# Supplementary Information (SI) for Inorganic Chemistry Frontiers.
# This journal is © the Partner Organisations 2025

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
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data_p21-m_sq
_database_code_depnum_ccdc_archive 'CCDC 2391027'
loop_
_audit_author_name
_audit_author_address
'shan jin'
;An Hui University
China
;
_audit_update_record             
;
2024-10-15 deposited with the CCDC.	2025-02-04 downloaded from the CCDC.
;
_audit_creation_date             2024-10-15
_audit_creation_method           
;
Olex2 1.2
(compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C190 H254 Ag20 Cl8 Cu10 P4 S14, C H2 Cl2'
_chemical_formula_sum            'C191 H256 Ag20 Cl10 Cu10 P4 S14'
_chemical_formula_weight         6271.96
_chemical_absolute_configuration ad
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag 0.1306 4.2820 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu -1.9646 0.5888 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           4
_space_group_name_H-M_alt        'P 1 21 1'
_space_group_name_Hall           'P 2yb'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z'

_cell_length_a                   21.403(2)
_cell_length_b                   20.1937(18)
_cell_length_c                   25.418(2)
_cell_angle_alpha                90
_cell_angle_beta                 94.635(7)
_cell_angle_gamma                90
_cell_volume                     10949.9(17)
_cell_formula_units_Z            2
_cell_measurement_reflns_used    55702
_cell_measurement_temperature    120(2)
_cell_measurement_theta_max      69.76
_cell_measurement_theta_min      4.71
_shelx_estimated_absorpt_T_max   ?
_shelx_estimated_absorpt_T_min   ?
_exptl_absorpt_coefficient_mu    17.964
_exptl_absorpt_correction_T_max  ?
_exptl_absorpt_correction_T_min  ?
_exptl_absorpt_correction_type   ?
_exptl_absorpt_process_details   ?
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            ?
_exptl_crystal_density_diffrn    1.902
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             6172
_exptl_crystal_size_max          ?
_exptl_crystal_size_mid          ?
_exptl_crystal_size_min          ?
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0288
_diffrn_reflns_av_unetI/netI     0.0241
_diffrn_reflns_Laue_measured_fraction_full 0.972
_diffrn_reflns_Laue_measured_fraction_max 0.953
_diffrn_reflns_limit_h_max       25
_diffrn_reflns_limit_h_min       -25
_diffrn_reflns_limit_k_max       24
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       26
_diffrn_reflns_limit_l_min       -30
_diffrn_reflns_number            55554
_diffrn_reflns_point_group_measured_fraction_full 0.670
_diffrn_reflns_point_group_measured_fraction_max 0.653
_diffrn_reflns_theta_full        67.686
_diffrn_reflns_theta_max         69.756
_diffrn_reflns_theta_min         5.603
_diffrn_ambient_temperature      120(2)
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.972
_diffrn_measured_fraction_theta_max 0.953
_diffrn_measurement_device_type  stoe
_diffrn_measurement_method       ?
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54186
_diffrn_source                   ?
_reflns_Friedel_coverage         0.331
_reflns_Friedel_fraction_full    0.349
_reflns_Friedel_fraction_max     0.335
_reflns_number_gt                25558
_reflns_number_total             27000
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       ?
_computing_data_collection       ?
_computing_data_reduction        ?
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    ?
_refine_diff_density_max         1.235
_refine_diff_density_min         -1.443
_refine_diff_density_rms         0.163
_refine_ls_abs_structure_details 
;
 Flack x determined using 5965 quotients [(I+)-(I-)]/[(I+)+(I-)]
 (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259).
;
_refine_ls_abs_structure_Flack   0.449(5)
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.022
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     2170
_refine_ls_number_reflns         27000
_refine_ls_number_restraints     2895
_refine_ls_R_factor_all          0.0578
_refine_ls_R_factor_gt           0.0551
_refine_ls_restrained_S_all      2.773
_refine_ls_shift/su_max          0.007
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.1102P)²+38.6624P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1491
_refine_ls_wR_factor_ref         0.1524
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups, All C(H,H) groups
2. Restrained distances
 C026-C023 = C026-C020 = C058-C020 = C045-C020 = C04L-C045 = C04Z-C04L = C04Z-
 C023 = C03R-C023 = C05D-C03R = C05D-C058 = C05D-C04K = C04L-C04K
 1.54 with sigma of 0.01
 C36-C02I = C040-C02I = C6AA-C02I = C5-C040 = C5-C4AA = C5AA-C5 = C7AA-C5AA =
 C7AA-C17 = C51-C17 = C51-C4AA = C51-C36 = C7AA-C6AA
 1.54 with sigma of 0.01
 C02I-C5
 2.54 with sigma of 0.01
 C02I-C51
 2.54 with sigma of 0.01
 C02I-C7AA
 2.54 with sigma of 0.01
 C040-C4AA
 2.54 with sigma of 0.01
 C040-C5AA
 2.54 with sigma of 0.01
 C040-C36
 2.54 with sigma of 0.01
 C36-C6AA
 2.54 with sigma of 0.01
 C36-C4AA
 2.54 with sigma of 0.01
 C36-C17
 2.54 with sigma of 0.01
 C51-C5
 2.54 with sigma of 0.01
 C4AA-C5AA
 2.54 with sigma of 0.01
 C5-C7AA
 2.54 with sigma of 0.01
 C5AA-C17
 2.54 with sigma of 0.01
 C7AA-C51
 2.54 with sigma of 0.01
 C02I-C4AA
 2.93 with sigma of 0.01
 C02I-C5AA
 2.93 with sigma of 0.01
 C02I-C17
 2.93 with sigma of 0.01
 C040-C7AA
 2.93 with sigma of 0.01
 C040-C51
 2.93 with sigma of 0.01
 C36-C5
 2.93 with sigma of 0.01
 C51-C5AA
 2.93 with sigma of 0.01
 C4AA-C7AA
 2.93 with sigma of 0.01
 C17-C5
 2.93 with sigma of 0.01
 C053-C037 = C053-C04Y = C04Y-C034 = C043-C034 = C03Z-C034 = C04I-C03Z = C04I-
 C032 = C04I-C04C = C053-C04C = C037-C02J = C043-C02J = C032-C02J
 1.54 with sigma of 0.01
 C03V-C03M = C1AA-C03V = C3AA-C1AA = C7-C3AA = C2AA-C1AA = C7-C05B = C05B-C03M
 = C04N-C03M = C2AA-C04X = C04X-C04N = C11-C04X = C7-C11
 1.54 with sigma of 0.01
 C026-C020 = C026-C023 = C03R-C023 = C04Z-C023 = C05D-C03R = C058-C020 = C05D-
 C058 = C05D-C04K = C04Z-C04L = C04L-C04K = C04L-C045 = C045-C020
 1.54 with sigma of 0.01
 C044-C03J = C55-C03J = C55-C03O = C04M-C03O = C03O-C02F = C02F-C01Y = C1-C01Y
 = C02O-C01Y = C046-C02O = C1-C03J = C04M-C046 = C046-C044
 1.54 with sigma of 0.01
 C01Y-C03J
 2.54 with sigma of 0.01
 C01Y-C046
 2.54 with sigma of 0.01
 C01Y-C03O
 2.54 with sigma of 0.01
 C02O-C044
 2.54 with sigma of 0.01
 C02O-C04M
 2.54 with sigma of 0.01
 C1-C55
 2.54 with sigma of 0.01
 C1-C02F
 2.54 with sigma of 0.01
 C03J-C03O
 2.54 with sigma of 0.01
 C55-C04M
 2.54 with sigma of 0.01
 C03O-C046
 2.54 with sigma of 0.01
 C04M-C044
 2.54 with sigma of 0.01
 C30-C21 = C33-C21 = C33-C04J = C04J-C02S = C04J-C02Q = C03B-C02Q = C03C-C03B =
  C03B-C01O = C01U-C01O = C02S-C01U = C30-C01U = C21-C03C
 1.54 with sigma of 0.01
 C70-C160 = C70-C161 = C70-C122 = C5BA-C160 = C5BA-C3BA = C5BA-C100 = C2BA-
 C100 = C4BA-C2BA = C4BA-C128 = C3BA-C128 = C2BA-C122 = C161-C128
 1.54 with sigma of 0.01
 C70-C5BA
 2.54 with sigma of 0.01
 C70-C2BA
 2.54 with sigma of 0.01
 C70-C128
 2.54 with sigma of 0.01
 C160-C3BA
 2.54 with sigma of 0.01
 C160-C100
 2.54 with sigma of 0.01
 C160-C122
 2.54 with sigma of 0.01
 C160-C161
 2.54 with sigma of 0.01
 C161-C122
 2.54 with sigma of 0.01
 C161-C3BA
 2.54 with sigma of 0.01
 C161-C4BA
 2.54 with sigma of 0.01
 C128-C5BA
 2.54 with sigma of 0.01
 C70-C3BA
 2.93 with sigma of 0.01
 C70-C100
 2.93 with sigma of 0.01
 C70-C4BA
 2.93 with sigma of 0.01
 C160-C2BA
 2.93 with sigma of 0.01
 C160-C128
 2.93 with sigma of 0.01
 C161-C5BA
 2.93 with sigma of 0.01
 C161-C2BA
 2.93 with sigma of 0.01
 C5BA-C4BA
 2.93 with sigma of 0.01
 C128-C100
 2.93 with sigma of 0.01
 C3BA-C100
 2.54 with sigma of 0.01
 C5BA-C2BA
 2.54 with sigma of 0.01
 C100-C4BA
 2.54 with sigma of 0.01
 C2BA-C128
 2.54 with sigma of 0.01
 C3BA-C2BA
 2.93 with sigma of 0.01
 C4BA-C5BA
 2.93 with sigma of 0.01
 C100-C128
 2.93 with sigma of 0.01
 C162-C04E = C6BA-C162 = C6BA-C132 = C92-C6BA = C92-C82 = C82-C37 = C82-C052 =
 C37-C34 = C34-C132 = C34-C0AA = C0AA-C04E = C052-C04E
 1.54 with sigma of 0.01
 C04E-C82
 2.54 with sigma of 0.01
 C04E-C34
 2.54 with sigma of 0.01
 C0AA-C132
 2.54 with sigma of 0.01
 C0AA-C052
 2.54 with sigma of 0.01
 C0AA-C162
 2.54 with sigma of 0.01
 C04E-C6BA
 2.54 with sigma of 0.01
 C162-C132
 2.54 with sigma of 0.01
 C162-C92
 2.54 with sigma of 0.01
 C34-C6BA
 2.54 with sigma of 0.01
 C132-C92
 2.54 with sigma of 0.01
 C6BA-C82
 2.54 with sigma of 0.01
 C92-C37
 2.54 with sigma of 0.01
 C82-C34
 2.54 with sigma of 0.01
 C04E-C132
 2.93 with sigma of 0.01
 C04E-C92
 2.93 with sigma of 0.01
 C04E-C37
 2.93 with sigma of 0.01
 C132-C82
 2.93 with sigma of 0.01
 C6BA-C37
 2.93 with sigma of 0.01
 C92-C34
 2.93 with sigma of 0.01
 C0AA-C82
 2.93 with sigma of 0.01
 C19-C03Q = C19-C0BA = C181-C0BA = C181-C055 = C9AA-C03Q = C9AA-C055 = C22-
 C153 = C1BA-C055 = C22-C1BA = C22-C051 = C0BA-C051 = C153-C03Q
 1.54 with sigma of 0.01
 C9AA-C1BA
 2.54 with sigma of 0.01
 C181-C051
 2.54 with sigma of 0.01
 C03Q-C181
 2.93 with sigma of 0.01
 C03Q-C051
 2.93 with sigma of 0.01
 C03Q-C1BA
 2.93 with sigma of 0.01
 C181-C22
 2.93 with sigma of 0.01
 C055-C051
 2.93 with sigma of 0.01
 C1BA-C0BA
 2.93 with sigma of 0.01
 C9AA-C0BA
 2.93 with sigma of 0.01
 C9AA-C22
 2.93 with sigma of 0.01
 C9AA-C03Q = C9AA-C055 = C1BA-C055 = C22-C1BA = C22-C153 = C153-C03Q = C0BA-
 C051 = C22-C051 = C181-C0BA = C181-C055
 1.54 with sigma of 0.01
 C153-C9AA
 2.54 with sigma of 0.01
 C153-C1BA
 2.54 with sigma of 0.01
 H16D-H19B
 1.99 with sigma of 0.001
 S1G-C161
 2.7 with sigma of 0.01
 S1G-C160
 2.7 with sigma of 0.01
 H16D-H19A
 1.94 with sigma of 0.001
 C161-C19
 3.8 with sigma of 0.001
 C19-C03Q = C19-C0BA = C181-C0BA = C0BA-C051 = C22-C051 = C22-C1BA = C1BA-C055
 = C181-C055 = C22-C153 = C153-C03Q = C9AA-C03Q = C9AA-C055
 1.54 with sigma of 0.001
 C03Q-C0BA
 2.54 with sigma of 0.001
 C03Q-C22
 2.54 with sigma of 0.001
 C03Q-C055
 2.54 with sigma of 0.001
 C19-C181
 2.54 with sigma of 0.001
 C19-C9AA
 2.54 with sigma of 0.001
 C19-C051
 2.54 with sigma of 0.001
 C0BA-C22
 2.54 with sigma of 0.001
 C051-C1BA
 2.54 with sigma of 0.001
 C22-C055
 2.54 with sigma of 0.001
 C1BA-C181
 2.54 with sigma of 0.001
 C055-C0BA
 2.54 with sigma of 0.001
 C9AA-C181
 2.54 with sigma of 0.001
 H18B_$1-H15
 2 with sigma of 0.001
 H51_$2-H98
 2 with sigma of 0.001
3. Uiso/Uaniso restraints and constraints
S1G \\sim C70 \\sim C161 \\sim C122 \\sim C160 \\sim C2BA \\sim C5BA \\sim C3BA
\\sim C128 \\sim C100 \\sim C4BA: within 3.8A with sigma of 0.01 and sigma for
terminal atoms of 0.02
S1I \\sim C9AA \\sim C03Q \\sim C19 \\sim C055 \\sim C0BA \\sim C181 \\sim C051
\\sim C1BA \\sim C22 \\sim C153: within 3.8A with sigma of 0.01 and sigma for
terminal atoms of 0.02
C76 \\sim C059 \\sim C9 \\sim C23 \\sim C6 \\sim C28 \\sim P1J \\sim C43 \\sim
C047 \\sim C103 \\sim C26 \\sim C04T \\sim C64 \\sim P1F \\sim C02K \\sim C15
\\sim C104 \\sim C03K \\sim C93 \\sim C98 \\sim C04B \\sim C04R \\sim C02Y
\\sim C04F \\sim C04O \\sim C4: within 3.8A with sigma of 0.01 and sigma for
terminal atoms of 0.02
S1C \\sim C02I \\sim C040 \\sim C5 \\sim C5AA \\sim C7AA \\sim C6AA \\sim C17
\\sim C51 \\sim C4AA \\sim C36: within 3.8A with sigma of 0.01 and sigma for
terminal atoms of 0.02
Uanis(C01N) \\sim Ueq, Uanis(C01O) \\sim Ueq, Uanis(C01P) \\sim Ueq,
Uanis(C01Q) \\sim Ueq, Uanis(C01S) \\sim Ueq, Uanis(C01T) \\sim Ueq,
Uanis(C01U) \\sim Ueq, Uanis(C01V) \\sim Ueq, Uanis(C01W) \\sim Ueq,
Uanis(C01X) \\sim Ueq, Uanis(C01Y) \\sim Ueq, Uanis(C020) \\sim Ueq,
Uanis(C021) \\sim Ueq, Uanis(C022) \\sim Ueq, Uanis(C023) \\sim Ueq,
Uanis(C024) \\sim Ueq, Uanis(C025) \\sim Ueq, Uanis(C026) \\sim Ueq,
Uanis(C027) \\sim Ueq, Uanis(C028) \\sim Ueq, Uanis(C029) \\sim Ueq,
Uanis(C02A) \\sim Ueq, Uanis(C02C) \\sim Ueq, Uanis(C02E) \\sim Ueq,
Uanis(C02F) \\sim Ueq, Uanis(C02G) \\sim Ueq, Uanis(C02H) \\sim Ueq,
Uanis(C02I) \\sim Ueq, Uanis(C02J) \\sim Ueq, Uanis(C02K) \\sim Ueq, Uanis(C15)
\\sim Ueq, Uanis(C104) \\sim Ueq, Uanis(C98) \\sim Ueq, Uanis(C93) \\sim Ueq,
Uanis(C03K) \\sim Ueq, Uanis(C02L) \\sim Ueq, Uanis(C02M) \\sim Ueq,
Uanis(C02N) \\sim Ueq, Uanis(C02O) \\sim Ueq, Uanis(C02P) \\sim Ueq,
Uanis(C02Q) \\sim Ueq, Uanis(C02R) \\sim Ueq, Uanis(C02S) \\sim Ueq,
Uanis(C02T) \\sim Ueq, Uanis(C02U) \\sim Ueq, Uanis(C02V) \\sim Ueq,
Uanis(C02W) \\sim Ueq, Uanis(C02X) \\sim Ueq, Uanis(C02Y) \\sim Ueq,
Uanis(C04F) \\sim Ueq, Uanis(C04O) \\sim Ueq, Uanis(C4) \\sim Ueq, Uanis(C04B)
\\sim Ueq, Uanis(C04R) \\sim Ueq, Uanis(C02Z) \\sim Ueq, Uanis(C031) \\sim Ueq,
Uanis(C032) \\sim Ueq, Uanis(C033) \\sim Ueq, Uanis(C034) \\sim Ueq,
Uanis(C036) \\sim Ueq, Uanis(C037) \\sim Ueq, Uanis(C038) \\sim Ueq, Uanis(C89)
\\sim Ueq, Uanis(C75) \\sim Ueq, Uanis(C71) \\sim Ueq, Uanis(C46) \\sim Ueq,
Uanis(C03X) \\sim Ueq, Uanis(C039) \\sim Ueq, Uanis(C03B) \\sim Ueq,
Uanis(C03C) \\sim Ueq, Uanis(C03D) \\sim Ueq, Uanis(C03E) \\sim Ueq,
Uanis(C03F) \\sim Ueq, Uanis(C03G) \\sim Ueq, Uanis(C03H) \\sim Ueq,
Uanis(C03I) \\sim Ueq, Uanis(C03J) \\sim Ueq, Uanis(C03L) \\sim Ueq,
Uanis(C03M) \\sim Ueq, Uanis(C03O) \\sim Ueq, Uanis(C03P) \\sim Ueq,
Uanis(C03Q) \\sim Ueq, Uanis(C03R) \\sim Ueq, Uanis(C03S) \\sim Ueq,
Uanis(C03T) \\sim Ueq, Uanis(C03U) \\sim Ueq, Uanis(C03V) \\sim Ueq,
Uanis(C03Y) \\sim Ueq, Uanis(C03Z) \\sim Ueq, Uanis(C040) \\sim Ueq,
Uanis(C041) \\sim Ueq, Uanis(C043) \\sim Ueq, Uanis(C044) \\sim Ueq,
Uanis(C045) \\sim Ueq, Uanis(C046) \\sim Ueq, Uanis(C047) \\sim Ueq, Uanis(C43)
\\sim Ueq, Uanis(C04T) \\sim Ueq, Uanis(C64) \\sim Ueq, Uanis(C26) \\sim Ueq,
Uanis(C103) \\sim Ueq, Uanis(C048) \\sim Ueq, Uanis(C04A) \\sim Ueq,
Uanis(C04C) \\sim Ueq, Uanis(C04D) \\sim Ueq, Uanis(C04E) \\sim Ueq,
Uanis(C04I) \\sim Ueq, Uanis(C04J) \\sim Ueq, Uanis(C04K) \\sim Ueq,
Uanis(C04L) \\sim Ueq, Uanis(C04M) \\sim Ueq, Uanis(C04N) \\sim Ueq,
Uanis(C04Q) \\sim Ueq, Uanis(C04S) \\sim Ueq, Uanis(C04U) \\sim Ueq,
Uanis(C04W) \\sim Ueq, Uanis(C04X) \\sim Ueq, Uanis(C04Y) \\sim Ueq,
Uanis(C04Z) \\sim Ueq, Uanis(C050) \\sim Ueq, Uanis(C051) \\sim Ueq,
Uanis(C052) \\sim Ueq, Uanis(C053) \\sim Ueq, Uanis(C054) \\sim Ueq,
Uanis(C055) \\sim Ueq, Uanis(C056) \\sim Ueq, Uanis(C057) \\sim Ueq,
Uanis(C03W) \\sim Ueq, Uanis(C042) \\sim Ueq, Uanis(C035) \\sim Ueq,
Uanis(C02D) \\sim Ueq, Uanis(C03A) \\sim Ueq, Uanis(C058) \\sim Ueq,
Uanis(C059) \\sim Ueq, Uanis(C76) \\sim Ueq, Uanis(C9) \\sim Ueq, Uanis(C23)
\\sim Ueq, Uanis(C6) \\sim Ueq, Uanis(C28) \\sim Ueq, Uanis(C05B) \\sim Ueq,
Uanis(C05D) \\sim Ueq, Uanis(C21) \\sim Ueq, Uanis(C30) \\sim Ueq, Uanis(C33)
\\sim Ueq, Uanis(C1) \\sim Ueq, Uanis(C34) \\sim Ueq, Uanis(C55) \\sim Ueq,
Uanis(C37) \\sim Ueq, Uanis(C82) \\sim Ueq, Uanis(C92) \\sim Ueq, Uanis(C2)
\\sim Ueq, Uanis(C0AA) \\sim Ueq, Uanis(C8) \\sim Ueq, Uanis(C13) \\sim Ueq,
Uanis(C67) \\sim Ueq, Uanis(C3AA) \\sim Ueq, Uanis(C7) \\sim Ueq, Uanis(C11)
\\sim Ueq, Uanis(C1AA) \\sim Ueq, Uanis(C2AA) \\sim Ueq, Uanis(C84) \\sim Ueq,
Uanis(C5) \\sim Ueq, Uanis(C4AA) \\sim Ueq, Uanis(C5AA) \\sim Ueq, Uanis(C6AA)
\\sim Ueq, Uanis(C17) \\sim Ueq, Uanis(C7AA) \\sim Ueq, Uanis(C36) \\sim Ueq,
Uanis(C51) \\sim Ueq, Uanis(C8AA) \\sim Ueq, Uanis(C3) \\sim Ueq, Uanis(C19)
\\sim Ueq, Uanis(C22) \\sim Ueq, Uanis(C9AA) \\sim Ueq, Uanis(C0BA) \\sim Ueq,
Uanis(C1BA) \\sim Ueq, Uanis(C2BA) \\sim Ueq, Uanis(C70) \\sim Ueq, Uanis(C100)
\\sim Ueq, Uanis(C122) \\sim Ueq, Uanis(C128) \\sim Ueq, Uanis(C160) \\sim Ueq,
Uanis(C161) \\sim Ueq, Uanis(C3BA) \\sim Ueq, Uanis(C5BA) \\sim Ueq,
Uanis(C4BA) \\sim Ueq, Uanis(C6BA) \\sim Ueq, Uanis(C132) \\sim Ueq,
Uanis(C162) \\sim Ueq, Uanis(C153) \\sim Ueq, Uanis(C181) \\sim Ueq: with sigma
of 0.005 and sigma for terminal atoms of 0.01
Uanis(S1G) \\sim Ueq, Uanis(C70) \\sim Ueq, Uanis(C161) \\sim Ueq, Uanis(C122)
\\sim Ueq, Uanis(C160) \\sim Ueq, Uanis(C5BA) \\sim Ueq, Uanis(C2BA) \\sim Ueq,
Uanis(C3BA) \\sim Ueq, Uanis(C128) \\sim Ueq, Uanis(C4BA) \\sim Ueq,
Uanis(C100) \\sim Ueq: with sigma of 0.005 and sigma for terminal atoms of 0.01
Uanis(S1I) \\sim Ueq, Uanis(C9AA) \\sim Ueq, Uanis(C1BA) \\sim Ueq, Uanis(C181)
\\sim Ueq, Uanis(C22) \\sim Ueq, Uanis(C051) \\sim Ueq, Uanis(C0BA) \\sim Ueq,
Uanis(C19) \\sim Ueq, Uanis(C03Q) \\sim Ueq, Uanis(C055) \\sim Ueq, Uanis(C153)
\\sim Ueq: with sigma of 0.005 and sigma for terminal atoms of 0.01
Uanis(P1J) \\sim Ueq, Uanis(C76) \\sim Ueq, Uanis(C059) \\sim Ueq, Uanis(C28)
\\sim Ueq, Uanis(C6) \\sim Ueq, Uanis(C23) \\sim Ueq, Uanis(C9) \\sim Ueq,
Uanis(C43) \\sim Ueq, Uanis(C047) \\sim Ueq, Uanis(C103) \\sim Ueq, Uanis(C26)
\\sim Ueq, Uanis(C04T) \\sim Ueq, Uanis(C64) \\sim Ueq, Uanis(C04R) \\sim Ueq,
Uanis(P1F) \\sim Ueq, Uanis(C02K) \\sim Ueq, Uanis(C03K) \\sim Ueq, Uanis(C93)
\\sim Ueq, Uanis(C98) \\sim Ueq, Uanis(C15) \\sim Ueq, Uanis(C104) \\sim Ueq,
Uanis(C04B) \\sim Ueq, Uanis(C4) \\sim Ueq, Uanis(C04O) \\sim Ueq, Uanis(C04F)
\\sim Ueq, Uanis(C02Y) \\sim Ueq: with sigma of 0.005 and sigma for terminal
atoms of 0.01
Uanis(Cu0W) \\sim Ueq, Uanis(Cu0R) \\sim Ueq, Uanis(Cu0P) \\sim Ueq: with sigma
of 0.01 and sigma for terminal atoms of 0.02
4.a Ternary CH refined with riding coordinates:
 C01W(H01W), C023(H023), C027(H027), C029(H029), C02G(H02J), C02L(H02M),
 C02R(H02U), C02Z(H2AA), C033(H033), C034(H034), C03B(H03L), C03I(H03W),
 C03J(H03Y), C03O(H03), C03U(H7AA), C046(H046), C04I(H04U), C04J(H04V),
 C04L(H04Y), C04U(H3BA), C04X(H5BA), C053(H053), C054(H054), C055(H055),
 C05D(H05K), C21(H21), C34(H34), C82(H82), C13(H13), C67(H67), C7(H7),
 C1AA(H1AB), C5(H5), C7AA(H7AB), C51(H51), C3(H3), C22(H22), C0BA(H0BB),
 C2BA(H2BB), C128(H128), C5BA(H5BB), C6BA(H6BB)
4.b Secondary CH2 refined with riding coordinates:
 C01N(H01A,H01B), C01O(H01C,H01D), C01P(H01E,H01F), C01Q(H01G,H01H), C01T(H01I,
 H01J), C026(H02A,H02B), C028(H02C,H02D), C02E(H02F,H02G), C02F(H02H,H02I),
 C02H(H02K,H02L), C02N(H02O,H02P), C02O(H02Q,H02R), C02Q(H02S,H02T), C02S(H02V,
 H02W), C02T(H02X,H02Y), C02W(H02,H), C02X(H0AA,HA), C031(H03A,H03B), C032(H03C,
 H03D), C036(H03E,H03F), C037(H03G,H03H), C039(H03I,H03J), C03C(H03M,H03N),
 C03D(H03O,H03P), C03F(H03R,H03S), C03H(H03U,H03V), C03L(H03Z,HB), C03P(H3AA,
 HC), C03R(H4AA,HD), C03S(H5AA,HE), C03T(H6AA,HF), C03V(H8AA,HG), C03Z(H0BA,HH),
  C040(H04A,H04B), C041(H0CA,HI), C043(H04C,H04D), C044(H04E,H04G), C045(H04H,
 H04I), C048(H04J,H04K), C04A(H04L,H04M), C04C(H04N,H04P), C04D(H04Q,H04S),
 C04K(H04W,H04X), C04M(H04Z,HJ), C04N(H04,HK), C04Q(H1BA,HL), C04S(H2BA,HM),
 C04W(H4BA,HN), C04Y(H6BA,HO), C04Z(H7BA,HP), C051(H05A,H05B), C052(H05C,H05D),
 C056(H05E,H05F), C058(H05G,H05H), C05B(H05I,H05J), C30(H30A,H30B), C33(H33A,
 H33B), C1(H1A,H1B), C55(H55A,H55B), C37(H37A,H37B), C92(H92A,H92B), C2(H2A,
 H2B), C0AA(H0AB,H0AC), C8(H8A,H8B), C3AA(H3AB,H3AC), C11(H11A,H11B), C2AA(H2AB,
 H2AC), C84(H84A,H84B), C4AA(H4AB,H4AC), C5AA(H5AB,H5AC), C6AA(H6AB,H6AC),
 C17(H17A,H17B), C36(H36A,H36B), C8AA(H8AB,H8AC), C19(H19A,H19B), C9AA(H9AB,
 H9AC), C1BA(H1BB,H1BC), C100(H10A,H10B), C122(H12A,H12B), C160(H16A,H16B),
 C161(H16C,H16D), C3BA(H3BB,H3BC), C4BA(H4BB,H4BC), C132(H13A,H13B), C162(H16E,
 H16F), C153(H15A,H15B), C181(H18A,H18B)
4.c Aromatic/amide H refined with riding coordinates:
 C01V(H01V), C021(H021), C024(H024), C025(H025), C02A(H02E), C15(H15),
 C104(H104), C98(H98), C93(H93), C03K(H03K), C02M(H02N), C02V(H02Z), C02Y(H1AA),
  C04F(H04F), C04O(H04O), C4(H4), C04R(H04R), C89(H89), C75(H75), C71(H71),
 C46(H46), C03X(H03X), C03E(H03Q), C03G(H03T), C03Y(H9AA), C047(H047),
 C04T(H04T), C64(H64), C26(H26), C103(H103), C057(H057), C03W(H8BA), C042(H042),
  C035(H035), C03A(H9BA), C059(H059), C9(H9), C23(H23), C6(H6), C28(H28)
4.d Fitted hexagon refined as free rotating group:
 C02K(C15,C104,C98,C93,C03K), C02Y(C04F,C04O,C4,C04B,C04R), C038(C89,C75,C71,
 C46,C03X), C047(C43,C04T,C64,C26,C103), C057(C03W,C042,C035,C02D,C03A),
 C059(C76,C9,C23,C6,C28)
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag01 Ag 0.79253(4) 0.47488(15) 0.26776(4) 0.0393(2) Uani 1 1 d . . . . .
Ag02 Ag 0.71074(4) 0.53344(15) 0.33662(4) 0.0393(2) Uani 1 1 d . . . . .
Ag03 Ag 0.61531(5) 0.60675(15) 0.27730(4) 0.0419(2) Uani 1 1 d . . . . .
Ag04 Ag 0.70346(5) 0.39223(15) 0.30814(4) 0.0409(2) Uani 1 1 d . . . . .
Ag05 Ag 0.74731(5) 0.61074(15) 0.24795(4) 0.0417(2) Uani 1 1 d . . . . .
Ag06 Ag 0.73100(5) 0.38149(15) 0.19755(4) 0.0420(2) Uani 1 1 d . . . . .
Ag07 Ag 0.66512(4) 0.49198(15) 0.23359(4) 0.0385(2) Uani 1 1 d . . . . .
Ag08 Ag 0.58529(5) 0.47646(15) 0.31977(4) 0.0450(2) Uani 1 1 d . . . . .
Ag09 Ag 0.75811(5) 0.51685(15) 0.16282(4) 0.0436(2) Uani 1 1 d . . . . .
Ag0A Ag 0.81875(5) 0.33765(15) 0.28334(4) 0.0437(2) Uani 1 1 d . . . . .
Ag0B Ag 0.86369(5) 0.42589(15) 0.18290(4) 0.0492(2) Uani 1 1 d . . . . .
Ag0C Ag 0.80515(5) 0.43015(15) 0.37605(4) 0.0478(2) Uani 1 1 d . . . . .
Ag0D Ag 0.86963(5) 0.56348(15) 0.21893(4) 0.0484(2) Uani 1 1 d . . . . .
Ag0E Ag 0.60801(5) 0.36093(15) 0.22488(5) 0.0498(3) Uani 1 1 d . . . . .
Ag0F Ag 0.64294(5) 0.44236(16) 0.12689(4) 0.0497(3) Uani 1 1 d . . . . .
Ag0G Ag 0.67692(6) 0.42473(16) 0.41750(5) 0.0545(3) Uani 1 1 d . . . . .
Ag0H Ag 0.63307(6) 0.60344(16) 0.16120(5) 0.0585(3) Uani 1 1 d . . . . .
Ag0I Ag 0.84972(6) 0.57402(16) 0.33603(5) 0.0566(3) Uani 1 1 d . . . . .
Ag0J Ag 0.76223(7) 0.39814(17) 0.08873(6) 0.0761(4) Uani 1 1 d . . . . .
Ag0K Ag 0.70240(8) 0.25945(16) 0.25722(8) 0.0837(5) Uani 1 1 d . . . . .
Cu0L Cu 0.64444(10) 0.60762(18) 0.43918(8) 0.0471(5) Uani 1 1 d . . . . .
Cu0M Cu 0.74675(11) 0.69304(19) 0.39571(10) 0.0529(5) Uani 1 1 d . . . . .
Cu0N Cu 0.51478(11) 0.5370(2) 0.22701(10) 0.0584(6) Uani 1 1 d . . . . .
Cu0O Cu 0.83851(12) 0.55490(19) 0.05525(10) 0.0584(6) Uani 1 1 d . . . . .
Cu0P Cu 0.82812(13) 0.29157(19) 0.38963(10) 0.0573(6) Uani 1 1 d . U . . .
Cu0Q Cu 0.76696(12) 0.67215(19) 0.09846(10) 0.0556(6) Uani 1 1 d . . . . .
Cu0R Cu 0.92732(12) 0.3784(2) 0.34998(10) 0.0596(6) Uani 1 1 d . U . . .
Cu0S Cu 0.59344(14) 0.3101(2) 0.11993(11) 0.0699(8) Uani 1 1 d . . . . .
Cu0T Cu 0.51842(12) 0.4294(2) 0.15798(11) 0.0683(7) Uani 1 1 d . . . . .
Cl0U Cl 0.63508(16) 0.6799(2) 0.36042(13) 0.0457(7) Uani 1 1 d . . . . .
S0V S 0.7128(2) 0.6867(3) 0.17013(15) 0.0538(9) Uani 1 1 d . . . . .
Cu0W Cu 0.94695(19) 0.4821(2) 0.2851(2) 0.1134(15) Uani 1 1 d . U . . .
Cl0X Cl 0.75394(16) 0.5767(2) 0.42854(14) 0.0494(8) Uani 1 1 d . . . . .
S0Y S 0.59817(18) 0.5092(2) 0.41508(14) 0.0482(8) Uani 1 1 d . . . . .
Cl0Z Cl 0.87312(18) 0.6264(2) 0.13095(16) 0.0548(9) Uani 1 1 d . . . . .
S10 S 0.50740(17) 0.4318(3) 0.24638(17) 0.0558(9) Uani 1 1 d . . . . .
Cl11 Cl 0.72574(17) 0.5636(3) 0.07000(14) 0.0519(8) Uani 1 1 d . . . . .
S12 S 0.51425(17) 0.6440(3) 0.22542(15) 0.0510(8) Uani 1 1 d . . . . .
Cl13 Cl 0.80563(18) 0.2938(2) 0.17030(15) 0.0530(8) Uani 1 1 d . . . . .
P14 P 0.73283(19) 0.7729(3) 0.45249(17) 0.0515(9) Uani 1 1 d . . . . .
Cl15 Cl 0.6118(2) 0.3299(3) 0.33826(16) 0.0616(10) Uani 1 1 d . . . . .
S16 S 0.91196(18) 0.4871(3) 0.37843(15) 0.0525(9) Uani 1 1 d . . . . .
P17 P 0.6409(2) 0.6788(2) 0.50574(16) 0.0495(8) Uani 1 1 d . . . . .
S18 S 0.7576(2) 0.3445(3) 0.43766(16) 0.0576(9) Uani 1 1 d . . . . .
S19 S 0.66879(19) 0.3447(3) 0.06693(16) 0.0590(10) Uani 1 1 d . . . . .
S1A S 0.80222(18) 0.6808(3) 0.32455(17) 0.0565(10) Uani 1 1 d . . . . .
S1B S 0.7787(2) 0.2301(2) 0.32375(18) 0.0569(9) Uani 1 1 d . . . . .
S1C S 0.6264(3) 0.2427(3) 0.1881(2) 0.0744(13) Uani 1 1 d . U . . .
S1D S 0.55595(19) 0.5262(3) 0.12716(15) 0.0614(11) Uani 1 1 d . . . . .
S1E S 0.8571(2) 0.4502(3) 0.08536(16) 0.0589(10) Uani 1 1 d . . . . .
P1F P 0.8582(2) 0.6163(3) -0.01334(18) 0.0604(10) Uani 1 1 d . U . . .
S1G S 0.9815(2) 0.5766(3) 0.2636(2) 0.0699(11) Uani 1 1 d D U . . .
Cl1H Cl 0.9347(2) 0.2917(3) 0.4058(2) 0.0748(12) Uani 1 1 d . . . . .
S1I S 0.9331(2) 0.3772(3) 0.25954(18) 0.0645(10) Uani 1 1 d . U . . .
P1J P 0.8024(3) 0.7374(3) 0.0385(2) 0.0708(12) Uani 1 1 d . U . . .
Cl01 Cl 0.4917(3) 0.3431(5) 0.1042(3) 0.113(3) Uani 1 1 d . . . . .
Cl1L Cl 0.7209(5) 0.0853(4) 0.1087(3) 0.119(2) Uani 1 1 d . . . . .
Cl1M Cl 0.7927(5) 0.1674(5) 0.0456(6) 0.176(5) Uani 1 1 d . . . . .
C01N C 0.5191(8) 0.4134(9) 0.4503(7) 0.057(4) Uani 1 1 d . U . . .
H01A H 0.555950 0.383706 0.453745 0.069 Uiso 1 1 calc R . . . .
H01B H 0.499962 0.410241 0.413607 0.069 Uiso 1 1 calc R . . . .
C01O C 0.8918(9) 0.7403(10) 0.2666(6) 0.070(5) Uani 1 1 d D U . . .
H01C H 0.904937 0.695426 0.256375 0.084 Uiso 1 1 calc R . . . .
H01D H 0.858494 0.755934 0.240177 0.084 Uiso 1 1 calc R . . . .
C01P C 0.5772(9) 0.8628(10) 0.1874(7) 0.060(4) Uani 1 1 d . U . . .
H01E H 0.560465 0.908136 0.190899 0.072 Uiso 1 1 calc R . . . .
H01F H 0.541763 0.831236 0.186124 0.072 Uiso 1 1 calc R . . . .
C01Q C 0.6578(8) 0.7641(10) 0.4852(7) 0.058(4) Uani 1 1 d . U . . .
H01G H 0.659783 0.793128 0.516731 0.070 Uiso 1 1 calc R . . . .
H01H H 0.622764 0.779764 0.460592 0.070 Uiso 1 1 calc R . . . .
C01S C 0.5627(7) 0.6969(8) 0.5290(6) 0.049(3) Uani 1 1 d . U . . .
C01T C 0.4277(11) 0.7515(11) 0.3627(8) 0.073(5) Uani 1 1 d . U . . .
H01I H 0.471110 0.759272 0.377927 0.088 Uiso 1 1 calc R . . . .
H01J H 0.398667 0.771865 0.386507 0.088 Uiso 1 1 calc R . . . .
C01U C 0.8676(7) 0.7391(8) 0.3219(5) 0.055(4) Uani 1 1 d D U . . .
C01V C 0.4931(10) 0.7276(11) 0.5937(8) 0.072(5) Uani 1 1 d . U . . .
H01V H 0.484920 0.735635 0.629343 0.087 Uiso 1 1 calc R . . . .
C01W C 0.4344(10) 0.5114(11) 0.4922(8) 0.071(5) Uani 1 1 d . U . . .
H01W H 0.397662 0.541779 0.486239 0.085 Uiso 1 1 calc R . . . .
C01X C 0.7179(8) 0.8546(9) 0.4223(6) 0.054(4) Uani 1 1 d . U . . .
C01Y C 0.9631(5) 0.5170(6) 0.4349(4) 0.051(3) Uani 1 1 d D U . . .
C020 C 0.4283(7) 0.4108(7) 0.2644(5) 0.052(3) Uani 1 1 d D U . . .
C021 C 0.6497(10) 0.9229(11) 0.3647(8) 0.071(5) Uani 1 1 d . U . . .
H021 H 0.613439 0.927205 0.340817 0.085 Uiso 1 1 calc R . . . .
C022 C 0.4570(8) 0.6768(9) 0.2708(6) 0.051(3) Uani 1 1 d . U . . .
C023 C 0.3435(7) 0.4376(9) 0.3259(7) 0.069(5) Uani 1 1 d D U . . .
H023 H 0.332665 0.466252 0.355932 0.083 Uiso 1 1 calc R . . . .
C024 C 0.5148(8) 0.7059(9) 0.4903(7) 0.058(4) Uani 1 1 d . U . . .
H024 H 0.521739 0.699966 0.454191 0.069 Uiso 1 1 calc R . . . .
C025 C 0.7587(11) 0.9084(12) 0.4316(9) 0.080(6) Uani 1 1 d . U . . .
H025 H 0.796749 0.904677 0.453431 0.096 Uiso 1 1 calc R . . . .
C026 C 0.4093(7) 0.4550(9) 0.3098(7) 0.068(5) Uani 1 1 d D U . . .
H02A H 0.410052 0.501980 0.298605 0.082 Uiso 1 1 calc R . . . .
H02B H 0.440197 0.449610 0.340626 0.082 Uiso 1 1 calc R . . . .
C027 C 0.4709(10) 0.3908(11) 0.4889(8) 0.070(5) Uani 1 1 d . U . . .
H027 H 0.458101 0.343680 0.482527 0.084 Uiso 1 1 calc R . . . .
C028 C 0.4650(8) 0.6478(9) 0.3248(6) 0.053(4) Uani 1 1 d . U . . .
H02C H 0.507577 0.657596 0.341133 0.064 Uiso 1 1 calc R . . . .
H02D H 0.459806 0.599155 0.322917 0.064 Uiso 1 1 calc R . . . .
C029 C 0.6236(8) 0.8471(9) 0.2340(6) 0.054(4) Uani 1 1 d . U . . .
H029 H 0.602086 0.850664 0.267329 0.064 Uiso 1 1 calc R . . . .
C02A C 0.5530(10) 0.7080(11) 0.5812(8) 0.067(5) Uani 1 1 d . U . . .
H02E H 0.586113 0.702531 0.608089 0.081 Uiso 1 1 calc R . . . .
C02C C 0.7807(9) 0.3537(10) 0.5090(7) 0.062(4) Uani 1 1 d . U . . .
C02E C 0.5010(11) 0.4016(12) 0.5481(8) 0.075(5) Uani 1 1 d . U . . .
H02F H 0.470506 0.387886 0.573348 0.090 Uiso 1 1 calc R . . . .
H02G H 0.538824 0.373575 0.554360 0.090 Uiso 1 1 calc R . . . .
C02F C 0.9895(9) 0.4588(7) 0.4691(6) 0.076(5) Uani 1 1 d D U . . .
H02H H 0.954404 0.432241 0.480945 0.091 Uiso 1 1 calc R . . . .
H02I H 1.014717 0.429763 0.447573 0.091 Uiso 1 1 calc R . . . .
C02G C 0.7115(9) 0.8910(10) 0.1842(8) 0.066(4) Uani 1 1 d . U . . .
H02J H 0.747368 0.922774 0.185552 0.079 Uiso 1 1 calc R . . . .
C02H C 0.6482(8) 0.7753(9) 0.2282(6) 0.055(4) Uani 1 1 d . U . . .
H02K H 0.677565 0.764187 0.259086 0.066 Uiso 1 1 calc R . . . .
H02L H 0.612707 0.743838 0.227178 0.066 Uiso 1 1 calc R . . . .
C02I C 0.5682(6) 0.1829(8) 0.2067(6) 0.103(3) Uani 1 1 d D U . . .
C02J C 0.8216(7) 0.1588(8) 0.3012(5) 0.055(4) Uani 1 1 d D U . . .
C02K C 0.7996(6) 0.6225(6) -0.0678(5) 0.089(2) Uani 1 1 d . U . . .
C15 C 0.8070(6) 0.6642(5) -0.1103(6) 0.093(2) Uani 1 1 d G U . . .
H15 H 0.843574 0.690765 -0.110924 0.111 Uiso 1 1 calc DR . . . .
C104 C 0.7608(7) 0.6672(7) -0.1520(5) 0.103(3) Uani 1 1 d G U . . .
H104 H 0.765912 0.695712 -0.181101 0.123 Uiso 1 1 calc R . . . .
C98 C 0.7073(5) 0.6284(9) -0.1512(5) 0.105(3) Uani 1 1 d G U . . .
H98 H 0.675765 0.630385 -0.179683 0.126 Uiso 1 1 calc DR . . . .
C93 C 0.6999(5) 0.5866(9) -0.1087(7) 0.101(3) Uani 1 1 d G U . . .
H93 H 0.663280 0.560110 -0.108087 0.121 Uiso 1 1 calc R . . . .
C03K C 0.7460(6) 0.5837(7) -0.0670(5) 0.094(3) Uani 1 1 d G U . . .
H03K H 0.740942 0.555162 -0.037909 0.113 Uiso 1 1 calc R . . . .
C02L C 0.4154(8) 0.6780(9) 0.3586(6) 0.053(4) Uani 1 1 d . U . . .
H02M H 0.420012 0.658080 0.394709 0.064 Uiso 1 1 calc R . . . .
C02M C 0.6657(8) 0.8627(9) 0.3885(6) 0.056(4) Uani 1 1 d . U . . .
H02N H 0.639156 0.825671 0.381002 0.067 Uiso 1 1 calc R . . . .
C02N C 0.7358(8) 0.8186(9) 0.1805(7) 0.055(4) Uani 1 1 d . U . . .
H02O H 0.759410 0.814002 0.148799 0.066 Uiso 1 1 calc R . . . .
H02P H 0.764773 0.808726 0.211885 0.066 Uiso 1 1 calc R . . . .
C02O C 0.9237(6) 0.5608(9) 0.4692(5) 0.065(4) Uani 1 1 d D U . . .
H02Q H 0.889064 0.534525 0.482159 0.079 Uiso 1 1 calc R . . . .
H02R H 0.905284 0.598053 0.447896 0.079 Uiso 1 1 calc R . . . .
C02P C 0.5398(8) 0.4831(9) 0.4613(6) 0.053(3) Uani 1 1 d . U . . .
C02Q C 0.9995(9) 0.7711(14) 0.3128(7) 0.087(6) Uani 1 1 d D U . . .
H02S H 1.016010 0.726092 0.306949 0.104 Uiso 1 1 calc R . . . .
H02T H 1.034518 0.802974 0.311843 0.104 Uiso 1 1 calc R . . . .
C02R C 0.6118(9) 0.8573(11) 0.1361(8) 0.067(4) Uani 1 1 d . U . . .
H02U H 0.582057 0.868239 0.104932 0.080 Uiso 1 1 calc R . . . .
C02S C 0.9194(8) 0.7217(10) 0.3657(7) 0.072(5) Uani 1 1 d D U . . .
H02V H 0.936844 0.677407 0.358903 0.087 Uiso 1 1 calc R . . . .
H02W H 0.901456 0.720621 0.400343 0.087 Uiso 1 1 calc R . . . .
C02T C 0.6661(10) 0.9068(11) 0.1395(8) 0.072(5) Uani 1 1 d . U . . .
H02X H 0.687338 0.905662 0.106335 0.086 Uiso 1 1 calc R . . . .
H02Y H 0.649646 0.952132 0.143917 0.086 Uiso 1 1 calc R . . . .
C02U C 0.6819(7) 0.7692(8) 0.1775(6) 0.049(3) Uani 1 1 d . U . . .
C02V C 0.6891(11) 0.9768(13) 0.3770(9) 0.083(6) Uani 1 1 d . U . . .
H02Z H 0.677731 1.019338 0.363467 0.100 Uiso 1 1 calc R . . . .
C02W C 0.4837(8) 0.5288(9) 0.4519(6) 0.056(4) Uani 1 1 d . U . . .
H02 H 0.464668 0.523383 0.415368 0.067 Uiso 1 1 calc R . . . .
H H 0.497243 0.575487 0.456649 0.067 Uiso 1 1 calc R . . . .
C02X C 0.3904(9) 0.6651(12) 0.2433(8) 0.072(5) Uani 1 1 d . U . . .
H0AA H 0.386724 0.686321 0.208032 0.087 Uiso 1 1 calc R . . . .
HA H 0.382458 0.617099 0.238690 0.087 Uiso 1 1 calc R . . . .
C02Y C 1.0457(5) 0.5983(9) -0.0274(5) 0.083(3) Uani 1 1 d . U . . .
H1AA H 1.082744 0.601868 -0.004297 0.099 Uiso 1 1 calc R . . . .
C04F C 1.0497(5) 0.5830(9) -0.0803(5) 0.084(3) Uani 1 1 d G U . . .
H04F H 1.089536 0.576087 -0.093408 0.100 Uiso 1 1 calc R . . . .
C04O C 0.9955(7) 0.5778(9) -0.1140(4) 0.088(3) Uani 1 1 d G U . . .
H04O H 0.998275 0.567366 -0.150218 0.105 Uiso 1 1 calc R . . . .
C4 C 0.9373(5) 0.5880(9) -0.0949(5) 0.083(3) Uani 1 1 d G U . . .
H4 H 0.900222 0.584427 -0.117919 0.099 Uiso 1 1 calc R . . . .
C04B C 0.9332(5) 0.6033(9) -0.0419(5) 0.078(3) Uani 1 1 d G U . . .
C04R C 0.9874(6) 0.6085(9) -0.0082(4) 0.077(3) Uani 1 1 d G U . . .
H04R H 0.984689 0.618930 0.028003 0.092 Uiso 1 1 calc R . . . .
C02Z C 0.5188(10) 0.4748(12) 0.5576(8) 0.072(5) Uani 1 1 d . U . . .
H2AA H 0.537296 0.481253 0.594679 0.087 Uiso 1 1 calc R . . . .
C031 C 0.8632(12) 0.4098(14) -0.0166(9) 0.084(6) Uani 1 1 d . U . . .
H03A H 0.864860 0.457181 -0.026511 0.101 Uiso 1 1 calc R . . . .
H03B H 0.818623 0.396960 -0.015800 0.101 Uiso 1 1 calc R . . . .
C032 C 0.8853(9) 0.1792(11) 0.2820(10) 0.089(6) Uani 1 1 d D U . . .
H03C H 0.912207 0.198071 0.311861 0.107 Uiso 1 1 calc R . . . .
H03D H 0.878893 0.213704 0.254441 0.107 Uiso 1 1 calc R . . . .
C033 C 0.3428(11) 0.6956(12) 0.2784(8) 0.077(5) Uani 1 1 d . U . . .
H033 H 0.299478 0.687319 0.261968 0.093 Uiso 1 1 calc R . . . .
C034 C 0.8684(9) 0.0490(10) 0.3280(8) 0.089(6) Uani 1 1 d D U . . .
H034 H 0.876982 0.016506 0.357412 0.106 Uiso 1 1 calc R . . . .
C036 C 0.3545(12) 0.7672(14) 0.2804(10) 0.090(6) Uani 1 1 d . U . . .
H03E H 0.321448 0.789060 0.299235 0.108 Uiso 1 1 calc R . . . .
H03F H 0.352280 0.785014 0.243995 0.108 Uiso 1 1 calc R . . . .
C037 C 0.7816(9) 0.1276(10) 0.2544(7) 0.075(5) Uani 1 1 d D U . . .
H03G H 0.776786 0.159702 0.224930 0.090 Uiso 1 1 calc R . . . .
H03H H 0.739380 0.117191 0.265351 0.090 Uiso 1 1 calc R . . . .
C038 C 0.6967(7) 0.6650(9) 0.5619(6) 0.080(6) Uani 1 1 d . U . . .
C89 C 0.7345(9) 0.6089(8) 0.5630(7) 0.106(8) Uani 1 1 d G U . . .
H89 H 0.727950 0.576250 0.536200 0.127 Uiso 1 1 calc R . . . .
C75 C 0.7818(9) 0.6007(10) 0.6032(9) 0.143(13) Uani 1 1 d G U . . .
H75 H 0.807649 0.562345 0.603902 0.172 Uiso 1 1 calc R . . . .
C71 C 0.7914(9) 0.6484(12) 0.6424(8) 0.143(13) Uani 1 1 d G U . . .
H71 H 0.823749 0.642794 0.669864 0.171 Uiso 1 1 calc R . . . .
C46 C 0.7536(9) 0.7045(10) 0.6413(6) 0.111(9) Uani 1 1 d G U . . .
H46 H 0.760149 0.737148 0.668125 0.133 Uiso 1 1 calc R . . . .
C03X C 0.7063(8) 0.7127(8) 0.6011(6) 0.084(6) Uani 1 1 d G U . . .
H03X H 0.680450 0.751054 0.600422 0.101 Uiso 1 1 calc R . . . .
C039 C 0.7707(13) 0.4184(14) 0.6104(10) 0.091(7) Uani 1 1 d . U . . .
H03I H 0.783167 0.422645 0.648647 0.110 Uiso 1 1 calc R . . . .
H03J H 0.739890 0.453714 0.600609 0.110 Uiso 1 1 calc R . . . .
C03B C 0.9479(8) 0.7879(9) 0.2691(9) 0.085(6) Uani 1 1 d D U . . .
H03L H 0.966707 0.786451 0.234374 0.102 Uiso 1 1 calc R . . . .
C03C C 0.9195(13) 0.8573(11) 0.2756(8) 0.099(8) Uani 1 1 d D U . . .
H03M H 0.884548 0.864903 0.248348 0.119 Uiso 1 1 calc R . . . .
H03N H 0.951664 0.891874 0.272121 0.119 Uiso 1 1 calc R . . . .
C03D C 0.3507(10) 0.6611(13) 0.3325(8) 0.076(5) Uani 1 1 d . U . . .
H03O H 0.317829 0.676403 0.354906 0.091 Uiso 1 1 calc R . . . .
H03P H 0.346594 0.612558 0.327983 0.091 Uiso 1 1 calc R . . . .
C03E C 0.4559(9) 0.7238(10) 0.5051(7) 0.060(4) Uani 1 1 d . U . . .
H03Q H 0.422097 0.727788 0.478631 0.072 Uiso 1 1 calc R . . . .
C03F C 0.4622(10) 0.5198(11) 0.5465(7) 0.069(5) Uani 1 1 d . U . . .
H03R H 0.430370 0.509353 0.571493 0.083 Uiso 1 1 calc R . . . .
H03S H 0.475084 0.566487 0.552094 0.083 Uiso 1 1 calc R . . . .
C03G C 0.7397(11) 0.9699(13) 0.4060(9) 0.080(6) Uani 1 1 d . U . . .
H03T H 0.766596 1.007220 0.411131 0.095 Uiso 1 1 calc R . . . .
C03H C 0.9633(13) 0.4189(16) 0.0359(11) 0.101(8) Uani 1 1 d . U . . .
H03U H 0.986303 0.408888 0.070345 0.121 Uiso 1 1 calc R . . . .
H03V H 0.965388 0.467328 0.030166 0.121 Uiso 1 1 calc R . . . .
C03I C 0.4184(11) 0.7835(12) 0.3082(8) 0.076(5) Uani 1 1 d . U . . .
H03W H 0.424910 0.832472 0.310542 0.091 Uiso 1 1 calc R . . . .
C03J C 1.0621(7) 0.5812(8) 0.4624(6) 0.088(6) Uani 1 1 d D U . . .
H03Y H 1.098220 0.606498 0.449734 0.106 Uiso 1 1 calc R . . . .
C03L C 0.6367(10) 0.7865(11) 0.1303(8) 0.072(5) Uani 1 1 d . U . . .
H03Z H 0.601226 0.754884 0.127840 0.086 Uiso 1 1 calc R . . . .
HB H 0.658407 0.783073 0.097449 0.086 Uiso 1 1 calc R . . . .
C03M C 0.6500(7) 0.3505(8) -0.0050(7) 0.063(4) Uani 1 1 d D U . . .
C03O C 1.0306(7) 0.4833(7) 0.5174(5) 0.084(6) Uani 1 1 d D U . . .
H03 H 1.046987 0.444677 0.538863 0.100 Uiso 1 1 calc R . . . .
C03P C 0.4125(11) 0.4394(13) 0.4808(10) 0.083(6) Uani 1 1 d . U . . .
H3AA H 0.393467 0.435993 0.444099 0.100 Uiso 1 1 calc R . . . .
HC H 0.380467 0.426919 0.504961 0.100 Uiso 1 1 calc R . . . .
C03Q C 1.0004(4) 0.3343(5) 0.2292(4) 0.118(3) Uani 1 1 d D U . . .
C03R C 0.2974(10) 0.4502(13) 0.2774(7) 0.092(7) Uani 1 1 d D U . . .
H4AA H 0.299975 0.497056 0.266342 0.110 Uiso 1 1 calc R . . . .
HD H 0.254028 0.441247 0.286317 0.110 Uiso 1 1 calc R . . . .
C03S C 0.5685(9) 0.4914(11) 0.5176(6) 0.062(4) Uani 1 1 d . U . . .
H5AA H 0.583282 0.537555 0.522993 0.075 Uiso 1 1 calc R . . . .
HE H 0.605072 0.461565 0.523728 0.075 Uiso 1 1 calc R . . . .
C03T C 0.8799(14) 0.3712(15) 0.5966(11) 0.100(8) Uani 1 1 d . U . . .
H6AA H 0.917220 0.375321 0.576164 0.120 Uiso 1 1 calc R . . . .
HF H 0.893561 0.375080 0.634591 0.120 Uiso 1 1 calc R . . . .
C03U C 0.7410(12) 0.3537(13) 0.6004(9) 0.085(6) Uani 1 1 d . U . . .
H7AA H 0.703058 0.348690 0.620584 0.102 Uiso 1 1 calc R . . . .
C03V C 0.6841(12) 0.2926(11) -0.0297(8) 0.088(6) Uani 1 1 d D U . . .
H8AA H 0.668759 0.249791 -0.016771 0.106 Uiso 1 1 calc R . . . .
HG H 0.729791 0.295493 -0.020157 0.106 Uiso 1 1 calc R . . . .
C03Y C 0.4458(11) 0.7352(12) 0.5535(9) 0.080(6) Uani 1 1 d . U . . .
H9AA H 0.405367 0.749095 0.561825 0.096 Uiso 1 1 calc R . . . .
C03Z C 0.9303(9) 0.0730(12) 0.3076(8) 0.080(5) Uani 1 1 d D U . . .
H0BA H 0.954945 0.097232 0.336020 0.096 Uiso 1 1 calc R . . . .
HH H 0.955177 0.034223 0.297761 0.096 Uiso 1 1 calc R . . . .
C040 C 0.5804(7) 0.1173(9) 0.1790(7) 0.105(3) Uani 1 1 d D U . . .
H04A H 0.623882 0.102469 0.188888 0.127 Uiso 1 1 calc R . . . .
H04B H 0.575661 0.123712 0.140244 0.127 Uiso 1 1 calc R . . . .
C041 C 0.7329(14) 0.1608(15) 0.0958(11) 0.099(7) Uani 1 1 d . U . . .
H0CA H 0.748254 0.184414 0.128487 0.119 Uiso 1 1 calc R . . . .
HI H 0.693204 0.181843 0.081816 0.119 Uiso 1 1 calc R . . . .
C043 C 0.8316(11) 0.1090(10) 0.3471(7) 0.084(6) Uani 1 1 d D U . . .
H04C H 0.790631 0.094293 0.358316 0.100 Uiso 1 1 calc R . . . .
H04D H 0.855417 0.130164 0.377585 0.100 Uiso 1 1 calc R . . . .
C044 C 1.0230(8) 0.6252(9) 0.4962(8) 0.087(6) Uani 1 1 d D U . . .
H04E H 1.007411 0.663723 0.474897 0.104 Uiso 1 1 calc R . . . .
H04G H 1.050124 0.642100 0.526586 0.104 Uiso 1 1 calc R . . . .
C045 C 0.4284(8) 0.3382(8) 0.2826(9) 0.082(6) Uani 1 1 d D U . . .
H04H H 0.440934 0.308806 0.254110 0.099 Uiso 1 1 calc R . . . .
H04I H 0.458516 0.332108 0.313905 0.099 Uiso 1 1 calc R . . . .
C046 C 0.9662(7) 0.5883(7) 0.5170(5) 0.094(7) Uani 1 1 d D U . . .
H046 H 0.941836 0.618832 0.538523 0.113 Uiso 1 1 calc R . . . .
C047 C 0.6867(8) 0.7378(9) -0.0185(6) 0.097(3) Uani 1 1 d . U . . .
H047 H 0.675725 0.709830 0.009340 0.116 Uiso 1 1 calc R . . . .
C43 C 0.7466(8) 0.7647(10) -0.0174(6) 0.097(2) Uani 1 1 d G U . . .
C04T C 0.7627(7) 0.8056(10) -0.0582(7) 0.099(2) Uani 1 1 d G U . . .
H04T H 0.803589 0.823952 -0.057379 0.119 Uiso 1 1 calc R . . . .
C64 C 0.7189(9) 0.8196(9) -0.1001(6) 0.106(3) Uani 1 1 d G U . . .
H64 H 0.729860 0.847528 -0.127934 0.127 Uiso 1 1 calc R . . . .
C26 C 0.6590(8) 0.7927(11) -0.1012(6) 0.108(3) Uani 1 1 d G U . . .
H26 H 0.629062 0.802256 -0.129851 0.129 Uiso 1 1 calc R . . . .
C103 C 0.6429(7) 0.7518(10) -0.0604(7) 0.105(3) Uani 1 1 d G U . . .
H103 H 0.601994 0.733406 -0.061215 0.126 Uiso 1 1 calc R . . . .
C048 C 0.8300(10) 0.2986(12) 0.5244(8) 0.073(5) Uani 1 1 d . U . . .
H04J H 0.866932 0.303201 0.503610 0.087 Uiso 1 1 calc R . . . .
H04K H 0.811520 0.254138 0.517887 0.087 Uiso 1 1 calc R . . . .
C04A C 0.4685(11) 0.7497(11) 0.2727(8) 0.074(5) Uani 1 1 d . U . . .
H04L H 0.464006 0.768293 0.236529 0.089 Uiso 1 1 calc R . . . .
H04M H 0.511581 0.758765 0.288108 0.089 Uiso 1 1 calc R . . . .
C04C C 0.8753(10) 0.0852(14) 0.2160(9) 0.095(7) Uani 1 1 d D U . . .
H04N H 0.896821 0.045982 0.202743 0.114 Uiso 1 1 calc R . . . .
H04P H 0.867363 0.116512 0.186205 0.114 Uiso 1 1 calc R . . . .
C04D C 0.6780(9) 0.8947(10) 0.2361(7) 0.064(4) Uani 1 1 d . U . . .
H04Q H 0.708049 0.883567 0.266500 0.077 Uiso 1 1 calc R . . . .
H04S H 0.662637 0.940319 0.241207 0.077 Uiso 1 1 calc R . . . .
C04E C 0.5226(8) 0.5605(10) 0.0617(5) 0.098(7) Uani 1 1 d D U . . .
C04I C 0.9183(11) 0.1185(10) 0.2594(7) 0.100(7) Uani 1 1 d D U . . .
H04U H 0.958768 0.131923 0.245446 0.120 Uiso 1 1 calc R . . . .
C04J C 0.9721(10) 0.7743(10) 0.3665(8) 0.090(6) Uani 1 1 d D U . . .
H04V H 1.005389 0.763378 0.395016 0.108 Uiso 1 1 calc R . . . .
C04K C 0.3134(12) 0.3312(11) 0.2491(9) 0.103(8) Uani 1 1 d D U . . .
H04W H 0.271130 0.318994 0.258928 0.124 Uiso 1 1 calc R . . . .
H04X H 0.323881 0.302672 0.219411 0.124 Uiso 1 1 calc R . . . .
C04L C 0.3617(7) 0.3210(9) 0.2965(6) 0.066(4) Uani 1 1 d D U . . .
H04Y H 0.360755 0.273480 0.307599 0.079 Uiso 1 1 calc R . . . .
C04M C 0.9912(8) 0.5281(10) 0.5510(6) 0.100(7) Uani 1 1 d D U . . .
H04Z H 1.017315 0.544007 0.582362 0.120 Uiso 1 1 calc R . . . .
HJ H 0.955586 0.502691 0.563202 0.120 Uiso 1 1 calc R . . . .
C04N C 0.6699(13) 0.4173(11) -0.0279(9) 0.097(7) Uani 1 1 d D U . . .
H04 H 0.645495 0.453609 -0.013307 0.116 Uiso 1 1 calc R . . . .
HK H 0.714892 0.425280 -0.017715 0.116 Uiso 1 1 calc R . . . .
C04Q C 0.7904(14) 0.2978(16) 0.6154(11) 0.100(8) Uani 1 1 d . U . . .
H1BA H 0.801567 0.298419 0.653992 0.120 Uiso 1 1 calc R . . . .
HL H 0.772037 0.254021 0.605922 0.120 Uiso 1 1 calc R . . . .
C04S C 0.9574(17) 0.391(2) -0.0589(15) 0.129(11) Uani 1 1 d . U . . .
H2BA H 0.955716 0.438016 -0.068695 0.155 Uiso 1 1 calc R . . . .
HM H 0.978698 0.366709 -0.086471 0.155 Uiso 1 1 calc R . . . .
C04U C 0.8953(15) 0.3662(16) -0.0585(12) 0.103(8) Uani 1 1 d . U . . .
H3BA H 0.872768 0.372662 -0.094106 0.124 Uiso 1 1 calc R . . . .
C04W C 0.7238(10) 0.3422(13) 0.5379(8) 0.075(5) Uani 1 1 d . U . . .
H4BA H 0.708525 0.296405 0.531627 0.090 Uiso 1 1 calc R . . . .
HN H 0.690142 0.373135 0.524920 0.090 Uiso 1 1 calc R . . . .
C04X C 0.6584(16) 0.4161(19) -0.0882(9) 0.137(12) Uani 1 1 d D U . . .
H5BA H 0.668656 0.460204 -0.103170 0.165 Uiso 1 1 calc R . . . .
C04Y C 0.8268(14) 0.0173(13) 0.2826(9) 0.114(9) Uani 1 1 d D U . . .
H6BA H 0.847994 -0.022814 0.270362 0.137 Uiso 1 1 calc R . . . .
HO H 0.786808 0.003113 0.296107 0.137 Uiso 1 1 calc R . . . .
C04Z C 0.3432(11) 0.3645(8) 0.3422(7) 0.081(6) Uani 1 1 d D U . . .
H7BA H 0.373142 0.357531 0.373470 0.097 Uiso 1 1 calc R . . . .
HP H 0.300877 0.351874 0.351764 0.097 Uiso 1 1 calc R . . . .
C050 C 0.8977(8) 0.3992(10) 0.0376(7) 0.059(4) Uani 1 1 d . U . . .
C051 C 1.1399(4) 0.3272(5) 0.2373(5) 0.127(3) Uani 1 1 d D U . . .
H05A H 1.178571 0.305616 0.226805 0.153 Uiso 1 1 calc R . . . .
H05B H 1.152375 0.363653 0.261987 0.153 Uiso 1 1 calc R . . . .
C052 C 0.4542(11) 0.5387(13) 0.0499(10) 0.129(11) Uani 1 1 d D U . . .
H05C H 0.429297 0.553148 0.079007 0.155 Uiso 1 1 calc R . . . .
H05D H 0.452232 0.489795 0.047841 0.155 Uiso 1 1 calc R . . . .
C053 C 0.8123(10) 0.0636(10) 0.2353(8) 0.090(6) Uani 1 1 d D U . . .
H053 H 0.785189 0.041457 0.206650 0.108 Uiso 1 1 calc R . . . .
C054 C 0.8497(13) 0.3089(15) 0.5860(10) 0.097(7) Uani 1 1 d . U . . .
H054 H 0.880331 0.273262 0.597278 0.117 Uiso 1 1 calc R . . . .
C055 C 1.0483(6) 0.2441(3) 0.1756(4) 0.126(3) Uani 1 1 d D U . . .
H055 H 1.038883 0.206559 0.150528 0.151 Uiso 1 1 calc R . . . .
C056 C 0.9903(18) 0.3117(19) 0.0058(16) 0.129(11) Uani 1 1 d . U . . .
H05E H 1.011930 0.305168 0.041308 0.155 Uiso 1 1 calc R . . . .
H05F H 1.013778 0.286135 -0.019384 0.155 Uiso 1 1 calc R . . . .
C057 C 0.8971(5) 0.7676(8) 0.5430(6) 0.097(7) Uani 1 1 d . U . . .
H057 H 0.935105 0.743210 0.543232 0.116 Uiso 1 1 calc R . . . .
C03W C 0.8912(6) 0.8179(9) 0.5796(6) 0.089(6) Uani 1 1 d G U . . .
H8BA H 0.925055 0.827883 0.604828 0.107 Uiso 1 1 calc R . . . .
C042 C 0.8356(7) 0.8535(7) 0.5794(5) 0.091(7) Uani 1 1 d G U . . .
H042 H 0.831496 0.887909 0.604358 0.109 Uiso 1 1 calc R . . . .
C035 C 0.7860(6) 0.8389(7) 0.5425(5) 0.075(5) Uani 1 1 d G U . . .
H035 H 0.747985 0.863263 0.542292 0.090 Uiso 1 1 calc R . . . .
C02D C 0.7919(5) 0.7886(7) 0.5059(5) 0.061(4) Uani 1 1 d G U . . .
C03A C 0.8475(6) 0.7529(7) 0.5062(5) 0.077(5) Uani 1 1 d G U . . .
H9BA H 0.851593 0.718563 0.481164 0.092 Uiso 1 1 calc R . . . .
C058 C 0.3802(7) 0.4221(12) 0.2167(6) 0.075(5) Uani 1 1 d D U . . .
H05G H 0.381302 0.468978 0.205448 0.091 Uiso 1 1 calc R . . . .
H05H H 0.390889 0.394024 0.186779 0.091 Uiso 1 1 calc R . . . .
C059 C 0.8859(8) 0.8067(7) 0.1052(7) 0.094(3) Uani 1 1 d . U . . .
H059 H 0.903165 0.764077 0.112603 0.113 Uiso 1 1 calc R . . . .
C76 C 0.8367(8) 0.8143(8) 0.0665(6) 0.095(3) Uani 1 1 d G U . . .
C9 C 0.8115(7) 0.8767(9) 0.0557(6) 0.098(3) Uani 1 1 d G U . . .
H9 H 0.777865 0.881939 0.029256 0.117 Uiso 1 1 calc R . . . .
C23 C 0.8354(9) 0.9316(7) 0.0836(7) 0.104(3) Uani 1 1 d G U . . .
H23 H 0.818105 0.974214 0.076269 0.124 Uiso 1 1 calc R . . . .
C6 C 0.8845(9) 0.9240(8) 0.1224(7) 0.100(3) Uani 1 1 d G U . . .
H6 H 0.900875 0.961421 0.141450 0.120 Uiso 1 1 calc R . . . .
C28 C 0.9098(7) 0.8615(10) 0.1332(6) 0.104(4) Uani 1 1 d G U . . .
H28 H 0.943405 0.856353 0.159617 0.124 Uiso 1 1 calc R . . . .
C05B C 0.5802(9) 0.3334(15) -0.0188(8) 0.092(7) Uani 1 1 d D U . . .
H05I H 0.553083 0.366481 -0.003124 0.110 Uiso 1 1 calc R . . . .
H05J H 0.570581 0.289152 -0.004631 0.110 Uiso 1 1 calc R . . . .
C05D C 0.3142(9) 0.4045(10) 0.2323(9) 0.094(7) Uani 1 1 d D U . . .
H05K H 0.283197 0.411173 0.201182 0.113 Uiso 1 1 calc R . . . .
C21 C 0.8954(9) 0.8596(11) 0.3312(7) 0.086(6) Uani 1 1 d D U . . .
H21 H 0.878219 0.904722 0.337265 0.103 Uiso 1 1 calc R . . . .
C30 C 0.8419(8) 0.8090(7) 0.3318(7) 0.064(4) Uani 1 1 d D U . . .
H30A H 0.808416 0.820114 0.304098 0.077 Uiso 1 1 calc R . . . .
H30B H 0.823735 0.810167 0.366434 0.077 Uiso 1 1 calc R . . . .
C33 C 0.9464(13) 0.8441(12) 0.3756(10) 0.109(8) Uani 1 1 d D U . . .
H33A H 0.928607 0.846265 0.410288 0.131 Uiso 1 1 calc R . . . .
H33B H 0.980694 0.877050 0.375350 0.131 Uiso 1 1 calc R . . . .
C1 C 1.0170(7) 0.5589(9) 0.4157(5) 0.069(5) Uani 1 1 d D U . . .
H1A H 1.040226 0.532525 0.390871 0.083 Uiso 1 1 calc R . . . .
H1B H 0.999467 0.598310 0.396600 0.083 Uiso 1 1 calc R . . . .
C34 C 0.5051(11) 0.6621(8) 0.0039(9) 0.139(12) Uani 1 1 d D U . . .
H34 H 0.510382 0.711246 0.002050 0.167 Uiso 1 1 calc R . . . .
C55 C 1.0854(7) 0.5219(11) 0.4965(7) 0.105(8) Uani 1 1 d D U . . .
H55A H 1.109903 0.491833 0.475247 0.126 Uiso 1 1 calc R . . . .
H55B H 1.113479 0.537897 0.526691 0.126 Uiso 1 1 calc R . . . .
C37 C 0.4358(10) 0.6440(11) -0.0043(10) 0.142(13) Uani 1 1 d D U . . .
H37A H 0.418293 0.661230 -0.038918 0.170 Uiso 1 1 calc R . . . .
H37B H 0.412859 0.665195 0.023480 0.170 Uiso 1 1 calc R . . . .
C82 C 0.4261(7) 0.5688(12) -0.0026(8) 0.159(15) Uani 1 1 d D U . . .
H82 H 0.380483 0.557766 -0.008386 0.191 Uiso 1 1 calc R . . . .
C92 C 0.4630(10) 0.5343(11) -0.0442(7) 0.115(9) Uani 1 1 d D U . . .
H92A H 0.446038 0.547970 -0.079918 0.138 Uiso 1 1 calc R . . . .
H92B H 0.458052 0.485715 -0.041300 0.138 Uiso 1 1 calc R . . . .
C2 C 0.8700(8) 0.7027(9) 0.0062(7) 0.055(4) Uani 1 1 d . U . . .
H2A H 0.876868 0.729462 -0.025477 0.066 Uiso 1 1 calc R . . . .
H2B H 0.908136 0.706123 0.030780 0.066 Uiso 1 1 calc R . . . .
C0AA C 0.5288(11) 0.6366(10) 0.0595(8) 0.152(14) Uani 1 1 d D U . . .
H0AB H 0.573249 0.649368 0.067412 0.182 Uiso 1 1 calc R . . . .
H0AC H 0.503956 0.656976 0.086393 0.182 Uiso 1 1 calc R . . . .
C8 C 0.8917(13) 0.3252(14) 0.0509(10) 0.092(7) Uani 1 1 d . U . . .
H8A H 0.846918 0.312709 0.050550 0.110 Uiso 1 1 calc R . . . .
H8B H 0.912137 0.316014 0.086446 0.110 Uiso 1 1 calc R . . . .
C13 C 0.9260(18) 0.282(2) 0.0059(14) 0.130(11) Uani 1 1 d . U . . .
H13 H 0.927525 0.233688 0.014174 0.156 Uiso 1 1 calc R . . . .
C67 C 0.9950(18) 0.3833(19) -0.0079(14) 0.123(10) Uani 1 1 d . U . . .
H67 H 1.039450 0.397786 -0.009945 0.148 Uiso 1 1 calc R . . . .
C3AA C 0.6021(12) 0.2751(14) -0.1033(12) 0.110(8) Uani 1 1 d D U . . .
H3AB H 0.591532 0.271046 -0.141762 0.131 Uiso 1 1 calc R . . . .
H3AC H 0.593159 0.232827 -0.085685 0.131 Uiso 1 1 calc R . . . .
C7 C 0.5686(15) 0.3337(14) -0.0796(8) 0.116(9) Uani 1 1 d D U . . .
H7 H 0.522558 0.328837 -0.088982 0.139 Uiso 1 1 calc R . . . .
C11 C 0.5915(18) 0.3958(19) -0.1077(17) 0.169(17) Uani 1 1 d D U . . .
H11A H 0.589792 0.387127 -0.146105 0.203 Uiso 1 1 calc R . . . .
H11B H 0.562733 0.433051 -0.101977 0.203 Uiso 1 1 calc R . . . .
C1AA C 0.6702(14) 0.2977(17) -0.0903(9) 0.127(11) Uani 1 1 d D U . . .
H1AB H 0.696063 0.261849 -0.104739 0.153 Uiso 1 1 calc R . . . .
C2AA C 0.6934(17) 0.3613(14) -0.1150(14) 0.134(12) Uani 1 1 d D U . . .
H2AB H 0.739321 0.366268 -0.107692 0.160 Uiso 1 1 calc R . . . .
H2AC H 0.683021 0.361610 -0.153662 0.160 Uiso 1 1 calc R . . . .
C84 C 0.8903(16) 0.2957(17) -0.0425(12) 0.112(9) Uani 1 1 d . U . . .
H84A H 0.845737 0.284891 -0.038693 0.135 Uiso 1 1 calc R . . . .
H84B H 0.905038 0.266971 -0.070532 0.135 Uiso 1 1 calc R . . . .
C5 C 0.5335(8) 0.0640(7) 0.1951(6) 0.111(3) Uani 1 1 d D U . . .
H5 H 0.541525 0.021264 0.177011 0.133 Uiso 1 1 calc R . . . .
C4AA C 0.4663(7) 0.0874(8) 0.1797(7) 0.110(3) Uani 1 1 d D U . . .
H4AB H 0.460153 0.093091 0.140984 0.133 Uiso 1 1 calc R . . . .
H4AC H 0.436217 0.053545 0.190232 0.133 Uiso 1 1 calc R . . . .
C5AA C 0.5430(9) 0.0546(8) 0.2558(7) 0.111(3) Uani 1 1 d D U . . .
H5AB H 0.514433 0.019591 0.266809 0.133 Uiso 1 1 calc R . . . .
H5AC H 0.586599 0.040470 0.265796 0.133 Uiso 1 1 calc R . . . .
C6AA C 0.5772(9) 0.1705(12) 0.2659(7) 0.107(3) Uani 1 1 d D U . . .
H6AB H 0.572029 0.212706 0.284909 0.129 Uiso 1 1 calc R . . . .
H6AC H 0.620288 0.154196 0.275209 0.129 Uiso 1 1 calc R . . . .
C17 C 0.4630(8) 0.1442(10) 0.2671(6) 0.111(3) Uani 1 1 d D U . . .
H17A H 0.431985 0.111891 0.278482 0.134 Uiso 1 1 calc R . . . .
H17B H 0.455906 0.186890 0.284776 0.134 Uiso 1 1 calc R . . . .
C7AA C 0.5296(8) 0.1193(9) 0.2838(5) 0.110(3) Uani 1 1 d D U . . .
H7AB H 0.535126 0.113149 0.322905 0.132 Uiso 1 1 calc R . . . .
C36 C 0.5005(8) 0.2064(7) 0.1897(7) 0.107(3) Uani 1 1 d D U . . .
H36A H 0.492268 0.249390 0.206558 0.129 Uiso 1 1 calc R . . . .
H36B H 0.495175 0.212302 0.150935 0.129 Uiso 1 1 calc R . . . .
C51 C 0.4538(5) 0.1533(8) 0.2071(7) 0.112(3) Uani 1 1 d D U . . .
H51 H 0.409894 0.167962 0.196956 0.134 Uiso 1 1 calc DR . . . .
C8AA C 0.8088(11) 0.4221(12) 0.5210(8) 0.074(5) Uani 1 1 d . U . . .
H8AB H 0.845331 0.429024 0.500084 0.089 Uiso 1 1 calc R . . . .
H8AC H 0.777305 0.456644 0.510777 0.089 Uiso 1 1 calc R . . . .
C3 C 0.8293(12) 0.4286(14) 0.5792(9) 0.089(6) Uani 1 1 d . U . . .
H3 H 0.847930 0.473326 0.586850 0.107 Uiso 1 1 calc R . . . .
C19 C 1.0405(5) 0.3867(2) 0.2031(4) 0.123(3) Uani 1 1 d D U . . .
H19A H 1.049768 0.423894 0.227950 0.147 Uiso 1 1 calc DR . . . .
H19B H 1.016792 0.404530 0.171155 0.147 Uiso 1 1 calc DR . . . .
C22 C 1.1002(6) 0.2763(5) 0.2652(4) 0.127(3) Uani 1 1 d D U . . .
H22 H 1.124049 0.259414 0.297965 0.152 Uiso 1 1 calc R . . . .
C9AA C 0.9869(4) 0.2750(5) 0.1919(5) 0.122(3) Uani 1 1 d D U . . .
H9AB H 0.962747 0.241121 0.209829 0.146 Uiso 1 1 calc R . . . .
H9AC H 0.961100 0.289831 0.159976 0.146 Uiso 1 1 calc R . . . .
C0BA C 1.1025(5) 0.3556(3) 0.1879(4) 0.128(3) Uani 1 1 d D U . . .
H0BB H 1.128135 0.389502 0.170730 0.154 Uiso 1 1 calc R . . . .
C1BA C 1.0808(7) 0.2183(3) 0.2279(5) 0.127(3) Uani 1 1 d D U . . .
H1BB H 1.118401 0.192418 0.220591 0.152 Uiso 1 1 calc R . . . .
H1BC H 1.051904 0.188618 0.245235 0.152 Uiso 1 1 calc R . . . .
C2BA C 1.1589(6) 0.5838(9) 0.2107(7) 0.117(3) Uani 1 1 d D U . . .
H2BB H 1.201224 0.571276 0.227284 0.141 Uiso 1 1 calc R . . . .
C70 C 1.0438(6) 0.5916(6) 0.2237(4) 0.112(3) Uani 1 1 d D U . . .
C100 C 1.1590(6) 0.6575(9) 0.1957(7) 0.117(3) Uani 1 1 d D U . . .
H10A H 1.192226 0.665993 0.171543 0.141 Uiso 1 1 calc R . . . .
H10B H 1.168094 0.684702 0.227773 0.141 Uiso 1 1 calc R . . . .
C122 C 1.1093(8) 0.5721(10) 0.2506(6) 0.113(3) Uani 1 1 d D U . . .
H12A H 1.119033 0.599376 0.282552 0.136 Uiso 1 1 calc R . . . .
H12B H 1.109240 0.524932 0.261255 0.136 Uiso 1 1 calc R . . . .
C128 C 1.0790(7) 0.5610(7) 0.1345(5) 0.118(3) Uani 1 1 d D U . . .
H128 H 1.069187 0.533197 0.102319 0.141 Uiso 1 1 calc R . . . .
C160 C 1.0440(7) 0.6651(4) 0.2080(6) 0.112(3) Uani 1 1 d D U . . .
H16A H 1.053201 0.692828 0.239821 0.135 Uiso 1 1 calc R . . . .
H16B H 1.002227 0.677809 0.191514 0.135 Uiso 1 1 calc R . . . .
C161 C 1.0293(6) 0.5490(2) 0.1742(4) 0.113(3) Uani 1 1 d D U . . .
H16C H 0.987212 0.560380 0.157578 0.135 Uiso 1 1 calc R . . . .
H16D H 1.029071 0.501576 0.184156 0.135 Uiso 1 1 calc DR . . . .
C3BA C 1.0796(9) 0.6341(8) 0.1190(5) 0.118(3) Uani 1 1 d D U . . .
H3BB H 1.038223 0.646715 0.101722 0.141 Uiso 1 1 calc R . . . .
H3BC H 1.111579 0.641587 0.093549 0.141 Uiso 1 1 calc R . . . .
C5BA C 1.0946(7) 0.6771(5) 0.1684(6) 0.116(3) Uani 1 1 d D U . . .
H5BB H 1.095019 0.724939 0.158134 0.139 Uiso 1 1 calc R . . . .
C4BA C 1.1437(7) 0.5415(8) 0.1609(8) 0.118(3) Uani 1 1 d D U . . .
H4BB H 1.143723 0.494033 0.170650 0.142 Uiso 1 1 calc R . . . .
H4BC H 1.176227 0.548450 0.135880 0.142 Uiso 1 1 calc R . . . .
C6BA C 0.5333(9) 0.5526(11) -0.0361(6) 0.160(15) Uani 1 1 d D U . . .
H6BB H 0.556646 0.531354 -0.064231 0.192 Uiso 1 1 calc R . . . .
C132 C 0.5407(11) 0.6286(11) -0.0385(8) 0.161(16) Uani 1 1 d D U . . .
H13A H 0.585674 0.640342 -0.033253 0.194 Uiso 1 1 calc R . . . .
H13B H 0.524427 0.644778 -0.073751 0.194 Uiso 1 1 calc R . . . .
C162 C 0.5599(9) 0.5276(10) 0.0193(7) 0.096(7) Uani 1 1 d D U . . .
H16E H 0.555981 0.478860 0.021274 0.115 Uiso 1 1 calc R . . . .
H16F H 0.604877 0.539283 0.025264 0.115 Uiso 1 1 calc R . . . .
C153 C 1.0411(7) 0.3137(9) 0.2793(3) 0.122(3) Uani 1 1 d D U . . .
H15A H 1.016286 0.284985 0.301271 0.147 Uiso 1 1 calc R . . . .
H15B H 1.053627 0.353652 0.300103 0.147 Uiso 1 1 calc R . . . .
C181 C 1.0891(6) 0.2963(4) 0.1504(4) 0.127(3) Uani 1 1 d D U . . .
H18A H 1.067273 0.312092 0.116932 0.152 Uiso 1 1 calc R . . . .
H18B H 1.129202 0.275860 0.142201 0.152 Uiso 1 1 calc DR . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag01 Ag02 2.8321(13) . ?
Ag01 Ag04 2.7909(14) . ?
Ag01 Ag05 2.9391(15) . ?
Ag01 Ag06 2.8452(14) . ?
Ag01 Ag07 2.8154(14) . ?
Ag01 Ag09 2.8388(14) . ?
Ag01 Ag0A 2.8487(15) . ?
Ag01 Ag0B 2.9123(14) . ?
Ag01 Ag0C 2.8888(14) . ?
Ag01 Ag0D 2.7920(15) . ?
Ag01 Ag0I 2.8591(16) . ?
Ag02 Ag03 2.8530(14) . ?
Ag02 Ag04 2.9430(15) . ?
Ag02 Ag05 2.9007(14) . ?
Ag02 Ag07 2.8460(13) . ?
Ag02 Ag08 2.9210(14) . ?
Ag02 Ag0C 3.0184(15) . ?
Ag02 Ag0G 3.1321(16) . ?
Ag02 Ag0I 3.0865(16) . ?
Ag02 Cl0X 2.594(4) . ?
Ag03 Ag05 2.9810(14) . ?
Ag03 Ag07 2.8168(14) . ?
Ag03 Ag08 2.9347(15) . ?
Ag03 Ag0H 3.0065(16) . ?
Ag03 Cu0N 2.794(3) . ?
Ag03 Cl0U 2.585(4) . ?
Ag03 S12 2.554(4) . ?
Ag04 Ag06 2.9264(14) . ?
Ag04 Ag07 2.8409(14) . ?
Ag04 Ag08 3.0820(15) . ?
Ag04 Ag0A 2.8201(14) . ?
Ag04 Ag0C 2.7741(15) . ?
Ag04 Ag0E 2.8903(15) . ?
Ag04 Ag0G 2.9554(15) . ?
Ag04 Ag0K 2.977(2) . ?
Ag04 Cl15 2.503(4) . ?
Ag05 Ag07 2.9791(15) . ?
Ag05 Ag09 2.9003(15) . ?
Ag05 Ag0D 2.9361(14) . ?
Ag05 Ag0H 3.1608(17) . ?
Ag05 Ag0I 3.0942(17) . ?
Ag05 S0V 2.564(4) . ?
Ag05 S1A 2.608(4) . ?
Ag06 Ag07 2.8310(14) . ?
Ag06 Ag09 2.9446(15) . ?
Ag06 Ag0A 2.8989(15) . ?
Ag06 Ag0B 3.0296(15) . ?
Ag06 Ag0E 2.8072(15) . ?
Ag06 Ag0F 2.7825(15) . ?
Ag06 Ag0J 2.9173(18) . ?
Ag06 Ag0K 2.983(2) . ?
Ag06 Cl13 2.519(4) . ?
Ag07 Ag08 2.9021(14) . ?
Ag07 Ag09 2.8333(14) . ?
Ag07 Ag0E 2.9160(16) . ?
Ag07 Ag0F 2.8941(14) . ?
Ag07 Ag0H 2.9526(16) . ?
Ag08 Ag0G 3.2126(16) . ?
Ag08 Cu0N 2.959(3) . ?
Ag08 S0Y 2.505(4) . ?
Ag08 S10 2.563(4) . ?
Ag09 Ag0B 2.9248(15) . ?
Ag09 Ag0D 2.8404(16) . ?
Ag09 Ag0F 2.9679(16) . ?
Ag09 Ag0H 3.1944(16) . ?
Ag09 Ag0J 3.054(2) . ?
Ag09 Cl11 2.583(4) . ?
Ag0A Ag0B 3.3187(15) . ?
Ag0A Ag0C 3.0394(15) . ?
Ag0A Ag0K 2.978(2) . ?
Ag0A Cu0P 2.849(3) . ?
Ag0A Cu0R 2.882(3) . ?
Ag0A S1B 2.579(4) . ?
Ag0A S1I 2.689(4) . ?
Ag0B Ag0D 2.9251(17) . ?
Ag0B Ag0J 3.149(2) . ?
Ag0B S1E 2.520(4) . ?
Ag0B S1I 2.550(5) . ?
Ag0C Ag0G 3.0202(16) . ?
Ag0C Ag0I 3.2467(18) . ?
Ag0C Cu0P 2.857(3) . ?
Ag0C Cu0R 2.941(3) . ?
Ag0C S16 2.555(4) . ?
Ag0C S18 2.596(5) . ?
Ag0D Ag0I 3.0482(17) . ?
Ag0D Cu0W 2.797(4) . ?
Ag0D Cl0Z 2.579(4) . ?
Ag0D S1G 2.579(5) . ?
Ag0E Ag0F 3.1252(17) . ?
Ag0E Ag0K 2.948(2) . ?
Ag0E Cu0S 2.852(3) . ?
Ag0E Cu0T 2.820(3) . ?
Ag0E S10 2.678(4) . ?
Ag0E S1C 2.604(5) . ?
Ag0F Ag0H 3.3787(18) . ?
Ag0F Ag0J 2.9424(18) . ?
Ag0F Cu0S 2.873(3) . ?
Ag0F Cu0T 2.852(3) . ?
Ag0F S19 2.580(4) . ?
Ag0F S1D 2.517(4) . ?
Ag0G S0Y 2.395(4) . ?
Ag0G S18 2.393(5) . ?
Ag0H S0V 2.393(5) . ?
Ag0H S1D 2.382(5) . ?
Ag0I Cu0W 3.145(6) . ?
Ag0I S16 2.405(4) . ?
Ag0I S1A 2.391(5) . ?
Ag0J S19 2.301(5) . ?
Ag0J S1E 2.295(5) . ?
Ag0K S1B 2.330(5) . ?
Ag0K S1C 2.319(6) . ?
Cu0L Cl0U 2.473(4) . ?
Cu0L Cl0X 2.461(4) . ?
Cu0L S0Y 2.283(4) . ?
Cu0L P17 2.225(4) . ?
Cu0M Cl0U 2.498(4) . ?
Cu0M Cl0X 2.493(5) . ?
Cu0M P14 2.201(5) . ?
Cu0M S1A 2.256(5) . ?
Cu0N Cu0T 2.797(4) . ?
Cu0N S10 2.189(5) . ?
Cu0N S12 2.162(5) . ?
Cu0N S1D 2.761(4) . ?
Cu0O Cl0Z 2.471(5) . ?
Cu0O Cl11 2.479(4) . ?
Cu0O S1E 2.272(5) . ?
Cu0O P1F 2.207(5) . ?
Cu0P Cu0R 2.990(4) . ?
Cu0P S18 2.282(5) . ?
Cu0P S1B 2.276(5) . ?
Cu0P Cl1H 2.284(6) . ?
Cu0Q S0V 2.256(4) . ?
Cu0Q Cl0Z 2.529(5) . ?
Cu0Q Cl11 2.450(5) . ?
Cu0Q P1J 2.196(5) . ?
Cu0R Cu0W 2.719(5) . ?
Cu0R S16 2.343(5) . ?
Cu0R Cl1H 2.251(6) . ?
Cu0R S1I 2.312(5) . ?
Cu0S S19 2.292(5) . ?
Cu0S S1C 2.271(7) . ?
Cu0S Cl01 2.282(7) . ?
Cu0T S10 2.279(5) . ?
Cu0T S1D 2.276(6) . ?
Cu0T Cl01 2.259(7) . ?
S0V C02U 1.807(17) . ?
Cu0W S16 2.547(7) . ?
Cu0W S1G 2.135(6) . ?
Cu0W S1I 2.228(7) . ?
S0Y C02P 1.860(16) . ?
S10 C020 1.838(15) . ?
S12 C022 1.871(15) . ?
P14 C01Q 1.875(17) . ?
P14 C01X 1.837(19) . ?
P14 C02D 1.807(11) . ?
S16 C01Y 1.836(10) . ?
P17 C01Q 1.845(19) . ?
P17 C01S 1.857(16) . ?
P17 C038 1.808(13) . ?
S18 C02C 1.849(18) . ?
S19 C03M 1.845(17) . ?
S1A C01U 1.835(17) . ?
S1B C02J 1.825(17) . ?
S1C C02I 1.825(12) . ?
S1D C04E 1.889(14) . ?
S1E C050 1.859(18) . ?
P1F C02K 1.796(12) . ?
P1F C04B 1.835(10) . ?
P1F C2 1.827(19) . ?
S1G C70 1.766(11) . ?
S1I C03Q 1.898(9) . ?
P1J C43 1.864(14) . ?
P1J C76 1.836(15) . ?
P1J C2 1.858(16) . ?
Cl1L C041 1.59(3) . ?
Cl1M C041 1.88(3) . ?
C01N C027 1.55(2) . ?
C01N C02P 1.49(3) . ?
C01O C01U 1.538(11) . ?
C01O C03B 1.535(11) . ?
C01P C029 1.52(2) . ?
C01P C02R 1.55(2) . ?
C01S C024 1.37(2) . ?
C01S C02A 1.38(2) . ?
C01T C02L 1.51(3) . ?
C01T C03I 1.53(3) . ?
C01U C02S 1.546(11) . ?
C01U C30 1.543(11) . ?
C01V C02A 1.40(3) . ?
C01V C03Y 1.39(3) . ?
C01W C02W 1.57(2) . ?
C01W C03F 1.47(3) . ?
C01W C03P 1.55(3) . ?
C01X C025 1.40(3) . ?
C01X C02M 1.36(2) . ?
C01Y C02F 1.541(10) . ?
C01Y C02O 1.541(11) . ?
C01Y C1 1.542(10) . ?
C020 C026 1.539(8) . ?
C020 C045 1.539(8) . ?
C020 C058 1.542(8) . ?
C021 C02M 1.39(3) . ?
C021 C02V 1.40(3) . ?
C022 C028 1.49(2) . ?
C022 C02X 1.55(2) . ?
C022 C04A 1.49(3) . ?
C023 C026 1.541(8) . ?
C023 C03R 1.535(8) . ?
C023 C04Z 1.535(8) . ?
C024 C03E 1.39(2) . ?
C025 C03G 1.45(3) . ?
C027 C02E 1.60(3) . ?
C027 C03P 1.59(3) . ?
C028 C02L 1.54(2) . ?
C029 C02H 1.55(2) . ?
C029 C04D 1.51(3) . ?
C02C C048 1.56(3) . ?
C02C C04W 1.49(3) . ?
C02C C8AA 1.53(3) . ?
C02E C02Z 1.54(3) . ?
C02F C03O 1.532(11) . ?
C02G C02N 1.56(3) . ?
C02G C02T 1.47(3) . ?
C02G C04D 1.55(3) . ?
C02H C02U 1.53(2) . ?
C02I C040 1.531(10) . ?
C02I C6AA 1.523(11) . ?
C02I C36 1.554(10) . ?
C02J C032 1.540(11) . ?
C02J C037 1.543(11) . ?
C02J C043 1.543(11) . ?
C02K C15 1.3900 . ?
C02K C03K 1.3900 . ?
C15 C104 1.3900 . ?
C104 C98 1.3900 . ?
C98 C93 1.3900 . ?
C93 C03K 1.3900 . ?
C02L C03D 1.52(3) . ?
C02N C02U 1.52(2) . ?
C02O C046 1.559(10) . ?
C02P C02W 1.52(2) . ?
C02P C03S 1.52(2) . ?
C02Q C03B 1.539(11) . ?
C02Q C04J 1.531(12) . ?
C02R C02T 1.53(3) . ?
C02R C03L 1.54(3) . ?
C02S C04J 1.547(11) . ?
C02U C03L 1.52(2) . ?
C02V C03G 1.27(3) . ?
C02X C033 1.53(3) . ?
C02Y C04F 1.3900 . ?
C02Y C04R 1.3900 . ?
C04F C04O 1.3900 . ?
C04O C4 1.3900 . ?
C4 C04B 1.3900 . ?
C04B C04R 1.3900 . ?
C02Z C03F 1.52(3) . ?
C02Z C03S 1.57(2) . ?
C031 C04U 1.58(4) . ?
C031 C050 1.53(3) . ?
C032 C04I 1.548(12) . ?
C033 C036 1.47(4) . ?
C033 C03D 1.54(3) . ?
C034 C03Z 1.539(12) . ?
C034 C043 1.544(12) . ?
C034 C04Y 1.540(12) . ?
C036 C03I 1.52(3) . ?
C037 C053 1.544(11) . ?
C038 C89 1.3900 . ?
C038 C03X 1.3900 . ?
C89 C75 1.3900 . ?
C75 C71 1.3900 . ?
C71 C46 1.3900 . ?
C46 C03X 1.3900 . ?
C039 C03U 1.47(4) . ?
C039 C3 1.55(3) . ?
C03B C03C 1.541(12) . ?
C03C C21 1.544(12) . ?
C03E C03Y 1.29(3) . ?
C03H C050 1.46(3) . ?
C03H C67 1.53(4) . ?
C03I C04A 1.61(3) . ?
C03J C044 1.531(11) . ?
C03J C1 1.535(10) . ?
C03J C55 1.539(11) . ?
C03M C03V 1.539(11) . ?
C03M C04N 1.541(12) . ?
C03M C05B 1.545(11) . ?
C03O C04M 1.540(11) . ?
C03O C55 1.538(11) . ?
C03Q C19 1.5442(12) . ?
C03Q C9AA 1.5417(12) . ?
C03Q C153 1.5401(12) . ?
C03R C05D 1.538(8) . ?
C03T C054 1.43(4) . ?
C03T C3 1.62(4) . ?
C03U C04Q 1.57(4) . ?
C03U C04W 1.62(3) . ?
C03V C1AA 1.548(12) . ?
C03Z C04I 1.536(12) . ?
C040 C5 1.550(9) . ?
C044 C046 1.553(11) . ?
C045 C04L 1.537(8) . ?
C046 C04M 1.560(10) . ?
C047 C43 1.3900 . ?
C047 C103 1.3900 . ?
C43 C04T 1.3900 . ?
C04T C64 1.3900 . ?
C64 C26 1.3900 . ?
C26 C103 1.3900 . ?
C048 C054 1.60(3) . ?
C04C C04I 1.533(12) . ?
C04C C053 1.535(12) . ?
C04E C052 1.535(11) . ?
C04E C0AA 1.542(10) . ?
C04E C162 1.543(11) . ?
C04J C33 1.537(12) . ?
C04K C04L 1.536(8) . ?
C04K C05D 1.539(8) . ?
C04L C04Z 1.534(8) . ?
C04N C04X 1.534(12) . ?
C04Q C054 1.54(4) . ?
C04S C04U 1.42(4) . ?
C04S C67 1.48(5) . ?
C04U C84 1.49(4) . ?
C04X C11 1.532(12) . ?
C04X C2AA 1.528(12) . ?
C04Y C053 1.534(12) . ?
C050 C8 1.54(3) . ?
C051 C22 1.5424(12) . ?
C051 C0BA 1.5439(12) . ?
C052 C82 1.544(12) . ?
C055 C9AA 1.5408(12) . ?
C055 C1BA 1.5419(12) . ?
C055 C181 1.5405(11) . ?
C056 C13 1.50(5) . ?
C056 C67 1.49(5) . ?
C057 C03W 1.3900 . ?
C057 C03A 1.3900 . ?
C03W C042 1.3900 . ?
C042 C035 1.3900 . ?
C035 C02D 1.3900 . ?
C02D C03A 1.3900 . ?
C058 C05D 1.540(8) . ?
C059 C76 1.3900 . ?
C059 C28 1.3900 . ?
C76 C9 1.3900 . ?
C9 C23 1.3900 . ?
C23 C6 1.3900 . ?
C6 C28 1.3900 . ?
C05B C7 1.546(12) . ?
C21 C30 1.536(11) . ?
C21 C33 1.537(12) . ?
C34 C37 1.527(10) . ?
C34 C0AA 1.551(10) . ?
C34 C132 1.526(10) . ?
C37 C82 1.535(10) . ?
C82 C92 1.536(10) . ?
C92 C6BA 1.548(10) . ?
C8 C13 1.66(4) . ?
C13 C84 1.42(5) . ?
C3AA C7 1.532(12) . ?
C3AA C1AA 1.536(12) . ?
C7 C11 1.542(12) . ?
C1AA C2AA 1.530(12) . ?
C5 C4AA 1.535(9) . ?
C5 C5AA 1.549(9) . ?
C4AA C51 1.535(10) . ?
C5AA C7AA 1.525(10) . ?
C6AA C7AA 1.546(11) . ?
C17 C7AA 1.537(10) . ?
C17 C51 1.534(10) . ?
C36 C51 1.553(9) . ?
C8AA C3 1.51(3) . ?
C19 C0BA 1.5461(12) . ?
C22 C1BA 1.5422(12) . ?
C22 C153 1.5404(12) . ?
C0BA C181 1.5424(12) . ?
C2BA C100 1.536(10) . ?
C2BA C122 1.546(11) . ?
C2BA C4BA 1.538(10) . ?
C70 C122 1.558(10) . ?
C70 C160 1.539(9) . ?
C70 C161 1.535(9) . ?
C100 C5BA 1.544(9) . ?
C128 C161 1.543(9) . ?
C128 C3BA 1.529(10) . ?
C128 C4BA 1.541(10) . ?
C160 C5BA 1.557(9) . ?
C3BA C5BA 1.539(9) . ?
C6BA C132 1.545(10) . ?
C6BA C162 1.559(10) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Ag02 Ag01 Ag05 60.31(3) . . ?
Ag02 Ag01 Ag06 112.74(4) . . ?
Ag02 Ag01 Ag09 109.25(4) . . ?
Ag02 Ag01 Ag0A 116.42(4) . . ?
Ag02 Ag01 Ag0B 170.36(5) . . ?
Ag02 Ag01 Ag0C 63.68(4) . . ?
Ag02 Ag01 Ag0I 65.68(4) . . ?
Ag04 Ag01 Ag02 63.11(4) . . ?
Ag04 Ag01 Ag05 113.33(4) . . ?
Ag04 Ag01 Ag06 62.55(4) . . ?
Ag04 Ag01 Ag07 60.89(4) . . ?
Ag04 Ag01 Ag09 113.02(5) . . ?
Ag04 Ag01 Ag0A 60.00(4) . . ?
Ag04 Ag01 Ag0B 118.87(5) . . ?
Ag04 Ag01 Ag0C 58.44(4) . . ?
Ag04 Ag01 Ag0D 172.97(5) . . ?
Ag04 Ag01 Ag0I 117.85(5) . . ?
Ag06 Ag01 Ag05 112.46(4) . . ?
Ag06 Ag01 Ag0A 61.21(4) . . ?
Ag06 Ag01 Ag0B 63.48(4) . . ?
Ag06 Ag01 Ag0C 113.16(5) . . ?
Ag06 Ag01 Ag0I 176.92(5) . . ?
Ag07 Ag01 Ag02 60.52(3) . . ?
Ag07 Ag01 Ag05 62.31(3) . . ?
Ag07 Ag01 Ag06 60.01(4) . . ?
Ag07 Ag01 Ag09 60.14(4) . . ?
Ag07 Ag01 Ag0A 109.71(4) . . ?
Ag07 Ag01 Ag0B 111.39(5) . . ?
Ag07 Ag01 Ag0C 110.24(4) . . ?
Ag07 Ag01 Ag0I 117.25(5) . . ?
Ag09 Ag01 Ag05 60.23(3) . . ?
Ag09 Ag01 Ag06 62.40(4) . . ?
Ag09 Ag01 Ag0A 117.02(5) . . ?
Ag09 Ag01 Ag0B 61.12(4) . . ?
Ag09 Ag01 Ag0C 170.36(5) . . ?
Ag09 Ag01 Ag0I 115.29(5) . . ?
Ag0A Ag01 Ag05 172.02(5) . . ?
Ag0A Ag01 Ag0B 70.34(4) . . ?
Ag0A Ag01 Ag0C 63.97(4) . . ?
Ag0A Ag01 Ag0I 121.79(5) . . ?
Ag0B Ag01 Ag05 112.02(4) . . ?
Ag0C Ag01 Ag05 117.34(4) . . ?
Ag0C Ag01 Ag0B 125.82(5) . . ?
Ag0D Ag01 Ag02 115.10(5) . . ?
Ag0D Ag01 Ag05 61.57(4) . . ?
Ag0D Ag01 Ag06 113.96(5) . . ?
Ag0D Ag01 Ag07 112.13(5) . . ?
Ag0D Ag01 Ag09 60.58(4) . . ?
Ag0D Ag01 Ag0A 124.63(5) . . ?
Ag0D Ag01 Ag0B 61.66(4) . . ?
Ag0D Ag01 Ag0C 127.64(5) . . ?
Ag0D Ag01 Ag0I 65.27(4) . . ?
Ag0I Ag01 Ag05 64.49(4) . . ?
Ag0I Ag01 Ag0B 117.61(5) . . ?
Ag0I Ag01 Ag0C 68.78(4) . . ?
Ag01 Ag02 Ag03 110.00(4) . . ?
Ag01 Ag02 Ag04 57.76(3) . . ?
Ag01 Ag02 Ag05 61.67(3) . . ?
Ag01 Ag02 Ag07 59.45(3) . . ?
Ag01 Ag02 Ag08 110.59(4) . . ?
Ag01 Ag02 Ag0C 59.07(3) . . ?
Ag01 Ag02 Ag0G 107.47(4) . . ?
Ag01 Ag02 Ag0I 57.58(4) . . ?
Ag03 Ag02 Ag04 110.57(4) . . ?
Ag03 Ag02 Ag05 62.40(3) . . ?
Ag03 Ag02 Ag08 61.08(4) . . ?
Ag03 Ag02 Ag0C 164.92(5) . . ?
Ag03 Ag02 Ag0G 121.13(4) . . ?
Ag03 Ag02 Ag0I 120.59(5) . . ?
Ag04 Ag02 Ag0C 55.45(4) . . ?
Ag04 Ag02 Ag0G 58.12(3) . . ?
Ag04 Ag02 Ag0I 106.74(4) . . ?
Ag05 Ag02 Ag04 110.03(4) . . ?
Ag05 Ag02 Ag08 113.62(4) . . ?
Ag05 Ag02 Ag0C 114.49(4) . . ?
Ag05 Ag02 Ag0G 168.06(5) . . ?
Ag05 Ag02 Ag0I 62.14(4) . . ?
Ag07 Ag02 Ag03 59.24(3) . . ?
Ag07 Ag02 Ag04 58.75(3) . . ?
Ag07 Ag02 Ag05 62.44(3) . . ?
Ag07 Ag02 Ag08 60.41(3) . . ?
Ag07 Ag02 Ag0C 105.84(4) . . ?
Ag07 Ag02 Ag0G 108.51(4) . . ?
Ag07 Ag02 Ag0I 109.44(4) . . ?
Ag08 Ag02 Ag04 63.41(4) . . ?
Ag08 Ag02 Ag0C 111.06(5) . . ?
Ag08 Ag02 Ag0G 64.00(4) . . ?
Ag08 Ag02 Ag0I 168.17(5) . . ?
Ag0C Ag02 Ag0G 58.78(4) . . ?
Ag0C Ag02 Ag0I 64.25(4) . . ?
Ag0I Ag02 Ag0G 117.59(5) . . ?
Cl0X Ag02 Ag01 120.28(9) . . ?
Cl0X Ag02 Ag03 119.27(9) . . ?
Cl0X Ag02 Ag04 123.78(10) . . ?
Cl0X Ag02 Ag05 114.81(10) . . ?
Cl0X Ag02 Ag07 177.17(10) . . ?
Cl0X Ag02 Ag08 121.42(9) . . ?
Cl0X Ag02 Ag0C 75.73(9) . . ?
Cl0X Ag02 Ag0G 74.31(10) . . ?
Cl0X Ag02 Ag0I 68.98(9) . . ?
Ag02 Ag03 Ag05 59.58(3) . . ?
Ag02 Ag03 Ag08 60.60(4) . . ?
Ag02 Ag03 Ag0H 111.42(4) . . ?
Ag05 Ag03 Ag0H 63.73(4) . . ?
Ag07 Ag03 Ag02 60.26(3) . . ?
Ag07 Ag03 Ag05 61.76(3) . . ?
Ag07 Ag03 Ag08 60.56(4) . . ?
Ag07 Ag03 Ag0H 60.83(4) . . ?
Ag08 Ag03 Ag05 110.88(4) . . ?
Ag08 Ag03 Ag0H 112.95(5) . . ?
Cu0N Ag03 Ag02 118.17(7) . . ?
Cu0N Ag03 Ag05 127.56(7) . . ?
Cu0N Ag03 Ag07 72.93(6) . . ?
Cu0N Ag03 Ag08 62.14(6) . . ?
Cu0N Ag03 Ag0H 72.15(6) . . ?
Cl0U Ag03 Ag02 78.57(9) . . ?
Cl0U Ag03 Ag05 95.35(8) . . ?
Cl0U Ag03 Ag07 138.65(9) . . ?
Cl0U Ag03 Ag08 103.78(9) . . ?
Cl0U Ag03 Ag0H 142.14(9) . . ?
Cl0U Ag03 Cu0N 137.02(10) . . ?
S12 Ag03 Ag02 165.03(11) . . ?
S12 Ag03 Ag05 130.02(9) . . ?
S12 Ag03 Ag07 111.74(10) . . ?
S12 Ag03 Ag08 104.63(11) . . ?
S12 Ag03 Ag0H 70.65(9) . . ?
S12 Ag03 Cu0N 47.43(12) . . ?
S12 Ag03 Cl0U 109.24(12) . . ?
Ag01 Ag04 Ag02 59.13(3) . . ?
Ag01 Ag04 Ag06 59.63(3) . . ?
Ag01 Ag04 Ag07 59.98(3) . . ?
Ag01 Ag04 Ag08 107.19(4) . . ?
Ag01 Ag04 Ag0A 61.02(4) . . ?
Ag01 Ag04 Ag0E 108.96(4) . . ?
Ag01 Ag04 Ag0G 113.71(5) . . ?
Ag01 Ag04 Ag0K 111.11(5) . . ?
Ag02 Ag04 Ag08 57.95(3) . . ?
Ag02 Ag04 Ag0G 64.15(4) . . ?
Ag02 Ag04 Ag0K 167.99(6) . . ?
Ag06 Ag04 Ag02 107.30(4) . . ?
Ag06 Ag04 Ag08 111.32(4) . . ?
Ag06 Ag04 Ag0G 171.42(5) . . ?
Ag06 Ag04 Ag0K 60.70(5) . . ?
Ag07 Ag04 Ag02 58.92(3) . . ?
Ag07 Ag04 Ag06 58.77(3) . . ?
Ag07 Ag04 Ag08 58.51(3) . . ?
Ag07 Ag04 Ag0E 61.16(4) . . ?
Ag07 Ag04 Ag0G 113.76(5) . . ?
Ag07 Ag04 Ag0K 110.92(5) . . ?
Ag0A Ag04 Ag02 113.81(4) . . ?
Ag0A Ag04 Ag06 60.56(4) . . ?
Ag0A Ag04 Ag07 109.80(4) . . ?
Ag0A Ag04 Ag08 167.65(5) . . ?
Ag0A Ag04 Ag0E 109.29(4) . . ?
Ag0A Ag04 Ag0G 122.36(5) . . ?
Ag0A Ag04 Ag0K 61.76(4) . . ?
Ag0C Ag04 Ag01 62.54(4) . . ?
Ag0C Ag04 Ag02 63.65(4) . . ?
Ag0C Ag04 Ag06 114.16(5) . . ?
Ag0C Ag04 Ag07 112.90(5) . . ?
Ag0C Ag04 Ag08 113.37(4) . . ?
Ag0C Ag04 Ag0A 65.81(4) . . ?
Ag0C Ag04 Ag0E 171.34(5) . . ?
Ag0C Ag04 Ag0G 63.53(4) . . ?
Ag0C Ag04 Ag0K 119.82(5) . . ?
Ag0E Ag04 Ag02 114.35(4) . . ?
Ag0E Ag04 Ag06 57.71(4) . . ?
Ag0E Ag04 Ag08 69.75(4) . . ?
Ag0E Ag04 Ag0G 123.99(5) . . ?
Ag0E Ag04 Ag0K 60.30(5) . . ?
Ag0G Ag04 Ag08 64.26(4) . . ?
Ag0G Ag04 Ag0K 127.85(6) . . ?
Ag0K Ag04 Ag08 124.15(5) . . ?
Cl15 Ag04 Ag01 171.48(13) . . ?
Cl15 Ag04 Ag02 116.07(11) . . ?
Cl15 Ag04 Ag06 118.69(10) . . ?
Cl15 Ag04 Ag07 111.67(12) . . ?
Cl15 Ag04 Ag08 65.07(12) . . ?
Cl15 Ag04 Ag0A 126.41(12) . . ?
Cl15 Ag04 Ag0C 122.94(11) . . ?
Cl15 Ag04 Ag0E 65.71(11) . . ?
Cl15 Ag04 Ag0G 66.99(10) . . ?
Cl15 Ag04 Ag0K 72.61(11) . . ?
Ag01 Ag05 Ag03 103.74(4) . . ?
Ag01 Ag05 Ag07 56.81(3) . . ?
Ag01 Ag05 Ag0H 107.54(4) . . ?
Ag01 Ag05 Ag0I 56.50(4) . . ?
Ag02 Ag05 Ag01 58.02(3) . . ?
Ag02 Ag05 Ag03 58.01(3) . . ?
Ag02 Ag05 Ag07 57.88(3) . . ?
Ag02 Ag05 Ag0D 108.80(4) . . ?
Ag02 Ag05 Ag0H 105.95(4) . . ?
Ag02 Ag05 Ag0I 61.88(4) . . ?
Ag03 Ag05 Ag0H 58.53(3) . . ?
Ag03 Ag05 Ag0I 116.28(4) . . ?
Ag07 Ag05 Ag03 56.41(3) . . ?
Ag07 Ag05 Ag0H 57.40(4) . . ?
Ag07 Ag05 Ag0I 105.81(4) . . ?
Ag09 Ag05 Ag01 58.17(3) . . ?
Ag09 Ag05 Ag02 105.70(4) . . ?
Ag09 Ag05 Ag03 107.66(4) . . ?
Ag09 Ag05 Ag07 57.60(3) . . ?
Ag09 Ag05 Ag0D 58.24(4) . . ?
Ag09 Ag05 Ag0H 63.44(4) . . ?
Ag09 Ag05 Ag0I 106.78(4) . . ?
Ag0D Ag05 Ag01 56.75(3) . . ?
Ag0D Ag05 Ag03 159.46(5) . . ?
Ag0D Ag05 Ag07 103.72(4) . . ?
Ag0D Ag05 Ag0H 117.70(5) . . ?
Ag0D Ag05 Ag0I 60.66(4) . . ?
Ag0I Ag05 Ag0H 163.02(5) . . ?
S0V Ag05 Ag01 139.55(10) . . ?
S0V Ag05 Ag02 147.38(10) . . ?
S0V Ag05 Ag03 89.40(10) . . ?
S0V Ag05 Ag07 104.87(11) . . ?
S0V Ag05 Ag09 81.43(10) . . ?
S0V Ag05 Ag0D 102.00(9) . . ?
S0V Ag05 Ag0H 48.04(11) . . ?
S0V Ag05 Ag0I 147.63(11) . . ?
S0V Ag05 S1A 109.62(16) . . ?
S1A Ag05 Ag01 104.83(11) . . ?
S1A Ag05 Ag02 81.10(11) . . ?
S1A Ag05 Ag03 101.93(9) . . ?
S1A Ag05 Ag07 138.93(11) . . ?
S1A Ag05 Ag09 148.56(10) . . ?
S1A Ag05 Ag0D 90.38(9) . . ?
S1A Ag05 Ag0H 145.34(11) . . ?
S1A Ag05 Ag0I 48.67(11) . . ?
Ag01 Ag06 Ag04 57.81(3) . . ?
Ag01 Ag06 Ag09 58.69(4) . . ?
Ag01 Ag06 Ag0A 59.45(4) . . ?
Ag01 Ag06 Ag0B 59.34(4) . . ?
Ag01 Ag06 Ag0J 112.85(5) . . ?
Ag01 Ag06 Ag0K 109.41(5) . . ?
Ag04 Ag06 Ag09 106.20(4) . . ?
Ag04 Ag06 Ag0B 111.08(4) . . ?
Ag04 Ag06 Ag0K 60.48(5) . . ?
Ag07 Ag06 Ag01 59.47(3) . . ?
Ag07 Ag06 Ag04 59.11(3) . . ?
Ag07 Ag06 Ag09 58.72(3) . . ?
Ag07 Ag06 Ag0A 107.86(4) . . ?
Ag07 Ag06 Ag0B 107.63(4) . . ?
Ag07 Ag06 Ag0J 111.97(5) . . ?
Ag07 Ag06 Ag0K 111.01(5) . . ?
Ag09 Ag06 Ag0B 58.60(4) . . ?
Ag09 Ag06 Ag0K 166.62(6) . . ?
Ag0A Ag06 Ag04 57.91(3) . . ?
Ag0A Ag06 Ag09 112.19(4) . . ?
Ag0A Ag06 Ag0B 68.04(4) . . ?
Ag0A Ag06 Ag0J 124.35(5) . . ?
Ag0A Ag06 Ag0K 60.82(4) . . ?
Ag0E Ag06 Ag01 109.79(4) . . ?
Ag0E Ag06 Ag04 60.50(4) . . ?
Ag0E Ag06 Ag07 62.29(4) . . ?
Ag0E Ag06 Ag09 115.02(5) . . ?
Ag0E Ag06 Ag0A 109.41(5) . . ?
Ag0E Ag06 Ag0B 168.90(5) . . ?
Ag0E Ag06 Ag0J 122.89(5) . . ?
Ag0E Ag06 Ag0K 61.11(5) . . ?
Ag0F Ag06 Ag01 111.53(5) . . ?
Ag0F Ag06 Ag04 114.13(4) . . ?
Ag0F Ag06 Ag07 62.06(4) . . ?
Ag0F Ag06 Ag09 62.35(4) . . ?
Ag0F Ag06 Ag0A 169.84(5) . . ?
Ag0F Ag06 Ag0B 112.50(5) . . ?
Ag0F Ag06 Ag0E 67.99(4) . . ?
Ag0F Ag06 Ag0J 62.11(4) . . ?
Ag0F Ag06 Ag0K 122.48(6) . . ?
Ag0J Ag06 Ag04 169.00(6) . . ?
Ag0J Ag06 Ag09 62.80(5) . . ?
Ag0J Ag06 Ag0B 63.92(4) . . ?
Ag0J Ag06 Ag0K 130.51(6) . . ?
Ag0K Ag06 Ag0B 122.68(5) . . ?
Cl13 Ag06 Ag01 111.52(10) . . ?
Cl13 Ag06 Ag04 119.85(10) . . ?
Cl13 Ag06 Ag07 170.56(10) . . ?
Cl13 Ag06 Ag09 115.17(10) . . ?
Cl13 Ag06 Ag0A 66.77(10) . . ?
Cl13 Ag06 Ag0B 63.42(10) . . ?
Cl13 Ag06 Ag0E 126.32(10) . . ?
Cl13 Ag06 Ag0F 122.99(10) . . ?
Cl13 Ag06 Ag0J 67.74(10) . . ?
Cl13 Ag06 Ag0K 73.74(10) . . ?
Ag01 Ag07 Ag02 60.03(3) . . ?
Ag01 Ag07 Ag03 111.55(4) . . ?
Ag01 Ag07 Ag04 59.13(3) . . ?
Ag01 Ag07 Ag05 60.88(3) . . ?
Ag01 Ag07 Ag06 60.52(3) . . ?
Ag01 Ag07 Ag08 111.63(4) . . ?
Ag01 Ag07 Ag09 60.34(3) . . ?
Ag01 Ag07 Ag0E 107.56(4) . . ?
Ag01 Ag07 Ag0F 109.15(4) . . ?
Ag01 Ag07 Ag0H 117.14(5) . . ?
Ag02 Ag07 Ag05 59.68(3) . . ?
Ag02 Ag07 Ag08 61.07(3) . . ?
Ag02 Ag07 Ag0E 116.58(4) . . ?
Ag02 Ag07 Ag0F 169.18(5) . . ?
Ag02 Ag07 Ag0H 113.22(5) . . ?
Ag03 Ag07 Ag02 60.50(3) . . ?
Ag03 Ag07 Ag04 114.73(4) . . ?
Ag03 Ag07 Ag05 61.83(4) . . ?
Ag03 Ag07 Ag06 172.06(5) . . ?
Ag03 Ag07 Ag08 61.73(4) . . ?
Ag03 Ag07 Ag09 114.35(5) . . ?
Ag03 Ag07 Ag0E 127.37(5) . . ?
Ag03 Ag07 Ag0F 128.01(5) . . ?
Ag03 Ag07 Ag0H 62.76(4) . . ?
Ag04 Ag07 Ag02 62.33(4) . . ?
Ag04 Ag07 Ag05 110.68(4) . . ?
Ag04 Ag07 Ag08 64.90(4) . . ?
Ag04 Ag07 Ag0E 60.26(4) . . ?
Ag04 Ag07 Ag0F 113.34(5) . . ?
Ag04 Ag07 Ag0H 175.02(5) . . ?
Ag06 Ag07 Ag02 112.75(4) . . ?
Ag06 Ag07 Ag04 62.12(4) . . ?
Ag06 Ag07 Ag05 111.69(4) . . ?
Ag06 Ag07 Ag08 119.88(5) . . ?
Ag06 Ag07 Ag09 62.65(4) . . ?
Ag06 Ag07 Ag0E 58.46(4) . . ?
Ag06 Ag07 Ag0F 58.15(4) . . ?
Ag06 Ag07 Ag0H 119.73(4) . . ?
Ag08 Ag07 Ag05 111.86(4) . . ?
Ag08 Ag07 Ag0E 71.97(4) . . ?
Ag08 Ag07 Ag0H 115.55(5) . . ?
Ag09 Ag07 Ag02 109.01(4) . . ?
Ag09 Ag07 Ag04 111.67(4) . . ?
Ag09 Ag07 Ag05 59.80(4) . . ?
Ag09 Ag07 Ag08 170.08(5) . . ?
Ag09 Ag07 Ag0E 115.11(4) . . ?
Ag09 Ag07 Ag0F 62.41(4) . . ?
Ag09 Ag07 Ag0H 66.99(4) . . ?
Ag0E Ag07 Ag05 168.42(5) . . ?
Ag0E Ag07 Ag0H 124.73(5) . . ?
Ag0F Ag07 Ag05 116.36(4) . . ?
Ag0F Ag07 Ag08 127.44(5) . . ?
Ag0F Ag07 Ag0E 65.08(4) . . ?
Ag0F Ag07 Ag0H 70.60(4) . . ?
Ag0H Ag07 Ag05 64.40(4) . . ?
Ag02 Ag08 Ag03 58.31(3) . . ?
Ag02 Ag08 Ag04 58.64(3) . . ?
Ag02 Ag08 Ag0G 61.20(4) . . ?
Ag02 Ag08 Cu0N 110.96(6) . . ?
Ag03 Ag08 Ag04 104.70(4) . . ?
Ag03 Ag08 Ag0G 115.96(4) . . ?
Ag03 Ag08 Cu0N 56.59(6) . . ?
Ag04 Ag08 Ag0G 55.96(3) . . ?
Ag07 Ag08 Ag02 58.52(3) . . ?
Ag07 Ag08 Ag03 57.71(3) . . ?
Ag07 Ag08 Ag04 56.59(3) . . ?
Ag07 Ag08 Ag0G 105.00(4) . . ?
Ag07 Ag08 Cu0N 69.35(5) . . ?
Cu0N Ag08 Ag04 121.41(6) . . ?
Cu0N Ag08 Ag0G 172.15(7) . . ?
S0Y Ag08 Ag02 74.12(9) . . ?
S0Y Ag08 Ag03 96.27(9) . . ?
S0Y Ag08 Ag04 102.19(10) . . ?
S0Y Ag08 Ag07 132.54(9) . . ?
S0Y Ag08 Ag0G 47.56(10) . . ?
S0Y Ag08 Cu0N 132.15(11) . . ?
S0Y Ag08 S10 144.20(13) . . ?
S10 Ag08 Ag02 141.39(10) . . ?
S10 Ag08 Ag03 101.34(11) . . ?
S10 Ag08 Ag04 103.09(10) . . ?
S10 Ag08 Ag07 82.91(9) . . ?
S10 Ag08 Ag0G 140.24(12) . . ?
S10 Ag08 Cu0N 46.02(12) . . ?
Ag01 Ag09 Ag05 61.60(4) . . ?
Ag01 Ag09 Ag06 58.91(3) . . ?
Ag01 Ag09 Ag0B 60.68(4) . . ?
Ag01 Ag09 Ag0D 58.90(4) . . ?
Ag01 Ag09 Ag0F 106.49(4) . . ?
Ag01 Ag09 Ag0H 109.21(4) . . ?
Ag01 Ag09 Ag0J 109.08(5) . . ?
Ag05 Ag09 Ag06 110.71(4) . . ?
Ag05 Ag09 Ag0B 112.79(5) . . ?
Ag05 Ag09 Ag0F 116.52(4) . . ?
Ag05 Ag09 Ag0H 62.26(4) . . ?
Ag05 Ag09 Ag0J 168.87(5) . . ?
Ag06 Ag09 Ag0F 56.15(4) . . ?
Ag06 Ag09 Ag0H 109.08(4) . . ?
Ag06 Ag09 Ag0J 58.16(4) . . ?
Ag07 Ag09 Ag01 59.52(3) . . ?
Ag07 Ag09 Ag05 62.60(3) . . ?
Ag07 Ag09 Ag06 58.64(3) . . ?
Ag07 Ag09 Ag0B 110.51(4) . . ?
Ag07 Ag09 Ag0D 110.17(4) . . ?
Ag07 Ag09 Ag0F 59.80(4) . . ?
Ag07 Ag09 Ag0H 58.29(3) . . ?
Ag07 Ag09 Ag0J 108.01(5) . . ?
Ag0B Ag09 Ag06 62.15(4) . . ?
Ag0B Ag09 Ag0F 110.25(5) . . ?
Ag0B Ag09 Ag0H 168.72(5) . . ?
Ag0B Ag09 Ag0J 63.53(4) . . ?
Ag0D Ag09 Ag05 61.51(4) . . ?
Ag0D Ag09 Ag06 109.58(4) . . ?
Ag0D Ag09 Ag0B 60.96(4) . . ?
Ag0D Ag09 Ag0F 164.98(5) . . ?
Ag0D Ag09 Ag0H 119.61(5) . . ?
Ag0D Ag09 Ag0J 120.32(5) . . ?
Ag0F Ag09 Ag0H 66.38(4) . . ?
Ag0F Ag09 Ag0J 58.48(4) . . ?
Ag0J Ag09 Ag0H 119.19(5) . . ?
Cl11 Ag09 Ag01 175.84(10) . . ?
Cl11 Ag09 Ag05 114.26(10) . . ?
Cl11 Ag09 Ag06 124.63(10) . . ?
Cl11 Ag09 Ag07 119.62(9) . . ?
Cl11 Ag09 Ag0B 122.37(9) . . ?
Cl11 Ag09 Ag0D 119.34(10) . . ?
Cl11 Ag09 Ag0F 75.49(9) . . ?
Cl11 Ag09 Ag0H 68.01(9) . . ?
Cl11 Ag09 Ag0J 75.09(10) . . ?
Ag01 Ag0A Ag06 59.33(3) . . ?
Ag01 Ag0A Ag0B 55.73(3) . . ?
Ag01 Ag0A Ag0C 58.65(3) . . ?
Ag01 Ag0A Ag0K 109.45(5) . . ?
Ag01 Ag0A Cu0P 116.58(6) . . ?
Ag01 Ag0A Cu0R 86.82(7) . . ?
Ag04 Ag0A Ag01 58.98(3) . . ?
Ag04 Ag0A Ag06 61.54(4) . . ?
Ag04 Ag0A Ag0B 105.98(4) . . ?
Ag04 Ag0A Ag0C 56.36(4) . . ?
Ag04 Ag0A Ag0K 61.71(5) . . ?
Ag04 Ag0A Cu0P 84.92(6) . . ?
Ag04 Ag0A Cu0R 115.82(6) . . ?
Ag06 Ag0A Ag0B 57.85(3) . . ?
Ag06 Ag0A Ag0C 107.38(4) . . ?
Ag06 Ag0A Ag0K 60.99(5) . . ?
Ag0C Ag0A Ag0B 108.56(4) . . ?
Ag0K Ag0A Ag0B 113.72(6) . . ?
Ag0K Ag0A Ag0C 111.59(5) . . ?
Cu0P Ag0A Ag06 143.57(7) . . ?
Cu0P Ag0A Ag0B 154.45(7) . . ?
Cu0P Ag0A Ag0C 57.95(6) . . ?
Cu0P Ag0A Ag0K 91.81(8) . . ?
Cu0P Ag0A Cu0R 62.90(8) . . ?
Cu0R Ag0A Ag06 142.88(7) . . ?
Cu0R Ag0A Ag0B 91.65(7) . . ?
Cu0R Ag0A Ag0C 59.48(6) . . ?
Cu0R Ag0A Ag0K 154.44(8) . . ?
S1B Ag0A Ag01 143.75(10) . . ?
S1B Ag0A Ag04 85.11(10) . . ?
S1B Ag0A Ag06 109.91(12) . . ?
S1B Ag0A Ag0B 152.25(10) . . ?
S1B Ag0A Ag0C 98.80(10) . . ?
S1B Ag0A Ag0K 48.93(12) . . ?
S1B Ag0A Cu0P 49.27(12) . . ?
S1B Ag0A Cu0R 106.54(13) . . ?
S1B Ag0A S1I 132.68(16) . . ?
S1I Ag0A Ag01 81.52(12) . . ?
S1I Ag0A Ag04 139.71(13) . . ?
S1I Ag0A Ag06 106.63(11) . . ?
S1I Ag0A Ag0B 48.85(11) . . ?
S1I Ag0A Ag0C 97.92(11) . . ?
S1I Ag0A Ag0K 150.13(12) . . ?
S1I Ag0A Cu0P 108.34(12) . . ?
S1I Ag0A Cu0R 48.88(11) . . ?
Ag01 Ag0B Ag06 57.18(3) . . ?
Ag01 Ag0B Ag09 58.20(3) . . ?
Ag01 Ag0B Ag0A 53.93(3) . . ?
Ag01 Ag0B Ag0D 57.15(4) . . ?
Ag01 Ag0B Ag0J 104.69(5) . . ?
Ag06 Ag0B Ag0A 54.11(3) . . ?
Ag06 Ag0B Ag0J 56.30(4) . . ?
Ag09 Ag0B Ag06 59.25(4) . . ?
Ag09 Ag0B Ag0A 101.75(4) . . ?
Ag09 Ag0B Ag0D 58.10(4) . . ?
Ag09 Ag0B Ag0J 60.23(4) . . ?
Ag0D Ag0B Ag06 105.07(4) . . ?
Ag0D Ag0B Ag0A 106.09(4) . . ?
Ag0D Ag0B Ag0J 114.63(5) . . ?
Ag0J Ag0B Ag0A 105.33(5) . . ?
S1E Ag0B Ag01 132.17(11) . . ?
S1E Ag0B Ag06 101.55(12) . . ?
S1E Ag0B Ag09 74.03(11) . . ?
S1E Ag0B Ag0A 149.87(12) . . ?
S1E Ag0B Ag0D 96.90(11) . . ?
S1E Ag0B Ag0J 46.11(12) . . ?
S1E Ag0B S1I 144.06(15) . . ?
S1I Ag0B Ag01 82.67(11) . . ?
S1I Ag0B Ag06 106.62(11) . . ?
S1I Ag0B Ag09 140.33(11) . . ?
S1I Ag0B Ag0A 52.59(10) . . ?
S1I Ag0B Ag0D 96.84(13) . . ?
S1I Ag0B Ag0J 146.67(13) . . ?
Ag01 Ag0C Ag02 57.25(3) . . ?
Ag01 Ag0C Ag0A 57.37(3) . . ?
Ag01 Ag0C Ag0G 109.03(5) . . ?
Ag01 Ag0C Ag0I 55.18(4) . . ?
Ag01 Ag0C Cu0R 85.00(6) . . ?
Ag02 Ag0C Ag0A 105.71(4) . . ?
Ag02 Ag0C Ag0G 62.49(4) . . ?
Ag02 Ag0C Ag0I 58.89(4) . . ?
Ag04 Ag0C Ag01 59.01(4) . . ?
Ag04 Ag0C Ag02 60.90(4) . . ?
Ag04 Ag0C Ag0A 57.82(4) . . ?
Ag04 Ag0C Ag0G 61.16(4) . . ?
Ag04 Ag0C Ag0I 106.72(4) . . ?
Ag04 Ag0C Cu0P 85.61(7) . . ?
Ag04 Ag0C Cu0R 115.39(6) . . ?
Ag0A Ag0C Ag0I 104.95(4) . . ?
Ag0G Ag0C Ag0A 113.26(5) . . ?
Ag0G Ag0C Ag0I 116.10(5) . . ?
Cu0P Ag0C Ag01 115.04(7) . . ?
Cu0P Ag0C Ag02 145.17(7) . . ?
Cu0P Ag0C Ag0A 57.68(6) . . ?
Cu0P Ag0C Ag0G 94.28(7) . . ?
Cu0P Ag0C Ag0I 149.56(7) . . ?
Cu0P Ag0C Cu0R 62.07(8) . . ?
Cu0R Ag0C Ag02 138.97(7) . . ?
Cu0R Ag0C Ag0A 57.60(6) . . ?
Cu0R Ag0C Ag0G 156.24(8) . . ?
Cu0R Ag0C Ag0I 87.62(7) . . ?
S16 Ag0C Ag01 84.06(9) . . ?
S16 Ag0C Ag02 105.69(10) . . ?
S16 Ag0C Ag04 142.59(10) . . ?
S16 Ag0C Ag0A 98.82(10) . . ?
S16 Ag0C Ag0G 147.62(10) . . ?
S16 Ag0C Ag0I 47.14(10) . . ?
S16 Ag0C Cu0P 107.04(12) . . ?
S16 Ag0C Cu0R 49.86(11) . . ?
S16 Ag0C S18 132.79(14) . . ?
S18 Ag0C Ag01 140.54(11) . . ?
S18 Ag0C Ag02 112.10(11) . . ?
S18 Ag0C Ag04 82.25(11) . . ?
S18 Ag0C Ag0A 97.17(11) . . ?
S18 Ag0C Ag0G 49.74(10) . . ?
S18 Ag0C Ag0I 157.63(11) . . ?
S18 Ag0C Cu0P 49.19(11) . . ?
S18 Ag0C Cu0R 107.35(12) . . ?
Ag01 Ag0D Ag05 61.68(4) . . ?
Ag01 Ag0D Ag09 60.52(4) . . ?
Ag01 Ag0D Ag0B 61.20(4) . . ?
Ag01 Ag0D Ag0I 58.43(4) . . ?
Ag01 Ag0D Cu0W 72.43(9) . . ?
Ag05 Ag0D Ag0I 62.24(4) . . ?
Ag09 Ag0D Ag05 60.25(4) . . ?
Ag09 Ag0D Ag0B 60.95(4) . . ?
Ag09 Ag0D Ag0I 109.60(4) . . ?
Ag0B Ag0D Ag05 111.74(5) . . ?
Ag0B Ag0D Ag0I 111.47(5) . . ?
Cu0W Ag0D Ag05 122.44(12) . . ?
Cu0W Ag0D Ag09 122.65(9) . . ?
Cu0W Ag0D Ag0B 68.81(10) . . ?
Cu0W Ag0D Ag0I 64.94(13) . . ?
Cl0Z Ag0D Ag01 139.55(10) . . ?
Cl0Z Ag0D Ag05 98.42(9) . . ?
Cl0Z Ag0D Ag09 79.05(10) . . ?
Cl0Z Ag0D Ag0B 101.55(10) . . ?
Cl0Z Ag0D Ag0I 145.95(10) . . ?
Cl0Z Ag0D Cu0W 138.95(14) . . ?
Cl0Z Ag0D S1G 103.89(15) . . ?
S1G Ag0D Ag01 115.55(12) . . ?
S1G Ag0D Ag05 132.15(13) . . ?
S1G Ag0D Ag09 165.37(13) . . ?
S1G Ag0D Ag0B 104.52(12) . . ?
S1G Ag0D Ag0I 76.19(12) . . ?
S1G Ag0D Cu0W 46.57(14) . . ?
Ag04 Ag0E Ag07 58.58(3) . . ?
Ag04 Ag0E Ag0F 105.54(4) . . ?
Ag04 Ag0E Ag0K 61.30(5) . . ?
Ag06 Ag0E Ag04 61.79(4) . . ?
Ag06 Ag0E Ag07 59.26(4) . . ?
Ag06 Ag0E Ag0F 55.63(4) . . ?
Ag06 Ag0E Ag0K 62.39(5) . . ?
Ag06 Ag0E Cu0S 81.70(6) . . ?
Ag06 Ag0E Cu0T 112.57(7) . . ?
Ag07 Ag0E Ag0F 57.12(4) . . ?
Ag07 Ag0E Ag0K 109.64(5) . . ?
Ag0K Ag0E Ag0F 112.67(6) . . ?
Cu0S Ag0E Ag04 141.36(7) . . ?
Cu0S Ag0E Ag07 114.27(7) . . ?
Cu0S Ag0E Ag0F 57.25(7) . . ?
Cu0S Ag0E Ag0K 91.80(9) . . ?
Cu0T Ag0E Ag04 137.74(8) . . ?
Cu0T Ag0E Ag07 82.02(7) . . ?
Cu0T Ag0E Ag0F 57.06(6) . . ?
Cu0T Ag0E Ag0K 157.88(8) . . ?
Cu0T Ag0E Cu0S 66.10(9) . . ?
S10 Ag0E Ag04 105.43(10) . . ?
S10 Ag0E Ag06 139.20(11) . . ?
S10 Ag0E Ag07 80.72(10) . . ?
S10 Ag0E Ag0F 97.45(11) . . ?
S10 Ag0E Ag0K 149.18(12) . . ?
S10 Ag0E Cu0S 110.75(12) . . ?
S10 Ag0E Cu0T 48.88(11) . . ?
S1C Ag0E Ag04 110.14(14) . . ?
S1C Ag0E Ag06 82.79(11) . . ?
S1C Ag0E Ag07 141.64(12) . . ?
S1C Ag0E Ag0F 98.25(13) . . ?
S1C Ag0E Ag0K 48.90(15) . . ?
S1C Ag0E Cu0S 48.94(16) . . ?
S1C Ag0E Cu0T 110.40(16) . . ?
S1C Ag0E S10 135.26(15) . . ?
Ag06 Ag0F Ag07 59.79(4) . . ?
Ag06 Ag0F Ag09 61.50(4) . . ?
Ag06 Ag0F Ag0E 56.38(4) . . ?
Ag06 Ag0F Ag0H 108.18(5) . . ?
Ag06 Ag0F Ag0J 61.20(4) . . ?
Ag06 Ag0F Cu0S 81.74(8) . . ?
Ag06 Ag0F Cu0T 112.34(8) . . ?
Ag07 Ag0F Ag09 57.79(3) . . ?
Ag07 Ag0F Ag0E 57.80(3) . . ?
Ag07 Ag0F Ag0H 55.51(4) . . ?
Ag07 Ag0F Ag0J 109.45(5) . . ?
Ag09 Ag0F Ag0E 105.53(4) . . ?
Ag09 Ag0F Ag0H 60.03(4) . . ?
Ag0E Ag0F Ag0H 106.08(4) . . ?
Ag0J Ag0F Ag09 62.22(4) . . ?
Ag0J Ag0F Ag0E 111.90(6) . . ?
Ag0J Ag0F Ag0H 116.83(6) . . ?
Cu0S Ag0F Ag07 114.28(7) . . ?
Cu0S Ag0F Ag09 141.53(8) . . ?
Cu0S Ag0F Ag0E 56.58(6) . . ?
Cu0S Ag0F Ag0H 151.68(7) . . ?
Cu0S Ag0F Ag0J 91.32(8) . . ?
Cu0T Ag0F Ag07 81.86(6) . . ?
Cu0T Ag0F Ag09 137.11(7) . . ?
Cu0T Ag0F Ag0E 56.08(7) . . ?
Cu0T Ag0F Ag0H 86.41(7) . . ?
Cu0T Ag0F Ag0J 156.72(9) . . ?
Cu0T Ag0F Cu0S 65.40(9) . . ?
S19 Ag0F Ag06 82.94(11) . . ?
S19 Ag0F Ag07 142.33(11) . . ?
S19 Ag0F Ag09 110.90(10) . . ?
S19 Ag0F Ag0E 98.34(12) . . ?
S19 Ag0F Ag0H 155.43(12) . . ?
S19 Ag0F Ag0J 48.70(10) . . ?
S19 Ag0F Cu0S 49.35(12) . . ?
S19 Ag0F Cu0T 110.08(12) . . ?
S1D Ag0F Ag06 139.30(10) . . ?
S1D Ag0F Ag07 80.21(10) . . ?
S1D Ag0F Ag09 104.74(13) . . ?
S1D Ag0F Ag0E 97.30(11) . . ?
S1D Ag0F Ag0H 44.77(12) . . ?
S1D Ag0F Ag0J 150.09(12) . . ?
S1D Ag0F Cu0S 110.86(14) . . ?
S1D Ag0F Cu0T 49.68(14) . . ?
S1D Ag0F S19 135.22(15) . . ?
Ag02 Ag0G Ag08 54.81(3) . . ?
Ag04 Ag0G Ag02 57.73(3) . . ?
Ag04 Ag0G Ag08 59.78(3) . . ?
Ag04 Ag0G Ag0C 55.31(4) . . ?
Ag0C Ag0G Ag02 58.73(4) . . ?
Ag0C Ag0G Ag08 103.52(4) . . ?
S0Y Ag0G Ag02 71.56(9) . . ?
S0Y Ag0G Ag04 108.80(10) . . ?
S0Y Ag0G Ag08 50.52(9) . . ?
S0Y Ag0G Ag0C 128.52(10) . . ?
S18 Ag0G Ag02 114.48(11) . . ?
S18 Ag0G Ag04 82.00(10) . . ?
S18 Ag0G Ag08 140.41(11) . . ?
S18 Ag0G Ag0C 55.89(11) . . ?
S18 Ag0G S0Y 169.04(14) . . ?
Ag03 Ag0H Ag05 57.74(4) . . ?
Ag03 Ag0H Ag09 99.89(4) . . ?
Ag03 Ag0H Ag0F 106.87(5) . . ?
Ag05 Ag0H Ag09 54.30(3) . . ?
Ag05 Ag0H Ag0F 99.44(4) . . ?
Ag07 Ag0H Ag03 56.41(4) . . ?
Ag07 Ag0H Ag05 58.21(4) . . ?
Ag07 Ag0H Ag09 54.72(3) . . ?
Ag07 Ag0H Ag0F 53.89(3) . . ?
Ag09 Ag0H Ag0F 53.59(3) . . ?
S0V Ag0H Ag03 92.12(10) . . ?
S0V Ag0H Ag05 52.82(10) . . ?
S0V Ag0H Ag07 110.40(11) . . ?
S0V Ag0H Ag09 78.07(10) . . ?
S0V Ag0H Ag0F 129.93(10) . . ?
S1D Ag0H Ag03 103.42(10) . . ?
S1D Ag0H Ag05 139.30(12) . . ?
S1D Ag0H Ag07 81.17(11) . . ?
S1D Ag0H Ag09 101.62(11) . . ?
S1D Ag0H Ag0F 48.07(11) . . ?
S1D Ag0H S0V 164.20(14) . . ?
Ag01 Ag0I Ag02 56.74(3) . . ?
Ag01 Ag0I Ag05 59.01(4) . . ?
Ag01 Ag0I Ag0C 56.04(4) . . ?
Ag01 Ag0I Ag0D 56.30(4) . . ?
Ag01 Ag0I Cu0W 66.53(8) . . ?
Ag02 Ag0I Ag05 55.98(3) . . ?
Ag02 Ag0I Ag0C 56.86(3) . . ?
Ag02 Ag0I Cu0W 121.01(8) . . ?
Ag05 Ag0I Ag0C 103.43(4) . . ?
Ag05 Ag0I Cu0W 107.30(8) . . ?
Ag0D Ag0I Ag02 101.36(5) . . ?
Ag0D Ag0I Ag05 57.10(4) . . ?
Ag0D Ag0I Ag0C 108.13(5) . . ?
Ag0D Ag0I Cu0W 53.66(8) . . ?
Cu0W Ag0I Ag0C 79.72(8) . . ?
S16 Ag0I Ag01 87.44(10) . . ?
S16 Ag0I Ag02 107.65(11) . . ?
S16 Ag0I Ag05 146.45(11) . . ?
S16 Ag0I Ag0C 51.15(11) . . ?
S16 Ag0I Ag0D 105.69(10) . . ?
S16 Ag0I Cu0W 52.59(12) . . ?
S1A Ag0I Ag01 113.59(11) . . ?
S1A Ag0I Ag02 80.77(10) . . ?
S1A Ag0I Ag05 54.99(10) . . ?
S1A Ag0I Ag0C 135.41(11) . . ?
S1A Ag0I Ag0D 92.03(11) . . ?
S1A Ag0I Cu0W 140.45(13) . . ?
S1A Ag0I S16 158.01(15) . . ?
Ag06 Ag0J Ag09 59.04(4) . . ?
Ag06 Ag0J Ag0B 59.77(4) . . ?
Ag06 Ag0J Ag0F 56.70(4) . . ?
Ag09 Ag0J Ag0B 56.24(4) . . ?
Ag0F Ag0J Ag09 59.30(4) . . ?
Ag0F Ag0J Ag0B 105.00(5) . . ?
S19 Ag0J Ag06 85.00(12) . . ?
S19 Ag0J Ag09 116.67(12) . . ?
S19 Ag0J Ag0B 143.03(13) . . ?
S19 Ag0J Ag0F 57.40(11) . . ?
S1E Ag0J Ag06 111.07(12) . . ?
S1E Ag0J Ag09 74.51(11) . . ?
S1E Ag0J Ag0B 52.34(11) . . ?
S1E Ag0J Ag0F 131.85(13) . . ?
S1E Ag0J S19 163.91(16) . . ?
Ag04 Ag0K Ag06 58.82(4) . . ?
Ag04 Ag0K Ag0A 56.53(4) . . ?
Ag0A Ag0K Ag06 58.20(4) . . ?
Ag0E Ag0K Ag04 58.40(4) . . ?
Ag0E Ag0K Ag06 56.50(4) . . ?
Ag0E Ag0K Ag0A 103.62(6) . . ?
S1B Ag0K Ag04 86.18(12) . . ?
S1B Ag0K Ag06 114.75(12) . . ?
S1B Ag0K Ag0A 56.56(11) . . ?
S1B Ag0K Ag0E 143.46(13) . . ?
S1C Ag0K Ag04 116.14(15) . . ?
S1C Ag0K Ag06 83.99(15) . . ?
S1C Ag0K Ag0A 140.20(16) . . ?
S1C Ag0K Ag0E 57.81(14) . . ?
S1C Ag0K S1B 156.86(19) . . ?
Cl0X Cu0L Cl0U 94.37(14) . . ?
S0Y Cu0L Cl0U 106.98(15) . . ?
S0Y Cu0L Cl0X 98.40(15) . . ?
P17 Cu0L Cl0U 103.22(16) . . ?
P17 Cu0L Cl0X 109.75(16) . . ?
P17 Cu0L S0Y 136.54(17) . . ?
Cl0X Cu0M Cl0U 92.97(14) . . ?
P14 Cu0M Cl0U 97.86(16) . . ?
P14 Cu0M Cl0X 118.63(18) . . ?
P14 Cu0M S1A 135.6(2) . . ?
S1A Cu0M Cl0U 104.52(16) . . ?
S1A Cu0M Cl0X 98.20(17) . . ?
Ag03 Cu0N Ag08 61.27(6) . . ?
Ag03 Cu0N Cu0T 128.26(10) . . ?
Cu0T Cu0N Ag08 98.10(11) . . ?
S10 Cu0N Ag03 116.96(15) . . ?
S10 Cu0N Ag08 57.41(13) . . ?
S10 Cu0N Cu0T 52.69(14) . . ?
S10 Cu0N S1D 99.47(18) . . ?
S12 Cu0N Ag03 60.45(12) . . ?
S12 Cu0N Ag08 115.42(14) . . ?
S12 Cu0N Cu0T 139.91(17) . . ?
S12 Cu0N S10 166.9(2) . . ?
S12 Cu0N S1D 93.63(18) . . ?
S1D Cu0N Ag03 99.74(13) . . ?
S1D Cu0N Ag08 121.32(12) . . ?
S1D Cu0N Cu0T 48.33(14) . . ?
Cl0Z Cu0O Cl11 94.31(15) . . ?
S1E Cu0O Cl0Z 104.37(17) . . ?
S1E Cu0O Cl11 99.27(18) . . ?
P1F Cu0O Cl0Z 102.85(19) . . ?
P1F Cu0O Cl11 109.27(18) . . ?
P1F Cu0O S1E 138.5(2) . . ?
Ag0A Cu0P Ag0C 64.37(6) . . ?
Ag0A Cu0P Cu0R 59.10(7) . . ?
Ag0C Cu0P Cu0R 60.34(7) . . ?
S18 Cu0P Ag0A 110.83(14) . . ?
S18 Cu0P Ag0C 59.44(13) . . ?
S18 Cu0P Cu0R 115.11(16) . . ?
S18 Cu0P Cl1H 126.7(2) . . ?
S1B Cu0P Ag0A 59.17(12) . . ?
S1B Cu0P Ag0C 112.34(15) . . ?
S1B Cu0P Cu0R 111.87(14) . . ?
S1B Cu0P S18 111.1(2) . . ?
S1B Cu0P Cl1H 122.1(2) . . ?
Cl1H Cu0P Ag0A 99.40(16) . . ?
Cl1H Cu0P Ag0C 100.39(17) . . ?
Cl1H Cu0P Cu0R 48.28(15) . . ?
S0V Cu0Q Cl0Z 106.89(17) . . ?
S0V Cu0Q Cl11 99.13(17) . . ?
Cl11 Cu0Q Cl0Z 93.57(15) . . ?
P1J Cu0Q S0V 135.3(2) . . ?
P1J Cu0Q Cl0Z 95.40(19) . . ?
P1J Cu0Q Cl11 118.0(2) . . ?
Ag0A Cu0R Ag0C 62.91(6) . . ?
Ag0A Cu0R Cu0P 58.01(8) . . ?
Ag0C Cu0R Cu0P 57.59(7) . . ?
Cu0W Cu0R Ag0A 91.15(11) . . ?
Cu0W Cu0R Ag0C 92.68(13) . . ?
Cu0W Cu0R Cu0P 143.57(13) . . ?
S16 Cu0R Ag0A 108.80(13) . . ?
S16 Cu0R Ag0C 56.49(11) . . ?
S16 Cu0R Cu0P 108.91(14) . . ?
S16 Cu0R Cu0W 59.87(17) . . ?
Cl1H Cu0R Ag0A 99.23(18) . . ?
Cl1H Cu0R Ag0C 98.76(16) . . ?
Cl1H Cu0R Cu0P 49.22(16) . . ?
Cl1H Cu0R Cu0W 167.2(2) . . ?
Cl1H Cu0R S16 122.6(2) . . ?
Cl1H Cu0R S1I 127.7(2) . . ?
S1I Cu0R Ag0A 61.20(13) . . ?
S1I Cu0R Ag0C 110.34(15) . . ?
S1I Cu0R Cu0P 115.18(16) . . ?
S1I Cu0R Cu0W 51.80(19) . . ?
S1I Cu0R S16 109.7(2) . . ?
Ag0E Cu0S Ag0F 66.17(7) . . ?
S19 Cu0S Ag0E 114.28(14) . . ?
S19 Cu0S Ag0F 58.65(13) . . ?
S1C Cu0S Ag0E 59.85(14) . . ?
S1C Cu0S Ag0F 114.79(17) . . ?
S1C Cu0S S19 116.2(2) . . ?
S1C Cu0S Cl01 122.8(3) . . ?
Cl01 Cu0S Ag0E 95.11(19) . . ?
Cl01 Cu0S Ag0F 94.7(2) . . ?
Cl01 Cu0S S19 121.0(3) . . ?
Ag0E Cu0T Ag0F 66.86(7) . . ?
Cu0N Cu0T Ag0E 93.13(10) . . ?
Cu0N Cu0T Ag0F 100.17(10) . . ?
S10 Cu0T Ag0E 62.31(13) . . ?
S10 Cu0T Ag0F 116.40(14) . . ?
S10 Cu0T Cu0N 49.82(14) . . ?
S1D Cu0T Ag0E 112.76(14) . . ?
S1D Cu0T Ag0F 57.47(12) . . ?
S1D Cu0T Cu0N 65.01(14) . . ?
S1D Cu0T S10 112.9(2) . . ?
Cl01 Cu0T Ag0E 96.5(3) . . ?
Cl01 Cu0T Ag0F 95.74(18) . . ?
Cl01 Cu0T Cu0N 163.67(19) . . ?
Cl01 Cu0T S10 124.8(3) . . ?
Cl01 Cu0T S1D 122.2(3) . . ?
Cu0L Cl0U Ag03 108.73(14) . . ?
Cu0L Cl0U Cu0M 76.07(13) . . ?
Cu0M Cl0U Ag03 116.28(14) . . ?
Ag0H S0V Ag05 79.14(12) . . ?
Cu0Q S0V Ag05 114.21(17) . . ?
Cu0Q S0V Ag0H 103.93(19) . . ?
C02U S0V Ag05 123.8(5) . . ?
C02U S0V Ag0H 113.1(5) . . ?
C02U S0V Cu0Q 114.8(5) . . ?
Ag0D Cu0W Ag0I 61.40(10) . . ?
Cu0R Cu0W Ag0D 134.80(16) . . ?
Cu0R Cu0W Ag0I 93.74(16) . . ?
S16 Cu0W Ag0D 109.4(2) . . ?
S16 Cu0W Ag0I 48.61(14) . . ?
S16 Cu0W Cu0R 52.72(14) . . ?
S1G Cu0W Ag0D 61.35(16) . . ?
S1G Cu0W Ag0I 80.3(2) . . ?
S1G Cu0W Cu0R 156.6(3) . . ?
S1G Cu0W S16 109.7(3) . . ?
S1G Cu0W S1I 144.7(3) . . ?
S1I Cu0W Ag0D 109.0(2) . . ?
S1I Cu0W Ag0I 127.2(2) . . ?
S1I Cu0W Cu0R 54.66(15) . . ?
S1I Cu0W S16 105.5(2) . . ?
Cu0L Cl0X Ag02 84.90(12) . . ?
Cu0L Cl0X Cu0M 76.38(13) . . ?
Cu0M Cl0X Ag02 90.47(13) . . ?
Ag0G S0Y Ag08 81.92(12) . . ?
Cu0L S0Y Ag08 120.04(16) . . ?
Cu0L S0Y Ag0G 108.91(17) . . ?
C02P S0Y Ag08 120.6(5) . . ?
C02P S0Y Ag0G 106.8(6) . . ?
C02P S0Y Cu0L 112.1(5) . . ?
Cu0O Cl0Z Ag0D 111.06(16) . . ?
Cu0O Cl0Z Cu0Q 75.77(14) . . ?
Cu0Q Cl0Z Ag0D 112.03(15) . . ?
Ag08 S10 Ag0E 81.39(12) . . ?
Cu0N S10 Ag08 76.57(14) . . ?
Cu0N S10 Ag0E 113.50(17) . . ?
Cu0N S10 Cu0T 77.49(19) . . ?
Cu0T S10 Ag08 127.73(18) . . ?
Cu0T S10 Ag0E 68.81(13) . . ?
C020 S10 Ag08 117.2(4) . . ?
C020 S10 Ag0E 134.4(5) . . ?
C020 S10 Cu0N 111.4(5) . . ?
C020 S10 Cu0T 114.3(4) . . ?
Cu0O Cl11 Ag09 85.39(13) . . ?
Cu0Q Cl11 Ag09 89.64(14) . . ?
Cu0Q Cl11 Cu0O 77.06(14) . . ?
Cu0N S12 Ag03 72.12(14) . . ?
C022 S12 Ag03 110.8(5) . . ?
C022 S12 Cu0N 110.2(6) . . ?
C01Q P14 Cu0M 112.8(6) . . ?
C01X P14 Cu0M 114.4(5) . . ?
C01X P14 C01Q 98.3(8) . . ?
C02D P14 Cu0M 119.8(5) . . ?
C02D P14 C01Q 104.8(7) . . ?
C02D P14 C01X 104.1(7) . . ?
Ag0I S16 Ag0C 81.71(12) . . ?
Ag0I S16 Cu0W 78.80(15) . . ?
Cu0R S16 Ag0C 73.65(14) . . ?
Cu0R S16 Ag0I 129.20(17) . . ?
Cu0R S16 Cu0W 67.41(15) . . ?
Cu0W S16 Ag0C 106.85(16) . . ?
C01Y S16 Ag0C 130.0(4) . . ?
C01Y S16 Ag0I 112.6(4) . . ?
C01Y S16 Cu0R 117.4(4) . . ?
C01Y S16 Cu0W 122.7(4) . . ?
C01Q P17 Cu0L 111.7(6) . . ?
C01Q P17 C01S 96.2(8) . . ?
C01S P17 Cu0L 117.1(5) . . ?
C038 P17 Cu0L 116.1(6) . . ?
C038 P17 C01Q 103.6(8) . . ?
C038 P17 C01S 109.5(8) . . ?
Ag0G S18 Ag0C 74.38(13) . . ?
Cu0P S18 Ag0C 71.37(13) . . ?
Cu0P S18 Ag0G 134.37(19) . . ?
C02C S18 Ag0C 115.9(6) . . ?
C02C S18 Ag0G 105.8(6) . . ?
C02C S18 Cu0P 115.8(6) . . ?
Ag0J S19 Ag0F 73.90(13) . . ?
Cu0S S19 Ag0F 72.00(13) . . ?
Cu0S S19 Ag0J 129.84(19) . . ?
C03M S19 Ag0F 119.8(6) . . ?
C03M S19 Ag0J 108.9(5) . . ?
C03M S19 Cu0S 119.7(5) . . ?
Ag0I S1A Ag05 76.33(12) . . ?
Cu0M S1A Ag05 115.05(17) . . ?
Cu0M S1A Ag0I 104.3(2) . . ?
C01U S1A Ag05 128.3(5) . . ?
C01U S1A Ag0I 105.4(5) . . ?
C01U S1A Cu0M 114.3(5) . . ?
Ag0K S1B Ag0A 74.50(13) . . ?
Cu0P S1B Ag0A 71.56(13) . . ?
Cu0P S1B Ag0K 130.7(2) . . ?
C02J S1B Ag0A 110.3(5) . . ?
C02J S1B Ag0K 108.3(5) . . ?
C02J S1B Cu0P 116.4(5) . . ?
Ag0K S1C Ag0E 73.29(15) . . ?
Cu0S S1C Ag0E 71.21(18) . . ?
Cu0S S1C Ag0K 130.3(2) . . ?
C02I S1C Ag0E 112.8(6) . . ?
C02I S1C Ag0K 110.6(6) . . ?
C02I S1C Cu0S 114.6(6) . . ?
Ag0F S1D Cu0N 110.28(16) . . ?
Ag0H S1D Ag0F 87.16(14) . . ?
Ag0H S1D Cu0N 82.98(14) . . ?
Cu0T S1D Ag0F 72.85(16) . . ?
Cu0T S1D Ag0H 133.69(19) . . ?
Cu0T S1D Cu0N 66.65(14) . . ?
C04E S1D Ag0F 118.1(6) . . ?
C04E S1D Ag0H 106.3(6) . . ?
C04E S1D Cu0N 130.9(6) . . ?
C04E S1D Cu0T 120.0(6) . . ?
Ag0J S1E Ag0B 81.55(14) . . ?
Cu0O S1E Ag0B 120.48(19) . . ?
Cu0O S1E Ag0J 107.9(2) . . ?
C050 S1E Ag0B 122.8(6) . . ?
C050 S1E Ag0J 103.4(6) . . ?
C050 S1E Cu0O 112.0(6) . . ?
C02K P1F Cu0O 118.8(4) . . ?
C02K P1F C04B 106.5(7) . . ?
C02K P1F C2 102.4(7) . . ?
C04B P1F Cu0O 117.5(5) . . ?
C2 P1F Cu0O 110.7(6) . . ?
C2 P1F C04B 98.0(8) . . ?
Cu0W S1G Ag0D 72.08(16) . . ?
C70 S1G Ag0D 118.8(5) . . ?
C70 S1G Cu0W 126.4(5) . . ?
Cu0R Cl1H Cu0P 82.49(18) . . ?
Ag0B S1I Ag0A 78.56(13) . . ?
Cu0R S1I Ag0A 69.92(13) . . ?
Cu0R S1I Ag0B 132.9(2) . . ?
Cu0W S1I Ag0A 108.6(2) . . ?
Cu0W S1I Ag0B 85.0(2) . . ?
Cu0W S1I Cu0R 73.5(2) . . ?
C03Q S1I Ag0A 133.7(4) . . ?
C03Q S1I Ag0B 106.3(4) . . ?
C03Q S1I Cu0R 120.8(4) . . ?
C03Q S1I Cu0W 117.7(4) . . ?
C43 P1J Cu0Q 118.0(6) . . ?
C76 P1J Cu0Q 112.9(6) . . ?
C76 P1J C43 104.9(9) . . ?
C76 P1J C2 100.9(8) . . ?
C2 P1J Cu0Q 113.9(6) . . ?
C2 P1J C43 104.3(8) . . ?
Cu0T Cl01 Cu0S 85.9(2) . . ?
C02P C01N C027 111.2(15) . . ?
C03B C01O C01U 106.9(15) . . ?
C029 C01P C02R 108.3(15) . . ?
P17 C01Q P14 114.1(10) . . ?
C024 C01S P17 116.0(12) . . ?
C024 C01S C02A 120.4(16) . . ?
C02A C01S P17 123.3(13) . . ?
C02L C01T C03I 110.1(18) . . ?
C01O C01U S1A 111.0(11) . . ?
C01O C01U C02S 112.8(14) . . ?
C01O C01U C30 106.6(13) . . ?
C02S C01U S1A 109.5(10) . . ?
C30 C01U S1A 107.3(10) . . ?
C30 C01U C02S 109.5(14) . . ?
C03Y C01V C02A 119.3(19) . . ?
C03F C01W C02W 110.2(16) . . ?
C03F C01W C03P 112.2(19) . . ?
C03P C01W C02W 107.4(17) . . ?
C025 C01X P14 122.7(15) . . ?
C02M C01X P14 118.5(14) . . ?
C02M C01X C025 118.8(18) . . ?
C02F C01Y S16 111.0(9) . . ?
C02F C01Y C1 110.3(8) . . ?
C02O C01Y S16 108.2(7) . . ?
C02O C01Y C02F 108.2(11) . . ?
C02O C01Y C1 108.7(12) . . ?
C1 C01Y S16 110.3(8) . . ?
C026 C020 S10 110.9(10) . . ?
C026 C020 C058 107.6(14) . . ?
C045 C020 S10 108.4(9) . . ?
C045 C020 C026 108.7(14) . . ?
C045 C020 C058 111.2(15) . . ?
C058 C020 S10 109.9(10) . . ?
C02M C021 C02V 117(2) . . ?
C028 C022 S12 113.4(12) . . ?
C028 C022 C02X 112.8(15) . . ?
C028 C022 C04A 110.6(15) . . ?
C02X C022 S12 106.9(11) . . ?
C04A C022 S12 104.8(12) . . ?
C04A C022 C02X 107.9(16) . . ?
C03R C023 C026 106.9(16) . . ?
C04Z C023 C026 108.4(16) . . ?
C04Z C023 C03R 111.1(17) . . ?
C01S C024 C03E 118.8(16) . . ?
C01X C025 C03G 116(2) . . ?
C020 C026 C023 111.7(14) . . ?
C01N C027 C02E 108.5(16) . . ?
C01N C027 C03P 107.0(17) . . ?
C03P C027 C02E 106.9(18) . . ?
C022 C028 C02L 108.9(14) . . ?
C01P C029 C02H 109.2(14) . . ?
C04D C029 C01P 110.5(15) . . ?
C04D C029 C02H 109.4(14) . . ?
C01S C02A C01V 118.4(19) . . ?
C048 C02C S18 107.2(13) . . ?
C04W C02C S18 107.7(13) . . ?
C04W C02C C048 109.1(17) . . ?
C04W C02C C8AA 111.5(18) . . ?
C8AA C02C S18 111.0(13) . . ?
C8AA C02C C048 110.3(17) . . ?
C02Z C02E C027 110.6(17) . . ?
C03O C02F C01Y 111.4(9) . . ?
C02T C02G C02N 111.2(17) . . ?
C02T C02G C04D 109.0(17) . . ?
C04D C02G C02N 106.0(15) . . ?
C02U C02H C029 109.9(14) . . ?
C040 C02I S1C 108.0(10) . . ?
C040 C02I C36 109.1(7) . . ?
C6AA C02I S1C 109.3(10) . . ?
C6AA C02I C040 107.5(12) . . ?
C6AA C02I C36 111.4(9) . . ?
C36 C02I S1C 111.6(10) . . ?
C032 C02J S1B 111.7(12) . . ?
C032 C02J C037 108.4(16) . . ?
C032 C02J C043 109.9(16) . . ?
C037 C02J S1B 107.6(11) . . ?
C037 C02J C043 110.5(15) . . ?
C043 C02J S1B 108.6(11) . . ?
C15 C02K P1F 121.7(6) . . ?
C15 C02K C03K 120.0 . . ?
C03K C02K P1F 118.3(6) . . ?
C02K C15 C104 120.0 . . ?
C98 C104 C15 120.0 . . ?
C104 C98 C93 120.0 . . ?
C03K C93 C98 120.0 . . ?
C93 C03K C02K 120.0 . . ?
C01T C02L C028 107.6(15) . . ?
C01T C02L C03D 113.5(17) . . ?
C03D C02L C028 108.1(14) . . ?
C01X C02M C021 122.7(18) . . ?
C02U C02N C02G 111.3(14) . . ?
C01Y C02O C046 109.5(8) . . ?
C01N C02P S0Y 110.6(11) . . ?
C01N C02P C02W 109.0(15) . . ?
C01N C02P C03S 111.9(15) . . ?
C02W C02P S0Y 106.9(11) . . ?
C02W C02P C03S 109.6(14) . . ?
C03S C02P S0Y 108.7(12) . . ?
C04J C02Q C03B 109.2(18) . . ?
C02T C02R C01P 108.4(16) . . ?
C02T C02R C03L 110.2(17) . . ?
C03L C02R C01P 109.8(16) . . ?
C01U C02S C04J 109.5(16) . . ?
C02G C02T C02R 110.7(18) . . ?
C02H C02U S0V 111.3(12) . . ?
C02N C02U S0V 109.1(11) . . ?
C02N C02U C02H 108.0(13) . . ?
C03L C02U S0V 110.2(12) . . ?
C03L C02U C02H 109.5(14) . . ?
C03L C02U C02N 108.7(15) . . ?
C03G C02V C021 121(3) . . ?
C02P C02W C01W 108.9(14) . . ?
C033 C02X C022 107.7(16) . . ?
C04F C02Y C04R 120.0 . . ?
C02Y C04F C04O 120.0 . . ?
C04F C04O C4 120.0 . . ?
C04B C4 C04O 120.0 . . ?
C4 C04B P1F 122.7(8) . . ?
C4 C04B C04R 120.0 . . ?
C04R C04B P1F 117.3(8) . . ?
C04B C04R C02Y 120.0 . . ?
C02E C02Z C03S 106.0(17) . . ?
C03F C02Z C02E 111.1(18) . . ?
C03F C02Z C03S 108.9(16) . . ?
C050 C031 C04U 109(2) . . ?
C02J C032 C04I 110.3(18) . . ?
C02X C033 C03D 108.0(18) . . ?
C036 C033 C02X 107(2) . . ?
C036 C033 C03D 114(2) . . ?
C03Z C034 C043 109.5(18) . . ?
C03Z C034 C04Y 109.8(19) . . ?
C04Y C034 C043 106.4(19) . . ?
C033 C036 C03I 112(2) . . ?
C02J C037 C053 111.1(16) . . ?
C89 C038 P17 119.1(10) . . ?
C89 C038 C03X 120.0 . . ?
C03X C038 P17 120.6(10) . . ?
C038 C89 C75 120.0 . . ?
C71 C75 C89 120.0 . . ?
C75 C71 C46 120.0 . . ?
C71 C46 C03X 120.0 . . ?
C46 C03X C038 120.0 . . ?
C03U C039 C3 113(2) . . ?
C01O C03B C02Q 113.9(17) . . ?
C01O C03B C03C 105.1(18) . . ?
C02Q C03B C03C 112.9(19) . . ?
C03B C03C C21 106.8(18) . . ?
C02L C03D C033 108.5(17) . . ?
C03Y C03E C024 122(2) . . ?
C01W C03F C02Z 111.2(17) . . ?
C02V C03G C025 124(2) . . ?
C050 C03H C67 112(3) . . ?
C01T C03I C04A 106.6(18) . . ?
C036 C03I C01T 112.1(19) . . ?
C036 C03I C04A 105.2(18) . . ?
C044 C03J C1 105.3(13) . . ?
C044 C03J C55 107.6(14) . . ?
C1 C03J C55 111.2(9) . . ?
C02U C03L C02R 110.0(17) . . ?
C03V C03M S19 106.4(12) . . ?
C03V C03M C04N 110.9(17) . . ?
C03V C03M C05B 102.7(17) . . ?
C04N C03M S19 112.6(12) . . ?
C04N C03M C05B 113.7(18) . . ?
C05B C03M S19 109.8(12) . . ?
C02F C03O C04M 109.3(13) . . ?
C02F C03O C55 107.0(13) . . ?
C55 C03O C04M 111.1(9) . . ?
C01W C03P C027 109.4(19) . . ?
C19 C03Q S1I 109.2(6) . . ?
C9AA C03Q S1I 119.6(6) . . ?
C9AA C03Q C19 110.63(11) . . ?
C153 C03Q S1I 100.7(6) . . ?
C153 C03Q C19 104.1(6) . . ?
C153 C03Q C9AA 111.3(5) . . ?
C023 C03R C05D 109.0(17) . . ?
C02P C03S C02Z 110.0(15) . . ?
C054 C03T C3 107(2) . . ?
C039 C03U C04Q 109(2) . . ?
C039 C03U C04W 111(2) . . ?
C04Q C03U C04W 103(2) . . ?
C03M C03V C1AA 107(2) . . ?
C03E C03Y C01V 121(2) . . ?
C04I C03Z C034 111.4(18) . . ?
C02I C040 C5 109.9(5) . . ?
Cl1L C041 Cl1M 109.8(17) . . ?
C02J C043 C034 108.5(16) . . ?
C03J C044 C046 113.0(12) . . ?
C04L C045 C020 107.9(14) . . ?
C02O C046 C04M 107.9(8) . . ?
C044 C046 C02O 109.2(9) . . ?
C044 C046 C04M 108.6(9) . . ?
C43 C047 C103 120.0 . . ?
C047 C43 P1J 115.7(10) . . ?
C04T C43 P1J 124.2(10) . . ?
C04T C43 C047 120.0 . . ?
C43 C04T C64 120.0 . . ?
C26 C64 C04T 120.0 . . ?
C64 C26 C103 120.0 . . ?
C26 C103 C047 120.0 . . ?
C02C C048 C054 105.8(18) . . ?
C022 C04A C03I 108.7(17) . . ?
C04I C04C C053 112.7(19) . . ?
C029 C04D C02G 110.2(16) . . ?
C052 C04E S1D 110.6(12) . . ?
C052 C04E C0AA 111.3(9) . . ?
C052 C04E C162 106.3(14) . . ?
C0AA C04E S1D 111.7(11) . . ?
C0AA C04E C162 110.7(8) . . ?
C162 C04E S1D 106.1(10) . . ?
C03Z C04I C032 103.3(18) . . ?
C04C C04I C032 110(2) . . ?
C04C C04I C03Z 111.3(19) . . ?
C02Q C04J C02S 106.9(17) . . ?
C02Q C04J C33 110(2) . . ?
C33 C04J C02S 111.3(19) . . ?
C04L C04K C05D 109.0(18) . . ?
C04K C04L C045 111.6(17) . . ?
C04Z C04L C045 110.2(16) . . ?
C04Z C04L C04K 108.5(17) . . ?
C03O C04M C046 109.2(8) . . ?
C04X C04N C03M 110(2) . . ?
C054 C04Q C03U 110(2) . . ?
C04U C04S C67 114(3) . . ?
C04S C04U C031 106(3) . . ?
C04S C04U C84 115(3) . . ?
C84 C04U C031 108(2) . . ?
C02C C04W C03U 109.4(18) . . ?
C11 C04X C04N 113(3) . . ?
C2AA C04X C04N 114(3) . . ?
C2AA C04X C11 98(3) . . ?
C053 C04Y C034 114(2) . . ?
C04L C04Z C023 109.9(15) . . ?
C031 C050 S1E 107.1(14) . . ?
C031 C050 C8 106.9(19) . . ?
C03H C050 S1E 111.6(16) . . ?
C03H C050 C031 109.3(19) . . ?
C03H C050 C8 112(2) . . ?
C8 C050 S1E 110.1(13) . . ?
C22 C051 C0BA 110.64(11) . . ?
C04E C052 C82 110.8(9) . . ?
C04C C053 C037 105.6(18) . . ?
C04Y C053 C037 109.2(19) . . ?
C04Y C053 C04C 107(2) . . ?
C03T C054 C048 112(2) . . ?
C03T C054 C04Q 114(3) . . ?
C04Q C054 C048 107(2) . . ?
C9AA C055 C1BA 103.9(2) . . ?
C181 C055 C9AA 111.09(11) . . ?
C181 C055 C1BA 110.94(11) . . ?
C67 C056 C13 118(3) . . ?
C03W C057 C03A 120.0 . . ?
C042 C03W C057 120.0 . . ?
C03W C042 C035 120.0 . . ?
C02D C035 C042 120.0 . . ?
C035 C02D P14 122.3(7) . . ?
C03A C02D P14 117.4(7) . . ?
C03A C02D C035 120.0 . . ?
C02D C03A C057 120.0 . . ?
C05D C058 C020 109.4(15) . . ?
C76 C059 C28 120.0 . . ?
C059 C76 P1J 115.9(11) . . ?
C059 C76 C9 120.0 . . ?
C9 C76 P1J 123.6(11) . . ?
C23 C9 C76 120.0 . . ?
C6 C23 C9 120.0 . . ?
C23 C6 C28 120.0 . . ?
C6 C28 C059 120.0 . . ?
C03M C05B C7 107.4(19) . . ?
C03R C05D C04K 111(2) . . ?
C03R C05D C058 109.1(18) . . ?
C04K C05D C058 108.9(19) . . ?
C30 C21 C03C 107.1(17) . . ?
C30 C21 C33 110.1(19) . . ?
C33 C21 C03C 113(2) . . ?
C21 C30 C01U 109.3(15) . . ?
C21 C33 C04J 108(2) . . ?
C03J C1 C01Y 110.9(9) . . ?
C37 C34 C0AA 106.7(10) . . ?
C132 C34 C37 109.4(9) . . ?
C132 C34 C0AA 110.5(9) . . ?
C03O C55 C03J 111.6(9) . . ?
C34 C37 C82 111.4(6) . . ?
C37 C82 C052 111.7(11) . . ?
C37 C82 C92 110.5(8) . . ?
C92 C82 C052 103.3(15) . . ?
C82 C92 C6BA 110.5(5) . . ?
P1F C2 P1J 112.7(9) . . ?
C04E C0AA C34 109.9(6) . . ?
C050 C8 C13 108(2) . . ?
C056 C13 C8 104(3) . . ?
C84 C13 C056 111(3) . . ?
C84 C13 C8 105(3) . . ?
C04S C67 C03H 110(3) . . ?
C04S C67 C056 105(3) . . ?
C056 C67 C03H 104(3) . . ?
C7 C3AA C1AA 99(3) . . ?
C3AA C7 C05B 110(2) . . ?
C3AA C7 C11 106(3) . . ?
C11 C7 C05B 116(3) . . ?
C04X C11 C7 113(3) . . ?
C3AA C1AA C03V 107(2) . . ?
C2AA C1AA C03V 115(2) . . ?
C2AA C1AA C3AA 120(3) . . ?
C04X C2AA C1AA 104(3) . . ?
C13 C84 C04U 112(3) . . ?
C4AA C5 C040 109.4(6) . . ?
C4AA C5 C5AA 109.6(7) . . ?
C5AA C5 C040 108.3(7) . . ?
C51 C4AA C5 110.1(5) . . ?
C7AA C5AA C5 110.2(5) . . ?
C02I C6AA C7AA 111.5(10) . . ?
C51 C17 C7AA 110.7(6) . . ?
C5AA C7AA C6AA 106.4(13) . . ?
C5AA C7AA C17 110.9(8) . . ?
C17 C7AA C6AA 108.6(12) . . ?
C51 C36 C02I 108.5(6) . . ?
C4AA C51 C36 109.3(7) . . ?
C17 C51 C4AA 109.5(8) . . ?
C17 C51 C36 109.4(8) . . ?
C3 C8AA C02C 110.6(19) . . ?
C039 C3 C03T 108(2) . . ?
C8AA C3 C039 108(2) . . ?
C8AA C3 C03T 110(2) . . ?
C03Q C19 C0BA 110.24(10) . . ?
C1BA C22 C051 110.74(11) . . ?
C153 C22 C051 105.8(6) . . ?
C153 C22 C1BA 109.2(5) . . ?
C055 C9AA C03Q 110.97(12) . . ?
C051 C0BA C19 110.34(11) . . ?
C181 C0BA C051 105.8(2) . . ?
C181 C0BA C19 110.47(11) . . ?
C055 C1BA C22 110.78(11) . . ?
C100 C2BA C122 109.0(9) . . ?
C100 C2BA C4BA 109.8(7) . . ?
C4BA C2BA C122 110.1(9) . . ?
C122 C70 S1G 113.5(9) . . ?
C160 C70 S1G 109.4(7) . . ?
C160 C70 C122 109.7(8) . . ?
C161 C70 S1G 105.2(7) . . ?
C161 C70 C122 109.5(8) . . ?
C161 C70 C160 109.5(6) . . ?
C2BA C100 C5BA 109.9(5) . . ?
C2BA C122 C70 108.3(7) . . ?
C3BA C128 C161 109.9(7) . . ?
C3BA C128 C4BA 109.4(7) . . ?
C4BA C128 C161 108.6(7) . . ?
C70 C160 C5BA 109.5(5) . . ?
C70 C161 C128 110.0(5) . . ?
C128 C3BA C5BA 109.9(5) . . ?
C100 C5BA C160 108.2(7) . . ?
C3BA C5BA C100 110.0(7) . . ?
C3BA C5BA C160 109.2(6) . . ?
C2BA C4BA C128 109.8(5) . . ?
C92 C6BA C162 108.8(8) . . ?
C132 C6BA C92 109.4(7) . . ?
C132 C6BA C162 109.0(8) . . ?
C34 C132 C6BA 110.8(6) . . ?
C04E C162 C6BA 108.6(7) . . ?
C03Q C153 C22 111.20(12) . . ?
C055 C181 C0BA 110.97(10) . . ?

_platon_squeeze_details          ?
loop_
_platon_squeeze_void_nr
_platon_squeeze_void_average_x
_platon_squeeze_void_average_y
_platon_squeeze_void_average_z
_platon_squeeze_void_volume
_platon_squeeze_void_count_electrons
_platon_squeeze_void_content
1 0.207 -0.026 0.256 374 98 ' '
2 0.717 0.007 0.938 191 38 ' '
3 0.754 0.105 0.543 209 57 ' '
4 0.793 0.474 0.744 374 98 ' '
5 0.991 0.318 0.515 9 0 ' '
6 0.283 0.507 1.062 190 38 ' '
7 0.493 0.424 0.672 6 1 ' '
8 0.246 0.605 0.458 208 57 ' '
9 0.009 0.818 0.485 8 0 ' '
10 0.507 0.924 0.328 6 1 ' '

_platon_squeeze_void_probe_radius 1.20
_olex2_submission_special_instructions 'No special instructions were received'
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_op_sq
_database_code_depnum_ccdc_archive 'CCDC 2391029'
loop_
_audit_author_name
_audit_author_address
'shan jin'
;An Hui University
China
;
_audit_update_record             
;
2024-10-15 deposited with the CCDC.	2025-02-04 downloaded from the CCDC.
;
_audit_creation_date             2024-10-14
_audit_creation_method           
;
Olex2 1.2
(compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         
'C180 H206 Ag8 Cl8 Cu12 P8 S8, 2(F6 Sb), 5.6(C H2 Cl2), 2(C4 H10 O)'
_chemical_formula_sum            
'C193.60 H237.20 Ag8 Cl19.20 Cu12 F12 O2 P8 S8 Sb2'
_chemical_formula_weight         5878.04
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag 0.1306 4.2820 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu -1.9646 0.5888 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0727 0.0534 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.0562 5.8946 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      orthorhombic
_space_group_IT_number           52
_space_group_name_H-M_alt        'P n n a'
_space_group_name_Hall           '-P 2a 2bc'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, -y, z'
'-x+1/2, y+1/2, -z+1/2'
'x, -y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, y, -z'
'x-1/2, -y-1/2, z-1/2'
'-x, y-1/2, z-1/2'

_cell_length_a                   28.677(2)
_cell_length_b                   27.162(2)
_cell_length_c                   27.948(2)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_volume                     21770(3)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    10168
_cell_measurement_temperature    120(2)
_cell_measurement_theta_max      30.00
_cell_measurement_theta_min      5.87
_shelx_estimated_absorpt_T_max   ?
_shelx_estimated_absorpt_T_min   ?
_exptl_absorpt_coefficient_mu    12.696
_exptl_absorpt_correction_T_max  ?
_exptl_absorpt_correction_T_min  ?
_exptl_absorpt_correction_type   ?
_exptl_absorpt_process_details   ?
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            ?
_exptl_crystal_density_diffrn    1.793
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             11693
_exptl_crystal_size_max          ?
_exptl_crystal_size_mid          ?
_exptl_crystal_size_min          ?
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0636
_diffrn_reflns_av_unetI/netI     0.0435
_diffrn_reflns_Laue_measured_fraction_full 0.995
_diffrn_reflns_Laue_measured_fraction_max 0.981
_diffrn_reflns_limit_h_max       23
_diffrn_reflns_limit_h_min       -34
_diffrn_reflns_limit_k_max       32
_diffrn_reflns_limit_k_min       -24
_diffrn_reflns_limit_l_max       30
_diffrn_reflns_limit_l_min       -34
_diffrn_reflns_number            127801
_diffrn_reflns_point_group_measured_fraction_full 0.995
_diffrn_reflns_point_group_measured_fraction_max 0.981
_diffrn_reflns_theta_full        67.686
_diffrn_reflns_theta_max         70.239
_diffrn_reflns_theta_min         5.840
_diffrn_ambient_temperature      120(2)
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.995
_diffrn_measured_fraction_theta_max 0.981
_diffrn_measurement_device_type  stoe
_diffrn_measurement_method       ?
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54186
_diffrn_source                   ?
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                15323
_reflns_number_total             20348
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       ?
_computing_data_collection       ?
_computing_data_reduction        ?
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    ?
_refine_diff_density_max         4.207
_refine_diff_density_min         -1.308
_refine_diff_density_rms         0.164
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.080
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1220
_refine_ls_number_reflns         20348
_refine_ls_number_restraints     664
_refine_ls_R_factor_all          0.0858
_refine_ls_R_factor_gt           0.0700
_refine_ls_restrained_S_all      1.112
_refine_ls_shift/su_max          0.003
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.1431P)²+24.4617P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2052
_refine_ls_wR_factor_ref         0.2196
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups, All C(H,H) groups, All C(H,H,H,H) groups
 At 1.5 times of:
  All C(H,H,H) groups
2. Restrained distances
 O03F-C03M = C03N-C03M = C15-C03J = O03F-C03J
 1.52 with sigma of 0.01
 C03N-O03F
 2.54 with sigma of 0.01
 C03M-C03J
 2.54 with sigma of 0.01
 O03F-C15
 2.54 with sigma of 0.01
 Cl3A-C2 = Cl2A-C2
 1.75 with sigma of 0.01
 Cl2A-Cl3A
 2.86 with sigma of 0.01
3. Rigid bond restraints
 F0A, F7, Sb8, F4A
 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01
4. Uiso/Uaniso restraints and constraints
Cl2A \\sim C2 \\sim Cl3A: within 3.8A with sigma of 0.01 and sigma for terminal
atoms of 0.02
F7 \\sim Sb8 \\sim F4A \\sim F0A \\sim F4A \\sim F7 \\sim F0A: within 3.8A with
sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(C00V) \\sim Ueq, Uanis(C00X) \\sim Ueq, Uanis(C00Y) \\sim Ueq,
Uanis(C00Z) \\sim Ueq, Uanis(C010) \\sim Ueq, Uanis(C011) \\sim Ueq,
Uanis(C012) \\sim Ueq, Uanis(C013) \\sim Ueq, Uanis(C015) \\sim Ueq,
Uanis(C016) \\sim Ueq, Uanis(C017) \\sim Ueq, Uanis(C018) \\sim Ueq,
Uanis(C019) \\sim Ueq, Uanis(C01A) \\sim Ueq, Uanis(C01B) \\sim Ueq,
Uanis(C01C) \\sim Ueq, Uanis(C01D) \\sim Ueq, Uanis(C01E) \\sim Ueq,
Uanis(C01F) \\sim Ueq, Uanis(C01G) \\sim Ueq, Uanis(C01H) \\sim Ueq,
Uanis(C01I) \\sim Ueq, Uanis(C01J) \\sim Ueq, Uanis(C01L) \\sim Ueq,
Uanis(C01M) \\sim Ueq, Uanis(C01N) \\sim Ueq, Uanis(C01O) \\sim Ueq,
Uanis(C01P) \\sim Ueq, Uanis(C01Q) \\sim Ueq, Uanis(C01R) \\sim Ueq,
Uanis(C01S) \\sim Ueq, Uanis(C01T) \\sim Ueq, Uanis(C01U) \\sim Ueq,
Uanis(C01V) \\sim Ueq, Uanis(C01W) \\sim Ueq, Uanis(C01X) \\sim Ueq,
Uanis(C01Y) \\sim Ueq, Uanis(C01Z) \\sim Ueq, Uanis(C020) \\sim Ueq,
Uanis(C021) \\sim Ueq, Uanis(C022) \\sim Ueq, Uanis(C023) \\sim Ueq,
Uanis(C024) \\sim Ueq, Uanis(C025) \\sim Ueq, Uanis(C026) \\sim Ueq,
Uanis(C027) \\sim Ueq, Uanis(C028) \\sim Ueq, Uanis(C029) \\sim Ueq,
Uanis(C02A) \\sim Ueq, Uanis(C02B) \\sim Ueq, Uanis(C02C) \\sim Ueq,
Uanis(C02D) \\sim Ueq, Uanis(C02E) \\sim Ueq, Uanis(C02F) \\sim Ueq,
Uanis(C02G) \\sim Ueq, Uanis(C02H) \\sim Ueq, Uanis(C02I) \\sim Ueq,
Uanis(C02J) \\sim Ueq, Uanis(C02K) \\sim Ueq, Uanis(C02M) \\sim Ueq,
Uanis(C02N) \\sim Ueq, Uanis(C02O) \\sim Ueq, Uanis(C02P) \\sim Ueq,
Uanis(C02Q) \\sim Ueq, Uanis(C02S) \\sim Ueq, Uanis(C02T) \\sim Ueq,
Uanis(C02U) \\sim Ueq, Uanis(C02V) \\sim Ueq, Uanis(C02W) \\sim Ueq,
Uanis(C02X) \\sim Ueq, Uanis(C02Y) \\sim Ueq, Uanis(C02Z) \\sim Ueq,
Uanis(C030) \\sim Ueq, Uanis(C031) \\sim Ueq, Uanis(C032) \\sim Ueq,
Uanis(C033) \\sim Ueq, Uanis(C034) \\sim Ueq, Uanis(C035) \\sim Ueq,
Uanis(C036) \\sim Ueq, Uanis(C037) \\sim Ueq, Uanis(C038) \\sim Ueq,
Uanis(C039) \\sim Ueq, Uanis(C03A) \\sim Ueq, Uanis(C03B) \\sim Ueq,
Uanis(C03C) \\sim Ueq, Uanis(C03D) \\sim Ueq, Uanis(C03E) \\sim Ueq,
Uanis(C03G) \\sim Ueq, Uanis(C03H) \\sim Ueq, Uanis(C03I) \\sim Ueq,
Uanis(C03J) \\sim Ueq, Uanis(C03K) \\sim Ueq, Uanis(C03L) \\sim Ueq,
Uanis(C03M) \\sim Ueq, Uanis(C03N) \\sim Ueq, Uanis(C15) \\sim Ueq: with sigma
of 0.01 and sigma for terminal atoms of 0.02
Uanis(Cl2A) \\sim Ueq, Uanis(C2) \\sim Ueq, Uanis(Cl3A) \\sim Ueq: with sigma
of 0.01 and sigma for terminal atoms of 0.02
5. Others
 Fixed Sof: C03I(0.8) H03V(0.4) H03W(0.4) H03X(0.4) H03Y(0.4) Cl4(0.4)
 Cl13(0.4) Cl14(0.4) Cl17(0.4)
6.a Ternary CH refined with riding coordinates:
 C011(H011), C015(H015), C01H(H01N), C01Q(H01U), C025(H025), C02C(H02G),
 C02G(H02M), C02N(H02V), C02X(H7AA), C030(H030), C033(H033), C03H(H03L)
6.b Secondary CH2 refined with riding coordinates:
 C00Z(H00A,H00B), C012(H01A,H01B), C017(H01C,H01D), C019(H01E,H01F), C01B(H01G,
 H01H), C01D(H01J,H01K), C01I(H01O,H01P), C01M(H01R,H01S), C01R(H01V,H01W),
 C01T(H01Y,H), C01X(H1AA,HA), C01Z(H3AA,HB), C020(H02A,H02B), C026(H02C,H02D),
 C02E(H02I,H02J), C02F(H02K,H02L), C02I(H02O,H02P), C02K(H02R,H02S), C02M(H02T,
 H02U), C02O(H02W,H02X), C02P(H02Y,HC), C02T(H4AA,HD), C02W(H0BA,HE), C032(H03A,
 H03B), C034(H03C,H03D), C03A(H03E,H03F), C03I(H03V,H03W), C03I(H03X,H03Y),
 C03J(H03O,H03P), C03M(H03Q,H03R), C2(H2A,H2B)
6.c Aromatic/amide H refined with riding coordinates:
 C01C(H01I), C01F(H01L), C01G(H01M), C01J(H01Q), C01P(H01T), C01S(H01X),
 C01U(H01Z), C01V(H01), C01W(H0AA), C01Y(H2AA), C021(H021), C022(H022),
 C023(H023), C024(H024), C027(H027), C028(H028), C029(H029), C02A(H02E),
 C02B(H02F), C02D(H02H), C02H(H02N), C02J(H02Q), C02Q(H02Z), C02S(H02),
 C02U(H5AA), C02V(H6AA), C02Y(H8AA), C02Z(H9AA), C031(H031), C035(H035),
 C036(H036), C037(H037), C038(H038), C039(H039), C03B(H03G), C03C(H03H),
 C03D(H03I), C03E(H03J), C03G(H03K), C03K(H03M), C03L(H03N)
6.d Idealised Me refined as rotating group:
 C03N(H03S,H03T,H03U), C15(H15A,H15B,H15C)
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag01 Ag 0.47583(2) 0.29912(2) 0.76655(2) 0.04571(15) Uani 1 1 d . . . . .
Ag02 Ag 0.54349(2) 0.26538(2) 0.70201(2) 0.04501(15) Uani 1 1 d . . . . .
Ag03 Ag 0.44093(2) 0.28266(2) 0.65759(2) 0.05325(17) Uani 1 1 d . . . . .
Sb04 Sb 0.250000 0.500000 0.65323(4) 0.0696(3) Uani 1 2 d S T P . .
Ag05 Ag 0.57898(2) 0.34403(3) 0.77448(3) 0.05885(18) Uani 1 1 d . . . . .
Cu07 Cu 0.63897(5) 0.250000 0.750000 0.0417(3) Uani 1 2 d S T P . .
Cu08 Cu 0.38337(5) 0.250000 0.750000 0.0430(3) Uani 1 2 d S T P . .
Cu09 Cu 0.38462(4) 0.35438(4) 0.82679(4) 0.0463(3) Uani 1 1 d . . . . .
Cu0A Cu 0.63271(4) 0.24844(5) 0.62393(4) 0.0515(3) Uani 1 1 d . . . . .
Cu0B Cu 0.45721(4) 0.42117(4) 0.78478(5) 0.0514(3) Uani 1 1 d . . . . .
Cu0C Cu 0.56124(4) 0.31888(5) 0.59233(4) 0.0521(3) Uani 1 1 d . . . . .
Cu0D Cu 0.50874(4) 0.37269(4) 0.69241(5) 0.0561(3) Uani 1 1 d . . . . .
Cl00 Cl 0.41020(6) 0.36232(7) 0.73833(7) 0.0445(4) Uani 1 1 d . . . . .
Cl1 Cl 0.60945(6) 0.32616(7) 0.66806(6) 0.0437(4) Uani 1 1 d . . . . .
Cl2 Cl 0.46705(6) 0.35435(7) 0.84439(7) 0.0465(4) Uani 1 1 d . . . . .
S00H S 0.37589(6) 0.27038(7) 0.82543(7) 0.0463(4) Uani 1 1 d . . . . .
Cl3 Cl 0.55050(7) 0.23289(7) 0.61318(7) 0.0488(4) Uani 1 1 d . . . . .
S00J S 0.64363(7) 0.19933(8) 0.68856(8) 0.0505(4) Uani 1 1 d . . . . .
S00K S 0.49122(7) 0.34312(8) 0.62193(8) 0.0527(5) Uani 1 1 d . . . . .
P00L P 0.33946(7) 0.41725(7) 0.84509(7) 0.0454(4) Uani 1 1 d . . . . .
P00M P 0.41571(7) 0.48564(7) 0.80647(8) 0.0469(4) Uani 1 1 d . . . . .
S00N S 0.53082(7) 0.41407(7) 0.75515(9) 0.0531(5) Uani 1 1 d . . . . .
P00O P 0.59578(7) 0.33185(8) 0.52371(7) 0.0493(4) Uani 1 1 d . . . . .
P00P P 0.67414(7) 0.26553(8) 0.56020(8) 0.0502(5) Uani 1 1 d . . . . .
Cl1A Cl 0.59384(18) 0.58096(19) 0.88519(17) 0.1323(15) Uani 1 1 d . . . . .
Cl5 Cl 0.51372(18) 0.6438(2) 0.8862(3) 0.155(2) Uani 1 1 d . . . . .
F00U F 0.2921(3) 0.5513(3) 0.6540(3) 0.103(2) Uani 1 1 d . . . . .
C00V C 0.4576(3) 0.3901(3) 0.5894(3) 0.0504(18) Uani 1 1 d . U . . .
C00X C 0.4171(3) 0.5396(3) 0.7673(3) 0.0518(18) Uani 1 1 d . U . . .
C00Y C 0.3194(3) 0.2426(3) 0.8443(3) 0.0438(16) Uani 1 1 d . U . . .
C00Z C 0.3532(3) 0.4729(3) 0.8109(3) 0.0488(17) Uani 1 1 d . U . . .
H00A H 0.340262 0.469439 0.778188 0.059 Uiso 1 1 calc R . . . .
H00B H 0.337624 0.501389 0.826153 0.059 Uiso 1 1 calc R . . . .
C010 C 0.5556(3) 0.3310(4) 0.4728(3) 0.060(2) Uani 1 1 d . U . . .
C011 C 0.2332(3) 0.2523(3) 0.8409(3) 0.055(2) Uani 1 1 d . U . . .
H011 H 0.206979 0.272144 0.827312 0.067 Uiso 1 1 calc R . . . .
C012 C 0.4903(3) 0.4318(3) 0.5741(4) 0.059(2) Uani 1 1 d . U . . .
H01A H 0.505093 0.446668 0.602615 0.071 Uiso 1 1 calc R . . . .
H01B H 0.515144 0.418624 0.553132 0.071 Uiso 1 1 calc R . . . .
C013 C 0.2774(3) 0.4086(3) 0.8331(3) 0.0495(18) Uani 1 1 d . U . . .
F014 F 0.2807(3) 0.4676(3) 0.6032(4) 0.141(4) Uani 1 1 d . . . . .
C015 C 0.2685(3) 0.1684(3) 0.8436(3) 0.0537(19) Uani 1 1 d . U . . .
H015 H 0.265383 0.133768 0.831984 0.064 Uiso 1 1 calc R . . . .
C016 C 0.5627(3) 0.4687(3) 0.7325(3) 0.0480(17) Uani 1 1 d . U . . .
C017 C 0.2799(3) 0.2737(3) 0.8241(3) 0.0515(18) Uani 1 1 d . U . . .
H01C H 0.281252 0.273630 0.788729 0.062 Uiso 1 1 calc R . . . .
H01D H 0.282943 0.308095 0.835334 0.062 Uiso 1 1 calc R . . . .
C018 C 0.6991(3) 0.1649(3) 0.6933(3) 0.0503(18) Uani 1 1 d . U . . .
C019 C 0.2291(3) 0.1993(4) 0.8240(4) 0.065(2) Uani 1 1 d . U . . .
H01E H 0.198915 0.185508 0.834810 0.077 Uiso 1 1 calc R . . . .
H01F H 0.229707 0.198383 0.788633 0.077 Uiso 1 1 calc R . . . .
C01A C 0.3413(3) 0.4383(3) 0.9066(3) 0.062(2) Uani 1 1 d . U . . .
C01B C 0.3153(3) 0.1897(3) 0.8277(3) 0.0519(18) Uani 1 1 d . U . . .
H01G H 0.341011 0.169963 0.841348 0.062 Uiso 1 1 calc R . . . .
H01H H 0.317685 0.188335 0.792342 0.062 Uiso 1 1 calc R . . . .
C01C C 0.7381(3) 0.3371(3) 0.5281(3) 0.060(2) Uani 1 1 d . U . . .
H01I H 0.729693 0.327639 0.496496 0.072 Uiso 1 1 calc R . . . .
C01D C 0.5973(3) 0.4543(4) 0.6931(4) 0.062(2) Uani 1 1 d . U . . .
H01J H 0.620599 0.430840 0.705791 0.074 Uiso 1 1 calc R . . . .
H01K H 0.580594 0.438325 0.666257 0.074 Uiso 1 1 calc R . . . .
C01E C 0.4330(3) 0.5083(3) 0.8644(3) 0.0552(19) Uani 1 1 d . U . . .
C01F C 0.2609(3) 0.4090(3) 0.7860(4) 0.060(2) Uani 1 1 d . U . . .
H01L H 0.281655 0.417087 0.760749 0.072 Uiso 1 1 calc R . . . .
C01G C 0.7714(3) 0.3725(4) 0.5350(4) 0.071(3) Uani 1 1 d . U . . .
H01M H 0.786837 0.386272 0.508034 0.085 Uiso 1 1 calc R . . . .
C01H C 0.4620(3) 0.4707(4) 0.5472(4) 0.068(2) Uani 1 1 d . U . . .
H01N H 0.483639 0.497676 0.537247 0.082 Uiso 1 1 calc R . . . .
C01I C 0.2310(3) 0.2534(4) 0.8950(4) 0.066(2) Uani 1 1 d . U . . .
H01O H 0.233647 0.287809 0.906297 0.079 Uiso 1 1 calc R . . . .
H01P H 0.200592 0.240209 0.905818 0.079 Uiso 1 1 calc R . . . .
C01J C 0.4427(4) 0.5814(4) 0.7794(4) 0.069(2) Uani 1 1 d . U . . .
H01Q H 0.457137 0.583092 0.809916 0.083 Uiso 1 1 calc R . . . .
C01L C 0.7163(3) 0.3147(3) 0.5676(3) 0.0528(19) Uani 1 1 d . U . . .
C01M C 0.3175(3) 0.2446(4) 0.9002(3) 0.060(2) Uani 1 1 d . U . . .
H01R H 0.343252 0.225005 0.913993 0.072 Uiso 1 1 calc R . . . .
H01S H 0.320531 0.279013 0.911357 0.072 Uiso 1 1 calc R . . . .
C01N C 0.7086(3) 0.2144(3) 0.5346(3) 0.060(2) Uani 1 1 d . U . . .
C01O C 0.6313(3) 0.3870(3) 0.5150(3) 0.0546(19) Uani 1 1 d . U . . .
C01P C 0.2155(3) 0.3981(4) 0.7757(4) 0.069(3) Uani 1 1 d . U . . .
H01T H 0.204719 0.399515 0.743584 0.083 Uiso 1 1 calc R . . . .
C01Q C 0.6217(4) 0.5011(4) 0.6754(4) 0.071(3) Uani 1 1 d . U . . .
H01U H 0.644083 0.492152 0.649363 0.085 Uiso 1 1 calc R . . . .
C01R C 0.4205(3) 0.4121(4) 0.6229(4) 0.064(2) Uani 1 1 d . U . . .
H01V H 0.435712 0.427347 0.650979 0.077 Uiso 1 1 calc R . . . .
H01W H 0.399421 0.385722 0.634435 0.077 Uiso 1 1 calc R . . . .
C01S C 0.1850(3) 0.3849(3) 0.8122(4) 0.067(2) Uani 1 1 d . U . . .
H01X H 0.153716 0.376051 0.804889 0.081 Uiso 1 1 calc R . . . .
C01T C 0.5271(3) 0.5051(4) 0.7126(4) 0.062(2) Uani 1 1 d . U . . .
H01Y H 0.504305 0.514039 0.737733 0.074 Uiso 1 1 calc R . . . .
H H 0.509969 0.490032 0.685559 0.074 Uiso 1 1 calc R . . . .
C01U C 0.7277(4) 0.3288(4) 0.6131(4) 0.066(2) Uani 1 1 d . U . . .
H01Z H 0.713806 0.313433 0.640044 0.079 Uiso 1 1 calc R . . . .
C01V C 0.2462(3) 0.3963(3) 0.8688(3) 0.057(2) Uani 1 1 d . U . . .
H01 H 0.256398 0.395685 0.901128 0.068 Uiso 1 1 calc R . . . .
C01W C 0.3939(3) 0.5376(4) 0.7247(4) 0.066(2) Uani 1 1 d . U . . .
H0AA H 0.375677 0.509609 0.716641 0.079 Uiso 1 1 calc R . . . .
C01X C 0.6367(3) 0.2824(3) 0.5097(3) 0.060(2) Uani 1 1 d . U . . .
H1AA H 0.656593 0.292836 0.482551 0.072 Uiso 1 1 calc R . . . .
HA H 0.618922 0.253023 0.499373 0.072 Uiso 1 1 calc R . . . .
C01Y C 0.1997(3) 0.3847(3) 0.8583(4) 0.066(2) Uani 1 1 d . U . . .
H2AA H 0.178657 0.376633 0.883295 0.079 Uiso 1 1 calc R . . . .
C01Z C 0.5899(3) 0.4922(4) 0.7738(3) 0.061(2) Uani 1 1 d . U . . .
H3AA H 0.568077 0.501650 0.799664 0.073 Uiso 1 1 calc R . . . .
HB H 0.612358 0.468062 0.787013 0.073 Uiso 1 1 calc R . . . .
C020 C 0.2663(4) 0.1697(4) 0.8985(4) 0.064(2) Uani 1 1 d . U . . .
H02A H 0.236498 0.155112 0.909516 0.077 Uiso 1 1 calc R . . . .
H02B H 0.292179 0.150062 0.912000 0.077 Uiso 1 1 calc R . . . .
C021 C 0.6385(3) 0.4179(3) 0.5530(4) 0.064(2) Uani 1 1 d . U . . .
H021 H 0.624094 0.411923 0.582997 0.077 Uiso 1 1 calc R . . . .
C022 C 0.5457(3) 0.3724(4) 0.4462(4) 0.066(2) Uani 1 1 d . U . . .
H022 H 0.561580 0.402282 0.453057 0.079 Uiso 1 1 calc R . . . .
C023 C 0.4087(4) 0.5432(4) 0.8897(4) 0.069(2) Uani 1 1 d . U . . .
H023 H 0.381472 0.557156 0.875843 0.083 Uiso 1 1 calc R . . . .
C024 C 0.7564(4) 0.2136(4) 0.5355(4) 0.067(2) Uani 1 1 d . U . . .
H024 H 0.773546 0.240700 0.547822 0.081 Uiso 1 1 calc R . . . .
C025 C 0.2699(4) 0.2231(4) 0.9158(4) 0.072(3) Uani 1 1 d . U . . .
H025 H 0.267683 0.223805 0.951540 0.086 Uiso 1 1 calc R . . . .
C026 C 0.7031(3) 0.1384(4) 0.7411(4) 0.063(2) Uani 1 1 d . U . . .
H02C H 0.676677 0.115230 0.744956 0.075 Uiso 1 1 calc R . . . .
H02D H 0.701847 0.162574 0.767571 0.075 Uiso 1 1 calc R . . . .
C027 C 0.6521(3) 0.3965(4) 0.4721(4) 0.070(3) Uani 1 1 d . U . . .
H027 H 0.646791 0.375441 0.445498 0.084 Uiso 1 1 calc R . . . .
C028 C 0.4476(4) 0.6203(4) 0.7481(5) 0.083(3) Uani 1 1 d . U . . .
H028 H 0.466702 0.647767 0.755915 0.100 Uiso 1 1 calc R . . . .
C029 C 0.5311(4) 0.2867(4) 0.4648(4) 0.077(3) Uani 1 1 d . U . . .
H029 H 0.536157 0.258318 0.483954 0.092 Uiso 1 1 calc R . . . .
C02A C 0.6897(4) 0.4654(4) 0.5031(5) 0.080(3) Uani 1 1 d . U . . .
H02E H 0.711683 0.491292 0.499409 0.096 Uiso 1 1 calc R . . . .
C02B C 0.3133(4) 0.4771(4) 0.9225(4) 0.078(3) Uani 1 1 d . U . . .
H02F H 0.292461 0.492927 0.901034 0.094 Uiso 1 1 calc R . . . .
C02C C 0.5533(4) 0.5516(4) 0.6954(4) 0.071(3) Uani 1 1 d . U . . .
H02G H 0.530495 0.576041 0.682403 0.085 Uiso 1 1 calc R . . . .
C02D C 0.7794(4) 0.1718(5) 0.5179(4) 0.082(3) Uani 1 1 d . U . . .
H02H H 0.812485 0.171521 0.516717 0.099 Uiso 1 1 calc R . . . .
C02E C 0.4348(4) 0.3674(4) 0.5468(4) 0.073(3) Uani 1 1 d . U . . .
H02I H 0.413295 0.341002 0.557357 0.087 Uiso 1 1 calc R . . . .
H02J H 0.458812 0.352371 0.525999 0.087 Uiso 1 1 calc R . . . .
C02F C 0.6488(4) 0.5249(4) 0.7166(4) 0.073(3) Uani 1 1 d . U . . .
H02K H 0.673315 0.502113 0.728092 0.087 Uiso 1 1 calc R . . . .
H02L H 0.664049 0.555492 0.705406 0.087 Uiso 1 1 calc R . . . .
C02G C 0.3920(3) 0.4514(4) 0.5951(4) 0.069(3) Uani 1 1 d . U . . .
H02M H 0.367192 0.465286 0.616285 0.083 Uiso 1 1 calc R . . . .
C02H C 0.7831(4) 0.3887(5) 0.5799(5) 0.085(3) Uani 1 1 d . U . . .
H02N H 0.805535 0.413954 0.584303 0.102 Uiso 1 1 calc R . . . .
C02I C 0.7402(3) 0.2003(4) 0.6871(4) 0.073(3) Uani 1 1 d . U . . .
H02O H 0.739769 0.225324 0.712907 0.087 Uiso 1 1 calc R . . . .
H02P H 0.737679 0.217572 0.656039 0.087 Uiso 1 1 calc R . . . .
C02J C 0.4233(5) 0.6183(4) 0.7039(5) 0.087(3) Uani 1 1 d . U . . .
H02Q H 0.425455 0.645243 0.682297 0.104 Uiso 1 1 calc R . . . .
C02K C 0.4256(4) 0.4923(4) 0.5796(5) 0.080(3) Uani 1 1 d . U . . .
H02R H 0.408156 0.518448 0.562596 0.096 Uiso 1 1 calc R . . . .
H02S H 0.440586 0.507104 0.608085 0.096 Uiso 1 1 calc R . . . .
F02L F 0.2876(6) 0.4676(6) 0.6939(6) 0.287(12) Uani 1 1 d . . . . .
C02M C 0.3699(3) 0.4275(4) 0.5512(4) 0.071(3) Uani 1 1 d . U . . .
H02T H 0.351505 0.452381 0.533530 0.085 Uiso 1 1 calc R . . . .
H02U H 0.348447 0.400992 0.561524 0.085 Uiso 1 1 calc R . . . .
C02N C 0.7491(4) 0.1102(4) 0.7429(4) 0.069(3) Uani 1 1 d . U . . .
H02V H 0.751925 0.092873 0.774372 0.083 Uiso 1 1 calc R . . . .
C02O C 0.7883(4) 0.1460(5) 0.7373(5) 0.084(3) Uani 1 1 d . U . . .
H02W H 0.818359 0.128425 0.740574 0.101 Uiso 1 1 calc R . . . .
H02X H 0.786506 0.171038 0.763008 0.101 Uiso 1 1 calc R . . . .
C02P C 0.5877(5) 0.5369(5) 0.6566(4) 0.088(3) Uani 1 1 d . U . . .
H02Y H 0.570624 0.522218 0.629291 0.105 Uiso 1 1 calc R . . . .
HC H 0.604254 0.566548 0.644884 0.105 Uiso 1 1 calc R . . . .
C02Q C 0.6675(4) 0.4584(4) 0.5463(5) 0.083(3) Uani 1 1 d . U . . .
H02Z H 0.672002 0.481309 0.571547 0.100 Uiso 1 1 calc R . . . .
C02S C 0.5131(4) 0.3711(5) 0.4096(5) 0.088(3) Uani 1 1 d . U . . .
H02 H 0.507062 0.400024 0.391536 0.105 Uiso 1 1 calc R . . . .
C02T C 0.4415(4) 0.4475(4) 0.5024(4) 0.075(3) Uani 1 1 d . U . . .
H4AA H 0.466713 0.433659 0.482266 0.090 Uiso 1 1 calc R . . . .
HD H 0.424612 0.472646 0.483458 0.090 Uiso 1 1 calc R . . . .
C02U C 0.6805(4) 0.4361(5) 0.4675(5) 0.083(3) Uani 1 1 d . U . . .
H5AA H 0.694044 0.442845 0.437190 0.099 Uiso 1 1 calc R . . . .
C02V C 0.7609(5) 0.3668(5) 0.6187(5) 0.089(3) Uani 1 1 d . U . . .
H6AA H 0.768277 0.377759 0.650106 0.107 Uiso 1 1 calc R . . . .
C02W C 0.5737(4) 0.6402(5) 0.8784(5) 0.092(4) Uani 1 1 d . U . . .
H0BA H 0.581874 0.652261 0.846012 0.110 Uiso 1 1 calc R . . . .
HE H 0.589275 0.661860 0.902028 0.110 Uiso 1 1 calc R . . . .
C02X C 0.7862(4) 0.1711(5) 0.6891(5) 0.091(4) Uani 1 1 d . U . . .
H7AA H 0.813377 0.193882 0.685226 0.110 Uiso 1 1 calc R . . . .
C02Y C 0.3729(4) 0.4165(5) 0.9375(4) 0.082(3) Uani 1 1 d . U . . .
H8AA H 0.392673 0.390736 0.926706 0.098 Uiso 1 1 calc R . . . .
C02Z C 0.4741(4) 0.4904(4) 0.8839(4) 0.073(3) Uani 1 1 d . U . . .
H9AA H 0.491688 0.466316 0.867171 0.088 Uiso 1 1 calc R . . . .
C030 C 0.4074(4) 0.4060(4) 0.5182(4) 0.077(3) Uani 1 1 d . U . . .
H030 H 0.392621 0.390423 0.489585 0.093 Uiso 1 1 calc R . . . .
C031 C 0.4986(5) 0.2870(5) 0.4270(5) 0.093(4) Uani 1 1 d . U . . .
H031 H 0.482021 0.257616 0.419760 0.112 Uiso 1 1 calc R . . . .
C032 C 0.5799(4) 0.5741(4) 0.7373(5) 0.075(3) Uani 1 1 d . U . . .
H03A H 0.557712 0.583394 0.762916 0.091 Uiso 1 1 calc R . . . .
H03B H 0.596276 0.604189 0.726601 0.091 Uiso 1 1 calc R . . . .
C033 C 0.6155(4) 0.5366(4) 0.7569(4) 0.072(3) Uani 1 1 d . U . . .
H033 H 0.633069 0.551554 0.784140 0.086 Uiso 1 1 calc R . . . .
C034 C 0.7495(5) 0.0728(5) 0.7027(6) 0.099(4) Uani 1 1 d . U . . .
H03C H 0.722318 0.050670 0.705889 0.119 Uiso 1 1 calc R . . . .
H03D H 0.778160 0.052593 0.704891 0.119 Uiso 1 1 calc R . . . .
C035 C 0.4221(4) 0.5583(5) 0.9339(5) 0.088(3) Uani 1 1 d . U . . .
H035 H 0.403386 0.580574 0.951738 0.106 Uiso 1 1 calc R . . . .
C036 C 0.3158(5) 0.4922(5) 0.9693(5) 0.096(4) Uani 1 1 d . U . . .
H036 H 0.296120 0.518054 0.979952 0.115 Uiso 1 1 calc R . . . .
C037 C 0.3972(4) 0.5786(5) 0.6920(5) 0.085(3) Uani 1 1 d . U . . .
H037 H 0.381187 0.577769 0.662290 0.102 Uiso 1 1 calc R . . . .
C038 C 0.6828(5) 0.1737(4) 0.5185(4) 0.082(3) Uani 1 1 d . U . . .
H038 H 0.649704 0.174074 0.518751 0.098 Uiso 1 1 calc R . . . .
C039 C 0.4901(5) 0.3295(5) 0.3996(5) 0.089(3) Uani 1 1 d . U . . .
H039 H 0.468172 0.328679 0.374112 0.107 Uiso 1 1 calc R . . . .
C03A C 0.6997(5) 0.1272(5) 0.6532(4) 0.085(3) Uani 1 1 d . U . . .
H03E H 0.695515 0.143879 0.622063 0.102 Uiso 1 1 calc R . . . .
H03F H 0.673743 0.103586 0.657592 0.102 Uiso 1 1 calc R . . . .
C03B C 0.7559(5) 0.1322(5) 0.5026(5) 0.089(3) Uani 1 1 d . U . . .
H03G H 0.772302 0.103741 0.492252 0.106 Uiso 1 1 calc R . . . .
C03C C 0.4638(4) 0.5406(5) 0.9525(5) 0.091(4) Uani 1 1 d . U . . .
H03H H 0.474424 0.551846 0.982757 0.109 Uiso 1 1 calc R . . . .
C03D C 0.3447(6) 0.4718(6) 0.9995(6) 0.110(4) Uani 1 1 d . U . . .
H03I H 0.345278 0.483191 1.031686 0.132 Uiso 1 1 calc R . . . .
C03E C 0.7074(5) 0.1326(5) 0.5020(5) 0.096(4) Uani 1 1 d . U . . .
H03J H 0.690913 0.104806 0.490242 0.116 Uiso 1 1 calc R . . . .
O03F O 0.4028(4) 0.2217(5) 0.4653(4) 0.213(10) Uani 1 1 d D . . . .
C03G C 0.4894(5) 0.5075(5) 0.9276(5) 0.092(4) Uani 1 1 d . U . . .
H03K H 0.518156 0.495984 0.940299 0.110 Uiso 1 1 calc R . . . .
C03H C 0.7479(5) 0.0986(5) 0.6538(5) 0.098(4) Uani 1 1 d . U . . .
H03L H 0.748833 0.073762 0.627402 0.118 Uiso 1 1 calc R . . . .
C03I C 0.5777(6) 0.3889(6) 0.9071(6) 0.087(4) Uani 0.8 1 d . U . . .
H03V H 0.600109 0.365636 0.892453 0.105 Uiso 0.4 1 calc R . . A 1
H03W H 0.551156 0.392825 0.884724 0.105 Uiso 0.4 1 calc R . . A 1
H03X H 0.599503 0.364391 0.893440 0.105 Uiso 0.4 1 calc R . . B 2
H03Y H 0.548683 0.387223 0.887914 0.105 Uiso 0.4 1 calc R . . B 2
C03J C 0.4206(6) 0.2175(7) 0.5160(5) 0.132(6) Uani 1 1 d D U . . .
H03O H 0.394426 0.208386 0.537335 0.159 Uiso 1 1 calc R . . . .
H03P H 0.432442 0.250022 0.526508 0.159 Uiso 1 1 calc R . . . .
C03K C 0.3753(6) 0.4333(7) 0.9858(6) 0.119(5) Uani 1 1 d . U . . .
H03M H 0.396569 0.419161 1.007931 0.143 Uiso 1 1 calc R . . . .
C03L C 0.7860(5) 0.1326(6) 0.6491(6) 0.109(4) Uani 1 1 d . U . . .
H03N H 0.808407 0.131398 0.624063 0.131 Uiso 1 1 calc R . . . .
C03M C 0.3758(9) 0.2671(7) 0.4535(7) 0.186(11) Uani 1 1 d D U . . .
H03Q H 0.395207 0.296217 0.461002 0.223 Uiso 1 1 calc R . . . .
H03R H 0.347812 0.268437 0.474208 0.223 Uiso 1 1 calc R . . . .
C03N C 0.3603(7) 0.2705(8) 0.4016(7) 0.183(9) Uani 1 1 d D U . . .
H03S H 0.339875 0.242565 0.394048 0.275 Uiso 1 1 calc GR . . . .
H03T H 0.387697 0.269628 0.380663 0.275 Uiso 1 1 calc GR . . . .
H03U H 0.343273 0.301317 0.396552 0.275 Uiso 1 1 calc GR . . . .
Cl4 Cl 0.6009(5) 0.4377(7) 0.9141(9) 0.143(9) Uani 0.4 1 d . . . C 1
Cl13 Cl 0.5536(11) 0.3598(12) 0.9709(12) 0.28(2) Uani 0.4 1 d . . . C 1
Cl14 Cl 0.6012(7) 0.4450(5) 0.8985(7) 0.116(6) Uani 0.4 1 d . . . C 2
C15 C 0.4594(8) 0.1795(10) 0.5213(8) 0.223(13) Uani 1 1 d D U . . .
H15A H 0.487872 0.195827 0.532444 0.334 Uiso 1 1 calc GR . . . .
H15B H 0.465230 0.163870 0.490320 0.334 Uiso 1 1 calc GR . . . .
H15C H 0.449933 0.154478 0.544625 0.334 Uiso 1 1 calc GR . . . .
Cl17 Cl 0.5640(7) 0.3698(7) 0.9651(3) 0.112(5) Uani 0.4 1 d . . . C 2
Sb8 Sb 0.56097(4) 0.750000 0.750000 0.0863(3) Uani 1 2 d S TU P . .
Cl2A Cl 0.5984(3) 0.1935(3) 0.3938(4) 0.253(4) Uani 1 1 d D U . . .
Cl3A Cl 0.6103(5) 0.2442(5) 0.3036(5) 0.353(6) Uani 1 1 d D U . . .
C2 C 0.5706(6) 0.2243(14) 0.3474(9) 0.294(9) Uani 1 1 d D U . . .
H2A H 0.553764 0.253148 0.360449 0.353 Uiso 1 1 calc R . . . .
H2B H 0.547373 0.202140 0.332489 0.353 Uiso 1 1 calc R . . . .
F4A F 0.6035(6) 0.7154(6) 0.7801(6) 0.220(5) Uani 1 1 d . U . . .
F0A F 0.5382(6) 0.7110(6) 0.7092(6) 0.227(5) Uani 1 1 d . U . . .
F7 F 0.5224(6) 0.7112(7) 0.7873(7) 0.237(5) Uani 1 1 d . U . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag01 Ag01 2.8241(11) 4_556 ?
Ag01 Ag02 2.7579(8) 4_556 ?
Ag01 Ag02 2.8034(8) . ?
Ag01 Ag03 3.2366(9) . ?
Ag01 Ag03 3.2296(8) 4_556 ?
Ag01 Ag05 3.2074(9) . ?
Ag01 Cu08 3.0039(14) . ?
Ag01 Cu0D 3.0295(14) . ?
Ag01 Cl00 2.6666(18) . ?
Ag01 Cl2 2.655(2) . ?
Ag02 Ag02 2.8096(11) 4_556 ?
Ag02 Ag03 3.2268(8) . ?
Ag02 Ag05 3.1149(10) . ?
Ag02 Ag05 3.2092(9) 4_556 ?
Ag02 Cu07 3.0774(13) . ?
Ag02 Cu0D 3.0921(14) . ?
Ag02 Cl1 2.6840(18) . ?
Ag02 Cl3 2.642(2) . ?
Ag03 Cu08 3.1909(10) . ?
Ag03 S00H 2.4041(19) 4_556 ?
Ag03 S00K 2.402(2) . ?
Sb04 F00U 1.844(7) . ?
Sb04 F00U 1.844(7) 2_565 ?
Sb04 F014 1.871(9) . ?
Sb04 F014 1.871(9) 2_565 ?
Sb04 F02L 1.796(10) . ?
Sb04 F02L 1.796(10) 2_565 ?
Ag05 Cu07 3.1546(10) . ?
Ag05 Cu0D 3.1502(14) . ?
Ag05 S00J 2.427(2) 4_556 ?
Ag05 S00N 2.412(2) . ?
Cu07 S00J 2.205(2) . ?
Cu07 S00J 2.205(2) 4_556 ?
Cu08 S00H 2.190(2) 4_556 ?
Cu08 S00H 2.190(2) . ?
Cu09 Cu0B 3.0005(16) . ?
Cu09 Cl00 2.588(2) . ?
Cu09 Cl2 2.414(2) . ?
Cu09 S00H 2.296(2) . ?
Cu09 P00L 2.203(2) . ?
Cu0A Cu0C 2.9396(17) . ?
Cu0A Cl1 2.534(2) . ?
Cu0A Cl3 2.414(2) . ?
Cu0A S00J 2.267(2) . ?
Cu0A P00P 2.191(2) . ?
Cu0B Cl00 2.461(2) . ?
Cu0B Cl2 2.480(2) . ?
Cu0B P00M 2.202(2) . ?
Cu0B S00N 2.276(2) . ?
Cu0C Cl1 2.536(2) . ?
Cu0C Cl3 2.427(2) . ?
Cu0C S00K 2.269(2) . ?
Cu0C P00O 2.187(2) . ?
Cu0D S00K 2.186(3) . ?
Cu0D S00N 2.177(3) . ?
S00H C00Y 1.864(8) . ?
S00J C018 1.851(8) . ?
S00K C00V 1.839(8) . ?
P00L C00Z 1.832(8) . ?
P00L C013 1.827(9) . ?
P00L C01A 1.812(10) . ?
P00M C00X 1.831(9) . ?
P00M C00Z 1.830(8) . ?
P00M C01E 1.802(10) . ?
S00N C016 1.856(8) . ?
P00O C010 1.832(9) . ?
P00O C01O 1.829(9) . ?
P00O C01X 1.826(9) . ?
P00P C01L 1.813(9) . ?
P00P C01N 1.849(9) . ?
P00P C01X 1.832(10) . ?
Cl1A C02W 1.721(14) . ?
Cl5 C02W 1.737(14) . ?
C00V C012 1.531(11) . ?
C00V C01R 1.537(12) . ?
C00V C02E 1.493(13) . ?
C00X C01J 1.393(13) . ?
C00X C01W 1.365(14) . ?
C00Y C017 1.521(11) . ?
C00Y C01B 1.514(11) . ?
C00Y C01M 1.562(12) . ?
C010 C022 1.377(14) . ?
C010 C029 1.410(15) . ?
C011 C017 1.532(11) . ?
C011 C019 1.517(13) . ?
C011 C01I 1.514(14) . ?
C012 C01H 1.530(13) . ?
C013 C01F 1.399(13) . ?
C013 C01V 1.380(12) . ?
C015 C019 1.509(13) . ?
C015 C01B 1.527(11) . ?
C015 C020 1.537(13) . ?
C016 C01D 1.533(12) . ?
C016 C01T 1.526(12) . ?
C016 C01Z 1.533(12) . ?
C018 C026 1.523(11) . ?
C018 C02I 1.531(14) . ?
C018 C03A 1.517(14) . ?
C01A C02B 1.399(14) . ?
C01A C02Y 1.384(16) . ?
C01C C01G 1.370(14) . ?
C01C C01L 1.407(12) . ?
C01D C01Q 1.532(13) . ?
C01E C023 1.371(13) . ?
C01E C02Z 1.388(14) . ?
C01F C01P 1.367(13) . ?
C01G C02H 1.369(17) . ?
C01H C02K 1.502(16) . ?
C01H C02T 1.520(16) . ?
C01I C025 1.504(16) . ?
C01J C028 1.380(16) . ?
C01L C01U 1.367(13) . ?
C01M C025 1.548(13) . ?
C01N C024 1.370(13) . ?
C01N C038 1.404(15) . ?
C01O C021 1.369(14) . ?
C01O C027 1.364(13) . ?
C01P C01S 1.392(15) . ?
C01Q C02F 1.532(15) . ?
C01Q C02P 1.476(17) . ?
C01R C02G 1.551(13) . ?
C01S C01Y 1.354(16) . ?
C01T C02C 1.544(13) . ?
C01U C02V 1.412(16) . ?
C01V C01Y 1.400(14) . ?
C01W C037 1.443(15) . ?
C01Z C033 1.488(13) . ?
C020 C025 1.533(14) . ?
C021 C02Q 1.391(15) . ?
C022 C02S 1.386(15) . ?
C023 C035 1.357(15) . ?
C024 C02D 1.403(15) . ?
C026 C02N 1.526(13) . ?
C027 C02U 1.355(16) . ?
C028 C02J 1.418(19) . ?
C029 C031 1.409(16) . ?
C02A C02Q 1.377(17) . ?
C02A C02U 1.301(18) . ?
C02B C036 1.372(17) . ?
C02C C02P 1.519(17) . ?
C02C C032 1.525(16) . ?
C02D C03B 1.339(18) . ?
C02E C030 1.533(14) . ?
C02F C033 1.509(15) . ?
C02G C02K 1.532(15) . ?
C02G C02M 1.526(16) . ?
C02H C02V 1.393(17) . ?
C02I C02X 1.539(15) . ?
C02J C037 1.354(18) . ?
C02M C030 1.533(17) . ?
C02N C02O 1.494(16) . ?
C02N C034 1.515(18) . ?
C02O C02X 1.513(17) . ?
C02S C039 1.339(19) . ?
C02T C030 1.557(15) . ?
C02X C03L 1.53(2) . ?
C02Y C03K 1.43(2) . ?
C02Z C03G 1.377(16) . ?
C031 C039 1.407(19) . ?
C032 C033 1.544(16) . ?
C034 C03H 1.54(2) . ?
C035 C03C 1.390(17) . ?
C036 C03D 1.31(2) . ?
C038 C03E 1.399(16) . ?
C03A C03H 1.585(17) . ?
C03B C03E 1.389(19) . ?
C03C C03G 1.354(18) . ?
C03D C03K 1.42(2) . ?
O03F C03J 1.511(9) . ?
O03F C03M 1.494(9) . ?
C03H C03L 1.44(2) . ?
C03I Cl4 1.50(3) . ?
C03I Cl13 2.07(4) . ?
C03I Cl14 1.68(2) . ?
C03I Cl17 1.75(2) . ?
C03J C15 1.523(9) . ?
C03M C03N 1.519(9) . ?
Sb8 F4A 1.755(14) . ?
Sb8 F4A 1.754(14) 4_566 ?
Sb8 F0A 1.687(14) . ?
Sb8 F0A 1.687(14) 4_566 ?
Sb8 F7 1.850(16) 4_566 ?
Sb8 F7 1.850(16) . ?
Cl2A C2 1.739(10) . ?
Cl3A C2 1.757(10) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Ag01 Ag01 Ag03 64.23(2) 4_556 4_556 ?
Ag01 Ag01 Ag03 63.98(2) 4_556 . ?
Ag01 Ag01 Ag05 112.457(16) 4_556 . ?
Ag01 Ag01 Cu08 61.961(16) 4_556 . ?
Ag01 Ag01 Cu0D 113.53(4) 4_556 . ?
Ag02 Ag01 Ag01 60.278(19) 4_556 4_556 ?
Ag02 Ag01 Ag01 58.691(19) . 4_556 ?
Ag02 Ag01 Ag02 60.68(2) 4_556 . ?
Ag02 Ag01 Ag03 64.12(2) . . ?
Ag02 Ag01 Ag03 115.44(2) 4_556 . ?
Ag02 Ag01 Ag03 64.657(19) 4_556 4_556 ?
Ag02 Ag01 Ag03 114.33(2) . 4_556 ?
Ag02 Ag01 Ag05 64.58(2) 4_556 . ?
Ag02 Ag01 Ag05 61.99(2) . . ?
Ag02 Ag01 Cu08 111.51(2) . . ?
Ag02 Ag01 Cu08 112.83(2) 4_556 . ?
Ag02 Ag01 Cu0D 114.69(3) 4_556 . ?
Ag02 Ag01 Cu0D 63.89(3) . . ?
Ag03 Ag01 Ag03 115.27(2) 4_556 . ?
Ag05 Ag01 Ag03 113.75(2) . . ?
Ag05 Ag01 Ag03 120.13(2) . 4_556 ?
Cu08 Ag01 Ag03 61.369(15) . . ?
Cu08 Ag01 Ag03 61.454(15) . 4_556 ?
Cu08 Ag01 Ag05 173.50(3) . . ?
Cu08 Ag01 Cu0D 117.56(3) . . ?
Cu0D Ag01 Ag03 62.86(3) . . ?
Cu0D Ag01 Ag03 177.74(4) . 4_556 ?
Cu0D Ag01 Ag05 60.59(3) . . ?
Cl00 Ag01 Ag01 120.75(4) . 4_556 ?
Cl00 Ag01 Ag02 120.57(5) . . ?
Cl00 Ag01 Ag02 178.60(5) . 4_556 ?
Cl00 Ag01 Ag03 114.72(4) . 4_556 ?
Cl00 Ag01 Ag03 65.95(4) . . ?
Cl00 Ag01 Ag05 115.24(4) . . ?
Cl00 Ag01 Cu08 67.51(4) . . ?
Cl00 Ag01 Cu0D 65.98(5) . . ?
Cl2 Ag01 Ag01 143.36(5) . 4_556 ?
Cl2 Ag01 Ag02 141.05(5) . . ?
Cl2 Ag01 Ag02 99.48(4) . 4_556 ?
Cl2 Ag01 Ag03 79.71(4) . 4_556 ?
Cl2 Ag01 Ag03 145.07(4) . . ?
Cl2 Ag01 Ag05 79.39(4) . . ?
Cl2 Ag01 Cu08 107.07(4) . . ?
Cl2 Ag01 Cu0D 102.55(5) . . ?
Cl2 Ag01 Cl00 79.14(6) . . ?
Ag01 Ag02 Ag01 61.03(2) 4_556 . ?
Ag01 Ag02 Ag02 60.456(19) 4_556 4_556 ?
Ag01 Ag02 Ag02 58.86(2) . 4_556 ?
Ag01 Ag02 Ag03 64.47(2) . . ?
Ag01 Ag02 Ag03 64.765(19) 4_556 . ?
Ag01 Ag02 Ag05 112.98(2) . 4_556 ?
Ag01 Ag02 Ag05 117.28(3) 4_556 . ?
Ag01 Ag02 Ag05 64.51(2) 4_556 4_556 ?
Ag01 Ag02 Ag05 65.39(2) . . ?
Ag01 Ag02 Cu07 113.64(2) 4_556 . ?
Ag01 Ag02 Cu07 112.32(2) . . ?
Ag01 Ag02 Cu0D 113.56(3) 4_556 . ?
Ag01 Ag02 Cu0D 61.61(3) . . ?
Ag02 Ag02 Ag03 114.240(15) 4_556 . ?
Ag02 Ag02 Ag05 61.91(2) 4_556 4_556 ?
Ag02 Ag02 Ag05 65.36(2) 4_556 . ?
Ag02 Ag02 Cu07 62.840(16) 4_556 . ?
Ag02 Ag02 Cu0D 111.29(4) 4_556 . ?
Ag05 Ag02 Ag03 120.17(2) 4_556 . ?
Ag05 Ag02 Ag03 116.63(2) . . ?
Ag05 Ag02 Ag05 113.48(2) . 4_556 ?
Cu07 Ag02 Ag03 176.77(3) . . ?
Cu07 Ag02 Ag05 61.249(16) . . ?
Cu07 Ag02 Ag05 60.195(16) . 4_556 ?
Cu07 Ag02 Cu0D 116.90(3) . . ?
Cu0D Ag02 Ag03 62.34(3) . . ?
Cu0D Ag02 Ag05 61.00(3) . . ?
Cu0D Ag02 Ag05 173.16(4) . 4_556 ?
Cl1 Ag02 Ag01 177.69(5) . 4_556 ?
Cl1 Ag02 Ag01 120.94(4) . . ?
Cl1 Ag02 Ag02 121.36(4) . 4_556 ?
Cl1 Ag02 Ag03 114.63(4) . . ?
Cl1 Ag02 Ag05 65.02(4) . . ?
Cl1 Ag02 Ag05 114.75(4) . 4_556 ?
Cl1 Ag02 Cu07 67.08(4) . . ?
Cl1 Ag02 Cu0D 67.45(5) . . ?
Cl3 Ag02 Ag01 98.09(5) . 4_556 ?
Cl3 Ag02 Ag01 140.03(5) . . ?
Cl3 Ag02 Ag02 142.91(5) . 4_556 ?
Cl3 Ag02 Ag03 75.90(4) . . ?
Cl3 Ag02 Ag05 81.89(5) . 4_556 ?
Cl3 Ag02 Ag05 144.60(5) . . ?
Cl3 Ag02 Cu07 107.25(5) . . ?
Cl3 Ag02 Cu0D 104.94(5) . . ?
Cl3 Ag02 Cl1 79.61(6) . . ?
Ag01 Ag03 Ag01 51.79(2) 4_556 . ?
Ag02 Ag03 Ag01 50.575(17) . 4_556 ?
Ag02 Ag03 Ag01 51.410(17) . . ?
Cu08 Ag03 Ag01 55.72(2) . . ?
Cu08 Ag03 Ag01 55.79(2) . 4_556 ?
Cu08 Ag03 Ag02 96.87(3) . . ?
S00H Ag03 Ag01 97.87(5) 4_556 . ?
S00H Ag03 Ag01 72.46(5) 4_556 4_556 ?
S00H Ag03 Ag02 122.96(5) 4_556 . ?
S00H Ag03 Cu08 43.31(5) 4_556 . ?
S00K Ag03 Ag01 123.82(5) . 4_556 ?
S00K Ag03 Ag01 96.33(6) . . ?
S00K Ag03 Ag02 73.25(5) . . ?
S00K Ag03 Cu08 146.77(6) . . ?
S00K Ag03 S00H 163.21(7) . 4_556 ?
F00U Sb04 F00U 178.7(5) 2_565 . ?
F00U Sb04 F014 93.2(4) . . ?
F00U Sb04 F014 87.7(4) . 2_565 ?
F00U Sb04 F014 93.2(4) 2_565 2_565 ?
F00U Sb04 F014 87.7(4) 2_565 . ?
F014 Sb04 F014 83.3(8) . 2_565 ?
F02L Sb04 F00U 90.9(5) . 2_565 ?
F02L Sb04 F00U 90.9(5) 2_565 . ?
F02L Sb04 F00U 88.3(5) . . ?
F02L Sb04 F00U 88.3(5) 2_565 2_565 ?
F02L Sb04 F014 87.7(8) . . ?
F02L Sb04 F014 87.7(8) 2_565 2_565 ?
F02L Sb04 F014 170.0(8) . 2_565 ?
F02L Sb04 F014 170.0(8) 2_565 . ?
F02L Sb04 F02L 101.5(15) . 2_565 ?
Ag01 Ag05 Ag02 50.911(17) . 4_556 ?
Ag02 Ag05 Ag01 52.620(18) . . ?
Ag02 Ag05 Ag02 52.73(2) . 4_556 ?
Ag02 Ag05 Cu07 58.79(2) . . ?
Ag02 Ag05 Cu0D 59.14(3) . . ?
Cu07 Ag05 Ag01 100.37(3) . . ?
Cu07 Ag05 Ag02 57.83(2) . 4_556 ?
Cu0D Ag05 Ag01 56.91(3) . . ?
Cu0D Ag05 Ag02 100.09(3) . 4_556 ?
Cu0D Ag05 Cu07 113.01(4) . . ?
S00J Ag05 Ag01 123.31(5) 4_556 . ?
S00J Ag05 Ag02 101.15(6) 4_556 . ?
S00J Ag05 Ag02 72.88(5) 4_556 4_556 ?
S00J Ag05 Cu07 44.18(6) 4_556 . ?
S00J Ag05 Cu0D 156.65(7) 4_556 . ?
S00N Ag05 Ag01 75.91(5) . . ?
S00N Ag05 Ag02 102.02(6) . . ?
S00N Ag05 Ag02 126.49(5) . 4_556 ?
S00N Ag05 Cu07 154.46(6) . . ?
S00N Ag05 Cu0D 43.61(6) . . ?
S00N Ag05 S00J 156.26(8) . 4_556 ?
Ag02 Cu07 Ag02 54.32(3) . 4_556 ?
Ag02 Cu07 Ag05 61.97(3) . 4_556 ?
Ag02 Cu07 Ag05 59.96(3) . . ?
Ag02 Cu07 Ag05 59.96(3) 4_556 4_556 ?
Ag02 Cu07 Ag05 61.97(3) 4_556 . ?
Ag05 Cu07 Ag05 113.90(5) . 4_556 ?
S00J Cu07 Ag02 78.41(6) . . ?
S00J Cu07 Ag02 107.98(6) . 4_556 ?
S00J Cu07 Ag02 107.98(6) 4_556 . ?
S00J Cu07 Ag02 78.41(6) 4_556 4_556 ?
S00J Cu07 Ag05 50.11(5) 4_556 . ?
S00J Cu07 Ag05 50.11(5) . 4_556 ?
S00J Cu07 Ag05 135.02(6) 4_556 4_556 ?
S00J Cu07 Ag05 135.02(6) . . ?
S00J Cu07 S00J 173.06(12) 4_556 . ?
Ag01 Cu08 Ag01 56.08(3) 4_556 . ?
Ag01 Cu08 Ag03 62.76(3) . 4_556 ?
Ag01 Cu08 Ag03 62.91(3) 4_556 4_556 ?
Ag01 Cu08 Ag03 62.76(3) 4_556 . ?
Ag01 Cu08 Ag03 62.91(3) . . ?
Ag03 Cu08 Ag03 117.70(5) 4_556 . ?
S00H Cu08 Ag01 79.98(6) . . ?
S00H Cu08 Ag01 110.31(6) . 4_556 ?
S00H Cu08 Ag01 79.98(6) 4_556 4_556 ?
S00H Cu08 Ag01 110.30(6) 4_556 . ?
S00H Cu08 Ag03 139.42(6) 4_556 4_556 ?
S00H Cu08 Ag03 48.84(5) 4_556 . ?
S00H Cu08 Ag03 48.85(5) . 4_556 ?
S00H Cu08 Ag03 139.42(6) . . ?
S00H Cu08 S00H 168.75(12) . 4_556 ?
Cl00 Cu09 Cu0B 51.62(5) . . ?
Cl2 Cu09 Cu0B 53.18(5) . . ?
Cl2 Cu09 Cl00 85.25(7) . . ?
S00H Cu09 Cu0B 132.08(7) . . ?
S00H Cu09 Cl00 95.62(8) . . ?
S00H Cu09 Cl2 96.30(7) . . ?
P00L Cu09 Cu0B 91.72(7) . . ?
P00L Cu09 Cl00 108.90(8) . . ?
P00L Cu09 Cl2 121.90(8) . . ?
P00L Cu09 S00H 135.23(9) . . ?
Cl1 Cu0A Cu0C 54.59(5) . . ?
Cl3 Cu0A Cu0C 52.81(6) . . ?
Cl3 Cu0A Cl1 87.09(7) . . ?
S00J Cu0A Cu0C 135.94(7) . . ?
S00J Cu0A Cl1 97.97(8) . . ?
S00J Cu0A Cl3 97.53(8) . . ?
P00P Cu0A Cu0C 89.77(7) . . ?
P00P Cu0A Cl1 111.22(9) . . ?
P00P Cu0A Cl3 117.75(9) . . ?
P00P Cu0A S00J 134.23(9) . . ?
Cl00 Cu0B Cu09 55.51(5) . . ?
Cl00 Cu0B Cl2 86.63(7) . . ?
Cl2 Cu0B Cu09 51.21(5) . . ?
P00M Cu0B Cu09 89.89(7) . . ?
P00M Cu0B Cl00 111.45(8) . . ?
P00M Cu0B Cl2 117.28(9) . . ?
P00M Cu0B S00N 131.97(9) . . ?
S00N Cu0B Cu09 137.28(7) . . ?
S00N Cu0B Cl00 105.14(9) . . ?
S00N Cu0B Cl2 94.41(8) . . ?
Cl1 Cu0C Cu0A 54.54(5) . . ?
Cl3 Cu0C Cu0A 52.40(6) . . ?
Cl3 Cu0C Cl1 86.78(7) . . ?
S00K Cu0C Cu0A 134.13(7) . . ?
S00K Cu0C Cl1 98.94(8) . . ?
S00K Cu0C Cl3 94.55(8) . . ?
P00O Cu0C Cu0A 93.01(7) . . ?
P00O Cu0C Cl1 118.19(8) . . ?
P00O Cu0C Cl3 115.03(9) . . ?
P00O Cu0C S00K 132.36(9) . . ?
Ag01 Cu0D Ag02 54.50(3) . . ?
Ag01 Cu0D Ag05 62.50(3) . . ?
Ag02 Cu0D Ag05 59.86(3) . . ?
S00K Cu0D Ag01 107.60(7) . . ?
S00K Cu0D Ag02 78.81(6) . . ?
S00K Cu0D Ag05 135.43(8) . . ?
S00N Cu0D Ag01 83.12(7) . . ?
S00N Cu0D Ag02 108.85(7) . . ?
S00N Cu0D Ag05 49.85(6) . . ?
S00N Cu0D S00K 169.26(10) . . ?
Cu09 Cl00 Ag01 82.18(6) . . ?
Cu0B Cl00 Ag01 82.85(6) . . ?
Cu0B Cl00 Cu09 72.87(6) . . ?
Cu0A Cl1 Ag02 81.09(6) . . ?
Cu0A Cl1 Cu0C 70.87(6) . . ?
Cu0C Cl1 Ag02 82.12(6) . . ?
Cu09 Cl2 Ag01 85.76(6) . . ?
Cu09 Cl2 Cu0B 75.61(6) . . ?
Cu0B Cl2 Ag01 82.75(6) . . ?
Cu08 S00H Ag03 87.85(7) . 4_556 ?
Cu08 S00H Cu09 104.86(8) . . ?
Cu09 S00H Ag03 120.51(8) . 4_556 ?
C00Y S00H Ag03 112.1(2) . 4_556 ?
C00Y S00H Cu08 104.8(3) . . ?
C00Y S00H Cu09 119.5(2) . . ?
Cu0A Cl3 Ag02 84.20(7) . . ?
Cu0A Cl3 Cu0C 74.78(7) . . ?
Cu0C Cl3 Ag02 85.06(7) . . ?
Cu07 S00J Ag05 85.71(7) . 4_556 ?
Cu07 S00J Cu0A 104.18(9) . . ?
Cu0A S00J Ag05 121.27(9) . 4_556 ?
C018 S00J Ag05 112.4(3) . 4_556 ?
C018 S00J Cu07 108.2(3) . . ?
C018 S00J Cu0A 118.2(3) . . ?
Cu0C S00K Ag03 118.96(9) . . ?
Cu0D S00K Ag03 90.88(8) . . ?
Cu0D S00K Cu0C 103.40(9) . . ?
C00V S00K Ag03 111.3(3) . . ?
C00V S00K Cu0C 119.0(3) . . ?
C00V S00K Cu0D 108.1(3) . . ?
C00Z P00L Cu09 113.1(3) . . ?
C013 P00L Cu09 115.5(3) . . ?
C013 P00L C00Z 102.7(4) . . ?
C01A P00L Cu09 116.6(3) . . ?
C01A P00L C00Z 103.2(4) . . ?
C01A P00L C013 104.1(4) . . ?
C00X P00M Cu0B 117.4(3) . . ?
C00Z P00M Cu0B 113.4(3) . . ?
C00Z P00M C00X 102.3(4) . . ?
C01E P00M Cu0B 111.8(3) . . ?
C01E P00M C00X 105.0(4) . . ?
C01E P00M C00Z 105.9(4) . . ?
Cu0B S00N Ag05 121.09(9) . . ?
Cu0D S00N Ag05 86.54(8) . . ?
Cu0D S00N Cu0B 93.85(9) . . ?
C016 S00N Ag05 115.2(3) . . ?
C016 S00N Cu0B 120.9(3) . . ?
C016 S00N Cu0D 106.3(3) . . ?
C010 P00O Cu0C 113.2(3) . . ?
C01O P00O Cu0C 120.1(3) . . ?
C01O P00O C010 104.9(4) . . ?
C01X P00O Cu0C 111.2(3) . . ?
C01X P00O C010 103.2(4) . . ?
C01X P00O C01O 102.5(4) . . ?
C01L P00P Cu0A 115.2(3) . . ?
C01L P00P C01N 103.9(4) . . ?
C01L P00P C01X 107.1(4) . . ?
C01N P00P Cu0A 116.5(3) . . ?
C01X P00P Cu0A 111.2(3) . . ?
C01X P00P C01N 101.7(4) . . ?
C012 C00V S00K 109.3(6) . . ?
C012 C00V C01R 107.9(7) . . ?
C01R C00V S00K 109.4(6) . . ?
C02E C00V S00K 109.8(6) . . ?
C02E C00V C012 110.5(8) . . ?
C02E C00V C01R 110.0(8) . . ?
C01J C00X P00M 121.2(8) . . ?
C01W C00X P00M 118.7(7) . . ?
C01W C00X C01J 120.0(9) . . ?
C017 C00Y S00H 108.5(5) . . ?
C017 C00Y C01M 109.0(7) . . ?
C01B C00Y S00H 111.4(5) . . ?
C01B C00Y C017 110.7(7) . . ?
C01B C00Y C01M 109.7(7) . . ?
C01M C00Y S00H 107.4(6) . . ?
P00M C00Z P00L 113.7(4) . . ?
C022 C010 P00O 122.5(8) . . ?
C022 C010 C029 120.6(9) . . ?
C029 C010 P00O 116.6(8) . . ?
C019 C011 C017 109.4(7) . . ?
C01I C011 C017 109.5(8) . . ?
C01I C011 C019 109.0(8) . . ?
C01H C012 C00V 108.9(7) . . ?
C01F C013 P00L 120.0(6) . . ?
C01V C013 P00L 122.1(7) . . ?
C01V C013 C01F 117.6(8) . . ?
C019 C015 C01B 110.0(7) . . ?
C019 C015 C020 108.5(8) . . ?
C01B C015 C020 108.6(7) . . ?
C01D C016 S00N 111.1(6) . . ?
C01D C016 C01Z 108.6(7) . . ?
C01T C016 S00N 108.2(5) . . ?
C01T C016 C01D 109.7(8) . . ?
C01T C016 C01Z 110.2(8) . . ?
C01Z C016 S00N 109.0(6) . . ?
C00Y C017 C011 109.1(7) . . ?
C026 C018 S00J 111.4(6) . . ?
C026 C018 C02I 109.8(8) . . ?
C02I C018 S00J 109.7(6) . . ?
C03A C018 S00J 107.3(6) . . ?
C03A C018 C026 109.1(8) . . ?
C03A C018 C02I 109.5(9) . . ?
C015 C019 C011 110.9(8) . . ?
C02B C01A P00L 121.5(8) . . ?
C02Y C01A P00L 118.5(8) . . ?
C02Y C01A C02B 120.0(10) . . ?
C00Y C01B C015 109.7(7) . . ?
C01G C01C C01L 120.2(9) . . ?
C01Q C01D C016 108.4(8) . . ?
C023 C01E P00M 124.0(8) . . ?
C023 C01E C02Z 118.1(9) . . ?
C02Z C01E P00M 117.8(7) . . ?
C01P C01F C013 121.3(9) . . ?
C02H C01G C01C 121.6(10) . . ?
C02K C01H C012 110.0(9) . . ?
C02K C01H C02T 113.0(9) . . ?
C02T C01H C012 108.9(9) . . ?
C025 C01I C011 110.2(8) . . ?
C028 C01J C00X 121.6(11) . . ?
C01C C01L P00P 121.7(7) . . ?
C01U C01L P00P 118.1(7) . . ?
C01U C01L C01C 120.1(9) . . ?
C025 C01M C00Y 107.5(8) . . ?
C024 C01N P00P 122.7(8) . . ?
C024 C01N C038 121.3(9) . . ?
C038 C01N P00P 115.7(8) . . ?
C021 C01O P00O 118.9(7) . . ?
C027 C01O P00O 121.1(8) . . ?
C027 C01O C021 120.0(9) . . ?
C01F C01P C01S 120.0(11) . . ?
C01D C01Q C02F 109.8(9) . . ?
C02P C01Q C01D 111.0(9) . . ?
C02P C01Q C02F 109.0(10) . . ?
C00V C01R C02G 109.1(8) . . ?
C01Y C01S C01P 120.1(10) . . ?
C016 C01T C02C 108.5(8) . . ?
C01L C01U C02V 118.1(10) . . ?
C013 C01V C01Y 121.3(9) . . ?
C00X C01W C037 119.3(10) . . ?
P00O C01X P00P 113.3(5) . . ?
C01S C01Y C01V 119.8(9) . . ?
C033 C01Z C016 110.3(8) . . ?
C025 C020 C015 109.5(8) . . ?
C01O C021 C02Q 118.1(10) . . ?
C010 C022 C02S 121.0(11) . . ?
C035 C023 C01E 122.3(11) . . ?
C01N C024 C02D 118.4(11) . . ?
C01I C025 C01M 109.7(8) . . ?
C01I C025 C020 110.2(9) . . ?
C020 C025 C01M 109.1(8) . . ?
C018 C026 C02N 109.3(8) . . ?
C02U C027 C01O 119.7(12) . . ?
C01J C028 C02J 118.2(11) . . ?
C031 C029 C010 116.3(12) . . ?
C02U C02A C02Q 119.5(11) . . ?
C036 C02B C01A 119.8(13) . . ?
C02P C02C C01T 108.9(9) . . ?
C02P C02C C032 109.2(10) . . ?
C032 C02C C01T 109.3(9) . . ?
C03B C02D C024 121.7(11) . . ?
C00V C02E C030 111.0(9) . . ?
C033 C02F C01Q 109.2(8) . . ?
C02K C02G C01R 108.1(8) . . ?
C02M C02G C01R 109.2(9) . . ?
C02M C02G C02K 110.0(9) . . ?
C01G C02H C02V 117.8(11) . . ?
C018 C02I C02X 109.4(9) . . ?
C037 C02J C028 121.0(11) . . ?
C01H C02K C02G 108.9(9) . . ?
C02G C02M C030 110.7(8) . . ?
C02O C02N C026 108.7(9) . . ?
C02O C02N C034 110.6(10) . . ?
C034 C02N C026 108.6(9) . . ?
C02N C02O C02X 111.0(10) . . ?
C01Q C02P C02C 110.3(9) . . ?
C02A C02Q C021 120.2(12) . . ?
C039 C02S C022 120.6(12) . . ?
C01H C02T C030 107.9(9) . . ?
C02A C02U C027 122.4(11) . . ?
C02H C02V C01U 122.1(12) . . ?
Cl1A C02W Cl5 111.7(8) . . ?
C02O C02X C02I 107.3(10) . . ?
C02O C02X C03L 110.0(12) . . ?
C03L C02X C02I 108.8(11) . . ?
C01A C02Y C03K 119.0(13) . . ?
C03G C02Z C01E 120.1(11) . . ?
C02E C030 C02T 108.8(9) . . ?
C02M C030 C02E 107.8(9) . . ?
C02M C030 C02T 109.6(9) . . ?
C039 C031 C029 121.8(13) . . ?
C02C C032 C033 109.8(9) . . ?
C01Z C033 C02F 112.3(9) . . ?
C01Z C033 C032 108.7(8) . . ?
C02F C033 C032 107.1(10) . . ?
C02N C034 C03H 110.8(11) . . ?
C023 C035 C03C 118.6(11) . . ?
C03D C036 C02B 121.6(14) . . ?
C02J C037 C01W 119.7(12) . . ?
C03E C038 C01N 117.9(12) . . ?
C02S C039 C031 119.6(12) . . ?
C018 C03A C03H 109.5(10) . . ?
C02D C03B C03E 120.1(11) . . ?
C03G C03C C035 120.3(12) . . ?
C036 C03D C03K 121.9(15) . . ?
C03B C03E C038 120.5(13) . . ?
C03M O03F C03J 116.5(9) . . ?
C03C C03G C02Z 120.4(12) . . ?
C034 C03H C03A 104.9(11) . . ?
C03L C03H C034 110.6(13) . . ?
C03L C03H C03A 110.3(12) . . ?
Cl4 C03I Cl13 112.0(15) . . ?
Cl14 C03I Cl17 119.4(13) . . ?
O03F C03J C15 112.9(9) . . ?
C03D C03K C02Y 117.5(16) . . ?
C03H C03L C02X 112.0(12) . . ?
O03F C03M C03N 114.4(10) . . ?
F4A Sb8 F4A 92.0(12) 4_566 . ?
F4A Sb8 F7 172.4(9) 4_566 . ?
F4A Sb8 F7 80.8(8) . . ?
F4A Sb8 F7 80.8(8) 4_566 4_566 ?
F4A Sb8 F7 172.4(9) . 4_566 ?
F0A Sb8 F4A 104.8(8) . . ?
F0A Sb8 F4A 104.8(8) 4_566 4_566 ?
F0A Sb8 F4A 106.3(9) 4_566 . ?
F0A Sb8 F4A 106.3(9) . 4_566 ?
F0A Sb8 F0A 134.6(13) . 4_566 ?
F0A Sb8 F7 75.3(8) . 4_566 ?
F0A Sb8 F7 75.3(8) 4_566 . ?
F0A Sb8 F7 78.0(9) 4_566 4_566 ?
F0A Sb8 F7 78.0(9) . . ?
F7 Sb8 F7 106.6(13) . 4_566 ?
Cl2A C2 Cl3A 111.8(9) . . ?

_platon_squeeze_details          ?
loop_
_platon_squeeze_void_nr
_platon_squeeze_void_average_x
_platon_squeeze_void_average_y
_platon_squeeze_void_average_z
_platon_squeeze_void_volume
_platon_squeeze_void_count_electrons
_platon_squeeze_void_content
1 0.250 0.500 0.104 56 4 ' '
2 0.250 0.000 0.149 44 2 ' '
3 0.250 0.500 0.351 44 2 ' '
4 0.250 0.000 0.396 56 4 ' '
5 0.750 0.000 0.604 56 4 ' '
6 0.750 0.500 0.649 44 2 ' '
7 0.750 0.000 0.851 44 2 ' '
8 0.750 0.500 0.896 56 4 ' '

_platon_squeeze_void_probe_radius 1.20
_olex2_submission_special_instructions 'No special instructions were received'
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_hp-1015_sq
_database_code_depnum_ccdc_archive 'CCDC 2391028'
loop_
_audit_author_name
_audit_author_address
'shan jin'
;An Hui University
China
;
_audit_update_record             
;
2024-10-15 deposited with the CCDC.	2025-02-04 downloaded from the CCDC.
;
_audit_creation_date             2024-10-15
_audit_creation_method           
;
Olex2 1.2
(compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         
'1(C205 H261 Ag17.11 Cl9 Cu14.89 P6 S13), 2.01(F6 Sb)'
_chemical_formula_sum            
'C205 H261 Ag17.11 Cl9 Cu14.89 F12.06 P6 S13 Sb2.01'
_chemical_formula_weight         6912.46
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag 0.1306 4.2820 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu -1.9646 0.5888 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0727 0.0534 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.0562 5.8946 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      trigonal
_space_group_IT_number           148
_space_group_name_H-M_alt        'R -3'
_space_group_name_Hall           '-R 3'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'
'x+2/3, y+1/3, z+1/3'
'-y+2/3, x-y+1/3, z+1/3'
'-x+y+2/3, -x+1/3, z+1/3'
'x+1/3, y+2/3, z+2/3'
'-y+1/3, x-y+2/3, z+2/3'
'-x+y+1/3, -x+2/3, z+2/3'
'-x, -y, -z'
'y, -x+y, -z'
'x-y, x, -z'
'-x+2/3, -y+1/3, -z+1/3'
'y+2/3, -x+y+1/3, -z+1/3'
'x-y+2/3, x+1/3, -z+1/3'
'-x+1/3, -y+2/3, -z+2/3'
'y+1/3, -x+y+2/3, -z+2/3'
'x-y+1/3, x+2/3, -z+2/3'

_cell_length_a                   26.715(4)
_cell_length_b                   26.715(4)
_cell_length_c                   68.924(9)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_volume                     42602(14)
_cell_formula_units_Z            5.99994
_cell_measurement_reflns_used    4155
_cell_measurement_temperature    120(2)
_cell_measurement_theta_max      29.96
_cell_measurement_theta_min      1.97
_shelx_estimated_absorpt_T_max   ?
_shelx_estimated_absorpt_T_min   ?
_exptl_absorpt_coefficient_mu    14.214
_exptl_absorpt_correction_T_max  ?
_exptl_absorpt_correction_T_min  ?
_exptl_absorpt_correction_type   ?
_exptl_absorpt_process_details   ?
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            ?
_exptl_crystal_density_diffrn    1.617
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             20334
_exptl_crystal_size_max          ?
_exptl_crystal_size_mid          ?
_exptl_crystal_size_min          ?
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0977
_diffrn_reflns_av_unetI/netI     0.0955
_diffrn_reflns_Laue_measured_fraction_full 0.960
_diffrn_reflns_Laue_measured_fraction_max 0.960
_diffrn_reflns_limit_h_max       23
_diffrn_reflns_limit_h_min       -31
_diffrn_reflns_limit_k_max       30
_diffrn_reflns_limit_k_min       -31
_diffrn_reflns_limit_l_max       80
_diffrn_reflns_limit_l_min       -73
_diffrn_reflns_number            76725
_diffrn_reflns_point_group_measured_fraction_full 0.960
_diffrn_reflns_point_group_measured_fraction_max 0.960
_diffrn_reflns_theta_full        64.993
_diffrn_reflns_theta_max         64.993
_diffrn_reflns_theta_min         3.828
_diffrn_ambient_temperature      120(2)
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.960
_diffrn_measured_fraction_theta_max 0.960
_diffrn_measurement_device_type  stoe
_diffrn_measurement_method       ?
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54186
_diffrn_source                   ?
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                8858
_reflns_number_total             15477
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       ?
_computing_data_collection       ?
_computing_data_reduction        ?
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    ?
_refine_diff_density_max         4.303
_refine_diff_density_min         -2.094
_refine_diff_density_rms         0.305
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.233
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     820
_refine_ls_number_reflns         15477
_refine_ls_number_restraints     1127
_refine_ls_R_factor_all          0.1839
_refine_ls_R_factor_gt           0.1507
_refine_ls_restrained_S_all      1.249
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.2000P)²] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.3664
_refine_ls_wR_factor_ref         0.3850
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups, All C(H,H) groups
2. Restrained distances
 C01M-C00Q = C01M-C01C = C01O-C01C = C01R-C01C = C46-C01R = C46-C02M = C02M-
 C01Y = C01Y-C01O = C46-C02N = C02N-C00Q = C00U-C00Q = C01Y-C00U
 1.54 with sigma of 0.01
 C00Q-C01Y
 2.54 with sigma of 0.01
 C00Q-C46
 2.54 with sigma of 0.01
 C00Q-C01C
 2.54 with sigma of 0.01
 C01M-C00U
 2.54 with sigma of 0.01
 C01M-C02N
 2.54 with sigma of 0.01
 C01M-C01R
 2.54 with sigma of 0.01
 C00U-C02M
 2.54 with sigma of 0.01
 C00U-C01O
 2.54 with sigma of 0.01
 C00U-C02N
 2.54 with sigma of 0.01
 C01C-C01Y
 2.54 with sigma of 0.01
 C01O-C02M
 2.54 with sigma of 0.01
 C01Y-C46
 2.54 with sigma of 0.01
 C02M-C01R
 2.54 with sigma of 0.01
 C46-C01C
 2.54 with sigma of 0.01
 C01R-C01O
 2.54 with sigma of 0.01
 C00Q-C01O
 2.93 with sigma of 0.01
 C00Q-C02M
 2.93 with sigma of 0.01
 C01R-C00Q
 2.93 with sigma of 0.01
 C00U-C46
 2.93 with sigma of 0.01
 C00U-C01C
 2.93 with sigma of 0.01
 C01M-C01Y
 2.93 with sigma of 0.01
 C01M-C46
 2.93 with sigma of 0.01
 C01O-C46
 2.93 with sigma of 0.01
 C01C-C02M
 2.93 with sigma of 0.01
 C01Y-C01R
 2.93 with sigma of 0.01
 C01I-C017 = C36-C017 = C36-C02W = C36-C01A = C024-C01A = C024-C01D = C01Q-
 C01D = C02W-C01Q = C024-C01G = C01Q-C013 = C01I-C013 = C01I-C01G
 1.54 with sigma of 0.01
 C01I-C36
 2.54 with sigma of 0.01
 C01I-C024
 2.54 with sigma of 0.01
 C01I-C01Q
 2.54 with sigma of 0.01
 C017-C01A
 2.54 with sigma of 0.01
 C017-C02W
 2.54 with sigma of 0.01
 C017-C01G
 2.54 with sigma of 0.01
 C017-C013
 2.54 with sigma of 0.01
 C013-C01G
 2.54 with sigma of 0.01
 C013-C02W
 2.54 with sigma of 0.01
 C013-C01D
 2.54 with sigma of 0.01
 C01Q-C36
 2.54 with sigma of 0.01
 C02W-C01A
 2.54 with sigma of 0.01
 C36-C024
 2.54 with sigma of 0.01
 C01A-C01D
 2.54 with sigma of 0.01
 C024-C01Q
 2.54 with sigma of 0.01
 C01I-C02W
 2.93 with sigma of 0.01
 C01I-C01A
 2.93 with sigma of 0.01
 C01I-C01D
 2.93 with sigma of 0.01
 C017-C01Q
 2.93 with sigma of 0.01
 C017-C024
 2.93 with sigma of 0.01
 C013-C36
 2.93 with sigma of 0.01
 C013-C024
 2.93 with sigma of 0.01
 C02W-C024
 2.93 with sigma of 0.01
 C01D-C36
 2.93 with sigma of 0.01
 C01A-C01Q
 2.93 with sigma of 0.01
 C36-C01G
 2.93 with sigma of 0.01
 C01G-C01Q
 2.93 with sigma of 0.01
 C02K-C00X = C02O-C02K = C29-C02O = C02O-C01U = C020-C01U = C028-C020 = C52-
 C29 = C52-C028 = C52-C30 = C014-C00X = C30-C00X
 1.54 with sigma of 0.01
 C00X-C02O
 2.54 with sigma of 0.01
 C00X-C020
 2.54 with sigma of 0.01
 C00X-C52
 2.54 with sigma of 0.01
 C02K-C29
 2.54 with sigma of 0.01
 C02K-C01U
 2.54 with sigma of 0.01
 C02K-C30
 2.54 with sigma of 0.01
 C30-C014
 2.54 with sigma of 0.01
 C30-C29
 2.54 with sigma of 0.01
 C30-C028
 2.54 with sigma of 0.01
 C52-C02O
 2.54 with sigma of 0.01
 C29-C01U
 2.54 with sigma of 0.01
 C02O-C020
 2.54 with sigma of 0.01
 C01U-C028
 2.54 with sigma of 0.01
 C020-C52
 2.54 with sigma of 0.01
 C00X-C29
 2.93 with sigma of 0.01
 C00X-C01U
 2.93 with sigma of 0.01
 C00X-C028
 2.93 with sigma of 0.01
 C30-C02O
 2.93 with sigma of 0.01
 C30-C020
 2.93 with sigma of 0.01
 C29-C020
 2.93 with sigma of 0.01
 C01U-C52
 2.93 with sigma of 0.01
 C028-C02O
 2.93 with sigma of 0.01
 C023-C00R = C01Z-C01T_$1 = C023-C01Z = C01Z-C01T = C01Z_$2-C01T = C01Z_$2-
 C01T_$2 = C01Z_$1-C01T_$2 = C01Z_$1-C01T_$1 = C023_$1-C01Z_$1 = C023_$1-C00R =
 C023_$2-C01Z_$2 = C023_$2-C00R
 1.54 with sigma of 0.01
 C00R-C01Z
 2.54 with sigma of 0.01
 C00R-C01Z_$2
 2.54 with sigma of 0.01
 C00R-C01Z_$1
 2.54 with sigma of 0.01
 C023_$1-C01T_$1
 2.54 with sigma of 0.01
 C023_$1-C023
 2.54 with sigma of 0.01
 C023_$1-C01T_$2
 2.54 with sigma of 0.01
 C023-C01T
 2.54 with sigma of 0.01
 C023-C01T_$1
 2.54 with sigma of 0.01
 C01Z_$1-C01Z
 2.54 with sigma of 0.01
 C01T_$1-C01T
 2.54 with sigma of 0.01
 C01Z-C01Z_$2
 2.54 with sigma of 0.01
 C01T-C01T_$2
 2.54 with sigma of 0.01
 C01Z_$2-C01Z_$1
 2.54 with sigma of 0.01
 C00R-C01T_$1
 2.93 with sigma of 0.01
 C00R-C01T
 2.93 with sigma of 0.01
 C00R-C01T_$2
 2.93 with sigma of 0.01
 C01Z_$1-C01T
 2.93 with sigma of 0.01
 C01T_$1-C01Z_$2
 2.93 with sigma of 0.01
 C01T_$2-C01Z
 2.93 with sigma of 0.01
 C01Z-C023_$2
 2.93 with sigma of 0.01
 C023_$2-C023_$1
 2.93 with sigma of 0.01
 Sb0D-F12 = Sb0D-F75 = Sb0D-F19 = Sb0D-F49 = Sb0D-F32 = Sb0D-F02H
 1.8 with sigma of 0.01
 F49-F02H
 2.6 with sigma of 0.01
 F02H-F12
 2.6 with sigma of 0.01
 F02H-F19
 2.6 with sigma of 0.01
 F02H-F32
 2.6 with sigma of 0.01
 F75-F19
 2.6 with sigma of 0.01
 F75-F12
 2.6 with sigma of 0.01
 F49-F12
 2.6 with sigma of 0.01
3. Uiso/Uaniso restraints and constraints
P0M \\sim C02D \\sim C02S \\sim C01E \\sim C02B \\sim C026 \\sim C01K: within
3.8A with sigma of 0.01 and sigma for terminal atoms of 0.02
C00X \\sim C02K \\sim C30 \\sim C014 \\sim C020 \\sim C028 \\sim C52 \\sim C01U
\\sim C02O \\sim C29: within 3.8A with sigma of 0.01 and sigma for terminal
atoms of 0.02
C02M \\sim C01R \\sim C46 \\sim C01C: within 3.8A with sigma of 0.01 and sigma
for terminal atoms of 0.02
P0N \\sim C010 \\sim C029 \\sim C022 \\sim C018 \\sim C00W \\sim C01N: within
3.8A with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(C00Q) \\sim Ueq, Uanis(C00R) \\sim Ueq, Uanis(C00S) \\sim Ueq,
Uanis(C00T) \\sim Ueq, Uanis(C00U) \\sim Ueq, Uanis(C00V) \\sim Ueq,
Uanis(C02V) \\sim Ueq, Uanis(C032) \\sim Ueq, Uanis(C01X) \\sim Ueq,
Uanis(C01P) \\sim Ueq, Uanis(C01B) \\sim Ueq, Uanis(C00W) \\sim Ueq,
Uanis(C010) \\sim Ueq, Uanis(C029) \\sim Ueq, Uanis(C022) \\sim Ueq,
Uanis(C018) \\sim Ueq, Uanis(C01N) \\sim Ueq, Uanis(C00X) \\sim Ueq,
Uanis(C00Y) \\sim Ueq, Uanis(C011) \\sim Ueq, Uanis(C012) \\sim Ueq,
Uanis(C013) \\sim Ueq, Uanis(C014) \\sim Ueq, Uanis(C015) \\sim Ueq,
Uanis(C016) \\sim Ueq, Uanis(C01V) \\sim Ueq, Uanis(C01H) \\sim Ueq,
Uanis(C02L) \\sim Ueq, Uanis(C02A) \\sim Ueq, Uanis(C01S) \\sim Ueq,
Uanis(C017) \\sim Ueq, Uanis(C01A) \\sim Ueq, Uanis(C01C) \\sim Ueq,
Uanis(C01D) \\sim Ueq, Uanis(C01E) \\sim Ueq, Uanis(C01K) \\sim Ueq,
Uanis(C026) \\sim Ueq, Uanis(C02B) \\sim Ueq, Uanis(C02S) \\sim Ueq,
Uanis(C02D) \\sim Ueq, Uanis(C01G) \\sim Ueq, Uanis(C01I) \\sim Ueq,
Uanis(C01J) \\sim Ueq, Uanis(C01M) \\sim Ueq, Uanis(C01O) \\sim Ueq,
Uanis(C01Q) \\sim Ueq, Uanis(C01R) \\sim Ueq, Uanis(C01T) \\sim Ueq,
Uanis(C01U) \\sim Ueq, Uanis(C01W) \\sim Ueq, Uanis(C01Y) \\sim Ueq,
Uanis(C01Z) \\sim Ueq, Uanis(C020) \\sim Ueq, Uanis(C021) \\sim Ueq,
Uanis(C023) \\sim Ueq, Uanis(C024) \\sim Ueq, Uanis(C025) \\sim Ueq,
Uanis(C028) \\sim Ueq, Uanis(C02G) \\sim Ueq, Uanis(C02K) \\sim Ueq,
Uanis(C02M) \\sim Ueq, Uanis(C02N) \\sim Ueq, Uanis(C02O) \\sim Ueq,
Uanis(C02W) \\sim Ueq, Uanis(C29) \\sim Ueq, Uanis(C30) \\sim Ueq, Uanis(C52)
\\sim Ueq, Uanis(C46) \\sim Ueq, Uanis(C36) \\sim Ueq: with sigma of 0.01 and
sigma for terminal atoms of 0.02
Uanis(F02H) \\sim Ueq, Uanis(F12) \\sim Ueq, Uanis(F19) \\sim Ueq, Uanis(F32)
\\sim Ueq, Uanis(F49) \\sim Ueq, Uanis(F75) \\sim Ueq: with sigma of 0.01 and
sigma for terminal atoms of 0.02
Uanis(C00Q) \\sim Ueq, Uanis(C00U) \\sim Ueq, Uanis(C01Y) \\sim Ueq,
Uanis(C01O) \\sim Ueq, Uanis(C02M) \\sim Ueq, Uanis(C01C) \\sim Ueq,
Uanis(C01M) \\sim Ueq, Uanis(C01R) \\sim Ueq, Uanis(C46) \\sim Ueq: with sigma
of 0.01 and sigma for terminal atoms of 0.02
4. Others
 Fixed Sof: Cu07(0.63) Sb0D(0.67) F02H(0.67) F12(0.67) F19(0.67) F32(0.67)
 F49(0.67) F75(0.67) Ag(0.37)
5.a Ternary CH refined with riding coordinates:
 C00T(H00T), C01C(H01R), C01Q(H1AA), C01W(H5AA), C01Y(H6AA), C01Z(H7AA),
 C020(H020), C024(H024), C025(H025), C02O(H02R), C52(H52), C46(H46), C36(H36)
5.b Secondary CH2 refined with riding coordinates:
 C00U(H00A,H00B), C00Y(H00C,H00D), C011(H01A,H01B), C012(H01C,H01D), C013(H01E,
 H01F), C014(H01G,H01H), C015(H01I,H01J), C017(H01L,H01M), C01A(H01O,H01Q),
 C01D(H01T,H01U), C01G(H01Y,H), C01J(H01Z,HA), C01M(H01,HB), C01O(H0AA,HC),
 C01R(H2AA,HD), C01T(H3AA,HE), C01U(H4AA,HF), C021(H02C,H02D), C023(H02E,H02F),
 C028(H02G,H02H), C02G(H02I,H02J), C02K(H02K,H02M), C02M(H02N,H02O), C02N(H02P,
 H02Q), C02W(H02T,H02U), C29(H29A,H29B), C30(H30A,H30B)
5.c Aromatic/amide H refined with riding coordinates:
 C00V(H00V), C02V(H02V), C032(H032), C01X(H01X), C01P(H01P), C00W(H00W),
 C029(H029), C022(H022), C018(H018), C01N(H01N), C016(H016), C01H(H01K),
 C02L(H02L), C02A(H02A), C01S(H01S), C01E(H01V), C01K(H01W), C026(H026),
 C02B(H02B), C02S(H02S)
5.d Fitted hexagon refined as free rotating group:
 C00V(C02V,C032,C01X,C01P,C01B), C00W(C010,C029,C022,C018,C01N), C016(C01V,
 C01H,C02L,C02A,C01S), C01E(C01K,C026,C02B,C02S,C02D)
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag01 Ag 0.333333 0.666667 0.37692(4) 0.0554(6) Uani 1 3 d S T P A .
Ag02 Ag 0.45306(6) 0.72898(7) 0.37084(2) 0.0600(4) Uani 1 1 d . . . . .
Ag03 Ag 0.39875(7) 0.61290(7) 0.38352(2) 0.0634(4) Uani 1 1 d . . . . .
Ag04 Ag 0.37811(7) 0.63624(7) 0.34466(2) 0.0647(4) Uani 1 1 d . . . . .
Ag05 Ag 0.31187(8) 0.59856(7) 0.40967(2) 0.0725(5) Uani 1 1 d . . . . .
Ag06 Ag 0.49915(8) 0.70390(9) 0.40769(3) 0.0800(5) Uani 1 1 d . . . . .
Cu07 Cu 0.4011(4) 0.6475(3) 0.44244(16) 0.055(4) Uani 0.63 1 d . . . A 1
Cu08 Cu 0.333333 0.666667 0.31068(8) 0.0629(13) Uani 1 3 d S T P . .
Cu09 Cu 0.29843(15) 0.51467(15) 0.33316(5) 0.0730(9) Uani 1 1 d . . . . .
Cu0A Cu 0.31136(16) 0.44368(15) 0.41193(5) 0.0728(9) Uani 1 1 d . . . . .
Cu0B Cu 0.33248(15) 0.48210(14) 0.37565(5) 0.0688(8) Uani 1 1 d . . . . .
Cu0C Cu 0.42631(16) 0.53535(15) 0.42720(5) 0.0756(9) Uani 1 1 d . . . . .
Sb0D Sb 0.19165(19) 0.4193(3) 0.54840(7) 0.178(2) Uani 0.67 1 d D . . . .
S0E S 0.333333 0.666667 0.45585(14) 0.077(3) Uani 1 3 d S T P . .
Cl0F Cl 0.2070(2) 0.4988(2) 0.34073(8) 0.0720(14) Uani 1 1 d . . . . .
Cl0G Cl 0.3269(3) 0.4558(3) 0.34455(8) 0.0777(15) Uani 1 1 d . . . . .
S0H S 0.4139(3) 0.5328(3) 0.39295(8) 0.0676(13) Uani 1 1 d . . . . .
S0I S 0.3438(2) 0.5891(3) 0.31258(8) 0.0677(13) Uani 1 1 d . . . . .
S0J S 0.2440(3) 0.4489(3) 0.39111(8) 0.0713(14) Uani 1 1 d . . . . .
S0K S 0.4750(3) 0.6344(3) 0.43266(9) 0.0810(16) Uani 1 1 d . . . . .
Cl0L Cl 0.3225(3) 0.5228(3) 0.43086(8) 0.0742(14) Uani 1 1 d . . . . .
P0M P 0.3337(3) 0.3751(3) 0.41872(10) 0.0753(15) Uani 1 1 d . U . . .
P0N P 0.4244(3) 0.4657(3) 0.44585(10) 0.0782(15) Uani 1 1 d . U . . .
C00Q C 0.4012(5) 0.5898(6) 0.29696(18) 0.075(6) Uani 1 1 d D U . . .
C00R C 0.333333 0.666667 0.4831(2) 0.078(8) Uani 1 3 d DS TU P A .
C00S C 0.1803(9) 0.3786(10) 0.3835(3) 0.066(5) Uani 1 1 d . U . . .
C00T C 0.1281(11) 0.3002(11) 0.3586(4) 0.083(7) Uani 1 1 d . U . . .
H00T H 0.131095 0.287195 0.345234 0.100 Uiso 1 1 calc R . . . .
C00U C 0.3689(4) 0.5460(6) 0.2805(2) 0.072(6) Uani 1 1 d D U . . .
H00A H 0.344998 0.558114 0.273098 0.086 Uiso 1 1 calc R . . . .
H00B H 0.342896 0.507325 0.286126 0.086 Uiso 1 1 calc R . . . .
C00V C 0.4985(7) 0.4654(8) 0.4751(2) 0.083(7) Uani 1 1 d . U . . .
H00V H 0.466543 0.450503 0.483771 0.100 Uiso 1 1 calc R . . . .
C02V C 0.5525(8) 0.4774(9) 0.4818(2) 0.126(12) Uani 1 1 d G U . . .
H02V H 0.557406 0.470600 0.494992 0.152 Uiso 1 1 calc R . . . .
C032 C 0.5992(6) 0.4992(8) 0.4691(3) 0.087(7) Uani 1 1 d G U . . .
H032 H 0.636098 0.507400 0.473687 0.104 Uiso 1 1 calc R . . . .
C01X C 0.5920(6) 0.5092(8) 0.4498(2) 0.087(7) Uani 1 1 d G U . . .
H01X H 0.623928 0.524104 0.441162 0.104 Uiso 1 1 calc R . . . .
C01P C 0.5380(7) 0.4972(8) 0.44315(19) 0.088(7) Uani 1 1 d G U . . .
H01P H 0.533066 0.504006 0.429940 0.106 Uiso 1 1 calc R . . . .
C01B C 0.4913(6) 0.4754(8) 0.4558(2) 0.082(7) Uani 1 1 d G U . . .
C00W C 0.3502(7) 0.3880(6) 0.4739(2) 0.081(3) Uani 1 1 d . U . . .
H00W H 0.361911 0.361758 0.469399 0.097 Uiso 1 1 calc R . . . .
C010 C 0.3740(7) 0.4428(7) 0.4657(2) 0.077(3) Uani 1 1 d G U . . .
C029 C 0.3569(7) 0.4812(6) 0.4722(2) 0.084(3) Uani 1 1 d G U . . .
H029 H 0.373174 0.518617 0.466634 0.101 Uiso 1 1 calc R . . . .
C022 C 0.3161(7) 0.4648(7) 0.4869(2) 0.081(4) Uani 1 1 d G U . . .
H022 H 0.304384 0.491076 0.491379 0.098 Uiso 1 1 calc R . . . .
C018 C 0.2923(6) 0.4101(7) 0.4951(2) 0.082(4) Uani 1 1 d G U . . .
H018 H 0.264357 0.398877 0.505135 0.099 Uiso 1 1 calc R . . . .
C01N C 0.3094(7) 0.3716(6) 0.4886(2) 0.086(4) Uani 1 1 d G U . . .
H01N H 0.293119 0.334217 0.494145 0.103 Uiso 1 1 calc R . . . .
C00X C 0.5338(7) 0.6667(8) 0.4504(2) 0.110(4) Uani 1 1 d D U . . .
C00Y C 0.1819(10) 0.3596(10) 0.3630(3) 0.069(6) Uani 1 1 d . U . . .
H00C H 0.217236 0.356923 0.361142 0.083 Uiso 1 1 calc R . . . .
H00D H 0.183369 0.388721 0.353781 0.083 Uiso 1 1 calc R . . . .
C011 C 0.1732(10) 0.3357(10) 0.3988(3) 0.069(6) Uani 1 1 d . U . . .
H01A H 0.169004 0.349684 0.411654 0.083 Uiso 1 1 calc R . . . .
H01B H 0.208112 0.331718 0.399138 0.083 Uiso 1 1 calc R . . . .
C012 C 0.4002(12) 0.3995(11) 0.4308(4) 0.084(7) Uani 1 1 d . U . . .
H01C H 0.430276 0.407450 0.420929 0.100 Uiso 1 1 calc R . . . .
H01D H 0.396887 0.368035 0.439199 0.100 Uiso 1 1 calc R . . . .
C013 C 0.5312(6) 0.5708(6) 0.39076(16) 0.067(5) Uani 1 1 d D U . . .
H01E H 0.538867 0.610747 0.392571 0.080 Uiso 1 1 calc R . . . .
H01F H 0.527537 0.553291 0.403730 0.080 Uiso 1 1 calc R . . . .
C014 C 0.5099(12) 0.6361(14) 0.4702(3) 0.112(4) Uani 1 1 d D U . . .
H01G H 0.477635 0.641744 0.474354 0.135 Uiso 1 1 calc R . . . .
H01H H 0.494660 0.594038 0.468664 0.135 Uiso 1 1 calc R . . . .
C015 C 0.1252(10) 0.2573(9) 0.3735(3) 0.067(5) Uani 1 1 d . U . . .
H01I H 0.160714 0.254392 0.372648 0.080 Uiso 1 1 calc R . . . .
H01J H 0.091769 0.218654 0.370615 0.080 Uiso 1 1 calc R . . . .
C016 C 0.3208(7) 0.3453(7) 0.3793(3) 0.072(6) Uani 1 1 d . U . . .
H016 H 0.298125 0.363640 0.378804 0.086 Uiso 1 1 calc R . . . .
C01V C 0.3437(8) 0.3407(8) 0.3969(2) 0.093(8) Uani 1 1 d G U . . .
C01H C 0.3769(8) 0.3139(8) 0.3976(2) 0.080(7) Uani 1 1 d G U . . .
H01K H 0.392574 0.310773 0.409587 0.097 Uiso 1 1 calc R . . . .
C02L C 0.3871(7) 0.2918(8) 0.3808(3) 0.084(7) Uani 1 1 d G U . . .
H02L H 0.409727 0.273472 0.381246 0.101 Uiso 1 1 calc R . . . .
C02A C 0.3641(9) 0.2964(9) 0.3632(2) 0.113(10) Uani 1 1 d G U . . .
H02A H 0.371080 0.281254 0.351683 0.136 Uiso 1 1 calc R . . . .
C01S C 0.3310(8) 0.3232(8) 0.3625(2) 0.097(8) Uani 1 1 d G U . . .
H01S H 0.315279 0.326338 0.350462 0.117 Uiso 1 1 calc R . . . .
C017 C 0.4628(5) 0.4727(4) 0.3767(2) 0.061(5) Uani 1 1 d D U . . .
H01L H 0.426401 0.449429 0.369446 0.073 Uiso 1 1 calc R . . . .
H01M H 0.458616 0.454639 0.389625 0.073 Uiso 1 1 calc R . . . .
C01A C 0.5188(7) 0.5013(7) 0.34544(18) 0.103(9) Uani 1 1 d D U . . .
H01O H 0.550521 0.501306 0.338000 0.124 Uiso 1 1 calc R . . . .
H01Q H 0.482409 0.478483 0.338131 0.124 Uiso 1 1 calc R . . . .
C01C C 0.4820(6) 0.5669(7) 0.2949(2) 0.087(5) Uani 1 1 d D U . . .
H01R H 0.505684 0.554224 0.302459 0.105 Uiso 1 1 calc R . . . .
C01D C 0.5876(5) 0.5993(6) 0.3595(2) 0.083(7) Uani 1 1 d D U . . .
H01T H 0.595481 0.639464 0.361005 0.099 Uiso 1 1 calc R . . . .
H01U H 0.620324 0.600464 0.352346 0.099 Uiso 1 1 calc R . . . .
C01E C 0.2356(8) 0.3234(6) 0.4424(3) 0.087(3) Uani 1 1 d . U . . .
H01V H 0.233859 0.357420 0.439766 0.105 Uiso 1 1 calc R . . . .
C01K C 0.1949(7) 0.2812(8) 0.4546(3) 0.092(4) Uani 1 1 d G U . . .
H01W H 0.165451 0.286392 0.460299 0.110 Uiso 1 1 calc R . . . .
C026 C 0.1975(7) 0.2315(7) 0.4585(2) 0.091(4) Uani 1 1 d G U . . .
H026 H 0.169683 0.202626 0.466816 0.109 Uiso 1 1 calc R . . . .
C02B C 0.2406(8) 0.2239(6) 0.4502(3) 0.092(4) Uani 1 1 d G U . . .
H02B H 0.242323 0.189887 0.452800 0.110 Uiso 1 1 calc R . . . .
C02S C 0.2812(7) 0.2661(8) 0.4380(3) 0.088(3) Uani 1 1 d G U . . .
H02S H 0.310731 0.260913 0.432266 0.106 Uiso 1 1 calc R . . . .
C02D C 0.2787(7) 0.3158(7) 0.4341(2) 0.085(3) Uani 1 1 d G U . . .
C01G C 0.4811(6) 0.5626(6) 0.35892(19) 0.061(5) Uani 1 1 d D U . . .
H01Y H 0.444823 0.540039 0.351476 0.074 Uiso 1 1 calc R . . . .
H H 0.488197 0.602549 0.360359 0.074 Uiso 1 1 calc R . . . .
C01I C 0.4747(5) 0.5352(5) 0.37919(17) 0.067(5) Uani 1 1 d D U . . .
C01J C 0.0754(10) 0.3078(11) 0.3599(4) 0.075(6) Uani 1 1 d . U . . .
H01Z H 0.039694 0.271258 0.356775 0.091 Uiso 1 1 calc R . . . .
HA H 0.079044 0.338347 0.350956 0.091 Uiso 1 1 calc R . . . .
C01M C 0.4377(7) 0.5699(7) 0.30848(17) 0.094(8) Uani 1 1 d D U . . .
H01 H 0.458152 0.597420 0.319172 0.113 Uiso 1 1 calc R . . . .
HB H 0.412140 0.531377 0.314216 0.113 Uiso 1 1 calc R . . . .
C01O C 0.4498(7) 0.5236(6) 0.2787(3) 0.099(8) Uani 1 1 d D U . . .
H0AA H 0.424193 0.484920 0.284288 0.118 Uiso 1 1 calc R . . . .
HC H 0.477899 0.520878 0.270014 0.118 Uiso 1 1 calc R . . . .
C01Q C 0.5817(4) 0.5717(6) 0.3796(2) 0.089(7) Uani 1 1 d D U . . .
H1AA H 0.618346 0.594852 0.387029 0.107 Uiso 1 1 calc R . . . .
C01R C 0.5218(5) 0.6277(7) 0.2863(2) 0.089(5) Uani 1 1 d D U . . .
H2AA H 0.542455 0.655594 0.296865 0.107 Uiso 1 1 calc R . . . .
HD H 0.550987 0.626610 0.277696 0.107 Uiso 1 1 calc R . . . .
C01T C 0.3415(8) 0.7247(3) 0.5200(2) 0.095(8) Uani 1 1 d D U . . .
H3AA H 0.346594 0.761899 0.515147 0.114 Uiso 1 1 calc R . . . .
HE H 0.341744 0.725866 0.534347 0.114 Uiso 1 1 calc R . . . .
C01U C 0.5749(9) 0.7234(9) 0.4881(2) 0.112(4) Uani 1 1 d D U . . .
H4AA H 0.603867 0.740154 0.498650 0.135 Uiso 1 1 calc R . . . .
HF H 0.541236 0.727392 0.491755 0.135 Uiso 1 1 calc R . . . .
C01W C 0.1192(11) 0.2757(11) 0.3946(4) 0.081(7) Uani 1 1 d . U . . .
H5AA H 0.117381 0.246636 0.404149 0.097 Uiso 1 1 calc R . . . .
C01Y C 0.4134(6) 0.5430(6) 0.26686(19) 0.111(10) Uani 1 1 d D U . . .
H6AA H 0.392788 0.514780 0.256177 0.133 Uiso 1 1 calc R . . . .
C01Z C 0.3914(3) 0.7169(5) 0.5128(2) 0.098(8) Uani 1 1 d D U . . .
H7AA H 0.428494 0.748863 0.518136 0.118 Uiso 1 1 calc R . . . .
C020 C 0.5558(8) 0.6591(8) 0.4855(2) 0.115(4) Uani 1 1 d D U . . .
H020 H 0.539566 0.637960 0.498014 0.138 Uiso 1 1 calc R . . . .
C021 C 0.1265(11) 0.3853(11) 0.3856(4) 0.078(6) Uani 1 1 d . U . . .
H02C H 0.124699 0.399000 0.398776 0.094 Uiso 1 1 calc R . . . .
H02D H 0.127735 0.413432 0.376008 0.094 Uiso 1 1 calc R . . . .
C023 C 0.3951(3) 0.7184(5) 0.4903(2) 0.096(8) Uani 1 1 d D U . . .
H02E H 0.426751 0.711966 0.485844 0.115 Uiso 1 1 calc R . . A .
H02F H 0.402124 0.756000 0.485222 0.115 Uiso 1 1 calc R . . . .
C024 C 0.5312(6) 0.5636(6) 0.34795(15) 0.093(8) Uani 1 1 d D U . . .
H024 H 0.535076 0.581546 0.334903 0.112 Uiso 1 1 calc R . . . .
C025 C 0.0745(12) 0.3259(12) 0.3820(4) 0.087(7) Uani 1 1 d . U . . .
H025 H 0.040319 0.331530 0.382913 0.104 Uiso 1 1 calc R . . . .
C028 C 0.6071(9) 0.6523(8) 0.4792(3) 0.113(4) Uani 1 1 d D U . . .
H02G H 0.594225 0.610827 0.477473 0.136 Uiso 1 1 calc R . . . .
H02H H 0.637246 0.667896 0.489401 0.136 Uiso 1 1 calc R . . . .
C02G C 0.0644(12) 0.2817(12) 0.3967(4) 0.089(7) Uani 1 1 d . U . . .
H02I H 0.028776 0.244672 0.393792 0.106 Uiso 1 1 calc R . . . .
H02J H 0.061427 0.294697 0.409839 0.106 Uiso 1 1 calc R . . . .
F02H F 0.1825(14) 0.3653(11) 0.5305(4) 0.26(3) Uani 0.67 1 d D U . . .
C02K C 0.5542(9) 0.7320(8) 0.4529(3) 0.111(4) Uani 1 1 d D U . . .
H02K H 0.521260 0.737009 0.456638 0.134 Uiso 1 1 calc R . . . .
H02M H 0.570271 0.752656 0.440491 0.134 Uiso 1 1 calc R . . . .
C02M C 0.4530(7) 0.6037(7) 0.25820(16) 0.092(5) Uani 1 1 d D U . . .
H02N H 0.481285 0.602411 0.249221 0.110 Uiso 1 1 calc R . . . .
H02O H 0.429517 0.616267 0.250757 0.110 Uiso 1 1 calc R . . . .
C02N C 0.4405(7) 0.6504(5) 0.2880(2) 0.075(6) Uani 1 1 d D U . . .
H02P H 0.416921 0.662572 0.280473 0.090 Uiso 1 1 calc R . . . .
H02Q H 0.460611 0.679050 0.298453 0.090 Uiso 1 1 calc R . . . .
C02O C 0.6015(8) 0.7566(6) 0.4690(3) 0.113(4) Uani 1 1 d D U . . .
H02R H 0.615222 0.798590 0.470887 0.136 Uiso 1 1 calc R . . . .
C02W C 0.5701(6) 0.5096(7) 0.3771(2) 0.100(9) Uani 1 1 d D U . . .
H02T H 0.566807 0.491798 0.389987 0.120 Uiso 1 1 calc R . . . .
H02U H 0.602724 0.510084 0.370076 0.120 Uiso 1 1 calc R . . . .
C29 C 0.6528(6) 0.7489(7) 0.4631(3) 0.112(4) Uani 1 1 d D U . . .
H29A H 0.670223 0.770470 0.450960 0.134 Uiso 1 1 calc R . . . .
H29B H 0.682639 0.764776 0.473370 0.134 Uiso 1 1 calc R . . . .
C30 C 0.5852(9) 0.6596(8) 0.4442(2) 0.113(4) Uani 1 1 d D U . . .
H30A H 0.601154 0.680050 0.431748 0.136 Uiso 1 1 calc R . . . .
H30B H 0.572048 0.618132 0.442188 0.136 Uiso 1 1 calc R . . . .
C52 C 0.6327(7) 0.6847(8) 0.4600(3) 0.114(4) Uani 1 1 d D U . . .
H52 H 0.666201 0.680122 0.456015 0.137 Uiso 1 1 calc R . . . .
C46 C 0.4852(6) 0.6470(5) 0.2746(2) 0.096(5) Uani 1 1 d D U . . .
H46 H 0.511200 0.686048 0.268913 0.115 Uiso 1 1 calc R . . . .
C36 C 0.5137(6) 0.4738(5) 0.3656(2) 0.106(9) Uani 1 1 d D U . . .
H36 H 0.506172 0.433444 0.363969 0.127 Uiso 1 1 calc R . . . .
F12 F 0.2569(11) 0.4230(15) 0.5575(6) 0.26(3) Uani 0.67 1 d D U . . .
F19 F 0.1199(8) 0.4071(16) 0.5436(6) 0.193(16) Uani 0.67 1 d D U . . .
F32 F 0.1558(18) 0.3649(12) 0.5667(4) 0.200(18) Uani 0.67 1 d D U . . .
F49 F 0.2316(15) 0.4772(11) 0.5315(4) 0.22(2) Uani 0.67 1 d D U . . .
F75 F 0.2160(18) 0.4928(12) 0.5560(12) 0.35(4) Uani 0.67 1 d D U . . .
Ag Ag 0.4003(6) 0.6462(6) 0.44283(18) 0.108(6) Uani 0.37 1 d . . . A 2


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag01 Ag02 2.8024(16) . ?
Ag01 Ag02 2.8025(16) 3_565 ?
Ag01 Ag02 2.8025(16) 2_665 ?
Ag01 Ag03 2.7991(17) 2_665 ?
Ag01 Ag03 2.7991(17) 3_565 ?
Ag01 Ag03 2.7990(17) . ?
Ag01 Ag04 2.830(2) 3_565 ?
Ag01 Ag04 2.830(2) 2_665 ?
Ag01 Ag04 2.830(2) . ?
Ag01 Ag05 2.773(3) 2_665 ?
Ag01 Ag05 2.773(3) . ?
Ag01 Ag05 2.773(3) 3_565 ?
Ag02 Ag03 2.826(2) . ?
Ag02 Ag03 2.976(2) 2_665 ?
Ag02 Ag04 2.906(2) . ?
Ag02 Ag04 3.145(2) 2_665 ?
Ag02 Ag05 2.943(2) 2_665 ?
Ag02 Ag06 3.040(2) . ?
Ag02 Cu09 2.893(4) 2_665 ?
Ag02 Cu0B 2.830(4) 2_665 ?
Ag02 Cl0F 2.643(6) 2_665 ?
Ag02 S0J 2.704(6) 2_665 ?
Ag03 Ag04 2.865(2) . ?
Ag03 Ag05 3.203(2) 2_665 ?
Ag03 Ag05 2.810(2) . ?
Ag03 Ag06 3.059(3) . ?
Ag03 Cu0B 3.074(4) . ?
Ag03 S0H 2.455(6) . ?
Ag04 Ag04 3.032(3) 3_565 ?
Ag04 Ag04 3.032(3) 2_665 ?
Ag04 Cu08 2.924(5) . ?
Ag04 Cu09 2.965(4) . ?
Ag04 Cl0F 2.874(6) 2_665 ?
Ag04 S0I 2.482(6) . ?
Ag05 Ag05 2.791(3) 3_565 ?
Ag05 Ag05 2.791(3) 2_665 ?
Ag05 Ag06 2.748(3) 3_565 ?
Ag05 Cu07 2.860(11) 3_565 ?
Ag05 Cu07 3.062(10) . ?
Ag05 Cl0L 2.623(6) . ?
Ag05 Ag 3.069(13) . ?
Ag06 S0J 2.408(6) 2_665 ?
Ag06 S0K 2.372(7) . ?
Ag06 Ag 3.338(14) . ?
Cu07 S0E 2.307(12) . ?
Cu07 S0K 2.273(14) . ?
Cu08 S0I 2.230(6) 3_565 ?
Cu08 S0I 2.230(6) . ?
Cu08 S0I 2.230(6) 2_665 ?
Cu09 Cl0F 2.321(7) . ?
Cu09 Cl0G 2.206(7) . ?
Cu09 S0I 2.241(7) . ?
Cu0A Cu0B 2.654(5) . ?
Cu0A Cu0C 3.003(5) . ?
Cu0A S0J 2.358(7) . ?
Cu0A Cl0L 2.373(7) . ?
Cu0A P0M 2.242(7) . ?
Cu0B Cl0G 2.238(7) . ?
Cu0B S0H 2.246(7) . ?
Cu0B S0J 2.325(7) . ?
Cu0C S0H 2.379(7) . ?
Cu0C S0K 2.322(8) . ?
Cu0C Cl0L 2.635(7) . ?
Cu0C P0N 2.241(7) . ?
Sb0D F02H 1.817(9) . ?
Sb0D F12 1.809(10) . ?
Sb0D F19 1.807(10) . ?
Sb0D F32 1.798(10) . ?
Sb0D F49 1.801(10) . ?
Sb0D F75 1.812(10) . ?
S0E C00R 1.88(2) . ?
S0E Ag 2.300(16) . ?
S0H C01I 1.854(11) . ?
S0I C00Q 1.865(12) . ?
S0J C00S 1.87(2) . ?
S0K C00X 1.831(14) . ?
S0K Ag 2.281(17) . ?
P0M C012 1.76(3) . ?
P0M C01V 1.853(14) . ?
P0M C02D 1.861(14) . ?
P0N C01B 1.807(14) . ?
P0N C010 1.798(14) . ?
P0N C012 1.87(3) . ?
C00Q C00U 1.545(8) . ?
C00Q C01M 1.543(8) . ?
C00Q C02N 1.550(8) . ?
C00R C023 1.612(4) . ?
C00R C023 1.612(4) 3_565 ?
C00R C023 1.612(4) 2_665 ?
C00S C00Y 1.51(3) . ?
C00S C011 1.50(3) . ?
C00S C021 1.54(3) . ?
C00T C00Y 1.55(3) . ?
C00T C015 1.51(4) . ?
C00T C01J 1.52(3) . ?
C00U C01Y 1.551(8) . ?
C00V C02V 1.3900 . ?
C00V C01B 1.3900 . ?
C02V C032 1.3900 . ?
C032 C01X 1.3900 . ?
C01X C01P 1.3900 . ?
C01P C01B 1.3900 . ?
C00W C010 1.3900 . ?
C00W C01N 1.3900 . ?
C010 C029 1.3900 . ?
C029 C022 1.3900 . ?
C022 C018 1.3900 . ?
C018 C01N 1.3900 . ?
C00X C014 1.555(10) . ?
C00X C02K 1.553(9) . ?
C00X C30 1.540(8) . ?
C011 C01W 1.56(3) . ?
C013 C01I 1.545(8) . ?
C013 C01Q 1.542(8) . ?
C014 C020 1.50(3) . ?
C015 C01W 1.57(3) . ?
C016 C01V 1.3900 . ?
C016 C01S 1.3900 . ?
C01V C01H 1.3900 . ?
C01H C02L 1.3900 . ?
C02L C02A 1.3900 . ?
C02A C01S 1.3900 . ?
C017 C01I 1.545(8) . ?
C017 C36 1.547(8) . ?
C01A C024 1.535(8) . ?
C01A C36 1.546(8) . ?
C01C C01M 1.540(8) . ?
C01C C01O 1.530(8) . ?
C01C C01R 1.547(8) . ?
C01D C01Q 1.541(8) . ?
C01D C024 1.540(8) . ?
C01E C01K 1.3900 . ?
C01E C02D 1.3900 . ?
C01K C026 1.3900 . ?
C026 C02B 1.3900 . ?
C02B C02S 1.3900 . ?
C02S C02D 1.3900 . ?
C01G C01I 1.547(8) . ?
C01G C024 1.527(9) . ?
C01J C025 1.60(4) . ?
C01O C01Y 1.541(8) . ?
C01Q C02W 1.538(8) . ?
C01R C46 1.541(8) . ?
C01T C01Z 1.546(5) 2_665 ?
C01T C01Z 1.531(5) . ?
C01U C020 1.539(8) . ?
C01U C02O 1.550(8) . ?
C01W C02G 1.56(4) . ?
C01Y C02M 1.546(8) . ?
C01Z C023 1.554(5) . ?
C020 C028 1.534(9) . ?
C021 C025 1.52(4) . ?
C025 C02G 1.47(4) . ?
C028 C52 1.540(9) . ?
C02K C02O 1.558(8) . ?
C02M C46 1.538(8) . ?
C02N C46 1.547(10) . ?
C02O C29 1.538(8) . ?
C02W C36 1.540(8) . ?
C29 C52 1.533(9) . ?
C30 C52 1.550(8) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Ag02 Ag01 Ag02 117.80(3) 2_665 . ?
Ag02 Ag01 Ag02 117.80(3) . 3_565 ?
Ag02 Ag01 Ag02 117.80(3) 2_665 3_565 ?
Ag02 Ag01 Ag04 67.88(6) 3_565 . ?
Ag02 Ag01 Ag04 119.45(9) . 3_565 ?
Ag02 Ag01 Ag04 119.46(9) 2_665 . ?
Ag02 Ag01 Ag04 67.87(6) . 2_665 ?
Ag02 Ag01 Ag04 62.11(5) 3_565 3_565 ?
Ag02 Ag01 Ag04 119.46(9) 3_565 2_665 ?
Ag02 Ag01 Ag04 62.11(5) . . ?
Ag02 Ag01 Ag04 67.88(6) 2_665 3_565 ?
Ag02 Ag01 Ag04 62.11(5) 2_665 2_665 ?
Ag03 Ag01 Ag02 178.00(7) 3_565 . ?
Ag03 Ag01 Ag02 60.60(5) 3_565 3_565 ?
Ag03 Ag01 Ag02 64.18(5) 3_565 2_665 ?
Ag03 Ag01 Ag02 60.60(5) . . ?
Ag03 Ag01 Ag02 64.18(5) 2_665 . ?
Ag03 Ag01 Ag02 60.60(5) 2_665 2_665 ?
Ag03 Ag01 Ag02 178.00(7) . 2_665 ?
Ag03 Ag01 Ag02 178.00(7) 2_665 3_565 ?
Ag03 Ag01 Ag02 64.18(5) . 3_565 ?
Ag03 Ag01 Ag03 117.41(3) 2_665 3_565 ?
Ag03 Ag01 Ag03 117.41(3) 2_665 . ?
Ag03 Ag01 Ag03 117.41(3) 3_565 . ?
Ag03 Ag01 Ag04 61.20(5) 2_665 2_665 ?
Ag03 Ag01 Ag04 61.20(5) 3_565 3_565 ?
Ag03 Ag01 Ag04 113.84(7) 2_665 . ?
Ag03 Ag01 Ag04 113.84(7) 3_565 2_665 ?
Ag03 Ag01 Ag04 61.19(5) . . ?
Ag03 Ag01 Ag04 117.42(7) . 2_665 ?
Ag03 Ag01 Ag04 117.42(7) 3_565 . ?
Ag03 Ag01 Ag04 117.43(7) 2_665 3_565 ?
Ag03 Ag01 Ag04 113.84(7) . 3_565 ?
Ag04 Ag01 Ag04 64.78(7) 3_565 . ?
Ag04 Ag01 Ag04 64.78(7) 2_665 . ?
Ag04 Ag01 Ag04 64.78(7) 2_665 3_565 ?
Ag05 Ag01 Ag02 108.16(7) . . ?
Ag05 Ag01 Ag02 119.76(8) 2_665 3_565 ?
Ag05 Ag01 Ag02 63.72(5) . 3_565 ?
Ag05 Ag01 Ag02 63.72(5) 2_665 . ?
Ag05 Ag01 Ag02 119.76(8) 3_565 . ?
Ag05 Ag01 Ag02 119.76(8) . 2_665 ?
Ag05 Ag01 Ag02 108.16(7) 3_565 3_565 ?
Ag05 Ag01 Ag02 63.72(5) 3_565 2_665 ?
Ag05 Ag01 Ag02 108.16(7) 2_665 2_665 ?
Ag05 Ag01 Ag03 60.55(6) 2_665 2_665 ?
Ag05 Ag01 Ag03 70.16(6) 2_665 . ?
Ag05 Ag01 Ag03 70.16(6) . 3_565 ?
Ag05 Ag01 Ag03 60.55(6) 3_565 3_565 ?
Ag05 Ag01 Ag03 115.74(9) . 2_665 ?
Ag05 Ag01 Ag03 115.74(9) 3_565 . ?
Ag05 Ag01 Ag03 70.16(6) 3_565 2_665 ?
Ag05 Ag01 Ag03 115.74(9) 2_665 3_565 ?
Ag05 Ag01 Ag03 60.56(6) . . ?
Ag05 Ag01 Ag04 119.47(5) . 3_565 ?
Ag05 Ag01 Ag04 175.62(6) 3_565 . ?
Ag05 Ag01 Ag04 115.43(5) . . ?
Ag05 Ag01 Ag04 115.43(5) 2_665 2_665 ?
Ag05 Ag01 Ag04 119.47(5) 2_665 . ?
Ag05 Ag01 Ag04 119.47(5) 3_565 2_665 ?
Ag05 Ag01 Ag04 175.63(6) 2_665 3_565 ?
Ag05 Ag01 Ag04 115.44(5) 3_565 3_565 ?
Ag05 Ag01 Ag04 175.62(6) . 2_665 ?
Ag05 Ag01 Ag05 60.42(7) 2_665 . ?
Ag05 Ag01 Ag05 60.42(7) 3_565 . ?
Ag05 Ag01 Ag05 60.42(7) 3_565 2_665 ?
Ag01 Ag02 Ag03 59.64(5) . . ?
Ag01 Ag02 Ag03 57.85(4) . 2_665 ?
Ag01 Ag02 Ag04 59.41(6) . . ?
Ag01 Ag02 Ag04 56.48(6) . 2_665 ?
Ag01 Ag02 Ag05 57.65(7) . 2_665 ?
Ag01 Ag02 Ag06 102.23(7) . . ?
Ag01 Ag02 Cu09 113.44(10) . 2_665 ?
Ag01 Ag02 Cu0B 121.73(9) . 2_665 ?
Ag03 Ag02 Ag03 111.05(8) . 2_665 ?
Ag03 Ag02 Ag04 55.75(5) 2_665 2_665 ?
Ag03 Ag02 Ag04 107.24(6) . 2_665 ?
Ag03 Ag02 Ag04 59.97(5) . . ?
Ag03 Ag02 Ag05 67.40(6) . 2_665 ?
Ag03 Ag02 Ag06 105.99(7) 2_665 . ?
Ag03 Ag02 Ag06 62.75(6) . . ?
Ag03 Ag02 Cu09 133.83(10) . 2_665 ?
Ag03 Ag02 Cu0B 154.88(10) . 2_665 ?
Ag04 Ag02 Ag03 106.63(6) . 2_665 ?
Ag04 Ag02 Ag04 60.00(7) . 2_665 ?
Ag04 Ag02 Ag05 111.67(7) . 2_665 ?
Ag04 Ag02 Ag06 120.88(7) . . ?
Ag05 Ag02 Ag03 56.67(6) 2_665 2_665 ?
Ag05 Ag02 Ag04 102.13(7) 2_665 2_665 ?
Ag05 Ag02 Ag06 54.65(6) 2_665 . ?
Ag06 Ag02 Ag04 156.44(7) . 2_665 ?
Cu09 Ag02 Ag03 96.20(9) 2_665 2_665 ?
Cu09 Ag02 Ag04 77.17(9) 2_665 . ?
Cu09 Ag02 Ag04 58.66(8) 2_665 2_665 ?
Cu09 Ag02 Ag05 152.65(10) 2_665 2_665 ?
Cu09 Ag02 Ag06 144.15(10) 2_665 . ?
Cu0B Ag02 Ag03 63.89(8) 2_665 2_665 ?
Cu0B Ag02 Ag04 144.67(9) 2_665 . ?
Cu0B Ag02 Ag04 90.28(9) 2_665 2_665 ?
Cu0B Ag02 Ag05 91.79(9) 2_665 2_665 ?
Cu0B Ag02 Ag06 94.09(9) 2_665 . ?
Cu0B Ag02 Cu09 70.65(10) 2_665 2_665 ?
Cl0F Ag02 Ag01 121.56(15) 2_665 . ?
Cl0F Ag02 Ag03 92.79(14) 2_665 . ?
Cl0F Ag02 Ag03 144.37(14) 2_665 2_665 ?
Cl0F Ag02 Ag04 62.17(14) 2_665 . ?
Cl0F Ag02 Ag04 92.75(14) 2_665 2_665 ?
Cl0F Ag02 Ag05 157.94(15) 2_665 2_665 ?
Cl0F Ag02 Ag06 108.45(14) 2_665 . ?
Cl0F Ag02 Cu09 49.33(14) 2_665 2_665 ?
Cl0F Ag02 Cu0B 104.47(16) 2_665 2_665 ?
Cl0F Ag02 S0J 97.42(19) 2_665 2_665 ?
S0J Ag02 Ag01 139.12(15) 2_665 . ?
S0J Ag02 Ag03 98.15(14) 2_665 2_665 ?
S0J Ag02 Ag03 110.85(14) 2_665 . ?
S0J Ag02 Ag04 139.90(14) 2_665 2_665 ?
S0J Ag02 Ag04 155.22(15) 2_665 . ?
S0J Ag02 Ag05 81.67(13) 2_665 2_665 ?
S0J Ag02 Ag06 49.13(13) 2_665 . ?
S0J Ag02 Cu09 100.76(15) 2_665 2_665 ?
S0J Ag02 Cu0B 49.62(15) 2_665 2_665 ?
Ag01 Ag03 Ag02 57.97(4) . 3_565 ?
Ag01 Ag03 Ag02 59.76(5) . . ?
Ag01 Ag03 Ag04 59.94(7) . . ?
Ag01 Ag03 Ag05 54.54(6) . 2_665 ?
Ag01 Ag03 Ag05 59.27(6) . . ?
Ag01 Ag03 Ag06 101.83(7) . . ?
Ag01 Ag03 Cu0B 113.71(8) . . ?
Ag02 Ag03 Ag02 111.60(7) . 3_565 ?
Ag02 Ag03 Ag04 61.40(6) . . ?
Ag02 Ag03 Ag05 58.04(5) . 2_665 ?
Ag02 Ag03 Ag05 102.57(6) 3_565 2_665 ?
Ag02 Ag03 Ag06 62.05(6) . . ?
Ag02 Ag03 Ag06 154.10(7) 3_565 . ?
Ag02 Ag03 Cu0B 151.71(9) . . ?
Ag02 Ag03 Cu0B 55.76(8) 3_565 . ?
Ag04 Ag03 Ag02 65.11(6) . 3_565 ?
Ag04 Ag03 Ag05 105.66(7) . 2_665 ?
Ag04 Ag03 Ag06 121.59(7) . . ?
Ag04 Ag03 Cu0B 91.05(8) . . ?
Ag05 Ag03 Ag02 61.08(6) . 3_565 ?
Ag05 Ag03 Ag02 106.49(7) . . ?
Ag05 Ag03 Ag04 113.18(7) . . ?
Ag05 Ag03 Ag05 54.84(7) . 2_665 ?
Ag05 Ag03 Ag06 95.46(7) . . ?
Ag05 Ag03 Cu0B 89.49(9) . . ?
Ag06 Ag03 Ag05 52.00(6) . 2_665 ?
Ag06 Ag03 Cu0B 140.99(9) . . ?
Cu0B Ag03 Ag05 144.12(9) . 2_665 ?
S0H Ag03 Ag01 155.16(16) . . ?
S0H Ag03 Ag02 100.11(16) . 3_565 ?
S0H Ag03 Ag02 145.07(16) . . ?
S0H Ag03 Ag04 124.79(15) . . ?
S0H Ag03 Ag05 129.51(15) . 2_665 ?
S0H Ag03 Ag05 101.33(15) . . ?
S0H Ag03 Ag06 94.98(16) . . ?
S0H Ag03 Cu0B 46.28(16) . . ?
Ag01 Ag04 Ag02 55.64(4) . 3_565 ?
Ag01 Ag04 Ag02 58.48(5) . . ?
Ag01 Ag04 Ag03 58.87(5) . . ?
Ag01 Ag04 Ag04 57.61(4) . 2_665 ?
Ag01 Ag04 Ag04 57.61(4) . 3_565 ?
Ag01 Ag04 Cu08 105.01(9) . . ?
Ag01 Ag04 Cu09 110.46(9) . . ?
Ag01 Ag04 Cl0F 112.87(13) . 2_665 ?
Ag02 Ag04 Ag02 104.91(7) . 3_565 ?
Ag02 Ag04 Ag04 63.91(6) . 2_665 ?
Ag02 Ag04 Ag04 110.00(5) . 3_565 ?
Ag02 Ag04 Cu08 117.62(7) . . ?
Ag02 Ag04 Cu09 155.66(10) . . ?
Ag03 Ag04 Ag02 58.64(5) . . ?
Ag03 Ag04 Ag02 59.14(5) . 3_565 ?
Ag03 Ag04 Ag04 109.28(5) . 2_665 ?
Ag03 Ag04 Ag04 106.19(5) . 3_565 ?
Ag03 Ag04 Cu08 163.57(9) . . ?
Ag03 Ag04 Cu09 97.03(9) . . ?
Ag03 Ag04 Cl0F 87.32(13) . 2_665 ?
Ag04 Ag04 Ag02 103.90(5) 2_665 3_565 ?
Ag04 Ag04 Ag02 56.09(6) 3_565 3_565 ?
Ag04 Ag04 Ag04 60.0 3_565 2_665 ?
Cu08 Ag04 Ag02 110.47(7) . 3_565 ?
Cu08 Ag04 Ag04 58.77(6) . 2_665 ?
Cu08 Ag04 Ag04 58.77(6) . 3_565 ?
Cu08 Ag04 Cu09 85.46(8) . . ?
Cu09 Ag04 Ag02 56.43(8) . 3_565 ?
Cu09 Ag04 Ag04 131.59(10) . 2_665 ?
Cu09 Ag04 Ag04 74.15(10) . 3_565 ?
Cl0F Ag04 Ag02 146.14(13) 2_665 3_565 ?
Cl0F Ag04 Ag02 54.42(12) 2_665 . ?
Cl0F Ag04 Ag04 90.72(14) 2_665 2_665 ?
Cl0F Ag04 Ag04 150.27(14) 2_665 3_565 ?
Cl0F Ag04 Cu08 103.24(13) 2_665 . ?
Cl0F Ag04 Cu09 131.44(14) 2_665 . ?
S0I Ag04 Ag01 138.08(15) . . ?
S0I Ag04 Ag02 155.24(15) . . ?
S0I Ag04 Ag02 99.55(15) . 3_565 ?
S0I Ag04 Ag03 141.67(15) . . ?
S0I Ag04 Ag04 80.64(14) . 3_565 ?
S0I Ag04 Ag04 106.63(14) . 2_665 ?
S0I Ag04 Cu08 47.88(15) . . ?
S0I Ag04 Cu09 47.57(15) . . ?
S0I Ag04 Cl0F 105.30(18) . 2_665 ?
Ag01 Ag05 Ag02 58.62(5) . 3_565 ?
Ag01 Ag05 Ag03 55.30(4) . 3_565 ?
Ag01 Ag05 Ag03 60.18(5) . . ?
Ag01 Ag05 Ag05 59.79(4) . 2_665 ?
Ag01 Ag05 Ag05 59.79(4) . 3_565 ?
Ag01 Ag05 Cu07 124.53(17) . 3_565 ?
Ag01 Ag05 Cu07 117.32(17) . . ?
Ag01 Ag05 Ag 118.1(3) . . ?
Ag02 Ag05 Ag03 54.55(5) 3_565 3_565 ?
Ag02 Ag05 Cu07 150.8(2) 3_565 . ?
Ag02 Ag05 Ag 151.0(3) 3_565 . ?
Ag03 Ag05 Ag02 62.25(6) . 3_565 ?
Ag03 Ag05 Ag03 105.25(8) . 3_565 ?
Ag03 Ag05 Cu07 90.1(2) . . ?
Ag03 Ag05 Cu07 166.2(3) . 3_565 ?
Ag03 Ag05 Ag 90.5(3) . . ?
Ag05 Ag05 Ag02 114.48(5) 2_665 3_565 ?
Ag05 Ag05 Ag02 103.87(6) 3_565 3_565 ?
Ag05 Ag05 Ag03 55.39(7) 3_565 3_565 ?
Ag05 Ag05 Ag03 103.66(6) 2_665 3_565 ?
Ag05 Ag05 Ag03 69.76(8) 2_665 . ?
Ag05 Ag05 Ag03 114.83(6) 3_565 . ?
Ag05 Ag05 Ag05 60.0 2_665 3_565 ?
Ag05 Ag05 Cu07 58.29(16) 2_665 . ?
Ag05 Ag05 Cu07 100.8(2) 2_665 3_565 ?
Ag05 Ag05 Cu07 65.62(16) 3_565 3_565 ?
Ag05 Ag05 Cu07 96.0(2) 3_565 . ?
Ag05 Ag05 Ag 59.0(3) 2_665 . ?
Ag05 Ag05 Ag 96.3(3) 3_565 . ?
Ag06 Ag05 Ag01 111.00(8) 3_565 . ?
Ag06 Ag05 Ag02 64.46(6) 3_565 3_565 ?
Ag06 Ag05 Ag03 61.32(6) 3_565 3_565 ?
Ag06 Ag05 Ag03 119.65(8) 3_565 . ?
Ag06 Ag05 Ag05 163.17(11) 3_565 2_665 ?
Ag06 Ag05 Ag05 103.39(11) 3_565 3_565 ?
Ag06 Ag05 Cu07 131.34(17) 3_565 . ?
Ag06 Ag05 Cu07 72.2(2) 3_565 3_565 ?
Ag06 Ag05 Ag 130.6(3) 3_565 . ?
Cu07 Ag05 Ag02 131.5(3) 3_565 3_565 ?
Cu07 Ag05 Ag03 151.0(2) . 3_565 ?
Cu07 Ag05 Ag03 86.4(2) 3_565 3_565 ?
Cu07 Ag05 Cu07 76.3(4) 3_565 . ?
Cl0L Ag05 Ag01 153.20(15) . . ?
Cl0L Ag05 Ag02 106.29(14) . 3_565 ?
Cl0L Ag05 Ag03 93.55(14) . . ?
Cl0L Ag05 Ag03 137.24(15) . 3_565 ?
Cl0L Ag05 Ag05 145.77(13) . 3_565 ?
Cl0L Ag05 Ag05 118.91(16) . 2_665 ?
Cl0L Ag05 Ag06 75.97(15) . 3_565 ?
Cl0L Ag05 Cu07 82.2(2) . 3_565 ?
Cl0L Ag05 Cu07 63.7(2) . . ?
Cl0L Ag05 Ag 63.1(3) . . ?
Ag02 Ag06 Ag03 55.20(5) . . ?
Ag02 Ag06 Ag 113.2(3) . . ?
Ag03 Ag06 Ag 81.4(2) . . ?
Ag05 Ag06 Ag02 60.88(6) 2_665 . ?
Ag05 Ag06 Ag03 66.68(6) 2_665 . ?
Ag05 Ag06 Ag 55.8(3) 2_665 . ?
S0J Ag06 Ag02 58.14(15) 2_665 . ?
S0J Ag06 Ag03 112.27(16) 2_665 . ?
S0J Ag06 Ag05 91.38(17) 2_665 2_665 ?
S0J Ag06 Ag 137.3(3) 2_665 . ?
S0K Ag06 Ag02 142.86(19) . . ?
S0K Ag06 Ag03 89.20(18) . . ?
S0K Ag06 Ag05 97.88(19) . 2_665 ?
S0K Ag06 S0J 158.5(2) . 2_665 ?
S0K Ag06 Ag 43.1(3) . . ?
Ag05 Cu07 Ag05 56.1(2) 2_665 . ?
S0E Cu07 Ag05 82.0(4) . . ?
S0E Cu07 Ag05 86.6(4) . 2_665 ?
S0K Cu07 Ag05 97.1(4) . 2_665 ?
S0K Cu07 Ag05 105.5(4) . . ?
S0K Cu07 S0E 172.6(6) . . ?
Ag04 Cu08 Ag04 62.47(11) 2_665 3_565 ?
Ag04 Cu08 Ag04 62.46(11) 3_565 . ?
Ag04 Cu08 Ag04 62.46(11) 2_665 . ?
S0I Cu08 Ag04 55.64(17) 2_665 2_665 ?
S0I Cu08 Ag04 87.29(19) . 3_565 ?
S0I Cu08 Ag04 87.29(19) 2_665 . ?
S0I Cu08 Ag04 118.1(2) . 2_665 ?
S0I Cu08 Ag04 118.1(2) 3_565 . ?
S0I Cu08 Ag04 55.64(17) 3_565 3_565 ?
S0I Cu08 Ag04 87.29(19) 3_565 2_665 ?
S0I Cu08 Ag04 118.1(2) 2_665 3_565 ?
S0I Cu08 Ag04 55.63(17) . . ?
S0I Cu08 S0I 119.66(4) 3_565 . ?
S0I Cu08 S0I 119.66(4) 2_665 . ?
S0I Cu08 S0I 119.66(4) 3_565 2_665 ?
Ag02 Cu09 Ag04 64.92(8) 3_565 . ?
Cl0F Cu09 Ag02 59.71(16) . 3_565 ?
Cl0F Cu09 Ag04 104.68(19) . . ?
Cl0G Cu09 Ag02 95.17(19) . 3_565 ?
Cl0G Cu09 Ag04 111.8(2) . . ?
Cl0G Cu09 Cl0F 119.8(3) . . ?
Cl0G Cu09 S0I 129.1(3) . . ?
S0I Cu09 Ag02 113.9(2) . 3_565 ?
S0I Cu09 Ag04 54.83(17) . . ?
S0I Cu09 Cl0F 111.0(3) . . ?
Cu0B Cu0A Cu0C 94.69(15) . . ?
S0J Cu0A Cu0B 54.89(18) . . ?
S0J Cu0A Cu0C 131.6(2) . . ?
S0J Cu0A Cl0L 92.4(2) . . ?
Cl0L Cu0A Cu0B 105.4(2) . . ?
Cl0L Cu0A Cu0C 57.28(18) . . ?
P0M Cu0A Cu0B 114.9(2) . . ?
P0M Cu0A Cu0C 90.6(2) . . ?
P0M Cu0A S0J 134.2(3) . . ?
P0M Cu0A Cl0L 130.3(3) . . ?
Ag02 Cu0B Ag03 60.36(8) 3_565 . ?
Cu0A Cu0B Ag02 105.77(14) . 3_565 ?
Cu0A Cu0B Ag03 99.42(13) . . ?
Cl0G Cu0B Ag02 96.2(2) . 3_565 ?
Cl0G Cu0B Ag03 115.9(2) . . ?
Cl0G Cu0B Cu0A 144.4(2) . . ?
Cl0G Cu0B S0H 126.2(3) . . ?
Cl0G Cu0B S0J 115.1(3) . . ?
S0H Cu0B Ag02 110.21(19) . 3_565 ?
S0H Cu0B Ag03 52.18(16) . . ?
S0H Cu0B Cu0A 71.81(19) . . ?
S0H Cu0B S0J 118.7(2) . . ?
S0J Cu0B Ag02 62.35(17) . 3_565 ?
S0J Cu0B Ag03 104.54(19) . . ?
S0J Cu0B Cu0A 56.07(18) . . ?
S0H Cu0C Cu0A 63.80(18) . . ?
S0H Cu0C Cl0L 88.2(2) . . ?
S0K Cu0C Cu0A 138.4(2) . . ?
S0K Cu0C S0H 100.6(2) . . ?
S0K Cu0C Cl0L 94.8(3) . . ?
Cl0L Cu0C Cu0A 49.26(16) . . ?
P0N Cu0C Cu0A 86.3(2) . . ?
P0N Cu0C S0H 126.9(3) . . ?
P0N Cu0C S0K 128.3(3) . . ?
P0N Cu0C Cl0L 104.7(3) . . ?
F12 Sb0D F02H 91.3(6) . . ?
F12 Sb0D F75 91.4(6) . . ?
F19 Sb0D F02H 91.3(6) . . ?
F19 Sb0D F12 168.5(19) . . ?
F19 Sb0D F75 91.2(6) . . ?
F32 Sb0D F02H 91.7(6) . . ?
F32 Sb0D F12 85(2) . . ?
F32 Sb0D F19 84(2) . . ?
F32 Sb0D F49 175.5(16) . . ?
F32 Sb0D F75 115(3) . . ?
F49 Sb0D F02H 91.7(6) . . ?
F49 Sb0D F12 92.2(7) . . ?
F49 Sb0D F19 98.9(18) . . ?
F49 Sb0D F75 61(3) . . ?
F75 Sb0D F02H 153(3) . . ?
Cu07 S0E Cu07 105.0(4) 2_665 . ?
Cu07 S0E Cu07 105.0(4) 2_665 3_565 ?
Cu07 S0E Cu07 105.0(4) 3_565 . ?
C00R S0E Cu07 113.6(4) . . ?
C00R S0E Cu07 113.6(4) . 3_565 ?
C00R S0E Cu07 113.6(4) . 2_665 ?
C00R S0E Ag 113.0(4) . . ?
Ag S0E Cu07 106.0(5) . 2_665 ?
Ag02 Cl0F Ag04 63.41(12) 3_565 3_565 ?
Cu09 Cl0F Ag02 70.96(17) . 3_565 ?
Cu09 Cl0F Ag04 87.56(19) . 3_565 ?
Cu09 Cl0G Cu0B 96.3(3) . . ?
Cu0B S0H Ag03 81.5(2) . . ?
Cu0B S0H Cu0C 128.5(3) . . ?
Cu0C S0H Ag03 108.6(2) . . ?
C01I S0H Ag03 111.0(4) . . ?
C01I S0H Cu0B 108.4(5) . . ?
C01I S0H Cu0C 113.6(5) . . ?
Cu08 S0I Ag04 76.5(2) . . ?
Cu08 S0I Cu09 126.7(3) . . ?
Cu09 S0I Ag04 77.6(2) . . ?
C00Q S0I Ag04 114.6(5) . . ?
C00Q S0I Cu08 116.2(5) . . ?
C00Q S0I Cu09 116.9(5) . . ?
Ag06 S0J Ag02 72.73(17) 3_565 3_565 ?
Cu0A S0J Ag02 119.4(3) . 3_565 ?
Cu0A S0J Ag06 108.1(2) . 3_565 ?
Cu0B S0J Ag02 68.02(18) . 3_565 ?
Cu0B S0J Ag06 130.5(3) . 3_565 ?
Cu0B S0J Cu0A 69.0(2) . . ?
C00S S0J Ag02 121.1(8) . 3_565 ?
C00S S0J Ag06 105.7(7) . 3_565 ?
C00S S0J Cu0A 116.7(8) . . ?
C00S S0J Cu0B 119.8(7) . . ?
Cu07 S0K Ag06 90.7(4) . . ?
Cu07 S0K Cu0C 100.8(3) . . ?
Cu0C S0K Ag06 123.5(3) . . ?
C00X S0K Ag06 106.4(6) . . ?
C00X S0K Cu07 109.6(7) . . ?
C00X S0K Cu0C 120.4(7) . . ?
C00X S0K Ag 109.4(8) . . ?
Ag S0K Ag06 91.7(4) . . ?
Ag S0K Cu0C 100.1(5) . . ?
Ag05 Cl0L Cu0C 111.2(2) . . ?
Cu0A Cl0L Ag05 111.6(2) . . ?
Cu0A Cl0L Cu0C 73.5(2) . . ?
C012 P0M Cu0A 115.3(10) . . ?
C012 P0M C01V 101.4(11) . . ?
C012 P0M C02D 105.5(11) . . ?
C01V P0M Cu0A 113.5(6) . . ?
C01V P0M C02D 106.8(9) . . ?
C02D P0M Cu0A 113.2(6) . . ?
C01B P0N Cu0C 119.3(7) . . ?
C01B P0N C012 101.4(11) . . ?
C010 P0N Cu0C 114.9(6) . . ?
C010 P0N C01B 106.2(8) . . ?
C010 P0N C012 104.8(11) . . ?
C012 P0N Cu0C 108.6(9) . . ?
C00U C00Q S0I 105.7(8) . . ?
C00U C00Q C02N 109.3(6) . . ?
C01M C00Q S0I 110.9(8) . . ?
C01M C00Q C00U 109.1(6) . . ?
C01M C00Q C02N 110.4(6) . . ?
C02N C00Q S0I 111.4(8) . . ?
C023 C00R S0E 107.9(2) 3_565 . ?
C023 C00R S0E 107.9(2) . . ?
C023 C00R S0E 107.9(2) 2_665 . ?
C023 C00R C023 111.0(2) 2_665 . ?
C023 C00R C023 111.0(2) . 3_565 ?
C023 C00R C023 111.0(2) 2_665 3_565 ?
C00Y C00S S0J 115.7(15) . . ?
C00Y C00S C021 108(2) . . ?
C011 C00S S0J 106.0(15) . . ?
C011 C00S C00Y 114(2) . . ?
C011 C00S C021 104.8(19) . . ?
C021 C00S S0J 107.0(16) . . ?
C015 C00T C00Y 108(2) . . ?
C015 C00T C01J 111(2) . . ?
C01J C00T C00Y 107(2) . . ?
C00Q C00U C01Y 109.3(4) . . ?
C02V C00V C01B 120.0 . . ?
C032 C02V C00V 120.0 . . ?
C02V C032 C01X 120.0 . . ?
C032 C01X C01P 120.0 . . ?
C01B C01P C01X 120.0 . . ?
C00V C01B P0N 123.9(10) . . ?
C01P C01B P0N 116.0(10) . . ?
C01P C01B C00V 120.0 . . ?
C010 C00W C01N 120.0 . . ?
C00W C010 P0N 122.5(9) . . ?
C029 C010 P0N 117.5(9) . . ?
C029 C010 C00W 120.0 . . ?
C010 C029 C022 120.0 . . ?
C018 C022 C029 120.0 . . ?
C01N C018 C022 120.0 . . ?
C018 C01N C00W 120.0 . . ?
C014 C00X S0K 108.0(15) . . ?
C02K C00X S0K 109.9(11) . . ?
C02K C00X C014 108.5(15) . . ?
C30 C00X S0K 111.2(11) . . ?
C30 C00X C014 109.6(8) . . ?
C30 C00X C02K 109.5(6) . . ?
C00S C00Y C00T 111(2) . . ?
C00S C011 C01W 111(2) . . ?
P0M C012 P0N 114.9(16) . . ?
C01Q C013 C01I 109.2(4) . . ?
C020 C014 C00X 111.6(17) . . ?
C00T C015 C01W 111.4(19) . . ?
C01V C016 C01S 120.0 . . ?
C016 C01V P0M 119.0(10) . . ?
C016 C01V C01H 120.0 . . ?
C01H C01V P0M 120.9(10) . . ?
C02L C01H C01V 120.0 . . ?
C02A C02L C01H 120.0 . . ?
C02L C02A C01S 120.0 . . ?
C02A C01S C016 120.0 . . ?
C01I C017 C36 109.2(4) . . ?
C024 C01A C36 109.5(4) . . ?
C01M C01C C01R 108.8(6) . . ?
C01O C01C C01M 109.1(7) . . ?
C01O C01C C01R 110.1(6) . . ?
C024 C01D C01Q 109.4(4) . . ?
C01K C01E C02D 120.0 . . ?
C026 C01K C01E 120.0 . . ?
C02B C026 C01K 120.0 . . ?
C026 C02B C02S 120.0 . . ?
C02D C02S C02B 120.0 . . ?
C01E C02D P0M 118.1(10) . . ?
C02S C02D P0M 121.9(10) . . ?
C02S C02D C01E 120.0 . . ?
C024 C01G C01I 110.0(4) . . ?
C013 C01I S0H 109.1(7) . . ?
C013 C01I C017 109.3(5) . . ?
C013 C01I C01G 109.4(6) . . ?
C017 C01I S0H 108.5(7) . . ?
C017 C01I C01G 109.1(6) . . ?
C01G C01I S0H 111.4(7) . . ?
C00T C01J C025 105(2) . . ?
C01C C01M C00Q 109.9(4) . . ?
C01C C01O C01Y 110.1(4) . . ?
C01D C01Q C013 109.7(6) . . ?
C02W C01Q C013 109.7(6) . . ?
C02W C01Q C01D 109.5(7) . . ?
C46 C01R C01C 109.5(4) . . ?
C01Z C01T C01Z 110.3(3) . 2_665 ?
C020 C01U C02O 110.0(5) . . ?
C011 C01W C015 108(2) . . ?
C011 C01W C02G 108(2) . . ?
C02G C01W C015 111(2) . . ?
C01O C01Y C00U 109.0(6) . . ?
C01O C01Y C02M 109.9(6) . . ?
C02M C01Y C00U 108.7(6) . . ?
C01T C01Z C01T 109.9(4) . 3_565 ?
C01T C01Z C023 111.7(4) . . ?
C01T C01Z C023 108.7(4) 3_565 . ?
C014 C020 C01U 106.6(14) . . ?
C014 C020 C028 110.3(10) . . ?
C028 C020 C01U 110.3(7) . . ?
C025 C021 C00S 106(2) . . ?
C01Z C023 C00R 105.1(3) . . ?
C01A C024 C01D 110.1(6) . . ?
C01G C024 C01A 109.0(7) . . ?
C01G C024 C01D 109.5(7) . . ?
C021 C025 C01J 109(2) . . ?
C02G C025 C01J 116(2) . . ?
C02G C025 C021 115(2) . . ?
C020 C028 C52 110.6(5) . . ?
C025 C02G C01W 102(2) . . ?
C00X C02K C02O 107.9(6) . . ?
C46 C02M C01Y 109.7(4) . . ?
C46 C02N C00Q 108.4(6) . . ?
C01U C02O C02K 108.8(7) . . ?
C29 C02O C01U 109.3(6) . . ?
C29 C02O C02K 110.2(6) . . ?
C01Q C02W C36 109.4(4) . . ?
C52 C29 C02O 110.5(5) . . ?
C00X C30 C52 109.7(4) . . ?
C028 C52 C30 108.9(7) . . ?
C29 C52 C028 108.6(7) . . ?
C29 C52 C30 109.5(7) . . ?
C01R C46 C02N 110.3(8) . . ?
C02M C46 C01R 110.0(6) . . ?
C02M C46 C02N 109.0(8) . . ?
C01A C36 C017 108.9(6) . . ?
C02W C36 C017 109.6(5) . . ?
C02W C36 C01A 109.9(6) . . ?
Ag05 Ag Ag05 55.7(2) 2_665 . ?
Ag05 Ag Ag06 51.7(2) 2_665 . ?
Ag05 Ag Ag06 85.3(3) . . ?
S0E Ag Ag05 85.9(5) . 2_665 ?
S0E Ag Ag05 81.9(5) . . ?
S0E Ag Ag06 134.7(6) . . ?
S0K Ag Ag05 105.1(5) . . ?
S0K Ag Ag05 96.0(5) . 2_665 ?
S0K Ag Ag06 45.3(3) . . ?
S0K Ag S0E 172.6(7) . . ?

_platon_squeeze_details          ?
loop_
_platon_squeeze_void_nr
_platon_squeeze_void_average_x
_platon_squeeze_void_average_y
_platon_squeeze_void_average_z
_platon_squeeze_void_volume
_platon_squeeze_void_count_electrons
_platon_squeeze_void_content
1 -0.107 -0.097 -0.002 13089 3958 ' '
2 0.447 0.053 0.991 8 0 ' '
3 0.280 0.061 0.658 8 0 ' '
4 0.727 0.114 0.675 7 0 ' '
5 0.939 0.220 0.658 8 0 ' '
6 0.386 0.273 0.675 7 0 ' '
7 0.220 0.280 0.342 8 0 ' '
8 0.114 0.386 0.325 6 0 ' '
9 0.947 0.394 0.991 7 0 ' '
10 0.394 0.447 0.009 7 0 ' '
11 0.606 0.553 0.991 7 0 ' '
12 0.053 0.606 0.009 7 0 ' '
13 0.886 0.614 0.675 6 0 ' '
14 0.780 0.720 0.658 8 0 ' '
15 0.614 0.727 0.325 7 0 ' '
16 0.061 0.780 0.342 8 0 ' '
17 0.273 0.886 0.325 7 0 ' '
18 0.720 0.939 0.342 8 0 ' '
19 0.553 0.947 0.009 8 0 ' '

_platon_squeeze_void_probe_radius 1.20
_olex2_submission_special_instructions 'No special instructions were received'
