Uani 1 1 d . . . . .
C21 C 0.8363(8) 0.3960(7) 0.7976(4) 0.0138(15) Uani 1 1 d . . . . .
C22 C 0.8179(8) 0.4178(6) 0.6442(4) 0.0106(14) Uani 1 1 d . . . . .
C23 C 0.5787(8) 0.2821(7) 0.7003(4) 0.0146(15) Uani 1 1 d . . . . .
C31 C 0.8306(9) 0.9289(7) 0.6701(4) 0.0189(17) Uani 1 1 d . . . . .
C32 C 0.5745(8) 0.8024(7) 0.5757(4) 0.0130(15) Uani 1 1 d . . . . .
C33 C 0.8071(8) 0.6937(6) 0.5722(4) 0.0104(14) Uani 1 1 d . U . . .
C41 C 0.3200(8) 0.6390(7) 0.8039(4) 0.0120(15) Uani 1 1 d . . . . .
C42 C 0.2959(8) 0.4104(7) 0.7127(4) 0.0156(16) Uani 1 1 d . . . . .
C43 C 0.2914(8) 0.6405(7) 0.6446(4) 0.0137(15) Uani 1 1 d . . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Re1 C11 2.090(7) . ?
Re1 C12 2.116(7) . ?
Re1 C13 2.123(8) . ?
Re1 As2 2.4406(12) . ?
Re1 As3 2.4474(9) . ?
Re1 As1 2.4566(11) . ?
Re1 Re2 2.7875(4) . ?
Re1 Re3 2.7921(4) . ?
Re1 Re4 2.7944(4) . ?
Re2 C22 2.094(7) . ?
Re2 C21 2.109(7) . ?
Re2 C23 2.114(7) . ?
Re2 As3 2.4376(10) . ?
Re2 As1 2.4443(10) . ?
Re2 As4 2.4485(11) . ?
Re2 Re3 2.7776(4) . ?
Re2 Re4 2.7924(4) . ?
Re3 C32 2.101(7) . ?
Re3 C33 2.107(7) . ?
Re3 C31 2.122(8) . ?
Re3 As2 2.4164(11) . ?
Re3 As1 2.4367(11) . ?
Re3 As4 2.4542(10) . ?
Re3 Re4 2.7755(4) . ?
Re4 C42 2.094(7) . ?
Re4 C41 2.111(7) . ?
Re4 C43 2.132(8) . ?
Re4 As2 2.4158(11) . ?
Re4 As3 2.4315(10) . ?
Re4 As4 2.4519(10) . ?
Na1 N33 2.514(6) . ?
Na1 N33 2.514(6) 2_766 ?
Na1 N22 2.519(6) 2_766 ?
Na1 N22 2.519(6) . ?
Na1 N43 2.569(6) 2_666 ?
Na1 N43 2.569(6) 1_655 ?
Na1 Na4 3.489(3) 1_655 ?
Na1 Na4 3.489(3) 2_666 ?
Na2 O3W 2.342(6) . ?
Na2 O1W 2.429(6) . ?
Na2 N41 2.488(6) 1_655 ?
Na2 N21 2.493(7) . ?
Na2 N11 2.560(6) 2_767 ?
Na2 N11 2.561(7) . ?
Na2 C21 3.117(8) . ?
Na2 Na6 3.630(4) . ?
Na2 Na6 3.685(4) 2_767 ?
Na2 Na2 3.698(6) 2_767 ?
Na2 Na3 3.754(4) 1_545 ?
Na3 N42 2.440(7) 1_665 ?
Na3 N12 2.463(7) . ?
Na3 O1W 2.479(6) 1_565 ?
Na3 O1 2.497(8) . ?
Na3 N31 2.584(7) . ?
Na3 N21 2.591(7) 1_565 ?
Na3 Na4 3.609(4) 1_665 ?
Na3 Na6 3.652(4) 1_565 ?
Na4 O6W 2.336(6) . ?
Na4 O5W 2.388(8) . ?
Na4 N22 2.441(7) 1_455 ?
Na4 N42 2.444(7) . ?
Na4 N33 2.504(6) 2_666 ?
Na4 N31 2.587(6) 1_445 ?
Na4 Na5 3.457(4) 1_445 ?
Na5 O6W 2.337(6) 1_665 ?
Na5 N32 2.390(7) 2_676 ?
Na5 N23 2.570(7) 1_565 ?
Na5 N32 2.664(6) . ?
Na5 N31 2.854(7) . ?
Na5 C23 2.993(7) 1_565 ?
Na5 N22 3.018(7) 1_565 ?
Na5 C32 3.044(7) . ?
Na5 Na5 3.792(6) 2_676 ?
Na6 O2W 2.401(6) . ?
Na6 O3W 2.457(6) 2_767 ?
Na6 O4W 2.511(7) 2_667 ?
Na6 N21 2.523(7) . ?
Na6 N11 2.577(7) 2_767 ?
Na6 N12 2.600(7) 1_545 ?
Na6 Na7 3.609(3) 1_545 ?
Na7 O4W 2.440(6) 2_677 ?
Na7 O4W 2.440(6) . ?
Na7 O2W 2.447(5) 2_667 ?
Na7 O2W 2.447(5) 1_565 ?
Na7 N13 2.495(6) . ?
Na7 N13 2.495(6) 2_677 ?
O1 C1 1.300(14) . ?
N11 C11 1.174(9) . ?
N12 C12 1.148(9) . ?
N13 C13 1.134(9) . ?
N21 C21 1.159(9) . ?
N22 C22 1.159(8) . ?
N23 C23 1.133(9) . ?
N31 C31 1.151(9) . ?
N32 C32 1.154(9) . ?
N33 C33 1.154(8) . ?
N41 C41 1.140(9) . ?
N42 C42 1.144(9) . ?
N43 C43 1.126(9) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C11 Re1 C12 82.2(3) . . ?
C11 Re1 C13 80.6(3) . . ?
C12 Re1 C13 81.5(3) . . ?
C11 Re1 As2 161.80(19) . . ?
C12 Re1 As2 83.7(2) . . ?
C13 Re1 As2 85.96(19) . . ?
C11 Re1 As3 84.30(18) . . ?
C12 Re1 As3 160.60(19) . . ?
C13 Re1 As3 82.66(19) . . ?
As2 Re1 As3 106.20(4) . . ?
C11 Re1 As1 84.12(19) . . ?
C12 Re1 As1 85.2(2) . . ?
C13 Re1 As1 160.94(19) . . ?
As2 Re1 As1 106.13(4) . . ?
As3 Re1 As1 107.19(3) . . ?
C11 Re1 Re2 95.56(18) . . ?
C12 Re1 Re2 140.21(19) . . ?
C13 Re1 Re2 137.65(19) . . ?
As2 Re1 Re2 102.64(3) . . ?
As3 Re1 Re2 55.04(2) . . ?
As1 Re1 Re2 55.13(2) . . ?
C11 Re1 Re3 138.81(19) . . ?
C12 Re1 Re3 96.63(19) . . ?
C13 Re1 Re3 140.22(19) . . ?
As2 Re1 Re3 54.50(3) . . ?
As3 Re1 Re3 102.70(2) . . ?
As1 Re1 Re3 54.87(3) . . ?
Re2 Re1 Re3 59.710(9) . . ?
C11 Re1 Re4 138.94(18) . . ?
C12 Re1 Re4 138.1(2) . . ?
C13 Re1 Re4 95.85(19) . . ?
As2 Re1 Re4 54.46(3) . . ?
As3 Re1 Re4 54.79(2) . . ?
As1 Re1 Re4 103.15(3) . . ?
Re2 Re1 Re4 60.035(10) . . ?
Re3 Re1 Re4 59.581(10) . . ?
C22 Re2 C21 80.3(3) . . ?
C22 Re2 C23 80.1(3) . . ?
C21 Re2 C23 79.6(3) . . ?
C22 Re2 As3 160.15(18) . . ?
C21 Re2 As3 83.90(19) . . ?
C23 Re2 As3 85.31(19) . . ?
C22 Re2 As1 83.08(18) . . ?
C21 Re2 As1 86.41(19) . . ?
C23 Re2 As1 159.7(2) . . ?
As3 Re2 As1 107.89(3) . . ?
C22 Re2 As4 84.91(19) . . ?
C21 Re2 As4 158.48(18) . . ?
C23 Re2 As4 82.5(2) . . ?
As3 Re2 As4 106.60(3) . . ?
As1 Re2 As4 107.28(3) . . ?
C22 Re2 Re3 96.46(18) . . ?
C21 Re2 Re3 141.45(18) . . ?
C23 Re2 Re3 138.1(2) . . ?
As3 Re2 Re3 103.38(2) . . ?
As1 Re2 Re3 55.19(3) . . ?
As4 Re2 Re3 55.59(2) . . ?
C22 Re2 Re1 138.58(18) . . ?
C21 Re2 Re1 97.29(18) . . ?
C23 Re2 Re1 140.56(19) . . ?
As3 Re2 Re1 55.37(2) . . ?
As1 Re2 Re1 55.54(3) . . ?
As4 Re2 Re1 104.13(3) . . ?
Re3 Re2 Re1 60.228(9) . . ?
C22 Re2 Re4 140.04(18) . . ?
C21 Re2 Re4 138.78(19) . . ?
C23 Re2 Re4 96.6(2) . . ?
As3 Re2 Re4 54.90(2) . . ?
As1 Re2 Re4 103.54(3) . . ?
As4 Re2 Re4 55.32(2) . . ?
Re3 Re2 Re4 59.775(10) . . ?
Re1 Re2 Re4 60.104(10) . . ?
C32 Re3 C33 79.9(3) . . ?
C32 Re3 C31 79.4(3) . . ?
C33 Re3 C31 83.6(3) . . ?
C32 Re3 As2 84.89(19) . . ?
C33 Re3 As2 161.10(18) . . ?
C31 Re3 As2 82.6(2) . . ?
C32 Re3 As1 159.41(19) . . ?
C33 Re3 As1 84.27(19) . . ?
C31 Re3 As1 85.9(2) . . ?
As2 Re3 As1 107.53(4) . . ?
C32 Re3 As4 83.57(18) . . ?
C33 Re3 As4 82.31(17) . . ?
C31 Re3 As4 159.51(19) . . ?
As2 Re3 As4 107.17(4) . . ?
As1 Re3 As4 107.35(3) . . ?
C32 Re3 Re4 96.34(19) . . ?
C33 Re3 Re4 137.73(17) . . ?
C31 Re3 Re4 137.6(2) . . ?
As2 Re3 Re4 54.93(3) . . ?
As1 Re3 Re4 104.24(3) . . ?
As4 Re3 Re4 55.51(2) . . ?
C32 Re3 Re2 138.90(18) . . ?
C33 Re3 Re2 95.27(18) . . ?
C31 Re3 Re2 141.1(2) . . ?
As2 Re3 Re2 103.57(3) . . ?
As1 Re3 Re2 55.44(2) . . ?
As4 Re3 Re2 55.40(2) . . ?
Re4 Re3 Re2 60.378(10) . . ?
C32 Re3 Re1 140.10(19) . . ?
C33 Re3 Re1 139.56(19) . . ?
C31 Re3 Re1 96.53(19) . . ?
As2 Re3 Re1 55.32(3) . . ?
As1 Re3 Re1 55.54(3) . . ?
As4 Re3 Re1 103.85(2) . . ?
Re4 Re3 Re1 60.249(10) . . ?
Re2 Re3 Re1 60.062(9) . . ?
C42 Re4 C41 79.9(3) . . ?
C42 Re4 C43 80.6(3) . . ?
C41 Re4 C43 81.8(3) . . ?
C42 Re4 As2 160.1(2) . . ?
C41 Re4 As2 83.44(18) . . ?
C43 Re4 As2 86.34(18) . . ?
C42 Re4 As3 82.02(19) . . ?
C41 Re4 As3 85.46(19) . . ?
C43 Re4 As3 160.03(18) . . ?
As2 Re4 As3 107.50(4) . . ?
C42 Re4 As4 85.8(2) . . ?
C41 Re4 As4 159.82(18) . . ?
C43 Re4 As4 81.84(18) . . ?
As2 Re4 As4 107.26(4) . . ?
As3 Re4 As4 106.69(3) . . ?
C42 Re4 Re3 141.2(2) . . ?
C41 Re4 Re3 138.33(18) . . ?
C43 Re4 Re3 96.11(18) . . ?
As2 Re4 Re3 54.95(3) . . ?
As3 Re4 Re3 103.61(3) . . ?
As4 Re4 Re3 55.59(2) . . ?
C42 Re4 Re2 96.7(2) . . ?
C41 Re4 Re2 140.36(18) . . ?
C43 Re4 Re2 136.99(18) . . ?
As2 Re4 Re2 103.16(3) . . ?
As3 Re4 Re2 55.11(2) . . ?
As4 Re4 Re2 55.21(3) . . ?
Re3 Re4 Re2 59.847(10) . . ?
C42 Re4 Re1 137.33(19) . . ?
C41 Re4 Re1 96.32(18) . . ?
C43 Re4 Re1 141.39(18) . . ?
As2 Re4 Re1 55.29(3) . . ?
As3 Re4 Re1 55.33(2) . . ?
As4 Re4 Re1 103.84(3) . . ?
Re3 Re4 Re1 60.170(10) . . ?
Re2 Re4 Re1 59.861(10) . . ?
Re3 As1 Re2 69.37(3) . . ?
Re3 As1 Re1 69.58(3) . . ?
Re2 As1 Re1 69.33(3) . . ?
Re4 As2 Re3 70.11(3) . . ?
Re4 As2 Re1 70.25(3) . . ?
Re3 As2 Re1 70.18(3) . . ?
Re4 As3 Re2 69.99(3) . . ?
Re4 As3 Re1 69.88(3) . . ?
Re2 As3 Re1 69.59(3) . . ?
Re2 As4 Re4 69.48(3) . . ?
Re2 As4 Re3 69.02(3) . . ?
Re4 As4 Re3 68.91(3) . . ?
N33 Na1 N33 180.0 . 2_766 ?
N33 Na1 N22 90.06(19) . 2_766 ?
N33 Na1 N22 89.94(19) 2_766 2_766 ?
N33 Na1 N22 89.94(19) . . ?
N33 Na1 N22 90.06(19) 2_766 . ?
N22 Na1 N22 180.0 2_766 . ?
N33 Na1 N43 96.9(2) . 2_666 ?
N33 Na1 N43 83.1(2) 2_766 2_666 ?
N22 Na1 N43 92.74(19) 2_766 2_666 ?
N22 Na1 N43 87.3(2) . 2_666 ?
N33 Na1 N43 83.1(2) . 1_655 ?
N33 Na1 N43 96.9(2) 2_766 1_655 ?
N22 Na1 N43 87.3(2) 2_766 1_655 ?
N22 Na1 N43 92.7(2) . 1_655 ?
N43 Na1 N43 180.0 2_666 1_655 ?
N33 Na1 Na4 134.17(14) . 1_655 ?
N33 Na1 Na4 45.83(14) 2_766 1_655 ?
N22 Na1 Na4 135.62(14) 2_766 1_655 ?
N22 Na1 Na4 44.38(14) . 1_655 ?
N43 Na1 Na4 86.18(15) 2_666 1_655 ?
N43 Na1 Na4 93.82(15) 1_655 1_655 ?
N33 Na1 Na4 45.83(14) . 2_666 ?
N33 Na1 Na4 134.17(14) 2_766 2_666 ?
N22 Na1 Na4 44.38(14) 2_766 2_666 ?
N22 Na1 Na4 135.62(14) . 2_666 ?
N43 Na1 Na4 93.82(15) 2_666 2_666 ?
N43 Na1 Na4 86.18(15) 1_655 2_666 ?
Na4 Na1 Na4 180.0 1_655 2_666 ?
O3W Na2 O1W 99.1(2) . . ?
O3W Na2 N41 76.9(2) . 1_655 ?
O1W Na2 N41 96.4(2) . 1_655 ?
O3W Na2 N21 175.7(2) . . ?
O1W Na2 N21 83.4(2) . . ?
N41 Na2 N21 106.5(2) 1_655 . ?
O3W Na2 N11 87.6(2) . 2_767 ?
O1W Na2 N11 83.0(2) . 2_767 ?
N41 Na2 N11 164.2(2) 1_655 2_767 ?
N21 Na2 N11 89.2(2) . 2_767 ?
O3W Na2 N11 85.3(2) . . ?
O1W Na2 N11 169.4(2) . . ?
N41 Na2 N11 94.0(2) 1_655 . ?
N21 Na2 N11 91.7(2) . . ?
N11 Na2 N11 87.6(2) 2_767 . ?
O3W Na2 C21 159.6(2) . . ?
O1W Na2 C21 99.5(2) . . ?
N41 Na2 C21 92.6(2) 1_655 . ?
N21 Na2 C21 20.17(18) . . ?
N11 Na2 C21 103.1(2) 2_767 . ?
N11 Na2 C21 77.9(2) . . ?
O3W Na2 Na6 132.79(17) . . ?
O1W Na2 Na6 80.50(15) . . ?
N41 Na2 Na6 150.36(18) 1_655 . ?
N21 Na2 Na6 43.95(15) . . ?
N11 Na2 Na6 45.22(15) 2_767 . ?
N11 Na2 Na6 89.44(16) . . ?
C21 Na2 Na6 59.39(14) . . ?
O3W Na2 Na6 41.01(14) . 2_767 ?
O1W Na2 Na6 139.59(17) . 2_767 ?
N41 Na2 Na6 81.97(16) 1_655 2_767 ?
N21 Na2 Na6 136.03(19) . 2_767 ?
N11 Na2 Na6 88.26(15) 2_767 2_767 ?
N11 Na2 Na6 44.36(15) . 2_767 ?
C21 Na2 Na6 120.93(17) . 2_767 ?
Na6 Na2 Na6 119.28(9) . 2_767 ?
O3W Na2 Na2 85.12(16) . 2_767 ?
O1W Na2 Na2 126.63(18) . 2_767 ?
N41 Na2 Na2 135.6(2) 1_655 2_767 ?
N21 Na2 Na2 90.59(18) . 2_767 ?
N11 Na2 Na2 43.79(15) 2_767 2_767 ?
N11 Na2 Na2 43.77(14) . 2_767 ?
C21 Na2 Na2 90.70(16) . 2_767 ?
Na6 Na2 Na2 60.36(9) . 2_767 ?
Na6 Na2 Na2 58.92(9) 2_767 2_767 ?
O3W Na2 Na3 139.42(18) . 1_545 ?
O1W Na2 Na3 40.59(14) . 1_545 ?
N41 Na2 Na3 99.56(17) 1_655 1_545 ?
N21 Na2 Na3 43.42(16) . 1_545 ?
N11 Na2 Na3 90.29(15) 2_767 1_545 ?
N11 Na2 Na3 135.09(17) . 1_545 ?
C21 Na2 Na3 58.96(15) . 1_545 ?
Na6 Na2 Na3 59.25(8) . 1_545 ?
Na6 Na2 Na3 178.47(11) 2_767 1_545 ?
Na2 Na2 Na3 119.61(12) 2_767 1_545 ?
N42 Na3 N12 171.1(3) 1_665 . ?
N42 Na3 O1W 83.3(2) 1_665 1_565 ?
N12 Na3 O1W 95.7(2) . 1_565 ?
N42 Na3 O1 74.5(2) 1_665 . ?
N12 Na3 O1 96.6(3) . . ?
O1W Na3 O1 80.4(2) 1_565 . ?
N42 Na3 N31 87.6(2) 1_665 . ?
N12 Na3 N31 92.8(2) . . ?
O1W Na3 N31 170.5(2) 1_565 . ?
O1 Na3 N31 94.4(2) . . ?
N42 Na3 N21 100.6(2) 1_665 1_565 ?
N12 Na3 N21 87.9(2) . 1_565 ?
O1W Na3 N21 80.4(2) 1_565 1_565 ?
O1 Na3 N21 160.7(3) . 1_565 ?
N31 Na3 N21 104.2(2) . 1_565 ?
N42 Na3 Na4 42.40(16) 1_665 1_665 ?
N12 Na3 Na4 138.59(18) . 1_665 ?
O1W Na3 Na4 125.52(16) 1_565 1_665 ?
O1 Na3 Na4 87.58(18) . 1_665 ?
N31 Na3 Na4 45.77(14) . 1_665 ?
N21 Na3 Na4 101.48(17) 1_565 1_665 ?
N42 Na3 Na6 142.4(2) 1_665 1_565 ?
N12 Na3 Na6 45.35(16) . 1_565 ?
O1W Na3 Na6 79.46(15) 1_565 1_565 ?
O1 Na3 Na6 133.8(2) . 1_565 ?
N31 Na3 Na6 109.71(18) . 1_565 ?
N21 Na3 Na6 43.68(15) 1_565 1_565 ?
Na4 Na3 Na6 137.26(12) 1_665 1_565 ?
N42 Na3 Na2 87.14(18) 1_665 1_565 ?
N12 Na3 Na2 97.80(17) . 1_565 ?
O1W Na3 Na2 39.61(14) 1_565 1_565 ?
O1 Na3 Na2 119.3(2) . 1_565 ?
N31 Na3 Na2 142.96(19) . 1_565 ?
N21 Na3 Na2 41.41(15) 1_565 1_565 ?
Na4 Na3 Na2 115.95(10) 1_665 1_565 ?
Na6 Na3 Na2 58.69(8) 1_565 1_565 ?
O6W Na4 O5W 114.2(2) . . ?
O6W Na4 N22 77.4(2) . 1_455 ?
O5W Na4 N22 160.8(3) . 1_455 ?
O6W Na4 N42 165.5(2) . . ?
O5W Na4 N42 78.4(3) . . ?
N22 Na4 N42 92.6(2) 1_455 . ?
O6W Na4 N33 83.1(2) . 2_666 ?
O5W Na4 N33 75.0(2) . 2_666 ?
N22 Na4 N33 92.1(2) 1_455 2_666 ?
N42 Na4 N33 108.0(2) . 2_666 ?
O6W Na4 N31 83.4(2) . 1_445 ?
O5W Na4 N31 100.0(3) . 1_445 ?
N22 Na4 N31 96.4(2) 1_455 1_445 ?
N42 Na4 N31 87.4(2) . 1_445 ?
N33 Na4 N31 162.0(2) 2_666 1_445 ?
O6W Na4 Na5 42.30(14) . 1_445 ?
O5W Na4 Na5 140.3(2) . 1_445 ?
N22 Na4 Na5 58.58(17) 1_455 1_445 ?
N42 Na4 Na5 123.4(2) . 1_445 ?
N33 Na4 Na5 119.51(18) 2_666 1_445 ?
N31 Na4 Na5 54.06(16) 1_445 1_445 ?
O6W Na4 Na1 78.92(14) . 1_455 ?
O5W Na4 Na1 118.7(2) . 1_455 ?
N22 Na4 Na1 46.22(15) 1_455 1_455 ?
N42 Na4 Na1 101.80(17) . 1_455 ?
N33 Na4 Na1 46.08(15) 2_666 1_455 ?
N31 Na4 Na1 141.26(18) 1_445 1_455 ?
Na5 Na4 Na1 91.04(8) 1_445 1_455 ?
O6W Na4 Na3 126.23(16) . 1_445 ?
O5W Na4 Na3 93.9(2) . 1_445 ?
N22 Na4 Na3 90.40(17) 1_455 1_445 ?
N42 Na4 Na3 42.31(16) . 1_445 ?
N33 Na4 Na3 150.32(18) 2_666 1_445 ?
N31 Na4 Na3 45.70(15) 1_445 1_445 ?
Na5 Na4 Na3 86.69(9) 1_445 1_445 ?
Na1 Na4 Na3 127.21(9) 1_455 1_445 ?
O6W Na5 N32 88.3(2) 1_665 2_676 ?
O6W Na5 N23 159.9(2) 1_665 1_565 ?
N32 Na5 N23 96.5(2) 2_676 1_565 ?
O6W Na5 N32 94.0(2) 1_665 . ?
N32 Na5 N32 82.9(2) 2_676 . ?
N23 Na5 N32 105.9(2) 1_565 . ?
O6W Na5 N31 77.7(2) 1_665 . ?
N32 Na5 N31 165.2(2) 2_676 . ?
N23 Na5 N31 98.3(2) 1_565 . ?
N32 Na5 N31 92.9(2) . . ?
O6W Na5 C23 138.4(2) 1_665 1_565 ?
N32 Na5 C23 96.2(2) 2_676 1_565 ?
N23 Na5 C23 21.85(18) 1_565 1_565 ?
N32 Na5 C23 127.7(2) . 1_565 ?
N31 Na5 C23 97.6(2) . 1_565 ?
O6W Na5 N22 66.41(18) 1_665 1_565 ?
N32 Na5 N22 99.9(2) 2_676 1_565 ?
N23 Na5 N22 93.6(2) 1_565 1_565 ?
N32 Na5 N22 159.9(2) . 1_565 ?
N31 Na5 N22 79.31(18) . 1_565 ?
C23 Na5 N22 72.04(19) 1_565 1_565 ?
O6W Na5 C32 97.2(2) 1_665 . ?
N32 Na5 C32 104.8(2) 2_676 . ?
N23 Na5 C32 100.3(2) 1_565 . ?
N32 Na5 C32 22.07(18) . . ?
N31 Na5 C32 72.45(19) . . ?
C23 Na5 C32 121.1(2) 1_565 . ?
N22 Na5 C32 150.0(2) 1_565 . ?
O6W Na5 Na4 42.29(14) 1_665 1_665 ?
N32 Na5 Na4 123.12(19) 2_676 1_665 ?
N23 Na5 Na4 121.73(18) 1_565 1_665 ?
N32 Na5 Na4 118.63(17) . 1_665 ?
N31 Na5 Na4 47.22(13) . 1_665 ?
C23 Na5 Na4 105.43(17) 1_565 1_665 ?
N22 Na5 Na4 43.63(13) 1_565 1_665 ?
C32 Na5 Na4 107.22(17) . 1_665 ?
O6W Na5 Na5 91.74(17) 1_665 2_676 ?
N32 Na5 Na5 44.21(15) 2_676 2_676 ?
N23 Na5 Na5 105.3(2) 1_565 2_676 ?
N32 Na5 Na5 38.72(15) . 2_676 ?
N31 Na5 Na5 130.17(18) . 2_676 ?
C23 Na5 Na5 119.9(2) 1_565 2_676 ?
N22 Na5 Na5 140.17(18) 1_565 2_676 ?
C32 Na5 Na5 60.66(16) . 2_676 ?
Na4 Na5 Na5 132.93(14) 1_665 2_676 ?
O2W Na6 O3W 80.6(2) . 2_767 ?
O2W Na6 O4W 84.7(2) . 2_667 ?
O3W Na6 O4W 78.3(2) 2_767 2_667 ?
O2W Na6 N21 169.3(2) . . ?
O3W Na6 N21 90.2(2) 2_767 . ?
O4W Na6 N21 98.9(2) 2_667 . ?
O2W Na6 N11 85.2(2) . 2_767 ?
O3W Na6 N11 82.7(2) 2_767 2_767 ?
O4W Na6 N11 159.7(2) 2_667 2_767 ?
N21 Na6 N11 88.2(2) . 2_767 ?
O2W Na6 N12 103.5(2) . 1_545 ?
O3W Na6 N12 170.8(2) 2_767 1_545 ?
O4W Na6 N12 93.7(2) 2_667 1_545 ?
N21 Na6 N12 86.5(2) . 1_545 ?
N11 Na6 N12 105.8(2) 2_767 1_545 ?
O2W Na6 Na7 42.38(14) . 1_545 ?
O3W Na6 Na7 73.44(14) 2_767 1_545 ?
O4W Na6 Na7 42.45(14) 2_667 1_545 ?
N21 Na6 Na7 139.72(19) . 1_545 ?
N11 Na6 Na7 124.42(16) 2_767 1_545 ?
N12 Na6 Na7 103.79(16) 1_545 1_545 ?
O2W Na6 Na2 129.44(17) . . ?
O3W Na6 Na2 85.07(15) 2_767 . ?
O4W Na6 Na2 138.84(18) 2_667 . ?
N21 Na6 Na2 43.32(15) . . ?
N11 Na6 Na2 44.84(14) 2_767 . ?
N12 Na6 Na2 98.30(17) 1_545 . ?
Na7 Na6 Na2 157.79(10) 1_545 . ?
O2W Na6 Na3 143.43(19) . 1_545 ?
O3W Na6 Na3 135.35(17) 2_767 1_545 ?
O4W Na6 Na3 106.18(17) 2_667 1_545 ?
N21 Na6 Na3 45.18(16) . 1_545 ?
N11 Na6 Na3 92.35(16) 2_767 1_545 ?
N12 Na6 Na3 42.37(15) 1_545 1_545 ?
Na7 Na6 Na3 138.89(10) 1_545 1_545 ?
Na2 Na6 Na3 62.06(8) . 1_545 ?
O2W Na6 Na2 78.92(15) . 2_767 ?
O3W Na6 Na2 38.72(13) 2_767 2_767 ?
O4W Na6 Na2 116.49(18) 2_667 2_767 ?
N21 Na6 Na2 90.44(16) . 2_767 ?
N11 Na6 Na2 44.01(15) 2_767 2_767 ?
N12 Na6 Na2 149.78(19) 1_545 2_767 ?
Na7 Na6 Na2 97.92(8) 1_545 2_767 ?
Na2 Na6 Na2 60.72(9) . 2_767 ?
Na3 Na6 Na2 122.79(10) 1_545 2_767 ?
O4W Na7 O4W 180.0 2_677 . ?
O4W Na7 O2W 94.70(19) 2_677 2_667 ?
O4W Na7 O2W 85.30(19) . 2_667 ?
O4W Na7 O2W 85.30(19) 2_677 1_565 ?
O4W Na7 O2W 94.70(19) . 1_565 ?
O2W Na7 O2W 180.0 2_667 1_565 ?
O4W Na7 N13 90.7(2) 2_677 . ?
O4W Na7 N13 89.3(2) . . ?
O2W Na7 N13 95.33(19) 2_667 . ?
O2W Na7 N13 84.67(19) 1_565 . ?
O4W Na7 N13 89.3(2) 2_677 2_677 ?
O4W Na7 N13 90.7(2) . 2_677 ?
O2W Na7 N13 84.67(19) 2_667 2_677 ?
O2W Na7 N13 95.33(19) 1_565 2_677 ?
N13 Na7 N13 180.0 . 2_677 ?
O4W Na7 Na6 43.99(15) 2_677 1_565 ?
O4W Na7 Na6 136.01(15) . 1_565 ?
O2W Na7 Na6 138.59(13) 2_667 1_565 ?
O2W Na7 Na6 41.41(13) 1_565 1_565 ?
N13 Na7 Na6 89.00(16) . 1_565 ?
N13 Na7 Na6 91.00(16) 2_677 1_565 ?
O4W Na7 Na6 136.01(15) 2_677 2_667 ?
O4W Na7 Na6 43.99(15) . 2_667 ?
O2W Na7 Na6 41.41(13) 2_667 2_667 ?
O2W Na7 Na6 138.59(13) 1_565 2_667 ?
N13 Na7 Na6 91.00(16) . 2_667 ?
N13 Na7 Na6 89.00(16) 2_677 2_667 ?
Na6 Na7 Na6 180.0 1_565 2_667 ?
C1 O1 Na3 114.7(7) . . ?
Na2 O1W Na3 99.8(2) . 1_545 ?
Na6 O2W Na7 96.2(2) . 1_545 ?
Na2 O3W Na6 100.3(2) . 2_767 ?
Na7 O4W Na6 93.6(2) . 2_667 ?
Na4 O6W Na5 95.4(2) . 1_445 ?
C11 N11 Na2 128.2(5) . 2_767 ?
C11 N11 Na2 114.9(5) . . ?
Na2 N11 Na2 92.4(2) 2_767 . ?
C11 N11 Na6 129.3(5) . 2_767 ?
Na2 N11 Na6 89.9(2) 2_767 2_767 ?
Na2 N11 Na6 91.6(2) . 2_767 ?
C12 N12 Na3 124.7(5) . . ?
C12 N12 Na6 120.6(6) . 1_565 ?
Na3 N12 Na6 92.3(2) . 1_565 ?
C13 N13 Na7 124.5(6) . . ?
C21 N21 Na2 111.9(5) . . ?
C21 N21 Na6 128.8(6) . . ?
Na2 N21 Na6 92.7(2) . . ?
C21 N21 Na3 127.9(5) . 1_545 ?
Na2 N21 Na3 95.2(2) . 1_545 ?
Na6 N21 Na3 91.1(2) . 1_545 ?
C22 N22 Na4 142.5(5) . 1_655 ?
C22 N22 Na1 124.7(5) . . ?
Na4 N22 Na1 89.4(2) 1_655 . ?
C22 N22 Na5 90.7(5) . 1_545 ?
Na4 N22 Na5 77.78(18) 1_655 1_545 ?
Na1 N22 Na5 126.8(2) . 1_545 ?
C23 N23 Na5 100.6(5) . 1_545 ?
C31 N31 Na3 120.9(6) . . ?
C31 N31 Na4 146.1(6) . 1_665 ?
Na3 N31 Na4 88.5(2) . 1_665 ?
C31 N31 Na5 94.2(5) . . ?
Na3 N31 Na5 126.2(3) . . ?
Na4 N31 Na5 78.73(19) 1_665 . ?
C32 N32 Na5 163.4(6) . 2_676 ?
C32 N32 Na5 97.8(5) . . ?
Na5 N32 Na5 97.1(2) 2_676 . ?
C33 N33 Na4 144.0(5) . 2_666 ?
C33 N33 Na1 125.5(5) . . ?
Na4 N33 Na1 88.1(2) 2_666 . ?
C41 N41 Na2 124.2(5) . 1_455 ?
C42 N42 Na3 141.2(6) . 1_445 ?
C42 N42 Na4 121.8(5) . . ?
Na3 N42 Na4 95.3(2) 1_445 . ?
C43 N43 Na1 130.3(6) . 1_455 ?
N11 C11 Re1 178.0(6) . . ?
N12 C12 Re1 176.6(7) . . ?
N13 C13 Re1 175.9(6) . . ?
N21 C21 Re2 175.7(6) . . ?
N21 C21 Na2 47.9(4) . . ?
Re2 C21 Na2 136.4(3) . . ?
N22 C22 Re2 176.7(6) . . ?
N23 C23 Re2 175.4(7) . . ?
N23 C23 Na5 57.6(5) . 1_545 ?
Re2 C23 Na5 118.6(3) . 1_545 ?
N31 C31 Re3 175.0(7) . . ?
N32 C32 Re3 174.0(6) . . ?
N32 C32 Na5 60.2(4) . . ?
Re3 C32 Na5 115.3(3) . . ?
N33 C33 Re3 176.4(6) . . ?
N41 C41 Re4 178.9(6) . . ?
N42 C42 Re4 173.9(7) . . ?
N43 C43 Re4 178.2(6) . . ?

_refine_diff_density_max         2.231
_refine_diff_density_min         -1.204
_refine_diff_density_rms         0.285


_vrf_PLAT430_LHY010              
;
PROBLEM: Short Inter D...A Contact O2 ..O6 . 2.68 Ang.
RESPONSE: H atoms of water molecules were not located but included in
the formula of the compound.
;

