# Supplementary Information (SI) for RSC Advances.
# This journal is © The Royal Society of Chemistry 2024

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
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data_khan1s_eu
_database_code_depnum_ccdc_archive 'CCDC 2370746'
loop_
_audit_author_name
_audit_author_address
'Craig Robertson'
;University of Sheffield
United Kingdom
;
_audit_update_record             
;
2024-07-15 deposited with the CCDC.	2024-10-08 downloaded from the CCDC.
;
_audit_creation_date             2024-04-30
_audit_creation_method           
;
Olex2 1.5
(compiled 2021.12.09 svn.r5202d8cf for OlexSys, GUI svn.r6439)
;
_shelx_SHELXL_version_number     2019/1
loop_
_audit_author_email
craig.robertson@sheffield.ac.uk
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C36 H18 Eu F18 N3 O6'
_chemical_formula_sum            'C36 H18 Eu F18 N3 O6'
_chemical_formula_weight         1082.49
_chemical_absolute_configuration ad
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Eu Eu -0.1578 3.6682 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      orthorhombic
_space_group_IT_number           29
_space_group_name_H-M_alt        'P c a 21'
_space_group_name_Hall           'P 2c -2ac'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, z+1/2'
'x+1/2, -y, z'
'-x+1/2, y, z+1/2'

_cell_length_a                   17.648(3)
_cell_length_b                   30.273(5)
_cell_length_c                   22.438(4)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_volume                     11988(3)
_cell_formula_units_Z            12
_cell_measurement_reflns_used    9153
_cell_measurement_temperature    100
_cell_measurement_theta_max      28.820
_cell_measurement_theta_min      2.480
_shelx_estimated_absorpt_T_max   0.755
_shelx_estimated_absorpt_T_min   0.454
_exptl_absorpt_coefficient_mu    1.702
_exptl_absorpt_correction_T_max  0.7458
_exptl_absorpt_correction_T_min  0.6037
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
SADABS-2016/2 (Bruker,2016/2) was used for absorption correction.
wR2(int) was 0.0690 before and 0.0493 after correction.
The Ratio of minimum to maximum transmission is 0.8095.
The λ/2 correction factor is Not present.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            colourless
_exptl_crystal_colour_primary    colourless
_exptl_crystal_density_diffrn    1.799
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             6336
_exptl_crystal_size_max          0.55
_exptl_crystal_size_mid          0.31
_exptl_crystal_size_min          0.175
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0407
_diffrn_reflns_av_unetI/netI     0.0303
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 0.999
_diffrn_reflns_limit_h_max       23
_diffrn_reflns_limit_h_min       -21
_diffrn_reflns_limit_k_max       40
_diffrn_reflns_limit_k_min       -35
_diffrn_reflns_limit_l_max       30
_diffrn_reflns_limit_l_min       -30
_diffrn_reflns_number            174199
_diffrn_reflns_point_group_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 0.998
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         28.701
_diffrn_reflns_theta_min         0.673
_diffrn_ambient_temperature      100
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_diffrn_source_current           30.0
_diffrn_source_power             1.5
_diffrn_source_voltage           50.0
_diffrn_standards_number         0
_reflns_Friedel_coverage         0.950
_reflns_Friedel_fraction_full    0.999
_reflns_Friedel_fraction_max     0.998
_reflns_number_gt                28144
_reflns_number_total             30923
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences. Completness statistics refer to single and
 composite reflections containing twin component 1 only.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT V8.40B (Bruker, 2016)'
_computing_data_collection       ?
_computing_data_reduction        'SAINT V8.40B (Bruker, 2016)'
_computing_molecular_graphics    'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_structure_refinement  'XL  (Sheldrick, 2008)'
_computing_structure_solution    'XT  (Sheldrick, 2015)'
_refine_diff_density_max         10.828
_refine_diff_density_min         -2.820
_refine_diff_density_rms         0.265
_refine_ls_abs_structure_details 
;
 Refined as an inversion twin.
;
_refine_ls_abs_structure_Flack   0.49(2)
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.079
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1755
_refine_ls_number_reflns         30923
_refine_ls_number_restraints     1907
_refine_ls_R_factor_all          0.1048
_refine_ls_R_factor_gt           0.0954
_refine_ls_restrained_S_all      1.072
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.1353P)²+157.5747P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2334
_refine_ls_wR_factor_ref         0.2444
_refine_special_details          
;
 Refined as a 2-component inversion twin.
;
_olex2_refinement_description    
;
1. Twinned data refinement
 Scales: 0.50794
 0.49206
2. Restrained distances
 F18D-C36D \\sim F17D-C36D \\sim F16D-C36D \\sim F17C-C36C \\sim F16C-C36C
\\sim F18C-C36C
 with sigma of 0.02
 C36C-C35C \\sim C36D-C35C
 with sigma of 0.02
3. Uiso/Uaniso restraints and constraints
Uanis(C33C) = Uanis(C34C) = Uanis(C35C)
4. Rigid body (RIGU) restrains
 All non-hydrogen atoms
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
5. Others
 Sof(F16D)=Sof(F17D)=Sof(F18D)=Sof(C36D)=1-FVAR(1)
 Sof(F16C)=Sof(F17C)=Sof(F18C)=Sof(C36C)=FVAR(1)
6.a Aromatic/amide H refined with riding coordinates:
 C1C(H1C), C2C(H2C), C3C(H3C), C4C(H4C), C7C(H7C), C9C(H9C), C12C(H12C),
 C13C(H13C), C14C(H14C), C15C(H15C), C17C(H17C), C18C(H18C), C19C(H19C),
 C20C(H20C), C21C(H21C), C24C(H24C), C29C(H29C), C34C(H34C), C1A(H1A), C2A(H2A),
  C3A(H3A), C4A(H4A), C7A(H7A), C9A(H9A), C12A(H12A), C13A(H13A), C14A(H14A),
 C15A(H15A), C17A(H17A), C18A(H18A), C19A(H19A), C20A(H20A), C21A(H21A),
 C24A(H24A), C29A(H29A), C34A(H34A), C1B(H1B), C2B(H2B), C3B(H3B), C4B(H4B),
 C7B(H7B), C9B(H9B), C12B(H12B), C13B(H13B), C14B(H14B), C15B(H15B), C17B(H17B),
  C18B(H18B), C19B(H19B), C20B(H20B), C21B(H21B), C24B(H24B), C29B(H29B),
 C34B(H34B)
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Eu1C Eu 0.64173(4) 0.09159(3) 0.71303(3) 0.02663(17) Uani 1 1 d . . . . .
F1C F 0.5193(11) 0.0219(7) 0.5433(8) 0.092(5) Uani 1 1 d . . . . .
F2C F 0.5288(11) 0.0852(6) 0.5028(9) 0.091(5) Uani 1 1 d . . . . .
F3C F 0.5925(9) 0.0353(7) 0.4709(6) 0.083(5) Uani 1 1 d . . . . .
F4C F 0.8490(7) 0.0070(4) 0.5565(6) 0.051(3) Uani 1 1 d . . . . .
F5C F 0.8619(8) 0.0758(5) 0.5355(6) 0.056(3) Uani 1 1 d . . . . .
F6C F 0.8904(7) 0.0514(4) 0.6219(5) 0.048(3) Uani 1 1 d . . . . .
F7C F 0.6394(12) -0.0745(5) 0.6428(8) 0.080(4) Uani 1 1 d . . . . .
F8C F 0.6195(11) -0.0964(5) 0.7329(8) 0.078(4) Uani 1 1 d . . . . .
F9C F 0.5378(10) -0.0563(6) 0.6907(11) 0.092(5) Uani 1 1 d . . . . .
F10C F 0.8657(13) 0.0292(10) 0.8197(15) 0.142(9) Uani 1 1 d . . . . .
F11C F 0.7786(15) 0.0126(10) 0.8828(10) 0.130(7) Uani 1 1 d . . . . .
F12C F 0.8288(14) -0.0363(9) 0.8328(12) 0.119(7) Uani 1 1 d . . . . .
F13C F 0.5177(12) -0.0144(5) 0.8529(7) 0.080(5) Uani 1 1 d . . . . .
F14C F 0.5760(13) 0.0067(6) 0.9318(8) 0.096(6) Uani 1 1 d . . . . .
F15C F 0.4748(13) 0.0316(7) 0.9087(12) 0.113(6) Uani 1 1 d . . . . .
F16C F 0.726(2) 0.1810(11) 0.8815(16) 0.087(9) Uani 0.60(3) 1 d D . P A 1
F16D F 0.633(2) 0.1669(17) 0.9494(14) 0.035(7) Uani 0.40(3) 1 d D . P A 2
F17C F 0.649(3) 0.1610(18) 0.9513(14) 0.088(11) Uani 0.60(3) 1 d D . P A 1
F17D F 0.698(2) 0.1960(10) 0.8790(16) 0.041(7) Uani 0.40(3) 1 d D . P A 2
F18C F 0.6077(19) 0.2068(7) 0.8774(10) 0.077(7) Uani 0.60(3) 1 d D . P A 1
F18D F 0.7478(18) 0.1410(12) 0.9216(16) 0.058(8) Uani 0.40(3) 1 d D . P A 2
O1C O 0.6046(6) 0.0851(4) 0.6094(5) 0.028(2) Uani 1 1 d . . . . .
O2C O 0.7519(7) 0.0733(4) 0.6480(5) 0.036(2) Uani 1 1 d . . . . .
O3C O 0.6300(6) 0.0141(4) 0.6913(5) 0.030(2) Uani 1 1 d . . . . .
O4C O 0.7369(7) 0.0543(5) 0.7703(5) 0.042(3) Uani 1 1 d . . . . .
O5C O 0.5806(6) 0.0522(4) 0.7945(5) 0.032(2) Uani 1 1 d . . . . .
O6C O 0.6416(7) 0.1362(4) 0.8021(5) 0.036(3) Uani 1 1 d . . . . .
N1C N 0.4978(7) 0.0952(4) 0.6985(5) 0.026(2) Uani 1 1 d . . . . .
N2C N 0.5900(7) 0.1661(4) 0.6822(5) 0.025(2) Uani 1 1 d . . . . .
N3C N 0.7371(7) 0.1558(5) 0.7082(6) 0.032(2) Uani 1 1 d . . . . .
C1C C 0.4585(9) 0.0591(6) 0.7032(7) 0.034(3) Uani 1 1 d . . . . .
H1C H 0.479406 0.035024 0.724885 0.040 Uiso 1 1 calc R U . . .
C2C C 0.3867(11) 0.0541(6) 0.6775(9) 0.041(4) Uani 1 1 d . . . . .
H2C H 0.358897 0.027455 0.682122 0.049 Uiso 1 1 calc R U . . .
C3C C 0.3576(10) 0.0887(6) 0.6456(9) 0.039(3) Uani 1 1 d . . . . .
H3C H 0.309850 0.086086 0.626419 0.047 Uiso 1 1 calc R U . . .
C4C C 0.3989(9) 0.1279(5) 0.6415(8) 0.031(3) Uani 1 1 d . . . . .
H4C H 0.379688 0.152566 0.620050 0.037 Uiso 1 1 calc R U . . .
C5C C 0.4695(8) 0.1298(5) 0.6699(7) 0.026(2) Uani 1 1 d . . . . .
C6C C 0.5158(8) 0.1713(5) 0.6691(6) 0.025(2) Uani 1 1 d . . . . .
C7C C 0.4826(9) 0.2122(5) 0.6579(6) 0.028(3) Uani 1 1 d . . . . .
H7C H 0.430440 0.213834 0.647699 0.033 Uiso 1 1 calc R U . . .
C8C C 0.5253(10) 0.2506(5) 0.6617(6) 0.028(2) Uani 1 1 d . . . . .
C9C C 0.6021(10) 0.2454(5) 0.6735(6) 0.031(3) Uani 1 1 d . . . . .
H9C H 0.633938 0.270672 0.675061 0.037 Uiso 1 1 calc R U . . .
C10C C 0.6330(9) 0.2034(5) 0.6830(5) 0.025(2) Uani 1 1 d . . . . .
C11C C 0.7158(9) 0.1964(6) 0.6953(6) 0.028(3) Uani 1 1 d . . . . .
C12C C 0.7666(10) 0.2319(6) 0.6927(7) 0.035(3) Uani 1 1 d . . . . .
H12C H 0.750380 0.260895 0.682475 0.042 Uiso 1 1 calc R U . . .
C13C C 0.8406(10) 0.2228(7) 0.7056(8) 0.040(3) Uani 1 1 d . . . . .
H13C H 0.876507 0.246180 0.704077 0.048 Uiso 1 1 calc R U . . .
C14C C 0.8647(9) 0.1821(6) 0.7202(7) 0.034(3) Uani 1 1 d . . . . .
H14C H 0.916345 0.176539 0.729614 0.041 Uiso 1 1 calc R U . . .
C15C C 0.8094(8) 0.1474(6) 0.7212(7) 0.033(3) Uani 1 1 d . . . . .
H15C H 0.824403 0.118213 0.731191 0.040 Uiso 1 1 calc R U . . .
C16C C 0.4881(11) 0.2954(6) 0.6552(7) 0.035(3) Uani 1 1 d . . . . .
C17C C 0.4128(12) 0.3010(6) 0.6645(9) 0.041(4) Uani 1 1 d . . . . .
H17C H 0.382739 0.276170 0.675064 0.049 Uiso 1 1 calc R U . . .
C18C C 0.3786(13) 0.3421(7) 0.6590(9) 0.045(4) Uani 1 1 d . . . . .
H18C H 0.325581 0.345338 0.664621 0.054 Uiso 1 1 calc R U . . .
C19C C 0.4233(12) 0.3782(7) 0.6452(9) 0.044(4) Uani 1 1 d . . . . .
H19C H 0.400717 0.406602 0.643367 0.052 Uiso 1 1 calc R U . . .
C20C C 0.4991(11) 0.3740(6) 0.6342(7) 0.036(3) Uani 1 1 d . . . . .
H20C H 0.528461 0.399137 0.623770 0.043 Uiso 1 1 calc R U . . .
C21C C 0.5337(11) 0.3315(5) 0.6386(7) 0.033(3) Uani 1 1 d . . . . .
H21C H 0.586145 0.327728 0.630604 0.040 Uiso 1 1 calc R U . . .
C22C C 0.5658(10) 0.0511(7) 0.5211(8) 0.042(3) Uani 1 1 d . . . . .
C23C C 0.6293(9) 0.0630(5) 0.5674(6) 0.027(3) Uani 1 1 d . . . . .
C24C C 0.7016(9) 0.0482(6) 0.5563(7) 0.032(3) Uani 1 1 d . . . . .
H24C H 0.711907 0.031481 0.521408 0.038 Uiso 1 1 calc R U . . .
C25C C 0.7611(9) 0.0578(4) 0.5972(6) 0.024(2) Uani 1 1 d . . . . .
C26C C 0.8423(10) 0.0474(6) 0.5786(8) 0.033(3) Uani 1 1 d . . . . .
C27C C 0.6113(15) -0.0626(7) 0.6972(12) 0.057(4) Uani 1 1 d . . . . .
C28C C 0.6500(9) -0.0187(6) 0.7161(10) 0.037(3) Uani 1 1 d . . . . .
C29C C 0.7062(12) -0.0233(8) 0.7633(11) 0.053(4) Uani 1 1 d . . . . .
H29C H 0.716171 -0.050911 0.781767 0.063 Uiso 1 1 calc R U . . .
C30C C 0.7455(10) 0.0162(8) 0.7804(8) 0.046(4) Uani 1 1 d . . . . .
C31C C 0.807(2) 0.0067(13) 0.8302(16) 0.091(6) Uani 1 1 d . . . . .
C32C C 0.5469(15) 0.0175(7) 0.8832(9) 0.053(4) Uani 1 1 d . . . . .
C33C C 0.5808(9) 0.0563(5) 0.8498(6) 0.0266(16) Uani 1 1 d . . . . .
C34C C 0.6100(9) 0.0898(5) 0.8843(6) 0.0266(16) Uani 1 1 d . . . . .
H34C H 0.612078 0.087093 0.926490 0.032 Uiso 1 1 calc R U . . .
C35C C 0.6361(9) 0.1276(5) 0.8562(6) 0.0266(16) Uani 1 1 d D . . . .
C36C C 0.6525(18) 0.1725(9) 0.8927(13) 0.068(7) Uani 0.60(3) 1 d D . P A 1
C36D C 0.6809(16) 0.1568(9) 0.9037(12) 0.030(6) Uani 0.40(3) 1 d D . P A 2
Eu1A Eu 0.66561(4) 0.42823(2) 0.29129(3) 0.02626(17) Uani 1 1 d . . . . .
F1A F 0.5432(9) 0.4378(6) 0.4941(6) 0.070(4) Uani 1 1 d . . . . .
F2A F 0.6403(11) 0.4243(8) 0.5494(6) 0.092(5) Uani 1 1 d . . . . .
F3A F 0.5909(9) 0.3747(4) 0.4956(6) 0.064(4) Uani 1 1 d . . . . .
F4A F 0.8714(8) 0.5039(4) 0.4437(6) 0.054(3) Uani 1 1 d . . . . .
F5A F 0.8893(8) 0.4373(4) 0.4741(5) 0.051(3) Uani 1 1 d . . . . .
F6A F 0.9131(6) 0.4544(4) 0.3838(5) 0.042(2) Uani 1 1 d . . . . .
F7A F 0.6252(14) 0.5839(5) 0.3715(8) 0.090(5) Uani 1 1 d . . . . .
F8A F 0.6181(8) 0.6158(4) 0.2899(7) 0.056(3) Uani 1 1 d . . . . .
F9A F 0.5331(8) 0.5684(4) 0.3091(11) 0.087(5) Uani 1 1 d . . . . .
F10A F 0.8680(8) 0.5107(8) 0.1749(8) 0.085(5) Uani 1 1 d . . . . .
F11A F 0.7770(9) 0.5082(6) 0.1177(6) 0.072(4) Uani 1 1 d . . . . .
F12A F 0.8055(11) 0.5702(7) 0.1597(9) 0.090(5) Uani 1 1 d . . . . .
F13A F 0.5131(6) 0.5176(3) 0.1495(5) 0.037(2) Uani 1 1 d . . . . .
F14A F 0.5971(7) 0.5118(4) 0.0811(5) 0.046(3) Uani 1 1 d . . . . .
F15A F 0.4987(7) 0.4708(4) 0.0793(6) 0.050(3) Uani 1 1 d . . . . .
F16A F 0.7664(8) 0.3374(4) 0.1302(5) 0.056(3) Uani 1 1 d . . . . .
F17A F 0.6578(8) 0.3118(4) 0.1168(6) 0.055(3) Uani 1 1 d . . . . .
F18A F 0.7033(9) 0.3589(5) 0.0539(5) 0.063(4) Uani 1 1 d . . . . .
O1A O 0.6270(7) 0.4249(4) 0.3947(5) 0.029(2) Uani 1 1 d . . . . .
O2A O 0.7692(6) 0.4528(4) 0.3561(4) 0.028(2) Uani 1 1 d . . . . .
O3A O 0.6356(6) 0.5026(4) 0.3145(5) 0.028(2) Uani 1 1 d . . . . .
O4A O 0.7508(6) 0.4748(4) 0.2324(5) 0.033(2) Uani 1 1 d . . . . .
O5A O 0.5972(6) 0.4611(4) 0.2059(5) 0.029(2) Uani 1 1 d . . . . .
O6A O 0.6742(8) 0.3820(4) 0.2046(5) 0.037(3) Uani 1 1 d . . . . .
N1A N 0.5215(7) 0.4174(4) 0.3014(5) 0.027(2) Uani 1 1 d . . . . .
N2A N 0.6223(8) 0.3499(4) 0.3208(5) 0.025(2) Uani 1 1 d . . . . .
N3A N 0.7689(8) 0.3683(4) 0.3000(6) 0.031(2) Uani 1 1 d . . . . .
C1A C 0.4755(9) 0.4529(5) 0.2959(8) 0.031(3) Uani 1 1 d . . . . .
H1A H 0.494499 0.478862 0.277322 0.037 Uiso 1 1 calc R U . . .
C2A C 0.4014(10) 0.4527(6) 0.3168(8) 0.033(3) Uani 1 1 d . . . . .
H2A H 0.370137 0.477948 0.311903 0.040 Uiso 1 1 calc R U . . .
C3A C 0.3740(10) 0.4160(6) 0.3441(9) 0.038(3) Uani 1 1 d . . . . .
H3A H 0.323920 0.415349 0.359536 0.046 Uiso 1 1 calc R U . . .
C4A C 0.4217(10) 0.3790(5) 0.3491(9) 0.036(3) Uani 1 1 d . . . . .
H4A H 0.403683 0.352513 0.366855 0.043 Uiso 1 1 calc R U . . .
C5A C 0.4955(9) 0.3816(5) 0.3276(6) 0.026(2) Uani 1 1 d . . . . .
C6A C 0.5480(9) 0.3418(5) 0.3305(6) 0.024(2) Uani 1 1 d . . . . .
C7A C 0.5207(9) 0.2994(5) 0.3430(6) 0.027(3) Uani 1 1 d . . . . .
H7A H 0.468310 0.294682 0.350373 0.033 Uiso 1 1 calc R U . . .
C8A C 0.5707(10) 0.2648(5) 0.3444(6) 0.028(3) Uani 1 1 d . . . . .
C9A C 0.6470(10) 0.2739(5) 0.3353(7) 0.030(3) Uani 1 1 d . . . . .
H9A H 0.683193 0.250722 0.337405 0.036 Uiso 1 1 calc R U . . .
C10A C 0.6703(9) 0.3160(5) 0.3235(6) 0.026(2) Uani 1 1 d . . . . .
C11A C 0.7524(10) 0.3265(5) 0.3129(7) 0.030(3) Uani 1 1 d . . . . .
C12A C 0.8073(10) 0.2946(6) 0.3135(7) 0.034(3) Uani 1 1 d . . . . .
H12A H 0.794705 0.264935 0.323001 0.041 Uiso 1 1 calc R U . . .
C13A C 0.8830(11) 0.3062(6) 0.2999(8) 0.040(3) Uani 1 1 d . . . . .
H13A H 0.921973 0.284557 0.300499 0.048 Uiso 1 1 calc R U . . .
C14A C 0.8990(10) 0.3489(6) 0.2858(8) 0.038(3) Uani 1 1 d . . . . .
H14A H 0.948754 0.357339 0.274368 0.045 Uiso 1 1 calc R U . . .
C15A C 0.8417(10) 0.3796(6) 0.2886(8) 0.034(3) Uani 1 1 d . . . . .
H15A H 0.853561 0.409799 0.282273 0.041 Uiso 1 1 calc R U . . .
C16A C 0.5431(10) 0.2189(5) 0.3514(7) 0.031(3) Uani 1 1 d . . . . .
C17A C 0.4714(13) 0.2072(6) 0.3338(9) 0.044(4) Uani 1 1 d . . . . .
H17A H 0.438294 0.229411 0.319077 0.053 Uiso 1 1 calc R U . . .
C18A C 0.4456(14) 0.1632(6) 0.3369(10) 0.050(4) Uani 1 1 d . . . . .
H18A H 0.395682 0.155367 0.325244 0.060 Uiso 1 1 calc R U . . .
C19A C 0.4985(15) 0.1306(7) 0.3587(11) 0.053(5) Uani 1 1 d . . . . .
H19A H 0.483960 0.100368 0.360509 0.063 Uiso 1 1 calc R U . . .
C20A C 0.5675(14) 0.1426(6) 0.3761(10) 0.050(4) Uani 1 1 d . . . . .
H20A H 0.601225 0.120379 0.389935 0.060 Uiso 1 1 calc R U . . .
C21A C 0.5928(11) 0.1863(5) 0.3752(7) 0.034(3) Uani 1 1 d . . . . .
H21A H 0.641478 0.194006 0.389867 0.040 Uiso 1 1 calc R U . . .
C22A C 0.6104(12) 0.4150(7) 0.4973(7) 0.043(3) Uani 1 1 d . . . . .
C23A C 0.6593(10) 0.4290(5) 0.4445(6) 0.028(3) Uani 1 1 d . . . . .
C24A C 0.7327(10) 0.4407(7) 0.4564(7) 0.038(4) Uani 1 1 d . . . . .
H24A H 0.749591 0.441963 0.496571 0.045 Uiso 1 1 calc R U . . .
C25A C 0.7835(9) 0.4510(5) 0.4101(6) 0.026(2) Uani 1 1 d . . . . .
C26A C 0.8652(11) 0.4613(6) 0.4286(7) 0.036(3) Uani 1 1 d . . . . .
C27A C 0.6049(14) 0.5769(7) 0.3143(11) 0.055(4) Uani 1 1 d . . . . .
C28A C 0.6534(8) 0.5387(5) 0.2905(7) 0.025(2) Uani 1 1 d . . . . .
C29A C 0.7038(10) 0.5474(6) 0.2455(8) 0.036(3) Uani 1 1 d . . . . .
H29A H 0.708604 0.576670 0.230718 0.043 Uiso 1 1 calc R U . . .
C30A C 0.7486(8) 0.5133(6) 0.2207(7) 0.032(3) Uani 1 1 d . . . . .
C31A C 0.8011(11) 0.5273(9) 0.1671(9) 0.051(4) Uani 1 1 d . . . . .
C32A C 0.5473(9) 0.4885(5) 0.1158(6) 0.026(2) Uani 1 1 d . . . . .
C33A C 0.5922(8) 0.4543(5) 0.1524(6) 0.022(2) Uani 1 1 d . . . . .
C34A C 0.6281(10) 0.4187(6) 0.1203(7) 0.031(3) Uani 1 1 d . . . . .
H34A H 0.627466 0.418475 0.077991 0.037 Uiso 1 1 calc R U . . .
C35A C 0.6636(10) 0.3847(6) 0.1511(6) 0.031(3) Uani 1 1 d . . . . .
C36A C 0.6951(14) 0.3483(7) 0.1126(8) 0.046(3) Uani 1 1 d . . . . .
Eu1B Eu 0.19522(4) 0.24631(2) 0.50851(3) 0.02857(17) Uani 1 1 d . . . . .
F1B F 0.2498(7) 0.3436(4) 0.3397(6) 0.049(3) Uani 1 1 d . . . . .
F2B F 0.3238(6) 0.2907(4) 0.3140(5) 0.042(2) Uani 1 1 d . . . . .
F3B F 0.2220(8) 0.3036(5) 0.2647(6) 0.055(3) Uani 1 1 d . . . . .
F4B F 0.030(2) 0.1936(13) 0.3037(9) 0.184(10) Uani 1 1 d . . . . .
F5B F 0.115(2) 0.1475(12) 0.3151(12) 0.190(10) Uani 1 1 d . . . . .
F6B F 0.036(2) 0.1524(11) 0.3796(9) 0.179(11) Uani 1 1 d . . . . .
F7B F -0.0082(12) 0.3333(9) 0.4095(9) 0.107(6) Uani 1 1 d . . . . .
F8B F -0.1047(11) 0.3069(10) 0.4598(12) 0.121(7) Uani 1 1 d . . . . .
F9B F -0.0312(15) 0.3510(9) 0.4969(11) 0.125(7) Uani 1 1 d . . . . .
F10B F -0.0018(10) 0.1320(7) 0.5465(9) 0.085(5) Uani 1 1 d . . . . .
F11B F 0.0051(13) 0.1616(10) 0.6299(11) 0.115(6) Uani 1 1 d . . . . .
F12B F -0.0884(11) 0.1768(8) 0.5762(9) 0.097(5) Uani 1 1 d . . . . .
F13B F 0.0265(13) 0.3412(9) 0.6268(9) 0.110(7) Uani 1 1 d . . . . .
F14B F 0.0141(14) 0.2978(10) 0.6995(10) 0.119(7) Uani 1 1 d . . . . .
F15B F 0.0989(13) 0.3426(7) 0.7028(9) 0.100(6) Uani 1 1 d . . . . .
F16B F 0.2338(9) 0.1510(5) 0.6850(10) 0.081(5) Uani 1 1 d . . . . .
F17B F 0.3104(6) 0.2028(4) 0.7093(6) 0.049(3) Uani 1 1 d . . . . .
F18B F 0.2039(8) 0.1974(6) 0.7536(6) 0.069(4) Uani 1 1 d . . . . .
O1B O 0.2356(6) 0.2714(4) 0.4136(5) 0.031(2) Uani 1 1 d . . . . .
O2B O 0.1324(9) 0.2051(5) 0.4280(6) 0.047(3) Uani 1 1 d . . . . .
O3B O 0.0890(8) 0.2873(5) 0.4746(6) 0.043(3) Uani 1 1 d . . . . .
O4B O 0.0930(8) 0.2048(5) 0.5467(6) 0.042(3) Uani 1 1 d . . . . .
O5B O 0.1368(8) 0.2919(5) 0.5884(6) 0.044(3) Uani 1 1 d . . . . .
O6B O 0.2363(7) 0.2222(5) 0.6058(6) 0.043(3) Uani 1 1 d . . . . .
N1B N 0.2699(9) 0.3186(5) 0.5189(7) 0.039(3) Uani 1 1 d . . . . .
N2B N 0.3411(8) 0.2398(5) 0.5012(6) 0.030(2) Uani 1 1 d . . . . .
N3B N 0.2490(10) 0.1682(5) 0.4987(9) 0.047(3) Uani 1 1 d . . . . .
C1B C 0.2322(14) 0.3567(7) 0.5200(10) 0.052(4) Uani 1 1 d . . . . .
H1B H 0.178887 0.356636 0.525919 0.062 Uiso 1 1 calc R U . . .
C2B C 0.2705(13) 0.3969(7) 0.5124(11) 0.053(4) Uani 1 1 d . . . . .
H2B H 0.243701 0.424122 0.513880 0.063 Uiso 1 1 calc R U . . .
C3B C 0.3492(12) 0.3963(6) 0.5025(10) 0.047(4) Uani 1 1 d . . . . .
H3B H 0.375829 0.423400 0.498609 0.056 Uiso 1 1 calc R U . . .
C4B C 0.3869(13) 0.3583(6) 0.4984(9) 0.045(4) Uani 1 1 d . . . . .
H4B H 0.439520 0.357870 0.489480 0.054 Uiso 1 1 calc R U . . .
C5B C 0.3457(10) 0.3178(6) 0.5079(7) 0.034(3) Uani 1 1 d . . . . .
C6B C 0.3837(9) 0.2749(5) 0.5061(8) 0.033(3) Uani 1 1 d . . . . .
C7B C 0.4657(9) 0.2732(5) 0.5083(7) 0.033(3) Uani 1 1 d . . . . .
H7B H 0.495729 0.299191 0.509766 0.040 Uiso 1 1 calc R U . . .
C8B C 0.4985(9) 0.2305(5) 0.5080(7) 0.031(3) Uani 1 1 d . . . . .
C9B C 0.4513(10) 0.1935(6) 0.4996(6) 0.033(3) Uani 1 1 d . . . . .
H9B H 0.473126 0.165015 0.495115 0.039 Uiso 1 1 calc R U . . .
C10B C 0.3740(10) 0.1982(6) 0.4978(7) 0.035(3) Uani 1 1 d . . . . .
C11B C 0.3229(11) 0.1600(6) 0.4909(8) 0.037(3) Uani 1 1 d . . . . .
C12B C 0.3499(11) 0.1185(6) 0.4792(10) 0.042(4) Uani 1 1 d . . . . .
H12B H 0.402310 0.113830 0.471841 0.051 Uiso 1 1 calc R U . . .
C13B C 0.2984(13) 0.0827(7) 0.4783(11) 0.050(4) Uani 1 1 d . . . . .
H13B H 0.315978 0.053405 0.471864 0.060 Uiso 1 1 calc R U . . .
C14B C 0.2247(14) 0.0906(7) 0.4865(13) 0.057(6) Uani 1 1 d . . . . .
H14B H 0.188720 0.067337 0.484733 0.069 Uiso 1 1 calc R U . . .
C15B C 0.2022(14) 0.1334(7) 0.4975(15) 0.066(7) Uani 1 1 d . . . . .
H15B H 0.149904 0.138597 0.504715 0.079 Uiso 1 1 calc R U . . .
C16B C 0.5837(9) 0.2266(5) 0.5130(7) 0.032(3) Uani 1 1 d . . . . .
C17B C 0.6304(11) 0.2617(6) 0.4988(8) 0.039(3) Uani 1 1 d . . . . .
H17B H 0.609161 0.288452 0.484201 0.047 Uiso 1 1 calc R U . . .
C18B C 0.7093(11) 0.2578(7) 0.5060(9) 0.045(3) Uani 1 1 d . . . . .
H18B H 0.741889 0.281813 0.496716 0.054 Uiso 1 1 calc R U . . .
C19B C 0.7372(13) 0.2200(8) 0.5258(9) 0.052(4) Uani 1 1 d . . . . .
H19B H 0.790643 0.217132 0.529409 0.063 Uiso 1 1 calc R U . . .
C20B C 0.6927(11) 0.1848(7) 0.5415(7) 0.040(3) Uani 1 1 d . . . . .
H20B H 0.714979 0.158671 0.556960 0.048 Uiso 1 1 calc R U . . .
C21B C 0.6146(10) 0.1877(6) 0.5348(6) 0.034(3) Uani 1 1 d . . . . .
H21B H 0.582932 0.163457 0.544865 0.041 Uiso 1 1 calc R U . . .
C22B C 0.2501(11) 0.3028(6) 0.3194(8) 0.037(3) Uani 1 1 d . . . . .
C23B C 0.2096(9) 0.2712(6) 0.3611(7) 0.029(3) Uani 1 1 d . . . . .
C24B C 0.1513(11) 0.2463(8) 0.3399(8) 0.045(4) Uani 1 1 d . . . . .
H24B H 0.131935 0.251268 0.300983 0.054 Uiso 1 1 calc R U . . .
C25B C 0.1199(18) 0.2130(11) 0.3761(9) 0.078(8) Uani 1 1 d . . . . .
C26B C 0.066(3) 0.1783(18) 0.3439(12) 0.156(10) Uani 1 1 d . . . . .
C27B C -0.0311(17) 0.3166(13) 0.4598(14) 0.081(5) Uani 1 1 d . . . . .
C28B C 0.0180(13) 0.2790(10) 0.4858(11) 0.062(4) Uani 1 1 d . . . . .
C29B C -0.0173(17) 0.2447(11) 0.5187(14) 0.077(6) Uani 1 1 d . . . . .
H29B H -0.070759 0.245059 0.523494 0.092 Uiso 1 1 calc R U . . .
C30B C 0.0250(14) 0.2098(11) 0.5448(12) 0.066(5) Uani 1 1 d . . . . .
C31B C -0.0198(19) 0.1703(13) 0.5781(16) 0.083(5) Uani 1 1 d . . . . .
C32B C 0.0620(16) 0.3171(10) 0.6677(9) 0.065(5) Uani 1 1 d . . . . .
C33B C 0.1210(14) 0.2879(9) 0.6393(10) 0.055(5) Uani 1 1 d . . . . .
C34B C 0.1466(12) 0.2509(8) 0.6749(9) 0.048(4) Uani 1 1 d . . . . .
H34B H 0.121907 0.244245 0.711471 0.058 Uiso 1 1 calc R U . . .
C35B C 0.2041(11) 0.2264(8) 0.6569(9) 0.045(3) Uani 1 1 d . . . . .
C36B C 0.2366(10) 0.1935(6) 0.7041(9) 0.041(3) Uani 1 1 d . . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Eu1C O1C 2.423(10) . ?
Eu1C O2C 2.493(13) . ?
Eu1C O3C 2.405(12) . ?
Eu1C O4C 2.398(12) . ?
Eu1C O5C 2.434(12) . ?
Eu1C O6C 2.411(11) . ?
Eu1C N1C 2.563(13) . ?
Eu1C N2C 2.531(14) . ?
Eu1C N3C 2.573(13) . ?
F1C C22C 1.31(3) . ?
F2C C22C 1.29(3) . ?
F3C C22C 1.31(2) . ?
F4C C26C 1.33(2) . ?
F5C C26C 1.34(2) . ?
F6C C26C 1.30(2) . ?
F7C C27C 1.37(3) . ?
F8C C27C 1.31(3) . ?
F9C C27C 1.32(3) . ?
F10C C31C 1.26(4) . ?
F11C C31C 1.29(5) . ?
F12C C31C 1.36(4) . ?
F13C C32C 1.29(2) . ?
F14C C32C 1.25(3) . ?
F15C C32C 1.46(3) . ?
F16C C36C 1.35(2) . ?
F16D C36D 1.36(2) . ?
F17C C36C 1.36(2) . ?
F17D C36D 1.35(2) . ?
F18C C36C 1.35(2) . ?
F18D C36D 1.33(2) . ?
O1C C23C 1.236(18) . ?
O2C C25C 1.244(18) . ?
O3C C28C 1.19(2) . ?
O4C C30C 1.19(3) . ?
O5C C33C 1.247(18) . ?
O6C C35C 1.247(18) . ?
N1C C1C 1.30(2) . ?
N1C C5C 1.33(2) . ?
N2C C6C 1.351(19) . ?
N2C C10C 1.359(18) . ?
N3C C11C 1.32(2) . ?
N3C C15C 1.33(2) . ?
C1C H1C 0.9500 . ?
C1C C2C 1.40(2) . ?
C2C H2C 0.9500 . ?
C2C C3C 1.37(3) . ?
C3C H3C 0.9500 . ?
C3C C4C 1.39(2) . ?
C4C H4C 0.9500 . ?
C4C C5C 1.40(2) . ?
C5C C6C 1.499(19) . ?
C6C C7C 1.39(2) . ?
C7C H7C 0.9500 . ?
C7C C8C 1.39(2) . ?
C8C C9C 1.39(2) . ?
C8C C16C 1.51(2) . ?
C9C H9C 0.9500 . ?
C9C C10C 1.40(2) . ?
C10C C11C 1.50(2) . ?
C11C C12C 1.40(2) . ?
C12C H12C 0.9500 . ?
C12C C13C 1.37(3) . ?
C13C H13C 0.9500 . ?
C13C C14C 1.35(3) . ?
C14C H14C 0.9500 . ?
C14C C15C 1.43(2) . ?
C15C H15C 0.9500 . ?
C16C C17C 1.36(3) . ?
C16C C21C 1.41(2) . ?
C17C H17C 0.9500 . ?
C17C C18C 1.39(3) . ?
C18C H18C 0.9500 . ?
C18C C19C 1.38(3) . ?
C19C H19C 0.9500 . ?
C19C C20C 1.37(3) . ?
C20C H20C 0.9500 . ?
C20C C21C 1.43(2) . ?
C21C H21C 0.9500 . ?
C22C C23C 1.57(2) . ?
C23C C24C 1.38(2) . ?
C24C H24C 0.9500 . ?
C24C C25C 1.42(2) . ?
C25C C26C 1.53(2) . ?
C27C C28C 1.55(3) . ?
C28C C29C 1.46(3) . ?
C29C H29C 0.9500 . ?
C29C C30C 1.43(3) . ?
C30C C31C 1.58(3) . ?
C32C C33C 1.52(2) . ?
C33C C34C 1.38(2) . ?
C34C H34C 0.9500 . ?
C34C C35C 1.39(2) . ?
C35C C36C 1.61(3) . ?
C35C C36D 1.59(3) . ?
Eu1A O1A 2.420(10) . ?
Eu1A O2A 2.452(11) . ?
Eu1A O3A 2.370(12) . ?
Eu1A O4A 2.449(12) . ?
Eu1A O5A 2.472(10) . ?
Eu1A O6A 2.401(12) . ?
Eu1A N1A 2.574(13) . ?
Eu1A N2A 2.577(13) . ?
Eu1A N3A 2.580(12) . ?
F1A C22A 1.37(3) . ?
F2A C22A 1.31(2) . ?
F3A C22A 1.27(2) . ?
F4A C26A 1.34(2) . ?
F5A C26A 1.32(2) . ?
F6A C26A 1.33(2) . ?
F7A C27A 1.35(3) . ?
F8A C27A 1.32(2) . ?
F9A C27A 1.30(3) . ?
F10A C31A 1.30(3) . ?
F11A C31A 1.32(3) . ?
F12A C31A 1.31(3) . ?
F13A C32A 1.309(17) . ?
F14A C32A 1.370(19) . ?
F15A C32A 1.302(19) . ?
F16A C36A 1.36(3) . ?
F17A C36A 1.29(3) . ?
F18A C36A 1.36(2) . ?
O1A C23A 1.260(18) . ?
O2A C25A 1.240(18) . ?
O3A C28A 1.260(19) . ?
O4A C30A 1.20(2) . ?
O5A C33A 1.222(17) . ?
O6A C35A 1.218(18) . ?
N1A C1A 1.355(18) . ?
N1A C5A 1.31(2) . ?
N2A C6A 1.35(2) . ?
N2A C10A 1.333(19) . ?
N3A C11A 1.33(2) . ?
N3A C15A 1.35(2) . ?
C1A H1A 0.9500 . ?
C1A C2A 1.39(2) . ?
C2A H2A 0.9500 . ?
C2A C3A 1.36(3) . ?
C3A H3A 0.9500 . ?
C3A C4A 1.40(2) . ?
C4A H4A 0.9500 . ?
C4A C5A 1.39(2) . ?
C5A C6A 1.52(2) . ?
C6A C7A 1.40(2) . ?
C7A H7A 0.9500 . ?
C7A C8A 1.37(2) . ?
C8A C9A 1.39(2) . ?
C8A C16A 1.48(2) . ?
C9A H9A 0.9500 . ?
C9A C10A 1.36(2) . ?
C10A C11A 1.50(2) . ?
C11A C12A 1.37(2) . ?
C12A H12A 0.9500 . ?
C12A C13A 1.41(3) . ?
C13A H13A 0.9500 . ?
C13A C14A 1.36(3) . ?
C14A H14A 0.9500 . ?
C14A C15A 1.37(2) . ?
C15A H15A 0.9500 . ?
C16A C17A 1.37(3) . ?
C16A C21A 1.42(2) . ?
C17A H17A 0.9500 . ?
C17A C18A 1.41(3) . ?
C18A H18A 0.9500 . ?
C18A C19A 1.44(3) . ?
C19A H19A 0.9500 . ?
C19A C20A 1.33(3) . ?
C20A H20A 0.9500 . ?
C20A C21A 1.40(3) . ?
C21A H21A 0.9500 . ?
C22A C23A 1.53(2) . ?
C23A C24A 1.37(2) . ?
C24A H24A 0.9500 . ?
C24A C25A 1.41(2) . ?
C25A C26A 1.53(2) . ?
C27A C28A 1.53(2) . ?
C28A C29A 1.37(2) . ?
C29A H29A 0.9500 . ?
C29A C30A 1.41(2) . ?
C30A C31A 1.57(2) . ?
C32A C33A 1.540(19) . ?
C33A C34A 1.44(2) . ?
C34A H34A 0.9500 . ?
C34A C35A 1.39(2) . ?
C35A C36A 1.51(2) . ?
Eu1B O1B 2.370(12) . ?
Eu1B O2B 2.459(12) . ?
Eu1B O3B 2.373(14) . ?
Eu1B O4B 2.359(13) . ?
Eu1B O5B 2.486(13) . ?
Eu1B O6B 2.412(14) . ?
Eu1B N1B 2.564(14) . ?
Eu1B N2B 2.587(14) . ?
Eu1B N3B 2.557(16) . ?
F1B C22B 1.32(2) . ?
F2B C22B 1.36(2) . ?
F3B C22B 1.32(2) . ?
F4B C26B 1.20(6) . ?
F5B C26B 1.42(8) . ?
F6B C26B 1.24(4) . ?
F7B C27B 1.30(4) . ?
F8B C27B 1.33(4) . ?
F9B C27B 1.33(4) . ?
F10B C31B 1.40(4) . ?
F11B C31B 1.27(4) . ?
F12B C31B 1.23(4) . ?
F13B C32B 1.33(3) . ?
F14B C32B 1.25(4) . ?
F15B C32B 1.28(3) . ?
F16B C36B 1.36(2) . ?
F17B C36B 1.34(2) . ?
F18B C36B 1.26(2) . ?
O1B C23B 1.27(2) . ?
O2B C25B 1.21(3) . ?
O3B C28B 1.30(3) . ?
O4B C30B 1.21(3) . ?
O5B C33B 1.18(3) . ?
O6B C35B 1.29(2) . ?
N1B C1B 1.33(3) . ?
N1B C5B 1.36(2) . ?
N2B C6B 1.31(2) . ?
N2B C10B 1.39(2) . ?
N3B C11B 1.34(2) . ?
N3B C15B 1.34(3) . ?
C1B H1B 0.9500 . ?
C1B C2B 1.40(3) . ?
C2B H2B 0.9500 . ?
C2B C3B 1.41(3) . ?
C3B H3B 0.9500 . ?
C3B C4B 1.33(3) . ?
C4B H4B 0.9500 . ?
C4B C5B 1.44(3) . ?
C5B C6B 1.46(2) . ?
C6B C7B 1.45(2) . ?
C7B H7B 0.9500 . ?
C7B C8B 1.42(2) . ?
C8B C9B 1.41(2) . ?
C8B C16B 1.51(2) . ?
C9B H9B 0.9500 . ?
C9B C10B 1.37(2) . ?
C10B C11B 1.48(3) . ?
C11B C12B 1.37(3) . ?
C12B H12B 0.9500 . ?
C12B C13B 1.42(3) . ?
C13B H13B 0.9500 . ?
C13B C14B 1.33(3) . ?
C14B H14B 0.9500 . ?
C14B C15B 1.38(3) . ?
C15B H15B 0.9500 . ?
C16B C17B 1.38(3) . ?
C16B C21B 1.39(2) . ?
C17B H17B 0.9500 . ?
C17B C18B 1.41(3) . ?
C18B H18B 0.9500 . ?
C18B C19B 1.32(3) . ?
C19B H19B 0.9500 . ?
C19B C20B 1.37(3) . ?
C20B H20B 0.9500 . ?
C20B C21B 1.39(3) . ?
C21B H21B 0.9500 . ?
C22B C23B 1.52(2) . ?
C23B C24B 1.36(2) . ?
C24B H24B 0.9500 . ?
C24B C25B 1.41(3) . ?
C25B C26B 1.59(3) . ?
C27B C28B 1.55(4) . ?
C28B C29B 1.42(4) . ?
C29B H29B 0.9500 . ?
C29B C30B 1.42(5) . ?
C30B C31B 1.62(4) . ?
C32B C33B 1.50(3) . ?
C33B C34B 1.45(3) . ?
C34B H34B 0.9500 . ?
C34B C35B 1.32(3) . ?
C35B C36B 1.56(3) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O1C Eu1C O2C 68.4(4) . . ?
O1C Eu1C O5C 124.1(4) . . ?
O1C Eu1C N1C 67.2(4) . . ?
O1C Eu1C N2C 73.3(4) . . ?
O1C Eu1C N3C 101.4(4) . . ?
O2C Eu1C N1C 135.1(4) . . ?
O2C Eu1C N2C 108.7(4) . . ?
O2C Eu1C N3C 68.5(4) . . ?
O3C Eu1C O1C 72.8(4) . . ?
O3C Eu1C O2C 74.4(4) . . ?
O3C Eu1C O5C 68.7(4) . . ?
O3C Eu1C O6C 135.6(4) . . ?
O3C Eu1C N1C 86.1(4) . . ?
O3C Eu1C N2C 141.6(4) . . ?
O3C Eu1C N3C 141.7(4) . . ?
O4C Eu1C O1C 131.7(4) . . ?
O4C Eu1C O2C 70.3(4) . . ?
O4C Eu1C O3C 73.1(5) . . ?
O4C Eu1C O5C 71.2(4) . . ?
O4C Eu1C O6C 79.6(5) . . ?
O4C Eu1C N1C 141.5(5) . . ?
O4C Eu1C N2C 145.0(4) . . ?
O4C Eu1C N3C 85.4(5) . . ?
O5C Eu1C O2C 132.5(4) . . ?
O5C Eu1C N1C 71.2(4) . . ?
O5C Eu1C N2C 118.8(4) . . ?
O5C Eu1C N3C 133.8(4) . . ?
O6C Eu1C O1C 147.1(4) . . ?
O6C Eu1C O2C 127.6(4) . . ?
O6C Eu1C O5C 69.6(4) . . ?
O6C Eu1C N1C 94.6(4) . . ?
O6C Eu1C N2C 74.1(4) . . ?
O6C Eu1C N3C 67.2(4) . . ?
N1C Eu1C N3C 127.6(4) . . ?
N2C Eu1C N1C 64.5(4) . . ?
N2C Eu1C N3C 63.3(4) . . ?
C23C O1C Eu1C 132.9(10) . . ?
C25C O2C Eu1C 136.2(11) . . ?
C28C O3C Eu1C 133.8(12) . . ?
C30C O4C Eu1C 130.6(13) . . ?
C33C O5C Eu1C 134.2(9) . . ?
C35C O6C Eu1C 133.7(11) . . ?
C1C N1C Eu1C 118.8(12) . . ?
C1C N1C C5C 120.2(14) . . ?
C5C N1C Eu1C 118.0(9) . . ?
C6C N2C Eu1C 120.8(10) . . ?
C6C N2C C10C 116.6(14) . . ?
C10C N2C Eu1C 122.3(10) . . ?
C11C N3C Eu1C 121.9(10) . . ?
C11C N3C C15C 119.8(14) . . ?
C15C N3C Eu1C 118.2(12) . . ?
N1C C1C H1C 118.7 . . ?
N1C C1C C2C 122.6(18) . . ?
C2C C1C H1C 118.7 . . ?
C1C C2C H2C 120.9 . . ?
C3C C2C C1C 118.2(17) . . ?
C3C C2C H2C 120.9 . . ?
C2C C3C H3C 120.3 . . ?
C2C C3C C4C 119.4(17) . . ?
C4C C3C H3C 120.3 . . ?
C3C C4C H4C 121.0 . . ?
C3C C4C C5C 118.0(17) . . ?
C5C C4C H4C 121.0 . . ?
N1C C5C C4C 121.6(14) . . ?
N1C C5C C6C 117.5(13) . . ?
C4C C5C C6C 120.9(15) . . ?
N2C C6C C5C 115.4(14) . . ?
N2C C6C C7C 123.4(13) . . ?
C7C C6C C5C 121.2(13) . . ?
C6C C7C H7C 119.8 . . ?
C8C C7C C6C 120.3(15) . . ?
C8C C7C H7C 119.8 . . ?
C7C C8C C9C 116.6(15) . . ?
C7C C8C C16C 120.6(16) . . ?
C9C C8C C16C 122.8(14) . . ?
C8C C9C H9C 119.6 . . ?
C8C C9C C10C 120.7(14) . . ?
C10C C9C H9C 119.6 . . ?
N2C C10C C9C 122.2(14) . . ?
N2C C10C C11C 115.5(14) . . ?
C9C C10C C11C 122.3(13) . . ?
N3C C11C C10C 116.6(13) . . ?
N3C C11C C12C 122.9(16) . . ?
C12C C11C C10C 120.5(16) . . ?
C11C C12C H12C 121.7 . . ?
C13C C12C C11C 116.6(18) . . ?
C13C C12C H12C 121.7 . . ?
C12C C13C H13C 118.7 . . ?
C14C C13C C12C 122.7(16) . . ?
C14C C13C H13C 118.7 . . ?
C13C C14C H14C 121.3 . . ?
C13C C14C C15C 117.3(15) . . ?
C15C C14C H14C 121.3 . . ?
N3C C15C C14C 120.6(18) . . ?
N3C C15C H15C 119.7 . . ?
C14C C15C H15C 119.7 . . ?
C17C C16C C8C 121.5(15) . . ?
C17C C16C C21C 120.2(17) . . ?
C21C C16C C8C 118.3(17) . . ?
C16C C17C H17C 119.2 . . ?
C16C C17C C18C 121.6(18) . . ?
C18C C17C H17C 119.2 . . ?
C17C C18C H18C 120.7 . . ?
C19C C18C C17C 119(2) . . ?
C19C C18C H18C 120.7 . . ?
C18C C19C H19C 119.1 . . ?
C20C C19C C18C 121.8(19) . . ?
C20C C19C H19C 119.1 . . ?
C19C C20C H20C 120.4 . . ?
C19C C20C C21C 119.3(17) . . ?
C21C C20C H20C 120.4 . . ?
C16C C21C C20C 118.3(17) . . ?
C16C C21C H21C 120.8 . . ?
C20C C21C H21C 120.8 . . ?
F1C C22C F3C 107.8(19) . . ?
F1C C22C C23C 110.5(16) . . ?
F2C C22C F1C 110(2) . . ?
F2C C22C F3C 101.6(19) . . ?
F2C C22C C23C 112.9(16) . . ?
F3C C22C C23C 113.4(15) . . ?
O1C C23C C22C 112.2(14) . . ?
O1C C23C C24C 129.9(15) . . ?
C24C C23C C22C 117.9(13) . . ?
C23C C24C H24C 120.0 . . ?
C23C C24C C25C 120.1(14) . . ?
C25C C24C H24C 120.0 . . ?
O2C C25C C24C 124.9(15) . . ?
O2C C25C C26C 116.7(14) . . ?
C24C C25C C26C 118.3(13) . . ?
F4C C26C F5C 107.5(15) . . ?
F4C C26C C25C 112.0(13) . . ?
F5C C26C C25C 108.0(15) . . ?
F6C C26C F4C 108.0(16) . . ?
F6C C26C F5C 108.1(14) . . ?
F6C C26C C25C 113.1(14) . . ?
F7C C27C C28C 108(2) . . ?
F8C C27C F7C 107(2) . . ?
F8C C27C F9C 107(2) . . ?
F8C C27C C28C 117(2) . . ?
F9C C27C F7C 107(2) . . ?
F9C C27C C28C 109.8(18) . . ?
O3C C28C C27C 117.0(18) . . ?
O3C C28C C29C 128.4(19) . . ?
C29C C28C C27C 114.6(18) . . ?
C28C C29C H29C 121.8 . . ?
C30C C29C C28C 116(2) . . ?
C30C C29C H29C 121.8 . . ?
O4C C30C C29C 134.2(18) . . ?
O4C C30C C31C 114(2) . . ?
C29C C30C C31C 112(2) . . ?
F10C C31C F11C 114(3) . . ?
F10C C31C F12C 107(3) . . ?
F10C C31C C30C 109(3) . . ?
F11C C31C F12C 102(3) . . ?
F11C C31C C30C 111(3) . . ?
F12C C31C C30C 113(3) . . ?
F13C C32C F15C 94(2) . . ?
F13C C32C C33C 118.6(17) . . ?
F14C C32C F13C 115(2) . . ?
F14C C32C F15C 95(2) . . ?
F14C C32C C33C 118.2(19) . . ?
F15C C32C C33C 108.1(19) . . ?
O5C C33C C32C 114.4(14) . . ?
O5C C33C C34C 129.4(14) . . ?
C34C C33C C32C 116.1(14) . . ?
C33C C34C H34C 120.8 . . ?
C33C C34C C35C 118.5(13) . . ?
C35C C34C H34C 120.8 . . ?
O6C C35C C34C 129.9(14) . . ?
O6C C35C C36C 107.7(16) . . ?
O6C C35C C36D 119.8(15) . . ?
C34C C35C C36C 121.6(15) . . ?
C34C C35C C36D 108.6(15) . . ?
F16C C36C F17C 106(3) . . ?
F16C C36C C35C 104(2) . . ?
F17C C36C C35C 106(3) . . ?
F18C C36C F16C 112(3) . . ?
F18C C36C F17C 115(3) . . ?
F18C C36C C35C 114(2) . . ?
F16D C36D C35C 109(3) . . ?
F17D C36D F16D 104(3) . . ?
F17D C36D C35C 109(2) . . ?
F18D C36D F16D 114(3) . . ?
F18D C36D F17D 104(3) . . ?
F18D C36D C35C 116(3) . . ?
O1A Eu1A O2A 69.7(4) . . ?
O1A Eu1A O4A 135.5(4) . . ?
O1A Eu1A O5A 128.5(4) . . ?
O1A Eu1A N1A 68.4(4) . . ?
O1A Eu1A N2A 68.4(4) . . ?
O1A Eu1A N3A 95.6(4) . . ?
O2A Eu1A O5A 134.5(4) . . ?
O2A Eu1A N1A 136.3(4) . . ?
O2A Eu1A N2A 110.4(4) . . ?
O2A Eu1A N3A 69.0(4) . . ?
O3A Eu1A O1A 76.5(4) . . ?
O3A Eu1A O2A 75.4(4) . . ?
O3A Eu1A O4A 73.1(4) . . ?
O3A Eu1A O5A 71.3(4) . . ?
O3A Eu1A O6A 138.2(4) . . ?
O3A Eu1A N1A 83.2(4) . . ?
O3A Eu1A N2A 138.7(4) . . ?
O3A Eu1A N3A 144.0(4) . . ?
O4A Eu1A O2A 71.8(4) . . ?
O4A Eu1A O5A 69.5(4) . . ?
O4A Eu1A N1A 136.7(4) . . ?
O4A Eu1A N2A 148.3(4) . . ?
O4A Eu1A N3A 90.7(4) . . ?
O5A Eu1A N1A 68.8(4) . . ?
O5A Eu1A N2A 115.1(4) . . ?
O5A Eu1A N3A 133.4(4) . . ?
O6A Eu1A O1A 140.4(4) . . ?
O6A Eu1A O2A 127.6(4) . . ?
O6A Eu1A O4A 82.0(4) . . ?
O6A Eu1A O5A 68.8(4) . . ?
O6A Eu1A N1A 93.4(4) . . ?
O6A Eu1A N2A 72.0(4) . . ?
O6A Eu1A N3A 66.8(4) . . ?
N1A Eu1A N2A 64.3(4) . . ?
N1A Eu1A N3A 127.0(4) . . ?
N2A Eu1A N3A 62.8(4) . . ?
C23A O1A Eu1A 135.9(11) . . ?
C25A O2A Eu1A 135.9(11) . . ?
C28A O3A Eu1A 132.5(10) . . ?
C30A O4A Eu1A 131.4(10) . . ?
C33A O5A Eu1A 136.9(10) . . ?
C35A O6A Eu1A 138.6(11) . . ?
C1A N1A Eu1A 118.9(10) . . ?
C5A N1A Eu1A 119.4(10) . . ?
C5A N1A C1A 119.0(14) . . ?
C6A N2A Eu1A 119.7(9) . . ?
C10A N2A Eu1A 122.2(11) . . ?
C10A N2A C6A 117.9(13) . . ?
C11A N3A Eu1A 122.1(11) . . ?
C11A N3A C15A 119.3(14) . . ?
C15A N3A Eu1A 118.6(11) . . ?
N1A C1A H1A 119.0 . . ?
N1A C1A C2A 122.0(16) . . ?
C2A C1A H1A 119.0 . . ?
C1A C2A H2A 120.3 . . ?
C3A C2A C1A 119.5(16) . . ?
C3A C2A H2A 120.3 . . ?
C2A C3A H3A 120.8 . . ?
C2A C3A C4A 118.4(17) . . ?
C4A C3A H3A 120.8 . . ?
C3A C4A H4A 120.4 . . ?
C5A C4A C3A 119.1(17) . . ?
C5A C4A H4A 120.4 . . ?
N1A C5A C4A 122.0(14) . . ?
N1A C5A C6A 117.2(14) . . ?
C4A C5A C6A 120.7(14) . . ?
N2A C6A C5A 116.2(13) . . ?
N2A C6A C7A 122.2(14) . . ?
C7A C6A C5A 121.6(14) . . ?
C6A C7A H7A 120.5 . . ?
C8A C7A C6A 119.0(15) . . ?
C8A C7A H7A 120.5 . . ?
C7A C8A C9A 117.9(15) . . ?
C7A C8A C16A 120.5(15) . . ?
C9A C8A C16A 121.4(14) . . ?
C8A C9A H9A 119.8 . . ?
C10A C9A C8A 120.4(15) . . ?
C10A C9A H9A 119.8 . . ?
N2A C10A C9A 122.6(15) . . ?
N2A C10A C11A 116.1(14) . . ?
C9A C10A C11A 121.3(14) . . ?
N3A C11A C10A 116.7(14) . . ?
N3A C11A C12A 121.3(16) . . ?
C12A C11A C10A 122.0(16) . . ?
C11A C12A H12A 120.3 . . ?
C11A C12A C13A 119.4(17) . . ?
C13A C12A H12A 120.3 . . ?
C12A C13A H13A 120.6 . . ?
C14A C13A C12A 118.8(16) . . ?
C14A C13A H13A 120.6 . . ?
C13A C14A H14A 120.7 . . ?
C13A C14A C15A 118.6(17) . . ?
C15A C14A H14A 120.7 . . ?
N3A C15A C14A 122.5(17) . . ?
N3A C15A H15A 118.8 . . ?
C14A C15A H15A 118.8 . . ?
C17A C16A C8A 120.9(16) . . ?
C17A C16A C21A 119.9(16) . . ?
C21A C16A C8A 119.2(16) . . ?
C16A C17A H17A 119.1 . . ?
C16A C17A C18A 122(2) . . ?
C18A C17A H17A 119.1 . . ?
C17A C18A H18A 121.5 . . ?
C17A C18A C19A 117(2) . . ?
C19A C18A H18A 121.5 . . ?
C18A C19A H19A 119.9 . . ?
C20A C19A C18A 120.2(19) . . ?
C20A C19A H19A 119.9 . . ?
C19A C20A H20A 118.4 . . ?
C19A C20A C21A 123(2) . . ?
C21A C20A H20A 118.4 . . ?
C16A C21A H21A 121.1 . . ?
C20A C21A C16A 117.7(19) . . ?
C20A C21A H21A 121.1 . . ?
F1A C22A C23A 107.9(16) . . ?
F2A C22A F1A 106.6(17) . . ?
F2A C22A C23A 113.7(16) . . ?
F3A C22A F1A 104.3(18) . . ?
F3A C22A F2A 110.2(18) . . ?
F3A C22A C23A 113.5(14) . . ?
O1A C23A C22A 113.9(15) . . ?
O1A C23A C24A 128.8(14) . . ?
C24A C23A C22A 117.1(14) . . ?
C23A C24A H24A 119.5 . . ?
C23A C24A C25A 121.0(14) . . ?
C25A C24A H24A 119.5 . . ?
O2A C25A C24A 127.1(16) . . ?
O2A C25A C26A 116.6(13) . . ?
C24A C25A C26A 116.4(14) . . ?
F4A C26A C25A 110.0(15) . . ?
F5A C26A F4A 107.9(15) . . ?
F5A C26A F6A 107.0(15) . . ?
F5A C26A C25A 113.6(14) . . ?
F6A C26A F4A 106.7(15) . . ?
F6A C26A C25A 111.2(14) . . ?
F7A C27A C28A 108(2) . . ?
F8A C27A F7A 102(2) . . ?
F8A C27A C28A 115.4(15) . . ?
F9A C27A F7A 112(2) . . ?
F9A C27A F8A 108(2) . . ?
F9A C27A C28A 111.3(19) . . ?
O3A C28A C27A 111.4(14) . . ?
O3A C28A C29A 130.0(15) . . ?
C29A C28A C27A 118.4(15) . . ?
C28A C29A H29A 119.5 . . ?
C28A C29A C30A 120.9(16) . . ?
C30A C29A H29A 119.5 . . ?
O4A C30A C29A 129.9(15) . . ?
O4A C30A C31A 114.2(16) . . ?
C29A C30A C31A 115.8(16) . . ?
F10A C31A F11A 104(2) . . ?
F10A C31A F12A 110(2) . . ?
F10A C31A C30A 109.2(17) . . ?
F11A C31A C30A 109.6(17) . . ?
F12A C31A F11A 110(2) . . ?
F12A C31A C30A 113.3(19) . . ?
F13A C32A F14A 106.1(13) . . ?
F13A C32A C33A 112.5(12) . . ?
F14A C32A C33A 108.6(12) . . ?
F15A C32A F13A 109.7(13) . . ?
F15A C32A F14A 106.1(13) . . ?
F15A C32A C33A 113.5(13) . . ?
O5A C33A C32A 116.7(12) . . ?
O5A C33A C34A 125.7(13) . . ?
C34A C33A C32A 117.5(12) . . ?
C33A C34A H34A 119.9 . . ?
C35A C34A C33A 120.3(13) . . ?
C35A C34A H34A 119.9 . . ?
O6A C35A C34A 127.5(14) . . ?
O6A C35A C36A 117.4(14) . . ?
C34A C35A C36A 115.1(13) . . ?
F16A C36A F18A 103.9(17) . . ?
F16A C36A C35A 110.6(16) . . ?
F17A C36A F16A 104.2(16) . . ?
F17A C36A F18A 109.1(17) . . ?
F17A C36A C35A 113.2(18) . . ?
F18A C36A C35A 114.8(15) . . ?
O1B Eu1B O2B 68.8(4) . . ?
O1B Eu1B O3B 77.4(4) . . ?
O1B Eu1B O5B 126.5(5) . . ?
O1B Eu1B O6B 145.0(4) . . ?
O1B Eu1B N1B 69.8(5) . . ?
O1B Eu1B N2B 70.6(4) . . ?
O1B Eu1B N3B 96.1(5) . . ?
O2B Eu1B O5B 128.6(5) . . ?
O2B Eu1B N1B 137.0(5) . . ?
O2B Eu1B N2B 111.3(5) . . ?
O2B Eu1B N3B 68.6(6) . . ?
O3B Eu1B O2B 71.0(5) . . ?
O3B Eu1B O5B 67.2(5) . . ?
O3B Eu1B O6B 133.3(4) . . ?
O3B Eu1B N1B 89.4(5) . . ?
O3B Eu1B N2B 143.6(5) . . ?
O3B Eu1B N3B 138.5(5) . . ?
O4B Eu1B O1B 136.6(4) . . ?
O4B Eu1B O2B 69.6(5) . . ?
O4B Eu1B O3B 77.9(5) . . ?
O4B Eu1B O5B 73.5(5) . . ?
O4B Eu1B O6B 74.9(5) . . ?
O4B Eu1B N1B 144.5(5) . . ?
O4B Eu1B N2B 138.1(5) . . ?
O4B Eu1B N3B 79.8(5) . . ?
O5B Eu1B N1B 71.0(5) . . ?
O5B Eu1B N2B 120.0(4) . . ?
O5B Eu1B N3B 136.8(6) . . ?
O6B Eu1B O2B 130.2(5) . . ?
O6B Eu1B O5B 68.9(5) . . ?
O6B Eu1B N1B 91.2(5) . . ?
O6B Eu1B N2B 74.7(4) . . ?
O6B Eu1B N3B 71.7(6) . . ?
N1B Eu1B N2B 63.8(5) . . ?
N3B Eu1B N1B 127.3(5) . . ?
N3B Eu1B N2B 63.6(5) . . ?
C23B O1B Eu1B 136.6(10) . . ?
C25B O2B Eu1B 133.5(15) . . ?
C28B O3B Eu1B 126.6(16) . . ?
C30B O4B Eu1B 132.8(19) . . ?
C33B O5B Eu1B 137.6(17) . . ?
C35B O6B Eu1B 130.1(13) . . ?
C1B N1B Eu1B 118.9(14) . . ?
C1B N1B C5B 120.5(17) . . ?
C5B N1B Eu1B 118.4(11) . . ?
C6B N2B Eu1B 120.4(12) . . ?
C6B N2B C10B 120.1(15) . . ?
C10B N2B Eu1B 119.2(11) . . ?
C11B N3B Eu1B 123.0(12) . . ?
C15B N3B Eu1B 120.0(15) . . ?
C15B N3B C11B 116.9(18) . . ?
N1B C1B H1B 119.7 . . ?
N1B C1B C2B 121(2) . . ?
C2B C1B H1B 119.7 . . ?
C1B C2B H2B 120.6 . . ?
C1B C2B C3B 119(2) . . ?
C3B C2B H2B 120.6 . . ?
C2B C3B H3B 119.5 . . ?
C4B C3B C2B 121(2) . . ?
C4B C3B H3B 119.5 . . ?
C3B C4B H4B 120.9 . . ?
C3B C4B C5B 118(2) . . ?
C5B C4B H4B 120.9 . . ?
N1B C5B C4B 120.7(17) . . ?
N1B C5B C6B 118.0(15) . . ?
C4B C5B C6B 121.3(16) . . ?
N2B C6B C5B 117.4(15) . . ?
N2B C6B C7B 123.2(16) . . ?
C7B C6B C5B 119.3(14) . . ?
C6B C7B H7B 121.9 . . ?
C8B C7B C6B 116.2(14) . . ?
C8B C7B H7B 121.9 . . ?
C7B C8B C16B 118.5(14) . . ?
C9B C8B C7B 119.0(15) . . ?
C9B C8B C16B 122.4(15) . . ?
C8B C9B H9B 119.7 . . ?
C10B C9B C8B 120.6(16) . . ?
C10B C9B H9B 119.7 . . ?
N2B C10B C11B 117.5(16) . . ?
C9B C10B N2B 120.6(16) . . ?
C9B C10B C11B 121.9(17) . . ?
N3B C11B C10B 115.8(16) . . ?
N3B C11B C12B 122.3(17) . . ?
C12B C11B C10B 121.8(17) . . ?
C11B C12B H12B 120.6 . . ?
C11B C12B C13B 118.8(19) . . ?
C13B C12B H12B 120.6 . . ?
C12B C13B H13B 120.5 . . ?
C14B C13B C12B 119(2) . . ?
C14B C13B H13B 120.5 . . ?
C13B C14B H14B 120.8 . . ?
C13B C14B C15B 118(2) . . ?
C15B C14B H14B 120.8 . . ?
N3B C15B C14B 124(2) . . ?
N3B C15B H15B 117.8 . . ?
C14B C15B H15B 117.8 . . ?
C17B C16B C8B 121.0(16) . . ?
C17B C16B C21B 120.1(17) . . ?
C21B C16B C8B 118.9(16) . . ?
C16B C17B H17B 120.1 . . ?
C16B C17B C18B 119.9(19) . . ?
C18B C17B H17B 120.1 . . ?
C17B C18B H18B 120.7 . . ?
C19B C18B C17B 119(2) . . ?
C19B C18B H18B 120.7 . . ?
C18B C19B H19B 118.5 . . ?
C18B C19B C20B 123(2) . . ?
C20B C19B H19B 118.5 . . ?
C19B C20B H20B 120.2 . . ?
C19B C20B C21B 120(2) . . ?
C21B C20B H20B 120.2 . . ?
C16B C21B C20B 118.8(18) . . ?
C16B C21B H21B 120.6 . . ?
C20B C21B H21B 120.6 . . ?
F1B C22B F2B 106.7(15) . . ?
F1B C22B F3B 107.7(16) . . ?
F1B C22B C23B 112.1(14) . . ?
F2B C22B C23B 109.6(15) . . ?
F3B C22B F2B 106.4(14) . . ?
F3B C22B C23B 113.9(15) . . ?
O1B C23B C22B 113.7(14) . . ?
O1B C23B C24B 126.9(17) . . ?
C24B C23B C22B 119.4(16) . . ?
C23B C24B H24B 120.2 . . ?
C23B C24B C25B 119.6(19) . . ?
C25B C24B H24B 120.2 . . ?
O2B C25B C24B 128.7(19) . . ?
O2B C25B C26B 115(2) . . ?
C24B C25B C26B 116(2) . . ?
F4B C26B F5B 104(3) . . ?
F4B C26B F6B 120(4) . . ?
F4B C26B C25B 114(4) . . ?
F5B C26B C25B 106(4) . . ?
F6B C26B F5B 98(5) . . ?
F6B C26B C25B 112(2) . . ?
F7B C27B F8B 113(3) . . ?
F7B C27B F9B 104(3) . . ?
F7B C27B C28B 116(2) . . ?
F8B C27B F9B 100(3) . . ?
F8B C27B C28B 113(3) . . ?
F9B C27B C28B 110(2) . . ?
O3B C28B C27B 109(3) . . ?
O3B C28B C29B 132(3) . . ?
C29B C28B C27B 119(2) . . ?
C28B C29B H29B 119.0 . . ?
C30B C29B C28B 122(3) . . ?
C30B C29B H29B 119.0 . . ?
O4B C30B C29B 129(3) . . ?
O4B C30B C31B 112(3) . . ?
C29B C30B C31B 119(3) . . ?
F10B C31B C30B 106(2) . . ?
F11B C31B F10B 102(3) . . ?
F11B C31B C30B 114(3) . . ?
F12B C31B F10B 110(3) . . ?
F12B C31B F11B 114(3) . . ?
F12B C31B C30B 110(3) . . ?
F13B C32B C33B 110.9(18) . . ?
F14B C32B F13B 109(3) . . ?
F14B C32B F15B 106(2) . . ?
F14B C32B C33B 116(3) . . ?
F15B C32B F13B 109(3) . . ?
F15B C32B C33B 105(2) . . ?
O5B C33B C32B 121(2) . . ?
O5B C33B C34B 123(2) . . ?
C34B C33B C32B 116(2) . . ?
C33B C34B H34B 119.8 . . ?
C35B C34B C33B 120(2) . . ?
C35B C34B H34B 119.8 . . ?
O6B C35B C34B 132(2) . . ?
O6B C35B C36B 112.3(17) . . ?
C34B C35B C36B 115.7(18) . . ?
F16B C36B C35B 112.1(18) . . ?
F17B C36B F16B 105.2(15) . . ?
F17B C36B C35B 106.4(15) . . ?
F18B C36B F16B 110.6(18) . . ?
F18B C36B F17B 110.5(17) . . ?
F18B C36B C35B 111.7(17) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Eu1C O1C C23C C22C 150.4(12) . . . . ?
Eu1C O1C C23C C24C -30(3) . . . . ?
Eu1C O2C C25C C24C 5(2) . . . . ?
Eu1C O2C C25C C26C -173.1(11) . . . . ?
Eu1C O3C C28C C27C 162.5(14) . . . . ?
Eu1C O3C C28C C29C -17(3) . . . . ?
Eu1C O4C C30C C29C 1(4) . . . . ?
Eu1C O4C C30C C31C -169.1(19) . . . . ?
Eu1C O5C C33C C32C -167.3(14) . . . . ?
Eu1C O5C C33C C34C 10(3) . . . . ?
Eu1C O6C C35C C34C -18(3) . . . . ?
Eu1C O6C C35C C36C 171.9(14) . . . . ?
Eu1C O6C C35C C36D 146.0(16) . . . . ?
Eu1C N1C C1C C2C -158.2(14) . . . . ?
Eu1C N1C C5C C4C 156.9(11) . . . . ?
Eu1C N1C C5C C6C -23.3(15) . . . . ?
Eu1C N2C C6C C5C -4.3(16) . . . . ?
Eu1C N2C C6C C7C 173.1(10) . . . . ?
Eu1C N2C C10C C9C -171.5(10) . . . . ?
Eu1C N2C C10C C11C 8.0(15) . . . . ?
Eu1C N3C C11C C10C -0.5(17) . . . . ?
Eu1C N3C C11C C12C 179.7(11) . . . . ?
Eu1C N3C C15C C14C -178.9(11) . . . . ?
F1C C22C C23C O1C -71(2) . . . . ?
F1C C22C C23C C24C 109(2) . . . . ?
F2C C22C C23C O1C 53(2) . . . . ?
F2C C22C C23C C24C -127(2) . . . . ?
F3C C22C C23C O1C 167.6(18) . . . . ?
F3C C22C C23C C24C -12(3) . . . . ?
F7C C27C C28C O3C 74(2) . . . . ?
F7C C27C C28C C29C -107(2) . . . . ?
F8C C27C C28C O3C -165(2) . . . . ?
F8C C27C C28C C29C 15(3) . . . . ?
F9C C27C C28C O3C -43(3) . . . . ?
F9C C27C C28C C29C 137(2) . . . . ?
F13C C32C C33C O5C -4(3) . . . . ?
F13C C32C C33C C34C 179(2) . . . . ?
F14C C32C C33C O5C 144(2) . . . . ?
F14C C32C C33C C34C -33(3) . . . . ?
F15C C32C C33C O5C -109(2) . . . . ?
F15C C32C C33C C34C 73(2) . . . . ?
O1C C23C C24C C25C 0(3) . . . . ?
O2C C25C C26C F4C 130.1(15) . . . . ?
O2C C25C C26C F5C -111.7(16) . . . . ?
O2C C25C C26C F6C 8(2) . . . . ?
O3C C28C C29C C30C -3(3) . . . . ?
O4C C30C C31C F10C -47(4) . . . . ?
O4C C30C C31C F11C 80(3) . . . . ?
O4C C30C C31C F12C -166(3) . . . . ?
O5C C33C C34C C35C 8(3) . . . . ?
O6C C35C C36C F16C -66(3) . . . . ?
O6C C35C C36C F17C -177(3) . . . . ?
O6C C35C C36C F18C 56(3) . . . . ?
O6C C35C C36D F16D 134(3) . . . . ?
O6C C35C C36D F17D 21(3) . . . . ?
O6C C35C C36D F18D -96(3) . . . . ?
N1C C1C C2C C3C 1(3) . . . . ?
N1C C5C C6C N2C 18.4(18) . . . . ?
N1C C5C C6C C7C -159.1(13) . . . . ?
N2C C6C C7C C8C -2(2) . . . . ?
N2C C10C C11C N3C -4.7(18) . . . . ?
N2C C10C C11C C12C 175.1(13) . . . . ?
N3C C11C C12C C13C -1(2) . . . . ?
C1C N1C C5C C4C -3(2) . . . . ?
C1C N1C C5C C6C 176.5(13) . . . . ?
C1C C2C C3C C4C -2(3) . . . . ?
C2C C3C C4C C5C 1(3) . . . . ?
C3C C4C C5C N1C 2(2) . . . . ?
C3C C4C C5C C6C -177.9(14) . . . . ?
C4C C5C C6C N2C -161.8(13) . . . . ?
C4C C5C C6C C7C 21(2) . . . . ?
C5C N1C C1C C2C 2(2) . . . . ?
C5C C6C C7C C8C 175.3(13) . . . . ?
C6C N2C C10C C9C 2.8(19) . . . . ?
C6C N2C C10C C11C -177.6(11) . . . . ?
C6C C7C C8C C9C 4(2) . . . . ?
C6C C7C C8C C16C -174.4(13) . . . . ?
C7C C8C C9C C10C -2(2) . . . . ?
C7C C8C C16C C17C 21(2) . . . . ?
C7C C8C C16C C21C -158.2(14) . . . . ?
C8C C9C C10C N2C -1(2) . . . . ?
C8C C9C C10C C11C 179.4(12) . . . . ?
C8C C16C C17C C18C 179.5(17) . . . . ?
C8C C16C C21C C20C -178.1(14) . . . . ?
C9C C8C C16C C17C -156.6(17) . . . . ?
C9C C8C C16C C21C 24(2) . . . . ?
C9C C10C C11C N3C 174.8(13) . . . . ?
C9C C10C C11C C12C -5(2) . . . . ?
C10C N2C C6C C5C -178.8(11) . . . . ?
C10C N2C C6C C7C -1(2) . . . . ?
C10C C11C C12C C13C 178.8(14) . . . . ?
C11C N3C C15C C14C -1(2) . . . . ?
C11C C12C C13C C14C 0(3) . . . . ?
C12C C13C C14C C15C 1(3) . . . . ?
C13C C14C C15C N3C 0(2) . . . . ?
C15C N3C C11C C10C -178.1(13) . . . . ?
C15C N3C C11C C12C 2(2) . . . . ?
C16C C8C C9C C10C 175.8(13) . . . . ?
C16C C17C C18C C19C -2(3) . . . . ?
C17C C16C C21C C20C 2(3) . . . . ?
C17C C18C C19C C20C 3(3) . . . . ?
C18C C19C C20C C21C -2(3) . . . . ?
C19C C20C C21C C16C -1(3) . . . . ?
C21C C16C C17C C18C -1(3) . . . . ?
C22C C23C C24C C25C -179.5(15) . . . . ?
C23C C24C C25C O2C 12(2) . . . . ?
C23C C24C C25C C26C -170.1(15) . . . . ?
C24C C25C C26C F4C -48(2) . . . . ?
C24C C25C C26C F5C 69.8(18) . . . . ?
C24C C25C C26C F6C -170.6(14) . . . . ?
C27C C28C C29C C30C 178(2) . . . . ?
C28C C29C C30C O4C 12(4) . . . . ?
C28C C29C C30C C31C -178(2) . . . . ?
C29C C30C C31C F10C 140(3) . . . . ?
C29C C30C C31C F11C -93(3) . . . . ?
C29C C30C C31C F12C 21(4) . . . . ?
C32C C33C C34C C35C -175.0(18) . . . . ?
C33C C34C C35C O6C -4(3) . . . . ?
C33C C34C C35C C36C 165.3(19) . . . . ?
C33C C34C C35C C36D -169.2(18) . . . . ?
C34C C35C C36C F16C 122(3) . . . . ?
C34C C35C C36C F17C 11(4) . . . . ?
C34C C35C C36C F18C -116(3) . . . . ?
C34C C35C C36D F16D -59(3) . . . . ?
C34C C35C C36D F17D -172(2) . . . . ?
C34C C35C C36D F18D 71(3) . . . . ?
Eu1A O1A C23A C22A -168.9(11) . . . . ?
Eu1A O1A C23A C24A 5(3) . . . . ?
Eu1A O2A C25A C24A -15(3) . . . . ?
Eu1A O2A C25A C26A 165.5(11) . . . . ?
Eu1A O3A C28A C27A 167.2(14) . . . . ?
Eu1A O3A C28A C29A -8(3) . . . . ?
Eu1A O4A C30A C29A 13(3) . . . . ?
Eu1A O4A C30A C31A -163.3(11) . . . . ?
Eu1A O5A C33A C32A -173.2(10) . . . . ?
Eu1A O5A C33A C34A 3(3) . . . . ?
Eu1A O6A C35A C34A -11(4) . . . . ?
Eu1A O6A C35A C36A 165.8(15) . . . . ?
Eu1A N1A C1A C2A -161.6(12) . . . . ?
Eu1A N1A C5A C4A 162.0(12) . . . . ?
Eu1A N1A C5A C6A -21.5(16) . . . . ?
Eu1A N2A C6A C5A -4.6(15) . . . . ?
Eu1A N2A C6A C7A 176.0(10) . . . . ?
Eu1A N2A C10A C9A -175.6(11) . . . . ?
Eu1A N2A C10A C11A 4.4(16) . . . . ?
Eu1A N3A C11A C10A -1.3(18) . . . . ?
Eu1A N3A C11A C12A 175.7(11) . . . . ?
Eu1A N3A C15A C14A -172.8(13) . . . . ?
F1A C22A C23A O1A -54(2) . . . . ?
F1A C22A C23A C24A 131.1(18) . . . . ?
F2A C22A C23A O1A -172.0(19) . . . . ?
F2A C22A C23A C24A 13(3) . . . . ?
F3A C22A C23A O1A 61(2) . . . . ?
F3A C22A C23A C24A -114(2) . . . . ?
F7A C27A C28A O3A 69(2) . . . . ?
F7A C27A C28A C29A -115(2) . . . . ?
F8A C27A C28A O3A -178(2) . . . . ?
F8A C27A C28A C29A -2(3) . . . . ?
F9A C27A C28A O3A -54(2) . . . . ?
F9A C27A C28A C29A 122(2) . . . . ?
F13A C32A C33A O5A -7(2) . . . . ?
F13A C32A C33A C34A 175.8(14) . . . . ?
F14A C32A C33A O5A 109.6(15) . . . . ?
F14A C32A C33A C34A -67.1(18) . . . . ?
F15A C32A C33A O5A -132.8(15) . . . . ?
F15A C32A C33A C34A 50.5(19) . . . . ?
O1A C23A C24A C25A 1(3) . . . . ?
O2A C25A C26A F4A 94.5(17) . . . . ?
O2A C25A C26A F5A -144.4(15) . . . . ?
O2A C25A C26A F6A -24(2) . . . . ?
O3A C28A C29A C30A -4(3) . . . . ?
O4A C30A C31A F10A -48(3) . . . . ?
O4A C30A C31A F11A 65(2) . . . . ?
O4A C30A C31A F12A -171.8(19) . . . . ?
O5A C33A C34A C35A 10(3) . . . . ?
O6A C35A C36A F16A -43(3) . . . . ?
O6A C35A C36A F17A 73(2) . . . . ?
O6A C35A C36A F18A -160(2) . . . . ?
N1A C1A C2A C3A 1(3) . . . . ?
N1A C5A C6A N2A 17.3(18) . . . . ?
N1A C5A C6A C7A -163.3(13) . . . . ?
N2A C6A C7A C8A -1(2) . . . . ?
N2A C10A C11A N3A -2.0(19) . . . . ?
N2A C10A C11A C12A -179.0(14) . . . . ?
N3A C11A C12A C13A 0(2) . . . . ?
C1A N1A C5A C4A 1(2) . . . . ?
C1A N1A C5A C6A 177.5(13) . . . . ?
C1A C2A C3A C4A -2(3) . . . . ?
C2A C3A C4A C5A 2(3) . . . . ?
C3A C4A C5A N1A -2(2) . . . . ?
C3A C4A C5A C6A -178.1(15) . . . . ?
C4A C5A C6A N2A -166.2(14) . . . . ?
C4A C5A C6A C7A 13(2) . . . . ?
C5A N1A C1A C2A -1(2) . . . . ?
C5A C6A C7A C8A 179.4(12) . . . . ?
C6A N2A C10A C9A 0(2) . . . . ?
C6A N2A C10A C11A -179.6(12) . . . . ?
C6A C7A C8A C9A 2(2) . . . . ?
C6A C7A C8A C16A -173.9(13) . . . . ?
C7A C8A C9A C10A -2(2) . . . . ?
C7A C8A C16A C17A 26(2) . . . . ?
C7A C8A C16A C21A -156.1(15) . . . . ?
C8A C9A C10A N2A 1(2) . . . . ?
C8A C9A C10A C11A -179.2(13) . . . . ?
C8A C16A C17A C18A 176.2(18) . . . . ?
C8A C16A C21A C20A -174.2(16) . . . . ?
C9A C8A C16A C17A -150.1(17) . . . . ?
C9A C8A C16A C21A 28(2) . . . . ?
C9A C10A C11A N3A 178.1(14) . . . . ?
C9A C10A C11A C12A 1(2) . . . . ?
C10A N2A C6A C5A 179.3(11) . . . . ?
C10A N2A C6A C7A -0.1(19) . . . . ?
C10A C11A C12A C13A 176.5(15) . . . . ?
C11A N3A C15A C14A 4(3) . . . . ?
C11A C12A C13A C14A -1(3) . . . . ?
C12A C13A C14A C15A 3(3) . . . . ?
C13A C14A C15A N3A -5(3) . . . . ?
C15A N3A C11A C10A -178.5(14) . . . . ?
C15A N3A C11A C12A -1(2) . . . . ?
C16A C8A C9A C10A 174.0(14) . . . . ?
C16A C17A C18A C19A -1(3) . . . . ?
C17A C16A C21A C20A 4(3) . . . . ?
C17A C18A C19A C20A 2(3) . . . . ?
C18A C19A C20A C21A 1(4) . . . . ?
C19A C20A C21A C16A -3(3) . . . . ?
C21A C16A C17A C18A -2(3) . . . . ?
C22A C23A C24A C25A 175.2(16) . . . . ?
C23A C24A C25A O2A 4(3) . . . . ?
C23A C24A C25A C26A -177.0(17) . . . . ?
C24A C25A C26A F4A -85.0(18) . . . . ?
C24A C25A C26A F5A 36(2) . . . . ?
C24A C25A C26A F6A 157.0(15) . . . . ?
C27A C28A C29A C30A -178.4(19) . . . . ?
C28A C29A C30A O4A 1(3) . . . . ?
C28A C29A C30A C31A 177.0(16) . . . . ?
C29A C30A C31A F10A 135(2) . . . . ?
C29A C30A C31A F11A -112(2) . . . . ?
C29A C30A C31A F12A 11(3) . . . . ?
C32A C33A C34A C35A -174.1(16) . . . . ?
C33A C34A C35A O6A -6(3) . . . . ?
C33A C34A C35A C36A 176.9(17) . . . . ?
C34A C35A C36A F16A 134.3(18) . . . . ?
C34A C35A C36A F17A -109(2) . . . . ?
C34A C35A C36A F18A 17(3) . . . . ?
Eu1B O1B C23B C22B 164.4(11) . . . . ?
Eu1B O1B C23B C24B -16(3) . . . . ?
Eu1B O2B C25B C24B 14(6) . . . . ?
Eu1B O2B C25B C26B -172(3) . . . . ?
Eu1B O3B C28B C27B 174.7(15) . . . . ?
Eu1B O3B C28B C29B -1(4) . . . . ?
Eu1B O4B C30B C29B -2(4) . . . . ?
Eu1B O4B C30B C31B 179.0(16) . . . . ?
Eu1B O5B C33B C32B -158.4(19) . . . . ?
Eu1B O5B C33B C34B 11(4) . . . . ?
Eu1B O6B C35B C34B -13(4) . . . . ?
Eu1B O6B C35B C36B 161.6(12) . . . . ?
Eu1B N1B C1B C2B -165.9(16) . . . . ?
Eu1B N1B C5B C4B 164.4(13) . . . . ?
Eu1B N1B C5B C6B -16(2) . . . . ?
Eu1B N2B C6B C5B -8(2) . . . . ?
Eu1B N2B C6B C7B 173.8(13) . . . . ?
Eu1B N2B C10B C9B -173.7(12) . . . . ?
Eu1B N2B C10B C11B 7.5(19) . . . . ?
Eu1B N3B C11B C10B 9(2) . . . . ?
Eu1B N3B C11B C12B -172.6(15) . . . . ?
Eu1B N3B C15B C14B 173(2) . . . . ?
F1B C22B C23B O1B -56(2) . . . . ?
F1B C22B C23B C24B 124.2(19) . . . . ?
F2B C22B C23B O1B 62.4(18) . . . . ?
F2B C22B C23B C24B -117.5(19) . . . . ?
F3B C22B C23B O1B -178.5(15) . . . . ?
F3B C22B C23B C24B 2(2) . . . . ?
F7B C27B C28B O3B 36(4) . . . . ?
F7B C27B C28B C29B -147(3) . . . . ?
F8B C27B C28B O3B 169(2) . . . . ?
F8B C27B C28B C29B -15(4) . . . . ?
F9B C27B C28B O3B -81(3) . . . . ?
F9B C27B C28B C29B 96(3) . . . . ?
F13B C32B C33B O5B 8(4) . . . . ?
F13B C32B C33B C34B -161(3) . . . . ?
F14B C32B C33B O5B 134(3) . . . . ?
F14B C32B C33B C34B -36(3) . . . . ?
F15B C32B C33B O5B -110(3) . . . . ?
F15B C32B C33B C34B 80(3) . . . . ?
O1B C23B C24B C25B -8(3) . . . . ?
O2B C25B C26B F4B 151(4) . . . . ?
O2B C25B C26B F5B -95(3) . . . . ?
O2B C25B C26B F6B 11(7) . . . . ?
O3B C28B C29B C30B -3(5) . . . . ?
O4B C30B C31B F10B -62(3) . . . . ?
O4B C30B C31B F11B 49(4) . . . . ?
O4B C30B C31B F12B 179(3) . . . . ?
O5B C33B C34B C35B 18(4) . . . . ?
O6B C35B C36B F16B -54(2) . . . . ?
O6B C35B C36B F17B 60(2) . . . . ?
O6B C35B C36B F18B -178.9(17) . . . . ?
N1B C1B C2B C3B 1(3) . . . . ?
N1B C5B C6B N2B 16(2) . . . . ?
N1B C5B C6B C7B -165.9(16) . . . . ?
N2B C6B C7B C8B -3(2) . . . . ?
N2B C10B C11B N3B -11(2) . . . . ?
N2B C10B C11B C12B 171.1(17) . . . . ?
N3B C11B C12B C13B -3(3) . . . . ?
C1B N1B C5B C4B 1(3) . . . . ?
C1B N1B C5B C6B -178.8(17) . . . . ?
C1B C2B C3B C4B 2(3) . . . . ?
C2B C3B C4B C5B -4(3) . . . . ?
C3B C4B C5B N1B 2(3) . . . . ?
C3B C4B C5B C6B -177.9(18) . . . . ?
C4B C5B C6B N2B -164.4(16) . . . . ?
C4B C5B C6B C7B 14(2) . . . . ?
C5B N1B C1B C2B -3(3) . . . . ?
C5B C6B C7B C8B 178.3(14) . . . . ?
C6B N2B C10B C9B 0(2) . . . . ?
C6B N2B C10B C11B -178.7(15) . . . . ?
C6B C7B C8B C9B 6(2) . . . . ?
C6B C7B C8B C16B -177.3(14) . . . . ?
C7B C8B C9B C10B -7(2) . . . . ?
C7B C8B C16B C17B -21(2) . . . . ?
C7B C8B C16B C21B 156.1(14) . . . . ?
C8B C9B C10B N2B 3(2) . . . . ?
C8B C9B C10B C11B -178.0(15) . . . . ?
C8B C16B C17B C18B 177.5(15) . . . . ?
C8B C16B C21B C20B -177.4(13) . . . . ?
C9B C8B C16B C17B 155.3(15) . . . . ?
C9B C8B C16B C21B -28(2) . . . . ?
C9B C10B C11B N3B 170.4(17) . . . . ?
C9B C10B C11B C12B -8(3) . . . . ?
C10B N2B C6B C5B 178.4(15) . . . . ?
C10B N2B C6B C7B 0(3) . . . . ?
C10B C11B C12B C13B 174.7(18) . . . . ?
C11B N3B C15B C14B -3(4) . . . . ?
C11B C12B C13B C14B 3(3) . . . . ?
C12B C13B C14B C15B -2(4) . . . . ?
C13B C14B C15B N3B 2(5) . . . . ?
C15B N3B C11B C10B -175(2) . . . . ?
C15B N3B C11B C12B 3(3) . . . . ?
C16B C8B C9B C10B 177.3(15) . . . . ?
C16B C17B C18B C19B 1(3) . . . . ?
C17B C16B C21B C20B 0(2) . . . . ?
C17B C18B C19B C20B -2(3) . . . . ?
C18B C19B C20B C21B 2(3) . . . . ?
C19B C20B C21B C16B -1(2) . . . . ?
C21B C16B C17B C18B 1(2) . . . . ?
C22B C23B C24B C25B 172(2) . . . . ?
C23B C24B C25B O2B 8(5) . . . . ?
C23B C24B C25B C26B -166(4) . . . . ?
C24B C25B C26B F4B -34(6) . . . . ?
C24B C25B C26B F5B 80(5) . . . . ?
C24B C25B C26B F6B -174(5) . . . . ?
C27B C28B C29B C30B -179(3) . . . . ?
C28B C29B C30B O4B 5(5) . . . . ?
C28B C29B C30B C31B -176(3) . . . . ?
C29B C30B C31B F10B 118(3) . . . . ?
C29B C30B C31B F11B -130(3) . . . . ?
C29B C30B C31B F12B -1(4) . . . . ?
C32B C33B C34B C35B -172(2) . . . . ?
C33B C34B C35B O6B -17(4) . . . . ?
C33B C34B C35B C36B 169(2) . . . . ?
C34B C35B C36B F16B 122(2) . . . . ?
C34B C35B C36B F17B -124(2) . . . . ?
C34B C35B C36B F18B -3(3) . . . . ?

_olex2_date_sample_data_collection 2023-07-20
_olex2_date_sample_submission    2023-07-20
_olex2_exptl_crystal_mounting_method 'MiTeGen microloop in fomblin oil'
_olex2_submission_original_sample_id Eu
_olex2_submission_special_instructions 'No special instructions were received'
loop_
_twin_individual_id
_twin_individual_mass_fraction_refined
1 0.50794
2 0.49206

