File Name : ghb-edc am figure s1.pdf Caption : figure s1. typical full scan mass spectra of ghb-edca / ghb-edcb (a) and d6-ghb-edca / d6-ghb-edcb (b) derivatives, and accurate mass measurements data of the four mh+ ions. File Name : ghb-edc am figure s2.pdf Caption : figure s2. derivatization yields of the ghb-edc derivatives at different temperature and time reaction conditions. File Name : ghb-edc am figure s3.pdf Caption : figure s3. stability of ghb-edc derivatives kept at different temperatures and times before instrumental injection. File Name : ghb-edc am figure s4.pdf Caption : figure s4. mh+ collision-induced product ion spectra (merging of collision energies at 10, 25, 50 ev) of ghb-edc, bhb-edc, and bhisob-edc for both type a and type b derivatives.