# Electronic Supplementary Material (ESI) for RSC Advances.
# This journal is © The Royal Society of Chemistry 2024

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
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data_5
_database_code_depnum_ccdc_archive 'CCDC 2327471'
loop_
_audit_author_name
_audit_author_address
'shuxin wang'
;Qingdao University of Science and Technology
China
;
_audit_update_record             
;
2024-01-20 deposited with the CCDC.	2024-03-22 downloaded from the CCDC.
;
_audit_creation_date             2024-01-19
_audit_creation_method           
;
Olex2 1.3
(compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6408)
;
_shelx_SHELXL_version_number     2019/2
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C48 H24 Ag4 Br3.69 Cl8.62 Pt S8, 2(C24 H20 P)'
_chemical_formula_sum            'C96 H64 Ag4 Br3.69 Cl8.62 P2 Pt S8'
_chemical_formula_weight         2762.91
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Br Br -0.2901 2.4595 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   17.7833(12)
_cell_length_b                   17.8696(12)
_cell_length_c                   18.2588(12)
_cell_angle_alpha                110.766(2)
_cell_angle_beta                 112.206(2)
_cell_angle_gamma                90.922(2)
_cell_volume                     4946.9(6)
_cell_formula_units_Z            2
_cell_measurement_reflns_used    9858
_cell_measurement_temperature    170
_cell_measurement_theta_max      27.83
_cell_measurement_theta_min      2.30
_shelx_estimated_absorpt_T_max   0.706
_shelx_estimated_absorpt_T_min   0.635
_exptl_absorpt_coefficient_mu    4.156
_exptl_absorpt_correction_T_max  0.2456
_exptl_absorpt_correction_T_min  0.1054
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
'SADABS-2016/2 was used for absorption correction.'
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            yellow
_exptl_crystal_colour_primary    yellow
_exptl_crystal_density_diffrn    1.855
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             2679
_exptl_crystal_size_max          0.12
_exptl_crystal_size_mid          0.11
_exptl_crystal_size_min          0.09
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  ?
_diffrn_reflns_av_unetI/netI     0.0574
_diffrn_reflns_Laue_measured_fraction_full 0.996
_diffrn_reflns_Laue_measured_fraction_max 0.996
_diffrn_reflns_limit_h_max       19
_diffrn_reflns_limit_h_min       -21
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -21
_diffrn_reflns_limit_l_max       21
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            17189
_diffrn_reflns_point_group_measured_fraction_full 0.996
_diffrn_reflns_point_group_measured_fraction_max 0.996
_diffrn_reflns_theta_full        24.999
_diffrn_reflns_theta_max         24.999
_diffrn_reflns_theta_min         1.910
_diffrn_ambient_temperature      170
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type  'D8 QUEST'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_diffrn_source_current           1.4
_diffrn_source_power             0.07
_diffrn_source_voltage           50.0
_diffrn_standards_number         0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                12676
_reflns_number_total             17189
_reflns_special_details          
;
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences. Completness statistics refer to single and
 composite reflections containing twin component 1 only.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       ?
_computing_data_collection       ?
_computing_data_reduction        ?
_computing_molecular_graphics    'Olex2 1.3 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.3 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2019/2 (Sheldrick, 2015)'
_computing_structure_solution    'SHELXT  (Sheldrick, 2015)'
_refine_diff_density_max         4.858
_refine_diff_density_min         -1.723
_refine_diff_density_rms         0.233
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.058
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     952
_refine_ls_number_reflns         17189
_refine_ls_number_restraints     1658
_refine_ls_R_factor_all          0.1436
_refine_ls_R_factor_gt           0.0994
_refine_ls_restrained_S_all      1.061
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0950P)²+115.3126P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2393
_refine_ls_wR_factor_ref         0.2635
_refine_special_details          
;
 Refined as a 2-component perfect twin.
;
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups
2. Shared sites
{Cl12, Br1}
{Cl8, Br4}
{Cl3, Br6}
{Cl1, Br7}
{Cl5, Br2}
{Cl16, Br5}
{Cl14, Br3}
{Cl10, Br8}
3. Restrained distances
 P2-C31 \\sim P2-C81 \\sim P2-C55 \\sim P2-C70
 with sigma of 0.02
 P1-C84 \\sim P1-C75 \\sim P1-C14 \\sim P1-C4
 with sigma of 0.02
4. Uiso/Uaniso restraints and constraints
S4 \\sim C8 \\sim C32 \\sim C34 \\sim C60 \\sim C62 \\sim C64: within 2A with
sigma of 0.01 and sigma for terminal atoms of 0.02 within 2A
C21 \\sim C38 \\sim C41 \\sim C72 \\sim C74 \\sim C76: within 2A with sigma of
0.01 and sigma for terminal atoms of 0.02 within 2A
S5 \\sim C3 \\sim C15 \\sim C30 \\sim C54 \\sim C56 \\sim C58: within 2A with
sigma of 0.01 and sigma for terminal atoms of 0.02 within 2A
C12 \\sim C28 \\sim C49 \\sim C89 \\sim C91 \\sim C93: within 2A with sigma of
0.01 and sigma for terminal atoms of 0.02 within 2A
P1 \\sim C1 \\sim C4 \\sim C5 \\sim C6 \\sim C9 \\sim C11 \\sim C13 \\sim C14
\\sim C44 \\sim C45 \\sim C46 \\sim C47 \\sim C48 \\sim C50 \\sim C52 \\sim C67
\\sim C69 \\sim C71 \\sim C73 \\sim C75 \\sim C77 \\sim C84 \\sim C86 \\sim
C88: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02 within 2A
S8 \\sim C29 \\sim C51 \\sim C53 \\sim C95 \\sim C96 \\sim C97: within 2A with
sigma of 0.01 and sigma for terminal atoms of 0.02 within 2A
S2 \\sim C7 \\sim C19 \\sim C26 \\sim C90 \\sim C92 \\sim C94: within 2A with
sigma of 0.01 and sigma for terminal atoms of 0.02 within 2A
P2 \\sim C2 \\sim C18 \\sim C31 \\sim C33 \\sim C35 \\sim C36 \\sim C37 \\sim
C39 \\sim C40 \\sim C42 \\sim C55 \\sim C57 \\sim C59 \\sim C61 \\sim C63 \\sim
C65 \\sim C66 \\sim C68 \\sim C70 \\sim C79 \\sim C81 \\sim C83 \\sim C85 \\sim
C87: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02 within 2A
S3 \\sim C10 \\sim C25 \\sim C43 \\sim C78 \\sim C80 \\sim C82: within 2A with
sigma of 0.01 and sigma for terminal atoms of 0.02 within 2A
Ag1 \\sim Ag2 \\sim S4: within 2A with sigma of 0.001 and sigma for terminal
atoms of 0.002 within 2A
Uanis(Cl12) = Uanis(Br1)
Uanis(Cl5) = Uanis(Br2)
Uanis(Cl14) = Uanis(Br3)
Uanis(Cl8) = Uanis(Br4)
Uanis(Cl16) = Uanis(Br5)
Uanis(Cl3) = Uanis(Br6)
Uanis(Cl10) = Uanis(Br8)
Uanis(Cl1) = Uanis(Br7)
5. Rigid body (RIGU) restrains
 All non-hydrogen atoms
 with sigma for 1-2 distances of 0.001 and sigma for 1-3 distances of 0.001
6. Others
 Fixed Sof: Cl2(0.55) Cl4(0.45) Cl7(0.59) Cl9(0.46) Cl11(0.47) Cl13(0.59)
 Cl15(0.67) Cl17(0.53) Cl12(0.59) Br1(0.41) Cl8(0.53) Br4(0.47) Cl3(0.59)
 Br6(0.41) Cl1(0.55) Br7(0.45) Cl5(0.46) Br2(0.54) Cl16(0.47) Br5(0.53)
 Cl14(0.67) Br3(0.33) Cl10(0.45) Br8(0.55)
7.a Aromatic/amide H refined with riding coordinates:
 C30(H30), C15(H15), C58(H58), C10(H10), C78(H78), C25(H25), C22(H22),
 C27(H27), C23(H23), C89(H89), C12(H12), C93(H93), C8(H8), C34(H34), C64(H64),
 C72(H72), C21(H21), C76(H76), C51(H51), C29(H29), C96(H96), C94(H94), C7(H7),
 C26(H26), C1(H1), C6(H6), C9(H9), C11(H11), C13(H13), C44(H44), C46(H46),
 C48(H48), C50(H50), C52(H52), C45(H45), C5(H5), C86(H86), C47(H47), C88(H88),
 C67(H67), C69(H69), C71(H71), C73(H73), C77(H77), C18(H18), C66(H66), C36(H36),
  C68(H68), C2(H2), C33(H33), C35(H35), C37(H37), C39(H39), C42(H42), C57(H57),
 C59(H59), C61(H61), C63(H63), C65(H65), C79(H79), C83(H83), C85(H85), C87(H87),
  C40(H40)
7.b Fitted hexagon refined as free rotating group:
 C3(C54,C30,C56,C15,C58), C10(C78,C43,C80,C25,C82), C17(C20,C22,C27,C24,C23),
 C28(C89,C49,C91,C12,C93), C32(C60,C8,C62,C34,C64), C38(C72,C21,C74,C41,C76),
 C51(C95,C29,C96,C53,C97), C90(C92,C94,C19,C7,C26), C1(C4,C6,C9,C11,C13),
 C44(C46,C48,C50,C52,C14), C45(C84,C5,C86,C47,C88), C67(C69,C71,C73,C75,C77),
 C18(C66,C36,C68,C2,C70), C31(C33,C35,C37,C39,C42), C55(C57,C59,C61,C63,C65),
 C79(C81,C83,C85,C87,C40)
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt Pt 0.16602(6) 0.67352(6) 0.29033(4) 0.04207(18) Uani 1 1 d . . . . .
Ag1 Ag 0.27364(16) 0.85392(13) 0.45699(14) 0.0728(6) Uani 1 1 d . . . . .
Ag2 Ag 0.11567(14) 0.77980(15) 0.45457(14) 0.0736(6) Uani 1 1 d . . . . .
Ag3 Ag 0.34883(12) 0.69722(15) 0.45850(13) 0.0692(6) Uani 1 1 d . . . . .
Ag4 Ag 0.19011(14) 0.62056(13) 0.45680(13) 0.0647(5) Uani 1 1 d . . . . .
Cl2 Cl 0.0357(10) 0.5935(11) 0.6057(9) 0.094(5) Uani 0.55 1 d . . P . .
Cl4 Cl 0.1853(15) 0.5372(11) 0.0939(11) 0.100(6) Uani 0.45 1 d . . P . .
Cl7 Cl 0.4853(9) 0.5341(10) 0.6202(9) 0.094(4) Uani 0.59 1 d . . P . .
Cl9 Cl 0.0105(8) 0.4890(11) 0.0887(9) 0.077(4) Uani 0.46 1 d . . P . .
Cl11 Cl -0.0207(10) 0.6650(9) 0.0861(9) 0.073(4) Uani 0.47 1 d . . P . .
Cl13 Cl 0.0925(8) 1.0493(8) 0.6064(7) 0.078(3) Uani 0.59 1 d . . P . .
Cl15 Cl 0.1572(8) 0.7044(10) 0.0908(8) 0.107(5) Uani 0.67 1 d . . P . .
Cl17 Cl 0.5545(11) 0.9917(10) 0.6136(9) 0.089(5) Uani 0.53 1 d . . P . .
S1 S 0.0840(5) 0.6819(5) 0.5079(4) 0.0713(17) Uani 1 1 d . . . . .
S2 S 0.2108(4) 0.7996(3) 0.2939(4) 0.0473(11) Uani 1 1 d . U . . .
S3 S 0.3297(5) 0.5892(5) 0.5113(5) 0.0765(17) Uani 1 1 d . U . . .
S4 S 0.1787(5) 0.9250(5) 0.5077(5) 0.0740(17) Uani 1 1 d . U . . .
S5 S 0.0425(4) 0.7148(4) 0.2913(4) 0.0520(12) Uani 1 1 d . U . . .
S6 S 0.4208(5) 0.8354(5) 0.5122(5) 0.0751(18) Uani 1 1 d . . . . .
S7 S 0.2917(3) 0.6364(3) 0.2951(4) 0.0451(11) Uani 1 1 d . . . . .
S8 S 0.1257(3) 0.5513(3) 0.2925(4) 0.0452(11) Uani 1 1 d . U . . .
C3 C 0.0196(10) 0.7876(8) 0.2378(9) 0.058(3) Uani 1 1 d G U . . .
C54 C -0.0078(11) 0.7600(7) 0.1491(9) 0.063(3) Uani 1 1 d G U . . .
C30 C -0.0309(11) 0.8139(10) 0.1085(7) 0.067(3) Uani 1 1 d G U . . .
H30 H -0.049618 0.795053 0.047943 0.080 Uiso 1 1 calc R U . . .
C56 C -0.0267(11) 0.8953(9) 0.1566(10) 0.065(3) Uani 1 1 d G U . . .
C15 C 0.0007(10) 0.9228(7) 0.2453(9) 0.064(3) Uani 1 1 d G U . . .
H15 H 0.003630 0.978409 0.278162 0.077 Uiso 1 1 calc R U . . .
C58 C 0.0238(10) 0.8689(9) 0.2859(7) 0.064(3) Uani 1 1 d G U . . .
H58 H 0.042526 0.887766 0.346496 0.076 Uiso 1 1 calc R U . . .
C10 C 0.3722(10) 0.7166(10) 0.7627(9) 0.076(4) Uani 1 1 d G U . . .
H10 H 0.346783 0.753518 0.793970 0.091 Uiso 1 1 calc R U . . .
C78 C 0.3376(8) 0.6865(11) 0.6735(9) 0.070(4) Uani 1 1 d G U . . .
H78 H 0.288604 0.702826 0.643771 0.084 Uiso 1 1 calc R U . . .
C43 C 0.3749(10) 0.6326(11) 0.6277(7) 0.070(3) Uani 1 1 d G U . . .
C80 C 0.4466(10) 0.6087(10) 0.6712(10) 0.065(3) Uani 1 1 d G U . . .
C25 C 0.4812(8) 0.6388(11) 0.7604(10) 0.069(4) Uani 1 1 d G U . . .
H25 H 0.530218 0.622526 0.790163 0.083 Uiso 1 1 calc R U . . .
C82 C 0.4440(11) 0.6928(11) 0.8062(7) 0.075(4) Uani 1 1 d G U . . .
C17 C 0.2272(11) 0.4859(9) 0.1580(9) 0.064(5) Uani 1 1 d G . . . .
C20 C 0.2768(11) 0.5240(7) 0.2453(10) 0.061(4) Uani 1 1 d G . . . .
C22 C 0.3204(11) 0.4790(9) 0.2904(8) 0.087(8) Uani 1 1 d G . . . .
H22 H 0.354274 0.505042 0.350085 0.105 Uiso 1 1 calc R U . . .
C27 C 0.3144(12) 0.3959(9) 0.2481(10) 0.076(6) Uani 1 1 d G . . . .
H27 H 0.344173 0.365146 0.278941 0.091 Uiso 1 1 calc R U . . .
C24 C 0.2648(12) 0.3578(7) 0.1608(10) 0.070(5) Uani 1 1 d G . . . .
C23 C 0.2212(12) 0.4028(9) 0.1157(8) 0.088(7) Uani 1 1 d G . . . .
H23 H 0.187356 0.376769 0.056009 0.106 Uiso 1 1 calc R U . . .
C28 C 0.1871(13) 0.7835(12) 0.8007(8) 0.088(4) Uani 1 1 d G U . . .
C89 C 0.1332(12) 0.7097(11) 0.7528(11) 0.082(4) Uani 1 1 d G U . D .
H89 H 0.117106 0.681018 0.780939 0.098 Uiso 1 1 calc R U . . .
C49 C 0.1029(10) 0.6778(9) 0.6637(11) 0.071(4) Uani 1 1 d G U . D .
C91 C 0.1265(11) 0.7198(11) 0.6225(8) 0.069(4) Uani 1 1 d G U . D .
C12 C 0.1803(11) 0.7936(11) 0.6704(11) 0.078(4) Uani 1 1 d G U . D .
H12 H 0.196452 0.822276 0.642194 0.093 Uiso 1 1 calc R U . . .
C93 C 0.2107(11) 0.8255(10) 0.7595(10) 0.087(4) Uani 1 1 d G U . D .
H93 H 0.247503 0.875966 0.792201 0.104 Uiso 1 1 calc R U . . .
C32 C 0.2185(11) 0.9706(11) 0.6229(7) 0.069(3) Uani 1 1 d G U . . .
C60 C 0.1738(9) 1.0199(10) 0.6624(9) 0.068(4) Uani 1 1 d G U . . .
C8 C 0.2053(10) 1.0565(10) 0.7515(10) 0.072(4) Uani 1 1 d G U . . .
H8 H 0.174734 1.090203 0.778471 0.087 Uiso 1 1 calc R U . . .
C62 C 0.2815(11) 1.0440(11) 0.8010(7) 0.080(4) Uani 1 1 d G U . . .
C34 C 0.3261(9) 0.9947(11) 0.7615(9) 0.081(4) Uani 1 1 d G U . . .
H34 H 0.378216 0.986136 0.795389 0.098 Uiso 1 1 calc R U . . .
C64 C 0.2947(10) 0.9581(10) 0.6724(10) 0.076(4) Uani 1 1 d G U . . .
H64 H 0.325195 0.924397 0.645440 0.091 Uiso 1 1 calc R U . . .
C38 C 0.5429(11) 0.9535(11) 0.8045(8) 0.079(4) Uani 1 1 d G U . . .
C72 C 0.4874(11) 0.8810(11) 0.7660(10) 0.083(4) Uani 1 1 d G U . B .
H72 H 0.475430 0.857589 0.800480 0.100 Uiso 1 1 calc R U . . .
C21 C 0.4495(10) 0.8428(10) 0.6770(10) 0.080(4) Uani 1 1 d G U . B .
H21 H 0.411548 0.793328 0.650635 0.096 Uiso 1 1 calc R U . . .
C74 C 0.4670(12) 0.8771(12) 0.6265(8) 0.075(4) Uani 1 1 d G U . B .
C41 C 0.5224(11) 0.9496(12) 0.6651(11) 0.076(4) Uani 1 1 d G U . B .
C76 C 0.5604(10) 0.9877(9) 0.7541(12) 0.077(4) Uani 1 1 d G U . B .
H76 H 0.598278 1.037241 0.780407 0.093 Uiso 1 1 calc R U . . .
C51 C -0.1166(9) 0.4771(12) 0.1190(8) 0.079(4) Uani 1 1 d G U . . .
H51 H -0.145290 0.460134 0.058538 0.095 Uiso 1 1 calc R U . . .
C95 C -0.1594(7) 0.4750(12) 0.1683(11) 0.077(4) Uani 1 1 d G U . . .
C29 C -0.1174(9) 0.4998(12) 0.2568(11) 0.078(4) Uani 1 1 d G U . . .
H29 H -0.146680 0.498420 0.290465 0.093 Uiso 1 1 calc R U . . .
C96 C -0.0327(9) 0.5267(11) 0.2959(8) 0.070(4) Uani 1 1 d G U . . .
H96 H -0.004005 0.543659 0.356325 0.084 Uiso 1 1 calc R U . . .
C53 C 0.0101(7) 0.5288(11) 0.2466(10) 0.061(3) Uani 1 1 d G U . . .
C97 C -0.0319(9) 0.5040(12) 0.1581(10) 0.070(4) Uani 1 1 d G U . . .
C90 C 0.2819(9) 0.7872(11) 0.2423(10) 0.061(3) Uani 1 1 d G U . . .
C92 C 0.2532(8) 0.7462(11) 0.1538(10) 0.069(4) Uani 1 1 d G U . . .
C94 C 0.3075(10) 0.7393(11) 0.1143(8) 0.078(4) Uani 1 1 d G U . . .
H94 H 0.287872 0.711281 0.053858 0.093 Uiso 1 1 calc R U . . .
C19 C 0.3904(10) 0.7732(12) 0.1633(11) 0.078(4) Uani 1 1 d G U . . .
C7 C 0.4190(8) 0.8142(11) 0.2518(11) 0.075(4) Uani 1 1 d G U . . .
H7 H 0.475704 0.837417 0.285264 0.090 Uiso 1 1 calc R U . . .
C26 C 0.3648(10) 0.8212(11) 0.2913(8) 0.071(4) Uani 1 1 d G U . . .
H26 H 0.384364 0.849160 0.351728 0.085 Uiso 1 1 calc R U . . .
Cl12 Cl 0.3112(4) 1.0817(4) 0.9180(3) 0.1143(19) Uani 0.59 1 d . . P A 3
Br1 Br 0.3112(4) 1.0817(4) 0.9180(3) 0.1143(19) Uani 0.41 1 d . . P A 4
Cl8 Cl 0.5830(4) 1.0048(4) 0.9219(3) 0.127(2) Uani 0.53 1 d . . P B 5
Br4 Br 0.5830(4) 1.0048(4) 0.9219(3) 0.127(2) Uani 0.47 1 d . . P B 6
Cl3 Cl 0.4920(4) 0.7363(5) 0.9212(3) 0.128(3) Uani 0.59 1 d . . P C 7
Br6 Br 0.4920(4) 0.7363(5) 0.9212(3) 0.128(3) Uani 0.41 1 d . . P C 8
Cl1 Cl 0.2375(4) 0.8119(4) 0.9173(3) 0.1165(19) Uani 0.55 1 d . . P D 9
Br7 Br 0.2375(4) 0.8119(4) 0.9173(3) 0.1165(19) Uani 0.45 1 d . . P D 10
Cl5 Cl -0.2643(3) 0.4258(5) 0.1179(4) 0.144(2) Uani 0.46 1 d . . P E 11
Br2 Br -0.2643(3) 0.4258(5) 0.1179(4) 0.144(2) Uani 0.54 1 d . . P E 12
Cl16 Cl -0.0720(5) 0.9540(4) 0.0954(4) 0.141(2) Uani 0.47 1 d . . P F 13
Br5 Br -0.0720(5) 0.9540(4) 0.0954(4) 0.141(2) Uani 0.53 1 d . . P F 14
Cl14 Cl 0.4457(4) 0.7711(6) 0.0986(5) 0.132(3) Uani 0.67 1 d . . P G 15
Br3 Br 0.4457(4) 0.7711(6) 0.0986(5) 0.132(3) Uani 0.33 1 d . . P G 16
Cl10 Cl 0.2692(4) 0.2537(3) 0.1023(3) 0.1045(16) Uani 0.45 1 d . . P H 17
Br8 Br 0.2692(4) 0.2537(3) 0.1023(3) 0.1045(16) Uani 0.55 1 d . . P H 18
P1 P 0.3421(4) 0.3378(4) 0.7250(3) 0.0572(11) Uani 1 1 d D U . . .
C1 C 0.3435(10) 0.1704(10) 0.6631(10) 0.067(3) Uani 1 1 d G U . . .
H1 H 0.323626 0.168226 0.703954 0.080 Uiso 1 1 calc R U . . .
C4 C 0.3584(10) 0.2441(8) 0.6570(10) 0.064(2) Uani 1 1 d DG U . . .
C6 C 0.3876(10) 0.2472(7) 0.5972(11) 0.067(3) Uani 1 1 d G U . . .
H6 H 0.397742 0.297600 0.593006 0.080 Uiso 1 1 calc R U . . .
C9 C 0.4018(11) 0.1768(10) 0.5436(10) 0.069(3) Uani 1 1 d G U . . .
H9 H 0.421691 0.178923 0.502760 0.083 Uiso 1 1 calc R U . . .
C11 C 0.3869(11) 0.1031(8) 0.5497(10) 0.071(3) Uani 1 1 d G U . . .
H11 H 0.396607 0.054896 0.513110 0.086 Uiso 1 1 calc R U . . .
C13 C 0.3578(11) 0.0999(7) 0.6095(11) 0.070(3) Uani 1 1 d G U . . .
H13 H 0.347575 0.049546 0.613706 0.084 Uiso 1 1 calc R U . . .
C44 C 0.2016(9) 0.3308(8) 0.5922(10) 0.062(3) Uani 1 1 d G U . . .
H44 H 0.190283 0.276073 0.585511 0.074 Uiso 1 1 calc R U . . .
C46 C 0.1446(7) 0.3611(9) 0.5382(9) 0.062(3) Uani 1 1 d G U . . .
H46 H 0.094436 0.327060 0.494579 0.075 Uiso 1 1 calc R U . . .
C48 C 0.1611(8) 0.4412(10) 0.5480(10) 0.065(4) Uani 1 1 d G U . . .
H48 H 0.122200 0.461904 0.511068 0.079 Uiso 1 1 calc R U . . .
C50 C 0.2345(10) 0.4910(8) 0.6118(11) 0.067(4) Uani 1 1 d G U . . .
H50 H 0.245811 0.545763 0.618490 0.080 Uiso 1 1 calc R U . . .
C52 C 0.2915(8) 0.4607(9) 0.6658(9) 0.063(3) Uani 1 1 d G U . . .
H52 H 0.341659 0.494778 0.709424 0.076 Uiso 1 1 calc R U . . .
C14 C 0.2750(8) 0.3806(10) 0.6560(9) 0.062(2) Uani 1 1 d DG U . . .
C45 C 0.5112(10) 0.3821(9) 0.7866(11) 0.083(5) Uani 1 1 d G U . . .
H45 H 0.509952 0.333135 0.742403 0.100 Uiso 1 1 calc R U . . .
C84 C 0.4385(7) 0.4015(10) 0.7946(10) 0.067(2) Uani 1 1 d DG U . . .
C5 C 0.4403(8) 0.4731(11) 0.8593(11) 0.075(4) Uani 1 1 d G U . . .
H5 H 0.390630 0.486394 0.864772 0.091 Uiso 1 1 calc R U . . .
C86 C 0.5147(10) 0.5252(9) 0.9161(10) 0.081(5) Uani 1 1 d G U . . .
H86 H 0.515919 0.574134 0.960294 0.097 Uiso 1 1 calc R U . . .
C47 C 0.5874(8) 0.5058(10) 0.9081(11) 0.089(5) Uani 1 1 d G U . . .
H47 H 0.638225 0.541375 0.946872 0.106 Uiso 1 1 calc R U . . .
C88 C 0.5856(7) 0.4342(11) 0.8434(12) 0.092(5) Uani 1 1 d G U . . .
H88 H 0.635243 0.420876 0.837927 0.111 Uiso 1 1 calc R U . . .
C67 C 0.1798(7) 0.3104(12) 0.8251(10) 0.073(3) Uani 1 1 d G U . . .
H67 H 0.123704 0.314828 0.813618 0.088 Uiso 1 1 calc R U . . .
C69 C 0.2261(9) 0.2869(12) 0.8912(10) 0.073(3) Uani 1 1 d G U . . .
H69 H 0.201682 0.275350 0.925030 0.088 Uiso 1 1 calc R U . . .
C71 C 0.3082(9) 0.2804(11) 0.9080(10) 0.073(3) Uani 1 1 d G U . . .
H71 H 0.339891 0.264339 0.953223 0.087 Uiso 1 1 calc R U . . .
C73 C 0.3440(7) 0.2973(11) 0.8586(11) 0.070(3) Uani 1 1 d G U . . .
H73 H 0.400122 0.292806 0.870005 0.084 Uiso 1 1 calc R U . . .
C75 C 0.2977(9) 0.3207(11) 0.7924(10) 0.065(2) Uani 1 1 d DG U . . .
C77 C 0.2156(9) 0.3273(11) 0.7756(9) 0.070(3) Uani 1 1 d G U . . .
H77 H 0.183937 0.343295 0.730399 0.083 Uiso 1 1 calc R U . . .
P2 P 0.1677(4) 1.1695(4) 1.2761(3) 0.0583(12) Uani 1 1 d D U . . .
C18 C 0.1983(11) 1.0705(7) 1.1389(10) 0.068(3) Uani 1 1 d G U . . .
H18 H 0.198788 1.116688 1.124684 0.081 Uiso 1 1 calc R U . . .
C66 C 0.2147(11) 0.9984(9) 1.0902(9) 0.069(3) Uani 1 1 d G U . . .
H66 H 0.226429 0.995343 1.042626 0.083 Uiso 1 1 calc R U . . .
C36 C 0.2141(11) 0.9308(7) 1.1110(10) 0.071(3) Uani 1 1 d G U . . .
H36 H 0.225274 0.881540 1.077645 0.085 Uiso 1 1 calc R U . . .
C68 C 0.1969(11) 0.9353(7) 1.1805(10) 0.071(3) Uani 1 1 d G U . . .
H68 H 0.196479 0.889080 1.194723 0.086 Uiso 1 1 calc R U . . .
C2 C 0.1805(11) 1.0074(9) 1.2293(9) 0.069(3) Uani 1 1 d G U . . .
H2 H 0.168838 1.010424 1.276783 0.082 Uiso 1 1 calc R U . . .
C70 C 0.1812(11) 1.0750(7) 1.2084(10) 0.065(2) Uani 1 1 d DG U . . .
C31 C 0.2641(8) 1.2361(9) 1.3454(10) 0.064(2) Uani 1 1 d DG U . . .
C33 C 0.3351(10) 1.2194(8) 1.3324(9) 0.065(4) Uani 1 1 d G U . . .
H33 H 0.333772 1.169876 1.288750 0.079 Uiso 1 1 calc R U . . .
C35 C 0.4082(8) 1.2750(10) 1.3832(11) 0.071(4) Uani 1 1 d G U . . .
H35 H 0.456784 1.263625 1.374314 0.086 Uiso 1 1 calc R U . . .
C37 C 0.4102(8) 1.3475(9) 1.4471(10) 0.073(4) Uani 1 1 d G U . . .
H37 H 0.460159 1.385512 1.481816 0.088 Uiso 1 1 calc R U . . .
C39 C 0.3392(10) 1.3642(8) 1.4601(9) 0.070(4) Uani 1 1 d G U . . .
H39 H 0.340521 1.413651 1.503754 0.084 Uiso 1 1 calc R U . . .
C42 C 0.2661(8) 1.3085(10) 1.4093(11) 0.066(4) Uani 1 1 d G U . . .
H42 H 0.217508 1.319903 1.418191 0.080 Uiso 1 1 calc R U . . .
C55 C 0.1230(10) 1.1527(11) 1.3435(10) 0.065(2) Uani 1 1 d DG U . . .
C57 C 0.1717(8) 1.1287(11) 1.4083(10) 0.065(3) Uani 1 1 d G U . . .
H57 H 0.227474 1.124358 1.417620 0.078 Uiso 1 1 calc R U . . .
C59 C 0.1389(10) 1.1112(11) 1.4596(9) 0.067(3) Uani 1 1 d G U . . .
H59 H 0.172145 1.094847 1.503945 0.080 Uiso 1 1 calc R U . . .
C61 C 0.0573(10) 1.1176(11) 1.4460(10) 0.070(3) Uani 1 1 d G U . . .
H61 H 0.034835 1.105653 1.481063 0.084 Uiso 1 1 calc R U . . .
C63 C 0.0086(8) 1.1416(11) 1.3811(11) 0.070(3) Uani 1 1 d G U . . .
H63 H -0.047146 1.145968 1.371856 0.084 Uiso 1 1 calc R U . . .
C65 C 0.0415(10) 1.1591(11) 1.3299(9) 0.067(3) Uani 1 1 d G U . . .
H65 H 0.008182 1.175479 1.285530 0.080 Uiso 1 1 calc R U . . .
C79 C 0.0294(11) 1.1639(8) 1.1369(11) 0.077(4) Uani 1 1 d G U . . .
H79 H 0.017523 1.108105 1.126441 0.093 Uiso 1 1 calc R U . . .
C81 C 0.1003(10) 1.2130(10) 1.2063(10) 0.067(2) Uani 1 1 d DG U . . .
C83 C 0.1176(9) 1.2946(9) 1.2216(9) 0.071(4) Uani 1 1 d G U . . .
H83 H 0.166034 1.328179 1.269011 0.085 Uiso 1 1 calc R U . . .
C85 C 0.0641(11) 1.3272(8) 1.1676(11) 0.073(4) Uani 1 1 d G U . . .
H85 H 0.075901 1.382961 1.178080 0.088 Uiso 1 1 calc R U . . .
C87 C -0.0068(10) 1.2781(10) 1.0982(10) 0.076(5) Uani 1 1 d G U . . .
H87 H -0.043422 1.300316 1.061329 0.091 Uiso 1 1 calc R U . . .
C40 C -0.0242(9) 1.1964(10) 1.0829(10) 0.080(5) Uani 1 1 d G U . . .
H40 H -0.072612 1.162889 1.035508 0.096 Uiso 1 1 calc R U . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt S2 2.347(6) . ?
Pt S5 2.332(5) . ?
Pt S7 2.321(5) . ?
Pt S8 2.306(6) . ?
Ag1 Ag2 3.065(4) . ?
Ag1 Ag3 3.127(3) . ?
Ag1 S2 2.541(6) . ?
Ag1 S4 2.396(8) . ?
Ag1 S6 2.499(8) . ?
Ag2 Ag4 3.164(3) . ?
Ag2 S1 2.433(8) . ?
Ag2 S4 2.496(9) . ?
Ag2 S5 2.548(7) . ?
Ag3 Ag4 3.102(3) . ?
Ag3 S3 2.513(9) . ?
Ag3 S6 2.435(9) . ?
Ag3 S7 2.548(6) . ?
Ag4 S1 2.510(8) . ?
Ag4 S3 2.458(8) . ?
Ag4 S8 2.562(6) . ?
Cl2 C49 1.63(2) . ?
Cl4 C17 1.70(2) . ?
Cl7 C80 1.660(18) . ?
Cl9 C97 1.652(19) . ?
Cl11 C54 1.632(18) . ?
Cl13 C60 1.644(17) . ?
Cl15 C92 1.632(17) . ?
Cl17 C41 1.63(2) . ?
S1 C91 1.786(14) . ?
S2 C90 1.815(13) . ?
S3 C43 1.813(13) . ?
S4 C32 1.796(13) . ?
S5 C3 1.851(12) . ?
S6 C74 1.779(14) . ?
S7 C20 1.854(13) . ?
S8 C53 1.877(12) . ?
C3 C54 1.3900 . ?
C3 C58 1.3900 . ?
C54 C30 1.3900 . ?
C30 H30 0.9500 . ?
C30 C56 1.3900 . ?
C56 C15 1.3900 . ?
C56 Cl16 1.783(12) . ?
C56 Br5 1.783(12) . ?
C15 H15 0.9500 . ?
C15 C58 1.3900 . ?
C58 H58 0.9500 . ?
C10 H10 0.9500 . ?
C10 C78 1.3900 . ?
C10 C82 1.3900 . ?
C78 H78 0.9500 . ?
C78 C43 1.3900 . ?
C43 C80 1.3900 . ?
C80 C25 1.3900 . ?
C25 H25 0.9500 . ?
C25 C82 1.3900 . ?
C82 Cl3 1.791(12) . ?
C82 Br6 1.791(12) . ?
C17 C20 1.3900 . ?
C17 C23 1.3900 . ?
C20 C22 1.3900 . ?
C22 H22 0.9500 . ?
C22 C27 1.3900 . ?
C27 H27 0.9500 . ?
C27 C24 1.3900 . ?
C24 C23 1.3900 . ?
C24 Cl10 1.807(12) . ?
C24 Br8 1.807(12) . ?
C23 H23 0.9500 . ?
C28 C89 1.3900 . ?
C28 C93 1.3900 . ?
C28 Cl1 1.837(13) . ?
C28 Br7 1.837(13) . ?
C89 H89 0.9500 . ?
C89 C49 1.3900 . ?
C49 C91 1.3900 . ?
C91 C12 1.3900 . ?
C12 H12 0.9500 . ?
C12 C93 1.3900 . ?
C93 H93 0.9500 . ?
C32 C60 1.3900 . ?
C32 C64 1.3900 . ?
C60 C8 1.3900 . ?
C8 H8 0.9500 . ?
C8 C62 1.3900 . ?
C62 C34 1.3900 . ?
C62 Cl12 1.847(12) . ?
C62 Br1 1.847(12) . ?
C34 H34 0.9500 . ?
C34 C64 1.3900 . ?
C64 H64 0.9500 . ?
C38 C72 1.3900 . ?
C38 C76 1.3900 . ?
C38 Cl8 1.837(13) . ?
C38 Br4 1.837(13) . ?
C72 H72 0.9500 . ?
C72 C21 1.3900 . ?
C21 H21 0.9500 . ?
C21 C74 1.3900 . ?
C74 C41 1.3900 . ?
C41 C76 1.3900 . ?
C76 H76 0.9500 . ?
C51 H51 0.9500 . ?
C51 C95 1.3900 . ?
C51 C97 1.3900 . ?
C95 C29 1.3900 . ?
C95 Cl5 1.782(12) . ?
C95 Br2 1.782(12) . ?
C29 H29 0.9500 . ?
C29 C96 1.3900 . ?
C96 H96 0.9500 . ?
C96 C53 1.3900 . ?
C53 C97 1.3900 . ?
C90 C92 1.3900 . ?
C90 C26 1.3900 . ?
C92 C94 1.3900 . ?
C94 H94 0.9500 . ?
C94 C19 1.3900 . ?
C19 C7 1.3900 . ?
C19 Cl14 1.792(13) . ?
C19 Br3 1.792(13) . ?
C7 H7 0.9500 . ?
C7 C26 1.3900 . ?
C26 H26 0.9500 . ?
P1 C4 1.802(10) . ?
P1 C14 1.781(10) . ?
P1 C84 1.766(10) . ?
P1 C75 1.794(10) . ?
C1 H1 0.9500 . ?
C1 C4 1.3900 . ?
C1 C13 1.3900 . ?
C4 C6 1.3900 . ?
C6 H6 0.9500 . ?
C6 C9 1.3900 . ?
C9 H9 0.9500 . ?
C9 C11 1.3900 . ?
C11 H11 0.9500 . ?
C11 C13 1.3900 . ?
C13 H13 0.9500 . ?
C44 H44 0.9500 . ?
C44 C46 1.3900 . ?
C44 C14 1.3900 . ?
C46 H46 0.9500 . ?
C46 C48 1.3900 . ?
C48 H48 0.9500 . ?
C48 C50 1.3900 . ?
C50 H50 0.9500 . ?
C50 C52 1.3900 . ?
C52 H52 0.9500 . ?
C52 C14 1.3900 . ?
C45 H45 0.9500 . ?
C45 C84 1.3900 . ?
C45 C88 1.3900 . ?
C84 C5 1.3900 . ?
C5 H5 0.9500 . ?
C5 C86 1.3900 . ?
C86 H86 0.9500 . ?
C86 C47 1.3900 . ?
C47 H47 0.9500 . ?
C47 C88 1.3900 . ?
C88 H88 0.9500 . ?
C67 H67 0.9500 . ?
C67 C69 1.3900 . ?
C67 C77 1.3900 . ?
C69 H69 0.9500 . ?
C69 C71 1.3900 . ?
C71 H71 0.9500 . ?
C71 C73 1.3900 . ?
C73 H73 0.9500 . ?
C73 C75 1.3900 . ?
C75 C77 1.3900 . ?
C77 H77 0.9500 . ?
P2 C70 1.787(10) . ?
P2 C31 1.784(10) . ?
P2 C55 1.797(10) . ?
P2 C81 1.801(10) . ?
C18 H18 0.9500 . ?
C18 C66 1.3900 . ?
C18 C70 1.3900 . ?
C66 H66 0.9500 . ?
C66 C36 1.3900 . ?
C36 H36 0.9500 . ?
C36 C68 1.3900 . ?
C68 H68 0.9500 . ?
C68 C2 1.3900 . ?
C2 H2 0.9500 . ?
C2 C70 1.3900 . ?
C31 C33 1.3900 . ?
C31 C42 1.3900 . ?
C33 H33 0.9500 . ?
C33 C35 1.3900 . ?
C35 H35 0.9500 . ?
C35 C37 1.3900 . ?
C37 H37 0.9500 . ?
C37 C39 1.3900 . ?
C39 H39 0.9500 . ?
C39 C42 1.3900 . ?
C42 H42 0.9500 . ?
C55 C57 1.3900 . ?
C55 C65 1.3900 . ?
C57 H57 0.9500 . ?
C57 C59 1.3900 . ?
C59 H59 0.9500 . ?
C59 C61 1.3900 . ?
C61 H61 0.9500 . ?
C61 C63 1.3900 . ?
C63 H63 0.9500 . ?
C63 C65 1.3900 . ?
C65 H65 0.9500 . ?
C79 H79 0.9500 . ?
C79 C81 1.3900 . ?
C79 C40 1.3900 . ?
C81 C83 1.3900 . ?
C83 H83 0.9500 . ?
C83 C85 1.3900 . ?
C85 H85 0.9500 . ?
C85 C87 1.3900 . ?
C87 H87 0.9500 . ?
C87 C40 1.3900 . ?
C40 H40 0.9500 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
S5 Pt S2 90.0(2) . . ?
S7 Pt S2 89.1(2) . . ?
S7 Pt S5 177.64(18) . . ?
S8 Pt S2 177.68(16) . . ?
S8 Pt S5 90.7(2) . . ?
S8 Pt S7 90.16(19) . . ?
Ag2 Ag1 Ag3 90.76(9) . . ?
S2 Ag1 Ag2 90.78(16) . . ?
S2 Ag1 Ag3 92.27(14) . . ?
S4 Ag1 Ag2 52.7(2) . . ?
S4 Ag1 Ag3 136.5(2) . . ?
S4 Ag1 S2 108.8(2) . . ?
S4 Ag1 S6 140.0(3) . . ?
S6 Ag1 Ag2 134.2(2) . . ?
S6 Ag1 Ag3 49.8(2) . . ?
S6 Ag1 S2 110.3(2) . . ?
Ag1 Ag2 Ag4 89.93(8) . . ?
S1 Ag2 Ag1 134.4(2) . . ?
S1 Ag2 Ag4 51.28(19) . . ?
S1 Ag2 S4 140.3(3) . . ?
S1 Ag2 S5 106.8(2) . . ?
S4 Ag2 Ag1 49.8(2) . . ?
S4 Ag2 Ag4 133.4(2) . . ?
S4 Ag2 S5 112.2(2) . . ?
S5 Ag2 Ag1 94.69(16) . . ?
S5 Ag2 Ag4 90.37(15) . . ?
Ag4 Ag3 Ag1 89.95(8) . . ?
S3 Ag3 Ag1 134.4(2) . . ?
S3 Ag3 Ag4 50.6(2) . . ?
S3 Ag3 S7 109.7(2) . . ?
S6 Ag3 Ag1 51.6(2) . . ?
S6 Ag3 Ag4 134.8(2) . . ?
S6 Ag3 S3 140.4(3) . . ?
S6 Ag3 S7 109.2(2) . . ?
S7 Ag3 Ag1 91.05(14) . . ?
S7 Ag3 Ag4 92.04(15) . . ?
Ag3 Ag4 Ag2 89.37(9) . . ?
S1 Ag4 Ag2 49.12(19) . . ?
S1 Ag4 Ag3 132.3(2) . . ?
S1 Ag4 S8 109.7(2) . . ?
S3 Ag4 Ag2 135.2(2) . . ?
S3 Ag4 Ag3 52.2(2) . . ?
S3 Ag4 S1 141.0(3) . . ?
S3 Ag4 S8 108.6(2) . . ?
S8 Ag4 Ag2 92.58(14) . . ?
S8 Ag4 Ag3 91.84(14) . . ?
Ag2 S1 Ag4 79.6(2) . . ?
C91 S1 Ag2 112.8(7) . . ?
C91 S1 Ag4 109.1(7) . . ?
Pt S2 Ag1 89.0(2) . . ?
C90 S2 Pt 109.4(6) . . ?
C90 S2 Ag1 117.0(6) . . ?
Ag4 S3 Ag3 77.2(2) . . ?
C43 S3 Ag3 109.0(7) . . ?
C43 S3 Ag4 109.7(7) . . ?
Ag1 S4 Ag2 77.5(2) . . ?
C32 S4 Ag1 112.9(7) . . ?
C32 S4 Ag2 110.1(7) . . ?
Pt S5 Ag2 87.7(2) . . ?
C3 S5 Pt 107.9(6) . . ?
C3 S5 Ag2 114.9(6) . . ?
Ag3 S6 Ag1 78.6(2) . . ?
C74 S6 Ag1 110.8(8) . . ?
C74 S6 Ag3 110.1(7) . . ?
Pt S7 Ag3 89.0(2) . . ?
C20 S7 Pt 108.3(6) . . ?
C20 S7 Ag3 115.1(6) . . ?
Pt S8 Ag4 87.6(2) . . ?
C53 S8 Pt 108.9(6) . . ?
C53 S8 Ag4 112.4(6) . . ?
C54 C3 S5 120.2(9) . . ?
C54 C3 C58 120.0 . . ?
C58 C3 S5 119.6(9) . . ?
C3 C54 Cl11 124.0(10) . . ?
C30 C54 Cl11 115.9(10) . . ?
C30 C54 C3 120.0 . . ?
C54 C30 H30 120.0 . . ?
C54 C30 C56 120.0 . . ?
C56 C30 H30 120.0 . . ?
C30 C56 Cl16 115.1(9) . . ?
C30 C56 Br5 115.1(9) . . ?
C15 C56 C30 120.0 . . ?
C15 C56 Cl16 124.3(9) . . ?
C15 C56 Br5 124.3(9) . . ?
C56 C15 H15 120.0 . . ?
C56 C15 C58 120.0 . . ?
C58 C15 H15 120.0 . . ?
C3 C58 H58 120.0 . . ?
C15 C58 C3 120.0 . . ?
C15 C58 H58 120.0 . . ?
C78 C10 H10 120.0 . . ?
C78 C10 C82 120.0 . . ?
C82 C10 H10 120.0 . . ?
C10 C78 H78 120.0 . . ?
C43 C78 C10 120.0 . . ?
C43 C78 H78 120.0 . . ?
C78 C43 S3 121.3(10) . . ?
C78 C43 C80 120.0 . . ?
C80 C43 S3 118.7(10) . . ?
C43 C80 Cl7 121.8(11) . . ?
C43 C80 C25 120.0 . . ?
C25 C80 Cl7 117.5(11) . . ?
C80 C25 H25 120.0 . . ?
C82 C25 C80 120.0 . . ?
C82 C25 H25 120.0 . . ?
C10 C82 Cl3 120.0(10) . . ?
C10 C82 Br6 120.0(10) . . ?
C25 C82 C10 120.0 . . ?
C25 C82 Cl3 119.9(10) . . ?
C25 C82 Br6 119.9(10) . . ?
C20 C17 Cl4 123.4(11) . . ?
C20 C17 C23 120.0 . . ?
C23 C17 Cl4 115.7(11) . . ?
C17 C20 S7 117.8(9) . . ?
C22 C20 S7 121.8(9) . . ?
C22 C20 C17 120.0 . . ?
C20 C22 H22 120.0 . . ?
C27 C22 C20 120.0 . . ?
C27 C22 H22 120.0 . . ?
C22 C27 H27 120.0 . . ?
C24 C27 C22 120.0 . . ?
C24 C27 H27 120.0 . . ?
C27 C24 C23 120.0 . . ?
C27 C24 Cl10 120.0(10) . . ?
C27 C24 Br8 120.0(10) . . ?
C23 C24 Cl10 119.3(9) . . ?
C23 C24 Br8 119.3(9) . . ?
C17 C23 H23 120.0 . . ?
C24 C23 C17 120.0 . . ?
C24 C23 H23 120.0 . . ?
C89 C28 C93 120.0 . . ?
C89 C28 Cl1 116.6(11) . . ?
C89 C28 Br7 116.6(11) . . ?
C93 C28 Cl1 122.6(11) . . ?
C93 C28 Br7 122.6(11) . . ?
C28 C89 H89 120.0 . . ?
C49 C89 C28 120.0 . . ?
C49 C89 H89 120.0 . . ?
C89 C49 Cl2 120.9(12) . . ?
C89 C49 C91 120.0 . . ?
C91 C49 Cl2 119.0(12) . . ?
C49 C91 S1 120.4(11) . . ?
C12 C91 S1 119.5(11) . . ?
C12 C91 C49 120.0 . . ?
C91 C12 H12 120.0 . . ?
C91 C12 C93 120.0 . . ?
C93 C12 H12 120.0 . . ?
C28 C93 H93 120.0 . . ?
C12 C93 C28 120.0 . . ?
C12 C93 H93 120.0 . . ?
C60 C32 S4 119.9(10) . . ?
C60 C32 C64 120.0 . . ?
C64 C32 S4 120.1(10) . . ?
C32 C60 Cl13 120.9(11) . . ?
C32 C60 C8 120.0 . . ?
C8 C60 Cl13 118.2(11) . . ?
C60 C8 H8 120.0 . . ?
C62 C8 C60 120.0 . . ?
C62 C8 H8 120.0 . . ?
C8 C62 Cl12 117.0(10) . . ?
C8 C62 Br1 117.0(10) . . ?
C34 C62 C8 120.0 . . ?
C34 C62 Cl12 122.4(10) . . ?
C34 C62 Br1 122.4(10) . . ?
C62 C34 H34 120.0 . . ?
C62 C34 C64 120.0 . . ?
C64 C34 H34 120.0 . . ?
C32 C64 H64 120.0 . . ?
C34 C64 C32 120.0 . . ?
C34 C64 H64 120.0 . . ?
C72 C38 C76 120.0 . . ?
C72 C38 Cl8 117.3(11) . . ?
C72 C38 Br4 117.3(11) . . ?
C76 C38 Cl8 122.5(11) . . ?
C76 C38 Br4 122.5(11) . . ?
C38 C72 H72 120.0 . . ?
C21 C72 C38 120.0 . . ?
C21 C72 H72 120.0 . . ?
C72 C21 H21 120.0 . . ?
C72 C21 C74 120.0 . . ?
C74 C21 H21 120.0 . . ?
C21 C74 S6 124.2(11) . . ?
C41 C74 S6 115.7(11) . . ?
C41 C74 C21 120.0 . . ?
C74 C41 Cl17 124.8(13) . . ?
C76 C41 Cl17 115.0(13) . . ?
C76 C41 C74 120.0 . . ?
C38 C76 H76 120.0 . . ?
C41 C76 C38 120.0 . . ?
C41 C76 H76 120.0 . . ?
C95 C51 H51 120.0 . . ?
C95 C51 C97 120.0 . . ?
C97 C51 H51 120.0 . . ?
C51 C95 C29 120.0 . . ?
C51 C95 Cl5 120.3(10) . . ?
C51 C95 Br2 120.3(10) . . ?
C29 C95 Cl5 118.9(10) . . ?
C29 C95 Br2 118.9(10) . . ?
C95 C29 H29 120.0 . . ?
C96 C29 C95 120.0 . . ?
C96 C29 H29 120.0 . . ?
C29 C96 H96 120.0 . . ?
C29 C96 C53 120.0 . . ?
C53 C96 H96 120.0 . . ?
C96 C53 S8 122.3(9) . . ?
C96 C53 C97 120.0 . . ?
C97 C53 S8 117.3(9) . . ?
C51 C97 Cl9 113.2(11) . . ?
C53 C97 Cl9 126.1(11) . . ?
C53 C97 C51 120.0 . . ?
C92 C90 S2 120.3(9) . . ?
C92 C90 C26 120.0 . . ?
C26 C90 S2 119.7(9) . . ?
C90 C92 Cl15 123.7(11) . . ?
C94 C92 Cl15 116.3(11) . . ?
C94 C92 C90 120.0 . . ?
C92 C94 H94 120.0 . . ?
C92 C94 C19 120.0 . . ?
C19 C94 H94 120.0 . . ?
C94 C19 Cl14 112.5(10) . . ?
C94 C19 Br3 112.5(10) . . ?
C7 C19 C94 120.0 . . ?
C7 C19 Cl14 126.8(11) . . ?
C7 C19 Br3 126.8(11) . . ?
C19 C7 H7 120.0 . . ?
C19 C7 C26 120.0 . . ?
C26 C7 H7 120.0 . . ?
C90 C26 H26 120.0 . . ?
C7 C26 C90 120.0 . . ?
C7 C26 H26 120.0 . . ?
C14 P1 C4 106.9(6) . . ?
C14 P1 C75 110.7(8) . . ?
C84 P1 C4 108.8(9) . . ?
C84 P1 C14 112.8(9) . . ?
C84 P1 C75 106.4(7) . . ?
C75 P1 C4 111.4(9) . . ?
C4 C1 H1 120.0 . . ?
C4 C1 C13 120.0 . . ?
C13 C1 H1 120.0 . . ?
C1 C4 P1 122.3(10) . . ?
C6 C4 P1 117.7(10) . . ?
C6 C4 C1 120.0 . . ?
C4 C6 H6 120.0 . . ?
C4 C6 C9 120.0 . . ?
C9 C6 H6 120.0 . . ?
C6 C9 H9 120.0 . . ?
C11 C9 C6 120.0 . . ?
C11 C9 H9 120.0 . . ?
C9 C11 H11 120.0 . . ?
C9 C11 C13 120.0 . . ?
C13 C11 H11 120.0 . . ?
C1 C13 H13 120.0 . . ?
C11 C13 C1 120.0 . . ?
C11 C13 H13 120.0 . . ?
C46 C44 H44 120.0 . . ?
C46 C44 C14 120.0 . . ?
C14 C44 H44 120.0 . . ?
C44 C46 H46 120.0 . . ?
C48 C46 C44 120.0 . . ?
C48 C46 H46 120.0 . . ?
C46 C48 H48 120.0 . . ?
C46 C48 C50 120.0 . . ?
C50 C48 H48 120.0 . . ?
C48 C50 H50 120.0 . . ?
C52 C50 C48 120.0 . . ?
C52 C50 H50 120.0 . . ?
C50 C52 H52 120.0 . . ?
C50 C52 C14 120.0 . . ?
C14 C52 H52 120.0 . . ?
C44 C14 P1 116.7(9) . . ?
C52 C14 P1 123.2(9) . . ?
C52 C14 C44 120.0 . . ?
C84 C45 H45 120.0 . . ?
C84 C45 C88 120.0 . . ?
C88 C45 H45 120.0 . . ?
C45 C84 P1 122.3(10) . . ?
C45 C84 C5 120.0 . . ?
C5 C84 P1 117.7(10) . . ?
C84 C5 H5 120.0 . . ?
C86 C5 C84 120.0 . . ?
C86 C5 H5 120.0 . . ?
C5 C86 H86 120.0 . . ?
C47 C86 C5 120.0 . . ?
C47 C86 H86 120.0 . . ?
C86 C47 H47 120.0 . . ?
C86 C47 C88 120.0 . . ?
C88 C47 H47 120.0 . . ?
C45 C88 H88 120.0 . . ?
C47 C88 C45 120.0 . . ?
C47 C88 H88 120.0 . . ?
C69 C67 H67 120.0 . . ?
C69 C67 C77 120.0 . . ?
C77 C67 H67 120.0 . . ?
C67 C69 H69 120.0 . . ?
C67 C69 C71 120.0 . . ?
C71 C69 H69 120.0 . . ?
C69 C71 H71 120.0 . . ?
C73 C71 C69 120.0 . . ?
C73 C71 H71 120.0 . . ?
C71 C73 H73 120.0 . . ?
C75 C73 C71 120.0 . . ?
C75 C73 H73 120.0 . . ?
C73 C75 P1 120.2(10) . . ?
C73 C75 C77 120.0 . . ?
C77 C75 P1 119.8(9) . . ?
C67 C77 H77 120.0 . . ?
C75 C77 C67 120.0 . . ?
C75 C77 H77 120.0 . . ?
C70 P2 C55 110.0(9) . . ?
C70 P2 C81 106.8(7) . . ?
C31 P2 C70 111.2(9) . . ?
C31 P2 C55 107.0(6) . . ?
C31 P2 C81 111.1(9) . . ?
C55 P2 C81 110.7(9) . . ?
C66 C18 H18 120.0 . . ?
C66 C18 C70 120.0 . . ?
C70 C18 H18 120.0 . . ?
C18 C66 H66 120.0 . . ?
C36 C66 C18 120.0 . . ?
C36 C66 H66 120.0 . . ?
C66 C36 H36 120.0 . . ?
C68 C36 C66 120.0 . . ?
C68 C36 H36 120.0 . . ?
C36 C68 H68 120.0 . . ?
C36 C68 C2 120.0 . . ?
C2 C68 H68 120.0 . . ?
C68 C2 H2 120.0 . . ?
C68 C2 C70 120.0 . . ?
C70 C2 H2 120.0 . . ?
C18 C70 P2 120.1(9) . . ?
C2 C70 P2 119.7(9) . . ?
C2 C70 C18 120.0 . . ?
C33 C31 P2 121.0(10) . . ?
C33 C31 C42 120.0 . . ?
C42 C31 P2 118.8(10) . . ?
C31 C33 H33 120.0 . . ?
C31 C33 C35 120.0 . . ?
C35 C33 H33 120.0 . . ?
C33 C35 H35 120.0 . . ?
C37 C35 C33 120.0 . . ?
C37 C35 H35 120.0 . . ?
C35 C37 H37 120.0 . . ?
C39 C37 C35 120.0 . . ?
C39 C37 H37 120.0 . . ?
C37 C39 H39 120.0 . . ?
C42 C39 C37 120.0 . . ?
C42 C39 H39 120.0 . . ?
C31 C42 H42 120.0 . . ?
C39 C42 C31 120.0 . . ?
C39 C42 H42 120.0 . . ?
C57 C55 P2 117.7(10) . . ?
C57 C55 C65 120.0 . . ?
C65 C55 P2 122.2(10) . . ?
C55 C57 H57 120.0 . . ?
C55 C57 C59 120.0 . . ?
C59 C57 H57 120.0 . . ?
C57 C59 H59 120.0 . . ?
C61 C59 C57 120.0 . . ?
C61 C59 H59 120.0 . . ?
C59 C61 H61 120.0 . . ?
C59 C61 C63 120.0 . . ?
C63 C61 H61 120.0 . . ?
C61 C63 H63 120.0 . . ?
C65 C63 C61 120.0 . . ?
C65 C63 H63 120.0 . . ?
C55 C65 H65 120.0 . . ?
C63 C65 C55 120.0 . . ?
C63 C65 H65 120.0 . . ?
C81 C79 H79 120.0 . . ?
C81 C79 C40 120.0 . . ?
C40 C79 H79 120.0 . . ?
C79 C81 P2 119.0(10) . . ?
C83 C81 P2 121.0(10) . . ?
C83 C81 C79 120.0 . . ?
C81 C83 H83 120.0 . . ?
C85 C83 C81 120.0 . . ?
C85 C83 H83 120.0 . . ?
C83 C85 H85 120.0 . . ?
C87 C85 C83 120.0 . . ?
C87 C85 H85 120.0 . . ?
C85 C87 H87 120.0 . . ?
C85 C87 C40 120.0 . . ?
C40 C87 H87 120.0 . . ?
C79 C40 H40 120.0 . . ?
C87 C40 C79 120.0 . . ?
C87 C40 H40 120.0 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Pt S2 C90 C92 70.8(10) . . . . ?
Pt S2 C90 C26 -111.2(9) . . . . ?
Pt S5 C3 C54 73.7(9) . . . . ?
Pt S5 C3 C58 -111.2(9) . . . . ?
Pt S7 C20 C17 66.2(11) . . . . ?
Pt S7 C20 C22 -120.9(9) . . . . ?
Pt S8 C53 C96 -113.8(10) . . . . ?
Pt S8 C53 C97 74.1(10) . . . . ?
Ag1 S2 C90 C92 169.9(8) . . . . ?
Ag1 S2 C90 C26 -12.1(12) . . . . ?
Ag1 S4 C32 C60 174.5(8) . . . . ?
Ag1 S4 C32 C64 -4.2(13) . . . . ?
Ag1 S6 C74 C21 72.2(13) . . . . ?
Ag1 S6 C74 C41 -106.4(10) . . . . ?
Ag2 S1 C91 C49 168.9(8) . . . . ?
Ag2 S1 C91 C12 -8.1(13) . . . . ?
Ag2 S4 C32 C60 -100.9(10) . . . . ?
Ag2 S4 C32 C64 80.4(11) . . . . ?
Ag2 S5 C3 C54 169.6(7) . . . . ?
Ag2 S5 C3 C58 -15.3(11) . . . . ?
Ag3 S3 C43 C78 72.5(11) . . . . ?
Ag3 S3 C43 C80 -109.6(9) . . . . ?
Ag3 S6 C74 C21 -12.9(14) . . . . ?
Ag3 S6 C74 C41 168.5(8) . . . . ?
Ag3 S7 C20 C17 163.9(9) . . . . ?
Ag3 S7 C20 C22 -23.2(12) . . . . ?
Ag4 S1 C91 C49 -104.6(10) . . . . ?
Ag4 S1 C91 C12 78.4(11) . . . . ?
Ag4 S3 C43 C78 -10.3(13) . . . . ?
Ag4 S3 C43 C80 167.6(8) . . . . ?
Ag4 S8 C53 C96 -18.4(12) . . . . ?
Ag4 S8 C53 C97 169.4(8) . . . . ?
Cl2 C49 C91 S1 -0.2(16) . . . . ?
Cl2 C49 C91 C12 176.8(16) . . . . ?
Cl4 C17 C20 S7 4.2(18) . . . . ?
Cl4 C17 C20 C22 -168.8(18) . . . . ?
Cl4 C17 C23 C24 169.6(17) . . . . ?
Cl7 C80 C25 C82 -170.7(15) . . . . ?
Cl11 C54 C30 C56 176.3(15) . . . . ?
Cl13 C60 C8 C62 -169.0(15) . . . . ?
Cl15 C92 C94 C19 180.0(16) . . . . ?
Cl17 C41 C76 C38 -174.7(16) . . . . ?
S1 C91 C12 C93 177.0(16) . . . . ?
S2 C90 C92 Cl15 -2.0(16) . . . . ?
S2 C90 C92 C94 177.9(13) . . . . ?
S2 C90 C26 C7 -177.9(13) . . . . ?
S3 C43 C80 Cl7 -7.6(15) . . . . ?
S3 C43 C80 C25 -177.9(15) . . . . ?
S4 C32 C60 Cl13 -10.0(15) . . . . ?
S4 C32 C60 C8 -178.7(15) . . . . ?
S4 C32 C64 C34 178.7(15) . . . . ?
S5 C3 C54 Cl11 -0.8(15) . . . . ?
S5 C3 C54 C30 175.2(13) . . . . ?
S5 C3 C58 C15 -175.2(13) . . . . ?
S6 C74 C41 Cl17 -7.1(16) . . . . ?
S6 C74 C41 C76 178.7(15) . . . . ?
S7 C20 C22 C27 -172.8(14) . . . . ?
S8 C53 C97 Cl9 2.5(17) . . . . ?
S8 C53 C97 C51 172.3(13) . . . . ?
C3 C54 C30 C56 0.0 . . . . ?
C54 C3 C58 C15 0.0 . . . . ?
C54 C30 C56 C15 0.0 . . . . ?
C54 C30 C56 Cl16 -171.3(13) . . . . ?
C54 C30 C56 Br5 -171.3(13) . . . . ?
C30 C56 C15 C58 0.0 . . . . ?
C56 C15 C58 C3 0.0 . . . . ?
C58 C3 C54 Cl11 -176.0(16) . . . . ?
C58 C3 C54 C30 0.0 . . . . ?
C10 C78 C43 S3 177.8(15) . . . . ?
C10 C78 C43 C80 0.0 . . . . ?
C78 C10 C82 C25 0.0 . . . . ?
C78 C10 C82 Cl3 176.2(16) . . . . ?
C78 C10 C82 Br6 176.2(16) . . . . ?
C78 C43 C80 Cl7 170.3(16) . . . . ?
C78 C43 C80 C25 0.0 . . . . ?
C43 C80 C25 C82 0.0 . . . . ?
C80 C25 C82 C10 0.0 . . . . ?
C80 C25 C82 Cl3 -176.2(16) . . . . ?
C80 C25 C82 Br6 -176.2(16) . . . . ?
C82 C10 C78 C43 0.0 . . . . ?
C17 C20 C22 C27 0.0 . . . . ?
C20 C17 C23 C24 0.0 . . . . ?
C20 C22 C27 C24 0.0 . . . . ?
C22 C27 C24 C23 0.0 . . . . ?
C22 C27 C24 Cl10 170.4(15) . . . . ?
C22 C27 C24 Br8 170.4(15) . . . . ?
C27 C24 C23 C17 0.0 . . . . ?
C23 C17 C20 S7 173.0(14) . . . . ?
C23 C17 C20 C22 0.0 . . . . ?
C28 C89 C49 Cl2 -176.7(17) . . . . ?
C28 C89 C49 C91 0.0 . . . . ?
C89 C28 C93 C12 0.0 . . . . ?
C89 C49 C91 S1 -176.9(16) . . . . ?
C89 C49 C91 C12 0.0 . . . . ?
C49 C91 C12 C93 0.0 . . . . ?
C91 C12 C93 C28 0.0 . . . . ?
C93 C28 C89 C49 0.0 . . . . ?
C32 C60 C8 C62 0.0 . . . . ?
C60 C32 C64 C34 0.0 . . . . ?
C60 C8 C62 C34 0.0 . . . . ?
C60 C8 C62 Cl12 -170.9(15) . . . . ?
C60 C8 C62 Br1 -170.9(15) . . . . ?
C8 C62 C34 C64 0.0 . . . . ?
C62 C34 C64 C32 0.0 . . . . ?
C64 C32 C60 Cl13 168.7(15) . . . . ?
C64 C32 C60 C8 0.0 . . . . ?
C38 C72 C21 C74 0.0 . . . . ?
C72 C38 C76 C41 0.0 . . . . ?
C72 C21 C74 S6 -178.5(16) . . . . ?
C72 C21 C74 C41 0.0 . . . . ?
C21 C74 C41 Cl17 174.2(17) . . . . ?
C21 C74 C41 C76 0.0 . . . . ?
C74 C41 C76 C38 0.0 . . . . ?
C76 C38 C72 C21 0.0 . . . . ?
C51 C95 C29 C96 0.0 . . . . ?
C95 C51 C97 Cl9 171.1(15) . . . . ?
C95 C51 C97 C53 0.0 . . . . ?
C95 C29 C96 C53 0.0 . . . . ?
C29 C96 C53 S8 -171.9(13) . . . . ?
C29 C96 C53 C97 0.0 . . . . ?
C96 C53 C97 Cl9 -169.9(18) . . . . ?
C96 C53 C97 C51 0.0 . . . . ?
C97 C51 C95 C29 0.0 . . . . ?
C97 C51 C95 Cl5 -169.9(15) . . . . ?
C97 C51 C95 Br2 -169.9(15) . . . . ?
C90 C92 C94 C19 0.0 . . . . ?
C92 C90 C26 C7 0.0 . . . . ?
C92 C94 C19 C7 0.0 . . . . ?
C92 C94 C19 Cl14 -170.9(13) . . . . ?
C92 C94 C19 Br3 -170.9(13) . . . . ?
C94 C19 C7 C26 0.0 . . . . ?
C19 C7 C26 C90 0.0 . . . . ?
C26 C90 C92 Cl15 -180.0(17) . . . . ?
C26 C90 C92 C94 0.0 . . . . ?
Cl12 C62 C34 C64 170.3(16) . . . . ?
Br1 C62 C34 C64 170.3(16) . . . . ?
Cl8 C38 C72 C21 174.5(14) . . . . ?
Cl8 C38 C76 C41 -174.2(15) . . . . ?
Br4 C38 C72 C21 174.5(14) . . . . ?
Br4 C38 C76 C41 -174.2(15) . . . . ?
Cl1 C28 C89 C49 -169.8(16) . . . . ?
Cl1 C28 C93 C12 169.1(17) . . . . ?
Br7 C28 C89 C49 -169.8(16) . . . . ?
Br7 C28 C93 C12 169.1(17) . . . . ?
Cl5 C95 C29 C96 170.0(14) . . . . ?
Br2 C95 C29 C96 170.0(14) . . . . ?
Cl16 C56 C15 C58 170.4(14) . . . . ?
Br5 C56 C15 C58 170.4(14) . . . . ?
Cl14 C19 C7 C26 169.5(15) . . . . ?
Br3 C19 C7 C26 169.5(15) . . . . ?
Cl10 C24 C23 C17 -170.4(15) . . . . ?
Br8 C24 C23 C17 -170.4(15) . . . . ?
P1 C4 C6 C9 179.5(13) . . . . ?
P1 C84 C5 C86 179.7(15) . . . . ?
P1 C75 C77 C67 176.9(14) . . . . ?
C1 C4 C6 C9 0.0 . . . . ?
C4 P1 C14 C44 53.1(12) . . . . ?
C4 P1 C14 C52 -129.6(10) . . . . ?
C4 P1 C84 C45 7.2(15) . . . . ?
C4 P1 C84 C5 -172.5(11) . . . . ?
C4 P1 C75 C73 69.4(12) . . . . ?
C4 P1 C75 C77 -107.5(11) . . . . ?
C4 C1 C13 C11 0.0 . . . . ?
C4 C6 C9 C11 0.0 . . . . ?
C6 C9 C11 C13 0.0 . . . . ?
C9 C11 C13 C1 0.0 . . . . ?
C13 C1 C4 P1 -179.5(13) . . . . ?
C13 C1 C4 C6 0.0 . . . . ?
C44 C46 C48 C50 0.0 . . . . ?
C46 C44 C14 P1 177.4(12) . . . . ?
C46 C44 C14 C52 0.0 . . . . ?
C46 C48 C50 C52 0.0 . . . . ?
C48 C50 C52 C14 0.0 . . . . ?
C50 C52 C14 P1 -177.2(13) . . . . ?
C50 C52 C14 C44 0.0 . . . . ?
C14 P1 C4 C1 -125.6(10) . . . . ?
C14 P1 C4 C6 54.9(12) . . . . ?
C14 P1 C84 C45 -111.3(13) . . . . ?
C14 P1 C84 C5 69.0(13) . . . . ?
C14 P1 C75 C73 -171.8(10) . . . . ?
C14 P1 C75 C77 11.2(13) . . . . ?
C14 C44 C46 C48 0.0 . . . . ?
C45 C84 C5 C86 0.0 . . . . ?
C84 P1 C4 C1 112.3(12) . . . . ?
C84 P1 C4 C6 -67.2(12) . . . . ?
C84 P1 C14 C44 172.6(9) . . . . ?
C84 P1 C14 C52 -10.1(13) . . . . ?
C84 P1 C75 C73 -48.9(14) . . . . ?
C84 P1 C75 C77 134.1(10) . . . . ?
C84 C45 C88 C47 0.0 . . . . ?
C84 C5 C86 C47 0.0 . . . . ?
C5 C86 C47 C88 0.0 . . . . ?
C86 C47 C88 C45 0.0 . . . . ?
C88 C45 C84 P1 -179.7(16) . . . . ?
C88 C45 C84 C5 0.0 . . . . ?
C67 C69 C71 C73 0.0 . . . . ?
C69 C67 C77 C75 0.0 . . . . ?
C69 C71 C73 C75 0.0 . . . . ?
C71 C73 C75 P1 -176.9(14) . . . . ?
C71 C73 C75 C77 0.0 . . . . ?
C73 C75 C77 C67 0.0 . . . . ?
C75 P1 C4 C1 -4.6(13) . . . . ?
C75 P1 C4 C6 175.9(9) . . . . ?
C75 P1 C14 C44 -68.3(11) . . . . ?
C75 P1 C14 C52 108.9(11) . . . . ?
C75 P1 C84 C45 127.2(11) . . . . ?
C75 P1 C84 C5 -52.5(14) . . . . ?
C77 C67 C69 C71 0.0 . . . . ?
P2 C31 C33 C35 175.2(13) . . . . ?
P2 C31 C42 C39 -175.3(13) . . . . ?
P2 C55 C57 C59 -176.9(13) . . . . ?
P2 C55 C65 C63 176.8(14) . . . . ?
P2 C81 C83 C85 -179.1(15) . . . . ?
C18 C66 C36 C68 0.0 . . . . ?
C66 C18 C70 P2 175.3(13) . . . . ?
C66 C18 C70 C2 0.0 . . . . ?
C66 C36 C68 C2 0.0 . . . . ?
C36 C68 C2 C70 0.0 . . . . ?
C68 C2 C70 P2 -175.3(13) . . . . ?
C68 C2 C70 C18 0.0 . . . . ?
C70 P2 C31 C33 12.2(13) . . . . ?
C70 P2 C31 C42 -172.5(9) . . . . ?
C70 P2 C55 C57 69.9(11) . . . . ?
C70 P2 C55 C65 -106.9(11) . . . . ?
C70 P2 C81 C79 46.0(13) . . . . ?
C70 P2 C81 C83 -134.9(11) . . . . ?
C70 C18 C66 C36 0.0 . . . . ?
C31 P2 C70 C18 -75.1(12) . . . . ?
C31 P2 C70 C2 100.2(11) . . . . ?
C31 P2 C55 C57 -51.1(13) . . . . ?
C31 P2 C55 C65 132.1(10) . . . . ?
C31 P2 C81 C79 167.5(10) . . . . ?
C31 P2 C81 C83 -13.4(14) . . . . ?
C31 C33 C35 C37 0.0 . . . . ?
C33 C31 C42 C39 0.0 . . . . ?
C33 C35 C37 C39 0.0 . . . . ?
C35 C37 C39 C42 0.0 . . . . ?
C37 C39 C42 C31 0.0 . . . . ?
C42 C31 C33 C35 0.0 . . . . ?
C55 P2 C70 C18 166.5(10) . . . . ?
C55 P2 C70 C2 -18.2(13) . . . . ?
C55 P2 C31 C33 132.5(10) . . . . ?
C55 P2 C31 C42 -52.3(13) . . . . ?
C55 P2 C81 C79 -73.8(12) . . . . ?
C55 P2 C81 C83 105.3(12) . . . . ?
C55 C57 C59 C61 0.0 . . . . ?
C57 C55 C65 C63 0.0 . . . . ?
C57 C59 C61 C63 0.0 . . . . ?
C59 C61 C63 C65 0.0 . . . . ?
C61 C63 C65 C55 0.0 . . . . ?
C65 C55 C57 C59 0.0 . . . . ?
C79 C81 C83 C85 0.0 . . . . ?
C81 P2 C70 C18 46.2(13) . . . . ?
C81 P2 C70 C2 -138.4(10) . . . . ?
C81 P2 C31 C33 -106.6(12) . . . . ?
C81 P2 C31 C42 68.7(12) . . . . ?
C81 P2 C55 C57 -172.2(9) . . . . ?
C81 P2 C55 C65 10.9(13) . . . . ?
C81 C79 C40 C87 0.0 . . . . ?
C81 C83 C85 C87 0.0 . . . . ?
C83 C85 C87 C40 0.0 . . . . ?
C85 C87 C40 C79 0.0 . . . . ?
C40 C79 C81 P2 179.1(14) . . . . ?
C40 C79 C81 C83 0.0 . . . . ?

_smtbx_masks_special_details     ?
loop_
_smtbx_masks_void_nr
_smtbx_masks_void_average_x
_smtbx_masks_void_average_y
_smtbx_masks_void_average_z
_smtbx_masks_void_volume
_smtbx_masks_void_count_electrons
_smtbx_masks_void_content
1 0.000 0.000 0.000 0.2 0.1 ?
2 0.073 0.219 0.620 7.2 0.5 ?
3 -0.073 0.781 0.380 7.2 0.4 ?
4 0.010 0.031 0.030 0.0 0.0 ?
5 0.021 0.031 0.010 0.0 0.0 ?
6 0.255 0.979 0.385 10.0 1.1 ?
7 0.407 0.896 0.895 15.9 0.8 ?
8 0.482 0.641 0.383 9.1 1.4 ?
9 0.518 0.359 0.617 9.1 1.6 ?
10 0.593 0.104 0.105 15.9 0.8 ?
11 0.745 0.021 0.615 10.0 1.0 ?
12 0.979 0.969 0.990 0.0 0.0 ?
13 0.990 0.969 0.970 0.0 0.0 ?

_smtbx_masks_void_probe_radius   1.2
_smtbx_masks_void_truncation_radius 1.2
_olex2_submission_special_instructions 'No special instructions were received'
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_1_pl
_database_code_depnum_ccdc_archive 'CCDC 2327472'
loop_
_audit_author_name
_audit_author_address
'shuxin wang'
;Qingdao University of Science and Technology
China
;
_audit_update_record             
;
2024-01-20 deposited with the CCDC.	2024-03-22 downloaded from the CCDC.
;
_audit_creation_date             2024-01-18
_audit_creation_method           
;
Olex2 1.3
(compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6408)
;
_shelx_SHELXL_version_number     2019/1
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         
'C120 H54 Ag24 Br17.72 Cl4.56 Pt S20, 4(C24 H20 P)'
_chemical_formula_sum            'C216 H134 Ag24 Br17.72 Cl4.56 P4 Pt S20'
_chemical_formula_weight         7855.93
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag 0.1306 4.2820 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Br Br -0.6763 1.2805 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -4.5932 6.9264 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           15
_space_group_name_H-M_alt        'C 1 2/c 1'
_space_group_name_Hall           '-C 2yc'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'

_cell_length_a                   32.937
_cell_length_b                   28.819
_cell_length_c                   28.779
_cell_angle_alpha                90
_cell_angle_beta                 93.52
_cell_angle_gamma                90
_cell_volume                     27265.8
_cell_formula_units_Z            4
_cell_measurement_reflns_used    1456
_cell_measurement_temperature    120.15
_cell_measurement_theta_max      130.51
_cell_measurement_theta_min      5.68
_shelx_estimated_absorpt_T_max   0.382
_shelx_estimated_absorpt_T_min   0.242
_exptl_absorpt_coefficient_mu    19.837
_exptl_absorpt_correction_T_max  1.0
_exptl_absorpt_correction_T_min  0.162
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
STOE LANA, absorption correction by scaling of reflection intensities.
J. Koziskova, F. Hahn, J. Richter, J. Kozisek, "Comparison of different
absorption corrections on the model structure of tetrakis(μ₂-acetato)-
diaqua-di-copper(II)", Acta Chimica Slovaca, vol. 9, no. 2, 2016, pp. 136 - 140.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            black
_exptl_crystal_colour_primary    black
_exptl_crystal_density_diffrn    1.914
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             14855
_exptl_crystal_size_max          0.1
_exptl_crystal_size_mid          0.08
_exptl_crystal_size_min          0.06
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0827
_diffrn_reflns_av_unetI/netI     0.0770
_diffrn_reflns_Laue_measured_fraction_full 0.989
_diffrn_reflns_Laue_measured_fraction_max 0.974
_diffrn_reflns_limit_h_max       38
_diffrn_reflns_limit_h_min       -39
_diffrn_reflns_limit_k_max       35
_diffrn_reflns_limit_k_min       -31
_diffrn_reflns_limit_l_max       34
_diffrn_reflns_limit_l_min       -14
_diffrn_reflns_number            91043
_diffrn_reflns_point_group_measured_fraction_full 0.989
_diffrn_reflns_point_group_measured_fraction_max 0.974
_diffrn_reflns_theta_full        67.686
_diffrn_reflns_theta_max         69.754
_diffrn_reflns_theta_min         4.302
_diffrn_ambient_temperature      120.15
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.989
_diffrn_measured_fraction_theta_max 0.974
_diffrn_measurement_device_type  STOE
_diffrn_measurement_method       ?
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54186
_diffrn_source                   ?
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                16328
_reflns_number_total             25046
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       ?
_computing_data_collection       ?
_computing_data_reduction        ?
_computing_molecular_graphics    'Olex2 1.3 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.3 (Dolomanov et al., 2009)'
_computing_structure_refinement  'XL  (Sheldrick, 2008)'
_computing_structure_solution    ?
_refine_diff_density_max         1.848
_refine_diff_density_min         -1.818
_refine_diff_density_rms         0.161
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.946
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1342
_refine_ls_number_reflns         25046
_refine_ls_number_restraints     181
_refine_ls_R_factor_all          0.0851
_refine_ls_R_factor_gt           0.0561
_refine_ls_restrained_S_all      0.953
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0897P)²] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1403
_refine_ls_wR_factor_ref         0.1526
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups
2. Shared sites
{Br10, Cl10}
{Br13, Cl13}
{Br1N, Cl1N}
{Br0X, Cl0X}
{Br1, Cl2}
3. Restrained distances
 Cl03-C046
 1.5 with sigma of 0.01
4. Uiso/Uaniso restraints and constraints
S3 \\sim C13 \\sim C2 \\sim C26 \\sim C35 \\sim C34 \\sim C27 \\sim Br2: within
2A with sigma of 0.01 and sigma for terminal atoms of 0.02 within 2A
P01U \\sim C072 \\sim C07P \\sim C07Z \\sim C07V \\sim C111 \\sim C1: within 2A
with sigma of 0.01 and sigma for terminal atoms of 0.02 within 2A
C06Q \\sim C06C \\sim C05S \\sim C05Q \\sim C07Q \\sim C07A: within 2A with
sigma of 0.005 and sigma for terminal atoms of 0.01 within 2A
S1Q \\sim C042 \\sim C03T \\sim C05I \\sim C06J \\sim C05M \\sim Cl15 \\sim
Br1N: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02 within
2A
Cl15 \\sim C070 \\sim C042 \\sim S1Q \\sim C03T \\sim C05I \\sim C06J \\sim
C05M \\sim Br1N: within 2A with sigma of 0.01 and sigma for terminal atoms of
0.02 within 2A
Uanis(Br10) = Uanis(Cl10)
Uanis(Br13) = Uanis(Cl13)
Uanis(Br1N) = Uanis(Cl1N)
Uanis(Br0X) = Uanis(Cl0X)
Uanis(Br1) = Uanis(Cl2)
5. Others
 Fixed Sof: Br1(0.36) Br1N(0.76) Br0X(0.75) Br10(0.71) Br13(0.78) S01X(0.5)
 S3(0.5) Cl07(0.22) Cl03(0.25) Br2(0.5) C10(0.5) C7(0.5) C8(0.5) C12(0.5)
 C5(0.5) C15(0.5) C35(0.5) C26(0.5) C2(0.5) C13(0.5) C27(0.5) C34(0.5)
 Cl5(0.29) Cl10(0.29) Cl13(0.22) Cl15(0.24) Cl1N(0.24) Cl0X(0.25) Cl1(0.14)
 Cl2(0.14)
6.a Aromatic/amide H refined with riding coordinates:
 C02C(H02C), C02J(H02J), C035(H035), C05D(H05D), C06Z(H06Z), C05B(H05B),
 C02Y(H02Y), C02Z(H02Z), C030(H030), C02H(H02H), C03K(H03K), C04P(H04P),
 C031(H031), C034(H034), C02L(H02L), C03A(H03A), C03H(H03H), C03P(H03P),
 C05V(H05V), C05Z(H05Z), C04I(H04I), C03T(H03T), C05I(H05I), C05M(H05M),
 C03V(H03V), C04Q(H04Q), C02U(H02U), C38(H38), C058(H058), C049(H049),
 C079(H079), C07S(H07S), C06W(H06W), C05G(H05G), C05Y(H05Y), C06O(H06O),
 C075(H075), C044(H044), C067(H067), C05L(H05L), C064(H064), C04C(H04C),
 C071(H071), C05W(H05W), C039(H039), C05N(H05N), C07F(H07F), C111(H111), C1(H1),
  C07P(H07P), C07Z(H07Z), C07V(H07V), C05S(H05S), C06C(H06C), C06Q(H06Q),
 C07A(H07A), C07Q(H07Q), C06K(H06K), C06H(H06H), C065(H065), C06Y(H06Y),
 C037(H037), C06V(H06V), C06G(H06G), C06L(H06L), C07N(H07N), C073(H073)
6.b Fitted hexagon refined as free rotating group:
 C070(C042,C03T,C05I,C06J,C05M), C111(C1,C072,C07P,C07Z,C07V), C05Q(C05S,C06C,
 C06Q,C07A,C07Q), C10(C7,C8,C12,C5,C15), C35(C26,C2,C13,C27,C34)
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt01 Pt -0.750000 0.250000 1.000000 0.03518(11) Uani 1 2 d S . P . .
Ag03 Ag -0.73637(2) 0.17626(2) 0.94267(2) 0.03993(14) Uani 1 1 d . . . . .
Ag04 Ag -0.73194(2) 0.26909(2) 0.91034(2) 0.04161(15) Uani 1 1 d . . . . .
Ag06 Ag -0.69000(2) 0.26898(2) 1.06854(2) 0.04085(14) Uani 1 1 d . . . . .
Ag08 Ag -0.71297(2) 0.17440(2) 1.04111(2) 0.03998(14) Uani 1 1 d . . . . .
Ag0B Ag -0.79725(2) 0.17235(2) 1.01230(2) 0.04234(15) Uani 1 1 d . . . . .
Ag0E Ag -0.67046(2) 0.23535(2) 0.98007(2) 0.04079(14) Uani 1 1 d . . . . .
Ag0G Ag -0.63064(2) 0.12421(2) 1.05750(2) 0.04928(17) Uani 1 1 d . . . . .
Ag0H Ag -0.60297(2) 0.22456(2) 1.07623(3) 0.05086(17) Uani 1 1 d . . . . .
Ag0J Ag -0.61797(2) 0.17172(3) 0.92094(3) 0.05215(18) Uani 1 1 d . . . . .
Ag0M Ag -0.70813(2) 0.07567(2) 0.95024(3) 0.05261(18) Uani 1 1 d . . . . .
Ag0O Ag -0.68654(3) 0.19975(3) 0.85425(3) 0.0620(2) Uani 1 1 d . . . . .
Ag0P Ag -0.76429(3) 0.07392(3) 1.02868(3) 0.0614(2) Uani 1 1 d . . . . .
Br1 Br -0.57974(11) 0.04983(11) 0.69080(11) 0.0756(8) Uani 0.36 1 d . . P A 1
Br0S Br -0.51871(4) -0.07010(4) 0.92974(5) 0.0724(4) Uani 1 1 d . . . B 1
Br1N Br -0.85798(14) -0.07381(8) 0.82909(10) 0.1899(18) Uani 0.76 1 d . U P C 1
Br0T Br -0.72617(5) 0.13871(6) 1.29516(5) 0.0883(4) Uani 1 1 d . . . D 1
Br0V Br -0.88777(5) 0.07663(5) 0.76039(6) 0.0967(5) Uani 1 1 d . . . E 1
Br0X Br -0.55535(6) 0.10449(6) 1.31323(5) 0.0837(5) Uani 0.75 1 d . . P F 1
Br10 Br -0.63958(6) 0.24021(7) 1.33052(5) 0.0855(5) Uani 0.71 1 d . . P G 1
Br11 Br -0.50933(7) 0.41704(6) 0.92548(8) 0.1203(7) Uani 1 1 d . . . H 1
Br13 Br -0.95212(9) 0.01524(9) 0.87792(8) 0.1341(10) Uani 0.78 1 d . . P I 1
Br15 Br -0.57493(8) 0.40899(11) 0.78793(10) 0.1608(11) Uani 1 1 d . . . J 1
S01X S -0.61498(16) 0.20665(16) 0.84224(18) 0.0500(11) Uani 0.5 1 d . . P A 1
S1A S -0.63556(7) 0.10317(8) 0.97157(8) 0.0469(5) Uani 1 1 d . . . . .
S1B S -0.69951(7) 0.09866(7) 1.07905(8) 0.0451(5) Uani 1 1 d . . . . .
S1D S -0.71968(7) 0.12306(7) 0.87839(8) 0.0452(5) Uani 1 1 d . . . . .
S1E S -0.59579(7) 0.22696(8) 0.98637(8) 0.0456(5) Uani 1 1 d . . . . .
S1G S -0.62858(8) 0.29426(8) 1.11457(8) 0.0488(5) Uani 1 1 d . . . . .
S1H S -0.72180(9) 0.27176(9) 0.82697(8) 0.0558(6) Uani 1 1 d . . . . .
S1K S -0.56601(8) 0.15071(9) 1.09401(9) 0.0515(6) Uani 1 1 d . . . . .
S1M S -0.83316(9) 0.10328(9) 1.03957(9) 0.0594(7) Uani 1 1 d . . . . .
S1Q S -0.73274(11) 0.00704(10) 0.98977(12) 0.0742(8) Uani 1 1 d . U . . .
S3 S -0.61475(18) 0.16023(19) 0.8388(2) 0.0600(13) Uani 0.5 1 d . U P A 2
Cl07 Cl -0.8937(6) 0.0149(7) 1.0487(6) 0.102(6) Uani 0.22 1 d . . P . .
Cl03 Cl -0.5689(4) 0.0488(3) 1.1343(4) 0.070(3) Uani 0.25 1 d D . P . .
C026 C -0.5552(3) -0.0205(3) 0.9435(4) 0.056(3) Uani 1 1 d . . . . .
C029 C -0.7677(3) 0.1125(3) 0.8463(3) 0.044(2) Uani 1 1 d . . . . .
C02A C -0.6046(3) 0.0547(3) 0.9606(3) 0.044(2) Uani 1 1 d . . . . .
C02C C -0.5548(3) -0.0030(4) 0.9860(3) 0.053(2) Uani 1 1 d . . . . .
H02C H -0.537984 -0.016680 1.010251 0.064 Uiso 1 1 calc R U . . .
C02J C -0.7795(3) 0.1398(4) 0.8098(4) 0.054(2) Uani 1 1 d . . . . .
H02J H -0.763471 0.165866 0.802486 0.065 Uiso 1 1 calc R U . . .
C02W C -0.8652(3) 0.0789(4) 0.9937(4) 0.055(3) Uani 1 1 d . . . . .
C02X C -0.6800(4) 0.3080(4) 0.8190(4) 0.063(3) Uani 1 1 d . . . . .
C035 C -0.6585(4) 0.3311(4) 0.8561(5) 0.072(3) Uani 1 1 d . . . . .
H035 H -0.665344 0.325288 0.887160 0.086 Uiso 1 1 calc R U . . .
C05D C -0.6276(5) 0.3622(5) 0.8478(6) 0.095(5) Uani 1 1 d . . . . .
H05D H -0.612849 0.378064 0.872367 0.114 Uiso 1 1 calc R U . . .
C05P C -0.6191(5) 0.3689(6) 0.8004(7) 0.097(5) Uani 1 1 d . . . . .
C06Z C -0.6374(6) 0.3450(7) 0.7656(6) 0.110(6) Uani 1 1 d . . . . .
H06Z H -0.628062 0.348447 0.735185 0.131 Uiso 1 1 calc R U . . .
C05B C -0.6686(4) 0.3159(5) 0.7720(5) 0.088(4) Uani 1 1 d . . . . .
H05B H -0.682781 0.301102 0.746376 0.105 Uiso 1 1 calc R U . . .
C02Y C -0.5799(4) -0.0020(4) 0.9079(4) 0.071(3) Uani 1 1 d . . . . .
H02Y H -0.579864 -0.014607 0.877445 0.085 Uiso 1 1 calc R U . . .
C02Z C -0.8155(4) 0.1298(4) 0.7826(4) 0.058(3) Uani 1 1 d . . . . .
H02Z H -0.823954 0.148803 0.756789 0.070 Uiso 1 1 calc R U . . .
C030 C -0.7502(3) 0.1083(3) 1.2032(4) 0.055(3) Uani 1 1 d . . . . .
H030 H -0.775590 0.102402 1.215968 0.066 Uiso 1 1 calc R U . . .
C02H C -0.7452(3) 0.1000(3) 1.1560(4) 0.052(2) Uani 1 1 d . . . . .
H02H H -0.767009 0.088413 1.136209 0.062 Uiso 1 1 calc R U . . .
C024 C -0.7066(3) 0.1094(3) 1.1385(3) 0.045(2) Uani 1 1 d . . . . .
C03K C -0.6754(3) 0.1265(3) 1.1687(3) 0.053(2) Uani 1 1 d . . . . .
H03K H -0.649788 0.133489 1.156943 0.063 Uiso 1 1 calc R U . . .
C04P C -0.6807(4) 0.1332(4) 1.2140(4) 0.063(3) Uani 1 1 d . . . . .
H04P H -0.658673 0.143698 1.234175 0.075 Uiso 1 1 calc R U . . .
C02T C -0.7179(4) 0.1249(4) 1.2310(3) 0.058(3) Uani 1 1 d . . . . .
C031 C -0.6047(4) 0.0348(4) 0.9168(4) 0.060(3) Uani 1 1 d . . . . .
H031 H -0.622255 0.046880 0.892380 0.072 Uiso 1 1 calc R U . . .
C033 C -0.8265(4) 0.0632(4) 0.8330(4) 0.067(3) Uani 1 1 d . . . . .
C034 C -0.5696(4) 0.1625(4) 1.2328(4) 0.067(3) Uani 1 1 d . . . . .
H034 H -0.574100 0.186413 1.254687 0.081 Uiso 1 1 calc R U . . .
C02L C -0.5712(4) 0.1729(4) 1.1878(3) 0.057(3) Uani 1 1 d . . . . .
H02L H -0.576184 0.204112 1.178397 0.068 Uiso 1 1 calc R U . . .
C02F C -0.5657(3) 0.1391(3) 1.1539(3) 0.047(2) Uani 1 1 d . . . . .
C046 C -0.5596(5) 0.0904(4) 1.1679(4) 0.078(4) Uani 1 1 d D . . . .
C057 C -0.5561(5) 0.0830(4) 1.2167(4) 0.081(4) Uani 1 1 d . . . . .
C043 C -0.5616(4) 0.1177(4) 1.2490(4) 0.064(3) Uani 1 1 d . . . . .
C03A C -0.8666(3) 0.0983(4) 0.9490(3) 0.052(2) Uani 1 1 d . . . . .
H03A H -0.849474 0.123694 0.942300 0.063 Uiso 1 1 calc R U . . .
C03H C -0.5784(3) 0.0350(4) 0.9955(3) 0.054(2) Uani 1 1 d . . . . .
H03H H -0.576946 0.047920 1.025892 0.064 Uiso 1 1 calc R U . . .
C03I C -0.8388(4) 0.0906(4) 0.7946(4) 0.062(3) Uani 1 1 d . . . . .
C03P C -0.5719(4) 0.3184(4) 0.9984(5) 0.075(4) Uani 1 1 d . . . . .
H03P H -0.583583 0.317049 1.027708 0.090 Uiso 1 1 calc R U . . .
C02Q C -0.5739(3) 0.2806(3) 0.9691(4) 0.050(2) Uani 1 1 d . . . . .
C05V C -0.5561(5) 0.2843(5) 0.9258(5) 0.090(5) Uani 1 1 d . . . . .
H05V H -0.556865 0.258616 0.905116 0.109 Uiso 1 1 calc R U . . .
C05Z C -0.5379(6) 0.3243(5) 0.9135(6) 0.109(6) Uani 1 1 d . . . . .
H05Z H -0.526491 0.326664 0.884031 0.131 Uiso 1 1 calc R U . . .
C04J C -0.5360(4) 0.3606(4) 0.9427(5) 0.079(4) Uani 1 1 d . . . . .
C04I C -0.5528(4) 0.3584(4) 0.9845(5) 0.078(4) Uani 1 1 d . . . . .
H04I H -0.551369 0.384580 1.004545 0.093 Uiso 1 1 calc R U . . .
C03R C -0.8913(4) 0.0428(4) 1.0029(5) 0.071(3) Uani 1 1 d . . . . .
C070 C -0.7534(3) -0.0376(3) 0.9070(3) 0.093(3) Uani 1 1 d G U . . .
C042 C -0.7681(3) -0.0174(3) 0.9465(3) 0.074(2) Uani 1 1 d G U . . .
C03T C -0.8097(3) -0.0158(3) 0.9518(2) 0.073(3) Uani 1 1 d G U . . .
H03T H -0.819751 -0.002023 0.978842 0.088 Uiso 1 1 calc R U . . .
C05I C -0.8366(2) -0.0344(3) 0.9177(3) 0.095(3) Uani 1 1 d G U . . .
H05I H -0.865088 -0.033278 0.921352 0.114 Uiso 1 1 calc R U . . .
C06J C -0.8219(3) -0.0546(3) 0.8782(3) 0.107(3) Uani 1 1 d G U . . .
C05M C -0.7803(4) -0.0562(3) 0.8729(3) 0.099(3) Uani 1 1 d G U . . .
H05M H -0.770250 -0.069968 0.845869 0.119 Uiso 1 1 calc R U . . .
C03V C -0.8938(4) 0.0796(4) 0.9138(4) 0.069(3) Uani 1 1 d . . . . .
H03V H -0.895422 0.092159 0.883219 0.083 Uiso 1 1 calc R U . . .
C04B C -0.7900(3) 0.0740(3) 0.8578(4) 0.055(3) Uani 1 1 d . . . . .
C04F C -0.9182(5) 0.0420(5) 0.9253(5) 0.083(4) Uani 1 1 d . . . . .
C04O C -0.9171(5) 0.0240(5) 0.9681(6) 0.093(4) Uani 1 1 d . . . . .
C04Q C -0.6679(4) 0.2438(4) 1.2362(4) 0.065(3) Uani 1 1 d . . . . .
H04Q H -0.690427 0.226559 1.246099 0.078 Uiso 1 1 calc R U . . .
C02U C -0.6649(3) 0.2551(3) 1.1896(3) 0.051(2) Uani 1 1 d . . . . .
H02U H -0.686143 0.245579 1.167840 0.062 Uiso 1 1 calc R U . . .
C02B C -0.6325(3) 0.2796(3) 1.1733(3) 0.051(2) Uani 1 1 d . . . . .
C03U C -0.6031(3) 0.2955(4) 1.2068(4) 0.059(3) Uani 1 1 d . . . . .
C052 C -0.6045(4) 0.2852(5) 1.2531(4) 0.070(3) Uani 1 1 d . . . . .
C03G C -0.6373(4) 0.2582(5) 1.2676(4) 0.073(4) Uani 1 1 d . . . . .
P01P P -0.71477(12) 0.05677(10) 0.68562(11) 0.0706(9) Uani 1 1 d . . . K 1
C38 C -0.6463(6) 0.0981(6) 0.5791(7) 0.119(7) Uani 1 1 d . . . K 1
H38 H -0.638385 0.126413 0.565448 0.143 Uiso 1 1 calc R U . K 1
C058 C -0.7847(6) 0.0134(5) 0.7051(6) 0.095(5) Uani 1 1 d . . . K 1
H058 H -0.775791 0.018182 0.736784 0.115 Uiso 1 1 calc R U . K 1
C04E C -0.7617(4) 0.0275(4) 0.6701(5) 0.072(3) Uani 1 1 d . . . K 1
C049 C -0.7752(5) 0.0210(5) 0.6242(5) 0.091(5) Uani 1 1 d . . . K 1
H049 H -0.758927 0.030567 0.599784 0.109 Uiso 1 1 calc R U . K 1
C079 C -0.8130(5) 0.0002(5) 0.6140(6) 0.101(5) Uani 1 1 d . . . K 1
H079 H -0.822730 -0.003727 0.582495 0.122 Uiso 1 1 calc R U . K 1
C07S C -0.8352(6) -0.0141(5) 0.6477(8) 0.113(6) Uani 1 1 d . . . K 1
H07S H -0.860741 -0.028396 0.640339 0.135 Uiso 1 1 calc R U . K 1
C06W C -0.8216(7) -0.0083(6) 0.6932(7) 0.111(6) Uani 1 1 d . . . K 1
H06W H -0.837762 -0.019399 0.717090 0.133 Uiso 1 1 calc R U . K 1
C05G C -0.6659(5) -0.0092(4) 0.7318(4) 0.077(4) Uani 1 1 d . . . K 1
H05G H -0.657794 -0.017167 0.701701 0.093 Uiso 1 1 calc R U . K 1
C05Y C -0.6524(5) -0.0344(5) 0.7690(5) 0.083(4) Uani 1 1 d . . . K 1
H05Y H -0.636973 -0.061855 0.764968 0.100 Uiso 1 1 calc R U . K 1
C06O C -0.6613(5) -0.0199(5) 0.8134(5) 0.093(5) Uani 1 1 d . . . K 1
H06O H -0.649543 -0.035124 0.840202 0.112 Uiso 1 1 calc R U . K 1
C075 C -0.6873(5) 0.0166(5) 0.8178(5) 0.095(5) Uani 1 1 d . . . K 1
H075 H -0.695102 0.025011 0.847925 0.114 Uiso 1 1 calc R U . K 1
C044 C -0.7023(5) 0.0412(4) 0.7801(4) 0.085(4) Uani 1 1 d . . . K 1
H044 H -0.719843 0.066949 0.783618 0.102 Uiso 1 1 calc R U . K 1
C04S C -0.6912(4) 0.0277(4) 0.7372(4) 0.072(4) Uani 1 1 d . . . K 1
C067 C -0.7021(5) 0.1909(4) 0.7316(4) 0.079(4) Uani 1 1 d . . . K 1
H067 H -0.683371 0.208618 0.750629 0.095 Uiso 1 1 calc R U . K 1
C05L C -0.7355(5) 0.2108(4) 0.7108(4) 0.084(5) Uani 1 1 d . . . K 1
H05L H -0.739329 0.243271 0.714084 0.100 Uiso 1 1 calc R U . K 1
C064 C -0.7641(5) 0.1853(4) 0.6849(4) 0.083(4) Uani 1 1 d . . . K 1
H064 H -0.788106 0.199484 0.671629 0.100 Uiso 1 1 calc R U . K 1
C04C C -0.7567(5) 0.1382(4) 0.6788(4) 0.081(4) Uani 1 1 d . . . K 1
H04C H -0.775499 0.120549 0.659763 0.098 Uiso 1 1 calc R U . K 1
C03Q C -0.7243(5) 0.1171(4) 0.6987(4) 0.070(4) Uani 1 1 d . . . K 1
C071 C -0.6956(5) 0.1428(4) 0.7245(4) 0.086(5) Uani 1 1 d . . . K 1
H071 H -0.671568 0.128412 0.737364 0.103 Uiso 1 1 calc R U . K 1
C05W C -0.6686(6) 0.0972(5) 0.6199(6) 0.106(6) Uani 1 1 d . . . K 1
H05W H -0.673202 0.125534 0.635545 0.128 Uiso 1 1 calc R U . K 1
C055 C -0.6841(5) 0.0558(4) 0.6378(4) 0.074(4) Uani 1 1 d . . . K 1
C039 C -0.6763(4) 0.0139(4) 0.6140(4) 0.068(3) Uani 1 1 d . . . K 1
H039 H -0.686942 -0.014545 0.624668 0.081 Uiso 1 1 calc R U . K 1
C05N C -0.6537(5) 0.0141(4) 0.5761(5) 0.081(4) Uani 1 1 d . . . K 1
H05N H -0.649529 -0.014215 0.560227 0.097 Uiso 1 1 calc R U . K 1
C07F C -0.6366(6) 0.0547(5) 0.5599(6) 0.106(6) Uani 1 1 d . . . K 1
H07F H -0.618280 0.053135 0.535798 0.128 Uiso 1 1 calc R U . K 1
P01U P -0.43325(9) 0.22295(13) 1.01696(13) 0.0733(9) Uani 1 1 d . U . L 1
C111 C -0.3996(4) 0.3561(4) 0.9892(5) 0.133(4) Uani 1 1 d G U . L 1
H111 H -0.389920 0.382228 1.006623 0.160 Uiso 1 1 calc R U . L 1
C1 C -0.4079(4) 0.3148(4) 1.0118(3) 0.118(4) Uani 1 1 d G U . L 1
H1 H -0.403914 0.312806 1.044665 0.141 Uiso 1 1 calc R U . L 1
C072 C -0.4221(3) 0.2766(3) 0.9862(4) 0.093(3) Uani 1 1 d G U . L 1
C07P C -0.4279(4) 0.2796(4) 0.9380(4) 0.112(4) Uani 1 1 d G U . L 1
H07P H -0.437579 0.253402 0.920581 0.134 Uiso 1 1 calc R U . L 1
C07Z C -0.4196(4) 0.3208(5) 0.9154(3) 0.129(4) Uani 1 1 d G U . L 1
H07Z H -0.423585 0.322824 0.882538 0.154 Uiso 1 1 calc R U . L 1
C07V C -0.4054(4) 0.3591(4) 0.9410(5) 0.133(4) Uani 1 1 d G U . L 1
H07V H -0.399756 0.387237 0.925559 0.160 Uiso 1 1 calc R U . L 1
C05Q C -0.3882(2) 0.1931(4) 1.0376(4) 0.103(3) Uani 1 1 d G U . L 1
C05S C -0.3892(2) 0.1451(4) 1.0422(4) 0.108(3) Uani 1 1 d G U . L 1
H05S H -0.412888 0.128293 1.031882 0.129 Uiso 1 1 calc R U . L 1
C06C C -0.3556(3) 0.1216(3) 1.0621(4) 0.110(3) Uani 1 1 d G U . L 1
H06C H -0.356247 0.088837 1.065243 0.132 Uiso 1 1 calc R U . L 1
C06Q C -0.3209(3) 0.1462(4) 1.0772(4) 0.110(3) Uani 1 1 d G U . L 1
H06Q H -0.297923 0.130164 1.090774 0.132 Uiso 1 1 calc R U . L 1
C07A C -0.3199(2) 0.1942(4) 1.0726(4) 0.109(3) Uani 1 1 d G U . L 1
H07A H -0.296240 0.210949 1.082943 0.131 Uiso 1 1 calc R U . L 1
C07Q C -0.3536(3) 0.2176(3) 1.0528(4) 0.106(3) Uani 1 1 d G U . L 1
H07Q H -0.352881 0.250406 1.049581 0.128 Uiso 1 1 calc R U . L 1
C06K C -0.5218(4) 0.1366(5) 0.9660(5) 0.082(4) Uani 1 1 d . . . L 1
H06K H -0.548438 0.127960 0.973473 0.098 Uiso 1 1 calc R U . L 1
C06H C -0.5045(5) 0.1161(6) 0.9297(6) 0.106(5) Uani 1 1 d . . . L 1
H06H H -0.518504 0.092113 0.912712 0.127 Uiso 1 1 calc R U . L 1
C065 C -0.4653(6) 0.1305(6) 0.9172(6) 0.111(6) Uani 1 1 d . . . L 1
H065 H -0.453293 0.116680 0.891411 0.134 Uiso 1 1 calc R U . L 1
C06Y C -0.4447(5) 0.1649(5) 0.9431(5) 0.094(5) Uani 1 1 d . . . L 1
H06Y H -0.418632 0.174887 0.934815 0.113 Uiso 1 1 calc R U . L 1
C05K C -0.4622(4) 0.1844(4) 0.9806(4) 0.068(3) Uani 1 1 d . . . L 1
C037 C -0.5006(4) 0.1707(4) 0.9924(5) 0.077(4) Uani 1 1 d . . . L 1
H037 H -0.512446 0.184271 1.018448 0.093 Uiso 1 1 calc R U . L 1
C06V C -0.4571(4) 0.2129(6) 1.1058(5) 0.085(4) Uani 1 1 d . . . L 1
H06V H -0.439097 0.187122 1.107784 0.103 Uiso 1 1 calc R U . L 1
C06G C -0.4804(5) 0.2249(7) 1.1441(6) 0.104(5) Uani 1 1 d . . . L 1
H06G H -0.477652 0.206809 1.171705 0.124 Uiso 1 1 calc R U . L 1
C06L C -0.5061(5) 0.2611(6) 1.1424(6) 0.099(5) Uani 1 1 d . . . L 1
H06L H -0.519760 0.269549 1.169206 0.119 Uiso 1 1 calc R U . L 1
C07N C -0.5128(4) 0.2868(7) 1.1003(7) 0.107(5) Uani 1 1 d . . . L 1
H07N H -0.532515 0.310909 1.098207 0.129 Uiso 1 1 calc R U . L 1
C073 C -0.4893(5) 0.2760(6) 1.0604(6) 0.098(5) Uani 1 1 d . . . L 1
H073 H -0.492691 0.292870 1.032078 0.118 Uiso 1 1 calc R U . L 1
C059 C -0.4611(4) 0.2391(5) 1.0658(5) 0.077(4) Uani 1 1 d . . . L 1
Br2 Br -0.47148(17) 0.3014(2) 0.7876(2) 0.179(2) Uani 0.5 1 d . U P A 2
C10 C -0.5899(5) 0.1403(5) 0.7229(3) 0.074(7) Uani 0.5 1 d G . P A 1
C7 C -0.5893(5) 0.0938(4) 0.7359(4) 0.070(7) Uani 0.5 1 d G . P A 1
C8 C -0.5980(5) 0.0812(3) 0.7808(5) 0.060(6) Uani 0.5 1 d G . P A 1
C12 C -0.6074(5) 0.1151(4) 0.8128(3) 0.059(5) Uani 0.5 1 d G . P A 1
C5 C -0.6081(4) 0.1616(4) 0.7998(4) 0.045(4) Uani 0.5 1 d G . P A 1
C15 C -0.5993(4) 0.1742(3) 0.7549(4) 0.047(4) Uani 0.5 1 d G . P A 1
C35 C -0.5117(5) 0.2597(7) 0.8031(8) 0.127(4) Uani 0.5 1 d G U P A 2
C26 C -0.5027(4) 0.2166(8) 0.8227(7) 0.106(5) Uani 0.5 1 d G U P A 2
C2 C -0.5339(6) 0.1867(6) 0.8334(7) 0.094(5) Uani 0.5 1 d G U P A 2
C13 C -0.5742(5) 0.1999(6) 0.8244(6) 0.078(4) Uani 0.5 1 d G U P A 2
C27 C -0.5833(4) 0.2431(7) 0.8048(7) 0.087(4) Uani 0.5 1 d G U P A 2
C34 C -0.5520(7) 0.2730(6) 0.7941(7) 0.107(5) Uani 0.5 1 d G U P A 2
Cl5 Cl -0.5657(6) 0.3345(8) 1.1896(7) 0.151(7) Uani 0.29 1 d . . P . .
Cl10 Cl -0.63958(6) 0.24021(7) 1.33052(5) 0.0855(5) Uani 0.29 1 d . . P G .
Cl13 Cl -0.95212(9) 0.01524(9) 0.87792(8) 0.1341(10) Uani 0.22 1 d . . P I .
Cl15 Cl -0.7034(8) -0.0395(7) 0.9143(8) 0.140(6) Uani 0.24 1 d . U P . .
Cl1N Cl -0.85798(14) -0.07381(8) 0.82909(10) 0.1899(18) Uani 0.24 1 d . . P C .
Cl0X Cl -0.55535(6) 0.10449(6) 1.31323(5) 0.0837(5) Uani 0.25 1 d . . P F .
Cl1 Cl -0.5955(7) 0.2279(5) 0.7393(7) 0.062(5) Uani 0.14 1 d . . P A 1
Cl2 Cl -0.57974(11) 0.04983(11) 0.69080(11) 0.0756(8) Uani 0.14 1 d . . P . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt01 Ag03 2.7442(6) 7_357 ?
Pt01 Ag03 2.7443(6) . ?
Pt01 Ag04 2.7391(6) 7_357 ?
Pt01 Ag04 2.7391(6) . ?
Pt01 Ag06 2.7601(6) 7_357 ?
Pt01 Ag06 2.7601(6) . ?
Pt01 Ag08 2.7308(6) 7_357 ?
Pt01 Ag08 2.7309(6) . ?
Pt01 Ag0B 2.7610(6) . ?
Pt01 Ag0B 2.7610(6) 7_357 ?
Pt01 Ag0E 2.7484(7) 7_357 ?
Pt01 Ag0E 2.7485(7) . ?
Ag03 Ag04 2.8392(9) . ?
Ag03 Ag06 2.8948(9) 7_357 ?
Ag03 Ag08 2.8907(9) . ?
Ag03 Ag0B 2.9228(9) . ?
Ag03 Ag0E 2.9127(9) . ?
Ag03 Ag0M 3.0480(9) . ?
Ag03 Ag0O 3.1843(11) . ?
Ag03 S1D 2.490(2) . ?
Ag04 Ag06 2.8941(9) 7_357 ?
Ag04 Ag08 2.8650(9) 7_357 ?
Ag04 Ag0B 2.9096(9) 7_357 ?
Ag04 Ag0E 2.9280(9) . ?
Ag04 Ag0O 3.0217(11) . ?
Ag04 S1H 2.444(2) . ?
Ag06 Ag08 2.9244(9) . ?
Ag06 Ag0B 2.8860(9) 7_357 ?
Ag06 Ag0E 2.8351(9) . ?
Ag06 Ag0H 3.1346(10) . ?
Ag06 S1G 2.459(3) . ?
Ag08 Ag0B 2.8487(10) . ?
Ag08 Ag0E 2.9040(9) . ?
Ag08 Ag0G 3.0840(10) . ?
Ag08 Ag0P 3.3612(10) . ?
Ag08 S1B 2.469(2) . ?
Ag0B Ag0E 2.8781(9) 7_357 ?
Ag0B Ag0P 3.0635(10) . ?
Ag0B S1M 2.468(2) . ?
Ag0E Ag0J 3.0997(9) . ?
Ag0E S1E 2.467(2) . ?
Ag0G Ag0H 3.0700(10) . ?
Ag0G S1A 2.542(2) . ?
Ag0G S1B 2.499(3) . ?
Ag0G S1K 2.438(3) . ?
Ag0H S1E 2.612(2) . ?
Ag0H S1G 2.465(3) . ?
Ag0H S1K 2.489(3) . ?
Ag0J Ag0O 2.9840(11) . ?
Ag0J S01X 2.486(5) . ?
Ag0J S1A 2.542(3) . ?
Ag0J S1E 2.539(2) . ?
Ag0J S3 2.395(6) . ?
Ag0M Ag0P 3.0052(12) . ?
Ag0M S1A 2.557(3) . ?
Ag0M S1D 2.488(2) . ?
Ag0M S1Q 2.445(3) . ?
Ag0O S01X 2.411(5) . ?
Ag0O S1D 2.579(2) . ?
Ag0O S1H 2.482(3) . ?
Ag0O S3 2.686(6) . ?
Ag0P S1B 2.605(3) . ?
Ag0P S1M 2.459(3) . ?
Ag0P S1Q 2.488(4) . ?
Br1 C7 1.854(9) . ?
Br0S C026 1.924(10) . ?
Br1N C06J 1.873(7) . ?
Br0T C02T 1.924(10) . ?
Br0V C03I 1.880(11) . ?
Br0X C043 1.885(10) . ?
Br10 C03G 1.890(12) . ?
Br11 C04J 1.928(11) . ?
Br13 C04F 1.874(12) . ?
Br15 C05P 1.909(13) . ?
S01X C5 1.806(10) . ?
S1A C02A 1.769(9) . ?
S1B C024 1.768(10) . ?
S1D C029 1.807(10) . ?
S1E C02Q 1.789(10) . ?
S1G C02B 1.754(10) . ?
S1H C02X 1.756(13) . ?
S1K C02F 1.756(10) . ?
S1M C02W 1.783(11) . ?
S1Q C042 1.795(7) . ?
S3 C13 1.826(14) . ?
Cl07 C03R 1.549(18) . ?
Cl03 C046 1.559(9) . ?
C026 C02C 1.322(14) . ?
C026 C02Y 1.376(15) . ?
C029 C02J 1.349(13) . ?
C029 C04B 1.384(14) . ?
C02A C031 1.384(13) . ?
C02A C03H 1.403(13) . ?
C02C H02C 0.9500 . ?
C02C C03H 1.381(14) . ?
C02J H02J 0.9500 . ?
C02J C02Z 1.412(15) . ?
C02W C03A 1.402(14) . ?
C02W C03R 1.386(14) . ?
C02X C035 1.409(18) . ?
C02X C05B 1.443(16) . ?
C035 H035 0.9500 . ?
C035 C05D 1.390(19) . ?
C05D H05D 0.9500 . ?
C05D C05P 1.42(2) . ?
C05P C06Z 1.33(2) . ?
C06Z H06Z 0.9500 . ?
C06Z C05B 1.35(2) . ?
C05B H05B 0.9500 . ?
C02Y H02Y 0.9500 . ?
C02Y C031 1.370(15) . ?
C02Z H02Z 0.9500 . ?
C02Z C03I 1.421(16) . ?
C030 H030 0.9500 . ?
C030 C02H 1.398(14) . ?
C030 C02T 1.377(15) . ?
C02H H02H 0.9500 . ?
C02H C024 1.421(14) . ?
C024 C03K 1.396(14) . ?
C03K H03K 0.9500 . ?
C03K C04P 1.337(15) . ?
C04P H04P 0.9500 . ?
C04P C02T 1.370(16) . ?
C031 H031 0.9500 . ?
C033 C03I 1.397(16) . ?
C033 C04B 1.397(16) . ?
C034 H034 0.9500 . ?
C034 C02L 1.328(15) . ?
C034 C043 1.393(16) . ?
C02L H02L 0.9500 . ?
C02L C02F 1.398(13) . ?
C02F C046 1.471(14) . ?
C046 C057 1.419(16) . ?
C057 C043 1.384(16) . ?
C03A H03A 0.9500 . ?
C03A C03V 1.417(15) . ?
C03H H03H 0.9500 . ?
C03P H03P 0.9500 . ?
C03P C02Q 1.375(15) . ?
C03P C04I 1.384(16) . ?
C02Q C05V 1.414(15) . ?
C05V H05V 0.9500 . ?
C05V C05Z 1.355(17) . ?
C05Z H05Z 0.9500 . ?
C05Z C04J 1.341(19) . ?
C04J C04I 1.355(18) . ?
C04I H04I 0.9500 . ?
C03R C04O 1.384(19) . ?
C070 C042 1.3900 . ?
C070 C05M 1.3900 . ?
C070 Cl15 1.65(3) . ?
C042 C03T 1.3900 . ?
C03T H03T 0.9500 . ?
C03T C05I 1.3900 . ?
C05I H05I 0.9500 . ?
C05I C06J 1.3900 . ?
C06J C05M 1.3900 . ?
C05M H05M 0.9500 . ?
C03V H03V 0.9500 . ?
C03V C04F 1.400(17) . ?
C04F C04O 1.34(2) . ?
C04Q H04Q 0.9500 . ?
C04Q C02U 1.390(14) . ?
C04Q C03G 1.376(18) . ?
C02U H02U 0.9500 . ?
C02U C02B 1.386(15) . ?
C02B C03U 1.401(14) . ?
C03U C052 1.369(16) . ?
C03U Cl5 1.76(2) . ?
C052 C03G 1.415(19) . ?
P01P C04E 1.794(15) . ?
P01P C04S 1.833(12) . ?
P01P C03Q 1.810(10) . ?
P01P C055 1.756(14) . ?
C38 H38 0.9500 . ?
C38 C05W 1.42(2) . ?
C38 C07F 1.41(2) . ?
C058 H058 0.9500 . ?
C058 C04E 1.36(2) . ?
C058 C06W 1.39(2) . ?
C04E C049 1.381(18) . ?
C049 H049 0.9500 . ?
C049 C079 1.40(2) . ?
C079 H079 0.9500 . ?
C079 C07S 1.31(2) . ?
C07S H07S 0.9500 . ?
C07S C06W 1.37(2) . ?
C06W H06W 0.9500 . ?
C05G H05G 0.9500 . ?
C05G C05Y 1.346(17) . ?
C05G C04S 1.367(16) . ?
C05Y H05Y 0.9500 . ?
C05Y C06O 1.394(17) . ?
C06O H06O 0.9500 . ?
C06O C075 1.366(19) . ?
C075 H075 0.9500 . ?
C075 C044 1.363(18) . ?
C044 H044 0.9500 . ?
C044 C04S 1.367(16) . ?
C067 H067 0.9500 . ?
C067 C05L 1.346(19) . ?
C067 C071 1.417(15) . ?
C05L H05L 0.9500 . ?
C05L C064 1.38(2) . ?
C064 H064 0.9500 . ?
C064 C04C 1.393(16) . ?
C04C H04C 0.9500 . ?
C04C C03Q 1.328(18) . ?
C03Q C071 1.380(18) . ?
C071 H071 0.9500 . ?
C05W H05W 0.9500 . ?
C05W C055 1.408(18) . ?
C055 C039 1.421(14) . ?
C039 H039 0.9500 . ?
C039 C05N 1.355(17) . ?
C05N H05N 0.9500 . ?
C05N C07F 1.390(18) . ?
C07F H07F 0.9500 . ?
P01U C072 1.830(9) . ?
P01U C05Q 1.785(8) . ?
P01U C05K 1.765(13) . ?
P01U C059 1.788(13) . ?
C111 H111 0.9500 . ?
C111 C1 1.3900 . ?
C111 C07V 1.3900 . ?
C1 H1 0.9500 . ?
C1 C072 1.3900 . ?
C072 C07P 1.3900 . ?
C07P H07P 0.9500 . ?
C07P C07Z 1.3900 . ?
C07Z H07Z 0.9500 . ?
C07Z C07V 1.3900 . ?
C07V H07V 0.9500 . ?
C05Q C05S 1.3900 . ?
C05Q C07Q 1.3900 . ?
C05S H05S 0.9500 . ?
C05S C06C 1.3900 . ?
C06C H06C 0.9500 . ?
C06C C06Q 1.3900 . ?
C06Q H06Q 0.9500 . ?
C06Q C07A 1.3900 . ?
C07A H07A 0.9500 . ?
C07A C07Q 1.3900 . ?
C07Q H07Q 0.9500 . ?
C06K H06K 0.9500 . ?
C06K C06H 1.36(2) . ?
C06K C037 1.402(18) . ?
C06H H06H 0.9500 . ?
C06H C065 1.42(2) . ?
C065 H065 0.9500 . ?
C065 C06Y 1.39(2) . ?
C06Y H06Y 0.9500 . ?
C06Y C05K 1.376(18) . ?
C05K C037 1.386(18) . ?
C037 H037 0.9500 . ?
C06V H06V 0.9500 . ?
C06V C06G 1.42(2) . ?
C06V C059 1.38(2) . ?
C06G H06G 0.9500 . ?
C06G C06L 1.34(2) . ?
C06L H06L 0.9500 . ?
C06L C07N 1.43(2) . ?
C07N H07N 0.9500 . ?
C07N C073 1.46(2) . ?
C073 H073 0.9500 . ?
C073 C059 1.41(2) . ?
Br2 Br2 2.776(13) 2_456 ?
Br2 C35 1.865(14) . ?
C10 C7 1.3900 . ?
C10 C15 1.3900 . ?
C7 C8 1.3900 . ?
C8 C12 1.3900 . ?
C12 C5 1.3900 . ?
C5 C15 1.3900 . ?
C15 Cl1 1.619(17) . ?
C35 C26 1.3900 . ?
C35 C34 1.3900 . ?
C26 C2 1.3900 . ?
C2 C13 1.3900 . ?
C13 C27 1.3900 . ?
C27 C34 1.3900 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Ag03 Pt01 Ag03 180.0 7_357 . ?
Ag03 Pt01 Ag06 116.539(19) . . ?
Ag03 Pt01 Ag06 116.543(19) 7_357 7_357 ?
Ag03 Pt01 Ag06 63.459(19) 7_357 . ?
Ag03 Pt01 Ag06 63.459(19) . 7_357 ?
Ag03 Pt01 Ag0B 64.130(19) 7_357 7_357 ?
Ag03 Pt01 Ag0B 64.134(19) . . ?
Ag03 Pt01 Ag0B 115.868(19) 7_357 . ?
Ag03 Pt01 Ag0B 115.868(19) . 7_357 ?
Ag03 Pt01 Ag0E 115.951(19) . 7_357 ?
Ag03 Pt01 Ag0E 64.052(19) 7_357 7_357 ?
Ag03 Pt01 Ag0E 115.95(2) 7_357 . ?
Ag03 Pt01 Ag0E 64.048(19) . . ?
Ag04 Pt01 Ag03 117.633(18) 7_357 . ?
Ag04 Pt01 Ag03 117.631(18) . 7_357 ?
Ag04 Pt01 Ag03 62.368(18) . . ?
Ag04 Pt01 Ag03 62.368(18) 7_357 7_357 ?
Ag04 Pt01 Ag04 180.0 7_357 . ?
Ag04 Pt01 Ag06 116.49(2) 7_357 7_357 ?
Ag04 Pt01 Ag06 63.51(2) 7_357 . ?
Ag04 Pt01 Ag06 116.49(2) . . ?
Ag04 Pt01 Ag06 63.51(2) . 7_357 ?
Ag04 Pt01 Ag0B 116.126(19) . . ?
Ag04 Pt01 Ag0B 63.875(19) . 7_357 ?
Ag04 Pt01 Ag0B 63.875(19) 7_357 . ?
Ag04 Pt01 Ag0B 116.124(19) 7_357 7_357 ?
Ag04 Pt01 Ag0E 115.51(2) 7_357 . ?
Ag04 Pt01 Ag0E 64.49(2) 7_357 7_357 ?
Ag04 Pt01 Ag0E 64.49(2) . . ?
Ag04 Pt01 Ag0E 115.51(2) . 7_357 ?
Ag06 Pt01 Ag06 180.0 . 7_357 ?
Ag06 Pt01 Ag0B 63.030(19) 7_357 . ?
Ag06 Pt01 Ag0B 63.029(19) . 7_357 ?
Ag06 Pt01 Ag0B 116.970(19) . . ?
Ag06 Pt01 Ag0B 116.970(19) 7_357 7_357 ?
Ag08 Pt01 Ag03 63.734(18) 7_357 7_357 ?
Ag08 Pt01 Ag03 63.736(18) . . ?
Ag08 Pt01 Ag03 116.264(18) . 7_357 ?
Ag08 Pt01 Ag03 116.266(18) 7_357 . ?
Ag08 Pt01 Ag04 116.832(19) . . ?
Ag08 Pt01 Ag04 63.171(19) 7_357 . ?
Ag08 Pt01 Ag04 116.829(19) 7_357 7_357 ?
Ag08 Pt01 Ag04 63.169(19) . 7_357 ?
Ag08 Pt01 Ag06 115.641(19) . 7_357 ?
Ag08 Pt01 Ag06 115.642(19) 7_357 . ?
Ag08 Pt01 Ag06 64.359(19) 7_357 7_357 ?
Ag08 Pt01 Ag06 64.358(19) . . ?
Ag08 Pt01 Ag08 180.0 7_357 . ?
Ag08 Pt01 Ag0B 62.49(2) 7_357 7_357 ?
Ag08 Pt01 Ag0B 62.49(2) . . ?
Ag08 Pt01 Ag0B 117.51(2) . 7_357 ?
Ag08 Pt01 Ag0B 117.51(2) 7_357 . ?
Ag08 Pt01 Ag0E 64.008(19) . . ?
Ag08 Pt01 Ag0E 115.992(19) . 7_357 ?
Ag08 Pt01 Ag0E 115.994(19) 7_357 . ?
Ag08 Pt01 Ag0E 64.006(19) 7_357 7_357 ?
Ag0B Pt01 Ag0B 180.0 . 7_357 ?
Ag0E Pt01 Ag06 61.951(19) 7_357 7_357 ?
Ag0E Pt01 Ag06 118.052(19) 7_357 . ?
Ag0E Pt01 Ag06 118.048(19) . 7_357 ?
Ag0E Pt01 Ag06 61.949(19) . . ?
Ag0E Pt01 Ag0B 117.014(19) 7_357 7_357 ?
Ag0E Pt01 Ag0B 117.015(19) . . ?
Ag0E Pt01 Ag0B 62.987(19) . 7_357 ?
Ag0E Pt01 Ag0B 62.985(19) 7_357 . ?
Ag0E Pt01 Ag0E 180.0 7_357 . ?
Pt01 Ag03 Ag04 58.726(18) . . ?
Pt01 Ag03 Ag06 58.537(18) . 7_357 ?
Pt01 Ag03 Ag08 57.906(17) . . ?
Pt01 Ag03 Ag0B 58.211(17) . . ?
Pt01 Ag03 Ag0E 58.047(17) . . ?
Pt01 Ag03 Ag0M 138.93(3) . . ?
Pt01 Ag03 Ag0O 115.28(2) . . ?
Ag04 Ag03 Ag06 60.62(2) . 7_357 ?
Ag04 Ag03 Ag08 108.82(3) . . ?
Ag04 Ag03 Ag0B 108.19(3) . . ?
Ag04 Ag03 Ag0E 61.19(2) . . ?
Ag04 Ag03 Ag0M 153.89(3) . . ?
Ag04 Ag03 Ag0O 59.89(2) . . ?
Ag06 Ag03 Ag0B 59.48(2) 7_357 . ?
Ag06 Ag03 Ag0E 108.83(3) 7_357 . ?
Ag06 Ag03 Ag0M 140.92(3) 7_357 . ?
Ag06 Ag03 Ag0O 105.33(3) 7_357 . ?
Ag08 Ag03 Ag06 106.89(3) . 7_357 ?
Ag08 Ag03 Ag0B 58.68(2) . . ?
Ag08 Ag03 Ag0E 60.05(2) . . ?
Ag08 Ag03 Ag0M 81.40(2) . . ?
Ag08 Ag03 Ag0O 131.88(3) . . ?
Ag0B Ag03 Ag0M 97.67(3) . . ?
Ag0B Ag03 Ag0O 164.81(3) . . ?
Ag0E Ag03 Ag0B 107.23(3) . . ?
Ag0E Ag03 Ag0M 108.20(3) . . ?
Ag0E Ag03 Ag0O 76.23(2) . . ?
Ag0M Ag03 Ag0O 95.13(3) . . ?
S1D Ag03 Pt01 167.22(6) . . ?
S1D Ag03 Ag04 108.58(6) . . ?
S1D Ag03 Ag06 118.33(6) . 7_357 ?
S1D Ag03 Ag08 131.22(6) . . ?
S1D Ag03 Ag0B 132.67(6) . . ?
S1D Ag03 Ag0E 116.17(6) . . ?
S1D Ag03 Ag0M 52.21(6) . . ?
S1D Ag03 Ag0O 52.35(6) . . ?
Pt01 Ag04 Ag03 58.906(17) . . ?
Pt01 Ag04 Ag06 58.600(18) . 7_357 ?
Pt01 Ag04 Ag08 58.274(17) . 7_357 ?
Pt01 Ag04 Ag0B 58.429(17) . 7_357 ?
Pt01 Ag04 Ag0E 57.910(18) . . ?
Pt01 Ag04 Ag0O 120.90(3) . . ?
Ag03 Ag04 Ag06 60.64(2) . 7_357 ?
Ag03 Ag04 Ag08 109.21(3) . 7_357 ?
Ag03 Ag04 Ag0B 108.49(3) . 7_357 ?
Ag03 Ag04 Ag0E 60.65(2) . . ?
Ag03 Ag04 Ag0O 65.73(2) . . ?
Ag06 Ag04 Ag0B 108.39(3) 7_357 7_357 ?
Ag06 Ag04 Ag0E 108.43(3) 7_357 . ?
Ag06 Ag04 Ag0O 109.67(3) 7_357 . ?
Ag08 Ag04 Ag06 61.03(2) 7_357 7_357 ?
Ag08 Ag04 Ag0B 59.11(2) 7_357 7_357 ?
Ag08 Ag04 Ag0E 106.66(3) 7_357 . ?
Ag08 Ag04 Ag0O 170.20(3) 7_357 . ?
Ag0B Ag04 Ag0E 59.08(2) 7_357 . ?
Ag0B Ag04 Ag0O 129.88(3) 7_357 . ?
Ag0E Ag04 Ag0O 78.60(3) . . ?
S1H Ag04 Pt01 169.05(7) . . ?
S1H Ag04 Ag03 111.35(6) . . ?
S1H Ag04 Ag06 113.24(8) . 7_357 ?
S1H Ag04 Ag08 126.13(7) . 7_357 ?
S1H Ag04 Ag0B 132.40(7) . 7_357 ?
S1H Ag04 Ag0E 123.57(8) . . ?
S1H Ag04 Ag0O 52.73(6) . . ?
Pt01 Ag06 Ag03 58.002(18) . 7_357 ?
Pt01 Ag06 Ag04 57.892(18) . 7_357 ?
Pt01 Ag06 Ag08 57.336(17) . . ?
Pt01 Ag06 Ag0B 58.501(18) . 7_357 ?
Pt01 Ag06 Ag0E 58.825(18) . . ?
Pt01 Ag06 Ag0H 125.53(3) . . ?
Ag03 Ag06 Ag08 106.08(3) 7_357 . ?
Ag03 Ag06 Ag0H 170.64(3) 7_357 . ?
Ag04 Ag06 Ag03 58.74(2) 7_357 7_357 ?
Ag04 Ag06 Ag08 58.99(2) 7_357 . ?
Ag04 Ag06 Ag0H 130.59(3) 7_357 . ?
Ag08 Ag06 Ag0H 81.88(2) . . ?
Ag0B Ag06 Ag03 60.74(2) 7_357 7_357 ?
Ag0B Ag06 Ag04 107.71(3) 7_357 7_357 ?
Ag0B Ag06 Ag08 107.82(3) 7_357 . ?
Ag0B Ag06 Ag0H 112.54(3) 7_357 . ?
Ag0E Ag06 Ag03 108.72(3) . 7_357 ?
Ag0E Ag06 Ag04 108.20(3) . 7_357 ?
Ag0E Ag06 Ag08 60.53(2) . . ?
Ag0E Ag06 Ag0B 60.40(2) . 7_357 ?
Ag0E Ag06 Ag0H 70.54(2) . . ?
S1G Ag06 Pt01 166.63(6) . . ?
S1G Ag06 Ag03 123.66(6) . 7_357 ?
S1G Ag06 Ag04 135.33(6) . 7_357 ?
S1G Ag06 Ag08 127.74(6) . . ?
S1G Ag06 Ag0B 109.57(6) . 7_357 ?
S1G Ag06 Ag0E 111.14(6) . . ?
S1G Ag06 Ag0H 50.55(6) . . ?
Pt01 Ag08 Ag03 58.358(17) . . ?
Pt01 Ag08 Ag04 58.556(17) . 7_357 ?
Pt01 Ag08 Ag06 58.306(17) . . ?
Pt01 Ag08 Ag0B 59.274(18) . . ?
Pt01 Ag08 Ag0E 58.292(17) . . ?
Pt01 Ag08 Ag0G 143.67(3) . . ?
Pt01 Ag08 Ag0P 115.65(3) . . ?
Ag03 Ag08 Ag06 107.24(3) . . ?
Ag03 Ag08 Ag0E 60.35(2) . . ?
Ag03 Ag08 Ag0G 109.73(3) . . ?
Ag03 Ag08 Ag0P 79.01(2) . . ?
Ag04 Ag08 Ag03 109.18(3) 7_357 . ?
Ag04 Ag08 Ag06 59.98(2) 7_357 . ?
Ag04 Ag08 Ag0E 107.13(3) 7_357 . ?
Ag04 Ag08 Ag0G 140.29(3) 7_357 . ?
Ag04 Ag08 Ag0P 102.25(3) 7_357 . ?
Ag06 Ag08 Ag0G 100.68(3) . . ?
Ag06 Ag08 Ag0P 162.16(3) . . ?
Ag0B Ag08 Ag03 61.22(2) . . ?
Ag0B Ag08 Ag04 61.23(2) . 7_357 ?
Ag0B Ag08 Ag06 109.23(3) . . ?
Ag0B Ag08 Ag0E 109.50(3) . . ?
Ag0B Ag08 Ag0G 150.09(3) . . ?
Ag0B Ag08 Ag0P 58.42(2) . . ?
Ag0E Ag08 Ag06 58.21(2) . . ?
Ag0E Ag08 Ag0G 85.65(3) . . ?
Ag0E Ag08 Ag0P 135.61(3) . . ?
Ag0G Ag08 Ag0P 92.52(3) . . ?
S1B Ag08 Pt01 163.82(6) . . ?
S1B Ag08 Ag03 118.67(6) . . ?
S1B Ag08 Ag04 112.89(6) . 7_357 ?
S1B Ag08 Ag06 131.94(6) . . ?
S1B Ag08 Ag0B 104.82(6) . . ?
S1B Ag08 Ag0E 136.24(6) . . ?
S1B Ag08 Ag0G 52.07(6) . . ?
S1B Ag08 Ag0P 50.27(6) . . ?
Pt01 Ag0B Ag03 57.655(17) . . ?
Pt01 Ag0B Ag04 57.695(17) . 7_357 ?
Pt01 Ag0B Ag06 58.470(17) . 7_357 ?
Pt01 Ag0B Ag08 58.236(18) . . ?
Pt01 Ag0B Ag0E 58.293(18) . 7_357 ?
Pt01 Ag0B Ag0P 124.96(3) . . ?
Ag03 Ag0B Ag0P 83.66(3) . . ?
Ag04 Ag0B Ag03 107.09(3) 7_357 . ?
Ag04 Ag0B Ag0P 108.79(3) 7_357 . ?
Ag06 Ag0B Ag03 59.78(2) 7_357 . ?
Ag06 Ag0B Ag04 107.57(3) 7_357 7_357 ?
Ag06 Ag0B Ag0P 134.36(3) 7_357 . ?
Ag08 Ag0B Ag03 60.10(2) . . ?
Ag08 Ag0B Ag04 59.66(2) . 7_357 ?
Ag08 Ag0B Ag06 108.27(3) . 7_357 ?
Ag08 Ag0B Ag0E 108.46(3) . 7_357 ?
Ag08 Ag0B Ag0P 69.18(2) . . ?
Ag0E Ag0B Ag03 106.79(3) 7_357 . ?
Ag0E Ag0B Ag04 60.78(2) 7_357 7_357 ?
Ag0E Ag0B Ag06 58.92(2) 7_357 7_357 ?
Ag0E Ag0B Ag0P 166.71(3) 7_357 . ?
S1M Ag0B Pt01 168.35(7) . . ?
S1M Ag0B Ag03 127.69(8) . . ?
S1M Ag0B Ag04 111.52(7) . 7_357 ?
S1M Ag0B Ag06 132.84(7) . 7_357 ?
S1M Ag0B Ag08 113.68(7) . . ?
S1M Ag0B Ag0E 122.33(8) . 7_357 ?
S1M Ag0B Ag0P 51.43(8) . . ?
Pt01 Ag0E Ag03 57.905(18) . . ?
Pt01 Ag0E Ag04 57.597(18) . . ?
Pt01 Ag0E Ag06 59.226(19) . . ?
Pt01 Ag0E Ag08 57.700(18) . . ?
Pt01 Ag0E Ag0B 58.719(18) . 7_357 ?
Pt01 Ag0E Ag0J 140.92(3) . . ?
Ag03 Ag0E Ag04 58.17(2) . . ?
Ag03 Ag0E Ag0J 83.07(3) . . ?
Ag04 Ag0E Ag0J 101.88(3) . . ?
Ag06 Ag0E Ag03 109.07(3) . . ?
Ag06 Ag0E Ag04 108.45(3) . . ?
Ag06 Ag0E Ag08 61.25(2) . . ?
Ag06 Ag0E Ag0B 60.68(2) . 7_357 ?
Ag06 Ag0E Ag0J 149.34(3) . . ?
Ag08 Ag0E Ag03 59.60(2) . . ?
Ag08 Ag0E Ag04 106.07(3) . . ?
Ag08 Ag0E Ag0J 106.27(3) . . ?
Ag0B Ag0E Ag03 107.34(3) 7_357 . ?
Ag0B Ag0E Ag04 60.14(2) 7_357 . ?
Ag0B Ag0E Ag08 108.59(3) 7_357 . ?
Ag0B Ag0E Ag0J 144.07(3) 7_357 . ?
S1E Ag0E Pt01 163.42(6) . . ?
S1E Ag0E Ag03 133.39(6) . . ?
S1E Ag0E Ag04 136.66(6) . . ?
S1E Ag0E Ag06 104.34(6) . . ?
S1E Ag0E Ag08 114.31(6) . . ?
S1E Ag0E Ag0B 117.15(6) . 7_357 ?
S1E Ag0E Ag0J 52.79(6) . . ?
Ag0H Ag0G Ag08 80.43(2) . . ?
S1A Ag0G Ag08 87.71(6) . . ?
S1A Ag0G Ag0H 113.33(6) . . ?
S1B Ag0G Ag08 51.18(5) . . ?
S1B Ag0G Ag0H 119.88(6) . . ?
S1B Ag0G S1A 99.59(8) . . ?
S1K Ag0G Ag08 130.94(7) . . ?
S1K Ag0G Ag0H 52.21(6) . . ?
S1K Ag0G S1A 119.73(9) . . ?
S1K Ag0G S1B 140.10(8) . . ?
Ag0G Ag0H Ag06 96.43(3) . . ?
S1E Ag0H Ag06 93.28(6) . . ?
S1E Ag0H Ag0G 83.97(6) . . ?
S1G Ag0H Ag06 50.38(6) . . ?
S1G Ag0H Ag0G 137.74(7) . . ?
S1G Ag0H S1E 118.42(8) . . ?
S1G Ag0H S1K 141.36(9) . . ?
S1K Ag0H Ag06 142.86(7) . . ?
S1K Ag0H Ag0G 50.71(6) . . ?
S1K Ag0H S1E 98.81(8) . . ?
Ag0O Ag0J Ag0E 76.54(3) . . ?
S01X Ag0J Ag0E 108.37(11) . . ?
S01X Ag0J Ag0O 51.33(12) . . ?
S01X Ag0J S1A 149.31(13) . . ?
S01X Ag0J S1E 113.33(13) . . ?
S1A Ag0J Ag0E 89.47(6) . . ?
S1A Ag0J Ag0O 112.89(6) . . ?
S1E Ag0J Ag0E 50.71(6) . . ?
S1E Ag0J Ag0O 118.64(6) . . ?
S1E Ag0J S1A 97.33(8) . . ?
S3 Ag0J Ag0E 133.11(13) . . ?
S3 Ag0J Ag0O 58.69(14) . . ?
S3 Ag0J S1A 118.92(15) . . ?
S3 Ag0J S1E 142.21(16) . . ?
Ag0P Ag0M Ag03 82.56(3) . . ?
S1A Ag0M Ag03 89.95(6) . . ?
S1A Ag0M Ag0P 115.74(6) . . ?
S1D Ag0M Ag03 52.27(5) . . ?
S1D Ag0M Ag0P 124.32(6) . . ?
S1D Ag0M S1A 97.03(8) . . ?
S1Q Ag0M Ag03 133.98(9) . . ?
S1Q Ag0M Ag0P 53.13(9) . . ?
S1Q Ag0M S1A 118.09(10) . . ?
S1Q Ag0M S1D 142.45(10) . . ?
Ag04 Ag0O Ag03 54.37(2) . . ?
Ag0J Ag0O Ag03 80.52(3) . . ?
Ag0J Ag0O Ag04 102.43(3) . . ?
S01X Ag0O Ag03 133.51(13) . . ?
S01X Ag0O Ag04 122.83(12) . . ?
S01X Ag0O Ag0J 53.61(12) . . ?
S01X Ag0O S1D 122.88(13) . . ?
S01X Ag0O S1H 109.17(14) . . ?
S1D Ag0O Ag03 49.84(5) . . ?
S1D Ag0O Ag04 101.03(6) . . ?
S1D Ag0O Ag0J 84.88(6) . . ?
S1D Ag0O S3 94.16(14) . . ?
S1H Ag0O Ag03 100.16(7) . . ?
S1H Ag0O Ag04 51.59(6) . . ?
S1H Ag0O Ag0J 138.67(7) . . ?
S1H Ag0O S1D 127.16(10) . . ?
S1H Ag0O S3 134.58(14) . . ?
S3 Ag0O Ag03 122.97(12) . . ?
S3 Ag0O Ag04 146.96(13) . . ?
S3 Ag0O Ag0J 49.64(13) . . ?
Ag0B Ag0P Ag08 52.39(2) . . ?
Ag0M Ag0P Ag08 74.74(2) . . ?
Ag0M Ag0P Ag0B 95.60(3) . . ?
S1B Ag0P Ag08 46.79(5) . . ?
S1B Ag0P Ag0B 95.89(5) . . ?
S1B Ag0P Ag0M 83.83(6) . . ?
S1M Ag0P Ag08 98.73(6) . . ?
S1M Ag0P Ag0B 51.68(6) . . ?
S1M Ag0P Ag0M 134.83(7) . . ?
S1M Ag0P S1B 124.43(9) . . ?
S1M Ag0P S1Q 137.56(10) . . ?
S1Q Ag0P Ag08 119.61(8) . . ?
S1Q Ag0P Ag0B 143.31(8) . . ?
S1Q Ag0P Ag0M 51.81(7) . . ?
S1Q Ag0P S1B 96.43(10) . . ?
Ag0O S01X Ag0J 75.06(14) . . ?
C5 S01X Ag0J 109.7(4) . . ?
C5 S01X Ag0O 101.7(5) . . ?
Ag0G S1A Ag0J 111.66(9) . . ?
Ag0G S1A Ag0M 108.08(9) . . ?
Ag0J S1A Ag0M 110.22(9) . . ?
C02A S1A Ag0G 111.1(3) . . ?
C02A S1A Ag0J 110.9(3) . . ?
C02A S1A Ag0M 104.6(3) . . ?
Ag08 S1B Ag0G 76.75(7) . . ?
Ag08 S1B Ag0P 82.94(7) . . ?
Ag0G S1B Ag0P 131.88(10) . . ?
C024 S1B Ag08 104.0(3) . . ?
C024 S1B Ag0G 111.4(3) . . ?
C024 S1B Ag0P 115.7(3) . . ?
Ag03 S1D Ag0O 77.81(7) . . ?
Ag0M S1D Ag03 75.52(7) . . ?
Ag0M S1D Ag0O 130.45(10) . . ?
C029 S1D Ag03 104.9(3) . . ?
C029 S1D Ag0M 114.6(3) . . ?
C029 S1D Ag0O 112.2(3) . . ?
Ag0E S1E Ag0H 85.69(7) . . ?
Ag0E S1E Ag0J 76.50(7) . . ?
Ag0J S1E Ag0H 132.71(9) . . ?
C02Q S1E Ag0E 108.2(3) . . ?
C02Q S1E Ag0H 111.1(4) . . ?
C02Q S1E Ag0J 116.0(4) . . ?
Ag06 S1G Ag0H 79.07(7) . . ?
C02B S1G Ag06 110.0(4) . . ?
C02B S1G Ag0H 106.4(3) . . ?
Ag04 S1H Ag0O 75.68(7) . . ?
C02X S1H Ag04 107.6(4) . . ?
C02X S1H Ag0O 100.6(4) . . ?
Ag0G S1K Ag0H 77.07(8) . . ?
C02F S1K Ag0G 108.4(3) . . ?
C02F S1K Ag0H 109.7(3) . . ?
Ag0P S1M Ag0B 76.89(8) . . ?
C02W S1M Ag0B 110.8(3) . . ?
C02W S1M Ag0P 106.2(4) . . ?
Ag0M S1Q Ag0P 75.06(8) . . ?
C042 S1Q Ag0M 102.4(3) . . ?
C042 S1Q Ag0P 110.2(3) . . ?
Ag0J S3 Ag0O 71.67(14) . . ?
C13 S3 Ag0J 102.4(6) . . ?
C13 S3 Ag0O 115.8(6) . . ?
C02C C026 Br0S 120.2(8) . . ?
C02C C026 C02Y 120.7(9) . . ?
C02Y C026 Br0S 119.0(8) . . ?
C02J C029 S1D 120.1(8) . . ?
C02J C029 C04B 121.4(10) . . ?
C04B C029 S1D 118.3(7) . . ?
C031 C02A S1A 121.5(7) . . ?
C031 C02A C03H 116.7(9) . . ?
C03H C02A S1A 121.8(7) . . ?
C026 C02C H02C 119.6 . . ?
C026 C02C C03H 120.8(9) . . ?
C03H C02C H02C 119.6 . . ?
C029 C02J H02J 119.8 . . ?
C029 C02J C02Z 120.4(10) . . ?
C02Z C02J H02J 119.8 . . ?
C03A C02W S1M 120.5(7) . . ?
C03R C02W S1M 120.0(9) . . ?
C03R C02W C03A 119.3(10) . . ?
C035 C02X S1H 122.9(8) . . ?
C035 C02X C05B 119.3(12) . . ?
C05B C02X S1H 117.8(11) . . ?
C02X C035 H035 119.6 . . ?
C05D C035 C02X 120.9(13) . . ?
C05D C035 H035 119.6 . . ?
C035 C05D H05D 121.9 . . ?
C035 C05D C05P 116.2(15) . . ?
C05P C05D H05D 121.9 . . ?
C05D C05P Br15 117.3(14) . . ?
C06Z C05P Br15 119.1(13) . . ?
C06Z C05P C05D 123.1(14) . . ?
C05P C06Z H06Z 118.9 . . ?
C05P C06Z C05B 122.2(16) . . ?
C05B C06Z H06Z 118.9 . . ?
C02X C05B H05B 121.0 . . ?
C06Z C05B C02X 118.0(16) . . ?
C06Z C05B H05B 121.0 . . ?
C026 C02Y H02Y 120.2 . . ?
C031 C02Y C026 119.5(10) . . ?
C031 C02Y H02Y 120.2 . . ?
C02J C02Z H02Z 120.8 . . ?
C02J C02Z C03I 118.4(10) . . ?
C03I C02Z H02Z 120.8 . . ?
C02H C030 H030 120.3 . . ?
C02T C030 H030 120.3 . . ?
C02T C030 C02H 119.5(10) . . ?
C030 C02H H02H 120.9 . . ?
C030 C02H C024 118.2(10) . . ?
C024 C02H H02H 120.9 . . ?
C02H C024 S1B 119.0(8) . . ?
C03K C024 S1B 121.9(8) . . ?
C03K C024 C02H 119.1(9) . . ?
C024 C03K H03K 119.2 . . ?
C04P C03K C024 121.5(10) . . ?
C04P C03K H03K 119.2 . . ?
C03K C04P H04P 120.1 . . ?
C03K C04P C02T 119.7(11) . . ?
C02T C04P H04P 120.1 . . ?
C030 C02T Br0T 118.7(8) . . ?
C04P C02T Br0T 119.3(9) . . ?
C04P C02T C030 121.9(10) . . ?
C02A C031 H031 119.2 . . ?
C02Y C031 C02A 121.6(10) . . ?
C02Y C031 H031 119.2 . . ?
C04B C033 C03I 118.6(11) . . ?
C02L C034 H034 119.0 . . ?
C02L C034 C043 122.1(11) . . ?
C043 C034 H034 119.0 . . ?
C034 C02L H02L 119.2 . . ?
C034 C02L C02F 121.6(10) . . ?
C02F C02L H02L 119.2 . . ?
C02L C02F S1K 124.0(7) . . ?
C02L C02F C046 119.7(9) . . ?
C046 C02F S1K 116.3(8) . . ?
C02F C046 Cl03 123.1(9) . . ?
C057 C046 Cl03 120.0(10) . . ?
C057 C046 C02F 114.6(9) . . ?
C043 C057 C046 123.4(11) . . ?
C034 C043 Br0X 121.5(9) . . ?
C057 C043 Br0X 120.1(9) . . ?
C057 C043 C034 118.4(10) . . ?
C02W C03A H03A 120.4 . . ?
C02W C03A C03V 119.2(10) . . ?
C03V C03A H03A 120.4 . . ?
C02A C03H H03H 119.7 . . ?
C02C C03H C02A 120.6(9) . . ?
C02C C03H H03H 119.7 . . ?
C02Z C03I Br0V 120.1(8) . . ?
C033 C03I Br0V 119.4(9) . . ?
C033 C03I C02Z 120.5(11) . . ?
C02Q C03P H03P 120.4 . . ?
C02Q C03P C04I 119.2(12) . . ?
C04I C03P H03P 120.4 . . ?
C03P C02Q S1E 121.2(9) . . ?
C03P C02Q C05V 118.2(10) . . ?
C05V C02Q S1E 120.5(9) . . ?
C02Q C05V H05V 119.7 . . ?
C05Z C05V C02Q 120.6(12) . . ?
C05Z C05V H05V 119.7 . . ?
C05V C05Z H05Z 119.9 . . ?
C04J C05Z C05V 120.2(13) . . ?
C04J C05Z H05Z 119.9 . . ?
C05Z C04J Br11 120.0(10) . . ?
C05Z C04J C04I 121.0(11) . . ?
C04I C04J Br11 119.0(10) . . ?
C03P C04I H04I 119.6 . . ?
C04J C04I C03P 120.8(12) . . ?
C04J C04I H04I 119.6 . . ?
C02W C03R Cl07 128.1(12) . . ?
C04O C03R Cl07 110.7(11) . . ?
C04O C03R C02W 121.0(12) . . ?
C042 C070 C05M 120.0 . . ?
C042 C070 Cl15 107.8(10) . . ?
C05M C070 Cl15 131.8(10) . . ?
C070 C042 S1Q 119.2(6) . . ?
C03T C042 S1Q 120.8(6) . . ?
C03T C042 C070 120.0 . . ?
C042 C03T H03T 120.0 . . ?
C042 C03T C05I 120.0 . . ?
C05I C03T H03T 120.0 . . ?
C03T C05I H05I 120.0 . . ?
C06J C05I C03T 120.0 . . ?
C06J C05I H05I 120.0 . . ?
C05I C06J Br1N 120.3(7) . . ?
C05M C06J Br1N 119.4(7) . . ?
C05M C06J C05I 120.0 . . ?
C070 C05M H05M 120.0 . . ?
C06J C05M C070 120.0 . . ?
C06J C05M H05M 120.0 . . ?
C03A C03V H03V 120.9 . . ?
C04F C03V C03A 118.3(11) . . ?
C04F C03V H03V 120.9 . . ?
C029 C04B C033 120.6(10) . . ?
C03V C04F Br13 118.2(11) . . ?
C04O C04F Br13 119.5(10) . . ?
C04O C04F C03V 122.3(12) . . ?
C04F C04O C03R 119.9(13) . . ?
C02U C04Q H04Q 121.0 . . ?
C03G C04Q H04Q 121.0 . . ?
C03G C04Q C02U 118.0(12) . . ?
C04Q C02U H02U 118.4 . . ?
C02B C02U C04Q 123.2(10) . . ?
C02B C02U H02U 118.4 . . ?
C02U C02B S1G 123.5(8) . . ?
C02U C02B C03U 116.6(9) . . ?
C03U C02B S1G 119.7(9) . . ?
C02B C03U Cl5 118.7(11) . . ?
C052 C03U C02B 122.3(11) . . ?
C052 C03U Cl5 118.7(11) . . ?
C03U C052 C03G 118.6(11) . . ?
C04Q C03G Br10 118.4(11) . . ?
C04Q C03G C052 121.0(11) . . ?
C052 C03G Br10 120.6(10) . . ?
C04E P01P C04S 107.6(7) . . ?
C04E P01P C03Q 110.2(6) . . ?
C03Q P01P C04S 109.9(5) . . ?
C055 P01P C04E 109.0(6) . . ?
C055 P01P C04S 113.0(7) . . ?
C055 P01P C03Q 107.1(6) . . ?
C05W C38 H38 121.7 . . ?
C07F C38 H38 121.7 . . ?
C07F C38 C05W 116.5(15) . . ?
C04E C058 H058 121.0 . . ?
C04E C058 C06W 118.0(16) . . ?
C06W C058 H058 121.0 . . ?
C058 C04E P01P 117.8(11) . . ?
C058 C04E C049 120.6(15) . . ?
C049 C04E P01P 121.6(12) . . ?
C04E C049 H049 120.4 . . ?
C04E C049 C079 119.3(17) . . ?
C079 C049 H049 120.4 . . ?
C049 C079 H079 119.7 . . ?
C07S C079 C049 120.5(18) . . ?
C07S C079 H079 119.7 . . ?
C079 C07S H07S 119.8 . . ?
C079 C07S C06W 120(2) . . ?
C06W C07S H07S 119.8 . . ?
C058 C06W H06W 119.4 . . ?
C07S C06W C058 121(2) . . ?
C07S C06W H06W 119.4 . . ?
C05Y C05G H05G 119.8 . . ?
C05Y C05G C04S 120.4(12) . . ?
C04S C05G H05G 119.8 . . ?
C05G C05Y H05Y 120.4 . . ?
C05G C05Y C06O 119.2(12) . . ?
C06O C05Y H05Y 120.4 . . ?
C05Y C06O H06O 120.5 . . ?
C075 C06O C05Y 119.1(14) . . ?
C075 C06O H06O 120.5 . . ?
C06O C075 H075 119.2 . . ?
C044 C075 C06O 121.6(14) . . ?
C044 C075 H075 119.2 . . ?
C075 C044 H044 121.0 . . ?
C075 C044 C04S 118.0(13) . . ?
C04S C044 H044 121.0 . . ?
C05G C04S P01P 119.7(10) . . ?
C044 C04S P01P 118.6(10) . . ?
C044 C04S C05G 121.4(12) . . ?
C05L C067 H067 120.7 . . ?
C05L C067 C071 118.6(13) . . ?
C071 C067 H067 120.7 . . ?
C067 C05L H05L 119.2 . . ?
C067 C05L C064 121.7(11) . . ?
C064 C05L H05L 119.2 . . ?
C05L C064 H064 121.0 . . ?
C05L C064 C04C 118.0(14) . . ?
C04C C064 H064 121.0 . . ?
C064 C04C H04C 118.8 . . ?
C03Q C04C C064 122.3(14) . . ?
C03Q C04C H04C 118.8 . . ?
C04C C03Q P01P 119.7(9) . . ?
C04C C03Q C071 119.3(11) . . ?
C071 C03Q P01P 120.5(10) . . ?
C067 C071 H071 120.1 . . ?
C03Q C071 C067 119.9(14) . . ?
C03Q C071 H071 120.1 . . ?
C38 C05W H05W 118.8 . . ?
C055 C05W C38 122.4(14) . . ?
C055 C05W H05W 118.8 . . ?
C05W C055 P01P 120.9(11) . . ?
C05W C055 C039 117.5(13) . . ?
C039 C055 P01P 121.4(9) . . ?
C055 C039 H039 119.7 . . ?
C05N C039 C055 120.6(11) . . ?
C05N C039 H039 119.7 . . ?
C039 C05N H05N 119.1 . . ?
C039 C05N C07F 121.8(12) . . ?
C07F C05N H05N 119.1 . . ?
C38 C07F H07F 119.7 . . ?
C05N C07F C38 120.6(15) . . ?
C05N C07F H07F 119.7 . . ?
C05Q P01U C072 112.4(5) . . ?
C05Q P01U C059 108.7(6) . . ?
C05K P01U C072 111.2(6) . . ?
C05K P01U C05Q 107.6(6) . . ?
C05K P01U C059 110.2(6) . . ?
C059 P01U C072 106.8(6) . . ?
C1 C111 H111 120.0 . . ?
C1 C111 C07V 120.0 . . ?
C07V C111 H111 120.0 . . ?
C111 C1 H1 120.0 . . ?
C111 C1 C072 120.0 . . ?
C072 C1 H1 120.0 . . ?
C1 C072 P01U 119.0(7) . . ?
C07P C072 P01U 121.0(7) . . ?
C07P C072 C1 120.0 . . ?
C072 C07P H07P 120.0 . . ?
C07Z C07P C072 120.0 . . ?
C07Z C07P H07P 120.0 . . ?
C07P C07Z H07Z 120.0 . . ?
C07P C07Z C07V 120.0 . . ?
C07V C07Z H07Z 120.0 . . ?
C111 C07V H07V 120.0 . . ?
C07Z C07V C111 120.0 . . ?
C07Z C07V H07V 120.0 . . ?
C05S C05Q P01U 119.2(7) . . ?
C05S C05Q C07Q 120.0 . . ?
C07Q C05Q P01U 120.5(7) . . ?
C05Q C05S H05S 120.0 . . ?
C06C C05S C05Q 120.0 . . ?
C06C C05S H05S 120.0 . . ?
C05S C06C H06C 120.0 . . ?
C05S C06C C06Q 120.0 . . ?
C06Q C06C H06C 120.0 . . ?
C06C C06Q H06Q 120.0 . . ?
C07A C06Q C06C 120.0 . . ?
C07A C06Q H06Q 120.0 . . ?
C06Q C07A H07A 120.0 . . ?
C06Q C07A C07Q 120.0 . . ?
C07Q C07A H07A 120.0 . . ?
C05Q C07Q H07Q 120.0 . . ?
C07A C07Q C05Q 120.0 . . ?
C07A C07Q H07Q 120.0 . . ?
C06H C06K H06K 119.8 . . ?
C06H C06K C037 120.3(14) . . ?
C037 C06K H06K 119.8 . . ?
C06K C06H H06H 120.1 . . ?
C06K C06H C065 119.9(16) . . ?
C065 C06H H06H 120.1 . . ?
C06H C065 H065 120.2 . . ?
C06Y C065 C06H 119.5(17) . . ?
C06Y C065 H065 120.2 . . ?
C065 C06Y H06Y 120.1 . . ?
C05K C06Y C065 119.9(15) . . ?
C05K C06Y H06Y 120.1 . . ?
C06Y C05K P01U 119.1(10) . . ?
C06Y C05K C037 120.5(13) . . ?
C037 C05K P01U 120.1(10) . . ?
C06K C037 H037 120.1 . . ?
C05K C037 C06K 119.9(14) . . ?
C05K C037 H037 120.1 . . ?
C06G C06V H06V 120.5 . . ?
C059 C06V H06V 120.5 . . ?
C059 C06V C06G 119.0(15) . . ?
C06V C06G H06G 119.0 . . ?
C06L C06G C06V 121.9(18) . . ?
C06L C06G H06G 119.0 . . ?
C06G C06L H06L 120.0 . . ?
C06G C06L C07N 120.0(17) . . ?
C07N C06L H06L 120.0 . . ?
C06L C07N H07N 120.2 . . ?
C06L C07N C073 119.6(16) . . ?
C073 C07N H07N 120.2 . . ?
C07N C073 H073 121.6 . . ?
C059 C073 C07N 116.8(16) . . ?
C059 C073 H073 121.6 . . ?
C06V C059 P01U 119.2(11) . . ?
C06V C059 C073 122.3(14) . . ?
C073 C059 P01U 118.3(12) . . ?
C35 Br2 Br2 74.3(8) . 2_456 ?
C7 C10 C15 120.0 . . ?
C10 C7 Br1 118.2(8) . . ?
C10 C7 C8 120.0 . . ?
C8 C7 Br1 121.7(8) . . ?
C12 C8 C7 120.0 . . ?
C5 C12 C8 120.0 . . ?
C12 C5 S01X 120.8(7) . . ?
C12 C5 C15 120.0 . . ?
C15 C5 S01X 118.8(7) . . ?
C10 C15 Cl1 117.6(10) . . ?
C5 C15 C10 120.0 . . ?
C5 C15 Cl1 122.2(10) . . ?
C26 C35 Br2 122.4(13) . . ?
C26 C35 C34 120.0 . . ?
C34 C35 Br2 117.6(13) . . ?
C2 C26 C35 120.0 . . ?
C26 C2 C13 120.0 . . ?
C2 C13 S3 119.3(12) . . ?
C27 C13 S3 120.7(12) . . ?
C27 C13 C2 120.0 . . ?
C13 C27 C34 120.0 . . ?
C27 C34 C35 120.0 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Ag03 S1D C029 C02J 91.7(8) . . . . ?
Ag03 S1D C029 C04B -93.3(8) . . . . ?
Ag04 S1H C02X C035 -1.5(10) . . . . ?
Ag04 S1H C02X C05B -178.5(8) . . . . ?
Ag06 S1G C02B C02U 3.2(10) . . . . ?
Ag06 S1G C02B C03U -172.5(7) . . . . ?
Ag08 S1B C024 C02H 94.7(7) . . . . ?
Ag08 S1B C024 C03K -86.0(8) . . . . ?
Ag0B S1M C02W C03A 1.9(11) . . . . ?
Ag0B S1M C02W C03R -173.3(9) . . . . ?
Ag0E S1E C02Q C03P 76.8(10) . . . . ?
Ag0E S1E C02Q C05V -106.7(11) . . . . ?
Ag0G S1A C02A C031 175.2(8) . . . . ?
Ag0G S1A C02A C03H -5.9(9) . . . . ?
Ag0G S1B C024 C02H 175.7(6) . . . . ?
Ag0G S1B C024 C03K -5.0(8) . . . . ?
Ag0G S1K C02F C02L -104.4(9) . . . . ?
Ag0G S1K C02F C046 75.0(9) . . . . ?
Ag0H S1E C02Q C03P -15.6(11) . . . . ?
Ag0H S1E C02Q C05V 160.9(10) . . . . ?
Ag0H S1G C02B C02U -80.9(9) . . . . ?
Ag0H S1G C02B C03U 103.5(8) . . . . ?
Ag0H S1K C02F C02L -21.9(10) . . . . ?
Ag0H S1K C02F C046 157.4(8) . . . . ?
Ag0J S01X C5 C12 3.4(9) . . . . ?
Ag0J S01X C5 C15 -170.2(7) . . . . ?
Ag0J S1A C02A C031 -60.0(9) . . . . ?
Ag0J S1A C02A C03H 118.9(8) . . . . ?
Ag0J S1E C02Q C03P 160.3(9) . . . . ?
Ag0J S1E C02Q C05V -23.1(12) . . . . ?
Ag0J S3 C13 C2 79.8(10) . . . . ?
Ag0J S3 C13 C27 -100.0(10) . . . . ?
Ag0M S1A C02A C031 58.8(9) . . . . ?
Ag0M S1A C02A C03H -122.2(8) . . . . ?
Ag0M S1D C029 C02J 172.3(7) . . . . ?
Ag0M S1D C029 C04B -12.7(9) . . . . ?
Ag0M S1Q C042 C070 70.2(4) . . . . ?
Ag0M S1Q C042 C03T -108.9(5) . . . . ?
Ag0O S01X C5 C12 -74.7(8) . . . . ?
Ag0O S01X C5 C15 111.7(7) . . . . ?
Ag0O S1D C029 C02J 9.0(9) . . . . ?
Ag0O S1D C029 C04B -176.0(7) . . . . ?
Ag0O S1H C02X C035 -79.7(10) . . . . ?
Ag0O S1H C02X C05B 103.3(9) . . . . ?
Ag0O S3 C13 C2 155.2(9) . . . . ?
Ag0O S3 C13 C27 -24.6(12) . . . . ?
Ag0P S1B C024 C02H 5.9(8) . . . . ?
Ag0P S1B C024 C03K -174.8(7) . . . . ?
Ag0P S1M C02W C03A -79.9(10) . . . . ?
Ag0P S1M C02W C03R 104.8(10) . . . . ?
Ag0P S1Q C042 C070 148.7(4) . . . . ?
Ag0P S1Q C042 C03T -30.5(5) . . . . ?
Br1 C7 C8 C12 -176.1(11) . . . . ?
Br0S C026 C02C C03H 174.8(8) . . . . ?
Br0S C026 C02Y C031 -176.9(10) . . . . ?
Br1N C06J C05M C070 173.4(6) . . . . ?
Br11 C04J C04I C03P -179.5(11) . . . . ?
Br13 C04F C04O C03R 178.2(12) . . . . ?
Br15 C05P C06Z C05B 179.7(13) . . . . ?
S01X C5 C15 C10 173.6(10) . . . . ?
S01X C5 C15 Cl1 -0.5(15) . . . . ?
S1A C02A C031 C02Y 178.2(10) . . . . ?
S1A C02A C03H C02C 179.7(8) . . . . ?
S1B C024 C03K C04P -177.9(9) . . . . ?
S1D C029 C02J C02Z 175.5(8) . . . . ?
S1D C029 C04B C033 -177.5(9) . . . . ?
S1E C02Q C05V C05Z -177.2(15) . . . . ?
S1G C02B C03U C052 -180.0(9) . . . . ?
S1G C02B C03U Cl5 6.0(14) . . . . ?
S1H C02X C035 C05D -175.1(10) . . . . ?
S1H C02X C05B C06Z 177.9(12) . . . . ?
S1K C02F C046 Cl03 -22.4(17) . . . . ?
S1K C02F C046 C057 174.9(11) . . . . ?
S1M C02W C03A C03V -177.1(9) . . . . ?
S1M C02W C03R Cl07 -8(2) . . . . ?
S1M C02W C03R C04O 178.5(11) . . . . ?
S1Q C042 C03T C05I 179.1(6) . . . . ?
S3 C13 C27 C34 179.8(14) . . . . ?
Cl07 C03R C04O C04F -177.1(16) . . . . ?
Cl03 C046 C057 C043 -157.6(14) . . . . ?
C026 C02C C03H C02A 2.5(17) . . . . ?
C026 C02Y C031 C02A 2(2) . . . . ?
C029 C02J C02Z C03I 0.2(16) . . . . ?
C02C C026 C02Y C031 -1(2) . . . . ?
C02J C029 C04B C033 -2.6(17) . . . . ?
C02J C02Z C03I Br0V 178.3(8) . . . . ?
C02J C02Z C03I C033 1.0(17) . . . . ?
C02W C03A C03V C04F -0.4(19) . . . . ?
C02W C03R C04O C04F -2(2) . . . . ?
C02X C035 C05D C05P 0(2) . . . . ?
C035 C02X C05B C06Z 0.7(19) . . . . ?
C035 C05D C05P Br15 -176.9(11) . . . . ?
C035 C05D C05P C06Z -5(3) . . . . ?
C05D C05P C06Z C05B 8(3) . . . . ?
C05P C06Z C05B C02X -5(3) . . . . ?
C05B C02X C035 C05D 1.9(18) . . . . ?
C02Y C026 C02C C03H -1.5(18) . . . . ?
C030 C02H C024 S1B 179.3(7) . . . . ?
C030 C02H C024 C03K 0.0(13) . . . . ?
C02H C030 C02T Br0T 177.2(7) . . . . ?
C02H C030 C02T C04P -0.9(17) . . . . ?
C02H C024 C03K C04P 1.4(15) . . . . ?
C024 C03K C04P C02T -2.5(17) . . . . ?
C03K C04P C02T Br0T -175.8(8) . . . . ?
C03K C04P C02T C030 2.2(18) . . . . ?
C02T C030 C02H C024 -0.2(14) . . . . ?
C031 C02A C03H C02C -1.3(16) . . . . ?
C034 C02L C02F S1K -178.2(10) . . . . ?
C034 C02L C02F C046 2.5(18) . . . . ?
C02L C034 C043 Br0X 175.1(10) . . . . ?
C02L C034 C043 C057 -2(2) . . . . ?
C02L C02F C046 Cl03 157.0(12) . . . . ?
C02L C02F C046 C057 -5.8(18) . . . . ?
C02F C046 C057 C043 6(2) . . . . ?
C046 C057 C043 Br0X -179.0(12) . . . . ?
C046 C057 C043 C034 -2(2) . . . . ?
C043 C034 C02L C02F 1(2) . . . . ?
C03A C02W C03R Cl07 177.0(15) . . . . ?
C03A C02W C03R C04O 3(2) . . . . ?
C03A C03V C04F Br13 -176.9(10) . . . . ?
C03A C03V C04F C04O 1(2) . . . . ?
C03H C02A C031 C02Y -0.8(17) . . . . ?
C03I C033 C04B C029 3.6(18) . . . . ?
C03P C02Q C05V C05Z 0(2) . . . . ?
C02Q C03P C04I C04J 0(2) . . . . ?
C02Q C05V C05Z C04J 1(3) . . . . ?
C05V C05Z C04J Br11 179.0(15) . . . . ?
C05V C05Z C04J C04I -1(3) . . . . ?
C05Z C04J C04I C03P 1(2) . . . . ?
C04I C03P C02Q S1E 176.6(10) . . . . ?
C04I C03P C02Q C05V 0(2) . . . . ?
C03R C02W C03A C03V -1.8(18) . . . . ?
C070 C042 C03T C05I 0.0 . . . . ?
C042 C070 C05M C06J 0.0 . . . . ?
C042 C03T C05I C06J 0.0 . . . . ?
C03T C05I C06J Br1N -173.3(6) . . . . ?
C03T C05I C06J C05M 0.0 . . . . ?
C05I C06J C05M C070 0.0 . . . . ?
C05M C070 C042 S1Q -179.1(6) . . . . ?
C05M C070 C042 C03T 0.0 . . . . ?
C03V C04F C04O C03R 0(3) . . . . ?
C04B C029 C02J C02Z 0.6(16) . . . . ?
C04B C033 C03I Br0V 179.8(9) . . . . ?
C04B C033 C03I C02Z -2.9(18) . . . . ?
C04Q C02U C02B S1G -179.7(9) . . . . ?
C04Q C02U C02B C03U -3.9(16) . . . . ?
C02U C04Q C03G Br10 -176.6(8) . . . . ?
C02U C04Q C03G C052 2.2(18) . . . . ?
C02U C02B C03U C052 4.1(16) . . . . ?
C02U C02B C03U Cl5 -170.0(11) . . . . ?
C02B C03U C052 C03G -1.3(18) . . . . ?
C03U C052 C03G Br10 176.8(9) . . . . ?
C03U C052 C03G C04Q -2.0(19) . . . . ?
C03G C04Q C02U C02B 0.9(17) . . . . ?
P01P C04E C049 C079 -176.7(11) . . . . ?
P01P C03Q C071 C067 175.4(11) . . . . ?
P01P C055 C039 C05N 177.6(11) . . . . ?
C38 C05W C055 P01P -175.1(15) . . . . ?
C38 C05W C055 C039 1(3) . . . . ?
C058 C04E C049 C079 1(2) . . . . ?
C04E P01P C04S C05G 88.5(13) . . . . ?
C04E P01P C04S C044 -85.9(12) . . . . ?
C04E P01P C03Q C04C -27.8(14) . . . . ?
C04E P01P C03Q C071 160.4(12) . . . . ?
C04E P01P C055 C05W 125.0(13) . . . . ?
C04E P01P C055 C039 -50.7(13) . . . . ?
C04E C058 C06W C07S -2(2) . . . . ?
C04E C049 C079 C07S -2(2) . . . . ?
C049 C079 C07S C06W 0(3) . . . . ?
C079 C07S C06W C058 1(3) . . . . ?
C06W C058 C04E P01P 178.5(11) . . . . ?
C06W C058 C04E C049 1(2) . . . . ?
C05G C05Y C06O C075 7(3) . . . . ?
C05Y C05G C04S P01P -171.7(12) . . . . ?
C05Y C05G C04S C044 2(2) . . . . ?
C05Y C06O C075 C044 -5(3) . . . . ?
C06O C075 C044 C04S 1(3) . . . . ?
C075 C044 C04S P01P 174.2(13) . . . . ?
C075 C044 C04S C05G 0(2) . . . . ?
C04S P01P C04E C058 39.5(12) . . . . ?
C04S P01P C04E C049 -143.0(10) . . . . ?
C04S P01P C03Q C04C -146.2(12) . . . . ?
C04S P01P C03Q C071 42.0(14) . . . . ?
C04S P01P C055 C05W -115.3(14) . . . . ?
C04S P01P C055 C039 69.0(13) . . . . ?
C04S C05G C05Y C06O -6(2) . . . . ?
C067 C05L C064 C04C -3(2) . . . . ?
C05L C067 C071 C03Q -3(2) . . . . ?
C05L C064 C04C C03Q 3(2) . . . . ?
C064 C04C C03Q P01P -175.3(11) . . . . ?
C064 C04C C03Q C071 -3(2) . . . . ?
C04C C03Q C071 C067 4(2) . . . . ?
C03Q P01P C04E C058 -80.3(12) . . . . ?
C03Q P01P C04E C049 97.2(11) . . . . ?
C03Q P01P C04S C05G -151.5(12) . . . . ?
C03Q P01P C04S C044 34.1(14) . . . . ?
C03Q P01P C055 C05W 5.8(15) . . . . ?
C03Q P01P C055 C039 -169.9(11) . . . . ?
C071 C067 C05L C064 3(2) . . . . ?
C05W C38 C07F C05N 10(3) . . . . ?
C05W C055 C039 C05N 2(2) . . . . ?
C055 P01P C04E C058 162.4(10) . . . . ?
C055 P01P C04E C049 -20.1(12) . . . . ?
C055 P01P C04S C05G -32.0(14) . . . . ?
C055 P01P C04S C044 153.7(12) . . . . ?
C055 P01P C03Q C04C 90.7(14) . . . . ?
C055 P01P C03Q C071 -81.1(12) . . . . ?
C055 C039 C05N C07F 2(2) . . . . ?
C039 C05N C07F C38 -8(3) . . . . ?
C07F C38 C05W C055 -7(3) . . . . ?
P01U C072 C07P C07Z 179.4(9) . . . . ?
P01U C05Q C05S C06C -174.4(8) . . . . ?
P01U C05Q C07Q C07A 174.3(8) . . . . ?
P01U C05K C037 C06K -173.8(10) . . . . ?
C111 C1 C072 P01U -179.4(8) . . . . ?
C111 C1 C072 C07P 0.0 . . . . ?
C1 C111 C07V C07Z 0.0 . . . . ?
C1 C072 C07P C07Z 0.0 . . . . ?
C072 P01U C05Q C05S -151.3(6) . . . . ?
C072 P01U C05Q C07Q 34.4(8) . . . . ?
C072 P01U C05K C06Y 67.1(13) . . . . ?
C072 P01U C05K C037 -119.1(11) . . . . ?
C072 P01U C059 C06V -148.9(11) . . . . ?
C072 P01U C059 C073 36.7(13) . . . . ?
C072 C07P C07Z C07V 0.0 . . . . ?
C07P C07Z C07V C111 0.0 . . . . ?
C07V C111 C1 C072 0.0 . . . . ?
C05Q P01U C072 C1 -74.0(8) . . . . ?
C05Q P01U C072 C07P 106.6(7) . . . . ?
C05Q P01U C05K C06Y -56.3(13) . . . . ?
C05Q P01U C05K C037 117.4(11) . . . . ?
C05Q P01U C059 C06V -27.4(13) . . . . ?
C05Q P01U C059 C073 158.2(11) . . . . ?
C05Q C05S C06C C06Q 0.0 . . . . ?
C05S C05Q C07Q C07A 0.0 . . . . ?
C05S C06C C06Q C07A 0.0 . . . . ?
C06C C06Q C07A C07Q 0.0 . . . . ?
C06Q C07A C07Q C05Q 0.0 . . . . ?
C07Q C05Q C05S C06C 0.0 . . . . ?
C06K C06H C065 C06Y 1(3) . . . . ?
C06H C06K C037 C05K 2(2) . . . . ?
C06H C065 C06Y C05K 0(3) . . . . ?
C065 C06Y C05K P01U 172.6(13) . . . . ?
C065 C06Y C05K C037 -1(2) . . . . ?
C06Y C05K C037 C06K 0(2) . . . . ?
C05K P01U C072 C1 165.3(7) . . . . ?
C05K P01U C072 C07P -14.0(9) . . . . ?
C05K P01U C05Q C05S -28.5(8) . . . . ?
C05K P01U C05Q C07Q 157.1(7) . . . . ?
C05K P01U C059 C06V 90.2(12) . . . . ?
C05K P01U C059 C073 -84.2(13) . . . . ?
C037 C06K C06H C065 -3(3) . . . . ?
C06V C06G C06L C07N 4(3) . . . . ?
C06G C06V C059 P01U -177.9(11) . . . . ?
C06G C06V C059 C073 -4(2) . . . . ?
C06G C06L C07N C073 -5(3) . . . . ?
C06L C07N C073 C059 1(2) . . . . ?
C07N C073 C059 P01U 177.3(11) . . . . ?
C07N C073 C059 C06V 3(2) . . . . ?
C059 P01U C072 C1 45.1(8) . . . . ?
C059 P01U C072 C07P -134.3(7) . . . . ?
C059 P01U C05Q C05S 90.7(7) . . . . ?
C059 P01U C05Q C07Q -83.6(8) . . . . ?
C059 P01U C05K C06Y -174.6(12) . . . . ?
C059 P01U C05K C037 -0.9(13) . . . . ?
C059 C06V C06G C06L 0(2) . . . . ?
Br2 Br2 C35 C26 135.5(12) 2_456 . . . ?
Br2 Br2 C35 C34 -44.1(9) 2_456 . . . ?
Br2 C35 C26 C2 -179.6(16) . . . . ?
Br2 C35 C34 C27 179.6(15) . . . . ?
C10 C7 C8 C12 0.0 . . . . ?
C7 C10 C15 C5 0.0 . . . . ?
C7 C10 C15 Cl1 174.4(14) . . . . ?
C7 C8 C12 C5 0.0 . . . . ?
C8 C12 C5 S01X -173.5(10) . . . . ?
C8 C12 C5 C15 0.0 . . . . ?
C12 C5 C15 C10 0.0 . . . . ?
C12 C5 C15 Cl1 -174.1(15) . . . . ?
C15 C10 C7 Br1 176.2(11) . . . . ?
C15 C10 C7 C8 0.0 . . . . ?
C35 C26 C2 C13 0.0 . . . . ?
C26 C35 C34 C27 0.0 . . . . ?
C26 C2 C13 S3 -179.8(14) . . . . ?
C26 C2 C13 C27 0.0 . . . . ?
C2 C13 C27 C34 0.0 . . . . ?
C13 C27 C34 C35 0.0 . . . . ?
C34 C35 C26 C2 0.0 . . . . ?
Cl5 C03U C052 C03G 172.8(12) . . . . ?
Cl15 C070 C042 S1Q 7.4(10) . . . . ?
Cl15 C070 C042 C03T -173.4(10) . . . . ?
Cl15 C070 C05M C06J 171.6(13) . . . . ?

_smtbx_masks_special_details     ?
loop_
_smtbx_masks_void_nr
_smtbx_masks_void_average_x
_smtbx_masks_void_average_y
_smtbx_masks_void_average_z
_smtbx_masks_void_volume
_smtbx_masks_void_count_electrons
_smtbx_masks_void_content
1 0.179 -0.848 -0.181 4310.4 983.9 '24 CH2Cl2'
2 0.000 0.459 0.250 117.8 6.7 ?
3 0.000 0.541 0.750 117.8 5.6 ?
4 0.500 -0.041 0.250 117.8 6.7 ?
5 0.500 0.041 0.750 117.8 5.6 ?

_smtbx_masks_void_probe_radius   1.2
_smtbx_masks_void_truncation_radius 1.2
_olex2_submission_special_instructions 'No special instructions were received'
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_1
_database_code_depnum_ccdc_archive 'CCDC 2327473'
loop_
_audit_author_name
_audit_author_address
'shuxin wang'
;Qingdao University of Science and Technology
China
;
_audit_update_record             
;
2024-01-20 deposited with the CCDC.	2024-03-22 downloaded from the CCDC.
;
_audit_creation_date             2024-01-19
_audit_creation_method           
;
Olex2 1.3
(compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6408)
;
_shelx_SHELXL_version_number     2019/1
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         
'0.333(Ag24 Br12.071 C120 Cl15.88 Pt S20), 0.333(Ag24 Br13.14 C120 Cl13.72 Pt S20), 0.333(Ag24 Br12.58 C120 Cl14.84 Pt S20), 2.667(C24 P), 0.867[C24PH20]'
_chemical_formula_sum            
'C184 H120.67 Ag24 Br12.49 Cl15.03 P2.67 Pt S20'
_chemical_formula_weight         7369.73
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag 0.1306 4.2820 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Br Br -0.6763 1.2805 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -4.5932 6.9264 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   26.638
_cell_length_b                   29.956
_cell_length_c                   31.053
_cell_angle_alpha                93.09
_cell_angle_beta                 90.67
_cell_angle_gamma                90.79
_cell_volume                     24739.4
_cell_formula_units_Z            3
_cell_measurement_reflns_used    1543
_cell_measurement_temperature    120
_cell_measurement_theta_max      130.15
_cell_measurement_theta_min      5.53
_shelx_estimated_absorpt_T_max   0.394
_shelx_estimated_absorpt_T_min   0.267
_exptl_absorpt_coefficient_mu    16.342
_exptl_absorpt_correction_T_max  1.0000
_exptl_absorpt_correction_T_min  0.1713
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
STOE LANA, absorption correction by scaling of reflection intensities.
J. Koziskova, F. Hahn, J. Richter, J. Kozisek, "Comparison of different
absorption corrections on the model structure of tetrakis(μ₂-acetato)-
diaqua-di-copper(II)", Acta Chimica Slovaca, vol. 9, no. 2, 2016, pp. 136 - 140.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            black
_exptl_crystal_colour_primary    black
_exptl_crystal_density_diffrn    1.484
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             10449
_exptl_crystal_size_max          0.11
_exptl_crystal_size_mid          0.08
_exptl_crystal_size_min          0.07
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0487
_diffrn_reflns_av_unetI/netI     0.0557
_diffrn_reflns_Laue_measured_fraction_full 0.946
_diffrn_reflns_Laue_measured_fraction_max 0.925
_diffrn_reflns_limit_h_max       29
_diffrn_reflns_limit_h_min       -32
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -36
_diffrn_reflns_limit_l_max       37
_diffrn_reflns_limit_l_min       -33
_diffrn_reflns_number            165059
_diffrn_reflns_point_group_measured_fraction_full 0.946
_diffrn_reflns_point_group_measured_fraction_max 0.925
_diffrn_reflns_theta_full        67.686
_diffrn_reflns_theta_max         69.759
_diffrn_reflns_theta_min         3.319
_diffrn_ambient_temperature      120
_diffrn_detector                 Pilatus300K
_diffrn_detector_area_resol_mean 5.81
_diffrn_detector_type            'DECTRIS PILATUS 300K'
_diffrn_measured_fraction_theta_full 0.946
_diffrn_measured_fraction_theta_max 0.925
_diffrn_measurement_details      
;
 1559 frames, detector distance = 60 mm
;
_diffrn_measurement_device       'Eulerian 4-circle diffractometer'
_diffrn_measurement_device_type  'STOE STADIVARI'
_diffrn_measurement_method       'rotation method, ω scans'
_diffrn_radiation_collimation    '1.2 mm, 0.6 diameter'
_diffrn_radiation_monochromator  'Graded multilayer mirror'
_diffrn_radiation_polarisn_norm  270
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           'Cu K\a'
_diffrn_radiation_wavelength     1.54186
_diffrn_source                   'GeniX 3D HF Cu'
_diffrn_source_current           0.600
_diffrn_source_power             0.030
_diffrn_source_voltage           50
_reflns_d_resolution_high        0.822
_reflns_d_resolution_low         13.317
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_limit_h_max              29
_reflns_limit_h_min              -32
_reflns_limit_k_max              19
_reflns_limit_k_min              -36
_reflns_limit_l_max              37
_reflns_limit_l_min              -33
_reflns_number_gt                56187
_reflns_number_total             90081
_reflns_special_details          'reflections have not been merged'
_reflns_threshold_expression     I>4u(I)
_computing_cell_refinement       
;
X-Area Recipe 1.33.0.0 (STOE, 2015)
;
_computing_data_collection       
;
X-Area Pilatus3_SV 1.31.153.0 (STOE, 2018)
;
_computing_data_reduction        
;
X-Area Integrate 1.74.2.0 (STOE, 2018)
X-Area LANA 1.75.3.0 (STOE, 2018)
;
_computing_molecular_graphics    'Olex2 1.3 (Dolomanov et al., 2009)'
_computing_publication_material  
;
STOE & Cie GmbH, X-Area, software package for collecting single-crystal or
multi-domain crystal data on STOE area-detector diffractometers, for image 
processing, for the correction and scaling of reflection intensities and 
for outlier rejection, version 1.86, Darmstadt 2018
;
_computing_structure_refinement  'XL  (Sheldrick, 2008)'
_computing_structure_solution    'SHELXT 2018/2 (Sheldrick, 2018)'
_refine_diff_density_max         1.492
_refine_diff_density_min         -2.317
_refine_diff_density_rms         0.135
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.041
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           fullcycle
_refine_ls_number_parameters     3334
_refine_ls_number_reflns         86370
_refine_ls_number_restraints     3301
_refine_ls_R_factor_all          0.0909
_refine_ls_R_factor_gt           0.0607
_refine_ls_restrained_S_all      1.139
_refine_ls_shift/su_max          0.037
_refine_ls_shift/su_mean         0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.1073P)²+7.5674P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1650
_refine_ls_wR_factor_ref         0.1850
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups
2. Shared sites
{Cl30, Br17}
{Cl22, Br3}
{Cl24, Br15}
{Br10, Cl14}
{Br13, Cl28}
{Br14, Cl2}
{Cl5, Br4}
{Cl21, Br18}
{Br1, Cl10}
{Br2, Cl9}
{Br24, Cl13}
{Cl27, Br5}
{Br19, Cl38}
{Cl19, Br9}
{Cl3, Br30}
{Cl32, Br25}
{Cl35, Br6}
{Cl26, Br16}
{Cl34, Br7}
3. Restrained distances
 Cl20-C144
 1.75 with sigma of 0.01
 Cl33-C61
 1.75 with sigma of 0.01
 Cl31-C147
 1.75 with sigma of 0.01
 Cl19-C146
 1.9 with sigma of 0.01
 C276-Cl19 \\sim Cl19-C273
 with sigma of 0.02
 C142-Cl20 \\sim Cl20-C135
 with sigma of 0.02
 C235-Cl33 \\sim Cl33-C171
 with sigma of 0.02
 C276-Cl31 \\sim Cl31-C274
 with sigma of 0.02
 C126-Cl9 \\sim Cl9-C235
 with sigma of 0.02
4. Restrained planarity
 Cl15, Cl26, C45, C82, C145, C270, C271, C272
 with sigma of 0.1
 Cl19, C23, C146, C147, C273, C274, C276
 with sigma of 0.1
 Cl20, C135, C140, C142, C144
 with sigma of 0.1
 Cl33, C30, C61, C171, C235
 with sigma of 0.1
 Cl33, C61, C126, C235
 with sigma of 0.1
 Cl31, C23, C147, C274, C276
 with sigma of 0.1
5. Uiso/Uaniso restraints and constraints
Cl31 \\sim S7 \\sim C23 \\sim C146 \\sim C147 \\sim C273 \\sim C274 \\sim C276
\\sim Br9: within 3.8A with sigma of 0.01 and sigma for terminal atoms of 0.02
within 3.8A
Ag36 \\sim Cl15 \\sim S29 \\sim C45 \\sim C82 \\sim C145 \\sim C270 \\sim C271
\\sim C272 \\sim Br16: within 3.8A with sigma of 0.01 and sigma for terminal
atoms of 0.02 within 3.8A
S26 \\sim C80 \\sim C141 \\sim C143 \\sim C264 \\sim C266 \\sim C268 \\sim
Br29: within 3.8A with sigma of 0.01 and sigma for terminal atoms of 0.02
within 3.8A
P3 \\sim C4 \\sim C11 \\sim C33 \\sim C42 \\sim C76 \\sim C78 \\sim C91 \\sim
C128 \\sim C136 \\sim C137 \\sim C139 \\sim C160 \\sim C166 \\sim C176 \\sim
C186 \\sim C198 \\sim C248 \\sim C253 \\sim C255 \\sim C257 \\sim C260 \\sim
C261 \\sim C263 \\sim C269: within 3.8A with sigma of 0.01 and sigma for
terminal atoms of 0.02 within 3.8A
S3 \\sim C19 \\sim C116 \\sim C118 \\sim C214 \\sim C216 \\sim C218 \\sim Br26:
within 3.8A with sigma of 0.01 and sigma for terminal atoms of 0.02 within 3.8A
All non-hydrogen atoms have similar U: within 2A with sigma of 0.02 and sigma
for terminal atoms of 0.04 within 2A
Cl15 \\sim C45 \\sim C82 \\sim C145 \\sim C270 \\sim C271 \\sim C272 \\sim
Br16: within 2A with sigma of 0.001 and sigma for terminal atoms of 0.002
within 2A
Cl31 \\sim C23 \\sim C146 \\sim C147 \\sim C273 \\sim C274 \\sim C276 \\sim
Br9: within 2A with sigma of 0.001 and sigma for terminal atoms of 0.002 within
2A
Cl33 \\sim S21 \\sim C28 \\sim C30 \\sim C61 \\sim C126 \\sim C171 \\sim C235:
within 2A with sigma of 0.001 and sigma for terminal atoms of 0.002 within 2A
Uanis(C30) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(C146) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(Cl9) \\sim Ueq, Uanis(Br2) \\sim Ueq: with sigma of 0.01 and sigma for
terminal atoms of 0.02
Uanis(Br9) \\sim Ueq, Uanis(Cl19) \\sim Ueq: with sigma of 0.01 and sigma for
terminal atoms of 0.02
Uanis(Cl30) = Uanis(Br17)
Uanis(Cl32) = Uanis(Br25)
Uanis(Cl27) = Uanis(Br5)
Uanis(Br2) = Uanis(Cl9)
Uanis(Cl22) = Uanis(Br3)
Uanis(Cl19) = Uanis(Br9)
Uanis(Cl24) = Uanis(Br15)
Uanis(Cl26) = Uanis(Br16)
Uanis(Br10) = Uanis(Cl14)
Uanis(Br24) = Uanis(Cl13)
Uanis(Br13) = Uanis(Cl28)
Uanis(Br19) = Uanis(Cl38)
Uanis(Br14) = Uanis(Cl2)
Uanis(Cl3) = Uanis(Br30)
Uanis(Cl5) = Uanis(Br4)
Uanis(Cl35) = Uanis(Br6)
Uanis(Cl21) = Uanis(Br18)
Uanis(Br1) = Uanis(Cl10)
Uanis(Cl34) = Uanis(Br7)
6. Others
 Fixed Sof: Cl4(0.79) Cl5(0.93) Cl6(0.56) Cl7(0.6) Cl9(0.59) Cl10(0.56)
 Cl13(0.5) Cl21(0.6) Cl23(0.93) Cl27(0.79) Cl33(0.59) Cl37(0.5) Br1(0.44)
 Br2(0.41) Br4(0.07) Br5(0.21) Br18(0.4) Br24(0.5) Cl3(0.45) Cl8(0.78)
 Cl11(0.78) Cl15(0.6) Cl17(0.61) Cl19(0.35) Cl25(0.3) Cl26(0.6) Cl29(0.45)
 Cl31(0.35) Cl32(0.61) Cl34(0.78) Cl35(0.78) Cl38(0.3) Br6(0.22) Br7(0.22)
 Br9(0.65) Br16(0.4) Br19(0.7) Br25(0.39) Br30(0.55) Cl1(0.32) Cl2(0.81)
 Cl14(0.32) Cl16(0.81) Cl18(0.66) Cl20(0.4) Cl22(0.58) Cl24(0.66) Cl28(0.4)
 Cl30(0.66) Cl36(0.66) Cl39(0.58) Br3(0.42) Br10(0.68) Br13(0.6) Br14(0.19)
 Br15(0.34) Br17(0.34)
7.a Aromatic/amide H refined with riding coordinates:
 C8(H8), C18(H18), C22(H22), C126(H126), C28(H28), C235(H235), C31(H31),
 C34(H34), C36(H36), C40(H40), C46(H46), C53(H53), C55(H55), C59(H59), C60(H60),
  C64(H64), C66(H66), C72(H72), C75(H75), C90(H90), C92(H92), C94(H94),
 C110(H110), C112(H112), C117(H117), C125(H125), C151(H151), C161(H161),
 C169(H169), C217(H217), C220(H220), C226(H226), C242(H242), C265(H265),
 C39(H39), C241(H241), C73(H73), C45(H45), C271(H271), C82(H82), C93(H93),
 C168(H168), C170(H170), C95(H95), C99(H99), C182(H182), C101(H101), C247(H247),
  C249(H249), C134(H134), C273(H273), C23(H23), C276(H276), C206(H206),
 C208(H208), C114(H114), C214(H214), C116(H116), C19(H19), C218(H218),
 C122(H122), C227(H227), C229(H229), C124(H124), C250(H250), C252(H252),
 C32(H32), C13(H13), C26(H26), C49(H49), C71(H71), C86(H86), C108(H108),
 C109(H109), C200(H200), C202(H202), C111(H111), C121(H121), C43(H43),
 C138(H138), C142(H142), C141(H141), C80(H80), C266(H266), C268(H268),
 C148(H148), C149(H149), C157(H157), C165(H165), C173(H173), C177(H177),
 C181(H181), C191(H191), C193(H193), C203(H203), C207(H207), C221(H221),
 C231(H231), C232(H232), C238(H238), C267(H267), C1(H1), C10(H10), C17(H17),
 C20(H20), C29(H29), C38(H38), C47(H47), C62(H62), C88(H88), C115(H115),
 C131(H131), C133(H133), C153(H153), C175(H175), C179(H179), C189(H189),
 C199(H199), C211(H211), C212(H212), C240(H240), C15(H15), C154(H154), C87(H87),
  C50(H50), C158(H158), C37(H37), C63(H63), C67(H67), C233(H233), C105(H105),
 C223(H223), C74(H74), C83(H83), C107(H107), C120(H120), C162(H162), C164(H164),
  C188(H188), C194(H194), C237(H237), C11(H11), C33(H33), C76(H76), C253(H253),
 C136(H136), C255(H255), C257(H257), C78(H78), C260(H260), C139(H139), C4(H4),
 C263(H263), C91(H91), C128(H128), C137(H137), C160(H160), C166(H166),
 C176(H176), C186(H186), C198(H198), C14(H14), C48(H48), C54(H54), C58(H58),
 C152(H152), C209(H209), C96(H96), C185(H185), C65(H65), C85(H85), C97(H97),
 C103(H103), C178(H178), C192(H192), C197(H197), C213(H213), C239(H239),
 C244(H244), C258(H258), C275(H275)
7.b Fitted hexagon refined as free rotating group:
 C30(C126,C28,C171,C61,C235), C217(C25,C220,C222,C224,C226), C39(C241,C130,
 C243,C73,C245), C45(C270,C145,C271,C82,C272), C93(C168,C9,C170,C95,C172),
 C99(C180,C56,C182,C101,C184), C132(C247,C21,C249,C134,C251), C146(C273,C23,
 C274,C147,C276), C206(C113,C208,C35,C210,C114), C214(C116,C216,C19,C218,C118),
 C225(C122,C227,C69,C229,C124), C250(C252,C254,C256,C32,C259), C109(C200,C5,
 C202,C111,C204), C135(C43,C138,C140,C142,C144), C141(C264,C80,C266,C143,C268),
 C15(C154,C87,C156,C50,C158), C63(C67,C233,C190,C105,C223), C76(C253,C136,C255,
 C42,C257), C78(C260,C139,C261,C4,C263), C58(C152,C183,C209,C96,C185)
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt1 Pt 1.000000 0.500000 0.500000 0.039 Uani 1 2 d S . P . .
Ag1 Ag 1.09598(2) 0.52876(2) 0.48584(2) 0.045 Uani 1 1 d . . . . .
Ag4 Ag 1.05967(2) 0.52051(2) 0.57096(2) 0.045 Uani 1 1 d . . . . .
Ag6 Ag 0.98786(2) 0.44591(2) 0.56799(2) 0.046 Uani 1 1 d . . . . .
Ag8 Ag 1.01849(2) 0.58943(2) 0.52001(2) 0.045 Uani 1 1 d . . . . .
Ag9 Ag 0.96871(3) 0.48034(2) 0.65967(2) 0.060 Uani 1 1 d . . . . .
Ag10 Ag 0.95342(2) 0.53568(2) 0.57182(2) 0.045 Uani 1 1 d . . . . .
Ag11 Ag 1.08224(3) 0.65465(2) 0.58211(2) 0.058 Uani 1 1 d . . . . .
Ag17 Ag 0.92411(2) 0.55864(2) 0.48494(2) 0.047 Uani 1 1 d . . . . .
Ag27 Ag 0.93683(3) 0.62560(2) 0.62073(3) 0.062 Uani 1 1 d . . . . .
Ag28 Ag 1.15244(3) 0.58096(2) 0.55418(2) 0.055 Uani 1 1 d . . . . .
Ag29 Ag 0.91706(3) 0.65379(2) 0.52892(3) 0.065 Uani 1 1 d . . . . .
Ag32 Ag 1.04960(3) 0.55298(2) 0.66700(2) 0.059 Uani 1 1 d . . . . .
Cl4 Cl 1.29546(15) 0.5832(2) 0.4684(2) 0.123 Uani 0.79 1 d . U P . .
Cl5 Cl 0.66700(14) 0.68050(13) 0.63995(15) 0.115 Uani 0.93 1 d . U P C .
Cl6 Cl 0.9552(3) 0.3395(2) 0.7095(2) 0.105 Uani 0.56 1 d . U P . .
Cl7 Cl 0.78999(18) 0.69043(16) 0.44521(19) 0.081 Uani 0.6 1 d . U P . .
Cl9 Cl 1.16437(15) 0.3987(2) 0.81912(16) 0.249 Uani 0.59 1 d D U P B .
Cl10 Cl 1.14184(16) 0.29099(15) 0.70172(17) 0.198 Uani 0.56 1 d . U P A .
Cl13 Cl 1.29802(9) 0.70818(6) 0.73719(6) 0.089 Uani 0.5 1 d . U P H .
Cl21 Cl 0.64081(9) 0.58483(10) 0.50716(9) 0.108 Uani 0.6 1 d . U P E .
Cl23 Cl 0.8608(2) 0.6985(3) 0.69394(17) 0.171 Uani 0.93 1 d . U P . .
Cl27 Cl 1.22865(11) 0.68540(8) 0.34560(9) 0.090 Uani 0.79 1 d . U P D .
Cl33 Cl 1.0511(2) 0.55946(19) 0.81088(18) 0.094 Uani 0.59 1 d D U P . .
Cl37 Cl 1.2822(2) 0.6991(2) 0.56279(18) 0.074 Uani 0.5 1 d . U P . .
S1 S 1.12702(9) 0.54536(7) 0.62355(7) 0.051 Uani 1 1 d . U . . .
S4 S 1.18639(8) 0.54438(8) 0.48626(8) 0.052 Uani 1 1 d . U . . .
S5 S 0.89946(11) 0.69486(9) 0.59860(10) 0.071 Uani 1 1 d . U . . .
S6 S 0.91328(9) 0.54962(8) 0.64233(8) 0.054 Uani 1 1 d . U . . .
S10 S 0.96150(9) 0.40313(8) 0.62926(8) 0.057 Uani 1 1 d . U . . .
S12 S 1.01201(9) 0.67206(7) 0.53001(8) 0.054 Uani 1 1 d . U . . .
S18 S 1.02887(9) 0.63126(8) 0.64407(8) 0.056 Uani 1 1 d . U . . .
S20 S 1.17014(10) 0.66436(8) 0.56360(8) 0.060 Uani 1 1 d . U . . .
S21 S 1.00400(13) 0.52079(11) 0.72568(9) 0.078 Uani 1 1 d . U . . .
S22 S 0.87170(10) 0.62122(9) 0.46604(9) 0.063 Uani 1 1 d . U . . .
C2 C 0.7078(4) 0.5959(4) 0.4961(4) 0.069 Uani 1 1 d . U . . .
C3 C 0.8487(3) 0.5386(3) 0.6327(3) 0.051 Uani 1 1 d . U . . .
C7 C 1.1966(3) 0.5861(3) 0.4499(3) 0.050 Uani 1 1 d . U . . .
C8 C 1.0168(6) 0.7182(4) 0.4109(4) 0.083 Uani 1 1 d . U . . .
H8 H 0.993770 0.725372 0.388825 0.100 Uiso 1 1 calc R U . . .
C12 C 1.1592(4) 0.4934(3) 0.6302(3) 0.059 Uani 1 1 d . U . . .
C18 C 1.1517(4) 0.4714(3) 0.6676(3) 0.062 Uani 1 1 d . U . . .
H18 H 1.126756 0.481341 0.687346 0.074 Uiso 1 1 calc R U . . .
C22 C 1.1944(3) 0.4793(3) 0.6017(3) 0.058 Uani 1 1 d . U . . .
H22 H 1.199029 0.494535 0.575986 0.070 Uiso 1 1 calc R U . . .
C24 C 1.2460(4) 0.6010(4) 0.4414(4) 0.063 Uani 1 1 d . U . . .
C27 C 1.0351(4) 0.6687(3) 0.6900(4) 0.066 Uani 1 1 d . U . . .
C30 C 1.1165(3) 0.4378(2) 0.7958(2) 0.086 Uani 1 1 d G U . . .
C126 C 1.0922(3) 0.41905(19) 0.7592(2) 0.085 Uani 1 1 d DG U . B .
H126 H 1.099883 0.389537 0.748820 0.102 Uiso 1 1 calc R U . . .
C28 C 1.0567(3) 0.4434(2) 0.7377(2) 0.084 Uani 1 1 d G U . B .
H28 H 1.040046 0.430598 0.712659 0.100 Uiso 1 1 calc R U . . .
C171 C 1.0454(3) 0.4866(2) 0.7528(2) 0.082 Uani 1 1 d DG U . B .
C61 C 1.0698(3) 0.50542(19) 0.7894(2) 0.085 Uani 1 1 d DG U . B .
C235 C 1.1053(3) 0.4810(2) 0.8109(2) 0.086 Uani 1 1 d DG U . B .
H235 H 1.121915 0.493876 0.835901 0.103 Uiso 1 1 calc R U . . .
C31 C 0.8183(4) 0.5712(3) 0.6162(3) 0.056 Uani 1 1 d . U . . .
H31 H 0.833189 0.598459 0.608074 0.067 Uiso 1 1 calc R U . . .
C34 C 1.1802(4) 0.4355(4) 0.6761(4) 0.072 Uani 1 1 d . U . . .
H34 H 1.174736 0.420184 0.701615 0.087 Uiso 1 1 calc R U . . .
C36 C 0.8274(4) 0.4977(3) 0.6425(3) 0.058 Uani 1 1 d . U . . .
H36 H 0.848095 0.475630 0.654099 0.070 Uiso 1 1 calc R U . . .
C40 C 0.7771(4) 0.4885(4) 0.6357(4) 0.065 Uani 1 1 d . U . . .
H40 H 0.763631 0.459581 0.640070 0.078 Uiso 1 1 calc R U . . .
C44 C 0.8088(4) 0.6126(3) 0.4807(3) 0.061 Uani 1 1 d . U . . .
C46 C 1.0089(5) 0.7341(4) 0.7319(5) 0.088 Uani 1 1 d . U . . .
H46 H 0.987081 0.758692 0.736362 0.106 Uiso 1 1 calc R U . . .
C53 C 0.7937(4) 0.5739(4) 0.5004(3) 0.064 Uani 1 1 d . U . . .
H53 H 0.818415 0.553410 0.508838 0.076 Uiso 1 1 calc R U . . .
C55 C 1.1686(4) 0.6323(4) 0.3928(4) 0.069 Uani 1 1 d . U . . .
H55 H 1.141935 0.641535 0.374926 0.082 Uiso 1 1 calc R U . . .
C59 C 0.7673(5) 0.6916(5) 0.6615(5) 0.091 Uani 1 1 d . U . . .
H59 H 0.757073 0.694909 0.690679 0.109 Uiso 1 1 calc R U . . .
C60 C 1.1586(3) 0.6030(3) 0.4247(3) 0.062 Uani 1 1 d . U . . .
H60 H 1.124865 0.594166 0.429531 0.074 Uiso 1 1 calc R U . . .
C64 C 1.2546(4) 0.6317(4) 0.4104(4) 0.069 Uani 1 1 d . U . . .
H64 H 1.287959 0.641625 0.405341 0.083 Uiso 1 1 calc R U . . .
C66 C 1.2238(4) 0.4427(4) 0.6098(4) 0.071 Uani 1 1 d . U . . .
H66 H 1.248200 0.432424 0.589585 0.085 Uiso 1 1 calc R U . . .
C70 C 1.0337(4) 0.6908(3) 0.4807(3) 0.059 Uani 1 1 d . U . . .
C72 C 0.7666(4) 0.5649(4) 0.6112(4) 0.066 Uani 1 1 d . U . . .
H72 H 0.745925 0.587708 0.600936 0.080 Uiso 1 1 calc R U . . .
C75 C 0.7429(4) 0.5644(4) 0.5081(4) 0.069 Uani 1 1 d . U . . .
H75 H 0.732771 0.537714 0.521011 0.083 Uiso 1 1 calc R U . . .
C79 C 1.2154(5) 0.6480(4) 0.3867(4) 0.073 Uani 1 1 d . U . . .
C81 C 0.7458(5) 0.5229(4) 0.6221(4) 0.076 Uani 1 1 d . U . . .
C90 C 1.0722(5) 0.6620(4) 0.7212(3) 0.074 Uani 1 1 d . U . . .
H90 H 1.093543 0.636855 0.718243 0.089 Uiso 1 1 calc R U . . .
C92 C 0.7222(4) 0.6325(4) 0.4769(4) 0.072 Uani 1 1 d . U . . .
H92 H 0.697520 0.652964 0.468439 0.086 Uiso 1 1 calc R U . . .
C94 C 1.2124(5) 0.6753(3) 0.6901(3) 0.068 Uani 1 1 d . U . . .
H94 H 1.197821 0.670638 0.717292 0.081 Uiso 1 1 calc R U . . .
C98 C 0.8361(5) 0.6906(4) 0.6103(4) 0.072 Uani 1 1 d . U . . .
C102 C 1.2052(4) 0.6728(3) 0.6120(3) 0.057 Uani 1 1 d . U . . .
C106 C 1.2613(5) 0.6926(3) 0.6877(4) 0.072 Uani 1 1 d . U . . .
C110 C 0.7993(4) 0.6848(3) 0.5772(4) 0.070 Uani 1 1 d . U . . .
H110 H 0.810196 0.681916 0.548161 0.084 Uiso 1 1 calc R U . . .
C112 C 1.2814(5) 0.7002(3) 0.6487(4) 0.069 Uani 1 1 d . U . . .
H112 H 1.314130 0.712992 0.647529 0.083 Uiso 1 1 calc R U . . .
C117 C 1.1008(5) 0.7168(4) 0.4348(4) 0.080 Uani 1 1 d . U . . .
H117 H 1.135471 0.722310 0.429963 0.096 Uiso 1 1 calc R U . . .
C123 C 0.7714(4) 0.6416(4) 0.4691(4) 0.069 Uani 1 1 d . U . . .
C125 C 1.0039(5) 0.7041(4) 0.6952(4) 0.079 Uani 1 1 d . U . . .
H125 H 0.978563 0.708746 0.674138 0.094 Uiso 1 1 calc R U . . .
C127 C 1.2548(4) 0.6894(3) 0.6102(3) 0.065 Uani 1 1 d . U . . .
C151 C 1.0852(5) 0.6992(4) 0.4743(4) 0.074 Uani 1 1 d . U . . .
H151 H 1.109143 0.693247 0.496126 0.089 Uiso 1 1 calc R U . . .
C159 C 1.2170(5) 0.4213(4) 0.6479(4) 0.076 Uani 1 1 d . U . . .
C161 C 0.7467(5) 0.6831(4) 0.5850(4) 0.078 Uani 1 1 d . U . . .
H161 H 0.722375 0.680600 0.562336 0.093 Uiso 1 1 calc R U . . .
C169 C 1.1857(4) 0.6650(3) 0.6525(3) 0.063 Uani 1 1 d . U . . .
H169 H 1.153042 0.652201 0.654197 0.075 Uiso 1 1 calc R U . . .
C196 C 1.0482(6) 0.7256(5) 0.7617(5) 0.100 Uani 1 1 d . U . . .
C201 C 0.7328(5) 0.6853(4) 0.6307(5) 0.090 Uani 1 1 d . U . . .
C215 C 0.8178(5) 0.6936(5) 0.6523(5) 0.089 Uani 1 1 d . U . . .
C217 C 1.0996(2) 0.3508(3) 0.6444(3) 0.092 Uani 1 1 d G U . . .
H217 H 1.131459 0.352656 0.631130 0.110 Uiso 1 1 calc R U . . .
C25 C 1.0927(3) 0.3229(3) 0.6783(3) 0.114 Uani 1 1 d G U . . .
C220 C 1.0462(4) 0.3202(3) 0.6978(3) 0.108 Uani 1 1 d G U . . .
H220 H 1.041448 0.301146 0.720939 0.130 Uiso 1 1 calc R U . . .
C222 C 1.0065(3) 0.3453(3) 0.6834(2) 0.081 Uani 1 1 d G U . . .
C224 C 1.0133(2) 0.3732(2) 0.6495(2) 0.061 Uani 1 1 d G U . . .
C226 C 1.0599(3) 0.3759(2) 0.6300(2) 0.065 Uani 1 1 d G U . . .
H226 H 1.064631 0.394948 0.606861 0.078 Uiso 1 1 calc R U . . .
C242 C 0.9996(5) 0.7010(4) 0.4483(4) 0.078 Uani 1 1 d . U . . .
H242 H 0.964680 0.696063 0.452060 0.094 Uiso 1 1 calc R U . . .
C246 C 1.0681(6) 0.7251(5) 0.4056(4) 0.088 Uani 1 1 d . U . . .
C265 C 1.0777(6) 0.6916(5) 0.7559(4) 0.092 Uani 1 1 d . U . . .
H265 H 1.103704 0.687272 0.776379 0.111 Uiso 1 1 calc R U . . .
Br1 Br 1.14184(16) 0.29099(15) 0.70172(17) 0.198 Uani 0.44 1 d . U P A 1
Br2 Br 1.16437(15) 0.3987(2) 0.81912(16) 0.249 Uani 0.41 1 d . U P B 1
Br4 Br 0.66700(14) 0.68050(13) 0.63995(15) 0.115 Uani 0.07 1 d . U P C 1
Br5 Br 1.22865(11) 0.68540(8) 0.34560(9) 0.090 Uani 0.21 1 d . U P D 1
Br18 Br 0.64081(9) 0.58483(10) 0.50716(9) 0.108 Uani 0.4 1 d . U P E 1
Br21 Br 1.25672(7) 0.37198(6) 0.65891(6) 0.107 Uani 1 1 d . U . F 1
Br22 Br 0.67717(6) 0.51312(7) 0.61274(7) 0.116 Uani 1 1 d . U . G 1
Br24 Br 1.29802(9) 0.70818(6) 0.73719(6) 0.089 Uani 0.5 1 d . U P H 1
Br27 Br 1.08889(10) 0.75037(10) 0.35368(7) 0.162 Uani 1 1 d . U . I 1
Br28 Br 1.05403(12) 0.76710(10) 0.81104(9) 0.187 Uani 1 1 d . U . J 1
Pt2 Pt 1.500000 1.000000 0.500000 0.055 Uani 1 2 d S . P . .
Ag2 Ag 1.31242(4) 0.97190(2) 0.48332(3) 0.077 Uani 1 1 d . . . . .
Ag7 Ag 1.50824(4) 0.83276(2) 0.47598(3) 0.072 Uani 1 1 d . . . . .
Ag13 Ag 1.52557(3) 0.91904(2) 0.52929(2) 0.061 Uani 1 1 d . . . . .
Ag14 Ag 1.53993(3) 1.02110(2) 0.42246(2) 0.064 Uani 1 1 d . . . . .
Ag20 Ag 1.33925(5) 0.95093(3) 0.39066(3) 0.089 Uani 1 1 d . . . . .
Ag21 Ag 1.51111(3) 0.93026(2) 0.43956(2) 0.061 Uani 1 1 d . . . . .
Ag23 Ag 1.40379(3) 1.02720(2) 0.51562(3) 0.064 Uani 1 1 d . . . . .
Ag25 Ag 1.43635(3) 0.99869(2) 0.42915(2) 0.065 Uani 1 1 d . . . . .
Ag30 Ag 1.42524(3) 0.93577(2) 0.49693(2) 0.059 Uani 1 1 d . . . . .
Ag31 Ag 1.40071(4) 0.84384(2) 0.45121(3) 0.072 Uani 1 1 d . . . . .
Ag35 Ag 1.47681(4) 0.89513(3) 0.34519(3) 0.084 Uani 1 1 d . . . . .
Ag36 Ag 1.49182(5) 0.99290(3) 0.33261(3) 0.092 Uani 1 1 d . U . . .
Cl3 Cl 1.23079(14) 1.20817(8) 0.44698(12) 0.150 Uani 0.45 1 d . U P T .
Cl8 Cl 1.6050(4) 1.0829(3) 0.2665(2) 0.213 Uani 0.78 1 d . U P . .
Cl11 Cl 1.3848(3) 0.68951(18) 0.41604(14) 0.137 Uani 0.78 1 d . U P . .
Cl15 Cl 1.4669(6) 0.8604(4) 0.1982(4) 0.207 Uani 0.6 1 d . U P . .
Cl17 Cl 1.5778(2) 0.75604(18) 0.5956(2) 0.101 Uani 0.61 1 d . U P . .
Cl19 Cl 1.1406(3) 1.1004(2) 0.3363(3) 0.351 Uani 0.35 1 d D U P M .
Cl25 Cl 1.3397(8) 0.9078(4) 0.2885(5) 0.145 Uani 0.3 1 d . U P . .
Cl26 Cl 1.6880(3) 0.8755(2) 0.1979(2) 0.284 Uani 0.6 1 d . U P O .
Cl29 Cl 1.2002(4) 1.0714(3) 0.5396(5) 0.138 Uani 0.45 1 d . U P . .
Cl31 Cl 1.2390(8) 0.9412(6) 0.3171(7) 0.243 Uani 0.35 1 d D U P . .
Cl32 Cl 1.4191(2) 0.76836(15) 0.69178(15) 0.210 Uani 0.61 1 d . U P R .
Cl34 Cl 1.3837(3) 0.63718(17) 0.57791(16) 0.211 Uani 0.78 1 d . U P L .
Cl35 Cl 1.7694(2) 0.9874(2) 0.2838(2) 0.234 Uani 0.78 1 d . U P K .
Cl38 Cl 1.26639(12) 0.74908(11) 0.24896(10) 0.166 Uani 0.3 1 d . U P P .
S2 S 1.34553(11) 0.89170(7) 0.49495(9) 0.066 Uani 1 1 d . U . . .
S3 S 1.39824(15) 1.00203(9) 0.35559(10) 0.085 Uani 1 1 d . U . . .
S7 S 1.25686(19) 0.94359(12) 0.42217(18) 0.126 Uani 1 1 d . U . . .
S9 S 1.55535(13) 0.84468(8) 0.54465(9) 0.070 Uani 1 1 d . U . . .
S11 S 1.39171(15) 0.88067(8) 0.37887(10) 0.082 Uani 1 1 d . U . . .
S15 S 1.52953(13) 0.85883(8) 0.39905(9) 0.070 Uani 1 1 d . U . . .
S23 S 1.31566(13) 1.03725(9) 0.53426(11) 0.079 Uani 1 1 d . U . . .
S25 S 1.55716(17) 1.04919(9) 0.35151(10) 0.091 Uani 1 1 d . U . . .
S28 S 1.44703(12) 0.77534(8) 0.44339(9) 0.067 Uani 1 1 d . U . . .
S29 S 1.4788(3) 0.93111(15) 0.27686(15) 0.153 Uani 1 1 d . U . . .
C39 C 1.4235(5) 0.7160(3) 0.55645(18) 0.115 Uani 1 1 d G U . . .
H39 H 1.431490 0.721603 0.586164 0.138 Uiso 1 1 calc R U . . .
C241 C 1.4377(4) 0.7468(2) 0.5267(2) 0.100 Uani 1 1 d G U . . .
H241 H 1.455461 0.773323 0.536150 0.120 Uiso 1 1 calc R U . . .
C130 C 1.4260(4) 0.7386(2) 0.4833(2) 0.066 Uani 1 1 d G U . . .
C243 C 1.4001(4) 0.6998(3) 0.46948(19) 0.093 Uani 1 1 d G U . . .
C73 C 1.3859(4) 0.6691(3) 0.4992(3) 0.116 Uani 1 1 d G U . . .
H73 H 1.368133 0.642506 0.489779 0.140 Uiso 1 1 calc R U . . .
C245 C 1.3976(5) 0.6772(3) 0.5427(2) 0.113 Uani 1 1 d G U . . .
C45 C 1.5753(9) 0.8718(3) 0.2009(3) 0.210 Uani 1 1 d G U . . .
H45 H 1.575588 0.846213 0.181376 0.252 Uiso 1 1 calc R U . . .
C270 C 1.5312(7) 0.8839(6) 0.2216(5) 0.208 Uani 1 1 d G U . . .
C145 C 1.5307(7) 0.9213(6) 0.2501(6) 0.207 Uani 1 1 d G U . . .
C271 C 1.5743(9) 0.9466(4) 0.2579(5) 0.208 Uani 1 1 d G U . . .
H271 H 1.574016 0.972109 0.277348 0.249 Uiso 1 1 calc R U . . .
C82 C 1.6184(7) 0.9345(6) 0.2371(6) 0.210 Uani 1 1 d G U . . .
H82 H 1.648250 0.951754 0.242355 0.252 Uiso 1 1 calc R U . . .
C272 C 1.6189(7) 0.8971(6) 0.2086(5) 0.212 Uani 1 1 d G U . . .
C93 C 1.3078(4) 0.8904(2) 0.6205(2) 0.095 Uani 1 1 d G U . . .
H93 H 1.300500 0.911749 0.643276 0.114 Uiso 1 1 calc R U . . .
C168 C 1.3219(4) 0.90468(14) 0.5805(2) 0.087 Uani 1 1 d G U . . .
H168 H 1.324207 0.935735 0.575881 0.104 Uiso 1 1 calc R U . . .
C9 C 1.3326(3) 0.8735(2) 0.54723(19) 0.075 Uani 1 1 d G U . . .
C170 C 1.3293(4) 0.82807(18) 0.5540(2) 0.082 Uani 1 1 d G U . . .
H170 H 1.336598 0.806758 0.531246 0.098 Uiso 1 1 calc R U . . .
C95 C 1.3152(4) 0.81382(15) 0.5940(2) 0.095 Uani 1 1 d G U . . .
H95 H 1.312891 0.782772 0.598641 0.114 Uiso 1 1 calc R U . . .
C172 C 1.3045(4) 0.8450(2) 0.62729(19) 0.092 Uani 1 1 d G U . . .
C99 C 1.4983(4) 0.7688(2) 0.6381(3) 0.101 Uani 1 1 d G U . . .
H99 H 1.507422 0.742283 0.651501 0.121 Uiso 1 1 calc R U . . .
C180 C 1.5283(3) 0.7852(2) 0.6060(3) 0.092 Uani 1 1 d G U . . .
C56 C 1.5149(3) 0.8240(2) 0.5864(2) 0.076 Uani 1 1 d G U . . .
C182 C 1.4717(3) 0.84643(19) 0.5988(3) 0.086 Uani 1 1 d G U . . .
H182 H 1.462570 0.872952 0.585386 0.103 Uiso 1 1 calc R U . . .
C101 C 1.4417(3) 0.8300(3) 0.6309(3) 0.104 Uani 1 1 d G U . . .
H101 H 1.412151 0.845314 0.639410 0.124 Uiso 1 1 calc R U . . .
C184 C 1.4550(4) 0.7912(3) 0.6505(3) 0.118 Uani 1 1 d G U . . .
C132 C 1.2417(3) 1.0969(3) 0.5134(3) 0.105 Uani 1 1 d G U . . .
C247 C 1.2244(3) 1.1351(3) 0.4947(4) 0.111 Uani 1 1 d G U . . .
H247 H 1.191164 1.144907 0.499893 0.133 Uiso 1 1 calc R U . . .
C21 C 1.2558(4) 1.1589(2) 0.4685(3) 0.108 Uani 1 1 d G U . . .
C249 C 1.3045(4) 1.1445(2) 0.4610(3) 0.092 Uani 1 1 d G U . . .
H249 H 1.325974 1.160798 0.443088 0.111 Uiso 1 1 calc R U . . .
C134 C 1.3218(3) 1.1064(2) 0.4796(3) 0.080 Uani 1 1 d G U . . .
H134 H 1.355012 1.096574 0.474479 0.096 Uiso 1 1 calc R U . . .
C251 C 1.2903(3) 1.0826(2) 0.5058(3) 0.086 Uani 1 1 d G U . . .
C146 C 1.1777(4) 1.0557(4) 0.3605(4) 0.247 Uani 1 1 d DG U . . .
C273 C 1.1921(6) 1.0591(5) 0.4037(4) 0.245 Uani 1 1 d DG U . M .
H273 H 1.182752 1.084355 0.421470 0.294 Uiso 1 1 calc R U . . .
C23 C 1.2202(7) 1.0255(6) 0.4211(5) 0.244 Uani 1 1 d G U . M .
H23 H 1.230019 1.027767 0.450614 0.292 Uiso 1 1 calc R U . . .
C274 C 1.2339(5) 0.9884(5) 0.3951(6) 0.243 Uani 1 1 d DG U . M .
C147 C 1.2195(5) 0.9851(4) 0.3519(6) 0.244 Uani 1 1 d DG U . M .
C276 C 1.1914(5) 1.0187(4) 0.3346(4) 0.245 Uani 1 1 d DG U . M .
H276 H 1.181612 1.016357 0.305026 0.295 Uiso 1 1 calc R U . . .
C206 C 1.6908(4) 0.9860(3) 0.3398(4) 0.143 Uani 1 1 d G U . . .
H206 H 1.709776 0.965448 0.355383 0.171 Uiso 1 1 calc R U . . .
C113 C 1.7098(4) 1.0028(5) 0.3024(4) 0.167 Uani 1 1 d G U . . .
C208 C 1.6820(5) 1.0328(5) 0.2797(3) 0.164 Uani 1 1 d G U . . .
H208 H 1.695046 1.044320 0.254095 0.197 Uiso 1 1 calc R U . . .
C35 C 1.6351(5) 1.0460(4) 0.2943(3) 0.143 Uani 1 1 d G U . . .
C210 C 1.6160(4) 1.0292(4) 0.3317(4) 0.113 Uani 1 1 d G U . . .
C114 C 1.6439(5) 0.9992(3) 0.3545(3) 0.120 Uani 1 1 d G U . . .
H114 H 1.630819 0.987661 0.380065 0.144 Uiso 1 1 calc R U . . .
C214 C 1.4057(4) 1.0934(3) 0.3478(4) 0.127 Uani 1 1 d G U . . .
H214 H 1.441084 1.089739 0.346783 0.153 Uiso 1 1 calc R U . . .
C116 C 1.3853(5) 1.1351(3) 0.3419(4) 0.136 Uani 1 1 d G U . . .
H116 H 1.406649 1.159937 0.336838 0.164 Uiso 1 1 calc R U . . .
C216 C 1.3336(5) 1.1406(2) 0.3433(4) 0.137 Uani 1 1 d G U . . .
C19 C 1.3023(4) 1.1043(4) 0.3507(5) 0.148 Uani 1 1 d G U . . .
H19 H 1.267012 1.108005 0.351691 0.177 Uiso 1 1 calc R U . . .
C218 C 1.3228(5) 1.0626(3) 0.3566(4) 0.134 Uani 1 1 d G U . . .
H218 H 1.301446 1.037806 0.361636 0.161 Uiso 1 1 calc R U . . .
C118 C 1.3745(5) 1.0572(2) 0.3551(4) 0.122 Uani 1 1 d G U . . .
C225 C 1.6969(3) 0.8657(3) 0.3705(4) 0.128 Uani 1 1 d G U . . .
C122 C 1.6622(4) 0.8797(3) 0.3404(3) 0.116 Uani 1 1 d G U . Q .
H122 H 1.673354 0.890083 0.313744 0.139 Uiso 1 1 calc R U . . .
C227 C 1.6113(4) 0.8785(2) 0.3494(3) 0.104 Uani 1 1 d G U . Q .
H227 H 1.587544 0.888065 0.328924 0.125 Uiso 1 1 calc R U . . .
C69 C 1.5950(3) 0.8633(2) 0.3885(3) 0.083 Uani 1 1 d G U . Q .
C229 C 1.6297(4) 0.8493(3) 0.4185(3) 0.101 Uani 1 1 d G U . Q .
H229 H 1.618537 0.838912 0.445214 0.121 Uiso 1 1 calc R U . . .
C124 C 1.6806(4) 0.8505(3) 0.4095(4) 0.113 Uani 1 1 d G U . Q .
H124 H 1.704347 0.840929 0.430035 0.136 Uiso 1 1 calc R U . . .
C250 C 1.3187(3) 0.7724(2) 0.3272(3) 0.087 Uani 1 1 d G U . . .
H250 H 1.310930 0.743180 0.335767 0.105 Uiso 1 1 calc R U . . .
C252 C 1.3458(3) 0.8020(2) 0.3549(2) 0.083 Uani 1 1 d G U . . .
H252 H 1.356574 0.793002 0.382370 0.099 Uiso 1 1 calc R U . . .
C254 C 1.3572(4) 0.8449(2) 0.3425(2) 0.077 Uani 1 1 d G U . . .
C256 C 1.3415(4) 0.8581(2) 0.3023(3) 0.118 Uani 1 1 d G U . . .
C32 C 1.3143(4) 0.8285(3) 0.2746(2) 0.116 Uani 1 1 d G U . . .
H32 H 1.303594 0.837513 0.247205 0.140 Uiso 1 1 calc R U . . .
C259 C 1.3030(4) 0.7857(3) 0.2871(3) 0.101 Uani 1 1 d G U . . .
Br6 Br 1.7694(2) 0.9874(2) 0.2838(2) 0.234 Uani 0.22 1 d . U P K 1
Br7 Br 1.3837(3) 0.63718(17) 0.57791(16) 0.211 Uani 0.22 1 d . U P L 1
Br9 Br 1.1406(3) 1.1004(2) 0.3363(3) 0.351 Uani 0.65 1 d . U P M 1
Br11 Br 1.28368(9) 0.82610(6) 0.68094(6) 0.129 Uani 1 1 d . U . N 1
Br16 Br 1.6880(3) 0.8755(2) 0.1979(2) 0.284 Uani 0.4 1 d . U P O 1
Br19 Br 1.26639(12) 0.74908(11) 0.24896(10) 0.166 Uani 0.7 1 d . U P P 1
Br20 Br 1.76538(11) 0.87049(12) 0.35807(14) 0.234 Uani 1 1 d . U . Q 1
Br25 Br 1.4191(2) 0.76836(15) 0.69178(15) 0.210 Uani 0.39 1 d . U P R 1
Br26 Br 1.30780(16) 1.19819(9) 0.33993(14) 0.241 Uani 1 1 d . U . S 1
Br30 Br 1.23079(14) 1.20817(8) 0.44698(12) 0.150 Uani 0.55 1 d . U P T 1
Pt3 Pt 0.500000 0.500000 1.000000 0.045 Uani 1 2 d S . P . .
Ag3 Ag 0.44756(3) 0.63004(3) 0.89177(2) 0.064 Uani 1 1 d . . . . .
Ag5 Ag 0.55186(3) 0.54395(3) 0.84031(2) 0.063 Uani 1 1 d . . . . .
Ag12 Ag 0.45726(3) 0.53933(2) 0.93180(2) 0.050 Uani 1 1 d . . . . .
Ag15 Ag 0.48048(3) 0.44706(2) 0.92650(2) 0.050 Uani 1 1 d . . . . .
Ag16 Ag 0.66191(3) 0.56428(3) 0.95349(2) 0.066 Uani 1 1 d . . . . .
Ag18 Ag 0.59577(3) 0.64155(3) 0.93803(3) 0.073 Uani 1 1 d . . . . .
Ag19 Ag 0.56157(3) 0.51384(2) 0.93191(2) 0.050 Uani 1 1 d . . . . .
Ag22 Ag 0.59949(3) 0.52035(2) 1.01811(2) 0.052 Uani 1 1 d . . . . .
Ag24 Ag 0.52771(3) 0.58714(2) 0.99040(2) 0.052 Uani 1 1 d . . . . .
Ag26 Ag 0.43058(3) 0.56532(2) 1.02025(2) 0.052 Uani 1 1 d . . . . .
Ag33 Ag 0.43121(4) 0.66050(3) 0.98584(3) 0.074 Uani 1 1 d . . . . .
Ag34 Ag 0.46266(3) 0.48127(2) 0.83936(2) 0.058 Uani 1 1 d . . . . .
Cl1 Cl 0.7998(4) 0.6741(5) 0.9596(3) 0.107 Uani 0.32 1 d . U P . .
Cl2 Cl 0.60948(19) 0.2701(2) 0.79004(17) 0.203 Uani 0.81 1 d . U P Y .
Cl14 Cl 0.80166(12) 0.69047(10) 0.78569(9) 0.154 Uani 0.32 1 d . U P V .
Cl16 Cl 0.42334(15) 0.33004(11) 0.78689(12) 0.077 Uani 0.81 1 d . U P . .
Cl18 Cl 0.3111(3) 0.7098(2) 1.0720(2) 0.118 Uani 0.66 1 d . U P . .
Cl20 Cl 0.5580(5) 0.5401(4) 0.6960(4) 0.188 Uani 0.4 1 d D U P . .
Cl22 Cl 0.75227(16) 0.69167(13) 1.14977(12) 0.165 Uani 0.58 1 d . U P U .
Cl24 Cl 0.18035(16) 0.71074(17) 0.88165(16) 0.173 Uani 0.66 1 d . U P Z .
Cl28 Cl 0.65498(11) 0.36917(12) 0.68743(9) 0.148 Uani 0.4 1 d . U P X .
Cl30 Cl 0.14960(12) 0.61419(17) 1.00960(12) 0.152 Uani 0.66 1 d . U P A .
Cl36 Cl 0.3725(2) 0.7011(3) 0.82555(17) 0.116 Uani 0.66 1 d . U P . .
Cl39 Cl 0.80466(19) 0.5677(2) 1.0332(2) 0.098 Uani 0.58 1 d . U P . .
S8 S 0.63099(9) 0.52986(9) 0.88144(7) 0.057 Uani 1 1 d . U . . .
S13 S 0.41605(13) 0.70218(10) 0.92041(10) 0.077 Uani 1 1 d . U . . .
S14 S 0.44569(10) 0.40494(8) 0.86237(7) 0.056 Uani 1 1 d . U . . .
S16 S 0.41529(10) 0.55501(8) 0.86326(7) 0.055 Uani 1 1 d . U . . .
S17 S 0.38511(12) 0.63180(10) 1.04620(9) 0.070 Uani 1 1 d . U . . .
S19 S 0.50504(12) 0.51456(10) 0.77674(8) 0.069 Uani 1 1 d . U . . .
S24 S 0.69134(10) 0.52875(10) 1.01954(8) 0.065 Uani 1 1 d . U . . .
S26 S 0.53977(11) 0.62303(9) 0.87268(8) 0.066 Uani 1 1 d . U . . .
S27 S 0.68446(13) 0.64668(12) 0.95745(10) 0.085 Uani 1 1 d . U . . .
S30 S 0.52796(12) 0.66984(9) 0.98853(9) 0.068 Uani 1 1 d . U . . .
C6 C 0.2496(6) 0.7084(5) 0.8893(6) 0.109 Uani 1 1 d . U . . .
C13 C 0.6951(4) 0.4607(4) 0.8944(3) 0.068 Uani 1 1 d . U . . .
H13 H 0.702552 0.475807 0.921398 0.082 Uiso 1 1 calc R U . . .
C16 C 0.3502(4) 0.5504(4) 0.8750(3) 0.062 Uani 1 1 d . U . . .
C26 C 0.2372(6) 0.6575(6) 1.0395(5) 0.102 Uani 1 1 d . U . . .
H26 H 0.215848 0.681021 1.049207 0.122 Uiso 1 1 calc R U . . .
C41 C 0.6579(4) 0.4774(4) 0.8689(3) 0.062 Uani 1 1 d . U . . .
C49 C 0.3247(4) 0.5102(4) 0.8634(3) 0.066 Uani 1 1 d . U . . .
H49 H 0.342338 0.485355 0.851155 0.079 Uiso 1 1 calc R U . . .
C51 C 0.7064(4) 0.5752(4) 1.0562(3) 0.061 Uani 1 1 d . U . . .
C52 C 0.7679(6) 0.6753(6) 0.8346(5) 0.111 Uani 1 1 d . U . . .
C57 C 0.3210(4) 0.6278(4) 1.0329(4) 0.069 Uani 1 1 d . U . . .
C71 C 0.2648(6) 0.7065(5) 0.9333(5) 0.103 Uani 1 1 d . U . . .
H71 H 0.241184 0.707491 0.955954 0.123 Uiso 1 1 calc R U . . .
C77 C 0.4937(4) 0.3685(3) 0.8427(3) 0.060 Uani 1 1 d . U . . .
C86 C 0.3243(4) 0.5856(4) 0.8925(3) 0.066 Uani 1 1 d . U . . .
H86 H 0.342132 0.612559 0.900356 0.080 Uiso 1 1 calc R U . . .
C89 C 0.2168(5) 0.6203(6) 1.0189(5) 0.101 Uani 1 1 d . U . . .
C100 C 0.4818(5) 0.3349(4) 0.8094(3) 0.071 Uani 1 1 d . U . . .
C108 C 0.6719(5) 0.5934(4) 1.0820(4) 0.071 Uani 1 1 d . U . . .
H108 H 0.638523 0.581846 1.080826 0.085 Uiso 1 1 calc R U . . .
C109 C 0.5174(3) 0.7094(3) 1.0707(3) 0.107 Uani 1 1 d G U . . .
H109 H 0.482268 0.705680 1.066127 0.128 Uiso 1 1 calc R U . . .
C200 C 0.5357(4) 0.7314(4) 1.1084(3) 0.129 Uani 1 1 d G U . . .
H200 H 0.512970 0.742705 1.129517 0.155 Uiso 1 1 calc R U . . .
C5 C 0.5871(5) 0.7369(4) 1.1150(3) 0.133 Uani 1 1 d G U . . .
C202 C 0.6203(3) 0.7205(4) 1.0841(4) 0.132 Uani 1 1 d G U . . .
H202 H 0.655494 0.724230 1.088652 0.158 Uiso 1 1 calc R U . . .
C111 C 0.6021(3) 0.6985(3) 1.0464(3) 0.120 Uani 1 1 d G U . . .
H111 H 0.624792 0.687204 1.025262 0.144 Uiso 1 1 calc R U . . .
C204 C 0.5506(4) 0.6930(3) 1.0397(2) 0.079 Uani 1 1 d G U . . .
C121 C 0.7216(4) 0.4240(4) 0.8830(3) 0.070 Uani 1 1 d . U . . .
H121 H 0.746757 0.414250 0.902110 0.084 Uiso 1 1 calc R U . . .
C129 C 0.7345(6) 0.6444(5) 1.1135(4) 0.093 Uani 1 1 d . U . . .
C135 C 0.5415(3) 0.4734(2) 0.7497(2) 0.077 Uani 1 1 d DG U . . .
C43 C 0.5451(3) 0.4297(3) 0.7623(2) 0.079 Uani 1 1 d G U . . .
H43 H 0.524550 0.419707 0.784722 0.095 Uiso 1 1 calc R U . . .
C138 C 0.5788(3) 0.4007(3) 0.7420(3) 0.098 Uani 1 1 d G U . . .
H138 H 0.581228 0.370837 0.750625 0.117 Uiso 1 1 calc R U . . .
C140 C 0.6088(3) 0.4153(4) 0.7092(3) 0.125 Uani 1 1 d G U . . .
C142 C 0.6052(3) 0.4590(4) 0.6966(3) 0.143 Uani 1 1 d DG U . . .
H142 H 0.625783 0.469042 0.674142 0.172 Uiso 1 1 calc R U . . .
C144 C 0.5716(3) 0.4881(3) 0.7168(2) 0.125 Uani 1 1 d DG U . . .
C141 C 0.5451(4) 0.7328(3) 0.8029(3) 0.125 Uani 1 1 d G U . . .
H141 H 0.532697 0.762414 0.805005 0.151 Uiso 1 1 calc R U . . .
C264 C 0.5734(5) 0.7185(3) 0.7676(3) 0.116 Uani 1 1 d G U . . .
C80 C 0.5915(4) 0.6752(4) 0.7646(3) 0.121 Uani 1 1 d G U . . .
H80 H 0.610855 0.665444 0.740475 0.145 Uiso 1 1 calc R U . . .
C266 C 0.5813(4) 0.6461(3) 0.7969(3) 0.111 Uani 1 1 d G U . . .
H266 H 0.593645 0.616496 0.794831 0.134 Uiso 1 1 calc R U . . .
C143 C 0.5529(4) 0.6604(3) 0.8322(3) 0.098 Uani 1 1 d G U . . .
C268 C 0.5348(4) 0.7037(3) 0.8352(3) 0.113 Uani 1 1 d G U . . .
H268 H 0.515487 0.713466 0.859361 0.135 Uiso 1 1 calc R U . . .
C148 C 0.2826(6) 0.7066(5) 0.8593(6) 0.102 Uani 1 1 d . U . . .
H148 H 0.271707 0.706881 0.830120 0.122 Uiso 1 1 calc R U . . .
C149 C 0.5420(5) 0.3687(4) 0.8586(4) 0.076 Uani 1 1 d . U . . .
H149 H 0.551342 0.391261 0.879989 0.092 Uiso 1 1 calc R U . . .
C157 C 0.6733(5) 0.4169(5) 0.8183(4) 0.085 Uani 1 1 d . U . . .
H157 H 0.665268 0.401686 0.791422 0.102 Uiso 1 1 calc R U . . .
C163 C 0.3504(5) 0.7027(4) 0.9089(4) 0.076 Uani 1 1 d . U . . .
C165 C 0.7179(6) 0.6595(5) 0.8323(5) 0.097 Uani 1 1 d . U . . .
H165 H 0.701300 0.655311 0.805147 0.116 Uiso 1 1 calc R U . . .
C167 C 0.3324(5) 0.7043(5) 0.8680(4) 0.087 Uani 1 1 d . U . . .
C173 C 0.6846(5) 0.6297(4) 1.1111(4) 0.081 Uani 1 1 d . U . . .
H173 H 0.659736 0.643751 1.128622 0.098 Uiso 1 1 calc R U . . .
C174 C 0.2875(6) 0.6618(5) 1.0464(5) 0.094 Uani 1 1 d . U . . .
C177 C 0.2998(5) 0.5899(4) 1.0102(3) 0.075 Uani 1 1 d . U . . .
H177 H 0.321147 0.566996 0.999129 0.090 Uiso 1 1 calc R U . . .
C181 C 0.6464(5) 0.4538(4) 0.8307(4) 0.084 Uani 1 1 d . U . . .
H181 H 0.619737 0.463143 0.812907 0.101 Uiso 1 1 calc R U . . .
C187 C 0.7578(5) 0.5902(5) 1.0596(4) 0.085 Uani 1 1 d . U . . .
C191 C 0.2720(4) 0.5073(4) 0.8702(3) 0.070 Uani 1 1 d . U . . .
H191 H 0.253763 0.480444 0.862860 0.083 Uiso 1 1 calc R U . . .
C193 C 0.7700(5) 0.6246(5) 1.0899(4) 0.094 Uani 1 1 d . U . . .
H193 H 0.803971 0.634004 1.093819 0.113 Uiso 1 1 calc R U . . .
C203 C 0.2493(5) 0.5856(6) 1.0038(4) 0.091 Uani 1 1 d . U . . .
H203 H 0.235653 0.559324 0.989283 0.109 Uiso 1 1 calc R U . . .
C207 C 0.2730(5) 0.5837(4) 0.8992(3) 0.074 Uani 1 1 d . U . . .
H207 H 0.255531 0.608748 0.911232 0.089 Uiso 1 1 calc R U . . .
C219 C 0.7645(6) 0.6715(5) 0.9103(5) 0.105 Uani 1 1 d . U . . .
C221 C 0.7913(7) 0.6801(6) 0.8742(5) 0.114 Uani 1 1 d . U . . .
H221 H 0.825562 0.689184 0.876484 0.137 Uiso 1 1 calc R U . . .
C228 C 0.2486(4) 0.5440(4) 0.8877(3) 0.072 Uani 1 1 d . U . . .
C230 C 0.7131(5) 0.4000(4) 0.8439(4) 0.076 Uani 1 1 d . U . . .
C231 C 0.3156(6) 0.7032(5) 0.9412(5) 0.098 Uani 1 1 d . U . . .
H231 H 0.326920 0.701221 0.970181 0.118 Uiso 1 1 calc R U . . .
C232 C 0.5179(6) 0.3062(5) 0.7955(4) 0.096 Uani 1 1 d . U . . .
H232 H 0.509649 0.284295 0.773142 0.115 Uiso 1 1 calc R U . . .
C234 C 0.7147(5) 0.6538(5) 0.9091(4) 0.087 Uani 1 1 d . U . . .
C238 C 0.6934(5) 0.6504(5) 0.8690(4) 0.086 Uani 1 1 d . U . . .
H238 H 0.659249 0.641049 0.866560 0.104 Uiso 1 1 calc R U . . .
C262 C 0.5643(6) 0.3074(6) 0.8118(5) 0.112 Uani 1 1 d . U . . .
C267 C 0.5770(5) 0.3391(5) 0.8460(4) 0.095 Uani 1 1 d . U . . .
H267 H 0.609201 0.339289 0.859558 0.114 Uiso 1 1 calc R U . . .
Br3 Br 0.75227(16) 0.69167(13) 1.14977(12) 0.165 Uani 0.42 1 d . U P U 1
Br10 Br 0.80166(12) 0.69047(10) 0.78569(9) 0.154 Uani 0.68 1 d . U P V 1
Br12 Br 0.74831(8) 0.34985(6) 0.82730(6) 0.109 Uani 1 1 d . U . W 1
Br13 Br 0.65498(11) 0.36917(12) 0.68743(9) 0.148 Uani 0.6 1 d . U P X 1
Br14 Br 0.60948(19) 0.2701(2) 0.79004(17) 0.203 Uani 0.19 1 d . U P Y 1
Br15 Br 0.18035(16) 0.71074(17) 0.88165(16) 0.173 Uani 0.34 1 d . U P Z 1
Br17 Br 0.14960(12) 0.61419(17) 1.00960(12) 0.152 Uani 0.34 1 d . U P A 1
Br23 Br 0.17896(6) 0.54023(8) 0.89948(6) 0.124 Uani 1 1 d . U . B 1
Br29 Br 0.59336(16) 0.75654(11) 0.72644(10) 0.220 Uani 1 1 d . U . C 1
Br31 Br 0.61252(17) 0.76859(12) 1.16414(9) 0.241 Uani 1 1 d . U . D 1
P1 P 0.31257(11) 0.55277(8) 0.71390(8) 0.059 Uani 1 1 d . U . . .
C1 C 0.2752(4) 0.5708(4) 0.5892(3) 0.065 Uani 1 1 d . U . . .
H1 H 0.257208 0.591453 0.572888 0.078 Uiso 1 1 calc R U . . .
C10 C 0.3396(4) 0.4215(3) 0.7758(3) 0.066 Uani 1 1 d . U . . .
H10 H 0.344612 0.394212 0.789403 0.079 Uiso 1 1 calc R U . . .
C17 C 0.3785(5) 0.6189(5) 0.6909(4) 0.088 Uani 1 1 d . U . . .
H17 H 0.360401 0.617939 0.664320 0.105 Uiso 1 1 calc R U . . .
C20 C 0.2763(4) 0.5754(3) 0.6329(3) 0.061 Uani 1 1 d . U . . .
H20 H 0.259865 0.599618 0.647614 0.074 Uiso 1 1 calc R U . . .
C29 C 0.3260(5) 0.5045(5) 0.5910(4) 0.090 Uani 1 1 d . U . . .
H29 H 0.341969 0.480056 0.576337 0.108 Uiso 1 1 calc R U . . .
C38 C 0.3800(5) 0.4446(3) 0.7615(4) 0.070 Uani 1 1 d . U . . .
H38 H 0.412947 0.433639 0.765366 0.083 Uiso 1 1 calc R U . . .
C47 C 0.2916(5) 0.4372(4) 0.7708(4) 0.071 Uani 1 1 d . U . . .
H47 H 0.263759 0.420756 0.780934 0.086 Uiso 1 1 calc R U . . .
C62 C 0.3729(4) 0.4844(3) 0.7412(3) 0.062 Uani 1 1 d . U . . .
H62 H 0.400723 0.500127 0.730282 0.075 Uiso 1 1 calc R U . . .
C68 C 0.3028(4) 0.5432(4) 0.6566(3) 0.063 Uani 1 1 d . U . . .
C84 C 0.2569(4) 0.5763(3) 0.7388(3) 0.059 Uani 1 1 d . U . . .
C88 C 0.1683(5) 0.5743(4) 0.7452(4) 0.073 Uani 1 1 d . U . . .
H88 H 0.135944 0.563793 0.735900 0.087 Uiso 1 1 calc R U . . .
C104 C 0.3648(4) 0.5905(4) 0.7227(3) 0.067 Uani 1 1 d . U . . .
C115 C 0.3935(5) 0.5921(4) 0.7603(4) 0.073 Uani 1 1 d . U . . .
H115 H 0.386504 0.571353 0.781577 0.087 Uiso 1 1 calc R U . . .
C119 C 0.3254(4) 0.5005(3) 0.7372(3) 0.062 Uani 1 1 d . U . . .
C131 C 0.2843(5) 0.4755(3) 0.7516(3) 0.068 Uani 1 1 d . U . . .
H131 H 0.251108 0.485984 0.747742 0.082 Uiso 1 1 calc R U . . .
C133 C 0.1737(5) 0.6012(4) 0.7830(4) 0.075 Uani 1 1 d . U . . .
H133 H 0.144710 0.611931 0.797415 0.090 Uiso 1 1 calc R U . . .
C153 C 0.2099(4) 0.5630(3) 0.7214(4) 0.064 Uani 1 1 d . U . . .
H153 H 0.206939 0.546755 0.694315 0.077 Uiso 1 1 calc R U . . .
C175 C 0.3280(5) 0.5091(4) 0.6344(4) 0.080 Uani 1 1 d . U . . .
H175 H 0.346893 0.488572 0.649983 0.096 Uiso 1 1 calc R U . . .
C179 C 0.2618(5) 0.6000(3) 0.7791(4) 0.070 Uani 1 1 d . U . . .
H179 H 0.293910 0.607106 0.791360 0.084 Uiso 1 1 calc R U . . .
C189 C 0.4312(5) 0.6223(4) 0.7677(4) 0.080 Uani 1 1 d . U . . .
H189 H 0.448108 0.624644 0.794872 0.096 Uiso 1 1 calc R U . . .
C199 C 0.2198(5) 0.6123(4) 0.7995(4) 0.076 Uani 1 1 d . U . . .
H199 H 0.222418 0.629186 0.826180 0.092 Uiso 1 1 calc R U . . .
C211 C 0.3009(5) 0.5354(4) 0.5681(4) 0.078 Uani 1 1 d . U . . .
H211 H 0.300819 0.532732 0.537444 0.093 Uiso 1 1 calc R U . . .
C212 C 0.4162(6) 0.6473(5) 0.6973(4) 0.101 Uani 1 1 d . U . . .
H212 H 0.424654 0.666898 0.675341 0.122 Uiso 1 1 calc R U . . .
C240 C 0.4445(5) 0.6491(4) 0.7359(4) 0.084 Uani 1 1 d . U . . .
H240 H 0.472507 0.668951 0.739586 0.101 Uiso 1 1 calc R U . . .
P2 P 1.59958(16) 0.70907(13) 0.35210(13) 0.096 Uani 1 1 d . U . . .
C15 C 1.7272(4) 0.7340(3) 0.2598(3) 0.111 Uani 1 1 d G U . . .
H15 H 1.753371 0.739587 0.240167 0.133 Uiso 1 1 calc R U . . .
C154 C 1.7025(4) 0.6928(3) 0.2579(3) 0.101 Uani 1 1 d G U . . .
H154 H 1.711699 0.670187 0.237031 0.122 Uiso 1 1 calc R U . . .
C87 C 1.6642(3) 0.6847(2) 0.2867(3) 0.083 Uani 1 1 d G U . . .
H87 H 1.647279 0.656522 0.285396 0.099 Uiso 1 1 calc R U . . .
C156 C 1.6507(3) 0.7178(3) 0.3173(3) 0.095 Uani 1 1 d G U . . .
C50 C 1.6754(4) 0.7590(2) 0.3191(3) 0.116 Uani 1 1 d G U . . .
H50 H 1.666199 0.781658 0.340033 0.139 Uiso 1 1 calc R U . . .
C158 C 1.7137(4) 0.7671(2) 0.2904(3) 0.125 Uani 1 1 d G U . . .
H158 H 1.730620 0.795324 0.291669 0.150 Uiso 1 1 calc R U . . .
C37 C 1.4653(8) 0.7834(6) 0.3013(6) 0.130 Uani 1 1 d . U . . .
H37 H 1.436933 0.799814 0.292668 0.156 Uiso 1 1 calc R U . . .
C63 C 1.5573(4) 0.5617(3) 0.3627(3) 0.102 Uani 1 1 d G U . . .
H63 H 1.547866 0.531295 0.365320 0.123 Uiso 1 1 calc R U . . .
C67 C 1.5864(4) 0.5840(3) 0.3947(3) 0.113 Uani 1 1 d G U . . .
H67 H 1.596987 0.568738 0.419204 0.136 Uiso 1 1 calc R U . . .
C233 C 1.6002(4) 0.6285(3) 0.3908(3) 0.109 Uani 1 1 d G U . . .
H233 H 1.620109 0.643697 0.412715 0.131 Uiso 1 1 calc R U . . .
C190 C 1.5847(4) 0.6508(2) 0.3550(3) 0.096 Uani 1 1 d G U . . .
C105 C 1.5555(4) 0.6285(3) 0.3230(2) 0.101 Uani 1 1 d G U . . .
H105 H 1.544991 0.643772 0.298456 0.121 Uiso 1 1 calc R U . . .
C223 C 1.5418(4) 0.5840(3) 0.3268(3) 0.107 Uani 1 1 d G U . . .
H223 H 1.521868 0.568813 0.304945 0.128 Uiso 1 1 calc R U . . .
C74 C 1.4999(7) 0.7239(7) 0.3403(5) 0.120 Uani 1 1 d . U . . .
H74 H 1.494670 0.698194 0.356403 0.143 Uiso 1 1 calc R U . . .
C83 C 1.5865(6) 0.7456(4) 0.4787(5) 0.097 Uani 1 1 d . U . . .
H83 H 1.559002 0.748404 0.497774 0.117 Uiso 1 1 calc R U . . .
C107 C 1.6636(6) 0.7323(4) 0.4204(5) 0.094 Uani 1 1 d . U . . .
H107 H 1.690349 0.725541 0.401271 0.113 Uiso 1 1 calc R U . . .
C120 C 1.5531(7) 0.7711(5) 0.3036(5) 0.119 Uani 1 1 d . U . . .
H120 H 1.586452 0.778157 0.295487 0.143 Uiso 1 1 calc R U . . .
C150 C 1.6158(6) 0.7294(4) 0.4056(5) 0.092 Uani 1 1 d . U . . .
C162 C 1.6745(6) 0.7452(4) 0.4639(5) 0.096 Uani 1 1 d . U . . .
H162 H 1.708286 0.750048 0.473435 0.115 Uiso 1 1 calc R U . . .
C164 C 1.6344(6) 0.7508(5) 0.4934(5) 0.099 Uani 1 1 d . U . . .
H164 H 1.641039 0.758197 0.523077 0.118 Uiso 1 1 calc R U . . .
C188 C 1.5788(6) 0.7360(4) 0.4350(4) 0.092 Uani 1 1 d . U . . .
H188 H 1.545101 0.733969 0.424670 0.110 Uiso 1 1 calc R U . . .
C194 C 1.4582(8) 0.7498(6) 0.3258(5) 0.121 Uani 1 1 d . U . . .
H194 H 1.425092 0.742271 0.334199 0.145 Uiso 1 1 calc R U . . .
C236 C 1.5451(7) 0.7373(6) 0.3306(5) 0.104 Uani 1 1 d . U . . .
C237 C 1.5125(8) 0.7961(6) 0.2873(6) 0.137 Uani 1 1 d . U . . .
H237 H 1.517355 0.819663 0.268342 0.164 Uiso 1 1 calc R U . . .
P3 P 1.14906(15) 0.83922(11) 0.53350(14) 0.092 Uani 1 1 d . U . . .
C11 C 1.2612(6) 0.7650(5) 0.4467(6) 0.106 Uani 1 1 d . U . . .
H11 H 1.284120 0.749009 0.428689 0.127 Uiso 1 1 calc R U . . .
C33 C 1.1053(6) 0.7544(5) 0.6437(6) 0.100 Uani 1 1 d . U . . .
H33 H 1.095942 0.737779 0.667560 0.120 Uiso 1 1 calc R U . . .
C76 C 1.0209(4) 0.8916(3) 0.4934(4) 0.127 Uani 1 1 d G U . . .
H76 H 0.997682 0.913003 0.504360 0.153 Uiso 1 1 calc R U . . .
C253 C 1.0128(4) 0.8704(4) 0.4529(4) 0.125 Uani 1 1 d G U . . .
H253 H 0.984111 0.877268 0.436262 0.150 Uiso 1 1 calc R U . . .
C136 C 1.0468(5) 0.8390(4) 0.4369(3) 0.126 Uani 1 1 d G U . . .
H136 H 1.041292 0.824532 0.409204 0.151 Uiso 1 1 calc R U . . .
C255 C 1.0888(4) 0.8289(3) 0.4612(4) 0.114 Uani 1 1 d G U . . .
H255 H 1.112043 0.807529 0.450244 0.137 Uiso 1 1 calc R U . . .
C42 C 1.0969(4) 0.8502(4) 0.5017(4) 0.111 Uani 1 1 d G U . . .
C257 C 1.0629(5) 0.8815(3) 0.5178(3) 0.117 Uani 1 1 d G U . . .
H257 H 1.068435 0.896000 0.545400 0.141 Uiso 1 1 calc R U . . .
C78 C 1.2002(4) 0.9742(3) 0.5943(4) 0.118 Uani 1 1 d G U . . .
H78 H 1.209832 1.002824 0.606528 0.142 Uiso 1 1 calc R U . . .
C260 C 1.1798(5) 0.9424(4) 0.6202(3) 0.125 Uani 1 1 d G U . . .
H260 H 1.175389 0.949254 0.650159 0.150 Uiso 1 1 calc R U . . .
C139 C 1.1657(4) 0.9004(3) 0.6024(3) 0.115 Uani 1 1 d G U . . .
H139 H 1.151694 0.878694 0.620070 0.138 Uiso 1 1 calc R U . . .
C261 C 1.1721(4) 0.8903(3) 0.5586(4) 0.109 Uani 1 1 d G U . . .
C4 C 1.1925(4) 0.9222(3) 0.5326(3) 0.112 Uani 1 1 d G U . . .
H4 H 1.196883 0.915271 0.502718 0.135 Uiso 1 1 calc R U . . .
C263 C 1.2066(4) 0.9641(3) 0.5505(4) 0.123 Uani 1 1 d G U . . .
H263 H 1.220579 0.985832 0.532806 0.148 Uiso 1 1 calc R U . . .
C91 C 1.2040(6) 0.7669(5) 0.5049(6) 0.102 Uani 1 1 d . U . . .
H91 H 1.189424 0.751245 0.527524 0.122 Uiso 1 1 calc R U . . .
C128 C 1.0831(6) 0.7859(5) 0.5781(6) 0.103 Uani 1 1 d . U . . .
H128 H 1.058266 0.790684 0.556671 0.123 Uiso 1 1 calc R U . . .
C137 C 1.2528(6) 0.8097(5) 0.4433(6) 0.110 Uani 1 1 d . U . . .
H137 H 1.269153 0.825076 0.421397 0.132 Uiso 1 1 calc R U . . .
C160 C 1.2344(6) 0.7453(5) 0.4775(6) 0.105 Uani 1 1 d . U . . .
H160 H 1.237486 0.713935 0.479611 0.126 Uiso 1 1 calc R U . . .
C166 C 1.1682(6) 0.7952(5) 0.6054(5) 0.101 Uani 1 1 d . U . . .
H166 H 1.201990 0.804681 0.601628 0.121 Uiso 1 1 calc R U . . .
C176 C 1.0706(6) 0.7603(4) 0.6129(5) 0.096 Uani 1 1 d . U . . .
H176 H 1.037981 0.747292 0.614798 0.115 Uiso 1 1 calc R U . . .
C186 C 1.1556(6) 0.7716(4) 0.6427(6) 0.099 Uani 1 1 d . U . . .
H186 H 1.179086 0.767608 0.665316 0.119 Uiso 1 1 calc R U . . .
C198 C 1.2216(6) 0.8327(5) 0.4706(6) 0.107 Uani 1 1 d . U . . .
H198 H 1.219156 0.864088 0.468595 0.129 Uiso 1 1 calc R U . . .
C248 C 1.1930(6) 0.8118(5) 0.5014(6) 0.102 Uani 1 1 d . U . . .
C269 C 1.1314(6) 0.8049(5) 0.5738(6) 0.102 Uani 1 1 d . U . . .
P4 P 0.81736(13) 0.53726(12) 0.79504(10) 0.081 Uani 1 1 d . U . . .
C14 C 0.8901(5) 0.5842(4) 0.7523(4) 0.080 Uani 1 1 d . U . . .
H14 H 0.878350 0.568007 0.726921 0.096 Uiso 1 1 calc R U . . .
C48 C 0.7920(6) 0.4576(5) 0.7507(4) 0.095 Uani 1 1 d . U . . .
H48 H 0.758085 0.465832 0.755503 0.114 Uiso 1 1 calc R U . . .
C54 C 0.8307(5) 0.4910(6) 0.8660(5) 0.101 Uani 1 1 d . U . . .
H54 H 0.846848 0.470286 0.846734 0.121 Uiso 1 1 calc R U . . .
C58 C 0.6706(2) 0.5579(3) 0.7696(3) 0.108 Uani 1 1 d G U . . .
H58 H 0.639101 0.550099 0.781411 0.130 Uiso 1 1 calc R U . . .
C152 C 0.7149(3) 0.5459(3) 0.7897(2) 0.092 Uani 1 1 d G U . . .
H152 H 0.713729 0.529971 0.815305 0.110 Uiso 1 1 calc R U . . .
C183 C 0.7609(3) 0.5573(3) 0.7724(2) 0.079 Uani 1 1 d G U . . .
C209 C 0.7626(3) 0.5807(3) 0.7349(2) 0.094 Uani 1 1 d G U . . .
H209 H 0.794032 0.588475 0.723101 0.113 Uiso 1 1 calc R U . . .
C96 C 0.7183(3) 0.5926(3) 0.7148(2) 0.095 Uani 1 1 d G U . . .
H96 H 0.719405 0.608603 0.689206 0.114 Uiso 1 1 calc R U . . .
C185 C 0.6722(3) 0.5812(3) 0.7321(3) 0.101 Uani 1 1 d G U . . .
H185 H 0.641939 0.589416 0.718361 0.122 Uiso 1 1 calc R U . . .
C65 C 0.8297(6) 0.4820(6) 0.9104(5) 0.114 Uani 1 1 d . U . . .
H65 H 0.845721 0.456594 0.920980 0.136 Uiso 1 1 calc R U . . .
C85 C 0.8021(7) 0.4174(5) 0.7300(4) 0.103 Uani 1 1 d . U . . .
H85 H 0.775091 0.397836 0.721123 0.123 Uiso 1 1 calc R U . . .
C97 C 0.9432(5) 0.6394(5) 0.7848(4) 0.098 Uani 1 1 d . U . . .
H97 H 0.966598 0.663206 0.781974 0.117 Uiso 1 1 calc R U . . .
C103 C 0.8503(6) 0.4049(5) 0.7219(4) 0.100 Uani 1 1 d . U . . .
H103 H 0.856913 0.377327 0.706553 0.120 Uiso 1 1 calc R U . . .
C155 C 0.8683(5) 0.5760(4) 0.7907(4) 0.080 Uani 1 1 d . U . . .
C178 C 0.8054(6) 0.5106(6) 0.9366(5) 0.111 Uani 1 1 d . U . . .
H178 H 0.801138 0.504026 0.965981 0.133 Uiso 1 1 calc R U . . .
C192 C 0.8895(6) 0.4331(5) 0.7366(4) 0.098 Uani 1 1 d . U . . .
H192 H 0.923165 0.423662 0.732582 0.117 Uiso 1 1 calc R U . . .
C195 C 0.8111(5) 0.5253(5) 0.8504(4) 0.080 Uani 1 1 d . U . . .
C197 C 0.7877(5) 0.5560(5) 0.8792(4) 0.085 Uani 1 1 d . U . . .
H197 H 0.772669 0.581590 0.868139 0.102 Uiso 1 1 calc R U . . .
C205 C 0.8304(5) 0.4864(4) 0.7648(4) 0.084 Uani 1 1 d . U . . .
C213 C 0.9283(5) 0.6147(5) 0.7488(4) 0.090 Uani 1 1 d . U . . .
H213 H 0.944021 0.618568 0.721958 0.108 Uiso 1 1 calc R U . . .
C239 C 0.8874(6) 0.6009(5) 0.8291(5) 0.107 Uani 1 1 d . U . . .
H239 H 0.872765 0.595621 0.856087 0.129 Uiso 1 1 calc R U . . .
C244 C 0.8806(6) 0.4748(5) 0.7569(4) 0.096 Uani 1 1 d . U . . .
H244 H 0.907531 0.494752 0.765227 0.116 Uiso 1 1 calc R U . . .
C258 C 0.9246(6) 0.6308(6) 0.8278(5) 0.121 Uani 1 1 d . U . . .
H258 H 0.938195 0.645699 0.853136 0.145 Uiso 1 1 calc R U . . .
C275 C 0.7857(5) 0.5506(6) 0.9217(4) 0.096 Uani 1 1 d . U . . .
H275 H 0.771614 0.572677 0.940856 0.115 Uiso 1 1 calc R U . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt1 Ag1 2.7346(6) 2_766 ?
Pt1 Ag1 2.7346(6) . ?
Pt1 Ag4 2.7393(6) . ?
Pt1 Ag4 2.7393(6) 2_766 ?
Pt1 Ag6 2.7491(6) . ?
Pt1 Ag6 2.7493(6) 2_766 ?
Pt1 Ag8 2.7538(5) 2_766 ?
Pt1 Ag8 2.7537(6) . ?
Pt1 Ag10 2.7387(6) . ?
Pt1 Ag10 2.7387(6) 2_766 ?
Pt1 Ag17 2.7488(6) 2_766 ?
Pt1 Ag17 2.7488(6) . ?
Ag1 Ag4 2.8472(9) . ?
Ag1 Ag6 2.9077(9) 2_766 ?
Ag1 Ag8 2.9389(9) . ?
Ag1 Ag10 2.8574(8) 2_766 ?
Ag1 Ag17 2.8621(8) 2_766 ?
Ag1 Ag28 2.9518(8) . ?
Ag1 S4 2.447(2) . ?
Ag4 Ag6 2.9183(8) . ?
Ag4 Ag8 2.8885(9) . ?
Ag4 Ag10 2.8730(9) . ?
Ag4 Ag17 2.9024(9) 2_766 ?
Ag4 Ag28 3.1091(9) . ?
Ag4 Ag32 3.1025(10) . ?
Ag4 S1 2.491(2) . ?
Ag6 Ag8 2.8791(9) 2_766 ?
Ag6 Ag9 3.0268(10) . ?
Ag6 Ag10 2.8502(9) . ?
Ag6 Ag17 2.8800(9) 2_766 ?
Ag6 S10 2.455(2) . ?
Ag8 Ag10 2.9076(8) . ?
Ag8 Ag11 3.1375(9) . ?
Ag8 Ag17 2.8498(8) . ?
Ag8 Ag29 3.3464(11) . ?
Ag8 S12 2.486(2) . ?
Ag9 Ag10 3.2917(10) . ?
Ag9 Ag32 3.0388(10) . ?
Ag9 S6 2.639(3) . ?
Ag9 S10 2.455(3) . ?
Ag9 S21 2.492(3) . ?
Ag10 Ag17 2.9198(9) . ?
Ag10 Ag27 3.0605(10) . ?
Ag10 S6 2.466(2) . ?
Ag11 Ag28 3.0113(11) . ?
Ag11 S12 2.537(3) . ?
Ag11 S18 2.529(3) . ?
Ag11 S20 2.435(3) . ?
Ag17 Ag29 3.1025(10) . ?
Ag17 S22 2.445(3) . ?
Ag27 Ag29 3.0586(12) . ?
Ag27 S5 2.442(3) . ?
Ag27 S6 2.482(2) . ?
Ag27 S18 2.549(3) . ?
Ag28 S1 2.549(2) . ?
Ag28 S4 2.508(2) . ?
Ag28 S20 2.537(2) . ?
Ag29 S5 2.484(3) . ?
Ag29 S12 2.580(3) . ?
Ag29 S22 2.435(3) . ?
Ag32 S1 2.484(3) . ?
Ag32 S18 2.553(3) . ?
Ag32 S21 2.436(3) . ?
Cl4 C24 1.664(12) . ?
Cl5 C201 1.784(13) . ?
Cl6 C222 1.609(9) . ?
Cl7 C123 1.744(12) . ?
Cl21 C2 1.849(11) . ?
Cl23 C215 1.717(16) . ?
Cl27 C79 1.776(11) . ?
Cl33 C61 1.796(7) . ?
Cl37 C127 1.689(12) . ?
S1 C12 1.809(11) . ?
S4 C7 1.751(9) . ?
S5 C98 1.736(12) . ?
S6 C3 1.765(9) . ?
S10 C224 1.784(6) . ?
S12 C70 1.761(10) . ?
S18 C27 1.770(11) . ?
S20 C102 1.765(10) . ?
S21 C171 1.754(7) . ?
S22 C44 1.760(11) . ?
C2 C75 1.400(16) . ?
C2 C92 1.331(16) . ?
C3 C31 1.395(14) . ?
C3 C36 1.392(12) . ?
C7 C24 1.414(12) . ?
C7 C60 1.388(13) . ?
C8 H8 0.9500 . ?
C8 C242 1.377(17) . ?
C8 C246 1.393(19) . ?
C12 C18 1.379(14) . ?
C12 C22 1.354(14) . ?
C18 H18 0.9500 . ?
C18 C34 1.360(16) . ?
C22 H22 0.9500 . ?
C22 C66 1.389(15) . ?
C24 C64 1.386(15) . ?
C27 C90 1.402(17) . ?
C27 C125 1.362(17) . ?
C30 C126 1.3900 . ?
C30 C235 1.3900 . ?
C30 Br2 1.907(7) . ?
C126 H126 0.9500 . ?
C126 C28 1.3900 . ?
C28 H28 0.9500 . ?
C28 C171 1.3900 . ?
C171 C61 1.3900 . ?
C61 C235 1.3900 . ?
C235 H235 0.9500 . ?
C31 H31 0.9500 . ?
C31 C72 1.393(15) . ?
C34 H34 0.9500 . ?
C34 C159 1.377(18) . ?
C36 H36 0.9500 . ?
C36 C40 1.376(15) . ?
C40 H40 0.9500 . ?
C40 C81 1.413(17) . ?
C44 C53 1.398(15) . ?
C44 C123 1.387(14) . ?
C46 H46 0.9500 . ?
C46 C125 1.415(16) . ?
C46 C196 1.43(2) . ?
C53 H53 0.9500 . ?
C53 C75 1.405(15) . ?
C55 H55 0.9500 . ?
C55 C60 1.385(14) . ?
C55 C79 1.345(15) . ?
C59 H59 0.9500 . ?
C59 C201 1.32(2) . ?
C59 C215 1.379(18) . ?
C60 H60 0.9500 . ?
C64 H64 0.9500 . ?
C64 C79 1.381(17) . ?
C66 H66 0.9500 . ?
C66 C159 1.390(17) . ?
C70 C151 1.409(15) . ?
C70 C242 1.394(16) . ?
C72 H72 0.9500 . ?
C72 C81 1.425(15) . ?
C75 H75 0.9500 . ?
C81 Br22 1.865(12) . ?
C90 H90 0.9500 . ?
C90 C265 1.362(16) . ?
C92 H92 0.9500 . ?
C92 C123 1.361(16) . ?
C94 H94 0.9500 . ?
C94 C106 1.399(16) . ?
C94 C169 1.378(14) . ?
C98 C110 1.415(17) . ?
C98 C215 1.395(18) . ?
C102 C127 1.408(14) . ?
C102 C169 1.395(15) . ?
C106 C112 1.358(16) . ?
C106 Br24 1.847(10) . ?
C110 H110 0.9500 . ?
C110 C161 1.426(16) . ?
C112 H112 0.9500 . ?
C112 C127 1.403(15) . ?
C117 H117 0.9500 . ?
C117 C151 1.427(16) . ?
C117 C246 1.287(18) . ?
C125 H125 0.9500 . ?
C151 H151 0.9500 . ?
C159 Br21 1.872(12) . ?
C161 H161 0.9500 . ?
C161 C201 1.468(19) . ?
C169 H169 0.9500 . ?
C196 C265 1.30(2) . ?
C196 Br28 1.924(13) . ?
C217 H217 0.9500 . ?
C217 C25 1.3900 . ?
C217 C226 1.3900 . ?
C25 C220 1.3900 . ?
C25 Br1 1.800(6) . ?
C220 H220 0.9500 . ?
C220 C222 1.3900 . ?
C222 C224 1.3900 . ?
C224 C226 1.3900 . ?
C226 H226 0.9500 . ?
C242 H242 0.9500 . ?
C246 Br27 1.902(13) . ?
C265 H265 0.9500 . ?
Pt2 Ag13 2.7282(7) 2_876 ?
Pt2 Ag13 2.7281(7) . ?
Pt2 Ag14 2.7449(8) . ?
Pt2 Ag14 2.7449(8) 2_876 ?
Pt2 Ag21 2.7537(7) . ?
Pt2 Ag21 2.7537(7) 2_876 ?
Pt2 Ag23 2.7407(9) 2_876 ?
Pt2 Ag23 2.7408(9) . ?
Pt2 Ag25 2.7599(8) . ?
Pt2 Ag25 2.7599(8) 2_876 ?
Pt2 Ag30 2.7473(6) 2_876 ?
Pt2 Ag30 2.7472(6) . ?
Ag2 Ag20 3.0085(14) . ?
Ag2 Ag23 3.0536(11) . ?
Ag2 Ag30 3.2390(13) . ?
Ag2 S2 2.613(3) . ?
Ag2 S7 2.498(4) . ?
Ag2 S23 2.449(3) . ?
Ag7 Ag13 3.0201(9) . ?
Ag7 Ag21 3.1885(10) . ?
Ag7 Ag31 2.9847(14) . ?
Ag7 S9 2.468(3) . ?
Ag7 S15 2.619(3) . ?
Ag7 S28 2.517(3) . ?
Ag13 Ag14 2.8919(12) 2_876 ?
Ag13 Ag21 2.8469(10) . ?
Ag13 Ag23 2.8809(10) 2_876 ?
Ag13 Ag25 2.8855(9) 2_876 ?
Ag13 Ag30 2.9038(12) . ?
Ag13 S9 2.444(3) . ?
Ag14 Ag21 2.8956(8) . ?
Ag14 Ag23 2.8864(12) 2_876 ?
Ag14 Ag25 2.8431(12) . ?
Ag14 Ag30 2.8914(10) 2_876 ?
Ag14 Ag36 3.1259(13) . ?
Ag14 S25 2.447(3) . ?
Ag20 Ag25 3.1316(12) . ?
Ag20 S3 2.480(3) . ?
Ag20 S7 2.425(6) . ?
Ag20 S11 2.555(4) . ?
Ag21 Ag23 2.8906(11) 2_876 ?
Ag21 Ag25 2.9055(12) . ?
Ag21 Ag30 2.9168(12) . ?
Ag21 Ag35 3.1793(11) . ?
Ag21 S15 2.481(3) . ?
Ag23 Ag25 2.9188(11) . ?
Ag23 Ag30 2.8363(9) . ?
Ag23 S23 2.443(4) . ?
Ag25 Ag30 2.9149(10) . ?
Ag25 Ag36 3.3549(14) . ?
Ag25 S3 2.496(3) . ?
Ag30 Ag31 3.0874(9) . ?
Ag30 S2 2.483(3) . ?
Ag31 S2 2.440(3) . ?
Ag31 S11 2.566(3) . ?
Ag31 S28 2.412(3) . ?
Ag35 Ag36 2.9974(11) . ?
Ag35 S11 2.549(4) . ?
Ag35 S15 2.477(3) . ?
Ag35 S29 2.432(5) . ?
Ag36 S3 2.615(4) . ?
Ag36 S25 2.451(3) . ?
Ag36 S29 2.483(4) . ?
Cl3 C21 1.788(6) . ?
Cl8 C35 1.649(15) . ?
Cl11 C243 1.715(7) . ?
Cl15 C270 1.959(19) . ?
Cl17 C180 1.619(9) . ?
Cl19 C146 1.863(8) . ?
Cl25 C256 1.574(13) . ?
Cl26 C272 1.986(17) . ?
Cl29 C132 1.593(11) . ?
Cl31 C147 1.745(10) . ?
Cl32 C184 1.770(6) . ?
Cl34 C245 1.706(6) . ?
Cl35 C113 1.755(10) . ?
S2 C9 1.776(6) . ?
S3 C118 1.778(8) . ?
S7 C274 1.737(10) . ?
S9 C56 1.822(7) . ?
S11 C254 1.758(6) . ?
S15 C69 1.782(8) . ?
S23 C251 1.794(7) . ?
S25 C210 1.790(10) . ?
S28 C130 1.789(5) . ?
S29 C145 1.643(16) . ?
C39 H39 0.9500 . ?
C39 C241 1.3900 . ?
C39 C245 1.3900 . ?
C241 H241 0.9500 . ?
C241 C130 1.3900 . ?
C130 C243 1.3900 . ?
C243 C73 1.3900 . ?
C73 H73 0.9500 . ?
C73 C245 1.3900 . ?
C45 H45 0.9500 . ?
C45 C270 1.3900 . ?
C45 C272 1.3900 . ?
C270 C145 1.3900 . ?
C145 C271 1.3900 . ?
C271 H271 0.9500 . ?
C271 C82 1.3900 . ?
C82 H82 0.9500 . ?
C82 C272 1.3900 . ?
C93 H93 0.9500 . ?
C93 C168 1.3900 . ?
C93 C172 1.3900 . ?
C168 H168 0.9500 . ?
C168 C9 1.3900 . ?
C9 C170 1.3900 . ?
C170 H170 0.9500 . ?
C170 C95 1.3900 . ?
C95 H95 0.9500 . ?
C95 C172 1.3900 . ?
C172 Br11 1.876(5) . ?
C99 H99 0.9500 . ?
C99 C180 1.3900 . ?
C99 C184 1.3900 . ?
C180 C56 1.3900 . ?
C56 C182 1.3900 . ?
C182 H182 0.9500 . ?
C182 C101 1.3900 . ?
C101 H101 0.9500 . ?
C101 C184 1.3900 . ?
C132 C247 1.3900 . ?
C132 C251 1.3900 . ?
C247 H247 0.9500 . ?
C247 C21 1.3900 . ?
C21 C249 1.3900 . ?
C249 H249 0.9500 . ?
C249 C134 1.3900 . ?
C134 H134 0.9500 . ?
C134 C251 1.3900 . ?
C146 C273 1.3900 . ?
C146 C276 1.3900 . ?
C273 H273 0.9500 . ?
C273 C23 1.3900 . ?
C23 H23 0.9500 . ?
C23 C274 1.3900 . ?
C274 C147 1.3900 . ?
C147 C276 1.3900 . ?
C276 H276 0.9500 . ?
C206 H206 0.9500 . ?
C206 C113 1.3900 . ?
C206 C114 1.3900 . ?
C113 C208 1.3900 . ?
C208 H208 0.9500 . ?
C208 C35 1.3900 . ?
C35 C210 1.3900 . ?
C210 C114 1.3900 . ?
C114 H114 0.9500 . ?
C214 H214 0.9500 . ?
C214 C116 1.3900 . ?
C214 C118 1.3900 . ?
C116 H116 0.9500 . ?
C116 C216 1.3900 . ?
C216 C19 1.3900 . ?
C216 Br26 1.874(8) . ?
C19 H19 0.9500 . ?
C19 C218 1.3900 . ?
C218 H218 0.9500 . ?
C218 C118 1.3900 . ?
C225 C122 1.3900 . ?
C225 C124 1.3900 . ?
C225 Br20 1.873(7) . ?
C122 H122 0.9500 . ?
C122 C227 1.3900 . ?
C227 H227 0.9500 . ?
C227 C69 1.3900 . ?
C69 C229 1.3900 . ?
C229 H229 0.9500 . ?
C229 C124 1.3900 . ?
C124 H124 0.9500 . ?
C250 H250 0.9500 . ?
C250 C252 1.3900 . ?
C250 C259 1.3900 . ?
C252 H252 0.9500 . ?
C252 C254 1.3900 . ?
C254 C256 1.3900 . ?
C256 C32 1.3900 . ?
C32 H32 0.9500 . ?
C32 C259 1.3900 . ?
C259 Br19 1.832(6) . ?
Pt3 Ag12 2.7237(6) . ?
Pt3 Ag12 2.7237(6) 2_667 ?
Pt3 Ag15 2.7484(6) 2_667 ?
Pt3 Ag15 2.7483(6) . ?
Pt3 Ag19 2.7368(6) . ?
Pt3 Ag19 2.7368(6) 2_667 ?
Pt3 Ag22 2.7557(7) 2_667 ?
Pt3 Ag22 2.7558(7) . ?
Pt3 Ag24 2.7356(7) . ?
Pt3 Ag24 2.7357(7) 2_667 ?
Pt3 Ag26 2.7639(7) . ?
Pt3 Ag26 2.7640(7) 2_667 ?
Ag3 Ag12 3.0615(10) . ?
Ag3 Ag33 3.0512(11) . ?
Ag3 S13 2.455(3) . ?
Ag3 S16 2.508(2) . ?
Ag3 S26 2.542(3) . ?
Ag5 Ag19 3.0393(10) . ?
Ag5 Ag34 3.0071(10) . ?
Ag5 S8 2.504(3) . ?
Ag5 S19 2.440(3) . ?
Ag5 S26 2.549(3) . ?
Ag12 Ag15 2.8373(10) . ?
Ag12 Ag19 2.8919(10) . ?
Ag12 Ag22 2.8602(9) 2_667 ?
Ag12 Ag24 2.9065(9) . ?
Ag12 Ag26 2.9129(9) . ?
Ag12 Ag34 3.2811(9) . ?
Ag12 S16 2.463(2) . ?
Ag15 Ag19 2.9208(9) . ?
Ag15 Ag22 2.9003(10) 2_667 ?
Ag15 Ag24 2.8370(9) 2_667 ?
Ag15 Ag26 2.9127(10) 2_667 ?
Ag15 Ag34 2.9798(10) . ?
Ag15 S14 2.464(2) . ?
Ag16 Ag18 2.9840(14) . ?
Ag16 Ag19 3.1008(10) . ?
Ag16 Ag22 2.9708(10) . ?
Ag16 S8 2.536(2) . ?
Ag16 S24 2.485(3) . ?
Ag16 S27 2.528(3) . ?
Ag18 Ag24 2.9769(10) . ?
Ag18 S26 2.537(3) . ?
Ag18 S27 2.432(4) . ?
Ag18 S30 2.531(3) . ?
Ag19 Ag22 2.8457(9) . ?
Ag19 Ag24 2.9321(10) . ?
Ag19 Ag26 2.8742(10) 2_667 ?
Ag19 S8 2.496(2) . ?
Ag22 Ag24 2.9414(11) . ?
Ag22 Ag26 2.8702(9) 2_667 ?
Ag22 S24 2.456(3) . ?
Ag24 Ag26 2.8383(10) . ?
Ag24 S30 2.481(3) . ?
Ag26 Ag33 3.0980(11) . ?
Ag26 S17 2.449(3) . ?
Ag33 S13 2.474(3) . ?
Ag33 S17 2.441(3) . ?
Ag33 S30 2.588(3) . ?
Ag34 S14 2.469(3) . ?
Ag34 S16 2.636(3) . ?
Ag34 S19 2.506(3) . ?
Cl1 C219 1.785(19) . ?
Cl16 C100 1.702(12) . ?
Cl18 C174 1.713(17) . ?
Cl20 C144 1.760(9) . ?
Cl22 C129 1.816(12) . ?
Cl24 C6 1.859(16) . ?
Cl30 C89 1.814(14) . ?
Cl36 C167 1.706(16) . ?
Cl39 C187 1.634(15) . ?
S8 C41 1.764(12) . ?
S13 C163 1.782(13) . ?
S14 C77 1.785(11) . ?
S16 C16 1.782(11) . ?
S17 C57 1.753(12) . ?
S19 C135 1.763(7) . ?
S24 C51 1.788(11) . ?
S26 C143 1.762(6) . ?
S27 C234 1.735(13) . ?
S30 C204 1.794(6) . ?
C6 C71 1.42(2) . ?
C6 C148 1.29(2) . ?
C13 H13 0.9500 . ?
C13 C41 1.377(16) . ?
C13 C121 1.347(16) . ?
C16 C49 1.400(14) . ?
C16 C86 1.359(15) . ?
C26 H26 0.9500 . ?
C26 C89 1.36(2) . ?
C26 C174 1.36(2) . ?
C41 C181 1.378(14) . ?
C49 H49 0.9500 . ?
C49 C191 1.424(15) . ?
C51 C108 1.328(16) . ?
C51 C187 1.436(15) . ?
C52 C165 1.40(2) . ?
C52 C221 1.37(2) . ?
C52 Br10 1.849(14) . ?
C57 C174 1.415(17) . ?
C57 C177 1.412(16) . ?
C71 H71 0.9500 . ?
C71 C231 1.38(2) . ?
C77 C100 1.433(14) . ?
C77 C149 1.373(16) . ?
C86 H86 0.9500 . ?
C86 C207 1.385(16) . ?
C89 C203 1.43(2) . ?
C100 C232 1.358(17) . ?
C108 H108 0.9500 . ?
C108 C173 1.411(15) . ?
C109 H109 0.9500 . ?
C109 C200 1.3900 . ?
C109 C204 1.3900 . ?
C200 H200 0.9500 . ?
C200 C5 1.3900 . ?
C5 C202 1.3900 . ?
C5 Br31 1.866(6) . ?
C202 H202 0.9500 . ?
C202 C111 1.3900 . ?
C111 H111 0.9500 . ?
C111 C204 1.3900 . ?
C121 H121 0.9500 . ?
C121 C230 1.390(15) . ?
C129 C173 1.394(18) . ?
C129 C193 1.33(2) . ?
C135 C43 1.3900 . ?
C135 C144 1.3900 . ?
C43 H43 0.9500 . ?
C43 C138 1.3900 . ?
C138 H138 0.9500 . ?
C138 C140 1.3900 . ?
C140 C142 1.3900 . ?
C140 Br13 1.961(8) . ?
C142 H142 0.9500 . ?
C142 C144 1.3900 . ?
C141 H141 0.9500 . ?
C141 C264 1.3900 . ?
C141 C268 1.3900 . ?
C264 C80 1.3900 . ?
C264 Br29 1.836(6) . ?
C80 H80 0.9500 . ?
C80 C266 1.3900 . ?
C266 H266 0.9500 . ?
C266 C143 1.3900 . ?
C143 C268 1.3900 . ?
C268 H268 0.9500 . ?
C148 H148 0.9500 . ?
C148 C167 1.352(19) . ?
C149 H149 0.9500 . ?
C149 C267 1.342(17) . ?
C157 H157 0.9500 . ?
C157 C181 1.365(18) . ?
C157 C230 1.431(18) . ?
C163 C167 1.356(17) . ?
C163 C231 1.374(19) . ?
C165 H165 0.9500 . ?
C165 C238 1.359(18) . ?
C173 H173 0.9500 . ?
C177 H177 0.9500 . ?
C177 C203 1.361(17) . ?
C181 H181 0.9500 . ?
C187 C193 1.389(18) . ?
C191 H191 0.9500 . ?
C191 C228 1.364(17) . ?
C193 H193 0.9500 . ?
C203 H203 0.9500 . ?
C207 H207 0.9500 . ?
C207 C228 1.377(16) . ?
C219 C221 1.371(19) . ?
C219 C234 1.421(18) . ?
C221 H221 0.9500 . ?
C228 Br23 1.897(11) . ?
C230 Br12 1.836(13) . ?
C231 H231 0.9500 . ?
C232 H232 0.9500 . ?
C232 C262 1.33(2) . ?
C234 C238 1.358(18) . ?
C238 H238 0.9500 . ?
C262 C267 1.421(18) . ?
C262 Br14 1.769(15) . ?
C267 H267 0.9500 . ?
P1 C68 1.802(10) . ?
P1 C84 1.815(12) . ?
P1 C104 1.788(10) . ?
P1 C119 1.794(10) . ?
C1 H1 0.9500 . ?
C1 C20 1.359(14) . ?
C1 C211 1.407(17) . ?
C10 H10 0.9500 . ?
C10 C38 1.364(16) . ?
C10 C47 1.378(16) . ?
C17 H17 0.9500 . ?
C17 C104 1.388(15) . ?
C17 C212 1.313(16) . ?
C20 H20 0.9500 . ?
C20 C68 1.434(14) . ?
C29 H29 0.9500 . ?
C29 C175 1.346(17) . ?
C29 C211 1.374(18) . ?
C38 H38 0.9500 . ?
C38 C62 1.390(14) . ?
C47 H47 0.9500 . ?
C47 C131 1.338(15) . ?
C62 H62 0.9500 . ?
C62 C119 1.367(15) . ?
C68 C175 1.386(16) . ?
C84 C153 1.403(14) . ?
C84 C179 1.406(14) . ?
C88 H88 0.9500 . ?
C88 C133 1.391(16) . ?
C88 C153 1.376(17) . ?
C104 C115 1.388(14) . ?
C115 H115 0.9500 . ?
C115 C189 1.349(14) . ?
C119 C131 1.411(16) . ?
C131 H131 0.9500 . ?
C133 H133 0.9500 . ?
C133 C199 1.355(17) . ?
C153 H153 0.9500 . ?
C175 H175 0.9500 . ?
C179 H179 0.9500 . ?
C179 C199 1.337(17) . ?
C189 H189 0.9500 . ?
C189 C240 1.355(16) . ?
C199 H199 0.9500 . ?
C211 H211 0.9500 . ?
C212 H212 0.9500 . ?
C212 C240 1.406(17) . ?
C240 H240 0.9500 . ?
P2 C156 1.774(10) . ?
P2 C190 1.792(8) . ?
P2 C150 1.786(12) . ?
P2 C236 1.829(16) . ?
C15 H15 0.9500 . ?
C15 C154 1.3900 . ?
C15 C158 1.3900 . ?
C154 H154 0.9500 . ?
C154 C87 1.3900 . ?
C87 H87 0.9500 . ?
C87 C156 1.3900 . ?
C156 C50 1.3900 . ?
C50 H50 0.9500 . ?
C50 C158 1.3900 . ?
C158 H158 0.9500 . ?
C37 H37 0.9500 . ?
C37 C194 1.31(3) . ?
C37 C237 1.39(3) . ?
C63 H63 0.9500 . ?
C63 C67 1.3900 . ?
C63 C223 1.3900 . ?
C67 H67 0.9500 . ?
C67 C233 1.3900 . ?
C233 H233 0.9500 . ?
C233 C190 1.3900 . ?
C190 C105 1.3900 . ?
C105 H105 0.9500 . ?
C105 C223 1.3900 . ?
C223 H223 0.9500 . ?
C74 H74 0.9500 . ?
C74 C194 1.44(2) . ?
C74 C236 1.31(2) . ?
C83 H83 0.9500 . ?
C83 C164 1.35(2) . ?
C83 C188 1.384(18) . ?
C107 H107 0.9500 . ?
C107 C150 1.349(18) . ?
C107 C162 1.411(18) . ?
C120 H120 0.9500 . ?
C120 C236 1.36(2) . ?
C120 C237 1.43(2) . ?
C150 C188 1.36(2) . ?
C162 H162 0.9500 . ?
C162 C164 1.42(2) . ?
C164 H164 0.9500 . ?
C188 H188 0.9500 . ?
C194 H194 0.9500 . ?
C237 H237 0.9500 . ?
P3 C42 1.741(10) . ?
P3 C261 1.778(8) . ?
P3 C248 1.734(17) . ?
P3 C269 1.726(17) . ?
C11 H11 0.9500 . ?
C11 C137 1.37(2) . ?
C11 C160 1.36(2) . ?
C33 H33 0.9500 . ?
C33 C176 1.34(2) . ?
C33 C186 1.43(2) . ?
C76 H76 0.9500 . ?
C76 C253 1.3900 . ?
C76 C257 1.3900 . ?
C253 H253 0.9500 . ?
C253 C136 1.3900 . ?
C136 H136 0.9500 . ?
C136 C255 1.3900 . ?
C255 H255 0.9500 . ?
C255 C42 1.3900 . ?
C42 C257 1.3900 . ?
C257 H257 0.9500 . ?
C78 H78 0.9500 . ?
C78 C260 1.3900 . ?
C78 C263 1.3900 . ?
C260 H260 0.9500 . ?
C260 C139 1.3900 . ?
C139 H139 0.9500 . ?
C139 C261 1.3900 . ?
C261 C4 1.3900 . ?
C4 H4 0.9500 . ?
C4 C263 1.3900 . ?
C263 H263 0.9500 . ?
C91 H91 0.9500 . ?
C91 C160 1.33(2) . ?
C91 C248 1.39(2) . ?
C128 H128 0.9500 . ?
C128 C176 1.40(2) . ?
C128 C269 1.41(2) . ?
C137 H137 0.9500 . ?
C137 C198 1.36(2) . ?
C160 H160 0.9500 . ?
C166 H166 0.9500 . ?
C166 C186 1.43(2) . ?
C166 C269 1.42(2) . ?
C176 H176 0.9500 . ?
C186 H186 0.9500 . ?
C198 H198 0.9500 . ?
C198 C248 1.40(2) . ?
P4 C183 1.779(8) . ?
P4 C155 1.783(11) . ?
P4 C195 1.784(12) . ?
P4 C205 1.786(14) . ?
C14 H14 0.9500 . ?
C14 C155 1.366(15) . ?
C14 C213 1.367(15) . ?
C48 H48 0.9500 . ?
C48 C85 1.365(19) . ?
C48 C205 1.382(17) . ?
C54 H54 0.9500 . ?
C54 C65 1.42(2) . ?
C54 C195 1.27(2) . ?
C58 H58 0.9500 . ?
C58 C152 1.3900 . ?
C58 C185 1.3900 . ?
C152 H152 0.9500 . ?
C152 C183 1.3900 . ?
C183 C209 1.3900 . ?
C209 H209 0.9500 . ?
C209 C96 1.3900 . ?
C96 H96 0.9500 . ?
C96 C185 1.3900 . ?
C185 H185 0.9500 . ?
C65 H65 0.9500 . ?
C65 C178 1.33(2) . ?
C85 H85 0.9500 . ?
C85 C103 1.37(2) . ?
C97 H97 0.9500 . ?
C97 C213 1.358(17) . ?
C97 C258 1.463(19) . ?
C103 H103 0.9500 . ?
C103 C192 1.392(19) . ?
C155 C239 1.456(17) . ?
C178 H178 0.9500 . ?
C178 C275 1.41(2) . ?
C192 H192 0.9500 . ?
C192 C244 1.397(19) . ?
C195 C197 1.404(18) . ?
C197 H197 0.9500 . ?
C197 C275 1.337(17) . ?
C205 C244 1.41(2) . ?
C213 H213 0.9500 . ?
C239 H239 0.9500 . ?
C239 C258 1.328(18) . ?
C244 H244 0.9500 . ?
C258 H258 0.9500 . ?
C275 H275 0.9500 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Ag1 Pt1 Ag1 180.0 2_766 . ?
Ag1 Pt1 Ag4 62.684(18) 2_766 2_766 ?
Ag1 Pt1 Ag4 117.316(18) . 2_766 ?
Ag1 Pt1 Ag4 62.683(18) . . ?
Ag1 Pt1 Ag4 117.317(18) 2_766 . ?
Ag1 Pt1 Ag6 64.040(19) 2_766 . ?
Ag1 Pt1 Ag6 64.040(19) . 2_766 ?
Ag1 Pt1 Ag6 115.959(19) 2_766 2_766 ?
Ag1 Pt1 Ag6 115.961(19) . . ?
Ag1 Pt1 Ag8 64.752(19) 2_766 2_766 ?
Ag1 Pt1 Ag8 115.247(19) 2_766 . ?
Ag1 Pt1 Ag8 64.752(19) . . ?
Ag1 Pt1 Ag8 115.250(19) . 2_766 ?
Ag1 Pt1 Ag10 117.061(18) . . ?
Ag1 Pt1 Ag10 62.942(17) . 2_766 ?
Ag1 Pt1 Ag10 117.059(17) 2_766 2_766 ?
Ag1 Pt1 Ag10 62.938(17) 2_766 . ?
Ag1 Pt1 Ag17 117.073(18) . . ?
Ag1 Pt1 Ag17 62.927(18) . 2_766 ?
Ag1 Pt1 Ag17 117.074(18) 2_766 2_766 ?
Ag1 Pt1 Ag17 62.926(18) 2_766 . ?
Ag4 Pt1 Ag4 180.0 . 2_766 ?
Ag4 Pt1 Ag6 115.759(17) . 2_766 ?
Ag4 Pt1 Ag6 64.240(17) 2_766 2_766 ?
Ag4 Pt1 Ag6 115.759(17) 2_766 . ?
Ag4 Pt1 Ag6 64.242(17) . . ?
Ag4 Pt1 Ag8 63.450(18) 2_766 2_766 ?
Ag4 Pt1 Ag8 116.552(18) . 2_766 ?
Ag4 Pt1 Ag8 116.548(18) 2_766 . ?
Ag4 Pt1 Ag8 63.450(18) . . ?
Ag4 Pt1 Ag17 63.855(19) . 2_766 ?
Ag4 Pt1 Ag17 63.855(19) 2_766 . ?
Ag4 Pt1 Ag17 116.146(19) 2_766 2_766 ?
Ag4 Pt1 Ag17 116.144(19) . . ?
Ag6 Pt1 Ag6 179.999(15) . 2_766 ?
Ag6 Pt1 Ag8 63.093(18) 2_766 . ?
Ag6 Pt1 Ag8 116.906(18) 2_766 2_766 ?
Ag6 Pt1 Ag8 63.093(18) . 2_766 ?
Ag6 Pt1 Ag8 116.907(18) . . ?
Ag8 Pt1 Ag8 180.0 . 2_766 ?
Ag10 Pt1 Ag4 116.737(19) 2_766 . ?
Ag10 Pt1 Ag4 63.265(19) . . ?
Ag10 Pt1 Ag4 63.263(19) 2_766 2_766 ?
Ag10 Pt1 Ag4 116.735(19) . 2_766 ?
Ag10 Pt1 Ag6 117.420(19) . 2_766 ?
Ag10 Pt1 Ag6 117.420(19) 2_766 . ?
Ag10 Pt1 Ag6 62.579(19) . . ?
Ag10 Pt1 Ag6 62.580(19) 2_766 2_766 ?
Ag10 Pt1 Ag8 63.928(18) . . ?
Ag10 Pt1 Ag8 63.926(18) 2_766 2_766 ?
Ag10 Pt1 Ag8 116.074(18) 2_766 . ?
Ag10 Pt1 Ag8 116.072(18) . 2_766 ?
Ag10 Pt1 Ag10 180.0 . 2_766 ?
Ag10 Pt1 Ag17 64.295(19) 2_766 2_766 ?
Ag10 Pt1 Ag17 115.706(19) . 2_766 ?
Ag10 Pt1 Ag17 115.706(19) 2_766 . ?
Ag10 Pt1 Ag17 64.293(19) . . ?
Ag17 Pt1 Ag6 63.180(19) 2_766 . ?
Ag17 Pt1 Ag6 116.82(2) 2_766 2_766 ?
Ag17 Pt1 Ag6 116.82(2) . . ?
Ag17 Pt1 Ag6 63.180(19) . 2_766 ?
Ag17 Pt1 Ag8 117.616(18) 2_766 . ?
Ag17 Pt1 Ag8 62.386(18) 2_766 2_766 ?
Ag17 Pt1 Ag8 117.614(18) . 2_766 ?
Ag17 Pt1 Ag8 62.384(18) . . ?
Ag17 Pt1 Ag17 180.0 2_766 . ?
Pt1 Ag1 Ag4 58.739(17) . . ?
Pt1 Ag1 Ag6 58.224(17) . 2_766 ?
Pt1 Ag1 Ag8 57.938(16) . . ?
Pt1 Ag1 Ag10 58.600(17) . 2_766 ?
Pt1 Ag1 Ag17 58.778(17) . 2_766 ?
Pt1 Ag1 Ag28 120.27(3) . . ?
Ag4 Ag1 Ag6 107.75(3) . 2_766 ?
Ag4 Ag1 Ag8 59.87(2) . . ?
Ag4 Ag1 Ag10 109.69(2) . 2_766 ?
Ag4 Ag1 Ag17 61.11(2) . 2_766 ?
Ag4 Ag1 Ag28 64.81(2) . . ?
Ag6 Ag1 Ag8 59.00(2) 2_766 . ?
Ag6 Ag1 Ag28 130.27(3) 2_766 . ?
Ag8 Ag1 Ag28 78.48(2) . . ?
Ag10 Ag1 Ag6 59.25(2) 2_766 2_766 ?
Ag10 Ag1 Ag8 107.00(3) 2_766 . ?
Ag10 Ag1 Ag17 61.40(2) 2_766 2_766 ?
Ag10 Ag1 Ag28 169.47(3) 2_766 . ?
Ag17 Ag1 Ag6 108.52(2) 2_766 2_766 ?
Ag17 Ag1 Ag8 108.46(3) 2_766 . ?
Ag17 Ag1 Ag28 108.55(3) 2_766 . ?
S4 Ag1 Pt1 167.49(6) . . ?
S4 Ag1 Ag4 111.36(6) . . ?
S4 Ag1 Ag6 134.28(6) . 2_766 ?
S4 Ag1 Ag8 125.85(6) . . ?
S4 Ag1 Ag10 124.16(6) . 2_766 ?
S4 Ag1 Ag17 110.55(6) . 2_766 ?
S4 Ag1 Ag28 54.39(6) . . ?
Pt1 Ag4 Ag1 58.578(17) . . ?
Pt1 Ag4 Ag6 58.042(16) . . ?
Pt1 Ag4 Ag8 58.518(17) . . ?
Pt1 Ag4 Ag10 58.357(17) . . ?
Pt1 Ag4 Ag17 58.231(17) . 2_766 ?
Pt1 Ag4 Ag28 114.85(2) . . ?
Pt1 Ag4 Ag32 139.48(3) . . ?
Ag1 Ag4 Ag6 107.49(2) . . ?
Ag1 Ag4 Ag8 61.64(2) . . ?
Ag1 Ag4 Ag10 109.39(3) . . ?
Ag1 Ag4 Ag17 59.70(2) . 2_766 ?
Ag1 Ag4 Ag28 59.22(2) . . ?
Ag1 Ag4 Ag32 152.81(3) . . ?
Ag6 Ag4 Ag28 162.73(3) . . ?
Ag6 Ag4 Ag32 99.45(2) . . ?
Ag8 Ag4 Ag6 107.73(3) . . ?
Ag8 Ag4 Ag17 108.75(3) . 2_766 ?
Ag8 Ag4 Ag28 76.73(2) . . ?
Ag8 Ag4 Ag32 106.93(3) . . ?
Ag10 Ag4 Ag6 58.96(2) . . ?
Ag10 Ag4 Ag8 60.62(2) . . ?
Ag10 Ag4 Ag17 107.12(2) . 2_766 ?
Ag10 Ag4 Ag28 133.41(3) . . ?
Ag10 Ag4 Ag32 81.32(2) . . ?
Ag17 Ag4 Ag6 59.31(2) 2_766 . ?
Ag17 Ag4 Ag28 103.42(3) 2_766 . ?
Ag17 Ag4 Ag32 142.69(3) 2_766 . ?
Ag32 Ag4 Ag28 94.96(2) . . ?
S1 Ag4 Pt1 167.33(6) . . ?
S1 Ag4 Ag1 108.85(6) . . ?
S1 Ag4 Ag6 132.73(6) . . ?
S1 Ag4 Ag8 115.69(6) . . ?
S1 Ag4 Ag10 130.70(6) . . ?
S1 Ag4 Ag17 118.63(6) . 2_766 ?
S1 Ag4 Ag28 52.76(6) . . ?
S1 Ag4 Ag32 51.33(6) . . ?
Pt1 Ag6 Ag1 57.737(17) . 2_766 ?
Pt1 Ag6 Ag4 57.716(16) . . ?
Pt1 Ag6 Ag8 58.532(17) . 2_766 ?
Pt1 Ag6 Ag9 123.99(3) . . ?
Pt1 Ag6 Ag10 58.531(17) . . ?
Pt1 Ag6 Ag17 58.404(18) . 2_766 ?
Ag1 Ag6 Ag4 106.74(3) 2_766 . ?
Ag1 Ag6 Ag9 108.26(3) 2_766 . ?
Ag4 Ag6 Ag9 82.40(2) . . ?
Ag8 Ag6 Ag1 61.04(2) 2_766 2_766 ?
Ag8 Ag6 Ag4 107.40(3) 2_766 . ?
Ag8 Ag6 Ag9 166.87(3) 2_766 . ?
Ag8 Ag6 Ag17 59.32(2) 2_766 2_766 ?
Ag10 Ag6 Ag1 59.49(2) . 2_766 ?
Ag10 Ag6 Ag4 59.73(2) . . ?
Ag10 Ag6 Ag8 108.84(3) . 2_766 ?
Ag10 Ag6 Ag9 68.05(2) . . ?
Ag10 Ag6 Ag17 108.35(3) . 2_766 ?
Ag17 Ag6 Ag1 107.83(3) 2_766 2_766 ?
Ag17 Ag6 Ag4 60.07(2) 2_766 . ?
Ag17 Ag6 Ag9 133.74(3) 2_766 . ?
S10 Ag6 Pt1 169.53(7) . . ?
S10 Ag6 Ag1 112.87(6) . 2_766 ?
S10 Ag6 Ag4 126.30(6) . . ?
S10 Ag6 Ag8 122.87(6) . 2_766 ?
S10 Ag6 Ag9 51.94(6) . . ?
S10 Ag6 Ag10 113.70(7) . . ?
S10 Ag6 Ag17 131.94(7) . 2_766 ?
Pt1 Ag8 Ag1 57.310(16) . . ?
Pt1 Ag8 Ag4 58.032(16) . . ?
Pt1 Ag8 Ag6 58.378(16) . 2_766 ?
Pt1 Ag8 Ag10 57.785(16) . . ?
Pt1 Ag8 Ag11 142.18(3) . . ?
Pt1 Ag8 Ag17 58.724(17) . . ?
Pt1 Ag8 Ag29 115.77(2) . . ?
Ag1 Ag8 Ag11 101.45(3) . . ?
Ag1 Ag8 Ag29 162.92(3) . . ?
Ag4 Ag8 Ag1 58.49(2) . . ?
Ag4 Ag8 Ag10 59.43(2) . . ?
Ag4 Ag8 Ag11 84.36(2) . . ?
Ag4 Ag8 Ag29 133.88(3) . . ?
Ag6 Ag8 Ag1 59.96(2) 2_766 . ?
Ag6 Ag8 Ag4 107.41(3) 2_766 . ?
Ag6 Ag8 Ag10 108.28(2) 2_766 . ?
Ag6 Ag8 Ag11 142.22(3) 2_766 . ?
Ag6 Ag8 Ag29 102.96(3) 2_766 . ?
Ag10 Ag8 Ag1 105.97(3) . . ?
Ag10 Ag8 Ag11 108.52(3) . . ?
Ag10 Ag8 Ag29 78.59(2) . . ?
Ag11 Ag8 Ag29 92.37(3) . . ?
Ag17 Ag8 Ag1 107.79(2) . . ?
Ag17 Ag8 Ag4 108.53(2) . . ?
Ag17 Ag8 Ag6 60.36(2) . 2_766 ?
Ag17 Ag8 Ag10 60.94(2) . . ?
Ag17 Ag8 Ag11 150.63(3) . . ?
Ag17 Ag8 Ag29 59.45(2) . . ?
S12 Ag8 Pt1 164.57(6) . . ?
S12 Ag8 Ag1 134.23(6) . . ?
S12 Ag8 Ag4 134.43(6) . . ?
S12 Ag8 Ag6 115.30(6) . 2_766 ?
S12 Ag8 Ag10 117.24(6) . . ?
S12 Ag8 Ag11 52.07(6) . . ?
S12 Ag8 Ag17 105.85(6) . . ?
S12 Ag8 Ag29 49.88(6) . . ?
Ag6 Ag9 Ag10 53.43(2) . . ?
Ag6 Ag9 Ag32 98.50(3) . . ?
Ag32 Ag9 Ag10 75.88(2) . . ?
S6 Ag9 Ag6 98.32(6) . . ?
S6 Ag9 Ag10 47.59(5) . . ?
S6 Ag9 Ag32 81.04(5) . . ?
S10 Ag9 Ag6 51.94(6) . . ?
S10 Ag9 Ag10 100.37(6) . . ?
S10 Ag9 Ag32 136.63(7) . . ?
S10 Ag9 S6 128.46(8) . . ?
S10 Ag9 S21 138.10(10) . . ?
S21 Ag9 Ag6 146.40(8) . . ?
S21 Ag9 Ag10 118.76(8) . . ?
S21 Ag9 Ag32 51.11(7) . . ?
S21 Ag9 S6 91.15(10) . . ?
Pt1 Ag10 Ag1 58.461(17) . 2_766 ?
Pt1 Ag10 Ag4 58.379(17) . . ?
Pt1 Ag10 Ag6 58.890(18) . . ?
Pt1 Ag10 Ag8 58.287(17) . . ?
Pt1 Ag10 Ag9 115.24(3) . . ?
Pt1 Ag10 Ag17 58.021(18) . . ?
Pt1 Ag10 Ag27 140.74(3) . . ?
Ag1 Ag10 Ag4 109.35(3) 2_766 . ?
Ag1 Ag10 Ag8 107.03(3) 2_766 . ?
Ag1 Ag10 Ag9 102.69(2) 2_766 . ?
Ag1 Ag10 Ag17 59.38(2) 2_766 . ?
Ag1 Ag10 Ag27 141.76(3) 2_766 . ?
Ag4 Ag10 Ag8 59.95(2) . . ?
Ag4 Ag10 Ag9 78.57(2) . . ?
Ag4 Ag10 Ag17 107.04(3) . . ?
Ag4 Ag10 Ag27 107.43(3) . . ?
Ag6 Ag10 Ag1 61.25(2) . 2_766 ?
Ag6 Ag10 Ag4 61.31(2) . . ?
Ag6 Ag10 Ag8 109.07(3) . . ?
Ag6 Ag10 Ag9 58.52(2) . . ?
Ag6 Ag10 Ag17 108.51(3) . . ?
Ag6 Ag10 Ag27 151.42(3) . . ?
Ag8 Ag10 Ag9 134.85(3) . . ?
Ag8 Ag10 Ag17 58.55(2) . . ?
Ag8 Ag10 Ag27 82.67(2) . . ?
Ag17 Ag10 Ag9 162.05(3) . . ?
Ag17 Ag10 Ag27 99.86(3) . . ?
Ag27 Ag10 Ag9 94.44(3) . . ?
S6 Ag10 Pt1 166.36(6) . . ?
S6 Ag10 Ag1 115.75(6) . 2_766 ?
S6 Ag10 Ag4 117.91(6) . . ?
S6 Ag10 Ag6 107.51(6) . . ?
S6 Ag10 Ag8 133.20(6) . . ?
S6 Ag10 Ag9 52.19(6) . . ?
S6 Ag10 Ag17 131.85(7) . . ?
S6 Ag10 Ag27 52.02(6) . . ?
Ag28 Ag11 Ag8 74.58(2) . . ?
S12 Ag11 Ag8 50.63(5) . . ?
S12 Ag11 Ag28 117.00(6) . . ?
S18 Ag11 Ag8 88.89(5) . . ?
S18 Ag11 Ag28 110.50(6) . . ?
S18 Ag11 S12 98.30(9) . . ?
S20 Ag11 Ag8 116.05(6) . . ?
S20 Ag11 Ag28 54.28(6) . . ?
S20 Ag11 S12 121.59(9) . . ?
S20 Ag11 S18 140.10(9) . . ?
Pt1 Ag17 Ag1 58.295(18) . 2_766 ?
Pt1 Ag17 Ag4 57.914(18) . 2_766 ?
Pt1 Ag17 Ag6 58.418(18) . 2_766 ?
Pt1 Ag17 Ag8 58.892(18) . . ?
Pt1 Ag17 Ag10 57.685(18) . . ?
Pt1 Ag17 Ag29 124.30(3) . . ?
Ag1 Ag17 Ag4 59.19(2) 2_766 2_766 ?
Ag1 Ag17 Ag6 108.14(3) 2_766 2_766 ?
Ag1 Ag17 Ag10 59.22(2) 2_766 . ?
Ag1 Ag17 Ag29 132.90(3) 2_766 . ?
Ag4 Ag17 Ag10 106.47(3) 2_766 . ?
Ag4 Ag17 Ag29 167.83(3) 2_766 . ?
Ag6 Ag17 Ag4 60.62(2) 2_766 2_766 ?
Ag6 Ag17 Ag10 107.91(3) 2_766 . ?
Ag6 Ag17 Ag29 109.24(3) 2_766 . ?
Ag8 Ag17 Ag1 108.48(3) . 2_766 ?
Ag8 Ag17 Ag4 108.63(3) . 2_766 ?
Ag8 Ag17 Ag6 60.32(2) . 2_766 ?
Ag8 Ag17 Ag10 60.51(2) . . ?
Ag8 Ag17 Ag29 68.27(2) . . ?
Ag10 Ag17 Ag29 82.56(3) . . ?
S22 Ag17 Pt1 167.30(7) . . ?
S22 Ag17 Ag1 134.36(7) . 2_766 ?
S22 Ag17 Ag4 124.41(7) . 2_766 ?
S22 Ag17 Ag6 110.59(7) . 2_766 ?
S22 Ag17 Ag8 111.14(7) . . ?
S22 Ag17 Ag10 126.44(7) . . ?
S22 Ag17 Ag29 50.38(7) . . ?
Ag29 Ag27 Ag10 81.03(3) . . ?
S5 Ag27 Ag10 131.78(8) . . ?
S5 Ag27 Ag29 52.23(8) . . ?
S5 Ag27 S6 141.29(9) . . ?
S5 Ag27 S18 115.71(9) . . ?
S6 Ag27 Ag10 51.56(6) . . ?
S6 Ag27 Ag29 121.01(6) . . ?
S6 Ag27 S18 101.77(8) . . ?
S18 Ag27 Ag10 91.65(6) . . ?
S18 Ag27 Ag29 113.92(6) . . ?
Ag1 Ag28 Ag4 55.966(19) . . ?
Ag1 Ag28 Ag11 104.20(3) . . ?
Ag11 Ag28 Ag4 82.86(2) . . ?
S1 Ag28 Ag1 104.16(5) . . ?
S1 Ag28 Ag4 51.07(5) . . ?
S1 Ag28 Ag11 85.36(6) . . ?
S4 Ag28 Ag1 52.49(5) . . ?
S4 Ag28 Ag4 101.89(5) . . ?
S4 Ag28 Ag11 139.57(6) . . ?
S4 Ag28 S1 128.93(8) . . ?
S4 Ag28 S20 114.54(8) . . ?
S20 Ag28 Ag1 130.35(6) . . ?
S20 Ag28 Ag4 133.97(7) . . ?
S20 Ag28 Ag11 51.19(7) . . ?
S20 Ag28 S1 113.76(8) . . ?
Ag17 Ag29 Ag8 52.28(2) . . ?
Ag27 Ag29 Ag8 75.85(3) . . ?
Ag27 Ag29 Ag17 95.97(3) . . ?
S5 Ag29 Ag8 119.74(8) . . ?
S5 Ag29 Ag17 143.09(7) . . ?
S5 Ag29 Ag27 51.00(8) . . ?
S5 Ag29 S12 95.45(9) . . ?
S12 Ag29 Ag8 47.47(5) . . ?
S12 Ag29 Ag17 96.79(6) . . ?
S12 Ag29 Ag27 84.00(6) . . ?
S22 Ag29 Ag8 97.04(7) . . ?
S22 Ag29 Ag17 50.67(6) . . ?
S22 Ag29 Ag27 135.06(7) . . ?
S22 Ag29 S5 139.24(10) . . ?
S22 Ag29 S12 123.80(9) . . ?
Ag9 Ag32 Ag4 79.24(2) . . ?
S1 Ag32 Ag4 51.51(5) . . ?
S1 Ag32 Ag9 120.00(6) . . ?
S1 Ag32 S18 95.53(8) . . ?
S18 Ag32 Ag4 90.00(6) . . ?
S18 Ag32 Ag9 119.09(6) . . ?
S21 Ag32 Ag4 130.85(8) . . ?
S21 Ag32 Ag9 52.76(7) . . ?
S21 Ag32 S1 142.97(11) . . ?
S21 Ag32 S18 120.13(11) . . ?
Ag4 S1 Ag28 76.17(6) . . ?
Ag32 S1 Ag4 77.16(7) . . ?
Ag32 S1 Ag28 130.89(10) . . ?
C12 S1 Ag4 101.0(3) . . ?
C12 S1 Ag28 111.6(4) . . ?
C12 S1 Ag32 113.5(4) . . ?
Ag1 S4 Ag28 73.12(7) . . ?
C7 S4 Ag1 106.9(3) . . ?
C7 S4 Ag28 107.8(3) . . ?
Ag27 S5 Ag29 76.77(8) . . ?
C98 S5 Ag27 105.8(4) . . ?
C98 S5 Ag29 110.1(4) . . ?
Ag10 S6 Ag9 80.23(7) . . ?
Ag10 S6 Ag27 76.42(7) . . ?
Ag27 S6 Ag9 131.28(10) . . ?
C3 S6 Ag9 116.3(3) . . ?
C3 S6 Ag10 105.2(3) . . ?
C3 S6 Ag27 110.9(3) . . ?
Ag6 S10 Ag9 76.12(7) . . ?
C224 S10 Ag6 110.0(3) . . ?
C224 S10 Ag9 107.4(3) . . ?
Ag8 S12 Ag11 77.30(7) . . ?
Ag8 S12 Ag29 82.65(6) . . ?
Ag11 S12 Ag29 132.36(10) . . ?
C70 S12 Ag8 103.0(3) . . ?
C70 S12 Ag11 113.4(4) . . ?
C70 S12 Ag29 113.1(4) . . ?
Ag11 S18 Ag27 110.11(10) . . ?
Ag11 S18 Ag32 112.37(10) . . ?
Ag27 S18 Ag32 104.32(8) . . ?
C27 S18 Ag11 112.3(3) . . ?
C27 S18 Ag27 109.3(4) . . ?
C27 S18 Ag32 108.1(4) . . ?
Ag11 S20 Ag28 74.53(6) . . ?
C102 S20 Ag11 108.1(4) . . ?
C102 S20 Ag28 106.3(3) . . ?
Ag32 S21 Ag9 76.13(9) . . ?
C171 S21 Ag9 110.6(3) . . ?
C171 S21 Ag32 107.9(3) . . ?
Ag29 S22 Ag17 78.94(8) . . ?
C44 S22 Ag17 111.4(4) . . ?
C44 S22 Ag29 108.0(4) . . ?
C75 C2 Cl21 118.1(10) . . ?
C92 C2 Cl21 121.2(9) . . ?
C92 C2 C75 120.8(11) . . ?
C31 C3 S6 120.1(7) . . ?
C36 C3 S6 120.6(8) . . ?
C36 C3 C31 119.2(9) . . ?
C24 C7 S4 120.4(8) . . ?
C60 C7 S4 123.0(7) . . ?
C60 C7 C24 116.2(9) . . ?
C242 C8 H8 120.1 . . ?
C242 C8 C246 119.7(13) . . ?
C246 C8 H8 120.1 . . ?
C18 C12 S1 118.5(9) . . ?
C22 C12 S1 120.4(8) . . ?
C22 C12 C18 120.6(10) . . ?
C12 C18 H18 120.1 . . ?
C34 C18 C12 119.8(12) . . ?
C34 C18 H18 120.1 . . ?
C12 C22 H22 119.7 . . ?
C12 C22 C66 120.5(11) . . ?
C66 C22 H22 119.7 . . ?
C7 C24 Cl4 121.8(9) . . ?
C64 C24 Cl4 117.5(8) . . ?
C64 C24 C7 120.7(11) . . ?
C90 C27 S18 120.1(9) . . ?
C125 C27 S18 120.3(10) . . ?
C125 C27 C90 119.6(11) . . ?
C126 C30 C235 120.0 . . ?
C126 C30 Br2 112.6(4) . . ?
C235 C30 Br2 127.4(4) . . ?
C30 C126 H126 120.0 . . ?
C28 C126 C30 120.0 . . ?
C28 C126 H126 120.0 . . ?
C126 C28 H28 120.0 . . ?
C126 C28 C171 120.0 . . ?
C171 C28 H28 120.0 . . ?
C28 C171 S21 122.7(4) . . ?
C61 C171 S21 117.1(4) . . ?
C61 C171 C28 120.0 . . ?
C171 C61 Cl33 119.2(4) . . ?
C171 C61 C235 120.0 . . ?
C235 C61 Cl33 120.6(4) . . ?
C30 C235 H235 120.0 . . ?
C61 C235 C30 120.0 . . ?
C61 C235 H235 120.0 . . ?
C3 C31 H31 119.2 . . ?
C72 C31 C3 121.7(9) . . ?
C72 C31 H31 119.2 . . ?
C18 C34 H34 119.7 . . ?
C18 C34 C159 120.6(12) . . ?
C159 C34 H34 119.7 . . ?
C3 C36 H36 119.2 . . ?
C40 C36 C3 121.6(10) . . ?
C40 C36 H36 119.2 . . ?
C36 C40 H40 120.7 . . ?
C36 C40 C81 118.7(9) . . ?
C81 C40 H40 120.7 . . ?
C53 C44 S22 121.2(8) . . ?
C123 C44 S22 121.4(9) . . ?
C123 C44 C53 117.1(10) . . ?
C125 C46 H46 121.6 . . ?
C125 C46 C196 116.8(13) . . ?
C196 C46 H46 121.6 . . ?
C44 C53 H53 119.1 . . ?
C44 C53 C75 121.7(11) . . ?
C75 C53 H53 119.1 . . ?
C60 C55 H55 119.4 . . ?
C79 C55 H55 119.4 . . ?
C79 C55 C60 121.3(11) . . ?
C201 C59 H59 119.2 . . ?
C201 C59 C215 121.7(15) . . ?
C215 C59 H59 119.2 . . ?
C7 C60 H60 119.1 . . ?
C55 C60 C7 121.8(9) . . ?
C55 C60 H60 119.1 . . ?
C24 C64 H64 119.6 . . ?
C79 C64 C24 120.9(10) . . ?
C79 C64 H64 119.6 . . ?
C22 C66 H66 120.6 . . ?
C22 C66 C159 118.8(12) . . ?
C159 C66 H66 120.6 . . ?
C151 C70 S12 120.9(9) . . ?
C242 C70 S12 120.3(9) . . ?
C242 C70 C151 118.7(11) . . ?
C31 C72 H72 121.2 . . ?
C31 C72 C81 117.6(11) . . ?
C81 C72 H72 121.2 . . ?
C2 C75 C53 117.3(11) . . ?
C2 C75 H75 121.4 . . ?
C53 C75 H75 121.4 . . ?
C55 C79 Cl27 121.6(10) . . ?
C55 C79 C64 119.0(10) . . ?
C64 C79 Cl27 119.2(9) . . ?
C40 C81 C72 120.8(11) . . ?
C40 C81 Br22 121.2(8) . . ?
C72 C81 Br22 117.8(10) . . ?
C27 C90 H90 120.1 . . ?
C265 C90 C27 119.8(14) . . ?
C265 C90 H90 120.1 . . ?
C2 C92 H92 119.0 . . ?
C2 C92 C123 122.0(11) . . ?
C123 C92 H92 119.0 . . ?
C106 C94 H94 120.4 . . ?
C169 C94 H94 120.4 . . ?
C169 C94 C106 119.2(11) . . ?
C110 C98 S5 121.3(10) . . ?
C215 C98 S5 123.0(11) . . ?
C215 C98 C110 115.6(12) . . ?
C127 C102 S20 118.9(8) . . ?
C169 C102 S20 123.3(8) . . ?
C169 C102 C127 117.8(9) . . ?
C94 C106 Br24 120.8(9) . . ?
C112 C106 C94 120.0(10) . . ?
C112 C106 Br24 119.1(9) . . ?
C98 C110 H110 118.3 . . ?
C98 C110 C161 123.5(12) . . ?
C161 C110 H110 118.2 . . ?
C106 C112 H112 119.4 . . ?
C106 C112 C127 121.3(10) . . ?
C127 C112 H112 119.4 . . ?
C151 C117 H117 120.0 . . ?
C246 C117 H117 120.0 . . ?
C246 C117 C151 120.1(13) . . ?
C44 C123 Cl7 117.4(9) . . ?
C92 C123 Cl7 121.5(9) . . ?
C92 C123 C44 121.1(11) . . ?
C27 C125 C46 120.3(13) . . ?
C27 C125 H125 119.9 . . ?
C46 C125 H125 119.9 . . ?
C102 C127 Cl37 121.5(8) . . ?
C112 C127 Cl37 119.0(8) . . ?
C112 C127 C102 119.5(10) . . ?
C70 C151 C117 119.0(12) . . ?
C70 C151 H151 120.5 . . ?
C117 C151 H151 120.5 . . ?
C34 C159 C66 119.8(12) . . ?
C34 C159 Br21 121.3(10) . . ?
C66 C159 Br21 118.8(10) . . ?
C110 C161 H161 122.4 . . ?
C110 C161 C201 115.1(13) . . ?
C201 C161 H161 122.4 . . ?
C94 C169 C102 122.2(10) . . ?
C94 C169 H169 118.9 . . ?
C102 C169 H169 118.9 . . ?
C46 C196 Br28 115.6(12) . . ?
C265 C196 C46 121.7(13) . . ?
C265 C196 Br28 122.6(13) . . ?
C59 C201 Cl5 124.5(12) . . ?
C59 C201 C161 121.0(13) . . ?
C161 C201 Cl5 114.5(12) . . ?
C59 C215 Cl23 119.3(12) . . ?
C59 C215 C98 123.0(14) . . ?
C98 C215 Cl23 117.7(11) . . ?
C25 C217 H217 120.0 . . ?
C25 C217 C226 120.0 . . ?
C226 C217 H217 120.0 . . ?
C217 C25 Br1 124.2(6) . . ?
C220 C25 C217 120.0 . . ?
C220 C25 Br1 115.7(6) . . ?
C25 C220 H220 120.0 . . ?
C25 C220 C222 120.0 . . ?
C222 C220 H220 120.0 . . ?
C220 C222 Cl6 114.4(5) . . ?
C220 C222 C224 120.0 . . ?
C224 C222 Cl6 125.6(5) . . ?
C222 C224 S10 119.8(4) . . ?
C226 C224 S10 120.1(4) . . ?
C226 C224 C222 120.0 . . ?
C217 C226 H226 120.0 . . ?
C224 C226 C217 120.0 . . ?
C224 C226 H226 120.0 . . ?
C8 C242 C70 119.8(13) . . ?
C8 C242 H242 120.1 . . ?
C70 C242 H242 120.1 . . ?
C8 C246 Br27 117.3(10) . . ?
C117 C246 C8 122.7(13) . . ?
C117 C246 Br27 120.0(11) . . ?
C90 C265 H265 119.1 . . ?
C196 C265 C90 121.7(15) . . ?
C196 C265 H265 119.1 . . ?
Ag13 Pt2 Ag13 180.00(3) . 2_876 ?
Ag13 Pt2 Ag14 116.20(2) 2_876 2_876 ?
Ag13 Pt2 Ag14 63.79(2) . 2_876 ?
Ag13 Pt2 Ag14 63.80(2) 2_876 . ?
Ag13 Pt2 Ag14 116.21(2) . . ?
Ag13 Pt2 Ag21 62.57(2) . . ?
Ag13 Pt2 Ag21 62.57(2) 2_876 2_876 ?
Ag13 Pt2 Ag21 117.43(2) . 2_876 ?
Ag13 Pt2 Ag21 117.43(2) 2_876 . ?
Ag13 Pt2 Ag23 116.42(2) 2_876 2_876 ?
Ag13 Pt2 Ag23 63.58(2) 2_876 . ?
Ag13 Pt2 Ag23 116.42(2) . . ?
Ag13 Pt2 Ag23 63.58(2) . 2_876 ?
Ag13 Pt2 Ag25 63.44(2) 2_876 . ?
Ag13 Pt2 Ag25 63.44(2) . 2_876 ?
Ag13 Pt2 Ag25 116.56(2) 2_876 2_876 ?
Ag13 Pt2 Ag25 116.56(2) . . ?
Ag13 Pt2 Ag30 115.94(2) 2_876 . ?
Ag13 Pt2 Ag30 64.06(2) . . ?
Ag13 Pt2 Ag30 64.06(2) 2_876 2_876 ?
Ag13 Pt2 Ag30 115.94(2) . 2_876 ?
Ag14 Pt2 Ag14 180.0 2_876 . ?
Ag14 Pt2 Ag21 116.447(19) . 2_876 ?
Ag14 Pt2 Ag21 116.445(19) 2_876 . ?
Ag14 Pt2 Ag21 63.555(19) 2_876 2_876 ?
Ag14 Pt2 Ag21 63.552(19) . . ?
Ag14 Pt2 Ag25 117.80(3) . 2_876 ?
Ag14 Pt2 Ag25 62.20(3) 2_876 2_876 ?
Ag14 Pt2 Ag25 62.19(3) . . ?
Ag14 Pt2 Ag25 117.81(3) 2_876 . ?
Ag14 Pt2 Ag30 63.53(2) 2_876 . ?
Ag14 Pt2 Ag30 63.53(2) . 2_876 ?
Ag14 Pt2 Ag30 116.46(2) . . ?
Ag14 Pt2 Ag30 116.47(2) 2_876 2_876 ?
Ag21 Pt2 Ag21 180.00(2) . 2_876 ?
Ag21 Pt2 Ag25 116.40(2) 2_876 . ?
Ag21 Pt2 Ag25 116.40(2) . 2_876 ?
Ag21 Pt2 Ag25 63.60(2) . . ?
Ag21 Pt2 Ag25 63.60(2) 2_876 2_876 ?
Ag23 Pt2 Ag14 116.51(3) 2_876 2_876 ?
Ag23 Pt2 Ag14 116.51(3) . . ?
Ag23 Pt2 Ag14 63.49(3) 2_876 . ?
Ag23 Pt2 Ag14 63.49(3) . 2_876 ?
Ag23 Pt2 Ag21 116.52(2) . . ?
Ag23 Pt2 Ag21 63.48(2) . 2_876 ?
Ag23 Pt2 Ag21 116.52(2) 2_876 2_876 ?
Ag23 Pt2 Ag21 63.48(2) 2_876 . ?
Ag23 Pt2 Ag23 180.0 2_876 . ?
Ag23 Pt2 Ag25 64.09(3) 2_876 2_876 ?
Ag23 Pt2 Ag25 115.91(3) . 2_876 ?
Ag23 Pt2 Ag25 115.91(3) 2_876 . ?
Ag23 Pt2 Ag25 64.09(3) . . ?
Ag23 Pt2 Ag30 62.24(2) . . ?
Ag23 Pt2 Ag30 62.24(2) 2_876 2_876 ?
Ag23 Pt2 Ag30 117.76(2) . 2_876 ?
Ag23 Pt2 Ag30 117.76(2) 2_876 . ?
Ag25 Pt2 Ag25 180.0 2_876 . ?
Ag30 Pt2 Ag21 115.96(2) . 2_876 ?
Ag30 Pt2 Ag21 64.04(2) 2_876 2_876 ?
Ag30 Pt2 Ag21 64.04(2) . . ?
Ag30 Pt2 Ag21 115.95(2) 2_876 . ?
Ag30 Pt2 Ag25 116.09(2) . 2_876 ?
Ag30 Pt2 Ag25 63.91(2) 2_876 2_876 ?
Ag30 Pt2 Ag25 63.91(2) . . ?
Ag30 Pt2 Ag25 116.08(2) 2_876 . ?
Ag30 Pt2 Ag30 179.998(17) . 2_876 ?
Ag20 Ag2 Ag23 101.41(4) . . ?
Ag20 Ag2 Ag30 80.59(4) . . ?
Ag23 Ag2 Ag30 53.48(2) . . ?
S2 Ag2 Ag20 84.16(7) . . ?
S2 Ag2 Ag23 99.62(7) . . ?
S2 Ag2 Ag30 48.78(6) . . ?
S7 Ag2 Ag20 51.25(14) . . ?
S7 Ag2 Ag23 149.33(13) . . ?
S7 Ag2 Ag30 122.40(13) . . ?
S7 Ag2 S2 91.71(11) . . ?
S23 Ag2 Ag20 137.02(8) . . ?
S23 Ag2 Ag23 51.29(8) . . ?
S23 Ag2 Ag30 99.29(9) . . ?
S23 Ag2 S2 127.86(11) . . ?
S23 Ag2 S7 136.63(15) . . ?
Ag13 Ag7 Ag21 54.50(2) . . ?
Ag31 Ag7 Ag13 99.58(3) . . ?
Ag31 Ag7 Ag21 78.85(3) . . ?
S9 Ag7 Ag13 51.70(6) . . ?
S9 Ag7 Ag21 101.90(6) . . ?
S9 Ag7 Ag31 133.26(9) . . ?
S9 Ag7 S15 129.85(10) . . ?
S9 Ag7 S28 136.51(9) . . ?
S15 Ag7 Ag13 100.45(5) . . ?
S15 Ag7 Ag21 49.39(6) . . ?
S15 Ag7 Ag31 86.33(8) . . ?
S28 Ag7 Ag13 148.36(8) . . ?
S28 Ag7 Ag21 119.09(7) . . ?
S28 Ag7 Ag31 51.14(7) . . ?
S28 Ag7 S15 90.32(9) . . ?
Pt2 Ag13 Ag7 122.16(3) . . ?
Pt2 Ag13 Ag14 58.39(2) . 2_876 ?
Pt2 Ag13 Ag21 59.15(2) . . ?
Pt2 Ag13 Ag23 58.43(2) . 2_876 ?
Pt2 Ag13 Ag25 58.82(2) . 2_876 ?
Pt2 Ag13 Ag30 58.29(2) . . ?
Ag14 Ag13 Ag7 133.55(4) 2_876 . ?
Ag14 Ag13 Ag30 59.85(3) 2_876 . ?
Ag21 Ag13 Ag7 65.76(2) . . ?
Ag21 Ag13 Ag14 109.08(3) . 2_876 ?
Ag21 Ag13 Ag23 60.61(3) . 2_876 ?
Ag21 Ag13 Ag25 109.66(3) . 2_876 ?
Ag21 Ag13 Ag30 60.95(3) . . ?
Ag23 Ag13 Ag7 107.85(3) 2_876 . ?
Ag23 Ag13 Ag14 107.82(3) 2_876 2_876 ?
Ag23 Ag13 Ag25 60.81(3) 2_876 2_876 ?
Ag23 Ag13 Ag30 108.62(3) 2_876 . ?
Ag25 Ag13 Ag7 167.14(4) 2_876 . ?
Ag25 Ag13 Ag14 58.96(3) 2_876 2_876 ?
Ag25 Ag13 Ag30 107.63(3) 2_876 . ?
Ag30 Ag13 Ag7 81.10(3) . . ?
S9 Ag13 Pt2 170.89(8) . . ?
S9 Ag13 Ag7 52.43(7) . . ?
S9 Ag13 Ag14 130.69(8) . 2_876 ?
S9 Ag13 Ag21 112.95(7) . . ?
S9 Ag13 Ag23 114.55(9) . 2_876 ?
S9 Ag13 Ag25 124.47(7) . 2_876 ?
S9 Ag13 Ag30 123.47(8) . . ?
Pt2 Ag14 Ag13 57.82(2) . 2_876 ?
Pt2 Ag14 Ag21 58.37(2) . . ?
Pt2 Ag14 Ag23 58.18(2) . 2_876 ?
Pt2 Ag14 Ag25 59.16(2) . . ?
Pt2 Ag14 Ag30 58.27(2) . 2_876 ?
Pt2 Ag14 Ag36 124.25(3) . . ?
Ag13 Ag14 Ag21 108.08(3) 2_876 . ?
Ag13 Ag14 Ag36 110.36(4) 2_876 . ?
Ag21 Ag14 Ag36 81.48(3) . . ?
Ag23 Ag14 Ag13 107.12(3) 2_876 2_876 ?
Ag23 Ag14 Ag21 59.99(2) 2_876 . ?
Ag23 Ag14 Ag30 58.80(2) 2_876 2_876 ?
Ag23 Ag14 Ag36 132.75(3) 2_876 . ?
Ag25 Ag14 Ag13 60.41(3) . 2_876 ?
Ag25 Ag14 Ag21 60.83(3) . . ?
Ag25 Ag14 Ag23 108.93(3) . 2_876 ?
Ag25 Ag14 Ag30 109.13(3) . 2_876 ?
Ag25 Ag14 Ag36 68.21(3) . . ?
Ag30 Ag14 Ag13 60.28(3) 2_876 2_876 ?
Ag30 Ag14 Ag21 107.40(3) 2_876 . ?
Ag30 Ag14 Ag36 168.42(4) 2_876 . ?
S25 Ag14 Pt2 166.63(11) . . ?
S25 Ag14 Ag13 110.63(10) . 2_876 ?
S25 Ag14 Ag21 125.92(7) . . ?
S25 Ag14 Ag23 135.13(11) . 2_876 ?
S25 Ag14 Ag25 110.32(11) . . ?
S25 Ag14 Ag30 124.14(8) . 2_876 ?
S25 Ag14 Ag36 50.39(8) . . ?
Ag2 Ag20 Ag25 76.86(3) . . ?
S3 Ag20 Ag2 118.46(8) . . ?
S3 Ag20 Ag25 51.23(8) . . ?
S3 Ag20 S11 96.16(12) . . ?
S7 Ag20 Ag2 53.45(12) . . ?
S7 Ag20 Ag25 129.50(12) . . ?
S7 Ag20 S3 145.19(13) . . ?
S7 Ag20 S11 118.33(12) . . ?
S11 Ag20 Ag2 113.94(8) . . ?
S11 Ag20 Ag25 87.36(8) . . ?
Pt2 Ag21 Ag7 115.59(3) . . ?
Pt2 Ag21 Ag13 58.273(19) . . ?
Pt2 Ag21 Ag14 58.076(19) . . ?
Pt2 Ag21 Ag23 58.04(2) . 2_876 ?
Pt2 Ag21 Ag25 58.30(2) . . ?
Pt2 Ag21 Ag30 57.870(19) . . ?
Pt2 Ag21 Ag35 142.65(4) . . ?
Ag13 Ag21 Ag7 59.73(2) . . ?
Ag13 Ag21 Ag14 108.02(3) . . ?
Ag13 Ag21 Ag23 60.28(3) . 2_876 ?
Ag13 Ag21 Ag25 108.49(3) . . ?
Ag13 Ag21 Ag30 60.49(3) . . ?
Ag13 Ag21 Ag35 152.31(3) . . ?
Ag14 Ag21 Ag7 163.09(4) . . ?
Ag14 Ag21 Ag25 58.70(3) . . ?
Ag14 Ag21 Ag30 106.90(3) . . ?
Ag14 Ag21 Ag35 99.65(3) . . ?
Ag23 Ag21 Ag7 103.27(3) 2_876 . ?
Ag23 Ag21 Ag14 59.85(3) 2_876 . ?
Ag23 Ag21 Ag25 107.11(3) 2_876 . ?
Ag23 Ag21 Ag30 108.00(3) 2_876 . ?
Ag23 Ag21 Ag35 140.28(4) 2_876 . ?
Ag25 Ag21 Ag7 133.94(4) . . ?
Ag25 Ag21 Ag30 60.08(3) . . ?
Ag25 Ag21 Ag35 84.78(3) . . ?
Ag30 Ag21 Ag7 78.10(3) . . ?
Ag30 Ag21 Ag35 110.63(4) . . ?
Ag35 Ag21 Ag7 93.38(3) . . ?
S15 Ag21 Pt2 167.01(8) . . ?
S15 Ag21 Ag7 53.27(7) . . ?
S15 Ag21 Ag13 108.97(7) . . ?
S15 Ag21 Ag14 130.19(7) . . ?
S15 Ag21 Ag23 115.03(8) . 2_876 ?
S15 Ag21 Ag25 133.43(8) . . ?
S15 Ag21 Ag30 119.96(7) . . ?
S15 Ag21 Ag35 50.06(8) . . ?
Pt2 Ag23 Ag2 122.05(3) . . ?
Pt2 Ag23 Ag13 58.00(2) . 2_876 ?
Pt2 Ag23 Ag14 58.32(2) . 2_876 ?
Pt2 Ag23 Ag21 58.47(2) . 2_876 ?
Pt2 Ag23 Ag25 58.27(2) . . ?
Pt2 Ag23 Ag30 58.99(2) . . ?
Ag13 Ag23 Ag2 131.31(4) 2_876 . ?
Ag13 Ag23 Ag14 107.35(4) 2_876 2_876 ?
Ag13 Ag23 Ag21 59.11(3) 2_876 2_876 ?
Ag13 Ag23 Ag25 59.67(2) 2_876 . ?
Ag14 Ag23 Ag2 110.10(3) 2_876 . ?
Ag14 Ag23 Ag21 60.16(3) 2_876 2_876 ?
Ag14 Ag23 Ag25 108.58(4) 2_876 . ?
Ag21 Ag23 Ag2 169.17(4) 2_876 . ?
Ag21 Ag23 Ag25 107.53(4) 2_876 . ?
Ag25 Ag23 Ag2 79.43(3) . . ?
Ag30 Ag23 Ag2 66.60(3) . . ?
Ag30 Ag23 Ag13 108.56(4) . 2_876 ?
Ag30 Ag23 Ag14 60.69(3) . 2_876 ?
Ag30 Ag23 Ag21 109.05(4) . 2_876 ?
Ag30 Ag23 Ag25 60.84(2) . . ?
S23 Ag23 Pt2 169.18(7) . . ?
S23 Ag23 Ag2 51.47(7) . . ?
S23 Ag23 Ag13 132.71(8) . 2_876 ?
S23 Ag23 Ag14 113.74(9) . 2_876 ?
S23 Ag23 Ag21 125.88(8) . 2_876 ?
S23 Ag23 Ag25 123.05(9) . . ?
S23 Ag23 Ag30 111.31(6) . . ?
Pt2 Ag25 Ag13 57.74(2) . 2_876 ?
Pt2 Ag25 Ag14 58.64(2) . . ?
Pt2 Ag25 Ag20 141.60(3) . . ?
Pt2 Ag25 Ag21 58.09(2) . . ?
Pt2 Ag25 Ag23 57.64(2) . . ?
Pt2 Ag25 Ag30 57.83(2) . . ?
Pt2 Ag25 Ag36 115.90(4) . . ?
Ag13 Ag25 Ag20 143.59(4) 2_876 . ?
Ag13 Ag25 Ag21 107.99(3) 2_876 . ?
Ag13 Ag25 Ag23 59.52(2) 2_876 . ?
Ag13 Ag25 Ag30 106.31(3) 2_876 . ?
Ag13 Ag25 Ag36 104.49(3) 2_876 . ?
Ag14 Ag25 Ag13 60.64(3) . 2_876 ?
Ag14 Ag25 Ag20 150.00(4) . . ?
Ag14 Ag25 Ag21 60.48(3) . . ?
Ag14 Ag25 Ag23 108.11(3) . . ?
Ag14 Ag25 Ag30 108.37(4) . . ?
Ag14 Ag25 Ag36 59.90(3) . . ?
Ag20 Ag25 Ag36 91.53(3) . . ?
Ag21 Ag25 Ag20 107.31(3) . . ?
Ag21 Ag25 Ag23 106.70(3) . . ?
Ag21 Ag25 Ag30 60.15(3) . . ?
Ag21 Ag25 Ag36 77.48(3) . . ?
Ag23 Ag25 Ag20 101.63(4) . . ?
Ag23 Ag25 Ag36 164.00(3) . . ?
Ag30 Ag25 Ag20 83.87(3) . . ?
Ag30 Ag25 Ag23 58.18(2) . . ?
Ag30 Ag25 Ag36 133.36(4) . . ?
S3 Ag25 Pt2 165.82(10) . . ?
S3 Ag25 Ag13 117.79(6) . 2_876 ?
S3 Ag25 Ag14 107.19(10) . . ?
S3 Ag25 Ag20 50.78(8) . . ?
S3 Ag25 Ag21 116.12(9) . . ?
S3 Ag25 Ag23 133.92(10) . . ?
S3 Ag25 Ag30 132.84(7) . . ?
S3 Ag25 Ag36 50.52(10) . . ?
Pt2 Ag30 Ag2 115.57(3) . . ?
Pt2 Ag30 Ag13 57.652(19) . . ?
Pt2 Ag30 Ag14 58.194(19) . 2_876 ?
Pt2 Ag30 Ag21 58.085(19) . . ?
Pt2 Ag30 Ag23 58.77(2) . . ?
Pt2 Ag30 Ag25 58.255(19) . . ?
Pt2 Ag30 Ag31 139.47(4) . . ?
Ag13 Ag30 Ag2 164.91(3) . . ?
Ag13 Ag30 Ag21 58.56(3) . . ?
Ag13 Ag30 Ag25 106.70(3) . . ?
Ag13 Ag30 Ag31 99.84(3) . . ?
Ag14 Ag30 Ag2 105.05(3) 2_876 . ?
Ag14 Ag30 Ag13 59.87(3) 2_876 . ?
Ag14 Ag30 Ag21 107.18(3) 2_876 . ?
Ag14 Ag30 Ag25 108.55(3) 2_876 . ?
Ag14 Ag30 Ag31 143.39(3) 2_876 . ?
Ag21 Ag30 Ag2 131.77(3) . . ?
Ag21 Ag30 Ag31 81.56(3) . . ?
Ag23 Ag30 Ag2 59.91(3) . . ?
Ag23 Ag30 Ag13 108.15(3) . . ?
Ag23 Ag30 Ag14 60.51(3) . 2_876 ?
Ag23 Ag30 Ag21 108.62(3) . . ?
Ag23 Ag30 Ag25 60.98(3) . . ?
Ag23 Ag30 Ag31 151.55(4) . . ?
Ag25 Ag30 Ag2 76.48(3) . . ?
Ag25 Ag30 Ag21 59.76(3) . . ?
Ag25 Ag30 Ag31 106.44(3) . . ?
Ag31 Ag30 Ag2 93.18(3) . . ?
S2 Ag30 Pt2 167.69(7) . . ?
S2 Ag30 Ag2 52.33(7) . . ?
S2 Ag30 Ag13 133.29(7) . . ?
S2 Ag30 Ag14 119.44(7) . 2_876 ?
S2 Ag30 Ag21 130.07(7) . . ?
S2 Ag30 Ag23 109.09(7) . . ?
S2 Ag30 Ag25 115.56(7) . . ?
S2 Ag30 Ag31 50.55(7) . . ?
Ag7 Ag31 Ag30 78.73(3) . . ?
S2 Ag31 Ag7 121.19(7) . . ?
S2 Ag31 Ag30 51.78(6) . . ?
S2 Ag31 S11 99.49(11) . . ?
S11 Ag31 Ag7 111.72(10) . . ?
S11 Ag31 Ag30 90.28(6) . . ?
S28 Ag31 Ag7 54.37(7) . . ?
S28 Ag31 Ag30 132.64(8) . . ?
S28 Ag31 S2 148.29(10) . . ?
S28 Ag31 S11 111.24(11) . . ?
Ag36 Ag35 Ag21 79.05(3) . . ?
S11 Ag35 Ag21 85.38(7) . . ?
S11 Ag35 Ag36 110.52(8) . . ?
S15 Ag35 Ag21 50.17(6) . . ?
S15 Ag35 Ag36 119.14(7) . . ?
S15 Ag35 S11 97.85(11) . . ?
S29 Ag35 Ag21 131.06(11) . . ?
S29 Ag35 Ag36 53.21(10) . . ?
S29 Ag35 S11 118.3(2) . . ?
S29 Ag35 S15 143.7(2) . . ?
Ag14 Ag36 Ag25 51.90(3) . . ?
Ag35 Ag36 Ag14 98.66(4) . . ?
Ag35 Ag36 Ag25 80.35(3) . . ?
S3 Ag36 Ag14 96.68(8) . . ?
S3 Ag36 Ag25 47.47(7) . . ?
S3 Ag36 Ag35 86.37(7) . . ?
S25 Ag36 Ag14 50.28(7) . . ?
S25 Ag36 Ag25 95.72(8) . . ?
S25 Ag36 Ag35 135.88(11) . . ?
S25 Ag36 S3 122.88(12) . . ?
S25 Ag36 S29 136.78(19) . . ?
S29 Ag36 Ag14 145.62(16) . . ?
S29 Ag36 Ag25 124.66(13) . . ?
S29 Ag36 Ag35 51.65(11) . . ?
S29 Ag36 S3 97.88(19) . . ?
Ag30 S2 Ag2 78.89(7) . . ?
Ag31 S2 Ag2 130.93(12) . . ?
Ag31 S2 Ag30 77.67(9) . . ?
C9 S2 Ag2 112.7(3) . . ?
C9 S2 Ag30 109.6(3) . . ?
C9 S2 Ag31 115.6(3) . . ?
Ag20 S3 Ag25 77.99(10) . . ?
Ag20 S3 Ag36 131.73(13) . . ?
Ag25 S3 Ag36 82.01(11) . . ?
C118 S3 Ag20 111.5(4) . . ?
C118 S3 Ag25 103.7(4) . . ?
C118 S3 Ag36 115.7(4) . . ?
Ag20 S7 Ag2 75.31(13) . . ?
C274 S7 Ag2 109.5(6) . . ?
C274 S7 Ag20 92.3(6) . . ?
Ag13 S9 Ag7 75.88(9) . . ?
C56 S9 Ag7 106.3(3) . . ?
C56 S9 Ag13 106.7(3) . . ?
Ag20 S11 Ag31 108.32(13) . . ?
Ag35 S11 Ag20 113.66(10) . . ?
Ag35 S11 Ag31 111.74(14) . . ?
C254 S11 Ag20 106.1(4) . . ?
C254 S11 Ag31 109.4(3) . . ?
C254 S11 Ag35 107.4(4) . . ?
Ag21 S15 Ag7 77.34(8) . . ?
Ag35 S15 Ag7 130.77(14) . . ?
Ag35 S15 Ag21 79.77(9) . . ?
C69 S15 Ag7 114.5(4) . . ?
C69 S15 Ag21 103.5(2) . . ?
C69 S15 Ag35 112.9(4) . . ?
Ag23 S23 Ag2 77.24(10) . . ?
C251 S23 Ag2 106.0(3) . . ?
C251 S23 Ag23 109.7(3) . . ?
Ag14 S25 Ag36 79.33(9) . . ?
C210 S25 Ag14 110.8(4) . . ?
C210 S25 Ag36 108.8(3) . . ?
Ag31 S28 Ag7 74.50(7) . . ?
C130 S28 Ag7 110.6(3) . . ?
C130 S28 Ag31 108.5(3) . . ?
Ag35 S29 Ag36 75.15(13) . . ?
C145 S29 Ag35 112.7(8) . . ?
C145 S29 Ag36 110.8(8) . . ?
C241 C39 H39 120.0 . . ?
C241 C39 C245 120.0 . . ?
C245 C39 H39 120.0 . . ?
C39 C241 H241 120.0 . . ?
C39 C241 C130 120.0 . . ?
C130 C241 H241 120.0 . . ?
C241 C130 S28 121.6(4) . . ?
C241 C130 C243 120.0 . . ?
C243 C130 S28 118.2(4) . . ?
C130 C243 Cl11 120.6(4) . . ?
C130 C243 C73 120.0 . . ?
C73 C243 Cl11 119.4(4) . . ?
C243 C73 H73 120.0 . . ?
C245 C73 C243 120.0 . . ?
C245 C73 H73 120.0 . . ?
C39 C245 Cl34 120.8(5) . . ?
C73 C245 Cl34 119.1(5) . . ?
C73 C245 C39 120.0 . . ?
C270 C45 H45 120.0 . . ?
C270 C45 C272 120.0 . . ?
C272 C45 H45 120.0 . . ?
C45 C270 Cl15 119.1(13) . . ?
C45 C270 C145 120.0 . . ?
C145 C270 Cl15 118.3(13) . . ?
C270 C145 S29 117.5(13) . . ?
C271 C145 S29 122.3(13) . . ?
C271 C145 C270 120.0 . . ?
C145 C271 H271 120.0 . . ?
C82 C271 C145 120.0 . . ?
C82 C271 H271 120.0 . . ?
C271 C82 H82 120.0 . . ?
C271 C82 C272 120.0 . . ?
C272 C82 H82 120.0 . . ?
C45 C272 Cl26 125.0(12) . . ?
C82 C272 Cl26 112.1(12) . . ?
C82 C272 C45 120.0 . . ?
C168 C93 H93 120.0 . . ?
C168 C93 C172 120.0 . . ?
C172 C93 H93 120.0 . . ?
C93 C168 H168 120.0 . . ?
C93 C168 C9 120.0 . . ?
C9 C168 H168 120.0 . . ?
C168 C9 S2 119.8(4) . . ?
C170 C9 S2 120.0(4) . . ?
C170 C9 C168 120.0 . . ?
C9 C170 H170 120.0 . . ?
C9 C170 C95 120.0 . . ?
C95 C170 H170 120.0 . . ?
C170 C95 H95 120.0 . . ?
C170 C95 C172 120.0 . . ?
C172 C95 H95 120.0 . . ?
C93 C172 Br11 119.7(4) . . ?
C95 C172 C93 120.0 . . ?
C95 C172 Br11 120.3(4) . . ?
C180 C99 H99 120.0 . . ?
C180 C99 C184 120.0 . . ?
C184 C99 H99 120.0 . . ?
C99 C180 Cl17 114.3(6) . . ?
C99 C180 C56 120.0 . . ?
C56 C180 Cl17 125.7(6) . . ?
C180 C56 S9 118.7(5) . . ?
C180 C56 C182 120.0 . . ?
C182 C56 S9 121.3(5) . . ?
C56 C182 H182 120.0 . . ?
C101 C182 C56 120.0 . . ?
C101 C182 H182 120.0 . . ?
C182 C101 H101 120.0 . . ?
C182 C101 C184 120.0 . . ?
C184 C101 H101 120.0 . . ?
C99 C184 Cl32 117.3(6) . . ?
C101 C184 Cl32 122.7(6) . . ?
C101 C184 C99 120.0 . . ?
C247 C132 Cl29 114.0(7) . . ?
C247 C132 C251 120.0 . . ?
C251 C132 Cl29 125.8(7) . . ?
C132 C247 H247 120.0 . . ?
C132 C247 C21 120.0 . . ?
C21 C247 H247 120.0 . . ?
C247 C21 Cl3 116.8(6) . . ?
C249 C21 Cl3 123.2(6) . . ?
C249 C21 C247 120.0 . . ?
C21 C249 H249 120.0 . . ?
C134 C249 C21 120.0 . . ?
C134 C249 H249 120.0 . . ?
C249 C134 H134 120.0 . . ?
C249 C134 C251 120.0 . . ?
C251 C134 H134 120.0 . . ?
C132 C251 S23 120.7(5) . . ?
C134 C251 S23 119.0(5) . . ?
C134 C251 C132 120.0 . . ?
C273 C146 Cl19 121.0(6) . . ?
C273 C146 C276 120.0 . . ?
C276 C146 Cl19 119.0(6) . . ?
C146 C273 H273 120.0 . . ?
C146 C273 C23 120.0 . . ?
C23 C273 H273 120.0 . . ?
C273 C23 H23 120.0 . . ?
C274 C23 C273 120.0 . . ?
C274 C23 H23 120.0 . . ?
C23 C274 S7 115.7(10) . . ?
C23 C274 C147 120.0 . . ?
C147 C274 S7 122.9(9) . . ?
C274 C147 Cl31 121.9(7) . . ?
C276 C147 Cl31 118.0(7) . . ?
C276 C147 C274 120.0 . . ?
C146 C276 H276 120.0 . . ?
C147 C276 C146 120.0 . . ?
C147 C276 H276 120.0 . . ?
C113 C206 H206 120.0 . . ?
C113 C206 C114 120.0 . . ?
C114 C206 H206 120.0 . . ?
C206 C113 Cl35 120.8(10) . . ?
C208 C113 Cl35 119.2(10) . . ?
C208 C113 C206 120.0 . . ?
C113 C208 H208 120.0 . . ?
C35 C208 C113 120.0 . . ?
C35 C208 H208 120.0 . . ?
C208 C35 Cl8 117.3(9) . . ?
C208 C35 C210 120.0 . . ?
C210 C35 Cl8 122.7(9) . . ?
C35 C210 S25 119.0(7) . . ?
C35 C210 C114 120.0 . . ?
C114 C210 S25 120.9(8) . . ?
C206 C114 H114 120.0 . . ?
C210 C114 C206 120.0 . . ?
C210 C114 H114 120.0 . . ?
C116 C214 H214 120.0 . . ?
C116 C214 C118 120.0 . . ?
C118 C214 H214 120.0 . . ?
C214 C116 H116 120.0 . . ?
C214 C116 C216 120.0 . . ?
C216 C116 H116 120.0 . . ?
C116 C216 Br26 118.7(7) . . ?
C19 C216 C116 120.0 . . ?
C19 C216 Br26 121.1(7) . . ?
C216 C19 H19 120.0 . . ?
C218 C19 C216 120.0 . . ?
C218 C19 H19 120.0 . . ?
C19 C218 H218 120.0 . . ?
C19 C218 C118 120.0 . . ?
C118 C218 H218 120.0 . . ?
C214 C118 S3 121.3(7) . . ?
C218 C118 S3 118.2(7) . . ?
C218 C118 C214 120.0 . . ?
C122 C225 C124 120.0 . . ?
C122 C225 Br20 118.5(8) . . ?
C124 C225 Br20 121.4(8) . . ?
C225 C122 H122 120.0 . . ?
C225 C122 C227 120.0 . . ?
C227 C122 H122 120.0 . . ?
C122 C227 H227 120.0 . . ?
C69 C227 C122 120.0 . . ?
C69 C227 H227 120.0 . . ?
C227 C69 S15 120.2(6) . . ?
C227 C69 C229 120.0 . . ?
C229 C69 S15 119.7(6) . . ?
C69 C229 H229 120.0 . . ?
C124 C229 C69 120.0 . . ?
C124 C229 H229 120.0 . . ?
C225 C124 H124 120.0 . . ?
C229 C124 C225 120.0 . . ?
C229 C124 H124 120.0 . . ?
C252 C250 H250 120.0 . . ?
C252 C250 C259 120.0 . . ?
C259 C250 H250 120.0 . . ?
C250 C252 H252 120.0 . . ?
C254 C252 C250 120.0 . . ?
C254 C252 H252 120.0 . . ?
C252 C254 S11 117.8(5) . . ?
C252 C254 C256 120.0 . . ?
C256 C254 S11 122.2(5) . . ?
C254 C256 Cl25 125.1(7) . . ?
C254 C256 C32 120.0 . . ?
C32 C256 Cl25 113.2(7) . . ?
C256 C32 H32 120.0 . . ?
C259 C32 C256 120.0 . . ?
C259 C32 H32 120.0 . . ?
C250 C259 Br19 122.9(6) . . ?
C32 C259 C250 120.0 . . ?
C32 C259 Br19 117.1(6) . . ?
Ag12 Pt3 Ag12 180.0 2_667 . ?
Ag12 Pt3 Ag15 62.46(2) . . ?
Ag12 Pt3 Ag15 117.54(2) . 2_667 ?
Ag12 Pt3 Ag15 117.54(2) 2_667 . ?
Ag12 Pt3 Ag15 62.46(2) 2_667 2_667 ?
Ag12 Pt3 Ag19 63.96(2) 2_667 2_667 ?
Ag12 Pt3 Ag19 116.04(2) 2_667 . ?
Ag12 Pt3 Ag19 116.04(2) . 2_667 ?
Ag12 Pt3 Ag19 63.96(2) . . ?
Ag12 Pt3 Ag22 117.07(2) 2_667 2_667 ?
Ag12 Pt3 Ag22 117.07(2) . . ?
Ag12 Pt3 Ag22 62.93(2) . 2_667 ?
Ag12 Pt3 Ag22 62.93(2) 2_667 . ?
Ag12 Pt3 Ag24 115.66(2) . 2_667 ?
Ag12 Pt3 Ag24 64.34(2) 2_667 2_667 ?
Ag12 Pt3 Ag24 64.33(2) . . ?
Ag12 Pt3 Ag24 115.66(2) 2_667 . ?
Ag12 Pt3 Ag26 64.116(19) . . ?
Ag12 Pt3 Ag26 64.115(19) 2_667 2_667 ?
Ag12 Pt3 Ag26 115.885(19) . 2_667 ?
Ag12 Pt3 Ag26 115.884(19) 2_667 . ?
Ag15 Pt3 Ag15 179.998(15) . 2_667 ?
Ag15 Pt3 Ag22 63.60(2) . 2_667 ?
Ag15 Pt3 Ag22 116.40(2) . . ?
Ag15 Pt3 Ag22 116.40(2) 2_667 2_667 ?
Ag15 Pt3 Ag22 63.60(2) 2_667 . ?
Ag15 Pt3 Ag26 116.21(2) . . ?
Ag15 Pt3 Ag26 63.79(2) . 2_667 ?
Ag15 Pt3 Ag26 116.21(2) 2_667 2_667 ?
Ag15 Pt3 Ag26 63.79(2) 2_667 . ?
Ag19 Pt3 Ag15 115.653(19) 2_667 . ?
Ag19 Pt3 Ag15 64.345(19) 2_667 2_667 ?
Ag19 Pt3 Ag15 115.654(19) . 2_667 ?
Ag19 Pt3 Ag15 64.347(19) . . ?
Ag19 Pt3 Ag19 180.0 . 2_667 ?
Ag19 Pt3 Ag22 117.592(19) 2_667 . ?
Ag19 Pt3 Ag22 62.407(19) . . ?
Ag19 Pt3 Ag22 117.591(19) . 2_667 ?
Ag19 Pt3 Ag22 62.409(19) 2_667 2_667 ?
Ag19 Pt3 Ag26 117.00(2) . . ?
Ag19 Pt3 Ag26 63.00(2) . 2_667 ?
Ag19 Pt3 Ag26 63.00(2) 2_667 . ?
Ag19 Pt3 Ag26 117.00(2) 2_667 2_667 ?
Ag22 Pt3 Ag22 180.0 2_667 . ?
Ag22 Pt3 Ag26 117.34(2) 2_667 2_667 ?
Ag22 Pt3 Ag26 62.66(2) 2_667 . ?
Ag22 Pt3 Ag26 62.66(2) . 2_667 ?
Ag22 Pt3 Ag26 117.34(2) . . ?
Ag24 Pt3 Ag15 117.694(19) 2_667 2_667 ?
Ag24 Pt3 Ag15 62.308(19) . 2_667 ?
Ag24 Pt3 Ag15 62.305(19) 2_667 . ?
Ag24 Pt3 Ag15 117.693(19) . . ?
Ag24 Pt3 Ag19 115.20(2) 2_667 . ?
Ag24 Pt3 Ag19 64.80(2) 2_667 2_667 ?
Ag24 Pt3 Ag19 64.80(2) . . ?
Ag24 Pt3 Ag19 115.20(2) . 2_667 ?
Ag24 Pt3 Ag22 64.77(2) . . ?
Ag24 Pt3 Ag22 115.22(2) . 2_667 ?
Ag24 Pt3 Ag22 64.78(2) 2_667 2_667 ?
Ag24 Pt3 Ag22 115.23(2) 2_667 . ?
Ag24 Pt3 Ag24 180.0 . 2_667 ?
Ag24 Pt3 Ag26 117.86(2) . 2_667 ?
Ag24 Pt3 Ag26 117.86(2) 2_667 . ?
Ag24 Pt3 Ag26 62.14(2) 2_667 2_667 ?
Ag24 Pt3 Ag26 62.14(2) . . ?
Ag26 Pt3 Ag26 180.00(2) . 2_667 ?
Ag33 Ag3 Ag12 81.47(3) . . ?
S13 Ag3 Ag12 131.98(8) . . ?
S13 Ag3 Ag33 52.03(8) . . ?
S13 Ag3 S16 139.95(11) . . ?
S13 Ag3 S26 119.49(10) . . ?
S16 Ag3 Ag12 51.33(5) . . ?
S16 Ag3 Ag33 120.15(6) . . ?
S16 Ag3 S26 99.96(9) . . ?
S26 Ag3 Ag12 86.65(7) . . ?
S26 Ag3 Ag33 113.16(7) . . ?
Ag34 Ag5 Ag19 81.57(3) . . ?
S8 Ag5 Ag19 52.45(5) . . ?
S8 Ag5 Ag34 122.51(6) . . ?
S8 Ag5 S26 95.63(9) . . ?
S19 Ag5 Ag19 133.13(7) . . ?
S19 Ag5 Ag34 53.57(7) . . ?
S19 Ag5 S8 139.95(10) . . ?
S19 Ag5 S26 122.31(11) . . ?
S26 Ag5 Ag19 87.63(7) . . ?
S26 Ag5 Ag34 117.24(7) . . ?
Pt3 Ag12 Ag3 141.68(3) . . ?
Pt3 Ag12 Ag15 59.194(18) . . ?
Pt3 Ag12 Ag19 58.240(18) . . ?
Pt3 Ag12 Ag22 59.084(19) . 2_667 ?
Pt3 Ag12 Ag24 58.030(18) . . ?
Pt3 Ag12 Ag26 58.612(19) . . ?
Pt3 Ag12 Ag34 115.06(3) . . ?
Ag3 Ag12 Ag34 95.19(3) . . ?
Ag15 Ag12 Ag3 151.75(3) . . ?
Ag15 Ag12 Ag19 61.29(2) . . ?
Ag15 Ag12 Ag22 61.20(2) . 2_667 ?
Ag15 Ag12 Ag24 109.58(3) . . ?
Ag15 Ag12 Ag26 108.94(3) . . ?
Ag15 Ag12 Ag34 57.75(2) . . ?
Ag19 Ag12 Ag3 109.22(3) . . ?
Ag19 Ag12 Ag24 60.75(2) . . ?
Ag19 Ag12 Ag26 107.80(3) . . ?
Ag19 Ag12 Ag34 79.29(2) . . ?
Ag22 Ag12 Ag3 140.09(3) 2_667 . ?
Ag22 Ag12 Ag19 109.52(3) 2_667 . ?
Ag22 Ag12 Ag24 107.05(3) 2_667 . ?
Ag22 Ag12 Ag26 59.61(2) 2_667 . ?
Ag22 Ag12 Ag34 101.00(3) 2_667 . ?
Ag24 Ag12 Ag3 83.93(3) . . ?
Ag24 Ag12 Ag26 58.38(2) . . ?
Ag24 Ag12 Ag34 136.78(3) . . ?
Ag26 Ag12 Ag3 99.28(3) . . ?
Ag26 Ag12 Ag34 160.51(3) . . ?
S16 Ag12 Pt3 165.38(6) . . ?
S16 Ag12 Ag3 52.65(6) . . ?
S16 Ag12 Ag15 106.51(6) . . ?
S16 Ag12 Ag19 119.61(7) . . ?
S16 Ag12 Ag22 112.89(6) . 2_667 ?
S16 Ag12 Ag24 135.42(6) . . ?
S16 Ag12 Ag26 130.20(7) . . ?
S16 Ag12 Ag34 52.29(6) . . ?
Pt3 Ag15 Ag12 58.344(18) . . ?
Pt3 Ag15 Ag19 57.634(17) . . ?
Pt3 Ag15 Ag22 58.326(18) . 2_667 ?
Pt3 Ag15 Ag24 58.628(18) . 2_667 ?
Pt3 Ag15 Ag26 58.364(18) . 2_667 ?
Pt3 Ag15 Ag34 124.69(3) . . ?
Ag12 Ag15 Ag19 60.28(2) . . ?
Ag12 Ag15 Ag22 59.79(2) . 2_667 ?
Ag12 Ag15 Ag26 107.96(3) . 2_667 ?
Ag12 Ag15 Ag34 68.62(2) . . ?
Ag19 Ag15 Ag34 84.03(2) . . ?
Ag22 Ag15 Ag19 107.62(3) 2_667 . ?
Ag22 Ag15 Ag26 108.40(3) 2_667 2_667 ?
Ag22 Ag15 Ag34 107.63(3) 2_667 . ?
Ag24 Ag15 Ag12 109.06(3) 2_667 . ?
Ag24 Ag15 Ag19 106.73(3) 2_667 . ?
Ag24 Ag15 Ag22 61.68(2) 2_667 2_667 ?
Ag24 Ag15 Ag26 59.14(2) 2_667 2_667 ?
Ag24 Ag15 Ag34 166.41(3) 2_667 . ?
Ag26 Ag15 Ag19 59.04(2) 2_667 . ?
Ag26 Ag15 Ag34 134.43(3) 2_667 . ?
S14 Ag15 Pt3 168.54(7) . . ?
S14 Ag15 Ag12 114.72(7) . . ?
S14 Ag15 Ag19 128.89(6) . . ?
S14 Ag15 Ag22 110.63(7) . 2_667 ?
S14 Ag15 Ag24 120.74(6) . 2_667 ?
S14 Ag15 Ag26 132.38(7) . 2_667 ?
S14 Ag15 Ag34 52.93(6) . . ?
Ag18 Ag16 Ag19 80.06(3) . . ?
Ag22 Ag16 Ag18 98.50(3) . . ?
Ag22 Ag16 Ag19 55.85(2) . . ?
S8 Ag16 Ag18 87.41(7) . . ?
S8 Ag16 Ag19 51.38(5) . . ?
S8 Ag16 Ag22 104.39(6) . . ?
S24 Ag16 Ag18 133.64(7) . . ?
S24 Ag16 Ag19 102.63(7) . . ?
S24 Ag16 Ag22 52.59(6) . . ?
S24 Ag16 S8 130.73(10) . . ?
S24 Ag16 S27 110.53(11) . . ?
S27 Ag16 Ag18 51.56(9) . . ?
S27 Ag16 Ag19 131.61(9) . . ?
S27 Ag16 Ag22 124.02(8) . . ?
S27 Ag16 S8 117.46(10) . . ?
Ag24 Ag18 Ag16 79.87(3) . . ?
S26 Ag18 Ag16 109.62(8) . . ?
S26 Ag18 Ag24 89.11(6) . . ?
S27 Ag18 Ag16 54.51(9) . . ?
S27 Ag18 Ag24 118.81(9) . . ?
S27 Ag18 S26 139.77(10) . . ?
S27 Ag18 S30 122.27(10) . . ?
S30 Ag18 Ag16 124.87(7) . . ?
S30 Ag18 Ag24 52.79(6) . . ?
S30 Ag18 S26 97.43(10) . . ?
Pt3 Ag19 Ag5 137.79(3) . . ?
Pt3 Ag19 Ag12 57.803(18) . . ?
Pt3 Ag19 Ag15 58.018(17) . . ?
Pt3 Ag19 Ag16 116.26(2) . . ?
Pt3 Ag19 Ag22 59.125(18) . . ?
Pt3 Ag19 Ag24 57.582(18) . . ?
Pt3 Ag19 Ag26 58.963(19) . 2_667 ?
Ag5 Ag19 Ag16 95.92(3) . . ?
Ag12 Ag19 Ag5 80.32(3) . . ?
Ag12 Ag19 Ag15 58.43(2) . . ?
Ag12 Ag19 Ag16 134.19(3) . . ?
Ag12 Ag19 Ag24 59.87(2) . . ?
Ag15 Ag19 Ag5 97.25(3) . . ?
Ag15 Ag19 Ag16 163.46(3) . . ?
Ag15 Ag19 Ag24 106.61(3) . . ?
Ag22 Ag19 Ag5 153.93(3) . . ?
Ag22 Ag19 Ag12 109.10(3) . . ?
Ag22 Ag19 Ag15 108.43(3) . . ?
Ag22 Ag19 Ag16 59.76(2) . . ?
Ag22 Ag19 Ag24 61.19(2) . . ?
Ag22 Ag19 Ag26 60.24(2) . 2_667 ?
Ag24 Ag19 Ag5 107.70(3) . . ?
Ag24 Ag19 Ag16 78.68(3) . . ?
Ag26 Ag19 Ag5 141.69(3) 2_667 . ?
Ag26 Ag19 Ag12 107.53(3) 2_667 . ?
Ag26 Ag19 Ag15 60.34(2) 2_667 . ?
Ag26 Ag19 Ag16 103.16(3) 2_667 . ?
Ag26 Ag19 Ag24 108.44(3) 2_667 . ?
S8 Ag19 Pt3 168.32(6) . . ?
S8 Ag19 Ag5 52.69(6) . . ?
S8 Ag19 Ag12 131.19(7) . . ?
S8 Ag19 Ag15 131.46(6) . . ?
S8 Ag19 Ag16 52.55(6) . . ?
S8 Ag19 Ag22 109.21(6) . . ?
S8 Ag19 Ag24 117.93(6) . . ?
S8 Ag19 Ag26 117.28(7) . 2_667 ?
Pt3 Ag22 Ag12 57.987(18) . 2_667 ?
Pt3 Ag22 Ag15 58.074(18) . 2_667 ?
Pt3 Ag22 Ag16 120.02(3) . . ?
Pt3 Ag22 Ag19 58.468(18) . . ?
Pt3 Ag22 Ag24 57.280(19) . . ?
Pt3 Ag22 Ag26 58.808(19) . 2_667 ?
Ag12 Ag22 Ag15 59.01(2) 2_667 2_667 ?
Ag12 Ag22 Ag16 167.28(3) 2_667 . ?
Ag12 Ag22 Ag24 105.59(3) 2_667 . ?
Ag12 Ag22 Ag26 61.10(2) 2_667 2_667 ?
Ag15 Ag22 Ag16 132.25(3) 2_667 . ?
Ag15 Ag22 Ag24 58.10(2) 2_667 . ?
Ag19 Ag22 Ag12 108.54(3) . 2_667 ?
Ag19 Ag22 Ag15 107.80(3) . 2_667 ?
Ag19 Ag22 Ag16 64.39(2) . . ?
Ag19 Ag22 Ag24 60.86(2) . . ?
Ag19 Ag22 Ag26 60.38(2) . 2_667 ?
Ag24 Ag22 Ag16 80.66(3) . . ?
Ag26 Ag22 Ag15 108.38(3) 2_667 2_667 ?
Ag26 Ag22 Ag16 106.59(3) 2_667 . ?
Ag26 Ag22 Ag24 108.29(3) 2_667 . ?
S24 Ag22 Pt3 167.46(7) . . ?
S24 Ag22 Ag12 125.45(7) . 2_667 ?
S24 Ag22 Ag15 134.47(7) . 2_667 ?
S24 Ag22 Ag16 53.49(7) . . ?
S24 Ag22 Ag19 111.10(7) . . ?
S24 Ag22 Ag24 125.96(8) . . ?
S24 Ag22 Ag26 110.88(7) . 2_667 ?
Pt3 Ag24 Ag12 57.635(18) . . ?
Pt3 Ag24 Ag15 59.067(18) . 2_667 ?
Pt3 Ag24 Ag18 140.36(3) . . ?
Pt3 Ag24 Ag19 57.620(18) . . ?
Pt3 Ag24 Ag22 57.946(19) . . ?
Pt3 Ag24 Ag26 59.420(19) . . ?
Ag12 Ag24 Ag18 107.92(3) . . ?
Ag12 Ag24 Ag19 59.38(2) . . ?
Ag12 Ag24 Ag22 106.11(3) . . ?
Ag15 Ag24 Ag12 109.10(3) 2_667 . ?
Ag15 Ag24 Ag18 141.48(3) 2_667 . ?
Ag15 Ag24 Ag19 107.16(3) 2_667 . ?
Ag15 Ag24 Ag22 60.23(2) 2_667 . ?
Ag15 Ag24 Ag26 61.76(2) 2_667 . ?
Ag19 Ag24 Ag18 82.97(3) . . ?
Ag19 Ag24 Ag22 57.96(2) . . ?
Ag22 Ag24 Ag18 99.33(3) . . ?
Ag26 Ag24 Ag12 60.92(2) . . ?
Ag26 Ag24 Ag18 151.10(4) . . ?
Ag26 Ag24 Ag19 108.73(3) . . ?
Ag26 Ag24 Ag22 109.31(3) . . ?
S30 Ag24 Pt3 163.62(8) . . ?
S30 Ag24 Ag12 115.93(7) . . ?
S30 Ag24 Ag15 115.49(7) . 2_667 ?
S30 Ag24 Ag18 54.35(8) . . ?
S30 Ag24 Ag19 134.77(7) . . ?
S30 Ag24 Ag22 135.21(8) . . ?
S30 Ag24 Ag26 104.21(8) . . ?
Pt3 Ag26 Ag12 57.272(19) . . ?
Pt3 Ag26 Ag15 57.844(19) . 2_667 ?
Pt3 Ag26 Ag19 58.041(19) . 2_667 ?
Pt3 Ag26 Ag22 58.53(2) . 2_667 ?
Pt3 Ag26 Ag24 58.44(2) . . ?
Pt3 Ag26 Ag33 125.24(3) . . ?
Ag12 Ag26 Ag33 83.09(3) . . ?
Ag15 Ag26 Ag12 106.87(3) 2_667 . ?
Ag15 Ag26 Ag33 110.25(3) 2_667 . ?
Ag19 Ag26 Ag12 106.33(3) 2_667 . ?
Ag19 Ag26 Ag15 60.62(2) 2_667 2_667 ?
Ag19 Ag26 Ag33 168.16(3) 2_667 . ?
Ag22 Ag26 Ag12 59.28(2) 2_667 . ?
Ag22 Ag26 Ag15 107.98(3) 2_667 2_667 ?
Ag22 Ag26 Ag19 59.39(2) 2_667 2_667 ?
Ag22 Ag26 Ag33 132.44(3) 2_667 . ?
Ag24 Ag26 Ag12 60.70(2) . . ?
Ag24 Ag26 Ag15 59.10(2) . 2_667 ?
Ag24 Ag26 Ag19 107.97(3) . 2_667 ?
Ag24 Ag26 Ag22 108.65(3) . 2_667 ?
Ag24 Ag26 Ag33 70.00(3) . . ?
S17 Ag26 Pt3 167.19(8) . . ?
S17 Ag26 Ag12 127.82(7) . . ?
S17 Ag26 Ag15 110.58(7) . 2_667 ?
S17 Ag26 Ag19 123.26(8) . 2_667 ?
S17 Ag26 Ag22 134.10(8) . 2_667 ?
S17 Ag26 Ag24 112.02(8) . . ?
S17 Ag26 Ag33 50.58(8) . . ?
Ag3 Ag33 Ag26 95.54(3) . . ?
S13 Ag33 Ag3 51.47(8) . . ?
S13 Ag33 Ag26 142.98(8) . . ?
S13 Ag33 S30 97.34(11) . . ?
S17 Ag33 Ag3 135.71(8) . . ?
S17 Ag33 Ag26 50.81(7) . . ?
S17 Ag33 S13 139.77(12) . . ?
S17 Ag33 S30 121.42(10) . . ?
S30 Ag33 Ag3 84.26(7) . . ?
S30 Ag33 Ag26 94.91(7) . . ?
Ag5 Ag34 Ag12 74.83(2) . . ?
Ag15 Ag34 Ag5 96.69(3) . . ?
Ag15 Ag34 Ag12 53.63(2) . . ?
S14 Ag34 Ag5 136.08(7) . . ?
S14 Ag34 Ag12 101.04(6) . . ?
S14 Ag34 Ag15 52.76(5) . . ?
S14 Ag34 S16 127.43(8) . . ?
S14 Ag34 S19 135.79(9) . . ?
S16 Ag34 Ag5 82.51(6) . . ?
S16 Ag34 Ag12 47.68(5) . . ?
S16 Ag34 Ag15 98.29(5) . . ?
S19 Ag34 Ag5 51.56(6) . . ?
S19 Ag34 Ag12 119.50(7) . . ?
S19 Ag34 Ag15 143.68(7) . . ?
S19 Ag34 S16 94.59(9) . . ?
Ag5 S8 Ag16 129.57(11) . . ?
Ag19 S8 Ag5 74.86(7) . . ?
Ag19 S8 Ag16 76.07(6) . . ?
C41 S8 Ag5 114.4(3) . . ?
C41 S8 Ag16 112.3(4) . . ?
C41 S8 Ag19 104.7(3) . . ?
Ag3 S13 Ag33 76.50(9) . . ?
C163 S13 Ag3 107.2(4) . . ?
C163 S13 Ag33 109.4(4) . . ?
Ag15 S14 Ag34 74.32(7) . . ?
C77 S14 Ag15 106.9(3) . . ?
C77 S14 Ag34 109.5(4) . . ?
Ag3 S16 Ag34 131.28(11) . . ?
Ag12 S16 Ag3 76.02(7) . . ?
Ag12 S16 Ag34 80.03(7) . . ?
C16 S16 Ag3 108.9(4) . . ?
C16 S16 Ag12 103.7(3) . . ?
C16 S16 Ag34 117.7(4) . . ?
Ag33 S17 Ag26 78.61(9) . . ?
C57 S17 Ag26 111.9(4) . . ?
C57 S17 Ag33 109.5(4) . . ?
Ag5 S19 Ag34 74.88(7) . . ?
C135 S19 Ag5 108.5(3) . . ?
C135 S19 Ag34 109.2(3) . . ?
Ag22 S24 Ag16 73.92(8) . . ?
C51 S24 Ag16 103.6(4) . . ?
C51 S24 Ag22 106.9(4) . . ?
Ag3 S26 Ag5 107.15(10) . . ?
Ag18 S26 Ag3 111.11(10) . . ?
Ag18 S26 Ag5 113.01(12) . . ?
C143 S26 Ag3 108.1(4) . . ?
C143 S26 Ag5 107.6(3) . . ?
C143 S26 Ag18 109.6(4) . . ?
Ag18 S27 Ag16 73.93(8) . . ?
C234 S27 Ag16 103.2(4) . . ?
C234 S27 Ag18 104.6(5) . . ?
Ag18 S30 Ag33 132.00(11) . . ?
Ag24 S30 Ag18 72.86(8) . . ?
Ag24 S30 Ag33 84.57(9) . . ?
C204 S30 Ag18 114.6(3) . . ?
C204 S30 Ag24 108.3(3) . . ?
C204 S30 Ag33 112.5(3) . . ?
C71 C6 Cl24 113.5(14) . . ?
C148 C6 Cl24 126.5(14) . . ?
C148 C6 C71 120.0(16) . . ?
C41 C13 H13 118.3 . . ?
C121 C13 H13 118.3 . . ?
C121 C13 C41 123.5(11) . . ?
C49 C16 S16 118.6(9) . . ?
C86 C16 S16 121.5(9) . . ?
C86 C16 C49 119.7(11) . . ?
C89 C26 H26 119.3 . . ?
C174 C26 H26 119.3 . . ?
C174 C26 C89 121.4(15) . . ?
C13 C41 S8 121.6(8) . . ?
C13 C41 C181 117.2(12) . . ?
C181 C41 S8 120.9(10) . . ?
C16 C49 H49 120.6 . . ?
C16 C49 C191 118.9(11) . . ?
C191 C49 H49 120.6 . . ?
C108 C51 S24 121.3(8) . . ?
C108 C51 C187 120.4(11) . . ?
C187 C51 S24 118.1(9) . . ?
C165 C52 Br10 121.3(13) . . ?
C221 C52 C165 118.7(14) . . ?
C221 C52 Br10 119.9(12) . . ?
C174 C57 S17 121.1(10) . . ?
C177 C57 S17 122.2(9) . . ?
C177 C57 C174 116.6(12) . . ?
C6 C71 H71 121.7 . . ?
C231 C71 C6 116.7(16) . . ?
C231 C71 H71 121.7 . . ?
C100 C77 S14 119.4(8) . . ?
C149 C77 S14 124.6(8) . . ?
C149 C77 C100 116.0(10) . . ?
C16 C86 H86 118.7 . . ?
C16 C86 C207 122.6(12) . . ?
C207 C86 H86 118.7 . . ?
C26 C89 Cl30 121.6(13) . . ?
C26 C89 C203 118.8(14) . . ?
C203 C89 Cl30 119.6(13) . . ?
C77 C100 Cl16 121.5(9) . . ?
C232 C100 Cl16 119.0(9) . . ?
C232 C100 C77 119.5(12) . . ?
C51 C108 H108 119.7 . . ?
C51 C108 C173 120.5(11) . . ?
C173 C108 H108 119.7 . . ?
C200 C109 H109 120.0 . . ?
C200 C109 C204 120.0 . . ?
C204 C109 H109 120.0 . . ?
C109 C200 H200 120.0 . . ?
C109 C200 C5 120.0 . . ?
C5 C200 H200 120.0 . . ?
C200 C5 Br31 120.9(7) . . ?
C202 C5 C200 120.0 . . ?
C202 C5 Br31 119.1(7) . . ?
C5 C202 H202 120.0 . . ?
C5 C202 C111 120.0 . . ?
C111 C202 H202 120.0 . . ?
C202 C111 H111 120.0 . . ?
C202 C111 C204 120.0 . . ?
C204 C111 H111 120.0 . . ?
C109 C204 S30 120.7(6) . . ?
C111 C204 S30 119.0(6) . . ?
C111 C204 C109 120.0 . . ?
C13 C121 H121 119.1 . . ?
C13 C121 C230 121.8(12) . . ?
C230 C121 H121 119.1 . . ?
C173 C129 Cl22 119.8(12) . . ?
C193 C129 Cl22 118.4(10) . . ?
C193 C129 C173 121.8(12) . . ?
C43 C135 S19 123.7(4) . . ?
C43 C135 C144 120.0 . . ?
C144 C135 S19 116.0(5) . . ?
C135 C43 H43 120.0 . . ?
C138 C43 C135 120.0 . . ?
C138 C43 H43 120.0 . . ?
C43 C138 H138 120.0 . . ?
C43 C138 C140 120.0 . . ?
C140 C138 H138 120.0 . . ?
C138 C140 Br13 112.3(6) . . ?
C142 C140 C138 120.0 . . ?
C142 C140 Br13 127.6(6) . . ?
C140 C142 H142 120.0 . . ?
C140 C142 C144 120.0 . . ?
C144 C142 H142 120.0 . . ?
C135 C144 Cl20 117.8(5) . . ?
C142 C144 Cl20 121.3(5) . . ?
C142 C144 C135 120.0 . . ?
C264 C141 H141 120.0 . . ?
C264 C141 C268 120.0 . . ?
C268 C141 H141 120.0 . . ?
C141 C264 Br29 122.3(6) . . ?
C80 C264 C141 120.0 . . ?
C80 C264 Br29 117.4(6) . . ?
C264 C80 H80 120.0 . . ?
C264 C80 C266 120.0 . . ?
C266 C80 H80 120.0 . . ?
C80 C266 H266 120.0 . . ?
C143 C266 C80 120.0 . . ?
C143 C266 H266 120.0 . . ?
C266 C143 S26 119.6(6) . . ?
C266 C143 C268 120.0 . . ?
C268 C143 S26 120.4(6) . . ?
C141 C268 H268 120.0 . . ?
C143 C268 C141 120.0 . . ?
C143 C268 H268 120.0 . . ?
C6 C148 H148 118.8 . . ?
C6 C148 C167 122.3(16) . . ?
C167 C148 H148 118.8 . . ?
C77 C149 H149 117.8 . . ?
C267 C149 C77 124.4(11) . . ?
C267 C149 H149 117.8 . . ?
C181 C157 H157 118.4 . . ?
C181 C157 C230 123.1(12) . . ?
C230 C157 H157 118.4 . . ?
C167 C163 S13 121.6(11) . . ?
C167 C163 C231 116.8(13) . . ?
C231 C163 S13 121.6(10) . . ?
C52 C165 H165 120.0 . . ?
C238 C165 C52 119.9(14) . . ?
C238 C165 H165 120.0 . . ?
C148 C167 Cl36 118.0(12) . . ?
C148 C167 C163 121.7(15) . . ?
C163 C167 Cl36 120.2(11) . . ?
C108 C173 H173 120.9 . . ?
C129 C173 C108 118.2(13) . . ?
C129 C173 H173 120.9 . . ?
C26 C174 Cl18 119.2(12) . . ?
C26 C174 C57 121.7(15) . . ?
C57 C174 Cl18 119.0(12) . . ?
C57 C177 H177 119.4 . . ?
C203 C177 C57 121.2(13) . . ?
C203 C177 H177 119.4 . . ?
C41 C181 H181 120.0 . . ?
C157 C181 C41 120.1(13) . . ?
C157 C181 H181 120.0 . . ?
C51 C187 Cl39 125.5(11) . . ?
C193 C187 Cl39 116.3(10) . . ?
C193 C187 C51 118.1(13) . . ?
C49 C191 H191 120.9 . . ?
C228 C191 C49 118.2(11) . . ?
C228 C191 H191 120.9 . . ?
C129 C193 C187 120.7(12) . . ?
C129 C193 H193 119.7 . . ?
C187 C193 H193 119.7 . . ?
C89 C203 H203 119.9 . . ?
C177 C203 C89 120.2(14) . . ?
C177 C203 H203 119.9 . . ?
C86 C207 H207 121.5 . . ?
C228 C207 C86 117.1(12) . . ?
C228 C207 H207 121.5 . . ?
C221 C219 Cl1 115.4(13) . . ?
C221 C219 C234 123.6(15) . . ?
C234 C219 Cl1 120.0(11) . . ?
C52 C221 C219 119.0(16) . . ?
C52 C221 H221 120.5 . . ?
C219 C221 H221 120.5 . . ?
C191 C228 C207 123.6(11) . . ?
C191 C228 Br23 119.0(9) . . ?
C207 C228 Br23 117.3(10) . . ?
C121 C230 C157 114.2(12) . . ?
C121 C230 Br12 123.0(10) . . ?
C157 C230 Br12 122.7(9) . . ?
C71 C231 H231 118.8 . . ?
C163 C231 C71 122.5(14) . . ?
C163 C231 H231 118.8 . . ?
C100 C232 H232 118.6 . . ?
C262 C232 C100 122.7(12) . . ?
C262 C232 H232 118.6 . . ?
C219 C234 S27 118.6(10) . . ?
C238 C234 S27 126.4(11) . . ?
C238 C234 C219 114.2(13) . . ?
C165 C238 C234 124.2(13) . . ?
C165 C238 H238 117.9 . . ?
C234 C238 H238 117.9 . . ?
C232 C262 C267 119.5(13) . . ?
C232 C262 Br14 119.5(10) . . ?
C267 C262 Br14 121.0(12) . . ?
C149 C267 C262 117.8(13) . . ?
C149 C267 H267 121.1 . . ?
C262 C267 H267 121.1 . . ?
C68 P1 C84 110.6(5) . . ?
C104 P1 C68 108.5(5) . . ?
C104 P1 C84 110.0(5) . . ?
C104 P1 C119 110.1(5) . . ?
C119 P1 C68 109.1(5) . . ?
C119 P1 C84 108.7(5) . . ?
C20 C1 H1 120.2 . . ?
C20 C1 C211 119.6(11) . . ?
C211 C1 H1 120.2 . . ?
C38 C10 H10 119.6 . . ?
C38 C10 C47 120.8(11) . . ?
C47 C10 H10 119.6 . . ?
C104 C17 H17 119.7 . . ?
C212 C17 H17 119.7 . . ?
C212 C17 C104 120.6(11) . . ?
C1 C20 H20 120.6 . . ?
C1 C20 C68 118.8(11) . . ?
C68 C20 H20 120.6 . . ?
C175 C29 H29 120.1 . . ?
C175 C29 C211 119.7(13) . . ?
C211 C29 H29 120.1 . . ?
C10 C38 H38 120.1 . . ?
C10 C38 C62 119.8(12) . . ?
C62 C38 H38 120.1 . . ?
C10 C47 H47 120.1 . . ?
C131 C47 C10 119.9(12) . . ?
C131 C47 H47 120.1 . . ?
C38 C62 H62 120.3 . . ?
C119 C62 C38 119.4(11) . . ?
C119 C62 H62 120.3 . . ?
C20 C68 P1 119.6(8) . . ?
C175 C68 P1 120.1(8) . . ?
C175 C68 C20 119.4(10) . . ?
C153 C84 P1 118.1(8) . . ?
C153 C84 C179 121.9(11) . . ?
C179 C84 P1 118.9(8) . . ?
C133 C88 H88 120.1 . . ?
C153 C88 H88 120.1 . . ?
C153 C88 C133 119.8(11) . . ?
C17 C104 P1 120.0(8) . . ?
C17 C104 C115 117.4(10) . . ?
C115 C104 P1 122.5(9) . . ?
C104 C115 H115 118.9 . . ?
C189 C115 C104 122.2(11) . . ?
C189 C115 H115 118.9 . . ?
C62 C119 P1 122.8(9) . . ?
C62 C119 C131 119.5(10) . . ?
C131 C119 P1 117.7(9) . . ?
C47 C131 C119 120.5(12) . . ?
C47 C131 H131 119.8 . . ?
C119 C131 H131 119.8 . . ?
C88 C133 H133 119.5 . . ?
C199 C133 C88 121.0(13) . . ?
C199 C133 H133 119.5 . . ?
C84 C153 H153 121.4 . . ?
C88 C153 C84 117.1(11) . . ?
C88 C153 H153 121.4 . . ?
C29 C175 C68 121.2(12) . . ?
C29 C175 H175 119.4 . . ?
C68 C175 H175 119.4 . . ?
C84 C179 H179 121.0 . . ?
C199 C179 C84 118.0(11) . . ?
C199 C179 H179 121.0 . . ?
C115 C189 H189 120.5 . . ?
C115 C189 C240 119.0(11) . . ?
C240 C189 H189 120.5 . . ?
C133 C199 H199 119.2 . . ?
C179 C199 C133 121.7(12) . . ?
C179 C199 H199 119.2 . . ?
C1 C211 H211 119.4 . . ?
C29 C211 C1 121.1(12) . . ?
C29 C211 H211 119.4 . . ?
C17 C212 H212 119.4 . . ?
C17 C212 C240 121.3(12) . . ?
C240 C212 H212 119.4 . . ?
C189 C240 C212 119.2(11) . . ?
C189 C240 H240 120.4 . . ?
C212 C240 H240 120.4 . . ?
C156 P2 C190 111.5(5) . . ?
C156 P2 C150 109.8(7) . . ?
C156 P2 C236 107.8(7) . . ?
C190 P2 C236 108.9(7) . . ?
C150 P2 C190 106.5(6) . . ?
C150 P2 C236 112.3(6) . . ?
C154 C15 H15 120.0 . . ?
C154 C15 C158 120.0 . . ?
C158 C15 H15 120.0 . . ?
C15 C154 H154 120.0 . . ?
C87 C154 C15 120.0 . . ?
C87 C154 H154 120.0 . . ?
C154 C87 H87 120.0 . . ?
C154 C87 C156 120.0 . . ?
C156 C87 H87 120.0 . . ?
C87 C156 P2 120.5(5) . . ?
C50 C156 P2 119.4(5) . . ?
C50 C156 C87 120.0 . . ?
C156 C50 H50 120.0 . . ?
C156 C50 C158 120.0 . . ?
C158 C50 H50 120.0 . . ?
C15 C158 H158 120.0 . . ?
C50 C158 C15 120.0 . . ?
C50 C158 H158 120.0 . . ?
C194 C37 H37 118.6 . . ?
C194 C37 C237 123(2) . . ?
C237 C37 H37 118.6 . . ?
C67 C63 H63 120.0 . . ?
C67 C63 C223 120.0 . . ?
C223 C63 H63 120.0 . . ?
C63 C67 H67 120.0 . . ?
C233 C67 C63 120.0 . . ?
C233 C67 H67 120.0 . . ?
C67 C233 H233 120.0 . . ?
C67 C233 C190 120.0 . . ?
C190 C233 H233 120.0 . . ?
C233 C190 P2 119.4(5) . . ?
C105 C190 P2 120.5(5) . . ?
C105 C190 C233 120.0 . . ?
C190 C105 H105 120.0 . . ?
C190 C105 C223 120.0 . . ?
C223 C105 H105 120.0 . . ?
C63 C223 H223 120.0 . . ?
C105 C223 C63 120.0 . . ?
C105 C223 H223 120.0 . . ?
C194 C74 H74 121.3 . . ?
C236 C74 H74 121.3 . . ?
C236 C74 C194 117(2) . . ?
C164 C83 H83 121.0 . . ?
C164 C83 C188 118.1(16) . . ?
C188 C83 H83 121.0 . . ?
C150 C107 H107 119.5 . . ?
C150 C107 C162 121.0(15) . . ?
C162 C107 H107 119.5 . . ?
C236 C120 H120 119.3 . . ?
C236 C120 C237 121(2) . . ?
C237 C120 H120 119.3 . . ?
C107 C150 P2 122.8(12) . . ?
C107 C150 C188 117.3(13) . . ?
C188 C150 P2 119.2(11) . . ?
C107 C162 H162 120.4 . . ?
C107 C162 C164 119.2(14) . . ?
C164 C162 H162 120.4 . . ?
C83 C164 C162 119.2(14) . . ?
C83 C164 H164 120.4 . . ?
C162 C164 H164 120.4 . . ?
C83 C188 H188 117.5 . . ?
C150 C188 C83 125.0(15) . . ?
C150 C188 H188 117.5 . . ?
C37 C194 C74 121(2) . . ?
C37 C194 H194 119.5 . . ?
C74 C194 H194 119.5 . . ?
C74 C236 P2 119.5(16) . . ?
C74 C236 C120 122.1(18) . . ?
C120 C236 P2 118.4(15) . . ?
C37 C237 C120 115(2) . . ?
C37 C237 H237 122.6 . . ?
C120 C237 H237 122.6 . . ?
C42 P3 C261 108.9(6) . . ?
C248 P3 C42 108.6(8) . . ?
C248 P3 C261 113.4(6) . . ?
C269 P3 C42 109.4(7) . . ?
C269 P3 C261 107.7(7) . . ?
C269 P3 C248 108.8(8) . . ?
C137 C11 H11 122.4 . . ?
C160 C11 H11 122.4 . . ?
C160 C11 C137 115.1(17) . . ?
C176 C33 H33 118.0 . . ?
C176 C33 C186 124.1(16) . . ?
C186 C33 H33 118.0 . . ?
C253 C76 H76 120.0 . . ?
C253 C76 C257 120.0 . . ?
C257 C76 H76 120.0 . . ?
C76 C253 H253 120.0 . . ?
C136 C253 C76 120.0 . . ?
C136 C253 H253 120.0 . . ?
C253 C136 H136 120.0 . . ?
C253 C136 C255 120.0 . . ?
C255 C136 H136 120.0 . . ?
C136 C255 H255 120.0 . . ?
C42 C255 C136 120.0 . . ?
C42 C255 H255 120.0 . . ?
C255 C42 P3 122.1(7) . . ?
C255 C42 C257 120.0 . . ?
C257 C42 P3 117.9(7) . . ?
C76 C257 H257 120.0 . . ?
C42 C257 C76 120.0 . . ?
C42 C257 H257 120.0 . . ?
C260 C78 H78 120.0 . . ?
C260 C78 C263 120.0 . . ?
C263 C78 H78 120.0 . . ?
C78 C260 H260 120.0 . . ?
C78 C260 C139 120.0 . . ?
C139 C260 H260 120.0 . . ?
C260 C139 H139 120.0 . . ?
C260 C139 C261 120.0 . . ?
C261 C139 H139 120.0 . . ?
C139 C261 P3 121.3(6) . . ?
C139 C261 C4 120.0 . . ?
C4 C261 P3 118.4(6) . . ?
C261 C4 H4 120.0 . . ?
C263 C4 C261 120.0 . . ?
C263 C4 H4 120.0 . . ?
C78 C263 H263 120.0 . . ?
C4 C263 C78 120.0 . . ?
C4 C263 H263 120.0 . . ?
C160 C91 H91 119.0 . . ?
C160 C91 C248 121.9(16) . . ?
C248 C91 H91 119.0 . . ?
C176 C128 H128 118.9 . . ?
C176 C128 C269 122.1(17) . . ?
C269 C128 H128 118.9 . . ?
C11 C137 H137 119.1 . . ?
C198 C137 C11 121.8(17) . . ?
C198 C137 H137 119.1 . . ?
C11 C160 H160 117.8 . . ?
C91 C160 C11 124.4(16) . . ?
C91 C160 H160 117.8 . . ?
C186 C166 H166 119.2 . . ?
C269 C166 H166 119.2 . . ?
C269 C166 C186 121.6(15) . . ?
C33 C176 C128 118.9(15) . . ?
C33 C176 H176 120.5 . . ?
C128 C176 H176 120.5 . . ?
C33 C186 C166 115.7(16) . . ?
C33 C186 H186 122.1 . . ?
C166 C186 H186 122.1 . . ?
C137 C198 H198 118.7 . . ?
C137 C198 C248 122.5(16) . . ?
C248 C198 H198 118.7 . . ?
C91 C248 P3 122.6(13) . . ?
C91 C248 C198 113.7(16) . . ?
C198 C248 P3 123.7(12) . . ?
C128 C269 P3 125.1(14) . . ?
C128 C269 C166 117.2(16) . . ?
C166 C269 P3 117.8(12) . . ?
C183 P4 C155 111.8(6) . . ?
C183 P4 C195 112.6(5) . . ?
C183 P4 C205 105.6(6) . . ?
C155 P4 C195 108.4(6) . . ?
C155 P4 C205 109.8(6) . . ?
C195 P4 C205 108.7(7) . . ?
C155 C14 H14 118.6 . . ?
C155 C14 C213 122.7(12) . . ?
C213 C14 H14 118.6 . . ?
C85 C48 H48 119.6 . . ?
C85 C48 C205 120.8(16) . . ?
C205 C48 H48 119.6 . . ?
C65 C54 H54 118.1 . . ?
C195 C54 H54 118.1 . . ?
C195 C54 C65 123.8(17) . . ?
C152 C58 H58 120.0 . . ?
C152 C58 C185 120.0 . . ?
C185 C58 H58 120.0 . . ?
C58 C152 H152 120.0 . . ?
C58 C152 C183 120.0 . . ?
C183 C152 H152 120.0 . . ?
C152 C183 P4 119.9(5) . . ?
C209 C183 P4 119.8(5) . . ?
C209 C183 C152 120.0 . . ?
C183 C209 H209 120.0 . . ?
C183 C209 C96 120.0 . . ?
C96 C209 H209 120.0 . . ?
C209 C96 H96 120.0 . . ?
C185 C96 C209 120.0 . . ?
C185 C96 H96 120.0 . . ?
C58 C185 H185 120.0 . . ?
C96 C185 C58 120.0 . . ?
C96 C185 H185 120.0 . . ?
C54 C65 H65 121.4 . . ?
C178 C65 C54 117.3(19) . . ?
C178 C65 H65 121.4 . . ?
C48 C85 H85 119.4 . . ?
C48 C85 C103 121.1(15) . . ?
C103 C85 H85 119.4 . . ?
C213 C97 H97 118.6 . . ?
C213 C97 C258 122.7(12) . . ?
C258 C97 H97 118.6 . . ?
C85 C103 H103 120.5 . . ?
C85 C103 C192 118.9(14) . . ?
C192 C103 H103 120.6 . . ?
C14 C155 P4 122.8(9) . . ?
C14 C155 C239 117.4(11) . . ?
C239 C155 P4 119.7(8) . . ?
C65 C178 H178 119.4 . . ?
C65 C178 C275 121.2(16) . . ?
C275 C178 H178 119.4 . . ?
C103 C192 H192 119.2 . . ?
C103 C192 C244 121.5(16) . . ?
C244 C192 H192 119.2 . . ?
C54 C195 P4 122.0(12) . . ?
C54 C195 C197 117.5(13) . . ?
C197 C195 P4 120.3(12) . . ?
C195 C197 H197 118.6 . . ?
C275 C197 C195 122.8(16) . . ?
C275 C197 H197 118.6 . . ?
C48 C205 P4 120.8(12) . . ?
C48 C205 C244 119.9(13) . . ?
C244 C205 P4 119.3(10) . . ?
C14 C213 H213 120.9 . . ?
C97 C213 C14 118.3(12) . . ?
C97 C213 H213 120.9 . . ?
C155 C239 H239 118.7 . . ?
C258 C239 C155 122.6(14) . . ?
C258 C239 H239 118.7 . . ?
C192 C244 C205 117.7(14) . . ?
C192 C244 H244 121.2 . . ?
C205 C244 H244 121.2 . . ?
C97 C258 H258 122.1 . . ?
C239 C258 C97 115.8(14) . . ?
C239 C258 H258 122.1 . . ?
C178 C275 H275 121.5 . . ?
C197 C275 C178 117.0(15) . . ?
C197 C275 H275 121.5 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Ag1 S4 C7 C24 -177.1(7) . . . . ?
Ag1 S4 C7 C60 -3.9(9) . . . . ?
Ag4 S1 C12 C18 -104.5(7) . . . . ?
Ag4 S1 C12 C22 83.4(8) . . . . ?
Ag6 S10 C224 C222 -177.7(4) . . . . ?
Ag6 S10 C224 C226 -0.9(5) . . . . ?
Ag8 S12 C70 C151 -87.8(8) . . . . ?
Ag8 S12 C70 C242 97.2(9) . . . . ?
Ag9 S6 C3 C31 -169.0(7) . . . . ?
Ag9 S6 C3 C36 12.5(9) . . . . ?
Ag9 S10 C224 C222 101.1(4) . . . . ?
Ag9 S10 C224 C226 -82.1(5) . . . . ?
Ag9 S21 C171 C28 1.3(5) . . . . ?
Ag9 S21 C171 C61 177.4(3) . . . . ?
Ag10 S6 C3 C31 -82.5(8) . . . . ?
Ag10 S6 C3 C36 98.9(8) . . . . ?
Ag11 S12 C70 C151 -6.2(10) . . . . ?
Ag11 S12 C70 C242 178.8(7) . . . . ?
Ag11 S18 C27 C90 -89.7(8) . . . . ?
Ag11 S18 C27 C125 90.5(9) . . . . ?
Ag11 S20 C102 C127 -165.4(8) . . . . ?
Ag11 S20 C102 C169 12.7(10) . . . . ?
Ag17 S22 C44 C53 -0.2(10) . . . . ?
Ag17 S22 C44 C123 -173.2(8) . . . . ?
Ag27 S5 C98 C110 -109.5(9) . . . . ?
Ag27 S5 C98 C215 72.1(11) . . . . ?
Ag27 S6 C3 C31 -1.6(9) . . . . ?
Ag27 S6 C3 C36 179.9(7) . . . . ?
Ag27 S18 C27 C90 147.8(7) . . . . ?
Ag27 S18 C27 C125 -32.0(9) . . . . ?
Ag28 S1 C12 C18 176.1(6) . . . . ?
Ag28 S1 C12 C22 4.0(8) . . . . ?
Ag28 S4 C7 C24 105.7(8) . . . . ?
Ag28 S4 C7 C60 -81.1(9) . . . . ?
Ag28 S20 C102 C127 115.9(8) . . . . ?
Ag28 S20 C102 C169 -66.0(10) . . . . ?
Ag29 S5 C98 C110 -28.1(10) . . . . ?
Ag29 S5 C98 C215 153.5(10) . . . . ?
Ag29 S12 C70 C151 -175.3(8) . . . . ?
Ag29 S12 C70 C242 9.7(10) . . . . ?
Ag29 S22 C44 C53 -85.1(9) . . . . ?
Ag29 S22 C44 C123 101.9(9) . . . . ?
Ag32 S1 C12 C18 -23.9(8) . . . . ?
Ag32 S1 C12 C22 164.0(7) . . . . ?
Ag32 S18 C27 C90 34.8(9) . . . . ?
Ag32 S18 C27 C125 -145.0(8) . . . . ?
Ag32 S21 C171 C28 -80.2(4) . . . . ?
Ag32 S21 C171 C61 95.8(4) . . . . ?
Cl4 C24 C64 C79 179.9(9) . . . . ?
Cl6 C222 C224 S10 -4.5(8) . . . . ?
Cl6 C222 C224 C226 178.7(8) . . . . ?
Cl21 C2 C75 C53 -178.5(8) . . . . ?
Cl21 C2 C92 C123 179.0(9) . . . . ?
Cl33 C61 C235 C30 175.0(5) . . . . ?
S1 C12 C18 C34 -171.5(8) . . . . ?
S1 C12 C22 C66 171.4(8) . . . . ?
S4 C7 C24 Cl4 -5.4(13) . . . . ?
S4 C7 C24 C64 175.3(8) . . . . ?
S4 C7 C60 C55 -172.7(9) . . . . ?
S5 C98 C110 C161 -177.2(8) . . . . ?
S5 C98 C215 Cl23 -3.8(16) . . . . ?
S5 C98 C215 C59 177.8(11) . . . . ?
S6 C3 C31 C72 -175.2(8) . . . . ?
S6 C3 C36 C40 179.3(8) . . . . ?
S10 C224 C226 C217 -176.8(6) . . . . ?
S12 C70 C151 C117 -176.5(9) . . . . ?
S12 C70 C242 C8 176.1(9) . . . . ?
S18 C27 C90 C265 178.3(9) . . . . ?
S18 C27 C125 C46 -180.0(9) . . . . ?
S20 C102 C127 Cl37 -2.9(14) . . . . ?
S20 C102 C127 C112 174.2(9) . . . . ?
S20 C102 C169 C94 -174.6(9) . . . . ?
S21 C171 C61 Cl33 8.8(6) . . . . ?
S21 C171 C61 C235 -176.2(6) . . . . ?
S22 C44 C53 C75 -173.2(8) . . . . ?
S22 C44 C123 Cl7 -7.7(14) . . . . ?
S22 C44 C123 C92 173.7(9) . . . . ?
C2 C92 C123 Cl7 -178.3(10) . . . . ?
C2 C92 C123 C44 0.2(19) . . . . ?
C3 C31 C72 C81 -2.4(16) . . . . ?
C3 C36 C40 C81 -5.6(16) . . . . ?
C7 C24 C64 C79 -0.7(16) . . . . ?
C12 C18 C34 C159 0.9(15) . . . . ?
C12 C22 C66 C159 -1.0(15) . . . . ?
C18 C12 C22 C66 -0.5(15) . . . . ?
C18 C34 C159 C66 -2.4(16) . . . . ?
C18 C34 C159 Br21 179.9(8) . . . . ?
C22 C12 C18 C34 0.6(14) . . . . ?
C22 C66 C159 C34 2.4(16) . . . . ?
C22 C66 C159 Br21 -179.8(8) . . . . ?
C24 C7 C60 C55 0.8(16) . . . . ?
C24 C64 C79 Cl27 -177.2(8) . . . . ?
C24 C64 C79 C55 -2.8(17) . . . . ?
C27 C90 C265 C196 2(2) . . . . ?
C30 C126 C28 C171 0.0 . . . . ?
C126 C30 C235 C61 0.0 . . . . ?
C126 C28 C171 S21 175.9(6) . . . . ?
C126 C28 C171 C61 0.0 . . . . ?
C28 C171 C61 Cl33 -175.0(5) . . . . ?
C28 C171 C61 C235 0.0 . . . . ?
C171 C61 C235 C30 0.0 . . . . ?
C235 C30 C126 C28 0.0 . . . . ?
C31 C3 C36 C40 0.8(15) . . . . ?
C31 C72 C81 C40 -2.5(17) . . . . ?
C31 C72 C81 Br22 -176.8(8) . . . . ?
C36 C3 C31 C72 3.4(15) . . . . ?
C36 C40 C81 C72 6.5(17) . . . . ?
C36 C40 C81 Br22 -179.4(8) . . . . ?
C44 C53 C75 C2 -1.3(16) . . . . ?
C46 C196 C265 C90 -1(2) . . . . ?
C53 C44 C123 Cl7 179.0(8) . . . . ?
C53 C44 C123 C92 0.4(17) . . . . ?
C60 C7 C24 Cl4 -179.0(9) . . . . ?
C60 C7 C24 C64 1.7(15) . . . . ?
C60 C55 C79 Cl27 179.6(9) . . . . ?
C60 C55 C79 C64 5.3(18) . . . . ?
C75 C2 C92 C123 -1.5(18) . . . . ?
C79 C55 C60 C7 -4.3(18) . . . . ?
C90 C27 C125 C46 0.3(16) . . . . ?
C92 C2 C75 C53 2.0(16) . . . . ?
C94 C106 C112 C127 -2.4(19) . . . . ?
C98 C110 C161 C201 -3.1(16) . . . . ?
C106 C94 C169 C102 -2.4(17) . . . . ?
C106 C112 C127 Cl37 -179.2(10) . . . . ?
C106 C112 C127 C102 3.6(18) . . . . ?
C110 C98 C215 Cl23 177.6(9) . . . . ?
C110 C98 C215 C59 -1(2) . . . . ?
C110 C161 C201 Cl5 -177.2(8) . . . . ?
C110 C161 C201 C59 4.4(18) . . . . ?
C123 C44 C53 C75 0.1(16) . . . . ?
C125 C27 C90 C265 -1.9(16) . . . . ?
C125 C46 C196 C265 -1(2) . . . . ?
C125 C46 C196 Br28 179.7(9) . . . . ?
C127 C102 C169 C94 3.5(16) . . . . ?
C151 C70 C242 C8 1.0(17) . . . . ?
C151 C117 C246 C8 1(2) . . . . ?
C151 C117 C246 Br27 177.8(9) . . . . ?
C169 C94 C106 C112 1.7(18) . . . . ?
C169 C94 C106 Br24 178.4(8) . . . . ?
C169 C102 C127 Cl37 178.9(9) . . . . ?
C169 C102 C127 C112 -4.1(16) . . . . ?
C196 C46 C125 C27 1.1(17) . . . . ?
C201 C59 C215 Cl23 -176.2(12) . . . . ?
C201 C59 C215 C98 2(2) . . . . ?
C215 C59 C201 Cl5 177.8(11) . . . . ?
C215 C59 C201 C161 -4(2) . . . . ?
C215 C98 C110 C161 1.4(16) . . . . ?
C217 C25 C220 C222 0.0 . . . . ?
C25 C217 C226 C224 0.0 . . . . ?
C25 C220 C222 Cl6 -178.8(7) . . . . ?
C25 C220 C222 C224 0.0 . . . . ?
C220 C222 C224 S10 176.8(6) . . . . ?
C220 C222 C224 C226 0.0 . . . . ?
C222 C224 C226 C217 0.0 . . . . ?
C226 C217 C25 C220 0.0 . . . . ?
C226 C217 C25 Br1 -176.7(8) . . . . ?
C242 C8 C246 C117 -1(2) . . . . ?
C242 C8 C246 Br27 -178.4(10) . . . . ?
C242 C70 C151 C117 -1.5(16) . . . . ?
C246 C8 C242 C70 0.4(19) . . . . ?
C246 C117 C151 C70 0.6(19) . . . . ?
Br1 C25 C220 C222 176.9(7) . . . . ?
Br2 C30 C126 C28 -179.0(6) . . . . ?
Br2 C30 C235 C61 178.8(7) . . . . ?
Br24 C106 C112 C127 -179.2(9) . . . . ?
Br28 C196 C265 C90 178.6(9) . . . . ?
Ag2 S2 C9 C168 -19.7(6) . . . . ?
Ag2 S2 C9 C170 155.1(4) . . . . ?
Ag2 S7 C274 C23 -40.0(7) . . . . ?
Ag2 S7 C274 C147 153.6(7) . . . . ?
Ag2 S23 C251 C132 102.7(5) . . . . ?
Ag2 S23 C251 C134 -84.2(5) . . . . ?
Ag7 S9 C56 C180 110.1(4) . . . . ?
Ag7 S9 C56 C182 -70.3(5) . . . . ?
Ag7 S15 C69 C227 -177.5(3) . . . . ?
Ag7 S15 C69 C229 5.9(5) . . . . ?
Ag7 S28 C130 C241 8.5(7) . . . . ?
Ag7 S28 C130 C243 -167.5(5) . . . . ?
Ag13 S9 C56 C180 -170.2(4) . . . . ?
Ag13 S9 C56 C182 9.5(5) . . . . ?
Ag14 S25 C210 C35 -172.2(4) . . . . ?
Ag14 S25 C210 C114 4.3(7) . . . . ?
Ag20 S3 C118 C214 162.9(6) . . . . ?
Ag20 S3 C118 C218 -25.6(8) . . . . ?
Ag20 S7 C274 C23 -115.3(6) . . . . ?
Ag20 S7 C274 C147 78.4(8) . . . . ?
Ag20 S11 C254 C252 -124.3(5) . . . . ?
Ag20 S11 C254 C256 55.8(6) . . . . ?
Ag21 S15 C69 C227 -95.4(4) . . . . ?
Ag21 S15 C69 C229 88.0(4) . . . . ?
Ag23 S23 C251 C132 -175.4(4) . . . . ?
Ag23 S23 C251 C134 -2.4(6) . . . . ?
Ag25 S3 C118 C214 80.6(7) . . . . ?
Ag25 S3 C118 C218 -107.9(6) . . . . ?
Ag30 S2 C9 C168 66.1(5) . . . . ?
Ag30 S2 C9 C170 -119.1(5) . . . . ?
Ag31 S2 C9 C168 151.5(4) . . . . ?
Ag31 S2 C9 C170 -33.7(6) . . . . ?
Ag31 S11 C254 C252 -7.7(7) . . . . ?
Ag31 S11 C254 C256 172.5(5) . . . . ?
Ag31 S28 C130 C241 -71.4(6) . . . . ?
Ag31 S28 C130 C243 112.6(6) . . . . ?
Ag35 S11 C254 C252 113.8(5) . . . . ?
Ag35 S11 C254 C256 -66.1(6) . . . . ?
Ag35 S15 C69 C227 -11.0(5) . . . . ?
Ag35 S15 C69 C229 172.4(3) . . . . ?
Ag35 S29 C145 C270 89.9(9) . . . . ?
Ag35 S29 C145 C271 -84.7(11) . . . . ?
Ag36 S3 C118 C214 -7.0(8) . . . . ?
Ag36 S3 C118 C218 164.5(6) . . . . ?
Ag36 S25 C210 C35 102.4(5) . . . . ?
Ag36 S25 C210 C114 -81.1(6) . . . . ?
Ag36 S29 C145 C270 171.9(6) . . . . ?
Ag36 S29 C145 C271 -2.6(13) . . . . ?
Cl3 C21 C249 C134 178.6(8) . . . . ?
Cl8 C35 C210 S25 -1.6(9) . . . . ?
Cl8 C35 C210 C114 -178.0(10) . . . . ?
Cl11 C243 C73 C245 -179.3(9) . . . . ?
Cl15 C270 C145 S29 23.9(8) . . . . ?
Cl15 C270 C145 C271 -161.5(12) . . . . ?
Cl17 C180 C56 S9 0.8(7) . . . . ?
Cl17 C180 C56 C182 -178.9(7) . . . . ?
Cl19 C146 C273 C23 -179.4(5) . . . . ?
Cl19 C146 C276 C147 179.4(5) . . . . ?
Cl25 C256 C32 C259 -165.9(13) . . . . ?
Cl29 C132 C247 C21 -175.8(9) . . . . ?
Cl29 C132 C251 S23 -11.8(10) . . . . ?
Cl29 C132 C251 C134 175.2(10) . . . . ?
Cl31 C147 C276 C146 -176.0(9) . . . . ?
Cl35 C113 C208 C35 -178.9(8) . . . . ?
S2 C9 C170 C95 -174.8(7) . . . . ?
S7 C274 C147 Cl31 -18.3(12) . . . . ?
S7 C274 C147 C276 165.8(10) . . . . ?
S9 C56 C182 C101 -179.6(6) . . . . ?
S11 C254 C256 Cl25 -16.0(14) . . . . ?
S11 C254 C256 C32 179.9(8) . . . . ?
S15 C69 C229 C124 176.6(5) . . . . ?
S25 C210 C114 C206 -176.4(7) . . . . ?
S28 C130 C243 Cl11 -4.7(9) . . . . ?
S28 C130 C243 C73 176.0(8) . . . . ?
S29 C145 C271 C82 174.4(16) . . . . ?
C39 C241 C130 S28 -175.9(8) . . . . ?
C39 C241 C130 C243 0.0 . . . . ?
C241 C39 C245 Cl34 175.3(10) . . . . ?
C241 C39 C245 C73 0.0 . . . . ?
C241 C130 C243 Cl11 179.3(9) . . . . ?
C241 C130 C243 C73 0.0 . . . . ?
C130 C243 C73 C245 0.0 . . . . ?
C243 C73 C245 Cl34 -175.3(10) . . . . ?
C243 C73 C245 C39 0.0 . . . . ?
C245 C39 C241 C130 0.0 . . . . ?
C45 C270 C145 S29 -174.7(15) . . . . ?
C45 C270 C145 C271 0.0 . . . . ?
C270 C45 C272 Cl26 159.1(13) . . . . ?
C270 C45 C272 C82 0.0 . . . . ?
C270 C145 C271 C82 0.0 . . . . ?
C145 C271 C82 C272 0.0 . . . . ?
C271 C82 C272 Cl26 -161.6(11) . . . . ?
C271 C82 C272 C45 0.0 . . . . ?
C272 C45 C270 Cl15 161.3(12) . . . . ?
C272 C45 C270 C145 0.0 . . . . ?
C93 C168 C9 S2 174.8(7) . . . . ?
C93 C168 C9 C170 0.0 . . . . ?
C168 C93 C172 C95 0.0 . . . . ?
C168 C93 C172 Br11 -178.3(8) . . . . ?
C168 C9 C170 C95 0.0 . . . . ?
C9 C170 C95 C172 0.0 . . . . ?
C170 C95 C172 C93 0.0 . . . . ?
C170 C95 C172 Br11 178.3(8) . . . . ?
C172 C93 C168 C9 0.0 . . . . ?
C99 C180 C56 S9 179.6(6) . . . . ?
C99 C180 C56 C182 0.0 . . . . ?
C180 C99 C184 Cl32 -179.7(7) . . . . ?
C180 C99 C184 C101 0.0 . . . . ?
C180 C56 C182 C101 0.0 . . . . ?
C56 C182 C101 C184 0.0 . . . . ?
C182 C101 C184 Cl32 179.7(7) . . . . ?
C182 C101 C184 C99 0.0 . . . . ?
C184 C99 C180 Cl17 179.0(7) . . . . ?
C184 C99 C180 C56 0.0 . . . . ?
C132 C247 C21 Cl3 -178.7(7) . . . . ?
C132 C247 C21 C249 0.0 . . . . ?
C247 C132 C251 S23 173.0(7) . . . . ?
C247 C132 C251 C134 0.0 . . . . ?
C247 C21 C249 C134 0.0 . . . . ?
C21 C249 C134 C251 0.0 . . . . ?
C249 C134 C251 S23 -173.1(7) . . . . ?
C249 C134 C251 C132 0.0 . . . . ?
C251 C132 C247 C21 0.0 . . . . ?
C146 C273 C23 C274 0.0 . . . . ?
C273 C146 C276 C147 0.0 . . . . ?
C273 C23 C274 S7 -166.8(9) . . . . ?
C273 C23 C274 C147 0.0 . . . . ?
C23 C274 C147 Cl31 175.9(9) . . . . ?
C23 C274 C147 C276 0.0 . . . . ?
C274 C147 C276 C146 0.0 . . . . ?
C276 C146 C273 C23 0.0 . . . . ?
C206 C113 C208 C35 0.0 . . . . ?
C113 C206 C114 C210 0.0 . . . . ?
C113 C208 C35 Cl8 178.1(9) . . . . ?
C113 C208 C35 C210 0.0 . . . . ?
C208 C35 C210 S25 176.5(7) . . . . ?
C208 C35 C210 C114 0.0 . . . . ?
C35 C210 C114 C206 0.0 . . . . ?
C114 C206 C113 Cl35 178.9(8) . . . . ?
C114 C206 C113 C208 0.0 . . . . ?
C214 C116 C216 C19 0.0 . . . . ?
C214 C116 C216 Br26 174.9(10) . . . . ?
C116 C214 C118 S3 171.4(10) . . . . ?
C116 C214 C118 C218 0.0 . . . . ?
C116 C216 C19 C218 0.0 . . . . ?
C216 C19 C218 C118 0.0 . . . . ?
C19 C218 C118 S3 -171.7(9) . . . . ?
C19 C218 C118 C214 0.0 . . . . ?
C118 C214 C116 C216 0.0 . . . . ?
C225 C122 C227 C69 0.0 . . . . ?
C122 C225 C124 C229 0.0 . . . . ?
C122 C227 C69 S15 -176.6(5) . . . . ?
C122 C227 C69 C229 0.0 . . . . ?
C227 C69 C229 C124 0.0 . . . . ?
C69 C229 C124 C225 0.0 . . . . ?
C124 C225 C122 C227 0.0 . . . . ?
C250 C252 C254 S11 -179.9(8) . . . . ?
C250 C252 C254 C256 0.0 . . . . ?
C252 C250 C259 C32 0.0 . . . . ?
C252 C250 C259 Br19 -179.2(8) . . . . ?
C252 C254 C256 Cl25 164.1(14) . . . . ?
C252 C254 C256 C32 0.0 . . . . ?
C254 C256 C32 C259 0.0 . . . . ?
C256 C32 C259 C250 0.0 . . . . ?
C256 C32 C259 Br19 179.2(8) . . . . ?
C259 C250 C252 C254 0.0 . . . . ?
Br20 C225 C122 C227 -177.1(5) . . . . ?
Br20 C225 C124 C229 177.0(6) . . . . ?
Br26 C216 C19 C218 -174.7(10) . . . . ?
Ag3 S13 C163 C167 -68.6(12) . . . . ?
Ag3 S13 C163 C231 113.9(11) . . . . ?
Ag3 S16 C16 C49 -177.6(7) . . . . ?
Ag3 S16 C16 C86 6.5(9) . . . . ?
Ag3 S26 C143 C266 -135.3(6) . . . . ?
Ag3 S26 C143 C268 44.1(7) . . . . ?
Ag5 S8 C41 C13 -166.6(8) . . . . ?
Ag5 S8 C41 C181 20.6(11) . . . . ?
Ag5 S19 C135 C43 79.9(5) . . . . ?
Ag5 S19 C135 C144 -93.5(4) . . . . ?
Ag5 S26 C143 C266 -19.9(7) . . . . ?
Ag5 S26 C143 C268 159.5(5) . . . . ?
Ag12 S16 C16 C49 -97.9(8) . . . . ?
Ag12 S16 C16 C86 86.2(9) . . . . ?
Ag15 S14 C77 C100 170.5(8) . . . . ?
Ag15 S14 C77 C149 -6.3(11) . . . . ?
Ag16 S8 C41 C13 -6.1(10) . . . . ?
Ag16 S8 C41 C181 -178.9(9) . . . . ?
Ag16 S24 C51 C108 88.4(10) . . . . ?
Ag16 S24 C51 C187 -96.7(9) . . . . ?
Ag16 S27 C234 C219 -122.7(12) . . . . ?
Ag16 S27 C234 C238 67.9(15) . . . . ?
Ag18 S26 C143 C266 103.4(6) . . . . ?
Ag18 S26 C143 C268 -77.2(6) . . . . ?
Ag18 S27 C234 C219 160.8(12) . . . . ?
Ag18 S27 C234 C238 -8.7(15) . . . . ?
Ag18 S30 C204 C109 -179.5(5) . . . . ?
Ag18 S30 C204 C111 7.1(6) . . . . ?
Ag19 S8 C41 C13 -86.8(9) . . . . ?
Ag19 S8 C41 C181 100.4(9) . . . . ?
Ag22 S24 C51 C108 11.4(11) . . . . ?
Ag22 S24 C51 C187 -173.7(8) . . . . ?
Ag24 S30 C204 C109 -100.5(6) . . . . ?
Ag24 S30 C204 C111 86.2(5) . . . . ?
Ag26 S17 C57 C174 177.3(9) . . . . ?
Ag26 S17 C57 C177 0.5(11) . . . . ?
Ag33 S13 C163 C167 -150.0(10) . . . . ?
Ag33 S13 C163 C231 32.5(12) . . . . ?
Ag33 S17 C57 C174 -97.4(10) . . . . ?
Ag33 S17 C57 C177 85.7(10) . . . . ?
Ag33 S30 C204 C109 -8.8(6) . . . . ?
Ag33 S30 C204 C111 177.8(5) . . . . ?
Ag34 S14 C77 C100 -110.6(8) . . . . ?
Ag34 S14 C77 C149 72.6(11) . . . . ?
Ag34 S16 C16 C49 -12.1(9) . . . . ?
Ag34 S16 C16 C86 172.0(7) . . . . ?
Ag34 S19 C135 C43 0.0(5) . . . . ?
Ag34 S19 C135 C144 -173.4(4) . . . . ?
Cl1 C219 C221 C52 174.9(15) . . . . ?
Cl1 C219 C234 S27 14(2) . . . . ?
Cl1 C219 C234 C238 -175.1(13) . . . . ?
Cl16 C100 C232 C262 -179.2(15) . . . . ?
Cl22 C129 C173 C108 178.8(10) . . . . ?
Cl22 C129 C193 C187 -175.7(11) . . . . ?
Cl24 C6 C71 C231 177.9(12) . . . . ?
Cl24 C6 C148 C167 -179.0(12) . . . . ?
Cl30 C89 C203 C177 179.3(10) . . . . ?
Cl39 C187 C193 C129 -178.8(13) . . . . ?
S8 C41 C181 C157 169.6(11) . . . . ?
S13 C163 C167 Cl36 5.7(18) . . . . ?
S13 C163 C167 C148 -177.2(12) . . . . ?
S13 C163 C231 C71 175.8(12) . . . . ?
S14 C77 C100 Cl16 2.2(14) . . . . ?
S14 C77 C100 C232 -177.8(11) . . . . ?
S14 C77 C149 C267 174.8(12) . . . . ?
S16 C16 C49 C191 -176.0(8) . . . . ?
S16 C16 C86 C207 175.5(8) . . . . ?
S17 C57 C174 Cl18 5.9(16) . . . . ?
S17 C57 C174 C26 -174.4(11) . . . . ?
S17 C57 C177 C203 173.6(10) . . . . ?
S19 C135 C43 C138 -173.2(6) . . . . ?
S19 C135 C144 Cl20 -17.0(7) . . . . ?
S19 C135 C144 C142 173.7(6) . . . . ?
S24 C51 C108 C173 179.1(9) . . . . ?
S24 C51 C187 Cl39 -1.1(16) . . . . ?
S24 C51 C187 C193 -176.2(10) . . . . ?
S26 C143 C268 C141 -179.4(9) . . . . ?
S27 C234 C238 C165 174.9(13) . . . . ?
C6 C71 C231 C163 1(2) . . . . ?
C6 C148 C167 Cl36 178.8(14) . . . . ?
C6 C148 C167 C163 2(3) . . . . ?
C13 C41 C181 C157 -3.5(18) . . . . ?
C13 C121 C230 C157 -1.9(18) . . . . ?
C13 C121 C230 Br12 -179.9(9) . . . . ?
C16 C49 C191 C228 0.4(16) . . . . ?
C16 C86 C207 C228 0.4(17) . . . . ?
C26 C89 C203 C177 0(2) . . . . ?
C41 C13 C121 C230 0.1(19) . . . . ?
C49 C16 C86 C207 -0.3(16) . . . . ?
C49 C191 C228 C207 -0.3(18) . . . . ?
C49 C191 C228 Br23 -177.2(8) . . . . ?
C51 C108 C173 C129 -3.2(19) . . . . ?
C51 C187 C193 C129 -3(2) . . . . ?
C52 C165 C238 C234 -3(3) . . . . ?
C57 C177 C203 C89 2(2) . . . . ?
C71 C6 C148 C167 -2(3) . . . . ?
C77 C100 C232 C262 1(2) . . . . ?
C77 C149 C267 C262 5(2) . . . . ?
C86 C16 C49 C191 -0.1(15) . . . . ?
C86 C207 C228 C191 -0.1(18) . . . . ?
C86 C207 C228 Br23 176.9(8) . . . . ?
C89 C26 C174 Cl18 179.3(12) . . . . ?
C89 C26 C174 C57 0(2) . . . . ?
C100 C77 C149 C267 -2(2) . . . . ?
C100 C232 C262 C267 2(3) . . . . ?
C100 C232 C262 Br14 -177.6(13) . . . . ?
C108 C51 C187 Cl39 173.8(11) . . . . ?
C108 C51 C187 C193 -1.3(19) . . . . ?
C109 C200 C5 C202 0.0 . . . . ?
C109 C200 C5 Br31 177.2(8) . . . . ?
C200 C109 C204 S30 -173.3(7) . . . . ?
C200 C109 C204 C111 0.0 . . . . ?
C200 C5 C202 C111 0.0 . . . . ?
C5 C202 C111 C204 0.0 . . . . ?
C202 C111 C204 S30 173.4(7) . . . . ?
C202 C111 C204 C109 0.0 . . . . ?
C204 C109 C200 C5 0.0 . . . . ?
C121 C13 C41 S8 -170.3(9) . . . . ?
C121 C13 C41 C181 2.7(17) . . . . ?
C135 C43 C138 C140 0.0 . . . . ?
C43 C135 C144 Cl20 169.3(6) . . . . ?
C43 C135 C144 C142 0.0 . . . . ?
C43 C138 C140 C142 0.0 . . . . ?
C43 C138 C140 Br13 177.7(6) . . . . ?
C138 C140 C142 C144 0.0 . . . . ?
C140 C142 C144 Cl20 -168.9(6) . . . . ?
C140 C142 C144 C135 0.0 . . . . ?
C144 C135 C43 C138 0.0 . . . . ?
C141 C264 C80 C266 0.0 . . . . ?
C264 C141 C268 C143 0.0 . . . . ?
C264 C80 C266 C143 0.0 . . . . ?
C80 C266 C143 S26 179.4(8) . . . . ?
C80 C266 C143 C268 0.0 . . . . ?
C266 C143 C268 C141 0.0 . . . . ?
C268 C141 C264 C80 0.0 . . . . ?
C268 C141 C264 Br29 -174.1(9) . . . . ?
C148 C6 C71 C231 1(2) . . . . ?
C149 C77 C100 Cl16 179.3(10) . . . . ?
C149 C77 C100 C232 -0.7(18) . . . . ?
C165 C52 C221 C219 -3(3) . . . . ?
C167 C163 C231 C71 -2(2) . . . . ?
C173 C129 C193 C187 5(2) . . . . ?
C174 C26 C89 Cl30 179.8(11) . . . . ?
C174 C26 C89 C203 -1(2) . . . . ?
C174 C57 C177 C203 -3.4(18) . . . . ?
C177 C57 C174 Cl18 -177.1(9) . . . . ?
C177 C57 C174 C26 3(2) . . . . ?
C181 C157 C230 C121 1(2) . . . . ?
C181 C157 C230 Br12 178.9(11) . . . . ?
C187 C51 C108 C173 4.4(18) . . . . ?
C193 C129 C173 C108 -1(2) . . . . ?
C219 C234 C238 C165 5(2) . . . . ?
C221 C52 C165 C238 2(3) . . . . ?
C221 C219 C234 S27 -177.5(15) . . . . ?
C221 C219 C234 C238 -7(3) . . . . ?
C230 C157 C181 C41 2(2) . . . . ?
C231 C163 C167 Cl36 -176.7(11) . . . . ?
C231 C163 C167 C148 0(2) . . . . ?
C232 C262 C267 C149 -4(3) . . . . ?
C234 C219 C221 C52 6(3) . . . . ?
Br10 C52 C165 C238 -177.3(12) . . . . ?
Br10 C52 C221 C219 175.6(14) . . . . ?
Br13 C140 C142 C144 -177.3(7) . . . . ?
Br14 C262 C267 C149 174.9(13) . . . . ?
Br29 C264 C80 C266 174.4(9) . . . . ?
Br31 C5 C202 C111 -177.3(8) . . . . ?
P1 C68 C175 C29 -172.0(11) . . . . ?
P1 C84 C153 C88 168.0(8) . . . . ?
P1 C84 C179 C199 -171.7(9) . . . . ?
P1 C104 C115 C189 -176.4(11) . . . . ?
P1 C119 C131 C47 -177.4(8) . . . . ?
C1 C20 C68 P1 171.1(8) . . . . ?
C1 C20 C68 C175 2.2(16) . . . . ?
C10 C38 C62 C119 2.2(15) . . . . ?
C10 C47 C131 C119 -1.1(16) . . . . ?
C17 C104 C115 C189 5(2) . . . . ?
C17 C212 C240 C189 -3(3) . . . . ?
C20 C1 C211 C29 1.8(18) . . . . ?
C20 C68 C175 C29 -3.1(19) . . . . ?
C38 C10 C47 C131 0.1(16) . . . . ?
C38 C62 C119 P1 176.9(7) . . . . ?
C38 C62 C119 C131 -3.2(15) . . . . ?
C47 C10 C38 C62 -0.6(16) . . . . ?
C62 C119 C131 C47 2.7(16) . . . . ?
C68 P1 C84 C153 33.6(9) . . . . ?
C68 P1 C84 C179 -158.5(8) . . . . ?
C68 P1 C104 C17 23.2(13) . . . . ?
C68 P1 C104 C115 -155.5(11) . . . . ?
C68 P1 C119 C62 89.7(9) . . . . ?
C68 P1 C119 C131 -90.2(9) . . . . ?
C84 P1 C68 C20 40.1(10) . . . . ?
C84 P1 C68 C175 -151.0(10) . . . . ?
C84 P1 C104 C17 -97.8(12) . . . . ?
C84 P1 C104 C115 83.5(12) . . . . ?
C84 P1 C119 C62 -149.7(8) . . . . ?
C84 P1 C119 C131 30.4(9) . . . . ?
C84 C179 C199 C133 2.1(17) . . . . ?
C88 C133 C199 C179 3.7(18) . . . . ?
C104 P1 C68 C20 -80.5(10) . . . . ?
C104 P1 C68 C175 88.4(11) . . . . ?
C104 P1 C84 C153 153.3(8) . . . . ?
C104 P1 C84 C179 -38.7(9) . . . . ?
C104 P1 C119 C62 -29.2(10) . . . . ?
C104 P1 C119 C131 150.9(8) . . . . ?
C104 C17 C212 C240 1(3) . . . . ?
C104 C115 C189 C240 -6(2) . . . . ?
C115 C189 C240 C212 5(2) . . . . ?
C119 P1 C68 C20 159.5(9) . . . . ?
C119 P1 C68 C175 -31.6(12) . . . . ?
C119 P1 C84 C153 -86.1(8) . . . . ?
C119 P1 C84 C179 81.9(9) . . . . ?
C119 P1 C104 C17 142.5(11) . . . . ?
C119 P1 C104 C115 -36.2(13) . . . . ?
C133 C88 C153 C84 5.3(16) . . . . ?
C153 C84 C179 C199 -4.3(16) . . . . ?
C153 C88 C133 C199 -7.6(18) . . . . ?
C175 C29 C211 C1 -3(2) . . . . ?
C179 C84 C153 C88 0.5(15) . . . . ?
C211 C1 C20 C68 -1.5(15) . . . . ?
C211 C29 C175 C68 3(2) . . . . ?
C212 C17 C104 P1 178.9(14) . . . . ?
C212 C17 C104 C115 -2(2) . . . . ?
P2 C156 C50 C158 -176.4(7) . . . . ?
P2 C190 C105 C223 -176.2(8) . . . . ?
P2 C150 C188 C83 170.6(11) . . . . ?
C15 C154 C87 C156 0.0 . . . . ?
C154 C15 C158 C50 0.0 . . . . ?
C154 C87 C156 P2 176.4(7) . . . . ?
C154 C87 C156 C50 0.0 . . . . ?
C87 C156 C50 C158 0.0 . . . . ?
C156 P2 C190 C233 102.5(6) . . . . ?
C156 P2 C190 C105 -81.3(7) . . . . ?
C156 P2 C150 C107 -26.0(14) . . . . ?
C156 P2 C150 C188 164.1(10) . . . . ?
C156 P2 C236 C74 156.2(12) . . . . ?
C156 P2 C236 C120 -22.0(12) . . . . ?
C156 C50 C158 C15 0.0 . . . . ?
C158 C15 C154 C87 0.0 . . . . ?
C63 C67 C233 C190 0.0 . . . . ?
C67 C63 C223 C105 0.0 . . . . ?
C67 C233 C190 P2 176.3(8) . . . . ?
C67 C233 C190 C105 0.0 . . . . ?
C233 C190 C105 C223 0.0 . . . . ?
C190 P2 C156 C87 19.5(7) . . . . ?
C190 P2 C156 C50 -164.1(5) . . . . ?
C190 P2 C150 C107 94.9(14) . . . . ?
C190 P2 C150 C188 -75.0(12) . . . . ?
C190 P2 C236 C74 35.1(14) . . . . ?
C190 P2 C236 C120 -143.1(11) . . . . ?
C190 C105 C223 C63 0.0 . . . . ?
C223 C63 C67 C233 0.0 . . . . ?
C107 C150 C188 C83 0(2) . . . . ?
C107 C162 C164 C83 -3(2) . . . . ?
C150 P2 C156 C87 137.3(6) . . . . ?
C150 P2 C156 C50 -46.2(7) . . . . ?
C150 P2 C190 C233 -17.3(8) . . . . ?
C150 P2 C190 C105 158.9(7) . . . . ?
C150 P2 C236 C74 -82.7(14) . . . . ?
C150 P2 C236 C120 99.1(12) . . . . ?
C150 C107 C162 C164 6(2) . . . . ?
C162 C107 C150 P2 -175.0(11) . . . . ?
C162 C107 C150 C188 -5(2) . . . . ?
C164 C83 C188 C150 3(2) . . . . ?
C188 C83 C164 C162 -2(2) . . . . ?
C194 C37 C237 C120 -3(2) . . . . ?
C194 C74 C236 P2 174.5(11) . . . . ?
C194 C74 C236 C120 -7(2) . . . . ?
C236 P2 C156 C87 -100.0(7) . . . . ?
C236 P2 C156 C50 76.4(7) . . . . ?
C236 P2 C190 C233 -138.7(7) . . . . ?
C236 P2 C190 C105 37.6(8) . . . . ?
C236 P2 C150 C107 -145.9(13) . . . . ?
C236 P2 C150 C188 44.2(15) . . . . ?
C236 C74 C194 C37 5(2) . . . . ?
C236 C120 C237 C37 0(2) . . . . ?
C237 C37 C194 C74 1(3) . . . . ?
C237 C120 C236 P2 -176.8(10) . . . . ?
C237 C120 C236 C74 5(2) . . . . ?
P3 C42 C257 C76 179.5(8) . . . . ?
P3 C261 C4 C263 174.0(9) . . . . ?
C11 C137 C198 C248 -5(3) . . . . ?
C76 C253 C136 C255 0.0 . . . . ?
C253 C76 C257 C42 0.0 . . . . ?
C253 C136 C255 C42 0.0 . . . . ?
C136 C255 C42 P3 -179.5(9) . . . . ?
C136 C255 C42 C257 0.0 . . . . ?
C255 C42 C257 C76 0.0 . . . . ?
C42 P3 C261 C139 107.3(8) . . . . ?
C42 P3 C261 C4 -66.7(8) . . . . ?
C42 P3 C248 C91 -109.2(15) . . . . ?
C42 P3 C248 C198 72.6(15) . . . . ?
C42 P3 C269 C128 4.6(16) . . . . ?
C42 P3 C269 C166 -174.9(12) . . . . ?
C257 C76 C253 C136 0.0 . . . . ?
C78 C260 C139 C261 0.0 . . . . ?
C260 C78 C263 C4 0.0 . . . . ?
C260 C139 C261 P3 -173.9(9) . . . . ?
C260 C139 C261 C4 0.0 . . . . ?
C139 C261 C4 C263 0.0 . . . . ?
C261 P3 C42 C255 139.5(6) . . . . ?
C261 P3 C42 C257 -40.0(8) . . . . ?
C261 P3 C248 C91 129.6(13) . . . . ?
C261 P3 C248 C198 -48.6(17) . . . . ?
C261 P3 C269 C128 122.9(14) . . . . ?
C261 P3 C269 C166 -56.6(14) . . . . ?
C261 C4 C263 C78 0.0 . . . . ?
C263 C78 C260 C139 0.0 . . . . ?
C137 C11 C160 C91 -4(3) . . . . ?
C137 C198 C248 P3 -174.4(14) . . . . ?
C137 C198 C248 C91 7(3) . . . . ?
C160 C11 C137 C198 3(3) . . . . ?
C160 C91 C248 P3 173.7(13) . . . . ?
C160 C91 C248 C198 -8(2) . . . . ?
C176 C33 C186 C166 -2(2) . . . . ?
C176 C128 C269 P3 -176.5(12) . . . . ?
C176 C128 C269 C166 3(2) . . . . ?
C186 C33 C176 C128 -2(2) . . . . ?
C186 C166 C269 P3 172.5(11) . . . . ?
C186 C166 C269 C128 -7(2) . . . . ?
C248 P3 C42 C255 15.6(8) . . . . ?
C248 P3 C42 C257 -163.9(7) . . . . ?
C248 P3 C261 C139 -131.7(9) . . . . ?
C248 P3 C261 C4 54.3(10) . . . . ?
C248 P3 C269 C128 -113.9(15) . . . . ?
C248 P3 C269 C166 66.7(14) . . . . ?
C248 C91 C160 C11 7(3) . . . . ?
C269 P3 C42 C255 -103.0(8) . . . . ?
C269 P3 C42 C257 77.5(8) . . . . ?
C269 P3 C261 C139 -11.3(10) . . . . ?
C269 P3 C261 C4 174.7(8) . . . . ?
C269 P3 C248 C91 9.8(17) . . . . ?
C269 P3 C248 C198 -168.3(14) . . . . ?
C269 C128 C176 C33 1(2) . . . . ?
C269 C166 C186 C33 6(2) . . . . ?
P4 C183 C209 C96 173.7(6) . . . . ?
P4 C155 C239 C258 -178.7(16) . . . . ?
P4 C195 C197 C275 -174.2(10) . . . . ?
P4 C205 C244 C192 174.4(10) . . . . ?
C14 C155 C239 C258 0(3) . . . . ?
C48 C85 C103 C192 2(2) . . . . ?
C48 C205 C244 C192 -3(2) . . . . ?
C54 C65 C178 C275 -6(2) . . . . ?
C54 C195 C197 C275 0.5(19) . . . . ?
C58 C152 C183 P4 -173.7(6) . . . . ?
C58 C152 C183 C209 0.0 . . . . ?
C152 C58 C185 C96 0.0 . . . . ?
C152 C183 C209 C96 0.0 . . . . ?
C183 P4 C155 C14 -70.6(14) . . . . ?
C183 P4 C155 C239 108.3(13) . . . . ?
C183 P4 C195 C54 139.5(11) . . . . ?
C183 P4 C195 C197 -46.1(11) . . . . ?
C183 P4 C205 C48 -37.2(12) . . . . ?
C183 P4 C205 C244 145.7(10) . . . . ?
C183 C209 C96 C185 0.0 . . . . ?
C209 C96 C185 C58 0.0 . . . . ?
C185 C58 C152 C183 0.0 . . . . ?
C65 C54 C195 P4 175.2(11) . . . . ?
C65 C54 C195 C197 1(2) . . . . ?
C65 C178 C275 C197 7(2) . . . . ?
C85 C48 C205 P4 -175.7(11) . . . . ?
C85 C48 C205 C244 1(2) . . . . ?
C85 C103 C192 C244 -4(2) . . . . ?
C103 C192 C244 C205 4(2) . . . . ?
C155 P4 C183 C152 -148.1(6) . . . . ?
C155 P4 C183 C209 38.2(6) . . . . ?
C155 P4 C195 C54 -96.4(13) . . . . ?
C155 P4 C195 C197 78.0(11) . . . . ?
C155 P4 C205 C48 -157.8(11) . . . . ?
C155 P4 C205 C244 25.1(13) . . . . ?
C155 C14 C213 C97 -3(3) . . . . ?
C155 C239 C258 C97 4(3) . . . . ?
C195 P4 C183 C152 -25.8(7) . . . . ?
C195 P4 C183 C209 160.4(6) . . . . ?
C195 P4 C155 C14 164.8(13) . . . . ?
C195 P4 C155 C239 -16.3(16) . . . . ?
C195 P4 C205 C48 83.8(13) . . . . ?
C195 P4 C205 C244 -93.3(11) . . . . ?
C195 C54 C65 C178 2(2) . . . . ?
C195 C197 C275 C178 -4(2) . . . . ?
C205 P4 C183 C152 92.6(6) . . . . ?
C205 P4 C183 C209 -81.2(6) . . . . ?
C205 P4 C155 C14 46.2(16) . . . . ?
C205 P4 C155 C239 -134.9(13) . . . . ?
C205 P4 C195 C54 22.9(14) . . . . ?
C205 P4 C195 C197 -162.6(10) . . . . ?
C205 C48 C85 C103 -1(2) . . . . ?
C213 C14 C155 P4 178.3(12) . . . . ?
C213 C14 C155 C239 -1(2) . . . . ?
C213 C97 C258 C239 -8(3) . . . . ?
C258 C97 C213 C14 8(3) . . . . ?

_smtbx_masks_special_details     ?
loop_
_smtbx_masks_void_nr
_smtbx_masks_void_average_x
_smtbx_masks_void_average_y
_smtbx_masks_void_average_z
_smtbx_masks_void_volume
_smtbx_masks_void_count_electrons
_smtbx_masks_void_content
1 -0.885 -0.057 -0.574 9772.4 915.4 '2.6 C24PH20'
2 0.500 0.500 0.500 625.3 163.5 ?

_smtbx_masks_void_probe_radius   1.2
_smtbx_masks_void_truncation_radius 1.2
_olex2_submission_special_instructions 'No special instructions were received'
