# Supplementary Information (SI) for Journal of Materials Chemistry C.
# This journal is © The Royal Society of Chemistry 2024

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_cmcm
_database_code_depnum_ccdc_archive 'CCDC 2357729'
loop_
_audit_author_name
_audit_author_address
'Xiuquan Zhou and Hengdi Zhao'
;Argonne National Laboratory
United States of America
;
_audit_update_record             
;
2024-05-23 deposited with the CCDC.	2024-10-25 downloaded from the CCDC.
;
_audit_creation_date             2024-02-14
_audit_creation_method           
;
Olex2 1.5
(compiled 2023.08.24 svn.re1ec1418 for OlexSys, GUI svn.r6817)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'Fe1.44 Ge8 Y4'
_chemical_formula_sum            'Fe1.44 Ge8 Y4'
_chemical_formula_weight         1016.78
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Fe Fe 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ge Ge 0.1547 1.8001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Y Y -2.7962 3.5667 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      orthorhombic
_space_group_IT_number           63
_space_group_name_H-M_alt        'C m c m'
_space_group_name_Hall           '-C 2c 2'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, z+1/2'
'-x, y, -z+1/2'
'x, -y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, -z+1/2'
'x+1/2, -y+1/2, -z'
'-x, -y, -z'
'x, y, -z-1/2'
'x, -y, z-1/2'
'-x, y, z'
'-x+1/2, -y+1/2, -z'
'x+1/2, y+1/2, -z-1/2'
'x+1/2, -y+1/2, z-1/2'
'-x+1/2, y+1/2, z'

_cell_length_a                   4.1384(2)
_cell_length_b                   15.8468(8)
_cell_length_c                   4.0178(2)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_volume                     263.49(2)
_cell_formula_units_Z            1
_cell_measurement_reflns_used    1867
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      30.419
_cell_measurement_theta_min      2.571
_shelx_estimated_absorpt_T_max   ?
_shelx_estimated_absorpt_T_min   ?
_exptl_absorpt_coefficient_mu    46.023
_exptl_absorpt_correction_T_max  0.5644
_exptl_absorpt_correction_T_min  0.3222
_exptl_absorpt_correction_type   ?
_exptl_absorpt_process_details   
;
SADABS-2016/2 (Bruker,2016/2) was used for absorption correction.
wR2(int) was 0.1429 before and 0.0367 after correction.
The Ratio of minimum to maximum transmission is 0.5709.
The λ/2 correction factor is Not present.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            silver
_exptl_crystal_density_diffrn    6.408
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       rod
_exptl_crystal_F_000             449
_exptl_crystal_size_max          ?
_exptl_crystal_size_mid          ?
_exptl_crystal_size_min          ?
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0298
_diffrn_reflns_av_unetI/netI     0.0101
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 1.000
_diffrn_reflns_limit_h_max       5
_diffrn_reflns_limit_h_min       -5
_diffrn_reflns_limit_k_max       22
_diffrn_reflns_limit_k_min       -22
_diffrn_reflns_limit_l_max       5
_diffrn_reflns_limit_l_min       -5
_diffrn_reflns_number            4690
_diffrn_reflns_point_group_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 1.000
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         30.478
_diffrn_reflns_theta_min         2.571
_diffrn_ambient_temperature      296.15
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_diffrn_source_current           30.0
_diffrn_source_power             1.35
_diffrn_source_voltage           45.0
_diffrn_standards_number         0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                245
_reflns_number_total             255
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT V8.38A (Bruker, 2018)'
_computing_data_collection       ?
_computing_data_reduction        'SAINT V8.38A (Bruker, 2018)'
_computing_molecular_graphics    'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2018/3 (Sheldrick, 2015)'
_computing_structure_solution    'ShelXT (Sheldrick, 2015)'
_refine_diff_density_max         0.962
_refine_diff_density_min         -0.759
_refine_diff_density_rms         0.148
_refine_ls_extinction_coef       0.0044(3)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     'SHELXL-2018/3 (Sheldrick 2018)'
_refine_ls_goodness_of_fit_ref   1.135
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     19
_refine_ls_number_reflns         255
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0150
_refine_ls_R_factor_gt           0.0138
_refine_ls_restrained_S_all      1.135
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0139P)²+0.4550P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0293
_refine_ls_wR_factor_ref         0.0298
_refine_special_details          ?
_olex2_refinement_description    
;
;
_atom_sites_solution_hydrogens   .
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Y001 Y 0.500000 0.39728(2) 0.750000 0.00791(12) Uani 1 4 d S T P . .
Ge00 Ge 0.000000 0.44766(3) 0.250000 0.01081(13) Uani 1 4 d S T P . .
Ge1 Ge 0.000000 0.25175(3) -0.250000 0.02737(16) Uani 1 4 d S T P . .
Fe04 Fe 0.000000 0.30308(10) 0.250000 0.0130(5) Uani 0.360(3) 4 d S T P . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Y001 Ge00 2.99243(19) . ?
Y001 Ge00 2.99244(19) 1_656 ?
Y001 Ge00 2.99244(19) 1_556 ?
Y001 Ge00 3.2123(4) 9_666 ?
Y001 Ge00 3.2123(4) 9_566 ?
Y001 Ge00 2.99244(18) 1_655 ?
Y001 Ge1 3.1005(5) 13 ?
Y001 Ge1 3.1005(5) 13_556 ?
Y001 Ge1 3.0984(5) 1_556 ?
Y001 Ge1 3.0984(5) 1_656 ?
Y001 Fe04 3.1751(16) 13_556 ?
Y001 Fe04 3.2474(7) . ?
Ge00 Ge00 2.6052(6) 9_566 ?
Ge00 Ge00 2.6052(6) 9_565 ?
Ge00 Fe04 2.2911(15) . ?
Ge1 Ge1 2.88450(10) 13_554 ?
Ge1 Ge1 2.88450(10) 13 ?
Ge1 Ge1 2.88450(10) 13_454 ?
Ge1 Ge1 2.88450(10) 13_455 ?
Ge1 Fe04 2.1673(6) 1_554 ?
Ge1 Fe04 2.2442(6) 13 ?
Ge1 Fe04 2.1673(6) . ?
Ge1 Fe04 2.2442(6) 13_455 ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Ge00 Y001 Ge00 149.05(2) . 1_656 ?
Ge00 Y001 Ge00 49.497(10) 1_655 9_666 ?
Ge00 Y001 Ge00 103.966(10) . 9_666 ?
Ge00 Y001 Ge00 84.339(7) 1_656 1_655 ?
Ge00 Y001 Ge00 87.494(7) 1_656 1_556 ?
Ge00 Y001 Ge00 103.965(10) 1_655 9_566 ?
Ge00 Y001 Ge00 49.497(10) 1_656 9_666 ?
Ge00 Y001 Ge00 103.965(10) 1_556 9_666 ?
Ge00 Y001 Ge00 49.498(10) . 9_566 ?
Ge00 Y001 Ge00 149.05(2) 1_556 1_655 ?
Ge00 Y001 Ge00 103.965(10) 1_656 9_566 ?
Ge00 Y001 Ge00 49.497(10) 1_556 9_566 ?
Ge00 Y001 Ge00 87.494(7) . 1_655 ?
Ge00 Y001 Ge00 84.339(7) . 1_556 ?
Ge00 Y001 Ge00 80.204(14) 9_666 9_566 ?
Ge00 Y001 Ge1 129.657(11) 1_656 13 ?
Ge00 Y001 Ge1 74.740(10) 1_656 1_656 ?
Ge00 Y001 Ge1 76.600(10) 1_656 13_556 ?
Ge00 Y001 Ge1 76.600(10) 1_556 13_556 ?
Ge00 Y001 Ge1 76.600(10) . 13 ?
Ge00 Y001 Ge1 74.740(10) 1_556 1_556 ?
Ge00 Y001 Ge1 76.600(10) 1_655 13 ?
Ge00 Y001 Ge1 131.327(10) . 1_656 ?
Ge00 Y001 Ge1 131.328(10) 1_556 1_656 ?
Ge00 Y001 Ge1 74.739(9) . 1_556 ?
Ge00 Y001 Ge1 129.656(10) . 13_556 ?
Ge00 Y001 Ge1 131.328(10) 1_656 1_556 ?
Ge00 Y001 Ge1 129.657(10) 1_556 13 ?
Ge00 Y001 Ge1 129.657(11) 1_655 13_556 ?
Ge00 Y001 Ge1 131.328(10) 1_655 1_556 ?
Ge00 Y001 Ge1 74.740(10) 1_655 1_656 ?
Ge00 Y001 Fe04 139.646(18) 9_666 . ?
Ge00 Y001 Fe04 168.11(3) 1_656 . ?
Ge00 Y001 Fe04 105.473(11) . 13_556 ?
Ge00 Y001 Fe04 42.84(2) . . ?
Ge00 Y001 Fe04 98.508(7) 1_655 . ?
Ge00 Y001 Fe04 105.474(11) 1_556 13_556 ?
Ge00 Y001 Fe04 86.63(2) 9_566 . ?
Ge00 Y001 Fe04 105.474(11) 1_655 13_556 ?
Ge00 Y001 Fe04 95.586(8) 1_556 . ?
Ge00 Y001 Fe04 105.474(11) 1_656 13_556 ?
Ge1 Y001 Ge00 97.999(10) 1_656 9_666 ?
Ge1 Y001 Ge00 178.202(11) 1_556 9_666 ?
Ge1 Y001 Ge00 125.636(5) 13_556 9_666 ?
Ge1 Y001 Ge00 178.202(11) 1_656 9_566 ?
Ge1 Y001 Ge00 97.999(10) 1_556 9_566 ?
Ge1 Y001 Ge00 125.636(5) 13_556 9_566 ?
Ge1 Y001 Ge00 125.636(5) 13 9_566 ?
Ge1 Y001 Ge00 125.636(5) 13 9_666 ?
Ge1 Y001 Ge1 83.799(16) 1_556 1_656 ?
Ge1 Y001 Ge1 55.462(6) 1_556 13 ?
Ge1 Y001 Ge1 80.770(16) 13 13_556 ?
Ge1 Y001 Ge1 55.462(6) 1_656 13_556 ?
Ge1 Y001 Ge1 55.462(6) 1_656 13 ?
Ge1 Y001 Ge1 55.462(6) 1_556 13_556 ?
Ge1 Y001 Fe04 41.899(8) 1_656 13_556 ?
Ge1 Y001 Fe04 94.78(2) 1_656 . ?
Ge1 Y001 Fe04 40.385(8) 13_556 13_556 ?
Ge1 Y001 Fe04 40.385(8) 13 13_556 ?
Ge1 Y001 Fe04 41.326(17) 13 . ?
Ge1 Y001 Fe04 92.90(2) 13_556 . ?
Ge1 Y001 Fe04 39.854(17) 1_556 . ?
Ge1 Y001 Fe04 41.899(8) 1_556 13_556 ?
Fe04 Y001 Ge00 139.898(7) 13_556 9_666 ?
Fe04 Y001 Ge00 139.898(7) 13_556 9_566 ?
Fe04 Y001 Fe04 62.63(2) 13_556 . ?
Y001 Ge00 Y001 76.034(10) . 9_666 ?
Y001 Ge00 Y001 84.339(7) 1_454 1_455 ?
Y001 Ge00 Y001 76.034(10) 1_454 9_566 ?
Y001 Ge00 Y001 87.495(7) 1_454 1_554 ?
Y001 Ge00 Y001 149.05(2) 1_454 . ?
Y001 Ge00 Y001 130.502(10) 1_455 9_666 ?
Y001 Ge00 Y001 130.502(10) 1_454 9_666 ?
Y001 Ge00 Y001 76.034(10) 1_455 9_566 ?
Y001 Ge00 Y001 84.339(7) . 1_554 ?
Y001 Ge00 Y001 80.203(14) 9_666 9_566 ?
Y001 Ge00 Y001 87.495(7) . 1_455 ?
Y001 Ge00 Y001 130.502(10) 1_554 9_566 ?
Y001 Ge00 Y001 149.05(2) 1_455 1_554 ?
Y001 Ge00 Y001 130.502(10) . 9_566 ?
Y001 Ge00 Y001 76.034(10) 1_554 9_666 ?
Ge00 Ge00 Y001 133.435(11) 9_566 1_554 ?
Ge00 Ge00 Y001 69.647(7) 9_566 1_455 ?
Ge00 Ge00 Y001 69.647(7) 9_565 1_554 ?
Ge00 Ge00 Y001 60.855(13) 9_566 9_666 ?
Ge00 Ge00 Y001 133.435(11) 9_566 1_454 ?
Ge00 Ge00 Y001 69.647(7) 9_565 1_454 ?
Ge00 Ge00 Y001 60.855(13) 9_566 9_566 ?
Ge00 Ge00 Y001 60.855(13) 9_565 9_566 ?
Ge00 Ge00 Y001 133.435(11) 9_565 1_455 ?
Ge00 Ge00 Y001 60.855(13) 9_565 9_666 ?
Ge00 Ge00 Y001 69.647(7) 9_566 . ?
Ge00 Ge00 Y001 133.435(11) 9_565 . ?
Ge00 Ge00 Ge00 100.91(3) 9_566 9_565 ?
Fe04 Ge00 Y001 74.527(11) . 1_454 ?
Fe04 Ge00 Y001 139.899(7) . 9_566 ?
Fe04 Ge00 Y001 74.527(11) . 1_455 ?
Fe04 Ge00 Y001 74.527(11) . 1_554 ?
Fe04 Ge00 Y001 139.899(7) . 9_666 ?
Fe04 Ge00 Y001 74.527(11) . . ?
Fe04 Ge00 Ge00 129.547(16) . 9_565 ?
Fe04 Ge00 Ge00 129.547(16) . 9_566 ?
Y001 Ge1 Y001 83.799(16) 1_554 1_454 ?
Y001 Ge1 Y001 124.538(6) 1_554 13 ?
Y001 Ge1 Y001 124.538(6) 1_454 13_556 ?
Y001 Ge1 Y001 80.770(16) 13 13_556 ?
Y001 Ge1 Y001 124.538(6) 1_454 13 ?
Y001 Ge1 Y001 124.538(6) 1_554 13_556 ?
Ge1 Ge1 Y001 119.56(2) 13_554 1_454 ?
Ge1 Ge1 Y001 62.232(14) 13_455 13_556 ?
Ge1 Ge1 Y001 119.56(2) 13_454 1_554 ?
Ge1 Ge1 Y001 62.307(15) 13_554 1_554 ?
Ge1 Ge1 Y001 62.307(15) 13_455 1_454 ?
Ge1 Ge1 Y001 62.307(15) 13_454 1_454 ?
Ge1 Ge1 Y001 119.56(2) 13 1_454 ?
Ge1 Ge1 Y001 115.89(2) 13_454 13_556 ?
Ge1 Ge1 Y001 62.232(14) 13_554 13 ?
Ge1 Ge1 Y001 115.89(2) 13 13 ?
Ge1 Ge1 Y001 119.56(2) 13_455 1_554 ?
Ge1 Ge1 Y001 62.232(14) 13_454 13 ?
Ge1 Ge1 Y001 62.307(15) 13 1_554 ?
Ge1 Ge1 Y001 115.89(2) 13_554 13_556 ?
Ge1 Ge1 Y001 62.232(14) 13 13_556 ?
Ge1 Ge1 Y001 115.89(2) 13_455 13 ?
Ge1 Ge1 Ge1 88.285(4) 13 13_554 ?
Ge1 Ge1 Ge1 177.79(4) 13_455 13_554 ?
Ge1 Ge1 Ge1 88.285(4) 13_454 13_455 ?
Ge1 Ge1 Ge1 91.672(4) 13 13_455 ?
Ge1 Ge1 Ge1 177.79(4) 13 13_454 ?
Ge1 Ge1 Ge1 91.672(4) 13_454 13_554 ?
Fe04 Ge1 Y001 70.88(4) 13 1_554 ?
Fe04 Ge1 Y001 154.68(4) 13_455 1_554 ?
Fe04 Ge1 Y001 73.78(3) 1_554 1_454 ?
Fe04 Ge1 Y001 73.78(3) . 1_454 ?
Fe04 Ge1 Y001 72.85(3) 13_455 13 ?
Fe04 Ge1 Y001 72.85(3) 13 13_556 ?
Fe04 Ge1 Y001 71.66(4) 1_554 13 ?
Fe04 Ge1 Y001 73.78(3) 1_554 1_554 ?
Fe04 Ge1 Y001 154.68(4) 13 1_454 ?
Fe04 Ge1 Y001 70.88(4) 13_455 1_454 ?
Fe04 Ge1 Y001 152.43(4) 1_554 13_556 ?
Fe04 Ge1 Y001 71.66(4) . 13_556 ?
Fe04 Ge1 Y001 72.85(3) 13_455 13_556 ?
Fe04 Ge1 Y001 72.85(3) 13 13 ?
Fe04 Ge1 Y001 152.43(4) . 13 ?
Fe04 Ge1 Y001 73.78(3) . 1_554 ?
Fe04 Ge1 Ge1 50.334(14) 1_554 13_454 ?
Fe04 Ge1 Ge1 50.334(14) . 13_455 ?
Fe04 Ge1 Ge1 48.021(14) 13 13 ?
Fe04 Ge1 Ge1 50.334(14) . 13 ?
Fe04 Ge1 Ge1 48.021(14) 13_455 13_454 ?
Fe04 Ge1 Ge1 130.75(2) . 13_554 ?
Fe04 Ge1 Ge1 130.84(2) 13 13_454 ?
Fe04 Ge1 Ge1 130.750(19) 1_554 13_455 ?
Fe04 Ge1 Ge1 50.334(14) 1_554 13_554 ?
Fe04 Ge1 Ge1 48.021(14) 13 13_554 ?
Fe04 Ge1 Ge1 130.84(2) 13 13_455 ?
Fe04 Ge1 Ge1 130.84(2) 13_455 13 ?
Fe04 Ge1 Ge1 48.021(14) 13_455 13_455 ?
Fe04 Ge1 Ge1 130.84(2) 13_455 13_554 ?
Fe04 Ge1 Ge1 130.750(19) 1_554 13 ?
Fe04 Ge1 Ge1 130.750(19) . 13_454 ?
Fe04 Ge1 Fe04 98.36(3) . 13_455 ?
Fe04 Ge1 Fe04 98.35(3) 1_554 13 ?
Fe04 Ge1 Fe04 98.36(3) . 13 ?
Fe04 Ge1 Fe04 134.44(7) 13_455 13 ?
Fe04 Ge1 Fe04 98.35(3) 1_554 13_455 ?
Fe04 Ge1 Fe04 135.91(8) 1_554 . ?
Y001 Fe04 Y001 125.27(5) 1_554 1_455 ?
Y001 Fe04 Y001 79.16(2) . 1_455 ?
Y001 Fe04 Y001 117.37(2) 13_556 1_455 ?
Y001 Fe04 Y001 79.16(2) 1_454 1_554 ?
Y001 Fe04 Y001 76.43(2) . 1_554 ?
Y001 Fe04 Y001 125.27(5) . 1_454 ?
Y001 Fe04 Y001 76.43(2) 1_454 1_455 ?
Y001 Fe04 Y001 117.37(2) 13_556 1_454 ?
Y001 Fe04 Y001 117.37(2) 13_556 . ?
Y001 Fe04 Y001 117.37(2) 13_556 1_554 ?
Ge00 Fe04 Y001 62.63(2) . 1_554 ?
Ge00 Fe04 Y001 180.0 . 13_556 ?
Ge00 Fe04 Y001 62.63(2) . 1_454 ?
Ge00 Fe04 Y001 62.63(2) . . ?
Ge00 Fe04 Y001 62.63(2) . 1_455 ?
Ge1 Fe04 Y001 139.949(9) 13 1_454 ?
Ge1 Fe04 Y001 139.949(9) 13_455 . ?
Ge1 Fe04 Y001 66.367(15) 1_556 . ?
Ge1 Fe04 Y001 66.367(15) 1_556 1_455 ?
Ge1 Fe04 Y001 139.949(9) 13_455 1_554 ?
Ge1 Fe04 Y001 65.826(14) 13 . ?
Ge1 Fe04 Y001 66.367(15) . 1_454 ?
Ge1 Fe04 Y001 67.22(4) 13 13_556 ?
Ge1 Fe04 Y001 138.238(11) 1_556 1_554 ?
Ge1 Fe04 Y001 65.826(14) 13_455 1_455 ?
Ge1 Fe04 Y001 67.22(4) 13_455 13_556 ?
Ge1 Fe04 Y001 67.96(4) 1_556 13_556 ?
Ge1 Fe04 Y001 138.238(11) 1_556 1_454 ?
Ge1 Fe04 Y001 138.238(11) . 1_455 ?
Ge1 Fe04 Y001 138.238(11) . . ?
Ge1 Fe04 Y001 67.96(4) . 13_556 ?
Ge1 Fe04 Y001 139.949(9) 13 1_455 ?
Ge1 Fe04 Y001 65.826(14) 13_455 1_454 ?
Ge1 Fe04 Y001 66.367(15) . 1_554 ?
Ge1 Fe04 Y001 65.826(14) 13 1_554 ?
Ge1 Fe04 Ge00 112.78(4) 13_455 . ?
Ge1 Fe04 Ge00 112.78(4) 13 . ?
Ge1 Fe04 Ge00 112.04(4) 1_556 . ?
Ge1 Fe04 Ge00 112.04(4) . . ?
Ge1 Fe04 Ge1 81.64(3) . 13 ?
Ge1 Fe04 Ge1 81.64(3) . 13_455 ?
Ge1 Fe04 Ge1 135.91(8) . 1_556 ?
Ge1 Fe04 Ge1 81.64(3) 1_556 13 ?
Ge1 Fe04 Ge1 81.64(3) 1_556 13_455 ?
Ge1 Fe04 Ge1 134.44(7) 13_455 13 ?


_olex2_submission_special_instructions 'No special instructions were received'
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_mus1042c_2_0m
_database_code_depnum_ccdc_archive 'CCDC 2357730'
loop_
_audit_author_name
_audit_author_address
'Xiuquan Zhou and Hengdi Zhao'
;Argonne National Laboratory
United States of America
;
_audit_update_record             
;
2024-05-23 deposited with the CCDC.	2024-10-25 downloaded from the CCDC.
;
# start Validation Reply Form
_vrf_SHFSU01_mus1042c_2_0m       
;
PROBLEM: The absolute value of parameter shift to su ratio > 0.20
RESPONSE: Due to weaker supercell reflections
;
_vrf_PLAT080_mus1042c_2_0m       
;
PROBLEM: Maximum Shift/Error ............................       0.75 Why ?
RESPONSE: Due to weaker supercell reflections
;
_vrf_PLAT211_mus1042c_2_0m       
;
PROBLEM: ADP of Atom Fe0D      is N.P.D. or (nearly) 2D .     Please Check
RESPONSE: Due to weaker supercell reflections
;
_vrf_PLAT112_mus1042c_2_0m       
;
PROBLEM: ADDSYM Detects New (Pseudo) Symm. Elem         d        100 %Fit
RESPONSE: The actual symmetry lowers to P-1 from Cmcm due to weak supercell reflections
;
# Added during the CSD deposition process: Thursday 23 May 2024 11:21 PM
# end Validation Reply Form

_audit_creation_date             2021-12-20
_audit_creation_method           
;
Olex2 1.2
(compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'Fe2.88 Ge16 Y8'
_chemical_formula_sum            'Fe2.87 Ge16 Y8'
_chemical_formula_weight         2033.01
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Fe Fe 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ge Ge 0.1547 1.8001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Y Y -2.7962 3.5667 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   5.7716(3)
_cell_length_b                   8.1916(4)
_cell_length_c                   11.5363(5)
_cell_angle_alpha                79.5610(10)
_cell_angle_beta                 88.3050(10)
_cell_angle_gamma                79.5490(10)
_cell_volume                     527.49(4)
_cell_formula_units_Z            1
_cell_measurement_reflns_used    1933
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      70.32
_cell_measurement_theta_min      3.59
_shelx_estimated_absorpt_T_max   ?
_shelx_estimated_absorpt_T_min   ?
_exptl_absorpt_coefficient_mu    45.972
_exptl_absorpt_correction_T_max  0.7469
_exptl_absorpt_correction_T_min  0.4433
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
SADABS-2016/2 (Bruker,2016/2) was used for absorption correction.
wR2(int) was 0.1233 before and 0.0441 after correction.
The Ratio of minimum to maximum transmission is 0.5935.
The λ/2 correction factor is Not present.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            silver
_exptl_crystal_density_diffrn    6.400
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       rod
_exptl_crystal_F_000             899
_exptl_crystal_size_max          ?
_exptl_crystal_size_mid          ?
_exptl_crystal_size_min          ?
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0532
_diffrn_reflns_av_unetI/netI     0.0501
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 0.956
_diffrn_reflns_limit_h_max       9
_diffrn_reflns_limit_h_min       -9
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_limit_l_min       -18
_diffrn_reflns_number            23168
_diffrn_reflns_point_group_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 0.956
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         35.160
_diffrn_reflns_theta_min         1.795
_diffrn_ambient_temperature      296.15
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 0.956
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_diffrn_standards_number         0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                993
_reflns_number_total             4508
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT V8.40A (?, 2016)'
_computing_data_collection       ?
_computing_data_reduction        'SAINT V8.40A (?, 2016)'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    'ShelXT (Sheldrick, 2015)'
_refine_diff_density_max         1.271
_refine_diff_density_min         -1.395
_refine_diff_density_rms         0.246
_refine_ls_extinction_coef       0.00131(10)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     'SHELXL-2018/3 (Sheldrick 2018)'
_refine_ls_goodness_of_fit_ref   0.946
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     150
_refine_ls_number_reflns         4508
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.1473
_refine_ls_R_factor_gt           0.0307
_refine_ls_restrained_S_all      0.946
_refine_ls_shift/su_max          0.755
_refine_ls_shift/su_mean         0.096
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0315P)²] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0749
_refine_ls_wR_factor_ref         0.1091
_refine_special_details          ?
_olex2_refinement_description    
;
;
_atom_sites_solution_hydrogens   .
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Y001 Y -0.3232(3) 0.7940(2) 0.71320(19) 0.0085(4) Uani 1 1 d . . . . .
Y002 Y -0.3237(3) 0.7943(2) 0.21295(19) 0.0082(4) Uani 1 1 d . . . . .
Y003 Y 0.8236(3) 0.2055(2) 0.03663(17) 0.0085(4) Uani 1 1 d . . . . .
Ge00 Ge 1.3487(4) 0.1045(3) 0.0493(2) 0.0109(5) Uani 1 1 d . . . . .
Y005 Y 0.1762(3) 0.7951(2) 0.46312(17) 0.0081(4) Uani 1 1 d . . . . .
Ge1 Ge 0.8480(3) 0.1054(3) 0.29939(19) 0.0114(5) Uani 1 1 d . . . . .
Ge2 Ge 0.1501(3) 0.8956(3) 0.20059(19) 0.0106(5) Uani 1 1 d . . . . .
Ge3 Ge -0.3488(4) 0.8959(3) 0.4505(2) 0.0114(5) Uani 1 1 d . . . . .
Ge4 Ge -0.0025(5) 0.5033(3) 0.3746(2) 0.0284(7) Uani 1 1 d . . . . .
Ge5 Ge 1.0007(5) 0.4966(3) 0.1254(3) 0.0284(7) Uani 1 1 d . . . . .
Ge6 Ge 0.5016(5) 0.5031(3) 0.1246(3) 0.0275(6) Uani 1 1 d . . . . .
Ge7 Ge 0.5021(5) 0.4952(3) 0.3755(3) 0.0269(6) Uani 1 1 d . . . . .
Fe0D Fe -0.2753(13) 0.6059(9) 0.4875(8) 0.007(2) Uani 0.320(7) 1 d . . . . .
Fe0E Fe 0.7772(15) 0.3931(10) 0.2627(8) 0.024(3) Uani 0.394(9) 1 d . . . . .
Fe0F Fe 0.2218(12) 0.6080(8) 0.2364(8) 0.014(2) Uani 0.385(8) 1 d . . . . .
Fe0G Fe 1.2747(15) 0.3956(10) 0.0141(7) 0.012(2) Uani 0.339(7) 1 d . . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Y001 Ge00 2.996(3) 2_666 ?
Y001 Ge1 2.992(3) 2_566 ?
Y001 Ge1 2.996(3) 2_666 ?
Y001 Ge2 3.217(3) 2_576 ?
Y001 Ge3 3.214(3) 2_476 ?
Y001 Ge3 2.995(3) . ?
Y001 Ge4 3.100(3) 2_566 ?
Y001 Ge5 3.097(3) 2_666 ?
Y001 Ge6 3.103(3) 2_566 ?
Y001 Ge7 3.090(3) 2_566 ?
Y001 Fe0D 3.238(9) . ?
Y001 Fe0F 3.186(7) 2_566 ?
Y002 Ge00 2.989(3) 2_665 ?
Y002 Ge00 3.213(3) 1_365 ?
Y002 Ge1 3.219(3) 1_465 ?
Y002 Ge2 3.000(3) 1_455 ?
Y002 Ge2 2.991(3) . ?
Y002 Ge3 2.997(3) . ?
Y002 Ge4 3.096(3) . ?
Y002 Ge5 3.098(3) 1_455 ?
Y002 Ge6 3.092(3) 1_455 ?
Y002 Ge7 3.106(3) 1_455 ?
Y002 Fe0E 3.180(8) 1_455 ?
Y002 Fe0F 3.236(7) . ?
Y003 Ge00 2.996(3) 1_455 ?
Y003 Ge00 2.994(3) . ?
Y003 Ge00 3.210(3) 2_755 ?
Y003 Ge1 2.994(3) . ?
Y003 Ge2 2.992(3) 2_665 ?
Y003 Ge2 3.210(3) 1_645 ?
Y003 Ge5 3.100(3) . ?
Y003 Ge5 3.100(3) 2_765 ?
Y003 Ge6 3.107(3) 2_665 ?
Y003 Ge6 3.093(3) . ?
Y003 Fe0F 3.238(9) 2_665 ?
Y003 Fe0G 3.162(8) 2_765 ?
Ge00 Ge00 2.603(4) 2_855 ?
Ge00 Ge2 2.607(3) 1_645 ?
Ge00 Fe0G 2.308(8) . ?
Y005 Ge1 3.216(3) 1_465 ?
Y005 Ge1 2.989(3) 2_666 ?
Y005 Ge2 2.992(3) . ?
Y005 Ge3 3.206(3) 2_576 ?
Y005 Ge3 2.993(3) . ?
Y005 Ge3 2.995(3) 1_655 ?
Y005 Ge4 3.108(3) . ?
Y005 Ge4 3.100(3) 2_566 ?
Y005 Ge7 3.116(3) . ?
Y005 Ge7 3.093(3) 2_666 ?
Y005 Fe0D 3.178(7) 2_566 ?
Y005 Fe0F 3.244(8) . ?
Ge1 Ge2 2.607(2) 1_645 ?
Ge1 Ge3 2.604(3) 1_645 ?
Ge1 Fe0E 2.280(8) . ?
Ge2 Fe0F 2.280(7) . ?
Ge3 Ge3 2.601(4) 2_476 ?
Ge3 Fe0D 2.298(7) . ?
Ge4 Ge4 2.886(6) 2_566 ?
Ge4 Ge5 2.884(3) 1_455 ?
Ge4 Ge7 2.872(3) 1_455 ?
Ge4 Ge7 2.901(3) . ?
Ge4 Fe0D 2.163(8) . ?
Ge4 Fe0D 2.241(9) 2_566 ?
Ge4 Fe0E 2.243(9) 1_455 ?
Ge4 Fe0F 2.176(8) . ?
Ge5 Ge5 2.884(6) 2_765 ?
Ge5 Ge6 2.901(3) 1_655 ?
Ge5 Ge6 2.871(3) . ?
Ge5 Fe0E 2.163(9) . ?
Ge5 Fe0F 2.246(9) 1_655 ?
Ge5 Fe0G 2.241(9) 2_765 ?
Ge5 Fe0G 2.150(9) . ?
Ge6 Ge6 2.884(6) 2_665 ?
Ge6 Ge7 2.883(3) . ?
Ge6 Fe0E 2.234(9) . ?
Ge6 Fe0F 2.188(8) . ?
Ge6 Fe0G 2.168(8) 2_765 ?
Ge6 Fe0G 2.245(10) 1_455 ?
Ge7 Ge7 2.888(6) 2_666 ?
Ge7 Fe0D 2.256(9) 1_655 ?
Ge7 Fe0D 2.167(8) 2_566 ?
Ge7 Fe0E 2.168(9) . ?
Ge7 Fe0F 2.262(8) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Ge00 Y001 Ge2 49.47(6) 2_666 2_576 ?
Ge00 Y001 Ge3 103.85(8) 2_666 2_476 ?
Ge00 Y001 Ge4 129.69(10) 2_666 2_566 ?
Ge00 Y001 Ge5 74.79(8) 2_666 2_666 ?
Ge00 Y001 Ge6 76.65(8) 2_666 2_566 ?
Ge00 Y001 Ge7 131.39(10) 2_666 2_566 ?
Ge00 Y001 Fe0D 168.17(15) 2_666 . ?
Ge00 Y001 Fe0F 105.55(17) 2_666 2_566 ?
Ge1 Y001 Ge00 87.47(8) 2_566 2_666 ?
Ge1 Y001 Ge00 84.33(8) 2_666 2_666 ?
Ge1 Y001 Ge1 149.11(11) 2_566 2_666 ?
Ge1 Y001 Ge2 104.04(8) 2_566 2_576 ?
Ge1 Y001 Ge2 49.46(6) 2_666 2_576 ?
Ge1 Y001 Ge3 104.04(8) 2_666 2_476 ?
Ge1 Y001 Ge3 49.46(6) 2_566 2_476 ?
Ge1 Y001 Ge3 84.28(8) 2_566 . ?
Ge1 Y001 Ge4 129.82(10) 2_566 2_566 ?
Ge1 Y001 Ge4 76.37(8) 2_666 2_566 ?
Ge1 Y001 Ge5 131.34(10) 2_566 2_666 ?
Ge1 Y001 Ge5 74.67(8) 2_666 2_666 ?
Ge1 Y001 Ge6 129.92(10) 2_666 2_566 ?
Ge1 Y001 Ge6 76.26(8) 2_566 2_566 ?
Ge1 Y001 Ge7 131.51(10) 2_666 2_566 ?
Ge1 Y001 Ge7 74.47(8) 2_566 2_566 ?
Ge1 Y001 Fe0D 98.41(15) 2_666 . ?
Ge1 Y001 Fe0D 95.67(15) 2_566 . ?
Ge1 Y001 Fe0F 105.55(15) 2_566 2_566 ?
Ge1 Y001 Fe0F 105.34(15) 2_666 2_566 ?
Ge2 Y001 Fe0D 139.56(15) 2_576 . ?
Ge3 Y001 Ge00 148.77(8) . 2_666 ?
Ge3 Y001 Ge1 87.47(8) . 2_666 ?
Ge3 Y001 Ge2 80.24(7) 2_476 2_576 ?
Ge3 Y001 Ge2 103.79(8) . 2_576 ?
Ge3 Y001 Ge3 49.38(8) . 2_476 ?
Ge3 Y001 Ge4 76.76(8) . 2_566 ?
Ge3 Y001 Ge5 131.51(9) . 2_666 ?
Ge3 Y001 Ge6 129.72(10) . 2_566 ?
Ge3 Y001 Ge7 74.81(8) . 2_566 ?
Ge3 Y001 Fe0D 86.71(14) 2_476 . ?
Ge3 Y001 Fe0D 43.05(14) . . ?
Ge3 Y001 Fe0F 105.68(17) . 2_566 ?
Ge4 Y001 Ge2 125.38(9) 2_566 2_576 ?
Ge4 Y001 Ge3 125.68(10) 2_566 2_476 ?
Ge4 Y001 Ge6 81.17(8) 2_566 2_566 ?
Ge4 Y001 Fe0D 41.33(14) 2_566 . ?
Ge4 Y001 Fe0F 40.48(15) 2_566 2_566 ?
Ge5 Y001 Ge2 97.92(9) 2_666 2_576 ?
Ge5 Y001 Ge3 178.16(10) 2_666 2_476 ?
Ge5 Y001 Ge4 55.48(7) 2_666 2_566 ?
Ge5 Y001 Ge6 55.81(7) 2_666 2_566 ?
Ge5 Y001 Fe0D 94.76(15) 2_666 . ?
Ge5 Y001 Fe0F 41.87(16) 2_666 2_566 ?
Ge6 Y001 Ge2 125.68(10) 2_566 2_576 ?
Ge6 Y001 Ge3 125.27(9) 2_566 2_476 ?
Ge6 Y001 Fe0D 92.99(15) 2_566 . ?
Ge6 Y001 Fe0F 40.69(15) 2_566 2_566 ?
Ge7 Y001 Ge2 177.99(10) 2_566 2_576 ?
Ge7 Y001 Ge3 97.75(9) 2_566 2_476 ?
Ge7 Y001 Ge4 55.89(7) 2_566 2_566 ?
Ge7 Y001 Ge5 84.09(9) 2_566 2_666 ?
Ge7 Y001 Ge6 55.49(7) 2_566 2_566 ?
Ge7 Y001 Fe0D 39.96(14) 2_566 . ?
Ge7 Y001 Fe0F 42.22(15) 2_566 2_566 ?
Fe0F Y001 Ge2 139.79(16) 2_566 2_576 ?
Fe0F Y001 Ge3 139.97(17) 2_566 2_476 ?
Fe0F Y001 Fe0D 62.63(18) 2_566 . ?
Ge00 Y002 Ge00 49.48(8) 2_665 1_365 ?
Ge00 Y002 Ge1 103.86(7) 2_665 1_465 ?
Ge00 Y002 Ge1 80.12(7) 1_365 1_465 ?
Ge00 Y002 Ge2 87.47(8) 2_665 . ?
Ge00 Y002 Ge2 84.40(8) 2_665 1_455 ?
Ge00 Y002 Ge3 148.86(8) 2_665 . ?
Ge00 Y002 Ge4 131.48(9) 2_665 . ?
Ge00 Y002 Ge5 76.69(8) 2_665 1_455 ?
Ge00 Y002 Ge6 74.87(8) 2_665 1_455 ?
Ge00 Y002 Ge7 129.76(10) 2_665 1_455 ?
Ge00 Y002 Fe0E 105.49(17) 2_665 1_455 ?
Ge00 Y002 Fe0F 139.54(16) 1_365 . ?
Ge00 Y002 Fe0F 98.50(16) 2_665 . ?
Ge1 Y002 Fe0F 86.53(14) 1_465 . ?
Ge2 Y002 Ge00 49.48(6) 1_455 1_365 ?
Ge2 Y002 Ge00 103.93(8) . 1_365 ?
Ge2 Y002 Ge1 49.48(6) . 1_465 ?
Ge2 Y002 Ge1 103.79(7) 1_455 1_465 ?
Ge2 Y002 Ge2 148.91(10) . 1_455 ?
Ge2 Y002 Ge3 84.19(8) . . ?
Ge2 Y002 Ge4 74.93(8) . . ?
Ge2 Y002 Ge4 131.17(9) 1_455 . ?
Ge2 Y002 Ge5 76.69(8) . 1_455 ?
Ge2 Y002 Ge5 129.76(10) 1_455 1_455 ?
Ge2 Y002 Ge6 75.05(8) 1_455 1_455 ?
Ge2 Y002 Ge6 131.23(10) . 1_455 ?
Ge2 Y002 Ge7 76.77(8) 1_455 1_455 ?
Ge2 Y002 Ge7 129.56(10) . 1_455 ?
Ge2 Y002 Fe0E 105.58(16) 1_455 1_455 ?
Ge2 Y002 Fe0E 105.51(16) . 1_455 ?
Ge2 Y002 Fe0F 168.36(15) 1_455 . ?
Ge2 Y002 Fe0F 42.72(14) . . ?
Ge3 Y002 Ge00 103.86(8) . 1_365 ?
Ge3 Y002 Ge1 49.37(6) . 1_465 ?
Ge3 Y002 Ge2 87.42(8) . 1_455 ?
Ge3 Y002 Ge4 74.76(9) . . ?
Ge3 Y002 Ge5 129.68(10) . 1_455 ?
Ge3 Y002 Ge6 131.48(9) . 1_455 ?
Ge3 Y002 Ge7 76.75(8) . 1_455 ?
Ge3 Y002 Fe0E 105.65(17) . 1_455 ?
Ge3 Y002 Fe0F 95.51(16) . . ?
Ge4 Y002 Ge00 178.24(10) . 1_365 ?
Ge4 Y002 Ge1 98.13(9) . 1_465 ?
Ge4 Y002 Ge5 55.50(7) . 1_455 ?
Ge4 Y002 Ge7 55.16(7) . 1_455 ?
Ge4 Y002 Fe0E 41.86(16) . 1_455 ?
Ge4 Y002 Fe0F 40.12(15) . . ?
Ge5 Y002 Ge00 125.70(10) 1_455 1_365 ?
Ge5 Y002 Ge1 125.71(9) 1_455 1_465 ?
Ge5 Y002 Ge7 80.62(8) 1_455 1_455 ?
Ge5 Y002 Fe0E 40.28(16) 1_455 1_455 ?
Ge5 Y002 Fe0F 41.47(15) 1_455 . ?
Ge6 Y002 Ge00 98.20(9) 1_455 1_365 ?
Ge6 Y002 Ge1 178.31(10) 1_455 1_465 ?
Ge6 Y002 Ge4 83.55(9) 1_455 . ?
Ge6 Y002 Ge5 55.26(7) 1_455 1_455 ?
Ge6 Y002 Ge7 55.44(7) 1_455 1_455 ?
Ge6 Y002 Fe0E 41.70(16) 1_455 1_455 ?
Ge6 Y002 Fe0F 94.75(14) 1_455 . ?
Ge7 Y002 Ge00 125.77(9) 1_455 1_365 ?
Ge7 Y002 Ge1 125.65(10) 1_455 1_465 ?
Ge7 Y002 Fe0E 40.33(16) 1_455 1_455 ?
Ge7 Y002 Fe0F 92.91(15) 1_455 . ?
Fe0E Y002 Ge00 139.89(17) 1_455 1_365 ?
Fe0E Y002 Ge1 139.99(17) 1_455 1_465 ?
Fe0E Y002 Fe0F 62.79(17) 1_455 . ?
Ge00 Y003 Ge00 103.94(7) . 2_755 ?
Ge00 Y003 Ge00 49.46(8) 1_455 2_755 ?
Ge00 Y003 Ge00 148.99(10) . 1_455 ?
Ge00 Y003 Ge1 84.42(7) . . ?
Ge00 Y003 Ge2 103.87(8) 1_455 1_645 ?
Ge00 Y003 Ge2 49.55(6) . 1_645 ?
Ge00 Y003 Ge5 131.32(9) 1_455 . ?
Ge00 Y003 Ge5 74.78(8) . . ?
Ge00 Y003 Ge5 76.59(8) . 2_765 ?
Ge00 Y003 Ge5 129.73(9) 1_455 2_765 ?
Ge00 Y003 Ge6 131.59(9) . 2_665 ?
Ge00 Y003 Ge6 74.56(8) 1_455 2_665 ?
Ge00 Y003 Ge6 76.81(8) 1_455 . ?
Ge00 Y003 Ge6 129.47(9) . . ?
Ge00 Y003 Fe0F 95.67(15) 1_455 2_665 ?
Ge00 Y003 Fe0F 86.56(14) 2_755 2_665 ?
Ge00 Y003 Fe0F 98.36(14) . 2_665 ?
Ge00 Y003 Fe0G 105.36(17) . 2_765 ?
Ge00 Y003 Fe0G 105.64(17) 1_455 2_765 ?
Ge1 Y003 Ge00 103.97(8) . 2_755 ?
Ge1 Y003 Ge00 87.44(8) . 1_455 ?
Ge1 Y003 Ge2 49.55(6) . 1_645 ?
Ge1 Y003 Ge5 74.66(8) . . ?
Ge1 Y003 Ge5 129.56(9) . 2_765 ?
Ge1 Y003 Ge6 131.03(9) . 2_665 ?
Ge1 Y003 Ge6 76.39(8) . . ?
Ge1 Y003 Fe0F 168.20(15) . 2_665 ?
Ge1 Y003 Fe0G 105.54(17) . 2_765 ?
Ge2 Y003 Ge00 49.57(6) 2_665 2_755 ?
Ge2 Y003 Ge00 87.37(8) 2_665 . ?
Ge2 Y003 Ge00 84.43(8) 2_665 1_455 ?
Ge2 Y003 Ge00 80.16(7) 1_645 2_755 ?
Ge2 Y003 Ge1 149.10(8) 2_665 . ?
Ge2 Y003 Ge2 103.92(7) 2_665 1_645 ?
Ge2 Y003 Ge5 76.65(8) 2_665 2_765 ?
Ge2 Y003 Ge5 131.33(8) 2_665 . ?
Ge2 Y003 Ge6 74.95(8) 2_665 2_665 ?
Ge2 Y003 Ge6 129.91(8) 2_665 . ?
Ge2 Y003 Fe0F 139.50(13) 1_645 2_665 ?
Ge2 Y003 Fe0F 42.70(13) 2_665 2_665 ?
Ge2 Y003 Fe0G 105.36(17) 2_665 2_765 ?
Ge5 Y003 Ge00 178.16(9) . 2_755 ?
Ge5 Y003 Ge00 125.74(9) 2_765 2_755 ?
Ge5 Y003 Ge2 125.67(8) 2_765 1_645 ?
Ge5 Y003 Ge2 98.00(8) . 1_645 ?
Ge5 Y003 Ge5 55.43(10) . 2_765 ?
Ge5 Y003 Ge6 83.88(9) . 2_665 ?
Ge5 Y003 Ge6 55.73(7) 2_765 2_665 ?
Ge5 Y003 Fe0F 41.44(15) 2_765 2_665 ?
Ge5 Y003 Fe0F 94.92(15) . 2_665 ?
Ge5 Y003 Fe0G 41.93(17) . 2_765 ?
Ge5 Y003 Fe0G 40.15(16) 2_765 2_765 ?
Ge6 Y003 Ge00 97.96(9) 2_665 2_755 ?
Ge6 Y003 Ge00 125.82(8) . 2_755 ?
Ge6 Y003 Ge2 125.46(9) . 1_645 ?
Ge6 Y003 Ge2 178.09(10) 2_665 1_645 ?
Ge6 Y003 Ge5 55.24(7) . . ?
Ge6 Y003 Ge5 80.69(8) . 2_765 ?
Ge6 Y003 Ge6 55.44(10) . 2_665 ?
Ge6 Y003 Fe0F 93.20(13) . 2_665 ?
Ge6 Y003 Fe0F 40.28(13) 2_665 2_665 ?
Ge6 Y003 Fe0G 40.54(16) . 2_765 ?
Ge6 Y003 Fe0G 41.96(17) 2_665 2_765 ?
Fe0G Y003 Ge00 139.91(18) 2_765 2_755 ?
Fe0G Y003 Ge2 139.93(18) 2_765 1_645 ?
Fe0G Y003 Fe0F 62.66(19) 2_765 2_665 ?
Y001 Ge00 Y002 76.16(8) 2_666 1_745 ?
Y001 Ge00 Y003 130.52(9) 2_666 2_755 ?
Y002 Ge00 Y001 148.86(9) 2_665 2_666 ?
Y002 Ge00 Y002 130.52(8) 2_665 1_745 ?
Y002 Ge00 Y003 87.42(8) 2_665 1_655 ?
Y002 Ge00 Y003 76.19(7) 2_665 2_755 ?
Y002 Ge00 Y003 84.34(8) 2_665 . ?
Y003 Ge00 Y001 84.32(8) 1_655 2_666 ?
Y003 Ge00 Y001 87.46(8) . 2_666 ?
Y003 Ge00 Y002 80.16(7) 2_755 1_745 ?
Y003 Ge00 Y002 130.56(9) . 1_745 ?
Y003 Ge00 Y002 76.04(7) 1_655 1_745 ?
Y003 Ge00 Y003 130.54(8) 1_655 2_755 ?
Y003 Ge00 Y003 148.99(10) . 1_655 ?
Y003 Ge00 Y003 76.06(7) . 2_755 ?
Ge00 Ge00 Y001 133.42(14) 2_855 2_666 ?
Ge00 Ge00 Y002 60.77(9) 2_855 1_745 ?
Ge00 Ge00 Y002 69.75(10) 2_855 2_665 ?
Ge00 Ge00 Y003 69.56(9) 2_855 1_655 ?
Ge00 Ge00 Y003 60.99(9) 2_855 2_755 ?
Ge00 Ge00 Y003 133.57(14) 2_855 . ?
Ge00 Ge00 Ge2 101.08(11) 2_855 1_645 ?
Ge2 Ge00 Y001 69.67(8) 1_645 2_666 ?
Ge2 Ge00 Y002 61.01(7) 1_645 1_745 ?
Ge2 Ge00 Y002 133.51(9) 1_645 2_665 ?
Ge2 Ge00 Y003 69.55(7) 1_645 . ?
Ge2 Ge00 Y003 60.85(7) 1_645 2_755 ?
Ge2 Ge00 Y003 133.55(9) 1_645 1_655 ?
Fe0G Ge00 Y001 74.1(2) . 2_666 ?
Fe0G Ge00 Y002 74.8(2) . 2_665 ?
Fe0G Ge00 Y002 139.8(2) . 1_745 ?
Fe0G Ge00 Y003 74.3(2) . . ?
Fe0G Ge00 Y003 140.0(2) . 2_755 ?
Fe0G Ge00 Y003 74.7(2) . 1_655 ?
Fe0G Ge00 Ge00 129.9(2) . 2_855 ?
Fe0G Ge00 Ge2 129.1(2) . 1_645 ?
Ge1 Y005 Ge1 104.12(7) 2_666 1_465 ?
Ge1 Y005 Ge2 149.26(8) 2_666 . ?
Ge1 Y005 Ge3 87.62(8) 2_666 . ?
Ge1 Y005 Ge3 84.31(8) 2_666 1_655 ?
Ge1 Y005 Ge3 49.55(6) 2_666 2_576 ?
Ge1 Y005 Ge4 131.14(8) 2_666 . ?
Ge1 Y005 Ge4 76.48(8) 2_666 2_566 ?
Ge1 Y005 Ge7 74.46(8) 2_666 2_666 ?
Ge1 Y005 Ge7 129.37(8) 2_666 . ?
Ge1 Y005 Fe0D 105.45(17) 2_666 2_566 ?
Ge1 Y005 Fe0F 86.45(14) 1_465 . ?
Ge1 Y005 Fe0F 168.10(15) 2_666 . ?
Ge2 Y005 Ge1 49.50(6) . 1_465 ?
Ge2 Y005 Ge3 104.11(8) . 2_576 ?
Ge2 Y005 Ge3 87.60(8) . 1_655 ?
Ge2 Y005 Ge3 84.23(8) . . ?
Ge2 Y005 Ge4 74.73(8) . . ?
Ge2 Y005 Ge4 129.62(9) . 2_566 ?
Ge2 Y005 Ge7 131.46(9) . 2_666 ?
Ge2 Y005 Ge7 76.74(7) . . ?
Ge2 Y005 Fe0D 105.29(17) . 2_566 ?
Ge2 Y005 Fe0F 42.65(14) . . ?
Ge3 Y005 Ge1 49.43(6) . 1_465 ?
Ge3 Y005 Ge1 104.02(8) 1_655 1_465 ?
Ge3 Y005 Ge1 80.31(7) 2_576 1_465 ?
Ge3 Y005 Ge3 104.03(7) . 2_576 ?
Ge3 Y005 Ge3 49.45(8) 1_655 2_576 ?
Ge3 Y005 Ge3 149.05(10) . 1_655 ?
Ge3 Y005 Ge4 131.45(9) 1_655 . ?
Ge3 Y005 Ge4 129.49(9) 1_655 2_566 ?
Ge3 Y005 Ge4 76.79(8) . 2_566 ?
Ge3 Y005 Ge4 74.63(8) . . ?
Ge3 Y005 Ge7 131.29(9) . 2_666 ?
Ge3 Y005 Ge7 74.76(8) 1_655 2_666 ?
Ge3 Y005 Ge7 129.66(9) . . ?
Ge3 Y005 Ge7 76.63(8) 1_655 . ?
Ge3 Y005 Fe0D 105.59(16) 1_655 2_566 ?
Ge3 Y005 Fe0D 105.36(16) . 2_566 ?
Ge3 Y005 Fe0F 98.58(15) 1_655 . ?
Ge3 Y005 Fe0F 139.63(15) 2_576 . ?
Ge3 Y005 Fe0F 95.42(14) . . ?
Ge4 Y005 Ge1 125.75(8) 2_566 1_465 ?
Ge4 Y005 Ge1 97.95(8) . 1_465 ?
Ge4 Y005 Ge3 125.56(9) 2_566 2_576 ?
Ge4 Y005 Ge3 178.26(9) . 2_576 ?
Ge4 Y005 Ge4 55.41(10) 2_566 . ?
Ge4 Y005 Ge7 55.56(7) . . ?
Ge4 Y005 Ge7 80.53(8) 2_566 . ?
Ge4 Y005 Fe0D 40.28(15) 2_566 2_566 ?
Ge4 Y005 Fe0D 41.74(16) . 2_566 ?
Ge4 Y005 Fe0F 92.98(15) 2_566 . ?
Ge4 Y005 Fe0F 40.00(15) . . ?
Ge7 Y005 Ge1 125.79(9) . 1_465 ?
Ge7 Y005 Ge1 178.16(10) 2_666 1_465 ?
Ge7 Y005 Ge3 97.86(9) 2_666 2_576 ?
Ge7 Y005 Ge3 125.60(8) . 2_576 ?
Ge7 Y005 Ge4 83.88(9) 2_666 . ?
Ge7 Y005 Ge4 55.26(7) 2_666 2_566 ?
Ge7 Y005 Ge7 55.44(10) 2_666 . ?
Ge7 Y005 Fe0D 42.14(16) 2_666 2_566 ?
Ge7 Y005 Fe0D 40.25(15) . 2_566 ?
Ge7 Y005 Fe0F 41.61(13) . . ?
Ge7 Y005 Fe0F 95.07(15) 2_666 . ?
Fe0D Y005 Ge1 139.69(17) 2_566 1_465 ?
Fe0D Y005 Ge3 140.00(17) 2_566 2_576 ?
Fe0D Y005 Fe0F 62.65(19) 2_566 . ?
Y001 Ge1 Y001 149.11(11) 2_566 2_666 ?
Y001 Ge1 Y002 76.12(7) 2_566 1_645 ?
Y001 Ge1 Y002 130.37(8) 2_666 1_645 ?
Y001 Ge1 Y003 84.44(8) 2_566 . ?
Y001 Ge1 Y005 75.95(7) 2_666 1_645 ?
Y001 Ge1 Y005 130.55(9) 2_566 1_645 ?
Y003 Ge1 Y001 87.46(8) . 2_666 ?
Y003 Ge1 Y002 75.98(7) . 1_645 ?
Y003 Ge1 Y005 130.32(8) . 1_645 ?
Y005 Ge1 Y001 87.62(7) 2_666 2_566 ?
Y005 Ge1 Y001 84.32(8) 2_666 2_666 ?
Y005 Ge1 Y002 130.43(8) 2_666 1_645 ?
Y005 Ge1 Y002 80.14(7) 1_645 1_645 ?
Y005 Ge1 Y003 149.34(9) 2_666 . ?
Y005 Ge1 Y005 75.87(7) 2_666 1_645 ?
Ge2 Ge1 Y001 69.68(7) 1_645 2_666 ?
Ge2 Ge1 Y001 133.38(9) 1_645 2_566 ?
Ge2 Ge1 Y002 60.69(6) 1_645 1_645 ?
Ge2 Ge1 Y003 69.55(7) 1_645 . ?
Ge2 Ge1 Y005 133.26(9) 1_645 2_666 ?
Ge2 Ge1 Y005 60.77(7) 1_645 1_645 ?
Ge3 Ge1 Y001 133.35(9) 1_645 2_666 ?
Ge3 Ge1 Y001 69.72(7) 1_645 2_566 ?
Ge3 Ge1 Y002 60.87(7) 1_645 1_645 ?
Ge3 Ge1 Y003 133.44(10) 1_645 . ?
Ge3 Ge1 Y005 60.83(7) 1_645 1_645 ?
Ge3 Ge1 Y005 69.56(7) 1_645 2_666 ?
Ge3 Ge1 Ge2 100.76(8) 1_645 1_645 ?
Fe0E Ge1 Y001 74.7(2) . 2_566 ?
Fe0E Ge1 Y001 74.4(2) . 2_666 ?
Fe0E Ge1 Y002 139.9(2) . 1_645 ?
Fe0E Ge1 Y003 74.4(2) . . ?
Fe0E Ge1 Y005 74.9(2) . 2_666 ?
Fe0E Ge1 Y005 139.9(2) . 1_645 ?
Fe0E Ge1 Ge2 129.4(2) . 1_645 ?
Fe0E Ge1 Ge3 129.9(2) . 1_645 ?
Y002 Ge2 Y001 130.69(8) . 2_576 ?
Y002 Ge2 Y001 76.05(7) 1_655 2_576 ?
Y002 Ge2 Y002 148.91(10) . 1_655 ?
Y002 Ge2 Y003 76.16(7) . 1_465 ?
Y002 Ge2 Y003 130.41(9) 1_655 1_465 ?
Y002 Ge2 Y003 84.34(8) . 2_665 ?
Y002 Ge2 Y005 87.64(8) . . ?
Y003 Ge2 Y001 80.22(7) 1_465 2_576 ?
Y003 Ge2 Y001 130.44(8) 2_665 2_576 ?
Y003 Ge2 Y002 87.30(7) 2_665 1_655 ?
Y003 Ge2 Y003 76.08(7) 2_665 1_465 ?
Ge00 Ge2 Y001 60.86(7) 1_465 2_576 ?
Ge00 Ge2 Y002 133.54(9) 1_465 . ?
Ge00 Ge2 Y002 69.52(7) 1_465 1_655 ?
Ge00 Ge2 Y003 69.58(7) 1_465 2_665 ?
Ge00 Ge2 Y003 60.90(7) 1_465 1_465 ?
Ge00 Ge2 Y005 133.33(10) 1_465 . ?
Y005 Ge2 Y001 75.99(7) . 2_576 ?
Y005 Ge2 Y002 84.29(8) . 1_655 ?
Y005 Ge2 Y003 149.02(8) . 2_665 ?
Y005 Ge2 Y003 130.63(8) . 1_465 ?
Ge1 Ge2 Y001 60.86(6) 1_465 2_576 ?
Ge1 Ge2 Y002 133.47(9) 1_465 1_655 ?
Ge1 Ge2 Y002 69.83(7) 1_465 . ?
Ge1 Ge2 Y003 60.90(7) 1_465 1_465 ?
Ge1 Ge2 Y003 133.56(8) 1_465 2_665 ?
Ge1 Ge2 Ge00 100.97(7) 1_465 1_465 ?
Ge1 Ge2 Y005 69.72(7) 1_465 . ?
Fe0F Ge2 Y001 139.9(2) . 2_576 ?
Fe0F Ge2 Y002 74.40(19) . . ?
Fe0F Ge2 Y002 74.51(19) . 1_655 ?
Fe0F Ge2 Y003 139.9(2) . 1_465 ?
Fe0F Ge2 Y003 74.4(2) . 2_665 ?
Fe0F Ge2 Ge00 129.4(2) . 1_465 ?
Fe0F Ge2 Y005 74.6(2) . . ?
Fe0F Ge2 Ge1 129.6(2) . 1_465 ?
Y001 Ge3 Y001 130.62(8) . 2_476 ?
Y001 Ge3 Y002 148.77(9) . . ?
Y001 Ge3 Y005 76.12(7) . 2_576 ?
Y001 Ge3 Y005 87.46(8) . 1_455 ?
Y002 Ge3 Y001 76.13(8) . 2_476 ?
Y002 Ge3 Y005 130.65(9) . 2_576 ?
Y005 Ge3 Y001 75.99(7) 1_455 2_476 ?
Y005 Ge3 Y001 84.27(8) . . ?
Y005 Ge3 Y001 80.32(7) 2_576 2_476 ?
Y005 Ge3 Y001 130.56(9) . 2_476 ?
Y005 Ge3 Y002 87.50(8) . . ?
Y005 Ge3 Y002 84.29(8) 1_455 . ?
Y005 Ge3 Y005 75.97(7) . 2_576 ?
Y005 Ge3 Y005 130.55(8) 1_455 2_576 ?
Y005 Ge3 Y005 149.05(10) . 1_455 ?
Ge1 Ge3 Y001 60.82(7) 1_465 2_476 ?
Ge1 Ge3 Y001 133.56(10) 1_465 . ?
Ge1 Ge3 Y002 69.77(8) 1_465 . ?
Ge1 Ge3 Y005 133.37(9) 1_465 1_455 ?
Ge1 Ge3 Y005 69.74(7) 1_465 . ?
Ge1 Ge3 Y005 60.88(7) 1_465 2_576 ?
Ge3 Ge3 Y001 60.91(9) 2_476 2_476 ?
Ge3 Ge3 Y001 69.70(10) 2_476 . ?
Ge3 Ge3 Y002 133.50(14) 2_476 . ?
Ge3 Ge3 Y005 69.49(10) 2_476 1_455 ?
Ge3 Ge3 Y005 61.05(9) 2_476 2_576 ?
Ge3 Ge3 Y005 133.53(14) 2_476 . ?
Ge3 Ge3 Ge1 101.01(12) 2_476 1_465 ?
Fe0D Ge3 Y001 140.1(2) . 2_476 ?
Fe0D Ge3 Y001 74.1(2) . . ?
Fe0D Ge3 Y002 74.6(2) . . ?
Fe0D Ge3 Y005 74.7(2) . 1_455 ?
Fe0D Ge3 Y005 139.5(2) . 2_576 ?
Fe0D Ge3 Y005 74.4(2) . . ?
Fe0D Ge3 Ge1 129.7(2) . 1_465 ?
Fe0D Ge3 Ge3 129.3(2) . 2_476 ?
Y001 Ge4 Y005 124.23(10) 2_566 . ?
Y002 Ge4 Y001 124.49(12) . 2_566 ?
Y002 Ge4 Y005 83.77(8) . . ?
Y002 Ge4 Y005 124.86(11) . 2_566 ?
Y005 Ge4 Y001 80.78(8) 2_566 2_566 ?
Y005 Ge4 Y005 124.59(10) 2_566 . ?
Ge4 Ge4 Y001 115.71(14) 2_566 2_566 ?
Ge4 Ge4 Y002 119.81(14) 2_566 . ?
Ge4 Ge4 Y005 62.45(10) 2_566 2_566 ?
Ge4 Ge4 Y005 62.14(10) 2_566 . ?
Ge4 Ge4 Ge7 87.92(13) 2_566 . ?
Ge5 Ge4 Y001 62.20(8) 1_455 2_566 ?
Ge5 Ge4 Y002 62.29(8) 1_455 . ?
Ge5 Ge4 Y005 119.36(9) 1_455 . ?
Ge5 Ge4 Y005 116.02(9) 1_455 2_566 ?
Ge5 Ge4 Ge4 177.81(15) 1_455 2_566 ?
Ge5 Ge4 Ge7 91.47(9) 1_455 . ?
Ge7 Ge4 Y001 115.90(10) 1_455 2_566 ?
Ge7 Ge4 Y001 61.88(7) . 2_566 ?
Ge7 Ge4 Y002 119.55(9) . . ?
Ge7 Ge4 Y002 62.60(8) 1_455 . ?
Ge7 Ge4 Y005 115.57(9) . 2_566 ?
Ge7 Ge4 Y005 119.86(9) 1_455 . ?
Ge7 Ge4 Y005 62.35(8) . . ?
Ge7 Ge4 Y005 62.26(8) 1_455 2_566 ?
Ge7 Ge4 Ge4 92.08(13) 1_455 2_566 ?
Ge7 Ge4 Ge5 88.42(9) 1_455 1_455 ?
Ge7 Ge4 Ge7 177.42(11) 1_455 . ?
Fe0D Ge4 Y001 152.6(2) . 2_566 ?
Fe0D Ge4 Y001 72.6(2) 2_566 2_566 ?
Fe0D Ge4 Y002 74.2(2) . . ?
Fe0D Ge4 Y002 154.6(2) 2_566 . ?
Fe0D Ge4 Y005 71.8(2) . 2_566 ?
Fe0D Ge4 Y005 73.6(2) . . ?
Fe0D Ge4 Y005 70.8(2) 2_566 . ?
Fe0D Ge4 Y005 72.9(2) 2_566 2_566 ?
Fe0D Ge4 Ge4 50.2(2) . 2_566 ?
Fe0D Ge4 Ge4 47.9(2) 2_566 2_566 ?
Fe0D Ge4 Ge5 131.3(3) . 1_455 ?
Fe0D Ge4 Ge5 130.5(2) 2_566 1_455 ?
Fe0D Ge4 Ge7 131.0(2) 2_566 1_455 ?
Fe0D Ge4 Ge7 47.7(2) 2_566 . ?
Fe0D Ge4 Ge7 50.9(2) . 1_455 ?
Fe0D Ge4 Ge7 130.4(2) . . ?
Fe0D Ge4 Fe0D 98.1(3) . 2_566 ?
Fe0D Ge4 Fe0E 134.3(3) 2_566 1_455 ?
Fe0D Ge4 Fe0E 99.2(3) . 1_455 ?
Fe0D Ge4 Fe0F 135.5(3) . . ?
Fe0E Ge4 Y001 72.7(2) 1_455 2_566 ?
Fe0E Ge4 Y002 71.1(2) 1_455 . ?
Fe0E Ge4 Y005 73.1(2) 1_455 2_566 ?
Fe0E Ge4 Y005 154.8(2) 1_455 . ?
Fe0E Ge4 Ge4 131.4(3) 1_455 2_566 ?
Fe0E Ge4 Ge5 47.9(2) 1_455 1_455 ?
Fe0E Ge4 Ge7 130.4(2) 1_455 . ?
Fe0E Ge4 Ge7 48.3(2) 1_455 1_455 ?
Fe0F Ge4 Y001 71.88(19) . 2_566 ?
Fe0F Ge4 Y002 73.4(2) . . ?
Fe0F Ge4 Y005 152.7(2) . 2_566 ?
Fe0F Ge4 Y005 73.4(2) . . ?
Fe0F Ge4 Ge4 130.2(3) . 2_566 ?
Fe0F Ge4 Ge5 50.4(2) . 1_455 ?
Fe0F Ge4 Ge7 130.8(2) . 1_455 ?
Fe0F Ge4 Ge7 50.5(2) . . ?
Fe0F Ge4 Fe0D 98.2(3) . 2_566 ?
Fe0F Ge4 Fe0E 98.3(3) . 1_455 ?
Y001 Ge5 Y002 124.53(12) 2_666 1_655 ?
Y001 Ge5 Y003 124.46(10) 2_666 2_765 ?
Y001 Ge5 Y003 83.86(8) 2_666 . ?
Y002 Ge5 Y003 80.76(8) 1_655 2_765 ?
Y002 Ge5 Y003 124.52(10) 1_655 . ?
Y003 Ge5 Y003 124.57(10) . 2_765 ?
Ge4 Ge5 Y001 62.32(8) 1_655 2_666 ?
Ge4 Ge5 Y002 62.21(8) 1_655 1_655 ?
Ge4 Ge5 Y003 115.95(9) 1_655 2_765 ?
Ge4 Ge5 Y003 119.47(9) 1_655 . ?
Ge4 Ge5 Ge6 88.46(9) 1_655 1_655 ?
Ge5 Ge5 Y001 119.57(14) 2_765 2_666 ?
Ge5 Ge5 Y002 115.89(14) 2_765 1_655 ?
Ge5 Ge5 Y003 62.30(10) 2_765 . ?
Ge5 Ge5 Y003 62.27(10) 2_765 2_765 ?
Ge5 Ge5 Ge4 177.84(14) 2_765 1_655 ?
Ge5 Ge5 Ge6 91.62(13) 2_765 1_655 ?
Ge6 Ge5 Y001 62.21(8) 1_655 2_666 ?
Ge6 Ge5 Y001 119.53(9) . 2_666 ?
Ge6 Ge5 Y002 62.27(7) . 1_655 ?
Ge6 Ge5 Y002 115.99(10) 1_655 1_655 ?
Ge6 Ge5 Y003 62.26(8) . . ?
Ge6 Ge5 Y003 119.48(9) 1_655 . ?
Ge6 Ge5 Y003 115.99(9) . 2_765 ?
Ge6 Ge5 Y003 62.25(8) 1_655 2_765 ?
Ge6 Ge5 Ge4 91.51(9) . 1_655 ?
Ge6 Ge5 Ge5 88.33(13) . 2_765 ?
Ge6 Ge5 Ge6 177.95(11) . 1_655 ?
Fe0E Ge5 Y001 73.7(2) . 2_666 ?
Fe0E Ge5 Y002 71.9(2) . 1_655 ?
Fe0E Ge5 Y003 152.7(2) . 2_765 ?
Fe0E Ge5 Y003 73.6(2) . . ?
Fe0E Ge5 Ge4 50.3(2) . 1_655 ?
Fe0E Ge5 Ge5 130.6(3) . 2_765 ?
Fe0E Ge5 Ge6 50.3(2) . . ?
Fe0E Ge5 Ge6 130.7(3) . 1_655 ?
Fe0E Ge5 Fe0F 98.6(3) . 1_655 ?
Fe0E Ge5 Fe0G 98.6(3) . 2_765 ?
Fe0F Ge5 Y001 71.2(2) 1_655 2_666 ?
Fe0F Ge5 Y002 72.56(18) 1_655 1_655 ?
Fe0F Ge5 Y003 155.1(2) 1_655 . ?
Fe0F Ge5 Y003 72.6(2) 1_655 2_765 ?
Fe0F Ge5 Ge4 48.2(2) 1_655 1_655 ?
Fe0F Ge5 Ge5 130.7(3) 1_655 2_765 ?
Fe0F Ge5 Ge6 130.7(2) 1_655 . ?
Fe0F Ge5 Ge6 48.27(19) 1_655 1_655 ?
Fe0G Ge5 Y001 154.4(2) 2_765 2_666 ?
Fe0G Ge5 Y001 73.9(2) . 2_666 ?
Fe0G Ge5 Y002 73.3(2) 2_765 1_655 ?
Fe0G Ge5 Y002 152.2(2) . 1_655 ?
Fe0G Ge5 Y003 74.0(2) . . ?
Fe0G Ge5 Y003 72.9(2) 2_765 2_765 ?
Fe0G Ge5 Y003 71.5(2) . 2_765 ?
Fe0G Ge5 Y003 70.5(2) 2_765 . ?
Fe0G Ge5 Ge4 130.8(3) . 1_655 ?
Fe0G Ge5 Ge4 131.2(2) 2_765 1_655 ?
Fe0G Ge5 Ge5 47.6(2) 2_765 2_765 ?
Fe0G Ge5 Ge5 50.3(2) . 2_765 ?
Fe0G Ge5 Ge6 130.9(3) . . ?
Fe0G Ge5 Ge6 130.7(2) 2_765 1_655 ?
Fe0G Ge5 Ge6 48.3(2) 2_765 . ?
Fe0G Ge5 Ge6 50.1(3) . 1_655 ?
Fe0G Ge5 Fe0E 135.9(3) . . ?
Fe0G Ge5 Fe0F 134.4(3) 2_765 1_655 ?
Fe0G Ge5 Fe0F 98.4(3) . 1_655 ?
Fe0G Ge5 Fe0G 97.9(3) . 2_765 ?
Y001 Ge6 Y003 124.00(11) 2_566 2_665 ?
Y002 Ge6 Y001 124.55(11) 1_655 2_566 ?
Y002 Ge6 Y003 83.68(8) 1_655 2_665 ?
Y003 Ge6 Y001 80.95(8) . 2_566 ?
Y003 Ge6 Y002 124.97(11) . 1_655 ?
Y003 Ge6 Y003 124.56(10) . 2_665 ?
Ge5 Ge6 Y001 116.26(9) . 2_566 ?
Ge5 Ge6 Y001 61.98(8) 1_455 2_566 ?
Ge5 Ge6 Y002 62.47(8) . 1_655 ?
Ge5 Ge6 Y002 119.26(9) 1_455 1_655 ?
Ge5 Ge6 Y003 62.50(7) . . ?
Ge5 Ge6 Y003 115.76(10) 1_455 . ?
Ge5 Ge6 Y003 119.73(9) . 2_665 ?
Ge5 Ge6 Y003 62.02(8) 1_455 2_665 ?
Ge5 Ge6 Ge5 177.95(11) . 1_455 ?
Ge5 Ge6 Ge6 92.24(13) . 2_665 ?
Ge5 Ge6 Ge7 88.46(9) . . ?
Ge6 Ge6 Y001 115.71(14) 2_665 2_566 ?
Ge6 Ge6 Y002 119.75(14) 2_665 1_655 ?
Ge6 Ge6 Y003 62.53(10) 2_665 . ?
Ge6 Ge6 Y003 62.03(10) 2_665 2_665 ?
Ge6 Ge6 Ge5 87.74(13) 2_665 1_455 ?
Ge6 Ge6 Ge7 177.67(14) 2_665 . ?
Ge7 Ge6 Y001 62.02(8) . 2_566 ?
Ge7 Ge6 Y002 62.53(8) . 1_655 ?
Ge7 Ge6 Y003 119.46(10) . 2_665 ?
Ge7 Ge6 Y003 115.96(10) . . ?
Ge7 Ge6 Ge5 91.49(9) . 1_455 ?
Fe0E Ge6 Y001 72.9(2) . 2_566 ?
Fe0E Ge6 Y002 71.2(2) . 1_655 ?
Fe0E Ge6 Y003 154.9(2) . 2_665 ?
Fe0E Ge6 Y003 72.9(2) . . ?
Fe0E Ge6 Ge5 48.2(2) . . ?
Fe0E Ge6 Ge5 130.7(2) . 1_455 ?
Fe0E Ge6 Ge6 131.4(3) . 2_665 ?
Fe0E Ge6 Ge7 48.1(2) . . ?
Fe0E Ge6 Fe0G 134.7(3) . 1_455 ?
Fe0F Ge6 Y001 71.7(2) . 2_566 ?
Fe0F Ge6 Y002 73.7(2) . 1_655 ?
Fe0F Ge6 Y003 152.6(2) . . ?
Fe0F Ge6 Y003 73.1(2) . 2_665 ?
Fe0F Ge6 Ge5 131.0(2) . . ?
Fe0F Ge6 Ge5 50.0(2) . 1_455 ?
Fe0F Ge6 Ge6 129.7(3) . 2_665 ?
Fe0F Ge6 Ge7 50.7(2) . . ?
Fe0F Ge6 Fe0E 98.9(3) . . ?
Fe0F Ge6 Fe0G 97.3(3) . 1_455 ?
Fe0G Ge6 Y001 72.6(2) 1_455 2_566 ?
Fe0G Ge6 Y001 152.4(2) 2_765 2_566 ?
Fe0G Ge6 Y002 154.0(2) 1_455 1_655 ?
Fe0G Ge6 Y002 74.3(2) 2_765 1_655 ?
Fe0G Ge6 Y003 70.3(2) 1_455 2_665 ?
Fe0G Ge6 Y003 74.0(2) 2_765 2_665 ?
Fe0G Ge6 Y003 71.4(2) 2_765 . ?
Fe0G Ge6 Y003 73.4(2) 1_455 . ?
Fe0G Ge6 Ge5 47.3(2) 1_455 1_455 ?
Fe0G Ge6 Ge5 50.5(2) 2_765 . ?
Fe0G Ge6 Ge5 130.5(3) 2_765 1_455 ?
Fe0G Ge6 Ge5 131.7(2) 1_455 . ?
Fe0G Ge6 Ge6 50.4(3) 2_765 2_665 ?
Fe0G Ge6 Ge6 48.0(2) 1_455 2_665 ?
Fe0G Ge6 Ge7 130.2(2) 1_455 . ?
Fe0G Ge6 Ge7 131.4(3) 2_765 . ?
Fe0G Ge6 Fe0E 98.7(3) 2_765 . ?
Fe0G Ge6 Fe0F 135.9(3) 2_765 . ?
Fe0G Ge6 Fe0G 98.4(3) 2_765 1_455 ?
Y001 Ge7 Y002 124.51(11) 2_566 1_655 ?
Y001 Ge7 Y005 124.31(10) 2_566 . ?
Y001 Ge7 Y005 84.08(8) 2_566 2_666 ?
Y002 Ge7 Y005 80.51(8) 1_655 . ?
Y005 Ge7 Y002 124.72(11) 2_666 1_655 ?
Y005 Ge7 Y005 124.56(10) 2_666 . ?
Ge4 Ge7 Y001 62.23(8) . 2_566 ?
Ge4 Ge7 Y001 119.98(10) 1_655 2_566 ?
Ge4 Ge7 Y002 115.59(9) . 1_655 ?
Ge4 Ge7 Y002 62.23(8) 1_655 1_655 ?
Ge4 Ge7 Y005 119.67(9) . 2_666 ?
Ge4 Ge7 Y005 62.48(7) 1_655 2_666 ?
Ge4 Ge7 Y005 115.68(10) 1_655 . ?
Ge4 Ge7 Y005 62.09(7) . . ?
Ge4 Ge7 Ge4 177.42(11) 1_655 . ?
Ge4 Ge7 Ge6 91.51(9) 1_655 . ?
Ge4 Ge7 Ge7 88.44(13) 1_655 2_666 ?
Ge6 Ge7 Y001 62.48(8) . 2_566 ?
Ge6 Ge7 Y002 62.03(8) . 1_655 ?
Ge6 Ge7 Y005 115.74(10) . . ?
Ge6 Ge7 Y005 119.68(10) . 2_666 ?
Ge6 Ge7 Ge4 88.48(9) . . ?
Ge6 Ge7 Ge7 177.23(14) . 2_666 ?
Ge7 Ge7 Y001 119.85(14) 2_666 2_566 ?
Ge7 Ge7 Y002 115.60(14) 2_666 1_655 ?
Ge7 Ge7 Y005 62.68(10) 2_666 2_666 ?
Ge7 Ge7 Y005 61.88(10) 2_666 . ?
Ge7 Ge7 Ge4 91.44(13) 2_666 . ?
Fe0D Ge7 Y001 155.0(2) 1_655 2_566 ?
Fe0D Ge7 Y001 73.7(2) 2_566 2_566 ?
Fe0D Ge7 Y002 72.9(2) 1_655 1_655 ?
Fe0D Ge7 Y002 151.9(2) 2_566 1_655 ?
Fe0D Ge7 Y005 71.0(2) 1_655 2_666 ?
Fe0D Ge7 Y005 74.2(2) 2_566 2_666 ?
Fe0D Ge7 Y005 72.7(2) 1_655 . ?
Fe0D Ge7 Y005 71.4(2) 2_566 . ?
Fe0D Ge7 Ge4 49.9(2) 2_566 . ?
Fe0D Ge7 Ge4 130.6(2) 1_655 . ?
Fe0D Ge7 Ge4 131.3(2) 2_566 1_655 ?
Fe0D Ge7 Ge4 48.1(2) 1_655 1_655 ?
Fe0D Ge7 Ge6 130.7(2) 2_566 . ?
Fe0D Ge7 Ge6 130.7(2) 1_655 . ?
Fe0D Ge7 Ge7 47.9(2) 1_655 2_666 ?
Fe0D Ge7 Ge7 50.6(2) 2_566 2_666 ?
Fe0D Ge7 Fe0D 98.5(3) 2_566 1_655 ?
Fe0D Ge7 Fe0E 136.4(3) 2_566 . ?
Fe0D Ge7 Fe0F 133.8(2) 1_655 . ?
Fe0D Ge7 Fe0F 97.8(3) 2_566 . ?
Fe0E Ge7 Y001 74.0(2) . 2_566 ?
Fe0E Ge7 Y002 71.7(2) . 1_655 ?
Fe0E Ge7 Y005 74.1(2) . 2_666 ?
Fe0E Ge7 Y005 152.2(2) . . ?
Fe0E Ge7 Ge4 50.5(2) . 1_655 ?
Fe0E Ge7 Ge4 130.8(3) . . ?
Fe0E Ge7 Ge6 50.1(2) . . ?
Fe0E Ge7 Ge7 131.3(3) . 2_666 ?
Fe0E Ge7 Fe0D 98.6(3) . 1_655 ?
Fe0E Ge7 Fe0F 98.6(3) . . ?
Fe0F Ge7 Y001 71.16(19) . 2_566 ?
Fe0F Ge7 Y002 72.5(2) . 1_655 ?
Fe0F Ge7 Y005 72.23(19) . . ?
Fe0F Ge7 Y005 155.2(2) . 2_666 ?
Fe0F Ge7 Ge4 47.9(2) . . ?
Fe0F Ge7 Ge4 130.8(2) . 1_655 ?
Fe0F Ge7 Ge6 48.5(2) . . ?
Fe0F Ge7 Ge7 130.0(2) . 2_666 ?
Y001 Fe0D Y002 125.3(2) . . ?
Y001 Fe0D Y005 76.57(18) . . ?
Y001 Fe0D Y005 79.19(18) . 1_455 ?
Y005 Fe0D Y001 117.6(3) 2_566 . ?
Y005 Fe0D Y002 76.20(18) 1_455 . ?
Y005 Fe0D Y002 79.12(17) . . ?
Y005 Fe0D Y002 117.1(3) 2_566 . ?
Y005 Fe0D Y005 117.6(2) 2_566 . ?
Y005 Fe0D Y005 117.3(2) 2_566 1_455 ?
Y005 Fe0D Y005 125.1(2) . 1_455 ?
Ge3 Fe0D Y001 62.8(2) . . ?
Ge3 Fe0D Y002 62.50(19) . . ?
Ge3 Fe0D Y005 62.46(18) . 1_455 ?
Ge3 Fe0D Y005 179.5(4) . 2_566 ?
Ge3 Fe0D Y005 62.64(18) . . ?
Ge4 Fe0D Y001 66.0(2) 2_566 . ?
Ge4 Fe0D Y001 138.8(3) . . ?
Ge4 Fe0D Y002 66.1(2) . . ?
Ge4 Fe0D Y002 139.9(3) 2_566 . ?
Ge4 Fe0D Y005 140.3(3) 2_566 1_455 ?
Ge4 Fe0D Y005 67.9(2) . 2_566 ?
Ge4 Fe0D Y005 137.7(4) . 1_455 ?
Ge4 Fe0D Y005 66.7(2) . . ?
Ge4 Fe0D Y005 67.45(19) 2_566 2_566 ?
Ge4 Fe0D Y005 65.9(2) 2_566 . ?
Ge4 Fe0D Ge3 113.0(4) 2_566 . ?
Ge4 Fe0D Ge3 112.0(3) . . ?
Ge4 Fe0D Ge4 81.9(3) . 2_566 ?
Ge4 Fe0D Ge7 136.2(3) . 2_566 ?
Ge4 Fe0D Ge7 81.0(3) . 1_455 ?
Ge4 Fe0D Ge7 134.4(3) 2_566 1_455 ?
Ge7 Fe0D Y001 140.0(3) 1_455 . ?
Ge7 Fe0D Y001 66.3(2) 2_566 . ?
Ge7 Fe0D Y002 137.7(3) 2_566 . ?
Ge7 Fe0D Y002 65.7(2) 1_455 . ?
Ge7 Fe0D Y005 68.32(19) 2_566 2_566 ?
Ge7 Fe0D Y005 138.6(4) 2_566 . ?
Ge7 Fe0D Y005 65.9(2) 1_455 1_455 ?
Ge7 Fe0D Y005 139.7(3) 1_455 . ?
Ge7 Fe0D Y005 66.0(2) 2_566 1_455 ?
Ge7 Fe0D Y005 66.91(19) 1_455 2_566 ?
Ge7 Fe0D Ge3 112.6(3) 1_455 . ?
Ge7 Fe0D Ge3 111.8(3) 2_566 . ?
Ge7 Fe0D Ge4 82.3(3) 2_566 2_566 ?
Ge7 Fe0D Ge7 81.5(3) 2_566 1_455 ?
Y001 Fe0E Y001 125.6(2) 2_666 2_566 ?
Y001 Fe0E Y003 79.42(19) 2_666 . ?
Y001 Fe0E Y005 76.43(19) 2_666 2_666 ?
Y001 Fe0E Y005 79.11(19) 2_566 2_666 ?
Y002 Fe0E Y001 117.3(3) 1_655 2_666 ?
Y002 Fe0E Y001 117.1(2) 1_655 2_566 ?
Y002 Fe0E Y003 117.4(3) 1_655 . ?
Y002 Fe0E Y005 117.2(3) 1_655 2_666 ?
Y003 Fe0E Y001 76.61(19) . 2_566 ?
Y003 Fe0E Y005 125.4(2) . 2_666 ?
Ge1 Fe0E Y001 62.7(2) . 2_566 ?
Ge1 Fe0E Y001 62.93(19) . 2_666 ?
Ge1 Fe0E Y002 179.6(4) . 1_655 ?
Ge1 Fe0E Y003 62.9(2) . . ?
Ge1 Fe0E Y005 62.5(2) . 2_666 ?
Ge4 Fe0E Y001 66.0(2) 1_655 2_666 ?
Ge4 Fe0E Y001 139.5(4) 1_655 2_566 ?
Ge4 Fe0E Y002 67.1(2) 1_655 1_655 ?
Ge4 Fe0E Y003 140.4(3) 1_655 . ?
Ge4 Fe0E Y005 65.7(2) 1_655 2_666 ?
Ge4 Fe0E Ge1 112.9(4) 1_655 . ?
Ge5 Fe0E Y001 138.5(4) . 2_566 ?
Ge5 Fe0E Y001 66.5(2) . 2_666 ?
Ge5 Fe0E Y002 67.8(2) . 1_655 ?
Ge5 Fe0E Y003 66.6(2) . . ?
Ge5 Fe0E Y005 138.3(4) . 2_666 ?
Ge5 Fe0E Ge1 112.5(4) . . ?
Ge5 Fe0E Ge4 81.8(3) . 1_655 ?
Ge5 Fe0E Ge6 81.5(3) . . ?
Ge5 Fe0E Ge7 135.8(4) . . ?
Ge6 Fe0E Y001 140.1(4) . 2_666 ?
Ge6 Fe0E Y001 66.0(2) . 2_566 ?
Ge6 Fe0E Y002 67.1(2) . 1_655 ?
Ge6 Fe0E Y003 65.8(2) . . ?
Ge6 Fe0E Y005 140.0(3) . 2_666 ?
Ge6 Fe0E Ge1 113.0(4) . . ?
Ge6 Fe0E Ge4 134.1(4) . 1_655 ?
Ge7 Fe0E Y001 137.9(4) . 2_666 ?
Ge7 Fe0E Y001 66.1(2) . 2_566 ?
Ge7 Fe0E Y002 68.0(2) . 1_655 ?
Ge7 Fe0E Y003 138.3(4) . . ?
Ge7 Fe0E Y005 66.1(2) . 2_666 ?
Ge7 Fe0E Ge1 111.6(4) . . ?
Ge7 Fe0E Ge4 81.2(3) . 1_655 ?
Ge7 Fe0E Ge6 81.8(3) . . ?
Y001 Fe0F Y002 117.0(2) 2_566 1_655 ?
Y001 Fe0F Y002 117.2(2) 2_566 . ?
Y001 Fe0F Y003 117.2(2) 2_566 2_665 ?
Y001 Fe0F Y005 117.2(3) 2_566 . ?
Y002 Fe0F Y002 125.8(2) . 1_655 ?
Y002 Fe0F Y003 76.68(18) . 2_665 ?
Y002 Fe0F Y005 79.47(16) . . ?
Y003 Fe0F Y002 79.24(18) 2_665 1_655 ?
Y003 Fe0F Y005 125.6(2) 2_665 . ?
Y005 Fe0F Y002 76.55(18) . 1_655 ?
Ge2 Fe0F Y001 179.9(4) . 2_566 ?
Ge2 Fe0F Y002 62.91(18) . 1_655 ?
Ge2 Fe0F Y002 62.88(16) . . ?
Ge2 Fe0F Y003 62.9(2) . 2_665 ?
Ge2 Fe0F Y005 62.77(18) . . ?
Ge4 Fe0F Y001 67.64(19) . 2_566 ?
Ge4 Fe0F Y002 66.47(19) . . ?
Ge4 Fe0F Y002 138.4(4) . 1_655 ?
Ge4 Fe0F Y003 138.4(3) . 2_665 ?
Ge4 Fe0F Y005 66.6(2) . . ?
Ge4 Fe0F Ge2 112.4(3) . . ?
Ge4 Fe0F Ge5 81.4(3) . 1_455 ?
Ge4 Fe0F Ge6 135.3(3) . . ?
Ge4 Fe0F Ge7 81.6(3) . . ?
Ge5 Fe0F Y001 66.93(19) 1_455 2_566 ?
Ge5 Fe0F Y002 65.98(19) 1_455 . ?
Ge5 Fe0F Y002 139.9(3) 1_455 1_655 ?
Ge5 Fe0F Y003 66.0(2) 1_455 2_665 ?
Ge5 Fe0F Y005 140.2(3) 1_455 . ?
Ge5 Fe0F Ge2 113.2(3) 1_455 . ?
Ge5 Fe0F Ge7 133.6(3) 1_455 . ?
Ge6 Fe0F Y001 67.62(18) . 2_566 ?
Ge6 Fe0F Y002 66.0(2) . 1_655 ?
Ge6 Fe0F Y002 138.7(4) . . ?
Ge6 Fe0F Y003 66.6(2) . 2_665 ?
Ge6 Fe0F Y005 137.8(3) . . ?
Ge6 Fe0F Ge2 112.3(3) . . ?
Ge6 Fe0F Ge5 81.7(3) . 1_455 ?
Ge6 Fe0F Ge7 80.7(2) . . ?
Ge7 Fe0F Y001 66.62(18) . 2_566 ?
Ge7 Fe0F Y002 140.3(3) . . ?
Ge7 Fe0F Y002 65.84(19) . 1_655 ?
Ge7 Fe0F Y003 139.7(3) . 2_665 ?
Ge7 Fe0F Y005 66.2(2) . . ?
Ge7 Fe0F Ge2 113.2(3) . . ?
Y001 Fe0G Y002 124.9(2) 2_666 2_665 ?
Y001 Fe0G Y003 76.39(19) 2_666 1_655 ?
Y001 Fe0G Y003 79.27(18) 2_666 . ?
Y002 Fe0G Y003 78.69(19) 2_665 1_655 ?
Y003 Fe0G Y001 117.8(3) 2_765 2_666 ?
Y003 Fe0G Y002 117.3(2) 2_765 2_665 ?
Y003 Fe0G Y002 76.2(2) . 2_665 ?
Y003 Fe0G Y003 117.4(3) 2_765 1_655 ?
Y003 Fe0G Y003 117.8(3) 2_765 . ?
Y003 Fe0G Y003 124.8(2) . 1_655 ?
Ge00 Fe0G Y001 62.71(19) . 2_666 ?
Ge00 Fe0G Y002 62.2(2) . 2_665 ?
Ge00 Fe0G Y003 179.4(4) . 2_765 ?
Ge00 Fe0G Y003 62.5(2) . . ?
Ge00 Fe0G Y003 62.33(19) . 1_655 ?
Ge5 Fe0G Y001 66.6(2) . 2_666 ?
Ge5 Fe0G Y001 140.3(3) 2_765 2_666 ?
Ge5 Fe0G Y002 138.2(4) . 2_665 ?
Ge5 Fe0G Y002 65.5(2) 2_765 2_665 ?
Ge5 Fe0G Y003 66.5(2) . . ?
Ge5 Fe0G Y003 67.6(2) 2_765 2_765 ?
Ge5 Fe0G Y003 139.3(3) 2_765 1_655 ?
Ge5 Fe0G Y003 138.5(4) . 1_655 ?
Ge5 Fe0G Y003 68.4(2) . 2_765 ?
Ge5 Fe0G Y003 65.8(2) 2_765 . ?
Ge5 Fe0G Ge00 112.3(4) 2_765 . ?
Ge5 Fe0G Ge00 112.2(3) . . ?
Ge5 Fe0G Ge5 82.1(3) . 2_765 ?
Ge5 Fe0G Ge6 136.4(4) . 2_765 ?
Ge5 Fe0G Ge6 82.6(3) . 1_655 ?
Ge5 Fe0G Ge6 135.3(4) 2_765 1_655 ?
Ge6 Fe0G Y001 66.0(2) 1_655 2_666 ?
Ge6 Fe0G Y001 138.3(4) 2_765 2_666 ?
Ge6 Fe0G Y002 65.9(2) 2_765 2_665 ?
Ge6 Fe0G Y002 139.1(3) 1_655 2_665 ?
Ge6 Fe0G Y003 137.6(4) 2_765 . ?
Ge6 Fe0G Y003 65.3(2) 1_655 1_655 ?
Ge6 Fe0G Y003 66.3(2) 2_765 1_655 ?
Ge6 Fe0G Y003 68.0(2) 2_765 2_765 ?
Ge6 Fe0G Y003 67.7(2) 1_655 2_765 ?
Ge6 Fe0G Y003 140.7(3) 1_655 . ?
Ge6 Fe0G Ge00 112.4(4) 1_655 . ?
Ge6 Fe0G Ge00 111.4(4) 2_765 . ?
Ge6 Fe0G Ge5 81.3(3) 2_765 2_765 ?
Ge6 Fe0G Ge6 81.6(3) 2_765 1_655 ?


_olex2_submission_special_instructions 'No special instructions were received'
