# Supplementary Information (SI) for ChemComm.
# This journal is © The Royal Society of Chemistry 2025

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
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data_mal20241025a
_database_code_depnum_ccdc_archive 'CCDC 2413801'
loop_
_audit_author_name
_audit_author_address
'Along Ma'
;qingdao university of science and technology
China
;
_audit_update_record             
;
2024-12-31 deposited with the CCDC.	2025-06-11 downloaded from the CCDC.
;
_audit_creation_date             2024-12-25
_audit_creation_method           
;
Olex2 1.5
(compiled 2024.02.16 svn.r378c4104 for OlexSys, GUI svn.r6928)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         
'C156 H84 Ag10 Cu4 F60 O12 P4 S12, 1[CH2Cl2], 3[CH3OH]'
_chemical_formula_sum            'C160 H98 Ag10 Cl2 Cu4 F60 O15 P4 S12'
_chemical_formula_weight         5312.74
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   18.7192(11)
_cell_length_b                   19.3113(13)
_cell_length_c                   25.7905(17)
_cell_angle_alpha                89.531(2)
_cell_angle_beta                 89.166(2)
_cell_angle_gamma                85.539(2)
_cell_volume                     9293.6(10)
_cell_formula_units_Z            2
_cell_measurement_reflns_used    9465
_cell_measurement_temperature    170
_cell_measurement_theta_max      27.205
_cell_measurement_theta_min      2.368
_shelx_estimated_absorpt_T_max   0.932
_shelx_estimated_absorpt_T_min   0.814
_exptl_absorpt_coefficient_mu    1.790
_exptl_absorpt_correction_T_max  0.1137
_exptl_absorpt_correction_T_min  0.0825
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   ?
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            yellow
_exptl_crystal_colour_primary    yellow
_exptl_crystal_density_diffrn    1.899
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             5180
_exptl_crystal_size_max          0.12
_exptl_crystal_size_mid          0.08
_exptl_crystal_size_min          0.04
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0454
_diffrn_reflns_av_unetI/netI     0.0315
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.999
_diffrn_reflns_limit_h_max       22
_diffrn_reflns_limit_h_min       -22
_diffrn_reflns_limit_k_max       22
_diffrn_reflns_limit_k_min       -22
_diffrn_reflns_limit_l_max       30
_diffrn_reflns_limit_l_min       -30
_diffrn_reflns_number            193338
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.999
_diffrn_reflns_theta_full        25.000
_diffrn_reflns_theta_max         25.000
_diffrn_reflns_theta_min         1.907
_diffrn_ambient_temperature      170.0
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       ?
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                24274
_reflns_number_total             32726
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT V8.40B (?, 2016)'
_computing_data_collection       ?
_computing_data_reduction        'SAINT V8.40B (?, 2016)'
_computing_molecular_graphics    'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2018/3 (Sheldrick, 2015)'
_computing_structure_solution    'SHELXT 2018/2 (Sheldrick, 2018)'
_refine_diff_density_max         1.184
_refine_diff_density_min         -0.771
_refine_diff_density_rms         0.082
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.112
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     2247
_refine_ls_number_reflns         32726
_refine_ls_number_restraints     4766
_refine_ls_R_factor_all          0.0568
_refine_ls_R_factor_gt           0.0389
_refine_ls_restrained_S_all      1.055
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0676P)²] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1110
_refine_ls_wR_factor_ref         0.1189
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups
 At 1.5 times of:
  All C(H,H,H) groups
2. Restrained distances
 O11-C73 = O13-C163
 1.45 with sigma of 0.001
 O7-C11 = O2-C153
 1.45 with sigma of 0.001
 C165-C163
 2.5 with sigma of 0.01
 O3-C159
 1.4 with sigma of 0.02
 C81-O3
 1.45 with sigma of 0.001
 O13-C165 = O11-C127
 1.4 with sigma of 0.001
3. Rigid bond restraints
 Ag11, S8
 with sigma for 1-2 distances of 0.0005 and sigma for 1-3 distances of 0.0005
 Cu4, S12
 with sigma for 1-2 distances of 0.001 and sigma for 1-3 distances of 0.001
 Ag3, S6
 with sigma for 1-2 distances of 0.001 and sigma for 1-3 distances of 0.001
 Cu4, S9
 with sigma for 1-2 distances of 0.001 and sigma for 1-3 distances of 0.001
 Ag3, S10
 with sigma for 1-2 distances of 0.0005 and sigma for 1-3 distances of 0.0005
 Cu3, S8
 with sigma for 1-2 distances of 0.0005 and sigma for 1-3 distances of 0.0005
 Cu2, S10
 with sigma for 1-2 distances of 0.001 and sigma for 1-3 distances of 0.001
4. Uiso/Uaniso restraints and constraints
All non-hydrogen atoms have similar U: within 2A with sigma of 0.04 and sigma
for terminal atoms of 0.08 within 2A
C167 \\sim C21 \\sim C169 \\sim C41 \\sim C165 \\sim C83 \\sim O13 \\sim C163:
within 2A with sigma of 0.001 and sigma for terminal atoms of 0.002 within 2A
C151 \\sim C19 \\sim C147 \\sim C37 \\sim C149 \\sim C75: within 2A with sigma
of 0.001 and sigma for terminal atoms of 0.002 within 2A
C81 \\sim O3 \\sim C159 \\sim C79 \\sim C157 \\sim C39 \\sim C161 \\sim C5:
within 2A with sigma of 0.001 and sigma for terminal atoms of 0.002 within 2A
C77 \\sim O5 \\sim C151 \\sim C75 \\sim C149 \\sim C37 \\sim C147 \\sim C19:
within 2A with sigma of 0.001 and sigma for terminal atoms of 0.002 within 2A
O11 \\sim C73 \\sim C127 \\sim C63 \\sim C125 \\sim C31 \\sim C129 \\sim C2:
within 2A with sigma of 0.001 and sigma for terminal atoms of 0.002 within 2A
5. Rigid body (RIGU) restrains
 All non-hydrogen atoms
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 C147, C19, C37, C151, C149, C75
 with sigma for 1-2 distances of 0.001 and sigma for 1-3 distances of 0.001
6. Others
 Sof(Ag9)=Sof(O2)=Sof(C31)=Sof(H31)=Sof(C125)=Sof(H125)=Sof(C63)=Sof(H63)=
 Sof(C127)=Sof(C2)=Sof(H2)=Sof(C129)=Sof(O5)=Sof(C131)=Sof(H131)=Sof(C33)=
 Sof(C133)=Sof(H133)=Sof(C67)=Sof(C135)=Sof(H135)=Sof(C17)=Sof(H17)=Sof(O11)=
 Sof(C73)=Sof(H73A)=Sof(H73B)=Sof(H73C)=Sof(C147)=Sof(C37)=Sof(H37)=Sof(C149)=
 Sof(H149)=Sof(C75)=Sof(H75)=Sof(C151)=Sof(C19)=Sof(H19)=Sof(C153)=Sof(H15A)=
 Sof(H15B)=Sof(H15C)=Sof(C77)=Sof(H77A)=Sof(H77B)=Sof(H77C)=Sof(P2)=1-FVAR(1)
 Sof(P3)=Sof(C39)=Sof(H39)=Sof(C157)=Sof(H157)=Sof(C79)=Sof(H79)=Sof(C159)=
 Sof(C5)=Sof(H5)=Sof(C161)=Sof(O3)=Sof(C81)=Sof(H81A)=Sof(H81B)=Sof(H81C)=
 Sof(O13)=Sof(C163)=Sof(H16A)=Sof(H16B)=Sof(H16C)=Sof(C41)=Sof(H41)=Sof(C165)=
 Sof(C83)=Sof(H83)=Sof(C167)=Sof(C21)=Sof(H21)=Sof(C169)=Sof(H169)=Sof(O7)=
 Sof(C85)=Sof(C171)=Sof(H171)=Sof(C43)=Sof(C173)=Sof(H173)=Sof(C87)=Sof(H87)=
 Sof(C175)=Sof(H175)=Sof(C11)=Sof(H11A)=Sof(H11B)=Sof(H11C)=Sof(Ag5)=FVAR(1)
7.a Riding coordinates:
 C153(H15A,H15B,H15C), C163(H16A,H16B,H16C)
7.b Aromatic/amide H refined with riding coordinates:
 C40(H40), C44(H44), C46(H46), C48(H48), C52(H52), C56(H56), C58(H58),
 C60(H60), C64(H64), C66(H66), C68(H68), C72(H72), C74(H74), C78(H78), C80(H80),
  C82(H82), C88(H88), C92(H92), C94(H94), C96(H96), C100(H100), C104(H104),
 C106(H106), C108(H108), C112(H112), C116(H116), C118(H118), C120(H120),
 C124(H124), C128(H128), C130(H130), C132(H132), C136(H136), C140(H140),
 C142(H142), C144(H144), C31(H31), C125(H125), C63(H63), C2(H2), C131(H131),
 C133(H133), C135(H135), C17(H17), C37(H37), C149(H149), C75(H75), C19(H19),
 C39(H39), C157(H157), C79(H79), C5(H5), C41(H41), C83(H83), C21(H21),
 C169(H169), C171(H171), C173(H173), C87(H87), C175(H175)
7.c Fitted hexagon refined as free rotating group:
 C1(C4,C6,C8,C10,C12), C14(C16,C18,C20,C22,C24), C26(C28,C30,C32,C34,C36),
 C38(C40,C42,C44,C46,C48), C50(C52,C54,C56,C58,C60), C62(C64,C66,C68,C70,C72),
 C74(C76,C78,C80,C82,C84), C86(C88,C90,C92,C94,C96), C98(C100,C102,C104,C106,
 C108), C110(C112,C114,C116,C118,C120), C122(C124,C126,C128,C130,C132),
 C134(C136,C138,C140,C142,C144), C146(C148,C150,C152,C154,C156), C158(C160,C162,
 C164,C166,C168), C170(C172,C174,C176,C177,C89), C45(C91,C23,C93,C47,C95),
 C3(C97,C49,C99,C25,C101), C51(C103,C13,C105,C53,C107), C27(C109,C55,C111,C7,
 C113), C115(C29,C117,C59,C119,C15), C31(C125,C63,C127,C2,C129), C131(C33,C133,
 C67,C135,C17), C139(C35,C141,C71,C143,C9), C147(C37,C149,C75,C151,C19),
 C39(C157,C79,C159,C5,C161), C41(C165,C83,C167,C21,C169), C85(C171,C43,C173,C87,
 C175)
7.d Idealised Me refined as rotating group:
 C57(H57A,H57B,H57C), C121(H12A,H12B,H12C), C61(H61A,H61B,H61C), C123(H12D,
 H12E,H12F), C65(H65A,H65B,H65C), C137(H13A,H13B,H13C), C69(H69A,H69B,H69C),
 C145(H14A,H14B,H14C), C73(H73A,H73B,H73C), C77(H77A,H77B,H77C), C155(H15D,H15E,
 H15F), C81(H81A,H81B,H81C), C11(H11A,H11B,H11C)
;
_atom_sites_solution_hydrogens   mixed
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.82283(2) 0.28081(2) 0.29058(2) 0.04720(9) Uani 1 1 d . . . . .
Ag4 Ag 0.67053(2) 0.28861(2) 0.31370(2) 0.04636(8) Uani 1 1 d . . . . .
Ag6 Ag 0.72631(2) 0.36384(2) 0.22786(2) 0.04772(9) Uani 1 1 d . . . . .
Ag8 Ag 0.64346(2) 0.24696(2) 0.21108(2) 0.05429(9) Uani 1 1 d . . . . .
Ag10 Ag 0.79426(2) 0.23790(2) 0.18727(2) 0.05746(10) Uani 1 1 d . . . . .
Ag11 Ag 0.77965(2) 0.19355(2) 0.40864(2) 0.05622(10) Uani 1 1 d . U . . .
Ag3 Ag 0.54348(2) 0.39485(2) 0.25596(2) 0.05672(10) Uani 1 1 d . U . . .
Ag7 Ag 0.74301(2) 0.16262(2) 0.27408(2) 0.05550(9) Uani 1 1 d . . . . .
Ag2 Ag 0.90741(2) 0.37383(2) 0.19548(2) 0.06265(11) Uani 1 1 d . . . . .
Ag9 Ag 0.71133(15) 0.0890(2) 0.15497(16) 0.1034(11) Uani 0.642(5) 1 d . U P A 2
Cu1 Cu 0.75502(2) 0.40778(3) 0.33225(2) 0.04385(12) Uani 1 1 d . . . . .
Cu4 Cu 0.59225(3) 0.16790(3) 0.30106(2) 0.05479(14) Uani 1 1 d . U . . .
Cu2 Cu 0.69669(3) 0.32588(3) 0.12405(2) 0.05920(15) Uani 1 1 d . U . . .
Cu3 Cu 0.89505(3) 0.15387(3) 0.25217(2) 0.05909(15) Uani 1 1 d . U . . .
S1 S 0.86474(5) 0.40419(6) 0.29121(4) 0.0495(3) Uani 1 1 d . U . . .
S4 S 0.73592(5) 0.32434(6) 0.39376(4) 0.0476(2) Uani 1 1 d . U . . .
S6 S 0.65827(5) 0.45309(6) 0.28596(4) 0.0484(2) Uani 1 1 d . U . . .
S8 S 0.88860(6) 0.17993(6) 0.33921(5) 0.0560(3) Uani 1 1 d . U . . .
S10 S 0.58484(5) 0.35048(7) 0.16032(4) 0.0587(3) Uani 1 1 d . U . . .
S12 S 0.53503(6) 0.27740(6) 0.31062(4) 0.0559(3) Uani 1 1 d . U . . .
S3 S 0.78727(6) 0.39633(7) 0.14250(4) 0.0607(3) Uani 1 1 d . U . . .
P1 P 0.42893(6) 0.46421(7) 0.25695(4) 0.0541(3) Uani 1 1 d . U . . .
P4 P 0.80753(6) 0.15822(6) 0.49717(5) 0.0528(3) Uani 1 1 d . U . . .
S7 S 0.68009(6) 0.12995(6) 0.35902(5) 0.0604(3) Uani 1 1 d . U . . .
S2 S 0.93025(6) 0.23687(7) 0.19394(5) 0.0669(3) Uani 1 1 d . U . . .
P5 P 1.01315(6) 0.43277(8) 0.16946(4) 0.0622(3) Uani 1 1 d . U . . .
S9 S 0.59895(6) 0.12515(7) 0.21726(5) 0.0676(3) Uani 1 1 d . U . . .
S5 S 0.73132(7) 0.21270(8) 0.10318(5) 0.0729(4) Uani 1 1 d . U . . .
S11 S 0.82095(7) 0.07548(7) 0.21870(6) 0.0745(4) Uani 1 1 d . U . . .
P3 P 0.6940(9) 0.0071(7) 0.0847(6) 0.077(3) Uani 0.358(5) 1 d . U P A 1
F1 F 1.12599(12) 0.34375(14) 0.33877(10) 0.0636(7) Uani 1 1 d . U . . .
F4 F 1.01086(12) 0.32650(13) 0.28267(9) 0.0566(6) Uani 1 1 d . U . . .
F6 F 0.72315(13) 0.47015(13) 0.43185(10) 0.0609(6) Uani 1 1 d . U . . .
F8 F 0.53784(13) 0.40653(14) 0.37647(10) 0.0666(7) Uani 1 1 d . U . . .
F10 F 0.87261(13) 0.48414(15) 0.38978(9) 0.0658(7) Uani 1 1 d . U . . .
F12 F 0.44844(13) 0.29036(15) 0.19592(10) 0.0681(7) Uani 1 1 d . U . . .
F14 F 0.63448(13) 0.25035(14) 0.46407(10) 0.0664(7) Uani 1 1 d . U . . .
F16 F 0.91402(14) 0.27903(13) 0.42598(10) 0.0677(7) Uani 1 1 d . U . . .
F18 F 1.03782(14) 0.12879(15) 0.30491(11) 0.0751(8) Uani 1 1 d . U . . .
F20 F 0.83490(15) 0.52316(16) 0.19724(10) 0.0768(8) Uani 1 1 d . U . . .
F22 F 1.11586(14) 0.42855(16) 0.42308(10) 0.0776(8) Uani 1 1 d . U . . .
F24 F 0.98826(15) 0.49786(17) 0.44761(10) 0.0831(9) Uani 1 1 d . U . . .
F26 F 0.33775(14) 0.26027(17) 0.13834(12) 0.0829(9) Uani 1 1 d . U . . .
F28 F 0.80741(15) 0.03139(15) 0.38686(15) 0.0921(10) Uani 1 1 d . U . . .
F30 F 0.57543(16) 0.34859(19) 0.04410(10) 0.0885(10) Uani 1 1 d . U . . .
F32 F 0.73603(18) 0.56600(15) 0.33317(13) 0.0915(10) Uani 1 1 d . U . . .
F34 F 1.03784(17) 0.29681(16) 0.47244(12) 0.0890(9) Uani 1 1 d . U . . .
F36 F 0.59467(17) 0.51962(16) 0.18934(11) 0.0834(9) Uani 1 1 d . U . . .
F38 F 0.65824(15) 0.51878(16) 0.51843(12) 0.0843(9) Uani 1 1 d . U . . .
F40 F 0.57069(15) 0.30036(19) 0.55144(11) 0.0909(10) Uani 1 1 d . U . . .
O1 O 0.81638(18) 0.41005(17) 0.56212(14) 0.0716(9) Uani 1 1 d . U . . .
F42 F 0.55808(16) 0.03759(16) 0.35798(15) 0.0964(11) Uani 1 1 d . U . . .
F44 F 0.69118(17) 0.45586(19) 0.05925(12) 0.0918(10) Uani 1 1 d . U . . .
F46 F 0.47910(17) 0.4292(2) 0.47023(12) 0.0964(10) Uani 1 1 d . U . . .
F48 F 0.55819(18) 0.14901(19) 0.10496(12) 0.0966(10) Uani 1 1 d . U . . .
F50 F 0.58236(17) 0.43543(19) 0.57948(11) 0.0963(10) Uani 1 1 d . U . . .
F52 F 0.46090(17) 0.17845(17) 0.37914(14) 0.0937(10) Uani 1 1 d . U . . .
F54 F 0.93579(17) 0.3014(2) 0.08641(11) 0.0921(10) Uani 1 1 d . U . . .
F56 F 1.16097(14) 0.14964(19) 0.35104(13) 0.0958(10) Uani 1 1 d . U . . .
F58 F 1.16264(15) 0.23150(19) 0.43612(13) 0.1008(11) Uani 1 1 d . U . . .
F60 F 0.46051(17) 0.09358(19) 0.26851(14) 0.1008(11) Uani 1 1 d . U . . .
F15 F 0.34481(16) 0.27097(19) 0.03301(12) 0.0988(11) Uani 1 1 d . U . . .
O4 O 1.04306(18) 0.03484(19) 0.42668(16) 0.0827(10) Uani 1 1 d . U . . .
F31 F 0.46545(18) 0.3131(2) -0.01296(11) 0.1052(12) Uani 1 1 d . U . . .
F2 F 0.95271(18) 0.00161(18) 0.26277(16) 0.1095(12) Uani 1 1 d . U . . .
F33 F 0.84827(19) 0.0997(2) 0.08218(16) 0.1178(13) Uani 1 1 d . U . . .
F17 F 0.70491(18) -0.02054(18) 0.24541(17) 0.1134(13) Uani 1 1 d . U . . .
F35 F 0.3992(2) 0.2038(2) 0.47198(16) 0.1292(15) Uani 1 1 d . U . . .
O6 O 0.29573(19) 0.2631(2) 0.33713(16) 0.0877(11) Uani 1 1 d . U . . .
O8 O 0.9899(2) 0.6028(2) 0.32337(15) 0.0865(11) Uani 1 1 d . U . . .
O10 O 0.87298(19) 0.5169(3) 0.00685(13) 0.1047(15) Uani 1 1 d . U . . .
F9 F 0.4068(2) 0.3283(2) 0.51817(13) 0.1317(16) Uani 1 1 d . U . . .
F37 F 0.7467(2) 0.3129(2) 0.01427(13) 0.1068(11) Uani 1 1 d . U . . .
F19 F 0.8124(2) 0.6536(2) 0.16639(16) 0.1245(14) Uani 1 1 d . U . . .
F39 F 0.8055(2) -0.10127(17) 0.41786(19) 0.1351(16) Uani 1 1 d . U . . .
O12 O 1.17891(19) 0.2051(2) 0.17437(16) 0.0962(12) Uani 1 1 d . U . . .
C1 C 1.06379(10) 0.37784(14) 0.35149(10) 0.0514(10) Uani 1 1 d G U . . .
C4 C 1.00391(13) 0.36942(13) 0.32162(8) 0.0472(9) Uani 1 1 d G U . . .
C6 C 0.93864(10) 0.40498(14) 0.33427(9) 0.0462(9) Uani 1 1 d G U . . .
C8 C 0.93325(11) 0.44895(14) 0.37678(10) 0.0532(10) Uani 1 1 d G U . . .
C10 C 0.99314(14) 0.45736(14) 0.40665(9) 0.0569(11) Uani 1 1 d G U . . .
C12 C 1.05841(11) 0.42181(15) 0.39401(9) 0.0564(11) Uani 1 1 d G U . . .
F5 F 0.4346(2) 0.1275(2) 0.05984(16) 0.1363(16) Uani 1 1 d . U . . .
F41 F 0.5866(2) 0.6548(2) 0.16336(15) 0.1227(14) Uani 1 1 d . U . . .
F21 F 0.6681(3) 0.5879(2) 0.03062(15) 0.1414(17) Uani 1 1 d . U . . .
F43 F 0.5589(2) -0.0957(2) 0.3879(2) 0.1399(17) Uani 1 1 d . U . . .
C14 C 0.68124(13) 0.35883(14) 0.44595(8) 0.0470(9) Uani 1 1 d G U . . .
C16 C 0.68672(14) 0.42755(13) 0.45994(10) 0.0508(10) Uani 1 1 d G U . . .
C18 C 0.65323(15) 0.45327(13) 0.50503(11) 0.0634(12) Uani 1 1 d G U . . .
C20 C 0.61426(15) 0.41026(18) 0.53614(9) 0.0692(13) Uani 1 1 d G U . . .
C22 C 0.60878(14) 0.34154(16) 0.52216(10) 0.0631(12) Uani 1 1 d G U . . .
C24 C 0.64227(14) 0.31582(12) 0.47706(11) 0.0550(10) Uani 1 1 d G U . . .
O14 O 0.57701(19) 0.0285(2) 0.51027(19) 0.1038(15) Uani 1 1 d . U . . .
F11 F 1.0146(2) 0.2556(3) 0.00490(14) 0.1340(16) Uani 1 1 d . U . . .
F45 F 1.0156(2) 0.1010(2) 0.18153(18) 0.1380(16) Uani 1 1 d . U . . .
C26 C 0.51476(12) 0.32117(18) 0.12164(10) 0.0599(12) Uani 1 1 d G U . . .
C28 C 0.51875(14) 0.3264(2) 0.06790(10) 0.0697(13) Uani 1 1 d G U . . .
C30 C 0.46144(17) 0.3094(2) 0.03810(8) 0.0790(15) Uani 1 1 d G U . . .
C32 C 0.40013(14) 0.2873(2) 0.06202(11) 0.0792(15) Uani 1 1 d G U . . .
C34 C 0.39613(12) 0.28208(19) 0.11576(12) 0.0694(13) Uani 1 1 d G U . . .
C36 C 0.45345(14) 0.29903(18) 0.14557(8) 0.0624(12) Uani 1 1 d G U . . .
O15 O 0.4379(2) 0.5039(3) 0.05894(14) 0.1117(16) Uani 1 1 d . U . . .
C38 C 0.78713(15) 0.22445(13) 0.54544(11) 0.0551(10) Uani 1 1 d G U . . .
C40 C 0.81046(14) 0.28969(15) 0.53461(9) 0.0533(10) Uani 1 1 d G U . . .
H40 H 0.836414 0.297353 0.503428 0.064 Uiso 1 1 calc R U . . .
C42 C 0.79582(16) 0.34371(12) 0.56940(12) 0.0611(11) Uani 1 1 d G U . . .
C44 C 0.75784(18) 0.33249(16) 0.61502(11) 0.0791(14) Uani 1 1 d G U . . .
H44 H 0.747834 0.369408 0.638798 0.095 Uiso 1 1 calc R U . . .
C46 C 0.73451(18) 0.26725(19) 0.62585(10) 0.0869(16) Uani 1 1 d G U . . .
H46 H 0.708562 0.259587 0.657036 0.104 Uiso 1 1 calc R U . . .
C48 C 0.74916(17) 0.21323(14) 0.59107(13) 0.0754(14) Uani 1 1 d G U . . .
H48 H 0.733215 0.168647 0.598469 0.090 Uiso 1 1 calc R U . . .
F23 F 0.33577(19) 0.0752(2) 0.2243(2) 0.1420(17) Uani 1 1 d . U . . .
F47 F 0.3210(2) 0.0909(2) 0.1202(2) 0.158(2) Uani 1 1 d . U . . .
F3 F 0.6815(3) -0.16564(18) 0.4191(2) 0.157(2) Uani 1 1 d . U . . .
C50 C 0.43325(18) 0.55525(14) 0.27214(13) 0.0648(12) Uani 1 1 d G U . . .
C52 C 0.48570(16) 0.57282(18) 0.30619(13) 0.0697(13) Uani 1 1 d G U . . .
H52 H 0.516464 0.537435 0.321834 0.084 Uiso 1 1 calc R U . . .
C54 C 0.4931(2) 0.6422(2) 0.31736(15) 0.0894(16) Uani 1 1 d G U . . .
C56 C 0.4481(3) 0.69395(14) 0.29448(19) 0.112(2) Uani 1 1 d G U . . .
H56 H 0.453182 0.741341 0.302108 0.134 Uiso 1 1 calc R U . . .
C58 C 0.3957(3) 0.67638(18) 0.26042(18) 0.136(3) Uani 1 1 d G U . . .
H58 H 0.364893 0.711768 0.244778 0.164 Uiso 1 1 calc R U . . .
C60 C 0.3882(2) 0.6070(2) 0.24925(15) 0.107(2) Uani 1 1 d G U . . .
H60 H 0.352388 0.595028 0.225975 0.128 Uiso 1 1 calc R U . . .
F49 F 0.7315(3) 0.70007(19) 0.30429(19) 0.1499(19) Uani 1 1 d . U . . .
C62 C 0.90276(10) 0.13427(15) 0.50334(11) 0.0555(11) Uani 1 1 d G U . . .
C64 C 0.94521(15) 0.16145(15) 0.54072(10) 0.0623(12) Uani 1 1 d G U . . .
H64 H 0.923850 0.190893 0.566910 0.075 Uiso 1 1 calc R U . . .
C66 C 1.01893(14) 0.14554(16) 0.53979(11) 0.0720(13) Uani 1 1 d G U . . .
H66 H 1.047940 0.164115 0.565341 0.086 Uiso 1 1 calc R U . . .
C68 C 1.05018(10) 0.10246(16) 0.50147(13) 0.0718(13) Uani 1 1 d G U . . .
H68 H 1.100563 0.091584 0.500836 0.086 Uiso 1 1 calc R U . . .
C70 C 1.00773(14) 0.07528(15) 0.46409(11) 0.0623(12) Uani 1 1 d G U . . .
C72 C 0.93402(13) 0.09118(14) 0.46502(10) 0.0564(11) Uani 1 1 d G U . . .
H72 H 0.905004 0.072609 0.439469 0.068 Uiso 1 1 calc R U . . .
C74 C 0.94476(16) 0.47991(16) 0.08145(11) 0.0710(14) Uani 1 1 d G U . . .
H74 H 0.930686 0.433765 0.079871 0.085 Uiso 1 1 calc R U . . .
C76 C 0.91944(15) 0.5291(2) 0.04517(10) 0.0817(16) Uani 1 1 d G U . . .
C78 C 0.94003(17) 0.59664(19) 0.04748(11) 0.0865(16) Uani 1 1 d G U . . .
H78 H 0.922725 0.630284 0.022681 0.104 Uiso 1 1 calc R U . . .
C80 C 0.98593(18) 0.61494(15) 0.08608(13) 0.0851(16) Uani 1 1 d G U . . .
H80 H 1.000004 0.661082 0.087660 0.102 Uiso 1 1 calc R U . . .
C82 C 1.01125(16) 0.56572(18) 0.12236(10) 0.0754(14) Uani 1 1 d G U . . .
H82 H 1.042624 0.578222 0.148745 0.090 Uiso 1 1 calc R U . . .
C84 C 0.99066(15) 0.49820(17) 0.12005(10) 0.0673(13) Uani 1 1 d G U . . .
C86 C 0.31030(15) 0.33127(13) 0.33625(12) 0.0674(12) Uani 1 1 d G U . . .
C88 C 0.35477(14) 0.36084(15) 0.30008(10) 0.0596(11) Uani 1 1 d G U . . .
H88 H 0.378080 0.332933 0.273754 0.072 Uiso 1 1 calc R U . . .
C90 C 0.36513(13) 0.43124(15) 0.30242(9) 0.0542(10) Uani 1 1 d G U . . .
C92 C 0.33102(15) 0.47206(13) 0.34093(11) 0.0644(12) Uani 1 1 d G U . . .
H92 H 0.338103 0.520177 0.342532 0.077 Uiso 1 1 calc R U . . .
C94 C 0.28655(14) 0.44250(17) 0.37711(10) 0.0701(13) Uani 1 1 d G U . . .
H94 H 0.263239 0.470402 0.403432 0.084 Uiso 1 1 calc R U . . .
C96 C 0.27619(13) 0.37210(18) 0.37477(10) 0.0698(13) Uani 1 1 d G U . . .
H96 H 0.245795 0.351892 0.399494 0.084 Uiso 1 1 calc R U . . .
F25 F 0.6536(3) 0.74646(19) 0.22162(19) 0.1532(19) Uani 1 1 d . U . . .
C98 C 0.76003(14) 0.08433(14) 0.51797(14) 0.0625(12) Uani 1 1 d G U . . .
C100 C 0.68760(14) 0.08672(14) 0.50635(14) 0.0665(13) Uani 1 1 d G U . . .
H100 H 0.665172 0.126470 0.489567 0.080 Uiso 1 1 calc R U . . .
C102 C 0.64798(12) 0.03095(17) 0.51928(17) 0.0845(17) Uani 1 1 d G U . . .
C104 C 0.68079(17) -0.02721(15) 0.54383(18) 0.101(2) Uani 1 1 d G U . . .
H104 H 0.653716 -0.065320 0.552668 0.121 Uiso 1 1 calc R U . . .
C106 C 0.75322(17) -0.02960(15) 0.55545(17) 0.101(2) Uani 1 1 d G U . . .
H106 H 0.775648 -0.069352 0.572233 0.121 Uiso 1 1 calc R U . . .
C108 C 0.79284(12) 0.02616(17) 0.54252(16) 0.0829(17) Uani 1 1 d G U . . .
H108 H 0.842343 0.024527 0.550465 0.099 Uiso 1 1 calc R U . . .
C110 C 1.08388(14) 0.37433(17) 0.14215(11) 0.0692(13) Uani 1 1 d G U . . .
C112 C 1.10494(15) 0.31476(19) 0.17036(9) 0.0719(14) Uani 1 1 d G U . . .
H112 H 1.085580 0.308059 0.204120 0.086 Uiso 1 1 calc R U . . .
C114 C 1.15433(16) 0.26501(16) 0.14918(12) 0.0776(14) Uani 1 1 d G U . . .
C116 C 1.18266(15) 0.27482(18) 0.09978(12) 0.0824(16) Uani 1 1 d G U . . .
H116 H 1.216413 0.240814 0.085302 0.099 Uiso 1 1 calc R U . . .
C118 C 1.16160(16) 0.3344(2) 0.07157(9) 0.0858(17) Uani 1 1 d G U . . .
H118 H 1.180964 0.341091 0.037807 0.103 Uiso 1 1 calc R U . . .
C120 C 1.11221(16) 0.38414(17) 0.09275(11) 0.0762(15) Uani 1 1 d G U . . .
H120 H 1.097823 0.424852 0.073469 0.091 Uiso 1 1 calc R U . . .
C122 C 0.38627(15) 0.46570(19) 0.19429(9) 0.0620(12) Uani 1 1 d G U . . .
C124 C 0.42794(13) 0.48522(19) 0.15241(12) 0.0658(12) Uani 1 1 d G U . . .
H124 H 0.475154 0.498242 0.157825 0.079 Uiso 1 1 calc R U . . .
C126 C 0.40054(17) 0.4857(2) 0.10259(10) 0.0857(17) Uani 1 1 d G U . . .
C128 C 0.33146(18) 0.4666(2) 0.09466(10) 0.104(2) Uani 1 1 d G U . . .
H128 H 0.312732 0.466967 0.060616 0.124 Uiso 1 1 calc R U . . .
C130 C 0.28979(14) 0.4471(2) 0.13655(13) 0.106(2) Uani 1 1 d G U . . .
H130 H 0.242580 0.434099 0.131127 0.127 Uiso 1 1 calc R U . . .
C132 C 0.31720(14) 0.4466(2) 0.18636(11) 0.0831(16) Uani 1 1 d G U . . .
H132 H 0.288715 0.433302 0.214988 0.100 Uiso 1 1 calc R U . . .
F51 F 0.7204(3) -0.1472(2) 0.2875(2) 0.162(2) Uani 1 1 d . U . . .
C134 C 1.05236(14) 0.47869(16) 0.22170(10) 0.0613(12) Uani 1 1 d G U . . .
C136 C 1.00631(11) 0.52355(17) 0.25079(11) 0.0615(12) Uani 1 1 d G U . . .
H136 H 0.957264 0.530885 0.241769 0.074 Uiso 1 1 calc R U . . .
C138 C 1.03202(16) 0.55768(16) 0.29308(11) 0.0704(13) Uani 1 1 d G U . . .
C140 C 1.10378(17) 0.54695(18) 0.30628(10) 0.0795(15) Uani 1 1 d G U . . .
H140 H 1.121350 0.570277 0.335187 0.095 Uiso 1 1 calc R U . . .
C142 C 1.14983(12) 0.50209(19) 0.27719(12) 0.0819(16) Uani 1 1 d G U . . .
H142 H 1.198871 0.494756 0.286215 0.098 Uiso 1 1 calc R U . . .
C144 C 1.12412(14) 0.46796(17) 0.23490(11) 0.0713(14) Uani 1 1 d G U . . .
H144 H 1.155590 0.437299 0.215019 0.086 Uiso 1 1 calc R U . . .
C146 C 0.76353(17) 0.48442(15) 0.12904(12) 0.0630(12) Uani 1 1 d G U . . .
C148 C 0.72061(19) 0.50113(19) 0.08651(12) 0.0769(14) Uani 1 1 d G U . . .
C150 C 0.7083(2) 0.5700(2) 0.07077(13) 0.104(2) Uani 1 1 d G U . . .
C152 C 0.7389(2) 0.62212(16) 0.09755(16) 0.115(2) Uani 1 1 d G U . . .
C154 C 0.7819(2) 0.60541(17) 0.14008(15) 0.0924(18) Uani 1 1 d G U . . .
C156 C 0.79415(17) 0.53656(19) 0.15582(11) 0.0695(13) Uani 1 1 d G U . . .
C158 C 0.47195(18) 0.36835(18) 0.44704(12) 0.0764(14) Uani 1 1 d G U . . .
C160 C 0.43673(17) 0.3163(2) 0.47174(10) 0.0917(17) Uani 1 1 d G U . . .
C162 C 0.43341(17) 0.2523(2) 0.44801(14) 0.0914(17) Uani 1 1 d G U . . .
C164 C 0.46530(17) 0.24033(15) 0.39957(14) 0.0744(14) Uani 1 1 d G U . . .
C166 C 0.50052(14) 0.29240(17) 0.37486(10) 0.0595(11) Uani 1 1 d G U . . .
C168 C 0.50385(15) 0.35641(16) 0.39860(12) 0.0616(11) Uani 1 1 d G U . . .
C170 C 0.97338(19) 0.2425(2) 0.09073(15) 0.0848(16) Uani 1 1 d G U . . .
C172 C 0.97349(18) 0.2034(2) 0.13621(13) 0.0811(15) Uani 1 1 d G U . . .
C174 C 1.0137(2) 0.1399(2) 0.13891(17) 0.110(2) Uani 1 1 d G U . . .
C176 C 1.0539(3) 0.1155(2) 0.0961(2) 0.149(3) Uani 1 1 d G U . . .
C177 C 1.0538(2) 0.1547(3) 0.05066(17) 0.135(3) Uani 1 1 d G U . . .
C89 C 1.0135(2) 0.2181(3) 0.04796(13) 0.107(2) Uani 1 1 d G U . . .
C45 C 1.03788(17) 0.25536(16) 0.43166(11) 0.0694(13) Uani 1 1 d G U . . .
C91 C 1.10143(12) 0.22253(18) 0.41249(13) 0.0741(14) Uani 1 1 d G U . . .
C23 C 1.10052(11) 0.17988(17) 0.36939(13) 0.0736(14) Uani 1 1 d G U . . .
C93 C 1.03606(15) 0.17008(15) 0.34544(11) 0.0633(12) Uani 1 1 d G U . . .
C47 C 0.97252(11) 0.20291(15) 0.36461(11) 0.0540(10) Uani 1 1 d G U . . .
C95 C 0.97343(13) 0.24555(15) 0.40772(11) 0.0571(11) Uani 1 1 d G U . . .
F13 F 0.8315(3) 0.2960(3) -0.06992(16) 0.169(2) Uani 1 1 d . U . . .
C3 C 0.69992(18) 0.58584(16) 0.29195(12) 0.0713(13) Uani 1 1 d G U . . .
C97 C 0.66449(16) 0.53935(12) 0.26273(12) 0.0522(10) Uani 1 1 d G U . . .
C49 C 0.62623(17) 0.56261(16) 0.21934(12) 0.0666(12) Uani 1 1 d G U . . .
C99 C 0.6234(2) 0.63237(18) 0.20517(13) 0.0867(16) Uani 1 1 d G U . . .
C25 C 0.6588(2) 0.67885(13) 0.23440(17) 0.0994(19) Uani 1 1 d G U . . .
C101 C 0.6971(2) 0.65559(15) 0.27779(16) 0.0947(19) Uani 1 1 d G U . . .
C51 C 0.51319(14) 0.12115(19) 0.18810(13) 0.0704(13) Uani 1 1 d G U . . .
C103 C 0.50591(18) 0.12928(19) 0.13479(13) 0.0798(15) Uani 1 1 d G U . . .
C13 C 0.4410(2) 0.1188(2) 0.11172(13) 0.105(2) Uani 1 1 d G U . . .
C105 C 0.38341(16) 0.1001(2) 0.14195(18) 0.110(2) Uani 1 1 d G U . . .
C53 C 0.39069(16) 0.0920(2) 0.19526(17) 0.105(2) Uani 1 1 d G U . . .
C107 C 0.45558(19) 0.1025(2) 0.21834(12) 0.0807(15) Uani 1 1 d G U . . .
F53 F 0.9667(3) -0.1245(2) 0.3071(3) 0.180(2) Uani 1 1 d . U . . .
F27 F 0.9288(2) 0.0817(3) -0.0042(2) 0.168(2) Uani 1 1 d . U . . .
O2 O 0.4803(8) -0.0736(10) 0.2066(6) 0.125(4) Uani 0.642(5) 1 d D U P A 2
C27 C 0.79403(18) 0.2062(2) 0.05013(13) 0.0841(15) Uani 1 1 d G U . . .
C109 C 0.8408(2) 0.1470(2) 0.04496(17) 0.1014(19) Uani 1 1 d G U . . .
C55 C 0.8838(2) 0.1381(3) 0.0008(2) 0.129(2) Uani 1 1 d G U . . .
C111 C 0.8801(2) 0.1883(3) -0.03824(15) 0.136(3) Uani 1 1 d G U . . .
C7 C 0.8333(3) 0.2474(3) -0.03307(14) 0.126(2) Uani 1 1 d G U . . .
C113 C 0.7903(2) 0.2564(2) 0.01112(16) 0.0933(17) Uani 1 1 d G U . . .
C57 C 0.8605(3) 0.4220(3) 0.5175(2) 0.0772(14) Uani 1 1 d . U . . .
H57A H 0.836266 0.408535 0.486185 0.116 Uiso 1 1 calc R U . . .
H57B H 0.906403 0.394219 0.520593 0.116 Uiso 1 1 calc R U . . .
H57C H 0.869128 0.471346 0.515379 0.116 Uiso 1 1 calc R U . . .
F55 F 0.7272(4) 0.6885(2) 0.0834(2) 0.192(3) Uani 1 1 d . U . . .
C115 C 0.61882(15) 0.00551(18) 0.37249(17) 0.0843(16) Uani 1 1 d G U . . .
C29 C 0.61909(18) -0.06357(19) 0.38810(19) 0.105(2) Uani 1 1 d G U . . .
C117 C 0.6827(2) -0.09951(14) 0.40328(19) 0.112(2) Uani 1 1 d G U . . .
C59 C 0.74598(18) -0.06636(17) 0.40285(19) 0.102(2) Uani 1 1 d G U . . .
C119 C 0.74572(14) 0.00272(17) 0.38724(17) 0.0845(17) Uani 1 1 d G U . . .
C15 C 0.68214(18) 0.03866(13) 0.37206(15) 0.0692(13) Uani 1 1 d G U . . .
O9 O 0.5464(3) 0.6554(3) 0.3494(2) 0.1366(19) Uani 1 1 d . U . . .
F7 F 1.0925(3) 0.1305(3) 0.0092(2) 0.192(3) Uani 1 1 d . U . . .
C121 C 1.0014(3) 0.0055(3) 0.3871(2) 0.0863(16) Uani 1 1 d . U . . .
H12A H 1.033576 -0.016583 0.360721 0.129 Uiso 1 1 calc R U . . .
H12B H 0.970090 0.042312 0.370956 0.129 Uiso 1 1 calc R U . . .
H12C H 0.972105 -0.029341 0.402711 0.129 Uiso 1 1 calc R U . . .
F57 F 1.0908(3) 0.0552(3) 0.0973(2) 0.224(3) Uani 1 1 d . U . . .
C61 C 0.8575(3) 0.4461(4) -0.0014(2) 0.113(2) Uani 1 1 d . U . . .
H61A H 0.828653 0.443390 -0.032574 0.170 Uiso 1 1 calc R U . . .
H61B H 0.830832 0.429464 0.028658 0.170 Uiso 1 1 calc R U . . .
H61C H 0.902477 0.417039 -0.005719 0.170 Uiso 1 1 calc R U . . .
F29 F 0.9211(3) 0.1810(3) -0.08123(18) 0.188(2) Uani 1 1 d . U . . .
F59 F 0.8501(3) -0.2013(2) 0.3192(3) 0.214(3) Uani 1 1 d . U . . .
C123 C 0.3266(3) 0.2199(3) 0.2971(3) 0.0943(18) Uani 1 1 d . U . . .
H12D H 0.308767 0.237029 0.263488 0.141 Uiso 1 1 calc R U . . .
H12E H 0.313560 0.172248 0.302716 0.141 Uiso 1 1 calc R U . . .
H12F H 0.378904 0.220716 0.297587 0.141 Uiso 1 1 calc R U . . .
C31 C 0.7512(5) -0.0201(4) -0.0021(3) 0.1278(17) Uani 0.642(5) 1 d G U P A 2
H31 H 0.772367 -0.063084 0.010643 0.153 Uiso 0.642(5) 1 calc R U P A 2
C125 C 0.7625(4) -0.0008(4) -0.0534(3) 0.1281(17) Uani 0.642(5) 1 d G U P A 2
H125 H 0.791329 -0.030598 -0.075774 0.154 Uiso 0.642(5) 1 calc R U P A 2
C63 C 0.7316(5) 0.0621(5) -0.0721(2) 0.1279(17) Uani 0.642(5) 1 d G U P A 2
H63 H 0.739274 0.075323 -0.107186 0.154 Uiso 0.642(5) 1 calc R U P A 2
C127 C 0.6894(5) 0.1058(4) -0.0394(3) 0.1277(16) Uani 0.642(5) 1 d DG U P A 2
C2 C 0.6781(6) 0.0865(5) 0.0119(3) 0.1270(17) Uani 0.642(5) 1 d G U P A 2
H2 H 0.649296 0.116274 0.034236 0.152 Uiso 0.642(5) 1 calc R U P A 2
C129 C 0.7090(6) 0.0235(6) 0.0306(2) 0.1270(17) Uani 0.642(5) 1 d G U P A 2
O5 O 0.9498(5) -0.1061(4) 0.1437(5) 0.1375(16) Uani 0.642(5) 1 d . U P A 2
C65 C 0.5070(4) 0.5276(4) 0.0670(2) 0.114(2) Uani 1 1 d . U . . .
H65A H 0.530495 0.534845 0.033394 0.171 Uiso 1 1 calc R U . . .
H65B H 0.535960 0.492765 0.087086 0.171 Uiso 1 1 calc R U . . .
H65C H 0.502086 0.571439 0.086027 0.171 Uiso 1 1 calc R U . . .
C131 C 0.4746(7) -0.0814(8) 0.1173(6) 0.141(6) Uani 0.642(5) 1 d G U P A 2
H131 H 0.428328 -0.097648 0.122025 0.169 Uiso 0.642(5) 1 calc R U P A 2
C33 C 0.5139(8) -0.0645(9) 0.1601(5) 0.115(4) Uani 0.642(5) 1 d G U P A 2
C133 C 0.5816(8) -0.0407(9) 0.1532(5) 0.103(4) Uani 0.642(5) 1 d G U P A 2
H133 H 0.608442 -0.029178 0.182475 0.123 Uiso 0.642(5) 1 calc R U P A 2
C67 C 0.6101(7) -0.0338(8) 0.1035(6) 0.117(4) Uani 0.642(5) 1 d G U P A 2
C135 C 0.5708(8) -0.0507(7) 0.0607(5) 0.134(5) Uani 0.642(5) 1 d G U P A 2
H135 H 0.590226 -0.046022 0.026769 0.161 Uiso 0.642(5) 1 calc R U P A 2
C17 C 0.5031(8) -0.0745(7) 0.0676(5) 0.146(6) Uani 0.642(5) 1 d G U P A 2
H17 H 0.476222 -0.086054 0.038370 0.176 Uiso 0.642(5) 1 calc R U P A 2
C137 C 1.1551(3) 0.1954(4) 0.2255(2) 0.106(2) Uani 1 1 d . U . . .
H13A H 1.102946 0.193354 0.226080 0.159 Uiso 1 1 calc R U . . .
H13B H 1.167861 0.234199 0.246865 0.159 Uiso 1 1 calc R U . . .
H13C H 1.177849 0.151818 0.239356 0.159 Uiso 1 1 calc R U . . .
C69 C 0.5399(3) 0.0911(3) 0.4907(3) 0.104(2) Uani 1 1 d . U . . .
H69A H 0.560827 0.103315 0.457154 0.156 Uiso 1 1 calc R U . . .
H69B H 0.544386 0.128912 0.515276 0.156 Uiso 1 1 calc R U . . .
H69C H 0.489109 0.083678 0.486426 0.156 Uiso 1 1 calc R U . . .
O11 O 0.6609(4) 0.1683(4) -0.0613(3) 0.1283(16) Uani 0.642(5) 1 d D U P A 2
C139 C 0.7774(2) -0.1108(2) 0.2814(2) 0.124(3) Uani 1 1 d G U . . .
C35 C 0.8447(3) -0.13771(17) 0.2972(2) 0.145(3) Uani 1 1 d G U . . .
C141 C 0.9038(2) -0.0990(2) 0.2904(2) 0.134(3) Uani 1 1 d G U . . .
C71 C 0.89551(18) -0.0333(2) 0.2677(2) 0.102(2) Uani 1 1 d G U . . .
C143 C 0.8282(2) -0.00640(16) 0.25196(16) 0.0860(17) Uani 1 1 d G U . . .
C9 C 0.76919(17) -0.0451(2) 0.25880(18) 0.0954(18) Uani 1 1 d G U . . .
C145 C 0.9184(4) 0.6182(4) 0.3087(3) 0.116(2) Uani 1 1 d . U . . .
H14A H 0.917265 0.637413 0.273413 0.174 Uiso 1 1 calc R U . . .
H14B H 0.895084 0.652350 0.332667 0.174 Uiso 1 1 calc R U . . .
H14C H 0.893056 0.575722 0.309852 0.174 Uiso 1 1 calc R U . . .
C73 C 0.6173(5) 0.2173(6) -0.0297(5) 0.1269(19) Uani 0.642(5) 1 d D U P A 2
H73A H 0.608338 0.261088 -0.048858 0.190 Uiso 0.642(5) 1 calc R U P A 2
H73B H 0.642556 0.225891 0.002385 0.190 Uiso 0.642(5) 1 calc R U P A 2
H73C H 0.571604 0.198134 -0.021203 0.190 Uiso 0.642(5) 1 calc R U P A 2
C147 C 0.7596(4) -0.0717(3) 0.1141(4) 0.1380(16) Uani 0.642(5) 1 d G U P A 2
C37 C 0.7361(3) -0.1358(4) 0.1283(4) 0.1387(16) Uani 0.642(5) 1 d G U P A 2
H37 H 0.686910 -0.143859 0.125592 0.166 Uiso 0.642(5) 1 calc R U P A 2
C149 C 0.7847(4) -0.1881(3) 0.1466(3) 0.1391(16) Uani 0.642(5) 1 d G U P A 2
H149 H 0.768687 -0.231943 0.156382 0.167 Uiso 0.642(5) 1 calc R U P A 2
C75 C 0.8567(4) -0.1764(3) 0.1507(3) 0.1388(16) Uani 0.642(5) 1 d G U P A 2
H75 H 0.889930 -0.212133 0.163160 0.167 Uiso 0.642(5) 1 calc R U P A 2
C151 C 0.8802(3) -0.1123(4) 0.1364(4) 0.1378(16) Uani 0.642(5) 1 d G U P A 2
C19 C 0.8316(4) -0.0600(3) 0.1181(4) 0.1376(16) Uani 0.642(5) 1 d G U P A 2
H19 H 0.847622 -0.016155 0.108358 0.165 Uiso 0.642(5) 1 calc R U P A 2
C153 C 0.5207(9) -0.0736(11) 0.2542(5) 0.136(6) Uani 0.642(5) 1 d D U P A 2
H15A H 0.569493 -0.093945 0.247366 0.204 Uiso 0.642(5) 1 d R U P A 2
H15B H 0.497853 -0.100925 0.280966 0.204 Uiso 0.642(5) 1 d R U P A 2
H15C H 0.522463 -0.025665 0.266036 0.204 Uiso 0.642(5) 1 d R U P A 2
C77 C 0.9791(7) -0.0398(6) 0.1244(6) 0.1376(19) Uani 0.642(5) 1 d . U P A 2
H77A H 0.956608 -0.025875 0.091489 0.206 Uiso 0.642(5) 1 calc R U P A 2
H77B H 1.031040 -0.047383 0.119262 0.206 Uiso 0.642(5) 1 calc R U P A 2
H77C H 0.968520 -0.003062 0.150053 0.206 Uiso 0.642(5) 1 calc R U P A 2
C155 C 0.5535(7) 0.7319(5) 0.3587(4) 0.215(6) Uani 1 1 d . U . . .
H15D H 0.556202 0.756286 0.325363 0.323 Uiso 1 1 calc R U . . .
H15E H 0.597178 0.737533 0.378278 0.323 Uiso 1 1 calc R U . . .
H15F H 0.511769 0.751411 0.378577 0.323 Uiso 1 1 calc R U . . .
C39 C 0.7368(7) -0.1334(8) 0.0567(6) 0.147(3) Uani 0.358(5) 1 d G U P A 1
H39 H 0.694049 -0.131705 0.037168 0.176 Uiso 0.358(5) 1 calc R U P A 1
C157 C 0.7830(8) -0.1933(7) 0.0570(6) 0.147(3) Uani 0.358(5) 1 d G U P A 1
H157 H 0.771892 -0.232563 0.037608 0.176 Uiso 0.358(5) 1 calc R U P A 1
C79 C 0.8456(8) -0.1957(6) 0.0856(7) 0.147(3) Uani 0.358(5) 1 d G U P A 1
H79 H 0.877163 -0.236625 0.085735 0.176 Uiso 0.358(5) 1 calc R U P A 1
C159 C 0.8619(7) -0.1382(9) 0.1139(7) 0.147(3) Uani 0.358(5) 1 d DG U P A 1
C5 C 0.8156(9) -0.0783(7) 0.1136(7) 0.147(3) Uani 0.358(5) 1 d G U P A 1
H5 H 0.826749 -0.038973 0.132983 0.176 Uiso 0.358(5) 1 calc R U P A 1
C161 C 0.7531(8) -0.0759(6) 0.0850(7) 0.147(3) Uani 0.358(5) 1 d G U P A 1
O3 O 0.9278(8) -0.1386(7) 0.1341(8) 0.147(3) Uani 0.358(5) 1 d D U P A 1
C81 C 0.9649(13) -0.0756(9) 0.1365(14) 0.147(3) Uani 0.358(5) 1 d D U P A 1
H81A H 0.965747 -0.053845 0.102044 0.220 Uiso 0.358(5) 1 calc R U P A 1
H81B H 1.014091 -0.086952 0.147996 0.220 Uiso 0.358(5) 1 calc R U P A 1
H81C H 0.939876 -0.043372 0.161068 0.220 Uiso 0.358(5) 1 calc R U P A 1
O13 O 0.6421(7) 0.1957(7) -0.0466(5) 0.129(2) Uani 0.358(5) 1 d D U P A 1
C163 C 0.5779(8) 0.2159(11) -0.0166(8) 0.131(3) Uani 0.358(5) 1 d D U P A 1
H16A H 0.546825 0.247561 -0.037865 0.197 Uiso 0.358(5) 1 d R U P A 1
H16B H 0.591765 0.240071 0.014485 0.197 Uiso 0.358(5) 1 d R U P A 1
H16C H 0.551975 0.175631 -0.006355 0.197 Uiso 0.358(5) 1 d R U P A 1
C41 C 0.7244(9) 0.1010(8) -0.0759(5) 0.128(2) Uani 0.358(5) 1 d G U P A 1
H41 H 0.729699 0.124182 -0.108240 0.153 Uiso 0.358(5) 1 calc R U P A 1
C165 C 0.6796(10) 0.1312(8) -0.0376(7) 0.128(2) Uani 0.358(5) 1 d DG U P A 1
C83 C 0.6718(11) 0.0973(11) 0.0097(6) 0.127(2) Uani 0.358(5) 1 d G U P A 1
H83 H 0.641170 0.117895 0.035909 0.153 Uiso 0.358(5) 1 calc R U P A 1
C167 C 0.7089(12) 0.0332(11) 0.0186(5) 0.127(2) Uani 0.358(5) 1 d G U P A 1
C21 C 0.7537(10) 0.0030(7) -0.0198(7) 0.127(2) Uani 0.358(5) 1 d G U P A 1
H21 H 0.779068 -0.040774 -0.013701 0.153 Uiso 0.358(5) 1 calc R U P A 1
C169 C 0.7615(8) 0.0369(8) -0.0670(6) 0.127(2) Uani 0.358(5) 1 d G U P A 1
H169 H 0.792122 0.016306 -0.093264 0.153 Uiso 0.358(5) 1 calc R U P A 1
O7 O 0.4912(15) -0.0924(18) 0.1940(9) 0.125(7) Uani 0.358(5) 1 d D U P A 1
C85 C 0.5152(15) -0.0655(16) 0.1452(8) 0.109(5) Uani 0.358(5) 1 d G U P A 1
C171 C 0.5848(14) -0.0472(15) 0.1370(8) 0.098(6) Uani 0.358(5) 1 d G U P A 1
H171 H 0.617607 -0.049403 0.164816 0.117 Uiso 0.358(5) 1 calc R U P A 1
C43 C 0.6065(12) -0.0258(11) 0.0880(9) 0.089(5) Uani 0.358(5) 1 d G U P A 1
C173 C 0.5585(13) -0.0226(9) 0.0473(7) 0.096(5) Uani 0.358(5) 1 d G U P A 1
H173 H 0.573271 -0.007935 0.013861 0.115 Uiso 0.358(5) 1 calc R U P A 1
C87 C 0.4888(12) -0.0409(10) 0.0555(9) 0.116(6) Uani 0.358(5) 1 d G U P A 1
H87 H 0.456019 -0.038749 0.027685 0.139 Uiso 0.358(5) 1 calc R U P A 1
C175 C 0.4672(12) -0.0624(13) 0.1045(10) 0.107(6) Uani 0.358(5) 1 d G U P A 1
H175 H 0.419560 -0.074890 0.110074 0.129 Uiso 0.358(5) 1 calc R U P A 1
C11 C 0.5402(13) -0.0898(17) 0.2369(9) 0.096(7) Uani 0.358(5) 1 d D U P A 1
H11A H 0.583253 -0.120638 0.229803 0.145 Uiso 0.358(5) 1 calc R U P A 1
H11B H 0.516748 -0.104979 0.268766 0.145 Uiso 0.358(5) 1 calc R U P A 1
H11C H 0.553551 -0.042153 0.240995 0.145 Uiso 0.358(5) 1 calc R U P A 1
P2 P 0.6975(6) -0.0037(5) 0.1001(4) 0.119(3) Uani 0.642(5) 1 d . U P A 2
Ag5 Ag 0.71026(18) 0.1005(3) 0.1544(2) 0.0621(7) Uani 0.358(5) 1 d . U P A 1


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 Ag4 2.8969(4) . ?
Ag1 Ag6 2.8362(4) . ?
Ag1 Ag10 2.8667(5) . ?
Ag1 Ag7 2.8614(5) . ?
Ag1 Cu1 2.8804(6) . ?
Ag1 Cu3 2.8817(6) . ?
Ag1 S1 2.5660(12) . ?
Ag1 S8 2.5526(12) . ?
Ag4 Ag6 2.8668(5) . ?
Ag4 Ag8 2.8366(5) . ?
Ag4 Ag3 3.3730(5) . ?
Ag4 Ag7 2.8795(5) . ?
Ag4 Cu1 2.9381(6) . ?
Ag4 Cu4 2.8715(6) . ?
Ag4 S4 2.5428(11) . ?
Ag4 S12 2.5648(11) . ?
Ag6 Ag8 2.8754(5) . ?
Ag6 Ag10 2.8549(5) . ?
Ag6 Cu1 2.8996(6) . ?
Ag6 Cu2 2.8550(6) . ?
Ag6 S6 2.5462(11) . ?
Ag6 S3 2.5609(12) . ?
Ag8 Ag10 2.8724(5) . ?
Ag8 Ag7 2.8875(5) . ?
Ag8 Cu4 2.9563(7) . ?
Ag8 Cu2 2.9101(7) . ?
Ag8 S10 2.5636(13) . ?
Ag8 S9 2.5588(14) . ?
Ag8 Ag5 3.341(6) . ?
Ag10 Ag7 2.8544(5) . ?
Ag10 Cu2 2.9051(7) . ?
Ag10 Cu3 2.9267(7) . ?
Ag10 S2 2.5524(12) . ?
Ag10 S5 2.5514(12) . ?
Ag10 Ag5 3.310(5) . ?
Ag11 S4 2.6208(11) . ?
Ag11 S8 2.6929(12) . ?
Ag11 P4 2.4299(13) . ?
Ag11 S7 2.6592(12) . ?
Ag3 S6 2.6306(10) . ?
Ag3 S10 2.7006(12) . ?
Ag3 S12 2.6747(13) . ?
Ag3 P1 2.4382(11) . ?
Ag7 Cu4 2.8910(6) . ?
Ag7 Cu3 2.8859(6) . ?
Ag7 S7 2.5693(14) . ?
Ag7 S11 2.5686(13) . ?
Ag2 S1 2.6404(11) . ?
Ag2 S3 2.6536(11) . ?
Ag2 S2 2.6466(15) . ?
Ag2 P5 2.4418(12) . ?
Ag9 S9 2.680(4) . ?
Ag9 S5 2.775(5) . ?
Ag9 S11 2.644(4) . ?
Ag9 P2 2.323(11) . ?
Cu1 S1 2.2932(11) . ?
Cu1 S4 2.2960(12) . ?
Cu1 S6 2.2958(11) . ?
Cu4 S12 2.3083(13) . ?
Cu4 S7 2.3111(13) . ?
Cu4 S9 2.3179(14) . ?
Cu2 S10 2.2978(12) . ?
Cu2 S3 2.3119(13) . ?
Cu2 S5 2.2969(16) . ?
Cu3 S8 2.3042(13) . ?
Cu3 S2 2.3139(16) . ?
Cu3 S11 2.3115(14) . ?
S1 C6 1.7875(19) . ?
S4 C14 1.781(2) . ?
S6 C97 1.777(2) . ?
S8 C47 1.799(2) . ?
S10 C26 1.789(2) . ?
S12 C166 1.787(3) . ?
S3 C146 1.758(3) . ?
P1 C50 1.813(3) . ?
P1 C90 1.809(2) . ?
P1 C122 1.812(2) . ?
P4 C38 1.808(3) . ?
P4 C62 1.815(2) . ?
P4 C98 1.813(2) . ?
S7 C15 1.790(3) . ?
S2 C172 1.786(3) . ?
P5 C84 1.818(3) . ?
P5 C110 1.810(3) . ?
P5 C134 1.814(2) . ?
S9 C51 1.790(2) . ?
S9 Ag5 2.637(4) . ?
S5 C27 1.789(3) . ?
S5 Ag5 2.583(6) . ?
S11 C143 1.789(3) . ?
S11 Ag5 2.684(5) . ?
P3 C161 1.874(17) . ?
P3 C167 1.798(19) . ?
P3 C43 1.80(3) . ?
P3 Ag5 2.595(17) . ?
F1 C1 1.330(3) . ?
F4 C4 1.306(3) . ?
F6 C16 1.315(3) . ?
F8 C168 1.320(4) . ?
F10 C8 1.317(3) . ?
F12 C36 1.311(3) . ?
F14 C24 1.330(3) . ?
F16 C95 1.324(3) . ?
F18 C93 1.318(4) . ?
F20 C156 1.334(3) . ?
F22 C12 1.335(3) . ?
F24 C10 1.317(3) . ?
F26 C34 1.327(3) . ?
F28 C119 1.319(4) . ?
F30 C28 1.317(3) . ?
F32 C3 1.307(4) . ?
F34 C45 1.327(4) . ?
F36 C49 1.318(4) . ?
F38 C18 1.325(4) . ?
F40 C22 1.332(4) . ?
O1 C42 1.377(4) . ?
O1 C57 1.434(6) . ?
F42 C115 1.310(4) . ?
F44 C148 1.288(4) . ?
F46 C158 1.340(4) . ?
F48 C103 1.314(4) . ?
F50 C20 1.337(3) . ?
F52 C164 1.319(4) . ?
F54 C170 1.295(5) . ?
F56 C23 1.316(4) . ?
F58 C91 1.329(3) . ?
F60 C107 1.308(4) . ?
F15 C32 1.345(3) . ?
O4 C70 1.375(4) . ?
O4 C121 1.440(6) . ?
F31 C30 1.319(3) . ?
F2 C71 1.314(5) . ?
F33 C109 1.322(5) . ?
F17 C9 1.309(4) . ?
F35 C162 1.320(4) . ?
O6 C86 1.365(4) . ?
O6 C123 1.420(7) . ?
O8 C138 1.370(5) . ?
O8 C145 1.405(7) . ?
O10 C76 1.360(4) . ?
O10 C61 1.439(8) . ?
F9 C160 1.329(4) . ?
F37 C113 1.313(5) . ?
F19 C154 1.325(4) . ?
F39 C59 1.318(4) . ?
O12 C114 1.373(5) . ?
O12 C137 1.402(7) . ?
C1 C4 1.3900 . ?
C1 C12 1.3900 . ?
C4 C6 1.3900 . ?
C6 C8 1.3900 . ?
C8 C10 1.3900 . ?
C10 C12 1.3900 . ?
F5 C13 1.353(5) . ?
F41 C99 1.339(4) . ?
F21 C150 1.317(4) . ?
F43 C29 1.329(4) . ?
C14 C16 1.3900 . ?
C14 C24 1.3900 . ?
C16 C18 1.3900 . ?
C18 C20 1.3900 . ?
C20 C22 1.3900 . ?
C22 C24 1.3900 . ?
O14 C102 1.357(4) . ?
O14 C69 1.438(6) . ?
F11 C89 1.321(5) . ?
F45 C174 1.325(5) . ?
C26 C28 1.3900 . ?
C26 C36 1.3900 . ?
C28 C30 1.3900 . ?
C30 C32 1.3900 . ?
C32 C34 1.3900 . ?
C34 C36 1.3900 . ?
O15 C126 1.375(5) . ?
O15 C65 1.423(7) . ?
C38 C40 1.3900 . ?
C38 C48 1.3900 . ?
C40 H40 0.9500 . ?
C40 C42 1.3900 . ?
C42 C44 1.3900 . ?
C44 H44 0.9500 . ?
C44 C46 1.3900 . ?
C46 H46 0.9500 . ?
C46 C48 1.3900 . ?
C48 H48 0.9500 . ?
F23 C53 1.322(5) . ?
F47 C105 1.328(4) . ?
F3 C117 1.339(4) . ?
C50 C52 1.3900 . ?
C50 C60 1.3900 . ?
C52 H52 0.9500 . ?
C52 C54 1.3900 . ?
C54 C56 1.3900 . ?
C54 O9 1.346(6) . ?
C56 H56 0.9500 . ?
C56 C58 1.3900 . ?
C58 H58 0.9500 . ?
C58 C60 1.3900 . ?
C60 H60 0.9500 . ?
F49 C101 1.315(4) . ?
C62 C64 1.3900 . ?
C62 C72 1.3900 . ?
C64 H64 0.9500 . ?
C64 C66 1.3900 . ?
C66 H66 0.9500 . ?
C66 C68 1.3900 . ?
C68 H68 0.9500 . ?
C68 C70 1.3900 . ?
C70 C72 1.3900 . ?
C72 H72 0.9500 . ?
C74 H74 0.9500 . ?
C74 C76 1.3900 . ?
C74 C84 1.3900 . ?
C76 C78 1.3900 . ?
C78 H78 0.9500 . ?
C78 C80 1.3900 . ?
C80 H80 0.9500 . ?
C80 C82 1.3900 . ?
C82 H82 0.9500 . ?
C82 C84 1.3900 . ?
C86 C88 1.3900 . ?
C86 C96 1.3900 . ?
C88 H88 0.9500 . ?
C88 C90 1.3900 . ?
C90 C92 1.3900 . ?
C92 H92 0.9500 . ?
C92 C94 1.3900 . ?
C94 H94 0.9500 . ?
C94 C96 1.3900 . ?
C96 H96 0.9500 . ?
F25 C25 1.340(4) . ?
C98 C100 1.3900 . ?
C98 C108 1.3900 . ?
C100 H100 0.9500 . ?
C100 C102 1.3900 . ?
C102 C104 1.3900 . ?
C104 H104 0.9500 . ?
C104 C106 1.3900 . ?
C106 H106 0.9500 . ?
C106 C108 1.3900 . ?
C108 H108 0.9500 . ?
C110 C112 1.3900 . ?
C110 C120 1.3900 . ?
C112 H112 0.9500 . ?
C112 C114 1.3900 . ?
C114 C116 1.3900 . ?
C116 H116 0.9500 . ?
C116 C118 1.3900 . ?
C118 H118 0.9500 . ?
C118 C120 1.3900 . ?
C120 H120 0.9500 . ?
C122 C124 1.3900 . ?
C122 C132 1.3900 . ?
C124 H124 0.9500 . ?
C124 C126 1.3900 . ?
C126 C128 1.3900 . ?
C128 H128 0.9500 . ?
C128 C130 1.3900 . ?
C130 H130 0.9500 . ?
C130 C132 1.3900 . ?
C132 H132 0.9500 . ?
F51 C139 1.330(5) . ?
C134 C136 1.3900 . ?
C134 C144 1.3900 . ?
C136 H136 0.9500 . ?
C136 C138 1.3900 . ?
C138 C140 1.3900 . ?
C140 H140 0.9500 . ?
C140 C142 1.3900 . ?
C142 H142 0.9500 . ?
C142 C144 1.3900 . ?
C144 H144 0.9500 . ?
C146 C148 1.3900 . ?
C146 C156 1.3900 . ?
C148 C150 1.3900 . ?
C150 C152 1.3900 . ?
C152 C154 1.3900 . ?
C152 F55 1.334(5) . ?
C154 C156 1.3900 . ?
C158 C160 1.3900 . ?
C158 C168 1.3900 . ?
C160 C162 1.3900 . ?
C162 C164 1.3900 . ?
C164 C166 1.3900 . ?
C166 C168 1.3900 . ?
C170 C172 1.3900 . ?
C170 C89 1.3900 . ?
C172 C174 1.3900 . ?
C174 C176 1.3900 . ?
C176 C177 1.3900 . ?
C176 F57 1.307(6) . ?
C177 C89 1.3900 . ?
C177 F7 1.348(4) . ?
C45 C91 1.3900 . ?
C45 C95 1.3900 . ?
C91 C23 1.3900 . ?
C23 C93 1.3900 . ?
C93 C47 1.3900 . ?
C47 C95 1.3900 . ?
F13 C7 1.330(6) . ?
C3 C97 1.3900 . ?
C3 C101 1.3900 . ?
C97 C49 1.3900 . ?
C49 C99 1.3900 . ?
C99 C25 1.3900 . ?
C25 C101 1.3900 . ?
C51 C103 1.3900 . ?
C51 C107 1.3900 . ?
C103 C13 1.3900 . ?
C13 C105 1.3900 . ?
C105 C53 1.3900 . ?
C53 C107 1.3900 . ?
F53 C141 1.318(5) . ?
F27 C55 1.331(6) . ?
O2 C33 1.361(17) . ?
O2 C153 1.4500(10) . ?
C27 C109 1.3900 . ?
C27 C113 1.3900 . ?
C109 C55 1.3900 . ?
C55 C111 1.3900 . ?
C111 C7 1.3900 . ?
C111 F29 1.342(4) . ?
C7 C113 1.3900 . ?
C57 H57A 0.9800 . ?
C57 H57B 0.9800 . ?
C57 H57C 0.9800 . ?
C115 C29 1.3900 . ?
C115 C15 1.3900 . ?
C29 C117 1.3900 . ?
C117 C59 1.3900 . ?
C59 C119 1.3900 . ?
C119 C15 1.3900 . ?
O9 C155 1.515(9) . ?
C121 H12A 0.9800 . ?
C121 H12B 0.9800 . ?
C121 H12C 0.9800 . ?
C61 H61A 0.9800 . ?
C61 H61B 0.9800 . ?
C61 H61C 0.9800 . ?
F59 C35 1.346(5) . ?
C123 H12D 0.9800 . ?
C123 H12E 0.9800 . ?
C123 H12F 0.9800 . ?
C31 H31 0.9500 . ?
C31 C125 1.3900 . ?
C31 C129 1.3900 . ?
C125 H125 0.9500 . ?
C125 C63 1.3900 . ?
C63 H63 0.9500 . ?
C63 C127 1.3900 . ?
C127 C2 1.3900 . ?
C127 O11 1.3997(10) . ?
C2 H2 0.9500 . ?
C2 C129 1.3900 . ?
C129 P2 1.879(11) . ?
O5 C151 1.335(10) . ?
O5 C77 1.509(14) . ?
C65 H65A 0.9800 . ?
C65 H65B 0.9800 . ?
C65 H65C 0.9800 . ?
C131 H131 0.9500 . ?
C131 C33 1.3900 . ?
C131 C17 1.3900 . ?
C33 C133 1.3900 . ?
C133 H133 0.9500 . ?
C133 C67 1.3900 . ?
C67 C135 1.3900 . ?
C67 P2 1.781(16) . ?
C135 H135 0.9500 . ?
C135 C17 1.3900 . ?
C17 H17 0.9500 . ?
C137 H13A 0.9800 . ?
C137 H13B 0.9800 . ?
C137 H13C 0.9800 . ?
C69 H69A 0.9800 . ?
C69 H69B 0.9800 . ?
C69 H69C 0.9800 . ?
O11 C73 1.4497(10) . ?
C139 C35 1.3900 . ?
C139 C9 1.3900 . ?
C35 C141 1.3900 . ?
C141 C71 1.3900 . ?
C71 C143 1.3900 . ?
C143 C9 1.3900 . ?
C145 H14A 0.9800 . ?
C145 H14B 0.9800 . ?
C145 H14C 0.9800 . ?
C73 H73A 0.9800 . ?
C73 H73B 0.9800 . ?
C73 H73C 0.9800 . ?
C147 C37 1.3900 . ?
C147 C19 1.3900 . ?
C147 P2 1.724(11) . ?
C37 H37 0.9500 . ?
C37 C149 1.3900 . ?
C149 H149 0.9500 . ?
C149 C75 1.3900 . ?
C75 H75 0.9500 . ?
C75 C151 1.3900 . ?
C151 C19 1.3900 . ?
C19 H19 0.9500 . ?
C153 H15A 0.9805 . ?
C153 H15B 0.9793 . ?
C153 H15C 0.9808 . ?
C77 H77A 0.9800 . ?
C77 H77B 0.9800 . ?
C77 H77C 0.9800 . ?
C155 H15D 0.9800 . ?
C155 H15E 0.9800 . ?
C155 H15F 0.9800 . ?
C39 H39 0.9500 . ?
C39 C157 1.3900 . ?
C39 C161 1.3900 . ?
C157 H157 0.9500 . ?
C157 C79 1.3900 . ?
C79 H79 0.9500 . ?
C79 C159 1.3900 . ?
C159 C5 1.3900 . ?
C159 O3 1.345(15) . ?
C5 H5 0.9500 . ?
C5 C161 1.3900 . ?
O3 C81 1.4500(10) . ?
C81 H81A 0.9800 . ?
C81 H81B 0.9800 . ?
C81 H81C 0.9800 . ?
O13 C163 1.4498(10) . ?
O13 C165 1.4000(10) . ?
C163 H16A 0.9805 . ?
C163 H16B 0.9801 . ?
C163 H16C 0.9794 . ?
C41 H41 0.9500 . ?
C41 C165 1.3900 . ?
C41 C169 1.3900 . ?
C165 C83 1.3900 . ?
C83 H83 0.9500 . ?
C83 C167 1.3900 . ?
C167 C21 1.3900 . ?
C21 H21 0.9500 . ?
C21 C169 1.3900 . ?
C169 H169 0.9500 . ?
O7 C85 1.44(3) . ?
O7 C11 1.4500(10) . ?
C85 C171 1.3900 . ?
C85 C175 1.3900 . ?
C171 H171 0.9500 . ?
C171 C43 1.3900 . ?
C43 C173 1.3900 . ?
C173 H173 0.9500 . ?
C173 C87 1.3900 . ?
C87 H87 0.9500 . ?
C87 C175 1.3900 . ?
C175 H175 0.9500 . ?
C11 H11A 0.9800 . ?
C11 H11B 0.9800 . ?
C11 H11C 0.9800 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Ag6 Ag1 Ag4 59.994(11) . . ?
Ag6 Ag1 Ag10 60.077(12) . . ?
Ag6 Ag1 Ag7 90.467(13) . . ?
Ag6 Ag1 Cu1 60.951(13) . . ?
Ag6 Ag1 Cu3 121.285(17) . . ?
Ag10 Ag1 Ag4 89.398(12) . . ?
Ag10 Ag1 Cu1 121.028(15) . . ?
Ag10 Ag1 Cu3 61.212(14) . . ?
Ag7 Ag1 Ag4 60.003(11) . . ?
Ag7 Ag1 Ag10 59.775(12) . . ?
Ag7 Ag1 Cu1 121.123(15) . . ?
Ag7 Ag1 Cu3 60.330(15) . . ?
Cu1 Ag1 Ag4 61.134(13) . . ?
Cu1 Ag1 Cu3 177.639(17) . . ?
Cu3 Ag1 Ag4 120.328(16) . . ?
S1 Ag1 Ag4 108.58(3) . . ?
S1 Ag1 Ag6 73.31(2) . . ?
S1 Ag1 Ag10 111.28(3) . . ?
S1 Ag1 Ag7 163.69(3) . . ?
S1 Ag1 Cu1 49.39(3) . . ?
S1 Ag1 Cu3 129.73(3) . . ?
S8 Ag1 Ag4 111.07(3) . . ?
S8 Ag1 Ag6 164.29(3) . . ?
S8 Ag1 Ag10 109.21(3) . . ?
S8 Ag1 Ag7 73.87(3) . . ?
S8 Ag1 Cu1 128.33(3) . . ?
S8 Ag1 Cu3 49.72(3) . . ?
S8 Ag1 S1 122.38(4) . . ?
Ag1 Ag4 Ag3 126.178(14) . . ?
Ag1 Ag4 Cu1 59.156(13) . . ?
Ag6 Ag4 Ag1 58.952(11) . . ?
Ag6 Ag4 Ag3 67.559(11) . . ?
Ag6 Ag4 Ag7 89.494(13) . . ?
Ag6 Ag4 Cu1 59.919(13) . . ?
Ag6 Ag4 Cu4 122.880(17) . . ?
Ag8 Ag4 Ag1 90.109(12) . . ?
Ag8 Ag4 Ag6 60.548(12) . . ?
Ag8 Ag4 Ag3 67.690(11) . . ?
Ag8 Ag4 Ag7 60.678(12) . . ?
Ag8 Ag4 Cu1 120.467(16) . . ?
Ag8 Ag4 Cu4 62.382(15) . . ?
Ag7 Ag4 Ag1 59.387(11) . . ?
Ag7 Ag4 Ag3 128.240(14) . . ?
Ag7 Ag4 Cu1 118.529(15) . . ?
Cu1 Ag4 Ag3 89.984(14) . . ?
Cu4 Ag4 Ag1 119.693(16) . . ?
Cu4 Ag4 Ag3 93.249(15) . . ?
Cu4 Ag4 Ag7 60.357(14) . . ?
Cu4 Ag4 Cu1 176.411(18) . . ?
S4 Ag4 Ag1 71.29(3) . . ?
S4 Ag4 Ag6 106.68(3) . . ?
S4 Ag4 Ag8 161.36(3) . . ?
S4 Ag4 Ag3 122.23(3) . . ?
S4 Ag4 Ag7 108.40(3) . . ?
S4 Ag4 Cu1 48.88(3) . . ?
S4 Ag4 Cu4 127.72(3) . . ?
S4 Ag4 S12 124.11(4) . . ?
S12 Ag4 Ag1 164.22(3) . . ?
S12 Ag4 Ag6 114.15(3) . . ?
S12 Ag4 Ag8 74.53(3) . . ?
S12 Ag4 Ag3 51.37(3) . . ?
S12 Ag4 Ag7 108.44(3) . . ?
S12 Ag4 Cu1 132.09(3) . . ?
S12 Ag4 Cu4 49.86(3) . . ?
Ag1 Ag6 Ag4 61.053(11) . . ?
Ag1 Ag6 Ag8 90.554(14) . . ?
Ag1 Ag6 Ag10 60.491(12) . . ?
Ag1 Ag6 Cu1 60.278(13) . . ?
Ag1 Ag6 Cu2 121.648(18) . . ?
Ag4 Ag6 Ag8 59.206(11) . . ?
Ag4 Ag6 Cu1 61.261(13) . . ?
Ag8 Ag6 Cu1 120.467(16) . . ?
Ag10 Ag6 Ag4 90.233(14) . . ?
Ag10 Ag6 Ag8 60.167(12) . . ?
Ag10 Ag6 Cu1 120.769(15) . . ?
Ag10 Ag6 Cu2 61.164(15) . . ?
Cu2 Ag6 Ag4 120.219(18) . . ?
Cu2 Ag6 Ag8 61.037(15) . . ?
Cu2 Ag6 Cu1 177.86(2) . . ?
S6 Ag6 Ag1 107.97(3) . . ?
S6 Ag6 Ag4 73.31(3) . . ?
S6 Ag6 Ag8 110.86(3) . . ?
S6 Ag6 Ag10 163.40(3) . . ?
S6 Ag6 Cu1 49.34(2) . . ?
S6 Ag6 Cu2 129.05(3) . . ?
S6 Ag6 S3 122.86(4) . . ?
S3 Ag6 Ag1 110.58(3) . . ?
S3 Ag6 Ag4 163.78(3) . . ?
S3 Ag6 Ag8 109.25(3) . . ?
S3 Ag6 Ag10 73.66(3) . . ?
S3 Ag6 Cu1 128.81(3) . . ?
S3 Ag6 Cu2 50.18(3) . . ?
Ag4 Ag8 Ag6 60.247(11) . . ?
Ag4 Ag8 Ag10 90.488(12) . . ?
Ag4 Ag8 Ag7 60.396(11) . . ?
Ag4 Ag8 Cu4 59.388(14) . . ?
Ag4 Ag8 Cu2 119.360(17) . . ?
Ag4 Ag8 Ag5 126.04(9) . . ?
Ag6 Ag8 Ag7 89.167(13) . . ?
Ag6 Ag8 Cu4 119.589(16) . . ?
Ag6 Ag8 Cu2 59.136(14) . . ?
Ag6 Ag8 Ag5 123.21(6) . . ?
Ag10 Ag8 Ag6 59.563(11) . . ?
Ag10 Ag8 Ag7 59.412(12) . . ?
Ag10 Ag8 Cu4 118.698(16) . . ?
Ag10 Ag8 Cu2 60.312(14) . . ?
Ag10 Ag8 Ag5 63.86(6) . . ?
Ag7 Ag8 Cu4 59.287(14) . . ?
Ag7 Ag8 Cu2 119.710(16) . . ?
Ag7 Ag8 Ag5 65.73(9) . . ?
Cu4 Ag8 Ag5 91.05(10) . . ?
Cu2 Ag8 Cu4 178.598(18) . . ?
Cu2 Ag8 Ag5 89.32(10) . . ?
S10 Ag8 Ag4 109.43(3) . . ?
S10 Ag8 Ag6 72.31(3) . . ?
S10 Ag8 Ag10 107.72(3) . . ?
S10 Ag8 Ag7 161.41(3) . . ?
S10 Ag8 Cu4 131.50(3) . . ?
S10 Ag8 Cu2 49.14(3) . . ?
S10 Ag8 Ag5 123.06(10) . . ?
S9 Ag8 Ag4 106.97(3) . . ?
S9 Ag8 Ag6 161.32(3) . . ?
S9 Ag8 Ag10 110.04(3) . . ?
S9 Ag8 Ag7 72.25(3) . . ?
S9 Ag8 Cu4 49.06(3) . . ?
S9 Ag8 Cu2 131.97(3) . . ?
S9 Ag8 S10 126.31(4) . . ?
S9 Ag8 Ag5 51.02(8) . . ?
Ag1 Ag10 Ag8 90.003(13) . . ?
Ag1 Ag10 Cu2 118.845(17) . . ?
Ag1 Ag10 Cu3 59.646(14) . . ?
Ag1 Ag10 Ag5 126.47(10) . . ?
Ag6 Ag10 Ag1 59.432(11) . . ?
Ag6 Ag10 Ag8 60.270(11) . . ?
Ag6 Ag10 Cu2 59.420(14) . . ?
Ag6 Ag10 Cu3 119.073(16) . . ?
Ag6 Ag10 Ag5 125.02(8) . . ?
Ag8 Ag10 Cu2 60.486(14) . . ?
Ag8 Ag10 Cu3 120.430(19) . . ?
Ag8 Ag10 Ag5 64.98(8) . . ?
Ag7 Ag10 Ag1 60.021(12) . . ?
Ag7 Ag10 Ag6 90.234(13) . . ?
Ag7 Ag10 Ag8 60.558(12) . . ?
Ag7 Ag10 Cu2 121.029(17) . . ?
Ag7 Ag10 Cu3 59.878(15) . . ?
Ag7 Ag10 Ag5 66.50(10) . . ?
Cu2 Ag10 Cu3 177.88(2) . . ?
Cu2 Ag10 Ag5 90.02(10) . . ?
Cu3 Ag10 Ag5 92.10(10) . . ?
S2 Ag10 Ag1 73.59(3) . . ?
S2 Ag10 Ag6 110.77(3) . . ?
S2 Ag10 Ag8 163.48(3) . . ?
S2 Ag10 Ag7 107.88(3) . . ?
S2 Ag10 Cu2 129.20(4) . . ?
S2 Ag10 Cu3 49.38(4) . . ?
S2 Ag10 Ag5 123.45(9) . . ?
S5 Ag10 Ag1 163.04(3) . . ?
S5 Ag10 Ag6 107.21(3) . . ?
S5 Ag10 Ag8 73.57(3) . . ?
S5 Ag10 Ag7 112.95(4) . . ?
S5 Ag10 Cu2 49.27(4) . . ?
S5 Ag10 Cu3 132.57(4) . . ?
S5 Ag10 S2 122.93(4) . . ?
S5 Ag10 Ag5 50.27(11) . . ?
S4 Ag11 S8 100.25(4) . . ?
S4 Ag11 S7 101.34(4) . . ?
P4 Ag11 S4 116.70(4) . . ?
P4 Ag11 S8 116.34(4) . . ?
P4 Ag11 S7 118.62(4) . . ?
S7 Ag11 S8 100.56(4) . . ?
S6 Ag3 Ag4 63.96(2) . . ?
S6 Ag3 S10 101.20(3) . . ?
S6 Ag3 S12 107.81(3) . . ?
S10 Ag3 Ag4 92.48(3) . . ?
S12 Ag3 Ag4 48.51(2) . . ?
S12 Ag3 S10 103.81(4) . . ?
P1 Ag3 Ag4 151.82(3) . . ?
P1 Ag3 S6 118.50(4) . . ?
P1 Ag3 S10 113.23(4) . . ?
P1 Ag3 S12 110.94(4) . . ?
Ag1 Ag7 Ag4 60.610(11) . . ?
Ag1 Ag7 Ag8 89.806(14) . . ?
Ag1 Ag7 Cu4 120.244(16) . . ?
Ag1 Ag7 Cu3 60.182(14) . . ?
Ag4 Ag7 Ag8 58.926(11) . . ?
Ag4 Ag7 Cu4 59.685(14) . . ?
Ag4 Ag7 Cu3 120.788(17) . . ?
Ag8 Ag7 Cu4 61.541(15) . . ?
Ag10 Ag7 Ag1 60.204(12) . . ?
Ag10 Ag7 Ag4 89.990(14) . . ?
Ag10 Ag7 Ag8 60.031(12) . . ?
Ag10 Ag7 Cu4 121.572(17) . . ?
Ag10 Ag7 Cu3 61.306(15) . . ?
Cu3 Ag7 Ag8 121.331(19) . . ?
Cu3 Ag7 Cu4 177.07(2) . . ?
S7 Ag7 Ag1 109.64(3) . . ?
S7 Ag7 Ag4 73.33(3) . . ?
S7 Ag7 Ag8 109.23(3) . . ?
S7 Ag7 Ag10 163.32(3) . . ?
S7 Ag7 Cu4 49.65(3) . . ?
S7 Ag7 Cu3 127.44(3) . . ?
S11 Ag7 Ag1 107.90(3) . . ?
S11 Ag7 Ag4 162.98(4) . . ?
S11 Ag7 Ag8 111.37(3) . . ?
S11 Ag7 Ag10 73.05(4) . . ?
S11 Ag7 Cu4 130.67(3) . . ?
S11 Ag7 Cu3 49.73(3) . . ?
S11 Ag7 S7 123.62(5) . . ?
S1 Ag2 S3 102.48(3) . . ?
S1 Ag2 S2 105.30(4) . . ?
S2 Ag2 S3 102.81(4) . . ?
P5 Ag2 S1 112.35(4) . . ?
P5 Ag2 S3 119.64(4) . . ?
P5 Ag2 S2 112.74(4) . . ?
S9 Ag9 S5 102.14(14) . . ?
S11 Ag9 S9 103.89(14) . . ?
S11 Ag9 S5 103.19(11) . . ?
P2 Ag9 S9 115.6(3) . . ?
P2 Ag9 S5 113.7(3) . . ?
P2 Ag9 S11 116.5(3) . . ?
Ag1 Cu1 Ag4 59.710(13) . . ?
Ag1 Cu1 Ag6 58.772(13) . . ?
Ag6 Cu1 Ag4 58.820(13) . . ?
S1 Cu1 Ag1 58.15(3) . . ?
S1 Cu1 Ag4 115.61(3) . . ?
S1 Cu1 Ag6 76.00(3) . . ?
S1 Cu1 S4 118.24(4) . . ?
S1 Cu1 S6 116.89(4) . . ?
S4 Cu1 Ag1 74.94(3) . . ?
S4 Cu1 Ag4 56.54(3) . . ?
S4 Cu1 Ag6 112.94(3) . . ?
S6 Cu1 Ag1 114.17(3) . . ?
S6 Cu1 Ag4 75.42(3) . . ?
S6 Cu1 Ag6 57.29(3) . . ?
S6 Cu1 S4 117.85(4) . . ?
Ag4 Cu4 Ag8 58.230(14) . . ?
Ag4 Cu4 Ag7 59.958(14) . . ?
Ag7 Cu4 Ag8 59.172(14) . . ?
S12 Cu4 Ag4 58.15(3) . . ?
S12 Cu4 Ag8 75.90(3) . . ?
S12 Cu4 Ag7 116.03(4) . . ?
S12 Cu4 S7 119.22(5) . . ?
S12 Cu4 S9 115.79(5) . . ?
S7 Cu4 Ag4 77.21(3) . . ?
S7 Cu4 Ag8 114.86(4) . . ?
S7 Cu4 Ag7 57.92(3) . . ?
S7 Cu4 S9 118.77(5) . . ?
S9 Cu4 Ag4 113.05(4) . . ?
S9 Cu4 Ag8 56.50(4) . . ?
S9 Cu4 Ag7 75.52(3) . . ?
Ag6 Cu2 Ag8 59.826(14) . . ?
Ag6 Cu2 Ag10 59.416(14) . . ?
Ag10 Cu2 Ag8 59.202(15) . . ?
S10 Cu2 Ag6 76.47(3) . . ?
S10 Cu2 Ag8 57.55(3) . . ?
S10 Cu2 Ag10 114.74(4) . . ?
S10 Cu2 S3 119.26(5) . . ?
S3 Cu2 Ag6 58.29(3) . . ?
S3 Cu2 Ag8 115.86(3) . . ?
S3 Cu2 Ag10 76.27(3) . . ?
S5 Cu2 Ag6 115.00(4) . . ?
S5 Cu2 Ag8 76.46(4) . . ?
S5 Cu2 Ag10 57.32(3) . . ?
S5 Cu2 S10 118.44(5) . . ?
S5 Cu2 S3 116.55(5) . . ?
Ag1 Cu3 Ag10 59.142(14) . . ?
Ag1 Cu3 Ag7 59.488(13) . . ?
Ag7 Cu3 Ag10 58.815(14) . . ?
S8 Cu3 Ag1 57.69(3) . . ?
S8 Cu3 Ag10 114.88(3) . . ?
S8 Cu3 Ag7 77.00(3) . . ?
S8 Cu3 S2 119.01(5) . . ?
S8 Cu3 S11 119.80(6) . . ?
S2 Cu3 Ag1 76.73(4) . . ?
S2 Cu3 Ag10 56.86(3) . . ?
S2 Cu3 Ag7 114.09(4) . . ?
S11 Cu3 Ag1 115.13(4) . . ?
S11 Cu3 Ag10 75.28(4) . . ?
S11 Cu3 Ag7 57.98(3) . . ?
S11 Cu3 S2 115.06(5) . . ?
Ag1 S1 Ag2 83.43(3) . . ?
Cu1 S1 Ag1 72.46(3) . . ?
Cu1 S1 Ag2 132.84(4) . . ?
C6 S1 Ag1 108.18(10) . . ?
C6 S1 Ag2 111.76(9) . . ?
C6 S1 Cu1 114.05(9) . . ?
Ag4 S4 Ag11 88.68(3) . . ?
Cu1 S4 Ag4 74.58(3) . . ?
Cu1 S4 Ag11 136.05(5) . . ?
C14 S4 Ag4 116.30(10) . . ?
C14 S4 Ag11 112.36(10) . . ?
C14 S4 Cu1 111.50(10) . . ?
Ag6 S6 Ag3 84.91(3) . . ?
Cu1 S6 Ag6 73.37(3) . . ?
Cu1 S6 Ag3 130.31(5) . . ?
C97 S6 Ag6 112.08(12) . . ?
C97 S6 Ag3 114.46(10) . . ?
C97 S6 Cu1 115.07(10) . . ?
Ag1 S8 Ag11 86.05(3) . . ?
Cu3 S8 Ag1 72.58(4) . . ?
Cu3 S8 Ag11 133.34(5) . . ?
C47 S8 Ag1 112.13(11) . . ?
C47 S8 Ag11 113.39(11) . . ?
C47 S8 Cu3 113.04(11) . . ?
Ag8 S10 Ag3 82.92(4) . . ?
Cu2 S10 Ag8 73.31(4) . . ?
Cu2 S10 Ag3 131.33(4) . . ?
C26 S10 Ag8 108.95(13) . . ?
C26 S10 Ag3 114.95(10) . . ?
C26 S10 Cu2 112.80(11) . . ?
Ag4 S12 Ag3 80.12(3) . . ?
Cu4 S12 Ag4 71.99(3) . . ?
Cu4 S12 Ag3 131.85(5) . . ?
C166 S12 Ag4 106.92(11) . . ?
C166 S12 Ag3 112.72(12) . . ?
C166 S12 Cu4 112.58(12) . . ?
Ag6 S3 Ag2 84.28(4) . . ?
Cu2 S3 Ag6 71.53(4) . . ?
Cu2 S3 Ag2 132.13(6) . . ?
C146 S3 Ag6 108.52(12) . . ?
C146 S3 Ag2 114.04(11) . . ?
C146 S3 Cu2 112.64(11) . . ?
C50 P1 Ag3 115.45(12) . . ?
C90 P1 Ag3 112.60(11) . . ?
C90 P1 C50 106.20(16) . . ?
C90 P1 C122 105.93(14) . . ?
C122 P1 Ag3 111.99(12) . . ?
C122 P1 C50 103.85(17) . . ?
C38 P4 Ag11 115.01(11) . . ?
C38 P4 C62 105.10(14) . . ?
C38 P4 C98 105.79(17) . . ?
C62 P4 Ag11 110.53(11) . . ?
C98 P4 Ag11 112.26(12) . . ?
C98 P4 C62 107.65(14) . . ?
Ag7 S7 Ag11 87.33(4) . . ?
Cu4 S7 Ag11 133.20(5) . . ?
Cu4 S7 Ag7 72.43(4) . . ?
C15 S7 Ag11 113.80(12) . . ?
C15 S7 Ag7 114.77(14) . . ?
C15 S7 Cu4 112.99(12) . . ?
Ag10 S2 Ag2 84.86(4) . . ?
Cu3 S2 Ag10 73.76(4) . . ?
Cu3 S2 Ag2 130.27(5) . . ?
C172 S2 Ag10 111.00(13) . . ?
C172 S2 Ag2 114.38(16) . . ?
C172 S2 Cu3 115.14(16) . . ?
C84 P5 Ag2 110.66(11) . . ?
C110 P5 Ag2 112.88(13) . . ?
C110 P5 C84 106.50(16) . . ?
C110 P5 C134 106.82(15) . . ?
C134 P5 Ag2 113.97(11) . . ?
C134 P5 C84 105.46(16) . . ?
Ag8 S9 Ag9 84.54(9) . . ?
Ag8 S9 Ag5 80.02(13) . . ?
Cu4 S9 Ag8 74.45(4) . . ?
Cu4 S9 Ag9 131.58(9) . . ?
Cu4 S9 Ag5 130.49(11) . . ?
C51 S9 Ag8 112.03(13) . . ?
C51 S9 Ag9 114.90(15) . . ?
C51 S9 Cu4 113.37(13) . . ?
C51 S9 Ag5 115.38(16) . . ?
Ag10 S5 Ag9 81.59(8) . . ?
Ag10 S5 Ag5 80.29(11) . . ?
Cu2 S5 Ag10 73.41(4) . . ?
Cu2 S5 Ag9 131.26(9) . . ?
Cu2 S5 Ag5 128.94(12) . . ?
C27 S5 Ag10 110.62(13) . . ?
C27 S5 Ag9 115.35(18) . . ?
C27 S5 Cu2 112.46(17) . . ?
C27 S5 Ag5 117.6(2) . . ?
Ag7 S11 Ag9 83.57(9) . . ?
Ag7 S11 Ag5 80.68(12) . . ?
Cu3 S11 Ag7 72.29(4) . . ?
Cu3 S11 Ag9 132.91(11) . . ?
Cu3 S11 Ag5 128.26(14) . . ?
C143 S11 Ag7 108.51(15) . . ?
C143 S11 Ag9 113.06(17) . . ?
C143 S11 Cu3 112.76(14) . . ?
C143 S11 Ag5 117.41(18) . . ?
C161 P3 Ag5 119.8(9) . . ?
C167 P3 C161 98.7(11) . . ?
C167 P3 C43 107.1(13) . . ?
C167 P3 Ag5 115.9(10) . . ?
C43 P3 C161 101.0(11) . . ?
C43 P3 Ag5 112.4(9) . . ?
C42 O1 C57 117.0(3) . . ?
C70 O4 C121 118.4(4) . . ?
C86 O6 C123 117.4(4) . . ?
C138 O8 C145 117.8(4) . . ?
C76 O10 C61 117.4(4) . . ?
C114 O12 C137 117.7(4) . . ?
F1 C1 C4 119.3(2) . . ?
F1 C1 C12 120.7(2) . . ?
C4 C1 C12 120.0 . . ?
F4 C4 C1 118.08(19) . . ?
F4 C4 C6 121.90(19) . . ?
C1 C4 C6 120.0 . . ?
C4 C6 S1 120.26(14) . . ?
C4 C6 C8 120.0 . . ?
C8 C6 S1 119.16(15) . . ?
F10 C8 C6 121.9(2) . . ?
F10 C8 C10 118.1(2) . . ?
C10 C8 C6 120.0 . . ?
F24 C10 C8 120.5(2) . . ?
F24 C10 C12 119.5(2) . . ?
C8 C10 C12 120.0 . . ?
F22 C12 C1 119.6(2) . . ?
F22 C12 C10 120.4(2) . . ?
C10 C12 C1 120.0 . . ?
C16 C14 S4 118.39(16) . . ?
C16 C14 C24 120.0 . . ?
C24 C14 S4 120.89(16) . . ?
F6 C16 C14 122.2(2) . . ?
F6 C16 C18 117.8(2) . . ?
C18 C16 C14 120.0 . . ?
F38 C18 C16 120.2(3) . . ?
F38 C18 C20 119.8(3) . . ?
C16 C18 C20 120.0 . . ?
F50 C20 C18 119.6(3) . . ?
F50 C20 C22 120.4(3) . . ?
C18 C20 C22 120.0 . . ?
F40 C22 C20 120.3(3) . . ?
F40 C22 C24 119.7(3) . . ?
C20 C22 C24 120.0 . . ?
F14 C24 C14 121.5(2) . . ?
F14 C24 C22 118.5(2) . . ?
C22 C24 C14 120.0 . . ?
C102 O14 C69 116.5(3) . . ?
C28 C26 S10 120.06(17) . . ?
C28 C26 C36 120.0 . . ?
C36 C26 S10 119.69(16) . . ?
F30 C28 C26 121.5(2) . . ?
F30 C28 C30 118.5(2) . . ?
C30 C28 C26 120.0 . . ?
F31 C30 C28 120.2(3) . . ?
F31 C30 C32 119.8(3) . . ?
C28 C30 C32 120.0 . . ?
F15 C32 C30 119.8(3) . . ?
F15 C32 C34 120.2(3) . . ?
C34 C32 C30 120.0 . . ?
F26 C34 C32 119.7(2) . . ?
F26 C34 C36 120.3(2) . . ?
C32 C34 C36 120.0 . . ?
F12 C36 C26 122.2(2) . . ?
F12 C36 C34 117.7(2) . . ?
C34 C36 C26 120.0 . . ?
C126 O15 C65 116.4(4) . . ?
C40 C38 P4 116.52(18) . . ?
C40 C38 C48 120.0 . . ?
C48 C38 P4 123.47(18) . . ?
C38 C40 H40 120.0 . . ?
C38 C40 C42 120.0 . . ?
C42 C40 H40 120.0 . . ?
O1 C42 C40 124.4(3) . . ?
O1 C42 C44 115.6(3) . . ?
C40 C42 C44 120.0 . . ?
C42 C44 H44 120.0 . . ?
C46 C44 C42 120.0 . . ?
C46 C44 H44 120.0 . . ?
C44 C46 H46 120.0 . . ?
C44 C46 C48 120.0 . . ?
C48 C46 H46 120.0 . . ?
C38 C48 H48 120.0 . . ?
C46 C48 C38 120.0 . . ?
C46 C48 H48 120.0 . . ?
C52 C50 P1 117.8(2) . . ?
C52 C50 C60 120.0 . . ?
C60 C50 P1 122.1(2) . . ?
C50 C52 H52 120.0 . . ?
C54 C52 C50 120.0 . . ?
C54 C52 H52 120.0 . . ?
C52 C54 C56 120.0 . . ?
O9 C54 C52 116.7(4) . . ?
O9 C54 C56 123.2(4) . . ?
C54 C56 H56 120.0 . . ?
C58 C56 C54 120.0 . . ?
C58 C56 H56 120.0 . . ?
C56 C58 H58 120.0 . . ?
C56 C58 C60 120.0 . . ?
C60 C58 H58 120.0 . . ?
C50 C60 H60 120.0 . . ?
C58 C60 C50 120.0 . . ?
C58 C60 H60 120.0 . . ?
C64 C62 P4 123.57(16) . . ?
C64 C62 C72 120.0 . . ?
C72 C62 P4 116.16(16) . . ?
C62 C64 H64 120.0 . . ?
C62 C64 C66 120.0 . . ?
C66 C64 H64 120.0 . . ?
C64 C66 H66 120.0 . . ?
C68 C66 C64 120.0 . . ?
C68 C66 H66 120.0 . . ?
C66 C68 H68 120.0 . . ?
C66 C68 C70 120.0 . . ?
C70 C68 H68 120.0 . . ?
O4 C70 C68 116.3(3) . . ?
O4 C70 C72 123.6(3) . . ?
C68 C70 C72 120.0 . . ?
C62 C72 H72 120.0 . . ?
C70 C72 C62 120.0 . . ?
C70 C72 H72 120.0 . . ?
C76 C74 H74 120.0 . . ?
C76 C74 C84 120.0 . . ?
C84 C74 H74 120.0 . . ?
O10 C76 C74 124.5(3) . . ?
O10 C76 C78 115.5(3) . . ?
C74 C76 C78 120.0 . . ?
C76 C78 H78 120.0 . . ?
C76 C78 C80 120.0 . . ?
C80 C78 H78 120.0 . . ?
C78 C80 H80 120.0 . . ?
C82 C80 C78 120.0 . . ?
C82 C80 H80 120.0 . . ?
C80 C82 H82 120.0 . . ?
C84 C82 C80 120.0 . . ?
C84 C82 H82 120.0 . . ?
C74 C84 P5 116.47(18) . . ?
C82 C84 P5 123.21(18) . . ?
C82 C84 C74 120.0 . . ?
O6 C86 C88 124.8(3) . . ?
O6 C86 C96 115.2(3) . . ?
C88 C86 C96 120.0 . . ?
C86 C88 H88 120.0 . . ?
C90 C88 C86 120.0 . . ?
C90 C88 H88 120.0 . . ?
C88 C90 P1 117.15(17) . . ?
C88 C90 C92 120.0 . . ?
C92 C90 P1 122.69(17) . . ?
C90 C92 H92 120.0 . . ?
C94 C92 C90 120.0 . . ?
C94 C92 H92 120.0 . . ?
C92 C94 H94 120.0 . . ?
C92 C94 C96 120.0 . . ?
C96 C94 H94 120.0 . . ?
C86 C96 H96 120.0 . . ?
C94 C96 C86 120.0 . . ?
C94 C96 H96 120.0 . . ?
C100 C98 P4 116.47(16) . . ?
C100 C98 C108 120.0 . . ?
C108 C98 P4 123.48(16) . . ?
C98 C100 H100 120.0 . . ?
C98 C100 C102 120.0 . . ?
C102 C100 H100 120.0 . . ?
O14 C102 C100 124.6(3) . . ?
O14 C102 C104 115.4(3) . . ?
C100 C102 C104 120.0 . . ?
C102 C104 H104 120.0 . . ?
C106 C104 C102 120.0 . . ?
C106 C104 H104 120.0 . . ?
C104 C106 H106 120.0 . . ?
C104 C106 C108 120.0 . . ?
C108 C106 H106 120.0 . . ?
C98 C108 H108 120.0 . . ?
C106 C108 C98 120.0 . . ?
C106 C108 H108 120.0 . . ?
C112 C110 P5 117.57(19) . . ?
C112 C110 C120 120.0 . . ?
C120 C110 P5 122.17(18) . . ?
C110 C112 H112 120.0 . . ?
C114 C112 C110 120.0 . . ?
C114 C112 H112 120.0 . . ?
O12 C114 C112 124.1(3) . . ?
O12 C114 C116 115.9(3) . . ?
C116 C114 C112 120.0 . . ?
C114 C116 H116 120.0 . . ?
C114 C116 C118 120.0 . . ?
C118 C116 H116 120.0 . . ?
C116 C118 H118 120.0 . . ?
C120 C118 C116 120.0 . . ?
C120 C118 H118 120.0 . . ?
C110 C120 H120 120.0 . . ?
C118 C120 C110 120.0 . . ?
C118 C120 H120 120.0 . . ?
C124 C122 P1 115.92(17) . . ?
C124 C122 C132 120.0 . . ?
C132 C122 P1 124.04(17) . . ?
C122 C124 H124 120.0 . . ?
C126 C124 C122 120.0 . . ?
C126 C124 H124 120.0 . . ?
O15 C126 C124 124.0(3) . . ?
O15 C126 C128 116.0(3) . . ?
C128 C126 C124 120.0 . . ?
C126 C128 H128 120.0 . . ?
C130 C128 C126 120.0 . . ?
C130 C128 H128 120.0 . . ?
C128 C130 H130 120.0 . . ?
C128 C130 C132 120.0 . . ?
C132 C130 H130 120.0 . . ?
C122 C132 H132 120.0 . . ?
C130 C132 C122 120.0 . . ?
C130 C132 H132 120.0 . . ?
C136 C134 P5 116.95(17) . . ?
C136 C134 C144 120.0 . . ?
C144 C134 P5 122.96(17) . . ?
C134 C136 H136 120.0 . . ?
C134 C136 C138 120.0 . . ?
C138 C136 H136 120.0 . . ?
O8 C138 C136 123.3(3) . . ?
O8 C138 C140 116.7(3) . . ?
C140 C138 C136 120.0 . . ?
C138 C140 H140 120.0 . . ?
C142 C140 C138 120.0 . . ?
C142 C140 H140 120.0 . . ?
C140 C142 H142 120.0 . . ?
C140 C142 C144 120.0 . . ?
C144 C142 H142 120.0 . . ?
C134 C144 H144 120.0 . . ?
C142 C144 C134 120.0 . . ?
C142 C144 H144 120.0 . . ?
C148 C146 S3 118.5(2) . . ?
C148 C146 C156 120.0 . . ?
C156 C146 S3 121.0(2) . . ?
F44 C148 C146 123.8(3) . . ?
F44 C148 C150 116.2(3) . . ?
C150 C148 C146 120.0 . . ?
F21 C150 C148 121.8(3) . . ?
F21 C150 C152 118.2(3) . . ?
C148 C150 C152 120.0 . . ?
C154 C152 C150 120.0 . . ?
F55 C152 C150 120.9(3) . . ?
F55 C152 C154 119.1(3) . . ?
F19 C154 C152 121.8(3) . . ?
F19 C154 C156 118.2(3) . . ?
C152 C154 C156 120.0 . . ?
F20 C156 C146 122.2(3) . . ?
F20 C156 C154 117.8(3) . . ?
C154 C156 C146 120.0 . . ?
F46 C158 C160 121.1(3) . . ?
F46 C158 C168 118.8(3) . . ?
C160 C158 C168 120.0 . . ?
F9 C160 C158 119.4(4) . . ?
F9 C160 C162 120.6(4) . . ?
C162 C160 C158 120.0 . . ?
F35 C162 C160 119.0(4) . . ?
F35 C162 C164 121.0(4) . . ?
C160 C162 C164 120.0 . . ?
F52 C164 C162 117.3(3) . . ?
F52 C164 C166 122.7(3) . . ?
C166 C164 C162 120.0 . . ?
C164 C166 S12 118.7(2) . . ?
C168 C166 S12 121.2(2) . . ?
C168 C166 C164 120.0 . . ?
F8 C168 C158 118.6(3) . . ?
F8 C168 C166 121.4(3) . . ?
C166 C168 C158 120.0 . . ?
F54 C170 C172 121.9(3) . . ?
F54 C170 C89 118.1(3) . . ?
C172 C170 C89 120.0 . . ?
C170 C172 S2 121.2(2) . . ?
C174 C172 S2 118.5(2) . . ?
C174 C172 C170 120.0 . . ?
F45 C174 C172 122.0(3) . . ?
F45 C174 C176 118.0(3) . . ?
C176 C174 C172 120.0 . . ?
C177 C176 C174 120.0 . . ?
F57 C176 C174 121.1(4) . . ?
F57 C176 C177 118.9(4) . . ?
C176 C177 C89 120.0 . . ?
F7 C177 C176 119.7(5) . . ?
F7 C177 C89 120.3(5) . . ?
F11 C89 C170 120.3(4) . . ?
F11 C89 C177 119.7(4) . . ?
C177 C89 C170 120.0 . . ?
F34 C45 C91 120.8(3) . . ?
F34 C45 C95 119.2(3) . . ?
C91 C45 C95 120.0 . . ?
F58 C91 C45 119.5(3) . . ?
F58 C91 C23 120.5(3) . . ?
C23 C91 C45 120.0 . . ?
F56 C23 C91 119.7(3) . . ?
F56 C23 C93 120.3(3) . . ?
C91 C23 C93 120.0 . . ?
F18 C93 C23 117.8(2) . . ?
F18 C93 C47 122.2(2) . . ?
C23 C93 C47 120.0 . . ?
C93 C47 S8 119.25(17) . . ?
C95 C47 S8 120.14(17) . . ?
C95 C47 C93 120.0 . . ?
F16 C95 C45 118.6(2) . . ?
F16 C95 C47 121.4(2) . . ?
C47 C95 C45 120.0 . . ?
F32 C3 C97 121.8(3) . . ?
F32 C3 C101 118.2(3) . . ?
C97 C3 C101 120.0 . . ?
C3 C97 S6 119.50(18) . . ?
C49 C97 S6 119.96(18) . . ?
C49 C97 C3 120.0 . . ?
F36 C49 C97 121.7(3) . . ?
F36 C49 C99 118.2(3) . . ?
C97 C49 C99 120.0 . . ?
F41 C99 C49 120.0(3) . . ?
F41 C99 C25 120.0(3) . . ?
C25 C99 C49 120.0 . . ?
F25 C25 C99 119.6(3) . . ?
F25 C25 C101 120.3(3) . . ?
C101 C25 C99 120.0 . . ?
F49 C101 C3 120.9(3) . . ?
F49 C101 C25 119.1(3) . . ?
C25 C101 C3 120.0 . . ?
C103 C51 S9 120.3(2) . . ?
C103 C51 C107 120.0 . . ?
C107 C51 S9 119.3(2) . . ?
F48 C103 C51 122.0(3) . . ?
F48 C103 C13 117.9(3) . . ?
C51 C103 C13 120.0 . . ?
F5 C13 C103 119.2(3) . . ?
F5 C13 C105 120.8(3) . . ?
C105 C13 C103 120.0 . . ?
F47 C105 C13 120.2(4) . . ?
F47 C105 C53 119.8(4) . . ?
C13 C105 C53 120.0 . . ?
F23 C53 C105 120.2(4) . . ?
F23 C53 C107 119.8(4) . . ?
C107 C53 C105 120.0 . . ?
F60 C107 C51 121.9(3) . . ?
F60 C107 C53 118.1(3) . . ?
C53 C107 C51 120.0 . . ?
C33 O2 C153 120.0(13) . . ?
C109 C27 S5 119.8(3) . . ?
C109 C27 C113 120.0 . . ?
C113 C27 S5 119.8(3) . . ?
F33 C109 C27 121.8(4) . . ?
F33 C109 C55 118.1(4) . . ?
C27 C109 C55 120.0 . . ?
F27 C55 C109 120.1(5) . . ?
F27 C55 C111 119.9(5) . . ?
C111 C55 C109 120.0 . . ?
C7 C111 C55 120.0 . . ?
F29 C111 C55 121.2(5) . . ?
F29 C111 C7 118.8(5) . . ?
F13 C7 C111 119.6(4) . . ?
F13 C7 C113 120.4(4) . . ?
C111 C7 C113 120.0 . . ?
F37 C113 C27 122.1(4) . . ?
F37 C113 C7 117.9(4) . . ?
C7 C113 C27 120.0 . . ?
O1 C57 H57A 109.5 . . ?
O1 C57 H57B 109.5 . . ?
O1 C57 H57C 109.5 . . ?
H57A C57 H57B 109.5 . . ?
H57A C57 H57C 109.5 . . ?
H57B C57 H57C 109.5 . . ?
F42 C115 C29 118.4(3) . . ?
F42 C115 C15 121.6(3) . . ?
C29 C115 C15 120.0 . . ?
F43 C29 C115 120.2(3) . . ?
F43 C29 C117 119.8(3) . . ?
C117 C29 C115 120.0 . . ?
F3 C117 C29 119.0(3) . . ?
F3 C117 C59 121.0(3) . . ?
C29 C117 C59 120.0 . . ?
F39 C59 C117 118.9(3) . . ?
F39 C59 C119 121.1(3) . . ?
C119 C59 C117 120.0 . . ?
F28 C119 C59 117.5(3) . . ?
F28 C119 C15 122.5(3) . . ?
C59 C119 C15 120.0 . . ?
C115 C15 S7 119.9(2) . . ?
C119 C15 S7 119.74(19) . . ?
C119 C15 C115 120.0 . . ?
C54 O9 C155 114.4(7) . . ?
O4 C121 H12A 109.5 . . ?
O4 C121 H12B 109.5 . . ?
O4 C121 H12C 109.5 . . ?
H12A C121 H12B 109.5 . . ?
H12A C121 H12C 109.5 . . ?
H12B C121 H12C 109.5 . . ?
O10 C61 H61A 109.5 . . ?
O10 C61 H61B 109.5 . . ?
O10 C61 H61C 109.5 . . ?
H61A C61 H61B 109.5 . . ?
H61A C61 H61C 109.5 . . ?
H61B C61 H61C 109.5 . . ?
O6 C123 H12D 109.5 . . ?
O6 C123 H12E 109.5 . . ?
O6 C123 H12F 109.5 . . ?
H12D C123 H12E 109.5 . . ?
H12D C123 H12F 109.5 . . ?
H12E C123 H12F 109.5 . . ?
C125 C31 H31 120.0 . . ?
C125 C31 C129 120.0 . . ?
C129 C31 H31 120.0 . . ?
C31 C125 H125 120.0 . . ?
C63 C125 C31 120.0 . . ?
C63 C125 H125 120.0 . . ?
C125 C63 H63 120.0 . . ?
C125 C63 C127 120.0 . . ?
C127 C63 H63 120.0 . . ?
C63 C127 O11 116.1(6) . . ?
C2 C127 C63 120.0 . . ?
C2 C127 O11 123.9(6) . . ?
C127 C2 H2 120.0 . . ?
C127 C2 C129 120.0 . . ?
C129 C2 H2 120.0 . . ?
C31 C129 P2 118.4(6) . . ?
C2 C129 C31 120.0 . . ?
C2 C129 P2 121.6(6) . . ?
C151 O5 C77 116.6(9) . . ?
O15 C65 H65A 109.5 . . ?
O15 C65 H65B 109.5 . . ?
O15 C65 H65C 109.5 . . ?
H65A C65 H65B 109.5 . . ?
H65A C65 H65C 109.5 . . ?
H65B C65 H65C 109.5 . . ?
C33 C131 H131 120.0 . . ?
C33 C131 C17 120.0 . . ?
C17 C131 H131 120.0 . . ?
O2 C33 C131 114.4(11) . . ?
O2 C33 C133 125.6(11) . . ?
C131 C33 C133 120.0 . . ?
C33 C133 H133 120.0 . . ?
C67 C133 C33 120.0 . . ?
C67 C133 H133 120.0 . . ?
C133 C67 C135 120.0 . . ?
C133 C67 P2 115.5(8) . . ?
C135 C67 P2 124.5(8) . . ?
C67 C135 H135 120.0 . . ?
C67 C135 C17 120.0 . . ?
C17 C135 H135 120.0 . . ?
C131 C17 H17 120.0 . . ?
C135 C17 C131 120.0 . . ?
C135 C17 H17 120.0 . . ?
O12 C137 H13A 109.5 . . ?
O12 C137 H13B 109.5 . . ?
O12 C137 H13C 109.5 . . ?
H13A C137 H13B 109.5 . . ?
H13A C137 H13C 109.5 . . ?
H13B C137 H13C 109.5 . . ?
O14 C69 H69A 109.5 . . ?
O14 C69 H69B 109.5 . . ?
O14 C69 H69C 109.5 . . ?
H69A C69 H69B 109.5 . . ?
H69A C69 H69C 109.5 . . ?
H69B C69 H69C 109.5 . . ?
C127 O11 C73 119.7(8) . . ?
F51 C139 C35 120.8(4) . . ?
F51 C139 C9 119.2(4) . . ?
C35 C139 C9 120.0 . . ?
F59 C35 C139 118.0(4) . . ?
F59 C35 C141 122.0(4) . . ?
C141 C35 C139 120.0 . . ?
F53 C141 C35 119.1(4) . . ?
F53 C141 C71 120.9(4) . . ?
C35 C141 C71 120.0 . . ?
F2 C71 C141 117.7(3) . . ?
F2 C71 C143 122.3(3) . . ?
C141 C71 C143 120.0 . . ?
C71 C143 S11 118.6(2) . . ?
C9 C143 S11 121.2(2) . . ?
C9 C143 C71 120.0 . . ?
F17 C9 C139 118.6(4) . . ?
F17 C9 C143 121.4(4) . . ?
C143 C9 C139 120.0 . . ?
O8 C145 H14A 109.5 . . ?
O8 C145 H14B 109.5 . . ?
O8 C145 H14C 109.5 . . ?
H14A C145 H14B 109.5 . . ?
H14A C145 H14C 109.5 . . ?
H14B C145 H14C 109.5 . . ?
O11 C73 H73A 109.5 . . ?
O11 C73 H73B 109.5 . . ?
O11 C73 H73C 109.5 . . ?
H73A C73 H73B 109.5 . . ?
H73A C73 H73C 109.5 . . ?
H73B C73 H73C 109.5 . . ?
C37 C147 C19 120.0 . . ?
C37 C147 P2 119.5(6) . . ?
C19 C147 P2 119.9(6) . . ?
C147 C37 H37 120.0 . . ?
C149 C37 C147 120.0 . . ?
C149 C37 H37 120.0 . . ?
C37 C149 H149 120.0 . . ?
C37 C149 C75 120.0 . . ?
C75 C149 H149 120.0 . . ?
C149 C75 H75 120.0 . . ?
C151 C75 C149 120.0 . . ?
C151 C75 H75 120.0 . . ?
O5 C151 C75 114.7(7) . . ?
O5 C151 C19 125.2(7) . . ?
C75 C151 C19 120.0 . . ?
C147 C19 H19 120.0 . . ?
C151 C19 C147 120.0 . . ?
C151 C19 H19 120.0 . . ?
O2 C153 H15A 109.0 . . ?
O2 C153 H15B 110.2 . . ?
O2 C153 H15C 109.2 . . ?
H15A C153 H15B 109.4 . . ?
H15A C153 H15C 109.4 . . ?
H15B C153 H15C 109.5 . . ?
O5 C77 H77A 109.5 . . ?
O5 C77 H77B 109.5 . . ?
O5 C77 H77C 109.5 . . ?
H77A C77 H77B 109.5 . . ?
H77A C77 H77C 109.5 . . ?
H77B C77 H77C 109.5 . . ?
O9 C155 H15D 109.5 . . ?
O9 C155 H15E 109.5 . . ?
O9 C155 H15F 109.5 . . ?
H15D C155 H15E 109.5 . . ?
H15D C155 H15F 109.5 . . ?
H15E C155 H15F 109.5 . . ?
C157 C39 H39 120.0 . . ?
C157 C39 C161 120.0 . . ?
C161 C39 H39 120.0 . . ?
C39 C157 H157 120.0 . . ?
C79 C157 C39 120.0 . . ?
C79 C157 H157 120.0 . . ?
C157 C79 H79 120.0 . . ?
C159 C79 C157 120.0 . . ?
C159 C79 H79 120.0 . . ?
C79 C159 C5 120.0 . . ?
O3 C159 C79 117.9(13) . . ?
O3 C159 C5 121.3(13) . . ?
C159 C5 H5 120.0 . . ?
C161 C5 C159 120.0 . . ?
C161 C5 H5 120.0 . . ?
C39 C161 P3 121.9(11) . . ?
C5 C161 P3 118.1(11) . . ?
C5 C161 C39 120.0 . . ?
C159 O3 C81 121.1(17) . . ?
O3 C81 H81A 109.5 . . ?
O3 C81 H81B 109.5 . . ?
O3 C81 H81C 109.5 . . ?
H81A C81 H81B 109.5 . . ?
H81A C81 H81C 109.5 . . ?
H81B C81 H81C 109.5 . . ?
C165 O13 C163 120.0(7) . . ?
O13 C163 H16A 108.2 . . ?
O13 C163 H16B 108.4 . . ?
O13 C163 H16C 111.8 . . ?
H16A C163 H16B 109.5 . . ?
H16A C163 H16C 109.5 . . ?
H16B C163 H16C 109.4 . . ?
C165 C41 H41 120.0 . . ?
C165 C41 C169 120.0 . . ?
C169 C41 H41 120.0 . . ?
C41 C165 O13 120.0(12) . . ?
C41 C165 C83 120.0 . . ?
C83 C165 O13 120.0(12) . . ?
C165 C83 H83 120.0 . . ?
C167 C83 C165 120.0 . . ?
C167 C83 H83 120.0 . . ?
C83 C167 P3 109.1(12) . . ?
C83 C167 C21 120.0 . . ?
C21 C167 P3 130.6(12) . . ?
C167 C21 H21 120.0 . . ?
C169 C21 C167 120.0 . . ?
C169 C21 H21 120.0 . . ?
C41 C169 H169 120.0 . . ?
C21 C169 C41 120.0 . . ?
C21 C169 H169 120.0 . . ?
C85 O7 C11 116(2) . . ?
C171 C85 O7 122.4(18) . . ?
C171 C85 C175 120.0 . . ?
C175 C85 O7 117.5(18) . . ?
C85 C171 H171 120.0 . . ?
C43 C171 C85 120.0 . . ?
C43 C171 H171 120.0 . . ?
C171 C43 P3 115.3(13) . . ?
C171 C43 C173 120.0 . . ?
C173 C43 P3 124.2(13) . . ?
C43 C173 H173 120.0 . . ?
C87 C173 C43 120.0 . . ?
C87 C173 H173 120.0 . . ?
C173 C87 H87 120.0 . . ?
C175 C87 C173 120.0 . . ?
C175 C87 H87 120.0 . . ?
C85 C175 H175 120.0 . . ?
C87 C175 C85 120.0 . . ?
C87 C175 H175 120.0 . . ?
O7 C11 H11A 109.5 . . ?
O7 C11 H11B 109.5 . . ?
O7 C11 H11C 109.5 . . ?
H11A C11 H11B 109.5 . . ?
H11A C11 H11C 109.5 . . ?
H11B C11 H11C 109.5 . . ?
C129 P2 Ag9 110.4(6) . . ?
C67 P2 Ag9 113.0(7) . . ?
C67 P2 C129 104.6(8) . . ?
C147 P2 Ag9 110.3(5) . . ?
C147 P2 C129 109.3(7) . . ?
C147 P2 C67 109.0(7) . . ?
Ag10 Ag5 Ag8 51.17(8) . . ?
S9 Ag5 Ag8 48.96(9) . . ?
S9 Ag5 Ag10 96.32(16) . . ?
S9 Ag5 S11 103.96(19) . . ?
S5 Ag5 Ag8 65.27(14) . . ?
S5 Ag5 Ag10 49.44(9) . . ?
S5 Ag5 S9 108.8(2) . . ?
S5 Ag5 S11 107.47(14) . . ?
S5 Ag5 P3 105.3(3) . . ?
S11 Ag5 Ag8 96.31(15) . . ?
S11 Ag5 Ag10 64.35(9) . . ?
P3 Ag5 Ag8 147.1(4) . . ?
P3 Ag5 Ag10 146.5(4) . . ?
P3 Ag5 S9 114.6(4) . . ?
P3 Ag5 S11 116.4(4) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Ag1 S1 C6 C4 68.58(16) . . . . ?
Ag1 S1 C6 C8 -120.16(14) . . . . ?
Ag1 S8 C47 C93 -114.73(15) . . . . ?
Ag1 S8 C47 C95 74.23(18) . . . . ?
Ag4 S4 C14 C16 -115.66(13) . . . . ?
Ag4 S4 C14 C24 74.01(16) . . . . ?
Ag4 S12 C166 C164 -120.70(15) . . . . ?
Ag4 S12 C166 C168 63.98(18) . . . . ?
Ag6 S6 C97 C3 -114.84(19) . . . . ?
Ag6 S6 C97 C49 73.6(2) . . . . ?
Ag6 S3 C146 C148 -112.74(19) . . . . ?
Ag6 S3 C146 C156 75.6(2) . . . . ?
Ag8 S10 C26 C28 -117.63(18) . . . . ?
Ag8 S10 C26 C36 68.1(2) . . . . ?
Ag8 S9 C51 C103 67.5(2) . . . . ?
Ag8 S9 C51 C107 -119.37(19) . . . . ?
Ag10 S2 C172 C170 74.2(3) . . . . ?
Ag10 S2 C172 C174 -112.3(2) . . . . ?
Ag10 S5 C27 C109 75.1(2) . . . . ?
Ag10 S5 C27 C113 -112.3(2) . . . . ?
Ag11 S4 C14 C16 144.24(12) . . . . ?
Ag11 S4 C14 C24 -26.09(17) . . . . ?
Ag11 S8 C47 C93 149.83(14) . . . . ?
Ag11 S8 C47 C95 -21.2(2) . . . . ?
Ag11 P4 C38 C40 -47.75(18) . . . . ?
Ag11 P4 C38 C48 131.13(15) . . . . ?
Ag11 P4 C62 C64 127.94(15) . . . . ?
Ag11 P4 C62 C72 -46.11(17) . . . . ?
Ag11 P4 C98 C100 -45.4(2) . . . . ?
Ag11 P4 C98 C108 132.1(2) . . . . ?
Ag11 S7 C15 C115 147.5(2) . . . . ?
Ag11 S7 C15 C119 -25.5(3) . . . . ?
Ag3 S6 C97 C3 150.61(17) . . . . ?
Ag3 S6 C97 C49 -20.9(2) . . . . ?
Ag3 S10 C26 C28 151.46(16) . . . . ?
Ag3 S10 C26 C36 -22.8(2) . . . . ?
Ag3 S12 C166 C164 153.15(13) . . . . ?
Ag3 S12 C166 C168 -22.17(19) . . . . ?
Ag3 P1 C50 C52 -32.6(3) . . . . ?
Ag3 P1 C50 C60 144.66(18) . . . . ?
Ag3 P1 C90 C88 -49.89(16) . . . . ?
Ag3 P1 C90 C92 125.49(14) . . . . ?
Ag3 P1 C122 C124 -52.8(2) . . . . ?
Ag3 P1 C122 C132 125.0(2) . . . . ?
Ag7 S7 C15 C115 -114.0(2) . . . . ?
Ag7 S7 C15 C119 72.9(2) . . . . ?
Ag7 S11 C143 C71 -117.0(2) . . . . ?
Ag7 S11 C143 C9 67.6(3) . . . . ?
Ag2 S1 C6 C4 -21.51(19) . . . . ?
Ag2 S1 C6 C8 149.75(13) . . . . ?
Ag2 S3 C146 C148 155.29(17) . . . . ?
Ag2 S3 C146 C156 -16.4(2) . . . . ?
Ag2 S2 C172 C170 -19.8(3) . . . . ?
Ag2 S2 C172 C174 153.7(2) . . . . ?
Ag2 P5 C84 C74 -41.57(19) . . . . ?
Ag2 P5 C84 C82 131.98(16) . . . . ?
Ag2 P5 C110 C112 -51.12(18) . . . . ?
Ag2 P5 C110 C120 122.92(17) . . . . ?
Ag2 P5 C134 C136 -50.5(2) . . . . ?
Ag2 P5 C134 C144 126.07(16) . . . . ?
Ag9 S9 C51 C103 -26.8(3) . . . . ?
Ag9 S9 C51 C107 146.4(2) . . . . ?
Ag9 S5 C27 C109 -15.2(3) . . . . ?
Ag9 S5 C27 C113 157.4(2) . . . . ?
Ag9 S11 C143 C71 152.2(2) . . . . ?
Ag9 S11 C143 C9 -23.2(3) . . . . ?
Cu1 S1 C6 C4 147.00(13) . . . . ?
Cu1 S1 C6 C8 -41.74(18) . . . . ?
Cu1 S4 C14 C16 -32.79(17) . . . . ?
Cu1 S4 C14 C24 156.88(12) . . . . ?
Cu1 S6 C97 C3 -33.5(2) . . . . ?
Cu1 S6 C97 C49 154.94(17) . . . . ?
Cu4 S12 C166 C164 -43.62(18) . . . . ?
Cu4 S12 C166 C168 141.06(15) . . . . ?
Cu4 S7 C15 C115 -33.6(3) . . . . ?
Cu4 S7 C15 C119 153.4(2) . . . . ?
Cu4 S9 C51 C103 149.42(18) . . . . ?
Cu4 S9 C51 C107 -37.4(2) . . . . ?
Cu2 S10 C26 C28 -38.3(2) . . . . ?
Cu2 S10 C26 C36 147.44(17) . . . . ?
Cu2 S3 C146 C148 -35.6(2) . . . . ?
Cu2 S3 C146 C156 152.71(18) . . . . ?
Cu2 S5 C27 C109 155.08(18) . . . . ?
Cu2 S5 C27 C113 -32.3(2) . . . . ?
Cu3 S8 C47 C93 -35.00(19) . . . . ?
Cu3 S8 C47 C95 153.96(14) . . . . ?
Cu3 S2 C172 C170 155.5(2) . . . . ?
Cu3 S2 C172 C174 -31.0(3) . . . . ?
Cu3 S11 C143 C71 -38.9(3) . . . . ?
Cu3 S11 C143 C9 145.7(2) . . . . ?
S1 C6 C8 F10 8.0(3) . . . . ?
S1 C6 C8 C10 -171.3(2) . . . . ?
S4 C14 C16 F6 9.4(3) . . . . ?
S4 C14 C16 C18 -170.4(2) . . . . ?
S4 C14 C24 F14 -11.6(3) . . . . ?
S4 C14 C24 C22 170.2(2) . . . . ?
S6 C97 C49 F36 -11.6(4) . . . . ?
S6 C97 C49 C99 171.5(3) . . . . ?
S8 C47 C95 F16 -10.9(3) . . . . ?
S8 C47 C95 C45 171.0(2) . . . . ?
S10 C26 C28 F30 4.3(4) . . . . ?
S10 C26 C28 C30 -174.2(3) . . . . ?
S10 C26 C36 F12 -8.9(3) . . . . ?
S10 C26 C36 C34 174.3(3) . . . . ?
S12 C166 C168 F8 -5.8(3) . . . . ?
S12 C166 C168 C158 175.3(2) . . . . ?
S3 C146 C148 F44 7.2(4) . . . . ?
S3 C146 C148 C150 -171.8(3) . . . . ?
S3 C146 C156 F20 -9.3(4) . . . . ?
S3 C146 C156 C154 171.6(3) . . . . ?
P1 C50 C52 C54 177.3(3) . . . . ?
P1 C50 C60 C58 -177.2(3) . . . . ?
P1 C90 C92 C94 -175.3(2) . . . . ?
P1 C122 C124 C126 177.9(3) . . . . ?
P1 C122 C132 C130 -177.7(3) . . . . ?
P4 C38 C40 C42 178.9(2) . . . . ?
P4 C38 C48 C46 -178.8(2) . . . . ?
P4 C62 C64 C66 -173.8(2) . . . . ?
P4 C62 C72 C70 174.3(2) . . . . ?
P4 C98 C100 C102 177.6(3) . . . . ?
P4 C98 C108 C106 -177.5(3) . . . . ?
S2 C172 C174 F45 6.2(5) . . . . ?
S2 C172 C174 C176 -173.6(3) . . . . ?
P5 C110 C112 C114 174.2(2) . . . . ?
P5 C110 C120 C118 -173.9(2) . . . . ?
P5 C134 C136 C138 176.7(2) . . . . ?
P5 C134 C144 C142 -176.5(2) . . . . ?
S9 C51 C103 F48 -9.1(4) . . . . ?
S9 C51 C103 C13 173.1(3) . . . . ?
S9 C51 C107 F60 6.0(4) . . . . ?
S9 C51 C107 C53 -173.2(3) . . . . ?
S5 C27 C109 F33 -10.5(4) . . . . ?
S5 C27 C109 C55 172.6(3) . . . . ?
S5 C27 C113 F37 7.1(4) . . . . ?
S5 C27 C113 C7 -172.6(3) . . . . ?
S11 C143 C9 F17 -6.2(4) . . . . ?
S11 C143 C9 C139 175.3(3) . . . . ?
P3 C167 C21 C169 -173(2) . . . . ?
P3 C43 C173 C87 -171.5(17) . . . . ?
F1 C1 C4 F4 1.8(3) . . . . ?
F1 C1 C4 C6 -179.7(3) . . . . ?
F1 C1 C12 F22 -1.6(3) . . . . ?
F1 C1 C12 C10 179.7(3) . . . . ?
F4 C4 C6 S1 -10.3(3) . . . . ?
F4 C4 C6 C8 178.5(3) . . . . ?
F6 C16 C18 F38 0.3(3) . . . . ?
F6 C16 C18 C20 -179.8(3) . . . . ?
F10 C8 C10 F24 2.0(3) . . . . ?
F10 C8 C10 C12 -179.3(3) . . . . ?
F18 C93 C47 S8 8.5(3) . . . . ?
F18 C93 C47 C95 179.5(3) . . . . ?
F24 C10 C12 F22 0.0(3) . . . . ?
F24 C10 C12 C1 178.7(3) . . . . ?
F26 C34 C36 F12 2.3(4) . . . . ?
F26 C34 C36 C26 179.3(4) . . . . ?
F28 C119 C15 S7 -8.0(4) . . . . ?
F28 C119 C15 C115 179.0(5) . . . . ?
F30 C28 C30 F31 2.6(4) . . . . ?
F30 C28 C30 C32 -178.6(4) . . . . ?
F32 C3 C97 S6 8.0(4) . . . . ?
F32 C3 C97 C49 179.6(4) . . . . ?
F32 C3 C101 F49 1.9(5) . . . . ?
F32 C3 C101 C25 -179.6(4) . . . . ?
F34 C45 C91 F58 1.6(3) . . . . ?
F34 C45 C91 C23 -179.3(3) . . . . ?
F34 C45 C95 F16 1.1(3) . . . . ?
F34 C45 C95 C47 179.3(3) . . . . ?
F36 C49 C99 F41 3.0(4) . . . . ?
F36 C49 C99 C25 -177.0(4) . . . . ?
F38 C18 C20 F50 -0.2(3) . . . . ?
F38 C18 C20 C22 179.9(3) . . . . ?
F40 C22 C24 F14 0.8(3) . . . . ?
F40 C22 C24 C14 179.1(3) . . . . ?
O1 C42 C44 C46 179.8(3) . . . . ?
F42 C115 C29 F43 0.3(5) . . . . ?
F42 C115 C29 C117 179.4(4) . . . . ?
F42 C115 C15 S7 7.6(4) . . . . ?
F42 C115 C15 C119 -179.3(5) . . . . ?
F44 C148 C150 F21 0.8(5) . . . . ?
F44 C148 C150 C152 -179.0(4) . . . . ?
F46 C158 C160 F9 3.1(3) . . . . ?
F46 C158 C160 C162 -176.5(3) . . . . ?
F46 C158 C168 F8 -2.4(3) . . . . ?
F46 C158 C168 C166 176.6(3) . . . . ?
F48 C103 C13 F5 1.5(4) . . . . ?
F48 C103 C13 C105 -177.9(4) . . . . ?
F50 C20 C22 F40 1.1(3) . . . . ?
F50 C20 C22 C24 -179.9(3) . . . . ?
F52 C164 C166 S12 5.2(3) . . . . ?
F52 C164 C166 C168 -179.5(3) . . . . ?
F54 C170 C172 S2 -7.6(4) . . . . ?
F54 C170 C172 C174 179.0(4) . . . . ?
F54 C170 C89 F11 2.0(5) . . . . ?
F54 C170 C89 C177 -179.0(4) . . . . ?
F56 C23 C93 F18 1.3(3) . . . . ?
F56 C23 C93 C47 -179.1(3) . . . . ?
F58 C91 C23 F56 -1.8(4) . . . . ?
F58 C91 C23 C93 179.1(3) . . . . ?
F15 C32 C34 F26 0.7(4) . . . . ?
F15 C32 C34 C36 -180.0(4) . . . . ?
O4 C70 C72 C62 -178.0(3) . . . . ?
F31 C30 C32 F15 -1.2(4) . . . . ?
F31 C30 C32 C34 178.8(4) . . . . ?
F2 C71 C143 S11 5.5(4) . . . . ?
F2 C71 C143 C9 -179.0(5) . . . . ?
F33 C109 C55 F27 2.7(5) . . . . ?
F33 C109 C55 C111 -177.0(4) . . . . ?
F35 C162 C164 F52 -1.1(4) . . . . ?
F35 C162 C164 C166 179.5(4) . . . . ?
O6 C86 C88 C90 179.2(3) . . . . ?
O6 C86 C96 C94 -179.2(3) . . . . ?
O8 C138 C140 C142 -179.7(3) . . . . ?
O10 C76 C78 C80 178.3(3) . . . . ?
F9 C160 C162 F35 0.9(4) . . . . ?
F9 C160 C162 C164 -179.6(3) . . . . ?
F19 C154 C156 F20 1.3(4) . . . . ?
F19 C154 C156 C146 -179.6(4) . . . . ?
F39 C59 C119 F28 1.6(5) . . . . ?
F39 C59 C119 C15 -179.4(5) . . . . ?
O12 C114 C116 C118 -179.2(3) . . . . ?
C1 C4 C6 S1 171.2(2) . . . . ?
C1 C4 C6 C8 0.0 . . . . ?
C4 C1 C12 F22 178.7(3) . . . . ?
C4 C1 C12 C10 0.0 . . . . ?
C4 C6 C8 F10 179.3(3) . . . . ?
C4 C6 C8 C10 0.0 . . . . ?
C6 C8 C10 F24 -178.7(3) . . . . ?
C6 C8 C10 C12 0.0 . . . . ?
C8 C10 C12 F22 -178.7(3) . . . . ?
C8 C10 C12 C1 0.0 . . . . ?
C12 C1 C4 F4 -178.6(3) . . . . ?
C12 C1 C4 C6 0.0 . . . . ?
F5 C13 C105 F47 -0.3(5) . . . . ?
F5 C13 C105 C53 -179.4(4) . . . . ?
F41 C99 C25 F25 2.5(5) . . . . ?
F41 C99 C25 C101 -180.0(4) . . . . ?
F21 C150 C152 C154 -179.9(5) . . . . ?
F21 C150 C152 F55 0.9(6) . . . . ?
F43 C29 C117 F3 -2.2(5) . . . . ?
F43 C29 C117 C59 179.1(5) . . . . ?
C14 C16 C18 F38 -179.9(3) . . . . ?
C14 C16 C18 C20 0.0 . . . . ?
C16 C14 C24 F14 178.3(3) . . . . ?
C16 C14 C24 C22 0.0 . . . . ?
C16 C18 C20 F50 179.9(3) . . . . ?
C16 C18 C20 C22 0.0 . . . . ?
C18 C20 C22 F40 -179.1(3) . . . . ?
C18 C20 C22 C24 0.0 . . . . ?
C20 C22 C24 F14 -178.3(3) . . . . ?
C20 C22 C24 C14 0.0 . . . . ?
C24 C14 C16 F6 179.8(3) . . . . ?
C24 C14 C16 C18 0.0 . . . . ?
O14 C102 C104 C106 -179.2(4) . . . . ?
F45 C174 C176 C177 -179.8(5) . . . . ?
F45 C174 C176 F57 1.9(6) . . . . ?
C26 C28 C30 F31 -178.8(4) . . . . ?
C26 C28 C30 C32 0.0 . . . . ?
C28 C26 C36 F12 176.9(4) . . . . ?
C28 C26 C36 C34 0.0 . . . . ?
C28 C30 C32 F15 180.0(4) . . . . ?
C28 C30 C32 C34 0.0 . . . . ?
C30 C32 C34 F26 -179.3(4) . . . . ?
C30 C32 C34 C36 0.0 . . . . ?
C32 C34 C36 F12 -177.0(3) . . . . ?
C32 C34 C36 C26 0.0 . . . . ?
C36 C26 C28 F30 178.5(4) . . . . ?
C36 C26 C28 C30 0.0 . . . . ?
O15 C126 C128 C130 179.7(4) . . . . ?
C38 P4 C62 C64 3.3(2) . . . . ?
C38 P4 C62 C72 -170.75(16) . . . . ?
C38 P4 C98 C100 80.8(2) . . . . ?
C38 P4 C98 C108 -101.7(2) . . . . ?
C38 C40 C42 O1 -179.8(3) . . . . ?
C38 C40 C42 C44 0.0 . . . . ?
C40 C38 C48 C46 0.0 . . . . ?
C40 C42 C44 C46 0.0 . . . . ?
C42 C44 C46 C48 0.0 . . . . ?
C44 C46 C48 C38 0.0 . . . . ?
C48 C38 C40 C42 0.0 . . . . ?
F23 C53 C107 F60 1.7(4) . . . . ?
F23 C53 C107 C51 -179.1(4) . . . . ?
F47 C105 C53 F23 0.0(5) . . . . ?
F47 C105 C53 C107 -179.1(4) . . . . ?
F3 C117 C59 F39 0.6(6) . . . . ?
F3 C117 C59 C119 -178.8(5) . . . . ?
C50 P1 C90 C88 -177.17(16) . . . . ?
C50 P1 C90 C92 -1.8(2) . . . . ?
C50 P1 C122 C124 72.4(2) . . . . ?
C50 P1 C122 C132 -109.7(2) . . . . ?
C50 C52 C54 C56 0.0 . . . . ?
C50 C52 C54 O9 -178.0(4) . . . . ?
C52 C50 C60 C58 0.0 . . . . ?
C52 C54 C56 C58 0.0 . . . . ?
C52 C54 O9 C155 178.0(6) . . . . ?
C54 C56 C58 C60 0.0 . . . . ?
C56 C54 O9 C155 0.1(8) . . . . ?
C56 C58 C60 C50 0.0 . . . . ?
C60 C50 C52 C54 0.0 . . . . ?
C62 P4 C38 C40 74.02(19) . . . . ?
C62 P4 C38 C48 -107.10(19) . . . . ?
C62 P4 C98 C100 -167.3(2) . . . . ?
C62 P4 C98 C108 10.3(3) . . . . ?
C62 C64 C66 C68 0.0 . . . . ?
C64 C62 C72 C70 0.0 . . . . ?
C64 C66 C68 C70 0.0 . . . . ?
C66 C68 C70 O4 178.1(3) . . . . ?
C66 C68 C70 C72 0.0 . . . . ?
C68 C70 C72 C62 0.0 . . . . ?
C72 C62 C64 C66 0.0 . . . . ?
C74 C76 C78 C80 0.0 . . . . ?
C76 C74 C84 P5 173.8(2) . . . . ?
C76 C74 C84 C82 0.0 . . . . ?
C76 C78 C80 C82 0.0 . . . . ?
C78 C80 C82 C84 0.0 . . . . ?
C80 C82 C84 P5 -173.3(2) . . . . ?
C80 C82 C84 C74 0.0 . . . . ?
C84 P5 C110 C112 -172.75(17) . . . . ?
C84 P5 C110 C120 1.3(2) . . . . ?
C84 P5 C134 C136 71.1(2) . . . . ?
C84 P5 C134 C144 -112.4(2) . . . . ?
C84 C74 C76 O10 -178.2(4) . . . . ?
C84 C74 C76 C78 0.0 . . . . ?
C86 C88 C90 P1 175.5(2) . . . . ?
C86 C88 C90 C92 0.0 . . . . ?
C88 C86 C96 C94 0.0 . . . . ?
C88 C90 C92 C94 0.0 . . . . ?
C90 P1 C50 C52 93.0(2) . . . . ?
C90 P1 C50 C60 -89.8(2) . . . . ?
C90 P1 C122 C124 -175.9(2) . . . . ?
C90 P1 C122 C132 1.9(3) . . . . ?
C90 C92 C94 C96 0.0 . . . . ?
C92 C94 C96 C86 0.0 . . . . ?
C96 C86 C88 C90 0.0 . . . . ?
F25 C25 C101 F49 -4.0(5) . . . . ?
F25 C25 C101 C3 177.5(5) . . . . ?
C98 P4 C38 C40 -172.24(16) . . . . ?
C98 P4 C38 C48 6.6(2) . . . . ?
C98 P4 C62 C64 -109.1(2) . . . . ?
C98 P4 C62 C72 76.8(2) . . . . ?
C98 C100 C102 O14 179.1(5) . . . . ?
C98 C100 C102 C104 0.0 . . . . ?
C100 C98 C108 C106 0.0 . . . . ?
C100 C102 C104 C106 0.0 . . . . ?
C102 C104 C106 C108 0.0 . . . . ?
C104 C106 C108 C98 0.0 . . . . ?
C108 C98 C100 C102 0.0 . . . . ?
C110 P5 C84 C74 81.5(2) . . . . ?
C110 P5 C84 C82 -105.0(2) . . . . ?
C110 P5 C134 C136 -175.87(18) . . . . ?
C110 P5 C134 C144 0.7(2) . . . . ?
C110 C112 C114 O12 179.1(4) . . . . ?
C110 C112 C114 C116 0.0 . . . . ?
C112 C110 C120 C118 0.0 . . . . ?
C112 C114 C116 C118 0.0 . . . . ?
C114 C116 C118 C120 0.0 . . . . ?
C116 C118 C120 C110 0.0 . . . . ?
C120 C110 C112 C114 0.0 . . . . ?
C122 P1 C50 C52 -155.6(2) . . . . ?
C122 P1 C50 C60 21.7(2) . . . . ?
C122 P1 C90 C88 72.83(19) . . . . ?
C122 P1 C90 C92 -111.79(19) . . . . ?
C122 C124 C126 O15 -179.7(5) . . . . ?
C122 C124 C126 C128 0.0 . . . . ?
C124 C122 C132 C130 0.0 . . . . ?
C124 C126 C128 C130 0.0 . . . . ?
C126 C128 C130 C132 0.0 . . . . ?
C128 C130 C132 C122 0.0 . . . . ?
C132 C122 C124 C126 0.0 . . . . ?
F51 C139 C35 F59 -0.6(6) . . . . ?
F51 C139 C35 C141 179.8(6) . . . . ?
F51 C139 C9 F17 1.7(5) . . . . ?
F51 C139 C9 C143 -179.8(5) . . . . ?
C134 P5 C84 C74 -165.26(17) . . . . ?
C134 P5 C84 C82 8.3(2) . . . . ?
C134 P5 C110 C112 74.9(2) . . . . ?
C134 P5 C110 C120 -111.0(2) . . . . ?
C134 C136 C138 O8 179.7(4) . . . . ?
C134 C136 C138 C140 0.0 . . . . ?
C136 C134 C144 C142 0.0 . . . . ?
C136 C138 C140 C142 0.0 . . . . ?
C138 C140 C142 C144 0.0 . . . . ?
C140 C142 C144 C134 0.0 . . . . ?
C144 C134 C136 C138 0.0 . . . . ?
C146 C148 C150 F21 179.9(5) . . . . ?
C146 C148 C150 C152 0.0 . . . . ?
C148 C146 C156 F20 179.1(4) . . . . ?
C148 C146 C156 C154 0.0 . . . . ?
C148 C150 C152 C154 0.0 . . . . ?
C148 C150 C152 F55 -179.3(6) . . . . ?
C150 C152 C154 F19 179.5(5) . . . . ?
C150 C152 C154 C156 0.0 . . . . ?
C152 C154 C156 F20 -179.1(4) . . . . ?
C152 C154 C156 C146 0.0 . . . . ?
C156 C146 C148 F44 179.0(4) . . . . ?
C156 C146 C148 C150 0.0 . . . . ?
C158 C160 C162 F35 -179.5(4) . . . . ?
C158 C160 C162 C164 0.0 . . . . ?
C160 C158 C168 F8 -179.0(3) . . . . ?
C160 C158 C168 C166 0.0 . . . . ?
C160 C162 C164 F52 179.5(3) . . . . ?
C160 C162 C164 C166 0.0 . . . . ?
C162 C164 C166 S12 -175.4(2) . . . . ?
C162 C164 C166 C168 0.0 . . . . ?
C164 C166 C168 F8 179.0(3) . . . . ?
C164 C166 C168 C158 0.0 . . . . ?
C168 C158 C160 F9 179.6(3) . . . . ?
C168 C158 C160 C162 0.0 . . . . ?
C170 C172 C174 F45 179.8(5) . . . . ?
C170 C172 C174 C176 0.0 . . . . ?
C172 C170 C89 F11 -178.9(4) . . . . ?
C172 C170 C89 C177 0.0 . . . . ?
C172 C174 C176 C177 0.0 . . . . ?
C172 C174 C176 F57 -178.3(6) . . . . ?
C174 C176 C177 C89 0.0 . . . . ?
C174 C176 C177 F7 -179.6(5) . . . . ?
C176 C177 C89 F11 178.9(4) . . . . ?
C176 C177 C89 C170 0.0 . . . . ?
C89 C170 C172 S2 173.4(3) . . . . ?
C89 C170 C172 C174 0.0 . . . . ?
C45 C91 C23 F56 179.2(3) . . . . ?
C45 C91 C23 C93 0.0 . . . . ?
C91 C45 C95 F16 -178.2(3) . . . . ?
C91 C45 C95 C47 0.0 . . . . ?
C91 C23 C93 F18 -179.5(3) . . . . ?
C91 C23 C93 C47 0.0 . . . . ?
C23 C93 C47 S8 -171.1(2) . . . . ?
C23 C93 C47 C95 0.0 . . . . ?
C93 C47 C95 F16 178.1(3) . . . . ?
C93 C47 C95 C45 0.0 . . . . ?
C95 C45 C91 F58 -179.1(3) . . . . ?
C95 C45 C91 C23 0.0 . . . . ?
F13 C7 C113 F37 2.1(5) . . . . ?
F13 C7 C113 C27 -178.2(5) . . . . ?
C3 C97 C49 F36 176.9(4) . . . . ?
C3 C97 C49 C99 0.0 . . . . ?
C97 C3 C101 F49 -178.5(5) . . . . ?
C97 C3 C101 C25 0.0 . . . . ?
C97 C49 C99 F41 180.0(4) . . . . ?
C97 C49 C99 C25 0.0 . . . . ?
C49 C99 C25 F25 -177.5(5) . . . . ?
C49 C99 C25 C101 0.0 . . . . ?
C99 C25 C101 F49 178.5(5) . . . . ?
C99 C25 C101 C3 0.0 . . . . ?
C101 C3 C97 S6 -171.5(3) . . . . ?
C101 C3 C97 C49 0.0 . . . . ?
C51 C103 C13 F5 179.4(4) . . . . ?
C51 C103 C13 C105 0.0 . . . . ?
C103 C51 C107 F60 179.2(4) . . . . ?
C103 C51 C107 C53 0.0 . . . . ?
C103 C13 C105 F47 179.1(4) . . . . ?
C103 C13 C105 C53 0.0 . . . . ?
C13 C105 C53 F23 179.1(4) . . . . ?
C13 C105 C53 C107 0.0 . . . . ?
C105 C53 C107 F60 -179.2(4) . . . . ?
C105 C53 C107 C51 0.0 . . . . ?
C107 C51 C103 F48 177.8(4) . . . . ?
C107 C51 C103 C13 0.0 . . . . ?
F53 C141 C71 F2 1.3(5) . . . . ?
F53 C141 C71 C143 -177.8(5) . . . . ?
F27 C55 C111 C7 -179.8(5) . . . . ?
F27 C55 C111 F29 0.1(5) . . . . ?
O2 C33 C133 C67 179.9(17) . . . . ?
C27 C109 C55 F27 179.8(5) . . . . ?
C27 C109 C55 C111 0.0 . . . . ?
C109 C27 C113 F37 179.7(4) . . . . ?
C109 C27 C113 C7 0.0 . . . . ?
C109 C55 C111 C7 0.0 . . . . ?
C109 C55 C111 F29 179.9(5) . . . . ?
C55 C111 C7 F13 178.2(5) . . . . ?
C55 C111 C7 C113 0.0 . . . . ?
C111 C7 C113 F37 -179.7(4) . . . . ?
C111 C7 C113 C27 0.0 . . . . ?
C113 C27 C109 F33 176.9(4) . . . . ?
C113 C27 C109 C55 0.0 . . . . ?
C57 O1 C42 C40 -5.1(5) . . . . ?
C57 O1 C42 C44 175.1(3) . . . . ?
F55 C152 C154 F19 -1.2(6) . . . . ?
F55 C152 C154 C156 179.3(5) . . . . ?
C115 C29 C117 F3 178.8(5) . . . . ?
C115 C29 C117 C59 0.0 . . . . ?
C29 C115 C15 S7 -173.0(3) . . . . ?
C29 C115 C15 C119 0.0 . . . . ?
C29 C117 C59 F39 179.4(5) . . . . ?
C29 C117 C59 C119 0.0 . . . . ?
C117 C59 C119 F28 -179.1(4) . . . . ?
C117 C59 C119 C15 0.0 . . . . ?
C59 C119 C15 S7 173.0(3) . . . . ?
C59 C119 C15 C115 0.0 . . . . ?
C15 C115 C29 F43 -179.1(5) . . . . ?
C15 C115 C29 C117 0.0 . . . . ?
O9 C54 C56 C58 177.9(5) . . . . ?
F7 C177 C89 F11 -1.5(5) . . . . ?
F7 C177 C89 C170 179.6(5) . . . . ?
C121 O4 C70 C68 180.0(3) . . . . ?
C121 O4 C70 C72 -2.0(5) . . . . ?
F57 C176 C177 C89 178.4(6) . . . . ?
F57 C176 C177 F7 -1.2(6) . . . . ?
C61 O10 C76 C74 -9.7(6) . . . . ?
C61 O10 C76 C78 172.1(4) . . . . ?
F29 C111 C7 F13 -1.7(5) . . . . ?
F29 C111 C7 C113 -179.9(5) . . . . ?
F59 C35 C141 F53 -1.7(6) . . . . ?
F59 C35 C141 C71 -179.6(6) . . . . ?
C123 O6 C86 C88 -2.0(5) . . . . ?
C123 O6 C86 C96 177.1(4) . . . . ?
C31 C125 C63 C127 0.0 . . . . ?
C31 C129 P2 Ag9 134.8(6) . . . . ?
C31 C129 P2 C67 -103.3(8) . . . . ?
C31 C129 P2 C147 13.3(10) . . . . ?
C125 C31 C129 C2 0.0 . . . . ?
C125 C31 C129 P2 -178.3(9) . . . . ?
C125 C63 C127 C2 0.0 . . . . ?
C125 C63 C127 O11 179.4(8) . . . . ?
C63 C127 C2 C129 0.0 . . . . ?
C63 C127 O11 C73 -179.0(7) . . . . ?
C127 C2 C129 C31 0.0 . . . . ?
C127 C2 C129 P2 178.3(9) . . . . ?
C2 C127 O11 C73 0.4(10) . . . . ?
C2 C129 P2 Ag9 -43.5(8) . . . . ?
C2 C129 P2 C67 78.4(8) . . . . ?
C2 C129 P2 C147 -165.0(6) . . . . ?
C129 C31 C125 C63 0.0 . . . . ?
O5 C151 C19 C147 -177.3(10) . . . . ?
C65 O15 C126 C124 -4.1(7) . . . . ?
C65 O15 C126 C128 176.2(5) . . . . ?
C131 C33 C133 C67 0.0 . . . . ?
C33 C131 C17 C135 0.0 . . . . ?
C33 C133 C67 C135 0.0 . . . . ?
C33 C133 C67 P2 -179.4(11) . . . . ?
C133 C67 C135 C17 0.0 . . . . ?
C133 C67 P2 Ag9 -44.4(9) . . . . ?
C133 C67 P2 C129 -164.5(7) . . . . ?
C133 C67 P2 C147 78.7(9) . . . . ?
C67 C135 C17 C131 0.0 . . . . ?
C135 C67 P2 Ag9 136.2(7) . . . . ?
C135 C67 P2 C129 16.1(11) . . . . ?
C135 C67 P2 C147 -100.7(10) . . . . ?
C17 C131 C33 O2 -179.9(15) . . . . ?
C17 C131 C33 C133 0.0 . . . . ?
C137 O12 C114 C112 -3.1(6) . . . . ?
C137 O12 C114 C116 176.0(4) . . . . ?
C69 O14 C102 C100 -6.5(7) . . . . ?
C69 O14 C102 C104 172.7(5) . . . . ?
O11 C127 C2 C129 -179.4(9) . . . . ?
C139 C35 C141 F53 177.8(5) . . . . ?
C139 C35 C141 C71 0.0 . . . . ?
C35 C139 C9 F17 -178.5(4) . . . . ?
C35 C139 C9 C143 0.0 . . . . ?
C35 C141 C71 F2 179.1(5) . . . . ?
C35 C141 C71 C143 0.0 . . . . ?
C141 C71 C143 S11 -175.5(3) . . . . ?
C141 C71 C143 C9 0.0 . . . . ?
C71 C143 C9 F17 178.4(4) . . . . ?
C71 C143 C9 C139 0.0 . . . . ?
C9 C139 C35 F59 179.6(6) . . . . ?
C9 C139 C35 C141 0.0 . . . . ?
C145 O8 C138 C136 -4.0(6) . . . . ?
C145 O8 C138 C140 175.7(4) . . . . ?
C147 C37 C149 C75 0.0 . . . . ?
C37 C147 C19 C151 0.0 . . . . ?
C37 C147 P2 Ag9 121.0(5) . . . . ?
C37 C147 P2 C129 -117.4(7) . . . . ?
C37 C147 P2 C67 -3.6(9) . . . . ?
C37 C149 C75 C151 0.0 . . . . ?
C149 C75 C151 O5 177.6(9) . . . . ?
C149 C75 C151 C19 0.0 . . . . ?
C75 C151 C19 C147 0.0 . . . . ?
C19 C147 C37 C149 0.0 . . . . ?
C19 C147 P2 Ag9 -50.0(8) . . . . ?
C19 C147 P2 C129 71.6(8) . . . . ?
C19 C147 P2 C67 -174.7(7) . . . . ?
C153 O2 C33 C131 165.7(13) . . . . ?
C153 O2 C33 C133 -14(2) . . . . ?
C77 O5 C151 C75 174.8(8) . . . . ?
C77 O5 C151 C19 -7.8(13) . . . . ?
C39 C157 C79 C159 0.0 . . . . ?
C157 C39 C161 P3 178.3(14) . . . . ?
C157 C39 C161 C5 0.0 . . . . ?
C157 C79 C159 C5 0.0 . . . . ?
C157 C79 C159 O3 -169.5(18) . . . . ?
C79 C159 C5 C161 0.0 . . . . ?
C79 C159 O3 C81 144(2) . . . . ?
C159 C5 C161 P3 -178.4(13) . . . . ?
C159 C5 C161 C39 0.0 . . . . ?
C5 C159 O3 C81 -26(3) . . . . ?
C161 P3 C167 C83 -177.2(10) . . . . ?
C161 P3 C167 C21 -3(2) . . . . ?
C161 P3 C43 C171 78.6(13) . . . . ?
C161 P3 C43 C173 -109.5(14) . . . . ?
C161 C39 C157 C79 0.0 . . . . ?
O3 C159 C5 C161 169.2(18) . . . . ?
O13 C165 C83 C167 179.9(17) . . . . ?
C163 O13 C165 C41 157.7(14) . . . . ?
C163 O13 C165 C83 -22(2) . . . . ?
C41 C165 C83 C167 0.0 . . . . ?
C165 C41 C169 C21 0.0 . . . . ?
C165 C83 C167 P3 174.8(16) . . . . ?
C165 C83 C167 C21 0.0 . . . . ?
C83 C167 C21 C169 0.0 . . . . ?
C167 P3 C161 C39 -68.1(14) . . . . ?
C167 P3 C161 C5 110.2(13) . . . . ?
C167 P3 C43 C171 -178.7(12) . . . . ?
C167 P3 C43 C173 -6.8(18) . . . . ?
C167 C21 C169 C41 0.0 . . . . ?
C169 C41 C165 O13 -179.9(17) . . . . ?
C169 C41 C165 C83 0.0 . . . . ?
O7 C85 C171 C43 176(3) . . . . ?
O7 C85 C175 C87 -176(3) . . . . ?
C85 C171 C43 P3 172.3(15) . . . . ?
C85 C171 C43 C173 0.0 . . . . ?
C171 C85 C175 C87 0.0 . . . . ?
C171 C43 C173 C87 0.0 . . . . ?
C43 P3 C161 C39 41.3(14) . . . . ?
C43 P3 C161 C5 -140.4(11) . . . . ?
C43 P3 C167 C83 78.4(12) . . . . ?
C43 P3 C167 C21 -107.6(17) . . . . ?
C43 C173 C87 C175 0.0 . . . . ?
C173 C87 C175 C85 0.0 . . . . ?
C175 C85 C171 C43 0.0 . . . . ?
C11 O7 C85 C171 9(3) . . . . ?
C11 O7 C85 C175 -175(2) . . . . ?
P2 C67 C135 C17 179.4(12) . . . . ?
P2 C147 C37 C149 -171.1(7) . . . . ?
P2 C147 C19 C151 171.0(8) . . . . ?
Ag5 S9 C51 C103 -21.7(3) . . . . ?
Ag5 S9 C51 C107 151.5(2) . . . . ?
Ag5 S5 C27 C109 -14.5(3) . . . . ?
Ag5 S5 C27 C113 158.1(2) . . . . ?
Ag5 S11 C143 C71 154.1(2) . . . . ?
Ag5 S11 C143 C9 -21.3(3) . . . . ?
Ag5 P3 C161 C39 165.2(8) . . . . ?
Ag5 P3 C161 C5 -16.5(14) . . . . ?
Ag5 P3 C167 C83 -47.9(13) . . . . ?
Ag5 P3 C167 C21 126.1(14) . . . . ?
Ag5 P3 C43 C171 -50.2(12) . . . . ?
Ag5 P3 C43 C173 121.7(12) . . . . ?

_smtbx_masks_special_details     
;
A solvent mask was calculated and 194 electrons were 
found in a volume of 1414Å³ in 2 voids per unit cell. 
This is consistent with the presence of 
1[CH2Cl2], 3[CH3OH] per formula unit 
which account for 192 electrons 
per unit cell.
;
loop_
_smtbx_masks_void_nr
_smtbx_masks_void_average_x
_smtbx_masks_void_average_y
_smtbx_masks_void_average_z
_smtbx_masks_void_volume
_smtbx_masks_void_count_electrons
_smtbx_masks_void_content
1 -0.166 0.210 0.726 690.4 95.8 '1 CH2Cl2,3 CH3OH'
2 0.166 0.790 0.274 690.4 96.3 '1 CH2Cl2,3 CH3OH'
3 0.420 0.460 0.585 17.1 1.2 ?
4 0.580 0.540 0.415 17.1 1.2 ?

_smtbx_masks_void_probe_radius   1.2
_smtbx_masks_void_truncation_radius 1.2
_olex2_submission_special_instructions 'No special instructions were received'
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_mal20240321b_0m
_database_code_depnum_ccdc_archive 'CCDC 2413802'
loop_
_audit_author_name
_audit_author_address
'Along Ma'
;qingdao university of science and technology
China
;
_audit_update_record             
;
2024-12-31 deposited with the CCDC.	2025-06-11 downloaded from the CCDC.
;
_audit_creation_date             2024-12-13
_audit_creation_method           
;
Olex2 1.5
(compiled 2024.02.16 svn.r378c4104 for OlexSys, GUI svn.r6928)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C156 H84 Ag14 F60 O12 P4 S12, [+ solvents]'
_chemical_formula_sum            'C159.73 H96.91 Ag14 Cl2 F60 O14.73 P4 S12'
_chemical_formula_weight         5481.40
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_H-M_alt        'P 1 21/c 1'
_space_group_name_Hall           '-P 2ybc'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'

_cell_length_a                   19.3202(8)
_cell_length_b                   19.1149(7)
_cell_length_c                   49.181(2)
_cell_angle_alpha                90
_cell_angle_beta                 95.3950(10)
_cell_angle_gamma                90
_cell_volume                     18082.2(13)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    9747
_cell_measurement_temperature    170
_cell_measurement_theta_max      27.134
_cell_measurement_theta_min      2.315
_shelx_estimated_absorpt_T_max   0.915
_shelx_estimated_absorpt_T_min   0.774
_exptl_absorpt_coefficient_mu    1.803
_exptl_absorpt_correction_T_max  0.1237
_exptl_absorpt_correction_T_min  0.0941
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
SADABS-2016/2 (Bruker,2016/2) was used for absorption correction.
wR2(int) was 0.0812 before and 0.0559 after correction.
The Ratio of minimum to maximum transmission is 0.7607.
The λ/2 correction factor is Not present.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            yellow
_exptl_crystal_colour_primary    yellow
_exptl_crystal_density_diffrn    2.013
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             10629
_exptl_crystal_size_max          0.15
_exptl_crystal_size_mid          0.1
_exptl_crystal_size_min          0.05
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0503
_diffrn_reflns_av_unetI/netI     0.0421
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.999
_diffrn_reflns_limit_h_max       22
_diffrn_reflns_limit_h_min       -22
_diffrn_reflns_limit_k_max       21
_diffrn_reflns_limit_k_min       -22
_diffrn_reflns_limit_l_max       58
_diffrn_reflns_limit_l_min       -58
_diffrn_reflns_number            191046
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.999
_diffrn_reflns_theta_full        25.000
_diffrn_reflns_theta_max         25.000
_diffrn_reflns_theta_min         1.886
_diffrn_ambient_temperature      170
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       ?
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_diffrn_source_current           1.4
_diffrn_source_power             0.07
_diffrn_source_voltage           50.0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                25407
_reflns_number_total             31803
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT V8.40B (?, 2016)'
_computing_data_collection       ?
_computing_data_reduction        'SAINT V8.40B (?, 2016)'
_computing_molecular_graphics    'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2018/3 (Sheldrick, 2015)'
_computing_structure_solution    'SHELXT  (Sheldrick, 2015)'
_refine_diff_density_max         1.013
_refine_diff_density_min         -0.892
_refine_diff_density_rms         0.150
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.197
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     2341
_refine_ls_number_reflns         31803
_refine_ls_number_restraints     3973
_refine_ls_R_factor_all          0.0863
_refine_ls_R_factor_gt           0.0695
_refine_ls_restrained_S_all      1.133
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+285.0516P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1524
_refine_ls_wR_factor_ref         0.1566
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups
 At 1.5 times of:
  All C(H,H,H) groups
2. Restrained distances
 O2-C39
 1.45 with sigma of 0.2
 O11-C77 = O3-C77
 1.4 with sigma of 0.02
 O11-C155 = O3-C157
 1.45 with sigma of 0.02
3. Uiso/Uaniso restraints and constraints
All non-hydrogen atoms have similar U: within 2A with sigma of 0.04 and sigma
for terminal atoms of 0.08 within 2A
C156 \\sim C81 \\sim C89 \\sim C149 \\sim C75 \\sim O11 \\sim C77 \\sim C155
\\sim O3 \\sim C157: within 2A with sigma of 0.001 and sigma for terminal atoms
of 0.002 within 2A
4. Rigid body (RIGU) restrains
 All non-hydrogen atoms
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
5. Others
 Sof(C39)=Sof(H39A)=Sof(H39B)=Sof(H39C)=1-FVAR(1)
 Sof(C37)=Sof(H37A)=Sof(H37B)=Sof(H37C)=FVAR(1)
 Sof(O3)=Sof(C157)=Sof(H15D)=Sof(H15E)=Sof(H15F)=1-FVAR(2)
 Sof(O11)=Sof(C155)=Sof(H15A)=Sof(H15B)=Sof(H15C)=FVAR(2)
6.a Riding coordinates:
 C133(H13A,H13B,H13C)
6.b Aromatic/amide H refined with riding coordinates:
 C66(H66), C74(H74), C76(H76), C88(H88), C100(H100), C106(H106), C108(H108),
 C110(H110), C114(H114), C120(H120), C124(H124), C128(H128), C132(H132),
 C134(H134), C136(H136), C140(H140), C148(H148), C156(H156), C21(H21), C43(H43),
  C89(H89), C91(H91), C23(H23), C95(H95), C3(H3), C99(H99), C103(H103),
 C109(H109), C111(H111), C115(H115), C117(H117), C119(H119), C61(H61),
 C123(H123), C31(H31), C63(H63), C2(H2), C131(H131), C135(H135), C17(H17),
 C137(H137), C69(H69), C139(H139), C141(H141), C9(H9), C145(H145), C149(H149),
 C75(H75)
6.c Fitted hexagon refined as free rotating group:
 C104(C106,C108,C110,C112,C114), C130(C132,C134,C136,C138,C140)
6.d Idealised Me refined as rotating group:
 C45(H45A,H45B,H45C), C59(H59A,H59B,H59C), C127(H12A,H12B,H12C), C129(H12D,
 H12E,H12F), C67(H67A,H67B,H67C), C71(H71A,H71B,H71C), C143(H14A,H14B,H14C),
 C73(H73A,H73B,H73C), C147(H14D,H14E,H14F), C37(H37A,H37B,H37C), C155(H15A,H15B,
 H15C), C39(H39A,H39B,H39C), C157(H15D,H15E,H15F)
;
_atom_sites_solution_hydrogens   mixed
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.23759(4) 0.80453(4) 0.65672(2) 0.03558(18) Uani 1 1 d . . . . .
Ag4 Ag 0.37017(4) 0.69107(4) 0.61509(2) 0.03507(18) Uani 1 1 d . . . . .
Ag6 Ag 0.23317(4) 0.74824(4) 0.60260(2) 0.03620(18) Uani 1 1 d . . . . .
Ag8 Ag 0.34621(4) 0.83730(4) 0.62297(2) 0.03535(18) Uani 1 1 d . . . . .
Ag10 Ag 0.37527(4) 0.74736(4) 0.66907(2) 0.03521(17) Uani 1 1 d . . . . .
Ag12 Ag 0.26206(4) 0.65889(4) 0.64916(2) 0.03562(18) Uani 1 1 d . . . . .
Ag14 Ag 0.40491(4) 0.59505(4) 0.66321(2) 0.03825(18) Uani 1 1 d . . . . .
Ag7 Ag 0.34398(4) 0.78166(4) 0.56537(2) 0.03869(19) Uani 1 1 d . . . . .
Ag2 Ag 0.11462(4) 0.71450(5) 0.63632(2) 0.0422(2) Uani 1 1 d . . . . .
Ag9 Ag 0.25411(4) 0.70428(5) 0.72099(2) 0.0439(2) Uani 1 1 d . . . . .
Ag5 Ag 0.18283(4) 0.93507(4) 0.60309(2) 0.0436(2) Uani 1 1 d . . . . .
Ag11 Ag 0.35343(5) 0.90190(5) 0.67968(2) 0.0455(2) Uani 1 1 d . . . . .
Ag3 Ag 0.24401(5) 0.56159(5) 0.58311(2) 0.0466(2) Uani 1 1 d . . . . .
Ag13 Ag 0.53538(4) 0.79280(5) 0.63503(2) 0.0472(2) Uani 1 1 d . . . . .
S1 S 0.15154(14) 0.74455(15) 0.68538(5) 0.0411(6) Uani 1 1 d . U . . .
S4 S 0.36190(14) 0.55806(14) 0.61439(5) 0.0399(6) Uani 1 1 d . U . . .
S6 S 0.30596(14) 0.60064(15) 0.69388(5) 0.0407(6) Uani 1 1 d . U . . .
S8 S 0.25627(14) 0.68312(14) 0.55896(5) 0.0396(6) Uani 1 1 d . U . . .
S10 S 0.34442(14) 0.80239(15) 0.71318(5) 0.0417(6) Uani 1 1 d . U . . .
S12 S 0.46172(13) 0.75164(15) 0.58940(5) 0.0401(6) Uani 1 1 d . U . . .
S3 S 0.29359(14) 0.89731(14) 0.57951(5) 0.0392(6) Uani 1 1 d . U . . .
S7 S 0.16174(14) 0.59850(15) 0.62095(5) 0.0414(6) Uani 1 1 d . U . . .
S2 S 0.49473(13) 0.69207(15) 0.66744(5) 0.0403(6) Uani 1 1 d . U . . .
S9 S 0.11718(14) 0.81248(14) 0.60221(5) 0.0413(6) Uani 1 1 d . U . . .
S5 S 0.23758(15) 0.93745(15) 0.65404(5) 0.0415(6) Uani 1 1 d . U . . .
S11 S 0.45240(14) 0.89298(15) 0.64910(6) 0.0439(6) Uani 1 1 d . U . . .
P1 P 0.22247(15) 0.68482(15) 0.76663(5) 0.0417(7) Uani 1 1 d . U . . .
P4 P 0.11534(16) 1.03273(15) 0.58358(6) 0.0453(7) Uani 1 1 d . U . . .
P2 P 0.65858(15) 0.80883(17) 0.63188(6) 0.0478(7) Uani 1 1 d . U . . .
P3 P 0.20587(18) 0.46195(18) 0.55574(6) 0.0534(8) Uani 1 1 d . U . . .
F1 F 0.3032(4) 1.0415(3) 0.60474(13) 0.0551(17) Uani 1 1 d . U . . .
F4 F 0.2276(3) 0.4565(3) 0.62911(12) 0.0501(15) Uani 1 1 d . U . . .
F6 F 0.1884(3) 0.8520(4) 0.72961(13) 0.0576(17) Uani 1 1 d . U . . .
F8 F 0.5169(4) 0.5738(3) 0.70747(14) 0.0619(19) Uani 1 1 d . U . . .
F10 F 0.1631(3) 0.5688(4) 0.71073(14) 0.0596(17) Uani 1 1 d . U . . .
F12 F 0.5704(4) 0.8123(3) 0.69685(13) 0.0629(19) Uani 1 1 d . U . . .
F14 F 0.1297(4) 0.8688(4) 0.54592(13) 0.0655(19) Uani 1 1 d . U . . .
F16 F 0.0342(3) 0.5882(4) 0.65178(14) 0.0588(17) Uani 1 1 d . U . . .
F18 F 0.3951(4) 0.9047(3) 0.53643(13) 0.0613(18) Uani 1 1 d . U . . .
F20 F 0.0017(3) 0.7747(4) 0.66752(15) 0.0666(19) Uani 1 1 d . U . . .
F22 F 0.4423(4) 0.7301(4) 0.52861(12) 0.0629(19) Uani 1 1 d . U . . .
F24 F 0.5688(3) 0.6424(3) 0.60807(13) 0.0570(17) Uani 1 1 d . U . . .
F26 F 0.3649(3) 0.4581(3) 0.68457(14) 0.0587(17) Uani 1 1 d . U . . .
F28 F 0.3796(4) 0.5572(4) 0.55384(13) 0.0642(19) Uani 1 1 d . U . . .
F30 F 0.0804(4) 0.9408(4) 0.64742(14) 0.067(2) Uani 1 1 d . U . . .
F32 F 0.1102(4) 0.6262(4) 0.54964(16) 0.070(2) Uani 1 1 d . U . . .
F34 F 0.2676(4) 0.7772(4) 0.51041(13) 0.068(2) Uani 1 1 d . U . . .
F36 F -0.0085(4) 0.7177(4) 0.59404(16) 0.071(2) Uani 1 1 d . U . . .
F38 F 0.4098(4) 0.6762(4) 0.74253(13) 0.0596(17) Uani 1 1 d . U . . .
F40 F 0.6436(4) 0.5641(4) 0.57682(17) 0.079(2) Uani 1 1 d . U . . .
F42 F 0.3670(4) 1.1532(3) 0.58689(14) 0.0647(19) Uani 1 1 d . U . . .
F44 F 0.1124(4) 0.4445(4) 0.72341(16) 0.080(2) Uani 1 1 d . U . . .
F46 F 0.1719(4) 0.3421(4) 0.64836(15) 0.071(2) Uani 1 1 d . U . . .
F48 F 0.6527(5) 0.8080(4) 0.74383(15) 0.084(3) Uani 1 1 d . U . . .
F50 F 0.4611(5) 1.0166(4) 0.52013(16) 0.084(3) Uani 1 1 d . U . . .
F52 F 0.5201(4) 0.9242(4) 0.59758(14) 0.0669(19) Uani 1 1 d . U . . .
F54 F 0.4238(5) 1.0374(4) 0.67097(15) 0.079(2) Uani 1 1 d . U . . .
F56 F 0.6670(5) 0.6887(5) 0.77290(15) 0.093(3) Uani 1 1 d . U . . .
F58 F 0.5971(5) 0.5726(4) 0.75483(15) 0.084(3) Uani 1 1 d . U . . .
F60 F 0.4705(5) 0.4840(4) 0.52817(15) 0.086(3) Uani 1 1 d . U . . .
F15 F 0.4976(4) 0.6756(5) 0.78765(16) 0.088(3) Uani 1 1 d . U . . .
F31 F 0.4852(4) 0.4773(5) 0.63857(15) 0.080(2) Uani 1 1 d . U . . .
F2 F -0.0822(4) 0.8663(5) 0.68904(19) 0.089(3) Uani 1 1 d . U . . .
F33 F 0.3120(5) 0.3348(4) 0.69638(17) 0.081(2) Uani 1 1 d . U . . .
F17 F 0.4469(5) 1.1423(4) 0.54440(17) 0.087(3) Uani 1 1 d . U . . .
F35 F 0.6185(5) 0.5670(4) 0.52154(18) 0.089(3) Uani 1 1 d . U . . .
F9 F 0.1026(4) 0.9397(5) 0.75239(15) 0.082(2) Uani 1 1 d . U . . .
F37 F -0.0325(4) 0.9484(5) 0.73252(18) 0.094(3) Uani 1 1 d . U . . .
F19 F 0.0387(5) 0.8578(5) 0.50182(15) 0.102(3) Uani 1 1 d . U . . .
F39 F 0.0480(5) 0.3480(4) 0.6699(2) 0.094(3) Uani 1 1 d . U . . .
F5 F 0.4225(4) 0.9214(4) 0.73970(17) 0.081(2) Uani 1 1 d . U . . .
F41 F 0.5153(5) 0.6502(5) 0.49802(15) 0.088(3) Uani 1 1 d . U . . .
F21 F -0.0185(4) 0.4726(5) 0.67247(19) 0.091(3) Uani 1 1 d . U . . .
O1 O -0.0383(4) 0.6892(6) 0.73095(19) 0.073(2) Uani 1 1 d . U . . .
F43 F 0.2740(5) 1.0187(5) 0.70537(16) 0.097(3) Uani 1 1 d . U . . .
F11 F 0.5635(5) 1.0483(5) 0.58084(18) 0.104(3) Uani 1 1 d . U . . .
O4 O 0.2537(5) 1.0265(6) 0.49859(18) 0.076(3) Uani 1 1 d . U . . .
F45 F 0.1869(5) 0.3263(4) 0.71690(19) 0.095(3) Uani 1 1 d . U . . .
O6 O -0.1078(4) 0.8841(5) 0.5866(2) 0.071(2) Uani 1 1 d . U . . .
O8 O -0.0364(5) 0.4789(6) 0.5923(2) 0.080(3) Uani 1 1 d . U . . .
O10 O 0.6302(7) 0.8021(6) 0.52635(19) 0.091(3) Uani 1 1 d . U . . .
F23 F 0.1771(5) 0.7904(6) 0.46645(16) 0.113(3) Uani 1 1 d . U . . .
F47 F -0.0042(5) 1.0185(6) 0.6749(2) 0.113(3) Uani 1 1 d . U . . .
F3 F 0.0222(4) 0.6377(6) 0.5048(2) 0.114(3) Uani 1 1 d . U . . .
F49 F 0.5107(6) 0.9212(5) 0.7852(2) 0.122(4) Uani 1 1 d . U . . .
F25 F 0.4632(7) 1.1599(5) 0.6522(2) 0.124(4) Uani 1 1 d . U . . .
F51 F -0.0958(4) 0.7033(6) 0.5495(2) 0.116(4) Uani 1 1 d . U . . .
O12 O 0.4017(6) 0.3115(5) 0.6040(2) 0.091(3) Uani 1 1 d . U . . .
C1 C 0.5414(5) 0.6917(6) 0.7000(2) 0.041(2) Uani 1 1 d . U . . .
C4 C 0.2026(6) 0.5119(6) 0.7079(2) 0.044(2) Uani 1 1 d . U . . .
F13 F -0.0752(5) 0.7758(6) 0.50292(19) 0.123(4) Uani 1 1 d . U . . .
C6 C 0.2672(5) 0.5189(5) 0.69835(18) 0.0342(19) Uani 1 1 d . U . . .
F53 F 0.5483(5) 0.7970(6) 0.80964(18) 0.120(4) Uani 1 1 d . U . . .
F27 F 0.5696(6) 0.4072(5) 0.5571(2) 0.128(4) Uani 1 1 d . U . . .
C8 C 0.5500(6) 0.6321(6) 0.7159(2) 0.047(2) Uani 1 1 d . U . . .
C10 C 0.5766(6) 0.7517(6) 0.7104(2) 0.044(2) Uani 1 1 d . U . . .
O13 O 0.2562(7) 0.5971(6) 0.4693(2) 0.096(3) Uani 1 1 d . U . . .
C12 C 0.0988(5) 0.8076(6) 0.6985(2) 0.041(2) Uani 1 1 d . U . . .
F55 F 0.5765(6) 0.4058(7) 0.6121(2) 0.149(5) Uani 1 1 d . U . . .
O7 O 0.2070(9) 1.1853(6) 0.6657(2) 0.112(4) Uani 1 1 d . U . . .
C14 C 0.1809(6) 0.9784(5) 0.6751(2) 0.043(2) Uani 1 1 d . U . . .
O2 O 0.7036(6) 0.5837(6) 0.6858(3) 0.104(4) Uani 1 1 d D U . . .
C16 C 0.4273(6) 0.5189(6) 0.5689(2) 0.047(2) Uani 1 1 d . U . . .
C18 C 0.3412(6) 1.0333(6) 0.58312(19) 0.041(2) Uani 1 1 d . U . . .
C20 C 0.3446(6) 0.9682(6) 0.57084(19) 0.042(2) Uani 1 1 d . U . . .
C22 C 0.5044(5) 0.6904(5) 0.5696(2) 0.037(2) Uani 1 1 d . U . . .
C24 C 0.4926(6) 0.6904(6) 0.5416(2) 0.048(2) Uani 1 1 d . U . . .
C26 C 0.6860(6) 0.7784(6) 0.5992(2) 0.050(2) Uani 1 1 d . U . . .
C28 C 0.3020(6) 0.4570(6) 0.6945(2) 0.045(2) Uani 1 1 d . U . . .
C30 C 0.0697(6) 0.5275(6) 0.6504(2) 0.049(2) Uani 1 1 d . U . . .
C32 C 0.1213(6) 0.8526(6) 0.7196(2) 0.048(2) Uani 1 1 d . U . . .
C34 C 0.4717(6) 0.9753(7) 0.6352(2) 0.051(2) Uani 1 1 d . U . . .
C36 C 0.0285(6) 0.8149(6) 0.6886(2) 0.048(2) Uani 1 1 d . U . . .
C38 C 0.1658(6) 0.4617(6) 0.6389(2) 0.043(2) Uani 1 1 d . U . . .
O9 O 0.3424(6) 0.9107(5) 0.8007(2) 0.096(3) Uani 1 1 d . U . . .
C40 C 0.2076(7) 0.7411(7) 0.5098(2) 0.057(3) Uani 1 1 d . U . . .
C42 C 0.0628(6) 0.7941(6) 0.5719(2) 0.046(2) Uani 1 1 d . U . . .
C44 C 0.5555(6) 0.6459(6) 0.5810(2) 0.046(2) Uani 1 1 d . U . . .
C46 C 0.1324(6) 0.7097(7) 0.7697(2) 0.054(3) Uani 1 1 d . U . . .
C48 C -0.0161(6) 0.8620(7) 0.6999(3) 0.060(3) Uani 1 1 d . U . . .
C50 C 0.0728(6) 0.8302(6) 0.5480(2) 0.052(3) Uani 1 1 d . U . . .
C52 C 0.1295(6) 0.6657(7) 0.5289(3) 0.058(3) Uani 1 1 d . U . . .
F7 F 0.5352(7) 1.1683(5) 0.6081(2) 0.133(4) Uani 1 1 d . U . . .
C54 C 0.1321(5) 0.5253(5) 0.63866(19) 0.036(2) Uani 1 1 d . U . . .
C56 C 0.4736(8) 0.4820(7) 0.5555(3) 0.067(3) Uani 1 1 d . U . . .
C58 C 0.4330(6) 0.7384(6) 0.7526(2) 0.048(2) Uani 1 1 d . U . . .
C60 C 0.1083(7) 0.9798(6) 0.6682(2) 0.053(2) Uani 1 1 d . U . . .
C62 C 0.1934(6) 0.6986(7) 0.5315(2) 0.053(3) Uani 1 1 d . U . . .
C64 C 0.4120(5) 0.8001(6) 0.73950(19) 0.041(2) Uani 1 1 d . U . . .
C66 C 0.0820(6) 0.6863(7) 0.7501(2) 0.049(3) Uani 1 1 d . U . . .
H66 H 0.093905 0.653817 0.736665 0.059 Uiso 1 1 calc R U . . .
C68 C 0.4271(6) 0.5195(6) 0.5974(2) 0.046(2) Uani 1 1 d . U . . .
C70 C 0.2756(6) 0.7347(6) 0.7927(2) 0.049(3) Uani 1 1 d . U . . .
C72 C 0.5941(6) 0.6062(6) 0.5648(3) 0.056(3) Uani 1 1 d . U . . .
C74 C 0.1849(6) 1.0339(7) 0.5377(2) 0.050(3) Uani 1 1 d . U . . .
H74 H 0.176760 0.984884 0.537841 0.060 Uiso 1 1 calc R U . . .
C76 C 0.6482(7) 0.8044(7) 0.5759(2) 0.055(3) Uani 1 1 d . U . . .
H76 H 0.611678 0.837020 0.577476 0.066 Uiso 1 1 calc R U . . .
C78 C 0.0303(6) 1.0044(6) 0.5685(2) 0.050(3) Uani 1 1 d . U . . .
C80 C 0.0145(6) 0.7098(7) 0.7499(3) 0.059(3) Uani 1 1 d . U . . .
C82 C 0.1580(6) 1.0761(6) 0.5569(2) 0.048(2) Uani 1 1 d . U . . .
C84 C 0.4796(6) 0.7366(8) 0.7758(2) 0.059(3) Uani 1 1 d . U . . .
F57 F 0.0545(6) 0.7197(7) 0.46262(19) 0.133(4) Uani 1 1 d . U . . .
C86 C 0.5052(7) 0.7977(8) 0.7865(3) 0.069(3) Uani 1 1 d . U . . .
C88 C 0.2905(8) 0.3649(7) 0.5308(3) 0.067(3) Uani 1 1 d . U . . .
H88 H 0.265812 0.375741 0.513686 0.081 Uiso 1 1 calc R U . . .
O5 O 0.3760(6) 0.4631(6) 0.7741(3) 0.099(3) Uani 1 1 d . U . . .
C90 C 0.5915(7) 0.6294(7) 0.7402(2) 0.055(3) Uani 1 1 d . U . . .
C92 C 0.2239(6) 1.0627(7) 0.5181(2) 0.053(3) Uani 1 1 d . U . . .
C94 C 0.4199(7) 1.0226(7) 0.5406(2) 0.059(3) Uani 1 1 d . U . . .
C96 C 0.3878(6) 0.9656(7) 0.5498(2) 0.052(3) Uani 1 1 d . U . . .
C98 C 0.0271(8) 0.8236(8) 0.5245(3) 0.069(3) Uani 1 1 d . U . . .
C100 C 0.2883(7) 0.8025(6) 0.7874(3) 0.057(3) Uani 1 1 d . U . . .
H100 H 0.267943 0.822892 0.770960 0.068 Uiso 1 1 calc R U . . .
C102 C 0.1387(7) 0.4015(6) 0.6492(2) 0.053(3) Uani 1 1 d . U . . .
C104 C 0.2337(4) 0.5943(3) 0.77581(16) 0.051(2) Uani 1 1 d G U . . .
C106 C 0.1821(4) 0.5508(5) 0.78419(18) 0.083(4) Uani 1 1 d G U . . .
H106 H 0.137779 0.569519 0.787065 0.100 Uiso 1 1 calc R U . . .
C108 C 0.1952(5) 0.4799(4) 0.78837(19) 0.093(4) Uani 1 1 d G U . . .
H108 H 0.159985 0.450224 0.794095 0.112 Uiso 1 1 calc R U . . .
C110 C 0.2600(5) 0.4526(3) 0.78416(19) 0.089(4) Uani 1 1 d G U . . .
H110 H 0.269053 0.404142 0.787014 0.107 Uiso 1 1 calc R U . . .
C112 C 0.3116(4) 0.4961(4) 0.77578(19) 0.072(3) Uani 1 1 d G U . . .
C114 C 0.2984(4) 0.5669(4) 0.77160(17) 0.062(3) Uani 1 1 d G U . . .
H114 H 0.333710 0.596651 0.765871 0.075 Uiso 1 1 calc R U . . .
C116 C 0.2766(7) 0.3920(6) 0.7005(2) 0.053(3) Uani 1 1 d . U . . .
C118 C 0.6256(7) 0.6902(7) 0.7491(2) 0.062(3) Uani 1 1 d . U . . .
C120 C 0.1687(7) 1.1486(6) 0.5567(3) 0.059(3) Uani 1 1 d . U . . .
H120 H 0.149526 1.178006 0.569654 0.070 Uiso 1 1 calc R U . . .
C122 C 0.4410(6) 0.8608(7) 0.7511(2) 0.056(3) Uani 1 1 d . U . . .
C124 C 0.2298(8) 0.5285(7) 0.5086(2) 0.063(3) Uani 1 1 d . U . . .
H124 H 0.272473 0.541090 0.518617 0.076 Uiso 1 1 calc R U . . .
C126 C 0.4576(8) 1.0365(7) 0.6484(3) 0.068(3) Uani 1 1 d . U . . .
C128 C -0.0070(6) 0.9590(6) 0.5841(2) 0.052(3) Uani 1 1 d . U . . .
H128 H 0.010702 0.947412 0.602202 0.062 Uiso 1 1 calc R U . . .
C130 C 0.1010(5) 1.0995(4) 0.60889(15) 0.059(3) Uani 1 1 d G U . . .
C132 C 0.0359(4) 1.1256(5) 0.6135(2) 0.084(4) Uani 1 1 d G U . . .
H132 H -0.003909 1.112528 0.601826 0.101 Uiso 1 1 calc R U . . .
C134 C 0.0292(5) 1.1707(5) 0.6353(2) 0.103(5) Uani 1 1 d G U . . .
H134 H -0.015191 1.188557 0.638438 0.124 Uiso 1 1 calc R U . . .
C136 C 0.0875(7) 1.1898(4) 0.65238(18) 0.103(4) Uani 1 1 d G U . . .
H136 H 0.082969 1.220666 0.667248 0.123 Uiso 1 1 calc R U . . .
C138 C 0.1526(6) 1.1637(5) 0.64775(17) 0.088(4) Uani 1 1 d G U . . .
C140 C 0.1593(4) 1.1185(4) 0.62600(17) 0.063(3) Uani 1 1 d G U . . .
H140 H 0.203695 1.100715 0.622834 0.076 Uiso 1 1 calc R U . . .
C142 C 0.5289(8) 1.0462(8) 0.6030(3) 0.076(3) Uani 1 1 d . U . . .
C144 C 0.5296(7) 0.6487(7) 0.5253(2) 0.060(3) Uani 1 1 d . U . . .
C146 C 0.5813(7) 0.6060(7) 0.5371(3) 0.064(3) Uani 1 1 d . U . . .
C148 C 0.3465(8) 0.3189(7) 0.5322(3) 0.072(3) Uani 1 1 d . U . . .
H148 H 0.360373 0.299499 0.515810 0.086 Uiso 1 1 calc R U . . .
C150 C 0.5066(6) 0.9814(7) 0.6120(2) 0.055(3) Uani 1 1 d . U . . .
C152 C 0.1763(7) 0.4478(7) 0.7146(2) 0.060(3) Uani 1 1 d . U . . .
C154 C 0.0783(7) 0.8986(7) 0.7315(2) 0.058(3) Uani 1 1 d . U . . .
C156 C 0.6713(9) 1.0132(8) 0.6521(3) 0.0866(17) Uani 1 1 d . U . . .
H156 H 0.649803 1.044165 0.663853 0.104 Uiso 1 1 calc R U . . .
C158 C -0.0691(7) 0.9310(8) 0.5732(3) 0.064(3) Uani 1 1 d . U . . .
C79 C 0.1820(8) 0.4852(7) 0.5204(2) 0.064(3) Uani 1 1 d . U . . .
C5 C 0.7104(6) 0.7604(7) 0.6581(2) 0.053(3) Uani 1 1 d . U . . .
C81 C 0.6852(9) 0.8989(8) 0.6342(3) 0.0861(17) Uani 1 1 d . U . . .
C41 C 0.2713(7) 0.3945(7) 0.5546(2) 0.058(3) Uani 1 1 d . U . . .
C83 C 0.6187(7) 0.7510(7) 0.7347(2) 0.058(3) Uani 1 1 d . U . . .
C21 C 0.3082(7) 0.3771(6) 0.5793(2) 0.059(3) Uani 1 1 d . U . . .
H21 H 0.295912 0.398003 0.595742 0.071 Uiso 1 1 calc R U . . .
C85 C 0.0089(7) 0.9039(7) 0.7215(3) 0.064(3) Uani 1 1 d . U . . .
C43 C 0.7665(7) 0.7880(8) 0.6743(3) 0.071(4) Uani 1 1 d . U . . .
H43 H 0.782571 0.833956 0.671083 0.085 Uiso 1 1 calc R U . . .
C87 C 0.0183(7) 0.4383(8) 0.5855(3) 0.066(3) Uani 1 1 d . U . . .
C11 C 0.6643(8) 0.7821(8) 0.5502(3) 0.072(3) Uani 1 1 d . U . . .
C89 C 0.6547(9) 0.9424(8) 0.6516(3) 0.0861(17) Uani 1 1 d . U . . .
H89 H 0.622474 0.924440 0.663323 0.103 Uiso 1 1 calc R U . . .
C45 C 0.2444(8) 0.9541(8) 0.4982(3) 0.082(4) Uani 1 1 d . U . . .
H45A H 0.268926 0.933763 0.483505 0.123 Uiso 1 1 calc R U . . .
H45B H 0.194669 0.943317 0.494961 0.123 Uiso 1 1 calc R U . . .
H45C H 0.262957 0.934308 0.515740 0.123 Uiso 1 1 calc R U . . .
F29 F 0.1865(8) 1.0951(7) 0.7333(3) 0.178(6) Uani 1 1 d . U . . .
C91 C 0.0767(7) 0.4635(7) 0.5744(2) 0.059(3) Uani 1 1 d . U . . .
H91 H 0.080464 0.512288 0.571076 0.071 Uiso 1 1 calc R U . . .
C23 C 0.1152(8) 0.7576(9) 0.7888(3) 0.082(4) Uani 1 1 d . U . . .
H23 H 0.149576 0.775157 0.802129 0.098 Uiso 1 1 calc R U . . .
C93 C 0.4133(7) 1.0877(6) 0.5528(2) 0.057(3) Uani 1 1 d . U . . .
C47 C 0.2047(9) 1.0183(7) 0.6976(3) 0.073(3) Uani 1 1 d . U . . .
C95 C 0.6894(7) 0.6927(7) 0.6623(3) 0.068(3) Uani 1 1 d . U . . .
H95 H 0.650931 0.673840 0.651182 0.082 Uiso 1 1 calc R U . . .
C3 C 0.7768(8) 0.6805(9) 0.6990(3) 0.083(4) Uani 1 1 d . U . . .
H3 H 0.798792 0.652964 0.713387 0.100 Uiso 1 1 calc R U . . .
C97 C 0.3620(8) 0.3301(6) 0.5804(3) 0.066(3) Uani 1 1 d . U . . .
C49 C 0.0054(6) 0.7547(7) 0.5716(3) 0.059(3) Uani 1 1 d . U . . .
C99 C 0.2087(8) 1.1764(7) 0.5368(3) 0.068(3) Uani 1 1 d . U . . .
H99 H 0.216612 1.225426 0.536413 0.082 Uiso 1 1 calc R U . . .
C25 C 0.0755(7) 0.4059(7) 0.6600(3) 0.065(3) Uani 1 1 d . U . . .
C101 C 0.5162(9) 1.1059(8) 0.6170(3) 0.087(4) Uani 1 1 d . U . . .
C51 C 0.5250(9) 0.4429(8) 0.5698(3) 0.084(4) Uani 1 1 d . U . . .
C103 C 0.1261(8) 0.3499(7) 0.5729(3) 0.072(4) Uani 1 1 d . U . . .
H103 H 0.163155 0.320177 0.568899 0.087 Uiso 1 1 calc R U . . .
C13 C 0.0831(8) 0.6709(9) 0.5060(3) 0.081(4) Uani 1 1 d . U . . .
F59 F 0.0479(8) 1.0958(6) 0.7179(3) 0.169(6) Uani 1 1 d . U . . .
C105 C 0.4871(8) 0.8595(8) 0.7743(3) 0.074(4) Uani 1 1 d . U . . .
C53 C 0.1294(7) 0.4200(7) 0.5679(2) 0.059(3) Uani 1 1 d . U . . .
C107 C 0.3721(7) 1.0922(6) 0.5744(2) 0.052(3) Uani 1 1 d . U . . .
C27 C -0.0308(8) 0.7821(9) 0.5254(3) 0.083(4) Uani 1 1 d . U . . .
C109 C 0.0030(7) 1.0224(8) 0.5427(3) 0.071(4) Uani 1 1 d . U . . .
H109 H 0.027034 1.054570 0.532222 0.085 Uiso 1 1 calc R U . . .
C55 C 0.0421(7) 0.4690(7) 0.6611(3) 0.062(3) Uani 1 1 d . U . . .
C111 C 0.2361(7) 1.1351(7) 0.5181(3) 0.066(3) Uani 1 1 d . U . . .
H111 H 0.263510 1.155177 0.505105 0.079 Uiso 1 1 calc R U . . .
C7 C 0.3304(8) 0.8430(8) 0.8055(3) 0.076(4) Uani 1 1 d . U . . .
C113 C 0.4794(7) 0.4810(6) 0.6112(3) 0.057(3) Uani 1 1 d . U . . .
C57 C 0.1606(8) 0.7498(9) 0.4869(3) 0.079(4) Uani 1 1 d . U . . .
C115 C -0.0955(7) 0.9485(9) 0.5469(3) 0.075(4) Uani 1 1 d . U . . .
H115 H -0.138434 0.929172 0.539410 0.090 Uiso 1 1 calc R U . . .
C29 C -0.0423(7) 0.7459(9) 0.5486(3) 0.078(4) Uani 1 1 d . U . . .
C117 C 0.7379(7) 0.7314(9) 0.5972(3) 0.078(4) Uani 1 1 d . U . . .
H117 H 0.763209 0.713986 0.613327 0.094 Uiso 1 1 calc R U . . .
C59 C 0.3203(9) 0.6159(9) 0.4832(3) 0.091(4) Uani 1 1 d . U . . .
H59A H 0.345154 0.647136 0.471588 0.137 Uiso 1 1 calc R U . . .
H59B H 0.348198 0.573791 0.487347 0.137 Uiso 1 1 calc R U . . .
H59C H 0.312446 0.640050 0.500173 0.137 Uiso 1 1 calc R U . . .
C119 C 0.0675(8) 0.3217(8) 0.5842(3) 0.081(4) Uani 1 1 d . U . . .
H119 H 0.064212 0.272909 0.587513 0.097 Uiso 1 1 calc R U . . .
C15 C 0.7230(8) 0.6526(8) 0.6821(4) 0.084(4) Uani 1 1 d . U . . .
C121 C 0.2124(8) 0.3889(7) 0.7106(3) 0.065(3) Uani 1 1 d . U . . .
C61 C 0.0152(8) 0.3666(8) 0.5902(3) 0.080(4) Uani 1 1 d . U . . .
H61 H -0.024245 0.347888 0.597765 0.096 Uiso 1 1 calc R U . . .
C123 C 0.3817(8) 0.3010(7) 0.5562(3) 0.074(4) Uani 1 1 d . U . . .
H123 H 0.419416 0.269027 0.556684 0.089 Uiso 1 1 calc R U . . .
C31 C 0.7990(8) 0.7473(9) 0.6952(3) 0.085(4) Uani 1 1 d . U . . .
H31 H 0.836522 0.765965 0.706863 0.102 Uiso 1 1 calc R U . . .
C125 C 0.5283(8) 0.4435(7) 0.5987(3) 0.077(4) Uani 1 1 d . U . . .
C63 C -0.0034(8) 0.7577(10) 0.7689(3) 0.090(4) Uani 1 1 d . U . . .
H63 H -0.049571 0.774940 0.768499 0.108 Uiso 1 1 calc R U . . .
C127 C -0.0862(7) 0.8697(8) 0.6151(3) 0.079(4) Uani 1 1 d . U . . .
H12A H -0.041359 0.845313 0.616510 0.119 Uiso 1 1 calc R U . . .
H12B H -0.121074 0.840160 0.622668 0.119 Uiso 1 1 calc R U . . .
H12C H -0.081535 0.913770 0.625225 0.119 Uiso 1 1 calc R U . . .
C2 C 0.1172(9) 0.4705(10) 0.5067(3) 0.093(5) Uani 1 1 d . U . . .
H2 H 0.084440 0.442707 0.515129 0.112 Uiso 1 1 calc R U . . .
C129 C 0.3751(11) 0.3292(8) 0.6293(3) 0.099(6) Uani 1 1 d . U . . .
H12D H 0.325664 0.317178 0.628389 0.148 Uiso 1 1 calc R U . . .
H12E H 0.380931 0.379504 0.632628 0.148 Uiso 1 1 calc R U . . .
H12F H 0.400611 0.303075 0.644180 0.148 Uiso 1 1 calc R U . . .
C65 C 0.4782(10) 1.1001(8) 0.6394(3) 0.086(4) Uani 1 1 d . U . . .
C131 C -0.0595(8) 0.9939(10) 0.5318(3) 0.089(5) Uani 1 1 d . U . . .
H131 H -0.077589 1.005714 0.513703 0.106 Uiso 1 1 calc R U . . .
C33 C 0.2137(10) 0.5525(8) 0.4821(3) 0.082(4) Uani 1 1 d . U . . .
C133 C -0.0234(7) 0.6332(9) 0.7134(3) 0.084(4) Uani 1 1 d . U . . .
H13A H -0.011054 0.651817 0.695963 0.127 Uiso 1 1 d R U . . .
H13B H -0.064494 0.603197 0.710263 0.127 Uiso 1 1 d R U . . .
H13C H 0.015536 0.605777 0.722053 0.127 Uiso 1 1 d R U . . .
C67 C -0.0328(8) 0.5534(9) 0.5876(3) 0.091(4) Uani 1 1 d . U . . .
H67A H -0.032907 0.562264 0.567991 0.136 Uiso 1 1 calc R U . . .
H67B H 0.010009 0.572076 0.597191 0.136 Uiso 1 1 calc R U . . .
H67C H -0.073081 0.576291 0.594476 0.136 Uiso 1 1 calc R U . . .
C135 C 0.7539(9) 0.7088(10) 0.5722(3) 0.095(5) Uani 1 1 d . U . . .
H135 H 0.790298 0.675865 0.571063 0.114 Uiso 1 1 calc R U . . .
C17 C 0.3049(9) 0.7049(8) 0.8164(3) 0.087(5) Uani 1 1 d . U . . .
H17 H 0.295830 0.657364 0.820478 0.105 Uiso 1 1 calc R U . . .
C137 C 0.7181(9) 0.7329(9) 0.5488(3) 0.085(4) Uani 1 1 d . U . . .
H137 H 0.729637 0.716489 0.531604 0.102 Uiso 1 1 calc R U . . .
C69 C 0.3590(10) 0.8134(9) 0.8290(4) 0.100(5) Uani 1 1 d . U . . .
H69 H 0.387015 0.840803 0.841844 0.120 Uiso 1 1 calc R U . . .
C139 C 0.1488(11) 0.5387(11) 0.4684(3) 0.113(6) Uani 1 1 d . U . . .
H139 H 0.137038 0.557780 0.450731 0.136 Uiso 1 1 calc R U . . .
C35 C 0.0997(9) 0.7143(10) 0.4850(3) 0.092(4) Uani 1 1 d . U . . .
C141 C 0.0471(8) 0.7796(10) 0.7882(4) 0.102(5) Uani 1 1 d . U . . .
H141 H 0.034843 0.811443 0.801781 0.123 Uiso 1 1 calc R U . . .
C71 C 0.5782(11) 0.8553(9) 0.5278(3) 0.103(5) Uani 1 1 d . U . . .
H71A H 0.562940 0.871769 0.509323 0.154 Uiso 1 1 calc R U . . .
H71B H 0.597846 0.894516 0.538795 0.154 Uiso 1 1 calc R U . . .
H71C H 0.538424 0.835924 0.536216 0.154 Uiso 1 1 calc R U . . .
C143 C 0.2789(12) 1.1654(12) 0.6605(4) 0.128(7) Uani 1 1 d . U . . .
H14A H 0.291660 1.189480 0.644060 0.192 Uiso 1 1 calc R U . . .
H14B H 0.281291 1.114694 0.657731 0.192 Uiso 1 1 calc R U . . .
H14C H 0.311278 1.178865 0.676136 0.192 Uiso 1 1 calc R U . . .
C9 C 0.3479(11) 0.7450(9) 0.8342(4) 0.114(6) Uani 1 1 d . U . . .
H9 H 0.369947 0.724347 0.850305 0.137 Uiso 1 1 calc R U . . .
C145 C 0.1012(11) 0.4972(10) 0.4805(3) 0.106(5) Uani 1 1 d . U . . .
H145 H 0.057488 0.486938 0.470834 0.127 Uiso 1 1 calc R U . . .
C73 C 0.4326(10) 0.5060(10) 0.7691(6) 0.150(10) Uani 1 1 d . U . . .
H73A H 0.422396 0.530370 0.751689 0.224 Uiso 1 1 calc R U . . .
H73B H 0.474283 0.477127 0.768398 0.224 Uiso 1 1 calc R U . . .
H73C H 0.440534 0.540407 0.783876 0.224 Uiso 1 1 calc R U . . .
C147 C 0.2926(15) 0.9455(12) 0.7764(5) 0.175(11) Uani 1 1 d . U . . .
H14D H 0.299644 0.922006 0.759127 0.262 Uiso 1 1 calc R U . . .
H14E H 0.303821 0.995246 0.774961 0.262 Uiso 1 1 calc R U . . .
H14F H 0.243995 0.940304 0.780193 0.262 Uiso 1 1 calc R U . . .
C37 C 0.6495(13) 0.5507(14) 0.6633(5) 0.100(8) Uani 0.68(2) 1 d . U P A 1
H37A H 0.609204 0.581798 0.660090 0.150 Uiso 0.68(2) 1 calc R U P A 1
H37B H 0.634328 0.505051 0.669534 0.150 Uiso 0.68(2) 1 calc R U P A 1
H37C H 0.671429 0.544895 0.646237 0.150 Uiso 0.68(2) 1 calc R U P A 1
C149 C 0.7202(9) 1.0386(9) 0.6351(3) 0.0871(17) Uani 1 1 d . U . . .
H149 H 0.733457 1.086336 0.636956 0.105 Uiso 1 1 calc R U . . .
C75 C 0.7313(9) 0.9280(8) 0.6162(3) 0.0867(17) Uani 1 1 d . U . . .
H75 H 0.750462 0.897462 0.603630 0.104 Uiso 1 1 calc R U . . .
O11 O 0.7732(17) 1.0223(14) 0.5898(5) 0.0878(17) Uani 0.398(16) 1 d D U P B 1
C151 C 0.0661(9) 1.0196(8) 0.6828(3) 0.082(4) Uani 1 1 d . U . . .
C19 C 0.0905(12) 1.0580(10) 0.7036(4) 0.108(5) Uani 1 1 d . U . . .
C153 C 0.1603(12) 1.0602(9) 0.7120(4) 0.109(5) Uani 1 1 d . U . . .
C77 C 0.7502(9) 0.9993(9) 0.6158(3) 0.0875(17) Uani 1 1 d D U . . .
C155 C 0.813(2) 1.0691(19) 0.5731(8) 0.0880(18) Uani 0.398(16) 1 d D U P B 1
H15A H 0.825843 1.043613 0.557054 0.132 Uiso 0.398(16) 1 calc R U P B 1
H15B H 0.854680 1.085469 0.583945 0.132 Uiso 0.398(16) 1 calc R U P B 1
H15C H 0.783719 1.109355 0.567097 0.132 Uiso 0.398(16) 1 calc R U P B 1
C39 C 0.737(2) 0.555(2) 0.7172(10) 0.079(13) Uani 0.32(2) 1 d D U P A 2
H39A H 0.767831 0.514371 0.714965 0.118 Uiso 0.32(2) 1 calc R U P A 2
H39B H 0.699448 0.540492 0.727947 0.118 Uiso 0.32(2) 1 calc R U P A 2
H39C H 0.764274 0.592165 0.726779 0.118 Uiso 0.32(2) 1 calc R U P A 2
O3 O 0.8075(10) 1.0180(9) 0.6013(4) 0.0878(17) Uani 0.602(16) 1 d D U P B 2
C157 C 0.8187(15) 1.0918(10) 0.5963(6) 0.0880(18) Uani 0.602(16) 1 d D U P B 2
H15D H 0.852121 1.097042 0.582640 0.132 Uiso 0.602(16) 1 calc R U P B 2
H15E H 0.836980 1.114563 0.613344 0.132 Uiso 0.602(16) 1 calc R U P B 2
H15F H 0.774511 1.113718 0.589547 0.132 Uiso 0.602(16) 1 calc R U P B 2


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 Ag6 2.8647(10) . ?
Ag1 Ag8 2.8646(11) . ?
Ag1 Ag10 2.8870(11) . ?
Ag1 Ag12 2.8540(11) . ?
Ag1 Ag2 3.0274(11) . ?
Ag1 Ag11 3.0451(12) . ?
Ag1 S1 2.551(3) . ?
Ag1 S5 2.544(3) . ?
Ag4 Ag6 2.8761(11) . ?
Ag4 Ag8 2.8656(11) . ?
Ag4 Ag10 2.8576(10) . ?
Ag4 Ag12 2.8646(11) . ?
Ag4 Ag14 3.0199(11) . ?
Ag4 Ag7 3.0002(11) . ?
Ag4 S4 2.548(3) . ?
Ag4 S12 2.547(3) . ?
Ag6 Ag8 2.8741(11) . ?
Ag6 Ag12 2.8691(11) . ?
Ag6 Ag7 3.0136(11) . ?
Ag6 Ag2 3.0210(11) . ?
Ag6 S8 2.557(3) . ?
Ag6 S9 2.554(3) . ?
Ag8 Ag10 2.8587(10) . ?
Ag8 Ag7 3.0223(10) . ?
Ag8 Ag11 3.0414(11) . ?
Ag8 S3 2.551(3) . ?
Ag8 S11 2.549(3) . ?
Ag10 Ag12 2.8636(11) . ?
Ag10 Ag14 2.9864(11) . ?
Ag10 Ag11 3.0361(12) . ?
Ag10 S10 2.532(3) . ?
Ag10 S2 2.547(3) . ?
Ag12 Ag14 3.0372(11) . ?
Ag12 Ag2 3.0505(11) . ?
Ag12 S6 2.539(3) . ?
Ag12 S7 2.551(3) . ?
Ag14 S4 2.565(3) . ?
Ag14 S6 2.546(3) . ?
Ag14 S2 2.535(3) . ?
Ag7 S8 2.534(3) . ?
Ag7 S12 2.529(3) . ?
Ag7 S3 2.539(3) . ?
Ag2 S1 2.517(3) . ?
Ag2 S7 2.539(3) . ?
Ag2 S9 2.518(3) . ?
Ag9 S1 2.633(3) . ?
Ag9 S6 2.637(3) . ?
Ag9 S10 2.614(3) . ?
Ag9 P1 2.410(3) . ?
Ag5 S3 2.629(3) . ?
Ag5 S9 2.663(3) . ?
Ag5 S5 2.627(3) . ?
Ag5 P4 2.423(3) . ?
Ag11 S10 2.533(3) . ?
Ag11 S5 2.556(3) . ?
Ag11 S11 2.547(3) . ?
Ag3 S4 2.627(3) . ?
Ag3 S8 2.630(3) . ?
Ag3 S7 2.654(3) . ?
Ag3 P3 2.408(3) . ?
Ag13 S12 2.661(3) . ?
Ag13 S2 2.664(3) . ?
Ag13 S11 2.631(3) . ?
Ag13 P2 2.419(3) . ?
S1 C12 1.742(11) . ?
S4 C68 1.739(11) . ?
S6 C6 1.755(10) . ?
S8 C62 1.754(11) . ?
S10 C64 1.750(10) . ?
S12 C22 1.776(10) . ?
S3 C20 1.751(12) . ?
S7 C54 1.772(10) . ?
S2 C1 1.763(10) . ?
S9 C42 1.777(11) . ?
S5 C14 1.760(11) . ?
S11 C34 1.769(12) . ?
P1 C46 1.825(12) . ?
P1 C70 1.831(11) . ?
P1 C104 1.796(7) . ?
P4 C78 1.820(12) . ?
P4 C82 1.815(12) . ?
P4 C130 1.822(7) . ?
P2 C26 1.832(12) . ?
P2 C5 1.809(12) . ?
P2 C81 1.797(16) . ?
P3 C79 1.811(12) . ?
P3 C41 1.810(14) . ?
P3 C53 1.831(13) . ?
F1 C18 1.358(11) . ?
F4 C38 1.334(12) . ?
F6 C32 1.344(13) . ?
F8 C8 1.331(13) . ?
F10 C4 1.344(13) . ?
F12 C10 1.337(12) . ?
F14 C50 1.336(14) . ?
F16 C30 1.352(13) . ?
F18 C96 1.352(13) . ?
F20 C36 1.355(14) . ?
F22 C24 1.345(13) . ?
F24 C44 1.335(12) . ?
F26 C28 1.352(13) . ?
F28 C16 1.343(14) . ?
F30 C60 1.336(14) . ?
F32 C52 1.350(15) . ?
F34 C40 1.345(15) . ?
F36 C49 1.358(15) . ?
F38 C58 1.348(13) . ?
F40 C72 1.345(14) . ?
F42 C107 1.326(13) . ?
F44 C152 1.349(14) . ?
F46 C102 1.308(14) . ?
F48 C83 1.330(14) . ?
F50 C94 1.344(13) . ?
F52 C150 1.343(14) . ?
F54 C126 1.341(16) . ?
F56 C118 1.353(12) . ?
F58 C90 1.300(13) . ?
F60 C56 1.342(15) . ?
F15 C84 1.335(15) . ?
F31 C113 1.342(13) . ?
F2 C48 1.339(14) . ?
F33 C116 1.315(13) . ?
F17 C93 1.315(14) . ?
F35 C146 1.327(14) . ?
F9 C154 1.341(14) . ?
F37 C85 1.318(13) . ?
F19 C98 1.331(16) . ?
F39 C25 1.342(14) . ?
F5 C122 1.320(14) . ?
F41 C144 1.343(14) . ?
F21 C55 1.346(14) . ?
O1 C80 1.373(15) . ?
O1 C133 1.421(17) . ?
F43 C47 1.358(18) . ?
F11 C142 1.330(17) . ?
O4 C92 1.355(15) . ?
O4 C45 1.395(17) . ?
F45 C121 1.342(15) . ?
O6 C158 1.372(16) . ?
O6 C127 1.449(16) . ?
O8 C87 1.378(17) . ?
O8 C67 1.444(19) . ?
O10 C11 1.344(18) . ?
O10 C71 1.44(2) . ?
F23 C57 1.333(17) . ?
F47 C151 1.376(19) . ?
F3 C13 1.334(18) . ?
F49 C105 1.357(16) . ?
F25 C65 1.347(18) . ?
F51 C29 1.319(17) . ?
O12 C97 1.377(17) . ?
O12 C129 1.432(18) . ?
C1 C8 1.383(15) . ?
C1 C10 1.405(15) . ?
C4 C6 1.380(14) . ?
C4 C152 1.378(16) . ?
F13 C27 1.339(15) . ?
C6 C28 1.384(15) . ?
F53 C86 1.345(13) . ?
F27 C51 1.304(15) . ?
C8 C90 1.377(15) . ?
C10 C83 1.380(15) . ?
O13 C59 1.40(2) . ?
O13 C33 1.377(19) . ?
C12 C32 1.383(16) . ?
C12 C36 1.406(15) . ?
F55 C125 1.306(16) . ?
O7 C138 1.373(15) . ?
O7 C143 1.49(2) . ?
C14 C60 1.411(17) . ?
C14 C47 1.386(16) . ?
O2 C15 1.386(18) . ?
O2 C37 1.58(3) . ?
O2 C39 1.72(4) . ?
C16 C56 1.356(16) . ?
C16 C68 1.406(15) . ?
C18 C20 1.387(15) . ?
C18 C107 1.363(16) . ?
C20 C96 1.390(15) . ?
C22 C24 1.374(15) . ?
C22 C44 1.381(15) . ?
C24 C144 1.376(16) . ?
C26 C76 1.393(17) . ?
C26 C117 1.357(18) . ?
C28 C116 1.377(16) . ?
C30 C54 1.384(15) . ?
C30 C55 1.366(17) . ?
C32 C154 1.378(16) . ?
C34 C126 1.379(18) . ?
C34 C150 1.380(16) . ?
C36 C48 1.395(16) . ?
C38 C54 1.377(15) . ?
C38 C102 1.378(15) . ?
O9 C7 1.340(17) . ?
O9 C147 1.61(2) . ?
C40 C62 1.389(17) . ?
C40 C57 1.389(17) . ?
C42 C50 1.392(16) . ?
C42 C49 1.338(16) . ?
C44 C72 1.370(16) . ?
C46 C66 1.378(16) . ?
C46 C23 1.373(17) . ?
C48 C85 1.383(18) . ?
C50 C98 1.392(16) . ?
C52 C62 1.381(17) . ?
C52 C13 1.374(17) . ?
F7 C101 1.334(16) . ?
C56 C51 1.38(2) . ?
C58 C64 1.387(15) . ?
C58 C84 1.386(15) . ?
C60 C151 1.368(17) . ?
C64 C122 1.387(16) . ?
C66 H66 0.9500 . ?
C66 C80 1.379(16) . ?
C68 C113 1.376(16) . ?
C70 C100 1.349(16) . ?
C70 C17 1.371(16) . ?
C72 C146 1.363(18) . ?
C74 H74 0.9500 . ?
C74 C82 1.380(16) . ?
C74 C92 1.391(16) . ?
C76 H76 0.9500 . ?
C76 C11 1.399(17) . ?
C78 C128 1.402(16) . ?
C78 C109 1.373(16) . ?
C80 C63 1.374(19) . ?
C82 C120 1.401(16) . ?
C84 C86 1.355(19) . ?
F57 C35 1.342(15) . ?
C86 C105 1.36(2) . ?
C88 H88 0.9500 . ?
C88 C148 1.39(2) . ?
C88 C41 1.381(16) . ?
O5 C112 1.403(13) . ?
O5 C73 1.41(2) . ?
C90 C118 1.388(18) . ?
C92 C111 1.405(18) . ?
C94 C96 1.353(17) . ?
C94 C93 1.393(17) . ?
C98 C27 1.38(2) . ?
C100 H100 0.9500 . ?
C100 C7 1.383(18) . ?
C102 C25 1.379(17) . ?
C104 C106 1.3900 . ?
C104 C114 1.3900 . ?
C106 H106 0.9500 . ?
C106 C108 1.3900 . ?
C108 H108 0.9500 . ?
C108 C110 1.3900 . ?
C110 H110 0.9500 . ?
C110 C112 1.3900 . ?
C112 C114 1.3900 . ?
C114 H114 0.9500 . ?
C116 C121 1.381(18) . ?
C118 C83 1.361(17) . ?
C120 H120 0.9500 . ?
C120 C99 1.408(17) . ?
C122 C105 1.381(17) . ?
C124 H124 0.9500 . ?
C124 C79 1.404(18) . ?
C124 C33 1.389(18) . ?
C126 C65 1.37(2) . ?
C128 H128 0.9500 . ?
C128 C158 1.375(17) . ?
C130 C132 1.3900 . ?
C130 C140 1.3900 . ?
C132 H132 0.9500 . ?
C132 C134 1.3900 . ?
C134 H134 0.9500 . ?
C134 C136 1.3900 . ?
C136 H136 0.9500 . ?
C136 C138 1.3900 . ?
C138 C140 1.3900 . ?
C140 H140 0.9500 . ?
C142 C150 1.398(18) . ?
C142 C101 1.37(2) . ?
C144 C146 1.375(18) . ?
C148 H148 0.9500 . ?
C148 C123 1.35(2) . ?
C152 C121 1.349(19) . ?
C154 C85 1.388(18) . ?
C156 H156 0.9500 . ?
C156 C89 1.39(2) . ?
C156 C149 1.41(2) . ?
C158 C115 1.385(18) . ?
C79 C2 1.394(19) . ?
C5 C43 1.388(17) . ?
C5 C95 1.379(18) . ?
C81 C89 1.37(2) . ?
C81 C75 1.43(2) . ?
C41 C21 1.394(17) . ?
C21 H21 0.9500 . ?
C21 C97 1.370(19) . ?
C43 H43 0.9500 . ?
C43 C31 1.393(18) . ?
C87 C91 1.387(18) . ?
C87 C61 1.39(2) . ?
C11 C137 1.41(2) . ?
C89 H89 0.9500 . ?
C45 H45A 0.9800 . ?
C45 H45B 0.9800 . ?
C45 H45C 0.9800 . ?
F29 C153 1.30(2) . ?
C91 H91 0.9500 . ?
C91 C53 1.373(18) . ?
C23 H23 0.9500 . ?
C23 C141 1.38(2) . ?
C93 C107 1.391(16) . ?
C47 C153 1.41(2) . ?
C95 H95 0.9500 . ?
C95 C15 1.36(2) . ?
C3 H3 0.9500 . ?
C3 C15 1.38(2) . ?
C3 C31 1.36(2) . ?
C97 C123 1.397(18) . ?
C49 C29 1.400(17) . ?
C99 H99 0.9500 . ?
C99 C111 1.355(18) . ?
C25 C55 1.371(19) . ?
C101 C65 1.39(2) . ?
C51 C125 1.41(2) . ?
C103 H103 0.9500 . ?
C103 C53 1.365(19) . ?
C103 C119 1.412(19) . ?
C13 C35 1.39(2) . ?
F59 C19 1.343(17) . ?
C27 C29 1.37(2) . ?
C109 H109 0.9500 . ?
C109 C131 1.387(19) . ?
C111 H111 0.9500 . ?
C7 C69 1.36(2) . ?
C113 C125 1.377(17) . ?
C57 C35 1.35(2) . ?
C115 H115 0.9500 . ?
C115 C131 1.38(2) . ?
C117 H117 0.9500 . ?
C117 C135 1.37(2) . ?
C59 H59A 0.9800 . ?
C59 H59B 0.9800 . ?
C59 H59C 0.9800 . ?
C119 H119 0.9500 . ?
C119 C61 1.38(2) . ?
C61 H61 0.9500 . ?
C123 H123 0.9500 . ?
C31 H31 0.9500 . ?
C63 H63 0.9500 . ?
C63 C141 1.36(2) . ?
C127 H12A 0.9800 . ?
C127 H12B 0.9800 . ?
C127 H12C 0.9800 . ?
C2 H2 0.9500 . ?
C2 C145 1.39(2) . ?
C129 H12D 0.9800 . ?
C129 H12E 0.9800 . ?
C129 H12F 0.9800 . ?
C131 H131 0.9500 . ?
C33 C139 1.39(2) . ?
C133 H13A 0.9800 . ?
C133 H13B 0.9798 . ?
C133 H13C 0.9800 . ?
C67 H67A 0.9800 . ?
C67 H67B 0.9800 . ?
C67 H67C 0.9800 . ?
C135 H135 0.9500 . ?
C135 C137 1.36(2) . ?
C17 H17 0.9500 . ?
C17 C9 1.38(2) . ?
C137 H137 0.9500 . ?
C69 H69 0.9500 . ?
C69 C9 1.35(2) . ?
C139 H139 0.9500 . ?
C139 C145 1.39(2) . ?
C141 H141 0.9500 . ?
C71 H71A 0.9800 . ?
C71 H71B 0.9800 . ?
C71 H71C 0.9800 . ?
C143 H14A 0.9800 . ?
C143 H14B 0.9800 . ?
C143 H14C 0.9800 . ?
C9 H9 0.9500 . ?
C145 H145 0.9500 . ?
C73 H73A 0.9800 . ?
C73 H73B 0.9800 . ?
C73 H73C 0.9800 . ?
C147 H14D 0.9800 . ?
C147 H14E 0.9800 . ?
C147 H14F 0.9800 . ?
C37 H37A 0.9800 . ?
C37 H37B 0.9800 . ?
C37 H37C 0.9800 . ?
C149 H149 0.9500 . ?
C149 C77 1.38(2) . ?
C75 H75 0.9500 . ?
C75 C77 1.41(2) . ?
O11 C77 1.460(17) . ?
O11 C155 1.476(19) . ?
C151 C19 1.31(3) . ?
C19 C153 1.37(3) . ?
C77 O3 1.417(16) . ?
C155 H15A 0.9800 . ?
C155 H15B 0.9800 . ?
C155 H15C 0.9800 . ?
C39 H39A 0.9800 . ?
C39 H39B 0.9800 . ?
C39 H39C 0.9800 . ?
O3 C157 1.453(17) . ?
C157 H15D 0.9800 . ?
C157 H15E 0.9800 . ?
C157 H15F 0.9800 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Ag6 Ag1 Ag10 89.99(3) . . ?
Ag6 Ag1 Ag2 61.62(3) . . ?
Ag6 Ag1 Ag11 122.06(3) . . ?
Ag8 Ag1 Ag6 60.22(3) . . ?
Ag8 Ag1 Ag10 59.61(3) . . ?
Ag8 Ag1 Ag2 121.81(3) . . ?
Ag8 Ag1 Ag11 61.86(3) . . ?
Ag10 Ag1 Ag2 122.24(3) . . ?
Ag10 Ag1 Ag11 61.50(3) . . ?
Ag12 Ag1 Ag6 60.23(3) . . ?
Ag12 Ag1 Ag8 89.91(3) . . ?
Ag12 Ag1 Ag10 59.84(3) . . ?
Ag12 Ag1 Ag2 62.40(3) . . ?
Ag12 Ag1 Ag11 121.30(3) . . ?
Ag2 Ag1 Ag11 175.47(4) . . ?
S1 Ag1 Ag6 112.37(7) . . ?
S1 Ag1 Ag8 165.82(7) . . ?
S1 Ag1 Ag10 110.43(7) . . ?
S1 Ag1 Ag12 76.00(7) . . ?
S1 Ag1 Ag2 52.81(6) . . ?
S1 Ag1 Ag11 124.35(7) . . ?
S5 Ag1 Ag6 109.10(6) . . ?
S5 Ag1 Ag8 75.41(7) . . ?
S5 Ag1 Ag10 112.61(7) . . ?
S5 Ag1 Ag12 165.16(7) . . ?
S5 Ag1 Ag2 123.66(7) . . ?
S5 Ag1 Ag11 53.51(7) . . ?
S5 Ag1 S1 118.72(9) . . ?
Ag6 Ag4 Ag14 122.04(3) . . ?
Ag6 Ag4 Ag7 61.66(3) . . ?
Ag8 Ag4 Ag6 60.08(3) . . ?
Ag8 Ag4 Ag14 120.91(3) . . ?
Ag8 Ag4 Ag7 61.98(3) . . ?
Ag10 Ag4 Ag6 90.35(3) . . ?
Ag10 Ag4 Ag8 59.93(3) . . ?
Ag10 Ag4 Ag12 60.06(3) . . ?
Ag10 Ag4 Ag14 61.00(3) . . ?
Ag10 Ag4 Ag7 121.89(3) . . ?
Ag12 Ag4 Ag6 59.97(3) . . ?
Ag12 Ag4 Ag8 89.68(3) . . ?
Ag12 Ag4 Ag14 62.08(3) . . ?
Ag12 Ag4 Ag7 121.62(3) . . ?
Ag7 Ag4 Ag14 175.90(4) . . ?
S4 Ag4 Ag6 108.72(7) . . ?
S4 Ag4 Ag8 164.72(7) . . ?
S4 Ag4 Ag10 112.65(7) . . ?
S4 Ag4 Ag12 75.25(7) . . ?
S4 Ag4 Ag14 54.07(6) . . ?
S4 Ag4 Ag7 124.01(7) . . ?
S12 Ag4 Ag6 112.92(7) . . ?
S12 Ag4 Ag8 75.65(7) . . ?
S12 Ag4 Ag10 108.95(7) . . ?
S12 Ag4 Ag12 165.10(7) . . ?
S12 Ag4 Ag14 123.47(7) . . ?
S12 Ag4 Ag7 53.49(6) . . ?
S12 Ag4 S4 119.51(9) . . ?
Ag1 Ag6 Ag4 89.87(3) . . ?
Ag1 Ag6 Ag8 59.89(3) . . ?
Ag1 Ag6 Ag12 59.70(3) . . ?
Ag1 Ag6 Ag7 121.60(3) . . ?
Ag1 Ag6 Ag2 61.84(3) . . ?
Ag4 Ag6 Ag7 61.20(3) . . ?
Ag4 Ag6 Ag2 122.12(3) . . ?
Ag8 Ag6 Ag4 59.78(3) . . ?
Ag8 Ag6 Ag7 61.72(3) . . ?
Ag8 Ag6 Ag2 121.71(3) . . ?
Ag12 Ag6 Ag4 59.82(3) . . ?
Ag12 Ag6 Ag8 89.42(3) . . ?
Ag12 Ag6 Ag7 121.00(3) . . ?
Ag12 Ag6 Ag2 62.32(3) . . ?
Ag7 Ag6 Ag2 175.87(3) . . ?
S8 Ag6 Ag1 166.08(7) . . ?
S8 Ag6 Ag4 76.38(7) . . ?
S8 Ag6 Ag8 113.21(7) . . ?
S8 Ag6 Ag12 110.12(7) . . ?
S8 Ag6 Ag7 53.35(6) . . ?
S8 Ag6 Ag2 123.93(7) . . ?
S9 Ag6 Ag1 77.05(6) . . ?
S9 Ag6 Ag4 166.80(7) . . ?
S9 Ag6 Ag8 110.81(7) . . ?
S9 Ag6 Ag12 113.39(7) . . ?
S9 Ag6 Ag7 124.51(7) . . ?
S9 Ag6 Ag2 52.89(6) . . ?
S9 Ag6 S8 116.75(9) . . ?
Ag1 Ag8 Ag4 90.08(3) . . ?
Ag1 Ag8 Ag6 59.89(3) . . ?
Ag1 Ag8 Ag7 121.30(3) . . ?
Ag1 Ag8 Ag11 61.99(3) . . ?
Ag4 Ag8 Ag6 60.14(3) . . ?
Ag4 Ag8 Ag7 61.20(3) . . ?
Ag4 Ag8 Ag11 121.73(3) . . ?
Ag6 Ag8 Ag7 61.41(3) . . ?
Ag6 Ag8 Ag11 121.87(3) . . ?
Ag10 Ag8 Ag1 60.59(3) . . ?
Ag10 Ag8 Ag4 59.90(3) . . ?
Ag10 Ag8 Ag6 90.36(3) . . ?
Ag10 Ag8 Ag7 121.08(3) . . ?
Ag10 Ag8 Ag11 61.85(3) . . ?
Ag7 Ag8 Ag11 176.18(4) . . ?
S3 Ag8 Ag1 109.14(7) . . ?
S3 Ag8 Ag4 112.46(7) . . ?
S3 Ag8 Ag6 75.19(7) . . ?
S3 Ag8 Ag10 165.45(7) . . ?
S3 Ag8 Ag7 53.38(6) . . ?
S3 Ag8 Ag11 124.48(7) . . ?
S11 Ag8 Ag1 113.45(7) . . ?
S11 Ag8 Ag4 110.05(7) . . ?
S11 Ag8 Ag6 166.47(7) . . ?
S11 Ag8 Ag10 76.26(7) . . ?
S11 Ag8 Ag7 124.01(7) . . ?
S11 Ag8 Ag11 53.33(7) . . ?
S11 Ag8 S3 118.23(9) . . ?
Ag1 Ag10 Ag14 122.00(3) . . ?
Ag1 Ag10 Ag11 61.81(3) . . ?
Ag4 Ag10 Ag1 89.79(3) . . ?
Ag4 Ag10 Ag8 60.17(3) . . ?
Ag4 Ag10 Ag12 60.09(3) . . ?
Ag4 Ag10 Ag14 62.18(3) . . ?
Ag4 Ag10 Ag11 122.20(3) . . ?
Ag8 Ag10 Ag1 59.81(3) . . ?
Ag8 Ag10 Ag12 89.84(3) . . ?
Ag8 Ag10 Ag14 122.33(3) . . ?
Ag8 Ag10 Ag11 62.04(3) . . ?
Ag12 Ag10 Ag1 59.51(3) . . ?
Ag12 Ag10 Ag14 62.51(3) . . ?
Ag12 Ag10 Ag11 121.29(3) . . ?
Ag14 Ag10 Ag11 174.97(3) . . ?
S10 Ag10 Ag1 74.73(7) . . ?
S10 Ag10 Ag4 164.16(7) . . ?
S10 Ag10 Ag8 112.66(7) . . ?
S10 Ag10 Ag12 107.73(7) . . ?
S10 Ag10 Ag14 123.40(7) . . ?
S10 Ag10 Ag11 53.19(7) . . ?
S10 Ag10 S2 119.12(9) . . ?
S2 Ag10 Ag1 165.99(7) . . ?
S2 Ag10 Ag4 76.50(6) . . ?
S2 Ag10 Ag8 109.60(7) . . ?
S2 Ag10 Ag12 114.17(7) . . ?
S2 Ag10 Ag14 53.83(7) . . ?
S2 Ag10 Ag11 123.39(7) . . ?
Ag1 Ag12 Ag4 90.32(3) . . ?
Ag1 Ag12 Ag6 60.07(3) . . ?
Ag1 Ag12 Ag10 60.65(3) . . ?
Ag1 Ag12 Ag14 121.36(3) . . ?
Ag1 Ag12 Ag2 61.58(3) . . ?
Ag4 Ag12 Ag6 60.21(3) . . ?
Ag4 Ag12 Ag14 61.47(3) . . ?
Ag4 Ag12 Ag2 121.48(3) . . ?
Ag6 Ag12 Ag14 121.68(3) . . ?
Ag6 Ag12 Ag2 61.28(3) . . ?
Ag10 Ag12 Ag4 59.85(3) . . ?
Ag10 Ag12 Ag6 90.37(3) . . ?
Ag10 Ag12 Ag14 60.72(3) . . ?
Ag10 Ag12 Ag2 122.23(3) . . ?
Ag14 Ag12 Ag2 176.38(4) . . ?
S6 Ag12 Ag1 111.16(7) . . ?
S6 Ag12 Ag4 113.47(7) . . ?
S6 Ag12 Ag6 167.57(7) . . ?
S6 Ag12 Ag10 77.33(7) . . ?
S6 Ag12 Ag14 53.44(6) . . ?
S6 Ag12 Ag2 124.16(7) . . ?
S6 Ag12 S7 116.58(9) . . ?
S7 Ag12 Ag1 112.68(7) . . ?
S7 Ag12 Ag4 109.73(7) . . ?
S7 Ag12 Ag6 75.78(7) . . ?
S7 Ag12 Ag10 165.93(7) . . ?
S7 Ag12 Ag14 124.72(7) . . ?
S7 Ag12 Ag2 53.00(7) . . ?
Ag4 Ag14 Ag12 56.45(2) . . ?
Ag10 Ag14 Ag4 56.82(2) . . ?
Ag10 Ag14 Ag12 56.76(2) . . ?
S4 Ag14 Ag4 53.53(7) . . ?
S4 Ag14 Ag10 108.12(7) . . ?
S4 Ag14 Ag12 71.96(6) . . ?
S6 Ag14 Ag4 108.35(7) . . ?
S6 Ag14 Ag10 74.96(7) . . ?
S6 Ag14 Ag12 53.21(6) . . ?
S6 Ag14 S4 111.77(9) . . ?
S2 Ag14 Ag4 73.72(6) . . ?
S2 Ag14 Ag10 54.19(6) . . ?
S2 Ag14 Ag12 108.97(7) . . ?
S2 Ag14 S4 115.94(9) . . ?
S2 Ag14 S6 117.84(9) . . ?
Ag4 Ag7 Ag6 57.14(2) . . ?
Ag4 Ag7 Ag8 56.82(2) . . ?
Ag6 Ag7 Ag8 56.87(2) . . ?
S8 Ag7 Ag4 74.45(6) . . ?
S8 Ag7 Ag6 54.05(6) . . ?
S8 Ag7 Ag8 109.19(7) . . ?
S8 Ag7 S3 114.35(9) . . ?
S12 Ag7 Ag4 54.04(6) . . ?
S12 Ag7 Ag6 109.10(7) . . ?
S12 Ag7 Ag8 73.08(6) . . ?
S12 Ag7 S8 116.83(9) . . ?
S12 Ag7 S3 114.89(9) . . ?
S3 Ag7 Ag4 108.60(7) . . ?
S3 Ag7 Ag6 72.88(7) . . ?
S3 Ag7 Ag8 53.77(6) . . ?
Ag1 Ag2 Ag12 56.01(3) . . ?
Ag6 Ag2 Ag1 56.54(2) . . ?
Ag6 Ag2 Ag12 56.40(2) . . ?
S1 Ag2 Ag1 53.83(7) . . ?
S1 Ag2 Ag6 108.44(7) . . ?
S1 Ag2 Ag12 72.91(6) . . ?
S1 Ag2 S7 114.05(9) . . ?
S1 Ag2 S9 116.57(10) . . ?
S7 Ag2 Ag1 107.63(7) . . ?
S7 Ag2 Ag6 73.22(7) . . ?
S7 Ag2 Ag12 53.37(6) . . ?
S9 Ag2 Ag1 74.57(7) . . ?
S9 Ag2 Ag6 53.99(7) . . ?
S9 Ag2 Ag12 108.70(7) . . ?
S9 Ag2 S7 114.91(9) . . ?
S1 Ag9 S6 100.45(9) . . ?
S10 Ag9 S1 99.42(9) . . ?
S10 Ag9 S6 100.03(9) . . ?
P1 Ag9 S1 115.05(10) . . ?
P1 Ag9 S6 119.76(10) . . ?
P1 Ag9 S10 118.60(9) . . ?
S3 Ag5 S9 99.06(9) . . ?
S5 Ag5 S3 98.86(9) . . ?
S5 Ag5 S9 100.31(9) . . ?
P4 Ag5 S3 117.84(10) . . ?
P4 Ag5 S9 115.71(10) . . ?
P4 Ag5 S5 121.18(10) . . ?
Ag8 Ag11 Ag1 56.15(3) . . ?
Ag10 Ag11 Ag1 56.69(3) . . ?
Ag10 Ag11 Ag8 56.12(2) . . ?
S10 Ag11 Ag1 71.89(7) . . ?
S10 Ag11 Ag8 106.95(7) . . ?
S10 Ag11 Ag10 53.15(7) . . ?
S10 Ag11 S5 114.21(10) . . ?
S10 Ag11 S11 115.79(10) . . ?
S5 Ag11 Ag1 53.17(7) . . ?
S5 Ag11 Ag8 72.12(6) . . ?
S5 Ag11 Ag10 107.66(7) . . ?
S11 Ag11 Ag1 107.84(7) . . ?
S11 Ag11 Ag8 53.38(7) . . ?
S11 Ag11 Ag10 73.09(7) . . ?
S11 Ag11 S5 113.43(9) . . ?
S4 Ag3 S8 100.21(9) . . ?
S4 Ag3 S7 98.04(8) . . ?
S8 Ag3 S7 99.63(9) . . ?
P3 Ag3 S4 120.67(11) . . ?
P3 Ag3 S8 118.82(10) . . ?
P3 Ag3 S7 115.49(10) . . ?
S12 Ag13 S2 97.26(9) . . ?
S11 Ag13 S12 98.40(9) . . ?
S11 Ag13 S2 98.48(9) . . ?
P2 Ag13 S12 115.78(10) . . ?
P2 Ag13 S2 118.49(10) . . ?
P2 Ag13 S11 123.51(10) . . ?
Ag1 S1 Ag9 90.57(9) . . ?
Ag2 S1 Ag1 73.36(7) . . ?
Ag2 S1 Ag9 134.30(11) . . ?
C12 S1 Ag1 109.2(4) . . ?
C12 S1 Ag2 113.0(4) . . ?
C12 S1 Ag9 112.7(4) . . ?
Ag4 S4 Ag14 72.40(7) . . ?
Ag4 S4 Ag3 91.84(9) . . ?
Ag14 S4 Ag3 136.70(11) . . ?
C68 S4 Ag4 112.4(4) . . ?
C68 S4 Ag14 112.3(4) . . ?
C68 S4 Ag3 111.0(4) . . ?
Ag12 S6 Ag14 73.35(7) . . ?
Ag12 S6 Ag9 89.80(9) . . ?
Ag14 S6 Ag9 132.29(12) . . ?
C6 S6 Ag12 112.8(3) . . ?
C6 S6 Ag14 112.9(3) . . ?
C6 S6 Ag9 114.7(3) . . ?
Ag6 S8 Ag3 91.18(9) . . ?
Ag7 S8 Ag6 72.60(7) . . ?
Ag7 S8 Ag3 133.47(11) . . ?
C62 S8 Ag6 113.6(4) . . ?
C62 S8 Ag7 112.1(4) . . ?
C62 S8 Ag3 114.3(4) . . ?
Ag10 S10 Ag9 92.40(9) . . ?
Ag10 S10 Ag11 73.66(7) . . ?
Ag11 S10 Ag9 136.20(11) . . ?
C64 S10 Ag10 113.8(4) . . ?
C64 S10 Ag9 109.6(4) . . ?
C64 S10 Ag11 114.1(4) . . ?
Ag4 S12 Ag13 93.29(9) . . ?
Ag7 S12 Ag4 72.47(7) . . ?
Ag7 S12 Ag13 135.51(11) . . ?
C22 S12 Ag4 110.7(3) . . ?
C22 S12 Ag7 109.6(4) . . ?
C22 S12 Ag13 114.8(4) . . ?
Ag8 S3 Ag5 91.76(9) . . ?
Ag7 S3 Ag8 72.85(7) . . ?
Ag7 S3 Ag5 135.14(11) . . ?
C20 S3 Ag8 111.3(3) . . ?
C20 S3 Ag7 111.6(4) . . ?
C20 S3 Ag5 113.2(4) . . ?
Ag12 S7 Ag3 91.55(9) . . ?
Ag2 S7 Ag12 73.64(8) . . ?
Ag2 S7 Ag3 134.12(11) . . ?
C54 S7 Ag12 110.8(3) . . ?
C54 S7 Ag2 113.7(3) . . ?
C54 S7 Ag3 112.2(3) . . ?
Ag10 S2 Ag13 92.18(9) . . ?
Ag14 S2 Ag10 71.99(7) . . ?
Ag14 S2 Ag13 135.86(10) . . ?
C1 S2 Ag10 111.1(4) . . ?
C1 S2 Ag14 111.1(4) . . ?
C1 S2 Ag13 113.1(4) . . ?
Ag6 S9 Ag5 90.39(9) . . ?
Ag2 S9 Ag6 73.12(7) . . ?
Ag2 S9 Ag5 133.08(11) . . ?
C42 S9 Ag6 111.1(4) . . ?
C42 S9 Ag2 111.4(4) . . ?
C42 S9 Ag5 115.5(4) . . ?
Ag1 S5 Ag5 91.73(9) . . ?
Ag1 S5 Ag11 73.32(8) . . ?
Ag11 S5 Ag5 136.18(11) . . ?
C14 S5 Ag1 114.3(3) . . ?
C14 S5 Ag5 110.6(4) . . ?
C14 S5 Ag11 113.1(4) . . ?
Ag8 S11 Ag13 92.58(9) . . ?
Ag11 S11 Ag8 73.28(8) . . ?
Ag11 S11 Ag13 135.53(12) . . ?
C34 S11 Ag8 111.4(4) . . ?
C34 S11 Ag11 111.5(4) . . ?
C34 S11 Ag13 112.9(4) . . ?
C46 P1 Ag9 111.4(4) . . ?
C46 P1 C70 106.5(6) . . ?
C70 P1 Ag9 113.3(4) . . ?
C104 P1 Ag9 110.3(3) . . ?
C104 P1 C46 108.9(5) . . ?
C104 P1 C70 106.2(5) . . ?
C78 P4 Ag5 111.3(4) . . ?
C78 P4 C130 107.2(5) . . ?
C82 P4 Ag5 112.0(4) . . ?
C82 P4 C78 107.2(5) . . ?
C82 P4 C130 106.5(5) . . ?
C130 P4 Ag5 112.3(3) . . ?
C26 P2 Ag13 112.6(4) . . ?
C5 P2 Ag13 111.8(4) . . ?
C5 P2 C26 106.0(6) . . ?
C81 P2 Ag13 113.3(6) . . ?
C81 P2 C26 104.8(7) . . ?
C81 P2 C5 108.0(7) . . ?
C79 P3 Ag3 112.3(4) . . ?
C79 P3 C53 106.3(6) . . ?
C41 P3 Ag3 113.8(4) . . ?
C41 P3 C79 105.0(6) . . ?
C41 P3 C53 106.6(6) . . ?
C53 P3 Ag3 112.2(4) . . ?
C80 O1 C133 116.5(10) . . ?
C92 O4 C45 117.1(11) . . ?
C158 O6 C127 117.9(10) . . ?
C87 O8 C67 117.8(12) . . ?
C11 O10 C71 116.5(11) . . ?
C97 O12 C129 117.0(13) . . ?
C8 C1 S2 122.7(9) . . ?
C8 C1 C10 116.1(9) . . ?
C10 C1 S2 121.1(8) . . ?
F10 C4 C6 119.8(10) . . ?
F10 C4 C152 117.9(10) . . ?
C152 C4 C6 122.3(11) . . ?
C4 C6 S6 122.6(8) . . ?
C4 C6 C28 115.4(10) . . ?
C28 C6 S6 121.8(8) . . ?
F8 C8 C1 119.1(9) . . ?
F8 C8 C90 117.5(10) . . ?
C90 C8 C1 123.4(11) . . ?
F12 C10 C1 120.5(9) . . ?
F12 C10 C83 117.3(10) . . ?
C83 C10 C1 122.1(11) . . ?
C33 O13 C59 118.4(12) . . ?
C32 C12 S1 123.7(8) . . ?
C32 C12 C36 115.0(10) . . ?
C36 C12 S1 121.3(9) . . ?
C138 O7 C143 119.0(12) . . ?
C60 C14 S5 121.7(8) . . ?
C47 C14 S5 122.5(11) . . ?
C47 C14 C60 115.4(12) . . ?
C15 O2 C37 117.2(14) . . ?
C15 O2 C39 110.0(18) . . ?
F28 C16 C56 117.9(11) . . ?
F28 C16 C68 118.6(10) . . ?
C56 C16 C68 123.5(12) . . ?
F1 C18 C20 119.8(10) . . ?
F1 C18 C107 115.8(10) . . ?
C107 C18 C20 124.4(10) . . ?
C18 C20 S3 122.5(8) . . ?
C18 C20 C96 114.3(11) . . ?
C96 C20 S3 123.0(9) . . ?
C24 C22 S12 120.6(8) . . ?
C24 C22 C44 116.9(10) . . ?
C44 C22 S12 122.2(8) . . ?
F22 C24 C22 121.2(10) . . ?
F22 C24 C144 116.3(10) . . ?
C22 C24 C144 122.5(11) . . ?
C76 C26 P2 115.8(9) . . ?
C117 C26 P2 123.4(11) . . ?
C117 C26 C76 120.7(12) . . ?
F26 C28 C6 120.0(10) . . ?
F26 C28 C116 116.2(10) . . ?
C116 C28 C6 123.8(11) . . ?
F16 C30 C54 120.9(10) . . ?
F16 C30 C55 117.6(11) . . ?
C55 C30 C54 121.5(11) . . ?
F6 C32 C12 119.5(10) . . ?
F6 C32 C154 116.6(11) . . ?
C154 C32 C12 123.9(11) . . ?
C126 C34 S11 120.9(10) . . ?
C126 C34 C150 116.7(12) . . ?
C150 C34 S11 122.1(10) . . ?
F20 C36 C12 119.7(10) . . ?
F20 C36 C48 117.7(10) . . ?
C48 C36 C12 122.6(12) . . ?
F4 C38 C54 120.0(9) . . ?
F4 C38 C102 117.0(10) . . ?
C54 C38 C102 123.0(11) . . ?
C7 O9 C147 115.4(14) . . ?
F34 C40 C62 121.0(10) . . ?
F34 C40 C57 117.0(12) . . ?
C57 C40 C62 122.1(13) . . ?
C50 C42 S9 119.5(9) . . ?
C49 C42 S9 122.9(9) . . ?
C49 C42 C50 116.8(11) . . ?
F24 C44 C22 120.0(10) . . ?
F24 C44 C72 119.2(11) . . ?
C72 C44 C22 120.8(11) . . ?
C66 C46 P1 118.2(9) . . ?
C23 C46 P1 121.6(10) . . ?
C23 C46 C66 119.7(12) . . ?
F2 C48 C36 118.9(12) . . ?
F2 C48 C85 121.5(11) . . ?
C85 C48 C36 119.7(12) . . ?
F14 C50 C42 121.3(10) . . ?
F14 C50 C98 116.7(11) . . ?
C98 C50 C42 121.8(13) . . ?
F32 C52 C62 119.5(11) . . ?
F32 C52 C13 117.0(13) . . ?
C13 C52 C62 123.5(14) . . ?
C30 C54 S7 121.0(8) . . ?
C38 C54 S7 121.8(8) . . ?
C38 C54 C30 116.9(10) . . ?
F60 C56 C16 120.1(14) . . ?
F60 C56 C51 119.3(12) . . ?
C16 C56 C51 120.7(13) . . ?
F38 C58 C64 120.4(9) . . ?
F38 C58 C84 116.7(11) . . ?
C84 C58 C64 122.9(12) . . ?
F30 C60 C14 119.6(10) . . ?
F30 C60 C151 119.6(13) . . ?
C151 C60 C14 120.8(14) . . ?
C40 C62 S8 121.2(10) . . ?
C52 C62 S8 122.9(10) . . ?
C52 C62 C40 115.7(11) . . ?
C58 C64 S10 122.0(9) . . ?
C58 C64 C122 115.6(10) . . ?
C122 C64 S10 121.8(9) . . ?
C46 C66 H66 119.9 . . ?
C80 C66 C46 120.3(12) . . ?
C80 C66 H66 119.9 . . ?
C16 C68 S4 123.6(9) . . ?
C113 C68 S4 121.4(9) . . ?
C113 C68 C16 114.6(10) . . ?
C100 C70 P1 117.8(9) . . ?
C100 C70 C17 119.6(12) . . ?
C17 C70 P1 122.5(10) . . ?
F40 C72 C44 118.7(11) . . ?
F40 C72 C146 119.5(11) . . ?
C146 C72 C44 121.7(12) . . ?
C82 C74 H74 119.8 . . ?
C82 C74 C92 120.4(12) . . ?
C92 C74 H74 119.8 . . ?
C26 C76 H76 120.2 . . ?
C26 C76 C11 119.5(13) . . ?
C11 C76 H76 120.2 . . ?
C128 C78 P4 116.9(8) . . ?
C109 C78 P4 123.8(10) . . ?
C109 C78 C128 119.2(12) . . ?
O1 C80 C66 123.7(12) . . ?
O1 C80 C63 115.6(12) . . ?
C63 C80 C66 120.7(13) . . ?
C74 C82 P4 117.0(9) . . ?
C74 C82 C120 120.6(11) . . ?
C120 C82 P4 122.2(9) . . ?
F15 C84 C58 120.2(12) . . ?
F15 C84 C86 120.8(11) . . ?
C86 C84 C58 118.9(13) . . ?
F53 C86 C84 119.6(14) . . ?
F53 C86 C105 119.9(13) . . ?
C84 C86 C105 120.5(11) . . ?
C148 C88 H88 120.5 . . ?
C41 C88 H88 120.5 . . ?
C41 C88 C148 119.1(13) . . ?
C112 O5 C73 117.1(12) . . ?
F58 C90 C8 121.6(12) . . ?
F58 C90 C118 120.7(10) . . ?
C8 C90 C118 117.6(11) . . ?
O4 C92 C74 125.6(12) . . ?
O4 C92 C111 115.0(11) . . ?
C74 C92 C111 119.4(12) . . ?
F50 C94 C96 120.3(11) . . ?
F50 C94 C93 118.8(11) . . ?
C96 C94 C93 120.8(11) . . ?
F18 C96 C20 119.4(11) . . ?
F18 C96 C94 117.3(10) . . ?
C94 C96 C20 123.2(11) . . ?
F19 C98 C50 120.5(14) . . ?
F19 C98 C27 120.8(12) . . ?
C27 C98 C50 118.7(13) . . ?
C70 C100 H100 119.3 . . ?
C70 C100 C7 121.5(13) . . ?
C7 C100 H100 119.3 . . ?
F46 C102 C38 120.7(11) . . ?
F46 C102 C25 121.3(11) . . ?
C38 C102 C25 118.0(12) . . ?
C106 C104 P1 125.3(5) . . ?
C106 C104 C114 120.0 . . ?
C114 C104 P1 114.5(5) . . ?
C104 C106 H106 120.0 . . ?
C108 C106 C104 120.0 . . ?
C108 C106 H106 120.0 . . ?
C106 C108 H108 120.0 . . ?
C106 C108 C110 120.0 . . ?
C110 C108 H108 120.0 . . ?
C108 C110 H110 120.0 . . ?
C108 C110 C112 120.0 . . ?
C112 C110 H110 120.0 . . ?
C110 C112 O5 114.4(8) . . ?
C110 C112 C114 120.0 . . ?
C114 C112 O5 125.5(8) . . ?
C104 C114 H114 120.0 . . ?
C112 C114 C104 120.0 . . ?
C112 C114 H114 120.0 . . ?
F33 C116 C28 121.2(11) . . ?
F33 C116 C121 121.1(11) . . ?
C28 C116 C121 117.7(11) . . ?
F56 C118 C90 118.7(11) . . ?
F56 C118 C83 119.3(12) . . ?
C83 C118 C90 122.0(10) . . ?
C82 C120 H120 121.0 . . ?
C82 C120 C99 117.9(12) . . ?
C99 C120 H120 121.0 . . ?
F5 C122 C64 118.6(10) . . ?
F5 C122 C105 119.6(12) . . ?
C105 C122 C64 121.8(12) . . ?
C79 C124 H124 120.6 . . ?
C33 C124 H124 120.6 . . ?
C33 C124 C79 118.9(14) . . ?
F54 C126 C34 122.3(12) . . ?
F54 C126 C65 115.8(14) . . ?
C65 C126 C34 121.9(14) . . ?
C78 C128 H128 119.9 . . ?
C158 C128 C78 120.2(11) . . ?
C158 C128 H128 119.9 . . ?
C132 C130 P4 124.2(5) . . ?
C132 C130 C140 120.0 . . ?
C140 C130 P4 115.5(5) . . ?
C130 C132 H132 120.0 . . ?
C130 C132 C134 120.0 . . ?
C134 C132 H132 120.0 . . ?
C132 C134 H134 120.0 . . ?
C136 C134 C132 120.0 . . ?
C136 C134 H134 120.0 . . ?
C134 C136 H136 120.0 . . ?
C134 C136 C138 120.0 . . ?
C138 C136 H136 120.0 . . ?
O7 C138 C136 115.9(9) . . ?
O7 C138 C140 124.1(9) . . ?
C140 C138 C136 120.0 . . ?
C130 C140 H140 120.0 . . ?
C138 C140 C130 120.0 . . ?
C138 C140 H140 120.0 . . ?
F11 C142 C150 118.9(15) . . ?
F11 C142 C101 121.0(13) . . ?
C101 C142 C150 120.1(14) . . ?
F41 C144 C24 119.9(12) . . ?
F41 C144 C146 120.4(11) . . ?
C146 C144 C24 119.6(12) . . ?
F35 C146 C72 121.4(13) . . ?
F35 C146 C144 120.1(12) . . ?
C72 C146 C144 118.4(11) . . ?
C88 C148 H148 119.0 . . ?
C123 C148 C88 122.0(13) . . ?
C123 C148 H148 119.0 . . ?
F52 C150 C34 120.0(11) . . ?
F52 C150 C142 118.1(12) . . ?
C34 C150 C142 121.9(14) . . ?
F44 C152 C4 119.3(12) . . ?
F44 C152 C121 120.6(12) . . ?
C121 C152 C4 120.0(12) . . ?
F9 C154 C32 121.3(11) . . ?
F9 C154 C85 119.0(11) . . ?
C32 C154 C85 119.7(12) . . ?
C89 C156 H156 120.2 . . ?
C89 C156 C149 119.6(17) . . ?
C149 C156 H156 120.2 . . ?
O6 C158 C128 124.2(12) . . ?
O6 C158 C115 115.8(12) . . ?
C128 C158 C115 120.0(13) . . ?
C124 C79 P3 115.0(10) . . ?
C2 C79 P3 123.3(11) . . ?
C2 C79 C124 121.1(13) . . ?
C43 C5 P2 124.4(10) . . ?
C95 C5 P2 115.9(10) . . ?
C95 C5 C43 119.7(12) . . ?
C89 C81 P2 119.0(14) . . ?
C89 C81 C75 118.9(16) . . ?
C75 C81 P2 121.7(13) . . ?
C88 C41 P3 124.3(11) . . ?
C88 C41 C21 119.1(13) . . ?
C21 C41 P3 116.3(9) . . ?
F48 C83 C10 121.1(11) . . ?
F48 C83 C118 120.1(10) . . ?
C118 C83 C10 118.8(11) . . ?
C41 C21 H21 119.6 . . ?
C97 C21 C41 120.9(12) . . ?
C97 C21 H21 119.6 . . ?
F37 C85 C48 120.5(12) . . ?
F37 C85 C154 120.4(13) . . ?
C48 C85 C154 119.1(11) . . ?
C5 C43 H43 120.4 . . ?
C5 C43 C31 119.1(14) . . ?
C31 C43 H43 120.4 . . ?
O8 C87 C91 124.9(14) . . ?
O8 C87 C61 118.0(13) . . ?
C91 C87 C61 117.1(15) . . ?
O10 C11 C76 124.7(15) . . ?
O10 C11 C137 117.0(13) . . ?
C76 C11 C137 118.3(15) . . ?
C156 C89 H89 120.3 . . ?
C81 C89 C156 119.3(17) . . ?
C81 C89 H89 120.3 . . ?
O4 C45 H45A 109.5 . . ?
O4 C45 H45B 109.5 . . ?
O4 C45 H45C 109.5 . . ?
H45A C45 H45B 109.5 . . ?
H45A C45 H45C 109.5 . . ?
H45B C45 H45C 109.5 . . ?
C87 C91 H91 119.0 . . ?
C53 C91 C87 121.9(13) . . ?
C53 C91 H91 119.0 . . ?
C46 C23 H23 120.7 . . ?
C46 C23 C141 118.7(15) . . ?
C141 C23 H23 120.7 . . ?
F17 C93 C94 120.5(11) . . ?
F17 C93 C107 121.7(11) . . ?
C107 C93 C94 117.8(11) . . ?
F43 C47 C14 118.2(12) . . ?
F43 C47 C153 118.9(14) . . ?
C14 C47 C153 122.9(16) . . ?
C5 C95 H95 119.6 . . ?
C15 C95 C5 120.7(14) . . ?
C15 C95 H95 119.6 . . ?
C15 C3 H3 119.7 . . ?
C31 C3 H3 119.7 . . ?
C31 C3 C15 120.6(15) . . ?
O12 C97 C123 116.0(14) . . ?
C21 C97 O12 124.2(12) . . ?
C21 C97 C123 119.7(14) . . ?
F36 C49 C29 115.3(12) . . ?
C42 C49 F36 120.7(10) . . ?
C42 C49 C29 123.9(13) . . ?
C120 C99 H99 119.1 . . ?
C111 C99 C120 121.7(13) . . ?
C111 C99 H99 119.1 . . ?
F39 C25 C102 119.1(13) . . ?
F39 C25 C55 120.5(12) . . ?
C55 C25 C102 120.4(12) . . ?
F7 C101 C142 120.9(16) . . ?
F7 C101 C65 120.9(17) . . ?
C142 C101 C65 118.0(14) . . ?
F27 C51 C56 120.9(14) . . ?
F27 C51 C125 121.1(15) . . ?
C56 C51 C125 118.0(12) . . ?
C53 C103 H103 120.1 . . ?
C53 C103 C119 119.9(15) . . ?
C119 C103 H103 120.1 . . ?
F3 C13 C52 120.4(16) . . ?
F3 C13 C35 121.1(13) . . ?
C52 C13 C35 118.4(15) . . ?
F49 C105 C122 118.5(14) . . ?
C86 C105 F49 121.2(12) . . ?
C86 C105 C122 120.2(13) . . ?
C91 C53 P3 116.6(10) . . ?
C103 C53 P3 122.8(12) . . ?
C103 C53 C91 120.3(13) . . ?
F42 C107 C18 121.8(10) . . ?
F42 C107 C93 118.8(11) . . ?
C18 C107 C93 119.3(11) . . ?
F13 C27 C98 119.0(15) . . ?
F13 C27 C29 120.1(15) . . ?
C29 C27 C98 120.9(12) . . ?
C78 C109 H109 119.8 . . ?
C78 C109 C131 120.3(13) . . ?
C131 C109 H109 119.8 . . ?
F21 C55 C30 120.4(13) . . ?
F21 C55 C25 119.5(12) . . ?
C30 C55 C25 120.1(12) . . ?
C92 C111 H111 120.0 . . ?
C99 C111 C92 119.9(12) . . ?
C99 C111 H111 120.0 . . ?
O9 C7 C100 122.0(15) . . ?
O9 C7 C69 119.3(15) . . ?
C69 C7 C100 118.7(14) . . ?
F31 C113 C68 120.7(10) . . ?
F31 C113 C125 115.2(12) . . ?
C68 C113 C125 124.1(12) . . ?
F23 C57 C40 119.7(15) . . ?
F23 C57 C35 120.5(13) . . ?
C35 C57 C40 119.7(15) . . ?
C158 C115 H115 120.1 . . ?
C131 C115 C158 119.9(14) . . ?
C131 C115 H115 120.1 . . ?
F51 C29 C49 120.5(15) . . ?
F51 C29 C27 121.8(13) . . ?
C27 C29 C49 117.7(14) . . ?
C26 C117 H117 119.8 . . ?
C26 C117 C135 120.3(15) . . ?
C135 C117 H117 119.8 . . ?
O13 C59 H59A 109.5 . . ?
O13 C59 H59B 109.5 . . ?
O13 C59 H59C 109.5 . . ?
H59A C59 H59B 109.5 . . ?
H59A C59 H59C 109.5 . . ?
H59B C59 H59C 109.5 . . ?
C103 C119 H119 120.8 . . ?
C61 C119 C103 118.4(14) . . ?
C61 C119 H119 120.8 . . ?
C95 C15 O2 120.9(16) . . ?
C95 C15 C3 119.9(15) . . ?
C3 C15 O2 119.1(15) . . ?
F45 C121 C116 118.9(13) . . ?
F45 C121 C152 120.3(13) . . ?
C152 C121 C116 120.7(12) . . ?
C87 C61 H61 118.8 . . ?
C119 C61 C87 122.3(14) . . ?
C119 C61 H61 118.8 . . ?
C148 C123 C97 119.2(14) . . ?
C148 C123 H123 120.4 . . ?
C97 C123 H123 120.4 . . ?
C43 C31 H31 120.1 . . ?
C3 C31 C43 119.8(16) . . ?
C3 C31 H31 120.1 . . ?
F55 C125 C51 117.7(12) . . ?
F55 C125 C113 123.2(14) . . ?
C113 C125 C51 119.0(14) . . ?
C80 C63 H63 121.0 . . ?
C141 C63 C80 118.0(15) . . ?
C141 C63 H63 121.0 . . ?
O6 C127 H12A 109.5 . . ?
O6 C127 H12B 109.5 . . ?
O6 C127 H12C 109.5 . . ?
H12A C127 H12B 109.5 . . ?
H12A C127 H12C 109.5 . . ?
H12B C127 H12C 109.5 . . ?
C79 C2 H2 120.5 . . ?
C79 C2 C145 118.9(16) . . ?
C145 C2 H2 120.5 . . ?
O12 C129 H12D 109.5 . . ?
O12 C129 H12E 109.5 . . ?
O12 C129 H12F 109.5 . . ?
H12D C129 H12E 109.5 . . ?
H12D C129 H12F 109.5 . . ?
H12E C129 H12F 109.5 . . ?
F25 C65 C126 121.6(16) . . ?
F25 C65 C101 117.2(14) . . ?
C126 C65 C101 121.3(16) . . ?
C109 C131 H131 119.9 . . ?
C115 C131 C109 120.3(13) . . ?
C115 C131 H131 119.9 . . ?
O13 C33 C124 122.8(15) . . ?
O13 C33 C139 116.4(14) . . ?
C124 C33 C139 120.4(16) . . ?
O1 C133 H13A 109.7 . . ?
O1 C133 H13B 109.3 . . ?
O1 C133 H13C 109.4 . . ?
H13A C133 H13B 109.5 . . ?
H13A C133 H13C 109.5 . . ?
H13B C133 H13C 109.5 . . ?
O8 C67 H67A 109.5 . . ?
O8 C67 H67B 109.5 . . ?
O8 C67 H67C 109.5 . . ?
H67A C67 H67B 109.5 . . ?
H67A C67 H67C 109.5 . . ?
H67B C67 H67C 109.5 . . ?
C117 C135 H135 119.6 . . ?
C137 C135 C117 120.9(16) . . ?
C137 C135 H135 119.6 . . ?
C70 C17 H17 120.5 . . ?
C70 C17 C9 118.9(14) . . ?
C9 C17 H17 120.5 . . ?
C11 C137 H137 119.9 . . ?
C135 C137 C11 120.3(14) . . ?
C135 C137 H137 119.9 . . ?
C7 C69 H69 119.8 . . ?
C9 C69 C7 120.3(15) . . ?
C9 C69 H69 119.8 . . ?
C33 C139 H139 119.9 . . ?
C145 C139 C33 120.1(16) . . ?
C145 C139 H139 119.9 . . ?
F57 C35 C13 118.6(16) . . ?
F57 C35 C57 120.9(17) . . ?
C57 C35 C13 120.5(13) . . ?
C23 C141 H141 118.7 . . ?
C63 C141 C23 122.6(15) . . ?
C63 C141 H141 118.7 . . ?
O10 C71 H71A 109.5 . . ?
O10 C71 H71B 109.5 . . ?
O10 C71 H71C 109.5 . . ?
H71A C71 H71B 109.5 . . ?
H71A C71 H71C 109.5 . . ?
H71B C71 H71C 109.5 . . ?
O7 C143 H14A 109.5 . . ?
O7 C143 H14B 109.5 . . ?
O7 C143 H14C 109.5 . . ?
H14A C143 H14B 109.5 . . ?
H14A C143 H14C 109.5 . . ?
H14B C143 H14C 109.5 . . ?
C17 C9 H9 119.5 . . ?
C69 C9 C17 120.9(14) . . ?
C69 C9 H9 119.5 . . ?
C2 C145 H145 119.8 . . ?
C139 C145 C2 120.5(17) . . ?
C139 C145 H145 119.8 . . ?
O5 C73 H73A 109.5 . . ?
O5 C73 H73B 109.5 . . ?
O5 C73 H73C 109.5 . . ?
H73A C73 H73B 109.5 . . ?
H73A C73 H73C 109.5 . . ?
H73B C73 H73C 109.5 . . ?
O9 C147 H14D 109.5 . . ?
O9 C147 H14E 109.5 . . ?
O9 C147 H14F 109.5 . . ?
H14D C147 H14E 109.5 . . ?
H14D C147 H14F 109.5 . . ?
H14E C147 H14F 109.5 . . ?
O2 C37 H37A 109.5 . . ?
O2 C37 H37B 109.5 . . ?
O2 C37 H37C 109.5 . . ?
H37A C37 H37B 109.5 . . ?
H37A C37 H37C 109.5 . . ?
H37B C37 H37C 109.5 . . ?
C156 C149 H149 117.6 . . ?
C77 C149 C156 124.8(16) . . ?
C77 C149 H149 117.6 . . ?
C81 C75 H75 117.9 . . ?
C77 C75 C81 124.2(16) . . ?
C77 C75 H75 117.9 . . ?
C77 O11 C155 152(3) . . ?
C60 C151 F47 117.7(16) . . ?
C19 C151 F47 120.1(15) . . ?
C19 C151 C60 122.1(18) . . ?
F59 C19 C153 117.3(19) . . ?
C151 C19 F59 121(2) . . ?
C151 C19 C153 121.6(16) . . ?
F29 C153 C47 119(2) . . ?
F29 C153 C19 123.6(18) . . ?
C19 C153 C47 117.2(16) . . ?
C149 C77 C75 113.0(15) . . ?
C149 C77 O11 128.4(19) . . ?
C149 C77 O3 127.4(16) . . ?
C75 C77 O11 113.7(17) . . ?
C75 C77 O3 117.7(16) . . ?
O11 C155 H15A 109.5 . . ?
O11 C155 H15B 109.5 . . ?
O11 C155 H15C 109.5 . . ?
H15A C155 H15B 109.5 . . ?
H15A C155 H15C 109.5 . . ?
H15B C155 H15C 109.5 . . ?
O2 C39 H39A 109.5 . . ?
O2 C39 H39B 109.5 . . ?
O2 C39 H39C 109.5 . . ?
H39A C39 H39B 109.5 . . ?
H39A C39 H39C 109.5 . . ?
H39B C39 H39C 109.5 . . ?
C77 O3 C157 117.7(19) . . ?
O3 C157 H15D 109.5 . . ?
O3 C157 H15E 109.5 . . ?
O3 C157 H15F 109.5 . . ?
H15D C157 H15E 109.5 . . ?
H15D C157 H15F 109.5 . . ?
H15E C157 H15F 109.5 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Ag1 S1 C12 C32 -73.5(9) . . . . ?
Ag1 S1 C12 C36 108.2(9) . . . . ?
Ag1 S5 C14 C60 -75.8(9) . . . . ?
Ag1 S5 C14 C47 112.1(10) . . . . ?
Ag4 S4 C68 C16 -75.4(10) . . . . ?
Ag4 S4 C68 C113 111.3(10) . . . . ?
Ag4 S12 C22 C24 108.8(9) . . . . ?
Ag4 S12 C22 C44 -77.8(9) . . . . ?
Ag6 S8 C62 C40 106.0(10) . . . . ?
Ag6 S8 C62 C52 -79.3(11) . . . . ?
Ag6 S9 C42 C50 -81.3(10) . . . . ?
Ag6 S9 C42 C49 109.4(10) . . . . ?
Ag8 S3 C20 C18 -80.8(9) . . . . ?
Ag8 S3 C20 C96 104.1(9) . . . . ?
Ag8 S11 C34 C126 105.9(10) . . . . ?
Ag8 S11 C34 C150 -79.7(10) . . . . ?
Ag10 S10 C64 C58 -71.0(10) . . . . ?
Ag10 S10 C64 C122 118.2(9) . . . . ?
Ag10 S2 C1 C8 104.0(9) . . . . ?
Ag10 S2 C1 C10 -80.8(9) . . . . ?
Ag12 S6 C6 C4 -81.8(8) . . . . ?
Ag12 S6 C6 C28 103.3(8) . . . . ?
Ag12 S7 C54 C30 106.2(8) . . . . ?
Ag12 S7 C54 C38 -80.8(9) . . . . ?
Ag14 S4 C68 C16 -154.8(9) . . . . ?
Ag14 S4 C68 C113 31.9(11) . . . . ?
Ag14 S6 C6 C4 -162.6(7) . . . . ?
Ag14 S6 C6 C28 22.5(9) . . . . ?
Ag14 S2 C1 C8 25.9(11) . . . . ?
Ag14 S2 C1 C10 -158.9(8) . . . . ?
Ag7 S8 C62 C40 26.0(12) . . . . ?
Ag7 S8 C62 C52 -159.3(10) . . . . ?
Ag7 S12 C22 C24 30.7(10) . . . . ?
Ag7 S12 C22 C44 -155.9(8) . . . . ?
Ag7 S3 C20 C18 -160.1(8) . . . . ?
Ag7 S3 C20 C96 24.8(10) . . . . ?
Ag2 S1 C12 C32 -153.0(8) . . . . ?
Ag2 S1 C12 C36 28.7(10) . . . . ?
Ag2 S7 C54 C30 25.6(10) . . . . ?
Ag2 S7 C54 C38 -161.4(8) . . . . ?
Ag2 S9 C42 C50 -160.7(8) . . . . ?
Ag2 S9 C42 C49 29.9(12) . . . . ?
Ag9 S1 C12 C32 25.5(10) . . . . ?
Ag9 S1 C12 C36 -152.8(8) . . . . ?
Ag9 S6 C6 C4 19.1(9) . . . . ?
Ag9 S6 C6 C28 -155.8(7) . . . . ?
Ag9 S10 C64 C58 30.9(10) . . . . ?
Ag9 S10 C64 C122 -139.9(9) . . . . ?
Ag9 P1 C46 C66 47.9(11) . . . . ?
Ag9 P1 C46 C23 -123.8(11) . . . . ?
Ag9 P1 C70 C100 44.7(11) . . . . ?
Ag9 P1 C70 C17 -132.5(12) . . . . ?
Ag9 P1 C104 C106 -123.2(5) . . . . ?
Ag9 P1 C104 C114 51.2(5) . . . . ?
Ag5 S3 C20 C18 20.9(10) . . . . ?
Ag5 S3 C20 C96 -154.2(8) . . . . ?
Ag5 S9 C42 C50 19.8(11) . . . . ?
Ag5 S9 C42 C49 -149.5(10) . . . . ?
Ag5 S5 C14 C60 26.0(10) . . . . ?
Ag5 S5 C14 C47 -146.1(9) . . . . ?
Ag5 P4 C78 C128 46.3(10) . . . . ?
Ag5 P4 C78 C109 -130.5(11) . . . . ?
Ag5 P4 C82 C74 46.1(10) . . . . ?
Ag5 P4 C82 C120 -128.7(10) . . . . ?
Ag5 P4 C130 C132 -126.9(4) . . . . ?
Ag5 P4 C130 C140 46.3(5) . . . . ?
Ag11 S10 C64 C58 -153.0(8) . . . . ?
Ag11 S10 C64 C122 36.2(10) . . . . ?
Ag11 S5 C14 C60 -157.2(8) . . . . ?
Ag11 S5 C14 C47 30.7(11) . . . . ?
Ag11 S11 C34 C126 26.2(11) . . . . ?
Ag11 S11 C34 C150 -159.5(9) . . . . ?
Ag3 S4 C68 C16 25.9(11) . . . . ?
Ag3 S4 C68 C113 -147.4(9) . . . . ?
Ag3 S8 C62 C40 -151.2(9) . . . . ?
Ag3 S8 C62 C52 23.5(12) . . . . ?
Ag3 S7 C54 C30 -153.1(8) . . . . ?
Ag3 S7 C54 C38 19.9(10) . . . . ?
Ag3 P3 C79 C124 46.8(12) . . . . ?
Ag3 P3 C79 C2 -124.3(13) . . . . ?
Ag3 P3 C41 C88 -129.2(10) . . . . ?
Ag3 P3 C41 C21 44.6(11) . . . . ?
Ag3 P3 C53 C91 45.3(10) . . . . ?
Ag3 P3 C53 C103 -128.8(10) . . . . ?
Ag13 S12 C22 C24 -147.2(8) . . . . ?
Ag13 S12 C22 C44 26.2(10) . . . . ?
Ag13 S2 C1 C8 -153.9(8) . . . . ?
Ag13 S2 C1 C10 21.3(10) . . . . ?
Ag13 S11 C34 C126 -151.5(10) . . . . ?
Ag13 S11 C34 C150 22.9(11) . . . . ?
Ag13 P2 C26 C76 51.9(10) . . . . ?
Ag13 P2 C26 C117 -125.4(11) . . . . ?
Ag13 P2 C5 C43 -133.0(11) . . . . ?
Ag13 P2 C5 C95 44.5(11) . . . . ?
Ag13 P2 C81 C89 37.3(15) . . . . ?
Ag13 P2 C81 C75 -135.4(13) . . . . ?
S1 C12 C32 F6 4.6(15) . . . . ?
S1 C12 C32 C154 -174.4(10) . . . . ?
S1 C12 C36 F20 -3.3(15) . . . . ?
S1 C12 C36 C48 175.9(10) . . . . ?
S4 C68 C113 F31 -6.2(18) . . . . ?
S4 C68 C113 C125 173.2(12) . . . . ?
S6 C6 C28 F26 -6.4(14) . . . . ?
S6 C6 C28 C116 173.0(9) . . . . ?
S10 C64 C122 F5 -8.0(16) . . . . ?
S10 C64 C122 C105 170.6(11) . . . . ?
S12 C22 C24 F22 -8.5(15) . . . . ?
S12 C22 C24 C144 173.3(10) . . . . ?
S12 C22 C44 F24 7.6(15) . . . . ?
S12 C22 C44 C72 -170.9(9) . . . . ?
S3 C20 C96 F18 -4.7(15) . . . . ?
S3 C20 C96 C94 170.8(10) . . . . ?
S2 C1 C8 F8 -6.0(16) . . . . ?
S2 C1 C8 C90 173.9(10) . . . . ?
S2 C1 C10 F12 5.9(15) . . . . ?
S2 C1 C10 C83 -173.9(10) . . . . ?
S9 C42 C50 F14 12.5(16) . . . . ?
S9 C42 C50 C98 -172.8(10) . . . . ?
S9 C42 C49 F36 -10.4(18) . . . . ?
S9 C42 C49 C29 172.6(11) . . . . ?
S5 C14 C60 F30 9.8(14) . . . . ?
S5 C14 C60 C151 -171.2(10) . . . . ?
S5 C14 C47 F43 -7.9(17) . . . . ?
S5 C14 C47 C153 169.7(13) . . . . ?
S11 C34 C126 F54 -5.5(18) . . . . ?
S11 C34 C126 C65 173.3(12) . . . . ?
S11 C34 C150 F52 7.7(16) . . . . ?
S11 C34 C150 C142 -172.3(10) . . . . ?
P1 C46 C66 C80 -173.0(9) . . . . ?
P1 C46 C23 C141 173.2(13) . . . . ?
P1 C70 C100 C7 -177.2(11) . . . . ?
P1 C70 C17 C9 176.0(14) . . . . ?
P1 C104 C106 C108 174.1(6) . . . . ?
P1 C104 C114 C112 -174.7(6) . . . . ?
P4 C78 C128 C158 -174.9(10) . . . . ?
P4 C78 C109 C131 174.4(12) . . . . ?
P4 C82 C120 C99 173.4(10) . . . . ?
P4 C130 C132 C134 172.9(7) . . . . ?
P4 C130 C140 C138 -173.5(6) . . . . ?
P2 C26 C76 C11 -178.0(9) . . . . ?
P2 C26 C117 C135 177.4(12) . . . . ?
P2 C5 C43 C31 175.0(11) . . . . ?
P2 C5 C95 C15 -177.6(12) . . . . ?
P2 C81 C89 C156 -175.3(13) . . . . ?
P2 C81 C75 C77 175.4(13) . . . . ?
P3 C79 C2 C145 173.1(14) . . . . ?
P3 C41 C21 C97 -175.5(10) . . . . ?
F1 C18 C20 S3 7.5(14) . . . . ?
F1 C18 C20 C96 -177.0(9) . . . . ?
F1 C18 C107 F42 2.1(17) . . . . ?
F1 C18 C107 C93 178.5(11) . . . . ?
F4 C38 C54 S7 9.7(14) . . . . ?
F4 C38 C54 C30 -177.0(9) . . . . ?
F4 C38 C102 F46 -1.9(17) . . . . ?
F4 C38 C102 C25 178.6(11) . . . . ?
F6 C32 C154 F9 -0.8(18) . . . . ?
F6 C32 C154 C85 177.7(11) . . . . ?
F8 C8 C90 F58 -1.5(19) . . . . ?
F8 C8 C90 C118 -179.5(11) . . . . ?
F10 C4 C6 S6 8.7(14) . . . . ?
F10 C4 C6 C28 -176.1(9) . . . . ?
F10 C4 C152 F44 0.6(17) . . . . ?
F10 C4 C152 C121 176.3(11) . . . . ?
F12 C10 C83 F48 -1.4(18) . . . . ?
F12 C10 C83 C118 179.4(12) . . . . ?
F14 C50 C98 F19 -3.7(19) . . . . ?
F14 C50 C98 C27 177.4(13) . . . . ?
F16 C30 C54 S7 -8.8(15) . . . . ?
F16 C30 C54 C38 177.9(10) . . . . ?
F16 C30 C55 F21 0.2(18) . . . . ?
F16 C30 C55 C25 179.4(12) . . . . ?
F20 C36 C48 F2 -1.5(18) . . . . ?
F20 C36 C48 C85 179.7(12) . . . . ?
F22 C24 C144 F41 0.9(18) . . . . ?
F22 C24 C144 C146 -179.3(12) . . . . ?
F24 C44 C72 F40 1.0(17) . . . . ?
F24 C44 C72 C146 177.8(12) . . . . ?
F26 C28 C116 F33 -0.6(17) . . . . ?
F26 C28 C116 C121 -179.9(10) . . . . ?
F28 C16 C56 F60 -0.8(18) . . . . ?
F28 C16 C56 C51 178.4(13) . . . . ?
F28 C16 C68 S4 8.7(15) . . . . ?
F28 C16 C68 C113 -177.6(10) . . . . ?
F30 C60 C151 F47 -1.1(19) . . . . ?
F30 C60 C151 C19 179.0(15) . . . . ?
F32 C52 C62 S8 8.3(17) . . . . ?
F32 C52 C62 C40 -176.8(11) . . . . ?
F32 C52 C13 F3 0(2) . . . . ?
F32 C52 C13 C35 176.3(14) . . . . ?
F34 C40 C62 S8 -6.6(18) . . . . ?
F34 C40 C62 C52 178.3(11) . . . . ?
F34 C40 C57 F23 2(2) . . . . ?
F34 C40 C57 C35 179.3(14) . . . . ?
F36 C49 C29 F51 -1(2) . . . . ?
F36 C49 C29 C27 180.0(13) . . . . ?
F38 C58 C64 S10 10.9(15) . . . . ?
F38 C58 C64 C122 -177.8(10) . . . . ?
F38 C58 C84 F15 -2.3(18) . . . . ?
F38 C58 C84 C86 179.2(12) . . . . ?
F40 C72 C146 F35 -3(2) . . . . ?
F40 C72 C146 C144 178.9(12) . . . . ?
F44 C152 C121 F45 -4(2) . . . . ?
F44 C152 C121 C116 177.2(12) . . . . ?
F46 C102 C25 F39 0(2) . . . . ?
F46 C102 C25 C55 178.9(12) . . . . ?
F50 C94 C96 F18 -4.3(19) . . . . ?
F50 C94 C96 C20 -179.9(11) . . . . ?
F50 C94 C93 F17 0(2) . . . . ?
F50 C94 C93 C107 -178.2(12) . . . . ?
F54 C126 C65 F25 -2(2) . . . . ?
F54 C126 C65 C101 177.2(14) . . . . ?
F56 C118 C83 F48 0(2) . . . . ?
F56 C118 C83 C10 179.7(12) . . . . ?
F58 C90 C118 F56 2(2) . . . . ?
F58 C90 C118 C83 -177.7(13) . . . . ?
F60 C56 C51 F27 -1(2) . . . . ?
F60 C56 C51 C125 178.2(13) . . . . ?
F15 C84 C86 F53 -1(2) . . . . ?
F15 C84 C86 C105 179.4(14) . . . . ?
F31 C113 C125 F55 1(2) . . . . ?
F31 C113 C125 C51 178.4(14) . . . . ?
F2 C48 C85 F37 1(2) . . . . ?
F2 C48 C85 C154 -178.3(12) . . . . ?
F33 C116 C121 F45 1.5(19) . . . . ?
F33 C116 C121 C152 -179.6(12) . . . . ?
F17 C93 C107 F42 -0.3(19) . . . . ?
F17 C93 C107 C18 -176.8(12) . . . . ?
F9 C154 C85 F37 0(2) . . . . ?
F9 C154 C85 C48 179.4(12) . . . . ?
F19 C98 C27 F13 1(2) . . . . ?
F19 C98 C27 C29 178.9(14) . . . . ?
F39 C25 C55 F21 1(2) . . . . ?
F39 C25 C55 C30 -178.6(12) . . . . ?
F5 C122 C105 F49 2(2) . . . . ?
F5 C122 C105 C86 178.4(14) . . . . ?
F41 C144 C146 F35 1(2) . . . . ?
F41 C144 C146 C72 -180.0(12) . . . . ?
O1 C80 C63 C141 179.8(15) . . . . ?
F43 C47 C153 F29 -4(3) . . . . ?
F43 C47 C153 C19 -179.6(16) . . . . ?
F11 C142 C150 F52 -1.3(19) . . . . ?
F11 C142 C150 C34 178.7(12) . . . . ?
F11 C142 C101 F7 3(2) . . . . ?
F11 C142 C101 C65 178.2(14) . . . . ?
O4 C92 C111 C99 179.9(12) . . . . ?
O6 C158 C115 C131 -178.5(14) . . . . ?
O8 C87 C91 C53 -179.9(11) . . . . ?
O8 C87 C61 C119 -179.6(13) . . . . ?
O10 C11 C137 C135 -178.2(15) . . . . ?
F23 C57 C35 F57 -1(3) . . . . ?
F23 C57 C35 C13 178.6(15) . . . . ?
F47 C151 C19 F59 1(3) . . . . ?
F47 C151 C19 C153 179.9(17) . . . . ?
F3 C13 C35 F57 -3(3) . . . . ?
F3 C13 C35 C57 177.5(15) . . . . ?
O12 C97 C123 C148 -177.7(13) . . . . ?
C1 C8 C90 F58 178.6(11) . . . . ?
C1 C8 C90 C118 0.6(19) . . . . ?
C1 C10 C83 F48 178.4(11) . . . . ?
C1 C10 C83 C118 -1(2) . . . . ?
C4 C6 C28 F26 178.3(9) . . . . ?
C4 C6 C28 C116 -2.2(16) . . . . ?
C4 C152 C121 F45 -179.6(12) . . . . ?
C4 C152 C121 C116 2(2) . . . . ?
F13 C27 C29 F51 1(3) . . . . ?
F13 C27 C29 C49 -179.5(14) . . . . ?
C6 C4 C152 F44 -179.0(10) . . . . ?
C6 C4 C152 C121 -3.4(19) . . . . ?
C6 C28 C116 F33 180.0(10) . . . . ?
C6 C28 C116 C121 0.7(18) . . . . ?
F53 C86 C105 F49 -1(2) . . . . ?
F53 C86 C105 C122 -177.8(13) . . . . ?
F27 C51 C125 F55 -2(3) . . . . ?
F27 C51 C125 C113 -178.9(15) . . . . ?
C8 C1 C10 F12 -178.6(10) . . . . ?
C8 C1 C10 C83 1.6(17) . . . . ?
C8 C90 C118 F56 -179.6(12) . . . . ?
C8 C90 C118 C83 0(2) . . . . ?
C10 C1 C8 F8 178.6(10) . . . . ?
C10 C1 C8 C90 -1.5(17) . . . . ?
O13 C33 C139 C145 -176.7(17) . . . . ?
C12 C32 C154 F9 178.2(11) . . . . ?
C12 C32 C154 C85 -3(2) . . . . ?
C12 C36 C48 F2 179.2(11) . . . . ?
C12 C36 C48 C85 0.4(19) . . . . ?
O7 C138 C140 C130 179.9(11) . . . . ?
C14 C60 C151 F47 179.9(11) . . . . ?
C14 C60 C151 C19 0(2) . . . . ?
C14 C47 C153 F29 178.6(15) . . . . ?
C14 C47 C153 C19 3(3) . . . . ?
C16 C56 C51 F27 179.8(14) . . . . ?
C16 C56 C51 C125 -1(2) . . . . ?
C16 C68 C113 F31 179.9(11) . . . . ?
C16 C68 C113 C125 -1(2) . . . . ?
C18 C20 C96 F18 179.8(10) . . . . ?
C18 C20 C96 C94 -4.7(17) . . . . ?
C20 C18 C107 F42 179.8(10) . . . . ?
C20 C18 C107 C93 -3.9(19) . . . . ?
C22 C24 C144 F41 179.2(11) . . . . ?
C22 C24 C144 C146 -1(2) . . . . ?
C22 C44 C72 F40 179.5(10) . . . . ?
C22 C44 C72 C146 -3.7(19) . . . . ?
C24 C22 C44 F24 -178.8(10) . . . . ?
C24 C22 C44 C72 2.8(16) . . . . ?
C24 C144 C146 F35 -178.4(12) . . . . ?
C24 C144 C146 C72 0(2) . . . . ?
C26 P2 C5 C43 104.1(12) . . . . ?
C26 P2 C5 C95 -78.5(11) . . . . ?
C26 P2 C81 C89 160.3(13) . . . . ?
C26 P2 C81 C75 -12.3(16) . . . . ?
C26 C76 C11 O10 178.0(12) . . . . ?
C26 C76 C11 C137 0.9(19) . . . . ?
C26 C117 C135 C137 0(3) . . . . ?
C28 C116 C121 F45 -179.2(11) . . . . ?
C28 C116 C121 C152 0(2) . . . . ?
C32 C12 C36 F20 178.2(10) . . . . ?
C32 C12 C36 C48 -2.6(16) . . . . ?
C32 C154 C85 F37 -178.9(12) . . . . ?
C32 C154 C85 C48 1(2) . . . . ?
C34 C126 C65 F25 178.8(13) . . . . ?
C34 C126 C65 C101 -2(2) . . . . ?
C36 C12 C32 F6 -177.0(9) . . . . ?
C36 C12 C32 C154 4.1(17) . . . . ?
C36 C48 C85 F37 -179.8(12) . . . . ?
C36 C48 C85 C154 0(2) . . . . ?
C38 C102 C25 F39 179.7(12) . . . . ?
C38 C102 C25 C55 -2(2) . . . . ?
O9 C7 C69 C9 -179.7(18) . . . . ?
C40 C57 C35 F57 -177.5(15) . . . . ?
C40 C57 C35 C13 2(3) . . . . ?
C42 C50 C98 F19 -178.7(12) . . . . ?
C42 C50 C98 C27 2(2) . . . . ?
C42 C49 C29 F51 176.3(13) . . . . ?
C42 C49 C29 C27 -3(2) . . . . ?
C44 C22 C24 F22 177.7(10) . . . . ?
C44 C22 C24 C144 -0.5(17) . . . . ?
C44 C72 C146 F35 -179.3(12) . . . . ?
C44 C72 C146 C144 2(2) . . . . ?
C46 P1 C70 C100 -78.1(11) . . . . ?
C46 P1 C70 C17 104.8(13) . . . . ?
C46 P1 C104 C106 -0.7(7) . . . . ?
C46 P1 C104 C114 173.7(5) . . . . ?
C46 C66 C80 O1 179.6(11) . . . . ?
C46 C66 C80 C63 1(2) . . . . ?
C46 C23 C141 C63 -2(3) . . . . ?
C50 C42 C49 F36 -180.0(11) . . . . ?
C50 C42 C49 C29 3(2) . . . . ?
C50 C98 C27 F13 179.6(13) . . . . ?
C50 C98 C27 C29 -2(2) . . . . ?
C52 C13 C35 F57 -179.9(14) . . . . ?
C52 C13 C35 C57 1(3) . . . . ?
F7 C101 C65 F25 -2(2) . . . . ?
F7 C101 C65 C126 178.8(14) . . . . ?
C54 C30 C55 F21 179.7(11) . . . . ?
C54 C30 C55 C25 -1(2) . . . . ?
C54 C38 C102 F46 178.3(10) . . . . ?
C54 C38 C102 C25 -1.2(18) . . . . ?
C56 C16 C68 S4 -172.1(10) . . . . ?
C56 C16 C68 C113 1.7(18) . . . . ?
C56 C51 C125 F55 179.3(15) . . . . ?
C56 C51 C125 C113 2(2) . . . . ?
C58 C64 C122 F5 -179.4(11) . . . . ?
C58 C64 C122 C105 -0.7(18) . . . . ?
C58 C84 C86 F53 177.4(12) . . . . ?
C58 C84 C86 C105 -2(2) . . . . ?
C60 C14 C47 F43 179.5(11) . . . . ?
C60 C14 C47 C153 -3(2) . . . . ?
C60 C151 C19 F59 -178.8(15) . . . . ?
C60 C151 C19 C153 0(3) . . . . ?
C62 C40 C57 F23 -179.0(13) . . . . ?
C62 C40 C57 C35 -2(2) . . . . ?
C62 C52 C13 F3 180.0(13) . . . . ?
C62 C52 C13 C35 -3(2) . . . . ?
C64 C58 C84 F15 179.5(11) . . . . ?
C64 C58 C84 C86 1.0(19) . . . . ?
C64 C122 C105 F49 -176.7(13) . . . . ?
C64 C122 C105 C86 0(2) . . . . ?
C66 C46 C23 C141 2(2) . . . . ?
C66 C80 C63 C141 -2(2) . . . . ?
C68 C16 C56 F60 180.0(11) . . . . ?
C68 C16 C56 C51 -1(2) . . . . ?
C68 C113 C125 F55 -178.3(15) . . . . ?
C68 C113 C125 C51 -1(2) . . . . ?
C70 P1 C46 C66 171.9(10) . . . . ?
C70 P1 C46 C23 0.2(14) . . . . ?
C70 P1 C104 C106 113.6(6) . . . . ?
C70 P1 C104 C114 -72.0(6) . . . . ?
C70 C100 C7 O9 -178.8(13) . . . . ?
C70 C100 C7 C69 0(2) . . . . ?
C70 C17 C9 C69 3(3) . . . . ?
C74 C82 C120 C99 -1.3(19) . . . . ?
C74 C92 C111 C99 -1(2) . . . . ?
C76 C26 C117 C135 0(2) . . . . ?
C76 C11 C137 C135 -1(2) . . . . ?
C78 P4 C82 C74 -76.2(10) . . . . ?
C78 P4 C82 C120 108.9(11) . . . . ?
C78 P4 C130 C132 -4.2(6) . . . . ?
C78 P4 C130 C140 169.0(5) . . . . ?
C78 C128 C158 O6 177.5(12) . . . . ?
C78 C128 C158 C115 -1(2) . . . . ?
C78 C109 C131 C115 1(3) . . . . ?
C80 C63 C141 C23 2(3) . . . . ?
C82 P4 C78 C128 169.1(9) . . . . ?
C82 P4 C78 C109 -7.8(13) . . . . ?
C82 P4 C130 C132 110.2(6) . . . . ?
C82 P4 C130 C140 -76.6(6) . . . . ?
C82 C74 C92 O4 179.0(11) . . . . ?
C82 C74 C92 C111 0.4(18) . . . . ?
C82 C120 C99 C111 0(2) . . . . ?
C84 C58 C64 S10 -171.0(10) . . . . ?
C84 C58 C64 C122 0.4(17) . . . . ?
C84 C86 C105 F49 178.1(14) . . . . ?
C84 C86 C105 C122 2(2) . . . . ?
C88 C148 C123 C97 -1(2) . . . . ?
C88 C41 C21 C97 -1.4(19) . . . . ?
O5 C112 C114 C104 -175.3(10) . . . . ?
C90 C118 C83 F48 -179.4(13) . . . . ?
C90 C118 C83 C10 0(2) . . . . ?
C92 C74 C82 P4 -174.0(9) . . . . ?
C92 C74 C82 C120 0.9(18) . . . . ?
C94 C93 C107 F42 177.7(12) . . . . ?
C94 C93 C107 C18 1.2(19) . . . . ?
C96 C94 C93 F17 177.4(12) . . . . ?
C96 C94 C93 C107 -1(2) . . . . ?
C98 C27 C29 F51 -176.9(15) . . . . ?
C98 C27 C29 C49 2(2) . . . . ?
C100 C70 C17 C9 -1(2) . . . . ?
C100 C7 C69 C9 2(3) . . . . ?
C102 C38 C54 S7 -170.5(9) . . . . ?
C102 C38 C54 C30 2.8(16) . . . . ?
C102 C25 C55 F21 -178.0(12) . . . . ?
C102 C25 C55 C30 3(2) . . . . ?
C104 P1 C46 C66 -74.0(11) . . . . ?
C104 P1 C46 C23 114.3(12) . . . . ?
C104 P1 C70 C100 166.0(10) . . . . ?
C104 P1 C70 C17 -11.1(14) . . . . ?
C104 C106 C108 C110 0.0 . . . . ?
C106 C104 C114 C112 0.0 . . . . ?
C106 C108 C110 C112 0.0 . . . . ?
C108 C110 C112 O5 175.8(9) . . . . ?
C108 C110 C112 C114 0.0 . . . . ?
C110 C112 C114 C104 0.0 . . . . ?
C114 C104 C106 C108 0.0 . . . . ?
C120 C99 C111 C92 1(2) . . . . ?
C124 C79 C2 C145 3(2) . . . . ?
C124 C33 C139 C145 -4(3) . . . . ?
C126 C34 C150 F52 -177.7(11) . . . . ?
C126 C34 C150 C142 2.3(18) . . . . ?
C128 C78 C109 C131 -2(2) . . . . ?
C128 C158 C115 C131 0(2) . . . . ?
C130 P4 C78 C128 -76.9(10) . . . . ?
C130 P4 C78 C109 106.2(12) . . . . ?
C130 P4 C82 C74 169.3(9) . . . . ?
C130 P4 C82 C120 -5.6(12) . . . . ?
C130 C132 C134 C136 0.0 . . . . ?
C132 C130 C140 C138 0.0 . . . . ?
C132 C134 C136 C138 0.0 . . . . ?
C134 C136 C138 O7 -179.9(10) . . . . ?
C134 C136 C138 C140 0.0 . . . . ?
C136 C138 C140 C130 0.0 . . . . ?
C140 C130 C132 C134 0.0 . . . . ?
C142 C101 C65 F25 -176.7(14) . . . . ?
C142 C101 C65 C126 4(2) . . . . ?
C148 C88 C41 P3 173.2(10) . . . . ?
C148 C88 C41 C21 -0.5(19) . . . . ?
C150 C34 C126 F54 179.8(11) . . . . ?
C150 C34 C126 C65 -1(2) . . . . ?
C150 C142 C101 F7 -177.8(13) . . . . ?
C150 C142 C101 C65 -3(2) . . . . ?
C152 C4 C6 S6 -171.7(9) . . . . ?
C152 C4 C6 C28 3.5(16) . . . . ?
C156 C149 C77 C75 -5(3) . . . . ?
C156 C149 C77 O11 148(2) . . . . ?
C156 C149 C77 O3 -168.7(18) . . . . ?
C158 C115 C131 C109 0(3) . . . . ?
C79 P3 C41 C88 -6.0(13) . . . . ?
C79 P3 C41 C21 167.8(10) . . . . ?
C79 P3 C53 C91 -77.8(10) . . . . ?
C79 P3 C53 C103 108.1(12) . . . . ?
C79 C124 C33 O13 177.6(14) . . . . ?
C79 C124 C33 C139 5(2) . . . . ?
C79 C2 C145 C139 -1(3) . . . . ?
C5 P2 C26 C76 174.4(9) . . . . ?
C5 P2 C26 C117 -3.0(13) . . . . ?
C5 P2 C81 C89 -87.1(15) . . . . ?
C5 P2 C81 C75 100.3(14) . . . . ?
C5 C43 C31 C3 2(2) . . . . ?
C5 C95 C15 O2 -177.7(14) . . . . ?
C5 C95 C15 C3 3(2) . . . . ?
C81 P2 C26 C76 -71.6(11) . . . . ?
C81 P2 C26 C117 111.1(13) . . . . ?
C81 P2 C5 C43 -7.7(14) . . . . ?
C81 P2 C5 C95 169.7(11) . . . . ?
C81 C75 C77 C149 1(3) . . . . ?
C81 C75 C77 O11 -157(2) . . . . ?
C81 C75 C77 O3 166.3(17) . . . . ?
C41 P3 C79 C124 -77.4(11) . . . . ?
C41 P3 C79 C2 111.6(14) . . . . ?
C41 P3 C53 C91 170.5(9) . . . . ?
C41 P3 C53 C103 -3.6(12) . . . . ?
C41 C88 C148 C123 2(2) . . . . ?
C41 C21 C97 O12 178.5(12) . . . . ?
C41 C21 C97 C123 2(2) . . . . ?
C21 C97 C123 C148 -1(2) . . . . ?
C43 C5 C95 C15 0(2) . . . . ?
C87 C91 C53 P3 -175.7(9) . . . . ?
C87 C91 C53 C103 -1.4(19) . . . . ?
C89 C156 C149 C77 5(3) . . . . ?
C89 C81 C75 C77 3(3) . . . . ?
C45 O4 C92 C74 -0.1(18) . . . . ?
C45 O4 C92 C111 178.5(12) . . . . ?
C91 C87 C61 C119 0(2) . . . . ?
C23 C46 C66 C80 -1.2(19) . . . . ?
C93 C94 C96 F18 178.2(12) . . . . ?
C93 C94 C96 C20 3(2) . . . . ?
C47 C14 C60 F30 -177.5(10) . . . . ?
C47 C14 C60 C151 1.4(17) . . . . ?
C95 C5 C43 C31 -2(2) . . . . ?
C49 C42 C50 F14 -177.5(11) . . . . ?
C49 C42 C50 C98 -2.7(18) . . . . ?
C101 C142 C150 F52 179.9(13) . . . . ?
C101 C142 C150 C34 0(2) . . . . ?
C103 C119 C61 C87 0(2) . . . . ?
C13 C52 C62 S8 -172.0(11) . . . . ?
C13 C52 C62 C40 3(2) . . . . ?
F59 C19 C153 F29 2(3) . . . . ?
F59 C19 C153 C47 177.5(15) . . . . ?
C53 P3 C79 C124 169.8(10) . . . . ?
C53 P3 C79 C2 -1.2(15) . . . . ?
C53 P3 C41 C88 106.6(12) . . . . ?
C53 P3 C41 C21 -79.6(11) . . . . ?
C53 C103 C119 C61 -1(2) . . . . ?
C107 C18 C20 S3 -170.1(9) . . . . ?
C107 C18 C20 C96 5.4(16) . . . . ?
C109 C78 C128 C158 2.1(19) . . . . ?
C55 C30 C54 S7 171.7(10) . . . . ?
C55 C30 C54 C38 -1.6(17) . . . . ?
C7 C69 C9 C17 -3(3) . . . . ?
C57 C40 C62 S8 174.9(11) . . . . ?
C57 C40 C62 C52 0(2) . . . . ?
C117 C26 C76 C11 -0.6(18) . . . . ?
C117 C135 C137 C11 0(3) . . . . ?
C59 O13 C33 C124 4(2) . . . . ?
C59 O13 C33 C139 176.1(16) . . . . ?
C119 C103 C53 P3 175.5(11) . . . . ?
C119 C103 C53 C91 2(2) . . . . ?
C15 C3 C31 C43 1(3) . . . . ?
C61 C87 C91 C53 0.6(18) . . . . ?
C31 C3 C15 O2 177.4(15) . . . . ?
C31 C3 C15 C95 -3(3) . . . . ?
C127 O6 C158 C128 8(2) . . . . ?
C127 O6 C158 C115 -173.8(13) . . . . ?
C129 O12 C97 C21 15(2) . . . . ?
C129 O12 C97 C123 -168.2(13) . . . . ?
C33 C124 C79 P3 -176.0(11) . . . . ?
C33 C124 C79 C2 -5(2) . . . . ?
C33 C139 C145 C2 2(3) . . . . ?
C133 O1 C80 C66 9.5(18) . . . . ?
C133 O1 C80 C63 -172.0(13) . . . . ?
C67 O8 C87 C91 0.0(18) . . . . ?
C67 O8 C87 C61 179.6(12) . . . . ?
C17 C70 C100 C7 0(2) . . . . ?
C71 O10 C11 C76 6(2) . . . . ?
C71 O10 C11 C137 -176.4(14) . . . . ?
C143 O7 C138 C136 -173.9(13) . . . . ?
C143 O7 C138 C140 6.2(18) . . . . ?
C73 O5 C112 C110 -172.1(15) . . . . ?
C73 O5 C112 C114 3(2) . . . . ?
C147 O9 C7 C100 13(2) . . . . ?
C147 O9 C7 C69 -165.9(18) . . . . ?
C37 O2 C15 C95 9(2) . . . . ?
C37 O2 C15 C3 -171.1(17) . . . . ?
C149 C156 C89 C81 -1(3) . . . . ?
C149 C77 O3 C157 -29(3) . . . . ?
C75 C81 C89 C156 -2(3) . . . . ?
C75 C77 O3 C157 168.2(19) . . . . ?
C151 C19 C153 F29 -176.7(18) . . . . ?
C151 C19 C153 C47 -1(3) . . . . ?
C155 O11 C77 C149 52(8) . . . . ?
C155 O11 C77 C75 -155(6) . . . . ?
C39 O2 C15 C95 -163(2) . . . . ?
C39 O2 C15 C3 16(3) . . . . ?

_smtbx_masks_special_details     
;
A solvent mask was calculated and 368 electrons were 
found in a volume of 2152Å³ in 2 voids per unit cell. 
This is consistent with the presence of 
[+ solvents] per formula unit 
which account for 364 electrons 
per unit cell.
;
loop_
_smtbx_masks_void_nr
_smtbx_masks_void_average_x
_smtbx_masks_void_average_y
_smtbx_masks_void_average_z
_smtbx_masks_void_volume
_smtbx_masks_void_count_electrons
_smtbx_masks_void_content
1 -0.227 0.327 0.605 522.1 91.1 '1 CH2Cl2,2.725 CH3OH'
2 -0.227 0.173 0.105 522.1 91.1 '1 CH2Cl2,2.725 CH3OH'
3 0.227 0.827 0.895 522.1 93.8 '1 CH2Cl2,2.725 CH3OH'
4 0.227 0.673 0.395 522.1 93.8 '1 CH2Cl2,2.725 CH3OH'
5 0.239 0.255 0.105 16.4 1.3 '0.25 ?'
6 0.239 0.245 0.605 16.4 1.3 '0.25 ?'
7 0.761 0.745 0.895 16.4 1.3 '0.25 ?'
8 0.761 0.755 0.395 16.4 1.3 '0.25 ?'

_smtbx_masks_void_probe_radius   1.2
_smtbx_masks_void_truncation_radius 1.2
_olex2_submission_special_instructions 'No special instructions were received'
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_mal20241108a
_database_code_depnum_ccdc_archive 'CCDC 2413803'
loop_
_audit_author_name
_audit_author_address
'Along Ma'
;qingdao university of science and technology
China
;
_audit_update_record             
;
2024-12-31 deposited with the CCDC.	2025-06-11 downloaded from the CCDC.
;
_audit_creation_date             2024-12-22
_audit_creation_method           
;
Olex2 1.5
(compiled 2024.02.16 svn.r378c4104 for OlexSys, GUI svn.r6928)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         
'C156 H84 Ag12 Cu2 F60 O12 P4 S12, 3[CH2Cl2], 6.5[CH3OH]'
_chemical_formula_sum            'C165.50 H116 Ag12 Cl6 Cu2 F60 O18.50 P4 S12'
_chemical_formula_weight         5683.40
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   18.7706(7)
_cell_length_b                   19.9187(9)
_cell_length_c                   25.5916(12)
_cell_angle_alpha                89.783(2)
_cell_angle_beta                 88.6660(10)
_cell_angle_gamma                87.6930(10)
_cell_volume                     9558.0(7)
_cell_formula_units_Z            2
_cell_measurement_reflns_used    9513
_cell_measurement_temperature    170
_cell_measurement_theta_max      27.733
_cell_measurement_theta_min      2.194
_shelx_estimated_absorpt_T_max   0.842
_shelx_estimated_absorpt_T_min   0.717
_exptl_absorpt_coefficient_mu    1.784
_exptl_absorpt_correction_T_max  0.1159
_exptl_absorpt_correction_T_min  0.0737
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
SADABS-2016/2 (Bruker,2016/2) was used for absorption correction.
wR2(int) was 0.1439 before and 0.0587 after correction.
The Ratio of minimum to maximum transmission is 0.6549.
The λ/2 correction factor is Not present.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            'metallic yellowish yellow'
_exptl_crystal_colour_lustre     metallic
_exptl_crystal_colour_modifier   yellowish
_exptl_crystal_colour_primary    yellow
_exptl_crystal_density_diffrn    1.975
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             5546
_exptl_crystal_size_max          0.2
_exptl_crystal_size_mid          0.1
_exptl_crystal_size_min          0.1
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0683
_diffrn_reflns_av_unetI/netI     0.0360
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.999
_diffrn_reflns_limit_h_max       23
_diffrn_reflns_limit_h_min       -23
_diffrn_reflns_limit_k_max       25
_diffrn_reflns_limit_k_min       -25
_diffrn_reflns_limit_l_max       32
_diffrn_reflns_limit_l_min       -32
_diffrn_reflns_number            327789
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.999
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         26.500
_diffrn_reflns_theta_min         1.948
_diffrn_ambient_temperature      170
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       ?
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_diffrn_source_current           1.4
_diffrn_source_power             0.07
_diffrn_source_voltage           50.0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                29435
_reflns_number_total             39570
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT V8.40B (?, 2016)'
_computing_data_collection       ?
_computing_data_reduction        'SAINT V8.40B (?, 2016)'
_computing_molecular_graphics    'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2018/3 (Sheldrick, 2015)'
_computing_structure_solution    'olex2.solve 1.5 (Bourhis et al., 2015)'
_refine_diff_density_max         1.140
_refine_diff_density_min         -1.444
_refine_diff_density_rms         0.095
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.086
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     2338
_refine_ls_number_reflns         39570
_refine_ls_number_restraints     4061
_refine_ls_R_factor_all          0.0628
_refine_ls_R_factor_gt           0.0419
_refine_ls_restrained_S_all      1.043
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0628P)²+9.9888P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1145
_refine_ls_wR_factor_ref         0.1242
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups
 At 1.5 times of:
  All C(H,H,H) groups
2. Shared sites
{Ag13, Cu13}
{Ag12, Cu12}
{Ag2, Cu2}
{Ag14, Cu14}
3. Rigid bond restraints
 Ag7, S2
 with sigma for 1-2 distances of 0.001 and sigma for 1-3 distances of 0.001
 Ag9, S10
 with sigma for 1-2 distances of 0.001 and sigma for 1-3 distances of 0.001
 Ag9, S11
 with sigma for 1-2 distances of 0.001 and sigma for 1-3 distances of 0.001
 Ag11, S3
 with sigma for 1-2 distances of 0.0005 and sigma for 1-3 distances of 0.0005
 Ag11, S8
 with sigma for 1-2 distances of 0.001 and sigma for 1-3 distances of 0.001
4. Uiso/Uaniso restraints and constraints
All non-hydrogen atoms have similar U: within 2A with sigma of 0.04 and sigma
for terminal atoms of 0.08 within 2A
Uanis(Ag13) = Uanis(Cu13)
Uanis(Ag12) = Uanis(Cu12)
Uanis(Ag2) = Uanis(Cu2)
Uanis(Ag14) = Uanis(Cu14)
5. Rigid body (RIGU) restrains
 All non-hydrogen atoms
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
6. Others
 1*[Sof(Ag13)+Sof(Cu13)]+1*[Sof(Ag12)+Sof(Cu12)]+1*[Sof(Ag2)+Sof(Cu2)]+1*
 [Sof(Ag14)+Sof(Cu14)]=2 with esd of 0.0001
 Sof(Cu13)=1-FVAR(1)
 Sof(Ag13)=FVAR(1)
 Sof(Cu12)=1-FVAR(2)
 Sof(Ag12)=FVAR(2)
 Sof(Cu2)=1-FVAR(3)
 Sof(Ag2)=FVAR(3)
 Sof(Cu14)=1-FVAR(4)
 Sof(Ag14)=FVAR(4)
7.a Riding coordinates:
 C19(H19A,H19B,H19C)
7.b Aromatic/amide H refined with riding coordinates:
 C20(H20), C38(H38), C50(H50), C62(H62), C64(H64), C80(H80), C86(H86),
 C94(H94), C96(H96), C108(H108), C114(H114), C124(H124), C126(H126), C132(H132),
  C138(H138), C148(H148), C79(H79), C81(H81), C41(H41), C21(H21), C43(H43),
 C45(H45), C91(H91), C23(H23), C103(H103), C105(H105), C55(H55), C7(H7),
 C113(H113), C115(H115), C59(H59), C119(H119), C61(H61), C31(H31), C125(H125),
 C63(H63), C65(H65), C131(H131), C17(H17), C143(H143), C73(H73), C147(H147),
 C37(H37), C149(H149), C151(H151), C153(H153), C77(H77), C155(H155)
7.c Idealised Me refined as rotating group:
 C100(H10A,H10B,H10C), C83(H83A,H83B,H83C), C89(H89A,H89B,H89C), C49(H49A,H49B,
 H49C), C99(H99A,H99B,H99C), C57(H57A,H57B,H57C), C129(H12A,H12B,H12C),
 C35(H35A,H35B,H35C), C9(H9A,H9B,H9C), C145(H14A,H14B,H14C), C75(H75A,H75B,H75C)
;
_atom_sites_solution_hydrogens   mixed
_atom_sites_solution_primary     iterative
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.73422(2) 0.35624(2) 0.23195(2) 0.03659(7) Uani 1 1 d . . . . .
Ag4 Ag 0.82897(2) 0.27409(2) 0.29268(2) 0.03747(7) Uani 1 1 d . . . . .
Ag6 Ag 0.79888(2) 0.23567(2) 0.18825(2) 0.03852(7) Uani 1 1 d . . . . .
Ag8 Ag 0.67835(2) 0.28101(2) 0.31770(2) 0.03959(7) Uani 1 1 d . . . . .
Ag10 Ag 0.64931(2) 0.24285(2) 0.21337(2) 0.04245(8) Uani 1 1 d . . . . .
Ag5 Ag 0.74542(2) 0.16009(2) 0.27464(2) 0.04292(8) Uani 1 1 d . . . . .
Ag3 Ag 0.91833(2) 0.37060(2) 0.19643(2) 0.04667(8) Uani 1 1 d . . . . .
Ag7 Ag 0.78479(2) 0.18828(2) 0.41062(2) 0.05092(9) Uani 1 1 d . U . . .
Ag11 Ag 0.55181(2) 0.38909(2) 0.26033(2) 0.05713(10) Uani 1 1 d . U . . .
Ag9 Ag 0.70956(2) 0.09477(2) 0.15366(2) 0.06023(10) Uani 1 1 d . U . . .
Ag13 Ag 0.70507(2) 0.32124(2) 0.12466(2) 0.05111(14) Uani 0.468(3) 1 d . U P A
1
Ag2 Ag 0.89925(3) 0.15205(2) 0.24987(2) 0.05818(14) Uani 0.577(3) 1 d . U P A 5
Ag12 Ag 0.59253(3) 0.16401(3) 0.30402(2) 0.06471(16) Uani 0.608(3) 1 d . U P A
3
Ag14 Ag 0.76539(2) 0.39654(3) 0.33718(2) 0.05237(15) Uani 0.346(3) 1 d . U P A
7
S1 S 0.79723(5) 0.39175(5) 0.14734(4) 0.0416(2) Uani 1 1 d . U . . .
S4 S 0.87457(5) 0.39311(6) 0.29339(4) 0.0429(2) Uani 1 1 d . U . . .
S6 S 0.74354(6) 0.31491(6) 0.39889(4) 0.0433(2) Uani 1 1 d . U . . .
S8 S 0.66947(5) 0.44157(6) 0.29191(4) 0.0444(2) Uani 1 1 d . U . . .
S10 S 0.73696(6) 0.20999(6) 0.10345(4) 0.0491(3) Uani 1 1 d . U . . .
S12 S 0.93466(5) 0.23788(6) 0.19167(5) 0.0474(3) Uani 1 1 d . U . . .
S3 S 0.59323(6) 0.34370(7) 0.16503(5) 0.0502(3) Uani 1 1 d . U . . .
S7 S 0.68432(6) 0.12641(6) 0.36068(5) 0.0515(3) Uani 1 1 d . U . . .
S2 S 0.89213(6) 0.17676(6) 0.33995(5) 0.0487(3) Uani 1 1 d . U . . .
P1 P 1.02318(6) 0.43060(6) 0.16955(4) 0.0458(3) Uani 1 1 d . U . . .
S9 S 0.54293(6) 0.27401(7) 0.31456(5) 0.0562(3) Uani 1 1 d . U . . .
S5 S 0.81751(7) 0.07589(6) 0.21707(5) 0.0553(3) Uani 1 1 d . U . . .
P4 P 0.81210(6) 0.15515(6) 0.49952(5) 0.0492(3) Uani 1 1 d . U . . .
S11 S 0.59919(7) 0.12602(7) 0.21615(5) 0.0599(3) Uani 1 1 d . U . . .
P2 P 0.43974(6) 0.45511(8) 0.26326(5) 0.0550(3) Uani 1 1 d . U . . .
P3 P 0.69339(9) 0.00287(8) 0.09378(7) 0.0729(4) Uani 1 1 d . U . . .
F1 F 1.01971(13) 0.32268(13) 0.28274(10) 0.0520(6) Uani 1 1 d . U . . .
F4 F 0.94243(15) 0.30349(15) 0.08506(11) 0.0614(7) Uani 1 1 d . U . . .
F6 F 0.84893(14) 0.51672(14) 0.19887(10) 0.0571(7) Uani 1 1 d . U . . .
F8 F 1.03872(15) 0.12960(16) 0.30396(13) 0.0687(8) Uani 1 1 d . U . . .
F10 F 0.92033(15) 0.27310(15) 0.42687(12) 0.0657(7) Uani 1 1 d . U . . .
F12 F 0.70399(16) 0.44649(15) 0.06263(11) 0.0639(7) Uani 1 1 d . U . . .
F14 F 0.58439(15) 0.34986(16) 0.04819(11) 0.0643(7) Uani 1 1 d . U . . .
F16 F 1.13507(14) 0.34291(17) 0.33843(12) 0.0673(8) Uani 1 1 d . U . . .
F18 F 0.45327(14) 0.28596(17) 0.19869(11) 0.0669(8) Uani 1 1 d . U . . .
F20 F 0.76157(18) 0.30576(16) 0.01472(12) 0.0710(8) Uani 1 1 d . U . . .
F22 F 0.88325(15) 0.46972(18) 0.39287(11) 0.0736(9) Uani 1 1 d . U . . .
F24 F 0.80984(16) 0.03265(16) 0.38464(14) 0.0743(9) Uani 1 1 d . U . . .
F26 F 0.63969(15) 0.23788(17) 0.46557(12) 0.0693(8) Uani 1 1 d . U . . .
F28 F 0.84853(17) 0.09927(16) 0.08328(13) 0.0736(8) Uani 1 1 d . U . . .
F30 F 0.72346(18) 0.45568(15) 0.43736(13) 0.0741(8) Uani 1 1 d . U . . .
F32 F 0.53779(17) 0.39859(18) 0.38105(12) 0.0756(9) Uani 1 1 d . U . . .
F34 F 0.61354(18) 0.50865(16) 0.19430(12) 0.0732(8) Uani 1 1 d . U . . .
F36 F 0.56342(18) 0.15157(18) 0.10342(13) 0.0800(9) Uani 1 1 d . U . . .
F38 F 0.47224(18) 0.3252(2) -0.01043(12) 0.0888(11) Uani 1 1 d . U . . .
F40 F 1.12562(17) 0.4253(2) 0.42349(13) 0.0901(11) Uani 1 1 d . U . . .
F42 F 1.02100(19) 0.26314(19) 0.00198(12) 0.0843(10) Uani 1 1 d . U . . .
F44 F 0.75520(19) 0.54748(17) 0.34003(14) 0.0838(10) Uani 1 1 d . U . . .
F46 F 0.8344(2) 0.64333(16) 0.16439(14) 0.0854(10) Uani 1 1 d . U . . .
F48 F 1.0443(2) 0.2931(2) 0.47218(14) 0.0922(11) Uani 1 1 d . U . . .
O1 O 0.88250(19) 0.5068(2) 0.00727(13) 0.0688(10) Uani 1 1 d . U . . .
F50 F 1.0152(2) 0.10680(18) 0.17515(15) 0.0925(12) Uani 1 1 d . U . . .
F52 F 0.56108(17) 0.03533(18) 0.36054(15) 0.0856(10) Uani 1 1 d . U . . .
F54 F 0.99878(19) 0.4868(3) 0.44999(13) 0.1103(16) Uani 1 1 d . U . . .
F56 F 0.7003(2) -0.01972(17) 0.24160(15) 0.0873(10) Uani 1 1 d . U . . .
O4 O 0.8140(2) 0.4014(2) 0.56381(16) 0.0746(10) Uani 1 1 d . U . . .
F58 F 0.34147(15) 0.2632(2) 0.13950(14) 0.0883(11) Uani 1 1 d . U . . .
F60 F 1.16274(15) 0.1511(2) 0.34922(15) 0.0968(13) Uani 1 1 d . U . . .
F15 F 0.9471(2) 0.00646(18) 0.26058(17) 0.0963(12) Uani 1 1 d . U . . .
F31 F 0.8500(2) 0.2885(2) -0.06805(14) 0.1027(13) Uani 1 1 d . U . . .
F2 F 0.6890(2) 0.57382(19) 0.03040(14) 0.1024(13) Uani 1 1 d . U . . .
F33 F 0.4583(2) 0.0984(2) 0.26691(17) 0.1055(13) Uani 1 1 d . U . . .
F17 F 1.16735(18) 0.2315(2) 0.43426(16) 0.1072(14) Uani 1 1 d . U . . .
F35 F 0.34960(17) 0.2823(2) 0.03413(13) 0.0927(12) Uani 1 1 d . U . . .
F9 F 0.56636(19) 0.2824(3) 0.55037(15) 0.1116(14) Uani 1 1 d . U . . .
O6 O 1.0431(2) 0.0376(2) 0.42783(17) 0.0824(12) Uani 1 1 d . U . . .
F37 F 0.9310(2) 0.0796(2) -0.00224(17) 0.1030(12) Uani 1 1 d . U . . .
F19 F 0.4700(2) 0.1719(2) 0.38106(18) 0.1047(13) Uani 1 1 d . U . . .
F39 F 0.6483(2) 0.4996(2) 0.52006(16) 0.1164(15) Uani 1 1 d . U . . .
F5 F 0.8081(2) -0.09594(19) 0.41458(18) 0.1042(13) Uani 1 1 d . U . . .
O8 O 1.18139(19) 0.2118(2) 0.16803(17) 0.0813(12) Uani 1 1 d . U . . .
F41 F 0.4389(2) 0.1361(2) 0.05737(17) 0.1175(15) Uani 1 1 d . U . . .
F21 F 1.0946(3) 0.1434(3) 0.00333(18) 0.1357(19) Uani 1 1 d . U . . .
O10 O 0.4525(2) 0.4923(3) 0.06384(14) 0.0845(13) Uani 1 1 d . U . . .
O12 O 0.5812(2) 0.0248(2) 0.5122(2) 0.0951(15) Uani 1 1 d . U . . .
C1 C 1.0128(2) 0.3647(2) 0.32337(16) 0.0457(10) Uani 1 1 d . U . . .
C4 C 0.9473(2) 0.3966(2) 0.33544(15) 0.0417(9) Uani 1 1 d . U . . .
O3 O 1.0051(2) 0.5892(2) 0.32755(17) 0.0895(13) Uani 1 1 d . U . . .
F43 F 0.4699(2) 0.4165(3) 0.47246(15) 0.1274(18) Uani 1 1 d . U . . .
F11 F 0.7134(3) -0.1436(2) 0.28119(19) 0.1241(16) Uani 1 1 d . U . . .
F45 F 0.7557(3) 0.67245(17) 0.07882(17) 0.1165(16) Uani 1 1 d . U . . .
C6 C 0.9449(2) 0.4366(3) 0.37883(18) 0.0577(12) Uani 1 1 d . U . . .
O7 O 0.3015(2) 0.2580(3) 0.3425(2) 0.0983(14) Uani 1 1 d . U . . .
C8 C 0.5229(2) 0.3193(2) 0.12602(18) 0.0486(10) Uani 1 1 d . U . . .
C10 C 0.6850(2) 0.3452(2) 0.44900(17) 0.0476(10) Uani 1 1 d . U . . .
F23 F 0.6236(3) 0.6367(2) 0.16578(17) 0.1315(18) Uani 1 1 d . U . . .
C12 C 0.5249(2) 0.3283(3) 0.07177(18) 0.0536(11) Uani 1 1 d . U . . .
F47 F 0.5704(2) 0.4145(3) 0.57875(15) 0.1369(19) Uani 1 1 d . U . . .
C14 C 0.8033(3) 0.2496(3) 0.01246(19) 0.0579(11) Uani 1 1 d . U . . .
C16 C 0.9765(2) 0.2074(2) 0.13379(18) 0.0486(10) Uani 1 1 d . U . . .
C18 C 1.0729(2) 0.3746(3) 0.35225(18) 0.0536(11) Uani 1 1 d . U . . .
F3 F 0.5601(2) -0.0939(2) 0.3891(2) 0.1321(18) Uani 1 1 d . U . . .
C20 C 0.9550(2) 0.4747(3) 0.08148(17) 0.0492(10) Uani 1 1 d . U . . .
H20 H 0.943129 0.429021 0.078511 0.059 Uiso 1 1 calc R U . . .
C22 C 1.0921(2) 0.3754(3) 0.13941(17) 0.0477(10) Uani 1 1 d . U . . .
C24 C 1.0676(3) 0.4155(3) 0.39471(19) 0.0656(14) Uani 1 1 d . U . . .
C26 C 0.9283(2) 0.5218(3) 0.04641(18) 0.0538(11) Uani 1 1 d . U . . .
C28 C 0.8008(2) 0.2028(2) 0.05194(17) 0.0489(10) Uani 1 1 d . U . . .
C30 C 0.9794(2) 0.2449(2) 0.08796(19) 0.0509(10) Uani 1 1 d . U . . .
C32 C 0.7776(2) 0.4773(2) 0.13196(16) 0.0435(9) Uani 1 1 d . U . . .
C34 C 0.9746(2) 0.2000(2) 0.36451(19) 0.0498(10) Uani 1 1 d . U . . .
C36 C 0.8091(2) 0.5292(2) 0.15653(18) 0.0500(10) Uani 1 1 d . U . . .
C38 C 1.1116(2) 0.3172(3) 0.16693(19) 0.0537(11) Uani 1 1 d . U . . .
H38 H 1.092127 0.309799 0.200973 0.064 Uiso 1 1 calc R U . . .
F49 F 0.7664(3) 0.6747(2) 0.3101(2) 0.1360(18) Uani 1 1 d . U . . .
C40 C 1.0387(2) 0.1702(3) 0.3453(2) 0.0587(12) Uani 1 1 d . U . . .
C42 C 0.6855(3) 0.0390(2) 0.37267(19) 0.0540(11) Uani 1 1 d . U . . .
C44 C 0.4596(2) 0.2971(3) 0.14695(19) 0.0553(12) Uani 1 1 d . U . . .
C46 C 0.7364(3) 0.4947(3) 0.08942(18) 0.0541(11) Uani 1 1 d . U . . .
C48 C 1.0038(3) 0.4462(3) 0.40840(18) 0.0697(15) Uani 1 1 d . U . . .
F25 F 0.4004(3) 0.3140(4) 0.51943(17) 0.174(3) Uani 1 1 d . U . . .
F51 F 0.6821(3) -0.16099(19) 0.4171(2) 0.1286(17) Uani 1 1 d . U . . .
C50 C 1.1207(2) 0.3868(3) 0.09004(18) 0.0525(11) Uani 1 1 d . U . . .
H50 H 1.108538 0.426963 0.071594 0.063 Uiso 1 1 calc R U . . .
C52 C 0.5058(2) 0.2846(3) 0.37741(19) 0.0635(13) Uani 1 1 d . U . . .
C54 C 0.9993(2) 0.4944(3) 0.12125(17) 0.0489(10) Uani 1 1 d . U . . .
F13 F 1.0889(3) 0.0656(3) 0.0900(2) 0.153(2) Uani 1 1 d . U . . .
C56 C 0.6833(2) 0.5232(2) 0.26815(18) 0.0483(10) Uani 1 1 d . U . . .
C58 C 0.6430(2) 0.3025(3) 0.47886(19) 0.0581(12) Uani 1 1 d . U . . .
C60 C 0.9795(3) 0.2413(3) 0.4071(2) 0.0566(11) Uani 1 1 d . U . . .
C62 C 0.6921(3) 0.0825(3) 0.5089(2) 0.0585(12) Uani 1 1 d . U . . .
H62 H 0.670531 0.120851 0.492567 0.070 Uiso 1 1 calc R U . . .
C64 C 0.8130(2) 0.2849(3) 0.53741(19) 0.0542(11) Uani 1 1 d . U . . .
H64 H 0.840580 0.293188 0.506618 0.065 Uiso 1 1 calc R U . . .
C66 C 0.7950(3) 0.3370(3) 0.5710(2) 0.0618(12) Uani 1 1 d . U . . .
F53 F 0.9325(2) 0.1751(3) -0.07909(16) 0.1225(16) Uani 1 1 d . U . . .
C68 C 0.7466(3) 0.0026(3) 0.3860(2) 0.0606(12) Uani 1 1 d . U . . .
C70 C 1.1589(2) 0.2706(3) 0.1447(2) 0.0592(12) Uani 1 1 d . U . . .
F27 F 0.3325(2) 0.0862(3) 0.2209(2) 0.153(2) Uani 1 1 d . U . . .
C72 C 0.9068(2) 0.1334(2) 0.50576(19) 0.0526(11) Uani 1 1 d . U . . .
F55 F 0.4017(3) 0.1922(3) 0.4730(2) 0.165(2) Uani 1 1 d . U . . .
C74 C 0.4675(3) 0.3162(3) 0.04149(19) 0.0625(13) Uani 1 1 d . U . . .
C76 C 0.8229(3) -0.0026(2) 0.24899(19) 0.0598(12) Uani 1 1 d . U . . .
C78 C 0.7911(2) 0.2196(3) 0.54820(18) 0.0531(11) Uani 1 1 d . U . . .
O2 O 0.6636(3) 0.1732(3) -0.05779(19) 0.1041(15) Uani 1 1 d . U . . .
C80 C 0.9365(2) 0.0914(3) 0.4667(2) 0.0569(12) Uani 1 1 d . U . . .
H80 H 0.907145 0.072927 0.441182 0.068 Uiso 1 1 calc R U . . .
C82 C 1.0644(2) 0.4745(3) 0.22212(17) 0.0505(11) Uani 1 1 d . U . . .
C84 C 0.5039(3) 0.3457(4) 0.4023(2) 0.0696(14) Uani 1 1 d . U . . .
C86 C 0.9453(3) 0.5884(3) 0.0506(2) 0.0623(13) Uani 1 1 d . U . . .
H86 H 0.926787 0.620763 0.026671 0.075 Uiso 1 1 calc R U . . .
C88 C 0.8460(3) 0.1463(3) 0.0458(2) 0.0593(12) Uani 1 1 d . U . . .
C90 C 0.6512(3) 0.5488(3) 0.2244(2) 0.0599(12) Uani 1 1 d . U . . .
C92 C 1.1025(3) 0.1817(3) 0.3690(2) 0.0707(14) Uani 1 1 d . U . . .
C94 C 1.0170(3) 0.5609(3) 0.12506(19) 0.0574(12) Uani 1 1 d . U . . .
H94 H 1.047733 0.574587 0.151615 0.069 Uiso 1 1 calc R U . . .
C96 C 1.0199(3) 0.5153(3) 0.25334(18) 0.0561(11) Uani 1 1 d . U . . .
H96 H 0.970819 0.520832 0.245352 0.067 Uiso 1 1 calc R U . . .
C98 C 1.0151(3) 0.1463(3) 0.1326(2) 0.0695(15) Uani 1 1 d . U . . .
C100 C 0.8660(3) 0.4379(3) 0.0000(2) 0.0691(15) Uani 1 1 d . U . . .
H10A H 0.833038 0.434538 -0.028881 0.104 Uiso 1 1 calc R U . . .
H10B H 0.843773 0.420659 0.032121 0.104 Uiso 1 1 calc R U . . .
H10C H 0.909978 0.411417 -0.008098 0.104 Uiso 1 1 calc R U . . .
C102 C 0.4454(3) 0.5437(3) 0.27834(18) 0.0637(13) Uani 1 1 d . U . . .
C104 C 0.3748(2) 0.4219(3) 0.30932(18) 0.0603(12) Uani 1 1 d . U . . .
C106 C 0.7646(2) 0.0817(2) 0.5200(2) 0.0547(11) Uani 1 1 d . U . . .
F7 F 0.3210(2) 0.1046(3) 0.1159(2) 0.154(2) Uani 1 1 d . U . . .
F57 F 0.9588(3) -0.1158(2) 0.3027(3) 0.162(2) Uani 1 1 d . U . . .
C108 C 1.1863(2) 0.2815(3) 0.0945(2) 0.0617(13) Uani 1 1 d . U . . .
H108 H 1.218098 0.248921 0.078626 0.074 Uiso 1 1 calc R U . . .
C110 C 0.6849(3) 0.4115(3) 0.4647(2) 0.0611(12) Uani 1 1 d . U . . .
C112 C 0.3983(2) 0.4555(3) 0.19981(18) 0.0598(13) Uani 1 1 d . U . . .
C114 C 0.9486(3) 0.1603(3) 0.5432(2) 0.0637(13) Uani 1 1 d . U . . .
H114 H 0.927821 0.188266 0.569942 0.076 Uiso 1 1 calc R U . . .
C116 C 0.7099(3) 0.0275(3) 0.0258(2) 0.0777(15) Uani 1 1 d . U . . .
C118 C 0.4018(3) 0.2852(3) 0.1172(2) 0.0665(14) Uani 1 1 d . U . . .
F29 F 0.7001(4) 0.7213(2) 0.2240(2) 0.155(2) Uani 1 1 d . U . . .
C120 C 0.3169(3) 0.3243(4) 0.3423(2) 0.0746(15) Uani 1 1 d . U . . .
C122 C 0.7221(3) 0.5680(3) 0.2964(2) 0.0654(13) Uani 1 1 d . U . . .
C124 C 0.3626(2) 0.3537(3) 0.3062(2) 0.0678(14) Uani 1 1 d . U . . .
H124 H 0.385424 0.327175 0.279437 0.081 Uiso 1 1 calc R U . . .
C126 C 0.9892(3) 0.6075(3) 0.0896(2) 0.0646(13) Uani 1 1 d . U . . .
H126 H 1.000745 0.653310 0.092392 0.077 Uiso 1 1 calc R U . . .
C128 C 0.5158(3) 0.1259(3) 0.1863(2) 0.0670(14) Uani 1 1 d . U . . .
C130 C 0.4056(3) 0.2945(3) 0.0636(2) 0.0699(15) Uani 1 1 d . U . . .
C132 C 0.2967(3) 0.4275(4) 0.3846(2) 0.0838(18) Uani 1 1 d . U . . .
H132 H 0.274138 0.452853 0.412149 0.101 Uiso 1 1 calc R U . . .
O9 O 0.5690(3) 0.6456(3) 0.3446(3) 0.145(3) Uani 1 1 d . U . . .
C134 C 0.8022(3) 0.5948(3) 0.1393(2) 0.0644(13) Uani 1 1 d . U . . .
C136 C 1.0095(3) 0.0771(3) 0.4658(2) 0.0654(13) Uani 1 1 d . U . . .
C138 C 1.1175(3) 0.5388(3) 0.3083(2) 0.0769(16) Uani 1 1 d . U . . .
H138 H 1.135876 0.561026 0.337555 0.092 Uiso 1 1 calc R U . . .
F59 F 0.8424(4) -0.1942(2) 0.3122(2) 0.168(3) Uani 1 1 d . U . . .
C140 C 0.4701(3) 0.2326(4) 0.4025(3) 0.0823(17) Uani 1 1 d . U . . .
C142 C 0.7289(3) 0.5589(3) 0.0722(2) 0.0682(14) Uani 1 1 d . U . . .
C144 C 1.0459(3) 0.5481(3) 0.2960(2) 0.0655(13) Uani 1 1 d . U . . .
C146 C 1.0195(3) 0.2252(3) 0.0447(2) 0.0674(13) Uani 1 1 d . U . . .
C148 C 1.1675(2) 0.3388(3) 0.06794(19) 0.0621(13) Uani 1 1 d . U . . .
H148 H 1.186776 0.345902 0.033801 0.074 Uiso 1 1 calc R U . . .
C150 C 1.0432(3) 0.2526(3) 0.4309(2) 0.0688(14) Uani 1 1 d . U . . .
C152 C 0.7652(4) -0.0428(3) 0.2555(2) 0.0719(14) Uani 1 1 d . U . . .
C154 C 0.6234(3) 0.0045(3) 0.3739(2) 0.0686(14) Uani 1 1 d . U . . .
C156 C 0.8873(4) -0.0288(3) 0.2660(3) 0.0793(16) Uani 1 1 d . U . . .
C39 C 0.6515(3) 0.0285(3) 0.5214(3) 0.0753(16) Uani 1 1 d . U . . .
C79 C 0.2852(3) 0.3618(4) 0.3811(2) 0.0816(17) Uani 1 1 d . U . . .
H79 H 0.254570 0.341229 0.405927 0.098 Uiso 1 1 calc R U . . .
C5 C 0.8479(3) 0.2411(3) -0.0310(2) 0.0742(15) Uani 1 1 d . U . . .
C81 C 0.3418(3) 0.4599(4) 0.3483(2) 0.0712(15) Uani 1 1 d . U . . .
H81 H 0.349104 0.506721 0.350754 0.085 Uiso 1 1 calc R U . . .
C41 C 0.6790(3) 0.0892(3) 0.0098(2) 0.0760(15) Uani 1 1 d . U . . .
H41 H 0.648979 0.114558 0.033470 0.091 Uiso 1 1 calc R U . . .
C83 C 0.8617(4) 0.4137(3) 0.5203(3) 0.0871(19) Uani 1 1 d . U . . .
H83A H 0.838934 0.402099 0.487695 0.131 Uiso 1 1 calc R U . . .
H83B H 0.905759 0.386176 0.524078 0.131 Uiso 1 1 calc R U . . .
H83C H 0.873004 0.461349 0.519604 0.131 Uiso 1 1 calc R U . . .
C21 C 1.1607(3) 0.4980(4) 0.2783(2) 0.0805(17) Uani 1 1 d . U . . .
H21 H 1.209333 0.491264 0.287188 0.097 Uiso 1 1 calc R U . . .
O5 O 0.9395(4) -0.1076(3) 0.1393(3) 0.137(2) Uani 1 1 d . U . . .
C85 C 0.6051(3) 0.3257(4) 0.5228(2) 0.0797(16) Uani 1 1 d . U . . .
C43 C 1.1354(3) 0.4654(3) 0.2343(2) 0.0636(13) Uani 1 1 d . U . . .
H43 H 1.166674 0.437581 0.213232 0.076 Uiso 1 1 calc R U . . .
C87 C 0.4148(3) 0.4750(3) 0.1072(2) 0.0707(15) Uani 1 1 d . U . . .
C11 C 0.5079(3) 0.1340(3) 0.1337(2) 0.0728(15) Uani 1 1 d . U . . .
C89 C 0.5235(4) 0.5136(4) 0.0710(2) 0.0856(19) Uani 1 1 d . U . . .
H89A H 0.544864 0.525331 0.037056 0.128 Uiso 1 1 calc R U . . .
H89B H 0.552086 0.477063 0.086945 0.128 Uiso 1 1 calc R U . . .
H89C H 0.522159 0.552945 0.093932 0.128 Uiso 1 1 calc R U . . .
C45 C 0.7494(4) 0.2070(3) 0.5922(2) 0.0815(17) Uani 1 1 d . U . . .
H45 H 0.734120 0.163080 0.599950 0.098 Uiso 1 1 calc R U . . .
C91 C 0.5028(3) 0.5637(4) 0.3065(2) 0.0765(16) Uani 1 1 d . U . . .
H91 H 0.537123 0.531218 0.318523 0.092 Uiso 1 1 calc R U . . .
C23 C 1.0224(3) 0.1457(3) 0.5412(2) 0.0731(15) Uani 1 1 d . U . . .
H23 H 1.052181 0.164739 0.566280 0.088 Uiso 1 1 calc R U . . .
C93 C 0.4344(4) 0.3038(6) 0.4727(3) 0.110(2) Uani 1 1 d . U . . .
C47 C 1.0571(4) 0.1647(4) 0.0454(3) 0.0879(19) Uani 1 1 d . U . . .
C95 C 0.8882(3) 0.1356(3) 0.0023(2) 0.0758(15) Uani 1 1 d . U . . .
C3 C 0.6026(4) -0.0259(3) 0.0974(3) 0.0883(19) Uani 1 1 d . U . . .
C97 C 1.1044(3) 0.2219(4) 0.4116(3) 0.0776(16) Uani 1 1 d . U . . .
C49 C 1.1572(3) 0.2015(4) 0.2211(3) 0.095(2) Uani 1 1 d . U . . .
H49A H 1.105093 0.200148 0.222375 0.142 Uiso 1 1 calc R U . . .
H49B H 1.172282 0.238442 0.242950 0.142 Uiso 1 1 calc R U . . .
H49C H 1.177885 0.158878 0.234194 0.142 Uiso 1 1 calc R U . . .
C99 C 1.0002(4) 0.0071(3) 0.3884(3) 0.0835(17) Uani 1 1 d . U . . .
H99A H 1.031188 -0.020478 0.364920 0.125 Uiso 1 1 calc R U . . .
H99B H 0.975482 0.042420 0.368147 0.125 Uiso 1 1 calc R U . . .
H99C H 0.965020 -0.021245 0.405468 0.125 Uiso 1 1 calc R U . . .
C25 C 0.7466(4) -0.0634(3) 0.4013(3) 0.0762(15) Uani 1 1 d . U . . .
C101 C 0.4692(3) 0.3575(5) 0.4499(2) 0.0949(19) Uani 1 1 d . U . . .
C51 C 0.6071(3) 0.3920(4) 0.5363(2) 0.0891(18) Uani 1 1 d . U . . .
C103 C 0.3297(3) 0.4355(4) 0.1915(2) 0.0808(19) Uani 1 1 d . U . . .
H103 H 0.300219 0.422592 0.220150 0.097 Uiso 1 1 calc R U . . .
C13 C 0.4550(3) 0.1093(4) 0.2152(3) 0.0850(18) Uani 1 1 d . U . . .
C105 C 0.7967(3) 0.0265(3) 0.5432(3) 0.0793(18) Uani 1 1 d . U . . .
H105 H 0.845821 0.025945 0.551491 0.095 Uiso 1 1 calc R U . . .
C53 C 0.6916(4) 0.1135(4) -0.0400(3) 0.0841(16) Uani 1 1 d . U . . .
C107 C 0.6562(4) 0.6140(3) 0.2096(3) 0.0886(18) Uani 1 1 d . U . . .
C27 C 0.6458(3) 0.4339(3) 0.5069(2) 0.0803(16) Uani 1 1 d . U . . .
C109 C 1.0531(4) 0.1254(4) 0.0888(3) 0.095(2) Uani 1 1 d . U . . .
C55 C 0.3043(3) 0.4345(5) 0.1409(2) 0.102(3) Uani 1 1 d . U . . .
H55 H 0.257856 0.419353 0.135007 0.123 Uiso 1 1 calc R U . . .
C111 C 0.6226(4) -0.0634(3) 0.3889(3) 0.0880(19) Uani 1 1 d . U . . .
C7 C 1.0515(3) 0.1040(3) 0.5033(2) 0.0723(15) Uani 1 1 d . U . . .
H7 H 1.101332 0.093524 0.502714 0.087 Uiso 1 1 calc R U . . .
C113 C 0.8228(4) -0.0612(3) 0.1159(3) 0.0890(18) Uani 1 1 d . U . . .
H113 H 0.841240 -0.017816 0.110822 0.107 Uiso 1 1 calc R U . . .
C57 C 0.5452(3) 0.0850(3) 0.4938(3) 0.093(2) Uani 1 1 d . U . . .
H57A H 0.564914 0.097083 0.459431 0.139 Uiso 1 1 calc R U . . .
H57B H 0.551988 0.121575 0.518500 0.139 Uiso 1 1 calc R U . . .
H57C H 0.494187 0.077406 0.491067 0.139 Uiso 1 1 calc R U . . .
C115 C 0.7537(4) 0.3248(4) 0.6152(2) 0.0839(17) Uani 1 1 d . U . . .
H115 H 0.741589 0.360308 0.638895 0.101 Uiso 1 1 calc R U . . .
C29 C 0.7622(4) 0.6091(3) 0.0965(2) 0.0759(16) Uani 1 1 d . U . . .
C117 C 0.6838(4) -0.0959(3) 0.4031(3) 0.0880(19) Uani 1 1 d . U . . .
C59 C 0.7630(4) 0.0150(5) -0.0593(3) 0.103(2) Uani 1 1 d . U . . .
H59 H 0.791097 -0.010572 -0.083957 0.123 Uiso 1 1 calc R U . . .
C119 C 0.7518(4) -0.0118(4) -0.0082(3) 0.096(2) Uani 1 1 d . U . . .
H119 H 0.772021 -0.054181 0.001982 0.115 Uiso 1 1 calc R U . . .
C15 C 0.4361(4) 0.2411(5) 0.4492(3) 0.110(2) Uani 1 1 d . U . . .
C121 C 0.7708(5) -0.1070(3) 0.2761(3) 0.097(2) Uani 1 1 d . U . . .
C61 C 0.3926(4) 0.5911(4) 0.2636(2) 0.093(2) Uani 1 1 d . U . . .
H61 H 0.351944 0.577266 0.245751 0.111 Uiso 1 1 calc R U . . .
C123 C 0.7273(4) 0.6332(3) 0.2821(3) 0.0872(18) Uani 1 1 d . U . . .
O11 O 0.4725(4) -0.0589(4) 0.2015(3) 0.189(4) Uani 1 1 d . U . . .
C31 C 0.6842(4) -0.0274(3) 0.5444(3) 0.102(2) Uani 1 1 d . U . . .
H31 H 0.656894 -0.065064 0.553434 0.123 Uiso 1 1 calc R U . . .
C125 C 0.5722(4) -0.0321(4) 0.1462(3) 0.106(2) Uani 1 1 d . U . . .
H125 H 0.599883 -0.022441 0.175621 0.127 Uiso 1 1 calc R U . . .
C63 C 0.3456(3) 0.4553(4) 0.0993(2) 0.092(2) Uani 1 1 d . U . . .
H63 H 0.326904 0.456158 0.065131 0.110 Uiso 1 1 calc R U . . .
C127 C 0.8896(3) 0.1844(4) -0.0365(2) 0.0826(17) Uani 1 1 d . U . . .
C2 C 0.4433(4) 0.1265(4) 0.1091(3) 0.0910(19) Uani 1 1 d . U . . .
C129 C 0.3304(4) 0.2173(4) 0.3010(3) 0.109(3) Uani 1 1 d . U . . .
H12A H 0.311105 0.233414 0.267815 0.164 Uiso 1 1 calc R U . . .
H12B H 0.317514 0.170593 0.306828 0.164 Uiso 1 1 calc R U . . .
H12C H 0.382423 0.219798 0.299922 0.164 Uiso 1 1 calc R U . . .
C65 C 0.7305(4) 0.2620(4) 0.6249(3) 0.098(2) Uani 1 1 d . U . . .
H65 H 0.700595 0.254907 0.654759 0.117 Uiso 1 1 calc R U . . .
C131 C 0.7347(4) 0.0761(5) -0.0741(3) 0.106(2) Uani 1 1 d . U . . .
H131 H 0.744810 0.092922 -0.108156 0.127 Uiso 1 1 calc R U . . .
C33 C 0.3847(4) 0.1103(4) 0.1390(4) 0.110(2) Uani 1 1 d . U . . .
C133 C 0.7505(4) -0.0701(3) 0.1075(3) 0.095(2) Uani 1 1 d . U . . .
C67 C 0.8939(5) -0.0920(4) 0.2866(3) 0.107(2) Uani 1 1 d . U . . .
C135 C 0.6948(5) 0.6568(3) 0.2386(3) 0.097(2) Uani 1 1 d . U . . .
C17 C 0.7553(4) -0.0289(3) 0.5542(3) 0.102(3) Uani 1 1 d . U . . .
H17 H 0.777145 -0.068279 0.568825 0.123 Uiso 1 1 calc R U . . .
C137 C 0.8688(6) -0.1139(4) 0.1314(4) 0.117(3) Uani 1 1 d . U . . .
C69 C 0.8361(6) -0.1318(3) 0.2913(3) 0.113(2) Uani 1 1 d . U . . .
C139 C 0.3904(3) 0.1029(5) 0.1912(4) 0.110(2) Uani 1 1 d . U . . .
C35 C 0.6167(4) 0.2125(4) -0.0242(3) 0.106(2) Uani 1 1 d . U . . .
H35A H 0.600360 0.253238 -0.042676 0.159 Uiso 1 1 calc R U . . .
H35B H 0.642033 0.224863 0.007126 0.159 Uiso 1 1 calc R U . . .
H35C H 0.575524 0.186181 -0.014154 0.159 Uiso 1 1 calc R U . . .
C141 C 0.5103(4) 0.6322(4) 0.3174(3) 0.101(2) Uani 1 1 d . U . . .
C71 C 0.5039(5) -0.0514(4) 0.1545(4) 0.132(3) Uani 1 1 d . U . . .
C143 C 0.4586(5) 0.6787(4) 0.3016(3) 0.111(2) Uani 1 1 d . U . . .
H143 H 0.463078 0.725124 0.308779 0.133 Uiso 1 1 calc R U . . .
C9 C 0.9706(5) -0.0457(5) 0.1251(4) 0.126(3) Uani 1 1 d . U . . .
H9A H 0.963183 -0.036582 0.087963 0.189 Uiso 1 1 calc R U . . .
H9B H 1.021880 -0.048725 0.131733 0.189 Uiso 1 1 calc R U . . .
H9C H 0.948163 -0.009141 0.146035 0.189 Uiso 1 1 calc R U . . .
C145 C 0.9332(4) 0.6035(5) 0.3143(4) 0.123(3) Uani 1 1 d . U . . .
H14A H 0.931437 0.621120 0.278555 0.185 Uiso 1 1 calc R U . . .
H14B H 0.911939 0.637077 0.338557 0.185 Uiso 1 1 calc R U . . .
H14C H 0.906487 0.562311 0.316748 0.185 Uiso 1 1 calc R U . . .
C73 C 0.3997(6) 0.6569(4) 0.2749(3) 0.115(3) Uani 1 1 d . U . . .
H73 H 0.363849 0.688913 0.264470 0.139 Uiso 1 1 calc R U . . .
C147 C 0.5632(5) -0.0389(5) 0.0550(3) 0.120(3) Uani 1 1 d . U . . .
H147 H 0.583175 -0.036160 0.020604 0.144 Uiso 1 1 calc R U . . .
C37 C 0.8469(7) -0.1730(5) 0.1403(5) 0.174(5) Uani 1 1 d . U . . .
H37 H 0.879007 -0.207941 0.151502 0.209 Uiso 1 1 calc R U . . .
C149 C 0.4647(5) -0.0645(5) 0.1145(5) 0.141(3) Uani 1 1 d . U . . .
H149 H 0.417727 -0.079491 0.120398 0.169 Uiso 1 1 calc R U . . .
C75 C 0.5795(6) 0.7209(5) 0.3531(5) 0.174(5) Uani 1 1 d . U . . .
H75A H 0.574856 0.744866 0.319788 0.260 Uiso 1 1 calc R U . . .
H75B H 0.627033 0.727188 0.366903 0.260 Uiso 1 1 calc R U . . .
H75C H 0.543216 0.738717 0.378142 0.260 Uiso 1 1 calc R U . . .
C151 C 0.4411(3) 0.4752(3) 0.15751(18) 0.0604(13) Uani 1 1 d . U . . .
H151 H 0.488233 0.488701 0.163152 0.073 Uiso 1 1 calc R U . . .
C19 C 0.5319(7) -0.0738(9) 0.2556(5) 0.266(9) Uani 1 1 d . U . . .
H19A H 0.547894 -0.027902 0.259103 0.400 Uiso 1 1 d R U . . .
H19B H 0.571754 -0.103192 0.243043 0.400 Uiso 1 1 d R U . . .
H19C H 0.514644 -0.089992 0.289613 0.400 Uiso 1 1 d R U . . .
C153 C 0.7259(6) -0.1332(4) 0.1170(5) 0.157(4) Uani 1 1 d . U . . .
H153 H 0.677058 -0.142523 0.113009 0.188 Uiso 1 1 calc R U . . .
C77 C 0.4905(5) -0.0569(5) 0.0636(5) 0.146(4) Uani 1 1 d . U . . .
H77 H 0.460483 -0.063596 0.034833 0.175 Uiso 1 1 calc R U . . .
C155 C 0.7771(8) -0.1847(4) 0.1333(5) 0.174(5) Uani 1 1 d . U . . .
H155 H 0.761111 -0.228791 0.139426 0.209 Uiso 1 1 calc R U . . .
Cu13 Cu 0.70507(2) 0.32124(2) 0.12466(2) 0.05111(14) Uani 0.532(3) 1 d . U P A
2
Cu12 Cu 0.59253(3) 0.16401(3) 0.30402(2) 0.06471(16) Uani 0.392(3) 1 d . U P A
4
Cu2 Cu 0.89925(3) 0.15205(2) 0.24987(2) 0.05818(14) Uani 0.423(3) 1 d . U P A 6
Cu14 Cu 0.76539(2) 0.39654(3) 0.33718(2) 0.05237(15) Uani 0.654(3) 1 d . U P A
8


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 Ag4 2.8517(4) . ?
Ag1 Ag6 2.8660(4) . ?
Ag1 Ag8 2.8558(4) . ?
Ag1 Ag10 2.8639(4) . ?
Ag1 Ag13 2.9050(6) . ?
Ag1 Ag14 2.8924(6) . ?
Ag1 S1 2.5543(11) . ?
Ag1 S8 2.5471(11) . ?
Ag1 Cu13 2.9050(6) . ?
Ag1 Cu14 2.8924(6) . ?
Ag4 Ag6 2.8579(4) . ?
Ag4 Ag8 2.8822(4) . ?
Ag4 Ag5 2.8560(4) . ?
Ag4 Ag2 2.9231(6) . ?
Ag4 Ag14 2.8971(6) . ?
Ag4 S4 2.5530(11) . ?
Ag4 S2 2.5477(12) . ?
Ag4 Cu2 2.9231(6) . ?
Ag4 Cu14 2.8971(6) . ?
Ag6 Ag10 2.8635(4) . ?
Ag6 Ag5 2.8555(5) . ?
Ag6 Ag13 2.9197(6) . ?
Ag6 Ag2 2.9456(6) . ?
Ag6 S10 2.5486(12) . ?
Ag6 S12 2.5543(11) . ?
Ag6 Cu13 2.9197(6) . ?
Ag6 Cu2 2.9456(6) . ?
Ag8 Ag10 2.8497(5) . ?
Ag8 Ag5 2.8829(5) . ?
Ag8 Ag12 2.9127(6) . ?
Ag8 Ag14 2.9262(6) . ?
Ag8 S6 2.5428(11) . ?
Ag8 S9 2.5545(11) . ?
Ag8 Cu12 2.9127(6) . ?
Ag8 Cu14 2.9262(6) . ?
Ag10 Ag5 2.8814(5) . ?
Ag10 Ag13 2.9464(6) . ?
Ag10 Ag12 2.9959(6) . ?
Ag10 S3 2.5584(13) . ?
Ag10 S11 2.5451(13) . ?
Ag10 Cu13 2.9464(6) . ?
Ag10 Cu12 2.9959(6) . ?
Ag5 Ag2 2.9401(6) . ?
Ag5 Ag12 2.9478(6) . ?
Ag5 S7 2.5587(12) . ?
Ag5 S5 2.5608(13) . ?
Ag5 Cu12 2.9478(6) . ?
Ag5 Cu2 2.9401(6) . ?
Ag3 S1 2.6410(11) . ?
Ag3 S4 2.6301(11) . ?
Ag3 S12 2.6520(13) . ?
Ag3 P1 2.4280(11) . ?
Ag7 S6 2.6266(12) . ?
Ag7 S7 2.6496(12) . ?
Ag7 S2 2.6793(12) . ?
Ag7 P4 2.4271(13) . ?
Ag11 S8 2.6266(11) . ?
Ag11 S3 2.6912(13) . ?
Ag11 S9 2.6840(14) . ?
Ag11 P2 2.4352(13) . ?
Ag9 S10 2.6878(13) . ?
Ag9 S5 2.6397(14) . ?
Ag9 S11 2.6432(14) . ?
Ag9 P3 2.4246(15) . ?
Ag13 S1 2.3559(11) . ?
Ag13 S10 2.3347(13) . ?
Ag13 S3 2.3455(12) . ?
Ag2 S12 2.3683(13) . ?
Ag2 S2 2.3588(13) . ?
Ag2 S5 2.3700(14) . ?
Ag12 S7 2.3742(13) . ?
Ag12 S9 2.3598(15) . ?
Ag12 S11 2.3743(14) . ?
Ag14 S4 2.3113(11) . ?
Ag14 S6 2.3042(12) . ?
Ag14 S8 2.3127(12) . ?
S1 C32 1.773(4) . ?
S1 Cu13 2.3559(11) . ?
S4 C4 1.762(4) . ?
S4 Cu14 2.3113(11) . ?
S6 C10 1.762(4) . ?
S6 Cu14 2.3042(12) . ?
S8 C56 1.761(5) . ?
S8 Cu14 2.3127(12) . ?
S10 C28 1.763(5) . ?
S10 Cu13 2.3347(13) . ?
S12 C16 1.759(4) . ?
S12 Cu2 2.3683(13) . ?
S3 C8 1.759(4) . ?
S3 Cu13 2.3455(12) . ?
S7 C42 1.767(5) . ?
S7 Cu12 2.3742(13) . ?
S2 C34 1.763(5) . ?
S2 Cu2 2.3588(13) . ?
P1 C22 1.823(5) . ?
P1 C54 1.819(5) . ?
P1 C82 1.812(5) . ?
S9 C52 1.748(5) . ?
S9 Cu12 2.3598(15) . ?
S5 C76 1.762(5) . ?
S5 Cu2 2.3700(14) . ?
P4 C72 1.822(5) . ?
P4 C78 1.817(5) . ?
P4 C106 1.813(5) . ?
S11 C128 1.758(5) . ?
S11 Cu12 2.3743(14) . ?
P2 C102 1.816(6) . ?
P2 C104 1.818(5) . ?
P2 C112 1.816(5) . ?
P3 C116 1.828(7) . ?
P3 C3 1.821(6) . ?
P3 C133 1.809(8) . ?
F1 C1 1.338(5) . ?
F4 C30 1.336(5) . ?
F6 C36 1.347(5) . ?
F8 C40 1.334(6) . ?
F10 C60 1.347(6) . ?
F12 C46 1.354(6) . ?
F14 C12 1.341(5) . ?
F16 C18 1.346(6) . ?
F18 C44 1.345(5) . ?
F20 C14 1.340(6) . ?
F22 C6 1.351(6) . ?
F24 C68 1.350(6) . ?
F26 C58 1.337(6) . ?
F28 C88 1.338(6) . ?
F30 C110 1.345(6) . ?
F32 C84 1.358(7) . ?
F34 C90 1.344(6) . ?
F36 C11 1.342(7) . ?
F38 C74 1.342(6) . ?
F40 C24 1.349(5) . ?
F42 C146 1.327(6) . ?
F44 C122 1.344(7) . ?
F46 C134 1.335(6) . ?
F48 C150 1.333(7) . ?
O1 C26 1.377(6) . ?
O1 C100 1.432(7) . ?
F50 C98 1.340(6) . ?
F52 C154 1.349(6) . ?
F54 C48 1.339(6) . ?
F56 C152 1.339(7) . ?
O4 C66 1.356(7) . ?
O4 C83 1.439(7) . ?
F58 C118 1.345(6) . ?
F60 C92 1.350(6) . ?
F15 C156 1.352(8) . ?
F31 C5 1.336(7) . ?
F2 C142 1.346(6) . ?
F33 C13 1.341(8) . ?
F17 C97 1.348(6) . ?
F35 C130 1.339(5) . ?
F9 C85 1.341(7) . ?
O6 C136 1.378(7) . ?
O6 C99 1.456(8) . ?
F37 C95 1.352(7) . ?
F19 C140 1.330(8) . ?
F39 C27 1.354(7) . ?
F5 C25 1.350(7) . ?
O8 C70 1.367(6) . ?
O8 C49 1.439(7) . ?
F41 C2 1.341(8) . ?
F21 C47 1.333(6) . ?
O10 C87 1.353(7) . ?
O10 C89 1.431(7) . ?
O12 C39 1.351(7) . ?
O12 C57 1.435(7) . ?
C1 C4 1.390(6) . ?
C1 C18 1.384(6) . ?
C4 C6 1.367(6) . ?
O3 C144 1.353(7) . ?
O3 C145 1.417(9) . ?
F43 C101 1.312(9) . ?
F11 C121 1.329(9) . ?
F45 C29 1.340(6) . ?
C6 C48 1.374(7) . ?
O7 C120 1.364(8) . ?
O7 C129 1.422(9) . ?
C8 C12 1.399(6) . ?
C8 C44 1.380(6) . ?
C10 C58 1.395(7) . ?
C10 C110 1.382(7) . ?
F23 C107 1.356(8) . ?
C12 C74 1.373(7) . ?
F47 C51 1.341(6) . ?
C14 C28 1.373(7) . ?
C14 C5 1.384(7) . ?
C16 C30 1.389(7) . ?
C16 C98 1.391(7) . ?
C18 C24 1.360(7) . ?
F3 C111 1.344(7) . ?
C20 H20 0.9500 . ?
C20 C26 1.382(6) . ?
C20 C54 1.396(6) . ?
C22 C38 1.394(6) . ?
C22 C50 1.383(6) . ?
C24 C48 1.362(8) . ?
C26 C86 1.382(7) . ?
C28 C88 1.389(7) . ?
C30 C146 1.373(7) . ?
C32 C36 1.373(6) . ?
C32 C46 1.385(6) . ?
C34 C40 1.400(7) . ?
C34 C60 1.374(7) . ?
C36 C134 1.381(7) . ?
C38 H38 0.9500 . ?
C38 C70 1.374(7) . ?
F49 C123 1.347(8) . ?
C40 C92 1.383(7) . ?
C42 C68 1.380(7) . ?
C42 C154 1.376(7) . ?
C44 C118 1.370(7) . ?
C46 C142 1.354(7) . ?
F25 C93 1.355(7) . ?
F51 C117 1.345(7) . ?
C50 H50 0.9500 . ?
C50 C148 1.385(7) . ?
C52 C84 1.376(9) . ?
C52 C140 1.401(8) . ?
C54 C94 1.384(7) . ?
F13 C109 1.345(7) . ?
C56 C90 1.371(7) . ?
C56 C122 1.389(7) . ?
C58 C85 1.387(7) . ?
C60 C150 1.381(7) . ?
C62 H62 0.9500 . ?
C62 C106 1.397(7) . ?
C62 C39 1.376(7) . ?
C64 H64 0.9500 . ?
C64 C66 1.377(7) . ?
C64 C78 1.405(7) . ?
C66 C115 1.383(8) . ?
F53 C127 1.348(6) . ?
C68 C25 1.372(7) . ?
C70 C108 1.393(7) . ?
F27 C139 1.363(8) . ?
C72 C80 1.396(7) . ?
C72 C114 1.377(7) . ?
F55 C15 1.328(9) . ?
C74 C130 1.366(8) . ?
C76 C152 1.380(8) . ?
C76 C156 1.377(8) . ?
C78 C45 1.383(7) . ?
O2 C53 1.362(9) . ?
O2 C35 1.427(9) . ?
C80 H80 0.9500 . ?
C80 C136 1.388(7) . ?
C82 C96 1.385(7) . ?
C82 C43 1.381(6) . ?
C84 C101 1.383(8) . ?
C86 H86 0.9500 . ?
C86 C126 1.372(7) . ?
C88 C95 1.364(7) . ?
C90 C107 1.358(8) . ?
C92 C97 1.358(9) . ?
C94 H94 0.9500 . ?
C94 C126 1.391(7) . ?
C96 H96 0.9500 . ?
C96 C144 1.383(7) . ?
C98 C109 1.372(8) . ?
C100 H10A 0.9800 . ?
C100 H10B 0.9800 . ?
C100 H10C 0.9800 . ?
C102 C91 1.382(8) . ?
C102 C61 1.399(8) . ?
C104 C124 1.389(8) . ?
C104 C81 1.376(7) . ?
C106 C105 1.371(7) . ?
F7 C33 1.355(7) . ?
F57 C67 1.362(9) . ?
C108 H108 0.9500 . ?
C108 C148 1.364(7) . ?
C110 C27 1.359(7) . ?
C112 C103 1.384(7) . ?
C112 C151 1.397(7) . ?
C114 H114 0.9500 . ?
C114 C23 1.404(7) . ?
C116 C41 1.402(9) . ?
C116 C119 1.382(9) . ?
C118 C130 1.382(8) . ?
F29 C135 1.344(7) . ?
C120 C124 1.389(7) . ?
C120 C79 1.355(9) . ?
C122 C123 1.354(8) . ?
C124 H124 0.9500 . ?
C126 H126 0.9500 . ?
C128 C11 1.366(8) . ?
C128 C13 1.396(8) . ?
C132 H132 0.9500 . ?
C132 C79 1.339(10) . ?
C132 C81 1.415(8) . ?
O9 C141 1.354(9) . ?
O9 C75 1.537(11) . ?
C134 C29 1.366(8) . ?
C136 C7 1.378(9) . ?
C138 H138 0.9500 . ?
C138 C144 1.392(8) . ?
C138 C21 1.354(9) . ?
F59 C69 1.353(7) . ?
C140 C15 1.350(9) . ?
C142 C29 1.360(8) . ?
C146 C47 1.373(9) . ?
C148 H148 0.9500 . ?
C150 C97 1.362(9) . ?
C152 C121 1.381(8) . ?
C154 C111 1.404(8) . ?
C156 C67 1.366(9) . ?
C39 C31 1.386(8) . ?
C79 H79 0.9500 . ?
C5 C127 1.355(9) . ?
C81 H81 0.9500 . ?
C41 H41 0.9500 . ?
C41 C53 1.382(9) . ?
C83 H83A 0.9800 . ?
C83 H83B 0.9800 . ?
C83 H83C 0.9800 . ?
C21 H21 0.9500 . ?
C21 C43 1.403(8) . ?
O5 C137 1.359(12) . ?
O5 C9 1.427(11) . ?
C85 C51 1.368(10) . ?
C43 H43 0.9500 . ?
C87 C63 1.391(8) . ?
C87 C151 1.390(7) . ?
C11 C2 1.392(8) . ?
C89 H89A 0.9800 . ?
C89 H89B 0.9800 . ?
C89 H89C 0.9800 . ?
C45 H45 0.9500 . ?
C45 C65 1.411(9) . ?
C91 H91 0.9500 . ?
C91 C141 1.407(10) . ?
C23 H23 0.9500 . ?
C23 C7 1.370(9) . ?
C93 C101 1.393(12) . ?
C93 C15 1.386(13) . ?
C47 C109 1.360(9) . ?
C95 C127 1.388(9) . ?
C3 C125 1.367(9) . ?
C3 C147 1.359(10) . ?
C49 H49A 0.9800 . ?
C49 H49B 0.9800 . ?
C49 H49C 0.9800 . ?
C99 H99A 0.9800 . ?
C99 H99B 0.9800 . ?
C99 H99C 0.9800 . ?
C25 C117 1.366(9) . ?
C51 C27 1.345(10) . ?
C103 H103 0.9500 . ?
C103 C55 1.391(8) . ?
C13 C139 1.384(9) . ?
C105 H105 0.9500 . ?
C105 C17 1.401(8) . ?
C53 C131 1.376(10) . ?
C107 C135 1.372(10) . ?
C55 H55 0.9500 . ?
C55 C63 1.374(9) . ?
C111 C117 1.352(10) . ?
C7 H7 0.9500 . ?
C113 H113 0.9500 . ?
C113 C133 1.398(10) . ?
C113 C137 1.394(11) . ?
C57 H57A 0.9800 . ?
C57 H57B 0.9800 . ?
C57 H57C 0.9800 . ?
C115 H115 0.9500 . ?
C115 C65 1.362(9) . ?
C59 H59 0.9500 . ?
C59 C119 1.426(11) . ?
C59 C131 1.363(11) . ?
C119 H119 0.9500 . ?
C121 C69 1.366(12) . ?
C61 H61 0.9500 . ?
C61 C73 1.356(11) . ?
C123 C135 1.356(10) . ?
O11 C71 1.339(11) . ?
O11 C19 1.813(17) . ?
C31 H31 0.9500 . ?
C31 C17 1.362(9) . ?
C125 H125 0.9500 . ?
C125 C71 1.365(10) . ?
C63 H63 0.9500 . ?
C2 C33 1.374(11) . ?
C129 H12A 0.9800 . ?
C129 H12B 0.9800 . ?
C129 H12C 0.9800 . ?
C65 H65 0.9500 . ?
C131 H131 0.9500 . ?
C33 C139 1.350(12) . ?
C133 C153 1.375(9) . ?
C67 C69 1.372(12) . ?
C17 H17 0.9500 . ?
C137 C37 1.280(12) . ?
C35 H35A 0.9800 . ?
C35 H35B 0.9800 . ?
C35 H35C 0.9800 . ?
C141 C143 1.381(12) . ?
C71 C149 1.307(14) . ?
C143 H143 0.9500 . ?
C143 C73 1.398(12) . ?
C9 H9A 0.9800 . ?
C9 H9B 0.9800 . ?
C9 H9C 0.9800 . ?
C145 H14A 0.9800 . ?
C145 H14B 0.9800 . ?
C145 H14C 0.9800 . ?
C73 H73 0.9500 . ?
C147 H147 0.9500 . ?
C147 C77 1.437(11) . ?
C37 H37 0.9500 . ?
C37 C155 1.358(17) . ?
C149 H149 0.9500 . ?
C149 C77 1.390(14) . ?
C75 H75A 0.9800 . ?
C75 H75B 0.9800 . ?
C75 H75C 0.9800 . ?
C151 H151 0.9500 . ?
C19 H19A 0.9798 . ?
C19 H19B 0.9800 . ?
C19 H19C 0.9796 . ?
C153 H153 0.9500 . ?
C153 C155 1.445(16) . ?
C77 H77 0.9500 . ?
C155 H155 0.9500 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Ag4 Ag1 Ag6 59.978(11) . . ?
Ag4 Ag1 Ag8 60.660(11) . . ?
Ag4 Ag1 Ag10 90.153(13) . . ?
Ag4 Ag1 Ag13 120.738(15) . . ?
Ag4 Ag1 Ag14 60.573(13) . . ?
Ag4 Ag1 Cu13 120.738(15) . . ?
Ag4 Ag1 Cu14 60.573(13) . . ?
Ag6 Ag1 Ag13 60.781(12) . . ?
Ag6 Ag1 Ag14 120.548(15) . . ?
Ag6 Ag1 Cu13 60.781(12) . . ?
Ag6 Ag1 Cu14 120.548(15) . . ?
Ag8 Ag1 Ag6 90.167(13) . . ?
Ag8 Ag1 Ag10 59.764(11) . . ?
Ag8 Ag1 Ag13 121.181(15) . . ?
Ag8 Ag1 Ag14 61.198(13) . . ?
Ag8 Ag1 Cu13 121.181(15) . . ?
Ag8 Ag1 Cu14 61.198(13) . . ?
Ag10 Ag1 Ag6 59.968(11) . . ?
Ag10 Ag1 Ag13 61.422(12) . . ?
Ag10 Ag1 Ag14 120.962(15) . . ?
Ag10 Ag1 Cu13 61.422(12) . . ?
Ag10 Ag1 Cu14 120.962(15) . . ?
S1 Ag1 Ag4 109.87(3) . . ?
S1 Ag1 Ag6 74.12(3) . . ?
S1 Ag1 Ag8 164.28(3) . . ?
S1 Ag1 Ag10 110.16(3) . . ?
S1 Ag1 Ag13 50.63(3) . . ?
S1 Ag1 Ag14 127.24(3) . . ?
S1 Ag1 Cu13 50.63(3) . . ?
S1 Ag1 Cu14 127.24(3) . . ?
S8 Ag1 Ag4 108.76(3) . . ?
S8 Ag1 Ag6 164.05(3) . . ?
S8 Ag1 Ag8 74.02(3) . . ?
S8 Ag1 Ag10 111.64(3) . . ?
S8 Ag1 Ag13 129.43(3) . . ?
S8 Ag1 Ag14 49.83(3) . . ?
S8 Ag1 S1 121.70(4) . . ?
S8 Ag1 Cu13 129.43(3) . . ?
S8 Ag1 Cu14 49.83(3) . . ?
Ag1 Ag4 Ag6 60.260(10) . . ?
Ag1 Ag4 Ag8 59.741(10) . . ?
Ag1 Ag4 Ag5 90.443(12) . . ?
Ag1 Ag4 Ag2 121.497(15) . . ?
Ag1 Ag4 Ag14 60.409(13) . . ?
Ag1 Ag4 Cu2 121.497(15) . . ?
Ag1 Ag4 Cu14 60.409(13) . . ?
Ag6 Ag4 Ag8 89.800(12) . . ?
Ag6 Ag4 Ag2 61.252(13) . . ?
Ag6 Ag4 Ag14 120.665(15) . . ?
Ag6 Ag4 Cu2 61.252(13) . . ?
Ag6 Ag4 Cu14 120.665(15) . . ?
Ag8 Ag4 Ag2 121.462(15) . . ?
Ag8 Ag4 Ag14 60.838(12) . . ?
Ag8 Ag4 Cu2 121.462(15) . . ?
Ag8 Ag4 Cu14 60.838(12) . . ?
Ag5 Ag4 Ag6 59.965(11) . . ?
Ag5 Ag4 Ag8 60.317(11) . . ?
Ag5 Ag4 Ag2 61.147(13) . . ?
Ag5 Ag4 Ag14 121.150(15) . . ?
Ag5 Ag4 Cu2 61.147(13) . . ?
Ag5 Ag4 Cu14 121.150(15) . . ?
S4 Ag4 Ag1 72.65(3) . . ?
S4 Ag4 Ag6 110.07(3) . . ?
S4 Ag4 Ag8 108.45(3) . . ?
S4 Ag4 Ag5 163.08(3) . . ?
S4 Ag4 Ag2 128.47(3) . . ?
S4 Ag4 Ag14 49.69(3) . . ?
S4 Ag4 Cu2 128.47(3) . . ?
S4 Ag4 Cu14 49.69(3) . . ?
S2 Ag4 Ag1 165.02(3) . . ?
S2 Ag4 Ag6 109.96(3) . . ?
S2 Ag4 Ag8 111.43(3) . . ?
S2 Ag4 Ag5 74.59(3) . . ?
S2 Ag4 Ag2 50.51(3) . . ?
S2 Ag4 Ag14 128.11(3) . . ?
S2 Ag4 S4 122.32(4) . . ?
S2 Ag4 Cu2 50.51(3) . . ?
S2 Ag4 Cu14 128.11(3) . . ?
Ag1 Ag6 Ag13 60.269(12) . . ?
Ag1 Ag6 Ag2 120.214(15) . . ?
Ag1 Ag6 Cu13 60.269(12) . . ?
Ag1 Ag6 Cu2 120.214(15) . . ?
Ag4 Ag6 Ag1 59.762(10) . . ?
Ag4 Ag6 Ag10 90.034(12) . . ?
Ag4 Ag6 Ag13 120.010(15) . . ?
Ag4 Ag6 Ag2 60.465(13) . . ?
Ag4 Ag6 Cu13 120.010(15) . . ?
Ag4 Ag6 Cu2 60.465(13) . . ?
Ag10 Ag6 Ag1 59.979(11) . . ?
Ag10 Ag6 Ag13 61.249(12) . . ?
Ag10 Ag6 Ag2 121.389(15) . . ?
Ag10 Ag6 Cu13 61.249(12) . . ?
Ag10 Ag6 Cu2 121.389(15) . . ?
Ag5 Ag6 Ag1 90.166(13) . . ?
Ag5 Ag6 Ag4 59.984(11) . . ?
Ag5 Ag6 Ag10 60.508(11) . . ?
Ag5 Ag6 Ag13 121.756(15) . . ?
Ag5 Ag6 Ag2 60.881(13) . . ?
Ag5 Ag6 Cu13 121.756(15) . . ?
Ag5 Ag6 Cu2 60.881(13) . . ?
S10 Ag6 Ag1 108.54(3) . . ?
S10 Ag6 Ag4 164.17(3) . . ?
S10 Ag6 Ag10 74.36(3) . . ?
S10 Ag6 Ag5 112.38(3) . . ?
S10 Ag6 Ag13 49.99(3) . . ?
S10 Ag6 Ag2 130.22(3) . . ?
S10 Ag6 S12 121.08(4) . . ?
S10 Ag6 Cu13 49.99(3) . . ?
S10 Ag6 Cu2 130.22(3) . . ?
S12 Ag6 Ag1 110.64(3) . . ?
S12 Ag6 Ag4 74.53(3) . . ?
S12 Ag6 Ag10 164.56(3) . . ?
S12 Ag6 Ag5 109.69(3) . . ?
S12 Ag6 Ag13 126.95(3) . . ?
S12 Ag6 Ag2 50.40(3) . . ?
S12 Ag6 Cu13 126.95(3) . . ?
S12 Ag6 Cu2 50.40(3) . . ?
Ag1 Ag8 Ag4 59.599(10) . . ?
Ag1 Ag8 Ag5 89.819(12) . . ?
Ag1 Ag8 Ag12 122.898(16) . . ?
Ag1 Ag8 Ag14 60.018(13) . . ?
Ag1 Ag8 Cu12 122.898(16) . . ?
Ag1 Ag8 Cu14 60.018(13) . . ?
Ag4 Ag8 Ag5 59.392(11) . . ?
Ag4 Ag8 Ag12 120.483(16) . . ?
Ag4 Ag8 Ag14 59.833(13) . . ?
Ag4 Ag8 Cu12 120.483(16) . . ?
Ag4 Ag8 Cu14 59.833(13) . . ?
Ag10 Ag8 Ag1 60.258(11) . . ?
Ag10 Ag8 Ag4 89.825(12) . . ?
Ag10 Ag8 Ag5 60.346(11) . . ?
Ag10 Ag8 Ag12 62.642(13) . . ?
Ag10 Ag8 Ag14 120.276(15) . . ?
Ag10 Ag8 Cu12 62.642(13) . . ?
Ag10 Ag8 Cu14 120.276(15) . . ?
Ag5 Ag8 Ag12 61.141(14) . . ?
Ag5 Ag8 Ag14 119.219(15) . . ?
Ag5 Ag8 Cu12 61.141(14) . . ?
Ag5 Ag8 Cu14 119.219(15) . . ?
S6 Ag8 Ag1 107.37(3) . . ?
S6 Ag8 Ag4 72.35(3) . . ?
S6 Ag8 Ag10 162.10(3) . . ?
S6 Ag8 Ag5 109.54(3) . . ?
S6 Ag8 Ag12 127.79(3) . . ?
S6 Ag8 Ag14 49.23(3) . . ?
S6 Ag8 S9 123.38(4) . . ?
S6 Ag8 Cu12 127.79(3) . . ?
S6 Ag8 Cu14 49.23(3) . . ?
S9 Ag8 Ag1 111.97(3) . . ?
S9 Ag8 Ag4 164.21(3) . . ?
S9 Ag8 Ag10 74.48(3) . . ?
S9 Ag8 Ag5 109.61(3) . . ?
S9 Ag8 Ag12 50.62(3) . . ?
S9 Ag8 Ag14 129.87(4) . . ?
S9 Ag8 Cu12 50.62(3) . . ?
S9 Ag8 Cu14 129.87(4) . . ?
Ag1 Ag10 Ag5 89.689(12) . . ?
Ag1 Ag10 Ag13 59.976(12) . . ?
Ag1 Ag10 Ag12 119.683(15) . . ?
Ag1 Ag10 Cu13 59.976(12) . . ?
Ag1 Ag10 Cu12 119.683(15) . . ?
Ag6 Ag10 Ag1 60.053(10) . . ?
Ag6 Ag10 Ag5 59.607(11) . . ?
Ag6 Ag10 Ag13 60.315(12) . . ?
Ag6 Ag10 Ag12 119.774(16) . . ?
Ag6 Ag10 Cu13 60.315(12) . . ?
Ag6 Ag10 Cu12 119.774(16) . . ?
Ag8 Ag10 Ag1 59.977(10) . . ?
Ag8 Ag10 Ag6 90.340(12) . . ?
Ag8 Ag10 Ag5 60.399(11) . . ?
Ag8 Ag10 Ag13 119.949(15) . . ?
Ag8 Ag10 Ag12 59.708(13) . . ?
Ag8 Ag10 Cu13 119.949(15) . . ?
Ag8 Ag10 Cu12 59.708(13) . . ?
Ag5 Ag10 Ag13 119.921(14) . . ?
Ag5 Ag10 Ag12 60.167(13) . . ?
Ag5 Ag10 Cu13 119.921(14) . . ?
Ag5 Ag10 Cu12 60.167(13) . . ?
S3 Ag10 Ag1 72.20(3) . . ?
S3 Ag10 Ag6 108.16(3) . . ?
S3 Ag10 Ag8 109.24(3) . . ?
S3 Ag10 Ag5 161.84(3) . . ?
S3 Ag10 Ag13 49.83(3) . . ?
S3 Ag10 Ag12 129.96(3) . . ?
S3 Ag10 Cu13 49.83(3) . . ?
S3 Ag10 Cu12 129.96(3) . . ?
S11 Ag10 Ag1 162.94(4) . . ?
S11 Ag10 Ag6 110.80(3) . . ?
S11 Ag10 Ag8 108.10(3) . . ?
S11 Ag10 Ag5 73.38(3) . . ?
S11 Ag10 Ag13 130.45(3) . . ?
S11 Ag10 Ag12 49.93(3) . . ?
S11 Ag10 S3 124.77(4) . . ?
S11 Ag10 Cu13 130.45(3) . . ?
S11 Ag10 Cu12 49.93(3) . . ?
Ag4 Ag5 Ag8 60.291(11) . . ?
Ag4 Ag5 Ag10 89.714(13) . . ?
Ag4 Ag5 Ag2 60.552(13) . . ?
Ag4 Ag5 Ag12 120.168(16) . . ?
Ag4 Ag5 Cu12 120.168(16) . . ?
Ag4 Ag5 Cu2 60.552(13) . . ?
Ag6 Ag5 Ag4 60.051(11) . . ?
Ag6 Ag5 Ag8 89.834(13) . . ?
Ag6 Ag5 Ag10 59.885(11) . . ?
Ag6 Ag5 Ag2 61.074(12) . . ?
Ag6 Ag5 Ag12 121.727(16) . . ?
Ag6 Ag5 Cu12 121.727(16) . . ?
Ag6 Ag5 Cu2 61.074(12) . . ?
Ag8 Ag5 Ag2 120.841(15) . . ?
Ag8 Ag5 Ag12 59.927(13) . . ?
Ag8 Ag5 Cu12 59.927(13) . . ?
Ag8 Ag5 Cu2 120.841(15) . . ?
Ag10 Ag5 Ag8 59.255(11) . . ?
Ag10 Ag5 Ag2 120.958(15) . . ?
Ag10 Ag5 Ag12 61.843(13) . . ?
Ag10 Ag5 Cu12 61.843(13) . . ?
Ag10 Ag5 Cu2 120.958(15) . . ?
S7 Ag5 Ag4 108.90(3) . . ?
S7 Ag5 Ag6 163.26(3) . . ?
S7 Ag5 Ag8 73.46(3) . . ?
S7 Ag5 Ag10 110.24(3) . . ?
S7 Ag5 Ag2 126.79(3) . . ?
S7 Ag5 Ag12 50.48(3) . . ?
S7 Ag5 S5 122.61(4) . . ?
S7 Ag5 Cu12 50.48(3) . . ?
S7 Ag5 Cu2 126.79(3) . . ?
S5 Ag5 Ag4 109.18(3) . . ?
S5 Ag5 Ag6 74.08(3) . . ?
S5 Ag5 Ag8 163.90(3) . . ?
S5 Ag5 Ag10 111.22(3) . . ?
S5 Ag5 Ag2 50.47(3) . . ?
S5 Ag5 Ag12 129.55(3) . . ?
S5 Ag5 Cu12 129.55(3) . . ?
S5 Ag5 Cu2 50.47(3) . . ?
S1 Ag3 S12 101.53(4) . . ?
S4 Ag3 S1 100.13(3) . . ?
S4 Ag3 S12 103.70(4) . . ?
P1 Ag3 S1 120.04(4) . . ?
P1 Ag3 S4 114.57(4) . . ?
P1 Ag3 S12 114.51(4) . . ?
S6 Ag7 S7 101.54(4) . . ?
S6 Ag7 S2 101.33(4) . . ?
S7 Ag7 S2 100.22(4) . . ?
P4 Ag7 S6 115.00(4) . . ?
P4 Ag7 S7 119.42(4) . . ?
P4 Ag7 S2 116.50(4) . . ?
S8 Ag11 S3 101.18(4) . . ?
S8 Ag11 S9 104.68(4) . . ?
S9 Ag11 S3 101.63(4) . . ?
P2 Ag11 S8 120.16(4) . . ?
P2 Ag11 S3 115.11(4) . . ?
P2 Ag11 S9 111.88(4) . . ?
S5 Ag9 S10 104.30(4) . . ?
S5 Ag9 S11 104.57(4) . . ?
S11 Ag9 S10 104.50(4) . . ?
P3 Ag9 S10 112.26(5) . . ?
P3 Ag9 S5 114.47(5) . . ?
P3 Ag9 S11 115.59(5) . . ?
Ag1 Ag13 Ag6 58.949(13) . . ?
Ag1 Ag13 Ag10 58.602(12) . . ?
Ag6 Ag13 Ag10 58.436(12) . . ?
S1 Ag13 Ag1 56.95(3) . . ?
S1 Ag13 Ag6 75.94(3) . . ?
S1 Ag13 Ag10 113.51(3) . . ?
S10 Ag13 Ag1 113.76(3) . . ?
S10 Ag13 Ag6 56.73(3) . . ?
S10 Ag13 Ag10 75.81(3) . . ?
S10 Ag13 S1 117.43(4) . . ?
S10 Ag13 S3 118.10(5) . . ?
S3 Ag13 Ag1 74.36(3) . . ?
S3 Ag13 Ag6 112.70(3) . . ?
S3 Ag13 Ag10 56.46(3) . . ?
S3 Ag13 S1 116.57(4) . . ?
Ag4 Ag2 Ag6 58.283(12) . . ?
Ag4 Ag2 Ag5 58.301(12) . . ?
Ag5 Ag2 Ag6 58.045(13) . . ?
S12 Ag2 Ag4 75.98(3) . . ?
S12 Ag2 Ag6 56.20(3) . . ?
S12 Ag2 Ag5 112.55(3) . . ?
S12 Ag2 S5 116.06(5) . . ?
S2 Ag2 Ag4 56.47(3) . . ?
S2 Ag2 Ag6 112.82(3) . . ?
S2 Ag2 Ag5 75.69(3) . . ?
S2 Ag2 S12 118.02(5) . . ?
S2 Ag2 S5 117.63(5) . . ?
S5 Ag2 Ag4 112.76(4) . . ?
S5 Ag2 Ag6 75.09(3) . . ?
S5 Ag2 Ag5 56.44(3) . . ?
Ag8 Ag12 Ag10 57.650(13) . . ?
Ag8 Ag12 Ag5 58.932(13) . . ?
Ag5 Ag12 Ag10 57.991(13) . . ?
S7 Ag12 Ag8 75.50(3) . . ?
S7 Ag12 Ag10 112.04(3) . . ?
S7 Ag12 Ag5 56.24(3) . . ?
S7 Ag12 S11 117.68(5) . . ?
S9 Ag12 Ag8 56.80(3) . . ?
S9 Ag12 Ag10 74.44(3) . . ?
S9 Ag12 Ag5 113.39(3) . . ?
S9 Ag12 S7 118.62(5) . . ?
S9 Ag12 S11 114.37(5) . . ?
S11 Ag12 Ag8 111.11(3) . . ?
S11 Ag12 Ag10 55.12(3) . . ?
S11 Ag12 Ag5 74.49(3) . . ?
Ag1 Ag14 Ag4 59.018(13) . . ?
Ag1 Ag14 Ag8 58.784(13) . . ?
Ag4 Ag14 Ag8 59.330(13) . . ?
S4 Ag14 Ag1 75.27(3) . . ?
S4 Ag14 Ag4 57.39(3) . . ?
S4 Ag14 Ag8 114.36(3) . . ?
S4 Ag14 S8 116.51(4) . . ?
S6 Ag14 Ag1 113.34(3) . . ?
S6 Ag14 Ag4 75.36(3) . . ?
S6 Ag14 Ag8 56.69(3) . . ?
S6 Ag14 S4 118.48(4) . . ?
S6 Ag14 S8 117.85(4) . . ?
S8 Ag14 Ag1 57.30(3) . . ?
S8 Ag14 Ag4 114.47(3) . . ?
S8 Ag14 Ag8 76.01(3) . . ?
Ag1 S1 Ag3 86.95(3) . . ?
Ag13 S1 Ag1 72.42(3) . . ?
Ag13 S1 Ag3 133.16(5) . . ?
C32 S1 Ag1 111.84(14) . . ?
C32 S1 Ag3 114.07(15) . . ?
C32 S1 Ag13 112.61(15) . . ?
C32 S1 Cu13 112.61(15) . . ?
Cu13 S1 Ag1 72.42(3) . . ?
Cu13 S1 Ag3 133.16(5) . . ?
Ag4 S4 Ag3 86.47(4) . . ?
Ag14 S4 Ag4 72.92(3) . . ?
Ag14 S4 Ag3 135.26(4) . . ?
C4 S4 Ag4 109.72(15) . . ?
C4 S4 Ag3 111.03(14) . . ?
C4 S4 Ag14 113.21(14) . . ?
C4 S4 Cu14 113.21(14) . . ?
Cu14 S4 Ag4 72.92(3) . . ?
Cu14 S4 Ag3 135.26(4) . . ?
Ag8 S6 Ag7 88.21(4) . . ?
Ag14 S6 Ag8 74.09(3) . . ?
Ag14 S6 Ag7 134.70(5) . . ?
C10 S6 Ag8 112.55(14) . . ?
C10 S6 Ag7 113.60(17) . . ?
C10 S6 Ag14 111.70(17) . . ?
C10 S6 Cu14 111.70(17) . . ?
Cu14 S6 Ag8 74.09(3) . . ?
Cu14 S6 Ag7 134.70(5) . . ?
Ag1 S8 Ag11 85.72(4) . . ?
Ag14 S8 Ag1 72.87(3) . . ?
Ag14 S8 Ag11 132.02(5) . . ?
C56 S8 Ag1 109.34(15) . . ?
C56 S8 Ag11 114.45(16) . . ?
C56 S8 Ag14 113.07(16) . . ?
C56 S8 Cu14 113.07(16) . . ?
Cu14 S8 Ag1 72.87(3) . . ?
Cu14 S8 Ag11 132.02(5) . . ?
Ag6 S10 Ag9 82.53(4) . . ?
Ag13 S10 Ag6 73.29(3) . . ?
Ag13 S10 Ag9 130.67(5) . . ?
C28 S10 Ag6 109.53(15) . . ?
C28 S10 Ag9 115.31(17) . . ?
C28 S10 Ag13 113.15(17) . . ?
C28 S10 Cu13 113.15(17) . . ?
Cu13 S10 Ag6 73.29(3) . . ?
Cu13 S10 Ag9 130.67(5) . . ?
Ag6 S12 Ag3 86.82(3) . . ?
Ag2 S12 Ag6 73.40(3) . . ?
Ag2 S12 Ag3 131.75(5) . . ?
C16 S12 Ag6 112.23(15) . . ?
C16 S12 Ag3 114.54(17) . . ?
C16 S12 Ag2 113.66(17) . . ?
C16 S12 Cu2 113.66(17) . . ?
Cu2 S12 Ag6 73.40(3) . . ?
Cu2 S12 Ag3 131.75(5) . . ?
Ag10 S3 Ag11 85.78(4) . . ?
Ag13 S3 Ag10 73.72(3) . . ?
Ag13 S3 Ag11 133.38(5) . . ?
C8 S3 Ag10 111.10(17) . . ?
C8 S3 Ag11 114.27(15) . . ?
C8 S3 Ag13 112.13(16) . . ?
C8 S3 Cu13 112.13(16) . . ?
Cu13 S3 Ag10 73.72(3) . . ?
Cu13 S3 Ag11 133.38(5) . . ?
Ag5 S7 Ag7 88.19(4) . . ?
Ag12 S7 Ag5 73.28(4) . . ?
Ag12 S7 Ag7 133.45(5) . . ?
C42 S7 Ag5 114.53(16) . . ?
C42 S7 Ag7 113.10(18) . . ?
C42 S7 Ag12 113.44(18) . . ?
C42 S7 Cu12 113.44(18) . . ?
Cu12 S7 Ag5 73.28(4) . . ?
Cu12 S7 Ag7 133.45(5) . . ?
Ag4 S2 Ag7 85.83(3) . . ?
Ag2 S2 Ag4 73.02(3) . . ?
Ag2 S2 Ag7 134.15(5) . . ?
C34 S2 Ag4 111.62(15) . . ?
C34 S2 Ag7 113.16(17) . . ?
C34 S2 Ag2 112.39(17) . . ?
C34 S2 Cu2 112.39(17) . . ?
Cu2 S2 Ag4 73.02(3) . . ?
Cu2 S2 Ag7 134.15(5) . . ?
C22 P1 Ag3 112.29(15) . . ?
C54 P1 Ag3 109.92(14) . . ?
C54 P1 C22 106.9(2) . . ?
C82 P1 Ag3 114.17(15) . . ?
C82 P1 C22 107.0(2) . . ?
C82 P1 C54 106.1(2) . . ?
Ag8 S9 Ag11 83.42(4) . . ?
Ag12 S9 Ag8 72.57(4) . . ?
Ag12 S9 Ag11 134.55(5) . . ?
C52 S9 Ag8 109.63(16) . . ?
C52 S9 Ag11 113.7(2) . . ?
C52 S9 Ag12 110.6(2) . . ?
C52 S9 Cu12 110.6(2) . . ?
Cu12 S9 Ag8 72.57(4) . . ?
Cu12 S9 Ag11 134.55(5) . . ?
Ag5 S5 Ag9 83.22(4) . . ?
Ag2 S5 Ag5 73.09(4) . . ?
Ag2 S5 Ag9 131.03(5) . . ?
C76 S5 Ag5 109.30(17) . . ?
C76 S5 Ag9 115.8(2) . . ?
C76 S5 Ag2 112.40(19) . . ?
C76 S5 Cu2 112.40(19) . . ?
Cu2 S5 Ag5 73.09(4) . . ?
Cu2 S5 Ag9 131.03(5) . . ?
C72 P4 Ag7 111.15(16) . . ?
C78 P4 Ag7 114.43(16) . . ?
C78 P4 C72 106.0(2) . . ?
C106 P4 Ag7 111.89(17) . . ?
C106 P4 C72 106.5(2) . . ?
C106 P4 C78 106.4(2) . . ?
Ag10 S11 Ag9 83.75(4) . . ?
Ag12 S11 Ag10 74.94(4) . . ?
Ag12 S11 Ag9 131.48(5) . . ?
C128 S11 Ag10 110.9(2) . . ?
C128 S11 Ag9 114.91(19) . . ?
C128 S11 Ag12 113.35(19) . . ?
C128 S11 Cu12 113.35(19) . . ?
Cu12 S11 Ag10 74.94(4) . . ?
Cu12 S11 Ag9 131.48(5) . . ?
C102 P2 Ag11 116.38(18) . . ?
C102 P2 C104 106.4(3) . . ?
C102 P2 C112 103.5(3) . . ?
C104 P2 Ag11 112.85(19) . . ?
C112 P2 Ag11 110.56(16) . . ?
C112 P2 C104 106.2(2) . . ?
C116 P3 Ag9 111.9(2) . . ?
C3 P3 Ag9 111.6(2) . . ?
C3 P3 C116 106.3(3) . . ?
C133 P3 Ag9 112.8(3) . . ?
C133 P3 C116 108.0(3) . . ?
C133 P3 C3 105.8(3) . . ?
C26 O1 C100 118.1(4) . . ?
C66 O4 C83 116.5(4) . . ?
C136 O6 C99 118.9(5) . . ?
C70 O8 C49 116.5(5) . . ?
C87 O10 C89 117.2(4) . . ?
C39 O12 C57 116.7(4) . . ?
F1 C1 C4 120.4(4) . . ?
F1 C1 C18 117.4(4) . . ?
C18 C1 C4 122.2(4) . . ?
C1 C4 S4 121.8(3) . . ?
C6 C4 S4 121.8(4) . . ?
C6 C4 C1 116.1(4) . . ?
C144 O3 C145 118.7(5) . . ?
F22 C6 C4 119.6(4) . . ?
F22 C6 C48 117.9(4) . . ?
C4 C6 C48 122.5(5) . . ?
C120 O7 C129 117.7(5) . . ?
C12 C8 S3 121.4(4) . . ?
C44 C8 S3 122.6(4) . . ?
C44 C8 C12 115.7(4) . . ?
C58 C10 S6 122.1(4) . . ?
C110 C10 S6 120.9(4) . . ?
C110 C10 C58 116.5(5) . . ?
F14 C12 C8 119.6(4) . . ?
F14 C12 C74 118.4(4) . . ?
C74 C12 C8 122.0(4) . . ?
F20 C14 C28 120.6(4) . . ?
F20 C14 C5 117.2(5) . . ?
C28 C14 C5 122.2(5) . . ?
C30 C16 S12 122.8(4) . . ?
C30 C16 C98 115.5(4) . . ?
C98 C16 S12 121.5(4) . . ?
F16 C18 C1 119.6(5) . . ?
F16 C18 C24 121.1(4) . . ?
C24 C18 C1 119.2(5) . . ?
C26 C20 H20 120.0 . . ?
C26 C20 C54 120.1(5) . . ?
C54 C20 H20 120.0 . . ?
C38 C22 P1 116.7(3) . . ?
C50 C22 P1 122.7(4) . . ?
C50 C22 C38 120.4(5) . . ?
F40 C24 C18 119.9(5) . . ?
F40 C24 C48 120.1(5) . . ?
C18 C24 C48 120.0(4) . . ?
O1 C26 C20 123.4(5) . . ?
O1 C26 C86 116.4(4) . . ?
C86 C26 C20 120.2(5) . . ?
C14 C28 S10 121.5(4) . . ?
C14 C28 C88 116.1(4) . . ?
C88 C28 S10 122.1(4) . . ?
F4 C30 C16 119.6(4) . . ?
F4 C30 C146 117.2(5) . . ?
C146 C30 C16 123.2(5) . . ?
C36 C32 S1 122.7(3) . . ?
C36 C32 C46 116.1(4) . . ?
C46 C32 S1 120.7(4) . . ?
C40 C34 S2 120.7(4) . . ?
C60 C34 S2 122.7(4) . . ?
C60 C34 C40 116.2(5) . . ?
F6 C36 C32 119.9(4) . . ?
F6 C36 C134 117.6(4) . . ?
C32 C36 C134 122.5(5) . . ?
C22 C38 H38 120.0 . . ?
C70 C38 C22 119.9(4) . . ?
C70 C38 H38 120.0 . . ?
F8 C40 C34 120.1(5) . . ?
F8 C40 C92 119.0(5) . . ?
C92 C40 C34 120.8(6) . . ?
C68 C42 S7 122.6(4) . . ?
C154 C42 S7 121.0(4) . . ?
C154 C42 C68 116.2(5) . . ?
F18 C44 C8 119.8(4) . . ?
F18 C44 C118 117.4(4) . . ?
C118 C44 C8 122.8(5) . . ?
F12 C46 C32 120.0(4) . . ?
C142 C46 F12 117.9(4) . . ?
C142 C46 C32 122.1(5) . . ?
F54 C48 C6 120.0(5) . . ?
F54 C48 C24 120.0(5) . . ?
C24 C48 C6 120.0(5) . . ?
C22 C50 H50 120.5 . . ?
C22 C50 C148 118.9(5) . . ?
C148 C50 H50 120.5 . . ?
C84 C52 S9 121.9(4) . . ?
C84 C52 C140 116.8(5) . . ?
C140 C52 S9 121.0(5) . . ?
C20 C54 P1 116.5(4) . . ?
C94 C54 P1 123.5(4) . . ?
C94 C54 C20 119.7(4) . . ?
C90 C56 S8 122.9(4) . . ?
C90 C56 C122 115.9(5) . . ?
C122 C56 S8 120.8(4) . . ?
F26 C58 C10 119.9(4) . . ?
F26 C58 C85 119.0(5) . . ?
C85 C58 C10 121.1(6) . . ?
F10 C60 C34 119.5(4) . . ?
F10 C60 C150 117.4(5) . . ?
C34 C60 C150 123.1(5) . . ?
C106 C62 H62 119.6 . . ?
C39 C62 H62 119.6 . . ?
C39 C62 C106 120.8(5) . . ?
C66 C64 H64 119.7 . . ?
C66 C64 C78 120.7(5) . . ?
C78 C64 H64 119.7 . . ?
O4 C66 C64 124.7(5) . . ?
O4 C66 C115 116.0(5) . . ?
C64 C66 C115 119.4(6) . . ?
F24 C68 C42 119.6(5) . . ?
F24 C68 C25 117.4(5) . . ?
C25 C68 C42 123.0(5) . . ?
O8 C70 C38 124.8(5) . . ?
O8 C70 C108 115.7(5) . . ?
C38 C70 C108 119.5(5) . . ?
C80 C72 P4 115.3(4) . . ?
C114 C72 P4 123.4(4) . . ?
C114 C72 C80 121.1(5) . . ?
F38 C74 C12 119.7(5) . . ?
F38 C74 C130 119.6(5) . . ?
C130 C74 C12 120.7(5) . . ?
C152 C76 S5 122.9(5) . . ?
C156 C76 S5 120.6(5) . . ?
C156 C76 C152 116.4(5) . . ?
C64 C78 P4 117.6(4) . . ?
C45 C78 P4 121.8(4) . . ?
C45 C78 C64 120.4(5) . . ?
C53 O2 C35 119.1(6) . . ?
C72 C80 H80 120.4 . . ?
C136 C80 C72 119.1(5) . . ?
C136 C80 H80 120.4 . . ?
C96 C82 P1 116.7(3) . . ?
C43 C82 P1 123.5(4) . . ?
C43 C82 C96 119.6(5) . . ?
F32 C84 C52 120.6(5) . . ?
F32 C84 C101 116.0(7) . . ?
C52 C84 C101 123.4(7) . . ?
C26 C86 H86 120.2 . . ?
C126 C86 C26 119.7(5) . . ?
C126 C86 H86 120.2 . . ?
F28 C88 C28 119.8(4) . . ?
F28 C88 C95 117.5(5) . . ?
C95 C88 C28 122.6(5) . . ?
F34 C90 C56 119.9(5) . . ?
F34 C90 C107 117.7(5) . . ?
C107 C90 C56 122.4(6) . . ?
F60 C92 C40 118.5(6) . . ?
F60 C92 C97 120.8(5) . . ?
C97 C92 C40 120.7(5) . . ?
C54 C94 H94 120.4 . . ?
C54 C94 C126 119.3(5) . . ?
C126 C94 H94 120.4 . . ?
C82 C96 H96 119.6 . . ?
C144 C96 C82 120.9(5) . . ?
C144 C96 H96 119.6 . . ?
F50 C98 C16 119.4(5) . . ?
F50 C98 C109 119.1(5) . . ?
C109 C98 C16 121.4(6) . . ?
O1 C100 H10A 109.5 . . ?
O1 C100 H10B 109.5 . . ?
O1 C100 H10C 109.5 . . ?
H10A C100 H10B 109.5 . . ?
H10A C100 H10C 109.5 . . ?
H10B C100 H10C 109.5 . . ?
C91 C102 P2 118.3(5) . . ?
C91 C102 C61 119.8(6) . . ?
C61 C102 P2 121.8(5) . . ?
C124 C104 P2 117.0(4) . . ?
C81 C104 P2 123.0(5) . . ?
C81 C104 C124 119.8(5) . . ?
C62 C106 P4 116.0(4) . . ?
C105 C106 P4 123.6(4) . . ?
C105 C106 C62 120.4(5) . . ?
C70 C108 H108 119.9 . . ?
C148 C108 C70 120.3(5) . . ?
C148 C108 H108 119.9 . . ?
F30 C110 C10 119.8(4) . . ?
F30 C110 C27 118.6(5) . . ?
C27 C110 C10 121.6(6) . . ?
C103 C112 P2 124.1(4) . . ?
C103 C112 C151 119.8(5) . . ?
C151 C112 P2 116.0(4) . . ?
C72 C114 H114 120.6 . . ?
C72 C114 C23 118.8(6) . . ?
C23 C114 H114 120.6 . . ?
C41 C116 P3 116.7(4) . . ?
C119 C116 P3 122.1(6) . . ?
C119 C116 C41 121.1(7) . . ?
F58 C118 C44 120.5(5) . . ?
F58 C118 C130 119.5(5) . . ?
C44 C118 C130 120.0(5) . . ?
O7 C120 C124 124.3(6) . . ?
C79 C120 O7 115.5(6) . . ?
C79 C120 C124 120.2(7) . . ?
F44 C122 C56 120.1(5) . . ?
F44 C122 C123 117.7(6) . . ?
C123 C122 C56 122.2(6) . . ?
C104 C124 C120 119.9(5) . . ?
C104 C124 H124 120.1 . . ?
C120 C124 H124 120.1 . . ?
C86 C126 C94 121.1(5) . . ?
C86 C126 H126 119.5 . . ?
C94 C126 H126 119.5 . . ?
C11 C128 S11 122.8(4) . . ?
C11 C128 C13 116.6(5) . . ?
C13 C128 S11 120.2(5) . . ?
F35 C130 C74 120.8(5) . . ?
F35 C130 C118 120.5(5) . . ?
C74 C130 C118 118.8(5) . . ?
C79 C132 H132 119.3 . . ?
C79 C132 C81 121.4(6) . . ?
C81 C132 H132 119.3 . . ?
C141 O9 C75 114.1(8) . . ?
F46 C134 C36 120.0(5) . . ?
F46 C134 C29 120.9(5) . . ?
C29 C134 C36 119.1(5) . . ?
O6 C136 C80 122.6(6) . . ?
O6 C136 C7 117.4(5) . . ?
C7 C136 C80 119.9(6) . . ?
C144 C138 H138 120.2 . . ?
C21 C138 H138 120.2 . . ?
C21 C138 C144 119.6(5) . . ?
F19 C140 C52 120.3(5) . . ?
F19 C140 C15 117.4(7) . . ?
C15 C140 C52 122.2(8) . . ?
F2 C142 C46 120.4(5) . . ?
F2 C142 C29 119.0(5) . . ?
C46 C142 C29 120.6(5) . . ?
O3 C144 C96 123.5(5) . . ?
O3 C144 C138 117.0(5) . . ?
C96 C144 C138 119.5(6) . . ?
F42 C146 C30 121.0(5) . . ?
F42 C146 C47 119.7(5) . . ?
C47 C146 C30 119.4(5) . . ?
C50 C148 H148 119.5 . . ?
C108 C148 C50 120.9(5) . . ?
C108 C148 H148 119.5 . . ?
F48 C150 C60 120.1(6) . . ?
F48 C150 C97 120.8(5) . . ?
C97 C150 C60 119.1(6) . . ?
F56 C152 C76 119.7(5) . . ?
F56 C152 C121 117.5(6) . . ?
C76 C152 C121 122.8(7) . . ?
F52 C154 C42 120.5(5) . . ?
F52 C154 C111 118.0(5) . . ?
C42 C154 C111 121.4(6) . . ?
F15 C156 C76 120.7(5) . . ?
F15 C156 C67 117.7(6) . . ?
C67 C156 C76 121.6(7) . . ?
O12 C39 C62 124.9(5) . . ?
O12 C39 C31 116.4(5) . . ?
C62 C39 C31 118.7(5) . . ?
C120 C79 H79 119.7 . . ?
C132 C79 C120 120.5(6) . . ?
C132 C79 H79 119.7 . . ?
F31 C5 C14 120.5(6) . . ?
F31 C5 C127 119.4(5) . . ?
C127 C5 C14 120.1(6) . . ?
C104 C81 C132 118.2(6) . . ?
C104 C81 H81 120.9 . . ?
C132 C81 H81 120.9 . . ?
C116 C41 H41 119.6 . . ?
C53 C41 C116 120.7(6) . . ?
C53 C41 H41 119.6 . . ?
O4 C83 H83A 109.5 . . ?
O4 C83 H83B 109.5 . . ?
O4 C83 H83C 109.5 . . ?
H83A C83 H83B 109.5 . . ?
H83A C83 H83C 109.5 . . ?
H83B C83 H83C 109.5 . . ?
C138 C21 H21 119.2 . . ?
C138 C21 C43 121.6(5) . . ?
C43 C21 H21 119.2 . . ?
C137 O5 C9 118.2(7) . . ?
F9 C85 C58 118.6(7) . . ?
F9 C85 C51 121.7(6) . . ?
C51 C85 C58 119.6(6) . . ?
C82 C43 C21 118.9(5) . . ?
C82 C43 H43 120.6 . . ?
C21 C43 H43 120.6 . . ?
O10 C87 C63 116.1(5) . . ?
O10 C87 C151 124.4(5) . . ?
C151 C87 C63 119.5(5) . . ?
F36 C11 C128 120.0(5) . . ?
F36 C11 C2 116.9(6) . . ?
C128 C11 C2 123.0(6) . . ?
O10 C89 H89A 109.5 . . ?
O10 C89 H89B 109.5 . . ?
O10 C89 H89C 109.5 . . ?
H89A C89 H89B 109.5 . . ?
H89A C89 H89C 109.5 . . ?
H89B C89 H89C 109.5 . . ?
C78 C45 H45 121.3 . . ?
C78 C45 C65 117.3(6) . . ?
C65 C45 H45 121.3 . . ?
C102 C91 H91 120.0 . . ?
C102 C91 C141 120.0(7) . . ?
C141 C91 H91 120.0 . . ?
C114 C23 H23 120.0 . . ?
C7 C23 C114 120.1(6) . . ?
C7 C23 H23 120.0 . . ?
F25 C93 C101 118.1(9) . . ?
F25 C93 C15 120.6(8) . . ?
C15 C93 C101 121.4(6) . . ?
F21 C47 C146 120.6(6) . . ?
F21 C47 C109 120.4(6) . . ?
C109 C47 C146 119.0(5) . . ?
F37 C95 C88 120.7(6) . . ?
F37 C95 C127 119.8(5) . . ?
C88 C95 C127 119.4(6) . . ?
C125 C3 P3 116.9(5) . . ?
C147 C3 P3 124.1(6) . . ?
C147 C3 C125 119.0(7) . . ?
F17 C97 C92 119.3(6) . . ?
F17 C97 C150 120.6(7) . . ?
C92 C97 C150 120.0(5) . . ?
O8 C49 H49A 109.5 . . ?
O8 C49 H49B 109.5 . . ?
O8 C49 H49C 109.5 . . ?
H49A C49 H49B 109.5 . . ?
H49A C49 H49C 109.5 . . ?
H49B C49 H49C 109.5 . . ?
O6 C99 H99A 109.5 . . ?
O6 C99 H99B 109.5 . . ?
O6 C99 H99C 109.5 . . ?
H99A C99 H99B 109.5 . . ?
H99A C99 H99C 109.5 . . ?
H99B C99 H99C 109.5 . . ?
F5 C25 C68 120.2(6) . . ?
F5 C25 C117 120.4(6) . . ?
C117 C25 C68 119.4(6) . . ?
F43 C101 C84 121.0(8) . . ?
F43 C101 C93 122.0(6) . . ?
C84 C101 C93 117.0(8) . . ?
F47 C51 C85 119.7(7) . . ?
F47 C51 C27 120.6(8) . . ?
C27 C51 C85 119.7(5) . . ?
C112 C103 H103 120.2 . . ?
C112 C103 C55 119.6(6) . . ?
C55 C103 H103 120.2 . . ?
F33 C13 C128 120.7(5) . . ?
F33 C13 C139 118.6(6) . . ?
C139 C13 C128 120.8(7) . . ?
C106 C105 H105 120.9 . . ?
C106 C105 C17 118.3(5) . . ?
C17 C105 H105 120.9 . . ?
O2 C53 C41 123.5(6) . . ?
O2 C53 C131 117.4(7) . . ?
C131 C53 C41 119.1(8) . . ?
F23 C107 C90 120.1(7) . . ?
F23 C107 C135 119.9(6) . . ?
C90 C107 C135 120.0(7) . . ?
F39 C27 C110 118.4(7) . . ?
C51 C27 F39 120.2(6) . . ?
C51 C27 C110 121.3(6) . . ?
F13 C109 C98 118.6(6) . . ?
F13 C109 C47 119.8(6) . . ?
C47 C109 C98 121.5(6) . . ?
C103 C55 H55 119.6 . . ?
C63 C55 C103 120.8(6) . . ?
C63 C55 H55 119.6 . . ?
F3 C111 C154 118.3(6) . . ?
F3 C111 C117 121.9(6) . . ?
C117 C111 C154 119.8(6) . . ?
C136 C7 H7 119.5 . . ?
C23 C7 C136 120.9(5) . . ?
C23 C7 H7 119.5 . . ?
C133 C113 H113 119.0 . . ?
C137 C113 H113 119.0 . . ?
C137 C113 C133 122.0(8) . . ?
O12 C57 H57A 109.5 . . ?
O12 C57 H57B 109.5 . . ?
O12 C57 H57C 109.5 . . ?
H57A C57 H57B 109.5 . . ?
H57A C57 H57C 109.5 . . ?
H57B C57 H57C 109.5 . . ?
C66 C115 H115 120.0 . . ?
C65 C115 C66 120.1(6) . . ?
C65 C115 H115 120.0 . . ?
F45 C29 C134 119.8(6) . . ?
F45 C29 C142 120.5(5) . . ?
C142 C29 C134 119.6(5) . . ?
F51 C117 C25 120.9(7) . . ?
F51 C117 C111 118.9(6) . . ?
C111 C117 C25 120.1(6) . . ?
C119 C59 H59 118.8 . . ?
C131 C59 H59 118.8 . . ?
C131 C59 C119 122.4(7) . . ?
C116 C119 C59 116.2(8) . . ?
C116 C119 H119 121.9 . . ?
C59 C119 H119 121.9 . . ?
F55 C15 C140 122.5(10) . . ?
F55 C15 C93 118.2(7) . . ?
C140 C15 C93 119.2(8) . . ?
F11 C121 C152 120.2(8) . . ?
F11 C121 C69 120.8(7) . . ?
C69 C121 C152 119.0(7) . . ?
C102 C61 H61 120.1 . . ?
C73 C61 C102 119.8(8) . . ?
C73 C61 H61 120.1 . . ?
F49 C123 C122 120.4(7) . . ?
F49 C123 C135 119.4(6) . . ?
C122 C123 C135 120.3(7) . . ?
C71 O11 C19 115.9(8) . . ?
C39 C31 H31 119.7 . . ?
C17 C31 C39 120.6(6) . . ?
C17 C31 H31 119.7 . . ?
C3 C125 H125 118.5 . . ?
C71 C125 C3 123.0(9) . . ?
C71 C125 H125 118.5 . . ?
C87 C63 H63 119.9 . . ?
C55 C63 C87 120.1(5) . . ?
C55 C63 H63 119.9 . . ?
F53 C127 C5 120.7(6) . . ?
F53 C127 C95 119.9(6) . . ?
C5 C127 C95 119.4(5) . . ?
F41 C2 C11 120.0(7) . . ?
F41 C2 C33 121.3(6) . . ?
C33 C2 C11 118.6(7) . . ?
O7 C129 H12A 109.5 . . ?
O7 C129 H12B 109.5 . . ?
O7 C129 H12C 109.5 . . ?
H12A C129 H12B 109.5 . . ?
H12A C129 H12C 109.5 . . ?
H12B C129 H12C 109.5 . . ?
C45 C65 H65 118.9 . . ?
C115 C65 C45 122.1(6) . . ?
C115 C65 H65 118.9 . . ?
C53 C131 H131 119.8 . . ?
C59 C131 C53 120.4(8) . . ?
C59 C131 H131 119.8 . . ?
F7 C33 C2 119.4(8) . . ?
C139 C33 F7 120.7(8) . . ?
C139 C33 C2 119.9(6) . . ?
C113 C133 P3 118.7(5) . . ?
C153 C133 P3 123.9(7) . . ?
C153 C133 C113 116.8(9) . . ?
F57 C67 C156 119.4(8) . . ?
F57 C67 C69 119.7(7) . . ?
C156 C67 C69 120.9(8) . . ?
F29 C135 C107 120.3(8) . . ?
F29 C135 C123 120.6(8) . . ?
C123 C135 C107 119.2(6) . . ?
C105 C17 H17 119.4 . . ?
C31 C17 C105 121.3(6) . . ?
C31 C17 H17 119.4 . . ?
O5 C137 C113 124.0(8) . . ?
C37 C137 O5 113.9(10) . . ?
C37 C137 C113 122.1(12) . . ?
F59 C69 C121 119.8(9) . . ?
F59 C69 C67 120.9(9) . . ?
C121 C69 C67 119.2(6) . . ?
F27 C139 C13 118.9(8) . . ?
C33 C139 F27 120.0(7) . . ?
C33 C139 C13 121.1(7) . . ?
O2 C35 H35A 109.5 . . ?
O2 C35 H35B 109.5 . . ?
O2 C35 H35C 109.5 . . ?
H35A C35 H35B 109.5 . . ?
H35A C35 H35C 109.5 . . ?
H35B C35 H35C 109.5 . . ?
O9 C141 C91 114.5(8) . . ?
O9 C141 C143 125.9(8) . . ?
C143 C141 C91 119.6(8) . . ?
O11 C71 C125 124.9(10) . . ?
C149 C71 O11 115.5(9) . . ?
C149 C71 C125 119.6(10) . . ?
C141 C143 H143 120.3 . . ?
C141 C143 C73 119.4(8) . . ?
C73 C143 H143 120.3 . . ?
O5 C9 H9A 109.5 . . ?
O5 C9 H9B 109.5 . . ?
O5 C9 H9C 109.5 . . ?
H9A C9 H9B 109.5 . . ?
H9A C9 H9C 109.5 . . ?
H9B C9 H9C 109.5 . . ?
O3 C145 H14A 109.5 . . ?
O3 C145 H14B 109.5 . . ?
O3 C145 H14C 109.5 . . ?
H14A C145 H14B 109.5 . . ?
H14A C145 H14C 109.5 . . ?
H14B C145 H14C 109.5 . . ?
C61 C73 C143 121.4(9) . . ?
C61 C73 H73 119.3 . . ?
C143 C73 H73 119.3 . . ?
C3 C147 H147 121.0 . . ?
C3 C147 C77 118.1(8) . . ?
C77 C147 H147 121.0 . . ?
C137 C37 H37 120.7 . . ?
C137 C37 C155 118.7(12) . . ?
C155 C37 H37 120.7 . . ?
C71 C149 H149 119.5 . . ?
C71 C149 C77 121.1(9) . . ?
C77 C149 H149 119.5 . . ?
O9 C75 H75A 109.5 . . ?
O9 C75 H75B 109.5 . . ?
O9 C75 H75C 109.5 . . ?
H75A C75 H75B 109.5 . . ?
H75A C75 H75C 109.5 . . ?
H75B C75 H75C 109.5 . . ?
C112 C151 H151 119.9 . . ?
C87 C151 C112 120.2(5) . . ?
C87 C151 H151 119.9 . . ?
O11 C19 H19A 97.8 . . ?
O11 C19 H19B 107.8 . . ?
O11 C19 H19C 121.9 . . ?
H19A C19 H19B 109.5 . . ?
H19A C19 H19C 109.5 . . ?
H19B C19 H19C 109.4 . . ?
C133 C153 H153 121.3 . . ?
C133 C153 C155 117.4(10) . . ?
C155 C153 H153 121.3 . . ?
C147 C77 H77 120.4 . . ?
C149 C77 C147 119.2(9) . . ?
C149 C77 H77 120.4 . . ?
C37 C155 C153 122.9(9) . . ?
C37 C155 H155 118.5 . . ?
C153 C155 H155 118.5 . . ?
Ag1 Cu13 Ag6 58.949(13) . . ?
Ag1 Cu13 Ag10 58.602(12) . . ?
Ag6 Cu13 Ag10 58.436(12) . . ?
S1 Cu13 Ag1 56.95(3) . . ?
S1 Cu13 Ag6 75.94(3) . . ?
S1 Cu13 Ag10 113.51(3) . . ?
S10 Cu13 Ag1 113.76(3) . . ?
S10 Cu13 Ag6 56.73(3) . . ?
S10 Cu13 Ag10 75.81(3) . . ?
S10 Cu13 S1 117.43(4) . . ?
S10 Cu13 S3 118.10(5) . . ?
S3 Cu13 Ag1 74.36(3) . . ?
S3 Cu13 Ag6 112.70(3) . . ?
S3 Cu13 Ag10 56.46(3) . . ?
S3 Cu13 S1 116.57(4) . . ?
Ag8 Cu12 Ag10 57.650(13) . . ?
Ag8 Cu12 Ag5 58.932(13) . . ?
Ag5 Cu12 Ag10 57.991(13) . . ?
S7 Cu12 Ag8 75.50(3) . . ?
S7 Cu12 Ag10 112.04(3) . . ?
S7 Cu12 Ag5 56.24(3) . . ?
S7 Cu12 S11 117.68(5) . . ?
S9 Cu12 Ag8 56.80(3) . . ?
S9 Cu12 Ag10 74.44(3) . . ?
S9 Cu12 Ag5 113.39(3) . . ?
S9 Cu12 S7 118.62(5) . . ?
S9 Cu12 S11 114.37(5) . . ?
S11 Cu12 Ag8 111.11(3) . . ?
S11 Cu12 Ag10 55.12(3) . . ?
S11 Cu12 Ag5 74.49(3) . . ?
Ag4 Cu2 Ag6 58.283(12) . . ?
Ag4 Cu2 Ag5 58.301(12) . . ?
Ag5 Cu2 Ag6 58.045(13) . . ?
S12 Cu2 Ag4 75.98(3) . . ?
S12 Cu2 Ag6 56.20(3) . . ?
S12 Cu2 Ag5 112.55(3) . . ?
S12 Cu2 S5 116.06(5) . . ?
S2 Cu2 Ag4 56.47(3) . . ?
S2 Cu2 Ag6 112.82(3) . . ?
S2 Cu2 Ag5 75.69(3) . . ?
S2 Cu2 S12 118.02(5) . . ?
S2 Cu2 S5 117.63(5) . . ?
S5 Cu2 Ag4 112.76(4) . . ?
S5 Cu2 Ag6 75.09(3) . . ?
S5 Cu2 Ag5 56.44(3) . . ?
Ag1 Cu14 Ag4 59.018(13) . . ?
Ag1 Cu14 Ag8 58.784(13) . . ?
Ag4 Cu14 Ag8 59.330(13) . . ?
S4 Cu14 Ag1 75.27(3) . . ?
S4 Cu14 Ag4 57.39(3) . . ?
S4 Cu14 Ag8 114.36(3) . . ?
S4 Cu14 S8 116.51(4) . . ?
S6 Cu14 Ag1 113.34(3) . . ?
S6 Cu14 Ag4 75.36(3) . . ?
S6 Cu14 Ag8 56.69(3) . . ?
S6 Cu14 S4 118.48(4) . . ?
S6 Cu14 S8 117.85(4) . . ?
S8 Cu14 Ag1 57.30(3) . . ?
S8 Cu14 Ag4 114.47(3) . . ?
S8 Cu14 Ag8 76.01(3) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Ag1 S1 C32 C36 77.6(4) . . . . ?
Ag1 S1 C32 C46 -111.1(4) . . . . ?
Ag1 S8 C56 C90 72.9(4) . . . . ?
Ag1 S8 C56 C122 -113.9(4) . . . . ?
Ag4 S4 C4 C1 69.3(3) . . . . ?
Ag4 S4 C4 C6 -117.8(4) . . . . ?
Ag4 S2 C34 C40 -115.1(3) . . . . ?
Ag4 S2 C34 C60 73.1(4) . . . . ?
Ag6 S10 C28 C14 -111.4(4) . . . . ?
Ag6 S10 C28 C88 75.8(4) . . . . ?
Ag6 S12 C16 C30 76.3(4) . . . . ?
Ag6 S12 C16 C98 -110.1(4) . . . . ?
Ag8 S6 C10 C58 74.2(4) . . . . ?
Ag8 S6 C10 C110 -113.7(4) . . . . ?
Ag8 S9 C52 C84 71.0(4) . . . . ?
Ag8 S9 C52 C140 -115.7(4) . . . . ?
Ag10 S3 C8 C12 -119.1(4) . . . . ?
Ag10 S3 C8 C44 68.1(5) . . . . ?
Ag10 S11 C128 C11 69.6(5) . . . . ?
Ag10 S11 C128 C13 -118.1(5) . . . . ?
Ag5 S7 C42 C68 72.2(5) . . . . ?
Ag5 S7 C42 C154 -113.9(4) . . . . ?
Ag5 S5 C76 C152 70.6(5) . . . . ?
Ag5 S5 C76 C156 -113.5(5) . . . . ?
Ag3 S1 C32 C36 -19.1(4) . . . . ?
Ag3 S1 C32 C46 152.3(3) . . . . ?
Ag3 S4 C4 C1 -24.6(4) . . . . ?
Ag3 S4 C4 C6 148.3(3) . . . . ?
Ag3 S12 C16 C30 -20.6(4) . . . . ?
Ag3 S12 C16 C98 153.0(4) . . . . ?
Ag3 P1 C22 C38 -50.8(4) . . . . ?
Ag3 P1 C22 C50 124.5(4) . . . . ?
Ag3 P1 C54 C20 -44.8(4) . . . . ?
Ag3 P1 C54 C94 129.0(4) . . . . ?
Ag3 P1 C82 C96 -49.8(4) . . . . ?
Ag3 P1 C82 C43 125.5(4) . . . . ?
Ag7 S6 C10 C58 -24.1(4) . . . . ?
Ag7 S6 C10 C110 148.0(3) . . . . ?
Ag7 S7 C42 C68 -26.8(5) . . . . ?
Ag7 S7 C42 C154 147.1(4) . . . . ?
Ag7 S2 C34 C40 150.0(3) . . . . ?
Ag7 S2 C34 C60 -21.8(4) . . . . ?
Ag7 P4 C72 C80 -46.3(4) . . . . ?
Ag7 P4 C72 C114 128.3(4) . . . . ?
Ag7 P4 C78 C64 -46.8(4) . . . . ?
Ag7 P4 C78 C45 127.3(4) . . . . ?
Ag7 P4 C106 C62 -46.5(5) . . . . ?
Ag7 P4 C106 C105 130.9(5) . . . . ?
Ag11 S8 C56 C90 -21.2(4) . . . . ?
Ag11 S8 C56 C122 151.9(4) . . . . ?
Ag11 S3 C8 C12 145.9(4) . . . . ?
Ag11 S3 C8 C44 -26.9(5) . . . . ?
Ag11 S9 C52 C84 -20.4(5) . . . . ?
Ag11 S9 C52 C140 153.0(4) . . . . ?
Ag11 P2 C102 C91 -25.1(5) . . . . ?
Ag11 P2 C102 C61 156.8(4) . . . . ?
Ag11 P2 C104 C124 -49.6(4) . . . . ?
Ag11 P2 C104 C81 126.1(4) . . . . ?
Ag11 P2 C112 C103 124.4(5) . . . . ?
Ag11 P2 C112 C151 -53.1(5) . . . . ?
Ag9 S10 C28 C14 157.8(3) . . . . ?
Ag9 S10 C28 C88 -15.0(4) . . . . ?
Ag9 S5 C76 C152 -21.1(5) . . . . ?
Ag9 S5 C76 C156 154.8(4) . . . . ?
Ag9 S11 C128 C11 -23.2(6) . . . . ?
Ag9 S11 C128 C13 149.1(5) . . . . ?
Ag9 P3 C116 C41 -45.6(5) . . . . ?
Ag9 P3 C116 C119 133.1(5) . . . . ?
Ag9 P3 C3 C125 -42.8(7) . . . . ?
Ag9 P3 C3 C147 134.6(7) . . . . ?
Ag9 P3 C133 C113 -47.5(6) . . . . ?
Ag9 P3 C133 C153 123.8(8) . . . . ?
Ag13 S1 C32 C36 156.9(3) . . . . ?
Ag13 S1 C32 C46 -31.7(4) . . . . ?
Ag13 S10 C28 C14 -31.8(4) . . . . ?
Ag13 S10 C28 C88 155.5(3) . . . . ?
Ag13 S3 C8 C12 -38.7(5) . . . . ?
Ag13 S3 C8 C44 148.5(4) . . . . ?
Ag2 S12 C16 C30 157.2(3) . . . . ?
Ag2 S12 C16 C98 -29.2(5) . . . . ?
Ag2 S2 C34 C40 -35.3(4) . . . . ?
Ag2 S2 C34 C60 152.9(3) . . . . ?
Ag2 S5 C76 C152 149.7(4) . . . . ?
Ag2 S5 C76 C156 -34.4(5) . . . . ?
Ag12 S7 C42 C68 153.8(4) . . . . ?
Ag12 S7 C42 C154 -32.3(5) . . . . ?
Ag12 S9 C52 C84 149.1(4) . . . . ?
Ag12 S9 C52 C140 -37.5(5) . . . . ?
Ag12 S11 C128 C11 151.6(5) . . . . ?
Ag12 S11 C128 C13 -36.1(6) . . . . ?
Ag14 S4 C4 C1 148.6(3) . . . . ?
Ag14 S4 C4 C6 -38.5(4) . . . . ?
Ag14 S6 C10 C58 155.3(3) . . . . ?
Ag14 S6 C10 C110 -32.5(4) . . . . ?
Ag14 S8 C56 C90 152.0(3) . . . . ?
Ag14 S8 C56 C122 -34.9(4) . . . . ?
S1 C32 C36 F6 -9.5(6) . . . . ?
S1 C32 C36 C134 169.9(4) . . . . ?
S1 C32 C46 F12 7.5(6) . . . . ?
S1 C32 C46 C142 -170.4(4) . . . . ?
S4 C4 C6 F22 6.2(6) . . . . ?
S4 C4 C6 C48 -171.8(4) . . . . ?
S6 C10 C58 F26 -8.5(6) . . . . ?
S6 C10 C58 C85 170.7(4) . . . . ?
S6 C10 C110 F30 8.2(6) . . . . ?
S6 C10 C110 C27 -172.7(4) . . . . ?
S8 C56 C90 F34 -7.5(6) . . . . ?
S8 C56 C90 C107 172.8(5) . . . . ?
S8 C56 C122 F44 6.2(7) . . . . ?
S8 C56 C122 C123 -172.8(5) . . . . ?
S10 C28 C88 F28 -9.0(7) . . . . ?
S10 C28 C88 C95 170.1(4) . . . . ?
S12 C16 C30 F4 -7.8(6) . . . . ?
S12 C16 C30 C146 171.4(4) . . . . ?
S12 C16 C98 F50 6.1(8) . . . . ?
S12 C16 C98 C109 -174.0(6) . . . . ?
S3 C8 C12 F14 6.6(7) . . . . ?
S3 C8 C12 C74 -173.0(4) . . . . ?
S3 C8 C44 F18 -8.0(7) . . . . ?
S3 C8 C44 C118 172.5(5) . . . . ?
S7 C42 C68 F24 -7.2(7) . . . . ?
S7 C42 C68 C25 172.1(5) . . . . ?
S7 C42 C154 F52 7.1(8) . . . . ?
S7 C42 C154 C111 -173.1(5) . . . . ?
S2 C34 C40 F8 7.8(6) . . . . ?
S2 C34 C40 C92 -171.4(4) . . . . ?
S2 C34 C60 F10 -9.6(6) . . . . ?
S2 C34 C60 C150 171.0(4) . . . . ?
P1 C22 C38 C70 174.8(4) . . . . ?
P1 C22 C50 C148 -173.5(4) . . . . ?
P1 C54 C94 C126 -172.4(4) . . . . ?
P1 C82 C96 C144 176.7(4) . . . . ?
P1 C82 C43 C21 -175.2(4) . . . . ?
S9 C52 C84 F32 -7.1(7) . . . . ?
S9 C52 C84 C101 173.8(4) . . . . ?
S9 C52 C140 F19 6.9(8) . . . . ?
S9 C52 C140 C15 -174.7(5) . . . . ?
S5 C76 C152 F56 -6.3(8) . . . . ?
S5 C76 C152 C121 173.7(5) . . . . ?
S5 C76 C156 F15 3.0(8) . . . . ?
S5 C76 C156 C67 -174.2(6) . . . . ?
P4 C72 C80 C136 174.3(4) . . . . ?
P4 C72 C114 C23 -173.3(4) . . . . ?
P4 C78 C45 C65 -174.0(5) . . . . ?
P4 C106 C105 C17 -176.0(6) . . . . ?
S11 C128 C11 F36 -9.1(8) . . . . ?
S11 C128 C11 C2 172.7(5) . . . . ?
S11 C128 C13 F33 5.2(9) . . . . ?
S11 C128 C13 C139 -174.0(6) . . . . ?
P2 C102 C91 C141 177.8(4) . . . . ?
P2 C102 C61 C73 -178.9(6) . . . . ?
P2 C104 C124 C120 176.1(4) . . . . ?
P2 C104 C81 C132 -174.8(4) . . . . ?
P2 C112 C103 C55 -176.7(6) . . . . ?
P2 C112 C151 C87 177.9(5) . . . . ?
P3 C116 C41 C53 176.5(4) . . . . ?
P3 C116 C119 C59 -177.1(5) . . . . ?
P3 C3 C125 C71 178.2(7) . . . . ?
P3 C3 C147 C77 -175.8(7) . . . . ?
P3 C133 C153 C155 -173.0(8) . . . . ?
F1 C1 C4 S4 -9.2(6) . . . . ?
F1 C1 C4 C6 177.5(4) . . . . ?
F1 C1 C18 F16 0.7(6) . . . . ?
F1 C1 C18 C24 -178.2(4) . . . . ?
F4 C30 C146 F42 -0.2(8) . . . . ?
F4 C30 C146 C47 -178.6(5) . . . . ?
F6 C36 C134 F46 -0.1(7) . . . . ?
F6 C36 C134 C29 -180.0(5) . . . . ?
F8 C40 C92 F60 0.0(7) . . . . ?
F8 C40 C92 C97 -179.0(5) . . . . ?
F10 C60 C150 F48 0.7(7) . . . . ?
F10 C60 C150 C97 -179.2(5) . . . . ?
F12 C46 C142 F2 1.4(8) . . . . ?
F12 C46 C142 C29 -177.8(5) . . . . ?
F14 C12 C74 F38 0.8(8) . . . . ?
F14 C12 C74 C130 -179.7(5) . . . . ?
F16 C18 C24 F40 0.6(8) . . . . ?
F16 C18 C24 C48 -178.9(5) . . . . ?
F18 C44 C118 F58 0.0(8) . . . . ?
F18 C44 C118 C130 -178.7(5) . . . . ?
F20 C14 C28 S10 6.7(6) . . . . ?
F20 C14 C28 C88 179.9(4) . . . . ?
F20 C14 C5 F31 1.8(8) . . . . ?
F20 C14 C5 C127 -177.7(6) . . . . ?
F22 C6 C48 F54 0.7(8) . . . . ?
F22 C6 C48 C24 -177.9(5) . . . . ?
F24 C68 C25 F5 0.3(9) . . . . ?
F24 C68 C25 C117 -179.9(6) . . . . ?
F26 C58 C85 F9 0.0(8) . . . . ?
F26 C58 C85 C51 -178.9(5) . . . . ?
F28 C88 C95 F37 -0.4(8) . . . . ?
F28 C88 C95 C127 -177.2(5) . . . . ?
F30 C110 C27 F39 -1.0(8) . . . . ?
F30 C110 C27 C51 -178.8(5) . . . . ?
F32 C84 C101 F43 -0.3(8) . . . . ?
F32 C84 C101 C93 -179.5(5) . . . . ?
F34 C90 C107 F23 0.1(9) . . . . ?
F34 C90 C107 C135 -179.2(6) . . . . ?
F36 C11 C2 F41 0.8(10) . . . . ?
F36 C11 C2 C33 -178.2(6) . . . . ?
F38 C74 C130 F35 -0.1(9) . . . . ?
F38 C74 C130 C118 179.7(6) . . . . ?
F40 C24 C48 F54 1.0(9) . . . . ?
F40 C24 C48 C6 179.6(5) . . . . ?
F42 C146 C47 F21 -0.6(10) . . . . ?
F42 C146 C47 C109 -177.7(7) . . . . ?
F44 C122 C123 F49 2.0(9) . . . . ?
F44 C122 C123 C135 -179.7(6) . . . . ?
F46 C134 C29 F45 0.9(10) . . . . ?
F46 C134 C29 C142 -178.8(6) . . . . ?
F48 C150 C97 F17 0.7(8) . . . . ?
F48 C150 C97 C92 -178.9(5) . . . . ?
O1 C26 C86 C126 178.2(5) . . . . ?
F50 C98 C109 F13 0.3(11) . . . . ?
F50 C98 C109 C47 -177.3(7) . . . . ?
F52 C154 C111 F3 -0.1(10) . . . . ?
F52 C154 C111 C117 -179.2(7) . . . . ?
F56 C152 C121 F11 0.4(10) . . . . ?
F56 C152 C121 C69 -179.3(7) . . . . ?
O4 C66 C115 C65 178.2(6) . . . . ?
F58 C118 C130 F35 0.5(9) . . . . ?
F58 C118 C130 C74 -179.3(6) . . . . ?
F60 C92 C97 F17 0.2(8) . . . . ?
F60 C92 C97 C150 179.8(5) . . . . ?
F15 C156 C67 F57 2.5(11) . . . . ?
F15 C156 C67 C69 -177.3(8) . . . . ?
F31 C5 C127 F53 -0.5(10) . . . . ?
F31 C5 C127 C95 179.2(6) . . . . ?
F2 C142 C29 F45 -0.4(10) . . . . ?
F2 C142 C29 C134 179.3(6) . . . . ?
F33 C13 C139 F27 0.3(12) . . . . ?
F33 C13 C139 C33 -177.0(8) . . . . ?
F9 C85 C51 F47 1.1(9) . . . . ?
F9 C85 C51 C27 -178.9(6) . . . . ?
O6 C136 C7 C23 177.7(5) . . . . ?
F37 C95 C127 F53 1.4(10) . . . . ?
F37 C95 C127 C5 -178.2(6) . . . . ?
F19 C140 C15 F55 -2.1(10) . . . . ?
F19 C140 C15 C93 -179.5(6) . . . . ?
F5 C25 C117 F51 -1.5(11) . . . . ?
F5 C25 C117 C111 -178.8(7) . . . . ?
O8 C70 C108 C148 -179.6(5) . . . . ?
F41 C2 C33 F7 -0.6(12) . . . . ?
F41 C2 C33 C139 -178.1(8) . . . . ?
F21 C47 C109 F13 2.1(13) . . . . ?
F21 C47 C109 C98 179.7(7) . . . . ?
O10 C87 C63 C55 177.7(7) . . . . ?
O10 C87 C151 C112 -179.1(6) . . . . ?
O12 C39 C31 C17 178.6(8) . . . . ?
C1 C4 C6 F22 179.4(4) . . . . ?
C1 C4 C6 C48 1.4(7) . . . . ?
C1 C18 C24 F40 179.5(4) . . . . ?
C1 C18 C24 C48 0.0(8) . . . . ?
C4 C1 C18 F16 -179.4(4) . . . . ?
C4 C1 C18 C24 1.7(7) . . . . ?
C4 C6 C48 F54 178.8(5) . . . . ?
C4 C6 C48 C24 0.2(9) . . . . ?
F11 C121 C69 F59 -0.7(13) . . . . ?
F11 C121 C69 C67 -178.4(8) . . . . ?
O7 C120 C124 C104 -180.0(5) . . . . ?
O7 C120 C79 C132 179.8(6) . . . . ?
C8 C12 C74 F38 -179.6(5) . . . . ?
C8 C12 C74 C130 0.0(9) . . . . ?
C8 C44 C118 F58 179.5(5) . . . . ?
C8 C44 C118 C130 0.8(9) . . . . ?
C10 C58 C85 F9 -179.2(5) . . . . ?
C10 C58 C85 C51 1.9(8) . . . . ?
C10 C110 C27 F39 179.9(5) . . . . ?
C10 C110 C27 C51 2.0(9) . . . . ?
F23 C107 C135 F29 0.4(11) . . . . ?
F23 C107 C135 C123 -179.6(7) . . . . ?
C12 C8 C44 F18 178.9(5) . . . . ?
C12 C8 C44 C118 -0.7(8) . . . . ?
C12 C74 C130 F35 -179.6(5) . . . . ?
C12 C74 C130 C118 0.2(9) . . . . ?
F47 C51 C27 F39 0.3(10) . . . . ?
F47 C51 C27 C110 178.1(5) . . . . ?
C14 C28 C88 F28 177.9(4) . . . . ?
C14 C28 C88 C95 -3.0(7) . . . . ?
C14 C5 C127 F53 179.0(6) . . . . ?
C14 C5 C127 C95 -1.4(10) . . . . ?
C16 C30 C146 F42 -179.3(5) . . . . ?
C16 C30 C146 C47 2.3(9) . . . . ?
C16 C98 C109 F13 -179.6(7) . . . . ?
C16 C98 C109 C47 2.8(12) . . . . ?
C18 C1 C4 S4 170.9(3) . . . . ?
C18 C1 C4 C6 -2.4(6) . . . . ?
C18 C24 C48 F54 -179.5(5) . . . . ?
C18 C24 C48 C6 -0.9(9) . . . . ?
F3 C111 C117 F51 1.2(12) . . . . ?
F3 C111 C117 C25 178.6(7) . . . . ?
C20 C26 C86 C126 0.4(8) . . . . ?
C20 C54 C94 C126 1.1(7) . . . . ?
C22 P1 C54 C20 77.4(4) . . . . ?
C22 P1 C54 C94 -108.9(4) . . . . ?
C22 P1 C82 C96 -174.8(4) . . . . ?
C22 P1 C82 C43 0.6(5) . . . . ?
C22 C38 C70 O8 -179.7(5) . . . . ?
C22 C38 C70 C108 -1.0(7) . . . . ?
C22 C50 C148 C108 -1.1(7) . . . . ?
C26 C20 C54 P1 173.3(3) . . . . ?
C26 C20 C54 C94 -0.7(7) . . . . ?
C26 C86 C126 C94 0.0(8) . . . . ?
C28 C14 C5 F31 -178.5(5) . . . . ?
C28 C14 C5 C127 2.0(9) . . . . ?
C28 C88 C95 F37 -179.5(5) . . . . ?
C28 C88 C95 C127 3.7(9) . . . . ?
C30 C16 C98 F50 -179.8(5) . . . . ?
C30 C16 C98 C109 0.0(9) . . . . ?
C30 C146 C47 F21 177.8(6) . . . . ?
C30 C146 C47 C109 0.7(11) . . . . ?
C32 C36 C134 F46 -179.5(5) . . . . ?
C32 C36 C134 C29 0.6(8) . . . . ?
C32 C46 C142 F2 179.3(5) . . . . ?
C32 C46 C142 C29 0.2(9) . . . . ?
C34 C40 C92 F60 179.3(4) . . . . ?
C34 C40 C92 C97 0.3(8) . . . . ?
C34 C60 C150 F48 -179.9(4) . . . . ?
C34 C60 C150 C97 0.3(8) . . . . ?
C36 C32 C46 F12 179.4(4) . . . . ?
C36 C32 C46 C142 1.5(7) . . . . ?
C36 C134 C29 F45 -179.2(6) . . . . ?
C36 C134 C29 C142 1.1(9) . . . . ?
C38 C22 C50 C148 1.7(7) . . . . ?
C38 C70 C108 C148 1.6(8) . . . . ?
F49 C123 C135 F29 -1.3(11) . . . . ?
F49 C123 C135 C107 178.7(7) . . . . ?
C40 C34 C60 F10 178.2(4) . . . . ?
C40 C34 C60 C150 -1.2(7) . . . . ?
C40 C92 C97 F17 179.2(5) . . . . ?
C40 C92 C97 C150 -1.2(8) . . . . ?
C42 C68 C25 F5 -179.0(5) . . . . ?
C42 C68 C25 C117 0.8(10) . . . . ?
C42 C154 C111 F3 -179.9(6) . . . . ?
C42 C154 C111 C117 1.0(11) . . . . ?
C44 C8 C12 F14 179.9(5) . . . . ?
C44 C8 C12 C74 0.3(8) . . . . ?
C44 C118 C130 F35 179.3(6) . . . . ?
C44 C118 C130 C74 -0.5(10) . . . . ?
C46 C32 C36 F6 178.7(4) . . . . ?
C46 C32 C36 C134 -1.9(7) . . . . ?
C46 C142 C29 F45 178.8(6) . . . . ?
C46 C142 C29 C134 -1.5(10) . . . . ?
F25 C93 C101 F43 0.3(9) . . . . ?
F25 C93 C101 C84 179.6(5) . . . . ?
F25 C93 C15 F55 2.1(11) . . . . ?
F25 C93 C15 C140 179.6(6) . . . . ?
C50 C22 C38 C70 -0.7(7) . . . . ?
C52 C84 C101 F43 178.9(5) . . . . ?
C52 C84 C101 C93 -0.3(8) . . . . ?
C52 C140 C15 F55 179.5(6) . . . . ?
C52 C140 C15 C93 2.1(10) . . . . ?
C54 P1 C22 C38 -171.4(3) . . . . ?
C54 P1 C22 C50 3.9(4) . . . . ?
C54 P1 C82 C96 71.3(4) . . . . ?
C54 P1 C82 C43 -113.3(4) . . . . ?
C54 C20 C26 O1 -177.8(4) . . . . ?
C54 C20 C26 C86 -0.1(7) . . . . ?
C54 C94 C126 C86 -0.8(8) . . . . ?
C56 C90 C107 F23 179.7(5) . . . . ?
C56 C90 C107 C135 0.5(10) . . . . ?
C56 C122 C123 F49 -178.9(5) . . . . ?
C56 C122 C123 C135 -0.7(10) . . . . ?
C58 C10 C110 F30 -179.3(4) . . . . ?
C58 C10 C110 C27 -0.1(7) . . . . ?
C58 C85 C51 F47 180.0(5) . . . . ?
C58 C85 C51 C27 0.0(9) . . . . ?
C60 C34 C40 F8 -179.9(4) . . . . ?
C60 C34 C40 C92 0.9(7) . . . . ?
C60 C150 C97 F17 -179.4(5) . . . . ?
C60 C150 C97 C92 1.0(8) . . . . ?
C62 C106 C105 C17 1.3(10) . . . . ?
C62 C39 C31 C17 -0.3(12) . . . . ?
C64 C66 C115 C65 -0.8(10) . . . . ?
C64 C78 C45 C65 0.0(9) . . . . ?
C66 C64 C78 P4 175.9(4) . . . . ?
C66 C64 C78 C45 1.7(8) . . . . ?
C66 C115 C65 C45 2.5(12) . . . . ?
C68 C42 C154 F52 -178.7(5) . . . . ?
C68 C42 C154 C111 1.1(9) . . . . ?
C68 C25 C117 F51 178.8(6) . . . . ?
C68 C25 C117 C111 1.5(11) . . . . ?
C70 C108 C148 C50 -0.5(8) . . . . ?
C72 P4 C78 C64 76.0(4) . . . . ?
C72 P4 C78 C45 -109.8(5) . . . . ?
C72 P4 C106 C62 -168.1(4) . . . . ?
C72 P4 C106 C105 9.3(6) . . . . ?
C72 C80 C136 O6 -178.3(4) . . . . ?
C72 C80 C136 C7 0.3(7) . . . . ?
C72 C114 C23 C7 -1.5(8) . . . . ?
C76 C152 C121 F11 -179.6(6) . . . . ?
C76 C152 C121 C69 0.7(11) . . . . ?
C76 C156 C67 F57 179.8(7) . . . . ?
C76 C156 C67 C69 -0.1(12) . . . . ?
C78 P4 C72 C80 -171.2(4) . . . . ?
C78 P4 C72 C114 3.4(5) . . . . ?
C78 P4 C106 C62 79.2(5) . . . . ?
C78 P4 C106 C105 -103.4(5) . . . . ?
C78 C64 C66 O4 179.8(5) . . . . ?
C78 C64 C66 C115 -1.3(8) . . . . ?
C78 C45 C65 C115 -2.1(11) . . . . ?
O2 C53 C131 C59 -178.3(7) . . . . ?
C80 C72 C114 C23 0.9(7) . . . . ?
C80 C136 C7 C23 -0.9(8) . . . . ?
C82 P1 C22 C38 75.3(4) . . . . ?
C82 P1 C22 C50 -109.4(4) . . . . ?
C82 P1 C54 C20 -168.6(3) . . . . ?
C82 P1 C54 C94 5.1(5) . . . . ?
C82 C96 C144 O3 179.3(5) . . . . ?
C82 C96 C144 C138 -1.3(8) . . . . ?
C84 C52 C140 F19 -179.4(5) . . . . ?
C84 C52 C140 C15 -1.0(8) . . . . ?
C88 C95 C127 F53 178.3(6) . . . . ?
C88 C95 C127 C5 -1.4(10) . . . . ?
C90 C56 C122 F44 179.8(5) . . . . ?
C90 C56 C122 C123 0.8(8) . . . . ?
C90 C107 C135 F29 179.7(6) . . . . ?
C90 C107 C135 C123 -0.3(11) . . . . ?
C96 C82 C43 C21 0.0(8) . . . . ?
C98 C16 C30 F4 178.3(5) . . . . ?
C98 C16 C30 C146 -2.6(7) . . . . ?
C100 O1 C26 C20 -5.0(7) . . . . ?
C100 O1 C26 C86 177.2(5) . . . . ?
C102 P2 C104 C124 -178.4(4) . . . . ?
C102 P2 C104 C81 -2.8(5) . . . . ?
C102 P2 C112 C103 -110.2(6) . . . . ?
C102 P2 C112 C151 72.3(5) . . . . ?
C102 C91 C141 O9 -179.2(6) . . . . ?
C102 C91 C141 C143 2.6(9) . . . . ?
C102 C61 C73 C143 -0.6(12) . . . . ?
C104 P2 C102 C91 101.7(4) . . . . ?
C104 P2 C102 C61 -76.4(5) . . . . ?
C104 P2 C112 C103 1.7(6) . . . . ?
C104 P2 C112 C151 -175.8(4) . . . . ?
C106 P4 C72 C80 75.8(4) . . . . ?
C106 P4 C72 C114 -109.6(4) . . . . ?
C106 P4 C78 C64 -170.9(4) . . . . ?
C106 P4 C78 C45 3.2(5) . . . . ?
C106 C62 C39 O12 -179.9(6) . . . . ?
C106 C62 C39 C31 -1.1(10) . . . . ?
C106 C105 C17 C31 -2.8(12) . . . . ?
F7 C33 C139 F27 3.3(14) . . . . ?
F7 C33 C139 C13 -179.5(7) . . . . ?
F57 C67 C69 F59 0.8(14) . . . . ?
F57 C67 C69 C121 178.6(8) . . . . ?
C110 C10 C58 F26 179.0(4) . . . . ?
C110 C10 C58 C85 -1.8(7) . . . . ?
C112 P2 C102 C91 -146.6(4) . . . . ?
C112 P2 C102 C61 35.3(5) . . . . ?
C112 P2 C104 C124 71.7(4) . . . . ?
C112 P2 C104 C81 -112.6(4) . . . . ?
C112 C103 C55 C63 -2.2(12) . . . . ?
C114 C72 C80 C136 -0.3(7) . . . . ?
C114 C23 C7 C136 1.5(8) . . . . ?
C116 P3 C3 C125 -165.0(6) . . . . ?
C116 P3 C3 C147 12.4(8) . . . . ?
C116 P3 C133 C113 76.7(6) . . . . ?
C116 P3 C133 C153 -112.0(8) . . . . ?
C116 C41 C53 O2 -179.5(6) . . . . ?
C116 C41 C53 C131 0.5(9) . . . . ?
C122 C56 C90 F34 179.0(4) . . . . ?
C122 C56 C90 C107 -0.7(7) . . . . ?
C122 C123 C135 F29 -179.6(6) . . . . ?
C122 C123 C135 C107 0.4(11) . . . . ?
C124 C104 C81 C132 0.8(7) . . . . ?
C124 C120 C79 C132 0.9(9) . . . . ?
C128 C11 C2 F41 179.0(6) . . . . ?
C128 C11 C2 C33 0.1(11) . . . . ?
C128 C13 C139 F27 179.5(7) . . . . ?
C128 C13 C139 C33 2.2(13) . . . . ?
O9 C141 C143 C73 -178.1(7) . . . . ?
C138 C21 C43 C82 -1.2(9) . . . . ?
C140 C52 C84 F32 179.3(4) . . . . ?
C140 C52 C84 C101 0.1(8) . . . . ?
C144 C138 C21 C43 1.1(10) . . . . ?
C146 C47 C109 F13 179.2(7) . . . . ?
C146 C47 C109 C98 -3.2(12) . . . . ?
C152 C76 C156 F15 179.1(6) . . . . ?
C152 C76 C156 C67 2.0(9) . . . . ?
C152 C121 C69 F59 179.0(7) . . . . ?
C152 C121 C69 C67 1.3(13) . . . . ?
C154 C42 C68 F24 178.7(5) . . . . ?
C154 C42 C68 C25 -2.0(8) . . . . ?
C154 C111 C117 F51 -179.7(6) . . . . ?
C154 C111 C117 C25 -2.3(12) . . . . ?
C156 C76 C152 F56 177.7(5) . . . . ?
C156 C76 C152 C121 -2.3(9) . . . . ?
C156 C67 C69 F59 -179.3(8) . . . . ?
C156 C67 C69 C121 -1.6(14) . . . . ?
C39 C62 C106 P4 178.1(5) . . . . ?
C39 C62 C106 C105 0.6(9) . . . . ?
C39 C31 C17 C105 2.3(14) . . . . ?
C79 C120 C124 C104 -1.2(8) . . . . ?
C79 C132 C81 C104 -1.0(9) . . . . ?
C5 C14 C28 S10 -173.1(4) . . . . ?
C5 C14 C28 C88 0.1(7) . . . . ?
C81 C104 C124 C120 0.3(8) . . . . ?
C81 C132 C79 C120 0.2(9) . . . . ?
C41 C116 C119 C59 1.6(9) . . . . ?
C41 C53 C131 C59 1.7(11) . . . . ?
C83 O4 C66 C64 -6.0(8) . . . . ?
C83 O4 C66 C115 175.1(5) . . . . ?
C21 C138 C144 O3 179.6(6) . . . . ?
C21 C138 C144 C96 0.2(9) . . . . ?
O5 C137 C37 C155 -179.7(11) . . . . ?
C85 C51 C27 F39 -179.8(6) . . . . ?
C85 C51 C27 C110 -2.0(10) . . . . ?
C43 C82 C96 C144 1.2(7) . . . . ?
C11 C128 C13 F33 178.0(6) . . . . ?
C11 C128 C13 C139 -1.2(10) . . . . ?
C11 C2 C33 F7 178.4(7) . . . . ?
C11 C2 C33 C139 0.9(12) . . . . ?
C89 O10 C87 C63 179.2(6) . . . . ?
C89 O10 C87 C151 -1.4(9) . . . . ?
C91 C102 C61 C73 3.1(10) . . . . ?
C91 C141 C143 C73 -0.2(11) . . . . ?
C3 P3 C116 C41 76.4(5) . . . . ?
C3 P3 C116 C119 -104.8(6) . . . . ?
C3 P3 C133 C113 -169.7(6) . . . . ?
C3 P3 C133 C153 1.5(9) . . . . ?
C3 C125 C71 O11 179.1(9) . . . . ?
C3 C125 C71 C149 -0.4(15) . . . . ?
C3 C147 C77 C149 -4.0(16) . . . . ?
C49 O8 C70 C38 -4.9(8) . . . . ?
C49 O8 C70 C108 176.3(5) . . . . ?
C99 O6 C136 C80 -2.8(7) . . . . ?
C99 O6 C136 C7 178.6(5) . . . . ?
C101 C93 C15 F55 -179.8(6) . . . . ?
C101 C93 C15 C140 -2.3(11) . . . . ?
C103 C112 C151 C87 0.3(9) . . . . ?
C103 C55 C63 C87 2.7(12) . . . . ?
C13 C128 C11 F36 178.3(6) . . . . ?
C13 C128 C11 C2 0.1(10) . . . . ?
C113 C133 C153 C155 -1.6(14) . . . . ?
C113 C137 C37 C155 1.3(19) . . . . ?
C57 O12 C39 C62 -8.0(10) . . . . ?
C57 O12 C39 C31 173.2(7) . . . . ?
C119 C116 C41 C53 -2.2(9) . . . . ?
C119 C59 C131 C53 -2.3(12) . . . . ?
C15 C93 C101 F43 -177.8(6) . . . . ?
C15 C93 C101 C84 1.4(10) . . . . ?
C61 C102 C91 C141 -4.1(8) . . . . ?
O11 C71 C149 C77 178.3(10) . . . . ?
C125 C3 C147 C77 1.5(14) . . . . ?
C125 C71 C149 C77 -2.2(18) . . . . ?
C63 C87 C151 C112 0.2(9) . . . . ?
C2 C33 C139 F27 -179.3(8) . . . . ?
C2 C33 C139 C13 -2.0(14) . . . . ?
C129 O7 C120 C124 -4.4(9) . . . . ?
C129 O7 C120 C79 176.7(6) . . . . ?
C131 C59 C119 C116 0.6(11) . . . . ?
C133 P3 C116 C41 -170.4(5) . . . . ?
C133 P3 C116 C119 8.4(6) . . . . ?
C133 P3 C3 C125 80.3(7) . . . . ?
C133 P3 C3 C147 -102.3(8) . . . . ?
C133 C113 C137 O5 179.1(7) . . . . ?
C133 C113 C137 C37 -2.0(14) . . . . ?
C133 C153 C155 C37 1.1(19) . . . . ?
C137 C113 C133 P3 174.0(6) . . . . ?
C137 C113 C133 C153 2.1(11) . . . . ?
C137 C37 C155 C153 -1(2) . . . . ?
C35 O2 C53 C41 -2.1(10) . . . . ?
C35 O2 C53 C131 177.9(7) . . . . ?
C141 C143 C73 C61 -0.8(12) . . . . ?
C71 C149 C77 C147 4.4(18) . . . . ?
C9 O5 C137 C113 -7.5(13) . . . . ?
C9 O5 C137 C37 173.5(9) . . . . ?
C145 O3 C144 C96 -4.8(9) . . . . ?
C145 O3 C144 C138 175.7(6) . . . . ?
C147 C3 C125 C71 0.7(13) . . . . ?
C75 O9 C141 C91 176.1(7) . . . . ?
C75 O9 C141 C143 -5.9(11) . . . . ?
C151 C112 C103 C55 0.7(10) . . . . ?
C151 C87 C63 C55 -1.6(11) . . . . ?
C19 O11 C71 C125 -23.0(15) . . . . ?
C19 O11 C71 C149 156.6(11) . . . . ?
Cu13 S1 C32 C36 156.9(3) . . . . ?
Cu13 S1 C32 C46 -31.7(4) . . . . ?
Cu13 S10 C28 C14 -31.8(4) . . . . ?
Cu13 S10 C28 C88 155.5(3) . . . . ?
Cu13 S3 C8 C12 -38.7(5) . . . . ?
Cu13 S3 C8 C44 148.5(4) . . . . ?
Cu12 S7 C42 C68 153.8(4) . . . . ?
Cu12 S7 C42 C154 -32.3(5) . . . . ?
Cu12 S9 C52 C84 149.1(4) . . . . ?
Cu12 S9 C52 C140 -37.5(5) . . . . ?
Cu12 S11 C128 C11 151.6(5) . . . . ?
Cu12 S11 C128 C13 -36.1(6) . . . . ?
Cu2 S12 C16 C30 157.2(3) . . . . ?
Cu2 S12 C16 C98 -29.2(5) . . . . ?
Cu2 S2 C34 C40 -35.3(4) . . . . ?
Cu2 S2 C34 C60 152.9(3) . . . . ?
Cu2 S5 C76 C152 149.7(4) . . . . ?
Cu2 S5 C76 C156 -34.4(5) . . . . ?
Cu14 S4 C4 C1 148.6(3) . . . . ?
Cu14 S4 C4 C6 -38.5(4) . . . . ?
Cu14 S6 C10 C58 155.3(3) . . . . ?
Cu14 S6 C10 C110 -32.5(4) . . . . ?
Cu14 S8 C56 C90 152.0(3) . . . . ?
Cu14 S8 C56 C122 -34.9(4) . . . . ?

_smtbx_masks_special_details     
;
A solvent mask was calculated and 486 electrons were 
found in a volume of 1792Å³ in 1 void per unit cell. 
This is consistent with the presence of 
3[CH2Cl2], 6.5[CH3OH] per formula unit 
which account for 486 electrons 
per unit cell.
;
loop_
_smtbx_masks_void_nr
_smtbx_masks_void_average_x
_smtbx_masks_void_average_y
_smtbx_masks_void_average_z
_smtbx_masks_void_volume
_smtbx_masks_void_count_electrons
_smtbx_masks_void_content
1 -0.194 0.224 0.746 896.2 242.6 '3 CH2Cl2,6.5 CH3OH'
2 0.194 0.776 0.254 896.2 241.8 '3 CH2Cl2,6.5 CH3OH'
3 0.220 0.343 0.252 7.2 0.0 ?
4 0.780 0.657 0.748 7.2 0.0 ?

_smtbx_masks_void_probe_radius   1.2
_smtbx_masks_void_truncation_radius 1.2
